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Sample records for calibration standards

  1. Calibration of Flick standards

    International Nuclear Information System (INIS)

    Thalmann, Ruedi; Spiller, Jürg; Küng, Alain; Jusko, Otto

    2012-01-01

    Flick standards or magnification standards are widely used for an efficient and functional calibration of the sensitivity of form measuring instruments. The results of a recent measurement comparison have shown to be partially unsatisfactory and revealed problems related to the calibration of these standards. In this paper the influence factors for the calibration of Flick standards using roundness measurement instruments are discussed in detail, in particular the bandwidth of the measurement chain, residual form errors of the device under test, profile distortions due to the diameter of the probing element and questions related to the definition of the measurand. The different contributions are estimated using simulations and are experimentally verified. Also alternative methods to calibrate Flick standards are investigated. Finally the practical limitations of Flick standard calibration are shown and the usability of Flick standards both to calibrate the sensitivity of roundness instruments and to check the filter function of such instruments is analysed. (paper)

  2. Radiological Calibration and Standards Facility

    Data.gov (United States)

    Federal Laboratory Consortium — PNNL maintains a state-of-the-art Radiological Calibration and Standards Laboratory on the Hanford Site at Richland, Washington. Laboratory staff provide expertise...

  3. Performance standard for dose Calibrator

    CERN Document Server

    Darmawati, S

    2002-01-01

    Dose calibrator is an instrument used in hospitals to determine the activity of radionuclide for nuclear medicine purposes. International Electrotechnical Commission (IEC) has published IEC 1303:1994 standard that can be used as guidance to test the performance of the instrument. This paper briefly describes content of the document,as well as explains the assessment that had been carried out to test the instrument accuracy in Indonesia through intercomparison measurement.Its is suggested that hospitals acquire a medical physicist to perform the test for its dose calibrator. The need for performance standard in the form of Indonesia Standard is also touched.

  4. Nuclear radiation moisture gauge calibration standard

    International Nuclear Information System (INIS)

    1977-01-01

    A hydrophobic standard for calibrating nuclear radiation moisture gauges is described. Each standard has physical characteristics and dimensions effective for representing to a nuclear gauge undergoing calibration, an infinite mass of homogeneous hydrogen content. Calibration standards are discussed which are suitable for use with surface gauges and with depth gauges. (C.F.)

  5. Nuclear radiation moisture gauge calibration standard

    International Nuclear Information System (INIS)

    Berry, R.L.

    1981-01-01

    A hydrophobic standard for calibrating radiation moisture gauges is described. This standard has little or no affinity for water and accordingly will not take up or give off water under ambient conditions of fluctuating humidity in such a manner as to change the hydrogen content presented to a nuclear gauge undergoing calibration. (O.T.)

  6. Calibration of surface roughness standards

    DEFF Research Database (Denmark)

    Thalmann, R.; Nicolet, A.; Meli, F.

    2016-01-01

    organisations. Five surface texture standards of different type were circulated and on each of the standards several roughness parameters according to the standard ISO 4287 had to be determined. 32 out of 395 individual results were not consistent with the reference value. After some corrective actions...

  7. EG type radioactive calibration standards

    International Nuclear Information System (INIS)

    1980-01-01

    EG standards are standards with a radioactive substance deposited as a solution on filtration paper and after drying sealed into a plastic disc or cylinder shaped casing. They serve the official testing of X-ray and gamma spectrometers and as test sources. The table shows the types of used radionuclides, nominal values of activity and total error of determination not exceeding +-4%. Activity of standards is calculated from the charge and the specific activity of standard solution used for the preparation of the standard. Tightness and surface contamination is measured for each standard. The manufacturer, UVVVR Praha, gives a guarantee for the given values of activity and total error of determination. (M.D.)

  8. Tour of the Standards and Calibrations Laboratory

    International Nuclear Information System (INIS)

    Elliott, J.H.

    1978-01-01

    This tour of Lawrence Livermore Laboratory's Standards and Calibrations Laboratory is intended as a guide to the capabilities of and services offered by this unique laboratory. Described are the Laboratory's ability to provide radiation fields and measurements for dosimeters, survey instruments, spectrometers, and sources and its available equipment and facilities. The tour also includes a survey of some Health Physics and interdepartmental programs supported by the Standards and Calibrations Laboratory and a listing of applicable publications

  9. Providing primary standard calibrations beyond 20 MHz

    International Nuclear Information System (INIS)

    Bickley, C J; Zeqiri, B; Robinson, S P

    2004-01-01

    The number of applications of medical ultrasound utilising frequencies in excess of 20 MHz has shown a consistent increase over recent years. Coupled with the commercial availability of wide-bandwidth hydrophones whose response extends beyond 40 MHz, this has driven a growing need to develop hydrophone calibration techniques at elevated frequencies. The current National Physical Laboratory primary standard method of calibrating hydrophones is based on an optical interferometer. This has been in operation for around 20 years and provides traceability over the frequency range of 0.3 to 20 MHz. More recently, calibrations carried out using the interferometer have been extended to 60 MHz, although the uncertainties associated with these calibrations are poor, being in excess of ±20% at high frequencies. Major contributions to the degraded calibration uncertainties arise from poor signal-to-noise at higher frequencies, the frequency response of the photodiodes used and the noise floor of the instrument. To improve the uncertainty of hydrophone calibrations above 20 MHz, it has been necessary to build and commission a new interferometer. Important features of the new primary standard are its use of a higher power laser to improve the signal-to-noise ratio, along with photodiodes whose greater bandwidth to improve the overall frequency response. This paper describes the design of key aspects of the new interferometer. It also presents some initial results of the performance assessment, including a detailed comparison of calibrations of NPL reference membrane hydrophones, undertaken using old and new interferometers for calibration up to 40 MHz

  10. Development of nano-roughness calibration standards

    International Nuclear Information System (INIS)

    Baršić, Gorana; Mahović, Sanjin; Zorc, Hrvoje

    2012-01-01

    At the Laboratory for Precise Measurements of Length, currently the Croatian National Laboratory for Length, unique nano-roughness calibration standards were developed, which have been physically implemented in cooperation with the company MikroMasch Trading OU and the Ruđer Bošković Institute. In this paper, a new design for a calibration standard with two measuring surfaces is presented. One of the surfaces is for the reproduction of roughness parameters, while the other is for the traceability of length units below 50 nm. The nominal values of the groove depths on these measuring surfaces are the same. Thus, a link between the measuring surfaces has been ensured, which makes these standards unique. Furthermore, the calibration standards available on the market are generally designed specifically for individual groups of measuring instrumentation, such as interferometric microscopes, stylus instruments, scanning electron microscopes (SEM) or scanning probe microscopes. In this paper, a new design for nano-roughness standards has been proposed for use in the calibration of optical instruments, as well as for stylus instruments, SEM, atomic force microscopes and scanning tunneling microscopes. Therefore, the development of these new nano-roughness calibration standards greatly contributes to the reproducibility of the results of groove depth measurement as well as the 2D and 3D roughness parameters obtained by various measuring methods. (paper)

  11. Status of Photovoltaic Calibration and Measurement Standards

    Science.gov (United States)

    Baraona, Cosmo; Bailey, Sheila; Curtis, Henry; Brinker, David; Jenkins, Phillip; Scheiman, David

    2001-01-01

    The 7th International Workshop on Space Solar Cell Calibration and Measurement was held on September 25-27, 2000 in Girdwood, Alaska. Representatives from eight countries discussed international standards for single and multijunction solar cell measurement and calibration methods, round robin intercomparisons, and irradiation test methods for space solar cells. Progress toward adoption of an ISO standard on single junction cells was made. Agreement was reached to begin work on new standards for multijunction cells and irradiation testing. Progress on present single junction round robin measurements was discussed and future multijunction round robins were planned. The next workshop will be held in Germany in October 2001.

  12. Gamma-ray standards for detector calibration

    International Nuclear Information System (INIS)

    Lorenz, A.

    1985-10-01

    The proceeedings are reported of a Consultants' Meeting on Gamma-ray Standards for Detector Calibration, held at the CEN, Grenoble in France, from 30-31 May 1985. The meeting provided a forum to assess the requirements for a suitable file to be used internationally for the calibration of X- and gamma-ray detectors. A provisional list of nuclides was drawn up, and an initial assessment of the status of the required data was agreed to be performed by the participants before the end of 1985. (author)

  13. Calibration of working standard ionization chambers and dose standardization

    International Nuclear Information System (INIS)

    Abd Elmahoud, A. A. B.

    2011-01-01

    Measurements were performed for the calibration of two working standard ionization chambers in the secondary standard dosimetry laboratory of Sudan. 600 cc cylindrical former type and 1800 cc cylindrical radical radiation protection level ionization chambers were calibrated against 1000 cc spherical reference standard ionization chamber. The chamber were calibrated at X-ray narrow spectrum series with beam energies ranged from (33-116 KeV) in addition to 1''3''7''Cs beam with 662 KeV energy. The chambers 0.6 cc and 0.3 cc therapy level ionization were used for dose standardization and beam output calibrations of cobalt-60 radiotherapy machine located at the National Cancer Institute, University of Gazira. Concerning beam output measurements for 6''0''Co radiotherapy machine, dosimetric measurements were performed in accordance with the relevant per IAEA dosimetry protocols TRS-277 and TRS-398. The kinetic energy released per unit mass in air (air kerma) were obtained by multiplying the corrected electrometer reading (nC/min) by the calibration factors (Gy/n C) of the chambers from given in the calibration certificate. The uncertainty of measurements of air kerma were calculated for the all ionization chambers (combined uncertainty) the calibration factors of these ionization chambers then were calculated by comparing the reading of air kerma of secondary standard ionization chambers to than from radical and farmer chambers. The result of calibration working standard ionization chambers showed different calibration factors ranged from 0.99 to 1.52 for different radiation energies and these differences were due to chambers response and specification. The absorbed dose to to water calculated for therapy ionization chamber using two code of practice TRS-277 and TRS-398 as beam output for 6''0''Co radiotherapy machine and it can be used as a reference for future beam output calibration in radiotherapy dosimetry. The measurement of absorbed dose to water showed that the

  14. Gamma-ray standards for detector calibration

    International Nuclear Information System (INIS)

    Christmas, P.; Nichols, A.L.; Lorenz, A.

    1987-09-01

    The first official meeting of the IAEA Coordinated Research Programme on the Measurement and Evaluation of X- and Gamma-ray Standards for Detector Calibration was held in Rome from 11 to 13 June 1987. Work undertaken by the CRP members was reviewed in detail: specific problems in the evaluations were identified and actions placed on the participants to resolve these issues. (author). 3 tabs

  15. Broadband standard dipole antenna for antenna calibration

    Science.gov (United States)

    Koike, Kunimasa; Sugiura, Akira; Morikawa, Takao

    1995-06-01

    Antenna calibration of EMI antennas is mostly performed by the standard antenna method at an open-field test site using a specially designed dipole antenna as a reference. In order to develop broadband standard antennas, the antenna factors of shortened dipples are theoretically investigated. First, the effects of the dipole length are analyzed using the induced emf method. Then, baluns and loads are examined to determine their influence on the antenna factors. It is found that transformer-type baluns are very effective for improving the height dependence of the antenna factors. Resistive loads are also useful for flattening the frequency dependence. Based on these studies, a specification is developed for a broadband standard antenna operating in the 30 to 150 MHz frequency range.

  16. LLNL X-ray Calibration and Standards Laboratory

    International Nuclear Information System (INIS)

    Anon.

    1982-01-01

    The LLNL X-ray Calibration and Standards Laboratory is a unique facility for developing and calibrating x-ray sources, detectors, and materials, and for conducting x-ray physics research in support of our weapon and fusion-energy programs

  17. Radioactive standards and calibration methods for contamination monitoring instruments

    Energy Technology Data Exchange (ETDEWEB)

    Yoshida, Makoto [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    1997-06-01

    Contamination monitoring in the facilities for handling unsealed radioactive materials is one of the most important procedures for radiation protection as well as radiation dose monitoring. For implementation of the proper contamination monitoring, radiation measuring instruments should not only be suitable to the purpose of monitoring, but also be well calibrated for the objective qualities of measurement. In the calibration of contamination monitoring instruments, quality reference activities need to be used. They are supplied in different such as extended sources, radioactive solutions or radioactive gases. These reference activities must be traceable to the national standards or equivalent standards. On the other hand, the appropriate calibration methods must be applied for each type of contamination monitoring instruments. In this paper, the concepts of calibration for contamination monitoring instruments, reference sources, determination methods of reference quantities and practical calibration methods of contamination monitoring instruments, including the procedures carried out in Japan Atomic Energy Research Institute and some relevant experimental data. (G.K.)

  18. Syringe calibration factors and volume correction factors for the NPL secondary standard radionuclide calibrator

    CERN Document Server

    Tyler, D K

    2002-01-01

    The activity assay of a radiopharmaceutical administration to a patient is normally achieved via the use of a radionuclide calibrator. Because of the different geometries and elemental compositions between plastic syringes and glass vials, the calibration factors for syringes may well be significantly different from those for the glass containers. The magnitude of these differences depends on the energies of the emitted photons. For some radionuclides variations have been observed of 70 %, it is therefore important to recalibrate for syringes or use syringe calibration factors. Calibration factors and volume correction factors have been derived for the NPL secondary standard radionuclide calibrator, for a variety of commonly used syringes and needles, for the most commonly used medical radionuclide.

  19. DNA origami structures as calibration standards for nanometrology

    International Nuclear Information System (INIS)

    Korpelainen, Virpi; Seppä, Jeremias; Lassila, Antti; Linko, Veikko; Kostiainen, Mauri A

    2017-01-01

    In this work we have studied the feasibility of DNA origami nanostructures as dimensional calibration standards for atomic force microscopes (AFMs) at the nanometre scale. The stability of the structures and repeatability of the measurement have been studied, and the applicability for calibration is discussed. A cross-like Seeman tile (ST) was selected for the studies and it was found suitable for repeatable calibration of AFMs. The height of the first height step of the ST was 2.0 nm. Expanded standard uncertainty (k   =  2) of the measurement U c was 0.2 nm. The width of the ST was 88 nm and width of its arm was 28 nm with U c   =  3 nm. In addition, prepared dry samples were found out to be stable at least for 12 months. (paper)

  20. Standard practice for torque calibration of testing machines and devices

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2009-01-01

    1.1 This practice covers procedures and requirements for the calibration of torque for static and quasi-static torque capable testing machines or devices. These may, or may not, have torque indicating systems and include those devices used for the calibration of hand torque tools. Testing machines may be calibrated by one of the three following methods or combination thereof: 1.1.1 Use of standard weights and lever arms. 1.1.2 Use of elastic torque measuring devices. 1.1.3 Use of elastic force measuring devices and lever arms. 1.1.4 Any of the methods require a specific uncertainty of measurement and a traceability derived from national standards of mass and length. 1.2 The procedures of 1.1.1, 1.1.2, and 1.1.3 apply to the calibration of the torque-indicating systems associated with the testing machine, such as a scale, dial, marked or unmarked recorder chart, digital display, etc. In all cases the buyer/owner/user must designate the torque-indicating system(s) to be calibrated and included in the repor...

  1. Standardization of calibration method of whole-body counter. 1. Calibration by using anthropometric phantoms

    International Nuclear Information System (INIS)

    Ishikawa, Tetsuo; Matsumoto, Masaki; Uchiyama, Masafumi; Kobayashi, Sadayoshi; Mizushita, Seiichi.

    1995-01-01

    To standardize the calibration methods of whole-body counters, three anthropometric phantoms were manufactured based on dozens of Japanese average value of body size data. Using these phantoms, the calibrations of some whole-body counters were carried out and the comparison of counting efficiency between anthropometric phantoms and block phantoms, which used to be used for the calibration of whole-body counters generally, was implemented. Five whole-body counters, one scanning system, two stationary systems and two chair systems, were used for this study. The following results were derived: As an example, in NIRS scanning system, the counting efficiency of anthropometric phantom of 162cm height was 12.7% greater than that of block phantom of the same height. This means 137 Cs body burdens in adult men used to be estimated with the excess of about 10%. Body burdens tended to be estimated excessively in adult because the difference of counting efficiency between anthropometric phantom and block phantom increases with increase of height. To standardize body burden data measured with various whole-body counters, the calibration of each whole-body counter should be conducted using anthropometric phantoms and phantoms which used to be used for the calibration of that whole-body counter. (author)

  2. Preparation of high purity plutonium oxide for radiochemistry instrument calibration standards and working standards

    International Nuclear Information System (INIS)

    Wong, A.S.; Stalnaker, N.D.

    1997-04-01

    Due to the lack of suitable high level National Institute of Standards and Technology (NIST) traceable plutonium solution standards from the NIST or commercial vendors, the CST-8 Radiochemistry team at Los Alamos National Laboratory (LANL) has prepared instrument calibration standards and working standards from a well-characterized plutonium oxide. All the aliquoting steps were performed gravimetrically. When a 241 Am standardized solution obtained from a commercial vendor was compared to these calibration solutions, the results agreed to within 0.04% for the total alpha activity. The aliquots of the plutonium standard solutions and dilutions were sealed in glass ampules for long term storage

  3. Advisory Committee for the calibration standards of ionizing radiation measurement

    International Nuclear Information System (INIS)

    1979-01-01

    The meeting consisted exceptionally of two sessions (in May and December 1977). The members discussed the comparisons of absorbed dose standards and exposure standards which had taken place since 1975 and suggested improvements for future comparisons. A recommendation was made concerning the humidity correction factor to be applied when using cavity chambers and free-air chambers. Further studies were requested concerning the effective point of measurement of ionization chambers. No method was recommended for the statement of uncertainty in calibration certificates. The exposure standards and calibrations in terms of exposure were maintained but it was agreed that other possibilities should be explored. Finally, progress reports of the national laboratories and a description of the recent work carried out at BIPM were presented and appear as appendices to the report [fr

  4. The Standard Temperature Calibration Center of the CEN Saclay

    International Nuclear Information System (INIS)

    Liermann, J.

    1978-01-01

    The first part of this article describes the instruments available at the Standard Temperature Calibration Center of the CEN Saclay. At the moment the Center has been approved by the BNM to make calibrations between 0 and 1050 0 C, but the Center has recently developed some ovens which will allow calibrations up to 2000 0 C. The Center can also perform thermal and mechanical tests on detector components under the influence of external factors. The second part concerns the development of platinum-resistance high temperature thermometer. The calibrations by comparison between 0 and 1000 0 C are, at the moment, made by using platinum resistance thermometer as a reference up to 630 0 C and a platinum-rhodied/platinum thermocouple above 630 0 C. The use of only one reference could represent for a calibration center a great improvement. For this reason a platinum-resistance high temperature thermometer has been developed. Great care was taken during the conceptual design and during the selection and the assembly of each component [fr

  5. A standard stellar library for evolutionary synthesis. III. Metallicity calibration

    Science.gov (United States)

    Westera, P.; Lejeune, T.; Buser, R.; Cuisinier, F.; Bruzual, G.

    2002-01-01

    We extend the colour calibration of the widely used BaSeL standard stellar library (Lejeune et al. 1997, 1998) to non-solar metallicities, down to [Fe/H] ~ -2.0 dex. Surprisingly, we find that at the present epoch it is virtually impossible to establish a unique calibration of UBVRIJHKL colours in terms of stellar metallicity [Fe/H] which is consistent simultaneously with both colour-temperature relations and colour-absolute magnitude diagrams (CMDs) based on observed globular cluster photometry data and on published, currently popular standard stellar evolutionary tracks and isochrones. The problem appears to be related to the long-standing incompleteness in our understanding of convection in late-type stellar evolution, but is also due to a serious lack of relevant observational calibration data that would help resolve, or at least further significant progress towards resolving this issue. In view of the most important applications of the BaSeL library, we here propose two different metallicity calibration versions: (1) the ``WLBC 99'' library, which consistently matches empirical colour-temperature relations and which, therefore, should make an ideal tool for the study of individual stars; and (2), the ``PADOVA 2000'' library, which provides isochrones from the Padova 2000 grid (Girardi et al. \\cite{padova}) that successfully reproduce Galactic globular-cluster colour-absolute magnitude diagrams and which thus should prove particularly useful for studies of collective phenomena in stellar populations in clusters and galaxies.

  6. Spectral responsivity-based calibration of photometer and colorimeter standards

    Science.gov (United States)

    Eppeldauer, George P.

    2013-08-01

    Several new generation transfer- and working-standard illuminance meters and tristimulus colorimeters have been developed at the National Institute of Standards and Technology (NIST) [1] to measure all kinds of light sources with low uncertainty. The spectral and broad-band (illuminance) responsivities of the photometer (Y) channels of two tristimulus meters were determined at both the Spectral Irradiance and Radiance Responsivity Calibrations using Uniform Sources (SIRCUS) facility and the Spectral Comparator Facility (SCF) [2]. The two illuminance responsivities agreed within 0.1% with an overall uncertainty of 0.2% (k = 2), which is a factor of two improvement over the present NIST photometric scale. The first detector-based tristimulus color scale [3] was realized. All channels of the reference tristimulus colorimeter were calibrated at the SIRCUS. The other tristimulus meters were calibrated at the SCF and also against the reference meter on the photometry bench in broad-band measurement mode. The agreement between detector- and source-based calibrations was within 3 K when a tungsten lamp-standard was measured at 2856 K and 3100 K [4]. The color-temperature uncertainty of tungsten lamp measurements was 4 K (k = 2) between 2300 K and 3200 K, which is a factor of two improvement over the presently used NIST source-based color temperature scale. One colorimeter was extended with an additional (fifth) channel to apply software implemented matrix corrections. With this correction, the spectral mismatch caused color difference errors were decreased by a factor of 20 for single-color LEDs.

  7. The transfer voltage standard for calibration outside of a laboratory

    Directory of Open Access Journals (Sweden)

    Urekar Marjan

    2017-01-01

    Full Text Available The transfer voltage standard is designed for transferring the analog voltage from a calibrator to the process control workstation for multi-electrode electrolysis process in a plating plant. Transfer voltage standard is based on polypropylene capacitors and operational amplifiers with tera-ohm range input resistance needed for capacitor self-discharging effect cancellation. Dielectric absorption effect is described. An instrument for comparison of reference and control voltages is devised, based on precise window comparator. Detailed description of the main task is given, including constraints, theoretical and practical solutions. Procedure for usage of the standard outside of a laboratory conditions is explained. Comparison of expected and realized standard characteristics is given. [Project of the Serbian Ministry of Education, Science and Technological Development, Grant no. TR-32019

  8. A report from the AVS Standards Committee - Comparison of ion gauge calibrations by several standards laboratories

    Science.gov (United States)

    Warshawsky, I.

    1982-01-01

    Calibrations by four U.S. laboratories of four hot-cathode ion gauges, in the range 0.07-13 mPa, showed systematic differences among laboratories that were much larger than the expected error of any one calibration. They also suggested that any of the four gauges tested, if properly packaged and shipped, was able to serve as a transfer standard with probable error of 2%. A second comparison was made of the calibrations by two U.S. laboratories of some other gauges that had also been calibrated by the National Physical Laboratory, England. Results did not permit conclusive determination of whether differences were due to the laboratories or to changes in the gauges.

  9. Management of vacuum leak-detection processes, calibration, and standards

    International Nuclear Information System (INIS)

    Wilson, N.G.

    1985-01-01

    Vacuum leak detection requires integrated management action to ensure the successful production of apparatus having required leak tightness. Implementation of properly planned, scheduled, and engineered procedures and test arrangements are an absolute necessity to prevent unexpected, impractical, technically inadequate, or unnecessarily costly incidents in leak-testing operations. The use of standard procedures, leak standards appropriate to the task, and accurate calibration systems or devices is necessary to validate the integrity of any leak-test procedure. In this paper, the need for implementing these practices is discussed using case histories of typical examples of large complex vacuum systems. Aggressive management practices are of primary importance throughout a project's life cycle to ensure the lowest cost; this includes successful leak testing of components. It should be noted that the opinions and conclusions expressed in this paper are those of the author and are not those of the Los Alamos National Laboratory or the Department of Energy

  10. Calibration of the NPL secondary standard radionuclide calibrator for the new 10R Schott, Type 1+ vials

    International Nuclear Information System (INIS)

    Baker, M.

    2005-01-01

    For many years, P6 vials have been used for the distribution of a wide range of diagnostic and therapeutic radioactive solutions. The activity measurements were performed in this geometry and, in time, the UK calibration system for nuclear medicine was based on this container as a standard. However, one major supplier of radiopharmaceuticals has replaced the P6 vial with the 10R Type 1+ Schott vial. As the dimensions of the new vial are different from those of the P6 vial and the responses of radionuclide calibrators are known to be container dependent, the need for re-calibration became apparent. Preliminary measurements made on some typical radionuclide calibrators for 125 I solution indicated a difference in response of about 10% between the two vials. The master ionisation chamber of the NPL secondary standard radionuclide calibrator has been re-calibrated and new calibration factors and volume correction factors for 10R Schott vials have been derived for the relevant medical radionuclides. The standard holder was also modified to accommodate the new larger vial. The complete list of factors and the method used to determine them is presented in this paper. The availability of these new factors will improve the quality of activity measurements in nuclear medicine, as calibration services can now be provided by NPL for the new container. These factors can also be employed for all commercial NPL secondary standard radionuclide calibrators (now known as the NPL-CRC and previously as the 671 or ISOCAL IV)

  11. Nuclear fuel technology - Tank calibration and volume determination for nuclear materials accountancy - Part 2: Data standardization for tank calibration

    International Nuclear Information System (INIS)

    2007-01-01

    Measurements of the volume and height of liquid in a process accountancy tank are often made in order to estimate or verify the tank's calibration or volume measurement equation. The calibration equation relates the response of the tank's measurement system to some independent measure of tank volume. The ultimate purpose of the calibration exercise is to estimate the tank's volume measurement equation (the inverse of the calibration equation), which relates tank volume to measurement system response. In this part of ISO 18213, it is assumed that the primary measurement-system response variable is liquid height and that the primary measure of liquid content is volume. This part of ISO 18213 presents procedures for standardizing a set of calibration data to a fixed set of reference conditions so as to minimize the effect of variations in ambient conditions that occur during the measurement process. The procedures presented herein apply generally to measurements of liquid height and volume obtained for the purpose of calibrating a tank (i.e. calibrating a tank's measurement system). When used in connection with other parts of ISO 18213, these procedures apply specifically to tanks equipped with bubbler probe systems for measuring liquid content. The standardization algorithms presented herein can be profitably applied when only estimates of ambient conditions, such as temperature, are available. However, the most reliable results are obtained when relevant ambient conditions are measured for each measurement of volume and liquid height in a set of calibration data. Information is provided on scope, physical principles, data required, calibration data, dimensional changes in the tank, multiple calibration runs and results on standardized calibration data. Four annexes inform about density of water, buoyancy corrections for mass determination, determination of tank heel volume and statistical method for aligning data from several calibration runs. A bibliography is

  12. STANDARD STARS AND EMPIRICAL CALIBRATIONS FOR Hα AND Hβ PHOTOMETRY

    International Nuclear Information System (INIS)

    Joner, Michael D.; Hintz, Eric G.

    2015-01-01

    We define an Hα photometric system that is designed as a companion to the well established Hβ index. The new system is built on spectrophotometric observations of field stars as well as stars in benchmark open clusters. We present data for 75 field stars, 12 stars from the Coma star cluster, 24 stars from the Hyades, 17 stars from the Pleiades, and 8 stars from NGC 752 to be used as primary standard stars in the new systems. We show that the system transformations are relatively insensitive to the shape of the filter functions. We make comparisons of the Hα index to the Hβ index and illustrate the relationship between the two systems. In addition, we present relations that relate both hydrogen indices to equivalent width and effective temperature. We derive equations to calibrate both systems for Main Sequence stars with spectral types in the range O9 to K2 for equivalent width and A2 to K2 for effective temperature

  13. STANDARD STARS AND EMPIRICAL CALIBRATIONS FOR Hα AND Hβ PHOTOMETRY

    Energy Technology Data Exchange (ETDEWEB)

    Joner, Michael D.; Hintz, Eric G., E-mail: joner@byu.edu, E-mail: hintz@byu.edu [Department of Physics and Astronomy, Brigham Young University, N283 ESC, Provo, UT 84602 (United States)

    2015-12-15

    We define an Hα photometric system that is designed as a companion to the well established Hβ index. The new system is built on spectrophotometric observations of field stars as well as stars in benchmark open clusters. We present data for 75 field stars, 12 stars from the Coma star cluster, 24 stars from the Hyades, 17 stars from the Pleiades, and 8 stars from NGC 752 to be used as primary standard stars in the new systems. We show that the system transformations are relatively insensitive to the shape of the filter functions. We make comparisons of the Hα index to the Hβ index and illustrate the relationship between the two systems. In addition, we present relations that relate both hydrogen indices to equivalent width and effective temperature. We derive equations to calibrate both systems for Main Sequence stars with spectral types in the range O9 to K2 for equivalent width and A2 to K2 for effective temperature.

  14. Standard-target calibration of an acoustic backscatter system

    Science.gov (United States)

    Foote, Kenneth G.; Martini, Marinna A.

    2010-01-01

    The standard-target method used to calibrate scientific echo sounders and other scientific sonars by a single, solid elastic sphere is being adapted to acoustic backscatter (ABS) systems. Its first application, to the AQUAscat 1000, is described. The on-axis sensitivity and directional properties of transducer beams at three operating frequencies, nominally 1, 2.5, and 4 MHz, have been determined using a 10-mm-diameter sphere of tungsten carbide with 6% cobalt binder. Preliminary results are reported for the 1-MHz transducer. Their application to measurements of suspended sediment made in situ with the same device is described. This will enable the data to be expressed directly in physical units of volume backscattering.

  15. On the long-term stability of calibration standards in different matrices

    International Nuclear Information System (INIS)

    Kandić, A.; Vukanac, I.; Djurašević, M.; Novković, D.; Šešlak, B.; Milošević, Z.

    2012-01-01

    In order to assure Quality Control in accordance with ISO/IEC 17025, it was important, from metrological point of view, to examine the long-term stability of calibration standards previously prepared. Comprehensive reconsideration on efficiency curves with respect to the ageing of calibration standards is presented in this paper. The calibration standards were re-used after a period of 5 years and analysis of the results showed discrepancies in efficiency values. - Highlights: ► Long-term stability of calibration standards (ISO 17025 Quality Control) was analyzed. ► Calibration standards covered the wide range of densities and chemical composition. ► Mineralized grass, powdered milk, surface soil and sand were used as standard matrices. ► Calibration standards were re-evaluated after 5 years. ► Results showed discrepancies of efficiency values.

  16. On the long-term stability of calibration standards in different matrices.

    Science.gov (United States)

    Kandić, A; Vukanac, I; Djurašević, M; Novković, D; Šešlak, B; Milošević, Z

    2012-09-01

    In order to assure Quality Control in accordance with ISO/IEC 17025, it was important, from metrological point of view, to examine the long-term stability of calibration standards previously prepared. Comprehensive reconsideration on efficiency curves with respect to the ageing of calibration standards is presented in this paper. The calibration standards were re-used after a period of 5 years and analysis of the results showed discrepancies in efficiency values. Copyright © 2012 Elsevier Ltd. All rights reserved.

  17. International comparison of calibration standards for exposure and absorbed dose

    International Nuclear Information System (INIS)

    Horakova, I.; Wagner, R.

    1990-01-01

    A comparison was performed of the primary calibration standards for 60 Co gamma radiation dose from Czechoslovakia (UDZ CSAV, Prague), Austria (OEFZS/BEV Seibersdorf) and Hungary (OMH Budapest) using ND 1005 (absolute measurement) and V-415 (by means of N x ) graphite ionization chambers. BEV achieved agreement better than 0.1%, OMH 0.35%. Good agreement was also achieved for the values of exposure obtained in absolute values and those obtained via N x , this for the ND 1005/8105 chamber. The first ever international comparison involving Czechoslovakia was also performed of the unit of absorbed gamma radiation in a water and/or graphite phantom. The participants included Czechoslovakia (UDZ CSAV Prague), the USSR (VNIIFTRI Moscow) and Austria (OEFZS/BEV Seibersdorf). In all measurements, the agreement was better than 1%, which, in view of the differences in methodologies (VNIIFTRI, BEV: calorimetry, UDZ, UVVVR: ionometry) and the overall inaccuracies in determining the absorbed dose values, is a good result. (author)

  18. Upgrading the Medical Physics Calibration Laboratory Towards ISO/IEC 17025: Radiation Standards and Calibration in Diagnostic Radiology

    International Nuclear Information System (INIS)

    Asmaliza Hashim; Muhammad Jamal Md Isa; Abd Aziz Mhd Ramli; Wan Hazlinda Ismail; Norhayati Abdullah; Shahrul Azlan Azizan; Siti Sara Deraman; Nor Azlin Azraai; Md Khairusalih Md Zin

    2010-01-01

    Calibration of quality control (QC) test tools used in diagnostic radiology is legally required under the Ministry of Health (MOH) requirement. The Medical Physics Calibration Laboratory of the Malaysian Nuclear Agency is the national focal point for the calibration of quality control test tools used in diagnostic radiology. The Medical Physics Calibration Laboratory has measurement traceability to primary standard dosimetry laboratory (Physikalisch-Technische Bundesanstalt (PTB)), thus providing an interface between the primary standard dosimetry laboratory and Malaysian hospitals, clinics and license class H holder. The Medical Physics Calibration Laboratory facility is comprised of a constant potential x-ray system with a capability of 160 kV tube and a series of reference and working standard ion chambers. The stability of reference and working standard ion chambers was measured using strontium-90. Dosimetric instruments used in diagnostic radiology is calibrated in terms of air kerma to comply with an International Code of Practices of dosimetry for example IAEA's Technical Report Series number 457. The new series of standard radiation qualities was established based on ISO/IEC 61267. The measurement of beam homogeneity was measured using film and ion chamber to define the field size at certain distance and kV output was measured using the spectrometer and non-invasive kVp meter. The uncertainties measurement was determined with expended uncertainties to a level of confidence of approximately 95% (coverage factor k=2). This paper describes the available facility and the effort of the Medical Physics Calibration Laboratory to upgrade the laboratory towards ISO/IEC 17025. (author)

  19. Standard practice for alternate actinide calibration for inductively coupled plasma-mass spectrometry

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2004-01-01

    1.1 This practice provides guidance for an alternate linear calibration for the determination of selected actinide isotopes in appropriately prepared aqueous solutions by Inductively Coupled Plasma-Mass Spectrometry (ICP-MS). This alternate calibration is mass bias adjusted using thorium-232 (232Th) and uranium-238 (238U) standards. One of the benefits of this standard practice is the ability to calibrate for the analysis of highly radioactive actinides using calibration standards at much lower specific activities. Environmental laboratories may find this standard practice useful if facilities are not available to handle the highly radioactive standards of the individual actinides of interest. 1.2 The instrument response for a series of determinations of known concentration of 232Th and 238U defines the mass versus response relationship. For each standard concentration, the slope of the line defined by 232Th and 238U is used to derive linear calibration curves for each mass of interest using interference equ...

  20. The calibration procedures in the Studsvik standardized personnel dosimetry system

    International Nuclear Information System (INIS)

    Widell, C.O.

    1978-01-01

    Every large nuclear installation in Sweden reads its own personnel TLDs. In order to supervise this decentralized reading of dose meters, the TLD readers are connected by telephone lines to a central computer for dose registration. This computer is used both for registering the personnel doses and for checking the TLD readers. This checking is performed by the use of pre-irradiated calibration dose meters which are always used when a batch of personnel dose meters are read. The pre-irradiated dose meters are either irradiated using 137 Cs to various doses up to 100mSv(10000mrem) or using a 90 Sr source in a reference dose irradiator to a dose equal to 3mSv(300mrem) from a 137 Cs source. The results from the reading of the pre-irradiated dose meters are processed by the computer and a calibration factor is calculated. The calibration factor is automatically used to calculate the doses to the personnel TLD's. However, if the calibration factor deviates by more than 10% from the previously used factor, this fact is shown to the operator - who then has to decide what calibration factor is going to be used. This calibration and supervisory procedure together with the safety interlocks in the TLD readers has resulted in a very reliable and accurate dosimetry system. (author)

  1. Standardization of irradiation values at the Radiation Calibration Laboratory

    International Nuclear Information System (INIS)

    Pham Van Dung; Hoang Van Nguyen; Phan Van Toan; Phan Dinh Sinh; Tran Thi Tuyet; Do Thi Phuong

    2007-01-01

    The objective of the theme is to determine dose rates around radiation facilities and sources in the NRI Radiation Calibration Laboratory. By improving equipment, calibrating a main dosemeter and carrying out experiments, the theme team received the following results: 1. The controller of a X-rays generator PY(-200 was improved. It permits to increase accuracy of radiation dose calibration up to 2-4 times; 2. The FAMER DOSEMETER 2570/1B with the ionization chamber NE 2575 C of the NRI Radiation Calibration Laboratory was calibrated at SSDL (Hanoi); 3. Dose rates at 4 positions around a high activity Co-60 source were determined; 4. Dose rates at 3 positions around a low activity Co-60 source were determined; 5. Dose rates at 3 positions around a low activity Cs-137 source were determined; 6. Dose rate at 1 position of a X-rays beam (Eaverage = 48 keV) was determined; 7. Dose rate at 1 position of a X-rays beam (Eaverage = 65 keV) was determined. (author)

  2. Traceable calibration and demonstration of a portable dynamic force transfer standard

    Science.gov (United States)

    Vlajic, Nicholas; Chijioke, Ako

    2017-08-01

    In general, the dynamic sensitivity of a force transducer depends upon the mechanical system in which it is used. This dependence serves as motivation to develop a dynamic force transfer standard, which can be used to calibrate an application transducer in situ. In this work, we SI-traceably calibrate a hand-held force transducer, namely an impact hammer, by using a mass suspended from a thin line which is cut to produce a known dynamic force in the form of a step function. We show that this instrument is a promising candidate as a transfer standard, since its dynamic response has small variance between different users. This calibrated transfer standard is then used to calibrate a secondary force transducer in an example application setting. The combined standard uncertainty (k  =  2) in the calibration of the transfer standard was determined to be 2.1% or less, up to a bandwidth of 5 kHz. The combined standard uncertainty (k  =  2) in the performed transfer calibration was less than 4%, up to 3 kHz. An advantage of the transfer calibration framework presented here, is that the transfer standard can be used to transfer SI-traceable calibrations without the use of any SI-traceable voltage metrology instrumentation.

  3. Calibration

    International Nuclear Information System (INIS)

    Greacen, E.L.; Correll, R.L.; Cunningham, R.B.; Johns, G.G.; Nicolls, K.D.

    1981-01-01

    Procedures common to different methods of calibration of neutron moisture meters are outlined and laboratory and field calibration methods compared. Gross errors which arise from faulty calibration techniques are described. The count rate can be affected by the dry bulk density of the soil, the volumetric content of constitutional hydrogen and other chemical components of the soil and soil solution. Calibration is further complicated by the fact that the neutron meter responds more strongly to the soil properties close to the detector and source. The differences in slope of calibration curves for different soils can be as much as 40%

  4. The 1998 calibration of Australian secondary standards of exposure and absorbed dose at 60Co

    International Nuclear Information System (INIS)

    Huntley, R.B.; Van der Gaast, H.

    1998-10-01

    New calibration factors are reported for several of the ionization chambers maintained at the Australian Radiation Laboratory (ARL) and at the Australian Nuclear Science and Technology Organisation (ANSTO) as Australian secondary standards of exposure/air kerma and absorbed dose at 60 Co. These calibration factors supplement or replace the calibration factors given in earlier reports. Updated 90 Sr reference source data are given for the ARL chambers, and for two of the ANSTO chambers. These results confirm the stability of the secondary standards. A re-calibration of the ANSTO reference electrometer is reported. This was carried out using an improved method, which is fully described

  5. Exploring a Black Body Source as an Absolute Radiometric Calibration Standard and Comparison with a NIST Traced Lamp Standard

    Science.gov (United States)

    Green, Robert O.; Chrien, Thomas; Sarture, Chuck

    2001-01-01

    Radiometric calibration of the Airborne Visible/Infrared Imaging Spectrometer (AVIRIS) is required for the scientific research and application objectives pursued with the spectroscopic measurements. Specifically calibration is required for: inter-comparison of AVIRIS data measured at different locations and at different times; analysis of AVIRIS data with data measured by other instruments; and analysis of AVIRIS data in conjunction with computer models. The primary effect of radiometric calibration is conversion of AVIRIS instrument response values (digitized numbers, or DN) to units of absolute radiance. For example, a figure shows the instrument response spectrum measured by AVIRIS over a portion of Rogers Dry Lake, California, and another figure shows the same spectrum calibrated to radiance. Only the calibrated spectrum may be quantitatively analyzed for science research and application objectives. Since the initial development of the AVIRIS instrument-radiometric calibration has been based upon a 1000-W irradiance lamp with a calibration traced to the National Institute of Standards and Technology (NIST). There are several advantages to this irradiance-lamp calibration approach. First, the considerable effort of NIST backs up the calibration. Second, by changing the distance to the lamp, the output can closely span the radiance levels measured by AVIRIS. Third, this type of standard is widely used. Fourth, these calibrated lamps are comparatively inexpensive. Conversely, there are several disadvantages to this approach as well. First, the lamp is not a primary standard. Second, the lamp output characteristics may change in an unknown manner through time. Third, it is difficult to assess, constrain, or improve the calibration uncertainty delivered with the lamp. In an attempt to explore the effect and potentially address some of these disadvantages a set of analyses and measurements comparing an irradiance lamp with a black-body source have been completed

  6. Calibration and consistency of results of an ionization-chamber secondary standard measuring system for activity

    International Nuclear Information System (INIS)

    Schrader, Heinrich

    2000-01-01

    Calibration in terms of activity of the ionization-chamber secondary standard measuring systems at the PTB is described. The measurement results of a Centronic IG12/A20, a Vinten ISOCAL IV and a radionuclide calibrator chamber for nuclear medicine applications are discussed, their energy-dependent efficiency curves established and the consistency checked using recently evaluated radionuclide decay data. Criteria for evaluating and transferring calibration factors (or efficiencies) are given

  7. Establishment of standard low energy x-ray, radioprotection levels, for calibration of instruments

    International Nuclear Information System (INIS)

    Oliveira, Eliane Carmo

    1995-01-01

    Seven standard low energy X-rays fields were established, radioprotection level, at the Calibration Laboratory of IPEN. Five of the standard calibration qualities used at the National Physical Laboratory, England, with energies between 16 and 38 keV, and two recommended by the International Standard Organization, with energies of 33 and 48 keV, were reproduced. The calibration conditions, radiotherapy level, from 14 to 21 keV, were also verified. Different portable radiation monitors as ionization chambers and Geiger-Mueller detectors were studied in relation to their energy dependence. (author)

  8. Overview of Photovoltaic Calibration and Measurement Standards at GRC

    Science.gov (United States)

    Baraona, Cosmo; Snyder, David; Brinker, David; Bailey, Sheila; Curtis, Henry; Scheiman, David; Jenkins, Phillip

    2002-01-01

    Photovoltaic (PV) systems (cells and arrays) for spacecraft power have become an international market. This market demands accurate prediction of the solar array power output in space throughout the mission life of the spacecraft. Since the beginning of space flight, space-faring nations have independently developed methods to calibrate solar cells for power output in low Earth orbit (LEO). These methods rely on terrestrial, laboratory, or extraterrestrial light sources to simulate or approximate the air mass zero (AM0) solar intensity and spectrum.

  9. Ultrasonic transverse velocity calibration of standard blocks for use in non-destructive testing

    International Nuclear Information System (INIS)

    Silva, C E R; Braz, D S; Maggi, L E; Felix, R P B Costa

    2015-01-01

    Standard blocks are employed in the verification of the equipment used in Ultrasound Non-Destructive Testing. To assure the metrology reliability of all the measurement process, it is necessary to calibrate or certify these Standard blocks. In this work, the transverse wave velocity and main dimensions were assessed according to the specifications ISO Standards. For transverse wave velocity measurement, a 5 MHz transverse wave transducer, a waveform generator, an oscilloscope and a computer with a program developed in LabVIEW TM were used. Concerning the transverse wave velocity calibration, only two Standard blocks of the 4 tested is in accordance with the standard

  10. Characterization of a 137Cs standard source for calibration purposes at CRCN-NE

    International Nuclear Information System (INIS)

    Oliveira, Mercia L.; Santos, Marcus A.P. dos; Benvides, Clayton A.

    2008-01-01

    Radiation protection monitoring instruments should be calibrated by accredited calibration laboratories. To offer calibration services, a laboratory must accomplish all requirements established by the national regulatory agency. The Calibration Service of the Centro Regional de Ciencias Nucleares (CRCN-NE), Comissao Nacional de Energia Nuclear, Recife, Brazil, is trying to achieve this accreditation. In the present work, a 137 Cs standard source was characterized following the national and international recommendations and the results are presented. This source is a commercially available single source irradiator model 28-8A, manufactured by J.L. Shepherd and Associates, with initial activity of 444 GBq (05/13/03). To provide different air kerma rates, as required for the calibration of portable radiation monitors, this irradiator have a set of four lead attenuators with different thickness, providing attenuation factors equal to 2, 4, 10 and 100 times (nominally). The performed tests included: size and uniformity of the radiation standard field at calibration reference position, variation of the air kerma rate for different lead attenuators, determination of attenuation factors for each lead attenuator configuration, and determination of the radiation scattering at the calibration reference position. The results showed the usefulness of the 137 Cs standard source for the calibration of radiation protection monitoring detectors. (author)

  11. Services of the CDRH X-ray calibration laboratory and their traceability to National Standards

    Energy Technology Data Exchange (ETDEWEB)

    Cerra, F.; Heaton, H.T. [Center for Devices and Radiological Health, Rockville, MD (United States)

    1993-12-31

    The X-ray Calibration Laboratory (XCL) of the Center for Devices and Radiological Health (CDRH) provides calibration services for the Food and Drug Administration (FDA). The instruments calibrated are used by FDA and contract state inspectors to verify compliance with federal x-ray performance standards and for national surveys of x-ray trends. In order to provide traceability of measurements, the CDRH XCL is accredited by the National Voluntary Laboratory Accreditation Program (NVLAP) for reference, diagnostic, and x-ray survey instrument calibrations. In addition to these accredited services, the CDRH XCL also calibrates non-invasive kVp meters in single- and three-phase x-ray beams, and thermoluminescent dosimeter (TLD) chips used to measure CT beam profiles. The poster illustrates these services and shows the traceability links back to the National Standards.

  12. Services of the CDRH X-ray calibration laboratory and their traceability to National Standards

    International Nuclear Information System (INIS)

    Cerra, F.; Heaton, H.T.

    1993-01-01

    The X-ray Calibration Laboratory (XCL) of the Center for Devices and Radiological Health (CDRH) provides calibration services for the Food and Drug Administration (FDA). The instruments calibrated are used by FDA and contract state inspectors to verify compliance with federal x-ray performance standards and for national surveys of x-ray trends. In order to provide traceability of measurements, the CDRH XCL is accredited by the National Voluntary Laboratory Accreditation Program (NVLAP) for reference, diagnostic, and x-ray survey instrument calibrations. In addition to these accredited services, the CDRH XCL also calibrates non-invasive kVp meters in single- and three-phase x-ray beams, and thermoluminescent dosimeter (TLD) chips used to measure CT beam profiles. The poster illustrates these services and shows the traceability links back to the National Standards

  13. Comparison Between a Reference Torque Standard Machine and a Deadweight Torque Standard Machine to BE Used in Torque Calibration

    Science.gov (United States)

    Meng, Feng; Zhang, Zhimin; Lin, Jing

    The paper describes the reference torque standard machine with high accuracy and multifunction, developed by our institute, and introduces the structure and working principle of this machine. It has three main functions. The first function is the hydraulic torque wrench calibration function. The second function is torque multiply calibration function. The third function is reference torque standard machine function. We can calibrate the torque multipliers, hydraulic wrenches and transducers by this machine. A comparison experiment has been done between this machine and a deadweight torque standard machine. The consistency between the 30 kNm reference torque machine and the 2000 Nm dead-weight torque standard machine under the claimed uncertainties was verified.

  14. Definition and production of calibration standard neutron sources for radiation protection device calibration

    International Nuclear Information System (INIS)

    De Matos, E.

    1987-01-01

    To improve the characterization of radioprotection devices performances, it would be advisable to calibrate these devices in neutron spectra which are nearly like those met in practice (nuclear reactors, plutonium technology laboratories...). The purpose of this work is, in a first time, to choose the nature and the dimensions of the different shields used to achieve broad typical neutron spectra extending to lower energies from a 14.8 MeV neutron beam. The second step is the evaluation of spectral distribution and calculation of associated dosimetric quantities. For that, several spectrometric techniques are employed: on one hand, activation detectors and Bonner spheres method named rough spectrometry; on the other hand, an accurate spectrometry which uses recoil proton counters. The dosimetric quantities, especially the value of kerma deduced from these spectra must be in good agreement with those measured with a tissue equivalent ionization chamber [fr

  15. Establishing a standard calibration methodology for MOSFET detectors in computed tomography dosimetry

    International Nuclear Information System (INIS)

    Brady, S. L.; Kaufman, R. A.

    2012-01-01

    Purpose: The use of metal-oxide-semiconductor field-effect transistor (MOSFET) detectors for patient dosimetry has increased by ∼25% since 2005. Despite this increase, no standard calibration methodology has been identified nor calibration uncertainty quantified for the use of MOSFET dosimetry in CT. This work compares three MOSFET calibration methodologies proposed in the literature, and additionally investigates questions relating to optimal time for signal equilibration and exposure levels for maximum calibration precision. Methods: The calibration methodologies tested were (1) free in-air (FIA) with radiographic x-ray tube, (2) FIA with stationary CT x-ray tube, and (3) within scatter phantom with rotational CT x-ray tube. Each calibration was performed at absorbed dose levels of 10, 23, and 35 mGy. Times of 0 min or 5 min were investigated for signal equilibration before or after signal read out. Results: Calibration precision was measured to be better than 5%–7%, 3%–5%, and 2%–4% for the 10, 23, and 35 mGy respective dose levels, and independent of calibration methodology. No correlation was demonstrated for precision and signal equilibration time when allowing 5 min before or after signal read out. Differences in average calibration coefficients were demonstrated between the FIA with CT calibration methodology 26.7 ± 1.1 mV cGy −1 versus the CT scatter phantom 29.2 ± 1.0 mV cGy −1 and FIA with x-ray 29.9 ± 1.1 mV cGy −1 methodologies. A decrease in MOSFET sensitivity was seen at an average change in read out voltage of ∼3000 mV. Conclusions: The best measured calibration precision was obtained by exposing the MOSFET detectors to 23 mGy. No signal equilibration time is necessary to improve calibration precision. A significant difference between calibration outcomes was demonstrated for FIA with CT compared to the other two methodologies. If the FIA with a CT calibration methodology was used to create calibration coefficients for the

  16. Establishing a standard calibration methodology for MOSFET detectors in computed tomography dosimetry.

    Science.gov (United States)

    Brady, S L; Kaufman, R A

    2012-06-01

    The use of metal-oxide-semiconductor field-effect transistor (MOSFET) detectors for patient dosimetry has increased by ~25% since 2005. Despite this increase, no standard calibration methodology has been identified nor calibration uncertainty quantified for the use of MOSFET dosimetry in CT. This work compares three MOSFET calibration methodologies proposed in the literature, and additionally investigates questions relating to optimal time for signal equilibration and exposure levels for maximum calibration precision. The calibration methodologies tested were (1) free in-air (FIA) with radiographic x-ray tube, (2) FIA with stationary CT x-ray tube, and (3) within scatter phantom with rotational CT x-ray tube. Each calibration was performed at absorbed dose levels of 10, 23, and 35 mGy. Times of 0 min or 5 min were investigated for signal equilibration before or after signal read out. Calibration precision was measured to be better than 5%-7%, 3%-5%, and 2%-4% for the 10, 23, and 35 mGy respective dose levels, and independent of calibration methodology. No correlation was demonstrated for precision and signal equilibration time when allowing 5 min before or after signal read out. Differences in average calibration coefficients were demonstrated between the FIA with CT calibration methodology 26.7 ± 1.1 mV cGy(-1) versus the CT scatter phantom 29.2 ± 1.0 mV cGy(-1) and FIA with x-ray 29.9 ± 1.1 mV cGy(-1) methodologies. A decrease in MOSFET sensitivity was seen at an average change in read out voltage of ~3000 mV. The best measured calibration precision was obtained by exposing the MOSFET detectors to 23 mGy. No signal equilibration time is necessary to improve calibration precision. A significant difference between calibration outcomes was demonstrated for FIA with CT compared to the other two methodologies. If the FIA with a CT calibration methodology was used to create calibration coefficients for the eventual use for phantom dosimetry, a measurement error ~12

  17. An accurate on-site calibration system for electronic voltage transformers using a standard capacitor

    Science.gov (United States)

    Hu, Chen; Chen, Mian-zhou; Li, Hong-bin; Zhang, Zhu; Jiao, Yang; Shao, Haiming

    2018-05-01

    Ordinarily electronic voltage transformers (EVTs) are calibrated off-line and the calibration procedure requires complex switching operations, which will influence the reliability of the power grid and induce large economic losses. To overcome this problem, this paper investigates a 110 kV on-site calibration system for EVTs, including a standard channel, a calibrated channel and a PC equipped with the LabView environment. The standard channel employs a standard capacitor and an analogue integrating circuit to reconstruct the primary voltage signal. Moreover, an adaptive full-phase discrete Fourier transform (DFT) algorithm is proposed to extract electrical parameters. The algorithm involves the process of extracting the frequency of the grid, adjusting the operation points, and calculating the results using DFT. In addition, an insulated automatic lifting device is designed to realize the live connection of the standard capacitor, which is driven by a wireless remote controller. A performance test of the capacitor verifies the accurateness of the standard capacitor. A system calibration test shows that the system ratio error is less than 0.04% and the phase error is below 2‧, which meets the requirement of the 0.2 accuracy class. Finally, the developed calibration system was used in a substation, and the field test data validates the availability of the system.

  18. Advisory Committee for the Calibration Standards of Ionizing Radiation Measurement

    International Nuclear Information System (INIS)

    1982-01-01

    An account of the activity during the past two years and of the plans for future work is given for the three Sections of the Comite Consultatif pour les Etalons de Mesure des Rayonnements Ionisants. Section I (Rayons X et #betta#, electrons) studied in detail the results of an intercomparison of Frike dosimeters. A recommendation was made concerning the possibility of expressing calibrations made in terms of exposure in terms of air kerma or water kerma. Section II (Mesure des radionucleides) studied the results of recent international comparisons ( 55 Fe, 133 Ba and 134 Cs) and made plans for new ones. Section III (Mesures neutroniques) presented the status of the international comparisons of neutron fluence rate in progress and decided to organize new ones. The reports of the Section chairmen are followed by the presentation of the work carried out at BIPM by the corresponding groups. The status of the proposal by Section III for a 14 MeV neutron dosimetry facility at BIPM is discussed in detail and a proposal is made for a neutron dosimetry intercomparison [fr

  19. Assuring Academic Achievement Standards: From Moderation to Calibration

    Science.gov (United States)

    Sadler, D. Royce

    2013-01-01

    The course (module) grades entered on higher education academic records (transcripts) purportedly represent substantive levels of student achievement. They are often taken at face value and accepted as comparable across courses. Research undertaken over several decades has shown that the underlying standards against which student works are…

  20. Calibration of the SH134-20 Standard Gain Horn

    DEFF Research Database (Denmark)

    Pivnenko, Sergey; Breinbjerg, Olav

    This report documents the measurement of the linearly polarized SH134-20 Standard Gain Horn. The measurement comprises on-axis gain, on-axis polarization characteristics, and reflection coefficient at 111 frequencies in the frequency range from 22-33 GHz. The measurement was carried out at the DTU...

  1. Standardization of Laser Methods and Techniques for Vibration Measurements and Calibrations

    International Nuclear Information System (INIS)

    Martens, Hans-Juergen von

    2010-01-01

    The realization and dissemination of the SI units of motion quantities (vibration and shock) have been based on laser interferometer methods specified in international documentary standards. New and refined laser methods and techniques developed by national metrology institutes and by leading manufacturers in the past two decades have been swiftly specified as standard methods for inclusion into in the series ISO 16063 of international documentary standards. A survey of ISO Standards for the calibration of vibration and shock transducers demonstrates the extended ranges and improved accuracy (measurement uncertainty) of laser methods and techniques for vibration and shock measurements and calibrations. The first standard for the calibration of laser vibrometers by laser interferometry or by a reference accelerometer calibrated by laser interferometry (ISO 16063-41) is on the stage of a Draft International Standard (DIS) and may be issued by the end of 2010. The standard methods with refined techniques proved to achieve wider measurement ranges and smaller measurement uncertainties than that specified in the ISO Standards. The applicability of different standardized interferometer methods to vibrations at high frequencies was recently demonstrated up to 347 kHz (acceleration amplitudes up to 350 km/s 2 ). The relative deviations between the amplitude measurement results of the different interferometer methods that were applied simultaneously, differed by less than 1% in all cases.

  2. Benefits of on-wafer calibration standards fabricated in membrane technology

    Science.gov (United States)

    Rohland, M.; Arz, U.; Büttgenbach, S.

    2011-07-01

    In this work we compare on-wafer calibration standards fabricated in membrane technology with standards built in conventional thin-film technology. We perform this comparison by investigating the propagation of uncertainties in the geometry and material properties to the broadband electrical properties of the standards. For coplanar waveguides used as line standards the analysis based on Monte Carlo simulations demonstrates an up to tenfold reduction in uncertainty depending on the electromagnetic waveguide property we look at.

  3. Comparative evaluations of surface contamination detectors calibration with radioactive sources - used in the Goiania accident, and standard sources

    International Nuclear Information System (INIS)

    Becker, P.H.B.; Marecha, M.H.H.

    1997-01-01

    The construction of Cs-137 standard flat sources for calibration of surface contamination detectors, used in the Goiania accident in 1987, is described and the procedures adopted are reported. At that time, standard sources were not available. Nowadays the Instituto de Radioprotecao e Dosimetria has standard sources acquired from Amersham which are used as calibration standards for surface contamination detectors. Comparative evaluations between the standard flat sources constructed for the accident and the calibrated ones are presented

  4. Bias in segmented gamma scans arising from size differences between calibration standards and assay samples

    International Nuclear Information System (INIS)

    Sampson, T.E.

    1991-01-01

    Recent advances in segmented gamma scanning have emphasized software corrections for gamma-ray self-adsorption in particulates or lumps of special nuclear material in the sample. another feature of this software is an attenuation correction factor formalism that explicitly accounts for differences in sample container size and composition between the calibration standards and the individual items being measured. Software without this container-size correction produces biases when the unknowns are not packaged in the same containers as the calibration standards. This new software allows the use of different size and composition containers for standards and unknowns, as enormous savings considering the expense of multiple calibration standard sets otherwise needed. This paper presents calculations of the bias resulting from not using this new formalism. These calculations may be used to estimate bias corrections for segmented gamma scanners that do not incorporate these advanced concepts

  5. Calibration of ARI QC ionisation chambers using the Australian secondary standards for activity

    International Nuclear Information System (INIS)

    Mo, L.; Van Der Gaast, H.A.; Alexiev, D.; Butcher, K.S.A.; Davies, J.

    1999-01-01

    The Secondary Standard Activity Laboratory (SSAL) in ANSTO routinely provides standardised radioactive sources, traceable activity measurements and custom source preparation services to customers. The most important activity carried out is the calibration of ionisation chambers located in the Quality Control (QC) section of Australian Radioisotopes (ARI). This ensures that their activity measurements are traceable to the Australian primary methods of standardisation. ARI QC ionisation chambers are calibrated for 99m Tc, 67 Ga, 131 I, 201 Tl and 153 Sm. The SSAL has a TPA ionisation chamber, which has been directly calibrated against a primary standard for a variety of radioactive nuclides. Calibration factors for this chamber were determined specifically for the actual volumes (5ml for 99m Tc, 131 I, 2ml for 67 Ga, 201 Tl and 3 ml for 153 Sm) and types of vial (Wheaton) which are routinely used at ARI. These calibration factors can be used to accurately measure the activity of samples prepared by ARI. The samples can subsequently be used to calibrate the QC ionisation chambers. QC ionisation chambers are re-calibrated biannually

  6. Standardization of the calibration of brachytherapy sources at the IAEA dosimetry laboratory

    International Nuclear Information System (INIS)

    Shanta, A.; Andreo, P.

    1996-01-01

    A new service to SSDLs has been initiated at the IAEA Dosimetry Laboratory for providing calibrations of well-type ionisation chambers, used in brachytherapy applications, which are traceable to the International Measurement System. Considering that the most common radionuclide used in the developing countries is 137 Cs, two such sources of the type used for gynaecological intracavitary applications have been purchased by the Agency and calibrated at the National Institute of Standards and Technology (NIST), USA. These 137 Cs reference sources together with a well-type ionization chamber constitute the IAEA brachytherapy dosimetry standard. Based on the recommendations by a group of experts, a method has been developed for transferring calibrations to SSDLs which is described in this paper. The method is based on the acquisition by the SSDLs of sources and equipment similar to those at the IAEA. The well-type chamber is to be calibrated at the IAEA Dosimetry Laboratory, and this will be used at the SSDL to calibrate its own reference sources. These sources can in turn by used to calibrate well-type chambers from hospital users and to calibrate other type of sources by performing measurements in air. In order to standardize the procedures for the two methods and to provide guidance to the SSDLs, measurements have been carried out at the IAEA Dosimetry Laboratory. The reproducibility of the two type of measurements has been found to be better than 0.5%, and the uncertainty of calibrations estimated to be less than 1.5% (one standard deviation). (author). 8 refs, 8 figs, 2 tabs

  7. Calibration of Modulation Transfer Function of Surface Profilometers with 1D and 2D Binary Pseudo-random Array Standards

    International Nuclear Information System (INIS)

    Yashchuk, Valeriy V.; McKinney, Wayne R.; Takacs, Peter Z.

    2008-01-01

    We suggest and describe the use of a binary pseudo-random grating as a standard test surface for calibration of the modulation transfer function of microscopes. Results from calibration of a MicromapTM-570 interferometric microscope are presented.

  8. Calibration Standards for Surface Topography Measuring Systems down to Nanometric Range

    DEFF Research Database (Denmark)

    Trumpold, H.; De Chiffre, Leonardo; Andreasen, Jan Lasson

    compression and injection moulded plastic negatives and Ni-negatives have been made from which again Ni-positives were produced. The replication processes showed negligible deviations from the Pt and Pa values compared to the primary standards. An important prerequisite is the cleanliness of the surfaces......Background For the precise and accurate measurement of surface topography a whole range of surface detection systems is available. With their application in research and production problems arise due to the lack of traceable standard artefacts for the instrument calibration in X, Y and Z directions...... and for the calibration of filters. Existing ISO standards on calibration specimens are inadequate and limited in that they only cover contacting instruments and only partially the measuring ranges for these instruments. The whole range of non-contacting instruments are not covered despite their increasing use...

  9. Uncertainty Analysis of Spectral Irradiance Reference Standards Used for NREL Calibrations

    Energy Technology Data Exchange (ETDEWEB)

    Habte, A.; Andreas, A.; Reda, I.; Campanelli, M.; Stoffel, T.

    2013-05-01

    Spectral irradiance produced by lamp standards such as the National Institute of Standards and Technology (NIST) FEL-type tungsten halogen lamps are used to calibrate spectroradiometers at the National Renewable Energy Laboratory. Spectroradiometers are often used to characterize spectral irradiance of solar simulators, which in turn are used to characterize photovoltaic device performance, e.g., power output and spectral response. Therefore, quantifying the calibration uncertainty of spectroradiometers is critical to understanding photovoltaic system performance. In this study, we attempted to reproduce the NIST-reported input variables, including the calibration uncertainty in spectral irradiance for a standard NIST lamp, and quantify uncertainty for measurement setup at the Optical Metrology Laboratory at the National Renewable Energy Laboratory.

