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Sample records for advanced fracture characterization

  1. Advanced Characterization of Fractured Reservoirs in Carbonate Rocks: The Michigan Basin

    Energy Technology Data Exchange (ETDEWEB)

    Wood, James R.; Harrison, William B.

    2000-10-24

    The main objective of this project is for a university-industry consortium to develop a comprehensive model for fracture carbonate reservoirs based on the ''data cube'' concept using the Michigan Basin as a prototype. This project combined traditional historical data with 2D and 3D seismic data as well as data from modern logging tools in a novel way to produce a new methodology for characterizing fractured reservoirs in carbonate rocks. Advanced visualization software was used to fuse the data and to image it on a variety of scales, ranging from basin-scale to well-scales.

  2. Advanced characterization of pores and fractures in coals by nuclear magnetic resonance and X-ray computed tomography

    Institute of Scientific and Technical Information of China (English)

    2010-01-01

    This paper demonstrates capabilities of low-field nuclear magnetic resonance (NMR) and microfocus X-ray computed tomography (μCT) in advanced, nondestructive, and quantitative characterization of pore types, producible porosity, pore structure, and spatial disposition of pore-fractures in coals. Results show that the NMR transverse relaxation time (T2) at 0.5–2.5, 20–50, and >100 ms correspond to pores of <0.1 μm, >0.1 μm, and fractures, respectively. A much higher T2 spectrum peak reflects a much better development of pores (or fractures) corresponding to the T2, and vice versa. Three basic components in coals, i.e., the pores (or fractures), coal matrix, and minerals have their distinctive range of CT numbers. Among these, the CT number of pores is commonly less than 600 HU. The producible porosity, which is a determination of permeability, can be calculated by T2 cutoff value (T2C) of coal NMR. The coal pore structure can be efficiently estimated by the newly proposed "T2C based model". Finally, μCT scan was proven capable of modeling and spatial visualization of pores and fractures.

  3. Geostatistics for fracture characterization

    International Nuclear Information System (INIS)

    As the critical role of fractures has become more apparent in fluid flow and contaminant transport studies, the characterization of fracture networks has received considerable attention in a wide variety of applications such as nuclear waste repository design. The application of geostatistics to fracture characterization has traditionally involved modelling fractures as thin disks; assumptions about the frequency, orientation, length and width of these disks allow the construction of a 3D model of the fracture network. This paper examines alternatives whose statistical parameters are more relevant for contaminant transport studies and are also easier to infer and validate. A new algorithm for conditional simulation is presented, one that is able to honor multipoint statistics through annealing. By honoring statistics that capture with two-point spatial convariances, this algorithm offers an important new tool not only for the specific problem of fracture characterization but also for the more general problem of spatial simulation

  4. FRACTURING FLUID CHARACTERIZATION FACILITY

    Energy Technology Data Exchange (ETDEWEB)

    Subhash Shah

    2000-08-01

    Hydraulic fracturing technology has been successfully applied for well stimulation of low and high permeability reservoirs for numerous years. Treatment optimization and improved economics have always been the key to the success and it is more so when the reservoirs under consideration are marginal. Fluids are widely used for the stimulation of wells. The Fracturing Fluid Characterization Facility (FFCF) has been established to provide the accurate prediction of the behavior of complex fracturing fluids under downhole conditions. The primary focus of the facility is to provide valuable insight into the various mechanisms that govern the flow of fracturing fluids and slurries through hydraulically created fractures. During the time between September 30, 1992, and March 31, 2000, the research efforts were devoted to the areas of fluid rheology, proppant transport, proppant flowback, dynamic fluid loss, perforation pressure losses, and frictional pressure losses. In this regard, a unique above-the-ground fracture simulator was designed and constructed at the FFCF, labeled ''The High Pressure Simulator'' (HPS). The FFCF is now available to industry for characterizing and understanding the behavior of complex fluid systems. To better reflect and encompass the broad spectrum of the petroleum industry, the FFCF now operates under a new name of ''The Well Construction Technology Center'' (WCTC). This report documents the summary of the activities performed during 1992-2000 at the FFCF.

  5. Advanced Characterization of Fractured Reservoirs in Carbonate Rocks: The Michigan Basin

    Energy Technology Data Exchange (ETDEWEB)

    Wood, James R.; Harrison, William B.

    2002-12-02

    The purpose of the study was to collect and analyze existing data on the Michigan Basin for fracture patterns on scales ranging form thin section to basin. The data acquisition phase has been successfully concluded with the compilation of several large digital databases containing nearly all the existing information on formation tops, lithology and hydrocarbon production over the entire Michigan Basin. These databases represent the cumulative result of over 80 years of drilling and exploration.

  6. ADVANCED CHARACTERIZATION OF FRACTURED RESERVOIRS IN CARBONATE ROCKS: THE MICHIGAN BASIN

    Energy Technology Data Exchange (ETDEWEB)

    James R. Wood; William B. Harrison

    2000-04-01

    Progress in year 2 of this project is highlighted by the completing of the writing and testing of the project database, ''Atlas'', and populating it with all the project data gathered to date. This includes digitization of 17,000+ original Scout Tickets for the Michigan Basin. Work continues on the Driller's Reports, where they have scanned about 50,000 pages out of an estimated 300,000 pages. All of the scanned images have been attached to ''Atlas'', the visual database viewer developed for this project. A complete set of the 1/24,000 USGS DEM (Digital Elevation Models) for the State of Michigan has been downloaded from the USGS Web sites, decompressed and converted to ArcView Grid files. A large-scale map (48 inches x 84 inches) has been constructed by mosaicking of the high-resolution files. This map shows excellent ground surface detail and has drawn much comment and requests for copies at the venues where it has been displayed. Although it was generated for mapping of surface lineations the map has other uses, particularly analysis of the glacial drift in Michigan. It presents unusual problems due to its size and they are working with vendors on compression and display algorithms (e.g. MrSID{copyright}) in an attempt to make it available over the Internet, both for viewing and download. A set of aeromagnetic data for the Michigan Basin has been acquired and is being incorporated into the study. As reported previously, the general fracture picture in the Michigan Basin is a dominant NW-SE trend with a conjugate NE-SW trend. Subsurface, DEM and gravity data support the interpretation of a graben-type deep basement structural trend coincident with the Michigan Basin Gravity High. They plan to incorporate the aeromagnetic data into this interpretation as well.

  7. Advanced Reservoir Characterization and Evaluation of C02 Gravity Drainage in the Naturally Fractured Sprayberry Trend Area

    Energy Technology Data Exchange (ETDEWEB)

    David S. Schechter

    1998-04-30

    The objective is to assess the economic feasibility of CO2 flooding of the naturally fractured Straberry Trend Area in west Texas. Research is being conducted in the extensive characterization of the reservoirs, the experimental studies of crude oil/brine/rock (COBR) interaction in the reservoirs, the analytical and numerical simulation of Spraberry reservoirs, and the experimental investigations on CO2 gravity drainage in Spraberry whole cores.

  8. Advanced Reservoir Characterization and Evaluation of CO2 Gravity Drainage in the Naturally Fractured Spraberry Trend Area, Class III

    Energy Technology Data Exchange (ETDEWEB)

    Knight, Bill; Schechter, David S.

    2002-07-26

    The goal of this project was to assess the economic feasibility of CO2 flooding the naturally fractured Spraberry Trend Area in west Texas. This objective was accomplished through research in four areas: (1) extensive characterization of the reservoirs, (2) experimental studies of crude oil/brine/rock (COBR) interactions in the reservoirs, (3) reservoir performance analysis, and (4) experimental investigations on CO2 gravity drainage in Spraberry whole cores. This provides results of the final year of the six-year project for each of the four areas.

  9. Advanced Reservoir Characterization and Evaluation of CO{sub 2} Gravity Drainage in the Naturally Fractured Spraberry Trend Area

    Energy Technology Data Exchange (ETDEWEB)

    Schechter, D.S.

    1999-02-03

    The overall goal of this project is to assess the economic feasibility of CO{sub 2} flooding the naturally fractured Spraberry Trend Area in West Texas. This objective is being accomplished by conducting research in four areas: (1) extensive characterization of the reservoirs, (2) experimental studies of crude oil/brine/rock (COBR) interactions in the reservoirs, (3) reservoir performance analysis, and, (4) experimental investigations on CO2 gravity drainage in Spraberry whole cores. This report provides results of the third year of the five-year project for each of the four areas including a status report of field activities leading up to injection of CO2.

  10. Advanced reservoir characterization and evaluation of CO2 gravity drainage in the naturally fractured Spraberry Trend Area. Annual report, September 1, 1996--August 31, 1997

    Energy Technology Data Exchange (ETDEWEB)

    McDonald, P.

    1998-06-01

    The objective of the Spraberry CO{sub 2} pilot project is to determine the technical and economic feasibility of continuous CO{sub 2} injection in the naturally fractured reservoirs of the Spraberry Trend. In order to describe, understand, and model CO{sub 2} flooding in the naturally fractured Spraberry reservoirs, characterization of the fracture system is a must. Additional reservoir characterization was based on horizontal coring in the second year of the project. In addition to characterization of natural fractures, horizontal coring has confirmed a previously developed rock model for describing the Spraberry Trend shaly sands. A better method for identifying Spraberry pay zones has been verified. The authors have completed the reservoir characterization, which includes matrix description and detection (from core-log integration) and fracture characterization. This information is found in Section 1. The authors have completed extensive imbibition experiments that strongly indicate that the weakly water-wet behavior of the reservoir rock may be responsible for poor waterflood response observed in many Spraberry fields. The authors have also made significant progress in analytical and numerical simulation of performance in Spraberry reservoirs as seen in Section 3. They have completed several suites of CO{sub 2} gravity drainage in Spraberry and Berea whole cores at reservoir conditions and reported in Section 4. The results of these experiments have been useful in developing a model for free-fall gravity drainage and have validated the premise that CO{sub 2} will recover oil from tight, unconfined Spraberry matrix.

  11. IPIRG programs - advances in pipe fracture technology

    Energy Technology Data Exchange (ETDEWEB)

    Wilkowski, G.; Olson, R.; Scott, P. [Batelle, Columbus, OH (United States)

    1997-04-01

    This paper presents an overview of the advances made in fracture control technology as a result of the research performed in the International Piping Integrity Research Group (IPIRG) program. The findings from numerous experiments and supporting analyses conducted to investigate the behavior of circumferentially flawed piping and pipe systems subjected to high-rate loading typical of seismic events are summarized. Topics to be discussed include; (1) Seismic loading effects on material properties, (2) Piping system behavior under seismic loads, (3) Advances in elbow fracture evaluations, and (4) {open_quotes}Real{close_quotes} piping system response. The presentation for each topic will be illustrated with data and analytical results. In each case, the state-of-the-art in fracture mechanics prior to the first IPIRG program will be contrasted with the state-of-the-art at the completion of the IPIRG-2 program.

  12. Advances in treating exposed fractures.

    Science.gov (United States)

    Nogueira Giglio, Pedro; Fogaça Cristante, Alexandre; Ricardo Pécora, José; Partezani Helito, Camilo; Lei Munhoz Lima, Ana Lucia; Dos Santos Silva, Jorge

    2015-01-01

    The management of exposed fractures has been discussed since ancient times and remains of great interest to present-day orthopedics and traumatology. These injuries are still a challenge. Infection and nonunion are feared complications. Aspects of the diagnosis, classification and initial management are discussed here. Early administration of antibiotics, surgical cleaning and meticulous debridement are essential. The systemic conditions of patients with multiple trauma and the local conditions of the limb affected need to be taken into consideration. Early skeletal stabilization is necessary. Definitive fixation should be considered when possible and provisional fixation methods should be used when necessary. Early closure should be the aim, and flaps can be used for this purpose. PMID:26229904

  13. Advances in treating exposed fractures

    Directory of Open Access Journals (Sweden)

    Pedro Nogueira Giglio

    2015-04-01

    Full Text Available The management of exposed fractures has been discussed since ancient times and remains of great interest to present-day orthopedics and traumatology. These injuries are still a challenge. Infection and nonunion are feared complications. Aspects of the diagnosis, classification and initial management are discussed here. Early administration of antibiotics, surgical cleaning and meticulous debridement are essential. The systemic conditions of patients with multiple trauma and the local conditions of the limb affected need to be taken into consideration. Early skeletal stabilization is necessary. Definitive fixation should be considered when possible and provisional fixation methods should be used when necessary. Early closure should be the aim, and flaps can be used for this purpose.

  14. Application of geophysical methods for fracture characterization

    International Nuclear Information System (INIS)

    One of the most crucial needs in the design and implementation of an underground waste isolation facility is a reliable method for the detection and characterization of fractures in zones away from boreholes or subsurface workings. Geophysical methods may represent a solution to this problem. If fractures represent anomalies in the elastic properties or conductive properties of the rocks, then the seismic and electrical techniques may be useful in detecting and characterizing fracture properties. 7 refs., 3 figs

  15. Seismic characterization of fracture properties

    International Nuclear Information System (INIS)

    The purpose of this paper is to show that there is a relationship, both empirical and theoretical, between the measured seismic response, the mechanical stiffness (also referred to as specific stiffness) of fractures and their hydraulic conductivity. Laboratory measurements of the mechanical stiffness, hydraulic conductivity and seismic properties of natural fractures are summarized. A theoretical model for the amplitude and group time delay for compressional and shear waves transmitted across a single fracture is presented. Predictions based on this model are compared with laboratory measurements. Finally, the results for a single fracture are extended to multiple parallel fractures. 13 refs., 6 figs

  16. Natural fracture characterization using passive seismic illumination

    Energy Technology Data Exchange (ETDEWEB)

    Nihei, K.T.

    2003-01-08

    The presence of natural fractures in reservoir rock can significantly enhance gas production, especially in tight gas formations. Any general knowledge of the existence, location, orientation, spatial density, and connectivity of natural fractures, as well as general reservoir structure, that can be obtained prior to active seismic acquisition and drilling can be exploited to identify key areas for subsequent higher resolution active seismic imaging. Current practices for estimating fracture properties before the acquisition of surface seismic data are usually based on the assumed geology and tectonics of the region, and empirical or fracture mechanics-based relationships between stratigraphic curvature and fracturing. The objective of this research is to investigate the potential of multicomponent surface sensor arrays, and passive seismic sources in the form of local earthquakes to identify and characterize potential fractured gas reservoirs located near seismically active regions. To assess the feasibility of passive seismic fracture detection and characterization, we have developed numerical codes for modeling elastic wave propagation in reservoir structures containing multiple, finite-length fractures. This article describes our efforts to determine the conditions for favorable excitation of fracture converted waves, and to develop an imaging method that can be used to locate and characterize fractures using multicomponent, passive seismic data recorded on a surface array.

  17. On the fracture toughness of advanced materials

    Energy Technology Data Exchange (ETDEWEB)

    Launey, Maximilien E.; Ritchie, Robert O.

    2008-11-24

    Few engineering materials are limited by their strength; rather they are limited by their resistance to fracture or fracture toughness. It is not by accident that most critical structures, such as bridges, ships, nuclear pressure vessels and so forth, are manufactured from materials that are comparatively low in strength but high in toughness. Indeed, in many classes of materials, strength and toughness are almost mutually exclusive. In the first instance, such resistance to fracture is a function of bonding and crystal structure (or lack thereof), but can be developed through the design of appropriate nano/microstructures. However, the creation of tough microstructures in structural materials, i.e., metals, polymers, ceramics and their composites, is invariably a compromise between resistance to intrinsic damage mechanisms ahead of the tip of a crack (intrinsic toughening) and the formation of crack-tip shielding mechanisms which principally act behind the tip to reduce the effective 'crack-driving force' (extrinsic toughening). Intrinsic toughening is essentially an inherent property of a specific microstructure; it is the dominant form of toughening in ductile (e.g., metallic) materials. However, for most brittle (e.g., ceramic) solids, and this includes many biological materials, it is largely ineffective and toughening conversely must be developed extrinsically, by such shielding mechanisms as crack bridging. From a fracture mechanics perspective, this results in toughening in the form of rising resistance-curve behavior where the fracture resistance actually increases with crack extension. The implication of this is that in many biological and high-strength advanced materials, toughness is developed primarily during crack growth and not for crack initiation. This is an important realization yet is still rarely reflected in the way that toughness is measured, which is invariably involves the use of single-value (crack-initiation) parameters such as

  18. Fractal characterization of fracture surfaces in concrete

    Science.gov (United States)

    Saouma, V.E.; Barton, C.C.; Gamaleldin, N.A.

    1990-01-01

    Fractal geometry is used to characterize the roughness of cracked concrete surfaces through a specially built profilometer, and the fractal dimension is subsequently correlated to the fracture toughness and direction of crack propagation. Preliminary results indicate that the fracture surface is indeed fractal over two orders of magnitudes with a dimension of approximately 1.20. ?? 1990.

  19. Laboratory Hydraulic Fracture Characterization Using Acoustic Emission

    Science.gov (United States)

    Gutierrez, M.

    2013-05-01

    For many years Acoustic Emission (AE) testing has aided in the understanding of fracture initiation and propagation in geologic materials. AEs occur when a material emits elastic waves caused by the sudden occurrence of fractures or frictional sliding along discontinuous surfaces and grain boundaries. One important application of AE is the monitoring of hydraulic fracturing of underground formations to create functional reservoirs at sites where the permeability of the rock is too limited to allow for cost effective fluid extraction. However, several challenges remain in the use of AE to locate and characterize fractures that are created hydraulically. Chief among these challenges is the often large scatter of the AE data that are generated during the fracturing process and the difficulty of interpreting the AE data so that hydraulic fractures can be reliably characterized. To improve the understanding of the link between AE and hydraulic fracturing, laboratory scale model testing of hydraulic fracturing were performed using a cubical true triaxial device. This device consist of a loading frame capable of loading a 30x30x30 cm3 rock sample with three independent principal stresses up to 13 MPa while simultaneously providing heating up to 180 degrees C. Several laboratory scale hydraulic fracture stimulation treatments were performed on granite and rock analogue fabricated using medium strength concrete. A six sensor acoustic emission (AE) array, using wideband piezoelectric transducers, is employed to monitor the fracturing process. AE monitoring of laboratory hydraulic fracturing experiments showed multiple phenomena including winged fracture growth from a borehole, cross-field well communication, fracture reorientation, borehole casing failure and much more. AE data analysis consisted of event source location determination, fracture surface generation and validation, source mechanism determination, and determining the overall effectiveness of the induced fracture

  20. Advanced reservoir characterization and evaluation of CO{sub 2} gravity drainage in the naturally fractured Spraberry Trend Area. Annual report, September 1, 1995--August 31, 1996

    Energy Technology Data Exchange (ETDEWEB)

    Schechter, D.S.

    1997-12-01

    The overall goal of this project is to assess the economic feasibility of CO{sub 2} flooding in the naturally fractured Spraberry Trend Area in West Texas. This objective is being accomplished by conducting research in four areas: (1) extensive characterization of the reservoirs, (2) experimental studies of crude oil/brine/rock (COBR) interaction in the reservoirs, (3) analytical and numerical simulation of Spraberry reservoirs, and, (4) experimental investigations on CO{sub 2} gravity drainage in Spraberry whole cores. This report provides results of the first year of the five-year project for each of the four areas.

  1. Advanced reservoir characterization and evaluation of CO{sub 2} gravity drainage in the naturally fractured Spraberry Trend Area, Class III

    Energy Technology Data Exchange (ETDEWEB)

    Heckman, Tracy; Schechter, David S.

    2000-04-11

    The overall goal of this project was to assess the economic feasibility of CO{sub 2} flooding the naturally fractured Spraberry Trend Area in West Texas. This objective was accomplished by conducting research in four areas: (1) extensive characterization of the reservoirs, (2) experimental studies of crude oil/brine/rock (COBR) interaction in the reservoirs, (3) analytical and numerical simulation of Spraberry reservoirs, and, (4) experimental investigations on CO{sub 2} gravity drainage in Spraberry whole cores. This report provides results of the fourth year of the five-year project for each of the four areas including a status report of field activities leading up to injection of CO{sub 2}.

  2. Advanced reservoir characterization and evaluation of CO{sub 2} gravity drainage in the naturally fractured Spraberry Trend Area. Annual report, September 1, 1996--August 31, 1997

    Energy Technology Data Exchange (ETDEWEB)

    Schechter, D.S.

    1998-07-01

    The overall goal of this project is to assess the economic feasibility of CO{sub 2} flooding the naturally fractured Spraberry Trend Area in West Texas. This objective is being accomplished by conducting research in four areas: (1) extensive characterization of the reservoirs, (2) experimental studies of crude oil/brine/rock (COBR) interaction in the reservoirs, (3) reservoir performance analysis, and (4) experimental investigations on CO{sub 2} gravity drainage in Spraberry whole cores. This report provides results of the second year of the five-year project for each of the four areas. In the first area, the author has completed the reservoir characterization, which includes matrix description and detection (from core-log integration) and fracture characterization. This information is found in Section 1. In the second area, the author has completed extensive inhibition experiments that strongly indicate that the weakly water-wet behavior of the reservoir rock may be responsible for poor waterflood response observed in many Spraberry fields. In the third area, the author has made significant progress in analytical and numerical simulation of performance in Spraberry reservoirs as seen in Section 3. In the fourth area, the author has completed several suites of CO{sub 2} gravity drainage in Spraberry and Berea whole cores at reservoir conditions and reported in Section 4. The results of these experiments have been useful in developing a model for free-fall gravity drainage and have validated the premise that CO{sub 2} will recover oil from tight, unconfined Spraberry matrix. The final three years of this project involves implementation of the CO{sub 2} pilot. Up to twelve new wells are planned in the pilot area; water injection wells to contain the CO{sub 2}, three production wells to monitor performance of CO{sub 2}, CO{sub 2} injection wells including one horizontal injection well and logging observation wells to monitor CO{sub 2} flood fronts. Results of drilling

  3. Advancements in classification, treatment and outcome of radial head fractures

    OpenAIRE

    Dijk, van, G.; Jupiter, J.B.; Kloen, P.; Ring, D.C.; Guitton, T.G.

    2011-01-01

    This thesis shows that advancements in technical head fractures analysis, imaging modalities, increased interest in psychosocial aspects of treatment and the availability of long-term outcome data can help improve classification, treatment and outcome in fractures of the radial head. It is science that created these advancements and through adequate scientific evaluation of these advancements we can continue creating more effective treatments for patients.

  4. Advancements in classification, treatment and outcome of radial head fractures

    NARCIS (Netherlands)

    T.G. Guitton

    2011-01-01

    This thesis shows that advancements in technical head fractures analysis, imaging modalities, increased interest in psychosocial aspects of treatment and the availability of long-term outcome data can help improve classification, treatment and outcome in fractures of the radial head. It is science t

  5. Advances and disputes of posterior malleolus fracture

    Institute of Scientific and Technical Information of China (English)

    FU Su; ZOU Zhen-yu; MEI Gang; JIN Dan

    2013-01-01

    Objective The objective of this article is to summarize the development of evaluation and treatment of posterior malleolus fracture (PMF).Data sources Data used in this review were mainly from English literature of PubMed data base.Study selection Articles were included in this review if they were related to the PMF or trimalleolar fracture.Results No consensus was found regarding what sizes of posterior malleolus fragments would lead to ankle instability thus affecting prognosis and should be fixed.Ⅹ-ray measurement is unreliable,while CT scan is widely recommended and it can recognize the occult posterior malleolus fractures associated with tibia shaft fractures,which are always undetected previously.Direct posterior malleolus fixation is suitable to stabilize syndesmotic injury.The basic and clinical researches support direct reduction and buttress plate fixation of posterior malleolus fracture through the posterolateral approach.Operative indications and timing of weight bearing are still in discussion.Conclusions Knowing whether ankle instability occurs and the proper methods to diagnose,evaluate,and operate can help manage the fracture.Further biomechanical research on ankle stability and clinical study to compare various treatment methods are required.

  6. Use of fracture mechanics parameters to characterize comminution

    OpenAIRE

    Hao, Bin

    1996-01-01

    This report is to investigate the use of fracture mechanics parameters (fracture toughness, specific work of fracture) to characterize comminution process. Comminution is a very important industrial process and is extremely low in efficiency. Establishment of a crushing index based on fracture mechanics principles is of great significance for improved machine design and enhanced efficiency. Single particle fracture study has been reviewed because it is considered the most eleme...

  7. Proceedings of the International Symposium on Dynamics of Fluids in Fractured Rocks: Concepts and Recent Advances

    Energy Technology Data Exchange (ETDEWEB)

    Faybishenko, B. (ed.)

    1999-02-01

    This publication contains extended abstracts of papers presented at the International Symposium ''Dynamics of Fluids in Fractured Rocks: Concepts and Recent Advances'' held at Ernest Orlando Lawrence Berkeley National Laboratory on February 10-12, 1999. This Symposium is organized in Honor of the 80th Birthday of Paul A. Witherspoon, who initiated some of the early investigations on flow and transport in fractured rocks at the University of California, Berkeley, and at Lawrence Berkeley National Laboratory. He is a key figure in the development of basic concepts, modeling, and field measurements of fluid flow and contaminant transport in fractured rock systems. The technical problems of assessing fluid flow, radionuclide transport, site characterization, modeling, and performance assessment in fractured rocks remain the most challenging aspects of subsurface flow and transport investigations. An understanding of these important aspects of hydrogeology is needed to assess disposal of nu clear wastes, development of geothermal resources, production of oil and gas resources, and remediation of contaminated sites. These Proceedings of more than 100 papers from 12 countries discuss recent scientific and practical developments and the status of our understanding of fluid flow and radionuclide transport in fractured rocks. The main topics of the papers are: Theoretical studies of fluid flow in fractured rocks; Multi-phase flow and reactive chemical transport in fractured rocks; Fracture/matrix interactions; Hydrogeological and transport testing; Fracture flow models; Vadose zone studies; Isotopic studies of flow in fractured systems; Fractures in geothermal systems; Remediation and colloid transport in fractured systems; and Nuclear waste disposal in fractured rocks.