  10. Development of composite calibration standard for quantitative NDE by ultrasound and thermography

    Science.gov (United States)

    Dayal, Vinay; Benedict, Zach G.; Bhatnagar, Nishtha; Harper, Adam G.

    2018-04-01

    Inspection of aircraft components for damage utilizing ultrasonic Non-Destructive Evaluation (NDE) is a time intensive endeavor. Additional time spent during aircraft inspections translates to added cost to the company performing them, and as such, reducing this expenditure is of great importance. There is also great variance in the calibration samples from one entity to another due to a lack of a common calibration set. By characterizing damage types, we can condense the required calibration sets and reduce the time required to perform calibration while also providing procedures for the fabrication of these standard sets. We present here our effort to fabricate composite samples with known defects and quantify the size and location of defects, such as delaminations, and impact damage. Ultrasonic and Thermographic images are digitally enhanced to accurately measure the damage size. Ultrasonic NDE is compared with thermography.

  11. Primary calibration of TXRF in comparison with the standard droplet procedure

    International Nuclear Information System (INIS)

    Dobler, M.; Reus, U.; Knoth, J.; Schwenke, H.

    2000-01-01

    For the determination of contamination on wafer surfaces with total reflection x-ray fluorescence spectrometry (TXRF) normally external 1 ng Ni droplet standards were used for calibration. This method is based on several assumptions about the properties of the standard droplet which are strongly affected by the preparation of the samples. In this paper a study is resented which compares the external droplet method with a calibration procedure using the fundamental physical background of total reflection x-ray fluorescence spectrometry and the properties of Ni bulk material. The particular features of the two methods will be discussed and the obtained results compared to each other. It is demonstrated in this study that the calibration with Ni bulk material is a primary method which offers several advantages compared to the calibration based on droplet standards. These advantages are unique and enable a more reliable and reproducible quantification of contamination on wafer surfaces. This is caused by the fact that the method is standardless and only based on fundamental parameters and natural constants. It is also demonstrated that effects which could be caused by especial features of the measured samples (particle or film, e.g.) or by the degradation of the calibration sample could be excluded. (author)

  12. Toward a standard line for use in multibeam echo sounder calibration

    Science.gov (United States)

    Weber, Thomas C.; Rice, Glen; Smith, Michael

    2018-06-01

    A procedure is suggested in which a relative calibration for the intensity output of a multibeam echo sounder (MBES) can be performed. This procedure identifies a common survey line (i.e., a standard line), over which acoustic backscatter from the seafloor is collected with multiple MBES systems or by the same system multiple times. A location on the standard line which exhibits temporal stability in its seafloor backscatter response is used to bring the intensity output of the multiple MBES systems to a common reference. This relative calibration procedure has utility for MBES users wishing to generate an aggregate seafloor backscatter mosaic using multiple systems, revisiting an area to detect changes in substrate type, and comparing substrate types in the same general area but with different systems or different system settings. The calibration procedure is demonstrated using three different MBES systems over 3 different years in New Castle, NH, USA.

  13. Re-Establishment of Standard Radiation Qualities for Calibration of Dosemeter in Diagnostic Radiology - RQR Series

    International Nuclear Information System (INIS)

    Asmaliza Hashim; Norhayati Abdullah; Mohd Firdaus Abd Rahman

    2016-01-01

    After repairing the high voltage (HV) generator for Philips MG165 X-Ray Machine, the reestablishment of the standard radiation qualities has been done at Medical Physics Calibration Laboratory to meet the IEC and IAEA standard. Standard radiation qualities are the important criteria for calibration of dosemeter in diagnostic radiology. Standard radiation qualities are defined as the added filtration needed to produce and the half value layer (HVL) of the beam for specifies x-ray tube kilo voltage (kV). For calibration of dosemeter in diagnostic radiology, standard radiation qualities RQR represent the beam incident on the patient in general radiography, fluoroscopy and dental application. The HVL were measured using PTW ion chamber of volume 1 cm"3 with PTW electrometer and aluminium filter with 99.9 % purity was used as additional filter for RQR and filter for HVL. The first establishment of standard radiation qualities was made in 2009 for the radiation qualities of RQR. The results of additional filter and 1st HVL from 2009 to 2016 will be discussed further in paper. The ratios of the measured HVL to the standard IEC HVL value for the RQR series also described in this paper. The details of the measurement and the results are described in this paper. (author)

  14. Transfer standard device to improve the traceable calibration of physiotherapy ultrasound machines

    NARCIS (Netherlands)

    Hekkenberg, R.T.; Richards, A.; Beissner, K.; Zeqiri, B.; Bezemer, R.A.; Hodnett, M.; Prout, G.; Cantrall, C.

    2006-01-01

    Ultrasound (US) physiotherapy as a clinical treatment is extremely common in the Western world. Internationally, regulation to ensure safe application of US physiotherapy by regular calibration ranges from nil to mandatory. The need for a portable power standard (PPS) has been addressed within a

  15. A standard 9MeV γ beam for detector calibration

    International Nuclear Information System (INIS)

    Troesch-Lasseur, G.; Bermann, F.; Gaulard, M.

    1975-01-01

    A γ capture irradiation device with beam extraction is being developed at Triton. The mean energy in the beam is 9MeV. The beam intensity has been determined from absorbed dose measurements according to ICRU specifications. The maximum dose rate taken as calibration standard is 125+-9rad/h [fr

  16. Secondary calibration laboratory for ionizing radiation laboratory accreitation program National Institute of Standards and Technology National Voluntary Laboratory Accreditation Program

    Energy Technology Data Exchange (ETDEWEB)

    Martin, P.R.

    1993-12-31

    This paper presents an overview of the procedures and requirements for accreditation under the Secondary Calibration Laboratory for Ionizing Radiation Program (SCLIR LAP). The requirements for a quality system, proficiency testing and the onsite assessment are discussed. The purpose of the accreditation program is to establish a network of secondary calibration laboratories that can provide calibrations traceable to the primary national standards.

  17. Secondary calibration laboratory for ionizing radiation laboratory accreitation program National Institute of Standards and Technology National Voluntary Laboratory Accreditation Program

    International Nuclear Information System (INIS)

    Martin, P.R.

    1993-01-01

    This paper presents an overview of the procedures and requirements for accreditation under the Secondary Calibration Laboratory for Ionizing Radiation Program (SCLIR LAP). The requirements for a quality system, proficiency testing and the onsite assessment are discussed. The purpose of the accreditation program is to establish a network of secondary calibration laboratories that can provide calibrations traceable to the primary national standards

  18. A primary standard for low-g shock calibration by laser interferometry

    Science.gov (United States)

    Sun, Qiao; Wang, Jian-lin; Hu, Hong-bo

    2014-07-01

    This paper presents a novel implementation of a primary standard for low-g shock acceleration calibration by laser interferometry based on rigid body collision at National Institute of Metrology, China. The mechanical structure of the standard device and working principles involved in the shock acceleration exciter, laser interferometers and virtual instruments are described. The novel combination of an electromagnetic exciter and a pneumatic exciter as the mechanical power supply of the standard device can deliver a wide range of shock acceleration levels. In addition to polyurethane rubber, two other types of material are investigated to ensure a wide selection of cushioning pads for shock pulse generation, with pulse shapes and data displayed. A heterodyne He-Ne laser interferometer is preferred for its precise and reliable measurement of shock acceleration while a homodyne one serves as a check standard. Some calibration results of a standard acceleration measuring chain are shown in company with the uncertainty evaluation budget. The expanded calibration uncertainty of shock sensitivity of the acceleration measuring chain is 0.8%, k = 2, with the peak acceleration range from 20 to 10 000 m s-2 and pulse duration from 0.5 to 10 ms. This primary shock standard can meet the traceability requirements of shock acceleration from various applications of industries from automobile to civil engineering and therefore is used for piloting the ongoing shock comparison of Technical Committee of Acoustics, Ultrasound and Vibration (TCAUV) of Asia Pacific Metrology Program (APMP), coded as APMP.AUV.V-P1.

  19. Experimental comparison between total calibration factors and components calibration factors of reference dosemeters used in secondary standard laboratory dosemeters

    International Nuclear Information System (INIS)

    Silva, T.A. da.

    1981-06-01

    A quantitative comparison of component calibration factors with the corresponding overall calibration factor was used to evaluate the adopted component calibration procedure in regard to parasitic elements. Judgement of significance is based upon the experimental uncertainty of a well established procedure for determination of the overall calibration factor. The experimental results obtained for different ionization chambers and different electrometers demonstrate that for one type of electrometer the parasitic elements have no influence on its sensitivity considering the experimental uncertainty of the calibration procedures. In this case the adopted procedure for determination of component calibration factors is considered to be equivalent to the procedure of determination of the overall calibration factor and thus might be used as a strong quality control measure in routine calibration. (Author) [pt

  20. Standard X ray beams for calibration of dosemeters used in radiation protection practice

    International Nuclear Information System (INIS)

    Pernicka, F.; Michalik, V.

    1992-01-01

    Kerma in air is a widely used reference quantity specified by different calibration laboratories. Calibration of dosemeters used for individual and environmental monitoring requires a knowledge of conversion coefficients between the air kerma and an appropriate protection quantity. These were determined for sets of standard X ray beams using measured spectral distributions, calculated mean energies and effective energies obtained from HVLs measured by an ionisation chamber. There is a good agreement among these three approaches for energies down to 60-70 keV. For lower energies one can expect differences up to 10% if the coefficients are determined from the mean or effective energy instead from the spectral distribution. (author)

  1. Calibration of a Noble Gas Mass Spectrometer with an Atmospheric Argon Standard (Invited)

    Science.gov (United States)

    Prasad, V.; Grove, M.

    2009-12-01

    Like other mass spectrometers, gas source instruments are very good at precisely measuring isotopic ratios but need to be calibrated with a standard to be accurate. The need for calibration arises due to the complicated ionization process which inefficiently and differentially creates ions from the various isotopes that make up the elemental gas. Calibration of the ionization process requires materials with well understood isotopic compositions as standards. Our project goal was to calibrate a noble gas (Noblesse) mass spectrometer with a purified air sample. Our sample obtained from Ocean Beach in San Francisco was under known temperature, pressure, volume, humidity. We corrected the pressure for humidity and used the ideal gas law to calculate the number of moles of argon gas. We then removed all active gasses using specialized equipment designed for this purpose at the United States Geological Survey. At the same time, we measured the volume ratios of various parts of the gas extraction line system associated with the Noblesse mass spectrometer. Using this data, we calculated how much Ar was transferred to the reservoir from the vacuum-sealed vial that contained the purified gas standard. Using similar measurements, we also calculated how much Ar was introduced into the extraction line from a pipette system and how much of this Ar was ultimately expanded into the Noblesse mass spectrometer. Based upon this information, it was possible to calibrate the argon sensitivity of the mass spectrometer. From a knowledge of the isotopic composition of air, it was also possible to characterize how ionized argon isotopes were fractionated during analysis. By repeatedly analyzing our standard we measured a 40Ar Sensitivity of 2.05 amps/bar and a 40Ar/36Ar ratio of 309.2 on the Faraday detector. In contrast, measurements carried out by ion counting using electron multipliers yield a value (296.8) which is much closer to the actual atmospheric 40Ar/36Ar value of 295.5.

  2. X radiation qualities characterization following the standard IEC 61267 recommendations at the calibration laboratory of IPEN

    International Nuclear Information System (INIS)

    Franciscatto, Priscila Cerutti

    2009-01-01

    This work presents a methodology for the X radiation qualities characterization following the new recommendations of the standard 61267 of the International Electrotechnical Commission (IEC) to establish a new procedure for calibration of dosimetric systems used in the field of diagnostic radiology. The reference qualities radiation of IEC 61267: RQR 2 to RQR 10, RQA 2 to RQA 10, RQB 2 to RQB 10 and RQN 2 to RQN 10 were implanted at the calibration laboratory of IPEN (LCI). Their characteristics were analyzed through measurements of beam parameters such as: Practical peak voltage (PPV), specific additional filtrations for each qualities (high purity aluminum of about 99.9%), 1st and 2nd Half Value Layers, homogeneity coefficient. The inherent filtration of the X ray tube was also determined. With the establishment of these radiation qualities, the LCI will be ready to calibrate the measuring instruments of radiation in the new qualities, allowing an improvement in radiological services offered by IPEN. (author)

  3. Transresistance calibrations and temperature dependence evaluation of a magnetic bridge current sensor with shunt standards

    International Nuclear Information System (INIS)

    Yamada, T; Kon, S; Tadatsu, T

    2011-01-01

    This paper deals with a magnetic bridge current sensor for dc current measurements and a calibration system developed for the current sensor. The current sensor forms a magnetic bridge structure with a magnetic fluid core. The calibration system has been developed by using standard shunts for a test current range of 1 mA to 100 A and establishing a comparison method with a switching/sampling system. In the calibration system, the transresistances of the current sensor are measured and the uncertainties of the system are estimated for the input test current range. Also, the temperature dependence on the transresistances is investigated for temperatures ranging from −40 to 100 °C

  4. ACCESS, Absolute Color Calibration Experiment for Standard Stars: Integration, Test, and Ground Performance

    Science.gov (United States)

    Kaiser, Mary Elizabeth; Morris, Matthew; Aldoroty, Lauren; Kurucz, Robert; McCandliss, Stephan; Rauscher, Bernard; Kimble, Randy; Kruk, Jeffrey; Wright, Edward L.; Feldman, Paul; Riess, Adam; Gardner, Jonathon; Bohlin, Ralph; Deustua, Susana; Dixon, Van; Sahnow, David J.; Perlmutter, Saul

    2018-01-01

    Establishing improved spectrophotometric standards is important for a broad range of missions and is relevant to many astrophysical problems. Systematic errors associated with astrophysical data used to probe fundamental astrophysical questions, such as SNeIa observations used to constrain dark energy theories, now exceed the statistical errors associated with merged databases of these measurements. ACCESS, “Absolute Color Calibration Experiment for Standard Stars”, is a series of rocket-borne sub-orbital missions and ground-based experiments designed to enable improvements in the precision of the astrophysical flux scale through the transfer of absolute laboratory detector standards from the National Institute of Standards and Technology (NIST) to a network of stellar standards with a calibration accuracy of 1% and a spectral resolving power of 500 across the 0.35‑1.7μm bandpass. To achieve this goal ACCESS (1) observes HST/ Calspec stars (2) above the atmosphere to eliminate telluric spectral contaminants (e.g. OH) (3) using a single optical path and (HgCdTe) detector (4) that is calibrated to NIST laboratory standards and (5) monitored on the ground and in-flight using a on-board calibration monitor. The observations are (6) cross-checked and extended through the generation of stellar atmosphere models for the targets. The ACCESS telescope and spectrograph have been designed, fabricated, and integrated. Subsystems have been tested. Performance results for subsystems, operations testing, and the integrated spectrograph will be presented. NASA sounding rocket grant NNX17AC83G supports this work.

  5. Calibration of photon and beta ray sources used in brachytherapy. Guidelines on standardized procedures at Secondary Standards Dosimetry Laboratories

    International Nuclear Information System (INIS)

    2004-03-01

    It has generally been recognized that international harmonization in radiotherapy dosimetry is essential. Consequently, the IAEA has given much effort to this, for example by publishing a number of reports in the Technical Reports Series (TRS) for external beam dosimetry, most notably TRS-277 and more recently TRS-398. Both of these reports describe in detail the steps to be taken for absorbed dose determination in water and they are often referred to as 'dosimetry protocols'. Similar to TRS-277, it is expected that TRS-398 will be adopted or used as a model by a large number of countries as their national protocol. In 1996, the IAEA established a calibration service for low dose rate (LDR) 137 Cs brachytherapy sources, which is the most widely used source for treatment of gynecological cancer. To further enhance harmonization in brachytherapy dosimetry, the IAEA published in 1999 IAEA-TECDOC-1079 entitled 'Calibration of Brachytherapy Sources. Guidelines on Standardized Procedures for the Calibration of Brachytherapy Sources at Secondary Standard Dosimetry Laboratories (SSDLs) and Hospitals'. The report was well received and was distributed in a large number of copies to the members of the IAEA/WHO network of SSDLs and to medical physicists working with brachytherapy. The present report is an update of the aforementioned TECDOC. Whereas TECDOC-1079 described methods for calibrating brachytherapy sources with photon energies at or above those of 192 Ir, the current report has a wider scope in that it deals with standardization of calibration of all the most commonly used brachytherapy sources, including both photon and beta emitting sources. The latter sources have been in use for a few decades already, but their calibration methods have been unclear. Methods are also described for calibrating sources used in the rapidly growing field of cardiovascular angioplasty. In this application, irradiation of the vessel wall is done in an attempt to prevent restenosis after

  6. Development of a Primary Standard for Calibration of [18F]FDG Activity Measurement Systems

    International Nuclear Information System (INIS)

    Capogni, M; Felice, P De; Fazio, A; Simonelli, F; Abbas, K

    2006-01-01

    The 18 F national primary standard was developed by the INMRI-ENEA using the 4πβ Liquid Scintillation Spectrometry Method with 3 H-Standard Efficiency Tracing. Measurements were performed at JRCIspra under a scientific collaboration between the Institute for Health and Consumer Production, the Amersham Health and the National Institute for Occupational Safety and Prevention (ISPESL). The goal of the work was to calibrate, with minimum uncertainty, the INMRI-ENEA transfer standard portable well-type ionisation chamber as well as other JRC-Ispra and Amersham Health reference Ionising Chambers used for FDG activity measurement

  7. Development of a Primary Standard for Calibration of [{sup 18}F]FDG Activity Measurement Systems

    Energy Technology Data Exchange (ETDEWEB)

    Capogni, M [ENEA Istituto Nazionale di Metrologia delle Radiazioni Ionizzanti (INMRI), Centro Ricerche Casaccia, I-00060 Rome (Italy); Felice, P De [ENEA Istituto Nazionale di Metrologia delle Radiazioni Ionizzanti (INMRI), Centro Ricerche Casaccia, I-00060 Rome (Italy); Fazio, A [ENEA Istituto Nazionale di Metrologia delle Radiazioni Ionizzanti (INMRI), Centro Ricerche Casaccia, I-00060 Rome (Italy); Simonelli, F [Institute for Health and Consumer Protection, Joint Research Centre (JRC), European Commission, I-21020 Ispra (Vatican City State, Holy See,), Italy; D' Ursi, V [Amersham Health Srl (AH), I-13040 Saluggia (Saint Vincent and the Grenadines), Italy; Pecorale, A [Amersham Health Srl (AH), I-13040 Saluggia (Saint Vincent and the Grenadines), Italy; Giliberti, C [Istituto Superiore per la Prevenzione e la Sicurezza del Lavoro (ISPESL), I-00184 Rome (Italy); Abbas, K [Institute for Health and Consumer Protection, Joint Research Centre (JRC), European Commission, I-21020 Ispra (Vatican City State, Holy See,), Italy

    2006-05-15

    The {sup 18}F national primary standard was developed by the INMRI-ENEA using the 4{pi}{beta} Liquid Scintillation Spectrometry Method with {sup 3}H-Standard Efficiency Tracing. Measurements were performed at JRCIspra under a scientific collaboration between the Institute for Health and Consumer Production, the Amersham Health and the National Institute for Occupational Safety and Prevention (ISPESL). The goal of the work was to calibrate, with minimum uncertainty, the INMRI-ENEA transfer standard portable well-type ionisation chamber as well as other JRC-Ispra and Amersham Health reference Ionising Chambers used for FDG activity measurement.

  8. Standards, calibration and quality assurance of 222Rn measurements in Sweden

    International Nuclear Information System (INIS)

    Falk, R.; Hagberg, N.; Mjoenes, L.; Moere, H.; Nyblom, L.; Swedjemark, G.A.

    1994-01-01

    Inhaled decay products of 222 Rn are the dominant components of the natural radiation exposure to the general population. Limits have been introduced in Sweden, and recommendations were made in 1980 for decreasing indoor 222 Rn concentration. The need for the coordinated calibration of measuring instruments as well as for quality assurance was obvious for both health and economic reasons. 222 Rn measurements in Sweden are based on standards traceable to the National Institute of Standard and Technology (NIST) through the use of standard reference material 226 Ra. Standards for both 222 Rn and short-lived 222 Rn progeny are described together with the reference instrument adopted for these studies. The calibration of field instruments was performed in a ''radon room'', a climate chamber in which it is possible to vary and monitor the concentration of 222 Rn as well as other characteristics of the indoor air such as temperature, humidity, ventilation rate and aerosol concentration. The rules and regulations for field measurements imply a calibration of the instruments yearly, as well as accreditation and training for the companies that carry out the measurements. Examples are given of the official measurement protocols used for the different types of instruments. (orig.)

  9. Standardization in dimensional nanometrology: development of a calibration guideline for Scanning Probe Microscopy

    Science.gov (United States)

    Dziomba, Thorsten; Koenders, Ludger; Wilkening, Günter

    2005-10-01

    The continuing miniaturization in many technologies - among them the optical systems - demands high-resolution measurements with uncertainties in the nanometre-range or even well below. A brief introduction of measurement methods used at the micro- & nanometre scale is therefore given as introduction. While a wide range of these methods are well established for the determination of various physical properties down to the nanometric scale, it is Scanning Probe Microscopy (SPM) that provides a unique direct access to topographic surface features in the size range from atomic diameters to some ten or hundred micrometres. With the increasing use of SPMs as quantitative measurement instruments, the demand for standardized calibration routines also for this type of instruments rises. However, except for a few specially designed set-ups mainly at National Metrology Institutes (e. g. PTB in Germany), measurements made with SPMs usually lack traceability to the metre definition. A number of physical transfer standards have therefore been developed and are already available commercially. While detailed knowledge of the standards' properties is a prerequisite for their practical applicability, the calibration procedure itself deserves careful consideration as well. As there is, up to now, no generally accepted concept how to perform SPM calibrations, guidelines are now being developed on various national and international levels, e. g. VDI/VDE-GMA in Germany and ISO. This papers discusses the draft of an SPM calibration guideline by focusing on several critical practical aspects of SPM calibration. The paper intends to invite the readers to take active part in guideline discussions.

  10. A primary standard for the calibration of sniffer test leak devices

    Science.gov (United States)

    Jousten, Karl; Becker, Ute

    2009-10-01

    Test leaks with a gas flow to atmospheric pressure are often called sniffer test leaks. They are used to calibrate leak detectors for sniffing applications. Sniffer test leaks need calibration against a standard. A primary standard for the calibration of sniffer test leaks with relatively low measurement uncertainties is described. It is assured that the measurement result is traceable to the relevant SI units and that there is a well-known and complete measurement uncertainty budget. The measurement range of the system is from 4 × 10-11 mol s-1 (corresponding to 10-4 Pa l s-1 at 23 °C) to 4 × 10-9 mol s-1 (10-2 Pa l s-1 at 23 °C), which is the most often needed range in industry of around 1 g loss per year of the cooling agent R134a. The temperature where the calibration can be carried out may vary from 18 °C to 30 °C. The flow rate of any test gas not condensing in this temperature range can be measured.

  11. Standard test method for calibration of surface/stress measuring devices

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    1997-01-01

    Return to Contents page 1.1 This test method covers calibration or verification of calibration, or both, of surface-stress measuring devices used to measure stress in annealed and heat-strengthened or tempered glass using polariscopic or refractometry based principles. 1.2 This test method is nondestructive. 1.3 This test method uses transmitted light, and therefore, is applicable to light-transmitting glasses. 1.4 This test method is not applicable to chemically tempered glass. 1.5 Using the procedure described, surface stresses can be measured only on the “tin” side of float glass. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

  12. Selection and evaluation of gamma decay standards for detector calibration using coincidence method

    International Nuclear Information System (INIS)

    Hlavac, S.

    2000-01-01

    Coincidence method for calibration of gamma detectors using suitable calibration standards with two cascading gamma rays is analyzed. From the list of recommended gamma ray standards currently under reevaluation by the CRP, 14 radionuclides were selected as the potential source candidates for the coincidence method. The following sources were selected 24 Na, 46 Sc, 60 Co, 66 Ga, 75 Se, 88 Y, Nb 94 , 111 In, 123m Te, 133 Ba, 134 Cs, 152 Eu, 154 Eu and 207 Bi. Reaction 11 B (p,γ) 12 C* was also selected as a source of high energy gamma rays. Experimental data on angular correlation coefficients for selected sources were collected from the literature and evaluated according to the recommended procedure. Theoretical angular correlation coefficients were calculated and compared to the evaluated data. (author)

  13. The standard calibration instrument automation system for the atomic absorption spectrophotometer. Part 3: Program documentation

    Science.gov (United States)

    Ryan, D. P.; Roth, G. S.

    1982-04-01

    Complete documentation of the 15 programs and 11 data files of the EPA Atomic Absorption Instrument Automation System is presented. The system incorporates the following major features: (1) multipoint calibration using first, second, or third degree regression or linear interpolation, (2) timely quality control assessments for spiked samples, duplicates, laboratory control standards, reagent blanks, and instrument check standards, (3) reagent blank subtraction, and (4) plotting of calibration curves and raw data peaks. The programs of this system are written in Data General Extended BASIC, Revision 4.3, as enhanced for multi-user, real-time data acquisition. They run in a Data General Nova 840 minicomputer under the operating system RDOS, Revision 6.2. There is a functional description, a symbol definitions table, a functional flowchart, a program listing, and a symbol cross reference table for each program. The structure of every data file is also detailed.

  14. Calibration of 1 ohm standard resistor in National Metrology Institute of Malaysia (NMIM)

    Science.gov (United States)

    Ishak, Nirul Irwani; Ibarahim, Zahari

    2018-04-01

    This paper describes the calibration of the National Standard of Resistance using an Automatic Direct Current Comparator Bridge (DCC Bridge). We will also discuss the various sources of uncertainty in the measurements and their estimations based on Type A and Type B evaluations. Furthermore, we discuss the uncertainty budget and report the results at k = 2 for the coverage probability of approximately 95% for a normal distribution.

  15. Air kerma standardization for diagnostic radiology, and requirements proposal for calibration laboratories

    International Nuclear Information System (INIS)

    Ramos, Manoel Mattos Oliveira

    2009-01-01

    The demand for calibration services and quality control in diagnostic radiology has grown in the country since the publication of the governmental regulation 453, issued by the Ministry of Health in 1998. At that time, to produce results facing the new legislation, many laboratories used different standards and radiation qualities, some of which could be inadequate. The international standards neither supplied consistent radiation qualities and standardization for the different types of equipment available. This situation changed with the publication of the new edition of the IEC 61267 standard, published in 2005. A metrology network was created, but it is not yet accredited by the accreditation organism of the country, INMETRO. The objective of this work was to implement the standardization of the air kerma for the un attenuated qualities (RQR) of IEC 61267, and to develop a requirement proposal for instruments calibration laboratories. Results of interlaboratory comparisons demonstrate that the quantity is standardized and internationally traceable. A laboratory requirement proposal was finalized and it shall be submitted to INMETRO to be used as auxiliary normative document in laboratory accreditation. (author)

  16. A primary standard for low-g shock calibration by laser interferometry

    International Nuclear Information System (INIS)

    Sun, Qiao; Wang, Jian-lin; Hu, Hong-bo

    2014-01-01

    This paper presents a novel implementation of a primary standard for low-g shock acceleration calibration by laser interferometry based on rigid body collision at National Institute of Metrology, China. The mechanical structure of the standard device and working principles involved in the shock acceleration exciter, laser interferometers and virtual instruments are described. The novel combination of an electromagnetic exciter and a pneumatic exciter as the mechanical power supply of the standard device can deliver a wide range of shock acceleration levels. In addition to polyurethane rubber, two other types of material are investigated to ensure a wide selection of cushioning pads for shock pulse generation, with pulse shapes and data displayed. A heterodyne He–Ne laser interferometer is preferred for its precise and reliable measurement of shock acceleration while a homodyne one serves as a check standard. Some calibration results of a standard acceleration measuring chain are shown in company with the uncertainty evaluation budget. The expanded calibration uncertainty of shock sensitivity of the acceleration measuring chain is 0.8%, k = 2, with the peak acceleration range from 20 to 10 000 m s −2  and pulse duration from 0.5 to 10 ms. This primary shock standard can meet the traceability requirements of shock acceleration from various applications of industries from automobile to civil engineering and therefore is used for piloting the ongoing shock comparison of Technical Committee of Acoustics, Ultrasound and Vibration (TCAUV) of Asia Pacific Metrology Program (APMP), coded as APMP.AUV.V-P1. (paper)

  17. Secondary standards laboratories for ionizing radiation calibrations: the national laboratory interests

    International Nuclear Information System (INIS)

    Roberson, P.L.; Campbell, G.W.

    1984-11-01

    The national laboratories are probable candidates to serve as secondary standards laboratories for the federal sector. Representatives of the major Department of Energy laboratories were polled concerning attitudes toward a secondary laboratory structure. Generally, the need for secondary laboratories was recognized and the development of such a program was encouraged. The secondary laboratories should be reviewed and inspected by the National Bureau of Standards. They should offer all of the essential, and preferably additional, calibration services in the field of radiological health protection. The selection of secondary laboratories should be based on economic and geographic criteria and/or be voluntary. 1 ref., 2 tabs

  18. Dental Hygiene Faculty Calibration Using Two Accepted Standards for Calculus Detection: A Pilot Study.

    Science.gov (United States)

    Santiago, Lisa J; Freudenthal, Jacqueline J; Peterson, Teri; Bowen, Denise M

    2016-08-01

    Faculty calibration studies for calculus detection use two different standards for examiner evaluation, yet the only therapeutic modality that can be used for nonsurgical periodontal treatment is scaling/root debridement or planing. In this study, a pretest-posttest design was used to assess the feasibility of faculty calibration for calculus detection using two accepted standards: that established by the Central Regional Dental Testing Service, Inc. (CRDTS; readily detectible calculus) and the gold standard for scaling/root debridement (root roughness). Four clinical dental hygiene faculty members out of five possible participants at Halifax Community College agreed to participate. The participants explored calculus on the 16 assigned teeth (64 surfaces) of four patients. Calculus detection scores were calculated before and after training. Kappa averages using CRDTS criteria were 0.561 at pretest and 0.631 at posttest. Kappa scores using the scaling/root debridement or planing standard were 0.152 at pretest and 0.271 at posttest. The scores indicated improvement from moderate (Kappa=0.41-0.60) to substantial agreement (Kappa=0.61-0.80) following training using the CRDTS standard. Although this result differed qualitatively and Kappas were significantly different from 0, the differences for pre- to post-Kappas for patient-rater dyads using CRDTS were not statistically significant (p=0.778). There was no difference (p=0.913) in Kappa scores pre- to post-training using the scaling/root debridement standard. Despite the small number of participants in this study, the results indicated that training to improve interrater reliability to substantial agreement was feasible using the CRDTS standard but not using the gold standard. The difference may have been due to greater difficulty in attaining agreement regarding root roughness. Future studies should include multiple training sessions with patients using the same standard for scaling/root debridement used for

  19. The development of an efficient mass balance approach for the purity assignment of organic calibration standards.

    Science.gov (United States)

    Davies, Stephen R; Alamgir, Mahiuddin; Chan, Benjamin K H; Dang, Thao; Jones, Kai; Krishnaswami, Maya; Luo, Yawen; Mitchell, Peter S R; Moawad, Michael; Swan, Hilton; Tarrant, Greg J

    2015-10-01

    The purity determination of organic calibration standards using the traditional mass balance approach is described. Demonstrated examples highlight the potential for bias in each measurement and the need to implement an approach that provides a cross-check for each result, affording fit for purpose purity values in a timely and cost-effective manner. Chromatographic techniques such as gas chromatography with flame ionisation detection (GC-FID) and high-performance liquid chromatography with UV detection (HPLC-UV), combined with mass and NMR spectroscopy, provide a detailed impurity profile allowing an efficient conversion of chromatographic peak areas into relative mass fractions, generally avoiding the need to calibrate each impurity present. For samples analysed by GC-FID, a conservative measurement uncertainty budget is described, including a component to cover potential variations in the response of each unidentified impurity. An alternative approach is also detailed in which extensive purification eliminates the detector response factor issue, facilitating the certification of a super-pure calibration standard which can be used to quantify the main component in less-pure candidate materials. This latter approach is particularly useful when applying HPLC analysis with UV detection. Key to the success of this approach is the application of both qualitative and quantitative (1)H NMR spectroscopy.

  20. Strain study of gold nanomaterials as HR-TEM calibration standard.

    Science.gov (United States)

    Peng, X Y; Zhou, L Q; Li, X; Tao, X F; Ren, L L; Cao, W H; Xu, G F

    2015-12-01

    This work presents the use of high resolution electron microscopy (HREM) and geometric phase analysis (GPA) to measure the interplanar spacing and strain distribution of three gold nanomaterials, respectively. The results showed that the {111} strain was smaller than the {002} strain for any kind of gold materials at the condition of same measuring method. The 0.65% of {111} strain in gold film measured by HREM (0.26% measured by GPA) was smaller than the {111} strains in two gold particles. The presence of lattice strain was interpreted according to the growth mechanism of metallic thin film. It is deduced that the {111} interplanar spacing of the gold thin film is suitable for high magnification calibration of transmission electron microscopy (TEM) and the gold film is potential to be a new calibration standard of TEM. Copyright © 2015 Elsevier Ltd. All rights reserved.

  1. Development and validation of a portable gas phase standard generation and calibration system for volatile organic compounds

    Science.gov (United States)

    P. Veres; J. B. Gilman; J. M. Roberts; W. C. Kuster; C. Warneke; I. R. Burling; J. de Gouw

    2010-01-01

    We report on the development of an accurate, portable, dynamic calibration system for volatile organic compounds (VOCs). The Mobile Organic Carbon Calibration System (MOCCS) combines the production of gas-phase VOC standards using permeation or diffusion sources with quantitative total organic carbon (TOC) conversion on a palladium surface to CO2 in the presence of...

  2. International collaborative study for the calibration of proposed International Standards for thromboplastin, rabbit, plain and for thromboplastin, recombinant, human, plain

    DEFF Research Database (Denmark)

    van den Besselaar, A M H P; Chantarangkul, V; Angeloni, F

    2018-01-01

    BACKGROUND: The availability of International Standards for thromboplastin is essential for the calibration of routine reagents and hence the calculation of the International Normalized Ratio (INR). Stocks of the current 4(th) International Standards are running low. Candidate replacement materia......) international standard (rTF/09). The candidate materials have been accepted by WHO as the 5(th) International Standards for thromboplastin, rabbit plain, and thromboplastin, recombinant, human, plain. This article is protected by copyright. All rights reserved.......BACKGROUND: The availability of International Standards for thromboplastin is essential for the calibration of routine reagents and hence the calculation of the International Normalized Ratio (INR). Stocks of the current 4(th) International Standards are running low. Candidate replacement materials...... have been prepared. This report describes the calibration of the proposed 5(th) International Standards for thromboplastin, rabbit, plain (coded RBT/16) and for thromboplastin, recombinant, human, plain (coded rTF/16). METHODS: An international collaborative study was carried out for the assignment...

  3. Development of a standard operating procedure for mammography equipment used in calibration of ionized chambers

    International Nuclear Information System (INIS)

    Rodrigues, Yklys Santos; Potiens, Maria da Penha Albuquerque

    2011-01-01

    Mammography is one widely used technique in the detection of breast cancer. In order to optimize the results achieving better images with lower dose rates, a quality assurance programme must be applied to the equipment. Some control tests use ionization chambers to measure air kerma and other quantities. These tests can only be reliable if the ionization chambers used on them are correctly calibrated. In the present work, it was developed a standard operating procedure (SOP) for quality control tests in a commercial mammography equipment installed in the Calibration Laboratory (LCI) at IPEN - Brazilian Institute for energy and nuclear research). Seven tests were performed in the equipment: Tube voltage and exposition time accuracy and reproducibility, linearity and reproducibility of Air kerma and Half Value Layer (HVL). Then, it was made a measurement of the air kerma in the mammography equipment, using a reference ionization chamber with traceability to a primary laboratory in Germany (Physikalisch-Technische Bundesanstalt - PTB), that was later compared with the air kerma measured in an industrial irradiator. This industrial X-ray generator was recently used in the implementation of X-radiation Standards beams, mammography level, following the Standard IEC 61267. The HVL values varied from 0.36 (25kV) to 0.41 mmA1 (35kV), and the measured air kerma rates were between 9.78 and 17.97 mGy/min. (author)

  4. Germanium detector calibration according to the standard NF M 60-810 without using radioactive sources

    Energy Technology Data Exchange (ETDEWEB)

    Duda, J. M.; Garell, I.; Losset, Y.; Vichot, L. [CEA de Valduc, Service de Protection Contre Les Rayonnements, 21110 Is sur Tille (France); Chazalet, J.; Tauvel, Y.; Poulet, F. [IUP Genie des Systemes Industriels, Universite Blaise Pascal, Departement de Physique, 24 avenue des Landais, 63177 Aubiere Cedex (France)

    2009-07-01

    In-situ gamma ray spectrometry is used to determine the specific activities of natural and artificial radioactive nuclides in the soil with a good accuracy. This method is very interesting for environmental measurements and leads to soil determination activity. It is a cheaper method than analysis of great amounts of soil samples in the laboratory. As there is no standard soil, detection efficiency can be estimated using either statistical tools or combination of radioactive point sources calibration thanks to mathematical models of NF-M-60-810 standard representing the radionuclide distribution in soil. Experimental determination of detection efficiency requires a large number of operations involving the handling of radioactive standards in the energy range from 0.06 - 2 MeV. For these reasons, detection efficiency model has been determined without using radioactive sources. In order to reduce analytical time and to simplify the efficiency detector calibration, it is possible to associate numerical and deterministic methods and to get a relative accuracy below 25 per cent

  5. Update of X- and γ-ray decay data standards for detector calibration and other applications

    International Nuclear Information System (INIS)

    Herman, M.; Nichols, A.L.

    2002-12-01

    The Third Research Co-ordination Meeting to Update X- and γ-ray Decay Data Standards for Detector Calibration and Other Applications was held at IAEA Headquarters, Vienna from 21 to 24 October 2002. A primary aim of ths meeting was to review progress in the evaluation and recommendation of the specified decay data. CRP participants reviewed the status of their evaluations, as agreed at the previous meetings, and demonstrated that good progress had been made. Details of the content and presentational format of the recommended database were agreed, with an aim of completion by the end of 2002 and publication of the IAEA-TECDOC report in 2003. (author)

  6. X-ray and gamma-ray standards for detector calibration

    International Nuclear Information System (INIS)

    1991-09-01

    The IAEA established a Co-ordinated Research Programme (CRP) on the Measurements and Evaluation of X- and Gamma-Ray Standards for Detector Efficiency Calibration in 1986 with the aim of alleviating the generation of such discrepancies. Within the framework of this CRP, representatives of nine research groups from six Member States and one international organization performed a number of precise measurements and systematic in-depth evaluations of the required decay data. They have also contributed to the development of evaluation methodology and measurement techniques, and stimulated a number of such studies at laboratories not directly involved in the IAEA project. The results of the work of the CRP, which was finished in 1990, are presented in this report. Recommended values of half-lives and photon emission probabilities are given for a carefully selected set of radionuclides that are suitable for detector efficiency calibration (X-rays from 5 to 90 keV and gamma-rays from 30 to about 3000 keV). Detector efficiency calibration for higher gamma-ray energies (up to 14 MeV) is also considered. The evaluation procedures used to obtain the recommended values and their estimated uncertainties are reported, and a summary of the remaining discrepancies is given. Refs and tabs

  7. Dynamic–gravimetric preparation of metrologically traceable primary calibration standards for halogenated greenhouse gases

    Directory of Open Access Journals (Sweden)

    M. Guillevic

    2018-06-01

    Full Text Available For many years, the comparability of measurements obtained with various instruments within a global-scale air quality monitoring network has been ensured by anchoring all results to a unique suite of reference gas mixtures, also called a primary calibration scale. Such suites of reference gas mixtures are usually prepared and then stored over decades in pressurised cylinders by a designated laboratory. For the halogenated gases which have been measured over the last 40 years, this anchoring method is highly relevant as measurement reproducibility is currently much better ( <  1 %, k  =  2 or 95 % confidence interval than the expanded uncertainty of a reference gas mixture (usually  >  2 %. Meanwhile, newly emitted halogenated gases are already measured in the atmosphere at pmol mol−1 levels, while still lacking an established reference standard. For compounds prone to adsorption on material surfaces, it is difficult to evaluate mixture stability and thus variations in the molar fractions over time in cylinders at pmol mol−1 levels.To support atmospheric monitoring of halogenated gases, we create new primary calibration scales for SF6 (sulfur hexafluoride, HFC-125 (pentafluoroethane, HFO-1234yf (or HFC-1234yf, 2,3,3,3-tetrafluoroprop-1-ene, HCFC-132b (1,2-dichloro-1,1-difluoroethane and CFC-13 (chlorotrifluoromethane. The preparation method, newly applied to halocarbons, is dynamic and gravimetric: it is based on the permeation principle followed by dynamic dilution and cryo-filling of the mixture in cylinders. The obtained METAS-2017 primary calibration scales are made of 11 cylinders containing these five substances at near-ambient and slightly varying molar fractions. Each prepared molar fraction is traceable to the realisation of SI units (International System of Units and is assigned an uncertainty estimate following international guidelines (JCGM, 2008, ranging from 0.6 % for SF6 to 1.3 % (k

  8. Compensation for the Effects of Ambient Conditions on the Calibration of Multi-Capillary Pressure Drop Standards

    Directory of Open Access Journals (Sweden)

    Colard S

    2014-12-01

    Full Text Available Cigarette draw resistance and filter pressure drop (PD are both major physical parameters for the tobacco industry. Therefore these parameters must be measured reliably. For these measurements, specific equipment calibrated with PD transfer standards is used. Each transfer standard must have a known and stable PD value, such standards usually being composed of several capillary tubes associated in parallel. However, PD values are modified by ambient conditions during calibration of such standards, i.e. by temperature and relative humidity (RH of air, and atmospheric pressure. In order to reduce the influence of these ambient factors, a simplified model was developed for compensating the effects of ambient conditions on the calibration of multi-capillary PD standards.

  9. Calibration standards for major greenhouse gases and carbon monoxide: status and challenges.

    Science.gov (United States)

    Zellweger, Christoph; Mohn, Joachim; Wyss, Simon A.; Brewer, Paul; Mace, Tatiana; Nieuwenkamp, Gerard; Pearce-Hill, Ruth; Tarhan, Tanil; Walden, Jari; Emmenegger, Lukas

    2017-04-01

    Human influence on increasing greenhouse gas mole fractions in the atmosphere and effects on positive radiative forcing as well as observed global warming and sea level rise are well accepted [1]. For interpretation of global or continental scale greenhouse gas data, obtained from different laboratories, measurement results have to coincide within compatibility goals set by the World Meteorological Organization (WMO) [2]. Despite significant advances in measurement techniques [3], WMO compatibility goals are regularly missed, shown by round-robin experiments of standard gases and comparisons of field samples or parallel measurements. Therefore, precise and accurate calibration using standards with good long-term stability is needed to reduce uncertainties of atmospheric measurements. This is addressed by the WMO Global Atmosphere Watch Programme (GAW), where Central Calibration Laboratories (CCLs) maintain calibration scales to ensure consistency of measurements within the network to primary reference materials. Furthermore, participating GAW laboratories are supported by World Calibration Centres (WCCs) performing audits and organizing round-robin comparisons. The CCL participates regularly in comparisons with independent primary scales to assure traceability of established primary reference materials to fundamental quantities (SI) [e.g. 4]. Within the European Metrology Research Programme (EMRP) ENV52 project "Metrology for high-impact greenhouse gases" (HIGHGAS), static and dynamic primary reference gas mixtures for ambient levels of CO2, CH4, N2O and CO in air were prepared by different National Metrology Institutes (NMIs). In order to progress beyond the state of the art, research focused on improving passivation chemistry, quantification of target impurities in the air matrix, and determining the isotopic composition. These primary reference gas mixtures were compared in a round robin experiment against standards calibrated against reference gases currently

  10. Airborne hygrometer calibration inter-comparison against a metrological water vapour standard

    Science.gov (United States)

    Smorgon, Denis; Boese, Norbert; Ebert, Volker

    2014-05-01

    Water vapour is the most important atmospheric greenhouse gas, which causes a major feedback to warming and other changes in the climate system. Knowledge of the distribution of water vapour and its climate induced changes is especially important in the upper troposphere and lower stratosphere (UT/LS) where vapour plays a critical role in atmospheric radiative balance, cirrus cloud formation, and photochemistry. But, our understanding of water in the UT/LS is limited by significant uncertainties in current UT/LS water measurements. One of the most comprehensive inter-comparison campaigns for airborne hygrometers, termed AQUAVIT (AV1) [1], took place in 2007 at the AIDA chamber at the Karlsruhe Institute of Technology (KIT) in Germany. AV1 was a well-defined, referred, blind inter-comparison of 22 airborne field instruments from 17 international research groups. One major metrological deficit of AV1, however, was, that no traceable reference instrument participated in the inter-comparison experiments and that the calibration procedures of the participating instruments were not monitored or interrogated. Consequently a follow-up inter-comparison was organized in April 2013, which for the first time also provides a traceable link to the international humidity scale. This AQUAVIT2 (AV2) campaign (details see: http://www.imk-aaf.kit.edu/aquavit/index.php/Main_Page) was again located at KIT/AIDA and organised by an international organizing committee including KIT, PTB, FZJ and others. Generally AV2 is divided in two parallel comparisons: 1) AV2-A uses the AIDA chamber for a simultaneous comparison of all instruments (incl. sampling and in-situ instruments) over a broad range of conditions characteristic for the UT/LS; 2) AV2-B, about which this paper is reporting, is a sequential comparison of selected hygrometers and (when possible) their reference calibration infrastructures by means of a chilled mirror hygrometer traced back to the primary National humidity standard

  11. A simple preparation of calibration curve standards of 134Cs and 137Cs by serial dilution of a standard reference material

    International Nuclear Information System (INIS)

    Labrecque, J.J.; Rosales, P.A.

    1990-01-01

    Two sets of calibration standards for 134 Cs and 137 Cs were prepared by small serial dilution of a natural matrix standard reference material, IAEA-154 whey powder. The first set was intended to screen imported milk powders which were suspected to be contaminated with 134 Cs and 137 Cs. Their concentration ranged from 40 to 400 Bq/kg. The other set of calibration standards was prepared to measure the environmental levels of 137 Cs in commercial Venezuelan milk powders. Their concentration ranged from 3 to 10 Bq/kg of 137 Cs. The accuracy of these calibration curves was checked by IAEA-152 and A-14 milk powders. Their measured values were in good agreement with their certified values. Finally, it is shown that these preparation techniques using serial dilution of a standard reference material were simple, rapid, precise, accurate and cost-effective. (author) 5 refs.; 5 figs.; 3 tabs

  12. Development, improvement and calibration of neutronic reaction rates measurements: elaboration of a standard techniques basis

    International Nuclear Information System (INIS)

    Hudelot, J.P.

    1998-06-01

    In order to improve and to validate the neutronics calculation schemes, perfecting integral measurements of neutronics parameters is necessary. This thesis focuses on the conception, the improvement and the development of neutronics reaction rates measurements, and aims at building a base of standard techniques. Two subjects are discussed. The first one deals with direct measurements by fission chambers. A short presentation of the different usual techniques is given. Then, those last ones are applied through the example of doubling time measurements on the EOLE facility during the MISTRAL 1 experimental programme. Two calibration devices of fission chambers are developed: a thermal column located in the central part of the MINERVE facility, and a calibration cell using a pulsed high flux neutron generator and based on the discrimination of the energy of the neutrons with a time-of-flight method. This second device will soon allow to measure the mass of fission chambers with a precision of about 1 %. Finally, the necessity of those calibrations will be shown through spectral indices measurements in core MISTRAL 1 (UO 2 ) and MISTRAL 2 (MOX) of the EOLE facility. In each case, the associated calculation schemes, performed using the Monte Carlo MCNP code with the ENDF-BV library, will be validated. Concerning the second one, the goal is to develop a method for measuring the modified conversion ratio of 238 U (defined as the ratio of 238 U capture rate to total fission rate) by gamma-ray spectrometry of fuel rods. Within the framework of the MISTRAL 1 and MISTRAL 2 programmes, the measurement device, the experimental results and the spectrometer calibration are described. Furthermore, the MCNP calculations of neutron self-shielding and gamma self-absorption are validated. It is finally shown that measurement uncertainties are better than 1 %. The extension of this technique to future modified conversion ratio measurements for 242 Pu (on MOX rods) and 232 Th (on

  13. Development, improvement and calibration of neutronic reaction rate measurements: elaboration of a base of standard techniques

    International Nuclear Information System (INIS)

    Hudelot, J.P.

    1998-01-01

    In order to improve and to validate the neutronic calculation schemes, perfecting integral measurements of neutronic parameters is necessary. This thesis focuses on the conception, the improvement and the development of neutronic reaction rates measurements, and aims at building a base of standard techniques. Two subjects are discussed. The first one deals with direct measurements by fission chambers. A short presentation of the different usual techniques is given. Then, those last ones are applied through the example of doubling time measurements on the EOLE facility during the MISTRAL 1 experimental programme. Two calibration devices of fission chambers are developed: a thermal column located in the central part of the MINERVE facility, and a calibration cell using a pulsed high flux neutron generator and based on the discrimination of the energy of the neutrons with a time-of-flight method. This second device will soon allow to measure the mass of fission chambers with a precision of about 1 %. Finally, the necessity of those calibrations will be shown through spectral indices measurements in core MISTRAL 1 (UO 2 ) and MISTRAL 2 (MOX) of the EOLE facility. In each case, the associated calculation schemes, performed using the Monte Carlo MCNP code with the ENDF-BV library, will be validated. Concerning the second one, the goal is to develop a method for measuring the modified conversion ratio of 238 U (defined as the ratio of 238 U capture rate to total fission rate) by gamma-ray spectrometry of fuel rods. Within the framework of the MISTRAL 1 and MISTRAL 2 programmes, the measurement device, the experimental results and the spectrometer calibration are described. Furthermore, the MCNP calculations of neutron self-shielding and gamma self-absorption are validated. It is finally shown that measurement uncertainties are better than 1 %. The extension of this technique to future modified conversion ratio measurements for 242 Pu (on MOX rods) and 232 Th (on Thorium

  14. SATELLITE-MOUNTED LIGHT SOURCES AS PHOTOMETRIC CALIBRATION STANDARDS FOR GROUND-BASED TELESCOPES

    Energy Technology Data Exchange (ETDEWEB)

    Albert, J., E-mail: jalbert@uvic.ca [Department of Physics and Astronomy, University of Victoria, Victoria, BC V8P 5C2 (Canada)

    2012-01-15

    A significant and growing portion of systematic error on a number of fundamental parameters in astrophysics and cosmology is due to uncertainties from absolute photometric and flux standards. A path toward achieving major reduction in such uncertainties may be provided by satellite-mounted light sources, resulting in improvement in the ability to precisely characterize atmospheric extinction, and thus helping to usher in the coming generation of precision results in astronomy. Using a campaign of observations of the 532 nm pulsed laser aboard the CALIPSO satellite, collected using a portable network of cameras and photodiodes, we obtain initial measurements of atmospheric extinction, which can apparently be greatly improved by further data of this type. For a future satellite-mounted precision light source, a high-altitude balloon platform under development (together with colleagues) can provide testing as well as observational data for calibration of atmospheric uncertainties.

  15. SATELLITE-MOUNTED LIGHT SOURCES AS PHOTOMETRIC CALIBRATION STANDARDS FOR GROUND-BASED TELESCOPES

    International Nuclear Information System (INIS)

    Albert, J.

    2012-01-01

    A significant and growing portion of systematic error on a number of fundamental parameters in astrophysics and cosmology is due to uncertainties from absolute photometric and flux standards. A path toward achieving major reduction in such uncertainties may be provided by satellite-mounted light sources, resulting in improvement in the ability to precisely characterize atmospheric extinction, and thus helping to usher in the coming generation of precision results in astronomy. Using a campaign of observations of the 532 nm pulsed laser aboard the CALIPSO satellite, collected using a portable network of cameras and photodiodes, we obtain initial measurements of atmospheric extinction, which can apparently be greatly improved by further data of this type. For a future satellite-mounted precision light source, a high-altitude balloon platform under development (together with colleagues) can provide testing as well as observational data for calibration of atmospheric uncertainties.

  16. Calibration and standards beamline 6.3.2 at the ALS

    International Nuclear Information System (INIS)

    Underwood, J.H.; Gullikson, E.M.; Koike, M.

    1997-01-01

    More sophisticated optics for the x-ray, soft x-ray and far ultraviolet spectral regions being developed for synchrotron radiation research and many other applications, require accurate calibration and standards facilities for measuring reflectivity of mirrors and multilayer coatings, transmission of thin films, bandpass of multilayers, efficiency of gratings or detectors, etc. For this purpose beamline 6.3.2 was built at the ALS. Its energy coverage, versatility, simplicity and convenience also make it useful for a wide range of other experiments. The paper describes the components of this beamline, consisting of: a four jaw aperture; a horizontal focusing mirror; a monochromator; exit slit; vertical focusing mirror; mechanical and vacuum system; reflectometer; filter wheels; and data acquisition system

  17. Calibration and standards beamline 6.3.2 at the ALS

    Energy Technology Data Exchange (ETDEWEB)

    Underwood, J.H.; Gullikson, E.M.; Koike, M. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)] [and others

    1997-04-01

    More sophisticated optics for the x-ray, soft x-ray and far ultraviolet spectral regions being developed for synchrotron radiation research and many other applications, require accurate calibration and standards facilities for measuring reflectivity of mirrors and multilayer coatings, transmission of thin films, bandpass of multilayers, efficiency of gratings or detectors, etc. For this purpose beamline 6.3.2 was built at the ALS. Its energy coverage, versatility, simplicity and convenience also make it useful for a wide range of other experiments. The paper describes the components of this beamline, consisting of: a four jaw aperture; a horizontal focusing mirror; a monochromator; exit slit; vertical focusing mirror; mechanical and vacuum system; reflectometer; filter wheels; and data acquisition system.

  18. Evaluation of the energy dependence of ionization chambers pencil type calibrated beam tomography standards

    International Nuclear Information System (INIS)

    Fontes, Ladyjane Pereira; Potiens, Maria da Penha A.

    2015-01-01

    The Instrument Calibration Laboratory of IPEN (LCI - IPEN) performs calibrations of pencil-type ionization chambers (IC) used in measures of dosimetric survey on clinical systems of Computed Tomography (CT). Many users make mistakes when using a calibrated ionization chamber in their CT dosimetry systems. In this work a methodology for determination of factors of correction for quality (Kq) through the calibration curve that is specific for each ionization chamber was established. Furthermore, it was possible to demonstrate the energy dependence on an pencil-type Ionization Chamber(IC) calibrated at the LCI - IPEN. (author)

  19. Efficiency calibration of electron spectrometers by the help of standard spectrum

    International Nuclear Information System (INIS)

    Toth, J.; Cserny, I.; Varga, D.; Koever, I.; Toekesi, K.

    2004-01-01

    Complete text of publication follows. For studying thin films and surface nanostructures quantitative analytical applications of electron spectroscopic techniques have a great importance. The most frequently used techniques are XPS, XAES and AES in quantitative surface electron spectroscopy. Applying these techniques changes in the detection efficiency vs. electron kinetic energy change the measured electron peak intensity ratios and in this way the neglect of the energy dependence of the spectrometer efficiency can influence surface atomic concentrations derived. The importance of the precise determination of the atomic concentrations is very crucial, especially in the determination of non-destructive depth profiles by the help of AR-XPS in which small changes in the relative concentrations can change dramatically the concentration depth profiles of a few nanometer depth ranges. In the present study the REELS technique was used to determine the relative detection efficiency by the help of a standard spectrum measured on the surface of fine microcrystalline Cu specimen. The experimental relative efficiency curves vs. electron kinetic energy were compared to the calculated efficiency curve. The efficiency calibration is discussed from the point of view of quantitative XPS, AR- XPS, AES and from the point of view of IMFP determination by XPS. The work was supported by the Hungarian National Science Foundation, OTKAT038016. For the Cu specimen and the standard spectrum the authors are indebted to the Sur- face Analysis Society of Japan, to Dr. Shigeo Tanuma and Professor Keisuke Goto (NIT). (author)

  20. Photovoltaic Device Performance Evaluation Using an Open-Hardware System and Standard Calibrated Laboratory Instruments

    Directory of Open Access Journals (Sweden)

    Jesús Montes-Romero

    2017-11-01

    Full Text Available This article describes a complete characterization system for photovoltaic devices designed to acquire the current-voltage curve and to process the obtained data. The proposed system can be replicated for educational or research purposes without having wide knowledge about electronic engineering. Using standard calibrated instrumentation, commonly available in any laboratory, the accuracy of measurements is ensured. A capacitive load is used to bias the device due to its versatility and simplicity. The system includes a common part and an interchangeable part that must be designed depending on the electrical characteristics of each PV device. Control software, developed in LabVIEW, controls the equipment, performs automatic campaigns of measurements, and performs additional calculations in real time. These include different procedures to extrapolate the measurements to standard test conditions and methods to obtain the intrinsic parameters of the single diode model. A deep analysis of the uncertainty of measurement is also provided. Finally, the proposed system is validated by comparing the results obtained from some commercial photovoltaic modules to the measurements given by an independently accredited laboratory.

  1. A standardized method for the calibration of thermodynamic data for the prediction of gas chromatographic retention times.

    Science.gov (United States)

    McGinitie, Teague M; Ebrahimi-Najafabadi, Heshmatollah; Harynuk, James J

    2014-02-21

    A new method for calibrating thermodynamic data to be used in the prediction of analyte retention times is presented. The method allows thermodynamic data collected on one column to be used in making predictions across columns of the same stationary phase but with varying geometries. This calibration is essential as slight variances in the column inner diameter and stationary phase film thickness between columns or as a column ages will adversely affect the accuracy of predictions. The calibration technique uses a Grob standard mixture along with a Nelder-Mead simplex algorithm and a previously developed model of GC retention times based on a three-parameter thermodynamic model to estimate both inner diameter and stationary phase film thickness. The calibration method is highly successful with the predicted retention times for a set of alkanes, ketones and alcohols having an average error of 1.6s across three columns. Copyright © 2014 Elsevier B.V. All rights reserved.

  2. Anatomical Calibration through Post-Processing of Standard Motion Tests Data.

    Science.gov (United States)

    Kong, Weisheng; Sessa, Salvatore; Zecca, Massimiliano; Takanishi, Atsuo

    2016-11-28

    The inertial measurement unit is popularly used as a wearable and flexible tool for human motion tracking. Sensor-to-body alignment, or anatomical calibration (AC), is fundamental to improve accuracy and reliability. Current AC methods either require extra movements or are limited to specific joints. In this research, the authors propose a novel method to achieve AC from standard motion tests (such as walking, or sit-to-stand), and compare the results with the AC obtained from specially designed movements. The proposed method uses the limited acceleration range on medial-lateral direction, and applies principal component analysis to estimate the sagittal plane, while the vertical direction is estimated from acceleration during quiet stance. The results show a good correlation between the two sets of IMUs placed on frontal/back and lateral sides of head, trunk and lower limbs. Moreover, repeatability and convergence were verified. The AC obtained from sit-to-stand and walking achieved similar results as the movements specifically designed for upper and lower body AC, respectively, except for the feet. Therefore, the experiments without AC performed can be recovered through post-processing on the walking and sit-to-stand data. Moreover, extra movements for AC can be avoided during the experiment and instead achieved through the proposed method.

  3. Anatomical Calibration through Post-Processing of Standard Motion Tests Data

    Directory of Open Access Journals (Sweden)

    Weisheng Kong

    2016-11-01

    Full Text Available The inertial measurement unit is popularly used as a wearable and flexible tool for human motion tracking. Sensor-to-body alignment, or anatomical calibration (AC, is fundamental to improve accuracy and reliability. Current AC methods either require extra movements or are limited to specific joints. In this research, the authors propose a novel method to achieve AC from standard motion tests (such as walking, or sit-to-stand, and compare the results with the AC obtained from specially designed movements. The proposed method uses the limited acceleration range on medial-lateral direction, and applies principal component analysis to estimate the sagittal plane, while the vertical direction is estimated from acceleration during quiet stance. The results show a good correlation between the two sets of IMUs placed on frontal/back and lateral sides of head, trunk and lower limbs. Moreover, repeatability and convergence were verified. The AC obtained from sit-to-stand and walking achieved similar results as the movements specifically designed for upper and lower body AC, respectively, except for the feet. Therefore, the experiments without AC performed can be recovered through post-processing on the walking and sit-to-stand data. Moreover, extra movements for AC can be avoided during the experiment and instead achieved through the proposed method.

  4. Standard practice of calibration of force-measuring instruments for verifying the force indication of testing machines

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2006-01-01

    1.1 The purpose of this practice is to specify procedures for the calibration of force-measuring instruments. Procedures are included for the following types of instruments: 1.1.1 Elastic force-measuring instruments, and 1.1.2 Force-multiplying systems, such as balances and small platform scales. Note 1Verification by deadweight loading is also an acceptable method of verifying the force indication of a testing machine. Tolerances for weights for this purpose are given in Practices E 4; methods for calibration of the weights are given in NIST Technical Note 577, Methods of Calibrating Weights for Piston Gages. 1.2 The values stated in SI units are to be regarded as the standard. Other metric and inch-pound values are regarded as equivalent when required. 1.3 This practice is intended for the calibration of static force measuring instruments. It is not applicable for dynamic or high speed force calibrations, nor can the results of calibrations performed in accordance with this practice be assumed valid for...

  5. Development of transfer standard devices for ensuring the accurate calibration of ultrasonic physical therapy machines in clinical use

    International Nuclear Information System (INIS)

    Hekkenberg, R T; Richards, A; Beissner, K; Zeqiri, B; Prout, G; Cantrall, Ch; Bezemer, R A; Koch, Ch; Hodnett, M

    2004-01-01

    Physical therapy ultrasound is widely applied to patients. However, many devices do not comply with the relevant standard stating that the actual power output shall be within ±20% of the device indication. Extreme cases have been reported: from delivering effectively no ultrasound or operating at maximum power at all powers indicated. This can potentially lead to patient injury as well as mistreatment. The present European (EC) project is an ongoing attempt to improve the quality of the treatment of patients being treated with ultrasonic physical-therapy. A Portable ultrasound Power Standard (PPS) is being developed and accurately calibrated. The PPS includes: Ultrasound transducers (including one exhibiting an unusual output) and a driver for the ultrasound transducers that has calibration and proficiency test functions. Also included with the PPS is a Cavitation Detector to determine the onset of cavitation occurring within the propagation medium. The PPS will be suitable for conducting in-the-field accreditation (proficiency testing and calibration). In order to be accredited it will be important to be able to show traceability of the calibration, the calibration process and qualification of testing staff. The clinical user will benefit from traceability because treatments will be performed more reliably

  6. Temperature calibration procedure for thin film substrates for thermo-ellipsometric analysis using melting point standards

    NARCIS (Netherlands)

    Kappert, Emiel; Raaijmakers, Michiel; Ogieglo, Wojciech; Nijmeijer, Arian; Huiskes, Cindy; Huiskes, C.; Benes, Nieck Edwin

    2015-01-01

    Precise and accurate temperature control is pertinent to studying thermally activated processes in thin films. Here, we present a calibration method for the substrate–film interface temperature using spectroscopic ellipsometry. The method is adapted from temperature calibration methods that are well

  7. Calibration uncertainty

    DEFF Research Database (Denmark)

    Heydorn, Kaj; Anglov, Thomas

    2002-01-01

    Methods recommended by the International Standardization Organisation and Eurachem are not satisfactory for the correct estimation of calibration uncertainty. A novel approach is introduced and tested on actual calibration data for the determination of Pb by ICP-AES. The improved calibration...