  8. Sensors for hydraulic-induced fracturing characterization

    Science.gov (United States)

    Mireles, Jose, Jr.; Estrada, Horacio; Ambrosio, Roberto C.

    2011-06-01

    Hydraulic induced fracturing (HIF) in oil wells is used to increase oil productivity by making the subterranean terrain more deep and permeable. In some cases HIF connects multiple oil pockets to the main well. Currently there is a need to understand and control with a high degree of precision the geometry, direction, and the physical properties of fractures. By knowing these characteristics (the specifications of fractures), other drill well locations and set-ups of wells can be designed to increase the probability of connection of the oil pockets to main well(s), thus, increasing productivity. The current state of the art of HIF characterization does not meet the requirements of the oil industry. In Mexico, the SENER-CONACyT funding program recently supported a three party collaborative effort between the Mexican Petroleum Institute, Schlumberger Dowell Mexico, and the Autonomous University of Juarez to develop a sensing scheme to measure physical parameters of a HIF like, but not limited to pressure, temperature, density and viscosity. We present in this paper a review of HIF process, its challenges and the progress of sensing development for down hole measurement parameters of wells for the Chicontepec region of Mexico.

  9. Characterization of borehole fractures by the body and interface waves

    NARCIS (Netherlands)

    Henry, F.

    2005-01-01

    The success of the fracturing process in the oil and gas industry depends on our ability to define the hydraulic fracture geometry. To have a method of measurement for characterizing completely the fracture dimensions from a single well in reliable way, will be a primordial importance, in term of ec

  10. Linking advanced fracture models to structural analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chiesa, Matteo

    2001-07-01

    Shell structures with defects occur in many situations. The defects are usually introduced during the welding process necessary for joining different parts of the structure. Higher utilization of structural materials leads to a need for accurate numerical tools for reliable prediction of structural response. The direct discretization of the cracked shell structure with solid finite elements in order to perform an integrity assessment of the structure in question leads to large size problems, and makes such analysis infeasible in structural application. In this study a link between local material models and structural analysis is outlined. An ''ad hoc'' element formulation is used in order to connect complex material models to the finite element framework used for structural analysis. An improved elasto-plastic line spring finite element formulation, used in order to take cracks into account, is linked to shell elements which are further linked to beam elements. In this way one obtain a global model of the shell structure that also accounts for local flexibilities and fractures due to defects. An important advantage with such an approach is a direct fracture mechanics assessment e.g. via computed J-integral or CTOD. A recent development in this approach is the notion of two-parameter fracture assessment. This means that the crack tip stress tri-axiality (constraint) is employed in determining the corresponding fracture toughness, giving a much more realistic capacity of cracked structures. The present thesis is organized in six research articles and an introductory chapter that reviews important background literature related to this work. Paper I and II address the performance of shell and line spring finite elements as a cost effective tool for performing the numerical calculation needed to perform a fracture assessment. In Paper II a failure assessment, based on the testing of a constraint-corrected fracture mechanics specimen under tension, is

  11. Fracture Characterization in the Astor Pass Geothermal Field, Nevada

    Science.gov (United States)

    Walsh, D. C.; Reeves, D. M.; Pohll, G.; Lyles, B. F.; Cooper, C. A.

    2011-12-01

    The Astor Pass geothermal field, near Pyramid Lake, NV, is under study as a site of potential geothermal energy production. Three wells have been completed in the graben of this typical Basin and Range geologic setting. Lithologies include a layer of unconsolidated sediment (basin fill) underlain by various tertiary volcanic units and granodiorite and metavolcanic basement rock. Characterization of fractures within the relatively impermeable rock matrix is being conducted for the three wells. Statistical analysis of fracture orientation, densities, and spacing obtained from borehole imaging logs is used to determine stress orientation and to generate a statistically equivalent Discrete Fracture Network (DFN) model. Fractures at depth are compared to fracture data collected in nearby outcrops of the same lithologic stratigraphy. Fracture geometry and density is correlated to mechanically discrete layers within the stratigraphy to test whether variations in fracturing can be attributed to variations in Young's modulus. Correlation of fracture geometry and densities with spinner flowmeter logs and distributed temperature sensor records are made in an effort to identify potential flowing fracture zones intersecting the borehole. Mean fracture aperture is obtained from open fracture counts and reservoir-scale transmissivity values (computed from a 30 day pump test) in the absence of readily available aperture data. The goal of this thorough fracture characterization is to create a physically relevant model which may be coupled with a multipurpose fluid flow and thermal simulator for investigation of geothermal reservoir behavior, particularly at the borehole scale.

  12. Experimental fracture toughness characterization using the modified TSD specimen

    DEFF Research Database (Denmark)

    Berggreen, Christian; Quispitupa, Amilcar; Alonso, Jose L.;

    2010-01-01

    The modified Tilted Sandwich Debond (TSD) specimen provides an improved methodology for characterization of the face/core fracture resistance. An experimental mixed mode characterization of the fracture toughness spanning a large range of phase angles has been achieved by specific steel bar...

  13. Approach for computing 1D fracture density: application to fracture corridor characterization

    Science.gov (United States)

    Viseur, Sophie; Chatelée, Sebastien; Akriche, Clement; Lamarche, Juliette

    2016-04-01

    Fracture density is an important parameter for characterizing fractured reservoirs. Many stochastic simulation algorithms that generate fracture networks indeed rely on the determination of a fracture density on volumes (P30) to populate the reservoir zones with individual fracture surfaces. However, only 1D fracture density (P10) are available from subsurface data and it is then important to be able to accurately estimate this entity. In this paper, a novel approach is proposed to estimate fracture density from scan-line or well data. This method relies on regression, hypothesis testing and clustering techniques. The objective of the proposed approach is to highlight zones where fracture density are statistically very different or similar. This technique has been applied on both synthetic and real case studies. These studies concern fracture corridors, which are particular tectonic features that are generally difficult to characterize from subsurface data. These tectonic features are still not well known and studies must be conducted to better understand their internal spatial organization and variability. The presented synthetic cases aim at showing the ability of the approach to extract known features. The real case study illustrates how this approach allows the internal spatial organization of fracture corridors to be characterized.

  14. Seismic Fracture Characterization Methodologies for Enhanced Geothermal Systems

    Energy Technology Data Exchange (ETDEWEB)

    Queen, John H. [Hi-Geophysical, Inc., Ponca, OK (United States)

    2016-05-09

    effective seismic tools for getting information on the internal structure of faults and fractures in support of fluid flow pathway management and EGS treatment. Scattered events similar to those expected from faults and fractures are seen in the VSP reported here. Unfortunately, the source offset and well depth coverage do not allow for detailed analysis of these events. This limited coverage also precluded the use of advanced migration and imaging algorithms. More extensive acquisition is needed to support fault and fracture characterization in the geothermal reservoir at Brady's Hot Springs. The VSP was effective in generating interval velocity estimates over the depths covered by the array. Upgoing reflection events are also visible in the VSP results at locations corresponding to reflection events in the surface seismic. Overall, the high temperature rated fiber optic sensors used in the VSP produced useful results. Modeling has been found useful in the interpretation of both surface reflection seismic and VSP data. It has helped identify possible near surface scattering in the surface seismic data. It has highlighted potential scattering events from deeper faults in the VSP data. Inclusion of more detailed fault and fracture specific stiffness parameters are needed to fully interpret fault and fracture scattered events for flow properties (Pyrak-Nolte and Morris, 2000, Zhu and Snieder, 2002). Shear wave methods were applied in both the surface seismic reflection and VSP work. They were not found to be effective in the Brady's Hot Springs area. This was due to the extreme attenuation of shear waves in the near surface at Brady's. This does not imply that they will be ineffective in general. In geothermal areas where good shear waves can be recorded, modeling suggests they should be very useful for characterizing faults and fractures.

  15. Advanced studies on Simulation Methodologies for very Complicated Fracture Phenomena

    Science.gov (United States)

    Nishioka, Toshihisa

    2010-06-01

    Although nowadays, computational techniques are well developed, for Extremely Complicated Fracture Phenomena, they are still very difficult to simulate, for general engineers, researchers. To overcome many difficulties in those simulations, we have developed not only Simulation Methodologies but also theoretical basis and concepts. We sometimes observe extremely complicated fracture patterns, especially in dynamic fracture phenomena such as dynamic crack branching, kinking, curving, etc. For examples, although the humankind, from primitive men to modern scientists such as Albert Einstein had watched the post-mortem patterns of dynamic crack branching, the governing condition for the onset of the phenomena had been unsolved until our experimental study. From in these studies, we found the governing condition of dynamic crack bifurcation, as follows. When the total energy flux per unit time into a propagating crack tip reaches the material crack resistance, the crack braches into two cracks [total energy flux criterion]. The crack branches many times whenever the criterion is satisfied. Furthermore, the complexities also arise due to their time-dependence and/or their-deformation dependence. In order to make it possible to simulate such extremely complicated fracture phenomena, we developed many original advanced computational methods and technologies. These are (i)moving finite element method based on Delaunay automatic triangulation (MFEMBOAT), path independent,(ii) equivalent domain integral expression of the dynamic J integral associated with a continuous auxiliary function,(iii) Mixed phase path-prediction mode simulation, (iv) implicit path prediction criterion. In this paper, these advanced computational methods are thoroughly explained together with successful comparison with the experimental results. Since multiple dynamic crack branching phenomena may be most complicated fracture due to complicated fracture paths, and its time dependence (transient), this

  16. FTIR characterization of advanced materials

    Science.gov (United States)

    Young, P. R.; Chang, A. C.

    1986-01-01

    This paper surveys the application of Fourier transform infrared spectroscopy to the characterization of advanced materials. FTIR sampling techniques including internal and external reflectance and photoacoustic spectroscopy are discussed. Representative examples from the literature of the analysis of resins, fibers, prepregs and composites are reviewed. A discussion of several promising specialized FTIR techniques is also presented.

  17. Characterizing Fracture Spatial Patterns by Using Semivariograms

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Semivariogram is applied to fracture data obtained from detailed scanline surveys of nine field sites in western New York, USA in order to investigate the spatial patterns of natural fractures. The length of the scanline is up to 36 m. How both fracture spacing and fracture length vary with distance is determined through semivariogram calculations. In this study, the authors developed a FORTRAN program to resample the fracture data from the scanline survey. By calculating experimental semivariogram, the authors found five different types of spatial patterns that can be described by linear, spherical, reversed spherical, polynomial I (for a0) models, of which the last three are newly proposed in this study. The well-structured semivariograms of fracture spacing and length indicate that both the location of the fractures and the length distribution within their structure domains are not random. The results of this study also suggest that semivariograms can provide useful information in terms of spatial correlation distance for fracture location and fracture length. These semivariograms can also be utilized to design more efficient sampling schemes for further surveys, as well as to define the limits of highly probable extrapolation of a structure domain.

  18. Characterization of reservoir fractures using conventional geophysical logging

    Directory of Open Access Journals (Sweden)

    Paitoon Laongsakul

    2011-04-01

    Full Text Available In hydrocarbon exploration fractures play an important role as possible pathways for the hydrocarbon flow and bythis enhancing the overall formation’s permeability. Advanced logging methods for fracture analysis, like the boreholeacoustic televiewer and Formation Microscanner (FMS are available, but these are additional and expensive tools. However,open and with water or hydrocarbon filled fractures are also sensitive to electrical and other conventional logging methods.For this study conventional logging data (electric, seismic, etc were available plus additional fracture information from FMS.Taking into account the borehole environment the results show that the micro-spherically focused log indicates fractures byshowing low resistivity spikes opposite open fractures, and high resistivity spikes opposite sealed ones. Compressional andshear wave velocities are reduced when passing trough the fracture zone, which are assumed to be more or less perpendicularto borehole axis. The photoelectric absorption curve exhibit a very sharp peak in front of a fracture filled with bariteloaded mud cake. The density log shows low density spikes that are not seen by the neutron log, usually where fractures,large vugs, or caverns exist. Borehole breakouts can cause a similar effect on the logging response than fractures, but fracturesare often present when this occurs. The fracture index calculation by using threshold and input weight was calculatedand there was in general a good agreement with the fracture data from FMS especially in fracture zones, which mainlycontribute to the hydraulic system of the reservoir. Finally, the overall results from this study using one well are promising,however further research in the combination of different tools for fracture identification is recommended as well as the useof core for further validation.

  19. Fracture characterization from formation microlmager data

    NARCIS (Netherlands)

    Ponziani, M.; Slob, E.C.; Luthi, S.M.; Bloemenkamp, R.F.; Le Nir, I.

    2013-01-01

    The Formation MicroImager (mark of Schlumberger) is an electric imaging tool that produces electrical scans of the borehole walls. These measurements provide useful information on the fracture aperture of naturally fractured reservoirs. In this paper, we present a laboratory set-up that was realized

  20. Characterization of fracture loci in metal forming

    DEFF Research Database (Denmark)

    Martins, P.A.F.; Bay, Niels; Tekkaya, A.E.;

    2014-01-01

    Fracture in metal forming can occur in three different modes: (i) tensile; (ii) in-plane shear; and (iii) out-of-plane shear (respectively the same as modes I, II and III of fracture mechanics). The circumstances under which each mode will occur are identified in terms of plastic flow and microst...