  8. Standard Test Method for Calibration of Non-Concentrator Photovoltaic Secondary Reference Cells

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2010-01-01

    1.1 This test method covers calibration and characterization of secondary terrestrial photovoltaic reference cells to a desired reference spectral irradiance distribution. The recommended physical requirements for these reference cells are described in Specification E1040. Reference cells are principally used in the determination of the electrical performance of a photovoltaic device. 1.2 Secondary reference cells are calibrated indoors using simulated sunlight or outdoors in natural sunlight by reference to a primary reference cell previously calibrated to the same desired reference spectral irradiance distribution. 1.3 Secondary reference cells calibrated according to this test method will have the same radiometric traceability as the of the primary reference cell used for the calibration. Therefore, if the primary reference cell is traceable to the World Radiometric Reference (WRR, see Test Method E816), the resulting secondary reference cell will also be traceable to the WRR. 1.4 This test method appli...

  9. EPMT: a portable transfer standard for telemetry system pressure-transducer calibration

    International Nuclear Information System (INIS)

    Hasbrouck, R.T.

    1977-01-01

    The LLL developed electronic pressure meter (EPMT) is a portable static-pressure calibration instrument for use with the LLL telemetry transducer system at the Nevada Test Site (NTS). It is significantly more accurate and rugged than the bourdon-tube pressure gauge it replaces, and can be incorporated into a field-use, semi-automatic, pressure calibration system. The process by which a transducer is selected for EPMT use from the inventory of field-service-certified transducers and subjected to an extensive preconditioning and calibration procedure is described. By combining this unusual calibration procedure with a unique, statistically based data-reduction routine, the total uncertainty of the measuring process at each calibration point can be determined with high accuracy

  10. Calibrating NIST SRM 683 as A New International Reference Standard for Zn Isotopes

    Science.gov (United States)

    Yang, Y.; Zhang, X.; Yu, H.; Huang, F.

    2017-12-01

    Zinc isotopes have been widely applied in the cosmochemical, geochemical, and environmental studies (Moynier et al. 2017). Obtaining precise Zn isotopic data for inter-laboratory comparison is a prerequisite to these applications. Currently, the JMC3-0749L is the primary reference standard for Zn isotopes (Albarède 2004), but it is not commercially available now. Thus, it is necessary to calibrate a new international primary reference standard for Zn isotopic analysis. Chen et al. (2016) showed that NIST SRM 683 (a pure Zn metal nugget of 140 grams) has a δ66ZnJMC of 0.12‰, which is falling within the range of natural Zn isotopic compositions, and it may a good candidate for the next generation of international reference standard (Chen et al. 2016). In order to further examine whether NIST SRM 683 has a homogeneous Zn isotopic composition, we measured more NIST SRM 683 by double-spike methods using MC-ICPMS (Conway et al. 2013). The metal nuggets of NIST SRM 683 were intensively sampled by micro-drilling. Zinc isotope analyses for two nuggets show that they have δ66Zn of 0.14 ± 0.02‰ (2SD, N = 32) and 0.13 ± 0.02‰ (2SD, N = 33), respectively. These values are similar to those of two Zn metal nuggets (0.11 ± 0.02‰ vs. 0.12 ± 0.02‰) reported previously by Chen et al. (2016). We fully dissolved one nugget, producing pure Zn solution with identical Zn isotopic composition with the drilling samples. All results strongly support that NIST SRM 683 is homogeneous in Zn isotopic compositions which could be an ideal candidate for the next reference for Zn isotopes. Tests on more metal nuggets will be performed in a few months for further confirming the Zn isotope compositions and homogeneity. Reference: Albarède et al., 2004. 'The stable isotope geochemistry of copper and zinc', Reviews in Mineralogy and Geochemistry, 55: 409-27. Chen et al., 2016. 'Zinc Isotopic Compositions of NIST SRM 683 and Whole-Rock Reference Materials', Geostandards and

  11. Nonlinear method for including the mass uncertainty of standards and the system measurement errors in the fitting of calibration curves

    International Nuclear Information System (INIS)

    Pickles, W.L.; McClure, J.W.; Howell, R.H.

    1978-01-01

    A sophisticated nonlinear multiparameter fitting program was used to produce a best fit calibration curve for the response of an x-ray fluorescence analyzer to uranium nitrate, freeze dried, 0.2% accurate, gravimetric standards. The program is based on unconstrained minimization subroutine, VA02A. The program considers the mass values of the gravimetric standards as parameters to be fit along with the normal calibration curve parameters. The fitting procedure weights with the system errors and the mass errors in a consistent way. The resulting best fit calibration curve parameters reflect the fact that the masses of the standard samples are measured quantities with a known error. Error estimates for the calibration curve parameters can be obtained from the curvature of the ''Chi-Squared Matrix'' or from error relaxation techniques. It was shown that nondispersive XRFA of 0.1 to 1 mg freeze-dried UNO 3 can have an accuracy of 0.2% in 1000 s. 5 figures

  12. Standardization of calibration of clinic dosemeters using electric currents and charges

    International Nuclear Information System (INIS)

    Peres, Marcos Antonio de Lima

    1999-09-01

    Clinical dosimeters used in radiotherapy are calibrated in Latin American countries, including Brazil, as a complete 'system, i.e., ionization chamber and electrometer together. Some countries, as European ones, and USA calibrate them by component, i.e., ionisation chamber apart from electrometer. This method is more advantageous than the previous one, since it makes possible the automation of the calibration process, allowing the acquisition of data related to the chamber and the electrometer measurements independently, as well as the substitution of one of the components, in case of failure. This work proposes a method for standardisation of low intensity electric charge and currents in order to implement electric calibration of electrometers. This will make possible the implementation of a by components calibration technique, by components, of clinical dosimeters in Brazil. The results obtained with the calibration by components prove that the proposed method of standardisation of low electric charges and currents is viable. The difficulties found for the generation and measurement of low intensity electric charges and currents and the procedures adopted for the calibration by components are presented. Additionally, a current source was built to yield reference electric charges that will make possible the quality control clinical dosimeters. This source will also allow the user to identify the defective components of the dosimeters, through a simple verification test. (author)

  13. Calibration of a tertiary standard in N-ISO qualities for radioprotection and personal dosimetry

    International Nuclear Information System (INIS)

    Rojas, Enrique; Seminario, Lizet

    2013-01-01

    Dosimetric calibration of radiation monitors and personal dosimeters in different radiological quantities are performed in order to obtain accurate measurements, for this reason the SSDL calculates the dosimetry calibration factor and its associated uncertainty, for each range of use. The calibration factor is performed using the known radiation field method and its uncertainty is calculated according to the ISO recommendations. The SSDL calculates the expanded uncertainty (U c ) with a coverage factor that provides a level of not less than 95 % of confidence. (authors).

  14. Direct calibration of GC/MS systems using SRM (Standard Reference Material) gas cylinders. Project report, January 1984-August 1985

    International Nuclear Information System (INIS)

    Byrd, G.D.; Richie, K.L.; Sniegoski, L.T.; White, E.

    1985-10-01

    A cryogenic trapping system has been developed for use in calibrating GC/MS systems for the analysis of volatile organic compounds. This system provides for direct Standard Reference Material (SRM) traceability on data generated on gaseous samples. The cryogenic trap is a coil of stainless steel tubing immersed in a cryogen to trap and preconcentrate organic species present in a gaseous sample. The trap also contains a heated injection port for the addition of isotopically labeled compounds for use in isotope dilution measurements. The first part of this research is concerned with the development of IDMS as an independent method for the quantification of analytes in gaseous samples to be used as standards. Results are presented for the determination of bromobenzene in nitrogen at nominal concentrations of 1 and 25 ppb. In the second part of the research, a calibration curve method was developed for using these standards in auditing the performance of GC/MS systems

  15. Spectral Irradiance Calibration in the Infrared 11: Comparison of (alpha) Boo and 1 Ceres with a Laboratory Standard

    Science.gov (United States)

    Witteborn, Fred C.; Cohen, Martin; Bregman, Jess D.; Wooden, Diane; Heere, Karen; Shirley, Eric L.

    1998-01-01

    Infrared spectra of two celestial objects frequently used as flux standards are calibrated against an absolute laboratory flux standard at a spectral resolving power of 100 to 200. The spectrum of the K1.5III star, alpha Boo, is measured from 3 microns to 30 microns and that of the C-type asteroid, 1 Ceres, from 5 microns to 30 microns. While these 'standard' spectra do not have the apparent precision of those based on calculated models, they do not require the assumptions involved in theoretical models of stars and asteroids. Specifically they provide a model-independent means of calibrating celestial flux in the spectral range from 12 microns to 30 microns where accurate absolute photometry is not available. The agreement found between the spectral shapes of alpha Boo and Ceres based on laboratory standards, and those based on observed ratios to alpha CMa (Sirius) and alpha Lyr (Vega), flux calibrated by theoretical modeling of these hot stars strengthens our confidence in the applicability of the stellar models as primary irradiance standards.

  16. Exploring the Feasibility cold-FET Calibration Standards to Improve Radiometric Measurements

    Data.gov (United States)

    National Aeronautics and Space Administration — This work seeks to further the development of the cold-FET calibration technology designed f next generation multi-band microwave instruments for space-based remote...

  17. EASYTRAC Project: Work package 6.4 Reversal technique to calibrate gear and thread standards

    DEFF Research Database (Denmark)

    Carmignato, Simone; De Chiffre, Leonardo; Larsen, Erik

    This report was produced as a part of the project EASYTRAC, an EU project under the programme Competitive and Sustainable Growth: Contract No. G6RD-CT-2000-00188, coordinated by UNIMETRIK S.A. (Spain). The project is concerned with low uncertainty calibrations on coordinate measuring machines (CM...... (PTB) - Germany and Tampere University of Technology (TUT) - Finland. The present report describes feasibility and experimental results of a reversal and substitute element technique application for thread calibration on CMMs....

  18. Quality control of secondary standards and calibration systems, therapy level, of National Laboratory of Metrology from Ionizing Radiations (LNMRI)

    International Nuclear Information System (INIS)

    Cecatti, E.R.; Freitas, L.C. de

    1992-01-01

    The results of quality control program of secondary standards, therapy level, and the calibration system of clinical dosemeters were analysed from 1984, when a change in the laboratory installation occurred and new standards were obtained. The national and the international intercomparisons were emphasised. The results for graphite wall chambers were compared, observing a maximum variation of about 0,6%. In the case of Delrin (TK01) wall chambers, the maximum variation was 1,7%. The results of post intercomparisons with thermoluminescent dosemeters have presented derivations lesser than 1%, securing the standards consistence at LNMRI with the international metrological system. (C.G.C.)

  19. Temperature calibration procedure for thin film substrates for thermo-ellipsometric analysis using melting point standards

    International Nuclear Information System (INIS)

    Kappert, Emiel J.; Raaijmakers, Michiel J.T.; Ogieglo, Wojciech; Nijmeijer, Arian; Huiskes, Cindy; Benes, Nieck E.

    2015-01-01

    Highlights: • Facile temperature calibration method for thermo-ellipsometric analysis. • The melting point of thin films of indium, lead, zinc, and water can be detected by ellipsometry. • In-situ calibration of ellipsometry hot stage, without using any external equipment. • High-accuracy temperature calibration (±1.3 °C). - Abstract: Precise and accurate temperature control is pertinent to studying thermally activated processes in thin films. Here, we present a calibration method for the substrate–film interface temperature using spectroscopic ellipsometry. The method is adapted from temperature calibration methods that are well developed for thermogravimetric analysis and differential scanning calorimetry instruments, and is based on probing a transition temperature. Indium, lead, and zinc could be spread on a substrate, and the phase transition of these metals could be detected by a change in the Ψ signal of the ellipsometer. For water, the phase transition could be detected by a loss of signal intensity as a result of light scattering by the ice crystals. The combined approach allowed for construction of a linear calibration curve with an accuracy of 1.3 °C or lower over the full temperature range

  20. Use of calibration standards and the correction for sample self-attenuation in gamma-ray nondestructive assay

    International Nuclear Information System (INIS)

    Parker, J.L.

    1984-08-01

    The efficient use of appropriate calibration standards and the correction for the attenuation of the gamma rays within an assay sample by the sample itself are two important and closely related subjects in gamma-ray nondestructive assay. Much research relating to those subjects has been done in the Nuclear Safeguards Research and Development program at the Los Alamos National Laboratory since 1970. This report brings together most of the significant results of that research. Also discussed are the nature of appropriate calibration standards and the necessary conditions on the composition, size, and shape of the samples to allow accurate assays. Procedures for determining the correction for the sample self-attenuation are described at length including both general principles and several specific useful cases. The most useful concept is that knowing the linear attenuation coefficient of the sample (which can usually be determined) and the size and shape of the sample and its position relative to the detector permits the computation of the correction factor for the self-attenuation. A major objective of the report is to explain how the procedures for determining the self-attenuation correction factor can be applied so that calibration standards can be entirely appropriate without being particularly similar, either physically or chemically, to the items to be assayed. This permits minimization of the number of standards required to assay items with a wide range of size, shape, and chemical composition. 17 references, 18 figures, 2 tables

  1. The use of calibration standards and the correction for sample self-attenuation in gamma-ray nondestructive assay

    International Nuclear Information System (INIS)

    Parker, J.L.

    1986-11-01

    The efficient use of appropriate calibration standards and the correction for the attenuation of the gamma rays within an assay sample by the sample itself are two important and closely related subjects in gamma-ray nondestructive assay. Much research relating to those subjects has been done in the Nuclear Safeguards Research and Development program at the Los Alamos National Laboratory since 1970. This report brings together most of the significant results of that research. Also discussed are the nature of appropriate calibration standards and the necessary conditions on the composition, size, and shape of the samples to allow accurate assays. Procedures for determining the correction for the sample self-attenuation are described at length including both general principles and several specific useful cases. The most useful concept is that knowing the linear attenuation coefficient of the sample (which can usually be determined) and the size and shape of the sample and its position relative to the detector permits the computation of the correction factor for the self-attenuation. A major objective of the report is to explain how the procedures for determining the self-attenuation correction factor can be applied so that calibration standards can be entirely appropriate without being particularly similar, either physically or chemically, to the items to be assayed. This permits minimization of the number of standards required to assay items with a wide range of size, shape, and chemical composition

  2. New blackbody standard for the evaluation and calibration of tympanic ear thermometers at the NPL, United Kingdom

    Science.gov (United States)

    McEvoy, Helen C.; Simpson, Robert; Machin, Graham

    2004-04-01

    The use of infrared tympanic thermometers for monitoring patient health is widespread. However, studies into the performance of these thermometers have questioned their accuracy and repeatability. To give users confidence in these devices, and to provide credibility in the measurements, it is necessary for them to be tested using an accredited, standard blackbody source, with a calibration traceable to the International Temperature Scale of 1990 (ITS-90). To address this need the National Physical Laboratory (NPL), UK, has recently set up a primary ear thermometer calibration (PET-C) source for the evaluation and calibration of tympanic (ear) thermometers over the range from 15 °C to 45 °C. The overall uncertainty of the PET-C source is estimated to be +/- 0.04 °C at k = 2. The PET-C source meets the requirements of the European Standard EN 12470-5: 2003 Clinical thermometers. It consists of a high emissivity blackbody cavity immersed in a bath of stirred liquid. The temperature of the blackbody is determined using an ITS-90 calibrated platinum resistance thermometer inserted close to the rear of the cavity. The temperature stability and uniformity of the PET-C source was evaluated and its performance validated. This paper provides a description of the PET-C along with the results of the validation measurements. To further confirm the performance of the PET-C source it was compared to the standard ear thermometer calibration sources of the National Metrology Institute of Japan (NMIJ), Japan and the Physikalisch-Technische Bundesanstalt (PTB), Germany. The results of this comparison will also be briefly discussed. The PET-C source extends the capability for testing ear thermometers offered by the NPL body temperature fixed-point source, described previously. An update on the progress with the commercialisation of the fixed-point source will be given.

  3. Calibration of atomic force microscope cantilevers using standard and inverted static methods assisted by FIB-milled spatial markers

    International Nuclear Information System (INIS)

    Slattery, Ashley D; Blanch, Adam J; Quinton, Jamie S; Gibson, Christopher T

    2013-01-01

    Static methods to determine the spring constant of AFM cantilevers have been widely used in the scientific community since the importance of such calibration techniques was established nearly 20 years ago. The most commonly used static techniques involve loading a trial cantilever with a known force by pressing it against a pre-calibrated standard or reference cantilever. These reference cantilever methods have a number of sources of uncertainty, which include the uncertainty in the measured spring constant of the standard cantilever, the exact position of the loading point on the reference cantilever and how closely the spring constant of the trial and reference cantilever match. We present a technique that enables users to minimize these uncertainties by creating spatial markers on reference cantilevers using a focused ion beam (FIB). We demonstrate that by combining FIB spatial markers with an inverted reference cantilever method, AFM cantilevers can be accurately calibrated without the tip of the test cantilever contacting a surface. This work also demonstrates that for V-shaped cantilevers it is possible to determine the precise loading position by AFM imaging the section of the cantilever where the two arms join. Removing tip-to-surface contact in both the reference cantilever method and sensitivity calibration is a significant improvement, since this is an important consideration for AFM users that require the imaging tip to remain in pristine condition before commencing measurements. Uncertainties of between 5 and 10% are routinely achievable with these methods. (paper)

  4. Simulation evaluation of NIST air-kerma rate calibration standard for electronic brachytherapy.

    Science.gov (United States)

    Hiatt, Jessica R; Rivard, Mark J; Hughes, H Grady

    2016-03-01

    Dosimetry for the model S700 50 kV electronic brachytherapy (eBT) source (Xoft, Inc., a subsidiary of iCAD, San Jose, CA) was simulated using Monte Carlo (MC) methods by Rivard et al. ["Calculated and measured brachytherapy dosimetry parameters in water for the Xoft Axxent x-ray source: An electronic brachytherapy source," Med. Phys. 33, 4020-4032 (2006)] and recently by Hiatt et al. ["A revised dosimetric characterization of the model S700 electronic brachytherapy source containing an anode-centering plastic insert and other components not included in the 2006 model," Med. Phys. 42, 2764-2776 (2015)] with improved geometric characterization. While these studies examined the dose distribution in water, there have not previously been reports of the eBT source calibration methods beyond that recently reported by Seltzer et al. ["New national air-kerma standard for low-energy electronic brachytherapy sources," J. Res. Natl. Inst. Stand. Technol. 119, 554-574 (2014)]. Therefore, the motivation for the current study was to provide an independent determination of air-kerma rate at 50 cm in air K̇air(d=50 cm) using MC methods for the model S700 eBT source. Using CAD information provided by the vendor and disassembled sources, an MC model was created for the S700 eBT source. Simulations were run using the mcnp6 radiation transport code for the NIST Lamperti air ionization chamber according to specifications by Boutillon et al. ["Comparison of exposure standards in the 10-50 kV x-ray region," Metrologia 5, 1-11 (1969)], in air without the Lamperti chamber, and in vacuum without the Lamperti chamber. K̇air(d=50 cm) was determined using the *F4 tally with NIST values for the mass energy-absorption coefficients for air. Photon spectra were evaluated over 2 π azimuthal sampling for polar angles of 0° ≤ θ ≤ 180° every 1°. Volume averaging was averted through tight radial binning. Photon energy spectra were determined over all polar angles in both air and vacuum using

  5. Implementation of ISO guide 25 in a medical dosimetry secondary standards calibration laboratory

    International Nuclear Information System (INIS)

    DeWerd, L.A.

    1995-01-01

    Currently, there is a great deal of discussion among industry and government agencies about ISO 9000 accreditation. U.S. manufacturers with ISO 9000 accreditation are regarded more favorably by European countries. The principles behind the ISO 9000 accreditation are based on the Total Quality Management (TQM) principles that are being implemented in many U.S. industries. This paper will deal only with the calibration issue. There is a difference in the areas covered by ISO 9000 and ISO Guide 25 documents. ISO 9000, in particular ISO 9001 - ISO 9003, cover the open-quotes calibrationclose quotes of inspection, measuring and test equipment. This equipment is basically used for open-quotes factory calibrationsclose quotes to determine that equipment is performing within manufacturer specifications. ISO Guide 25 is specifically for open-quotes calibration and testing laboratories,close quotes generally laboratories that have painstaking procedures to reduce uncertainties and establish high accuracy of the transfer of calibration. The experience of the University of Wisconsin Accredited Dosimetry Calibration Laboratory in conforming to ISO Guide 25 will be outlined. The entire laboratory staff must become familiar with the process and an individual with direct authority must become the one to maintain the quality of equipment and calibrations in the role of open-quotes quality-assurance manager.close quotes

  6. Solid energy calibration standards for P K-edge XANES: electronic structure analysis of PPh4Br.

    Science.gov (United States)

    Blake, Anastasia V; Wei, Haochuan; Donahue, Courtney M; Lee, Kyounghoon; Keith, Jason M; Daly, Scott R

    2018-03-01

    P K-edge X-ray absorption near-edge structure (XANES) spectroscopy is a powerful method for analyzing the electronic structure of organic and inorganic phosphorus compounds. Like all XANES experiments, P K-edge XANES requires well defined and readily accessible calibration standards for energy referencing so that spectra collected at different beamlines or under different conditions can be compared. This is especially true for ligand K-edge X-ray absorption spectroscopy, which has well established energy calibration standards for Cl (Cs 2 CuCl 4 ) and S (Na 2 S 2 O 3 ·5H 2 O), but not neighboring P. This paper presents a review of common P K-edge XANES energy calibration standards and analysis of PPh 4 Br as a potential alternative. The P K-edge XANES region of commercially available PPh 4 Br revealed a single, highly resolved pre-edge feature with a maximum at 2146.96 eV. PPh 4 Br also showed no evidence of photodecomposition when repeatedly scanned over the course of several days. In contrast, we found that PPh 3 rapidly decomposes under identical conditions. Density functional theory calculations performed on PPh 3 and PPh 4 + revealed large differences in the molecular orbital energies that were ascribed to differences in the phosphorus oxidation state (III versus V) and molecular charge (neutral versus +1). Time-dependent density functional theory calculations corroborated the experimental data and allowed the spectral features to be assigned. The first pre-edge feature in the P K-edge XANES spectrum of PPh 4 Br was assigned to P 1s → P-C π* transitions, whereas those at higher energy were P 1s → P-C σ*. Overall, the analysis suggests that PPh 4 Br is an excellent alternative to other solid energy calibration standards commonly used in P K-edge XANES experiments.

  7. Linear model correction: A method for transferring a near-infrared multivariate calibration model without standard samples

    Science.gov (United States)

    Liu, Yan; Cai, Wensheng; Shao, Xueguang

    2016-12-01

    Calibration transfer is essential for practical applications of near infrared (NIR) spectroscopy because the measurements of the spectra may be performed on different instruments and the difference between the instruments must be corrected. For most of calibration transfer methods, standard samples are necessary to construct the transfer model using the spectra of the samples measured on two instruments, named as master and slave instrument, respectively. In this work, a method named as linear model correction (LMC) is proposed for calibration transfer without standard samples. The method is based on the fact that, for the samples with similar physical and chemical properties, the spectra measured on different instruments are linearly correlated. The fact makes the coefficients of the linear models constructed by the spectra measured on different instruments are similar in profile. Therefore, by using the constrained optimization method, the coefficients of the master model can be transferred into that of the slave model with a few spectra measured on slave instrument. Two NIR datasets of corn and plant leaf samples measured with different instruments are used to test the performance of the method. The results show that, for both the datasets, the spectra can be correctly predicted using the transferred partial least squares (PLS) models. Because standard samples are not necessary in the method, it may be more useful in practical uses.

  8. Test and calibration of the Digital World-Wide Standardized Seismograph

    Science.gov (United States)

    Peterson, Jon; Hutt, Charles R.

    1982-01-01

    During the past decade there has been steady progress in the modernization of the global seismograph network operated by the U.S. Geological Survey (USGS). The World-Wide Standardized Seismograph Network (WWSSN) has been augmented by new stations with advanced instrumentation, including the Seismic Research Observatories (SRO) and the modified High-Gain Long-Period (ASRO) stations. One goal in the modernization effort has been to improve signal resolution in the long-period band. A second goal has been to generate a global digital data base to support contemporary computer-based analysis and research. In 1976, a Panel on Seismograph Networks was established by the Committee on Seismology of the National Academy of Sciences to review progress in network seismology and recommend actions that would lead to an improved global data base for seismology. One recommendation in the Panel report (Engdahl, 1977) called for upgrading selected WWSSN stations by the installation of digital recorders. This was viewed as an economical way of expanding the digital network, which had proven itself to be a very promising new tool for earthquake and explosion research. Funds for the development and assembly of 15 digital recorders were provided to the USGS by the Defense Advanced Research Projects Agency and an ad Inoc panel of scientists was convened by the Committee on Seismology to advise the USGS on the selection of stations to be upgraded and on data recording requirements, A total of 19 digital World-Wide Standardized Seismograph (DWWSS) systems will be operational when all are installed. The additional systems were made available through purchase by the USGS and other organizations; for example, the University of Bergen purchased and installed a DWWSS-type recorder and agreed to furnish the USGS with the data. A list of operational and planned DWWSS network stations is given in Table 1.1.As one might expect, the digital recorder turned out to be somewhat more sophisticated than

  9. First-principles calibration of 40Ar/39Ar mineral standards and complete extraction of 40Ar* from sanidine

    Science.gov (United States)

    Morgan, L. E.; Kuiper, K.; Mark, D.; Postma, O.; Villa, I. M.; Wijbrans, J. R.

    2010-12-01

    40Ar/39Ar geochronology relies on comparing argon isotopic data for unknowns to those for knowns. Mineral standards used as neutron fluence monitors must be dated by the K-Ar method (or at least referenced to a mineral of known K-Ar age). The commonly used age of 28.02 ± 0.28 Ma for the Fish Canyon sanidine (FCs) (Renne et al., 1998) is based upon measurements of radiogenic 40Ar in GA1550 biotite (McDougall and Roksandic, 1974), but underlying full data were not published (these measurements were never intended for use as an international standard), so uncertainties are difficult to assess. Recent developments by Kuiper et al. (2008) and Renne et al. (2010) are limited by their reliance on the accuracy of other systems. Modern technology should allow for more precise and accurate calibration of primary K-Ar and 40Ar/39Ar standards. From the ideal gas law, the number of moles of 40Ar in a system can be calculated from measurements of pressure, volume, and temperature. Thus we have designed and are proceeding to build a pipette system to introduce well-determined amounts of 40Ar into noble gas extraction lines and mass spectrometers. This system relies on components with calibrations traceable to SI unit prototypes, including a diaphragm pressure gauge (MKS Instruments), thermocouples, and a “slug” of an accurately determined volume to be inserted into the reservoir for volume determinations of the reservoir and pipette. The system will be renewable, with a lifetime of ca. 1 month for gas in the reservoir, and portable, to permit interlaboratory calibrations. The quantitative extraction of 40Ar* from the mineral standard is of highest importance; for sanidine standards this is complicated by high melt viscosity during heating. Experiments adding basaltic “zero age glass” (ZAG) to decrease melt viscosity are underway. This has previously been explored by McDowell (1983) with a resistance furnace, but has not been quantitatively addressed with laser heating

  10. Calibration of photon and beta ray sources used in brachytherapy. Guidelines on standardized procedures at Secondary Standards Dosimetry Laboratories (SSDLs) and hospitals

    International Nuclear Information System (INIS)

    2002-03-01

    It has generally been recognized that international harmonization in radiotherapy dosimetry is essential. Consequently, the IAEA has given much effort to this, for example by publishing a number of reports in the Technical Reports Series (TRS) for external beam dosimetry, most notably TRS-277 and more recently TRS-398. Both of these reports describe in detail the steps to be taken for absorbed dose determination in water and they are often referred to as 'dosimetry protocols'. Similar to TRS-277, it is expected that TRS-398 will be adopted or used as a model by a large number of countries as their national protocol. In 1996, the IAEA established a calibration service for low dose rate (LDR) 137 Cs brachytherapy sources, which is the most widely used source for treatment of gynecological cancer. To further enhance harmonization in brachytherapy dosimetry, the IAEA published in 1999 IAEA-TECDOC-1079 entitled 'Calibration of Brachytherapy Sources. Guidelines on Standardized Procedures for the Calibration of Brachytherapy Sources at Secondary Standard Dosimetry Laboratories (SSDLs) and Hospitals'. The report was well received and was distributed in a large number of copies to the members of the IAEA/WHO network of SSDLs and to medical physicists working with brachytherapy. The present report is an update of the aforementioned TECDOC. Whereas TECDOC-1079 described methods for calibrating brachytherapy sources with photon energies at or above those of 192 Ir, the current report has a wider scope in that it deals with standardization of calibration of all the most commonly used brachytherapy sources, including both photon and beta emitting sources. The latter sources have been in use for a few decades already, but their calibration methods have been unclear. Methods are also described for calibrating sources used in the rapidly growing field of cardiovascular angioplasty. In this application, irradiation of the vessel wall is done in an attempt to prevent restenosis after

  11. Free-field reciprocity calibration of laboratory standard (LS) microphones using a time selective technique

    DEFF Research Database (Denmark)

    Rasmussen, Knud; Barrera Figueroa, Salvador

    2006-01-01

    Although the basic principle of reciprocity calibration of microphones in a free field is simple, the practical problems are complicated due to the low signal-to-noise ratio and the influence of cross talk and reflections from the surroundings. The influence of uncorrelated noise can be reduced...

  12. Simulation and Evaluation of ECT Signals From MRPC Probe in Combo Calibration Standard Tube Using Electromagnetic Numerical Analysis

    International Nuclear Information System (INIS)

    Yoo, Joo Young; Song, Sung Jin; Jung, Hee Jun; Kong, Young Bae

    2006-01-01

    Signals captured from a Combo calibration standard tube play a crucial role in the evaluation of motorized rotating pancake coil (MRPC) probe signals from steam generator (SG) tubes in nuclear power plants (NPPs). Therefore, the Combo tube signals should be consistent and accurate. However, MRPC probe signals are very easily affected by various factors around the tubes so that they can be distorted in their amplitudes and phase angles which are the values specifically used in the evaluation. To overcome this problem, in this study, we explored possibility of simulation to be used as a practical calibration tool far the evaluation of real field signals. For this purpose, we investigated the characteristics of a MRPC probe and a Combo tube. And then using commercial software (VIC-3D) we simulated a set of calibration signals and compared to the experimental signals. From this comparison, we verified the accuracy of the simulated signals. Finally, we evaluated two defects using the simulated Combo tube signals, and the results were compared with those obtained using the actual field calibration signals

  13. Exploitation of secondary standard for calibration in units of Dw,1cm and assessment of several HDR brachytherapy planning systems

    International Nuclear Information System (INIS)

    Gabris, F.; Zeman, J.; Valenta, J.; Gabris, F.; Selbach, H.J.

    2012-01-01

    A secondary standard of the BEV, calibrated at the PTB in terms of D w,1c m, was used for calibration of the well-type chamber-based measuring systems used in clinics. In addition to the calibration, we tried to employ it for assessment of treatment planning systems (TPS) used for each particular after-loader. The dose to water at 1 cm distance from the source position was calculated by the TPS, using reference data from the source producer certificate. The values were compared directly with the dose measured at the same distance from the source. The comparison has been carried out for GammaMed Plus and MicroSelectron HDR sources. Differences of secondary standard measurements and TPS calculations were lower than ±5%, which is below the achievable uncertainty of both dose measurement and dose determination by the TPS. Nevertheless, it is higher than generally accepted in the case of external beam radiotherapy. Additional direct measurements in terms of D w,1c m may improve the safety and reliability of patient treatment. (authors)

  14. Variations in performance of LCDs are still evident after DICOM gray-scale standard display calibration.

    LENUS (Irish Health Repository)

    Lowe, Joanna M

    2010-07-01

    Quality assurance in medical imaging is directly beneficial to image quality. Diagnostic images are frequently displayed on secondary-class displays that have minimal or no regular quality assurance programs, and treatment decisions are being made from these display types. The purpose of this study is to identify the impact of calibration on physical and psychophysical performance of liquid crystal displays (LCDs) and the extent of potential variance across various types of LCDs.

  15. Loop system for creating jet fuel vapor standards used in the calibration of infrared spectrophotometers and gas chromatographs.

    Science.gov (United States)

    Reboulet, James; Cunningham, Robert; Gunasekar, Palur G; Chapman, Gail D; Stevens, Sean C

    2009-02-01

    A whole body inhalation study of mixed jet fuel vapor and its aerosol necessitated the development of a method for preparing vapor only standards from the neat fuel. Jet fuel is a complex mixture of components which partitions between aerosol and vapor when aspirated based on relative volatility of the individual compounds. A method was desired which could separate the vapor portion from the aerosol component to prepare standards for the calibration of infrared spectrophotometers and a head space gas chromatography system. A re-circulating loop system was developed which provided vapor only standards whose composition matched those seen in an exposure system. Comparisons of nominal concentrations in the exposure system to those determined by infrared spectrophotometry were in 92-95% agreement. Comparison of jet fuel vapor concentrations determined by infrared spectrophotometry compared to head space gas chromatography yielded a 93% overall agreement in trial runs. These levels of agreement show the loop system to be a viable method for creating jet fuel vapor standards for calibrating instruments.

  16. International collaborative study for the calibration of proposed International Standards for thromboplastin, rabbit, plain, and for thromboplastin, recombinant, human, plain.

    Science.gov (United States)

    van den Besselaar, A M H P; Chantarangkul, V; Angeloni, F; Binder, N B; Byrne, M; Dauer, R; Gudmundsdottir, B R; Jespersen, J; Kitchen, S; Legnani, C; Lindahl, T L; Manning, R A; Martinuzzo, M; Panes, O; Pengo, V; Riddell, A; Subramanian, S; Szederjesi, A; Tantanate, C; Herbel, P; Tripodi, A

    2018-01-01

    Essentials Two candidate International Standards for thromboplastin (coded RBT/16 and rTF/16) are proposed. International Sensitivity Index (ISI) of proposed standards was assessed in a 20-centre study. The mean ISI for RBT/16 was 1.21 with a between-centre coefficient of variation of 4.6%. The mean ISI for rTF/16 was 1.11 with a between-centre coefficient of variation of 5.7%. Background The availability of International Standards for thromboplastin is essential for the calibration of routine reagents and hence the calculation of the International Normalized Ratio (INR). Stocks of the current Fourth International Standards are running low. Candidate replacement materials have been prepared. This article describes the calibration of the proposed Fifth International Standards for thromboplastin, rabbit, plain (coded RBT/16) and for thromboplastin, recombinant, human, plain (coded rTF/16). Methods An international collaborative study was carried out for the assignment of International Sensitivity Indexes (ISIs) to the candidate materials, according to the World Health Organization (WHO) guidelines for thromboplastins and plasma used to control oral anticoagulant therapy with vitamin K antagonists. Results Results were obtained from 20 laboratories. In several cases, deviations from the ISI calibration model were observed, but the average INR deviation attributabled to the model was not greater than 10%. Only valid ISI assessments were used to calculate the mean ISI for each candidate. The mean ISI for RBT/16 was 1.21 (between-laboratory coefficient of variation [CV]: 4.6%), and the mean ISI for rTF/16 was 1.11 (between-laboratory CV: 5.7%). Conclusions The between-laboratory variation of the ISI for candidate material RBT/16 was similar to that of the Fourth International Standard (RBT/05), and the between-laboratory variation of the ISI for candidate material rTF/16 was slightly higher than that of the Fourth International Standard (rTF/09). The candidate materials

  17. Quality control of the NPL-CRC secondary standard system used for activimeters calibration at IPEN, Sao Paulo, Brazil

    International Nuclear Information System (INIS)

    Martins, Elaine W.; Potiens, Maria da P.A.

    2009-01-01

    The objective of this study was to establish a quality control program to be applied at the NPL-CRC activimeter secondary standard system, used as reference to comparison in tests made with the work tertiary standard activimeter, Capintec basic CRC R -15BT, both belonging to the Calibration Laboratory of IPEN. The repeatability, reproducibility and the precision tests were performed using a sealed check source of 133 Ba, from Amersham. It was made 70 series of 10 measurements to each activimeter, totaling 1400 measurements. Considering the variation limit of 5% to precision and reproducibility tests in the nuclear medicine services, recommended by the Brazilian standard CNEN-NN-3.05, the results observed in the behavior of the IPEN activimeter were satisfactory. (author)

  18. PROCAL: A Set of 40 Peptide Standards for Retention Time Indexing, Column Performance Monitoring, and Collision Energy Calibration.

    Science.gov (United States)

    Zolg, Daniel Paul; Wilhelm, Mathias; Yu, Peng; Knaute, Tobias; Zerweck, Johannes; Wenschuh, Holger; Reimer, Ulf; Schnatbaum, Karsten; Kuster, Bernhard

    2017-11-01

    Beyond specific applications, such as the relative or absolute quantification of peptides in targeted proteomic experiments, synthetic spike-in peptides are not yet systematically used as internal standards in bottom-up proteomics. A number of retention time standards have been reported that enable chromatographic aligning of multiple LC-MS/MS experiments. However, only few peptides are typically included in such sets limiting the analytical parameters that can be monitored. Here, we describe PROCAL (ProteomeTools Calibration Standard), a set of 40 synthetic peptides that span the entire hydrophobicity range of tryptic digests, enabling not only accurate determination of retention time indices but also monitoring of chromatographic separation performance over time. The fragmentation characteristics of the peptides can also be used to calibrate and compare collision energies between mass spectrometers. The sequences of all selected peptides do not occur in any natural protein, thus eliminating the need for stable isotope labeling. We anticipate that this set of peptides will be useful for multiple purposes in individual laboratories but also aiding the transfer of data acquisition and analysis methods between laboratories, notably the use of spectral libraries. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  19. Transition Radiation Tracker calibration, searches beyond the Standard Model and multiparticle correlations in ATLAS

    CERN Document Server

    Alonso, Alejandro; Torsten, Akesson

    This thesis contains two different aspects of my research work towards physics in proton-proton collisions in the ATLAS experiment at the LHC. The first part is focused on the understanding and developing of a calibration system to obtain the best possible charged particle reconstruction in the Transition Radiation Tracker. The method explained in this thesis is the current calibration technique used in the TRT and it is applied to all the data collected by ATLAS. Thanks to the method developed, the detector design resolution is achieved, and even improved in the central region of the TRT. In the second part, three different analyses are presented. Due to my interest in tracking and thanks to the new energy range available at the LHC, the first analysis is the study of multiparticle correlations at 900 GeV and 7 TeV. This analysis is performed with the first ATLAS data collected during 2010. Two different aspects are studied: the high order moments and an attempt to measure the normalized factorial moments ...

  20. Limitations of turbidity process probes and formazine as their calibration standard.

    Science.gov (United States)

    Münzberg, Marvin; Hass, Roland; Dinh Duc Khanh, Ninh; Reich, Oliver

    2017-01-01

    Turbidity measurements are frequently implemented for the monitoring of heterogeneous chemical, physical, or biotechnological processes. However, for quantitative measurements, turbidity probes need calibration, as is requested and regulated by the ISO 7027:1999. Accordingly, a formazine suspension has to be produced. Despite this regulatory demand, no scientific publication on the stability and reproducibility of this polymerization process is available. In addition, no characterization of the optical properties of this calibration material with other optical methods had been achieved so far. Thus, in this contribution, process conditions such as temperature and concentration have been systematically investigated by turbidity probe measurements and Photon Density Wave (PDW) spectroscopy, revealing an influence on the temporal formazine formation onset. In contrast, different reaction temperatures do not lead to different scattering properties for the final formazine suspensions, but give an access to the activation energy for this condensation reaction. Based on PDW spectroscopy data, the synthesis of formazine is reproducible. However, very strong influences of the ambient conditions on the measurements of the turbidity probe have been observed, limiting its applicability. The restrictions of the turbidity probe with respect to scatterer concentration are examined on the basis of formazine and polystyrene suspensions. Compared to PDW spectroscopy data, signal saturation is observed at already low reduced scattering coefficients.

  1. Instrumentation calibration

    International Nuclear Information System (INIS)

    Mack, D.A.

    1976-08-01

    Procedures for the calibration of different types of laboratory equipment are described. Provisions for maintaining the integrity of reference and working standards traceable back to a national standard are discussed. Methods of validation and certification methods are included. An appendix lists available publications and services of national standardizing agencies

  2. Calibration of a detector by activation with a continuous neutron source used as a transfer standard for measuring pulsed neutron beams

    International Nuclear Information System (INIS)

    Moreno, Jose; Silva, Patricio; Birstein, Lipo; Soto, Leopoldo

    2002-01-01

    This paper presents a method for calibrating activation detectors. These detectors will be used as transfer standard in measuring neutron fluxes produced by pulsed plasma sources. A standard neutron source is used as a secondary standard. The activation detector is being shielded in order to substantially reduce detection of gamma emission coming from the source. The detector's calibration factor is obtained by considering also the standard neutron source as a free source of gamma radiation so that the measurements can be done without quickly withdrawing the neutron source as it is usually done. This will substantially simplify the traditionally established method (JM)

  3. Development, improvement and calibration of neutronic reaction rate measurements: elaboration of a base of standard techniques; Developpement, amelioration et calibration des mesures de taux de reaction neutroniques: elaboration d`une base de techniques standards

    Energy Technology Data Exchange (ETDEWEB)

    Hudelot, J.P

    1998-06-19

    In order to improve and to validate the neutronic calculation schemes, perfecting integral measurements of neutronic parameters is necessary. This thesis focuses on the conception, the improvement and the development of neutronic reaction rates measurements, and aims at building a base of standard techniques. Two subjects are discussed. The first one deals with direct measurements by fission chambers. A short presentation of the different usual techniques is given. Then, those last ones are applied through the example of doubling time measurements on the EOLE facility during the MISTRAL 1 experimental programme. Two calibration devices of fission chambers are developed: a thermal column located in the central part of the MINERVE facility, and a calibration cell using a pulsed high flux neutron generator and based on the discrimination of the energy of the neutrons with a time-of-flight method. This second device will soon allow to measure the mass of fission chambers with a precision of about 1 %. Finally, the necessity of those calibrations will be shown through spectral indices measurements in core MISTRAL 1 (UO{sub 2}) and MISTRAL 2 (MOX) of the EOLE facility. In each case, the associated calculation schemes, performed using the Monte Carlo MCNP code with the ENDF-BV library, will be validated. Concerning the second one, the goal is to develop a method for measuring the modified conversion ratio of {sup 238}U (defined as the ratio of {sup 238}U capture rate to total fission rate) by gamma-ray spectrometry of fuel rods. Within the framework of the MISTRAL 1 and MISTRAL 2 programmes, the measurement device, the experimental results and the spectrometer calibration are described. Furthermore, the MCNP calculations of neutron self-shielding and gamma self-absorption are validated. It is finally shown that measurement uncertainties are better than 1 %. The extension of this technique to future modified conversion ratio measurements for {sup 242}Pu (on MOX rods) and

  4. Development of the neutron reference calibration field using a {sup 252}Cf standard source surrounded with PMMA moderators

    Energy Technology Data Exchange (ETDEWEB)

    Yoshida, T.; Kanai, K.; Tsujimura, N. [Japan Nuclear Cycle Development Institute, Ibaraki-ken (Japan)

    2002-07-01

    The authors developed the neutron reference calibration fields using a {sup 252} Cf standard source surrounded with PMMA moderators at the Japan Nuclear Cycle Development (JNC), Tokai Works. The moderators are co-axial, hollow cylinders made of lead-contained PMMA with a thickness of 13.5, 35.0, 59.5 and 77.0mm, and the {sup 252} Cf source is guided to the geometric center of moderators by the pneumatic system. These fields can provide the moderated neutron spectra very similar to those encountered around the globe-boxes of the fabrication process of MOX (PuO{sub 2}-UO{sub 2} mixed oxide) fuel. The neutron energy spectrum at the reference calibration point was evaluated from the calculations by MCNP4B and the measurements by the INS-type Bonner multi-sphere spectrometer and the hydrogen-filled proportional counters. The calculated neutron spectra were in good agreements with the measured ones. These fields were characterized in terms of the neutron fluence rate, spectral composition and ambient dose equivalent rate, and have served for the response-characterization of various neutron survey instruments.

  5. Development of the neutron reference calibration field using a 252Cf standard source surrounded with PMMA moderators

    International Nuclear Information System (INIS)

    Yoshida, T.; Kanai, K.; Tsujimura, N.

    2002-01-01

    The authors developed the neutron reference calibration fields using a 252 Cf standard source surrounded with PMMA moderators at the Japan Nuclear Cycle Development (JNC), Tokai Works. The moderators are co-axial, hollow cylinders made of lead-contained PMMA with a thickness of 13.5, 35.0, 59.5 and 77.0mm, and the 252 Cf source is guided to the geometric center of moderators by the pneumatic system. These fields can provide the moderated neutron spectra very similar to those encountered around the globe-boxes of the fabrication process of MOX (PuO 2 -UO 2 mixed oxide) fuel. The neutron energy spectrum at the reference calibration point was evaluated from the calculations by MCNP4B and the measurements by the INS-type Bonner multi-sphere spectrometer and the hydrogen-filled proportional counters. The calculated neutron spectra were in good agreements with the measured ones. These fields were characterized in terms of the neutron fluence rate, spectral composition and ambient dose equivalent rate, and have served for the response-characterization of various neutron survey instruments

  6. Contributed Review: Absolute spectral radiance calibration of fiber-optic shock-temperature pyrometers using a coiled-coil irradiance standard lamp

    Energy Technology Data Exchange (ETDEWEB)

    Fat’yanov, O. V., E-mail: fatyan1@gps.caltech.edu; Asimow, P. D., E-mail: asimow@gps.caltech.edu [Division of Geological and Planetary Sciences 252-21, California Institute of Technology, Pasadena, California 91125 (United States)

    2015-10-15

    We describe an accurate and precise calibration procedure for multichannel optical pyrometers such as the 6-channel, 3-ns temporal resolution instrument used in the Caltech experimental geophysics laboratory. We begin with a review of calibration sources for shock temperatures in the 3000-30 000 K range. High-power, coiled tungsten halogen standards of spectral irradiance appear to be the only practical alternative to NIST-traceable tungsten ribbon lamps, which are no longer available with large enough calibrated area. However, non-uniform radiance complicates the use of such coiled lamps for reliable and reproducible calibration of pyrometers that employ imaging or relay optics. Careful analysis of documented methods of shock pyrometer calibration to coiled irradiance standard lamps shows that only one technique, not directly applicable in our case, is free of major radiometric errors. We provide a detailed description of the modified Caltech pyrometer instrument and a procedure for its absolute spectral radiance calibration, accurate to ±5%. We employ a designated central area of a 0.7× demagnified image of a coiled-coil tungsten halogen lamp filament, cross-calibrated against a NIST-traceable tungsten ribbon lamp. We give the results of the cross-calibration along with descriptions of the optical arrangement, data acquisition, and processing. We describe a procedure to characterize the difference between the static and dynamic response of amplified photodetectors, allowing time-dependent photodiode correction factors for spectral radiance histories from shock experiments. We validate correct operation of the modified Caltech pyrometer with actual shock temperature experiments on single-crystal NaCl and MgO and obtain very good agreement with the literature data for these substances. We conclude with a summary of the most essential requirements for error-free calibration of a fiber-optic shock-temperature pyrometer using a high-power coiled tungsten halogen

  7. Advisory Committee for the Calibration Standards of Ionizing Radiation Measurement. Section 1. X and #betta# radiations, electrons

    International Nuclear Information System (INIS)

    1982-01-01

    Section I (Rayons X et #betta#, electrons) of the Comite Consultatif pour les Etalons de Mesure des Rayonnements Ionisants held its sixth meeting in June 1981. The work carried out recently in various laboratories represented at the meeting is contained in a series of Progress Reports. Several international comparisons of exposure standards performed at BIPM between 5 keV and 1.2 MeV were presented and the question of exposure measurements at protection-level exposure rates was raised. The work of the three existing Working Parties was discussed at length: comparison of Fricke chemical dosimetry systems, conversion of exposure to absorbed dose in water, conversion of graphite absorbed dose into water absorbed dose. A recommendation was made concerning the possibility of expressing in terms of air kerma or water kerma calibrations made in terms of exposure [fr

  8. Air kerma standard for calibration of well-type chambers in Brazil using {sup 192}Ir HDR sources and its traceability

    Energy Technology Data Exchange (ETDEWEB)

    Di Prinzio, Renato; Almeida, Carlos Eduardo de [Laboratorio de Ciencias Radiologicas-Universidade do Estado do Rio de Janeiro (LCR/UERJ), R. Sao Francisco Xavier, 524, Pavilhao Haroldo Lisboa da Cunha, Terreo, Sala 136-Maracana, CEP 20550-900-Rio de Janeiro/RJ-Rio de Janeiro, RJ (Brazil) and Instituto de Radioprotecao e Dosimetria-Comissao Nacional de Energia Nuclear (IRD/CNEN), Av. Salvador Allende, s/n, Jacarepagua-CE22780-160-Rio de Janeiro, RJ (Brazil); Laboratorio de Ciencias Radiologicas-Universidade do Estado do Rio de Janeiro (LCR/UERJ), R. Sao Francisco Xavier, 524, Pavilhao Haroldo Lisboa da Cunha, Terreo, Sala 136-Maracana, CEP 20550-900-Rio de Janeiro/RJ-Rio de Janeiro, RJ (Brazil)

    2009-03-15

    In Brazil there are over 100 high dose rate (HDR) brachytherapy facilities using well-type chambers for the determination of the air kerma rate of {sup 192}Ir sources. This paper presents the methodology developed and extensively tested by the Laboratorio de Ciencias Radiologicas (LCR) and presently in use to calibrate those types of chambers. The system was initially used to calibrate six well-type chambers of brachytherapy services, and the maximum deviation of only 1.0% was observed between the calibration coefficients obtained and the ones in the calibration certificate provided by the UWADCL. In addition to its traceability to the Brazilian National Standards, the whole system was taken to University of Wisconsin Accredited Dosimetry Calibration Laboratory (UWADCL) for a direct comparison and the same formalism to calculate the air kerma was used. The comparison results between the two laboratories show an agreement of 0.9% for the calibration coefficients. Three Brazilian well-type chambers were calibrated at the UWADCL, and by LCR, in Brazil, using the developed system and a clinical HDR machine. The results of the calibration of three well chambers have shown an agreement better than 1.0%. Uncertainty analyses involving the measurements made both at the UWADCL and LCR laboratories are discussed.

  9. Use of a non-linear method for including the mass uncertainty of gravimetric standards and system measurement errors in the fitting of calibration curves for XRFA freeze-dried UNO3 standards

    International Nuclear Information System (INIS)

    Pickles, W.L.; McClure, J.W.; Howell, R.H.

    1978-05-01

    A sophisticated nonlinear multiparameter fitting program was used to produce a best fit calibration curve for the response of an x-ray fluorescence analyzer to uranium nitrate, freeze dried, 0.2% accurate, gravimetric standards. The program is based on unconstrained minimization subroutine, VA02A. The program considers the mass values of the gravimetric standards as parameters to be fit along with the normal calibration curve parameters. The fitting procedure weights with the system errors and the mass errors in a consistent way. The resulting best fit calibration curve parameters reflect the fact that the masses of the standard samples are measured quantities with a known error. Error estimates for the calibration curve parameters can be obtained from the curvature of the ''Chi-Squared Matrix'' or from error relaxation techniques. It was shown that nondispersive XRFA of 0.1 to 1 mg freeze-dried UNO 3 can have an accuracy of 0.2% in 1000 s

  10. Advisory Committee for the Calibration Standards of Ionizing Radiation Measurement: Section 3. Neutron measurements

    International Nuclear Information System (INIS)

    1982-01-01

    Section III (Mesures neutroniques) of the Comite Consultatif pour les Etalons de Mesure des Rayonnements Ionisants held its fifth meeting in May 1981. Recent work carried out at BIPM in the field of neutron measurements was reported. The status of a full-scale 252 Cf neutron source intercomparison (10 7 s - 1 ) and of several restricted comparisons was discussed. Intercomparisons of fast neutron fluence rates are in progress ( 115 In(n,n') 115 Insup(m); NB/Zr) or will take place in the near future ( 115 n(n,#betta#) 116 Insup(m); 235 U and 238 U fission chambers). An intercomparison of neutron dosimetry standards by circulating tissue-equivalent ion chambers will be prepared and organized by BIPM. Finally, there was a broad exchange of information on work in progress at the various laboratories represented at the meeting [fr

  11. CRM Assessment: Determining the Generalization of Rater Calibration Training. Summary of Research Report: Gold Standards Training

    Science.gov (United States)

    Baker, David P.

    2002-01-01

    The extent to which pilot instructors are trained to assess crew resource management (CRM) skills accurately during Line-Oriented Flight Training (LOFT) and Line Operational Evaluation (LOE) scenarios is critical. Pilot instructors must make accurate performance ratings to ensure that proper feedback is provided to flight crews and appropriate decisions are made regarding certification to fly the line. Furthermore, the Federal Aviation Administration's (FAA) Advanced Qualification Program (AQP) requires that instructors be trained explicitly to evaluate both technical and CRM performance (i.e., rater training) and also requires that proficiency and standardization of instructors be verified periodically. To address the critical need for effective pilot instructor training, the American Institutes for Research (AIR) reviewed the relevant research on rater training and, based on "best practices" from this research, developed a new strategy for training pilot instructors to assess crew performance. In addition, we explored new statistical techniques for assessing the effectiveness of pilot instructor training. The results of our research are briefly summarized below. This summary is followed by abstracts of articles and book chapters published under this grant.

  12. UV scale calibration transfer from an improved pyroelectric detector standard to field UV-A meters and 365 nm excitation sources

    Science.gov (United States)

    Eppeldauer, G. P.; Podobedov, V. B.; Cooksey, C. C.

    2017-05-01

    Calibration of the emitted radiation from UV sources peaking at 365 nm, is necessary to perform the ASTM required 1 mW/cm2 minimum irradiance in certain military material (ships, airplanes etc) tests. These UV "black lights" are applied for crack-recognition using fluorescent liquid penetrant inspection. At present, these nondestructive tests are performed using Hg-lamps. Lack of a proper standard and the different spectral responsivities of the available UV meters cause significant measurement errors even if the same UV-365 source is measured. A pyroelectric radiometer standard with spectrally flat (constant) response in the UV-VIS range has been developed to solve the problem. The response curve of this standard determined from spectral reflectance measurement, is converted into spectral irradiance responsivity with UV sources (with different peaks and distributions) without using any source standard. Using this broadband calibration method, yearly spectral calibrations for the reference UV (LED) sources and irradiance meters is not needed. Field UV sources and meters can be calibrated against the pyroelectric radiometer standard for broadband (integrated) irradiance and integrated responsivity. Using the broadband measurement procedure, the UV measurements give uniform results with significantly decreased uncertainties.

  13. Update of X- and γ-ray decay data standards for detector calibration and other applications. Summary report of the 1. research co-ordination meeting

    International Nuclear Information System (INIS)

    Herman, M.; Nichols, A.

    1999-07-01

    The discussions and conclusions of the First Research Co-ordination Meeting to Update X- and γ-ray Decay Data Standards for Detector Calibration are described in this summary report. The agreed list of radionuclides to be evaluated is given, along with the evaluation procedures and assignment of tasks among participants of the CRP. 14 presentations given at the meeting were indexed separately

  14. The standardization methods of radioactive sources (125I, 131I, 99mTc, and 18F) for calibrating nuclear medicine equipment in Indonesia

    International Nuclear Information System (INIS)

    Wurdiyanto, G; Candra, H

    2016-01-01

    The standardization of radioactive sources ( 125 I, 131 I, 99m Tc and 18 F) to calibrate the nuclear medicine equipment had been carried out in PTKMR-BATAN. This is necessary because the radioactive sources used in the field of nuclear medicine has a very short half-life in other that to obtain a quality measurement results require special treatment. Besides that, the use of nuclear medicine techniques in Indonesia develop rapidly. All the radioactive sources were prepared by gravimetric methods. Standardization of 125 I has been carried out by photon- photon coincidence methods, while the others have been carried out by gamma spectrometry methods. The standar sources are used to calibrate a Capintec CRC-7BT radionuclide calibrator. The results shows that calibration factor for Capintec CRC-7BT dose calibrator is 1,03; 1,02; 1,06; and 1,04 for 125 I, 131 I, 99m Tc and 18 F respectively, by about 5 to 6% of the expanded uncertainties. (paper)

  15. The standardization methods of radioactive sources (125I, 131I, 99mTc, and 18F) for calibrating nuclear medicine equipment in Indonesia

    Science.gov (United States)

    Wurdiyanto, G.; Candra, H.

    2016-03-01

    The standardization of radioactive sources (125I, 131I, 99mTc and 18F) to calibrate the nuclear medicine equipment had been carried out in PTKMR-BATAN. This is necessary because the radioactive sources used in the field of nuclear medicine has a very short half-life in other that to obtain a quality measurement results require special treatment. Besides that, the use of nuclear medicine techniques in Indonesia develop rapidly. All the radioactive sources were prepared by gravimetric methods. Standardization of 125I has been carried out by photon- photon coincidence methods, while the others have been carried out by gamma spectrometry methods. The standar sources are used to calibrate a Capintec CRC-7BT radionuclide calibrator. The results shows that calibration factor for Capintec CRC-7BT dose calibrator is 1,03; 1,02; 1,06; and 1,04 for 125I, 131I, 99mTc and 18F respectively, by about 5 to 6% of the expanded uncertainties.

  16. Report on the consultants' meeting on preparation of the proposal for a coordinated research project to update X- and γ-ray decay data standards for detector calibration

    International Nuclear Information System (INIS)

    Nichols, A.; Herman, M.

    1998-05-01

    The IAEA Nuclear Data Section has been charged by the International Nuclear Data Committee to consider the establishment of a Coordinated Research Project (CRP) to update the IAEA database of X-ray and γ-ray Standards for Detector Calibration. This CRP should re-define the radionuclides most suited for detector calibration, extending applications to safeguards, materials analysis, environmental monitoring, and medical use. This document is a report on the Consultants' Meeting held at IAEA, Vienna, between 24-25 November 1997 to assess the current needs, re-define the most suitable radionuclides, and advise the IAEA Nuclear Data Section on the need and form of such a CRP

  17. Development of the 60Co gamma-ray standard field for therapy-level dosimeter calibration in terms of absorbed dose to water (ND,W)

    International Nuclear Information System (INIS)

    Fukumura, Akifumi; Mizuno, Hideyuki; Fukahori, Mai; Sakata, Suoh

    2013-01-01

    A primary standard for the absorbed dose rate to water in a 60 Co gamma-ray field was established at National Metrology Institute of Japan (NMIJ) in fiscal year 2011. Then, a 60 Co gamma-ray standard field for therapy-level dosimeter calibration in terms of absorbed dose to water was developed at National Institute of Radiological Sciences (NIRS) as a secondary standard dosimetry laboratory (SSDL). The results of an International Atomic Energy Agency (IAEA)/World Health Organization (WHO) TLD SSDL audit demonstrated that there was good agreement between NIRS stated absorbed dose to water and IAEA measurements. The IAEA guide based on the International Organization for Standardization (ISO) standard was used to estimate the relative expanded uncertainty of the calibration factor for a therapy-level Farmer type ionization chamber in terms of absorbed dose to water (N D,W ) with the new field. The uncertainty of N D,W was estimated to be 1.1% (k=2), which corresponds to approximately one third of the value determined in the existing air kerma field. The dissemination of traceability of the calibration factor determined in the new field is expected to diminish the uncertainty of dose delivered to patients significantly. (author)

  18. A novel strategy for preparing calibration standards for the analysis of plant materials by laser-induced breakdown spectroscopy: A case study with pellets of sugar cane leaves

    Energy Technology Data Exchange (ETDEWEB)

    Silva Gomes, Marcos da [Universidade de São Paulo, Centro de Energia Nuclear na Agricultura (CENA), Laboratório de Química Analítica, Caixa Postal 96, CEP 13416-000, Piracicaba, SP (Brazil); Universidade Federal de São Carlos, Departamento de Química, Rodovia Washington Luiz km 235, São Carlos, SP (Brazil); Gustinelli Arantes de Carvalho, Gabriel [Universidade de São Paulo, Centro de Energia Nuclear na Agricultura (CENA), Laboratório de Química Analítica, Caixa Postal 96, CEP 13416-000, Piracicaba, SP (Brazil); Santos, Dário [Universidade Federal de São Paulo, Departamento de Ciências Exatas e da Terra, Rua Professor Arthur Riedel 275, Diadema, SP (Brazil); Krug, Francisco José, E-mail: fjkrug@cena.usp.br [Universidade de São Paulo, Centro de Energia Nuclear na Agricultura (CENA), Laboratório de Química Analítica, Caixa Postal 96, CEP 13416-000, Piracicaba, SP (Brazil)

    2013-08-01

    Calibration is still a challenging task when dealing with the direct analysis of solids. This is particularly true for laser-induced breakdown spectroscopy (LIBS), and laser ablation inductively coupled plasma optical emission spectrometry/mass spectrometry, when the calibrations are matrix-dependent and/or appropriate certified reference materials are generally not available. Looking at the analysis of plant materials in the form of pressed pellets by LIBS, a new method to overcome and/or minimize this difficulty is proposed by keeping the matrix constant in order to produce matrix-matched calibration pellets. To achieve this goal and to test this novel approach, ground sugar cane leaves were chosen and submitted to acid extractions for obtaining the corresponding blank or a material containing very low concentrations of the analytes. The resulting dried solid material was used either as a blank or a low concentration standard, and also homogeneously mixed with the original plant material at appropriate ratios as well. The corresponding pellets were used as calibration standards and ablated at 30 different sites by applying 25 laser pulses per site with a Q-switched Nd:YAG at 1064 nm. The plasma emission collected by lenses was directed through an optical fiber towards a spectrometer equipped with Echelle optics and intensified charge-coupled device. Delay time and integration time gate were fixed at 2.0 and 5.0 μs, respectively. This calibration strategy was tested for the determination of Ca, Mg, K, P, Cu, Mn, and Zn by LIBS in pellets of leaves from 17 varieties of sugar cane and good correlations were obtained with inductively coupled plasma optical emission spectrometry results in the corresponding acid digests. The proposed approach was also useful to estimate the limits of detection based on measurements of blanks, as recommended by IUPAC, or with the aid of a low concentration standard. - Highlights: • Blanks and/or low concentration standards of plant

  19. Standard Test Method for Calibration of Primary Non-Concentrator Terrestrial Photovoltaic Reference Cells Using a Tabular Spectrum

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2010-01-01

    1.1 This test method is intended to be used for calibration and characterization of primary terrestrial photovoltaic reference cells to a desired reference spectral irradiance distribution, such as Tables G173. The recommended physical requirements for these reference cells are described in Specification E1040. Reference cells are principally used in the determination of the electrical performance of photovoltaic devices. 1.2 Primary photovoltaic reference cells are calibrated in natural sunlight using the relative spectral response of the cell, the relative spectral distribution of the sunlight, and a tabulated reference spectral irradiance distribution. 1.3 This test method requires the use of a pyrheliometer that is calibrated according to Test Method E816, which requires the use of a pyrheliometer that is traceable to the World Radiometric Reference (WRR). Therefore, reference cells calibrated according to this test method are traceable to the WRR. 1.4 This test method is a technique that may be used ...

  20. State special calibration standard of acoustic pressure in aqueous medium within frequency range of 0.001 to 200 khz

    International Nuclear Information System (INIS)

    Golenkov, A.N.; Golub', S.G.; Likhachev, S.M.; Makarevich, B.N.; Fadeev, V.G.