  1. AN ADVANCED FRACTURE CHARACTERIZATION AND WELL PATH NAVIGATION SYSTEM FOR EFFECTIVE RE-DEVELOPMENT AND ENHANCEMENT OF ULTIMATE RECOVERY FROM THE COMPLEX MONTEREY RESERVOIR OF SOUTH ELLWOOD FIELD, OFFSHORE CALIFORNIA

    Energy Technology Data Exchange (ETDEWEB)

    Steve Horner

    2004-04-29

    Venoco Inc, intends to re-develop the Monterey Formation, a Class III basin reservoir, at South Ellwood Field, Offshore Santa Barbara, California. Well productivity in this field varies significantly. Cumulative Monterey production for individual wells has ranged from 260 STB to 8,700,000 STB. Productivity is primarily affected by how well the well path connects with the local fracture system and the degree of aquifer support. Cumulative oil recovery to date is a small percentage of the original oil in place. To embark upon successful re-development and to optimize reservoir management, Venoco intends to investigate, map and characterize field fracture patterns and the reservoir conduit system. State of the art borehole imaging technologies including FMI, dipole sonic and cross-well seismic, interference tests and production logs will be employed to characterize fractures and micro faults. These data along with the existing database will be used for construction of a novel geologic model of the fracture network. Development of an innovative fracture network reservoir simulator is proposed to monitor and manage the aquifer's role in pressure maintenance and water production. The new fracture simulation model will be used for both planning optimal paths for new wells and improving ultimate recovery. In the second phase of this project, the model will be used for the design of a pilot program for downhole water re-injection into the aquifer simultaneously with oil production. Downhole water separation units attached to electric submersible pumps will be used to minimize surface fluid handling thereby improving recoveries per well and field economics while maintaining aquifer support. In cooperation with the DOE, results of the field studies as well as the new models developed and the fracture database will be shared with other operators. Numerous fields producing from the Monterey and analogous fractured reservoirs both onshore and offshore will benefit from the

  2. AN ADVANCED FRACTURE CHARACTERIZATION AND WELL PATH NAVIGATION SYSTEM FOR EFFECTIVE RE-DEVELOPMENT AND ENHANCEMENT OF ULTIMATE RECOVERY FROM THE COMPLEX MONTEREY RESERVOIR OF SOUTH ELLWOOD FIELD, OFFSHORE CALIFORNIA

    Energy Technology Data Exchange (ETDEWEB)

    Steve Horner; Iraj Ershaghi

    2002-04-30

    Venoco Inc, intends to re-develop the Monterey Formation, a Class III basin reservoir, at South Ellwood Field, Offshore Santa Barbara, California. Well productivity in this field varies significantly. Cumulative Monterey production for individual wells has ranged from 260 STB to 8,700,000 STB. Productivity is primarily affected by how well the well path connects with the local fracture system and the degree of aquifer support. Cumulative oil recovery to date is a small percentage of the original oil in place. To embark upon successful redevelopment and to optimize reservoir management, Venoco intends to investigate, map and characterize field fracture patterns and the reservoir conduit system. State of the art borehole imaging technologies including FMI, dipole sonic and cross-well seismic, interference tests and production logs will be employed to characterize fractures and micro faults. These data along with the existing database will be used for construction of a novel geologic model of the fracture network. Development of an innovative fracture network reservoir simulator is proposed to monitor and manage the aquifer's role in pressure maintenance and water production. The new fracture simulation model will be used for both planning optimal paths for new wells and improving ultimate recovery. In the second phase of this project, the model will be used for the design of a pilot program for downhole water re-injection into the aquifer simultaneously with oil production. Downhole water separation units attached to electric submersible pumps will be used to minimize surface fluid handling thereby improving recoveries per well and field economics while maintaining aquifer support. In cooperation with the DOE, results of the field studies as well as the new models developed and the fracture database will be shared with other operators. Numerous fields producing from the Monterey and analogous fractured reservoirs both onshore and offshore will benefit from the

  3. Site characterization in densely fractured dolomite: Comparison of methods

    Science.gov (United States)

    Muldoon, M.; Bradbury, K.R.

    2005-01-01

    One of the challenges in characterizing fractured-rock aquifers is determining whether the equivalent porous medium approximation is valid at the problem scale. Detailed hydrogeologic characterization completed at a small study site in a densely fractured dolomite has yielded an extensive data set that was used to evaluate the utility of the continuum and discrete-fracture approaches to aquifer characterization. There are two near-vertical sets of fractures at the site; near-horizontal bedding-plane partings constitute a third fracture set. Eighteen boreholes, including five coreholes, were drilled to a depth of ???10.6 m. Borehole geophysical logs revealed several laterally extensive horizontal fractures and dissolution zones. Flowmeter and short-interval packer testing identified which of these features were hydraulically important. A monitoring system, consisting of short-interval piezometers and multilevel samplers, was designed to monitor four horizontal fractures and two dissolution zones. The resulting network consisted of >70 sampling points and allowed detailed monitoring of head distributions in three dimensions. Comparison of distributions of hydraulic head - and hydraulic conductivity determined by these two approaches suggests that even in a densely fractured-carbonate aquifer, a characterization approach using traditional long-interval monitoring wells is inadequate to characterize ground water movement for the purposes of regulatory monitoring or site remediation. In addition, traditional multiwell pumping tests yield an average or bulk hydraulic conductivity that is not adequate for predicting rapid ground water travel times through the fracture network, and the pumping test response does not appear to be an adequate tool for assessing whether the porous medium approximation is valid. Copyright ?? 2005 National Ground Water Association.

  4. Development of Reservoir Characterization Techniques and Production Models for Exploiting Naturally Fractured Reservoirs

    Energy Technology Data Exchange (ETDEWEB)

    Wiggins, Michael L.; Brown, Raymon L.; Civan, Frauk; Hughes, Richard G.

    2001-08-15

    Research continues on characterizing and modeling the behavior of naturally fractured reservoir systems. Work has progressed on developing techniques for estimating fracture properties from seismic and well log data, developing naturally fractured wellbore models, and developing a model to characterize the transfer of fluid from the matrix to the fracture system for use in the naturally fractured reservoir simulator.

  5. Characterization of fracture toughness of epoxy resin after hygrothermal aging

    KAUST Repository

    Quispe, Gustavo Q.

    2013-07-01

    Characterization of fracture toughness of epoxy resin after hygrothermal ageing Gustavo Quino Quispe The aim of this work is to characterize the e ects of hygrothermal aging in the plain strain fracture toughness of the epoxy system composed by cycloaliphatic epoxy resin and diglycidyl ether of bisphenol-A (DGEBA). For this, after having been under hygrothermal aging in a climatic chamber, epoxy samples were studied using ASTM D5045 fracture toughness test, and micrography and roughness measurements of the fracture surface. It is reported a rapid decrease of GIc and KIc during the rst 2 days. Moreover, a numerical model [13] was used to simulate and see with more detail the water absorption in the aged samples. From that, it was observed the heterogeneous distribution of water. Accordingly, it was proposed that the results should be correlated with the water content at the vicinity of the crack tip. Consequently, it was possible to obtain, by quasi-static simulations, the ideal load-displacement curves of crack propagation in the heterogeneous samples. Finally, another contribution of this work is the study of the fracture surface, that gives a clue of the relationship among the fracture energy, the appearance of microcracks in the fracture surface, and the roughness (Ra).

  6. Advanced reservoir characterization and evaluation of CO{sub 2} gravity drainage in the naturally fractured Spraberry Trend Area. First annual technical progress report, September 1, 1995--August 31, 1996

    Energy Technology Data Exchange (ETDEWEB)

    Schechter, D.S.

    1996-12-17

    The overall goal of this project is to assess the economic feasibility of CO{sub 2} flooding the naturally fractured Spraberry Trend Area in West Texas. This objective is being accomplished by conducting research in four areas: (1) extensive characterization of the reservoirs, (2) experimental studies of crude oil/brine/rock (COBR) interaction in the reservoirs, (3) analytical and numerical simulation of Spraberry reservoirs, and, (4) experimental investigations on CO{sub 2} gravity drainage in Spraberry whole cores. This report provides results of the first year of the five-year project for each of the four areas.

  7. Advanced fracture modeling in the Uinta Basin (Utah) for optimized primary and secondary recovery. Final report, September 1998

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1998-12-01

    The completed study focused on an area fracture-controlled highly unpredictable, fracture-controlled production near the Duchesne Fault Zone, Uinta Basin, in northeastern Utah. Production is seriously influenced by numerous high-angle faults and associated fractures--represented at the surface by a set of parallel, N80{degree}W-trending lineaments, and intricate fracture patterns in outcrop. Specific production is erratic and secondary recovery design is difficult because well-specific structural characterization and local fracture patterns are poorly understood. Furthermore, numerical models to simulate fluid flow in fractured reservoirs were either overly simplistic (did not adequately account for mechanical contrasts between matrix and fractures) or were extremely complex, requiring volumes of data typically not available to the operator. The contractors proposed implementing advanced geological, geomechanical and reservoir engineering methods to recognize and model the complex fracture networks exhibited at the surface and suggested in the shallow subsurface in the Duchesne Fault Zone. The intended methodology was to be developed in a data-limited environment, recognizing that operators in the basin will not have the financial resources or motivation to perform sophisticated and expensive reservoir engineering programs. User-friendly models for permeability, stress, and production using key geological and geophysical data, developed in this study can then be used to determine: economic placement of future operations, assessment of recoverable hydrocarbons, and forecasting of primary and secondary recovery.

  8. Characterization of EGS Fracture Network Lifecycles

    Energy Technology Data Exchange (ETDEWEB)

    Gillian R. Foulger

    2008-03-31

    Geothermal energy is relatively clean, and is an important non-hydrocarbon source of energy. It can potentially reduce our dependence on fossil fuels and contribute to reduction in carbon emissions. High-temperature geothermal areas can be used for electricity generation if they contain permeable reservoirs of hot water or steam that can be extracted. The biggest challenge to achieving the full potential of the nation’s resources of this kind is maintaining and creating the fracture networks required for the circulation, heating, and extraction of hot fluids. The fundamental objective of the present research was to understand how fracture networks are created in hydraulic borehole injection experiments, and how they subsequently evolve. When high-pressure fluids are injected into boreholes in geothermal areas, they flow into hot rock at depth inducing thermal cracking and activating critically stressed pre-existing faults. This causes earthquake activity which, if monitored, can provide information on the locations of the cracks formed, their time-development and the type of cracking underway, e.g., whether shear movement on faults occurred or whether cracks opened up. Ultimately it may be possible to monitor the critical earthquake parameters in near-real-time so the information can be used to guide the hydraulic injection while it is in progress, e.g., how to adjust factors such as injectate pressure, volume and temperature. In order to achieve this, it is necessary to mature analysis techniques and software that were, at the start of this project, in an embryonic developmental state. Task 1 of the present project was to develop state-of-the-art techniques and software for calculating highly accurate earthquake locations, earthquake source mechanisms (moment tensors) and temporal changes in reservoir structure. Task 2 was to apply the new techniques to hydrofracturing (Enhanced Geothermal Systems, or “EGS”) experiments performed at the Coso geothermal field

  9. Statistical analysis of surface lineaments and fractures for characterizing naturally fractured reservoirs

    Energy Technology Data Exchange (ETDEWEB)

    Guo, Genliang; George, S.A.; Lindsey, R.P.

    1997-08-01

    Thirty-six sets of surface lineaments and fractures mapped from satellite images and/or aerial photos from parts of the Mid-continent and Colorado Plateau regions were collected, digitized, and statistically analyzed in order to obtain the probability distribution functions of natural fractures for characterizing naturally fractured reservoirs. The orientations and lengths of the surface linear features were calculated using the digitized coordinates of the two end points of each individual linear feature. The spacing data of the surface linear features within an individual set were, obtained using a new analytical sampling technique. Statistical analyses were then performed to find the best-fit probability distribution functions for the orientation, length, and spacing of each data set. Twenty-five hypothesized probability distribution functions were used to fit each data set. A chi-square goodness-of-fit test was used to rank the significance of each fit. A distribution which provides the lowest chi-square goodness-of-fit value was considered the best-fit distribution. The orientations of surface linear features were best-fitted by triangular, normal, or logistic distributions; the lengths were best-fitted by PearsonVI, PearsonV, lognormal2, or extreme-value distributions; and the spacing data were best-fitted by lognormal2, PearsonVI, or lognormal distributions. These probability functions can be used to stochastically characterize naturally fractured reservoirs.

  10. Site characterization in fractured crystalline rock

    International Nuclear Information System (INIS)

    This report concerns a study which is part of the SKI performance assessment project SITE-94. SITE-94 is a performance assessment of a hypothetical repository at a real site. The main objective of the project is to determine how site specific data should be assimilated into the performance assessment process and to evaluate how uncertainties inherent in site characterization will influence performance assessment results. Other important elements of SITE-94 are the development of a practical and defensible methodology for defining, constructing and analyzing scenarios, the development of approaches for treatment of uncertainties, evaluation of canister integrity, and the development and application of an appropriate Quality Assurance plan for Performance Assessments. (111 refs.)

  11. Development of an Advanced Hydraulic Fracture Mapping System

    Energy Technology Data Exchange (ETDEWEB)

    Norm Warpinski; Steve Wolhart; Larry Griffin; Eric Davis

    2007-01-31

    The project to develop an advanced hydraulic fracture mapping system consisted of both hardware and analysis components in an effort to build, field, and analyze combined data from tiltmeter and microseismic arrays. The hardware sections of the project included: (1) the building of new tiltmeter housings with feedthroughs for use in conjunction with a microseismic array, (2) the development of a means to use separate telemetry systems for the tilt and microseismic arrays, and (3) the selection and fabrication of an accelerometer sensor system to improve signal-to-noise ratios. The analysis sections of the project included a joint inversion for analysis and interpretation of combined tiltmeter and microseismic data and improved methods for extracting slippage planes and other reservoir information from the microseisms. In addition, testing was performed at various steps in the process to assess the data quality and problems/issues that arose during various parts of the project. A prototype array was successfully tested and a full array is now being fabricated for industrial use.

  12. NATO Advanced Study Institute on Disorder and Fracture

    CERN Document Server

    Roux, S; Guyon, E

    1990-01-01

    Fracture, and particularly brittle fracture, is a good example of an instability. For a homogeneous solid, subjected to a uniform stress field, a crack may appear anywhere in the structure once the threshold stress is reached. However, once a crack has been nucleated in some place, further damage in the solid will in most cases propagate from the initial crack, and not somewhere else in the solid. In this sense fracture is an unstable process. This property makes the process extremely sensitive to any heterogeneity present in the medium, which selects the location of the first crack nucleated. In particular, fracture appears to be very sensitive to disorder, which can favor or impede local cracks. Therefore, in most realistic cases, a good description of fracture mechanics should include the effect of disorder. Recently this need has motivated work in this direction starting from the usual description of fracture mechanics. Parallel with this first trend, statistical physics underwent a very important develop...

  13. Advanced Hydraulic Fracturing Technology for Unconventional Tight Gas Reservoirs

    Energy Technology Data Exchange (ETDEWEB)

    Stephen Holditch; A. Daniel Hill; D. Zhu

    2007-06-19

    The objectives of this project are to develop and test new techniques for creating extensive, conductive hydraulic fractures in unconventional tight gas reservoirs by statistically assessing the productivity achieved in hundreds of field treatments with a variety of current fracturing practices ranging from 'water fracs' to conventional gel fracture treatments; by laboratory measurements of the conductivity created with high rate proppant fracturing using an entirely new conductivity test - the 'dynamic fracture conductivity test'; and by developing design models to implement the optimal fracture treatments determined from the field assessment and the laboratory measurements. One of the tasks of this project is to create an 'advisor' or expert system for completion, production and stimulation of tight gas reservoirs. A central part of this study is an extensive survey of the productivity of hundreds of tight gas wells that have been hydraulically fractured. We have been doing an extensive literature search of the SPE eLibrary, DOE, Gas Technology Institute (GTI), Bureau of Economic Geology and IHS Energy, for publicly available technical reports about procedures of drilling, completion and production of the tight gas wells. We have downloaded numerous papers and read and summarized the information to build a database that will contain field treatment data, organized by geographic location, and hydraulic fracture treatment design data, organized by the treatment type. We have conducted experimental study on 'dynamic fracture conductivity' created when proppant slurries are pumped into hydraulic fractures in tight gas sands. Unlike conventional fracture conductivity tests in which proppant is loaded into the fracture artificially; we pump proppant/frac fluid slurries into a fracture cell, dynamically placing the proppant just as it occurs in the field. From such tests, we expect to gain new insights into some of the critical

  14. Characterization of hydrogen embrittlement in automotive advanced high strength steels

    Energy Technology Data Exchange (ETDEWEB)

    Kolk, O.; Veith, S.; Goebel, T. [BMW Group, Muenchen (Germany); Loidl, M.

    2011-12-15

    Hydrogen embrittlement is the limiting factor when it comes to the utilization of advanced highest strength steels in a car body frame. Steels with a tensile strength of greater than 1000 MPa are deemed to be susceptible to hydrogen induced delayed fracture and therefore are not yet widely used. To characterize the deleterious effects of hydrogen embrittlement in advanced highest strength steels the slow strain rate testing in gaseous hydrogen atmosphere is a suitable method for investigating the effect of hydrogen on the materials ductility. Additionally the hydrogen content after slow strain rate testing was measured by means of thermal desorption spectroscopy. By using this technique it is possible to differentiate between diffusible and trapped hydrogen. Diffusible hydrogen may interact with dislocations and therefore changes the fracture behaviour of metals. This was also documented by analysing the fracture surface of the tensile specimen by optical and scanning electron microscopy. The investigations yield a comprehensive view on the susceptibility towards hydrogen induced cracking and allow a comparative view among different steel grades. (Copyright copyright 2011 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  15. Computational characterization of fracture healing under reduced gravity loading conditions.

    Science.gov (United States)

    Gadomski, Benjamin C; Lerner, Zachary F; Browning, Raymond C; Easley, Jeremiah T; Palmer, Ross H; Puttlitz, Christian M

    2016-07-01

    The literature is deficient with regard to how the localized mechanical environment of skeletal tissue is altered during reduced gravitational loading and how these alterations affect fracture healing. Thus, a finite element model of the ovine hindlimb was created to characterize the local mechanical environment responsible for the inhibited fracture healing observed under experimental simulated hypogravity conditions. Following convergence and verification studies, hydrostatic pressure and strain within a diaphyseal fracture of the metatarsus were evaluated for models under both 1 and 0.25 g loading environments and compared to results of a related in vivo study. Results of the study suggest that reductions in hydrostatic pressure and strain of the healing fracture for animals exposed to reduced gravitational loading conditions contributed to an inhibited healing process, with animals exposed to the simulated hypogravity environment subsequently initiating an intramembranous bone formation process rather than the typical endochondral ossification healing process experienced by animals healing in a 1 g gravitational environment. © 2015 Orthopaedic Research Society. Published by Wiley Periodicals, Inc. J Orthop Res 34:1206-1215, 2016. PMID:26704186

  16. Advanced Nanomeasuring Techniques for Surface Characterization

    OpenAIRE

    Salah H. R. Ali

    2012-01-01

    Advanced precise and accurate nanomeasurement techniques play an important role to improve the function and quality of surface characterization. There are two basic approaches, the hard measuring techniques and the soft computing measuring techniques. The advanced soft measuring techniques include coordinate measuring machines, roundness testing facilities, surface roughness, interferometric methods, confocal optical microscopy, scanning probe microscopy, and computed tomography at the level ...

  17. Fracture Characterization of Sandwich Face/Core Interfaces

    DEFF Research Database (Denmark)

    Manca, Marcello

    Sandwich structures are nowadays widely used in lightweight structural applications because oftheir superior stiffness/weight and strength/weight ratios compared with traditional metallic as well as monolithic structures made from composite materials. A major limiting factor of wider application...... of load transfer between the faces and the core layer is lost, the debonds are considered as primary damage initiators. Under fatigue loading the debonds may evolve into cracks that cause a reduction in structural performance and consequent failure. At present most structural design is based on “life-time...... such result it is important to devise new experimental and analytical techniques to establish the multi-mode fracture characteristics of sandwich plate structures and accordingly develop methods to inhibit defect propagation. This thesis deals with characterization of fracture between face and core...

  18. Thermo-hydro-mechanical processes in fractured rock formations during glacial advance

    Science.gov (United States)

    Selvadurai, A. P. S.; Suvorov, A. P.; Selvadurai, P. A.

    2014-11-01

    The paper examines the coupled thermo-hydro-mechanical (THM) processes that develop in a fractured rock region within a fluid-saturated rock mass due to loads imposed by an advancing glacier. This scenario needs to be examined in order to assess the suitability of potential sites for the location of deep geologic repositories for the storage of high-level nuclear waste. The THM processes are examined using a computational multiphysics approach that takes into account thermo-poroelasticity of the intact geological formation and the presence of a system of sessile but hydraulically interacting fractures (fracture zones). The modeling considers coupled thermo-hydro-mechanical effects in both the intact rock and the fracture zones due to contact normal stresses and fluid pressure at the base of the advancing glacier. Computational modelling provides an assessment of the role of fractures that can modify the pore pressure generation within the entire rock mass.

  19. Thermo-hydro-mechanical processes in fractured rock formations during a glacial advance

    Science.gov (United States)

    Selvadurai, A. P. S.; Suvorov, A. P.; Selvadurai, P. A.

    2015-07-01

    The paper examines the coupled thermo-hydro-mechanical (THM) processes that develop in a fractured rock region within a fluid-saturated rock mass due to loads imposed by an advancing glacier. This scenario needs to be examined in order to assess the suitability of potential sites for the location of deep geologic repositories for the storage of high-level nuclear waste. The THM processes are examined using a computational multiphysics approach that takes into account thermo-poroelasticity of the intact geological formation and the presence of a system of sessile but hydraulically interacting fractures (fracture zones). The modelling considers coupled thermo-hydro-mechanical effects in both the intact rock and the fracture zones due to contact normal stresses and fluid pressure at the base of the advancing glacier. Computational modelling provides an assessment of the role of fractures in modifying the pore pressure generation within the entire rock mass.

  20. Research advances in fracturing mechanism of amorphous materials

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    @@ The fracture behavior of brittle materials is a timehonored problem. Archeologists discover that prehistoric people created their primitive tools using this behavior. During the Stone Age, for example, they made simple wooden butchery implements by taking advantage of a sharp edge caused by the brittle fracture on flint. According to archeologists, the application of brittle fracture to the tool-making was one of monumental inventions to mark the very beginning of human civilization.Afterwards, ancient potters succeeded in decorating their works by having the surface of pottery inlaid with cracks and fissures.

  1. Analog site for fractured rock characterization. Annual report FY 1995

    Energy Technology Data Exchange (ETDEWEB)

    Long, J.C.S.; Loughty, C.; Faybishenko, B. [and others

    1995-10-01

    This report describes the accomplishments of the Analog Site for Fracture Rock Characterization Project during fiscal year 1995. This project is designed to address the problem of characterizing contaminated fractured rock. In order to locate contaminant plumes, develop monitoring schemes, and predict future fate and transport, the project will address the following questions: What parts of the system control flow-geometry of a fracture network? What physical processes control flow and transport? What are the limits on measurements to determine the above? What instrumentation should be used? How should it be designed and implemented? How can field tests be designed to provide information for predicting behavior? What numerical models are good predictors of the behavior of the system? The answers to these question can be used to help plan drilling programs that are likely to intersect plumes and provide effective monitoring of plume movement. The work is done at an {open_quotes}analogue{close_quotes} site, i.e., a site that is not contaminated, but has similar geology to sites that are contaminated, in order to develop tools and techniques without the financial, time and legal burdens of a contaminated site. The idea is to develop conceptual models and investigations tools and methodology that will apply to the contaminated sites in the same geologic regimes. The Box Canyon site, chosen for most of this work represents a unique opportunity because the Canyon walls allow us to see a vertical plane through the rock. The work represents a collaboration between the Lawrence Berkeley National Laboratory (LBL), Stanford University (Stanford), Idaho National Engineering Laboratory (INEL) and Parsons Environmental Engineering (Parsons). LBL and Stanford bring extensive experience in research in fractured rock systems. INEL and Parsons bring significant experience with the contamination problem at INEL.

  2. Analog site for fractured rock characterization. Annual report FY 1995

    International Nuclear Information System (INIS)

    This report describes the accomplishments of the Analog Site for Fracture Rock Characterization Project during fiscal year 1995. This project is designed to address the problem of characterizing contaminated fractured rock. In order to locate contaminant plumes, develop monitoring schemes, and predict future fate and transport, the project will address the following questions: What parts of the system control flow-geometry of a fracture network? What physical processes control flow and transport? What are the limits on measurements to determine the above? What instrumentation should be used? How should it be designed and implemented? How can field tests be designed to provide information for predicting behavior? What numerical models are good predictors of the behavior of the system? The answers to these question can be used to help plan drilling programs that are likely to intersect plumes and provide effective monitoring of plume movement. The work is done at an open-quotes analogueclose quotes site, i.e., a site that is not contaminated, but has similar geology to sites that are contaminated, in order to develop tools and techniques without the financial, time and legal burdens of a contaminated site. The idea is to develop conceptual models and investigations tools and methodology that will apply to the contaminated sites in the same geologic regimes. The Box Canyon site, chosen for most of this work represents a unique opportunity because the Canyon walls allow us to see a vertical plane through the rock. The work represents a collaboration between the Lawrence Berkeley National Laboratory (LBL), Stanford University (Stanford), Idaho National Engineering Laboratory (INEL) and Parsons Environmental Engineering (Parsons). LBL and Stanford bring extensive experience in research in fractured rock systems. INEL and Parsons bring significant experience with the contamination problem at INEL

  3. Characterization of fracture processes by continuum and discrete modelling

    Science.gov (United States)

    Kaliske, M.; Dal, H.; Fleischhauer, R.; Jenkel, C.; Netzker, C.