    1974-01-01

    A standard approved by the State Standard Specification (GOST) is described. The standard has been developed at the VNIIFTRI. The metrology characteristics and main data of the standard units are presented

  1. Spectral Irradiance Calibration in the Infrared. XVI. Improved Accuracy in the Infrared Spectra of the Secondary and Tertiary Standard Calibration Stars

    Science.gov (United States)

    2006-10-01

    resolution ( AlA ). -, 400) spectroscopy obtained on infrared standard stars by the Short Wavelength Spectrometer on the Infrared Space Observatory with high...1995): 2.1-2.4 pm Strecker et al. (1979): 1.22-2.4 pm 6 See http://vizier.hia.nrc.ca/viz-bin/VizieR. REFERENCES Alonso, A., Salaris, M., Arribas , S...Haddock, D. J., Arribas , S., Leggett, S. K., & Mountain, C. M. 1988, A&AS, 74, 127

  2. Calibration of GafChromic XR-RV3 radiochromic film for skin dose measurement using standardized x-ray spectra and a commercial flatbed scanner

    International Nuclear Information System (INIS)

    McCabe, Bradley P.; Speidel, Michael A.; Pike, Tina L.; Van Lysel, Michael S.

    2011-01-01

    Purpose: In this study, newly formulated XR-RV3 GafChromic film was calibrated with National Institute of Standards and Technology (NIST) traceability for measurement of patient skin dose during fluoroscopically guided interventional procedures. Methods: The film was calibrated free-in-air to air kerma levels between 15 and 1100 cGy using four moderately filtered x-ray beam qualities (60, 80, 100, and 120 kVp). The calibration films were scanned with a commercial flatbed document scanner. Film reflective density-to-air kerma calibration curves were constructed for each beam quality, with both the orange and white sides facing the x-ray source. A method to correct for nonuniformity in scanner response (up to 25% depending on position) was developed to enable dose measurement with large films. The response of XR-RV3 film under patient backscattering conditions was examined using on-phantom film exposures and Monte Carlo simulations. Results: The response of XR-RV3 film to a given air kerma depended on kVp and film orientation. For a 200 cGy air kerma exposure with the orange side of the film facing the source, the film response increased by 20% from 60 to 120 kVp. At 500 cGy, the increase was 12%. When 500 cGy exposures were performed with the white side facing the x-ray source, the film response increased by 4.0% (60 kVp) to 9.9% (120 kVp) compared to the orange-facing orientation. On-phantom film measurements and Monte Carlo simulations show that using a NIST-traceable free-in-air calibration curve to determine air kerma in the presence of backscatter results in an error from 2% up to 8% depending on beam quality. The combined uncertainty in the air kerma measurement from the calibration curves and scanner nonuniformity correction was ±7.1% (95% C.I.). The film showed notable stability. Calibrations of film and scanner separated by 1 yr differed by 1.0%. Conclusions: XR-RV3 radiochromic film response to a given air kerma shows dependence on beam quality and film

  3. Mechanics of log calibration

    International Nuclear Information System (INIS)

    Waller, W.C.; Cram, M.E.; Hall, J.E.

    1975-01-01

    For any measurement to have meaning, it must be related to generally accepted standard units by a valid and specified system of comparison. To calibrate well-logging tools, sensing systems are designed which produce consistent and repeatable indications over the range for which the tool was intended. The basics of calibration theory, procedures, and calibration record presentations are reviewed. Calibrations for induction, electrical, radioactivity, and sonic logging tools will be discussed. The authors' intent is to provide an understanding of the sources of errors, of the way errors are minimized in the calibration process, and of the significance of changes in recorded calibration data

  4. Update of X- and γ-ray decay data standards for detector calibration and other applications. Summary report of the second research co-ordination meeting

    International Nuclear Information System (INIS)

    Herman, M.; Nichols, A.L.

    2000-09-01

    The Second Research Co-ordination Meeting to Update X- and γ-ray Decay Data Standards for Detector Calibration was held at PTB Braunschweig from 10 to 12 May 2000. A primary aim of this meeting was to review progress in the evaluation and recommendation of data under the auspices of the CRP. All CRP activities were reviewed, and actions agreed for the remaining 18 months of the programme. Separate indexing was provided for 13 contributions to the meeting

  5. Update of X- and {gamma}-ray decay data standards for detector calibration and other applications. Summary report of the second research co-ordination meeting

    Energy Technology Data Exchange (ETDEWEB)

    Herman, M [International Atomic Energy Agency, Nuclear Data Section, Vienna (Austria); Nichols, A L [AEA Technology, Harwell (United Kingdom)

    2000-09-01

    The Second Research Co-ordination Meeting to Update X- and {gamma}-ray Decay Data Standards for Detector Calibration was held at PTB Braunschweig from 10 to 12 May 2000. A primary aim of this meeting was to review progress in the evaluation and recommendation of data under the auspices of the CRP. All CRP activities were reviewed, and actions agreed for the remaining 18 months of the programme. Separate indexing was provided for 13 contributions to the meeting.

  6. Fabrication of SO/sub 2/preparation system and calibration of PINSTECH sulfur standard for /sup 34/S/sup 32/S mass spectrometric analysis

    International Nuclear Information System (INIS)

    Sajjad, M.I.; Latif, Z.; Ali, M.; Qureshi, R.M.; Tasneem, M.A.; Khan, I.H.; Ahmed, M.; Ahmed, I.

    1994-05-01

    This report describes the fabrication and standardization of operation procedures of a SO/sub 2/ preparation system used for the extraction of sulfur dioxide gas from sulfur minerals (aqueous sulfate, elemental sulfur, and sulfides) for sulfur isotope ratio measurements on a gas source mass spectrometer for hydrological, geological and environmental applications. SO/sub 2/ preparation procedure as described by Fumitaka Yanagisawa and Hitoshi Sakai (1983) is adopted with some modifications. A chemically pure BaSO/sub 4/ powder is chosen as PINSTECH Sulfur Standard PSS-I for routine laboratory /sup 34/S analysis. PSS-1 is calibrated against the International Atomic Energy Agency (IAEA) standard Cannon Diablo Troilite (CDT) using the NBS-127 sulfur standard Sigma /sup 34/S values of PSS-1 as analyzed at PINSTECH and Institute fur Hydorlogie, Munich are found to be 14.58 +-0.07 % CDT (n=6) and 14.59+-0.15% CDT (n=2) respectively. NBS-127 is BaSO/sub 4/ powder from the National Bureau of Standards, USA and has been calibrated against CDT. Interlaboratory comparison of various standards is also documented. Using this system, the reproducibility of sulfur isotope ratio measurements is better than +-0.2 % (n=10). (author)

  7. Fabrication of SO/sub 2/preparation system and calibration of PINSTECH sulfur standard for /sup 34/S/sup 32/S mass spectrometric analysis

    Energy Technology Data Exchange (ETDEWEB)

    Sajjad, M I; Latif, Z; Ali, M; Qureshi, R M; Tasneem, M A; Khan, I H; Ahmed, M; Ahmed, I

    1994-05-01

    This report describes the fabrication and standardization of operation procedures of a SO/sub 2/ preparation system used for the extraction of sulfur dioxide gas from sulfur minerals (aqueous sulfate, elemental sulfur, and sulfides) for sulfur isotope ratio measurements on a gas source mass spectrometer for hydrological, geological and environmental applications. SO/sub 2/ preparation procedure as described by Fumitaka Yanagisawa and Hitoshi Sakai (1983) is adopted with some modifications. A chemically pure BaSO/sub 4/ powder is chosen as PINSTECH Sulfur Standard PSS-I for routine laboratory /sup 34/S analysis. PSS-1 is calibrated against the International Atomic Energy Agency (IAEA) standard Cannon Diablo Troilite (CDT) using the NBS-127 sulfur standard Sigma /sup 34/S values of PSS-1 as analyzed at PINSTECH and Institute fur Hydorlogie, Munich are found to be 14.58 +-0.07 % CDT (n=6) and 14.59+-0.15% CDT (n=2) respectively. NBS-127 is BaSO/sub 4/ powder from the National Bureau of Standards, USA and has been calibrated against CDT. Interlaboratory comparison of various standards is also documented. Using this system, the reproducibility of sulfur isotope ratio measurements is better than +-0.2 % (n=10). (author).

  8. Air kerma standardization for diagnostic radiology, and requirements proposal for calibration laboratories; Padronizacao da grandeza Kerma no ar para radiodiagnostico e proposta de requisitos para laboratorios de calibracao

    Energy Technology Data Exchange (ETDEWEB)

    Ramos, Manoel Mattos Oliveira

    2009-07-01

    The demand for calibration services and quality control in diagnostic radiology has grown in the country since the publication of the governmental regulation 453, issued by the Ministry of Health in 1998. At that time, to produce results facing the new legislation, many laboratories used different standards and radiation qualities, some of which could be inadequate. The international standards neither supplied consistent radiation qualities and standardization for the different types of equipment available. This situation changed with the publication of the new edition of the IEC 61267 standard, published in 2005. A metrology network was created, but it is not yet accredited by the accreditation organism of the country, INMETRO. The objective of this work was to implement the standardization of the air kerma for the un attenuated qualities (RQR) of IEC 61267, and to develop a requirement proposal for instruments calibration laboratories. Results of interlaboratory comparisons demonstrate that the quantity is standardized and internationally traceable. A laboratory requirement proposal was finalized and it shall be submitted to INMETRO to be used as auxiliary normative document in laboratory accreditation. (author)

  9. International Union of Geological Sciences Subcommission on Geochronology recommendation for the standardization of fission track dating calibration and data reporting

    International Nuclear Information System (INIS)

    Hurford, A.J.

    1990-01-01

    Because of the difficulties of calibration in fission track (FT) dating over the last 20 yr, including uncertainty of the absolute λ f value, complexities of neutron dosimetry, complexities of neutron irradiation, correction factors necessary in some methodological procedures, and personal factors in track counting, the Working Group elected at the Cambridge ICOG meeting in 1986 recommended to FT workers meeting at the 6th International Fission Track Dating Workshop in Besancon on 9 September 1988, a uniform approach to system calibration, sample irradiation, calculation of FT age, and presentation of data. After discussion and modification, the recommendation was accepted. This modified recommendation is presented. (author)

  10. ORNL calibrations facility

    International Nuclear Information System (INIS)

    Berger, C.D.; Gupton, E.D.; Lane, B.H.; Miller, J.H.; Nichols, S.W.

    1982-08-01

    The ORNL Calibrations Facility is operated by the Instrumentation Group of the Industrial Safety and Applied Health Physics Division. Its primary purpose is to maintain radiation calibration standards for calibration of ORNL health physics instruments and personnel dosimeters. This report includes a discussion of the radioactive sources and ancillary equipment in use and a step-by-step procedure for calibration of those survey instruments and personnel dosimeters in routine use at ORNL

  11. Calibration of the modulation transfer function of surface profilometers with binary pseudo-random test standards: expanding the application range

    International Nuclear Information System (INIS)

    Yashchuk, Valeriy V.; Anderson, Erik H.; Barber, Samuel K.; Bouet, Nathalie; Cambie, Rossana; Conley, Raymond; McKinney, Wayne R.; Takacs, Peter Z.; Voronov, Dmitriy L.

    2011-01-01

    A modulation transfer function (MTF) calibration method based on binary pseudo-random (BPR) gratings and arrays (Proc. SPIE 7077-7 (2007), Opt. Eng. 47, 073602 (2008)) has been proven to be an effective MTF calibration method for a number of interferometric microscopes and a scatterometer (Nucl. Instr. and Meth. A616, 172 (2010)). Here we report on a further expansion of the application range of the method. We describe the MTF calibration of a 6 inch phase shifting Fizeau interferometer. Beyond providing a direct measurement of the interferometer's MTF, tests with a BPR array surface have revealed an asymmetry in the instrument's data processing algorithm that fundamentally limits its bandwidth. Moreover, the tests have illustrated the effects of the instrument's detrending and filtering procedures on power spectral density measurements. The details of the development of a BPR test sample suitable for calibration of scanning and transmission electron microscopes are also presented. Such a test sample is realized as a multilayer structure with the layer thicknesses of two materials corresponding to BPR sequence. The investigations confirm the universal character of the method that makes it applicable to a large variety of metrology instrumentation with spatial wavelength bandwidths from a few nanometers to hundreds of millimeters.

  12. FIELD-PRODUCED JP-8 STANDARD FOR CALIBRATION OF LOWER EXPLOSIVE LIMIT METERS USED BY JET FUEL TANK MAINTENANCE PERSONNEL

    Science.gov (United States)

    Thousands of military personnel and tens of thousands of civilian workers perform jet fuel tank entry procedures. Before entering the confined space of a jet fuel tank, OSHA regulations (29CFR1910.146) require the internal atmosphere be tested with a calibrated, direct-reading...

  13. Low-temperature thermometry. Use of a gas thermometer as a calibration standard between 4 and 300 K

    International Nuclear Information System (INIS)

    Combarieu, A. de

    1978-01-01

    A constant volume gas thermometer was built to calibrate the various secondary thermometers used at low temperature. This gas thermometer is placed in a cryostat where any stable temperature between 4 and 300 K may be obtained. After some words about low temperature thermometry, the gas thermometer and its auxiliary equipment are described briefly; the corrections to be applied to the results are given and the article ends with a table showing the values obtained [fr

  14. Standard Reference Line Combined with One-Point Calibration-Free Laser-Induced Breakdown Spectroscopy (CF-LIBS) to Quantitatively Analyze Stainless and Heat Resistant Steel.

    Science.gov (United States)

    Fu, Hongbo; Wang, Huadong; Jia, Junwei; Ni, Zhibo; Dong, Fengzhong

    2018-01-01

    Due to the influence of major elements' self-absorption, scarce observable spectral lines of trace elements, and relative efficiency correction of experimental system, accurate quantitative analysis with calibration-free laser-induced breakdown spectroscopy (CF-LIBS) is in fact not easy. In order to overcome these difficulties, standard reference line (SRL) combined with one-point calibration (OPC) is used to analyze six elements in three stainless-steel and five heat-resistant steel samples. The Stark broadening and Saha - Boltzmann plot of Fe are used to calculate the electron density and the plasma temperature, respectively. In the present work, we tested the original SRL method, the SRL with the OPC method, and intercept with the OPC method. The final calculation results show that the latter two methods can effectively improve the overall accuracy of quantitative analysis and the detection limits of trace elements.

  15. Establishing the standard X-ray beam qualities for calibration of dosimeters used in diagnostic radiology following IAEA-TRS457

    International Nuclear Information System (INIS)

    Duong Van Trieu; Ho Quang Tuan; Bui Duc Ky

    2014-01-01

    The determination of the patient dose needs to provide a reference dose for the patient that reference dose levels to assess the relative risk during X- ray diagnostic. This mission, We had established a number of standard beam qualities to perform calibrations of diagnostic dosimeters and methods of measuring patient dose in X-ray diagnostic. At radiation dosimetry room, we had establish RQR2, RQR3, RQR4, RQR5, RQR6 beam qualities based on IAEA-TRS457 documentation with homogeneity coefficient (h) for each beam quality in the range 0.7 - 0.8, and haft-value layers HVL1, HVL2 of experimental and IAEA is different about 10%. Established calibration method for diagnostic dosimeters as KAP meters, UNFORS dosimeters, and the TLD dosimeters, practical measurements of entrance surface air kerma on Shimadzu X-ray machines used phantom. (author)

  16. Reference standards for quantitative trace analysis of PCB's by GC. Technical PCB formulations for the calibration of ECD and MSD responses

    Energy Technology Data Exchange (ETDEWEB)

    Krupcik, J. (Slovak Technical Univ., Department of Analytical Chemistry, Bratislava (Slovakia)); Kocan, A. (Institute of Preventive Medicine, Bratislava (Slovakia)); Petrik, J. (Institute of Preventive Medicine, Bratislava (Slovakia)); Leclercq, P.A. (Eindhoven University of Technology, Dept. of Chemical Engineering, Lab. of Instrumental Analysis (Netherlands)); Ballschmiter, K. (University of Ulm, Dept. of Analytical and Environmental Chemistry (Germany))

    1993-04-01

    The composition of any technical PCB formulation can be determined directly by analyzing the PCB sample by gas chromatography with a flame ionization detector (GC-FID), provided the relative molecular masses of the components are known. The response of electron capture and selected-ion monitoring, mass-spectra detectors can then be calibrated for individual PCB congeners by correlation of the chromatographic patterns with those of concentrated PCB samples obtained by GC-FID. This procedure, which uses a given technical PCB formulation as a secondary reference standard mixture, is to be preferred over existing calibration methods, when results with [+-]10% errors are acceptable because commercial PCB formulations cover the whole range of chlorination products. (orig.)

  17. In-situ calibration of clinical built-in KAP meters with traceability to a primary standard using a reference KAP meter.

    Science.gov (United States)

    Malusek, A; Helmrot, E; Sandborg, M; Grindborg, J-E; Carlsson, G Alm

    2014-12-07

    The air kerma-area product (KAP) is used for settings of diagnostic reference levels. The International Atomic Energy Agency (IAEA) recommends that doses in diagnostic radiology (including the KAP values) be estimated with an accuracy of at least ± 7% (k = 2). Industry standards defined by the International Electrotechnical Commission (IEC) specify that the uncertainty of KAP meter measurements should be less than ± 25% (k = 2). Medical physicists willing to comply with the IAEA's recommendation need to apply correction factors to KAP values reported by x-ray units. The aim of this work is to present and evaluate a calibration method for built-in KAP meters on clinical x-ray units. The method is based on (i) a tandem calibration method, which uses a reference KAP meter calibrated to measure the incident radiation, (ii) measurements using an energy-independent ionization chamber to correct for the energy dependence of the reference KAP meter, and (iii) Monte Carlo simulations of the beam quality correction factors that correct for differences between beam qualities at a standard laboratory and the clinic. The method was applied to the KAP meter in a Siemens Aristos FX plus unit. It was found that values reported by the built-in KAP meter differed from the more accurate values measured by the reference KAP meter by more than 25% for high tube voltages (more than 140 kV) and heavily filtered beams (0.3 mm Cu). Associated uncertainties were too high to claim that the IEC's limit of 25% was exceeded. Nevertheless the differences were high enough to justify the need for a more accurate calibration of built-in KAP meters.

  18. A comparative uncertainty study of the calibration of macrolide antibiotic reference standards using quantitative nuclear magnetic resonance and mass balance methods

    International Nuclear Information System (INIS)

    Liu Shuyu; Hu Changqin

    2007-01-01

    This study introduces the general method of quantitative nuclear magnetic resonance (qNMR) for the calibration of reference standards of macrolide antibiotics. Several qNMR experimental conditions were optimized including delay, which is an important parameter of quantification. Three kinds of macrolide antibiotics were used to validate the accuracy of the qNMR method by comparison with the results obtained by the high performance liquid chromatography (HPLC) method. The purities of five common reference standards of macrolide antibiotics were measured by the 1 H qNMR method and the mass balance method, respectively. The analysis results of the two methods were compared. The qNMR is quick and simple to use. In a new medicine research and development process, qNMR provides a new and reliable method for purity analysis of the reference standard

  19. (60)Co in cast steel matrix: A European interlaboratory comparison for the characterisation of new activity standards for calibration of gamma-ray spectrometers in metallurgy.

    Science.gov (United States)

    Tzika, Faidra; Burda, Oleksiy; Hult, Mikael; Arnold, Dirk; Marroyo, Belén Caro; Dryák, Pavel; Fazio, Aldo; Ferreux, Laurent; García-Toraño, Eduardo; Javornik, Andrej; Klemola, Seppo; Luca, Aurelian; Moser, Hannah; Nečemer, Marijan; Peyrés, Virginia; Reis, Mario; Silva, Lidia; Šolc, Jaroslav; Svec, Anton; Tyminski, Zbigniew; Vodenik, Branko; Wätjen, Uwe

    2016-08-01

    Two series of activity standards of (60)Co in cast steel matrix, developed for the calibration of gamma-ray spectrometry systems in the metallurgical sector, were characterised using a European interlaboratory comparison among twelve National Metrology Institutes and one international organisation. The first standard, consisting of 14 disc shaped samples, was cast from steel contaminated during production ("originally"), and the second, consisting of 15 similar discs, from artificially-contaminated ("spiked") steel. The reference activity concentrations of (60)Co in the cast steel standards were (1.077±0.019) Bqg(-1) on 1 January 2013 12h00 UT and (1.483±0.022) Bqg(-1) on 1 June 2013 12h00 UT, respectively. Copyright © 2016 The Authors. Published by Elsevier Ltd.. All rights reserved.

  20. IAEA research coordination meeting on X- and gamma-ray standards for detector efficiency calibration, Braunschweig, FRG, 31 May - 2 June 1989. Summary report

    International Nuclear Information System (INIS)

    Christmas, P.; Nichols, A.L.; Lemmel, H.D.

    1989-07-01

    The final official meeting of the IAEA Coordinated Research Programme on the Measurement and Evaluation of X- and Gamma-ray Standards for Detector Efficiency Calibration was held in Braunschweig from 31 May to 2 June 1989. Work undertaken by the participants was reviewed in detail, and actions were agreed to resolve specific issues and problems. Initial steps were also made to establish a format and procedure for the preparation by mid-1990 of an IAEA Technical Reports Series booklet; the measurements and recommended data will be listed, and an IAEA data file established for issue to all interested organisations. (author). 3 tabs

  1. Critical issues for implementation of the standard NBR ISO/IEC 17025:2005 in Testing and Calibration Laboratory: case study at a public institution

    International Nuclear Information System (INIS)

    Castro, Denise Confar Carvalho de

    2013-01-01

    The public institution aims to promote excellence in public management to contribute to the quality of services provided to its customers and to increase competitiveness in the country, as well as its international projection. A technical barrier to trade that can lead to dissatisfaction and achieve the reputation of the institution is failing the test or calibration results and measurement data, thereby accreditation is regarded as the first essential step to facilitate the mutual acceptance of test results and calibration or measurement data. For recognition, laboratories need to demonstrate full compliance with both the sections of ISO/IEC 17025:2005, i.e. management and technical requirements. This research aims to discuss the critical aspects for implementation of ABNT NBR ISO / IEC 17025:2005 for calibration and testing of a Public Institution seeking accreditation of its laboratories with INMETRO, national accreditation body Laboratories. Besides getting preventive, corrective and improvement actions continues guidelines. Furthermore, the methodology used was to conduct a literature search and apply a questionnaire to identify the degree of agreement / disagreement of the foundations of the standard servers. Analysis of the results showed that the critical issues were: commitment, training, resources (infrastructure, human) and culture. (author)

  2. RF impedance measurement calibration

    International Nuclear Information System (INIS)

    Matthews, P.J.; Song, J.J.

    1993-01-01

    The intent of this note is not to explain all of the available calibration methods in detail. Instead, we will focus on the calibration methods of interest for RF impedance coupling measurements and attempt to explain: (1). The standards and measurements necessary for the various calibration techniques. (2). The advantages and disadvantages of each technique. (3). The mathematical manipulations that need to be applied to the measured standards and devices. (4). An outline of the steps needed for writing a calibration routine that operated from a remote computer. For further details of the various techniques presented in this note, the reader should consult the references

  3. Optical Path Length Calibration: A Standard Approach for Use in Absorption Cell-Based IR-Spectrometric Gas Analysis

    Directory of Open Access Journals (Sweden)

    Javis Anyangwe Nwaboh

    2014-01-01

    Full Text Available We employed a comparison method to determine the optical path length of gas cells which can be used in spectroscopic setup based on laser absorption spectroscopy or FTIR. The method is based on absorption spectroscopy itself. A reference gas cell, whose length is a priori known and desirably traceable to the international system of units (SI, and a gas mixture are used to calibrate the path length of a cell under test. By comparing spectra derived from pressure-dependent measurements on the two cells, the path length of the gas cell under test is determined. The method relies neither on the knowledge of the gas concentration nor on the line strength parameter of the probed transition which is very rarely traceable to the SI and of which the uncertainty is often relatively large. The method is flexible such that any infrared light source and infrared active molecule with isolated lines can be used. We elaborate on the method, substantiate the method by reporting results of this calibration procedure applied to multipass and single pass gas cells of lengths from 0.38 m to 21 m, and compare this to other methods. The relative combined uncertainty of the path length results determined using the comparison method was found to be in the ±0.4% range.

  4. Use of CRM's as mutual calibrating materials and control of synthetic multielement standards as used in INAA

    International Nuclear Information System (INIS)

    Rossbach, M.; Stoeppler, M.

    1986-01-01

    The comparability of analytical results from different laboratories requires accurately known concentrations in the applied standards. Dilution effects of different multielement synthetic standard solutions have been studied by measuring 10 - 12 different concentrations of the same solution. Peak area comparison of four Certified Reference Materials (CRM's) using one value for the evaluation of the other three repetitively led to the intercomparison (degree of compatibility) of the certified values. The idea of the preparation of each laboratory's ''secondary reference standard'' by comparison of synthetic multielement standards with as many CRM's as practically feasible is advocated to improve the reliability of analytical results. (author)

  5. Update of X ray and gamma ray decay data standards for detector calibration and other applications. V. 2: Data selection, assessment and evaluation procedures

    International Nuclear Information System (INIS)

    2007-05-01

    Various factors such as source preparation and source detector geometry may affect the quality of measurements made with intrinsic germanium and other γ ray spectrometers. However, the accuracy of such measurements invariably depends on the accuracy of the efficiency versus energy calibration curve and hence on the accuracy of the decay data for the radionuclides from which calibration standard sources are prepared. Both half-lives and X and γ ray emission probabilities need to be known to good accuracy. The recommendations and report of this work are published in two volumes: Volume 1 - Recommended Decay Data, High Energy Gamma Ray Standards and Angular Correlation Coefficients; Volume 2 - Data Selection, Assessment and Evaluation Procedures. Volume 1 is a self-contained assembly of the recommended decay data covering half-lives and the X ray and γ ray emission probabilities of the selected radionuclides, and listings of various high energy γ ray standards and a set of angular correlation coefficients; these data are presented in a concise manner for rapid and easy access. More detailed technical features of the CRP are described in Volume 2, including the evaluation procedures adopted and extensive traceable explanations of the origins of the nuclear data used to produce the recommended values listed in Volume 1. This detail was judged to be essential in order to record and demonstrate the quality of the resulting data files and allow the reader to trace the origins of the nuclear data used to determine the recommended values. All evaluations were based on the available experimental data, supplemented with the judicious use of well established theory. Three types of data (half-lives, energies and emission probabilities) were compiled and evaluated (Annex II). Consideration was also given to the adoption of a number of prompt high energy γ rays from specific nuclear reactions (Annex III), as well as to using the γ-γ coincidence technique for efficiency

  6. Use of CRM's as mutual calibrating materials and control of synthetic multielement standards as used in INAA

    International Nuclear Information System (INIS)

    Rossbach, M.; Stoeppler, M.

    1987-01-01

    Dilution effects of different multielement synthetic standard solutions were studied by measuring 10-12 different concentrations of the same solution. Peak area comparison of four Certified Reference Materials (CRMs) using one value for the evaluation of the other three repetitively led to the intercomparison (degree of compatibility) of the certified values. The idea of the preparation of each laboratory's 'secondary reference standard' by comparison of synthetic multielement standards with as many CRMs as practically feasible is advocated to improve the reliability of analytical results. (author)

  7. Electroluminescent TCC, C3dg and fB/Bb epitope assays for profiling complement cascade activation in vitro using an activated complement serum calibration standard.

    Science.gov (United States)

    van Vuuren, B Jansen; Bergseth, G; Mollnes, T E; Shaw, A M

    2014-01-15

    Electroluminescent assays for epitopes on the complement components C3dg, terminal complement complex (TCC) and factor B/Bb (fB/Bb) have been developed with capture and detection antibodies to produce detection limits C3dg=91±9ng/mL, TCC=3±0.1ng/mL and fB=55.7±0.1ng/mL. The assay performance was assessed against a series of zymosan and heat aggregated IgG (HAIgG) in vitro activations of complement using a calibrated activated complement serum (ACS) as calibration standard. The ACS standard was stable within 20% accuracy over a 6-month period with freeze-thaw cycles as required. Differential activation of the complement cascade was observed for TCC showing a pseudo-first order formation half-life of 3.5h after activation with zymosan. The C3dg activation fragment indicates a 10% total activation for both activation agents. The kinetic-epitope analysis for fB indicates that the capture epitope is on the fB/Bb protein fragment which can then become covered by the formation of C3bBb or C3bBbP complexes during the time course of the cascade. Copyright © 2013 Elsevier B.V. All rights reserved.

  8. Reference sources for the calibration of surface contamination monitors - Beta-emitters (maximum beta energy greater than MeV) and alpha-emitters (International Standard Publication ISO 8769:1988)

    International Nuclear Information System (INIS)

    Stefanik, J.

    2001-01-01

    This International Standard specifies the characteristics of reference sources of radioactive surface contamination, traceable to national measurement standards, for the calibration of surface contamination monitors. This International Standard relates to alpha-emitters and to beta-emitters of maximum beta energy greater than 0,15 MeV. It does not describe the procedures involved in the use of these reference sources for the calibration of surface contamination monitors. Such procedures are specified in IEC Publication 325 and other documents. This International Standard specifies reference radiations for the calibration of surface contamination monitors which take the form of adequately characterized large area sources specified, without exception, in terms of activity and surface emission rate, the evaluation of these quantities being traceable to national standards

  9. Advisory Committee for the calibration standards of ionizing radiation measurement. Section 1.- X and γ radiations, electrons

    International Nuclear Information System (INIS)

    1980-01-01

    Section I (Rayons X et γ, electrons) of the Comite Consultatif pour les Etalons de Mesure des Rayonnements Ionisants held its fifth meeting in May 1979. The members of the Section presented the work in progress in their respective laboratories; then they studied two documents describing the exposure measurements at BIPM and the conditions in which the comparisons are made. They also reviewed the exposure and absorbed dose comparisons performed at BIPM and elsewhere since 1977. New conditions of measurement were defined for the comparison of calorimeters in the BIPM 60 Co beam. Three working groups were set up to investigate the following problems: conversion from absorbed dose in graphite to absorbed dose in water, conversion from exposure to absorbed dose in water, and organization of an international comparison of Fricke chemical dosimeter systems. The growing importance of the radiation processing industry was stressed. Finally, the recent research work carried out at BIPM was presented and plans for the coming years were discussed. A recommendation was made concerning the study of calibrations in terms of absorbed dose in water [fr

  10. State-of-the art comparability of corrected emission spectra. 2. Field laboratory assessment of calibration performance using spectral fluorescence standards.

    Science.gov (United States)

    Resch-Genger, Ute; Bremser, Wolfram; Pfeifer, Dietmar; Spieles, Monika; Hoffmann, Angelika; DeRose, Paul C; Zwinkels, Joanne C; Gauthier, François; Ebert, Bernd; Taubert, R Dieter; Voigt, Jan; Hollandt, Jörg; Macdonald, Rainer

    2012-05-01

    In the second part of this two-part series on the state-of-the-art comparability of corrected emission spectra, we have extended this assessment to the broader community of fluorescence spectroscopists by involving 12 field laboratories that were randomly selected on the basis of their fluorescence measuring equipment. These laboratories performed a reference material (RM)-based fluorometer calibration with commercially available spectral fluorescence standards following a standard operating procedure that involved routine measurement conditions and the data evaluation software LINKCORR developed and provided by the Federal Institute for Materials Research and Testing (BAM). This instrument-specific emission correction curve was subsequently used for the determination of the corrected emission spectra of three test dyes, X, QS, and Y, revealing an average accuracy of 6.8% for the corrected emission spectra. This compares well with the relative standard uncertainties of 4.2% for physical standard-based spectral corrections demonstrated in the first part of this study (previous paper in this issue) involving an international group of four expert laboratories. The excellent comparability of the measurements of the field laboratories also demonstrates the effectiveness of RM-based correction procedures.

  11. The PROMIS Physical Function item bank was calibrated to a standardized metric and shown to improve measurement efficiency

    DEFF Research Database (Denmark)

    Rose, Matthias; Bjørner, Jakob; Gandek, Barbara

    2014-01-01

    OBJECTIVE: To document the development and psychometric evaluation of the Patient-Reported Outcomes Measurement Information System (PROMIS) Physical Function (PF) item bank and static instruments. STUDY DESIGN AND SETTING: The items were evaluated using qualitative and quantitative methods. A total...... response model was used to estimate item parameters, which were normed to a mean of 50 (standard deviation [SD]=10) in a US general population sample. RESULTS: The final bank consists of 124 PROMIS items covering upper, central, and lower extremity functions and instrumental activities of daily living...... to identify differences between age and disease groups. CONCLUSION: The item bank provides a common metric and can improve the measurement of PF by facilitating the standardization of patient-reported outcome measures and implementation of CATs for more efficient PF assessments over a larger range....

  12. Calibration of thermoluminiscent materials

    International Nuclear Information System (INIS)

    Bos, A.J.J.

    1989-07-01

    In this report the relation between exposure and absorbed radiation dose in various materials is represented, on the base of recent data. With the help of this a calibration procedure for thermoluminescent materials, adapted to the IRI radiation standard is still the exposure in rontgen. In switching to the air kerma standard the calibration procedure will have to be adapted. (author). 6 refs.; 4 tabs

  13. The energy calibration and precision of a gamma spectrometry unit - Method using the electron annihilation energy as the only standard

    International Nuclear Information System (INIS)

    Hoclet, Michel

    1971-06-01

    Spectrometry using Ge(Li) detectors is discussed. The excellent resolution of this type of detector, the mathematical analysis of the spectral lines of the pulses, and the reproducibility of the spectrometer enable highly accurate measurements of the abscises (some 10 -5 ) corresponding to the peaks. A method using the annihilation energy of the electron as the only standard was developed. The method is applied to the measurement of the gamma ray energies of the radioelements: 22 Na, 24 Na, 56 Mn, 56 Co, 59 Fe, 72 Ga, 88 Y, 122 Sb, 124 Sb and 137 Cs. (author) [fr

  14. The PROMIS Physical Function item bank was calibrated to a standardized metric and shown to improve measurement efficiency.

    Science.gov (United States)

    Rose, Matthias; Bjorner, Jakob B; Gandek, Barbara; Bruce, Bonnie; Fries, James F; Ware, John E

    2014-05-01

    To document the development and psychometric evaluation of the Patient-Reported Outcomes Measurement Information System (PROMIS) Physical Function (PF) item bank and static instruments. The items were evaluated using qualitative and quantitative methods. A total of 16,065 adults answered item subsets (n>2,200/item) on the Internet, with oversampling of the chronically ill. Classical test and item response theory methods were used to evaluate 149 PROMIS PF items plus 10 Short Form-36 and 20 Health Assessment Questionnaire-Disability Index items. A graded response model was used to estimate item parameters, which were normed to a mean of 50 (standard deviation [SD]=10) in a US general population sample. The final bank consists of 124 PROMIS items covering upper, central, and lower extremity functions and instrumental activities of daily living. In simulations, a 10-item computerized adaptive test (CAT) eliminated floor and decreased ceiling effects, achieving higher measurement precision than any comparable length static tool across four SDs of the measurement range. Improved psychometric properties were transferred to the CAT's superior ability to identify differences between age and disease groups. The item bank provides a common metric and can improve the measurement of PF by facilitating the standardization of patient-reported outcome measures and implementation of CATs for more efficient PF assessments over a larger range. Copyright © 2014. Published by Elsevier Inc.

  15. Dosemeter calibration in X-ray and in cobalt-60

    International Nuclear Information System (INIS)

    Silva, T.A. da

    1988-01-01

    Some tests about quality security for clinical dosemeter calibration in secondary standard dosimetry laboratory are described. The tests in gama calibration system, in X-ray calibration, in secondary standard dosimeter, in the dosemeter that will be calibrated, during the calibration and after the calibration are shown. (C.G.C.) [pt

  16. Quantitative analysis of phosphosilicate glass films on silicon wafers for calibration of x-ray fluorescence spectrometry standards

    International Nuclear Information System (INIS)

    Weissman, S.H.

    1983-01-01

    The phosphorus and silicon contents of phosphosilicate glass films deposited by chemical vapor deposition (CVD) on silicon wafers were determined. These films were prepared for use as x-ray fluorescence (XRF) spectrometry standards. The thin films were removed from the wafer by etching with dilute hydrofluoric acid, and the P and Si concentrations in solution were determined by inductively coupled plasma atomic emission spectroscopy (ICP). The calculated phosphorus concentration ranged from 2.2 to 12 wt %, with an uncertainty of 2.73 to 10.1 relative percent. Variation between the calculated weight loss (summation of P 2 O 5 and SiO 2 amounts as determined by ICP) and the measured weight loss (determined gravimetrically) averaged 4.9%. Results from the ICP method, Fourier transform-infrared spectroscopy (FT-IR), dispersive infrared spectroscopy, electron microprobe, and x-ray fluorescence spectroscopy for the same samples are compared

  17. The New LMK Primary Standard for Dew-Point Sensor Calibration: Evaluation of the High-Range Saturator Efficiency

    Science.gov (United States)

    Hudoklin, Domen; Drnovšek, Janko

    2008-10-01

    In the field of hygrometry, a primary dew-point standard can be realized according to several proven principles, such as single-pressure (1-P), two-pressure (2-P), or divided flow. Different realizations have been introduced by various national laboratories, each resulting in a stand-alone complex generation system. Recent trends in generator design favor the single-pressure principle without recirculation because it promises theoretically lower uncertainty and because it avoids problems regarding the leak tightness of the recirculation. Instead of recirculation, the efficiency of saturation, the key factor, is increased by preconditioning the inlet gas entering the saturator. For preconditioning, a presaturator or purifier is used to bring the dew point of the inlet stream close to the saturator temperature. The purpose of the paper is to identify the minimum requirements for the preconditioning system and the main saturator to assure efficient saturation for the LMK generator. Moreover, the aim is also to find out if the preconditioning system can be avoided despite the rather simple construction of the main saturator. If this proves to be the case, the generator design can be simplified while maintaining an accurate value of the generated dew point. Experiments were carried out within the scope of improving our existing primary generator in the above-ambient dew-point range up to +70°C. These results show the generated dew point is within the measurement uncertainty for any dew-point value of the inlet gas. Thus, the preconditioning subsystem can be avoided, which leads to a simplified generator design.

  18. Calibration-Free Laser-Induced Breakdown Spectroscopy (CF-LIBS) with Standard Reference Line for the Analysis of Stainless Steel.

    Science.gov (United States)

    Fu, Hongbo; Dong, Fengzhong; Wang, Huadong; Jia, Junwei; Ni, Zhibo

    2017-08-01

    In this work, calibration-free laser-induced breakdown spectroscopy (CF-LIBS) is used to analyze a certified stainless steel sample. Due to self-absorption of the spectral lines from the major element Fe and the sparse lines of trace elements, it is usually not easy to construct the Boltzmann plots of all species. A standard reference line method is proposed here to solve this difficulty under the assumption of local thermodynamic equilibrium so that the same temperature value for all elements present into the plasma can be considered. Based on the concentration and rich spectral lines of Fe, the Stark broadening of Fe(I) 381.584 nm and Saha-Boltzmann plots of this element are used to calculate the electron density and the plasma temperature, respectively. In order to determine the plasma temperature accurately, which is seriously affected by self-absorption, a pre-selection procedure for eliminating those spectral lines with strong self-absorption is employed. Then, one spectral line of each element is selected to calculate its corresponding concentration. The results from the standard reference lines with and without self-absorption of Fe are compared. This method allows us to measure trace element content and effectively avoid the adverse effects due to self-absorption.

  19. Observation models in radiocarbon calibration

    International Nuclear Information System (INIS)

    Jones, M.D.; Nicholls, G.K.

    2001-01-01

    The observation model underlying any calibration process dictates the precise mathematical details of the calibration calculations. Accordingly it is important that an appropriate observation model is used. Here this is illustrated with reference to the use of reservoir offsets where the standard calibration approach is based on a different model to that which the practitioners clearly believe is being applied. This sort of error can give rise to significantly erroneous calibration results. (author). 12 refs., 1 fig

  20. Sandia WIPP calibration traceability

    Energy Technology Data Exchange (ETDEWEB)

    Schuhen, M.D. [Sandia National Labs., Albuquerque, NM (United States); Dean, T.A. [RE/SPEC, Inc., Albuquerque, NM (United States)

    1996-05-01

    This report summarizes the work performed to establish calibration traceability for the instrumentation used by Sandia National Laboratories at the Waste Isolation Pilot Plant (WIPP) during testing from 1980-1985. Identifying the calibration traceability is an important part of establishing a pedigree for the data and is part of the qualification of existing data. In general, the requirement states that the calibration of Measuring and Test equipment must have a valid relationship to nationally recognized standards or the basis for the calibration must be documented. Sandia recognized that just establishing calibration traceability would not necessarily mean that all QA requirements were met during the certification of test instrumentation. To address this concern, the assessment was expanded to include various activities.

  1. Sandia WIPP calibration traceability

    International Nuclear Information System (INIS)

    Schuhen, M.D.; Dean, T.A.

    1996-05-01

    This report summarizes the work performed to establish calibration traceability for the instrumentation used by Sandia National Laboratories at the Waste Isolation Pilot Plant (WIPP) during testing from 1980-1985. Identifying the calibration traceability is an important part of establishing a pedigree for the data and is part of the qualification of existing data. In general, the requirement states that the calibration of Measuring and Test equipment must have a valid relationship to nationally recognized standards or the basis for the calibration must be documented. Sandia recognized that just establishing calibration traceability would not necessarily mean that all QA requirements were met during the certification of test instrumentation. To address this concern, the assessment was expanded to include various activities

  2. Calibration factor or calibration coefficient?

    International Nuclear Information System (INIS)

    Meghzifene, A.; Shortt, K.R.

    2002-01-01

    Full text: The IAEA/WHO network of SSDLs was set up in order to establish links between SSDL members and the international measurement system. At the end of 2001, there were 73 network members in 63 Member States. The SSDL network members provide calibration services to end-users at the national or regional level. The results of the calibrations are summarized in a document called calibration report or calibration certificate. The IAEA has been using the term calibration certificate and will continue using the same terminology. The most important information in a calibration certificate is a list of calibration factors and their related uncertainties that apply to the calibrated instrument for the well-defined irradiation and ambient conditions. The IAEA has recently decided to change the term calibration factor to calibration coefficient, to be fully in line with ISO [ISO 31-0], which recommends the use of the term coefficient when it links two quantities A and B (equation 1) that have different dimensions. The term factor should only be used for k when it is used to link the terms A and B that have the same dimensions A=k.B. However, in a typical calibration, an ion chamber is calibrated in terms of a physical quantity such as air kerma, dose to water, ambient dose equivalent, etc. If the chamber is calibrated together with its electrometer, then the calibration refers to the physical quantity to be measured per electrometer unit reading. In this case, the terms referred have different dimensions. The adoption by the Agency of the term coefficient to express the results of calibrations is consistent with the 'International vocabulary of basic and general terms in metrology' prepared jointly by the BIPM, IEC, ISO, OIML and other organizations. The BIPM has changed from factor to coefficient. The authors believe that this is more than just a matter of semantics and recommend that the SSDL network members adopt this change in terminology. (author)

  3. Calibration of farmer dosemeters

    International Nuclear Information System (INIS)

    Ahmad, S.S.; Anwar, K.; Arshed, W.; Mubarak, M.A.; Orfi, S.D.

    1984-08-01

    The Farmer Dosemeters of Atomic Energy Medical Centre (AEMC) Jamshoro were calibrated in the Secondary Standard Dosimetry Laboratory (SSDL) at PINSTECH, using the NPL Secondary Standard Therapy level X-ray exposure meter. The results are presented in this report. (authors)

  4. Lidar to lidar calibration

    DEFF Research Database (Denmark)

    Fernandez Garcia, Sergio; Villanueva, Héctor

    This report presents the result of the lidar to lidar calibration performed for ground-based lidar. Calibration is here understood as the establishment of a relation between the reference lidar wind speed measurements with measurement uncertainties provided by measurement standard and corresponding...... lidar wind speed indications with associated measurement uncertainties. The lidar calibration concerns the 10 minute mean wind speed measurements. The comparison of the lidar measurements of the wind direction with that from the reference lidar measurements are given for information only....

  5. Brief Report: Relationship Between ADOS-2, Module 4 Calibrated Severity Scores (CSS) and Social and Non-Social Standardized Assessment Measures in Adult Males with Autism Spectrum Disorder (ASD)

    Science.gov (United States)

    Morrier, Michael J.; Ousley, Opal Y.; Caceres-Gamundi, Gabriella A.; Segall, Matthew J.; Cubells, Joseph F.; Young, Larry J.; Andari, Elissar

    2017-01-01

    The ADOS-2 Modules 1-3 now include a standardized calibrated severity score (CSS) from 1 to 10 based on the overall total raw score. Subsequent research published CSS for Module 4 (Hus, Lord, "Journal of Autism and Developmental Disorders" 44(8):1996-2012, 2014); however more research is needed to examine the psychometric properties of…

  6. Standardization of the 24-hour diet recall calibration method used in the european prospective investigation into cancer and nutrition (EPIC): general concepts and preliminary results.

    Science.gov (United States)

    Slimani, N; Ferrari, P; Ocké, M; Welch, A; Boeing, H; Liere, M; Pala, V; Amiano, P; Lagiou, A; Mattisson, I; Stripp, C; Engeset, D; Charrondière, R; Buzzard, M; Staveren, W; Riboli, E

    2000-12-01

    Despite increasing interest in the concept of calibration in dietary surveys, there is still little experience in the use and standardization of a common reference dietary method, especially in international studies. In this paper, we present the general theoretical framework and the approaches developed to standardize the computer-assisted 24 h diet recall method (EPIC-SOFT) used to collect about 37 000 24-h dietary recall measurements (24-HDR) from the 10 countries participating in the European Prospective Investigation into Cancer and Nutrition (EPIC). In addition, an analysis of variance was performed to examine the level of standardization of EPIC-SOFT across the 90 interviewers involved in the study. The analysis of variance used a random effects model in which mean energy intake per interviewer was used as the dependent variable, while age, body mass index (BMI), energy requirement, week day, season, special diet, special day, physical activity and the EPIC-SOFT version were used as independent variables. The analysis was performed separately for men and women. The results show no statistical difference between interviewers in all countries for men and five out of eight countries for women, after adjustment for physical activity and the EPIC-SOFT program version used, and the exclusion of one interviewer in Germany (for men), and one in Denmark (for women). These results showed an interviewer effect in certain countries and a significant difference between gender, suggesting an underlying respondent's effect due to the higher under-reporting among women that was consistently observed in EPIC. However, the actual difference between interviewer and country mean energy intakes is about 10%. Furthermore, no statistical differences in mean energy intakes were observed across centres from the same country, except in Italy and Germany for men, and France and Spain for women, where the populations were recruited from areas scattered throughout the countries. Despite

  7. Primary calibration in acoustics metrology

    International Nuclear Information System (INIS)

    Milhomem, T A Bacelar; Soares, Z M Defilippo

    2015-01-01

    SI unit in acoustics is realized by the reciprocity calibrations of laboratory standard microphones in pressure field, free field and diffuse field. Calibrations in pressure field and in free field are already consolidated and the Inmetro already done them. Calibration in diffuse field is not yet consolidated, however, some national metrology institutes, including Inmetro, are conducting researches on this subject. This paper presents the reciprocity calibration, the results of Inmetro in recent key comparisons and the research that is being developed for the implementation of reciprocity calibration in diffuse field

  8. The use of a secondary standard x-ray exposure meter to calibrate a field instrument for use in output measurements

    International Nuclear Information System (INIS)

    1974-11-01

    It is stated that the recommended procedures have been closely correlated with ICRU Report 23 (1973), 'Measurements of absorbed dose in a phantom irradiated by a single beam of X- or gamma-rays'. The present report is contained in sections entitled: introduction; equipment and outline of procedures; calibration and use of field instrument in a phantom; calibration and use of the field instrument in air; local reference instrument; summary of recommended procedures. Appendices are entitled: the Perspex Intercomparison Phantom; the implications of applying an in-air calibration factor to readings made in a water phantom. (U.K.)

  9. SPOTS Calibration Example

    Directory of Open Access Journals (Sweden)

    Patterson E.

    2010-06-01

    Full Text Available The results are presented using the procedure outlined by the Standardisation Project for Optical Techniques of Strain measurement to calibrate a digital image correlation system. The process involves comparing the experimental data obtained with the optical measurement system to the theoretical values for a specially designed specimen. The standard states the criteria which must be met in order to achieve successful calibration, in addition to quantifying the measurement uncertainty in the system. The system was evaluated at three different displacement load levels, generating strain ranges from 289 µstrain to 2110 µstrain. At the 289 µstrain range, the calibration uncertainty was found to be 14.1 µstrain, and at the 2110 µstrain range it was found to be 28.9 µstrain. This calibration procedure was performed without painting a speckle pattern on the surface of the metal. Instead, the specimen surface was prepared using different grades of grit paper to produce the desired texture.

  10. Parameters influencing SPET regional brain uptake of technetium-99m hexamethylpropylene amine oxime measured by calibrated point sources as an external standard

    International Nuclear Information System (INIS)

    Dierckx, R.A.; Dobbeleir, A.; Maes, M.; Pickut, B.A.; Vervaet, A.; Deyn, P.P. de

    1994-01-01

    Using calibrated point sources as an external standard to convert SPET brain counts into absolute values of regional brain uptake (rBU) of technetium-99m hexamethylpropylene amine oxime (HMPAO), the relative contribution of different parameters to interindividual variability of cerebellar rBU was examined in 33 healthy volunteers. Stepwise regression analysis identified body surface as the most important factor underlying interindividual variability, when compared with brain volume. In the normal volunteer population presented, age decrement of rBU corrected for body surface and brain volume equalled 60.5-0.20xage. Based on the data of eight normal volunteers, including four test-retest studies with heart rate (HR) differences greater than 5 units and four test-stress studies with doubling of heart rate after bicycle exercise, influence of heart rate may be expressed by the equation ΔrBU = 0.35 ΔHR. Clinically, estimation of the relative influence of different factors allows normalization and extension of the applicability of the rBU quantification method used from longitudinal studies to group comparisons. Interestingly, results of the Daily Stress Inventory Scale and a subjective rating scale suggest the absence of a significant influence of minor stress on rBU. When using one vial per patient, chromatography may be omitted in clinical routine practice and lipophilicity may be estimated as 90% of the injected dose, if administered within 10 min after preparation. Finally, sensitivity of the quantification method was tested in eight volunteers using acetazolamide brain activation and showed a mean increase in cerebellar rBU of 30.2%, varying between 14.1% and 75.9%. (orig./MG)

  11. Standards for holdup measurement

    International Nuclear Information System (INIS)

    Zucker, M.S.

    1982-01-01

    Holdup measurement, needed for material balance, depend intensively on standards and on interpretation of the calibration procedure. More than other measurements, the calibration procedure using the standard becomes part of the standard. Standards practical for field use and calibration techniques have been developed. While accuracy in holdup measurements is comparatively poor, avoidance of bias is a necessary goal

  12. Comparative evaluations of surface contamination detectors calibration with radioactive sources - used in the Goiania accident, and standard sources; Estudo comparativo da calibracao dos monitores de contaminacao superficial com as fontes radiativas utilizadas durante o acidente de Goiania e com fontes padrao

    Energy Technology Data Exchange (ETDEWEB)

    Becker, P.H.B.; Marecha, M.H.H. [Instituto de Radioprotecao e Dosimetria (IRD), Rio de Janeiro, RJ (Brazil)

    1997-12-31

    The construction of Cs-137 standard flat sources for calibration of surface contamination detectors, used in the Goiania accident in 1987, is described and the procedures adopted are reported. At that time, standard sources were not available. Nowadays the Instituto de Radioprotecao e Dosimetria has standard sources acquired from Amersham which are used as calibration standards for surface contamination detectors. Comparative evaluations between the standard flat sources constructed for the accident and the calibrated ones are presented 6 refs., 1 fig., 4 tabs.; e-mail: pbecker at ird.gov.br; mhelena at ird. gov.br

  13. The influence of the calibration standard and the chemical composition of the water samples residue in the counting efficiency of proportional detectors for gross alpha and beta counting. Application on the radiologic control of the IPEN-CNEN/SP

    International Nuclear Information System (INIS)

    Santos, Cecilia Martins

    2003-01-01

    In this work the efficiency calibration curves of thin-window and low background gas-flow proportional counters were determined for calibration standards with different energies and different absorber thicknesses. For the gross alpha counting we have used 241 Am and natural uranium standards and for the gross beta counting we have used 90 Sr/ 90 Y and 137 Cs standards in residue thicknesses ranging from 0 to approximately 18 mg/cm 2 . These sample thicknesses were increased with a previously determined salted solution prepared simulating the chemical composition of the underground water of IPEN The counting efficiency for alpha emitters ranged from 0,273 +- 0,038 for a weightless residue to only 0,015 +- 0,002 in a planchet containing 15 mg/cm 2 of residue for 241 Am standard. For natural uranium standard the efficiency ranged from 0,322 +- 0,030 for a weightless residue to 0,023 +- 0,003 in a planchet containing 14,5 mg/cm 2 of residue. The counting efficiency for beta emitters ranged from 0,430 +- 0,036 for a weightless residue to 0,247 +- 0,020 in a planchet containing 17 mg/cm 2 of residue for 137 Cs standard. For 90 Sr/ 90 Y standard the efficiency ranged from 0,489 +- 0,041 for a weightless residue to 0,323 +- 0,026 in a planchet containing 18 mg/cm 2 of residue. Results make evident the counting efficiency variation with the alpha or beta emitters energies and the thickness of the water samples residue. So, the calibration standard, the thickness and the chemical composition of the residue must always be considered in the gross alpha and beta radioactivity determination in water samples. (author)

  14. Exposure-rate calibration using large-area calibration pads

    International Nuclear Information System (INIS)

    Novak, E.F.

    1988-09-01

    The US Department of Energy (DOE) Office of Remedial Action and Waste Technology established the Technical Measurements Center (TMC) at the DOE Grand Junction Projects Office (GJPO) in Grand Junction, Colorado, to standardize, calibrate, and compare measurements made in support of DOE remedial action programs. A set of large-area, radioelement-enriched concrete pads was constructed by the DOE in 1978 at the Walker Field Airport in Grand Junction for use as calibration standards for airborne gamma-ray spectrometer systems. The use of these pads was investigated by the TMC as potential calibration standards for portable scintillometers employed in measuring gamma-ray exposure rates at Uranium Mill Tailings Remedial Action (UMTRA) project sites. Data acquired on the pads using a pressurized ionization chamber (PIC) and three scintillometers are presented as an illustration of an instrumental calibration. Conclusions and recommended calibration procedures are discussed, based on the results of these data

  15. Calibration bench of flowmeters

    International Nuclear Information System (INIS)

    Bremond, J.; Da Costa, D.; Calvet, A.; Vieuxmaire, C.

    1966-01-01

    This equipment is devoted to the comparison of signals from two turbines installed in the Cabri experimental loop. The signal is compared to the standard turbine. The characteristics and the performance of the calibration bench are presented. (A.L.B.)

  16. NVLAP calibration laboratory program

    Energy Technology Data Exchange (ETDEWEB)

    Cigler, J.L.

    1993-12-31

    This paper presents an overview of the progress up to April 1993 in the development of the Calibration Laboratories Accreditation Program within the framework of the National Voluntary Laboratory Accreditation Program (NVLAP) at the National Institute of Standards and Technology (NIST).

  17. NVLAP calibration laboratory program

    International Nuclear Information System (INIS)

    Cigler, J.L.

    1993-01-01

    This paper presents an overview of the progress up to April 1993 in the development of the Calibration Laboratories Accreditation Program within the framework of the National Voluntary Laboratory Accreditation Program (NVLAP) at the National Institute of Standards and Technology (NIST)

  18. Calibration and uncertainty in electromagnetic fields measuring methods

    International Nuclear Information System (INIS)

    Anglesio, L.; Crotti, G.; Borsero, M.; Vizio, G.

    1999-01-01

    Calibration and reliability in electromagnetic field measuring methods are assured by calibration of measuring instruments. In this work are illustrated systems for generation of electromagnetic fields at low and high frequency, calibration standard and accuracy [it

  19. Radiation Calibration Measurements

    International Nuclear Information System (INIS)

    Omondi, C.

    2017-01-01

    KEBS Radiation Dosimetry mandate are: Custodian of Kenya Standards on Ionizing radiation, Ensure traceability to International System (SI ) and Calibration radiation equipment. RAF 8/040 on Radioisotope applications for troubleshooting and optimizing industrial process established Radiotracer Laboratory objective is to introduce and implement radiotracer technique for problem solving of industrial challenges. Gamma ray scanning technique applied is to Locate blockages, Locate liquid in vapor lines, Locate areas of lost refractory or lining in a pipe and Measure flowing densities. Equipment used for diagnostic and radiation protection must be calibrated to ensure Accuracy and Traceability

  20. Calibration of nuclear medicine gamma counters

    International Nuclear Information System (INIS)

    Orlic, M.; Spasic-Jokic, V.; Jovanovic, M.; Vranjes, S. . E-mail address of corresponding author: morlic@vin.bg.ac.yu; Orlic, M.)

    2005-01-01

    In this paper the practical problem of nuclear medicine gamma counters calibration has been solved by using dose calibrators CRC-15R with standard error ±5%. The samples from technetium generators have been measured both by dose calibrators CRC-15R and gamma counter ICN Gamma 3.33 taking into account decay correction. Only the linear part of the curve has practical meaning. The advantage of this procedure satisfies the requirements from international standards: the calibration of sources used for medical exposure be traceable to a standard dosimetry laboratory and radiopharmaceuticals for nuclear medicine procedures be calibrated in terms of activity of the radiopharmaceutical to be administered. (author)

  1. Development of portable flow calibrator

    International Nuclear Information System (INIS)

    Akiyama, Kiyomitsu; Iijima, Nobuo

    1995-01-01

    In the nuclear facilities, air sniffer system is often utilized to evaluate atmospheric concentration of radioactivity in the working environment. The system collects airborne dust on the filter during some sampling period. In this method, total air flow during the sampling period is an important parameter to evaluate the radioactivity concentration correctly. Therefore, calibration for the flow meter of air sniffer system must be done periodically according to Japan Industry Standards (JIS). As we have had to available device to calibrate the flow meter in the working area, we had to remove the flow meters from the installed place and carry them to another place where calibration can be made. This work required a great deal of labor. Now we have developed a portable flow calibrator for air sniffer system which enables us to make in-site calibration of the flow meter in the working area more easily. This report describes the outline of portable flow calibrator and it's experimental results. (author)

  2. Physiotherapy ultrasound calibrations

    International Nuclear Information System (INIS)

    Gledhill, M.

    1996-01-01

    Calibration of physiotherapy ultrasound equipment has long been a problem. Numerous surveys around the world over the past 20 years have all found that only a low percentage of the units tested had an output within 30% of that indicatd. In New Zealand, a survey carried out by the NRL in 1985 found that only 24% had an output, at the maximum setting, within + or - 20% of that indicated. The present performance Standard for new equipment (NZS 3200.2.5:1992) requires that the measured output should not deviate from that indicated by more than + or - 30 %. This may be tightened to + or - 20% in the next few years. Any calibration is only as good as the calibration equipment. Some force balances can be tested with small weights to simulate the force exerted by an ultrasound beam, but with others this is not possible. For such balances, testing may only be feasible with a calibrated source which could be used like a transfer standard. (author). 4 refs., 3 figs

  3. Recommended inorganic chemicals for calibration

    International Nuclear Information System (INIS)

    Moody, J.R.; Greenberg, R.R.; Pratt, K.W.; Rains, T.C.

    1988-01-01

    All analytical techniques depend on the use of calibration chemicals to relate analyte concentration to an instrumental parameter. A fundamental component in the preparation of calibration solutions is the weighing of a pure chemical or metal before preparing a solution standard. The analyst must be assured that the purity, stoichiometry, and assay of the chemical are known. These terms have different meanings, and each has an important influence. This report is intended to assist the analyst in the selection and use of chemical standards for instrumental calibration. Purity, stoichiometry, and preparation of solutions for different purposes are discussed, and a critical evaluation of the best materials available for each element is presented for use in preparing solutions or calibration standards. Information on the chemical form, source, purity, drying, and appropriate precautions is given. In some cases, multiple sources or chemical forms are available. Certain radioactive elements, the transuranic elements, and the noble gases are not considered

  4. Quality control of the NPL-CRC secondary standard system used for activimeters calibration at IPEN, Sao Paulo, Brazil;Ccontrole de qualidade do sistema padrao secundario NPL-CRC utilizado na calibracao de ativimetros no IPEN

    Energy Technology Data Exchange (ETDEWEB)

    Martins, Elaine W.; Potiens, Maria da P.A. [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2009-07-01

    The objective of this study was to establish a quality control program to be applied at the NPL-CRC activimeter secondary standard system, used as reference to comparison in tests made with the work tertiary standard activimeter, Capintec basic CRC{sup R}-15BT, both belonging to the Calibration Laboratory of IPEN. The repeatability, reproducibility and the precision tests were performed using a sealed check source of {sup 133}Ba, from Amersham. It was made 70 series of 10 measurements to each activimeter, totaling 1400 measurements. Considering the variation limit of 5% to precision and reproducibility tests in the nuclear medicine services, recommended by the Brazilian standard CNEN-NN-3.05, the results observed in the behavior of the IPEN activimeter were satisfactory. (author)

  5. POLCAL - POLARIMETRIC RADAR CALIBRATION

    Science.gov (United States)

    Vanzyl, J.

    1994-01-01

    Calibration of polarimetric radar systems is a field of research in which great progress has been made over the last few years. POLCAL (Polarimetric Radar Calibration) is a software tool intended to assist in the calibration of Synthetic Aperture Radar (SAR) systems. In particular, POLCAL calibrates Stokes matrix format data produced as the standard product by the NASA/Jet Propulsion Laboratory (JPL) airborne imaging synthetic aperture radar (AIRSAR). POLCAL was designed to be used in conjunction with data collected by the NASA/JPL AIRSAR system. AIRSAR is a multifrequency (6 cm, 24 cm, and 68 cm wavelength), fully polarimetric SAR system which produces 12 x 12 km imagery at 10 m resolution. AIRSTAR was designed as a testbed for NASA's Spaceborne Imaging Radar program. While the images produced after 1991 are thought to be calibrated (phase calibrated, cross-talk removed, channel imbalance removed, and absolutely calibrated), POLCAL can and should still be used to check the accuracy of the calibration and to correct it if necessary. Version 4.0 of POLCAL is an upgrade of POLCAL version 2.0 released to AIRSAR investigators in June, 1990. New options in version 4.0 include automatic absolute calibration of 89/90 data, distributed target analysis, calibration of nearby scenes with calibration parameters from a scene with corner reflectors, altitude or roll angle corrections, and calibration of errors introduced by known topography. Many sources of error can lead to false conclusions about the nature of scatterers on the surface. Errors in the phase relationship between polarization channels result in incorrect synthesis of polarization states. Cross-talk, caused by imperfections in the radar antenna itself, can also lead to error. POLCAL reduces cross-talk and corrects phase calibration without the use of ground calibration equipment. Removing the antenna patterns during SAR processing also forms a very important part of the calibration of SAR data. Errors in the

  6. Technical guidelines for personnel dosimetry calibrations

    International Nuclear Information System (INIS)

    Roberson, P.L.; Fox, R.A.; Hadley, R.T.; Holbrook, K.L.; Hooker, C.D.; McDonald, J.C.