    2012-09-01

    A large number of methods to describe fracture mechanical features of structures on basis of computational algorithms have been developed in the past due to the importance of the topic. In this paper, current and promising numerical approaches for the characterization of fracture processes are presented. A fracture phenomenon can either be depicted by a continuum formulation or a discrete notch. Thus, starting point of the description is a micromechanically motivated formulation for the development of a local failure situation. A current, generalized method without any restriction to material modelling and loading situation in order to describe an existing crack in a structure is available through the material force approach. One possible strategy to simulate arbitrary crack growth is based on an adaptive implementation of cohesive elements in combination with the standard discretization of the body. In this case, crack growth criteria and the determination of the crack propagation direction in combination with the modification of the finite element mesh are required. The nonlinear structural behaviour of a fibre reinforced composite material is based on the heterogeneous microstructure. A two-scale simulation is therefore an appropriate and effective way to take into account the scale differences of macroscopic structures with microscopic elements. In addition, fracture mechanical structural properties are far from being sharp and deterministic. Moreover, a wide range of uncertainties influence the ultimate load bearing behaviour. Therefore, it is evident that the deterministic modelling has to be expanded by a characterization of the uncertainty in order to achieve a reliable and realistic simulation result. The employed methods are illustrated by numerical examples.

  4. Characterization of preferential flow paths between boreholes in fractured rock using a nanoscale zero-valent iron tracer test

    Science.gov (United States)

    Chuang, Po-Yu; Chia, Yeeping; Liou, Ya-Hsuan; Teng, Mao-Hua; Liu, Ching-Yi; Lee, Tsai-Ping

    2016-05-01

    Recent advances in borehole geophysical techniques have improved characterization of cross-hole fracture flow. The direct detection of preferential flow paths in fractured rock, however, remains to be resolved. In this study, a novel approach using nanoscale zero-valent iron (nZVI or `nano-iron') as a tracer was developed for detecting fracture flow paths directly. Generally, only a few rock fractures are permeable while most are much less permeable. A heat-pulse flowmeter can be used to detect changes in flow velocity for delineating permeable fracture zones in the borehole and providing the design basis for the tracer test. When nano-iron particles are released in an injection well, they can migrate through the connecting permeable fracture and be attracted to a magnet array when arriving in an observation well. Such an attraction of incoming iron nanoparticles by the magnet can provide quantitative information for locating the position of the tracer inlet. A series of field experiments were conducted in two wells in fractured rock at a hydrogeological research station in Taiwan, to test the cross-hole migration of the nano-iron tracer through permeable connected fractures. The fluid conductivity recorded in the observation well confirmed the arrival of the injected nano-iron slurry. All of the iron nanoparticles attracted to the magnet array in the observation well were found at the depth of a permeable fracture zone delineated by the flowmeter. This study has demonstrated that integrating the nano-iron tracer test with flowmeter measurement has the potential to characterize preferential flow paths in fractured rock.

  5. A Modified TSD Specimen for Fracture Toughness CharacterizationFracture Mechanics Analysis and Design

    DEFF Research Database (Denmark)

    Berggreen, Christian; Carlsson, Leif A.

    2010-01-01

    The tilted sandwich debond (TSD) specimen has been recognized as a viable candidate for characterization of the face/core fracture resistance. Analysis, however, shows that the range of phase angles that can be realized by altering the tilt angle and other parameters of the test is quite limited....... A method to extend the range of mode-mixities of the TSD specimen is to introduce a larger amount of transverse shear by reinforcing the loaded upper face with a stiff metal plate. Analysis shows that this method extends the range of phase angles to a practically useful range. Guidelines on selection...

  6. Characterizing Fractured Rock with Geo-structural and Micro-structural Models

    Science.gov (United States)

    Dershowitz, William

    2015-04-01

    Fracture spatial structure and hydro-mechanical properties are key to the understanding of fractured rock geomechanical stability, hydrodynamics, and solute transport. This paper presents a quantitative approach to fracture characterization to provide information useful for stability and flow analysis, and for coupled flow/geomechanics. The approach presented is based on the concept of geo-structural, hydro-mechanical, and microstructural models. This approach is applicable for data collected from exposed surfaces (mapping, LiDAR, aero-magnetics), boreholes (core, optical images, and images based on resistivity and geophysical methods), and three dimensional imaging (seismic attributes and microseismics). Examples are presented comparing the results of conventional fracture characterization procedures and the recommended procedure. Fracture characterization for geo-structural fracture models is based on the idea that the geologically based fracture spatial pattern is the key, rather than individual fracture statistics. For example, while fracture intensity statistics can useful, the three dimensional fracture pattern for a bedded sedimentary rock can be better reproduced from the combination of a mechanical bedding model and a correlation between fracture spacing and bed height. In a fracture geo-structural model, the fracture spatial pattern, orientation, and intensity should be characterized in a combination of global and local coordinate systems. While some fracture sets may be oriented relative to the regional tectonics (the global coordinate system), other fracture sets are oriented relative to bedding (a local coordinate system). Fracture hydro-mechanical models define the combination of (a) conductive fractures, (b) flow-barrier fractures, (c) fractures which provide storage porosity, (d) fractures of significance for kinematic stability, and (e) fractures of significance for rock mass strength and deformability. The hydromechanical fractures are a subset of

  7. Advanced Fine Particulate Characterization Methods

    Energy Technology Data Exchange (ETDEWEB)

    Steven Benson; Lingbu Kong; Alexander Azenkeng; Jason Laumb; Robert Jensen; Edwin Olson; Jill MacKenzie; A.M. Rokanuzzaman

    2007-01-31

    The characterization and control of emissions from combustion sources are of significant importance in improving local and regional air quality. Such emissions include fine particulate matter, organic carbon compounds, and NO{sub x} and SO{sub 2} gases, along with mercury and other toxic metals. This project involved four activities including Further Development of Analytical Techniques for PM{sub 10} and PM{sub 2.5} Characterization and Source Apportionment and Management, Organic Carbonaceous Particulate and Metal Speciation for Source Apportionment Studies, Quantum Modeling, and High-Potassium Carbon Production with Biomass-Coal Blending. The key accomplishments included the development of improved automated methods to characterize the inorganic and organic components particulate matter. The methods involved the use of scanning electron microscopy and x-ray microanalysis for the inorganic fraction and a combination of extractive methods combined with near-edge x-ray absorption fine structure to characterize the organic fraction. These methods have direction application for source apportionment studies of PM because they provide detailed inorganic analysis along with total organic and elemental carbon (OC/EC) quantification. Quantum modeling using density functional theory (DFT) calculations was used to further elucidate a recently developed mechanistic model for mercury speciation in coal combustion systems and interactions on activated carbon. Reaction energies, enthalpies, free energies and binding energies of Hg species to the prototype molecules were derived from the data obtained in these calculations. Bimolecular rate constants for the various elementary steps in the mechanism have been estimated using the hard-sphere collision theory approximation, and the results seem to indicate that extremely fast kinetics could be involved in these surface reactions. Activated carbon was produced from a blend of lignite coal from the Center Mine in North Dakota and

  8. A new device for characterizing fracture networks and measuring groundwater and contaminant fluxes in fractured rock aquifers

    Science.gov (United States)

    Klammler, Harald; Hatfield, Kirk; Newman, Mark A.; Cho, Jaehyun; Annable, Michael D.; Parker, Beth L.; Cherry, John A.; Perminova, Irina

    2016-07-01

    This paper presents the fundamental theory and laboratory test results on a new device that is deployed in boreholes in fractured rock aquifers to characterize vertical distributions of water and contaminant fluxes, aquifer hydraulic properties, and fracture network properties (e.g., active fracture density and orientation). The device, a fractured rock passive flux meter (FRPFM), consists of an inflatable core assembled with upper and lower packers that isolate the zone of interest from vertical gradients within the borehole. The outer layer of the core consists of an elastic fabric mesh equilibrated with a visible dye which is used to provide visual indications of active fractures and measures of fracture location, orientation, groundwater flux, and the direction of that flux. Beneath the outer layer is a permeable sorbent that is preloaded with known amounts of water soluble tracers which are eluted at rates proportional to groundwater flow. This sorbent also captures target contaminants present in intercepted groundwater. The mass of contaminant sorbed is used to quantify cumulative contaminant flux; whereas, the mass fractions of resident tracers lost are used to provide measures of water flux. In this paper, the FRPFM is bench tested over a range of fracture velocities (2-20 m/day) using a single fracture flow apparatus (fracture aperture = 0.5 mm). Test results show a discoloration in visible dye corresponding to the location of the active fracture. The geometry of the discoloration can be used to discern fracture orientation as well as direction and magnitude of flow in the fracture. Average contaminant fluxes were measured within 16% and water fluxes within 25% of known imposed fluxes.

  9. Nondestructive characterization of advanced composite materials

    International Nuclear Information System (INIS)

    A comprehensive review of nondestructive characterization (NDC) techniques and their application to metal-matrix, polymer-matrix and ceramic-matrix composites is presented. Particular attention is given to the identification of critical materials properties and defects in these advanced composites. NDC is required: (i) to detect discrete defects, such as delaminations and cracking, and (ii) to measure distributed material properties, such as density, resistivity and elastic constants. Ultrasonic and eddy-current characterization are described in detail, along with new NDC results obtained at the Aeronautical and Maritime Research Laboratory. These include a method for the determination of fibre volume fraction in continuous fibre reinforced metal-matrix composites using eddy-current NDC, and the use of eddy-current methods to complement ultrasonic testing for characterization of impact damage in graphite-epoxy laminates. Future problem areas and possible solutions in NDC of advanced composites are also discussed. 90 refs., 1 tab., 6 figs

  10. Mixed mode fracture toughness characterization of sandwich interfaces using the modified TSD specimen

    DEFF Research Database (Denmark)

    Berggreen, Christian; Andreasen, J.H.; Carlsson, L.A.;

    2009-01-01

    An extensive parametric analysis shows that the modified Tilted Sandwich Debond (TSD) specimen provides a methodology for characterization of the face/core fracture resistance over a range of mode-mixities. A pilot experimental mixed mode characterization of the fracture toughness of sandwich spe...

  11. Characterization and flow simulations of discrete fracture networks

    OpenAIRE

    Zeeb, Conny

    2013-01-01

    Fractures, such as joints, faults and veins, strongly influence the transport of fluids through rocks by either enhancing or inhibiting flow. Especially in rocks with negligible permeability fractures can act as major for fluid conduits. Therefore, the contribution of fracture networks to the overall flow behavior is of high interest to, for example, the hydrocarbon industry, the power generation using deep geothermal systems, the sustainable management of fractured rock aquifers, the plannin...

  12. Characterization of fracture zone 2, Finnsjoen study-site

    International Nuclear Information System (INIS)

    Part 1. Overview of the fracture zone project at Finnsjoen, Sweden. Part 2 Geological setting and deformation history of a low angle fracture zone at Finnsjoen, Sweden. Part 3 Hydraulic testing and modelling of a lowangle fracture zone at Finnsjoen, Sweden. Part 4 Groundwater flow conditions in a low angle fracture zone at Finnsjoen, Sweden. Part 5 Hydrochemical investigations at Finnsjoen, Sweden. Effects of gas-lift pumping on hydraulic borehole conditions at Finnsjoen, Sweden

  13. Advanced hydraulic fracturing methods to create in situ reactive barriers

    Energy Technology Data Exchange (ETDEWEB)

    Murdoch, L. [FRx Inc., Cincinnati, OH (United States)]|[Clemson Univ., SC (United States); Siegrist, B. [Oak Ridge National Lab., TN (United States); Vesper, S. [Univ. of Cincinnati, OH (United States)] [and others

    1997-12-31

    Many contaminated areas consist of a source area and a plume. In the source area, the contaminant moves vertically downward from a release point through the vadose zone to an underlying saturated region. Where contaminants are organic liquids, NAPL may accumulate on the water table, or it may continue to migrate downward through the saturated region. Early developments of permeable barrier technology have focused on intercepting horizontally moving plumes with vertical structures, such as trenches, filled with reactive material capable of immobilizing or degrading dissolved contaminants. This focus resulted in part from a need to economically treat the potentially large volumes of contaminated water in a plume, and in part from the availability of construction technology to create the vertical structures that could house reactive compounds. Contaminant source areas, however, have thus far remained largely excluded from the application of permeable barrier technology. One reason for this is the lack of conventional construction methods for creating suitable horizontal structures that would place reactive materials in the path of downward-moving contaminants. Methods of hydraulic fracturing have been widely used to create flat-lying to gently dipping layers of granular material in unconsolidated sediments. Most applications thus far have involved filling fractures with coarse-grained sand to create permeable layers that will increase the discharge of wells recovering contaminated water or vapor. However, it is possible to fill fractures with other compounds that alter the chemical composition of the subsurface. One early application involved development and field testing micro-encapsulated sodium percarbonate, a solid compound that releases oxygen and can create aerobic conditions suitable for biodegradation in the subsurface for several months.

  14. San Juan Fracture Characterization Project: Status and current results

    Energy Technology Data Exchange (ETDEWEB)

    Majer, E.L.; Daley, T.M.; Myer, L.R.; Nihei, K.; Queen, J.; Sinton, J.; Murphy, J.; Fortuna, M.; Lynn, H.B.; Imhoff, M.A.; Wilson, R.

    2001-02-26

    The overall objectives of this report are to extend current state-of-the-art 3-D imaging to extract the optimal information for fracture quantification and to develop next generation capability in fracture imaging for true 3-D imaging of the static and dynamic fracture properties.

  15. Advanced MOSFET variability and reliability characterization array

    OpenAIRE

    Simicic, Marko; Putcha, Vamsi; Parvais, Bertrand; Weckx, Pieter; Kaczer, Ben; Groeseneken, Guido; Gielen, Georges; Linten, Dimitri; Thean, Aaron

    2015-01-01

    Time-zero variability, bias temperature instability (BTI) and random telegraph noise (RTN) are issues that both analog and digital designers using scaled CMOS technologies have to face. In order to address them at design time, access to a sufficiently large number of individual devices is required for statistical technology characterization and modeling. In this paper we present a large MOSFET array designed and fabricated in an advanced 28nm technology, containing both nMOS and pMOS devices ...

  16. Mode II Interlaminar Fracture Toughness and Fatigue Characterization of a Graphite Epoxy Composite Material

    Science.gov (United States)

    O'Brien, T. Kevin; Johnston, William M.; Toland, Gregory J.

    2010-01-01

    Mode II interlaminar fracture toughness and delamination onset and growth characterization data were generated for IM7/8552 graphite epoxy composite materials from two suppliers for use in fracture mechanics analyses. Both the fracture toughness testing and the fatigue testing were conducted using the End-notched Flexure (ENF) test. The ENF test for mode II fracture toughness is currently under review by ASTM as a potential standard test method. This current draft ASTM protocol was used as a guide to conduct the tests on the IM7/8552 material. This report summarizes the test approach, methods, procedures and results of this characterization effort.

  17. Modeling and characterization of interfacial adhesion and fracture

    Science.gov (United States)

    Yao, Qizhou

    2000-09-01

    The loss of interfacial adhesion is mostly seen in the failure of polymer adhesive joints. In addition to the intrinsic physical attraction across the interface, the interfacial adhesion strength is believed to highly depend on a number of factors, such as adhesive chemistry/structure, surface topology, fracture pattern, thermal and elastic mismatch across the interface. The fracture failure of an adhesive joint involves basically three aspects, namely, the intrinsic interfacial strength, the driving force for fracture and other energy dissipation. One may define the intrinsic interfacial strength as the maximum value of the intrinsic interfacial adhesion. The total work done by external forces to the component that contains the interface is partitioned into two parts. The first part is consumed by all other energy dissipation mechanisms (plasticity, heat generation, viscosity, etc.). The second part is used to debond the interface. This amount should equal to the intrinsic adhesion of the interface according to the laws of conservation of energy. It is clear that in order to understand the fundamental physics of adhesive joint failure, one must be able to characterize the intrinsic interfacial adhesion and be able to identify all the major energy dissipation mechanisms involved in the debonding process. In this study, both physical and chemical adhesion mechanisms were investigated for an aluminum-epoxy interface. The physical bonding energy was estimated by computing the Van de Waals forces across the interface. A hydration model was proposed and the associated chemical bonding energy was calculated through molecular simulations. Other energy dissipation mechanisms such as plasticity and thermal residual stresses were also identified and investigated for several four-point bend specimens. In particular, a micromechanics based model was developed to estimate the adhesion enhancement due to surface roughness. It is found that for this Al-epoxy system the major

  18. Hydraulic anisotropy characterization of pneumatic-fractured sediments using azimuthal self potential gradient

    Science.gov (United States)

    Wishart, DeBonne N.; Slater, Lee D.; Schnell, Deborah L.; Herman, Gregory C.

    2009-01-01

    The pneumatic fracturing technique is used to enhance the permeability and porosity of tight unconsolidated soils (e.g. clays), thereby improving the effectiveness of remediation treatments. Azimuthal self potential gradient (ASPG) surveys were performed on a compacted, unconsolidated clay block in order to evaluate their potential to delineate contaminant migration pathways in a mechanically-induced fracture network. Azimuthal resistivity (ARS) measurements were also made for comparative purposes. Following similar procedures to those used in the field, compressed kaolinite sediments were pneumatically fractured and the resulting fracture geometry characterized from strike analysis of visible fractures combined with strike data from optical borehole televiewer (BHTV) imaging. We subsequently injected a simulated treatment (electrolyte/dye) into the fractures. Both ASPG and ARS data exhibit anisotropic geoelectric signatures resulting from the fracturing. Self potentials observed during injection of electrolyte are consistent with electrokinetic theory and previous laboratory results on a fracture block model. Visual (polar plot) analysis and linear regression of cross plots show ASPG lobes are correlated with azimuths of high fracture strike density, evidence that the ASPG anisotropy is a proxy measure of hydraulic anisotropy created by the pneumatic fracturing. However, ARS data are uncorrelated with fracture strike maxima and resistivity anisotropy is probably dominated by enhanced surface conduction along azimuths of weak 'starter paths' formed from pulverization of the clay and increases in interfacial surface area. We find the magnitude of electrokinetic SP scales with the applied N 2 gas pressure gradient (Δ PN2) for any particular hydraulically-active fracture set and that the positive lobe of the ASPG anomaly indicates the flow direction within the fracture network. These findings demonstrate the use of ASPG in characterizing the effectiveness of (1

  19. MULTI-ATTRIBUTE SEISMIC/ROCK PHYSICS APPROACH TO CHARACTERIZING FRACTURED RESERVOIRS

    Energy Technology Data Exchange (ETDEWEB)

    Gary Mavko

    2000-10-01

    This project consists of three key interrelated Phases, each focusing on the central issue of imaging and quantifying fractured reservoirs, through improved integration of the principles of rock physics, geology, and seismic wave propagation. This report summarizes the results of Phase I of the project. The key to successful development of low permeability reservoirs lies in reliably characterizing fractures. Fractures play a crucial role in controlling almost all of the fluid transport in tight reservoirs. Current seismic methods to characterize fractures depend on various anisotropic wave propagation signatures that can arise from aligned fractures. We are pursuing an integrated study that relates to high-resolution seismic images of natural fractures to the rock parameters that control the storage and mobility of fluids. Our goal is to go beyond the current state-of-the art to develop and demonstrate next generation methodologies for detecting and quantitatively characterizing fracture zones using seismic measurements. Our study incorporates 3 key elements: (1) Theoretical rock physics studies of the anisotropic viscoelastic signatures of fractured rocks, including up scaling analysis and rock-fluid interactions to define the factors relating fractures in the lab and in the field. (2) Modeling of optimal seismic attributes, including offset and azimuth dependence of travel time, amplitude, impedance and spectral signatures of anisotropic fractured rocks. We will quantify the information content of combinations of seismic attributes, and the impact of multi-attribute analyses in reducing uncertainty in fracture interpretations. (3) Integration and interpretation of seismic, well log, and laboratory data, incorporating field geologic fracture characterization and the theoretical results of items 1 and 2 above. The focal point for this project is the demonstration of these methodologies in the Marathon Oil Company Yates Field in West Texas.

  20. Development of Reservoir Characterization Techniques and Production Models for Exploiting Naturally Fractured Reservoirs

    Energy Technology Data Exchange (ETDEWEB)

    Wiggins, Michael L; Brown, Raymon L.; Civan, Faruk; Hughes, Richard G.

    2002-10-08

    During this reporting period, research was continued on characterizing and modeling the behavior of naturally fractured reservoir systems. This report proposed a model to relate the seismic response to production data to determine crack spacing and aperture, provided details of tests of proposed models to obtain fracture properties from conventional well logs with actual field data, and verification of the naturally fractured reservoir simulator developed in this project.

  1. Characterization of Fractured Reservoirs Using a Combination of Downhole Pressure and Self-Potential Transient Data

    OpenAIRE

    Yuji Nishi; Tsuneo Ishido

    2012-01-01

    In order to appraise the utility of self-potential (SP) measurements to characterize fractured reservoirs, we carried out continuous SP monitoring using multi Ag-AgCl electrodes installed within two open holes at the Kamaishi Mine, Japan. The observed ratio of SP change to pressure change associated with fluid flow showed different behaviors between intact host rock and fractured rock regions. Characteristic behavior peculiar to fractured reservoirs, which is predicted from numerical simulati...

  2. Characterizing and Modelling Preferential Flow Path in Fractured Rock Aquifer: A Case Study at Shuangliou Fractured Rock Hydrogeology Research Site

    Science.gov (United States)

    Hsu, Shih-Meng; Ke, Chien-Chung; Lo, Hung-Chieh; Lin, Yen-Tsu; Huang, Chi-Chao

    2016-04-01

    On the basis of a relatively sparse data set, fractured aquifers are difficult to be characterized and modelled. The three-dimensional configuration of transmissive fractures and fracture zones is needed to be understood flow heterogeneity in the aquifer. Innovative technologies for the improved interpretation are necessary to facilitate the development of accurate predictive models of ground-water flow and solute transport or to precisely estimate groundwater potential. To this end, this paper presents a procedure for characterizing and modelling preferential flow path in the fractured rock aquifer carried out at Fractured Rock Hydrogeology Research Site in Shuangliou Forest Recreation Area, Pingtung County, Southern Taiwan. The Shuangliou well field is a 40 by 30-meter area consisting of 6 wells (one geological well, one pumping well and four hydrogeological testing wells). The bedrock at the site is mainly composed of slate and intercalated by meta-sandstone. The overburden consists of about 5.6 m of gravel deposits. Based on results of 100 m geological borehole with borehole televiewer logging, vertical flow logging and full-wave sonic logging, high transmissivity zones in the bedrock underlying the well field were identified. One of transmissivity zone (at the depths of 30~32 m) and its fracture orientation(N56/54) selected for devising a multiple well system with 4 boreholes (borehole depths :45m, 35m, 35m and 25m, respectively), which were utilized to perform cross-borehole flow velocity data under the ambient flow and pumped flow conditions to identify preferential flow paths. Results from the cross-borehole test show the preferential flow pathways are corresponding to the predicted ones. Subsequently, a 3-D discrete fracture network model based on outcrop data was generated by the FracMan code. A validation between observed and simulated data has proved that the present model can accurately predict the hydrogeological properties (e.g., number of fractures

  3. Geophysical characterization of fractured bedrock at Site 8, former Pease Air Force Base, Newington, New Hampshire

    Science.gov (United States)

    Mack, Thomas J.; Degnan, James R.

    2003-01-01

    Borehole-geophysical logs collected from eight wells and direct-current resistivity data from three survey lines were analyzed to characterize the fractured bedrock and identify transmissive fractures beneath the former Pease Air Force Base, Newington, N.H. The following logs were used: caliper, fluid temperature and conductivity, natural gamma radiation, electromagnetic conductivity, optical and acoustic televiewer, and heat-pulse flowmeter. The logs indicate several foliation and fracture trends in the bedrock. Two fracture-correlated lineaments trending 28? and 29?, identified with low-altitude aerial photography, are coincident with the dominant structural trend. The eight boreholes logged at Site 8 generally have few fractures and have yields ranging from 0 to 40 gallons per minute. The fractures that probably resulted in high well yields (20?40 gallons per minute) strike northeast-southwest or by the right hand rule, have an orientation of 215?, 47?, and 51?. Two-dimensional direct-current resistivity methods were used to collect detailed subsurface information about the overburden, bedrock-fracture zone depths, and apparent-dip directions. Analysis of data inversions from data collected with dipole-dipole and Schlumberger arrays indicated electrically conductive zones in the bedrock that are probably caused by fractured rock. These zones are coincident with extensions of fracture-correlated lineaments. The fracture-correlated lineaments and geophysical-survey results indicate a possible northeast-southwest anisotropy to the fractured rock.