    1983-01-01

    A base of technical information has been acquire and used to evaluate the calibration, design, and performance of selected personnel systems in use at Department of Energy (DOE) facilites. A technical document was prepared to guide DOE and DOE contractors in selecting and evaluating personnel dosimetry systems and calibration. A parallel effort was initiated to intercompare the adiological calibrations standards used to calibrate DOE personnel dosimeters

  7. Mercury CEM Calibration

    Energy Technology Data Exchange (ETDEWEB)

    John F. Schabron; Joseph F. Rovani; Susan S. Sorini

    2007-03-31

    The Clean Air Mercury Rule (CAMR) which was published in the Federal Register on May 18, 2005, requires that calibration of mercury continuous emissions monitors (CEMs) be performed with NIST-traceable standards. Western Research Institute (WRI) is working closely with the Electric Power Research Institute (EPRI), the National Institute of Standards and Technology (NIST), and the Environmental Protection Agency (EPA) to facilitate the development of the experimental criteria for a NIST traceability protocol for dynamic elemental mercury vapor generators. The traceability protocol will be written by EPA. Traceability will be based on the actual analysis of the output of each calibration unit at several concentration levels ranging from about 2-40 ug/m{sup 3}, and this analysis will be directly traceable to analyses by NIST using isotope dilution inductively coupled plasma/mass spectrometry (ID ICP/MS) through a chain of analyses linking the calibration unit in the power plant to the NIST ID ICP/MS. Prior to this project, NIST did not provide a recommended mercury vapor pressure equation or list mercury vapor pressure in its vapor pressure database. The NIST Physical and Chemical Properties Division in Boulder, Colorado was subcontracted under this project to study the issue in detail and to recommend a mercury vapor pressure equation that the vendors of mercury vapor pressure calibration units can use to calculate the elemental mercury vapor concentration in an equilibrium chamber at a particular temperature. As part of this study, a preliminary evaluation of calibration units from five vendors was made. The work was performed by NIST in Gaithersburg, MD and Joe Rovani from WRI who traveled to NIST as a Visiting Scientist.

  8. British Association for the Study of Community Dentistry (BASCD) guidance on the statistical aspects of training and calibration of examiners for surveys of child dental health. A BASCD coordinated dental epidemiology programme quality standard.

    Science.gov (United States)

    Pine, C M; Pitts, N B; Nugent, Z J

    1997-03-01

    The British Association for the Study of Community Dentistry (BASCD) is responsible for the coordination of locally based surveys of child dental health which permit local and national comparisons between health authorities and regions. These surveys began in 1985/86 in England and Wales, 1987/88 in Scotland and 1993/94 in Northern Ireland. BASCD has taken an increasing lead in setting quality standards in discussion with the NHS Epidemiology Coordinators of the Dental Epidemiology Programme. This paper comprises guidance on the statistical aspects of training and calibration of examiners for these surveys.

  9. Liquid Krypton Calorimeter Calibration Software

    CERN Document Server

    Hughes, Christina Lindsay

    2013-01-01

    Calibration of the liquid krypton calorimeter (LKr) of the NA62 experiment is managed by a set of standalone programs, or an online calibration driver. These programs are similar to those used by NA48, but have been updated to utilize classes and translated to C++ while maintaining a common functionality. A set of classes developed to handle communication with hardware was used to develop the three standalone programs as well as the main driver program for online calibration between bursts. The main calibration driver has been designed to respond to run control commands and receive burst data, both transmitted via DIM. In order to facilitate the process of reading in calibration parameters, a serializable class has been introduced, allowing the replacement of standard text files with XML configuration files.

  10. Calibrating Legal Judgments

    Directory of Open Access Journals (Sweden)

    Frederick Schauer

    2017-09-01

    Full Text Available Objective to study the notion and essence of legal judgments calibration the possibilities of using it in the lawenforcement activity to explore the expenses and advantages of using it. Methods dialectic approach to the cognition of social phenomena which enables to analyze them in historical development and functioning in the context of the integrity of objective and subjective factors it determined the choice of the following research methods formallegal comparative legal sociological methods of cognitive psychology and philosophy. Results In ordinary life people who assess other peoplersaquos judgments typically take into account the other judgments of those they are assessing in order to calibrate the judgment presently being assessed. The restaurant and hotel rating website TripAdvisor is exemplary because it facilitates calibration by providing access to a raterrsaquos previous ratings. Such information allows a user to see whether a particular rating comes from a rater who is enthusiastic about every place she patronizes or instead from someone who is incessantly hard to please. And even when less systematized as in assessing a letter of recommendation or college transcript calibration by recourse to the decisional history of those whose judgments are being assessed is ubiquitous. Yet despite the ubiquity and utility of such calibration the legal system seems perversely to reject it. Appellate courts do not openly adjust their standard of review based on the previous judgments of the judge whose decision they are reviewing nor do judges in reviewing legislative or administrative decisions magistrates in evaluating search warrant representations or jurors in assessing witness perception. In most legal domains calibration by reference to the prior decisions of the reviewee is invisible either because it does not exist or because reviewing bodies are unwilling to admit using what they in fact know and employ. Scientific novelty for the first

  11. Mercury Continuous Emmission Monitor Calibration

    Energy Technology Data Exchange (ETDEWEB)

    John Schabron; Eric Kalberer; Ryan Boysen; William Schuster; Joseph Rovani

    2009-03-12

    Mercury continuous emissions monitoring systems (CEMs) are being implemented in over 800 coal-fired power plant stacks throughput the U.S. Western Research Institute (WRI) is working closely with the Electric Power Research Institute (EPRI), the National Institute of Standards and Technology (NIST), and the Environmental Protection Agency (EPA) to facilitate the development of the experimental criteria for a NIST traceability protocol for dynamic elemental mercury vapor calibrators/generators. These devices are used to calibrate mercury CEMs at power plant sites. The Clean Air Mercury Rule (CAMR) which was published in the Federal Register on May 18, 2005 and vacated by a Federal appeals court in early 2008 required that calibration be performed with NIST-traceable standards. Despite the vacature, mercury emissions regulations in the future will require NIST traceable calibration standards, and EPA does not want to interrupt the effort towards developing NIST traceability protocols. The traceability procedures will be defined by EPA. An initial draft traceability protocol was issued by EPA in May 2007 for comment. In August 2007, EPA issued a conceptual interim traceability protocol for elemental mercury calibrators. The protocol is based on the actual analysis of the output of each calibration unit at several concentration levels ranging initially from about 2-40 {micro}g/m{sup 3} elemental mercury, and in the future down to 0.2 {micro}g/m{sup 3}, and this analysis will be directly traceable to analyses by NIST. The EPA traceability protocol document is divided into two separate sections. The first deals with the qualification of calibrator models by the vendors for use in mercury CEM calibration. The second describes the procedure that the vendors must use to certify the calibrators that meet the qualification specifications. The NIST traceable certification is performance based, traceable to analysis using isotope dilution inductively coupled plasma

  12. An empirical calibration for 4He quantification in minerals and rocks by laser fusion and noble gas mass spectrometry using Cerro de Mercado (Durango, Mexico) fluorapatite as a standard

    International Nuclear Information System (INIS)

    Sole, Jesus; Pi, Teresa

    2005-01-01

    An empirical calibration with a natural mineral standard (fluorapatite from Cerro de Mercado, Mexico) is proposed as a method to determine the 4 He concentration of mineral and rock samples. The procedure is based on the fusion of several aliquots of the fluorapatite standard with a well-spaced weight distribution in order to obtain a good correlation in coordinates of 4 He peak height versus fluorapatite weight. The weight is then converted to moles using the accepted mineral age (31.4 Ma) and appropriate formula. Experimental peak height of 4 He for the unknown samples are converted to moles with the regression determined for fluorapatite. The procedure is fast and inexpensive, and both precision and accuracy are always below 10% and usually about 3-5%

  13. Automated Calibration of Dosimeters for Diagnostic Radiology

    International Nuclear Information System (INIS)

    Romero Acosta, A.; Gutierrez Lores, S.

    2015-01-01

    Calibration of dosimeters for diagnostic radiology includes current and charge measurements, which are often repetitive. However, these measurements are usually done using modern electrometers, which are equipped with an RS-232 interface that enables instrument control from a computer. This paper presents an automated system aimed to the measurements for the calibration of dosimeters used in diagnostic radiology. A software application was developed, in order to achieve the acquisition of the electric charge readings, measured values of the monitor chamber, calculation of the calibration coefficient and issue of a calibration certificate. A primary data record file is filled and stored in the computer hard disk. The calibration method used was calibration by substitution. With this system, a better control over the calibration process is achieved and the need for human intervention is reduced. the automated system will be used in the calibration of dosimeters for diagnostic radiology at the Cuban Secondary Standard Dosimetry Laboratory of the Center for Radiation Protection and Hygiene. (Author)

  14. Calibration of photon and beta ray sources used in brachytherapy. Guidelines on standardized procedures at Secondary Standards Dosimetry Laboratories; Calibracion de fuentes de fotones y rayos beta usadas en braquiterapia. Guia de procedimiento estandarizados en Laboratorios Secundarios de Calibracion Dosimetrica (LSCD) y en hospitales

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2004-03-01

    It has generally been recognized that international harmonization in radiotherapy dosimetry is essential. Consequently, the IAEA has given much effort to this, for example by publishing a number of reports in the Technical Reports Series (TRS) for external beam dosimetry, most notably TRS-277 and more recently TRS-398. Both of these reports describe in detail the steps to be taken for absorbed dose determination in water and they are often referred to as 'dosimetry protocols'. Similar to TRS-277, it is expected that TRS-398 will be adopted or used as a model by a large number of countries as their national protocol. In 1996, the IAEA established a calibration service for low dose rate (LDR) 137 Cs brachytherapy sources, which is the most widely used source for treatment of gynecological cancer. To further enhance harmonization in brachytherapy dosimetry, the IAEA published in 1999 IAEA-TECDOC-1079 entitled 'Calibration of Brachytherapy Sources. Guidelines on Standardized Procedures for the Calibration of Brachytherapy Sources at Secondary Standard Dosimetry Laboratories (SSDLs) and Hospitals'. The report was well received and was distributed in a large number of copies to the members of the IAEA/WHO network of SSDLs and to medical physicists working with brachytherapy. The present report is an update of the aforementioned TECDOC. Whereas TECDOC-1079 described methods for calibrating brachytherapy sources with photon energies at or above those of {sup 192}Ir, the current report has a wider scope in that it deals with standardization of calibration of all the most commonly used brachytherapy sources, including both photon and beta emitting sources. The latter sources have been in use for a few decades already, but their calibration methods have been unclear. Methods are also described for calibrating sources used in the rapidly growing field of cardiovascular angioplasty. In this application, irradiation of the vessel wall is done in an attempt to prevent restenosis

  15. Tests with different kind of k Vp-meters in standard X-rays beams used for instruments calibration, in diagnostic radiology level

    International Nuclear Information System (INIS)

    Lucena, Rodrigo Ferreira de; Potiens, Maria da Penha A.; Caldas, Linda V. E.; Vivolo, Vitor

    2008-01-01

    In this work, tests were carried out in one X-ray system, Medicor Moevek Roentgengyara, Model Neo-Diagnomax, (single-phase, full wave rectified) that operate in the range from 40 kV to 100 kV, and fixed 6 mA in the fluoroscopic mode, with total filtration of 2.5 mmAl. It was used as reference system an invasive system from Radcal, model Dynalyzer III (trade mark). The equipment tested were three non-invasive instruments, one PTW,model Diavolt (trade mark), and two Victoreen, model NERO (trade mark). It was performed measurements with those equipment, in the range from 50 kV to 100 kV, in steps of 10 kV and current of 6 mA (fixed). The quantity measured was kVp max . The results showed the maximum variation of 3 % for one NERO (trade mark) and 1 % for the other equipment of the same type, and 0,3 % for Diavolt (trade mark) related to the invasive reference measurement system. The differences in the obtained values could be caused by the different kind of equipment used in that, their manufacturer calibration and aged. (author)

  16. Ørsted Pre-Flight Magnetometer Calibration Mission

    DEFF Research Database (Denmark)

    Risbo, T.; Brauer, Peter; Merayo, José M.G.

    2003-01-01

    and the overall calibration results are given. The temperature calibrations are explained and reported on. The overall calibration model standard deviation is about 100 pT rms. Comparisons with the later in-flight calibrations show that, except for the unknown satellite offsets, an agreement within 4 n...

  17. Calibrating Fundamental British Values: How Head Teachers Are Approaching Appraisal in the Light of the Teachers' Standards 2012, Prevent and the Counter-Terrorism and Security Act, 2015

    Science.gov (United States)

    Revell, Lynn; Bryan, Hazel

    2016-01-01

    In requiring that teachers should "not undermine fundamental British values (FBV)," a phrase originally articulated in the Home Office counter-terrorism document, Prevent, the Teachers' Standards has brought into focus the nature of teacher professionalism. Teachers in England are now required to promote FBV within and outside school,…

  18. Laboratory implantation for well type ionization chambers calibration

    International Nuclear Information System (INIS)

    Vianello, E.A.; Dias, D.J.; Almeida, C.E. de

    1998-01-01

    The Radiological Science Laboratory is implanting a service for calibration of well type chambers by IAEA training program. The kerma rate in the air (mu Gy/h) of the linear Cs-137 reference source CDCS-J4 have been determined using a well type chamber Standard Imaging HDR-1000 model, which have been calibrated at Secondary Standard Laboratory Calibration of IAEA, whereas two HDR-1000 Plus chambers were calibrated too, following the same standards. The results were compared with Wisconsin University calibration certification and has demonstrated that well type ionization chamber calibration can be used in brachytherapy for several kinds of radionuclides. (Author)

  19. NIST display colorimeter calibration facility

    Science.gov (United States)

    Brown, Steven W.; Ohno, Yoshihiro

    2003-07-01

    A facility has been developed at the National Institute of Standards and Technology (NIST) to provide calibration services for color-measuring instruments to address the need for improving and certifying the measurement uncertainties of this type of instrument. While NIST has active programs in photometry, flat panel display metrology, and color and appearance measurements, these are the first services offered by NIST tailored to color-measuring instruments for displays. An overview of the facility, the calibration approach, and associated uncertainties are presented. Details of a new tunable colorimetric source and the development of new transfer standard instruments are discussed.

  20. Solid laboratory calibration of a nonimaging spectroradiometer.

    Science.gov (United States)

    Schaepman, M E; Dangel, S

    2000-07-20

    Field-based nonimaging spectroradiometers are often used in vicarious calibration experiments for airborne or spaceborne imaging spectrometers. The calibration uncertainties associated with these ground measurements contribute substantially to the overall modeling error in radiance- or reflectance-based vicarious calibration experiments. Because of limitations in the radiometric stability of compact field spectroradiometers, vicarious calibration experiments are based primarily on reflectance measurements rather than on radiance measurements. To characterize the overall uncertainty of radiance-based approaches and assess the sources of uncertainty, we carried out a full laboratory calibration. This laboratory calibration of a nonimaging spectroradiometer is based on a measurement plan targeted at achieving a calibration. The individual calibration steps include characterization of the signal-to-noise ratio, the noise equivalent signal, the dark current, the wavelength calibration, the spectral sampling interval, the nonlinearity, directional and positional effects, the spectral scattering, the field of view, the polarization, the size-of-source effects, and the temperature dependence of a particular instrument. The traceability of the radiance calibration is established to a secondary National Institute of Standards and Technology calibration standard by use of a 95% confidence interval and results in an uncertainty of less than ?7.1% for all spectroradiometer bands.

  1. Individual dosimetry and calibration

    International Nuclear Information System (INIS)

    Otto, T.

    1997-01-01

    In 1996, the Dosimetry and Calibration Section was, as in previous years, mainly engaged in routine tasks: the distribution of over 6000 dosimeters (with a total of more than 10,000 films) every two months and the calibration of about 900 fixed and mobile instruments used in the radiation survey sections of RP group. These tasks were, thanks to an experienced team, well mastered. Special efforts had to be made in a number of areas to modernize the service or to keep it in line with new prescriptions. The Individual Dosimetry Service had to assure that CERN's contracting firms comply with the prescriptions in the Radiation Safety Manual (1996) that had been inspired by the Swiss Ordinance of 1994: Companies must file for authorizations with the Swiss Federal Office for Public Health requiring that in every company an 'Expert in Radiation Protection' be nominated and subsequently trained. CERN's Individual Dosimetry Service is accredited by the Swiss Federal Authorities and works closely together with other, similar services on a rigorous quality assurance programme. Within this framework, CERN was mandated to organize this year the annual Swiss 'Intercomparison of Dosimeters'. All ten accredited dosimetry services - among others those of the Paul Scherrer Institute (PSI) in Villigen and of the four Swiss nuclear power stations - sent dosimeters to CERN, where they were irradiated in CERN's calibration facility with precise photon doses. After return to their origin they were processed and evaluated. The results were communicated to CERN and were compared with the originally given doses. A report on the results was subsequently prepared and submitted to the Swiss 'Group of Experts on Personal Dosimetry'. Reference monitors for photon and neutron radiation were brought to standard laboratories to assure the traceability of CERN's calibration service to the fundamental quantities. For photon radiation, a set of ionization chambers was calibrated in the reference field

  2. Automatic calibration of gamma spectrometers

    International Nuclear Information System (INIS)

    Tluchor, D.; Jiranek, V.

    1989-01-01

    The principle is described of energy calibration of the spectrometric path based on the measurement of the standard of one radionuclide or a set of them. The entire computer-aided process is divided into three main steps, viz.: the insertion of the calibration standard by the operator; the start of the calibration program; energy calibration by the computer. The program was selected such that the spectrum identification should not depend on adjustment of the digital or analog elements of the gamma spectrometric measuring path. The ECL program is described for automatic energy calibration as is its control, the organization of data file ECL.DAT and the necessary hardware support. The computer-multichannel analyzer communication was provided using an interface pair of Canberra 8673V and Canberra 8573 operating in the RS-422 standard. All subroutines for communication with the multichannel analyzer were written in MACRO 11 while the main program and the other subroutines were written in FORTRAN-77. (E.J.). 1 tab., 4 refs

  3. An expanded calibration study of the explicitly correlated CCSD(T)-F12b method using large basis set standard CCSD(T) atomization energies.

    Science.gov (United States)

    Feller, David; Peterson, Kirk A

    2013-08-28

    The effectiveness of the recently developed, explicitly correlated coupled cluster method CCSD(T)-F12b is examined in terms of its ability to reproduce atomization energies derived from complete basis set extrapolations of standard CCSD(T). Most of the standard method findings were obtained with aug-cc-pV7Z or aug-cc-pV8Z basis sets. For a few homonuclear diatomic molecules it was possible to push the basis set to the aug-cc-pV9Z level. F12b calculations were performed with the cc-pVnZ-F12 (n = D, T, Q) basis set sequence and were also extrapolated to the basis set limit using a Schwenke-style, parameterized formula. A systematic bias was observed in the F12b method with the (VTZ-F12/VQZ-F12) basis set combination. This bias resulted in the underestimation of reference values associated with small molecules (valence correlation energies 0.5 E(h)) and an even larger overestimation of atomization energies for bigger systems. Consequently, caution should be exercised in the use of F12b for high accuracy studies. Root mean square and mean absolute deviation error metrics for this basis set combination were comparable to complete basis set values obtained with standard CCSD(T) and the aug-cc-pVDZ through aug-cc-pVQZ basis set sequence. However, the mean signed deviation was an order of magnitude larger. Problems partially due to basis set superposition error were identified with second row compounds which resulted in a weak performance for the smaller VDZ-F12/VTZ-F12 combination of basis sets.

  4. 40 CFR 160.63 - Maintenance and calibration of equipment.

    Science.gov (United States)

    2010-07-01

    ...) PESTICIDE PROGRAMS GOOD LABORATORY PRACTICE STANDARDS Equipment § 160.63 Maintenance and calibration of..., maintenance, testing, calibration, and/ or standardization of equipment, and shall specify, when appropriate... 40 Protection of Environment 23 2010-07-01 2010-07-01 false Maintenance and calibration of...

  5. Linear Calibration – Is It so Simple?

    International Nuclear Information System (INIS)

    Arsova, Diana; Babanova, Sofia; Mandjukov, Petko

    2009-01-01

    Calibration procedure is an important part of instrumental analysis. Usually it is not the major uncertainty source in whole analytical procedure. However, improper calibration might cause a significant bias of the analytical results from the real (certified) value. Standard Gaussian linear regression is the most frequently used mathematical approach for estimation of calibration function parameters. In the present article are discussed some not quite popular, but highly recommended in certain cases methods for parameter estimation, such as: weighted regression, orthogonal regression, robust regression, bracketing calibration etc. Some useful approximations are also presented. Special attention is paid to the statistical criteria which to be used for selection of proper calibration model. Standard UV-VIS spectrometric procedure for determination of phosphates in water was used as a practical example. Several different approaches for estimation of the contribution of calibration to the general un-certainty of the analytical result are presented and compared

  6. Intercomparison and calibration of dose calibrators used in nuclear medicine facilities

    CERN Document Server

    Costa, A M D

    2003-01-01

    The aim of this work was to establish a working standard for intercomparison and calibration of dose calibrators used in most of nuclear medicine facilities for the determination of the activity of radionuclides administered to patients in specific examinations or therapeutic procedures. A commercial dose calibrator, a set of standard radioactive sources, and syringes, vials and ampoules with radionuclide solutions used in nuclear medicine were utilized in this work. The commercial dose calibrator was calibrated for radionuclide solutions used in nuclear medicine. Simple instrument tests, such as linearity response and variation response with the source volume at a constant source activity concentration were performed. This instrument may be used as a reference system for intercomparison and calibration of other activity meters, as a method of quality control of dose calibrators utilized in nuclear medicine facilities.

  7. Synthetic multi-element standards: a good tool for calibration and quality control of irradiation facilities used for neutron activation analysis

    International Nuclear Information System (INIS)

    Vermaercke, P.

    2007-01-01

    Neutron activation analysis (NAA) is a physical technique used for the absolute measurement of the concentration of substances in solids and liquids. The method uses neutron irradiation which is commonly realised using a nuclear reactor in order to activate (make radioactive) different isotopes of the elements present in the sample. The radionuclides produced in this way emit gamma-rays that are characteristic of the elements present in the sample. Using gamma-ray spectrometry these radionuclides can then be identified and quantified, and hence their concentration in the sample can be determined. Although NAA is a straightforward method it requires a sound control of the many physical parameters involved to obtain accurate results and to guarantee a set accuracy in routine analysis. The accuracy of NAA depends on the specific measurement method used. One can perform NAA in a relative way by co-irradiating a known standard and the unknown sample in the same conditions and by comparing the ratio of gamma-rays they emit. Relative NAA has limited applicability since it requires reference standards with a comparable composition as the unknown. A more generally applicable method is the k0-NAA method. In the k0-NAA method all measurements are relative to the element Au resulting in 198Au when irradiated. The k0-NAA method further relies on the fact that the neutron energy spectrum produced in a given position in the reactor can be parameterised with two parameters: the shape factor of the epithermal neutron flux, indicating the deviation of the epithermal neutron spectrum from the ideal 1/E shape approximated by a 1/E1+a distribution, with E the neutron energy; f: the thermal-to-epithermal neutron flux ratio. The parameters f and a are characteristic for the irradiation facility (reactor and irradiation channels) and may change or fluctuate in time according to the irradiation conditions. The way elements activate (become radioactive) when interacting with neutrons is

  8. Mercury CEM Calibration

    Energy Technology Data Exchange (ETDEWEB)

    John Schabron; Joseph Rovani; Mark Sanderson

    2008-02-29

    Mercury continuous emissions monitoring systems (CEMS) are being implemented in over 800 coal-fired power plant stacks. The power industry desires to conduct at least a full year of monitoring before the formal monitoring and reporting requirement begins on January 1, 2009. It is important for the industry to have available reliable, turnkey equipment from CEM vendors. Western Research Institute (WRI) is working closely with the Electric Power Research Institute (EPRI), the National Institute of Standards and Technology (NIST), and the Environmental Protection Agency (EPA) to facilitate the development of the experimental criteria for a NIST traceability protocol for dynamic elemental mercury vapor generators. The generators are used to calibrate mercury CEMs at power plant sites. The Clean Air Mercury Rule (CAMR) which was published in the Federal Register on May 18, 2005 requires that calibration be performed with NIST-traceable standards (Federal Register 2007). Traceability procedures will be defined by EPA. An initial draft traceability protocol was issued by EPA in May 2007 for comment. In August 2007, EPA issued an interim traceability protocol for elemental mercury generators (EPA 2007). The protocol is based on the actual analysis of the output of each calibration unit at several concentration levels ranging initially from about 2-40 {micro}g/m{sup 3} elemental mercury, and in the future down to 0.2 {micro}g/m{sup 3}, and this analysis will be directly traceable to analyses by NIST. The document is divided into two separate sections. The first deals with the qualification of generators by the vendors for use in mercury CEM calibration. The second describes the procedure that the vendors must use to certify the generator models that meet the qualification specifications. The NIST traceable certification is performance based, traceable to analysis using isotope dilution inductively coupled plasma/mass spectrometry performed by NIST in Gaithersburg, MD. The

  9. Calibration Laboratory of the Paul Scherrer Institute

    International Nuclear Information System (INIS)

    Gmuer, K.; Wernli, C.

    1994-01-01

    Calibration and working checks of radiation protection instruments are carried out at the Calibration Laboratory of the Paul Scherrer Institute. In view of the new radiation protection regulation, the calibration laboratory received an official federal status. The accreditation procedure in cooperation with the Federal Office of Metrology enabled a critical review of the techniques and methods applied. Specifically, personal responsibilities, time intervals for recalibration of standard instruments, maximum permissible errors of verification, traceability and accuracy of the standard instruments, form and content of the certificates were defined, and the traceability of the standards and quality assurance were reconsidered. (orig.) [de

  10. NIST high-dose calibration services

    International Nuclear Information System (INIS)

    Humphreys, J.C.

    1989-01-01

    There is a need for the standardization of high-dose measurements used in the radiation-processing industry in order to provide assured traceability to national standards. NIST provides dosimetry calibration services to this industry. One of these services involves administration of known absorbed doses of gamma rays to customer-supplied dosimeters. The dosimeters are packaged to provide electron equilibrium conditions and are irradiated in a standard 60 Co calibration facility; this provides a calibration of that batch of dosimeters. Another service consists of supplying to a customer calibrated transfer dosimeters for irradiation with the customer's radiation source. The irradiated transfer dosimeters are then returned to NIST for analysis; the results are reported to the customer, providing a calibration of the dose rate of the customer's source. (orig.)

  11. Comparison of liquid crystal display monitors calibrated with gray-scale standard display function and with γ 2.2 and iPad: observer performance in detection of cerebral infarction on brain CT.

    Science.gov (United States)

    Yoshimura, Kumiko; Nihashi, Takashi; Ikeda, Mitsuru; Ando, Yoshio; Kawai, Hisashi; Kawakami, Kenichi; Kimura, Reiko; Okada, Yumiko; Okochi, Yoshiyuki; Ota, Naotoshi; Tsuchiya, Kenichi; Naganawa, Shinji

    2013-06-01

    The purpose of the study was to compare observer performance in the detection of cerebral infarction on a brain CT using medical-grade liquid crystal display (LCD) monitors calibrated with the gray-scale standard display function and with γ 2.2 and using an iPad with a simulated screen setting. We amassed 97 sample sets, from 47 patients with proven cerebral infarction and 50 healthy control subjects. Nine radiologists independently assessed brain CT on a gray-scale standard display function LCD, a γ 2.2 LCD, and an iPad in random order over 4-week intervals. Receiver operating characteristic (ROC) analysis was performed by using the continuous scale, and the area under the ROC curve (A(z)) was calculated for each monitor. The A(z) values for gray-scale standard display function LCD, γ 2.2 LCD, and iPad were 0.875, 0.884, and 0.839, respectively. The difference among the three monitors was very small. There was no significant difference between gray-scale standard display function LCD and γ 2.2 LCD. However, the A(z) value was statistically significantly smaller for the iPad than the γ 2.2 LCD (p iPad was poorer than that using the other LCDs, the difference was small. Therefore, the iPad could not substitute for other LCD monitors. However, owing to the promising potential advantages of tablet PCs, such as portability, further examination is needed into the clinical use of tablet PCs.

  12. The ENEA calibration service for ionising radiations

    International Nuclear Information System (INIS)

    Monteventi, F.; Sermenghi, I.

    1999-01-01

    The report describes all the facilities available at the the service of the ENEA Calibration Service for Ionising Radiations at Bologna (Italy). It gives a detailed description of all equipments qualified for photon fields metrology including the secondary standards and the calibration procedures performed for radiation monitoring devices and dosemeters [it

  13. A statistical approach to instrument calibration

    Science.gov (United States)

    Robert R. Ziemer; David Strauss

    1978-01-01

    Summary - It has been found that two instruments will yield different numerical values when used to measure identical points. A statistical approach is presented that can be used to approximate the error associated with the calibration of instruments. Included are standard statistical tests that can be used to determine if a number of successive calibrations of the...

  14. A simple method for measurement of cerebral blood flow using 123I-IMP SPECT with calibrated standard input function by one point blood sampling. Validation of calibration by one point venous blood sampling as a substitute for arterial blood sampling

    International Nuclear Information System (INIS)

    Ito, Hiroshi; Akaizawa, Takashi; Goto, Ryoui

    1994-01-01

    In a simplified method for measurement of cerebral blood flow using one 123 I-IMP SPECT scan and one point arterial blood sampling (Autoradiography method), input function is obtained by calibrating a standard input function by one point arterial blood sampling. A purpose of this study is validation of calibration by one point venous blood sampling as a substitute for one point arterial blood sampling. After intravenous infusion of 123 I-IMP, frequent arterial and venous blood sampling were simultaneously performed on 12 patients of CNS disease without any heart and lung disease and 5 normal volunteers. The radioactivity ratio of venous whole blood which obtained from cutaneous cubital vein to arterial whole blood were 0.76±0.08, 0.80±0.05, 0.81±0.06, 0.83±0.11 at 10, 20, 30, 50 min after 123 I-IMP infusion, respectively. The venous blood radioactivities were always 20% lower than those of arterial blood radioactivity during 50 min. However, the ratio which obtained from cutaneous dorsal hand vein to artery were 0.93±0.02, 0.94±0.05, 0.98±0.04, 0.98±0.03, at 10, 20, 30, 50 min after 123 I-IMP infusion, respectively. The venous blood radioactivity was consistent with artery. These indicate that arterio-venous difference of radioactivity in a peripheral cutaneous vein like a dorsal hand vein is minimal due to arteriovenous shunt in palm. Therefore, a substitution by blood sampling from cutaneous dorsal hand vein for artery will be possible. Optimized time for venous blood sampling evaluated by error analysis was 20 min after 123 I-IMP infusion, which is 10 min later than that of arterial blood sampling. (author)

  15. Tank calibration; Arqueacao de tanques

    Energy Technology Data Exchange (ETDEWEB)

    Chan, Ana [PETROBRAS S.A., Rio de Janeiro, RJ (Brazil)

    2003-07-01

    This work relates the analysis of the norms ISO (International Organization for Standardization) for calibration of vertical cylindrical tanks used in fiscal measurement, established on Joint Regulation no 1 of June 19, 2000 between the ANP (National Agency of Petroleum) and the INMETRO (National Institute of Metrology, Normalization and Industrial Quality). In this work a comparison between norms ISO and norms published by the API (American Petroleum Institute) and the IP (Institute of Petroleum) up to 2001 was made. It was concluded that norms ISO are wider than norms API, IP, and INMETRO methods in the calibration of vertical cylindrical tanks. (author)

  16. Calibration services for medical applications of radiation

    Energy Technology Data Exchange (ETDEWEB)

    DeWerd, L.A.

    1993-12-31

    Calibration services for the medical community applications of radiation involve measuring radiation precisely and having traceability to the National Institute of Standards and Technology (NIST). Radiation therapy applications involve the use of ionization chambers and electrometers for external beams and well-type ionization chamber systems as well as radioactive sources for brachytherapy. Diagnostic x-ray applications involve ionization chamber systems and devices to measure other parameters of the x-ray machine, such as non-invasive kVp meters. Calibration laboratories have been established to provide radiation calibration services while maintaining traceability to NIST. New radiation applications of the medical community spur investigation to provide the future calibration needs.

  17. Calibration services for medical applications of radiation

    International Nuclear Information System (INIS)

    DeWerd, L.A.

    1993-01-01

    Calibration services for the medical community applications of radiation involve measuring radiation precisely and having traceability to the National Institute of Standards and Technology (NIST). Radiation therapy applications involve the use of ionization chambers and electrometers for external beams and well-type ionization chamber systems as well as radioactive sources for brachytherapy. Diagnostic x-ray applications involve ionization chamber systems and devices to measure other parameters of the x-ray machine, such as non-invasive kVp meters. Calibration laboratories have been established to provide radiation calibration services while maintaining traceability to NIST. New radiation applications of the medical community spur investigation to provide the future calibration needs

  18. Compilation and evaluation of high energy γ-ray standards from nuclear reactions. Work performed under the coordinated research project 'Update of X- and γ-ray decay data standards for detector calibration'

    International Nuclear Information System (INIS)

    Marcinkowski, A.; Marianski, B.

    1999-02-01

    The report presents the following aspects needed for the compilation and evaluation of high energy γ-ray standards from nuclear reactions: evaluation of emission probabilities of γ-rays with energies 4.44 MeV and 15.11 MeV from 12 C * , preparation of the list of reactions suitable for production of the above mentioned excited radionuclide, and compilation and evaluation of cross sections for these reactions, including inelastic proton scattering on 12 C and radiative capture on 11 B

  19. Calibration of dose meters used in radiotherapy

    International Nuclear Information System (INIS)

    1979-01-01

    This manual is a practical guide, not a comprehensive textbook, to the instrumentation and procedures necessary to calibrate a radiation dose meter used in clinical practice against a secondary standard dose meter

  20. Calibration of a Modified Californium Shuffler

    International Nuclear Information System (INIS)

    Sadowski, E.T.; Armstrong, F.; Oldham, R.; Ceo, R.; Williams, N.

    1995-01-01

    A californium shuffler originally designed to assay hollow cylindrical pieces of UA1 has been modified to assay solid cylinders. Calibration standards were characterized via chemical analysis of the molten UA1 taken during casting of the standards. The melt samples yielded much more reliable characterization data than drill samples taken from standards after the standards had solidified. By normalizing one well-characterized calibration curve to several standards at different enrichments, a relatively small number of standards was required to develop an enrichment-dependent calibration. The precision of this shuffler is 0.65%, and the typical random and systematic uncertainties are 0.53% and 0.73%, respectively, for a six minute assay of an ingot containing approximately 700 grams of 235 U. This paper will discuss (1) the discrepancies encountered when UA1 standards were characterized via melt samples versus drill samples, (2) a calibration methodology employing a small number of standards, and (3) a comparison of results from a previously unused shuffler with an existing shuffler. A small number of UA1 standards have been characterized using samples from the homogeneous molten state and have yielded enrichment-dependent and enrichment-independent calibration curves on two different shufflers

  1. Radiation protection dosimetry and calibrations

    International Nuclear Information System (INIS)

    Verhavere, Ph.

    2007-01-01

    At the SCK-CEN different specialised services are delivered for a whole range of external and internal customers in the radiation protection area. For the expertise group of radiation protection dosimetry and calibrations, these services are organized in four different laboratories: dosimetry, anthropogammametry, nuclear calibrations and non-nuclear calibrations. The services are given by a dedicated technical staff who has experience in the handling of routine and specialised cases. The scientific research that is performed by the expertise group makes sure that state-of-the-art techniques are being used, and that constant improvements and developments are implemented. Quality Assurance is an important aspect for the different services, and accreditation according national and international standards is achieved for all laboratories

  2. Calibration and intercomparison methods of dose calibrators used in nuclear medicine facilities

    International Nuclear Information System (INIS)

    Costa, Alessandro Martins da

    1999-01-01

    Dose calibrators are used in most of the nuclear medicine facilities to determine the amount of radioactivity administered to a patient in a particular investigation or therapeutic procedure. It is therefore of vital importance that the equipment used presents good performance and is regular;y calibrated at a authorized laboratory. This occurs of adequate quality assurance procedures are carried out. Such quality control tests should be performed daily, other biannually or yearly, testing, for example, its accuracy and precision, the reproducibility and response linearity. In this work a commercial dose calibrator was calibrated with solution of radionuclides used in nuclear medicine. Simple instrument tests, such as response linearity and the response variation of the source volume increase at a constant source activity concentration, were performed. This instrument can now be used as a working standard for calibration of other dose calibrators/ An intercomparison procedure was proposed as a method of quality control of dose calibrators used in nuclear medicine facilities. (author)

  3. Guidelines on calibration of neutron measuring devices

    International Nuclear Information System (INIS)

    Burger, G.

    1988-01-01

    The International Atomic Energy Agency and the World Health Organization have agreed to establish an IAEA/WHO Network of Secondary Standard Dosimetry Laboratories (SSDLs) in order to improve accuracy in applied radiation dosimetry throughout the world. These SSDLs must be equipped with, and maintain, secondary standard instruments, which have been calibrated against primary standards, and must be nominated by their governments for membership of the network. The majority of the existing SSDLs were established primarily to work with photon radiation (X-rays and gamma rays). Neutron sources are, however, increasingly being applied in industrial processes, research, nuclear power development and radiation biology and medicine. Thus, it is desirable that the SSDLs in countries using neutron sources on a regular basis should also fulfil the minimum requirements to calibrate neutron measuring devices. It is the primary purpose of this handbook to provide guidance on calibration of instruments for radiation protection. A calibration laboratory should also be in a position to calibrate instrumentation being used for the measurement of kerma and absorbed dose and their corresponding rates. This calibration is generally done with photons. In addition, since each neutron field is usually contaminated by photons produced in the source or by scatter in the surrounding media, neutron protection instrumentation has to be tested with respect to its intrinsic photon response. The laboratory will therefore need to possess equipment for photon calibration. This publication deals primarily with methods of applying radioactive neutron sources for calibration of instrumentation, and gives an indication of the space, manpower and facilities needed to fulfil the minimum requirements of a calibration laboratory for neutron work. It is intended to serve as a guide for centres about to start on neutron dosimetry standardization and calibration. 94 refs, 8 figs, 12 tabs

  4. Absolute, pressure-dependent validation of a calibration-free, airborne laser hygrometer transfer standard (SEALDH-II from 5 to 1200 ppmv using a metrological humidity generator

    Directory of Open Access Journals (Sweden)

    B. Buchholz

    2018-01-01

    Full Text Available Highly accurate water vapor measurements are indispensable for understanding a variety of scientific questions as well as industrial processes. While in metrology water vapor concentrations can be defined, generated, and measured with relative uncertainties in the single percentage range, field-deployable airborne instruments deviate even under quasistatic laboratory conditions up to 10–20 %. The novel SEALDH-II hygrometer, a calibration-free, tuneable diode laser spectrometer, bridges this gap by implementing a new holistic concept to achieve higher accuracy levels in the field. We present in this paper the absolute validation of SEALDH-II at a traceable humidity generator during 23 days of permanent operation at 15 different H2O mole fraction levels between 5 and 1200 ppmv. At each mole fraction level, we studied the pressure dependence at six different gas pressures between 65 and 950 hPa. Further, we describe the setup for this metrological validation, the challenges to overcome when assessing water vapor measurements on a high accuracy level, and the comparison results. With this validation, SEALDH-II is the first airborne, metrologically validated humidity transfer standard which links several scientific airborne and laboratory measurement campaigns to the international metrological water vapor scale.

  5. Synthesis Polarimetry Calibration

    Science.gov (United States)

    Moellenbrock, George

    2017-10-01

    Synthesis instrumental polarization calibration fundamentals for both linear (ALMA) and circular (EVLA) feed bases are reviewed, with special attention to the calibration heuristics supported in CASA. Practical problems affecting modern instruments are also discussed.

  6. Improvement of the calibration technique of clinical dosemeters

    International Nuclear Information System (INIS)

    Ehlin Caldas, L.V.

    1988-08-01

    Clinical dosemeters constituted of ionization chambers connected to electrometers are usually calibrated as whole systems in appropriate radiation fields against secondary standard dosemeters in calibration laboratories. This work reports on a technique of component calibration procedures separately for chambers and electrometers applied in the calibration laboratory of IPEN-CNEN, Brazil. For electrometer calibration, redundancy was established by using a standard capacitor of 1000pF (General Radio, USA) and a standard current source based on air ionization with Sr 90 (PTW, Germany). The results from both methods applied to several electrometers of clinical dosemeters agreed within 0.4%. The calibration factors for the respective chambers were determined by intercomparing their response to the response of a certified calibrated chamber in a Co 60 calibration beam using a Keithley electrometer type 617. Overall calibration factors compared with the product of the respective component calibration factors for the tested dosemeters showed an agreement better than 0.7%. This deviation has to be considered with regard to an uncertainty of 2.5% in routine calibration of clinical dosemeters. Calibration by components permits to calibrate ionization chambers one at a time for those hospitals who have several ionization chambers but only one electrometer (small hospitals, hospitals in developing countries). 6 refs, 2 figs, 2 tabs

  7. Another look at volume self-calibration: calibration and self-calibration within a pinhole model of Scheimpflug cameras

    International Nuclear Information System (INIS)

    Cornic, Philippe; Le Besnerais, Guy; Champagnat, Frédéric; Illoul, Cédric; Cheminet, Adam; Le Sant, Yves; Leclaire, Benjamin

    2016-01-01

    We address calibration and self-calibration of tomographic PIV experiments within a pinhole model of cameras. A complete and explicit pinhole model of a camera equipped with a 2-tilt angles Scheimpflug adapter is presented. It is then used in a calibration procedure based on a freely moving calibration plate. While the resulting calibrations are accurate enough for Tomo-PIV, we confirm, through a simple experiment, that they are not stable in time, and illustrate how the pinhole framework can be used to provide a quantitative evaluation of geometrical drifts in the setup. We propose an original self-calibration method based on global optimization of the extrinsic parameters of the pinhole model. These methods are successfully applied to the tomographic PIV of an air jet experiment. An unexpected by-product of our work is to show that volume self-calibration induces a change in the world frame coordinates. Provided the calibration drift is small, as generally observed in PIV, the bias on the estimated velocity field is negligible but the absolute location cannot be accurately recovered using standard calibration data. (paper)

  8. Validation of a densimeter calibration procedure for a secondary calibration laboratory

    International Nuclear Information System (INIS)

    Alpizar Herrera, Juan Carlos

    2014-01-01

    A survey was conducted to quantify the need for calibration of a density measurement instrument at the research units at the Sede Rodrigo Facio of the Universidad de Costa Rica. A calibration procedure was documented for the instrument that presented the highest demand in the survey by the calibration service. A study of INTE-ISO/IEC 17025: 2005 and specifically in section 5.4 of this standard was done, to document the procedure for calibrating densimeters. Densimeter calibration procedures and standards were sought from different national and international sources. The method of hydrostatic weighing or Cuckow method was the basis of the defined procedure. Documenting the calibration procedure and creating other documents was performed for data acquisition log, intermediate calculation log and calibration certificate copy. A veracity test was performed using as reference laboratory a laboratory of calibration secondary national as part of the validation process of the documented procedure. The results of the E_n statistic of 0.41; 0.34 and 0.46 for the calibration points 90%, 50% and 10% were obtained for the densimeter scale respectively. A reproducibility analysis of the method was performed with satisfactory results. Different suppliers were contacted to estimate the economic costs of the equipment and materials, needed to develop the documented method of densimeter calibration. The acquisition of an analytical balance was recommended, instead of a precision scale, in order to improve the results obtained with the documented method [es

  9. Radioactivity measurement of 18F in 16 ml vials for calibration of radionuclide calibrators

    International Nuclear Information System (INIS)

    Wurdiyanto, Gatot; Marsoem, Pujadi; Candra, Hermawan; Wijono, Paidi

    2012-01-01

    Fluorine-18 is obtained through the reaction 18 O(p, n) 18 F using a cyclotron that is situated in a hospital in Jakarta. Standardization of the 18 F solution is performed by gamma spectrometry using calibration sources of 152 Eu, 60 Co and 137 Cs that have traceability to the International System of units (SI). The activities in the 16 ml vials that were used for calibrating the radionuclide calibrators were between 1 and 2 GBq, with expanded uncertainties of 3.8%. The expanded uncertainty, at a coverage factor of k=2, on the derived calibration factor for the radionuclide calibrator was 6.6%. - Highlights: ► PTKMR–BATAN as a NMI of Indonesia is required to have procedures to calibrate the radionuclide calibrators. ► Standardizations were carried out on a solution of [ 18 F]FDG using gamma spectrometry. ► The volume of 18 F solutions used was 16 ml because this is the volume often used in hospitals. ► The Secondary Standard ionization chamber is a CRC-7BT Capintec radionuclide calibrator. ► A dial setting for 16 ml of [ 18 F]FDG solution in a vial is 443 for the Capintec dose calibrator.

  10. e-Calibrations: using the Internet to deliver calibration services in real time at lower cost

    International Nuclear Information System (INIS)

    Desrosiers, Marc; Nagy, Vitaly; Puhl, James; Glenn, Robert; Densock, Robert; Stieren, David; Lang, Brian; Kamlowski, Andreas; Maier, Diether; Heiss, Arthur

    2002-01-01

    The National Institute of Standards and Technology (NIST) is expanding into a new frontier in the delivery of measurement services. The Internet will be employed to provide industry with electronic traceability to national standards. This is a radical departure from the traditional modes of traceability and presents many new challenges. The traditional mail-based calibration service relies on sending artifacts to the user, who then mails them back to NIST for evaluation. The new service will deliver calibration results to the industry customer on-demand, in real-time, at a lower cost. The calibration results can be incorporated rapidly into the production process to ensure the highest quality manufacturing. The service would provide the US radiation processing industry with a direct link to the NIST calibration facilities and its expertise, and provide an interactive feedback process between industrial processing and the national measurement standard. Moreover, an Internet calibration system should contribute to the removal of measurement-related trade barriers

  11. Sensor Calibration Design Based on D-Optimality Criterion

    Directory of Open Access Journals (Sweden)

    Hajiyev Chingiz

    2016-09-01

    Full Text Available In this study, a procedure for optimal selection of measurement points using the D-optimality criterion to find the best calibration curves of measurement sensors is proposed. The coefficients of calibration curve are evaluated by applying the classical Least Squares Method (LSM. As an example, the problem of optimal selection for standard pressure setters when calibrating a differential pressure sensor is solved. The values obtained from the D-optimum measurement points for calibration of the differential pressure sensor are compared with those from actual experiments. Comparison of the calibration errors corresponding to the D-optimal, A-optimal and Equidistant calibration curves is done.

  12. SPRT Calibration Uncertainties and Internal Quality Control at a Commercial SPRT Calibration Facility

    Science.gov (United States)

    Wiandt, T. J.

    2008-06-01

    The Hart Scientific Division of the Fluke Corporation operates two accredited standard platinum resistance thermometer (SPRT) calibration facilities, one at the Hart Scientific factory in Utah, USA, and the other at a service facility in Norwich, UK. The US facility is accredited through National Voluntary Laboratory Accreditation Program (NVLAP), and the UK facility is accredited through UKAS. Both provide SPRT calibrations using similar equipment and procedures, and at similar levels of uncertainty. These uncertainties are among the lowest available commercially. To achieve and maintain low uncertainties, it is required that the calibration procedures be thorough and optimized. However, to minimize customer downtime, it is also important that the instruments be calibrated in a timely manner and returned to the customer. Consequently, subjecting the instrument to repeated calibrations or extensive repeated measurements is not a viable approach. Additionally, these laboratories provide SPRT calibration services involving a wide variety of SPRT designs. These designs behave differently, yet predictably, when subjected to calibration measurements. To this end, an evaluation strategy involving both statistical process control and internal consistency measures is utilized to provide confidence in both the instrument calibration and the calibration process. This article describes the calibration facilities, procedure, uncertainty analysis, and internal quality assurance measures employed in the calibration of SPRTs. Data will be reviewed and generalities will be presented. Finally, challenges and considerations for future improvements will be discussed.

  13. Quality assurance programs at the PNL calibrations laboratory

    International Nuclear Information System (INIS)

    Piper, R.K.; McDonald, J.C.; Fox, R.A.; Eichner, F.N.

    1993-03-01

    The calibrations laboratory at Pacific Northwest Laboratory (PNL) serves as a radiological standardization facility for personnel and environmental dosimetry and radiological survey instruments. As part of this function, the calibrations laboratory must maintain radiological reference fields with calibrations traceable to the National Institute of Standards and Technology (NIST). This task is accomplished by a combination of (1) sources or reference instruments calibrated at or by NIST, (2) measurement quality assurance (MQA) interactions with NIST, and (3) rigorous internal annual and quarterly calibration verifications. This paper describes a representative sample of the facilities, sources, and actions used to maintain accurate and traceable fields

  14. Calibration of NS value of magnetic probe on EAST

    International Nuclear Information System (INIS)

    Sun Jiuyu; Shen Biao; Liu Guangjun; Sun Youwen; Qian Jinping; Li Shi; Xiao Bingjia; Chen Dalong; Shi Tonghui

    2014-01-01

    Based on the basic principle of measuring magnetic field by magnetic probe, a solenoid calibration system is constructed by a long solenoid, alternating current power, standard probe and data acquisition system in order to get the accurate magnetic field data. The NS value of magnetic probe on EAST is calibrated accurately by the solenoid calibration system and the data of the calibration is analysed. The obtained results are what we expected and provide the prerequisite for accurate magnetic field measurement in tokamak. (authors)

  15. Calibration of Nanopositioning Stages

    Directory of Open Access Journals (Sweden)

    Ning Tan

    2015-12-01

    Full Text Available Accuracy is one of the most important criteria for the performance evaluation of micro- and nanorobots or systems. Nanopositioning stages are used to achieve the high positioning resolution and accuracy for a wide and growing scope of applications. However, their positioning accuracy and repeatability are not well known and difficult to guarantee, which induces many drawbacks for many applications. For example, in the mechanical characterisation of biological samples, it is difficult to perform several cycles in a repeatable way so as not to induce negative influences on the study. It also prevents one from controlling accurately a tool with respect to a sample without adding additional sensors for closed loop control. This paper aims at quantifying the positioning repeatability and accuracy based on the ISO 9283:1998 standard, and analyzing factors influencing positioning accuracy onto a case study of 1-DoF (Degree-of-Freedom nanopositioning stage. The influence of thermal drift is notably quantified. Performances improvement of the nanopositioning stage are then investigated through robot calibration (i.e., open-loop approach. Two models (static and adaptive models are proposed to compensate for both geometric errors and thermal drift. Validation experiments are conducted over a long period (several days showing that the accuracy of the stage is improved from typical micrometer range to 400 nm using the static model and even down to 100 nm using the adaptive model. In addition, we extend the 1-DoF calibration to multi-DoF with a case study of a 2-DoF nanopositioning robot. Results demonstrate that the model efficiently improved the 2D accuracy from 1400 nm to 200 nm.

  16. Calibration of Photon Sources for Brachytherapy

    Science.gov (United States)

    Rijnders, Alex

    Source calibration has to be considered an essential part of the quality assurance program in a brachytherapy department. Not only it will ensure that the source strength value used for dose calculation agrees within some predetermined limits to the value stated on the source certificate, but also it will ensure traceability to international standards. At present calibration is most often still given in terms of reference air kerma rate, although calibration in terms of absorbed dose to water would be closer to the users interest. It can be expected that in a near future several standard laboratories will be able to offer this latter service, and dosimetry protocols will have to be adapted in this way. In-air measurement using ionization chambers (e.g. a Baldwin—Farmer ionization chamber for 192Ir high dose rate HDR or pulsed dose rate PDR sources) is still considered the method of choice for high energy source calibration, but because of their ease of use and reliability well type chambers are becoming more popular and are nowadays often recommended as the standard equipment. For low energy sources well type chambers are in practice the only equipment available for calibration. Care should be taken that the chamber is calibrated at the standard laboratory for the same source type and model as used in the clinic, and using the same measurement conditions and setup. Several standard laboratories have difficulties to provide these calibration facilities, especially for the low energy seed sources (125I and 103Pd). Should a user not be able to obtain properly calibrated equipment to verify the brachytherapy sources used in his department, then at least for sources that are replaced on a regular basis, a consistency check program should be set up to ensure a minimal level of quality control before these sources are used for patient treatment.

  17. Direct megavoltage photon calibration service in Australia

    International Nuclear Information System (INIS)

    Butler, D.J.; Ramanthan, G.; Oliver, C.; Cole, A.; Harty, P.D.; Wright, T.; Webb, D.V.; Lye, J.; Followill, D.S.

    2014-01-01

    The Australian Radiation Protection and Nuclear Safety Agency (ARPANSA) maintains the Australian primary standard of absorbed dose. Until recently, the standard was used to calibrate ionisation chambers only in 60 Co gamma rays. These chambers are then used by radiotherapy clinics to determine linac output, using a correction factor (k Q ) to take into account the different spectra of 60 Co and the linac. Over the period 2010–2013, ARPANSA adapted the primary standard to work in megavoltage linac beams, and has developed a calibration service at three photon beams (6, 10 and 18 MV) from an Elekta Synergy linac. We describe the details of the new calibration service, the method validation and the use of the new calibration factors with the International Atomic Energy Agency’s TRS-398 dosimetry Code of Practice. The expected changes in absorbed dose measurements in the clinic when shifting from 60 Co to the direct calibration are determined. For a Farmer chamber (model 2571), the measured chamber calibration coefficient is expected to be reduced by 0.4, 1.0 and 1.1 % respectively for these three beams when compared to the factor derived from 60 Co. These results are in overall agreement with international absorbed dose standards and calculations by Muir and Rogers in 2010 of k Q factors using Monte Carlo techniques. The reasons for and against moving to the new service are discussed in the light of the requirements of clinical dosimetry.

  18. Electromagnetic Calorimeter Calibration with $\\pi^{0}$

    CERN Multimedia

    Puig Navarro, A

    2009-01-01

    Several methods can be used in order to achieve precise calibration of the LHCb Electromagnetic Calorimeter (ECAL) once reasonable cell equalization has been reached. At low transverse energy, the standard calibration procedure is an iterative method based on the fit of the $\\gamma\\gamma$ invariant mass distribution for each cell of the decay $\\pi^{0}\\to\\gamma\\gamma$ with resolved photons. A new technique for generating the combinatorial background of such decays directly from data has been developed. Knowledge of the background could allow an alternative calibration method based on a event by event fit of the same $\\gamma\\gamma$ invariant mass distribution where contributions from groups of cells are considered in a single fit. The background generation procedure and this possible new calibration method are presented in this poster, in addition to an overview of the LHCb Calorimetry system and ECAL calibration techniques.

  19. Cryogenic Thermometer Calibration Facility at CERN

    CERN Document Server

    Balle, C; Thermeau, J P

    1998-01-01

    A cryogenic thermometer calibration facility has been designed and is being commissioned in preparation for the very stringent requirements on the temperature control of the LHC superconducting magnets. The temperature is traceable in the 1.5 to 30 K range to standards maintained in a national metrological laboratory by using a set of Rhodium-Iron temperature sensors of metrological quality. The calibration facility is designed for calibrating simultaneously 60 industrial cryogenic thermometers in the 1.5 K to 300 K temperature range, a thermometer being a device that includes both a temperature sensor and the wires heat-intercept. The thermometers can be calibrated in good and degraded vacuum or immersed in the surrounding fluid and at different Joule self-heating conditions that match those imposed by signal conditioners used in large cryogenic machinery. The calibration facility can be operated in an automatic mode and all the control and safety routines are handled by a Programmable Logic Controller (PLC)...

  20. Cumulative sum quality control for calibrated breast density measurements

    International Nuclear Information System (INIS)

    Heine, John J.; Cao Ke; Beam, Craig

    2009-01-01

    Purpose: Breast density is a significant breast cancer risk factor. Although various methods are used to estimate breast density, there is no standard measurement for this important factor. The authors are developing a breast density standardization method for use in full field digital mammography (FFDM). The approach calibrates for interpatient acquisition technique differences. The calibration produces a normalized breast density pixel value scale. The method relies on first generating a baseline (BL) calibration dataset, which required extensive phantom imaging. Standardizing prospective mammograms with calibration data generated in the past could introduce unanticipated error in the standardized output if the calibration dataset is no longer valid. Methods: Sample points from the BL calibration dataset were imaged approximately biweekly over an extended timeframe. These serial samples were used to evaluate the BL dataset reproducibility and quantify the serial calibration accuracy. The cumulative sum (Cusum) quality control method was used to evaluate the serial sampling. Results: There is considerable drift in the serial sample points from the BL calibration dataset that is x-ray beam dependent. Systematic deviation from the BL dataset caused significant calibration errors. This system drift was not captured with routine system quality control measures. Cusum analysis indicated that the drift is a sign of system wear and eventual x-ray tube failure. Conclusions: The BL calibration dataset must be monitored and periodically updated, when necessary, to account for sustained system variations to maintain the calibration accuracy.

  1. Cumulative sum quality control for calibrated breast density measurements

    Energy Technology Data Exchange (ETDEWEB)

    Heine, John J.; Cao Ke; Beam, Craig [Cancer Prevention and Control Division, Moffitt Cancer Center, 12902 Magnolia Drive, Tampa, Florida 33612 (United States); Division of Epidemiology and Biostatistics, School of Public Health, University of Illinois at Chicago, 1603 W. Taylor St., Chicago, Illinois 60612 (United States)

    2009-12-15

    Purpose: Breast density is a significant breast cancer risk factor. Although various methods are used to estimate breast density, there is no standard measurement for this important factor. The authors are developing a breast density standardization method for use in full field digital mammography (FFDM). The approach calibrates for interpatient acquisition technique differences. The calibration produces a normalized breast density pixel value scale. The method relies on first generating a baseline (BL) calibration dataset, which required extensive phantom imaging. Standardizing prospective mammograms with calibration data generated in the past could introduce unanticipated error in the standardized output if the calibration dataset is no longer valid. Methods: Sample points from the BL calibration dataset were imaged approximately biweekly over an extended timeframe. These serial samples were used to evaluate the BL dataset reproducibility and quantify the serial calibration accuracy. The cumulative sum (Cusum) quality control method was used to evaluate the serial sampling. Results: There is considerable drift in the serial sample points from the BL calibration dataset that is x-ray beam dependent. Systematic deviation from the BL dataset caused significant calibration errors. This system drift was not captured with routine system quality control measures. Cusum analysis indicated that the drift is a sign of system wear and eventual x-ray tube failure. Conclusions: The BL calibration dataset must be monitored and periodically updated, when necessary, to account for sustained system variations to maintain the calibration accuracy.

  2. Unexplored Indoors method for pyranometers calibration traceable to SI

    International Nuclear Information System (INIS)

    Castillo-Matadamas, H A; Molina-Vazquez, J C; Quintero-Torres, R

    2015-01-01

    A method to calibrate pyranometers with direct traceability to the International System of Units (SI) is presented, the method use an electrically calibrated pyroelectric detector (ECPR) as standard and offers numerous advantages over outdoors conventional calibration methods, such as reducing the uncertainty from the reference standard and the final uncertainty of the sensitivity coefficient of the calibrated pyranometer; the measurement uncertainty achieved with this method at normal irradiance is 2.1% for a coverage factor k = 2 and could be reduce if one reduces the uncertainty level of the reference standard

  3. HPS instrument calibration laboratory accreditation program

    Energy Technology Data Exchange (ETDEWEB)

    Masse, F.X; Eisenhower, E.H.; Swinth, K.L.

    1993-12-31

    The purpose of this paper is to provide an accurate overview of the development and structure of the program established by the Health Physics Society (HPS) for accrediting instrument calibration laboratories relative to their ability to accurately calibrate portable health physics instrumentation. The purpose of the program is to provide radiation protection professionals more meaningful direct and indirect access to the National Institute of Standards and Technology (NIST) national standards, thus introducing a means for improving the uniformity, accuracy, and quality of ionizing radiation field measurements. The process is designed to recognize and document the continuing capability of each accredited laboratory to accurately perform instrument calibration. There is no intent to monitor the laboratory to the extent that each calibration can be guaranteed by the program; this responsibility rests solely with the accredited laboratory.

  4. The Observability Calibration Test Development Framework

    Energy Technology Data Exchange (ETDEWEB)

    Endicott-Popovsky, Barbara E.; Frincke, Deborah A.

    2007-06-20

    Abstract— Formal standards, precedents, and best practices for verifying and validating the behavior of low layer network devices used for digital evidence-collection on networks are badly needed— initially so that these can be employed directly by device owners and data users to document the behaviors of these devices for courtroom presentation, and ultimately so that calibration testing and calibration regimes are established and standardized as common practice for both vendors and their customers [1]. The ultimate intent is to achieve a state of confidence in device calibration that allows the network data gathered by them to be relied upon by all parties in a court of law. This paper describes a methodology for calibrating forensic-ready low layer network devices based on the Flaw Hypothesis Methodology [2,3].

  5. Monitoring coordinate measuring machines by calibrated parts

    International Nuclear Information System (INIS)

    Weckenmann, A; Lorz, J

    2005-01-01

    Coordinate measuring machines (CMM) are essential for quality assurance and production control in modern manufacturing. Due to the necessity of assuring traceability during the use of CMM, interim checks with calibrated objects carried out periodically. For this purpose usually special artefacts like standardized ball plates, hole plates, ball bars or step gages are measured. Measuring calibrated series parts would be more advantageous. Applying the substitution method of ISO 15530-3: 2000 such parts can be used. It is less cost intensive and less time consuming than measuring expensive special standardized objects in special programmed measurement routines. Moreover, the measurement results can directly compare with the calibration values; thus, direct information on systematic measurement deviations and uncertainty of the measured features are available. The paper describes a procedure for monitoring horizontal-arm CMMs with calibrated sheet metal series parts

  6. Calibration of Ground-based Lidar instrument

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Gómez Arranz, Paula

    This report presents the result of the lidar calibration performed for the given Ground-based Lidar at DTU’s test site for large wind turbines at Høvsøre, Denmark. Calibration is here understood as the establishment of a relation between the reference wind speed measurements with measurement...... uncertainties provided by measurement standard and corresponding lidar wind speed indications with associated measurement uncertainties. The lidar calibration concerns the 10 minute mean wind speed measurements. The comparison of the lidar measurements of the wind direction with that from wind vanes...

  7. Error-in-variables models in calibration

    Science.gov (United States)

    Lira, I.; Grientschnig, D.

    2017-12-01

    In many calibration operations, the stimuli applied to the measuring system or instrument under test are derived from measurement standards whose values may be considered to be perfectly known. In that case, it is assumed that calibration uncertainty arises solely from inexact measurement of the responses, from imperfect control of the calibration process and from the possible inaccuracy of the calibration model. However, the premise that the stimuli are completely known is never strictly fulfilled and in some instances it may be grossly inadequate. Then, error-in-variables (EIV) regression models have to be employed. In metrology, these models have been approached mostly from the frequentist perspective. In contrast, not much guidance is available on their Bayesian analysis. In this paper, we first present a brief summary of the conventional statistical techniques that have been developed to deal with EIV models in calibration. We then proceed to discuss the alternative Bayesian framework under some simplifying assumptions. Through a detailed example about the calibration of an instrument for measuring flow rates, we provide advice on how the user of the calibration function should employ the latter framework for inferring the stimulus acting on the calibrated device when, in use, a certain response is measured.

  8. Self-Calibration of CMB Polarimeters

    Science.gov (United States)

    Keating, Brian

    2013-01-01

    Precision measurements of the polarization of the cosmic microwave background (CMB) radiation, especially experiments seeking to detect the odd-parity "B-modes", have far-reaching implications for cosmology. To detect the B-modes generated during inflation the flux response and polarization angle of these experiments must be calibrated to exquisite precision. While suitable flux calibration sources abound, polarization angle calibrators are deficient in many respects. Man-made polarized sources are often not located in the antenna's far-field, have spectral properties that are radically different from the CMB's, are cumbersome to implement and may be inherently unstable over the (long) duration these searches require to detect the faint signature of the inflationary epoch. Astrophysical sources suffer from time, frequency and spatial variability, are not visible from all CMB observatories, and none are understood with sufficient accuracy to calibrate future CMB polarimeters seeking to probe inflationary energy scales of ~1000 TeV. CMB TB and EB modes, expected to identically vanish in the standard cosmological model, can be used to calibrate CMB polarimeters. By enforcing the observed EB and TB power spectra to be consistent with zero, CMB polarimeters can be calibrated to levels not possible with man-made or astrophysical sources. All of this can be accomplished without any loss of observing time using a calibration source which is spectrally identical to the CMB B-modes. The calibration procedure outlined here can be used for any CMB polarimeter.

  9. Logarithmic transformed statistical models in calibration

    International Nuclear Information System (INIS)

    Zeis, C.D.

    1975-01-01

    A general type of statistical model used for calibration of instruments having the property that the standard deviations of the observed values increase as a function of the mean value is described. The application to the Helix Counter at the Rocky Flats Plant is primarily from a theoretical point of view. The Helix Counter measures the amount of plutonium in certain types of chemicals. The method described can be used also for other calibrations. (U.S.)

  10. Calibration and quality control for personnel dose meter

    International Nuclear Information System (INIS)

    Wu Rongtao; Zhang Dianqin

    1999-01-01

    Calibration and quality control are the important aspects to assure thermoluminescence dose measurement compliance with the technical standards. The author discussed some problems to implement technical standards and regulations

  11. In-Flight Calibrations of UFFO-Pathfinder

    DEFF Research Database (Denmark)

    Řípa, J.; Ahmad, S.; Barrillon, P.

    2013-01-01

    for the observation of the prompt optical/UV counterparts. Here we discuss the in-space calibrations of the UBAT detector and SMT telescope. After the launch, the observations of the standard X-ray sources such as pulsar in Crab nebula will provide data for necessary calibrations of UBAT. Several standard stars...

  12. 40 CFR 792.63 - Maintenance and calibration of equipment.

    Science.gov (United States)

    2010-07-01

    ... SUBSTANCES CONTROL ACT (CONTINUED) GOOD LABORATORY PRACTICE STANDARDS Equipment § 792.63 Maintenance and..., maintenance, testing, calibration, and/or standardization of equipment, and shall specify, when appropriate... 40 Protection of Environment 31 2010-07-01 2010-07-01 true Maintenance and calibration of...

  13. Use of Ethanol/Diesel Blend and Advanced Calibration Methods to Satisfy Euro 5 Emission Standards without DPF Utilisation d’un carburant Diesel éthanolé à l’aide de méthodes de calibration avancées afin de satisfaire les normes Euro 5 sans filtre à particules

    Directory of Open Access Journals (Sweden)

    Magand S.

    2011-11-01

    innovative calibration methods, based on the simultaneous optimisation of engine basic settings and cold correction maps, are introduced in order to better suit to the new formulation impact on combustion and catalyst light-off and to drop off engine-out unburned hydrocarbons and carbon monoxide emissions. This stage allows pushing forward the work on test bed facilities in order to reduce the amount of vehicle tests. Tests on a chassis dynamometer are only used to validate the engine test bed results and to perform final tuning of cold correction maps. This alternative blend shows potential to achieve Euro 5 standard with Euro 4 Diesel vehicle configuration, without any hardware modification and without a Diesel particulate filter in the exhaust line. Such an innovative fuel formulation seems to be an interesting answer to the trade-off in the forthcoming years between cost and emissions reduction to achieve sustainable mobility. The presented calibration methods and tools allow to fully take advantage of this alternative fuel in a reduced time scale. L’utilisation des biocarburants s’est développée durant ces dernières années de façon importante afin de diversifier les sources d’énergies et de limiter la hausse des émissions de gaz à effet de serre du secteur des transports. L’un des carburants renouvelables les plus adaptés à une production de masse est l’éthanol. Celui-ci est aujourd’hui principalement utilisé dans les moteurs à allumage commandé, alors que la part des véhicules Diesel sur le marché européen est de l’ordre de 60 %. Ce constat nous a incité à proposer une formulation innovante utilisant de l’éthanol pour les applications Diesel. Les principaux verrous technologiques pour cette utilisation sont la miscibilité, la température d’éclair, la lubrification ou encore l’indice de cétane. Des travaux ont été réalisés pour optimiser la formulation contenant de l’éthanol, des biodiesels de première et seconde g

  14. Calibration method of radiation monitoring system at TQNPC

    International Nuclear Information System (INIS)

    Liu Zhengshan; Zhang Qingli; Liu Jinjin; Miao Yuxing; Geng Lixin; Zhuang Yun; Dong Jianfeng; He Change

    2009-04-01

    The calibration methods and calibration device for standard monitor of radioactive particulate, iodine, noble gas and so on are not yet set up at home. On consideration of the present situation of the radiation monitoring system at the Third Qinshan Nuclear Power Co. Ltd., we have studied the calibration method of these radiation monitoring instruments used for measuring the waste liquid, particulate, iodine and noble gas produced during the operation of nuclear reactor. Through the check against these instruments during the No. 202 and No. 103 overhaul, we got initially the method of the calibration and obtained the transfer coefficient of calibration when secondary solid sources are used for calibration. Through the testing and calibration, the credibility of the radiation monitoring system is enhanced. And at the same time, the problems existing in the calibration are discussed. (authors)

  15. Calibration of moisture monitors

    International Nuclear Information System (INIS)

    Gutierrez, R.L.

    1979-02-01

    A method for calibrating an aluminum oxide hygrometer against an optical chilled mirror dew-point hygrometer has been established. A theoretical cross-point line of dew points from both hygrometers and a maximum moisture content of 10 ppM/sub v/ are used to define an area for calibrating the sensor probes of the aluminum oxide hygrometer

  16. Site Calibration report

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Vesth, Allan

    The report describes site calibration measurements carried out on a site in Denmark. The measurements are carried out in accordance to Ref. [1]. The site calibration is carried out before a power performance measurement on a given turbine to clarify the influence from the terrain on the ratio...

  17. Topics in Statistical Calibration

    Science.gov (United States)

    2014-03-27

    Natural cubic spline speed di st 110 B.2 The calibrate function The most basic calibration problem, the one often encountered in more advanced ...0040-1706, 1537-2723. A. M. Mood, F. A. Graybill, and D. C. Boes. Introduction to the Theory of Statistics. McGraw-Hill, Auckland , U.A, 1974. ISBN

  18. The GERDA calibration system

    Energy Technology Data Exchange (ETDEWEB)

    Baudis, Laura; Froborg, Francis; Tarka, Michael; Bruch, Tobias; Ferella, Alfredo [Physik-Institut, Universitaet Zuerich (Switzerland); Collaboration: GERDA-Collaboration

    2012-07-01

    A system with three identical custom made units is used for the energy calibration of the GERDA Ge diodes. To perform a calibration the {sup 228}Th sources are lowered from the parking positions at the top of the cryostat. Their positions are measured by two independent modules. One, the incremental encoder, counts the holes in the perforated steel band holding the sources, the other measures the drive shaft's angular position even if not powered. The system can be controlled remotely by a Labview program. The calibration data is analyzed by an iterative calibration algorithm determining the calibration functions for different energy reconstruction algorithms and the resolution of several peaks in the {sup 228}Th spectrum is determined. A Monte Carlo simulation using the GERDA simulation software MAGE has been performed to determine the background induced by the sources in the parking positions.

  19. Evaluating uncertainties in the cross-calibration of parallel ion chambers used in electron beam radiotherapy

    International Nuclear Information System (INIS)

    Anderson, Ernani; Travassos, Paulo; Ferreira, Max da Silva; Carvalho, Samira Marques de; Silva, Michele Maria da; Peixoto, Jose Guilherme Pereira; Salmon Junior, Helio Augusto

    2015-01-01

    This study aims to estimative the combined standard uncertainty for a detector parallel plate used for dosimetry of electron beams in linear accelerators for radiotherapy, which has been calibrated by the cross-calibration method. Keeping the combined standard uncertainty next of the uncertainty informed in the calibration certificate of the reference chamber, become possible establish the calibration factor of the detector. The combined standard uncertainty obtained in this study was 2.5 %. (author)

  20. Calibration of reference KAP-meters at SSDL and cross calibration of clinical KAP-meters

    International Nuclear Information System (INIS)

    Hetland, Per O.; Friberg, Eva G.; Oevreboe, Kirsti M.; Bjerke, Hans H.

    2009-01-01

    In the summer of 2007 the secondary standard dosimetry laboratory (SSDL) in Norway established a calibration service for reference air-kerma product meter (KAP-meter). The air-kerma area product, PKA, is a dosimetric quantity that can be directly related to the patient dose and used for risk assessment associated with different x-ray examinations. The calibration of reference KAP-meters at the SSDL gives important information on parameters influencing the calibration factor for different types of KAP-meters. The use of reference KAP-meters calibrated at the SSDL is an easy and reliable way to calibrate or verify the PKA indicated by the x-ray equipment out in the clinics. Material and methods. Twelve KAP-meters were calibrated at the SSDL by use of the substitution method at five diagnostic radiation qualities (RQRs). Results. The calibration factors varied from 0.94 to 1.18. The energy response of the individual KAP-meters varied by a total of 20% between the different RQRs and the typical chamber transmission factors ranged from 0.78 to 0.91. Discussion. It is important to use a calibrated reference KAP-meter and a harmonised calibration method in the PKA calibration in hospitals. The obtained uncertainty in the PKA readings is comparable with other calibration methods if the information in the calibration certificate is correct used, corrections are made and proper positioning of the KAP-chamber is performed. This will ensure a reliable estimate of the patient dose and a proper optimisation of conventional x-ray examinations and interventional procedures

  1. Nuclear radiation gauge standard

    International Nuclear Information System (INIS)

    Berry, R.L.

    1977-01-01

    A hydrophobic standard for calibrating nuclear radiation moisture gauges is described, comprising a body of superposed interleaved thin layers of a moderating material containing hydrogen in the molecular structure thereof and of a substantially non-moderating material

  2. Calibration guidelines for surface texture instruments - horizontal axis

    DEFF Research Database (Denmark)

    Andreasen, Jan Lasson; Shem, R. Krüger

    The present report is a documentation of the work carried out at DTU, on TASK 5.1: PROCEDURES FOR CALIBRATION IN X- AND Y- DIRECTION the project with contract SMT4-CT97-2176 with title: Calibration Standards for Surface Topography Measuring Systems down to Nanometric Scale. After a short introduc......The present report is a documentation of the work carried out at DTU, on TASK 5.1: PROCEDURES FOR CALIBRATION IN X- AND Y- DIRECTION the project with contract SMT4-CT97-2176 with title: Calibration Standards for Surface Topography Measuring Systems down to Nanometric Scale. After a short...

  3. Calibration of optical cantilever deflection readers

    International Nuclear Information System (INIS)

    Hu Zhiyu; Seeley, Tim; Kossek, Sebastian; Thundat, Thomas

    2004-01-01

    Because of its ultrahigh sensitivity, the optical lever detection method similar to that used in the atomic force microscope (AFM) has been widely employed as a standard technique for measuring microcantilever deflection. Along with the increasing interest in using the microcantilever as a sensing platform, there is also a requirement for a reliable calibration technique. Many researchers have used the concept of optical lever detection to construct microcantilever deflection readout instruments for chemical, physical, and biological detection. However, without an AFM piezo z scanner, it is very difficult to precisely calibrate these instruments. Here, we present a step-by-step method to conveniently calibrate an instrument using commercially available piezoresistive cantilevers. The experimental results closely match the theoretical calculation. Following this procedure, one can easily calibrate any optical cantilever deflection detection system with high reproducibility, precision, and reliability. A detailed discussion of the optical lever readout system design has been addressed in this article

  4. Laboratory panel and radiometer calibration

    CSIR Research Space (South Africa)

    Deadman, AJ

    2011-07-01

    Full Text Available stream_source_info Griffith1_2011.pdf.txt stream_content_type text/plain stream_size 16659 Content-Encoding ISO-8859-1 stream_name Griffith1_2011.pdf.txt Content-Type text/plain; charset=ISO-8859-1 LABORATORY PANEL... of Land surface imaging through a ground reference standard test site?, on http://qa4eo.org/documentation.html, 2009. [2] K. J. Thome, D. L. Helder, D. Aaron, and J. D. Dewald, ?Landsat-5 TM and Landsat-7 ETM+ Absolute Radiometric Calibration Using...

  5. Compact radiometric microwave calibrator

    International Nuclear Information System (INIS)

    Fixsen, D. J.; Wollack, E. J.; Kogut, A.; Limon, M.; Mirel, P.; Singal, J.; Fixsen, S. M.

    2006-01-01

    The calibration methods for the ARCADE II instrument are described and the accuracy estimated. The Steelcast coated aluminum cones which comprise the calibrator have a low reflection while maintaining 94% of the absorber volume within 5 mK of the base temperature (modeled). The calibrator demonstrates an absorber with the active part less than one wavelength thick and only marginally larger than the mouth of the largest horn and yet black (less than -40 dB or 0.01% reflection) over five octaves in frequency

  6. SU-E-T-749: Thorough Calibration of MOSFET Dosimeters

    International Nuclear Information System (INIS)

    Plenkovich, D; Thomas, J

    2015-01-01

    Purpose: To improve the accuracy of the MOSFET calibration procedure by performing the measurement several times and calculating the average value of the calibration factor for various photon and electron energies. Methods: The output of three photon and six electron beams of Varian Trilogy linear accelerator SN 5878 was calibrated. Five reinforced standard sensitivity MOSFET dosimeters were placed in the calibration jig and connected to the Reader Module. As the backscatter material was used 7 cm of Virtual Water. The MOSFET dosimeters were covered with 1.5 cm thick bolus for the regular and SRS 6 MV beams, 3 cm bolus for 15 MV beam, 1.5 cm bolus for 6 MeV electron beam, and 2 cm bolus for the electron energies of 9, 12, 15, 18, and 22 MeV. The dosimeters were exposed to 100 MU, and the calibration factor was determined using the mobileMOSFET software. To improve the accuracy of calibration, this procedure was repeated ten times and the calibration factors were averaged. Results: As the number of calibrations was increasing the variability of calibration factors of different dosimeters was decreasing. After ten calibrations, the calibration factors for all five dosimeters were within 1% of one another for all energies, except 6 MV SRS photons and 6 MeV electrons, for which the variability was 2%. Conclusions: The described process results in calibration factors which are almost independent of modality or energy. Once calibrated, the dosimeters may be used for in-vivo dosimetry or for daily verification of the beam output. Measurement of the radiation dose under bolus and scatter to the eye are examples of frequent use of calibrated MOSFET dosimeters. The calibration factor determined for full build-up is used under these circumstances. To the best of our knowledge, such thorough procedure for calibrating MOSFET dosimeters has not been reported previously. Best Medical Canada provided MOSFET dosimeters for this project

  7. Air Data Calibration Facility

    Data.gov (United States)

    Federal Laboratory Consortium — This facility is for low altitude subsonic altimeter system calibrations of air vehicles. Mission is a direct support of the AFFTC mission. Postflight data merge is...

  8. SRHA calibration curve

    Data.gov (United States)

    U.S. Environmental Protection Agency — an UV calibration curve for SRHA quantitation. This dataset is associated with the following publication: Chang, X., and D. Bouchard. Surfactant-Wrapped Multiwalled...

  9. BES online calibration system

    International Nuclear Information System (INIS)

    Zhang Bingyun; Li Xiaonan; Zhu Kejun; Zhang Jiawen; Gong Mingyu

    2003-01-01

    We constructed BES (Beijing Spectrometer) online calibration system to ensure the coherence of readout electronic channels due to huge data volume in high energy physics experiment. This paper describes the structure of hardware and software, and its characteristic and function

  10. Calibrated Properties Model

    International Nuclear Information System (INIS)

    Ahlers, C.F.; Liu, H.H.

    2001-01-01

    The purpose of this Analysis/Model Report (AMR) is to document the Calibrated Properties Model that provides calibrated parameter sets for unsaturated zone (UZ) flow and transport process models for the Yucca Mountain Site Characterization Project (YMP). This work was performed in accordance with the AMR Development Plan for U0035 Calibrated Properties Model REV00 (CRWMS M and O 1999c). These calibrated property sets include matrix and fracture parameters for the UZ Flow and Transport Model (UZ Model), drift seepage models, drift-scale and mountain-scale coupled-processes models, and Total System Performance Assessment (TSPA) models as well as Performance Assessment (PA) and other participating national laboratories and government agencies. These process models provide the necessary framework to test conceptual hypotheses of flow and transport at different scales and predict flow and transport behavior under a variety of climatic and thermal-loading conditions

  11. Calibrated Properties Model

    International Nuclear Information System (INIS)

    Ahlers, C.; Liu, H.

    2000-01-01

    The purpose of this Analysis/Model Report (AMR) is to document the Calibrated Properties Model that provides calibrated parameter sets for unsaturated zone (UZ) flow and transport process models for the Yucca Mountain Site Characterization Project (YMP). This work was performed in accordance with the ''AMR Development Plan for U0035 Calibrated Properties Model REV00. These calibrated property sets include matrix and fracture parameters for the UZ Flow and Transport Model (UZ Model), drift seepage models, drift-scale and mountain-scale coupled-processes models, and Total System Performance Assessment (TSPA) models as well as Performance Assessment (PA) and other participating national laboratories and government agencies. These process models provide the necessary framework to test conceptual hypotheses of flow and transport at different scales and predict flow and transport behavior under a variety of climatic and thermal-loading conditions

  12. Scanner calibration revisited

    Directory of Open Access Journals (Sweden)

    Pozhitkov Alexander E

    2010-07-01

    Full Text Available Abstract Background Calibration of a microarray scanner is critical for accurate interpretation of microarray results. Shi et al. (BMC Bioinformatics, 2005, 6, Art. No. S11 Suppl. 2. reported usage of a Full Moon BioSystems slide for calibration. Inspired by the Shi et al. work, we have calibrated microarray scanners in our previous research. We were puzzled however, that most of the signal intensities from a biological sample fell below the sensitivity threshold level determined by the calibration slide. This conundrum led us to re-investigate the quality of calibration provided by the Full Moon BioSystems slide as well as the accuracy of the analysis performed by Shi et al. Methods Signal intensities were recorded on three different microarray scanners at various photomultiplier gain levels using the same calibration slide from Full Moon BioSystems. Data analysis was conducted on raw signal intensities without normalization or transformation of any kind. Weighted least-squares method was used to fit the data. Results We found that initial analysis performed by Shi et al. did not take into account autofluorescence of the Full Moon BioSystems slide, which led to a grossly distorted microarray scanner response. Our analysis revealed that a power-law function, which is explicitly accounting for the slide autofluorescence, perfectly described a relationship between signal intensities and fluorophore quantities. Conclusions Microarray scanners respond in a much less distorted fashion than was reported by Shi et al. Full Moon BioSystems calibration slides are inadequate for performing calibration. We recommend against using these slides.

  13. Calibrating nacelle lidars

    Energy Technology Data Exchange (ETDEWEB)

    Courtney, M.

    2013-01-15

    Nacelle mounted, forward looking wind lidars are beginning to be used to provide reference wind speed measurements for the power performance testing of wind turbines. In such applications, a formal calibration procedure with a corresponding uncertainty assessment will be necessary. This report presents four concepts for performing such a nacelle lidar calibration. Of the four methods, two are found to be immediately relevant and are pursued in some detail. The first of these is a line of sight calibration method in which both lines of sight (for a two beam lidar) are individually calibrated by accurately aligning the beam to pass close to a reference wind speed sensor. A testing procedure is presented, reporting requirements outlined and the uncertainty of the method analysed. It is seen that the main limitation of the line of sight calibration method is the time required to obtain a representative distribution of radial wind speeds. An alternative method is to place the nacelle lidar on the ground and incline the beams upwards to bisect a mast equipped with reference instrumentation at a known height and range. This method will be easier and faster to implement and execute but the beam inclination introduces extra uncertainties. A procedure for conducting such a calibration is presented and initial indications of the uncertainties given. A discussion of the merits and weaknesses of the two methods is given together with some proposals for the next important steps to be taken in this work. (Author)

  14. Calibration curve for germanium spectrometers from solutions calibrated by liquid scintillation counting

    International Nuclear Information System (INIS)

    Grau, A.; Navarro, N.; Rodriguez, L.; Alvarez, A.; Salvador, S.; Diaz, C.

    1996-01-01

    The beta-gamma emitters ''60Co, ''137 Cs, ''131 I, ''210 Pb y ''129 Iare radionuclides for which the calibration by the CIEMAT/NIST method ispossible with uncertainties less than 1%. We prepared, from standardized solutions of these radionuclides, samples in vials of 20 ml. We obtained the calibration curves, efficiency as a function of energy, for two germanium detectors. (Author) 5 refs

  15. Calibration of the Herschel SPIRE Fourier Transform Spectrometer

    OpenAIRE

    Swinyard, Bruce; Polehampton, E. T.; Hopwood, R.; Valtchanov, I.; Lu, N.; Fulton, T.; Benielli, D.; Imhof, P.; Marchili, N.; Baluteau, J.- P.; Bendo, G. J.; Ferlet, M.; Griffin, Matthew Jason; Lim, T. L.; Makiwa, G.

    2014-01-01

    The Herschel Spectral and Photometric REceiver (SPIRE) instrument consists of an imaging photometric camera and an imaging Fourier Transform Spectrometer (FTS), both operating over a frequency range of ∼450–1550 GHz. In this paper, we briefly review the FTS design, operation, and data reduction, and describe in detail the approach taken to relative calibration (removal of instrument signatures) and absolute calibration against standard astronomical sources. The calibration scheme assumes a sp...

  16. U.S. Department of Energy Office of Legacy Management Calibration Facilities - 12103

    Energy Technology Data Exchange (ETDEWEB)

    Barr, Deborah [U.S. Department of Energy Office of Legacy Management, Grand Junction, Colorado (United States); Traub, David; Widdop, Michael [S.M. Stoller Corporation, Grand Junction, Colorado (United States)

    2012-07-01

    This paper describes radiometric calibration facilities located in Grand Junction, Colorado, and at three secondary calibration sites. These facilities are available to the public for the calibration of radiometric field instrumentation for in-situ measurements of radium (uranium), thorium, and potassium. Both borehole and hand-held instruments may be calibrated at the facilities. Aircraft or vehicle mounted systems for large area surveys may be calibrated at the Grand Junction Regional Airport facility. These calibration models are recognized internationally as stable, well-characterized radiation sources for calibration. Calibration models built in other countries are referenced to the DOE models, which are also widely used as a standard for calibration within the U.S. Calibration models are used to calibrate radiation detectors used in uranium exploration, remediation, and homeland security. (authors)

  17. The Utilization of Background Spectrum to Calibrate Gamma Spectrometry

    International Nuclear Information System (INIS)

    Mahrouka, M. M.; Mutawa, A. M.

    2004-01-01

    Many developed countries have very poor reference standards to calibrate their nuclear instrumentations or may find some difficulties to obtain a reference standard. In this work a simple way for Gamma spectrometry calibration was developed. The method depends on one reference point and additional points from the background. The two derived equations were applied to the analyses of radioactive nuclides in soil and liquid samples prepared by IAEA laboratories through AL MERA Project. The results showed the precision of the methodology used, as well as, the possibility of using some points in the background spectrum as a replacement for reference standards of Gamma spectrometry calibration. (authors)

  18. User-calibration of Mettler AT200 analytical balance

    International Nuclear Information System (INIS)

    Estill, J.

    1996-01-01

    The purpose of this technical implementing procedure (TIP) is to describe the calibration of the Mettler AT200 analytical balance or similar type balance (henceforth called the balance). This balance is used for activities of the Scientific Investigation Plan (SIP) ''Metal Barrier Selection and Testing'' (SIP-CM-01, WBS nr. 1.2.2.5.1). In particular, it will be used for Activity E-20-50, ''Long-Term Corrosion Studies.'' The balance will be used for weighing test specimens and reagent chemicals. However, it is not limited to these uses. The calibration procedures consist of activating the internal (self) calibration of the apparatus, and weighing and recording of traceable standards. The balance is equipped with self (internal) calibration and linearization capabilities. It has an internal (built in) set of weights which are used for self calibration. The standard weights are traceable to National Institute of Standards and Technology (NIST)

  19. Calibration of areal surface topography measuring instruments

    Science.gov (United States)

    Seewig, J.; Eifler, M.

    2017-06-01

    The ISO standards which are related to the calibration of areal surface topography measuring instruments are the ISO 25178-6xx series which defines the relevant metrological characteristics for the calibration of different measuring principles and the ISO 25178-7xx series which defines the actual calibration procedures. As the field of areal measurement is however not yet fully standardized, there are still open questions to be addressed which are subject to current research. Based on this, selected research results of the authors in this area are presented. This includes the design and fabrication of areal material measures. For this topic, two examples are presented with the direct laser writing of a stepless material measure for the calibration of the height axis which is based on the Abbott- Curve and the manufacturing of a Siemens star for the determination of the lateral resolution limit. Based on these results, as well a new definition for the resolution criterion, the small scale fidelity, which is still under discussion, is presented. Additionally, a software solution for automated calibration procedures is outlined.

  20. Vibration transducer calibration techniques

    Science.gov (United States)

    Brinkley, D. J.

    1980-09-01

    Techniques for the calibration of vibration transducers used in the Aeronautical Quality Assurance Directorate of the British Ministry of Defence are presented. Following a review of the types of measurements necessary in the calibration of vibration transducers, the performance requirements of vibration transducers, which can be used to measure acceleration, velocity or vibration amplitude, are discussed, with particular attention given to the piezoelectric accelerometer. Techniques for the accurate measurement of sinusoidal vibration amplitude in reference-grade transducers are then considered, including the use of a position sensitive photocell and the use of a Michelson laser interferometer. Means of comparing the output of working-grade accelerometers with that of previously calibrated reference-grade devices are then outlined, with attention given to a method employing a capacitance bridge technique and a method to be used at temperatures between -50 and 200 C. Automatic calibration procedures developed to speed up the calibration process are outlined, and future possible extensions of system software are indicated.

  1. Calibration Under Uncertainty.

    Energy Technology Data Exchange (ETDEWEB)

    Swiler, Laura Painton; Trucano, Timothy Guy

    2005-03-01

    This report is a white paper summarizing the literature and different approaches to the problem of calibrating computer model parameters in the face of model uncertainty. Model calibration is often formulated as finding the parameters that minimize the squared difference between the model-computed data (the predicted data) and the actual experimental data. This approach does not allow for explicit treatment of uncertainty or error in the model itself: the model is considered the %22true%22 deterministic representation of reality. While this approach does have utility, it is far from an accurate mathematical treatment of the true model calibration problem in which both the computed data and experimental data have error bars. This year, we examined methods to perform calibration accounting for the error in both the computer model and the data, as well as improving our understanding of its meaning for model predictability. We call this approach Calibration under Uncertainty (CUU). This talk presents our current thinking on CUU. We outline some current approaches in the literature, and discuss the Bayesian approach to CUU in detail.

  2. Automated intraoperative calibration for prostate cancer brachytherapy

    International Nuclear Information System (INIS)

    Kuiran Chen, Thomas; Heffter, Tamas; Lasso, Andras; Pinter, Csaba; Abolmaesumi, Purang; Burdette, E. Clif; Fichtinger, Gabor

    2011-01-01

    Purpose: Prostate cancer brachytherapy relies on an accurate spatial registration between the implant needles and the TRUS image, called ''calibration''. The authors propose a new device and a fast, automatic method to calibrate the brachytherapy system in the operating room, with instant error feedback. Methods: A device was CAD-designed and precision-engineered, which mechanically couples a calibration phantom with an exact replica of the standard brachytherapy template. From real-time TRUS images acquired from the calibration device and processed by the calibration system, the coordinate transformation between the brachytherapy template and the TRUS images was computed automatically. The system instantly generated a report of the target reconstruction accuracy based on the current calibration outcome. Results: Four types of validation tests were conducted. First, 50 independent, real-time calibration trials yielded an average of 0.57 ± 0.13 mm line reconstruction error (LRE) relative to ground truth. Second, the averaged LRE was 0.37 ± 0.25 mm relative to ground truth in tests with six different commercial TRUS scanners operating at similar imaging settings. Furthermore, testing with five different commercial stepper systems yielded an average of 0.29 ± 0.16 mm LRE relative to ground truth. Finally, the system achieved an average of 0.56 ± 0.27 mm target registration error (TRE) relative to ground truth in needle insertion tests through the template in a water tank. Conclusions: The proposed automatic, intraoperative calibration system for prostate cancer brachytherapy has achieved high accuracy, precision, and robustness.

  3. System for calibration of SPEAR transport line toroids

    International Nuclear Information System (INIS)

    Huang, T.V.; Smith, H.; Crook, K.

    1977-01-01

    A one nanosecond pulse generator was developed for calibration of the intensity monitors (toroids) in the SPEAR transport lines. The generator, located at the toroid, is simple, low cost and resistant to radiation. The generator and its connection to the standard SLAC toroid calibration system are described

  4. 30 CFR 90.203 - Certified person; maintenance and calibration.

    Science.gov (United States)

    2010-07-01

    ... COAL MINE SAFETY AND HEALTH MANDATORY HEALTH STANDARDS-COAL MINERS WHO HAVE EVIDENCE OF THE DEVELOPMENT OF PNEUMOCONIOSIS Sampling Procedures § 90.203 Certified person; maintenance and calibration. (a) Approved sampling devices shall be maintained and calibrated by a certified person. (b) To be certified, a...

  5. The NRPB Chilton Calibration Laboratory for radiological protection measurements

    International Nuclear Information System (INIS)

    Iles, W.J.

    1982-01-01

    The Calibration Laboratory in NRPB Headquarters is intended as an authoritative reference laboratory for all aspects of radiation protection level instrument calibrations for X-, gamma and beta radiations and to be complementary to the national primary standards of the National Physical Laboratory. The gamma ray, filtered X-ray, fluorescence X-ray and beta ray facilities are described. (U.K.)

  6. 21 CFR 58.63 - Maintenance and calibration of equipment.

    Science.gov (United States)

    2010-04-01

    ... GOOD LABORATORY PRACTICE FOR NONCLINICAL LABORATORY STUDIES Equipment § 58.63 Maintenance and... 21 Food and Drugs 1 2010-04-01 2010-04-01 false Maintenance and calibration of equipment. 58.63..., maintenance, testing, calibration, and/or standardization of equipment, and shall specify, when appropriate...

  7. Ibis ground calibration

    International Nuclear Information System (INIS)

    Bird, A.J.; Barlow, E.J.; Tikkanen, T.; Bazzano, A.; Del Santo, M.; Ubertini, P.; Blondel, C.; Laurent, P.; Lebrun, F.; Di Cocco, G.; Malaguti, E.; Gabriele, M.; La Rosa, G.; Segreto, A.; Quadrini, E.; Volkmer, R.

    2003-01-01

    We present an overview of results obtained from IBIS ground calibrations. The spectral and spatial characteristics of the detector planes and surrounding passive materials have been determined through a series of calibration campaigns. Measurements of pixel gain, energy resolution, detection uniformity, efficiency and imaging capability are presented. The key results obtained from the ground calibration have been: - optimization of the instrument tunable parameters, - determination of energy linearity for all detection modes, - determination of energy resolution as a function of energy through the range 20 keV - 3 MeV, - demonstration of imaging capability in each mode, - measurement of intrinsic detector non-uniformity and understanding of the effects of passive materials surrounding the detector plane, and - discovery (and closure) of various leakage paths through the passive shielding system

  8. Gamma counter calibration system

    International Nuclear Information System (INIS)

    1977-01-01

    A method and apparatus are described for the calibration of a gamma radiation measurement instrument to be used over any of a number of different absolute energy ranges. The method includes the steps of adjusting the overall signal gain associated with pulses which are derived from detected gamma rays, until the instrument is calibrated for a particular absolute energy range; then storing parameter settings corresponding to the adjusted overall signal gain, and repeating the process for other desired absolute energy ranges. The stored settings can be subsequently retrieved and reapplied so that test measurements can be made using a selected one of the absolute energy ranges. Means are provided for adjusting the overall signal gain and a specific technique is disclosed for making coarse, then fine adjustments to the signal gain, for rapid convergence of the required calibration settings. (C.F.)

  9. Individual dosimetry and calibration

    International Nuclear Information System (INIS)

    Hoefert, M.; Nielsen, M.

    1996-01-01

    In 1995 both the Individual Dosimetry and Calibration Sections worked under the condition of a status quo and concentrated fully on the routine part of their work. Nevertheless, the machine for printing the bar code which will be glued onto the film holder and hence identify the people when entering into high radiation areas was put into operation and most of the holders were equipped with the new identification. As far as the Calibration Section is concerned the project of the new source control system that is realized by the Technical Support Section was somewhat accelerated

  10. Calibration of scanning Lidar

    DEFF Research Database (Denmark)

    Gómez Arranz, Paula; Courtney, Michael

    This report describes the tests carried out on a scanning lidar at the DTU Test Station for large wind turbines, Høvsøre. The tests were divided in two parts. In the first part, the purpose was to obtain wind speed calibrations at two heights against two cup anemometers mounted on a mast. Additio......This report describes the tests carried out on a scanning lidar at the DTU Test Station for large wind turbines, Høvsøre. The tests were divided in two parts. In the first part, the purpose was to obtain wind speed calibrations at two heights against two cup anemometers mounted on a mast...

  11. Calibration of ionization chambers used in LDR brachytherapy

    International Nuclear Information System (INIS)

    Alvarez, Oscar T.B.; Caldas, Linda V.E.

    2005-01-01

    In this work was developed a calibration procedure of well-type ionization chambers used for measurements of I-125, seed type. It was used as a standard an ionization chamber Capintec CRC-15BT, with calibration certificate of the University of Wisconsin. It were calibrated two well-type ionization chambers of Capintec CRC-15R model. A source of I-125 was used in clinical use (18.5 to 7.4 MBq). The results showed that with the application of calibration factors was possible to decrease read deviate from 16% to just 1.0%

  12. AFM lateral force calibration for an integrated probe using a calibration grating

    International Nuclear Information System (INIS)

    Wang, Huabin; Gee, Michelle L.

    2014-01-01

    Atomic force microscopy (AFM) friction measurements on hard and soft materials remain a challenge due to the difficulties associated with accurately calibrating the cantilever for lateral force measurement. One of the most widely accepted lateral force calibration methods is the wedge method. This method is often used in a simplified format but in so doing sacrifices accuracy. In the present work, we have further developed the wedge method to provide a lateral force calibration method for integrated AFM probes that is easy to use without compromising accuracy and reliability. Raw friction calibration data are collected from a single scan image by continuous ramping of the set point as the facets of a standard grating are scanned. These data are analysed to yield an accurate lateral force conversion/calibration factor that is not influenced by adhesion forces or load deviation. By demonstrating this new calibration method, we illustrate its reliability, speed and ease of execution. This method makes accessible reliable boundary lubrication studies on adhesive and heterogeneous surfaces that require spatial resolution of frictional forces. - Highlights: • We develop a simple and accurate method for lateral force calibration in AFM friction measurements. • We detail the basis of the method and illustrate how to use it and its reliability with example data. • Our method is easy, accurate and accounts for the affects of adhesion on friction measurements. • The method is applicable to integrated probes, as opposed to colloidal probes. • This allows accurate AFM friction measurements on spatially heterogeneous and adhesive surfaces

  13. Critical issues for implementation of the standard NBR ISO/IEC 17025:2005 in Testing and Calibration Laboratory: case study at a public institution; Aspectos criticos para implantacao da norma NBR ISO/IEC 17025:2005 em laboratorio de ensaio e calibracao: estudo de caso em uma instituicao publica

    Energy Technology Data Exchange (ETDEWEB)

    Castro, Denise Confar Carvalho de

    2013-07-01

    The public institution aims to promote excellence in public management to contribute to the quality of services provided to its customers and to increase competitiveness in the country, as well as its international projection. A technical barrier to trade that can lead to dissatisfaction and achieve the reputation of the institution is failing the test or calibration results and measurement data, thereby accreditation is regarded as the first essential step to facilitate the mutual acceptance of test results and calibration or measurement data. For recognition, laboratories need to demonstrate full compliance with both the sections of ISO/IEC 17025:2005, i.e. management and technical requirements. This research aims to discuss the critical aspects for implementation of ABNT NBR ISO / IEC 17025:2005 for calibration and testing of a Public Institution seeking accreditation of its laboratories with INMETRO, national accreditation body Laboratories. Besides getting preventive, corrective and improvement actions continues guidelines. Furthermore, the methodology used was to conduct a literature search and apply a questionnaire to identify the degree of agreement / disagreement of the foundations of the standard servers. Analysis of the results showed that the critical issues were: commitment, training, resources (infrastructure, human) and culture. (author)

  14. Calibration-measurement unit for the automation of vector network analyzer measurements

    Directory of Open Access Journals (Sweden)

    I. Rolfes

    2008-05-01

    Full Text Available With the availability of multi-port vector network analyzers, the need for automated, calibrated measurement facilities increases. In this contribution, a calibration-measurement unit is presented which realizes a repeatable automated calibration of the measurement setup as well as a user-friendly measurement of the device under test (DUT. In difference to commercially available calibration units, which are connected to the ports of the vector network analyzer preceding a measurement and which are then removed so that the DUT can be connected, the presented calibration-measurement unit is permanently connected to the ports of the VNA for the calibration as well as for the measurement of the DUT. This helps to simplify the calibrated measurement of complex scattering parameters. Moreover, a full integration of the calibration unit into the analyzer setup becomes possible. The calibration-measurement unit is based on a multiport switch setup of e.g. electromechanical relays. Under the assumption of symmetry of a switch, on the one hand the unit realizes the connection of calibration standards like one-port reflection standards and two-port through connections between different ports and on the other hand it enables the connection of the DUT. The calibration-measurement unit is applicable for two-port VNAs as well as for multiport VNAs. For the calibration of the unit, methods with completely known calibration standards like SOLT (short, open, load, through as well as self-calibration procedures like TMR or TLR can be applied.

  15. Measurement quality assurance for beta particle calibrations at NIST

    International Nuclear Information System (INIS)

    Soares, C.G.; Pruitt, J.S.

    1993-01-01

    Standardized beta-particle fields have been established in an international standard and have been adopted for use in several U.S. dosimeter and instrument testing standards. Calibration methods and measurement quality assurance procedures employed at the National Institute of Standards and Technology (NIST) for beta-particle calibrations in these reference fields are discussed. The calibration facility including the NIST-automated extrapolation ionization chamber is described, and some sample results of calibrations are shown. Methods for establishing and maintaining traceability to NIST of secondary laboratories are discussed. Currently, there are problems in finding a good method for routine testing of traceability to NIST. Some examples of past testing methods are given and solutions to this problem are proposed

  16. Measurement quality assurance for beta particle calibrations at NIST

    Energy Technology Data Exchange (ETDEWEB)

    Soares, C.G.; Pruitt, J.S. [National Institute of Standards and Technology, Gaithersburg, MD (United States)

    1993-12-31

    Standardized beta-particle fields have been established in an international standard and have been adopted for use in several U.S. dosimeter and instrument testing standards. Calibration methods and measurement quality assurance procedures employed at the National Institute of Standards and Technology (NIST) for beta-particle calibrations in these reference fields are discussed. The calibration facility including the NIST-automated extrapolation ionization chamber is described, and some sample results of calibrations are shown. Methods for establishing and maintaining traceability to NIST of secondary laboratories are discussed. Currently, there are problems in finding a good method for routine testing of traceability to NIST. Some examples of past testing methods are given and solutions to this problem are proposed.

  17. Weston Standard battery

    CERN Multimedia

    This is a Weston AOIP standard battery with its calibration certificate (1956). Inside, the glassware forms an "H". Its name comes from the British physicist Edward Weston. A standard is the materialization of a given quantity whose value is known with great accuracy.

  18. ECAL Energy Flow Calibration

    CERN Multimedia

    CERN. Geneva

    2015-01-01

    My talk will be covering my work as a whole over the course of the semester. The focus will be on using energy flow calibration in ECAL to check the precision of the corrections made by the light monitoring system used to account for transparency loss within ECAL crystals due to radiation damage over time.

  19. Calibration with Absolute Shrinkage

    DEFF Research Database (Denmark)

    Øjelund, Henrik; Madsen, Henrik; Thyregod, Poul

    2001-01-01

    In this paper, penalized regression using the L-1 norm on the estimated parameters is proposed for chemometric je calibration. The algorithm is of the lasso type, introduced by Tibshirani in 1996 as a linear regression method with bound on the absolute length of the parameters, but a modification...

  20. Gamma ray calibration system

    International Nuclear Information System (INIS)

    Rosauer, P.J.; Flaherty, J.J.

    1981-01-01

    This invention is in the field of gamma ray inspection devices for tubular products and the like employing an improved calibrating block which prevents the sensing system from being overloaded when no tubular product is present, and also provides the operator with a means for visually detecting the presence of wall thicknesses which are less than a required minimum. (author)

  1. PLEIADES ABSOLUTE CALIBRATION : INFLIGHT CALIBRATION SITES AND METHODOLOGY

    Directory of Open Access Journals (Sweden)

    S. Lachérade

    2012-07-01

    Full Text Available In-flight calibration of space sensors once in orbit is a decisive step to be able to fulfil the mission objectives. This article presents the methods of the in-flight absolute calibration processed during the commissioning phase. Four In-flight calibration methods are used: absolute calibration, cross-calibration with reference sensors such as PARASOL or MERIS, multi-temporal monitoring and inter-bands calibration. These algorithms are based on acquisitions over natural targets such as African deserts, Antarctic sites, La Crau (Automatic calibration station and Oceans (Calibration over molecular scattering or also new extra-terrestrial sites such as the Moon and selected stars. After an overview of the instrument and a description of the calibration sites, it is pointed out how each method is able to address one or several aspects of the calibration. We focus on how these methods complete each other in their operational use, and how they help building a coherent set of information that addresses all aspects of in-orbit calibration. Finally, we present the perspectives that the high level of agility of PLEIADES offers for the improvement of its calibration and a better characterization of the calibration sites.

  2. Characterisation of a protection level Am-241 calibration source

    Science.gov (United States)

    Bass, G. A.; Rossiter, M. J.; Williams, T. T.

    1992-11-01

    The various measurements involved in the commissioning process of an Am-241 radioactive source and transport mechanisms to be used for protection level calibration work are detailed. The source and its handling mechanisms are described and measurements to characterize the resultant gamma ray beam are described. For the beam measurements, the inverse square law is investigated and beam uniformity is assessed. A trial calibration of ionization chambers is described. The Am-241 irradiation facility is concluded to be suitable for calibrating secondary standards as part of the calibration service offered for protection level instruments. The umbra part of beam is acceptably uniform for a range of chambers and the measurements obtained were predictable and consistent. This quality will be added to the range of qualities offered as part of the protection level secondary standard calibration service.

  3. Proceedings of the workshop on radiation survey instruments and calibrations

    International Nuclear Information System (INIS)

    Selby, J.M.; Swinth, K.L.; Vallario, E.J.; Murphy, B.L.

    1985-11-01

    The workshop was held to discuss two topics: first, a performance standard for radiation survey instruments and the potential for a testing program based on that standard; and second, a system of secondary standards laboratories to provide instrument calibrations and related services. Separate abstracts have been prepared for the individual presentations

  4. Field calibration of cup anemometers

    DEFF Research Database (Denmark)

    Schmidt Paulsen, Uwe; Mortensen, Niels Gylling; Hansen, Jens Carsten

    2007-01-01

    A field calibration method and results are described along with the experience gained with the method. The cup anemometers to be calibrated are mounted in a row on a 10-m high rig and calibrated in the free wind against a reference cup anemometer. The method has been reported [1] to improve...... the statistical bias on the data relative to calibrations carried out in a wind tunnel. The methodology is sufficiently accurate for calibration of cup anemometers used for wind resource assessments and provides a simple, reliable and cost-effective solution to cup anemometer calibration, especially suited...

  5. Calibration of the MACHO Photometry Database

    International Nuclear Information System (INIS)

    Alcock, C.; Allsman, R. A.; Alves, D. R.; Axelrod, T. S.; Becker, A. C.; Bennett, D. P.; Cook, K. H.; Drake, A. J.; Freeman, K. C.; Geha, M.

    1999-01-01

    The MACHO Project is a microlensing survey that monitors the brightnesses of ∼60 million stars in the Large Magellanic Cloud (LMC), Small Magellanic Cloud, and Galactic bulge. Our database presently contains about 80 billion photometric measurements, a significant fraction of all astronomical photometry. We describe the calibration of MACHO two-color photometry and transformation to the standard Kron-Cousins V and R system. Calibrated MACHO photometry may be properly compared with all other observations on the Kron-Cousins standard system, enhancing the astrophysical value of these data. For ∼9 million stars in the LMC bar, independent photometric measurements of ∼20,000 stars with V(less-or-similar sign)18 mag in field-overlap regions demonstrate an internal precision σ V =0.021, σ R =0.019, σ V-R =0.028 mag. The accuracy of the zero point in this calibration is estimated to be ±0.035 mag for stars with colors in the range -0.1 mag< V-R<1.2 mag. A comparison of calibrated MACHO photometry with published photometric sequences and new Hubble Space Telescope observations shows agreement. The current calibration zero-point uncertainty for the remainder of the MACHO photometry database is estimated to be ±0.10 mag in V or R and ±0.04 mag in V-R. We describe the first application of calibrated MACHO data: the construction of a color-magnitude diagram used to calculate our experimental sensitivity for detecting microlensing in the LMC. (c) (c) 1999. The Astronomical Society of the Pacific

  6. Calibration of the MACHO Photometry Database

    Energy Technology Data Exchange (ETDEWEB)

    Alcock, C.; Allsman, R. A.; Alves, D. R.; Axelrod, T. S.; Becker, A. C.; Bennett, D. P.; Cook, K. H.; Drake, A. J.; Freeman, K. C.; Geha, M. (and others)

    1999-12-01

    The MACHO Project is a microlensing survey that monitors the brightnesses of {approx}60 million stars in the Large Magellanic Cloud (LMC), Small Magellanic Cloud, and Galactic bulge. Our database presently contains about 80 billion photometric measurements, a significant fraction of all astronomical photometry. We describe the calibration of MACHO two-color photometry and transformation to the standard Kron-Cousins V and R system. Calibrated MACHO photometry may be properly compared with all other observations on the Kron-Cousins standard system, enhancing the astrophysical value of these data. For {approx}9 million stars in the LMC bar, independent photometric measurements of {approx}20,000 stars with V(less-or-similar sign)18 mag in field-overlap regions demonstrate an internal precision {sigma}{sub V} =0.021, {sigma}{sub R} =0.019, {sigma}{sub V-R} =0.028 mag. The accuracy of the zero point in this calibration is estimated to be {+-}0.035 mag for stars with colors in the range -0.1 magcalibrated MACHO photometry with published photometric sequences and new Hubble Space Telescope observations shows agreement. The current calibration zero-point uncertainty for the remainder of the MACHO photometry database is estimated to be {+-}0.10 mag in V or R and {+-}0.04 mag in V-R. We describe the first application of calibrated MACHO data: the construction of a color-magnitude diagram used to calculate our experimental sensitivity for detecting microlensing in the LMC. (c) (c) 1999. The Astronomical Society of the Pacific.

  7. Improving calibration accuracy in gel dosimetry

    International Nuclear Information System (INIS)

    Oldham, M.; McJury, M.; Webb, S.; Baustert, I.B.; Leach, M.O.

    1998-01-01

    A new method of calibrating gel dosimeters (applicable to both Fricke and polyacrylamide gels) is presented which has intrinsically higher accuracy than current methods, and requires less gel. Two test-tubes of gel (inner diameter 2.5 cm, length 20 cm) are irradiated separately with a 10x10cm 2 field end-on in a water bath, such that the characteristic depth-dose curve is recorded in the gel. The calibration is then determined by fitting the depth-dose measured in water, against the measured change in relaxivity with depth in the gel. Increased accuracy is achieved in this simple depth-dose geometry by averaging the relaxivity at each depth. A large number of calibration data points, each with relatively high accuracy, are obtained. Calibration data over the full range of dose (1.6-10 Gy) is obtained by irradiating one test-tube to 10 Gy at dose maximum (D max ), and the other to 4.5 Gy at D max . The new calibration method is compared with a 'standard method' where five identical test-tubes of gel were irradiated to different known doses between 2 and 10 Gy. The percentage uncertainties in the slope and intercept of the calibration fit are found to be lower with the new method by a factor of about 4 and 10 respectively, when compared with the standard method and with published values. The gel was found to respond linearly within the error bars up to doses of 7 Gy, with a slope of 0.233±0.001 s -1 Gy -1 and an intercept of 1.106±0.005 Gy. For higher doses, nonlinear behaviour was observed. (author)

  8. Thermal neutron calibration of a tritium extraction facility using the 6Li(n,t)4He/197Au(n,γ)198Au cross section ratio for standardization

    International Nuclear Information System (INIS)

    Bretscher, M.M.; Smith, D.L.

    1980-08-01

    Absolute tritium activities in a neutron-activated metallic lithium samples have been measured by liquid scintillation methods to provide data needed for the determination of capture-to-fission ratios in fast breeder reactor spectra and for recent measurements of the 7 Li(n,n't) 4 He cross section. The tritium extraction facility used for all these experiments has now been calibrated by measuring the 6 Li(n,t) 4 He/ 197 Au/n,γ) 198 Au activity ratio for thermal neutrons and comparing the result with the well-known cross sections. The calculated-to-measured activity ratio was found to be 1.033 +- 0.018. 2 figures, 20 tables

  9. A portable, automated, inexpensive mass and balance calibration system

    International Nuclear Information System (INIS)

    Maxwell, S.L. III; Clark, J.P.

    1987-01-01

    Reliable mass measurements are essential for a nuclear production facility or process control laboratory. DOE Order 5630.2 requires that traceable standards be used to calibrate and monitor equipment used for nuclear material measurements. To ensure the reliability of mass measurements and to comply with DOE traceable requirements, a portable, automated mass and balance calibration system is used at the Savannah River Plant. Automation is achieved using an EPSON HX-20 notebook computer, which can be operated via RS232C interfacing to electronic balances or function with manual data entry if computer interfacing is not feasible. This economical, comprehensive, user-friendly system has three main functions in a mass measurement control program (MMCP): balance certification, calibration of mass standards, and daily measurement of traceable standards. The balance certification program tests for accuracy, precision, sensitivity, linearity, and cornerloading versus specific requirements. The mass calibration program allows rapid calibration of inexpensive mass standards traceable to certified Class S standards. This MMCP permits daily measurement of traceable standards to monitor the reliability of balances during routine use. The automated system verifies balance calibration, stores results for future use, and provides a printed control chart of the stored data. Another feature of the system permits three different weighing routines that accommodate our need for varying degrees of reliability in routine weighing operations. 1 ref

  10. A portable, automated, inexpensive mass and balance calibration system

    International Nuclear Information System (INIS)

    Maxwell, S.L. III; Clark, J.P.

    1987-01-01

    Reliable mass measurements are essential for a nuclear production facility or process control laboratory. DOE Order 5630.2 requires that traceable standards be used to calibrate and monitor equipment used for nuclear material measurements. To ensure the reliability of mass measurements and to comply with DOE traceability requirements, a portable, automated mass and balance calibration system is used at the Savannah River Plant. Automation is achieved using an EPSON HX-20 notebook computer, which can be operated via RS232C interfacing to electronic balances or function with manual data entry if computer interfacing is not feasible. This economical, comprehensive, user-friendly system has three main functions in a mass measurement control program (MMCP): balance certification, calibration of mass standards, and daily measurement of traceable standards. The balance certification program tests for accuracy, precision, sensitivity, linearity, and cornerloading versus specific requirements. The mass calibration program allows rapid calibration of inexpensive mass standards traceable to certified Class S standards. This MMCP permits daily measurement of traceable standards to monitor the reliability of balances during routine use. The automated system verifies balance calibration, stores results for future use, and provides a printed control chart of the stored data. Another feature of the system permits three different weighing routines that accommodate their need for varying degrees of reliability in routine weighing operations

  11. Metrological reliability of the calibration procedure in terms of air kerma using the ionization chamber NE2575

    International Nuclear Information System (INIS)

    Guimaraes, Margarete Cristina; Silva, Teogenes Augusto da; Rosado, Paulo H.G.

    2016-01-01

    Metrology laboratories are expected to provide X radiation beams that were established by international standardization organizations to perform calibration and testing of dosimeters. Reliable and traceable standard dosimeters should be used in the calibration procedure. The aim of this work was to study the reliability of the NE 2575 ionization chamber used as standard dosimeter for the air kerma calibration procedure adopted in the CDTN Calibration Laboratory. (author)

  12. Computerized 50 liter volume calibration system

    International Nuclear Information System (INIS)

    Proffitt, T.H.

    1990-01-01

    A system has been designed for the Savannah River Site that will be used to calibrate product shipping containers. For accountability purposes, it is necessary that these containers be calibrated to a very high precision. The Computerized 50 Liter Volume Calibration System (CVCS), which is based on the Ideal Gas Law (IGL), will use reference volumes with precision of no less ±0.03%, and helium to calibrate the containers to have a total error of no greater than ±0.10%. A statistical interpretation of the system has given a theoretical total calculated error of ±0.08%. Tests with the system will be performed once fabrication is complete to experimentally verify the calculated error. Since the total error was calculated using the worst case scenario, the actual error should be significantly less than the calculated value. The computer controlled, totally automated system is traceable to the National Institute of Standards and Technology. The design, calibration procedure, and statistical interpretation of the system will be discussed. 1 ref

  13. Comparison of infusion pumps calibration methods

    Science.gov (United States)

    Batista, Elsa; Godinho, Isabel; do Céu Ferreira, Maria; Furtado, Andreia; Lucas, Peter; Silva, Claudia

    2017-12-01

    Nowadays, several types of infusion pump are commonly used for drug delivery, such as syringe pumps and peristaltic pumps. These instruments present different measuring features and capacities according to their use and therapeutic application. In order to ensure the metrological traceability of these flow and volume measuring equipment, it is necessary to use suitable calibration methods and standards. Two different calibration methods can be used to determine the flow error of infusion pumps. One is the gravimetric method, considered as a primary method, commonly used by National Metrology Institutes. The other calibration method, a secondary method, relies on an infusion device analyser (IDA) and is typically used by hospital maintenance offices. The suitability of the IDA calibration method was assessed by testing several infusion instruments at different flow rates using the gravimetric method. In addition, a measurement comparison between Portuguese Accredited Laboratories and hospital maintenance offices was performed under the coordination of the Portuguese Institute for Quality, the National Metrology Institute. The obtained results were directly related to the used calibration method and are presented in this paper. This work has been developed in the framework of the EURAMET projects EMRP MeDD and EMPIR 15SIP03.

  14. Laboratory implantation for well type ionization chambers calibration; Implantacao de um laboratorio para calibracao de camaras de ionizacao tipo poco

    Energy Technology Data Exchange (ETDEWEB)

    Vianello, E.A.; Dias, D.J.; Almeida, C.E. de [Laboratorio de Ciencias Radiologicas- LCR- DBB (UERJ). R. Sao Francisco Xavier, 524- Pav. HLC, sala 136 terreo- CEP 20.550-013. Rio de Janeiro (Brazil)

    1998-12-31

    The Radiological Science Laboratory is implanting a service for calibration of well type chambers by IAEA training program. The kerma rate in the air (mu Gy/h) of the linear Cs-137 reference source CDCS-J4 have been determined using a well type chamber Standard Imaging HDR-1000 model, which have been calibrated at Secondary Standard Laboratory Calibration of IAEA, whereas two HDR-1000 Plus chambers were calibrated too, following the same standards. The results were compared with Wisconsin University calibration certification and has demonstrated that well type ionization chamber calibration can be used in brachytherapy for several kinds of radionuclides. (Author)

  15. New Theoretical Analysis of the LRRM Calibration Technique for Vector Network Analyzers

    OpenAIRE

    Purroy Martín, Francesc; Pradell i Cara, Lluís

    2001-01-01

    In this paper, a new theoretical analysis of the four-standards line-reflect-reflect-match (LRRM) vector network-analyzer (VNA) calibration technique is presented. As a result, it is shown that the reference-impedance (to which the LRRM calibration is referred) cannot generally be defined whenever nonideal standards are used. Based on this consideration, a new algorithm to determine the on-wafer match standard is proposed that improves the LRRM calibration accuracy. Experimental verification ...

  16. MAVEN SEP Calibrated Data Bundle

    Data.gov (United States)

    National Aeronautics and Space Administration — The maven.sep.calibrated Level 2 Science Data Bundle contains fully calibrated SEP data, as well as the raw count data from which they are derived, and ancillary...

  17. Ultrasonic calibration assembly

    International Nuclear Information System (INIS)

    1981-01-01

    Ultrasonic transducers for in-service inspection of nuclear reactor vessels have several problems associated with them which this invention seeks to overcome. The first is that of calibration or referencing a zero start point for the vertical axis of transducer movement to locate a weld defect. The second is that of verifying the positioning (vertically or at a predetermined angle). Thirdly there is the problem of ascertaining the speed per unit distance in the operating medium of the transducer beam prior to the actual inspection. The apparatus described is a calibration assembly which includes a fixed, generally spherical body having a surface for reflecting an ultrasonic beam from one of the transducers which can be moved until the reflection from the spherical body is the highest amplitude return signal indicating radial alignment from the body. (U.K.)

  18. Travelling gradient thermocouple calibration

    International Nuclear Information System (INIS)

    Broomfield, G.H.

    1975-01-01

    A short discussion of the origins of the thermocouple EMF is used to re-introduce the idea that the Peltier and Thompson effects are indistinguishable from one another. Thermocouples may be viewed as devices which generate an EMF at junctions or as integrators of EMF's developed in thermal gradients. The thermal gradient view is considered the more appropriate, because of its better accord with theory and behaviour, the correct approach to calibration, and investigation of service effects is immediately obvious. Inhomogeneities arise in thermocouples during manufacture and in service. The results of travelling gradient measurements are used to show that such effects are revealed with a resolution which depends on the length of the gradient although they may be masked during simple immersion calibration. Proposed tests on thermocouples irradiated in a nuclear reactor are discussed

  19. Mesoscale hybrid calibration artifact

    Science.gov (United States)

    Tran, Hy D.; Claudet, Andre A.; Oliver, Andrew D.

    2010-09-07

    A mesoscale calibration artifact, also called a hybrid artifact, suitable for hybrid dimensional measurement and the method for make the artifact. The hybrid artifact has structural characteristics that make it suitable for dimensional measurement in both vision-based systems and touch-probe-based systems. The hybrid artifact employs the intersection of bulk-micromachined planes to fabricate edges that are sharp to the nanometer level and intersecting planes with crystal-lattice-defined angles.

  20. Calibration of germanium detectors

    International Nuclear Information System (INIS)

    Bjurman, B.; Erlandsson, B.

    1985-01-01

    This paper describes problems concerning the calibration of germanium detectors for the measurement of gamma-radiation from environmental samples. It also contains a brief description of some ways of reducing the uncertainties concerning the activity determination. These uncertainties have many sources, such as counting statistics, full energy peak efficiency determination, density correction and radionuclide specific-coincidence effects, when environmental samples are investigated at close source-to-detector distances

  1. Calibration of hydrometers

    Science.gov (United States)

    Lorefice, Salvatore; Malengo, Andrea

    2006-10-01

    After a brief description of the different methods employed in periodic calibration of hydrometers used in most cases to measure the density of liquids in the range between 500 kg m-3 and 2000 kg m-3, particular emphasis is given to the multipoint procedure based on hydrostatic weighing, known as well as Cuckow's method. The features of the calibration apparatus and the procedure used at the INRiM (formerly IMGC-CNR) density laboratory have been considered to assess all relevant contributions involved in the calibration of different kinds of hydrometers. The uncertainty is strongly dependent on the kind of hydrometer; in particular, the results highlight the importance of the density of the reference buoyant liquid, the temperature of calibration and the skill of operator in the reading of the scale in the whole assessment of the uncertainty. It is also interesting to realize that for high-resolution hydrometers (division of 0.1 kg m-3), the uncertainty contribution of the density of the reference liquid is the main source of the total uncertainty, but its importance falls under about 50% for hydrometers with a division of 0.5 kg m-3 and becomes somewhat negligible for hydrometers with a division of 1 kg m-3, for which the reading uncertainty is the predominant part of the total uncertainty. At present the best INRiM result is obtained with commercially available hydrometers having a scale division of 0.1 kg m-3, for which the relative uncertainty is about 12 × 10-6.

  2. Dosimetry and Calibration Section

    International Nuclear Information System (INIS)

    Otto, T.

    1998-01-01

    The two tasks of the Dosimetry and Calibration Section at CERN are the Individual Dosimetry Service which assures the personal monitoring of about 5000 persons potentially exposed to ionizing radiation at CERN, and the Calibration Laboratory which verifies all the instruments and monitors. This equipment is used by the sections of the RP Group for assuring radiation protection around CERN's accelerators, and by the Environmental Section of TISTE. In addition, nearly 250 electronic and 300 quartz fibre dosimeters, employed in operational dosimetry, are calibrated at least once a year. The Individual Dosimetry Service uses an extended database (INDOS) which contains information about all the individual doses ever received at CERN. For most of 1997 it was operated without the support of a database administrator as the technician who had assured this work retired. The Software Support Section of TIS-TE took over the technical responsibility of the database, but in view of the many other tasks of this Section and the lack of personnel, only a few interventions for solving immediate problems were possible

  3. Calibrated Properties Model

    International Nuclear Information System (INIS)

    Ghezzehej, T.

    2004-01-01

    The purpose of this model report is to document the calibrated properties model that provides calibrated property sets for unsaturated zone (UZ) flow and transport process models (UZ models). The calibration of the property sets is performed through inverse modeling. This work followed, and was planned in, ''Technical Work Plan (TWP) for: Unsaturated Zone Flow Analysis and Model Report Integration'' (BSC 2004 [DIRS 169654], Sections 1.2.6 and 2.1.1.6). Direct inputs to this model report were derived from the following upstream analysis and model reports: ''Analysis of Hydrologic Properties Data'' (BSC 2004 [DIRS 170038]); ''Development of Numerical Grids for UZ Flow and Transport Modeling'' (BSC 2004 [DIRS 169855]); ''Simulation of Net Infiltration for Present-Day and Potential Future Climates'' (BSC 2004 [DIRS 170007]); ''Geologic Framework Model'' (GFM2000) (BSC 2004 [DIRS 170029]). Additionally, this model report incorporates errata of the previous version and closure of the Key Technical Issue agreement TSPAI 3.26 (Section 6.2.2 and Appendix B), and it is revised for improved transparency

  4. Development of a quality assured calibration method for the PSI radon chamber reference atmosphere

    International Nuclear Information System (INIS)

    Schuler, C.; Butterweck-Dempewolf, G.; Vezzu, G.

    1997-01-01

    Radon detectors and measuring instruments are calibrated at the PSI Reference Laboratory for Radon Gas Concentration Measurements by exposing them to a calibrated radon reference atmosphere in the PSI radon chamber. A sophisticated and quality assured calibration technique was developed which guarantees the traceability of this radon chamber reference atmosphere to standards of internationally acknowledged primary laboratories. (author) 2 figs., 2 refs

  5. Re-calibration of coronary risk prediction : An example of the Seven Countries Study

    NARCIS (Netherlands)

    Puddu, Paolo Emilio; Piras, Paolo; Kromhout, Daan; Tolonen, Hanna; Kafatos, Anthony; Menotti, Alessandro

    2017-01-01

    We aimed at performing a calibration and re-calibration process using six standard risk factors from Northern (NE, N = 2360) or Southern European (SE, N = 2789) middle-aged men of the Seven Countries Study, whose parameters and data were fully known, to establish whether re-calibration gave the

  6. Calibration of modified parallel-plate rheometer through calibrated oil and lattice Boltzmann simulation

    DEFF Research Database (Denmark)

    Ferraris, Chiara F; Geiker, Mette Rica; Martys, Nicos S

    2007-01-01

    inapplicable here. This paper presents the analysis of a modified parallel plate rheometer for measuring cement mortar and propose a methodology for calibration using standard oils and numerical simulation of the flow. A lattice Boltzmann method was used to simulate the flow in the modified rheometer, thus...

  7. Traceable calibration of hospital 192Ir HDR sources

    International Nuclear Information System (INIS)

    Govinda Rajan, K.N.; Sharma, S.D.; Palaniselvam, T.; Vandana, S.; Bhatt, B.C.; Vinatha, S.; Patki, V.S.; Pendse, A.M.; Kannan, V.

    2004-01-01

    A HDR 1000 PLUS well type ionization chamber, procured from Standard Imaging, USA, and maintained by medical Physics and Safety Section (MPSS), Bhabha Atomic Research Centre (BARC), India, as a reference well chamber 1 (RWCH1), was traceably calibrated against the primary standard established by Radiological Standards Laboratory (RSL), BARC for 192 Ir HDR source, in terms of air kerma strength (AKS). An indigenously developed well-type ionization chamber, reference well chamber 2 (RWCH2) and electrometer system, fabricated by CD High Tech (CDHT) Instruments Private Ltd., Bangalore, India, was in turn calibrated against RWCH1. The CDHT system (i.e. RWCH2 and CDHT electrometer system) was taken to several hospitals, in different regions of the country, to check the calibration status of 192 Ir HDR sources. The result of this calibration audit work is reported here. (author)

  8. On the calibration of radiotherapy dosemeters in Australia

    International Nuclear Information System (INIS)

    Huntley, R.; Kotler, L.; Webb, D.

    2000-01-01

    Full text: Dosemeters for external beam radiotherapy are calibrated in Australia by ARPANSA, against the national primary standards of exposure and absorbed dose. The primary standards are free air chambers for exposure at low and medium energy X-rays, a graphite cavity chamber for exposure at 60 Co, and a graphite calorimeter for absorbed dose at 60 Co and high energy (MV) X -rays. Radiotherapy dosemeters are calibrated against these standards using a well documented formalism to provide calibration factors suitable for use with dosimetry protocols. A dosemeter usually comprises an ionization chamber connected to an independent electrometer. These are calibrated separately if possible. A combined calibration factor is reported together with the electrometer calibration factor (sensitivity). The dosimetry protocol used in radiotherapy centres in Australia and New Zealand is currently the simplified version of the IAEA TRS277 protocol, published by the New Zealand NRL and recommended by the ACPSEM. This protocol requires the use of an exposure or air kerma calibration factor at 60 Co (Nx or Nk) to evaluate the absorbed dose to air calibration factor N D . The chamber is then placed in a water phantom with its centre displaced from the reference point by p eff . ARPANSA can also supply calibration factors in absorbed dose to water (N D,w ), as required as input to the new IAEA CoP. If an absorbed dose to water calibration factor is used by the radiotherapy centre, the chamber should be placed with its centre at the reference point in the water phantom. ARPANSA has for some years coordinated the participation of Australian radiotherapy centres in the IAEA TLD Quality Audit service. Note that this service does not represent a calibration and should not be referred to as such. The only calibration is that provided by ARPANSA for a reference dosemeter at each radiotherapy centre. As soon as the ANSTO SSDL is operational, calibrations of reference dosemeters will also be

  9. Reducing the Variance of Intrinsic Camera Calibration Results in the ROS Camera_Calibration Package

    Science.gov (United States)

    Chiou, Geoffrey Nelson

    The intrinsic calibration of a camera is the process in which the internal optical and geometric characteristics of the camera are determined. If accurate intrinsic parameters of a camera are known, the ray in 3D space that every point in the image lies on can be determined. Pairing with another camera allows for the position of the points in the image to be calculated by intersection of the rays. Accurate intrinsics also allow for the position and orientation of a camera relative to some world coordinate system to be calculated. These two reasons for having accurate intrinsic calibration for a camera are especially important in the field of industrial robotics where 3D cameras are frequently mounted on the ends of manipulators. In the ROS (Robot Operating System) ecosystem, the camera_calibration package is the default standard for intrinsic camera calibration. Several researchers from the Industrial Robotics & Automation division at Southwest Research Institute have noted that this package results in large variances in the intrinsic parameters of the camera when calibrating across multiple attempts. There are also open issues on this matter in their public repository that have not been addressed by the developers. In this thesis, we confirm that the camera_calibration package does indeed return different results across multiple attempts, test out several possible hypothesizes as to why, identify the reason, and provide simple solution to fix the cause of the issue.

  10. Automation of the Calibration of Reference Dosimeters Used in Radiotherapy

    International Nuclear Information System (INIS)

    Romero Acosta, A.; Gutierrez Lores, S.

    2013-01-01

    Traceability, accuracy and consistency of radiation measurements are essential in radiation dosimetry, particularly in radiotherapy, where the outcome of treatments is highly dependent on the radiation dose delivered to patients. The role of Secondary Standard Dosimetry Laboratories (SSDLs) is crucial in providing traceable calibrations to hospitals, since these laboratories disseminate calibrations at specific radiation qualities appropriate to the use of radiation measuring instruments. These laboratories follow IAEA/WHO guidelines for calibration procedures, often being current and charge measurements described in these guidelines a tedious task. However, these measurements are usually done using modern electrometers which are equipped with a RS-232 interface that allows instrument control from a PC. This paper presents the design and employment of an automated system aimed to the measurements of the radiotherapy dosimeters calibration process for Cobalt-60 gamma rays. A software was developed using Lab View, in order to achieve the acquisition of the charge values measured, calculation of the calibration coefficient and issue of a calibration certificate. A primary data report file is filled and stored in the PC's hard disk. By using this software tool, a better control over the calibration process is achieved, it reduces the need for human intervention and it also reduces the exposure of the laboratory staff. The automated system has been used for the calibration of reference dosimeters used in radiotherapy at the Cuban Secondary Standard Dosimetry Laboratory of the Center for Radiation Protection and Hygiene (Author)

  11. A single model procedure for estimating tank calibration equations

    International Nuclear Information System (INIS)

    Liebetrau, A.M.

    1997-10-01

    A fundamental component of any accountability system for nuclear materials is a tank calibration equation that relates the height of liquid in a tank to its volume. Tank volume calibration equations are typically determined from pairs of height and volume measurements taken in a series of calibration runs. After raw calibration data are standardized to a fixed set of reference conditions, the calibration equation is typically fit by dividing the data into several segments--corresponding to regions in the tank--and independently fitting the data for each segment. The estimates obtained for individual segments must then be combined to obtain an estimate of the entire calibration function. This process is tedious and time-consuming. Moreover, uncertainty estimates may be misleading because it is difficult to properly model run-to-run variability and between-segment correlation. In this paper, the authors describe a model whose parameters can be estimated simultaneously for all segments of the calibration data, thereby eliminating the need for segment-by-segment estimation. The essence of the proposed model is to define a suitable polynomial to fit to each segment and then extend its definition to the domain of the entire calibration function, so that it (the entire calibration function) can be expressed as the sum of these extended polynomials. The model provides defensible estimates of between-run variability and yields a proper treatment of between-segment correlations. A portable software package, called TANCS, has been developed to facilitate the acquisition, standardization, and analysis of tank calibration data. The TANCS package was used for the calculations in an example presented to illustrate the unified modeling approach described in this paper. With TANCS, a trial calibration function can be estimated and evaluated in a matter of minutes

  12. IAEA workshop/seminar on calibration procedures in dosimetry, Quito, 6-24 October 1986

    International Nuclear Information System (INIS)

    1987-01-01

    The International Atomic Energy Agency in co-operation with the Ecuadorian Atomic Energy Commission organized a workshop and seminar on calibration procedures in dosimetry at the SSDL Quito, 6 to 24 October 1986. All calibration laboratories in the Latin American region were invited to participate. The purpose of the workshop were calibration exercises with therapy-level and protection-level secondary standards at various calibration qualities, discussions on progress made in the different SSDLs in the region and delivering lectures on pertinent subjects. A total of 15 Secondary Standards (10 therapy-level and 5 protection-level) were brought along by the participants and 35 calibration comparisons were performed with those having a valid calibration factor. Thirty-three determinations of calibration factors were performed for secondary standards not having had a calibration before. Twelve different calibration qualities were available (Cobalt-60 and X-rays) and Agency's Secondary Standards traceable to BIPM were the reference standards. The participants were divided into two working groups, each one week and each group into two sub-groups. Both irradiation bunkers were used simultaneously. The one houses the teletherapy Cobalt-60 unit and the protection-level Cobalt-60 irradiator, the other one the constant potential X-ray machine with maximum generating potential of 320 KV and suitable for both therapy-level as well as protection-level calibrations. Due to the heavy workload and limited time available some nightshifts were required to accomplish the requested calibration comparisons

  13. Viscometry for liquids calibration of viscometers

    CERN Document Server

    Gupta, S V

    2014-01-01

    This book is written for scientists involved in the calibration of viscometers. A detailed description for stepping up procedures to establish the viscosity scale and obtaining sets of master viscometers is given in the book. Uncertainty considerations for standard oils of known viscosity are presented. The modern viscometers based on principles of  tuning fork, ultrasonic, PZT, plate waves, Love waves, micro-cantilever and vibration of optical fiber are discussed to inspire the reader to further research and to generate improved versions. The primary standard for viscosity is pure water. Measurements of its viscosity with accuracy/uncertainty achieved are described. The principles of rotational and oscillation viscometers are explained to enhance the knowledge in calibration work. Devices used for specific materials and viscosity in non SI units are discussed with respect to the need to correlate viscosity values obtained by various devices. The description of commercial viscometers meets the needs of the u...

  14. Method of calibration for portable detectors of ionizing radiation

    International Nuclear Information System (INIS)

    Leal, Carlos; Carrizales, Lila; Guacaran, Douglas; Moreno, Ailed; Duran, Jose

    2008-01-01

    Full text: The LSCD is beginning a process of accreditation by the national authority of Venezuela (CENCAMER), so we felt the need to modify existing protocols calibration, suggested by the IAEA (Technical Reports Series No 133) to be adjusted in accordance with international standards of ISO 17025 EA-4/02 and Mexican standard NOM-021-NUCL-2002, adapting the calibration procedure of portable radiation detectors to those standards. The procedure used in the LSCD, conducts an intercomparison between measures between the standard reference and to calibrate the instrument, thus verifying the correct operation of the equipment and its usefulness to the individual or environmental radiation monitoring, not to exceed the limits primary for the public and occupationally Staff Exposed (POE), and propose a simple way to perform this calibration procedure and comply with the standard international and national standards, ensuring the proper functioning of the instruments calibrated. One of the calculations that has proven to be a useful tool in the verification of the conditions of operating the same, it is uncertainty, this procedure allows to characterize the response of individual detector, depending on the constraints specified by the manufacturer, to optimize the calibration is necessary to consider the multiple factors that can affect the measure and evaluate the response of the same, so it is vitally important estimating the typical uncertainty associated with the calibration technique employed, but this calculation is not trivial, depends on the type of detector found usually between 5% to 20%, both in uncertainty as the linearity, which are the parameters that are set to consider an instrument in good or bad condition. Typical are calibrated are: monitors air Geiger-Muller, Ionization cameras, detector of Neutron's, Proportional Counter, Personal dosimeters. (author)

  15. Final report on COOMET.AUV.A-S1: Technical report on supplementary comparison 'Comparison of national standards of the sound pressure unit in air through calibration of working reference microphones'

    Science.gov (United States)

    Pozdeeva, Valentina; Chalyy, Vladimir

    2014-01-01

    The supplementary comparison COOMET.AUV.A-S1 for secondary calibration methods using WS1 and WS2 measurement microphones was carried out from 2009 to 2010. The results were submitted to and approved by CCAUV in April 2014. Four National Metrology Institutes took part in this comparison and are as follows: BelGIM (Belarus), VNIIFTRI (Russia), SMU (Slovakia) and DP NDI 'Sistema' (Ukraine). Three of the above NMIs (VNIIFTRI, SMU and DP NDI 'Sistema') had earlier participated in COOMET key comparisons and one NMI (VNIIFTRI) had also participated in CCAUV key comparisons. The Comparison Reference Values were calculated as the weighted mean values from results obtained by three institutes. The comparison results show agreement for all participants in the frequency range from 20 Hz to 12.5 kHz for WS1 microphones, and in the frequency range from 20 Hz to 16 kHz for WS2 microphones. Main text. To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/. The final report has been peer-reviewed and approved for publication by the CCAUV, according to the provisions of the CIPM Mutual Recognition Arrangement (CIPM MRA).

  16. CERN radiation protection (RP) calibration facilities

    Energy Technology Data Exchange (ETDEWEB)

    Pozzi, Fabio

    2016-04-14

    Radiation protection calibration facilities are essential to ensure the correct operation of radiation protection instrumentation. Calibrations are performed in specific radiation fields according to the type of instrument to be calibrated: neutrons, photons, X-rays, beta and alpha particles. Some of the instruments are also tested in mixed radiation fields as often encountered close to high-energy particle accelerators. Moreover, calibration facilities are of great importance to evaluate the performance of prototype detectors; testing and measuring the response of a prototype detector to well-known and -characterized radiation fields contributes to improving and optimizing its design and capabilities. The CERN Radiation Protection group is in charge of performing the regular calibrations of all CERN radiation protection devices; these include operational and passive dosimeters, neutron and photon survey-meters, and fixed radiation detectors to monitor the ambient dose equivalent, H*(10), inside CERN accelerators and at the CERN borders. A new state-of-the-art radiation protection calibration facility was designed, constructed and commissioned following the related ISO recommendations to replace the previous ageing (more than 30 years old) laboratory. In fact, the new laboratory aims also at the official accreditation according to the ISO standards in order to be able to release certified calibrations. Four radiation fields are provided: neutrons, photons and beta sources and an X-ray generator. Its construction did not only involve a pure civil engineering work; many radiation protection studies were performed to provide a facility that could answer the CERN calibration needs and fulfill all related safety requirements. Monte Carlo simulations have been confirmed to be a valuable tool for the optimization of the building design, the radiation protection aspects, e.g. shielding, and, as consequence, the overall cost. After the source and irradiator installation

  17. Calibration and Propagation of Uncertainty for Independence

    Energy Technology Data Exchange (ETDEWEB)

    Holland, Troy Michael [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Kress, Joel David [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Bhat, Kabekode Ghanasham [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-06-30

    This document reports on progress and methods for the calibration and uncertainty quantification of the Independence model developed at UT Austin. The Independence model is an advanced thermodynamic and process model framework for piperazine solutions as a high-performance CO2 capture solvent. Progress is presented in the framework of the CCSI standard basic data model inference framework. Recent work has largely focused on the thermodynamic submodels of Independence.

  18. Shipboard Calibration Network Extension Utilizing COTS Products

    Science.gov (United States)

    2014-09-01

    Identification TCP Transport Control Protocol VNC Virtual Network Computing WLAN Wireless Local Area Network xvi THIS PAGE INTENTIONALLY...available at the location of the sensor to be calibrated. With the wide adoption of the wireless local area network ( WLAN ) protocol, IEEE 802.11...standard devices have been proven to provide a stable, wireless infrastructure for many applications . The fast setup, wire-free configuration and

  19. Electroweak Calibration of the Higgs Characterization Model

    CERN Multimedia

    CERN. Geneva

    2015-01-01

    I will present the preliminary results of histogram fits using the Higgs Combine histogram fitting package. These fits can be used to estimate the effects of electroweak contributions to the p p -> H mu+ mu- Higgs production channel and calibrate Beyond Standard Model (BSM) simulations which ignore these effects. I will emphasize my findings' significance in the context of other research here at CERN and in the broader world of high energy physics.

  20. Calibration of triaxial fluxgate gradiometer

    International Nuclear Information System (INIS)

    Vcelak, Jan

    2006-01-01

    The description of simple and fast calibration procedures used for double-probe triaxial fluxgate gradiometer is provided in this paper. The calibration procedure consists of three basic steps. In the first step both probes are calibrated independently in order to reach constant total field reading in every position. Both probes are numerically aligned in the second step in order that the gradient reading is zero in homogenous magnetic field. The third step consists of periodic drift calibration during measurement. The results and detailed description of each calibration step are presented and discussed in the paper. The gradiometer is finally verified during the detection of the metal object in the measuring grid

  1. Invited Article: Deep Impact instrument calibration

    International Nuclear Information System (INIS)

    Klaasen, Kenneth P.; Mastrodemos, Nickolaos; A'Hearn, Michael F.; Farnham, Tony; Groussin, Olivier; Ipatov, Sergei; Li Jianyang; McLaughlin, Stephanie; Sunshine, Jessica; Wellnitz, Dennis; Baca, Michael; Delamere, Alan; Desnoyer, Mark; Thomas, Peter; Hampton, Donald; Lisse, Carey

    2008-01-01

    Calibration of NASA's Deep Impact spacecraft instruments allows reliable scientific interpretation of the images and spectra returned from comet Tempel 1. Calibrations of the four onboard remote sensing imaging instruments have been performed in the areas of geometric calibration, spatial resolution, spectral resolution, and radiometric response. Error sources such as noise (random, coherent, encoding, data compression), detector readout artifacts, scattered light, and radiation interactions have been quantified. The point spread functions (PSFs) of the medium resolution instrument and its twin impactor targeting sensor are near the theoretical minimum [∼1.7 pixels full width at half maximum (FWHM)]. However, the high resolution instrument camera was found to be out of focus with a PSF FWHM of ∼9 pixels. The charge coupled device (CCD) read noise is ∼1 DN. Electrical cross-talk between the CCD detector quadrants is correctable to <2 DN. The IR spectrometer response nonlinearity is correctable to ∼1%. Spectrometer read noise is ∼2 DN. The variation in zero-exposure signal level with time and spectrometer temperature is not fully characterized; currently corrections are good to ∼10 DN at best. Wavelength mapping onto the detector is known within 1 pixel; spectral lines have a FWHM of ∼2 pixels. About 1% of the IR detector pixels behave badly and remain uncalibrated. The spectrometer exhibits a faint ghost image from reflection off a beamsplitter. Instrument absolute radiometric calibration accuracies were determined generally to <10% using star imaging. Flat-field calibration reduces pixel-to-pixel response differences to ∼0.5% for the cameras and <2% for the spectrometer. A standard calibration image processing pipeline is used to produce archival image files for analysis by researchers.

  2. Invited Article: Deep Impact instrument calibration.

    Science.gov (United States)

    Klaasen, Kenneth P; A'Hearn, Michael F; Baca, Michael; Delamere, Alan; Desnoyer, Mark; Farnham, Tony; Groussin, Olivier; Hampton, Donald; Ipatov, Sergei; Li, Jianyang; Lisse, Carey; Mastrodemos, Nickolaos; McLaughlin, Stephanie; Sunshine, Jessica; Thomas, Peter; Wellnitz, Dennis

    2008-09-01

    Calibration of NASA's Deep Impact spacecraft instruments allows reliable scientific interpretation of the images and spectra returned from comet Tempel 1. Calibrations of the four onboard remote sensing imaging instruments have been performed in the areas of geometric calibration, spatial resolution, spectral resolution, and radiometric response. Error sources such as noise (random, coherent, encoding, data compression), detector readout artifacts, scattered light, and radiation interactions have been quantified. The point spread functions (PSFs) of the medium resolution instrument and its twin impactor targeting sensor are near the theoretical minimum [ approximately 1.7 pixels full width at half maximum (FWHM)]. However, the high resolution instrument camera was found to be out of focus with a PSF FWHM of approximately 9 pixels. The charge coupled device (CCD) read noise is approximately 1 DN. Electrical cross-talk between the CCD detector quadrants is correctable to <2 DN. The IR spectrometer response nonlinearity is correctable to approximately 1%. Spectrometer read noise is approximately 2 DN. The variation in zero-exposure signal level with time and spectrometer temperature is not fully characterized; currently corrections are good to approximately 10 DN at best. Wavelength mapping onto the detector is known within 1 pixel; spectral lines have a FWHM of approximately 2 pixels. About 1% of the IR detector pixels behave badly and remain uncalibrated. The spectrometer exhibits a faint ghost image from reflection off a beamsplitter. Instrument absolute radiometric calibration accuracies were determined generally to <10% using star imaging. Flat-field calibration reduces pixel-to-pixel response differences to approximately 0.5% for the cameras and <2% for the spectrometer. A standard calibration image processing pipeline is used to produce archival image files for analysis by researchers.

  3. Activities of Radiation Standard Section

    International Nuclear Information System (INIS)

    Kannan, A.; Rao, P.S.; Sachadev, R.N.; Shaha, V.V.; Sharma, D.; Srivastava, P.K.

    1992-01-01

    A brief account of the various facilities and services provided by the Radiation Standards Section (RSS) of the Bhabha Atomic Research Centre, Bombay is given. RSS maintains the primary and secondary standards of various parameters of radiation measurements. It ensures accurate radiological measurements as per international requirements, through periodic international intercomparisons of national standards. It also provides calibration services to various users of radiation sources and instruments. The activities of RSS are described under the headings: (1) Radiological Metrology Standards, (2) Radionuclide Standards, Neutron Metrology, (4) Instruments Calibration, (5) Non-ionizing Radiations, and (6) Instrumentation. (author). figs., tabs

  4. The CHEOPS calibration bench

    Science.gov (United States)

    Wildi, F.; Chazelas, B.; Deline, A.; Sarajlic, M.; Sordet, M.

    2017-09-01

    CHEOPS is an ESA Class S Mission aiming at the characterization of exoplanets through the precise measurement of their radius, using the transit method [1]. To achieve this goal, the payload is designed to be a high precision "absolute" photometer, looking at one star at a time. It will be able to cover la large fraction of the sky by repointing. Its launch is expected at the end of 2017 [2, this conference]. CHEOPS' main science is the measure of the transit of exoplanets of radius ranging from 1 to 6 Earth radii orbiting bright stars. The required photometric stability to reach this goal is of 20 ppm in 6 hours for a 9th magnitude star. The CHEOPS' only instrument is a Ritchey-Chretien style telescope with 300 mm effective aperture diameter, which provides a defocussed image of the target star on a single frame-transfer backside illuminated CCD detector cooled to -40°C and stabilized within 10 mK [2]. CHEOPS being in a LEO, it is equipped with a high performance baffle. The spacecraft platform provides a pointing stability of < 2 arcsec rms. This relatively modest pointing performance makes high quality flat-fielding necessary In the rest of this article we will refer to the only CHEOPS instrument simply as "CHEOP" Its behavior will be calibrated thoroughly on the ground and only a small subset of the calibrations can be redone in flight. The main focuses of the calibrations are the photonic gain stability and sensibility to the environment variations and the Flat field that has to be known at a precision better than 0.1%.

  5. CALIBRATED HYDRODYNAMIC MODEL

    Directory of Open Access Journals (Sweden)

    Sezar Gülbaz

    2015-01-01

    Full Text Available The land development and increase in urbanization in a watershed affect water quantityand water quality. On one hand, urbanization provokes the adjustment of geomorphicstructure of the streams, ultimately raises peak flow rate which causes flood; on theother hand, it diminishes water quality which results in an increase in Total SuspendedSolid (TSS. Consequently, sediment accumulation in downstream of urban areas isobserved which is not preferred for longer life of dams. In order to overcome thesediment accumulation problem in dams, the amount of TSS in streams and inwatersheds should be taken under control. Low Impact Development (LID is a BestManagement Practice (BMP which may be used for this purpose. It is a land planningand engineering design method which is applied in managing storm water runoff inorder to reduce flooding as well as simultaneously improve water quality. LID includestechniques to predict suspended solid loads in surface runoff generated over imperviousurban surfaces. In this study, the impact of LID-BMPs on surface runoff and TSS isinvestigated by employing a calibrated hydrodynamic model for Sazlidere Watershedwhich is located in Istanbul, Turkey. For this purpose, a calibrated hydrodynamicmodel was developed by using Environmental Protection Agency Storm WaterManagement Model (EPA SWMM. For model calibration and validation, we set up arain gauge and a flow meter into the field and obtain rainfall and flow rate data. Andthen, we select several LID types such as retention basins, vegetative swales andpermeable pavement and we obtain their influence on peak flow rate and pollutantbuildup and washoff for TSS. Consequently, we observe the possible effects ofLID on surface runoff and TSS in Sazlidere Watershed.

  6. Radionuclide calibrators performance evaluation

    International Nuclear Information System (INIS)

    Mora Ramirez, E.; Zeledon Fonseca, P.; Jimenez Cordero, M.

    2008-01-01

    Radionuclide calibrators are used to estimate accurately activity prior to administration to a patient, so it is very important that this equipment meets its performance requirements. The purpose of this paper is to compare the commercially available 'Calicheck' (Calcorp. Inc), used to assess linearity, versus the well-known source decay method, and also to show our results after performing several recommended quality control tests. The parameters that we wanted to evaluate were carried on using the Capintec CRC-15R and CRC-15 β radionuclide calibrators. The evaluated tests were: high voltage, display, zero adjust, background, reproducibility, source constancy, accuracy, precision and linearity. The first six tests were evaluated on the daily practice, here we analyzed the 2007 recorded data; and the last three were evaluated once a year. During the daily evaluation both calibrators performance were satisfactory comparing with the manufacture's requirements. The accuracy test show result within the ± 10% allowed for a field instrument. Precision performance is within the ± 1 % allowed. On the other hand, the linearity test shows that using the source decay method the relative coefficient is 0.9998, for both equipment and using the Calicheck the relative coefficient is 0.997. However, looking the percentage of error, during the 'Calicheck' test, its range goes from 0.0 % up to -25.35%, and using the source decay method, the range goes from 0.0 % up to -31.05 %, taking into account both instruments. Checking the 'Calicheck' results we can see that the results varying randomly, but using the source decay method the percentage of error increase as the source activity decrease. We conclude that both devices meet its manufactures requirements, in the case of the linearity using the decay method, decreasing the activity source, increasing the percentage of error, this may happen because of the equipment age. (author)

  7. Self-calibrating interferometer

    International Nuclear Information System (INIS)

    Nussmeier, T.A.

    1982-01-01

    A self-calibrating interferometer is disclosed which forms therein a pair of Michelson interferometers with one beam length of each Michelson interferometer being controlled by a common phase shifter. The transfer function measured from the phase shifter to either of a pair of detectors is sinusoidal with a full cycle for each half wavelength of phase shifter travel. The phase difference between these two sinusoidal detector outputs represents the optical phase difference between a path of known distance and a path of unknown distance

  8. Forward Global Photometric Calibration of the Dark Energy Survey

    Energy Technology Data Exchange (ETDEWEB)

    Burke, D. L.; Rykoff, E. S.; Allam, S.; Annis, J.; Bechtol, K.; Bernstein, G. M.; Drlica-Wagner, A.; Finley, D. A.; Gruendl, R. A.; James, D. J.; Kent, S.; Kessler, R.; Kuhlmann, S.; Lasker, J.; Li, T. S.; Scolnic, D.; Smith, J.; Tucker, D. L.; Wester, W.; Yanny, B.; Abbott, T. M. C.; Abdalla, F. B.; Benoit-Lévy, A.; Bertin, E.; Rosell, A. Carnero; Kind, M. Carrasco; Carretero, J.; Cunha, C. E.; D’Andrea, C. B.; da Costa, L. N.; Desai, S.; Diehl, H. T.; Doel, P.; Estrada, J.; García-Bellido, J.; Gruen, D.; Gutierrez, G.; Honscheid, K.; Kuehn, K.; Kuropatkin, N.; Maia, M. A. G.; March, M.; Marshall, J. L.; Melchior, P.; Menanteau, F.; Miquel, R.; Plazas, A. A.; Sako, M.; Sanchez, E.; Scarpine, V.; Schindler, R.; Sevilla-Noarbe, I.; Smith, M.; Smith, R. C.; Soares-Santos, M.; Sobreira, F.; Suchyta, E.; Tarle, G.; Walker, A. R.

    2017-12-28

    Many scientific goals for the Dark Energy Survey (DES) require calibration of optical/NIR broadband $b = grizY$ photometry that is stable in time and uniform over the celestial sky to one percent or better. It is also necessary to limit to similar accuracy systematic uncertainty in the calibrated broadband magnitudes due to uncertainty in the spectrum of the source. Here we present a "Forward Global Calibration Method (FGCM)" for photometric calibration of the DES, and we present results of its application to the first three years of the survey (Y3A1). The FGCM combines data taken with auxiliary instrumentation at the observatory with data from the broad-band survey imaging itself and models of the instrument and atmosphere to estimate the spatial- and time-dependence of the passbands of individual DES survey exposures. "Standard" passbands are chosen that are typical of the passbands encountered during the survey. The passband of any individual observation is combined with an estimate of the source spectral shape to yield a magnitude $m_b^{\\mathrm{std}}$ in the standard system. This "chromatic correction" to the standard system is necessary to achieve sub-percent calibrations. The FGCM achieves reproducible and stable photometric calibration of standard magnitudes $m_b^{\\mathrm{std}}$ of stellar sources over the multi-year Y3A1 data sample with residual random calibration errors of $\\sigma=5-6\\,\\mathrm{mmag}$ per exposure. The accuracy of the calibration is uniform across the $5000\\,\\mathrm{deg}^2$ DES footprint to within $\\sigma=7\\,\\mathrm{mmag}$. The systematic uncertainties of magnitudes in the standard system due to the spectra of sources are less than $5\\,\\mathrm{mmag}$ for main sequence stars with $0.5

  9. Safety enhancement through calibration and maintenance

    International Nuclear Information System (INIS)

    Mohammad Ali Khalid; Taiman Kadni

    2000-01-01

    Although radiation causes an alarming effect to living organism, it has been accepted for diagnostic and therapy in medicine as well as quality control and test method in industry. Due to the benefit gained, public at large is willing to accept the risk on condition that proper protection and safety standard is implemented and practised. Instrument plays a very important role not only in generation radiation but also measuring it. Therefore to ensure safety it is fair to say that all instrument must be calibrated to a certain standard and maintained to operate to its design specifications from time to time. (author)

  10. Dosimetry and Calibration Section

    International Nuclear Information System (INIS)

    Otto, T.

    1999-01-01

    The Dosimetry and Calibration Section fulfils two tasks within CERN's Radiation Protection Group: the Individual Dosimetry Service monitors more than 5000 persons potentially exposed to ionizing radiation on the CERN sites, and the Calibration Laboratory verifies throughout the year, at regular intervals, over 1000 instruments, monitors, and electronic dosimeters used by RP Group. The establishment of a Quality Assurance System for the Individual Dosimetry Service, a requirement of the new Swiss Ordinance for personal dosimetry, put a considerable workload on the section. Together with an external consultant it was decided to identify and then describe the different 'processes' of the routine work performed in the dosimetry service. The resulting Quality Manual was submitted to the Federal Office for Public Health in Bern in autumn. The CERN Individual Dosimetry Service will eventually be officially endorsed after a successful technical test in March 1999. On the technical side, the introduction of an automatic development machine for gamma films was very successful. It processes the dosimetric films without an operator being present, and its built-in regeneration mechanism keeps the concentration of the processing chemicals at a constant level

  11. Piezoelectric trace vapor calibrator

    International Nuclear Information System (INIS)

    Verkouteren, R. Michael; Gillen, Greg; Taylor, David W.

    2006-01-01

    The design and performance of a vapor generator for calibration and testing of trace chemical sensors are described. The device utilizes piezoelectric ink-jet nozzles to dispense and vaporize precisely known amounts of analyte solutions as monodisperse droplets onto a hot ceramic surface, where the generated vapors are mixed with air before exiting the device. Injected droplets are monitored by microscope with strobed illumination, and the reproducibility of droplet volumes is optimized by adjustment of piezoelectric wave form parameters. Complete vaporization of the droplets occurs only across a 10 deg. C window within the transition boiling regime of the solvent, and the minimum and maximum rates of trace analyte that may be injected and evaporated are determined by thermodynamic principles and empirical observations of droplet formation and stability. By varying solution concentrations, droplet injection rates, air flow, and the number of active nozzles, the system is designed to deliver--on demand--continuous vapor concentrations across more than six orders of magnitude (nominally 290 fg/l to 1.05 μg/l). Vapor pulses containing femtogram to microgram quantities of analyte may also be generated. Calibrated ranges of three explosive vapors at ng/l levels were generated by the device and directly measured by ion mobility spectrometry (IMS). These data demonstrate expected linear trends within the limited working range of the IMS detector and also exhibit subtle nonlinear behavior from the IMS measurement process

  12. A Simple Accelerometer Calibrator

    International Nuclear Information System (INIS)

    Salam, R A; Islamy, M R F; Khairurrijal; Munir, M M; Latief, H; Irsyam, M

    2016-01-01

    High possibility of earthquake could lead to the high number of victims caused by it. It also can cause other hazards such as tsunami, landslide, etc. In that case it requires a system that can examine the earthquake occurrence. Some possible system to detect earthquake is by creating a vibration sensor system using accelerometer. However, the output of the system is usually put in the form of acceleration data. Therefore, a calibrator system for accelerometer to sense the vibration is needed. In this study, a simple accelerometer calibrator has been developed using 12 V DC motor, optocoupler, Liquid Crystal Display (LCD) and AVR 328 microcontroller as controller system. The system uses the Pulse Wave Modulation (PWM) form microcontroller to control the motor rotational speed as response to vibration frequency. The frequency of vibration was read by optocoupler and then those data was used as feedback to the system. The results show that the systems could control the rotational speed and the vibration frequencies in accordance with the defined PWM. (paper)

  13. Calibration of neutrons monitors with moderators and application in the calibration factors of albedo dosemeters

    International Nuclear Information System (INIS)

    Schuch, L.A.

    1978-11-01

    The calibration factors and the reproducibility of an Albedo Dosimeter designed for personal neutron monitoring were determined. These factor were obtained simulating the dosimeter reading and the equivalent dose in the locality by a convenient combination of responses of the Bonner Sphere Spectrometer. The results obtained in the simulation were verified experimentally for different spectra employing the Am-Be, bare 252 Cf source and 253 Cf source with graphite sields of varying thickness. Different standards were used in the procedures necessary for the determination of the calibration factors. An Am-Be neutron source, standardized by the activation of a manganese sulphate bath was used as a primary standard. As a secondary standard, for the measurement of the neutron fluence, a De Pangher Long Counter was used and the scattering effects were determined using the shadow cone method. The other monitors such as the Rem-Counter and the Bonner Sphere Spectrometer were also calibrated with reference to the secondary standard with a view to comparing the results obtained with those furnished by the Albedo Dosimeter. (Author) [pt

  14. A convenient calibrator for tritium survey meters

    International Nuclear Information System (INIS)

    Cutler, J.M.; Janmohamed, S.R.; Surette, R.A.; Wood, M.J.

    1993-06-01

    Staff in Ontario Hydro's CANDU nuclear power stations were having difficulty calibrating their tritium-in-air survey meters. Chalk River Laboratories suggested using a standard silica gel collector loaded with tritiated water vapour as a radiation source. The collector is a polyethylene tube with a length of rubber tubing attached to each end. The plastic tube is filled with dry silica gel, and cotton wool is stuffed into each end to retain the gel. To load the source with tritiated vapour, a bubbler containing tritiated water is connected to the collector until the gel is completely pink. The end tubes of the source are then connected to each other to seal the source. To use the source, the rubber tubes are connected to the intake and exhaust fittings of the survey meter to be calibrated. No tritium vapour is released during loading or calibration. This source not only verifies that the ion chamber and electrometer are working, but also checks whether the air sample is reaching the detector. It is more direct and credible than a gamma source, and is inexpensive and convenient to construct and calibrate at the power station. 5 figs

  15. The Calibration Home Base for Imaging Spectrometers

    Directory of Open Access Journals (Sweden)

    Johannes Felix Simon Brachmann

    2016-08-01

    Full Text Available The Calibration Home Base (CHB is an optical laboratory designed for the calibration of imaging spectrometers for the VNIR/SWIR wavelength range. Radiometric, spectral and geometric calibration as well as the characterization of sensor signal dependency on polarization are realized in a precise and highly automated fashion. This allows to carry out a wide range of time consuming measurements in an ecient way. The implementation of ISO 9001 standards in all procedures ensures a traceable quality of results. Spectral measurements in the wavelength range 380–1000 nm are performed to a wavelength uncertainty of +- 0.1 nm, while an uncertainty of +-0.2 nm is reached in the wavelength range 1000 – 2500 nm. Geometric measurements are performed at increments of 1.7 µrad across track and 7.6 µrad along track. Radiometric measurements reach an absolute uncertainty of +-3% (k=1. Sensor artifacts, such as caused by stray light will be characterizable and correctable in the near future. For now, the CHB is suitable for the characterization of pushbroom sensors, spectrometers and cameras. However, it is planned to extend the CHBs capabilities in the near future such that snapshot hyperspectral imagers can be characterized as well. The calibration services of the CHB are open to third party customers from research institutes as well as industry.

  16. Rectifying calibration error of Goldmann applanation tonometer is easy!

    Directory of Open Access Journals (Sweden)

    Nikhil S Choudhari

    2014-01-01

    Full Text Available Purpose: Goldmann applanation tonometer (GAT is the current Gold standard tonometer. However, its calibration error is common and can go unnoticed in clinics. Its company repair has limitations. The purpose of this report is to describe a self-taught technique of rectifying calibration error of GAT. Materials and Methods: Twenty-nine slit-lamp-mounted Haag-Streit Goldmann tonometers (Model AT 900 C/M; Haag-Streit, Switzerland were included in this cross-sectional interventional pilot study. The technique of rectification of calibration error of the tonometer involved cleaning and lubrication of the instrument followed by alignment of weights when lubrication alone didn′t suffice. We followed the South East Asia Glaucoma Interest Group′s definition of calibration error tolerance (acceptable GAT calibration error within ±2, ±3 and ±4 mm Hg at the 0, 20 and 60-mm Hg testing levels, respectively. Results: Twelve out of 29 (41.3% GATs were out of calibration. The range of positive and negative calibration error at the clinically most important 20-mm Hg testing level was 0.5 to 20 mm Hg and -0.5 to -18 mm Hg, respectively. Cleaning and lubrication alone sufficed to rectify calibration error of 11 (91.6% faulty instruments. Only one (8.3% faulty GAT required alignment of the counter-weight. Conclusions: Rectification of calibration error of GAT is possible in-house. Cleaning and lubrication of GAT can be carried out even by eye care professionals and may suffice to rectify calibration error in the majority of faulty instruments. Such an exercise may drastically reduce the downtime of the Gold standard tonometer.

  17. Present status of calibration system and implementation of the new ICRU operational quantities in China

    International Nuclear Information System (INIS)

    Zhang Qingli

    1995-01-01

    Accompanying the wide use of ionizing radiation, general public have gradually become aware of the detriments of ionizing radiation. The adequate calibration standards, calibration facilities and calibration techniques, and the proper use of radiation-measuring instruments are the key steps of the measurements. In China, national standards are maintained by the National Institute of Metrology. The secondary standards including standard reference radiation sources, standard reference instruments and calibration phantoms in the Secondary Standard Dose Laboratory (SSDL) and other main calibration services are calibrated directly and periodically with the national (primary) standards. ICRU dose equivalent standards are established, and the calibration procedures being followed are consistent with the suggestions of International Standard Organization. γ ray and X-ray calibration facilities are explained. Since the issue of ICRU Report 39, ambient dose equivalent and directional dose equivalent for area monitoring and individual dose equivalent, penetrating and superficial, have been introduced. The concepts of quality assurance in radiation monitoring have been introduced. (K.I.)

  18. Calibration procedure of Hukseflux SR25 to Establish the Diffuse Reference for the Outdoor Broadband Radiometer Calibration

    Energy Technology Data Exchange (ETDEWEB)

    Reda, Ibrahim M. [National Renewable Energy Laboratory (NREL), Golden, CO (United States); Andreas, Afshin M. [National Renewable Energy Laboratory (NREL), Golden, CO (United States)

    2017-08-01

    Accurate pyranometer calibrations, traceable to internationally recognized standards, are critical for solar irradiance measurements. One calibration method is the component summation method, where the pyranometers are calibrated outdoors under clear sky conditions, and the reference global solar irradiance is calculated as the sum of two reference components, the diffuse horizontal and subtended beam solar irradiances. The beam component is measured with pyrheliometers traceable to the World Radiometric Reference, while there is no internationally recognized reference for the diffuse component. In the absence of such a reference, we present a method to consistently calibrate pyranometers for measuring the diffuse component. The method is based on using a modified shade/unshade method and a pyranometer with less than 0.5 W/m2 thermal offset. The calibration result shows that the responsivity of Hukseflux SR25 pyranometer equals 10.98 uV/(W/m2) with +/-0.86 percent uncertainty.

  19. High-dose secondary calibration laboratory accreditation program

    Energy Technology Data Exchange (ETDEWEB)

    Humphreys, J.C. [National Institute of Standards and Technology, Gaithersburg, MD (United States)

    1993-12-31

    There is a need for high-dose secondary calibration laboratories to serve the multi-billion dollar radiation processing industry. This need is driven by the desires of industry for less costly calibrations and faster calibration-cycle response time. Services needed include calibration irradiations of routine processing dosimeters and the supply of reference standard transfer dosimeters for irradiation in the production processing facility. In order to provide measurement quality assurance and to demonstrate consistency with national standards, the high-dose secondary laboratories would be accredited by means of an expansion of an existing National Voluntary Laboratory Accreditation Program. A laboratory performance criteria document is under development to implement the new program.

  20. NVLAP activities at Department of Defense calibration laboratories

    Energy Technology Data Exchange (ETDEWEB)

    Schaeffer, D.M. [Defense Nuclear Agency, Alexandria, VA (United States)

    1993-12-31

    There are 367 active radiological instrument calibration laboratories within the U.S. Department of Defense (DoD). Each of the four services in DoD manages, operates, and certifies the technical proficiency and competency of those laboratories under their cognizance. Each service has designated secondary calibration laboratories to trace all calibration source standards to the National Institute of Standards and Technology. Individual service radiological calibration programs and capabilities, present and future, are described, as well as the measurement quality assurance (MQA) processes for their traceability. National Voluntary Laboratory Accreditation Program (NVLAP) programs for dosimetry systems are briefly summarized. Planned NVLAP accreditation of secondary laboratories is discussed in the context of current technical challenges and future efforts.

  1. Calibration of F-18 activity for PET applications in Cuba

    International Nuclear Information System (INIS)

    León, Yecenia Moreno; Verdecia, Pilar Oropesa; Rodríguez, Lourdes García; Águila, Rolando A. Serra; Magaña, Yoel Jénez; Hechavarría, Ailec Bell; Pérez, Nayla; Cacero, Maray Dubalón; Ruiz, Javier Mas

    2016-01-01

    In the paper we present the results of the calibration of the concentration of F-18 dissolution activity in Cuba. Methods of measurement in a calibrated well ionization chamber, traceable to the UK national standard and gamma spectrometry yielded equivalent results within the limit of the associated uncertainties, respectively. The measurement uncertainties of the F-18 activity of the secondary standard activity activator, CAPINTEC CRCTM 15R, obtained from calibration of the instrument with the calibrated solutions of radionuclide, are also shown for the measurement of samples in the geometries of interest in Nuclear Medicine: glass jars and plastic syringes. The results presented in this paper constitute the necessary metrological support for the use of F-18 radiopharmaceuticals and the new PET and PET / CT technologies in medical practice in Cuba.

  2. NVLAP activities at Department of Defense calibration laboratories

    International Nuclear Information System (INIS)

    Schaeffer, D.M.

    1993-01-01

    There are 367 active radiological instrument calibration laboratories within the U.S. Department of Defense (DoD). Each of the four services in DoD manages, operates, and certifies the technical proficiency and competency of those laboratories under their cognizance. Each service has designated secondary calibration laboratories to trace all calibration source standards to the National Institute of Standards and Technology. Individual service radiological calibration programs and capabilities, present and future, are described, as well as the measurement quality assurance (MQA) processes for their traceability. National Voluntary Laboratory Accreditation Program (NVLAP) programs for dosimetry systems are briefly summarized. Planned NVLAP accreditation of secondary laboratories is discussed in the context of current technical challenges and future efforts

  3. High-dose secondary calibration laboratory accreditation program

    International Nuclear Information System (INIS)

    Humphreys, J.C.

    1993-01-01

    There is a need for high-dose secondary calibration laboratories to serve the multi-billion dollar radiation processing industry. This need is driven by the desires of industry for less costly calibrations and faster calibration-cycle response time. Services needed include calibration irradiations of routine processing dosimeters and the supply of reference standard transfer dosimeters for irradiation in the production processing facility. In order to provide measurement quality assurance and to demonstrate consistency with national standards, the high-dose secondary laboratories would be accredited by means of an expansion of an existing National Voluntary Laboratory Accreditation Program. A laboratory performance criteria document is under development to implement the new program

  4. Estimation of photon energy distribution in gamma calibration field

    International Nuclear Information System (INIS)

    Takahashi, Fumiaki; Shimizu, Shigeru; Yamaguchi, Yasuhiro

    1997-03-01

    Photon survey instruments used for radiation protection are usually calibrated at gamma radiation fields, which are traceable to the national standard with regard to exposure. Whereas scattered radiations as well as primary gamma-rays exit in the calibration field, no consideration for the effect of the scattered radiations on energy distribution is given in routine calibration works. The scattered radiations can change photon energy spectra in the field, and this can result in misinterpretations of energy-dependent instrument responses. Construction materials in the field affect the energy distribution and magnitude of the scattered radiations. The geometric relationship between a gamma source and an instrument can determine the energy distribution at the calibration point. Therefore, it is essential for the assurance of quality calibration to estimate the energy spectra at the gamma calibration fields. Then, photon energy distributions at some fields in the Facility of Radiation Standard of the Japan Atomic Energy Research Institute (JAERI) were estimated by measurements using a NaI(Tl) detector and Monte Carlo calculations. It was found that the use of collimator gives a different feature in photon energy distribution. The origin of scattered radiations and the ratio of the scattered radiations to the primary gamma-rays were obtained. The results can help to improve the calibration of photon survey instruments in the JAERI. (author)

  5. On chromatic and geometrical calibration

    DEFF Research Database (Denmark)

    Folm-Hansen, Jørgen

    1999-01-01

    The main subject of the present thesis is different methods for the geometrical and chromatic calibration of cameras in various environments. For the monochromatic issues of the calibration we present the acquisition of monochrome images, the classic monochrome aberrations and the various sources...... the correct interpolation method is described. For the chromatic issues of calibration we present the acquisition of colour and multi-spectral images, the chromatic aberrations and the various lens/camera based non-uniformities of the illumination of the image plane. It is described how the monochromatic...... to design calibration targets for both geometrical and chromatic calibration are described. We present some possible systematical errors on the detection of the objects in the calibration targets, if viewed in a non orthogonal angle, if the intensities are uneven or if the image blurring is uneven. Finally...

  6. Calibration Device Designed for proof ring used in SCC Experiment

    Science.gov (United States)

    Hu, X. Y.; Kang, Z. Y.; Yu, Y. L.

    2017-11-01

    In this paper, a calibration device for proof ring used in SCC (Stress Corrosion Cracking) experiment was designed. A compact size loading device was developed to replace traditional force standard machine or a long screw nut. The deformation of the proof ring was measured by a CCD (Charge-Coupled Device) during the calibration instead of digital caliper or a dial gauge. The calibration device was verified at laboratory that the precision of force loading is ±0.1% and the precision of deformation measurement is ±0.002mm.

  7. Lidar to lidar calibration of Ground-based Lidar

    DEFF Research Database (Denmark)

    Fernandez Garcia, Sergio; Courtney, Michael

    This report presents the result of the lidar to lidar calibration performed for ground-based lidar. Calibration is here understood as the establishment of a relation between the reference lidar wind speed measurements with measurement uncertainties provided by measurement standard and corresponding...... lidar wind speed indications with associated measurement uncertainties. The lidar calibration concerns the 10 minute mean wind speed measurements. The comparison of the lidar measurements of the wind direction with that from the reference lidar measurements are given for information only....

  8. Calibration of EFOSC2 Broadband Linear Imaging Polarimetry

    Science.gov (United States)

    Wiersema, K.; Higgins, A. B.; Covino, S.; Starling, R. L. C.

    2018-03-01

    The European Southern Observatory Faint Object Spectrograph and Camera v2 is one of the workhorse instruments on ESO's New Technology Telescope, and is one of the most popular instruments at La Silla observatory. It is mounted at a Nasmyth focus, and therefore exhibits strong, wavelength and pointing-direction-dependent instrumental polarisation. In this document, we describe our efforts to calibrate the broadband imaging polarimetry mode, and provide a calibration for broadband B, V, and R filters to a level that satisfies most use cases (i.e. polarimetric calibration uncertainty 0.1%). We make our calibration codes public. This calibration effort can be used to enhance the yield of future polarimetric programmes with the European Southern Observatory Faint Object Spectrograph and Camera v2, by allowing good calibration with a greatly reduced number of standard star observations. Similarly, our calibration model can be combined with archival calibration observations to post-process data taken in past years, to form the European Southern Observatory Faint Object Spectrograph and Camera v2 legacy archive with substantial scientific potential.

  9. Forward Global Photometric Calibration of the Dark Energy Survey

    Science.gov (United States)

    Burke, D. L.; Rykoff, E. S.; Allam, S.; Annis, J.; Bechtol, K.; Bernstein, G. M.; Drlica-Wagner, A.; Finley, D. A.; Gruendl, R. A.; James, D. J.; Kent, S.; Kessler, R.; Kuhlmann, S.; Lasker, J.; Li, T. S.; Scolnic, D.; Smith, J.; Tucker, D. L.; Wester, W.; Yanny, B.; Abbott, T. M. C.; Abdalla, F. B.; Benoit-Lévy, A.; Bertin, E.; Carnero Rosell, A.; Carrasco Kind, M.; Carretero, J.; Cunha, C. E.; D’Andrea, C. B.; da Costa, L. N.; Desai, S.; Diehl, H. T.; Doel, P.; Estrada, J.; García-Bellido, J.; Gruen, D.; Gutierrez, G.; Honscheid, K.; Kuehn, K.; Kuropatkin, N.; Maia, M. A. G.; March, M.; Marshall, J. L.; Melchior, P.; Menanteau, F.; Miquel, R.; Plazas, A. A.; Sako, M.; Sanchez, E.; Scarpine, V.; Schindler, R.; Sevilla-Noarbe, I.; Smith, M.; Smith, R. C.; Soares-Santos, M.; Sobreira, F.; Suchyta, E.; Tarle, G.; Walker, A. R.; DES Collaboration

    2018-01-01

    Many scientific goals for the Dark Energy Survey (DES) require the calibration of optical/NIR broadband b = grizY photometry that is stable in time and uniform over the celestial sky to one percent or better. It is also necessary to limit to similar accuracy systematic uncertainty in the calibrated broadband magnitudes due to uncertainty in the spectrum of the source. Here we present a “Forward Global Calibration Method (FGCM)” for photometric calibration of the DES, and we present results of its application to the first three years of the survey (Y3A1). The FGCM combines data taken with auxiliary instrumentation at the observatory with data from the broadband survey imaging itself and models of the instrument and atmosphere to estimate the spatial and time dependences of the passbands of individual DES survey exposures. “Standard” passbands that are typical of the passbands encountered during the survey are chosen. The passband of any individual observation is combined with an estimate of the source spectral shape to yield a magnitude {m}b{std} in the standard system. This “chromatic correction” to the standard system is necessary to achieve subpercent calibrations and in particular, to resolve ambiguity between the broadband brightness of a source and the shape of its SED. The FGCM achieves a reproducible and stable photometric calibration of standard magnitudes {m}b{std} of stellar sources over the multiyear Y3A1 data sample with residual random calibration errors of σ =6{--}7 {mmag} per exposure. The accuracy of the calibration is uniform across the 5000 {\\deg }2 DES footprint to within σ =7 {mmag}. The systematic uncertainties of magnitudes in the standard system due to the spectra of sources are less than 5 {mmag} for main-sequence stars with 0.5< g-i< 3.0.

  10. Quality Management and Calibration

    Science.gov (United States)

    Merkus, Henk G.

    Good specification of a product’s performance requires adequate characterization of relevant properties. Particulate products are usually characterized by some PSD, shape or porosity parameter(s). For proper characterization, adequate sampling, dispersion, and measurement procedures should be available or developed and skilful personnel should use appropriate, well-calibrated/qualified equipment. The characterization should be executed, in agreement with customers, in a wellorganized laboratory. All related aspects should be laid down in a quality handbook. The laboratory should provide proof for its capability to perform the characterization of stated products and/or reference materials within stated confidence limits. This can be done either by internal validation and audits or by external GLP accreditation.

  11. SURF Model Calibration Strategy

    Energy Technology Data Exchange (ETDEWEB)

    Menikoff, Ralph [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-03-10

    SURF and SURFplus are high explosive reactive burn models for shock initiation and propagation of detonation waves. They are engineering models motivated by the ignition & growth concept of high spots and for SURFplus a second slow reaction for the energy release from carbon clustering. A key feature of the SURF model is that there is a partial decoupling between model parameters and detonation properties. This enables reduced sets of independent parameters to be calibrated sequentially for the initiation and propagation regimes. Here we focus on a methodology for tting the initiation parameters to Pop plot data based on 1-D simulations to compute a numerical Pop plot. In addition, the strategy for tting the remaining parameters for the propagation regime and failure diameter is discussed.

  12. Intersatellite Calibration of Microwave Radiometers for GPM

    Science.gov (United States)

    Wilheit, T. T.

    2010-12-01

    The aim of the GPM mission is to measure precipitation globally with high temporal resolution by using a constellation of satellites logically united by the GPM Core Satellite which will be in a non-sunsynchronous, medium inclination orbit. The usefulness of the combined product depends on the consistency of precipitation retrievals from the various microwave radiometers. The calibration requirements for this consistency are quite daunting requiring a multi-layered approach. The radiometers can vary considerably in their frequencies, view angles, polarizations and spatial resolutions depending on their primary application and other constraints. The planned parametric algorithms will correct for the varying viewing parameters, but they are still vulnerable to calibration errors, both relative and absolute. The GPM Intersatellite Calibration Working Group (aka X-CAL) will adjust the calibration of all the radiometers to a common consensus standard for the GPM Level 1C product to be used in precipitation retrievals. Finally, each Precipitation Algorithm Working Group must have its own strategy for removing the residual errors. If the final adjustments are small, the credibility of the precipitation retrievals will be enhanced. Before intercomparing, the radiometers must be self consistent on a scan-wise and orbit-wise basis. Pre-screening for this consistency constitutes the first step in the intercomparison. The radiometers are then compared pair-wise with the microwave radiometer (GMI) on the GPM Core Satellite. Two distinct approaches are used for sake of cross-checking the results. On the one hand, nearly simultaneous observations are collected at the cross-over points of the orbits and the observations of one are converted to virtual observations of the other using a radiative transfer model to permit comparisons. The complementary approach collects histograms of brightness temperature from each instrument. In each case a model is needed to translate the

  13. Portable compact multifunction IR calibrator

    International Nuclear Information System (INIS)

    Wyatt, C.L.; Jacobsen, L.; Steed, A.

    1988-01-01

    A compact portable multifunction calibrator designed for future sensor systems is described which enables a linearity calibration for all detectors simultaneously using a near small-area source, a high-resolution mapping of the focal plane with 10 microrad setability and with a blur of less than 100 microrad, system spectral response calibration (radiometer) using a Michelson interferometer source, relative spectral response (spectrometer) using high-temperature external commercial blackbody simulators, and an absolute calibration using an internal low-temperature extended-area source. 5 references

  14. BXS Re-calibration

    International Nuclear Information System (INIS)

    Welch, J.

    2010-01-01

    Early in the commissioning it was noticed by Cecile Limborg that the calibration of the BXS spectrometer magnet seemed to be different from the strength of the BX01/BX02 magnets. First the BX01/BX02 currents were adjusted to 135 MeV and the beam energy was adjusted to make the horizontal orbit flat. Then BX01/BX02 magnets were switched off and BXS was adjusted to make the horizontal orbit in the spectrometer line flat, without changing the energy of the beam. The result was that about 140-141 MeV were required on the BXS magnet. This measurement was repeated several times by others with the same results. It was not clear what was causing the error: magnet strength or layout. A position error of about 19 mm of the BXS magnet could explain the difference. Because there was a significant misalignment of the vacuum chamber in the BXS line, the alignment of the whole spectrometer line was checked. The vacuum chamber was corrected, but the magnets were found to be in the proper alignment. So we were left with one (or conceivably two) magnet calibration errors. Because BXS is a wedged shaped magnet, the bend angle depends on the horizontal position of the incoming beam. As mentioned, an offset of the beam position of 19 mm would increase or decrease the bend angle roughly by the ratio of 135/141. The figure of 19 mm is special and caused a considerable confusion during the design and measurement of the BXS magnet. This is best illustrated in Figure 1 which was taken out of the BXS Traveler document. The distance between the horizontal midplanes of the poles and the apex of the beam path was chosen to be 19 mm so the beam is close to the good field region throughout its entire path. Thus it seemed possible that there was an error that resulted in the beam not being on this trajectory, or conversely, that the magnetic measurements were done on the wrong trajectory and the magnet was then mis-calibrated. Mechanical measurements of the vacuum chamber made in the tunnel

  15. Reliability of an x-ray system for calibrating and testing personal radiation dosimeters

    Energy Technology Data Exchange (ETDEWEB)

    Guimarães, M.C.; Silva, C.R.E.; Silva, T.A. da [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil); Rosado, P.H.G.; Cunha, P.G. [Instituto de Radioproteção e Dosimetria (IRD/CNEN-RJ), Rio de Janeiro, RJ (Brazil)

    2017-07-01

    Metrology laboratories are expected to maintain standardized radiation beams and traceable standard dosimeters to provide reliable calibrations or testing of detectors. Results of the characterization of an x-ray system for performing calibration and testing of radiation dosimeters used for individual monitoring are shown in this work. (author)

  16. Reliability of an x-ray system for calibrating and testing personal radiation dosimeters

    Science.gov (United States)

    Guimarães, M. C.; Silva, C. R. E.; Rosado, P. H. G.; Cunha, P. G.; Da Silva, T. A.

    2018-03-01

    Metrology laboratories are expected to maintain standardized radiation beams and traceable standard dosimeters to provide reliable calibrations or testing of detectors. Results of the characterization of an x-ray system for performing calibration and testing of radiation dosimeters used for individual monitoring are shown in this work.

  17. Reliability of an x-ray system for calibrating and testing personal radiation dosimeters

    International Nuclear Information System (INIS)

    Guimarães, M.C.; Silva, C.R.E.; Silva, T.A. da; Rosado, P.H.G.; Cunha, P.G.

    2017-01-01

    Metrology laboratories are expected to maintain standardized radiation beams and traceable standard dosimeters to provide reliable calibrations or testing of detectors. Results of the characterization of an x-ray system for performing calibration and testing of radiation dosimeters used for individual monitoring are shown in this work. (author)

  18. Summary of KOMPSAT-5 Calibration and Validation

    Science.gov (United States)

    Yang, D.; Jeong, H.; Lee, S.; Kim, B.

    2013-12-01

    Korean Multi-Purpose Satellite 5 (KOMPSAT-5), equipped with high resolution X-band (9.66 GHz) Synthetic Aperture Radar (SAR), is planning to be launched on August 22, 2013. With the satellite's primary mission objective being providing Geographical Information System (GIS), Ocean monitoring and Land management, and Disaster and ENvironment monitoring (GOLDEN), it is expected that its applications for scientific research on geographical processes will be extensive. In order to meet its mission objective, the KOMPSAT-5 will provide three different kinds of SAR imaging modes; High Resolution Mode (1 m resolution, 5 km swath), Standard Mode (3 m resolution, 30 km swath), and Wide Swath Mode (20 m resolution, 100 km swath). The KOMPSAT-5 will be operated in a 550 km sun-synchronous, dawn- dusk orbit with a 28-day ground repeat cycle providing valuable image information on Earth surface day-or-night and even in bad weather condition. After successful launch of the satellite, it will go through Launch and Early Operation (LEOP) and In-Orbit Testing (IOT) period about for 6 months to carry out various tests on satellite bus and payload systems. The satellite bus system will be tested during the first 3 weeks after the launch focusing on the Attitude and Orbit Control Subsystem (AOCS) and Integrated GPS Occultation Receiver (IGOR) calibration. With the completion of bus system test, the SAR payload system will be calibrated during initial In-Flight check period (11 weeks) by the joint effort of Thales Alenia Space Italy (TAS-I) and Korea Aerospace Research Institute (KARI). The pointing and relative calibration will be carried out during this period by analyzing the doppler frequency and antenna beam pattern of reflected microwave signal from selected regions with uniform backscattering coefficients (e.g. Amazon rainforest). A dedicated SAR calibration, called primary calibration, will be allocated at the end of LEOP for 12 weeks to perform thorough calibration activities

  19. Generic System for Remote Testing and Calibration of Measuring Instruments: Security Architecture

    Science.gov (United States)

    Jurčević, M.; Hegeduš, H.; Golub, M.

    2010-01-01

    Testing and calibration of laboratory instruments and reference standards is a routine activity and is a resource and time consuming process. Since many of the modern instruments include some communication interfaces, it is possible to create a remote calibration system. This approach addresses a wide range of possible applications and permits to drive a number of different devices. On the other hand, remote calibration process involves a number of security issues due to recommendations specified in standard ISO/IEC 17025, since it is not under total control of the calibration laboratory personnel who will sign the calibration certificate. This approach implies that the traceability and integrity of the calibration process directly depends on the collected measurement data. The reliable and secure remote control and monitoring of instruments is a crucial aspect of internet-enabled calibration procedure.

  20. Calibration of high resolution digital camera based on different photogrammetric methods

    International Nuclear Information System (INIS)

    Hamid, N F A; Ahmad, A

    2014-01-01

    This paper presents method of calibrating high-resolution digital camera based on different configuration which comprised of stereo and convergent. Both methods are performed in the laboratory and in the field calibration. Laboratory calibration is based on a 3D test field where a calibration plate of dimension 0.4 m × 0.4 m with grid of targets at different height is used. For field calibration, it uses the same concept of 3D test field which comprised of 81 target points located on a flat ground and the dimension is 9 m × 9 m. In this study, a non-metric high resolution digital camera called Canon Power Shot SX230 HS was calibrated in the laboratory and in the field using different configuration for data acquisition. The aim of the calibration is to investigate the behavior of the internal digital camera whether all the digital camera parameters such as focal length, principal point and other parameters remain the same or vice-versa. In the laboratory, a scale bar is placed in the test field for scaling the image and approximate coordinates were used for calibration process. Similar method is utilized in the field calibration. For both test fields, the digital images were acquired within short period using stereo and convergent configuration. For field calibration, aerial digital images were acquired using unmanned aerial vehicle (UAV) system. All the images were processed using photogrammetric calibration software. Different calibration results were obtained for both laboratory and field calibrations. The accuracy of the results is evaluated based on standard deviation. In general, for photogrammetric applications and other applications the digital camera must be calibrated for obtaining accurate measurement or results. The best method of calibration depends on the type of applications. Finally, for most applications the digital camera is calibrated on site, hence, field calibration is the best method of calibration and could be employed for obtaining accurate

  1. IAEA/SSDL intercomparison of calibration factors for therapy level ionization chambers

    International Nuclear Information System (INIS)

    Lu Jilong; Cheng Jinsheng; Guo Zhaohui; Li Kaibao

    2005-01-01

    Objective: By participating in IAEA-SSDL intercomparison, a dose to water calibration factor was introduced in order to check the measuring accuracy of 60 Co radiotherapy dose level standard and ensure the reliability and consistency of our calibration. Methods: The authors carried out both air kerma and absorbed dose to water calibrations against 60 Co γ-rays for one of our field class ionization chambers, and sent the results together with the chamber to IAEA dosimetry laboratory for calibration, then IAEA calibrated it and gave the deviation of the intercomparison. Results: The deviation of our air kerma calibration factors is -0.5%, and the deviation of our absorbed dose to water calibration factors is 0.4%. Conclusion: The deviation of calibration factors between IAEA and SSDL should be no more than ±1.5%. Therefore, the result of this intercomparison is considered satisfactory. (authors)

  2. Gravimetric gas determinations for volume calibration

    International Nuclear Information System (INIS)

    Gibbs, P.W.

    1991-01-01

    Gravimetric measurements of gases is one of the methods available for calibrating gas volumes. By inputting a known quantity of gas and measuring the resulting pressure and temperature, the system volume can be calculated using gas law principles. Historically, this method has been less accurate due to the difficulty in the mass determination. This difficulty comes from several sources. Two examples are the large tare weight of the gas container relative to the weight of gas and the external volume of the gas container relative to the standards. The application of a gravimetric gas determination to tank volume calibrations at the savannah River Site is discussed. Mass determinations on a 25,00 gram gas container were such that a 1500 gram quantity of gas was routinely determined to within ±0.2 gram at the 99% confidence level. In this paper the weighting design and the methods used to address the difficulties of the mass determination are detailed

  3. Guidelines for the calibration of personnel dosimeters

    International Nuclear Information System (INIS)

    Roberson, P.L.; Holbrook, K.L.

    1984-01-01

    This guide describes minimum acceptable performance levels for personnel dosimetry systems used at Department of Energy (DOE) facilities. The goal is to improve both the quality of radiological calibrations and the methods of comparing reported occupational doses between DOE facilities. Reference calibration techniques are defined. A standard for evaluation of personnel dosimetry systems and recommended design parameters for personnel dosimeters are also included. Approximate intervals for the radiation energies for which these guidelines are appropriate are 15 keV to 2 MeV for photons; above 0.3 MeV for beta particles; and 1 keV to 2 MeV for neutrons. An analysis of ANSI N13.11 was completed using performance evaluations of selected personnel dosimetry systems in use at DOE facilities. The results of this analysis are incorporated in the guidelines

  4. Calibration and intercomparison methods of dose calibrators used in nuclear medicine facilities; Metodos de calibracao e de intercomparacao de calibradores de dose utilizados em servicos de medicina nuclear

    Energy Technology Data Exchange (ETDEWEB)

    Costa, Alessandro Martins da

    1999-07-01

    Dose calibrators are used in most of the nuclear medicine facilities to determine the amount of radioactivity administered to a patient in a particular investigation or therapeutic procedure. It is therefore of vital importance that the equipment used presents good performance and is regular;y calibrated at a authorized laboratory. This occurs of adequate quality assurance procedures are carried out. Such quality control tests should be performed daily, other biannually or yearly, testing, for example, its accuracy and precision, the reproducibility and response linearity. In this work a commercial dose calibrator was calibrated with solution of radionuclides used in nuclear medicine. Simple instrument tests, such as response linearity and the response variation of the source volume increase at a constant source activity concentration, were performed. This instrument can now be used as a working standard for calibration of other dose calibrators/ An intercomparison procedure was proposed as a method of quality control of dose calibrators used in nuclear medicine facilities. (author)

  5. Dynamic photogrammetric calibration of industrial robots

    Science.gov (United States)

    Maas, Hans-Gerd

    1997-07-01

    Today's developments in industrial robots focus on aims like gain of flexibility, improvement of the interaction between robots and reduction of down-times. A very important method to achieve these goals are off-line programming techniques. In contrast to conventional teach-in-robot programming techniques, where sequences of actions are defined step-by- step via remote control on the real object, off-line programming techniques design complete robot (inter-)action programs in a CAD/CAM environment. This poses high requirements to the geometric accuracy of a robot. While the repeatability of robot poses in the teach-in mode is often better than 0.1 mm, the absolute pose accuracy potential of industrial robots is usually much worse due to tolerances, eccentricities, elasticities, play, wear-out, load, temperature and insufficient knowledge of model parameters for the transformation from poses into robot axis angles. This fact necessitates robot calibration techniques, including the formulation of a robot model describing kinematics and dynamics of the robot, and a measurement technique to provide reference data. Digital photogrammetry as an accurate, economic technique with realtime potential offers itself for this purpose. The paper analyzes the requirements posed to a measurement technique by industrial robot calibration tasks. After an overview on measurement techniques used for robot calibration purposes in the past, a photogrammetric robot calibration system based on off-the- shelf lowcost hardware components will be shown and results of pilot studies will be discussed. Besides aspects of accuracy, reliability and self-calibration in a fully automatic dynamic photogrammetric system, realtime capabilities are discussed. In the pilot studies, standard deviations of 0.05 - 0.25 mm in the three coordinate directions could be achieved over a robot work range of 1.7 X 1.5 X 1.0 m3. The realtime capabilities of the technique allow to go beyond kinematic robot

  6. A study of batch calibrations on 4 inch open faced charcoal adsorbers from four different manufacturers and how they compare to EERF's published calibration curves

    International Nuclear Information System (INIS)

    Jones, D.L.; Howell, T.E.

    1990-01-01

    The EERF Standard Operating Procedures for Rn-222 Measurements Using Charcoal Canisters is quite explicit in stating that the calibration tables and curves published in this manual are only typical calibration data that were developed for a particular batch of canisters from a supplier, and that new calibration data are developed and used with each different lot of canisters. In this paper, batch calibrations were performed in the authors' radon chambers on so called EPA style canisters from four different companies. The authors then prepared calibration tables and curves for each batch and compared them to the EERF published tables. it was our premise that EPA never intended for their curves to be considered standard and that with more and more companies manufacturing canisters, the calibration factors could certainly vary and might significantly differ from those derived by EERF several years ago

  7. Pilot study to verify the calibration of electrometers

    International Nuclear Information System (INIS)

    Becker, P.; Meghzifene, A.

    2002-01-01

    Full text: The main detector used for standardization of the quantities used in measurements of ionizing radiation is the ionization chamber. The interaction of the radiation with this detector produces electrical charge, usually, in the range of pC to nC. The instrument used to measure such small charges (or currents) is the electrometer. As part of a good practice, the measured charge (current) must be traceable to a primary or secondary standard. Some calibration laboratories can only provide a system calibration coefficient, i.e. a calibration coefficient for the combination of electrometer plus ionization chamber (Gy/scale division). This practice is acceptable, but it can impose a limitation to the automation of their calibration procedures (using computerized application for the acquisition of current/charge). Not all models have the possibility of a connection to a computer and in the case of those that don't have this capability, automation is not possible without the development of a specific interface. In addition, end-users receive a calibration coefficient, which is only valid for the set ion chamber and electrometer. In case of a broken chamber, the end-user cannot connect another chamber to their electrometer without knowing its calibration coefficient. If the calibration laboratories had the capability of calibrating the chamber separately from the electrometer, for example, using an electrometer calibrated in terms of charge, all the chambers could be calibrated using this electrometer. The laboratory can also benefit from the automation of the measurements. This requires that the laboratory must be able to cross-calibrate the electrometers (associated to the chambers) also in terms of charge (Coulombs). Electrical charge is standardized by the use of a standard air capacitor and a standard voltage source (Q=CV) and the National Laboratory for Metrology of Ionizing Radiation (IRD) in Brazil has also adopted this procedure. Since the Brazilian

  8. LANL MTI calibration team experience

    Science.gov (United States)

    Bender, Steven C.; Atkins, William H.; Clodius, William B.; Little, Cynthia K.; Christensen, R. Wynn

    2004-01-01

    The Multispectral Thermal Imager (MTI) was designed as an imaging radiometer with absolute calibration requirements established by Department of Energy (DOE) mission goals. Particular emphasis was given to water surface temperature retrieval using two mid wave and three long wave infrared spectral bands, the fundamental requirement was a surface temperature determination of 1K at the 68% confidence level. For the ten solar reflective bands a one-sigma radiometric performance goal of 3% was established. In order to address these technical challenges a calibration facility was constructed containing newly designed sources that were calibrated at NIST. Additionally, the design of the payload and its onboard calibration system supported post launch maintenance and update of the ground calibration. The on-orbit calibration philosophy also included vicarious techniques using ocean buoys, playas and other instrumented sites; these became increasingly important subsequent to an electrical failure which disabled the onboard calibration system. This paper offers various relevant lessons learned in the eight-year process of reducing to practice the calibration capability required by the scientific mission. The discussion presented will include observations pertinent to operational and procedural issues as well as hardware experiences; the validity of some of the initial assumptions will also be explored.

  9. Field calibration of cup anemometers

    DEFF Research Database (Denmark)

    Kristensen, L.; Jensen, G.; Hansen, A.

    2001-01-01

    An outdoor calibration facility for cup anemometers, where the signals from 10 anemometers of which at least one is a reference can be can be recorded simultaneously, has been established. The results are discussed with special emphasis on the statisticalsignificance of the calibration expressions...

  10. Cobalt source calibration

    International Nuclear Information System (INIS)

    Rizvi, H.M.

    1999-01-01

    The data obtained from these tests determine the dose rate of the two cobalt sources in SRTC. Building 774-A houses one of these sources while the other resides in room C-067 of Building 773-A. The data from this experiment shows the following: (1) The dose rate of the No.2 cobalt source in Building 774-A measured 1.073 x 10 5 rad/h (June 17, 1999). The dose rate of the Shepherd Model 109 Gamma cobalt source in Building 773-A measured 9.27 x 10 5 rad/h (June 25, 1999). These rates come from placing the graduated cylinder containing the dosimeter solution in the center of the irradiation chamber. (2) Two calibration tests in the 774-A source placed the graduated cylinder with the dosimeter solution approximately 1.5 inches off center in the axial direction. This movement of the sample reduced the measured dose rate 0.92% from 1.083 x 10 5 rad/h to 1.073 x 10 5 rad/h. and (3) A similar test in the cobalt source in 773-A placed the graduated cylinder approximately 2.0 inches off center in the axial direction. This change in position reduced the measured dose rate by 10.34% from 1.036 x 10 6 to 9.27 x 10 5 . This testing used chemical dosimetry to measure the dose rate of a radioactive source. In this method, one determines the dose by the chemical change that takes place in the dosimeter. For this calibration experiment, the author used a Fricke (ferrous ammonium sulfate) dosimeter. This solution works well for dose rates to 10 7 rad/h. During irradiation of the Fricke dosimeter solution the Fe 2+ ions ionize to Fe 3+ . When this occurs, the solution acquires a slightly darker tint (not visible to the human eye). To determine the magnitude of the change in Fe ions, one places the solution in an UV-VIS Spectrophotometer. The UV-VIS Spectrophotometer measures the absorbency of the solution. Dividing the absorbency by the total time (in minutes) of exposure yields the dose rate

  11. Verification of the ISO calibration method for field pyranometers under tropical sky conditions

    Science.gov (United States)

    Janjai, Serm; Tohsing, Korntip; Pattarapanitchai, Somjet; Detkhon, Pasakorn

    2017-02-01

    Field pyranomters need to be annually calibrated and the International Organization for Standardization (ISO) has defined a standard method (ISO 9847) for calibrating these pyranometers. According to this standard method for outdoor calibration, the field pyranometers have to be compared to a reference pyranometer for the period of 2 to 14 days, depending on sky conditions. In this work, the ISO 9847 standard method was verified under tropical sky conditions. To verify the standard method, calibration of field pyranometers was conducted at a tropical site located in Nakhon Pathom (13.82o N, 100.04o E), Thailand under various sky conditions. The conditions of the sky were monitored by using a sky camera. The calibration results for different time periods used for the calibration under various sky conditions were analyzed. It was found that the calibration periods given by this standard method could be reduced without significant change in the final calibration result. In addition, recommendation and discussion on the use of this standard method in the tropics were also presented.

  12. Calibration of dosemeters and survey instruments for photon

    International Nuclear Information System (INIS)

    Alamares, A.L.; Caseria, E.S.

    1995-01-01

    The Philippine Nuclear Research Institute (PNRI), the country's regulatory agency, through its Radiation Protection Unit of the Nuclear Regulations Licensing and Safeguard Division provides the calibration services of nuclear instruments used by various institutions. The periodic calibration and standardization of radiation and protection survey instruments are done to insure correct and valid radiation readings. It is also a regulatory requirement for radiation workers to use only operable and precalibrated survey instruments for their work with radioactive materials. The PNRI maintains and operates the Secondary Standard Dosimetry Laboratory (SSDL). It provides the periodic calibration and standardization of radiation monitoring and protection survey instruments, and also the radiological hazard and performance evaluation surveys of radiotherapy facilities and others. For the calibration of survey instruments, the standard sources of Cs-137 and Co-60 are used. The calibration procedures for survey meters and pocket dosimeters are explained. The clients served are shown. The personnel dosimetry using film badges, the application of ICRU operational quantities, and the problems encountered and recommendations are reported. (K.I.)

  13. Permanently calibrated interpolating time counter

    International Nuclear Information System (INIS)

    Jachna, Z; Szplet, R; Kwiatkowski, P; Różyc, K

    2015-01-01

    We propose a new architecture of an integrated time interval counter that provides its permanent calibration in the background. Time interval measurement and the calibration procedure are based on the use of a two-stage interpolation method and parallel processing of measurement and calibration data. The parallel processing is achieved by a doubling of two-stage interpolators in measurement channels of the counter, and by an appropriate extension of control logic. Such modification allows the updating of transfer characteristics of interpolators without the need to break a theoretically infinite measurement session. We describe the principle of permanent calibration, its implementation and influence on the quality of the counter. The precision of the presented counter is kept at a constant level (below 20 ps) despite significant changes in the ambient temperature (from −10 to 60 °C), which can cause a sevenfold decrease in the precision of the counter with a traditional calibration procedure. (paper)

  14. TIME CALIBRATED OSCILLOSCOPE SWEEP CIRCUIT

    Science.gov (United States)

    Smith, V.L.; Carstensen, H.K.

    1959-11-24

    An improved time calibrated sweep circuit is presented, which extends the range of usefulness of conventional oscilloscopes as utilized for time calibrated display applications in accordance with U. S. Patent No. 2,832,002. Principal novelty resides in the provision of a pair of separate signal paths, each of which is phase and amplitude adjustable, to connect a high-frequency calibration oscillator to the output of a sawtooth generator also connected to the respective horizontal deflection plates of an oscilloscope cathode ray tube. The amplitude and phase of the calibration oscillator signals in the two signal paths are adjusted to balance out feedthrough currents capacitively coupled at high frequencies of the calibration oscillator from each horizontal deflection plate to the vertical plates of the cathode ray tube.

  15. Calibrating the Cryogenian

    Science.gov (United States)

    MacDonald, F. A.; Schmitz, M. D.; Crowley, J. L.; Haam, E.; Huybers, P.; Cohen, P. A.; Johnston, D. T.

    2009-12-01

    The IGCP 512 sub-commission on the Neoproterozoic is currently discussing criteria for the definition of the Cryogenian period. Herein we provide new U/Pb ID-TIMS ages and carbon and oxygen isotope data from Fifteenmile and Mt. Harper Groups in the Yukon Territory that inform the basis for the placement of the basal Cryogenian “golden spike”. Our U/Pb ages are from volcanic tuffs interbedded within glaciogenic, fossiliferous, and carbonate strata. With the current lack of Neoproterozoic index fossils and the paucity of radiogenic age constraints, chemo-stratigraphic correlations are particularly important for tuning the Neoproterozoic timescale. In an effort to move beyond conventional 'wiggle matching', chemostratigraphic correlations are determined using a new statistical method1, which indicates that the resulting chemo-stratigraphic correlations are statistically significant. These results permit us to refine and integrate Neoproterozoic climate, microfossil, and geochemical proxy records both regionally and globally. The newly calibrated microfossil record points to a eukaryotic radiation roughly coincident with the Bitter Springs isotopic stage and a barren interval between the Sturtian and Marinoan glaciations. 1 Haam, E. & Huybers, P., 2009, A test for the presence of covariance between time-uncertain series of data with applications to the Dongge Cave speleothem and atmospheric radiocarbon records, Paleoceanography, in press.

  16. Solar Cell Calibration and Measurement Techniques

    Science.gov (United States)

    Bailey, Sheila; Brinker, Dave; Curtis, Henry; Jenkins, Phillip; Scheiman, Dave

    2004-01-01

    The increasing complexity of space solar cells and the increasing international markets for both cells and arrays has resulted in workshops jointly sponsored by NASDA, ESA and NASA. These workshops are designed to obtain international agreement on standardized values for the AMO spectrum and constant, recommend laboratory measurement practices and establish a set of protocols for international comparison of laboratory measurements. A working draft of an ISO standard, WD15387, "Requirements for Measurement and Calibration Procedures for Space Solar Cells" was discussed with a focus on the scope of the document, a definition of primary standard cell, and required error analysis for all measurement techniques. Working groups addressed the issues of Air Mass Zero (AMO) solar constant and spectrum, laboratory measurement techniques, and te international round robin methodology. A summary is presented of the current state of each area and the formulation of the ISO document.

  17. Measuring Systems for Thermometer Calibration in Low-Temperature Range

    Science.gov (United States)

    Szmyrka-Grzebyk, A.; Lipiński, L.; Manuszkiewicz, H.; Kowal, A.; Grykałowska, A.; Jancewicz, D.

    2011-12-01

    The national temperature standard for the low-temperature range between 13.8033 K and 273.16 K has been established in Poland at the Institute of Low Temperature and Structure Research (INTiBS). The standard consists of sealed cells for realization of six fixed points of the International Temperature Scale of 1990 (ITS-90) in the low-temperature range, an adiabatic cryostat and Isotech water and mercury triple-point baths, capsule standard resistance thermometers (CSPRT), and AC and DC bridges with standard resistors for thermometers resistance measurements. INTiBS calibrates CSPRTs at the low-temperature fixed points with uncertainties less than 1 mK. In lower temperature range—between 2.5 K and about 25 K — rhodium-iron (RhFe) resistance thermometers are calibrated by comparison with a standard which participated in the EURAMET.T-K1.1 comparison. INTiBS offers a calibration service for industrial platinum resistance thermometers and for digital thermometers between 77 K and 273 K. These types of thermometers may be calibrated at INTiBS also in a higher temperature range up to 550°C. The Laboratory of Temperature Standard at INTiBS acquired an accreditation from the Polish Centre for Accreditation. A management system according to EN ISO/IEC 17025:2005 was established at the Laboratory and presented on EURAMET QSM Forum.

  18. Calibration of germanium detectors

    International Nuclear Information System (INIS)

    Debertin, K.

    1983-01-01

    The process of determining the energy-dependent detection probability with measurements using Ge (Li) and high-grade germanium detectors is described. The paper explains which standards are best for a given purpose and given requirements as to accuracy, and how to assess measuring geometry variations and summation corrections. (DG) [de

  19. Novel crystal timing calibration method based on total variation

    Science.gov (United States)

    Yu, Xingjian; Isobe, Takashi; Watanabe, Mitsuo; Liu, Huafeng

    2016-11-01

    A novel crystal timing calibration method based on total variation (TV), abbreviated as ‘TV merge’, has been developed for a high-resolution positron emission tomography (PET) system. The proposed method was developed for a system with a large number of crystals, it can provide timing calibration at the crystal level. In the proposed method, the timing calibration process was formulated as a linear problem. To robustly optimize the timing resolution, a TV constraint was added to the linear equation. Moreover, to solve the computer memory problem associated with the calculation of the timing calibration factors for systems with a large number of crystals, the merge component was used for obtaining the crystal level timing calibration values. Compared with other conventional methods, the data measured from a standard cylindrical phantom filled with a radioisotope solution was sufficient for performing a high-precision crystal-level timing calibration. In this paper, both simulation and experimental studies were performed to demonstrate the effectiveness and robustness of the TV merge method. We compare the timing resolutions of a 22Na point source, which was located in the field of view (FOV) of the brain PET system, with various calibration techniques. After implementing the TV merge method, the timing resolution improved from 3.34 ns at full width at half maximum (FWHM) to 2.31 ns FWHM.

  20. Performance evaluation of commercial radionuclide calibrators in Indonesian hospitals

    International Nuclear Information System (INIS)

    Candra, Hermawan; Marsoem, Pujadi; Wurdiyanto, Gatot

    2012-01-01

    Dose calibrator is one of the supporting equipments in the field of nuclear medicine. At the hospitals, dose calibrator is used for activity measurement of radiopharmaceutical before it is administered to patients. Comparison of activity measurements of 131 I and 99m Tc with dose calibrators was organized in Indonesia during 2007–2010 with the the aim of obtaining information dose calibrator performance in the hospitals. Seven Indonesian hospitals participated in this comparison. The measurement results were evaluated using the E n criteria. The result presented in this paper facilitated the evaluation of dose calibrator performance at several hospitals. - Highlights: ► National comparisons of 131 I and 99m Tc radionuclides in Indonesian hospitals. ► Standardization using a Centronic IG11/A20 4πγ Ionization Chamber and participants using commercial radionuclide calibrators. ► Performance radionuclide calibrator in nuclear medicine in Indonesia. ► Measurement of activity of 99m Tc and 131 I was found satisfactory.

  1. Calibration techniques and results for the Portsmouth Cf shuffler

    International Nuclear Information System (INIS)

    Gross, J.C.; Wines, K.M.

    1993-01-01

    As environmental concerns over radioactive waste disposal continue to rise, the importance of Californium shufflers as a versatile waste monitoring and segregation instrument also continue to increase. The extent to which different amounts and types of materials can be measured by the shuffler is directly related to the extent of its calibration. As shufflers become more common place and their waste management uses also rise, the importance of a wide ranging and thorough calibration becomes critical. This paper presents the techniques used at the Portsmouth Gaseous Diffusion Plant for calibrating the shuffler to detect levels of U-235 in radioactive waste. While the calibration techniques are similar to those used by Los Alamos, the standards that were used were constructed somewhat differently so that geometric effects are maximized. Also presented are shuffler transmission measurements that are used to determine the matrix type and the corresponding calibration. A discussion of the calibration data is given. This discussion includes specific aspects of the calibration such as overall range, high end limits, and poly shielding range and usefulness

  2. Calibration of energy dispersive x-ray spectrometers for analysis of thin environmental samples

    International Nuclear Information System (INIS)

    Giauque, R.D.; Garrett, R.B.; Goda, L.Y.

    1976-01-01

    Four separate techniques for calibrating energy dispersive x-ray spectrometers are described. They include the use of (1) individual evaporated elemental thin-film standards, (2) nebulized multielement standard solution deposits to determine relative elemental sensitivity factors, (3) a semi-empirical approach to calculate relative elemental sensitivity factors, and (4) thick pure element disks. The first three techniques are applicable for a broad range of elements. The utilization of nebulized multielement standard solution deposits, along with an evaporated single element thin-film standard for absolute system calibration, is the most accurate method of the calibration techniques described

  3. Coincidence corrected efficiency calibration of Compton-suppressed HPGe detectors

    Energy Technology Data Exchange (ETDEWEB)

    Aucott, Timothy [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Brand, Alexander [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); DiPrete, David [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

    2015-04-20

    The authors present a reliable method to calibrate the full-energy efficiency and the coincidence correction factors using a commonly-available mixed source gamma standard. This is accomplished by measuring the peak areas from both summing and non-summing decay schemes and simultaneously fitting both the full-energy efficiency, as well as the total efficiency, as functions of energy. By using known decay schemes, these functions can then be used to provide correction factors for other nuclides not included in the calibration standard.

  4. Calibration of PKA meters against ion chambers of two geometries

    International Nuclear Information System (INIS)

    Almeida Junior, Jose N.; Terini, Ricardo A.; Pereira, Marco A.G.; Herdade, Silvio B.

    2011-01-01

    Kerma-area product (KAP or PKA) is a quantity that is independent of the distance to the X-ray tube focal spot and that can be used in radiological exams to assess the effective dose in patients. Clinical KAP meters are generally fixed in tube output and they are usually calibrated on-site by measuring the air kerma with an ion chamber and by evaluating the irradiated area by means of a radiographic image. Recently, a device was marketed (PDC, Patient Dose Calibrator, Radcal Co.), which was designed for calibrating clinical KAP meters with traceability to a standard laboratory. This paper presents a metrological evaluation of two methods that can be used in standard laboratories for the calibration of this device, namely, against a reference 30 cc ionization chamber or a reference parallel plates monitor chamber. Lower energy dependence was also obtained when the PDC calibration was made with the monitor chamber. Results are also shown of applying the PDC in hospital environment to the cross calibration of a clinical KAP meter from a radiology equipment. Results confirm lower energy dependence of the PDC relatively to the tested clinical meter. (author)

  5. Calibration of radiation protection area monitoring instruments in Sudan

    International Nuclear Information System (INIS)

    Suliman, I.I.; Youssif, B.E.; Beineen, A.A.; Hassan, M.

    2010-01-01

    This article presents results of measurements for the calibration of radiation protection area monitoring instruments carried out during the period 2006-2008 at Secondary Standard Dosimetry Laboratory of Sudan. The work performed included quality assurance measurements, measurements for the dosimeter calibrations and uncertainty analysis. Calibrations were performed using 137 Cs gamma ray sources produced by OB 85 and OB 34/1 gamma calibrators producing air kerma rate that ranged from 10 μGy/h to 50 mGy/h. Area monitoring instruments were calibrated in terms of ambient dose equivalent, H*(10) derived using air kerma to ambient dose equivalent conversion coefficients. Results are presented for 78 area monitoring instruments representing most commonly used types in Sudan. Radioactive check source measurements for the reference chamber showed deviation within 1% limit. The accuracy in the beam output measurements was within 5% internationally considered as acceptable. The results highlighted the importance of radiation protection calibrations. Regulations are further need to ensure safety aspect really meet the required international standards.

  6. Dimensional accuracy of aluminium extrusions in mechanical calibration

    Science.gov (United States)

    Raknes, Christian Arne; Welo, Torgeir; Paulsen, Frode

    2018-05-01

    Reducing dimensional variations in the extrusion process without increasing cost is challenging due to the nature of the process itself. An alternative approach—also from a cost perspective—is using extruded profiles with standard tolerances and utilize downstream processes, and thus calibrate the part within tolerance limits that are not achievable directly from the extrusion process. In this paper, two mechanical calibration strategies for the extruded product are investigated, utilizing the forming lines of the manufacturer. The first calibration strategy is based on global, longitudinal stretching in combination with local bending, while the second strategy utilizes the principle of transversal stretching and local bending of the cross-section. An extruded U-profile is used to make a comparison between the two methods using numerical analyses. To provide response surfaces with the FEA program, ABAQUS is used in combination with Design of Experiment (DOE). DOE is conducted with a two-level fractional factorial design to collect the appropriate data. The aim is to find the main factors affecting the dimension accuracy of the final part obtained by the two calibration methods. The results show that both calibration strategies have proven to reduce cross-sectional variations effectively form standard extrusion tolerances. It is concluded that mechanical calibration is a viable, low-cost alternative for aluminium parts that demand high dimensional accuracy, e.g. due to fit-up or welding requirements.

  7. The Pelindaba facility for calibrating radiometric field instruments

    International Nuclear Information System (INIS)

    Corner, B.; Toens, P.D.; Van As, D.; Vleggaar, C.M.; Richards, D.J.

    1979-04-01

    The tremendous upsurge in uranium exploration activity, experienced in recent years, has made the need for the standardisation and calibration of radiometric field instruments apparent. In order to fulfill this need, construction of a calibration facility at the National Nuclear Research Centre, Pelindaba, was commenced in 1972 and has since been extended according the the requirements of the mining industry. The facility currently comprises 11 surface standard sources suitable for the calibration, in terms of radio-element concentration, of portable scintillometers and spectrometers, and single uranium and thorium model-borehole sources which make possible the accurate calibration of borehole logging instruments both for gross-count and spectrometric surveys. Portable potassium, uranium and thorium sources are also available for the purposes of establishing airborne-spectrometer stripping ratios. The relevant physico-chemical properties of the standards are presented in this report and calibration procedures and data reduction techniques recommended. Examples are given of in situ measurements, both on surface and down-the-hole, which show that the derived calibration constants yield radiometric grades which are, on average, accurate to within 5% of the true radio-element concentrations. A secondary facility comprising single borehole- and surface-uranium sources has also been constructed in Beaufort West in the southern Karoo [af

  8. Construction and operation of an improved radiation calibration facility at Brookhaven National Laboratory. Environmental assessment

    International Nuclear Information System (INIS)

    1994-10-01

    Calibration of instruments used to detect and measure ionizing radiation has been conducted over the last 20 years at Brookhaven National Laboratory's (BNL) Radiation Calibration Facility, Building 348. Growth of research facilities, projects in progress, and more stringent Department of Energy (DOE) orders which involve exposure to nuclear radiation have placed substantial burdens on the existing radiation calibration facility. The facility currently does not meet the requirements of DOE Order 5480.4 or American National Standards Institute (ANSI) N323-1978, which establish calibration methods for portable radiation protection instruments used in the detection and measurement of levels of ionizing radiation fields or levels of radioactive surface contaminations. Failure to comply with this standard could mean instrumentation is not being calibrated to necessary levels of sensitivity. The Laboratory has also recently obtained a new neutron source and gamma beam irradiator which can not be made operational at existing facilities because of geometry and shielding inadequacies. These sources are needed to perform routine periodic calibrations of radiation detecting instruments used by scientific and technical personnel and to meet BNL's substantial increase in demand for radiation monitoring capabilities. To place these new sources into operation, it is proposed to construct an addition to the existing radiation calibration facility that would house all calibration sources and bring BNL calibration activities into compliance with DOE and ANSI standards. The purpose of this assessment is to identify potential significant environmental impacts associated with the construction and operation of an improved radiation calibration facility at BNL

  9. Calibration service of radiation detectors and dosemeters at IPEN/ Sao Paulo

    Energy Technology Data Exchange (ETDEWEB)

    Potiens, M.P.A.; Caldas, L.V.E. [IPEN, CNEN/SP, Sao Paulo (Brazil)]. e-mail: mppalbu@ipen.br

    2006-07-01

    The Calibration Laboratory of Instituto de Pesquisas Energeticas e Nucleares, IPEN, has already over 25 years been calibrating instruments used in radiation protection and therapy measurements and belonging to hospitals, industries, clinics and other users located in Sao Paulo and in other parts of Brazil. At the present time, the Calibration Laboratory is part of the Radiation Metrology Center and it acts in the Radiation Protection, Radiation Therapy, Nuclear Medicine and Diagnostic Radiology areas, using special set-ups with gamma and beta radiation sealed sources, alpha and beta radiation plane sources and low and intermediate energies of X radiation. Moreover, it has reference instruments for each calibration area with traceability to the Brazilian National Laboratory for Metrology of Ionizing Radiation (secondary standards) and international laboratories (primary standards). The number of tested instruments is increasing annually (from 170 in 1980 to 1871 in 2005), and for the development of new techniques and radiation detectors the continuous improvement of the existing calibration methods is necessary, as well as the establishment of new calibration services to be offered by the Calibration Laboratory for Brazilian and South American users. The objective of this study is to show the evolution of the calibration service developed at IPEN, describing the applied methods and the calibrated instruments types. The quality system implantation process following the basis of the NBR IEC/ISO 17025 standard is also presented with some tools used in the calibration procedures. (Author)

  10. Calibration service of radiation detectors and dosemeters at IPEN/ Sao Paulo

    International Nuclear Information System (INIS)

    Potiens, M.P.A.; Caldas, L.V.E.

    2006-01-01

    The Calibration Laboratory of Instituto de Pesquisas Energeticas e Nucleares, IPEN, has already over 25 years been calibrating instruments used in radiation protection and therapy measurements and belonging to hospitals, industries, clinics and other users located in Sao Paulo and in other parts of Brazil. At the present time, the Calibration Laboratory is part of the Radiation Metrology Center and it acts in the Radiation Protection, Radiation Therapy, Nuclear Medicine and Diagnostic Radiology areas, using special set-ups with gamma and beta radiation sealed sources, alpha and beta radiation plane sources and low and intermediate energies of X radiation. Moreover, it has reference instruments for each calibration area with traceability to the Brazilian National Laboratory for Metrology of Ionizing Radiation (secondary standards) and international laboratories (primary standards). The number of tested instruments is increasing annually (from 170 in 1980 to 1871 in 2005), and for the development of new techniques and radiation detectors the continuous improvement of the existing calibration methods is necessary, as well as the establishment of new calibration services to be offered by the Calibration Laboratory for Brazilian and South American users. The objective of this study is to show the evolution of the calibration service developed at IPEN, describing the applied methods and the calibrated instruments types. The quality system implantation process following the basis of the NBR IEC/ISO 17025 standard is also presented with some tools used in the calibration procedures. (Author)

  11. One step geometrical calibration method for optical coherence tomography

    International Nuclear Information System (INIS)

    Díaz, Jesús Díaz; Ortmaier, Tobias; Stritzel, Jenny; Rahlves, Maik; Reithmeier, Eduard; Roth, Bernhard; Majdani, Omid

    2016-01-01

    We present a novel one-step calibration methodology for geometrical distortion correction for optical coherence tomography (OCT). A calibration standard especially designed for OCT is introduced, which consists of an array of inverse pyramidal structures. The use of multiple landmarks situated on four different height levels on the pyramids allow performing a 3D geometrical calibration. The calibration procedure itself is based on a parametric model of the OCT beam propagation. It is validated by experimental results and enables the reduction of systematic errors by more than one order of magnitude. In future, our results can improve OCT image reconstruction and interpretation for medical applications such as real time monitoring of surgery. (paper)

  12. Statistical design of mass spectrometry calibration procedures

    International Nuclear Information System (INIS)

    Bayne, C.K.

    1996-11-01

    The main objective of this task was to agree on calibration procedures to estimate the system parameters (i.e., dead-time correction, ion-counting conversion efficiency, and detector efficiency factors) for SAL's new Finnigan MAT-262 mass spectrometer. SAL will use this mass spectrometer in a clean-laboratory which was opened in December 1995 to measure uranium and plutonium isotopes on environmental samples. The Finnigan MAT-262 mass spectrometer has a multi-detector system with seven Faraday cup detectors and one ion- counter for the measurement of very small signals (e.g. 10 -17 Ampere range). ORNL has made preliminary estimates of the system parameters based on SAL's experimental data measured in late 1994 when the Finnigan instrument was relatively new. SAL generated additional data in 1995 to verify the calibration procedures for estimating the dead-time correction factor, the ion-counting conversion factor and the Faraday cup detector efficiency factors. The system parameters estimated on the present data will have to be reestablished when the Finnigan MAT-262 is moved-to the new clean- laboratory. Different methods will be used to analyzed environmental samples than the current measurement methods being used. For example, the environmental samples will be electroplated on a single filament rather than using the current two filament system. An outline of the calibration standard operating procedure (SOP) is included

  13. Linear accelerator calibration monitor with a memory

    International Nuclear Information System (INIS)

    Dixon, R.L.; Ekstrand, K.E.

    1979-01-01

    A calibration monitor has been designed for measuring the constancy of linear accelerator or cobalt unit output between full calibrations. This monitor is battery-operated, light-weight, and slides into the shadow tray attachment on a linear accelerator or cobalt unit for easy setup. It provides a digital readout of the dose delivered, and a consistency check can be made in less than two minutes. The precision of the monitor, determined by cobalt-60 irradiations over a 2 1/2 month period, is +- 0.6% (standard deviation). The monitor also retains the dose reading in a CMOS digital counter indefinitely, hence it can be used in the same fashion as mailed thermoluminescent dosimeters (TLD) for calibration checks at remote facilities without the complicated readout procedures associated with TLD. The monitor can be mailed to a remote facility, positioned without ambiguity, and irradiated; and the reading can be verified on return to the originating center simply by pressing a switch. The monitor can easily be set up to carry out a ''blind'' check in which the reading obtained is not known to the remote facility

  14. Calibration of High Frequency MEMS Microphones

    Science.gov (United States)

    Shams, Qamar A.; Humphreys, William M.; Bartram, Scott M.; Zuckewar, Allan J.

    2007-01-01

    calibrate these microphones at frequencies up to 80 kHz. The technique relied on the use of a random, ultrasonic broadband centrifugal sound source located in a small anechoic chamber. Phase calibrations of the MEMS microphones were derived from cross spectral phase comparisons between the reference and test substitution microphones and an adjacent and invariant grazing-incidence 1/8-inch standard microphone.

  15. X-ray calibration qualities

    International Nuclear Information System (INIS)

    Burns, J.E.

    1998-01-01

    Since the recent publication of IAEA Technical Reports Series No. 374 ''Calibration of Dosimeters Used in Radiotheraphy'', there have been a number of queries about the origin of, and the rationale behind, the X-ray qualities recommended for calibration purposes. The simple answer is that these are the qualities derived at the UK National Physical Laboratory (NPL) in 1971 for calibration of therapy-level dosimeters and which are still in use for that purpose. As some SSDLs may have difficulties in adopting these exact combinations of kV and filtration. This paper discusses the basic ideas involved, and how to go about deriving a different series of qualities

  16. Traceable calibration of hospital 192Ir HDR sources

    International Nuclear Information System (INIS)

    Govinda Rajan, K.N.; Bhatt, B.C.; Pendse, A.M.; Kannan, V.

    2002-01-01

    Presently, no primary standard exists for the standardization of remote afterloading 192 Ir HDR sources. These sources are, therefore, being standardized by a few Secondary Standard Dosimetry Laboratories (SSDLs), in terms of Air Kerma Strength (AKS) or Reference Air Kerma Rate (RAKR) using a 0.6 cc Farmer type chamber, set up as an Interim Standard. These SSDLs offer calibration to well type of ionization chambers that are normally used by the hospitals for calibrating the 192 lr HDR source. Presently, in many countries, including India, well chambers are not commercially available. Nor do these countries offer any calibration service for 192 lr HDR source. With the result users make use of well chambers imported from different countries with their calibration traceable to the country of origin. Since no intercomparisons between these countries have been reported, the measurement consistency between hospitals becomes questionable. The problem is compounded by the fact that these chambers are used for several years without re-calibration since no calibration service is locally available. For instance, in India, the chambers have been in use in hospitals, since 1994, without a second calibration. Not all hospitals use the well chamber for the calibration of the 192 lr HDR source. Many hospitals make use of 0.6 cc chambers, in air, at short source to chamber distances, for measuring the AKS of the source. The latter method is prone to much larger inaccuracy due to the use of very short source to chamber distances without proper calibration jigs, use of 60 Co calibration factor for 192 Ir HDR source calibrations, neglecting correction factors for room scatter, fluence non-uniformity, use of arbitrary buildup factors for the buildup cap of the chamber etc. A comparison of the procedures used at hospitals revealed that various arbitrary methods are in use at hospitals. An indigenously developed well chamber was calibrated against a Reference Standard traceable to the

  17. Tritium monitor calibration at Los Alamos National Laboratory

    International Nuclear Information System (INIS)

    Bjork, C.J.; Aikin, D.J.; Houlton, T.W.

    1997-08-01

    Tritium in air is monitored at Los Alamos National Laboratory (LANL) with air breathing instruments based on ionization chambers. Stack emissions are continuously monitored from sample tubes which each connect to a Tritium bubble which differentially collects HTO and HT. A set of glass vials of glycol capture the HTO. The HT is oxidized with a palladium catalyst and the resultant HTO is captured in a second set of vials of glycol. The glycol is counted with a liquid scintillation counter. All calibrations are performed with tritium containing gas. The Radiation Instrumentation and Calibration (RIC) Team has constructed and maintains two closed loop gas handling systems based on femto TECH model U24 tritium ion chamber monitors: a fixed system housed in a fume hood and a portable system mounted on two two wheeled hand trucks. The U24 monitors are calibrated against tritium in nitrogen gas standards. They are used as standard transfer instruments to calibrate other ion chamber monitors with tritium in nitrogen, diluted with air. The gas handling systems include a circulation pump which permits a closed circulation loop to be established among the U24 monitor and typically two to four other monitors of a given model during calibration. Fixed and portable monitors can be calibrated. The stack bubblers are calibrated in the field by: blending a known concentration of tritium in air within the known volume of the two portable carts, coupled into a common loop; releasing that gas mixture into a ventilation intake to the stack; collecting oxidized tritium in the bubbler; counting the glycol; and using the stack and bubbler flow rates, computing the bubbler's efficiency. Gas calibration has become a convenient and quality tool in maintaining the tritium monitors at LANL

  18. Drift-insensitive distributed calibration of probe microscope scanner in nanometer range: Virtual mode

    Science.gov (United States)

    Lapshin, Rostislav V.

    2016-08-01

    A method of distributed calibration of a probe microscope scanner is suggested. The main idea consists in a search for a net of local calibration coefficients (LCCs) in the process of automatic measurement of a standard surface, whereby each point of the movement space of the scanner can be characterized by a unique set of scale factors. Feature-oriented scanning (FOS) methodology is used as a basis for implementation of the distributed calibration permitting to exclude in situ the negative influence of thermal drift, creep and hysteresis on the obtained results. Possessing the calibration database enables correcting in one procedure all the spatial systematic distortions caused by nonlinearity, nonorthogonality and spurious crosstalk couplings of the microscope scanner piezomanipulators. To provide high precision of spatial measurements in nanometer range, the calibration is carried out using natural standards - constants of crystal lattice. One of the useful modes of the developed calibration method is a virtual mode. In the virtual mode, instead of measurement of a real surface of the standard, the calibration program makes a surface image ;measurement; of the standard, which was obtained earlier using conventional raster scanning. The application of the virtual mode permits simulation of the calibration process and detail analysis of raster distortions occurring in both conventional and counter surface scanning. Moreover, the mode allows to estimate the thermal drift and the creep velocities acting while surface scanning. Virtual calibration makes possible automatic characterization of a surface by the method of scanning probe microscopy (SPM).

  19. A critical comparison of systematic calibration protocols for activated sludge models: a SWOT analysis.

    Science.gov (United States)

    Sin, Gürkan; Van Hulle, Stijn W H; De Pauw, Dirk J W; van Griensven, Ann; Vanrolleghem, Peter A

    2005-07-01

    Modelling activated sludge systems has gained an increasing momentum after the introduction of activated sludge models (ASMs) in 1987. Application of dynamic models for full-scale systems requires essentially a calibration of the chosen ASM to the case under study. Numerous full-scale model applications have been performed so far which were mostly based on ad hoc approaches and expert knowledge. Further, each modelling study has followed a different calibration approach: e.g. different influent wastewater characterization methods, different kinetic parameter estimation methods, different selection of parameters to be calibrated, different priorities within the calibration steps, etc. In short, there was no standard approach in performing the calibration study, which makes it difficult, if not impossible, to (1) compare different calibrations of ASMs with each other and (2) perform internal quality checks for each calibration study. To address these concerns, systematic calibration protocols have recently been proposed to bring guidance to the modeling of activated sludge systems and in particular to the calibration of full-scale models. In this contribution four existing calibration approaches (BIOMATH, HSG, STOWA and WERF) will be critically discussed using a SWOT (Strengths, Weaknesses, Opportunities, Threats) analysis. It will also be assessed in what way these approaches can be further developed in view of further improving the quality of ASM calibration. In this respect, the potential of automating some steps of the calibration procedure by use of mathematical algorithms is highlighted.

  20. The Impact of Indoor and Outdoor Radiometer Calibration on Solar Measurements: Preprint

    Energy Technology Data Exchange (ETDEWEB)

    Habte, Aron; Sengupta, Manajit; Andreas, Afshin; Reda, Ibrahim; Robinson, Justin

    2016-07-01

    Accurate solar radiation data sets are critical to reducing the expenses associated with mitigating performance risk for solar energy conversion systems, and they help utility planners and grid system operators understand the impacts of solar resource variability. The accuracy of solar radiation measured by radiometers depends on the instrument performance specification, installation method, calibration procedure, measurement conditions, maintenance practices, location, and environmental conditions. This study addresses the effect of calibration methodologies and the resulting calibration responsivities provided by radiometric calibration service providers such as the National Renewable Energy Laboratory (NREL) and manufacturers of radiometers. Some of these radiometers are calibrated indoors, and some are calibrated outdoors. To establish or understand the differences in calibration methodology, we processed and analyzed field-measured data from these radiometers. This study investigates calibration responsivities provided by NREL's broadband outdoor radiometer calibration (BORCAL) and a few prominent manufacturers. The reference radiometer calibrations are traceable to the World Radiometric Reference. These different methods of calibration demonstrated 1% to 2% differences in solar irradiance measurement. Analyzing these values will ultimately assist in determining the uncertainties of the radiometer data and will assist in developing consensus on a standard for calibration.

  1. Radiometric calibration of the in-flight blackbody calibration system of the GLORIA interferometer

    Directory of Open Access Journals (Sweden)

    C. Monte

    2014-01-01

    Atmosphere is an airborne, imaging, infrared Fourier transform spectrometer that applies the limb-imaging technique to perform trace gas and temperature measurements in the Earth's atmosphere with three-dimensional resolution. To ensure the traceability of these measurements to the International Temperature Scale and thereby to an absolute radiance scale, GLORIA carries an on-board calibration system. Basically, it consists of two identical large-area and high-emissivity infrared radiators, which can be continuously and independently operated at two adjustable temperatures in a range from −50 °C to 0 °C during flight. Here we describe the radiometric and thermometric characterization and calibration of the in-flight calibration system at the Reduced Background Calibration Facility of the Physikalisch-Technische Bundesanstalt. This was performed with a standard uncertainty of less than 110 mK. Extensive investigations of the system concerning its absolute radiation temperature and spectral radiance, its temperature homogeneity and its short- and long-term stability are discussed. The traceability chain of these measurements is presented.

  2. Calibration procedures for mammography dosemeters in Poland

    International Nuclear Information System (INIS)

    Gwiazdowska, B.; Ulkowski, P.; Tolwinski, J.; Bulski, W.

    2002-01-01

    Breast cancer is the most frequent tumour in women and the effectiveness of the treatment depends dramatically on the early detection of the disease. That is the reason why in Poland the mammography control examinations are strongly supported by the Centre of Oncology. In Poland there are over 400 mammography units which account for about 300,000 examinations per year. An investigation performed by the Medical Physics Department of the Centre of Oncology in Warsaw at about 100 mammography facilities proved that in most cases the doses absorbed by the patients could be reduced without decrease of image quality. This is one of the reasons why the Polish Secondary Standard Dosimetry Laboratory (SSDL) dealing mainly with calibration of radiotherapy dosemeters is extending its activities and therefore new facilities and equipment adapted for calibration of mammographic dosemeters have been installed. The mammography dosimetry calibration equipment is permanently installed in the same laboratory room where the radiotherapy dosemeters are calibrated. A base of a mammography unit no longer in clinical use, together with its movable system has been adapted to handle ionization chamber holders. An X-ray tube with a 50 kV high frequency generator was also installed. The tube, a Varian type OEG-50-2, (designed for laboratory applications) with molybdenum anode of an anode angle 23,7 deg. and with a large focus, effective size approximately 5 mm 2 , has an inherent filtration of 0,25 mm beryllium. It is installed in a housing with 2mm lead shielding; a cone shaped beam is formed by a system of three collimators

  3. Regression calibration with more surrogates than mismeasured variables

    KAUST Repository

    Kipnis, Victor

    2012-06-29

    In a recent paper (Weller EA, Milton DK, Eisen EA, Spiegelman D. Regression calibration for logistic regression with multiple surrogates for one exposure. Journal of Statistical Planning and Inference 2007; 137: 449-461), the authors discussed fitting logistic regression models when a scalar main explanatory variable is measured with error by several surrogates, that is, a situation with more surrogates than variables measured with error. They compared two methods of adjusting for measurement error using a regression calibration approximate model as if it were exact. One is the standard regression calibration approach consisting of substituting an estimated conditional expectation of the true covariate given observed data in the logistic regression. The other is a novel two-stage approach when the logistic regression is fitted to multiple surrogates, and then a linear combination of estimated slopes is formed as the estimate of interest. Applying estimated asymptotic variances for both methods in a single data set with some sensitivity analysis, the authors asserted superiority of their two-stage approach. We investigate this claim in some detail. A troubling aspect of the proposed two-stage method is that, unlike standard regression calibration and a natural form of maximum likelihood, the resulting estimates are not invariant to reparameterization of nuisance parameters in the model. We show, however, that, under the regression calibration approximation, the two-stage method is asymptotically equivalent to a maximum likelihood formulation, and is therefore in theory superior to standard regression calibration. However, our extensive finite-sample simulations in the practically important parameter space where the regression calibration model provides a good approximation failed to uncover such superiority of the two-stage method. We also discuss extensions to different data structures.

  4. Regression calibration with more surrogates than mismeasured variables

    KAUST Repository

    Kipnis, Victor; Midthune, Douglas; Freedman, Laurence S.; Carroll, Raymond J.

    2012-01-01

    In a recent paper (Weller EA, Milton DK, Eisen EA, Spiegelman D. Regression calibration for logistic regression with multiple surrogates for one exposure. Journal of Statistical Planning and Inference 2007; 137: 449-461), the authors discussed fitting logistic regression models when a scalar main explanatory variable is measured with error by several surrogates, that is, a situation with more surrogates than variables measured with error. They compared two methods of adjusting for measurement error using a regression calibration approximate model as if it were exact. One is the standard regression calibration approach consisting of substituting an estimated conditional expectation of the true covariate given observed data in the logistic regression. The other is a novel two-stage approach when the logistic regression is fitted to multiple surrogates, and then a linear combination of estimated slopes is formed as the estimate of interest. Applying estimated asymptotic variances for both methods in a single data set with some sensitivity analysis, the authors asserted superiority of their two-stage approach. We investigate this claim in some detail. A troubling aspect of the proposed two-stage method is that, unlike standard regression calibration and a natural form of maximum likelihood, the resulting estimates are not invariant to reparameterization of nuisance parameters in the model. We show, however, that, under the regression calibration approximation, the two-stage method is asymptotically equivalent to a maximum likelihood formulation, and is therefore in theory superior to standard regression calibration. However, our extensive finite-sample simulations in the practically important parameter space where the regression calibration model provides a good approximation failed to uncover such superiority of the two-stage method. We also discuss extensions to different data structures.

  5. Spectrophotometric calibration system for DECam

    Science.gov (United States)

    Rheault, J.-P.; DePoy, D. L.; Marshall, J. L.; Prochaska, T.; Allen, R.; Wise, J.; Martin, E.; Williams, P.

    2012-09-01

    We describe a spectrophotometric calibration system that is being implemented as part of the DES DECam project at the Blanco 4 meter at CTIO. Our calibration system uses a 1nm wide tunable source to measure the instrumental response function of the telescope optics and detector from 300nm up to 1100nm. This calibration will be performed regularly to monitor any change in the transmission function of the telescope during the 5 year survey. The system consists of a monochromator based tunable light source that provides illumination on a dome flat that is monitored by calibrated photodiodes that allow us to measure the telescope throughput as a function of wavelength. Our system has a peak output power of 2 mW, equivalent to a flux of approximately 800 photons/s/pixel on DECam.

  6. Field calibration of cup anemometers

    Energy Technology Data Exchange (ETDEWEB)

    Kristensen, L.; Jensen, G.; Hansen, A.; Kirkegaard, P.

    2001-01-01

    An outdoor calibration facility for cup anemometers, where the signals from 10 anemometers of which at least one is a reference can be recorded simultaneously, has been established. The results are discussed with special emphasis on the statistical significance of the calibration expressions. It is concluded that the method has the advantage that many anemometers can be calibrated accurately with a minimum of work and cost. The obvious disadvantage is that the calibration of a set of anemometers may take more than one month in order to have wind speeds covering a sufficiently large magnitude range in a wind direction sector where we can be sure that the instruments are exposed to identical, simultaneous wind flows. Another main conclusion is that statistical uncertainty must be carefully evaluated since the individual 10 minute wind-speed averages are not statistically independent. (au)

  7. Calibration of radiation monitoring instruments

    International Nuclear Information System (INIS)

    1973-01-01

    Radiation protection is dependent on good radiation monitoring, and properly calibrated instruments are essential for this work. Simple procedures for periodically checking and recalibrating different kinds of radiation monitoring instruments are shown in this training film

  8. Calibration of "Babyline" RP instruments

    CERN Multimedia

    2015-01-01

      If you have old RP instrumentation of the “Babyline” type, as shown in the photo, please contact the Radiation Protection Group (Joffrey Germa, 73171) to have the instrument checked and calibrated. Thank you. Radiation Protection Group

  9. Calibration of radiation monitoring instruments

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1974-12-31

    Radiation protection is dependent on good radiation monitoring, and properly calibrated instruments are essential for this work. Simple procedures for periodically checking and recalibrating different kinds of radiation monitoring instruments are shown in this training film

  10. Development of a correction factor for Xe-133 vials for use with a dose calibrator

    International Nuclear Information System (INIS)

    Gels, G.L.; Piltingsrud, H.V.

    1982-01-01

    Manufacturers of dose calibrators who give calibration settings for various radionuclies sometimes do not specify the type of radionuclide container the calibration is for. The container, moreover, may not be of the same type as those a user might purchase. When these factors are not considered, the activity administered to the patient may be significantly different from that intended. An experiment is described in which calibration factors are determined for measurement of Xe-133 activity in vials in a dose calibrator. This was accomplished by transferring the Xe-133 from the commercial vials to standard NBS calibration ampules. Based on ten such transfers, the resulting correction factor for the dose calibrator was 1.22

  11. Rotary mode system initial instrument calibration

    International Nuclear Information System (INIS)

    Johns, B.R.

    1994-01-01

    The attached report contains the vendor calibration procedures used for the initial instrument calibration of the rotary core sampling equipment. The procedures are from approved vendor information files

  12. Pressures Detector Calibration and Measurement

    CERN Document Server

    AUTHOR|(CDS)2156315

    2016-01-01

    This is report of my first and second projects (of 3) in NA61. I did data taking and analysis in order to do calibration of pressure detectors and verified it. I analyzed the data by ROOT software using the C ++ programming language. The first part of my project was determination of calibration factor of pressure sensors. Based on that result, I examined the relation between pressure drop, gas flow rate of in paper filter and its diameter.

  13. The KLOE online calibration system

    International Nuclear Information System (INIS)

    Pasqualucci, E.; Alexander, G.; Aloisio, A.

    2001-01-01

    Based on all the features of the KLOE online software, the online calibration system performs current calibration quality checking in real time and starts automatically new calibration procedures when needed. A calibration manager process controls the system, implementing the interface to the online system, receiving information from the run control and translating its state transitions to a separate state machine. It acts as a 'calibration run controller' and performs failure recovery when requested by a set of process checkers. The core of the system is a multi-threaded OO histogram server that receives histogramming commands by remote processes and operates on local ROOT histograms. A client library and C, fortran and C++ application interface libraries allow the user to connect and define his own histogram or read histograms owned by others using an book-like interface. Several calibration processes running in parallel in a distributed, multiplatform environment can fill the same histograms, allowing fast external information check. A monitor thread allow remote browsing for visual inspection. Pre-filtered data are read in non-privileged spy mode from the data acquisition system via the Kloe Integrated Dataflow. The main characteristics of the system are presented

  14. The ENEA calibration service for ionising radiations. Part 1: Photons

    International Nuclear Information System (INIS)

    Monteventi, F.; Sermenghi, I.

    1999-01-01

    The ENEA (National Agency for New Technology, Energy and the Environment) calibration service for ionizing radiations has been active for 40 years in the secondary standard dosimetry laboratory web. It has been the first center, in 1985, to be acknowledges by the Italian calibration service (SIT) for the two quantities for photons: exposure and air kerma. Since the Institute for the Radiation Protection of ENEA has moved to the new site in Montecuccolino (Bologna, Italy) in 1995, the whole laboratory has been renovated and all irradiation rooms together with radiation source and equipment have been reorganized according to the Χ, γ, β and neutron fields metrology requirements. The aim of this report, as the first part of a report describing all facilities available at the service, is to give a detailed description of all equipment s qualified for photon fields metrology including the secondary standards and the calibration procedures performed for radiation monitoring devices and dosemeters [it

  15. High dose calibrations at the Pacific Northwest Laboratory

    International Nuclear Information System (INIS)

    McDonald, J.C.; Fox, R.A.

    1988-10-01

    The need is increasing for both high radiation exposures and calibration measurements that provide traceability of such exposures to national standards. The applications of high exposures include: electronic component damage studies, sterilization of medical products and food irradiation. Accurate high exposure measurements are difficult to obtain and cannot, in general, be carried out with a single dose measurement system or technique because of the wide range of doses and the variety of materials involved. This paper describes the dosimetric measurement and calibration techniques used at the Pacific Northwest Laboratory (PNL) that make use of radiochromic dye films, thermoluminescent dosimeters (TLDs), ionization chambers, and calorimetric dosimeters. The methods used to demonstrate the consistency of PNL calibrations with national standards will also be discussed. 4 refs

  16. Improving quantitative precision and throughput by reducing calibrator use in liquid chromatography-tandem mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Rule, Geoffrey S., E-mail: geoffrey.s.rule@aruplab.com [ARUP Institute for Clinical and Experimental Pathology, 500 Chipeta Way, Salt Lake City, UT 84108 (United States); Rockwood, Alan L. [ARUP Institute for Clinical and Experimental Pathology, 500 Chipeta Way, Salt Lake City, UT 84108 (United States); Department of Pathology, University of Utah School of Medicine, 2100 Jones Medical Research Bldg., Salt Lake City, UT 84132 (United States)

    2016-05-05

    To improve efficiency in our mass spectrometry laboratories we have made efforts to reduce the number of calibration standards utilized for quantitation over time. We often analyze three or more batches of 96 samples per day, on a single instrument, for a number of assays. With a conventional calibration scheme at six concentration levels this amounts to more than 5000 calibration points per year. Modern LC-tandem mass spectrometric instrumentation is extremely rugged however, and isotopically labelled internal standards are widely available. This made us consider whether alternative calibration strategies could be utilized to reduce the number of calibration standards analyzed while still retaining high precision and accurate quantitation. Here we demonstrate how, by utilizing a single calibration point in each sample batch, and using the resulting response factor (RF) to update an existing, historical response factor (HRF), we are able to obtain improved precision over a conventional multipoint calibration approach, as judged by quality control samples. The laboratory component of this study was conducted with an existing LC tandem mass spectrometric method for three androgen analytes in our production laboratory. Using examples from both simulated and laboratory data we illustrate several aspects of our single point alternative calibration strategy and compare it with a conventional, multipoint calibration approach. We conclude that both the cost and burden of preparing multiple calibration standards with every batch of samples can be reduced while at the same time maintaining, or even improving, analytical quality. - Highlights: • Use of a weighted single point calibration approach improves quantitative precision. • A weighted response factor approach incorporates historical calibration information. • Several scenarios are discussed with regard to their influence on quantitation.

  17. Improving quantitative precision and throughput by reducing calibrator use in liquid chromatography-tandem mass spectrometry

    International Nuclear Information System (INIS)

    Rule, Geoffrey S.; Rockwood, Alan L.

    2016-01-01

    To improve efficiency in our mass spectrometry laboratories we have made efforts to reduce the number of calibration standards utilized for quantitation over time. We often analyze three or more batches of 96 samples per day, on a single instrument, for a number of assays. With a conventional calibration scheme at six concentration levels this amounts to more than 5000 calibration points per year. Modern LC-tandem mass spectrometric instrumentation is extremely rugged however, and isotopically labelled internal standards are widely available. This made us consider whether alternative calibration strategies could be utilized to reduce the number of calibration standards analyzed while still retaining high precision and accurate quantitation. Here we demonstrate how, by utilizing a single calibration point in each sample batch, and using the resulting response factor (RF) to update an existing, historical response factor (HRF), we are able to obtain improved precision over a conventional multipoint calibration approach, as judged by quality control samples. The laboratory component of this study was conducted with an existing LC tandem mass spectrometric method for three androgen analytes in our production laboratory. Using examples from both simulated and laboratory data we illustrate several aspects of our single point alternative calibration strategy and compare it with a conventional, multipoint calibration approach. We conclude that both the cost and burden of preparing multiple calibration standards with every batch of samples can be reduced while at the same time maintaining, or even improving, analytical quality. - Highlights: • Use of a weighted single point calibration approach improves quantitative precision. • A weighted response factor approach incorporates historical calibration information. • Several scenarios are discussed with regard to their influence on quantitation.

  18. X-ray photoelectron spectrometer calibration and thin film investigations on germanium oxides

    OpenAIRE

    Deegan, Terri

    1998-01-01

    The first aim of this project was the characterisation of the VG Scientific Clam 100 based, XPS (X-ray Photoelectron Spectroscopy). Spectrometer in the Physics department at Dublin City University Detailed energy scale and intensity scale calibrations were carried out using sputter-cleaned Au (Gold), Ag (Silver), Cu (Copper) and Pd (Palladium) foil samples. Analysis of these calibration spectra against standard reference spectra led to an accurate energy calibration and the production of indi...

  19. Calibration of ratemeters used for gamma radiation detection

    International Nuclear Information System (INIS)

    Hantanirina, P.A.

    2017-01-01

    The Secondary Standard Dosimetry Laboratory (SSDL) of INSTN-Madagascar is in charge of the calibration of every dosimetry measurement instrument in hospitals and companies using radioactive sources in Madagascar. It has a secondary standard delivered and calibrated by a Primary Standard Laboratory in Dosimetry (PSLD). This standard is used to compare its reference values with those displayed on the instruments to be calibrated. During our training period, three (3) ratemeters were calibrated, the Graetz X5DE, the Graetz X5C and the Identifinder 2. We have determined the calibration factor for every ratemeter by doing calculation with the reference value. By using the three surveymeters for direct radiations measurements, it has been found that the difference between the displayed values and the real values for every ratemeter does not exceed the tolerance limit which is 20 %. Then we can conclude that these ratemeters are still in good condition of functioning. Concerning the calibration factor curve N_k with the K_a_i_r , we can observe that for the Graetz X5C ratemeter, this curve is almost constant. As well as for the linearity, it is still the Graetz X5C ratemeter which is linear almost integrally for the measured and calculated dose rate values. So we can say that this ratemeter is the most recommended for the radiations measurements.This work which has been carried within the framework of collaboration between the section PNAE (Physique Nucléaire Appliquée et Environnement) of the University of Antananarivo and INSTN-Madagascar has been a good and rewarding experience which allowed us to put into practice all knowledges acquired during our years of studies. [fr

  20. Calibration of Ga-68 activity for PET applications in Cuba

    International Nuclear Information System (INIS)

    García Rodríguez, Lourdes; Oropesa Verdecia, Pilar; Serra Águila, Rolando A.; Moreno León, Yecenia; Jénez Magaña, Yoel; Pérez LoretdeMola, Nayla; Bell Hechavarría, Ailec; Mas Ruiz, Javier; Cassette, Philippe

    2016-01-01

    A Ga-68 solution was used to calibrate the activity concentration using the double-triple coincidence ratio (TDCR) method of liquid scintillation for the first time in the country. The expanded uncertainty (k = 2) of the concentration of Ga-68 activity in the calibrated solution was equal to 2%. For measurements, the commercial liquid scintillation counter HIDEXTM was used. Samples were prepared by adding between 40 and 50 mg of the radioactive solution to 15 mL of ULTIMAGOLD ™ scintillating cocktail. For the estimation of Ga-68 counting efficiencies in the samples used for the calibration, a FORTRAN program developed by the National Institute of Metrology of France for the magnitudes of ionizing radiation, LNHB, was used. The validation of the method was carried out by the calibration of a standard solution of Na-22, also positronic emitter with similar disintegration scheme to Ga-68. The difference between the concentration of Na-22 activity measured using the TDCR method and the certified reference value traceable to the National Institute of Metrology of the United States (NIST) was 0.15%. With the solution of Ga-68 standardized by the TDCR method the calibration of the secondary standard activity meter, model CAPINTEC CRCTM 15R, was carried out for a geometry of 2R flask with 1mL of radioactive solution. Afterwards, this standard activity meter was calibrated for the measurement of Ga-68 in the geometries of interest in nuclear medicine: Flask 15R with 6 mL of radioactive solution, 2.5 mL syringe with 2 mL of radioactive solution and 5 mL syringe with 2 mL of radioactive solution. The results presented in this paper constitute the necessary metrological support for the introduction of new PET and PET / CT technologies into medical practice in Cuba.