  4. DEVELOPMENT OF RESERVOIR CHARACTERIZATION TECHNIQUES AND PRODUCTION MODELS FOR EXPLOITING NATURALLY FRACTURED RESERVOIRS

    Energy Technology Data Exchange (ETDEWEB)

    Michael L. Wiggins; Raymon L. Brown; Faruk Civan; Richard G. Hughes

    2002-12-31

    For many years, geoscientists and engineers have undertaken research to characterize naturally fractured reservoirs. Geoscientists have focused on understanding the process of fracturing and the subsequent measurement and description of fracture characteristics. Engineers have concentrated on the fluid flow behavior in the fracture-porous media system and the development of models to predict the hydrocarbon production from these complex systems. This research attempts to integrate these two complementary views to develop a quantitative reservoir characterization methodology and flow performance model for naturally fractured reservoirs. The research has focused on estimating naturally fractured reservoir properties from seismic data, predicting fracture characteristics from well logs, and developing a naturally fractured reservoir simulator. It is important to develop techniques that can be applied to estimate the important parameters in predicting the performance of naturally fractured reservoirs. This project proposes a method to relate seismic properties to the elastic compliance and permeability of the reservoir based upon a sugar cube model. In addition, methods are presented to use conventional well logs to estimate localized fracture information for reservoir characterization purposes. The ability to estimate fracture information from conventional well logs is very important in older wells where data are often limited. Finally, a desktop naturally fractured reservoir simulator has been developed for the purpose of predicting the performance of these complex reservoirs. The simulator incorporates vertical and horizontal wellbore models, methods to handle matrix to fracture fluid transfer, and fracture permeability tensors. This research project has developed methods to characterize and study the performance of naturally fractured reservoirs that integrate geoscience and engineering data. This is an important step in developing exploitation strategies for

  5. Fracture toughness of advanced alumina ceramics and alumina matrix composites used for cutting tool edges

    Directory of Open Access Journals (Sweden)

    M. Szutkowska

    2012-10-01

    Full Text Available Purpose: Specific characteristics in fracture toughness measurements of advanced alumina ceramics and alumina matrix composites with particular reference to α-Al2O3, Al2O3-ZrO2, Al2O3-ZrO2-TiC and Al2O3-Ti(C,N has been presented.Design/methodology/approach: The present study reports fracture toughness obtained by means of the conventional method and direct measurements of the Vickers crack length (DCM method of selected tool ceramics based on alumina: pure alumina, alumina-zirconia composite with unstabilized and stabilized zirconia, alumina–zirconia composite with addition of TiC and alumina–nitride-carbide titanium composite with 2wt% of zirconia. Specimens were prepared from submicro-scale trade powders. Vicker’s hardness (HV1, fracture toughness (KIC at room temperature, the indentation fracture toughness, Young’s modulus and apparent density were also evaluated. The microstructure was observed by means of scanning electron microscopy (SEM.Findings: The lowest value of KIC is revealed by pure alumina ceramics. The addition of (10 wt% unstabilized zirconia to alumina or a small amount (5 wt% of TiC to alumina–zirconia composite improve fracture toughness of these ceramics in comparison to alumina ceramics. Alumina ceramics and alumina-zirconia ceramics reveal the pronounced character of R-curve because of an increasing dependence on crack growth resistance with crack extension as opposed to the titanium carbide-nitride reinforced composite based on alumina. R-curve has not been observed for this composite.Practical implications: The results show the method of fracture toughness improvement of alumina tool ceramics.Originality/value: Taking into account the values of fracture toughness a rational use of existing ceramic tools should be expected.

  6. Tensile Fracture Location Characterizations of Friction Stir Welded Joints of Different Aluminum Alloys

    Institute of Scientific and Technical Information of China (English)

    Huijie LIU; Hidetoshi FUJII; Masakatsu MAEDA; Kiyoshi NOGI

    2004-01-01

    The tensile fracture location characterizations of the friction stir welded joints of the AA1050-H24 and AA6061-T6Al alloys were evaluated in this study. The experimental results show that the fracture locations of the joints are different for the different Al alloys, and they are affected by the FSW parameters. When the joints are free of welding defects, the AA1050-H24 joints are fractured in the HAZ and TMAZ on the AS and the fracture parts undergo a large amount of plastic deformation, while the AA6061-T6 joints are fractured in the HAZ on the RS and the fracture surfaces are inclined a certain degree to the bottom surfaces of the joints. When some welding defects exist in the joints, the AA1050-H24 joints are fractured on the RS or AS, the AA6061-T6 joints are fractured on the RS, and all the fracture locations are near to the weld center. The fracture locations of the joints are dependent on the internal structures of the joints and can be explained by the microhardness profiles and defect morphologies of the joints.

  7. Final Report - Advanced Conceptual Models for Unsaturated and Two-Phase Flow in Fractured Rock

    Energy Technology Data Exchange (ETDEWEB)

    Nicholl, Michael J.

    2006-07-10

    The Department of Energy Environmental Management Program is faced with two major issues involving two-phase flow in fractured rock; specifically, transport of dissolved contaminants in the Vadose Zone, and the fate of Dense Nonaqueous Phase Liquids (DNAPLs) below the water table. Conceptual models currently used to address these problems do not correctly include the influence of the fractures, thus leading to erroneous predictions. Recent work has shown that it is crucial to understand the topology, or ''structure'' of the fluid phases (air/water or water/DNAPL) within the subsurface. It has also been shown that even under steady boundary conditions, the influence of fractures can lead to complex and dynamic phase structure that controls system behavior, with or without the presence of a porous rock matrix. Complicated phase structures within the fracture network can facilitate rapid transport, and lead to a sparsely populated and widespread distribution of concentrated contaminants; these qualities are highly difficult to describe with current conceptual models. The focus of our work is to improve predictive modeling through the development of advanced conceptual models for two-phase flow in fractured rock.

  8. Investigations on fracture curves in strain and stress space for advanced high strength steel forming

    Science.gov (United States)

    Panich, S.; Drotleff, K.; Liewald, M.; Uthaisangsuk, V.

    2016-08-01

    Conventional forming limit curves (FLCs) are inappropriate for describing formability for advanced high strength (AHS) steel sheets, since such steel grades experience fracture without localized necking occurrence. The aim of this work was to develop a fracture curve (FC) for the AHS steel grade DP980. The FC was determined by means of the Nakajima stretch forming test and tensile tests of various sample geometries, by which shear fracture governed. An optical strain measurement system was used to capture strain histories of deformed samples up to failure. From these results, fracture strains were gathered and plotted in a strain space. Subsequently, the strain based curve was transformed to space between stress triaxiality and plastic strain. Hereby, effects of anisotropic yield function, namely, the Hill’48 model on obtained stress fracture loci were investigated. In order to verify applicability of the determined limit curves, a Mini-tunnel part was pressed and simulated. It was found that the stress based FC do predict failure of the DP980 steel sheet more accurately than the strain based F C.

  9. Fracture behavior of advanced ceramic hot gas filters: Final report

    Energy Technology Data Exchange (ETDEWEB)

    Singh, J.P.; Majumdar, S.; Sutaria, M.; Bielke, W. [Argonne National Lab., IL (United States). Energy Technology Div.

    1997-03-01

    This report presents the results of mechanical/microstructural evaluation, thermal shock/fatigue testing, and stress analyses of advanced hot-gas filters obtained from different manufacturers. These filters were fabricated from both monolithic ceramics and composites. The composite filters, made of both oxide and nonoxide materials, were in both as-fabricated and exposed conditions, whereas the monolithic filters were made only of nonoxide materials. Mechanical property measurement of composite filters included diametral compression testing with O-ring specimens and burst-testing of short filter segments with rubber plugs. In-situ strength of fibers in the composite filters was evaluated by microscopic technique. Thermal shock/fatigue resistance was estimated by measuring the strengths of filter specimens before and after thermal cycling from an air environment at elevated temperatures to a room temperature oil bath. Filter performance during mechanical and thermal shock/fatigue loadings was correlated with microstructural observations. Micromechanical models were developed to derive properties of composite filter constituents on the basis of measured mechanical properties of the filters. Subsequently, these properties were used to analytically predict the performance of composite filters during thermal shock loading.

  10. Thermo-hydro-mechanical processes in fractured rock formations during a glacial advance

    OpenAIRE

    Selvadurai, A. P. S.; Suvorov, A. P.; Selvadurai, P. A.

    2015-01-01

    The paper examines the coupled thermo-hydro-mechanical (THM) processes that develop in a fractured rock region within a fluid-saturated rock mass due to loads imposed by an advancing glacier. This scenario needs to be examined in order to assess the suitability of potential sites for the location of deep geologic repositories for the storage of high-level nuclear waste. The THM processes are examined using a computational multiphysics approach that takes into account thermo-...

  11. Use of markers of paleo-circulations to characterize the porous network of fractured granite.

    Science.gov (United States)

    Bertrand, L.; LeGarzic, E.; Géraud, Y.; Diraison, M.

    2012-04-01

    Fractured reservoirs in crystalline rocks are well studied nowadays for their application in water resources, oil exploitation or geothermics. In this king of rock, the matrice has a very low permeability and the fluid flow is localized in the fracture pattern. Thus, the characterization and the modeling of such reservoirs require the good knowledge of the fractures, in particular the orientation, density or spatial distribution. In actual fractured reservoirs, the access on those parameters are with seismic and borehole data. The two prospection techniques are at different scale and dimensions, and correlations between them are difficult to make. In consequence, it is necessary to study field rocks analogues on the underground fractured reservoirs. Tamariu's granite, Catalunya, is one of those fields' analogues. Previous studies have highlighted a structuration of the granite in structural blocs of different sizes, separated by faults, and internal fracture patterns in each bloc. Markers of intense paleofluids circulations have been seen in the faults and fractures of those blocs. This study follows the structural characterization of the fracture pattern and as the aim to study the fluid circulation in those fractures. With precise fracture maps, we have analyzed the principal flow direction and the nature of the hydrothermal deposits. Aside from primary hydrothermal quartz, the main secondary minerals are calcite and dolomite, and a little part of iron oxides. This observation, combined on the fracture maps, has allowed us to try a semi-quantification of the usable volume by the fluid in the granite at the circulations time. The fracture pattern has been the host of fluids of around 3% of their volume. Therefore, we have identified a diffuse flow in the grain matrice and which creates primary minerals alteration. The volume of alteration represent around 0,1-0,3% of the rock. In consequence, this study highlights a double-porosity behavior of the granite. On one

  12. Experimental Hydromechanical Characterization and Numerical Modelling of a Fractured and Porous Sandstone

    Science.gov (United States)

    Souley, Mountaka; Lopez, Philippe; Boulon, Marc; Thoraval, Alain

    2015-05-01

    The experimental device previously used to study the hydromechanical behaviour of individual fractures on a laboratory scale, was adapted to make it possible to measure flow through porous rock mass samples in addition to fracture flows. A first series of tests was performed to characterize the hydromechanical behaviour of the fracture individually as well as the porous matrix (sandstone) comprising the fracture walls. A third test in this series was used to validate the experimental approach. These tests showed non-linear evolution of the contact area on the fracture walls with respect to effective normal stress. Consequently, a non-linear relationship was noted between the hydraulic aperture on the one hand, and the effective normal stress and mechanical opening on the other hand. The results of the three tests were then analysed by numerical modelling. The VIPLEF/HYDREF numerical codes used take into account the dual-porosity of the sample (fracture + rock matrix) and can be used to reproduce hydromechanical loading accurately. The analyses show that the relationship between the hydraulic aperture of the fracture and the mechanical closure has a significant effect on fracture flow rate predictions. By taking simultaneous measurements of flow in both fracture and rock matrix, we were able to carry out a global evaluation of the conceptual approach used.

  13. Advancement in polymer therapeutics and characterization

    Directory of Open Access Journals (Sweden)

    Shah Pratik

    2009-01-01

    Full Text Available The beauty of the discipline, polymers in drug delivery, is its longevity and self-transforming quality. Polymers have, for decades, performed a valuable function as excipients in tablet and capsule formulations, moving steadily into the parenteral arena as blood circulation time enhancers, and are now capable of offering advanced and sophisticated functions (such as drug targeting to medicine. Polymers have unique cooperative properties that are not found with low-molecular weight compounds and therein lies the root of their success. Polymers are used as carriers for the delivery of drugs, proteins, targeting moieties, and imaging agents. Several polymers, polyethylene glycol, N-(2-hydroxypropyl methacrylamide, and polylactide-co-glycolidecopolymers have been successfully utilized in clinical research. Recently, interest in polymer conjugation with biologically active components has increased remarkably as such conjugates are preferably accumulated in solid tumors and can reduce systemic toxicity. Further, it is essential to elucidate the structure-activity relationshipof a drug when it is conjugated with a polymer using different conjugation sites as this can vary the efficacy and mechanism of action when compared with its free form. This review will discuss the current advancement in drug targeting with polymers, smart polymers and recombinant polymers for drug delivery. Finally, it will also highlight on various methods of polymer characterization, including various techniques for polymer molecular weight measurement.

  14. Multi-Attribute Seismic/Rock Physics Approach to Characterizing Fractured Reservoirs

    Energy Technology Data Exchange (ETDEWEB)

    Gary Mavko

    2004-11-30

    Most current seismic methods to seismically characterize fractures in tight reservoirs depend on a few anisotropic wave propagation signatures that can arise from aligned fractures. While seismic anisotropy can be a powerful fracture diagnostic, a number of situations can lessen its usefulness or introduce interpretation ambiguities. Fortunately, laboratory and theoretical work in rock physics indicates that a much broader spectrum of fracture seismic signatures can occur, including a decrease in P- and S-wave velocities, a change in Poisson's ratio, an increase in velocity dispersion and wave attenuation, as well as well as indirect images of structural features that can control fracture occurrence. The goal of this project was to demonstrate a practical interpretation and integration strategy for detecting and characterizing natural fractures in rocks. The approach was to exploit as many sources of information as possible, and to use the principles of rock physics as the link among seismic, geologic, and log data. Since no single seismic attribute is a reliable fracture indicator in all situations, the focus was to develop a quantitative scheme for integrating the diverse sources of information. The integrated study incorporated three key elements: The first element was establishing prior constraints on fracture occurrence, based on laboratory data, previous field observations, and geologic patterns of fracturing. The geologic aspects include analysis of the stratigraphic, structural, and tectonic environments of the field sites. Field observations and geomechanical analysis indicates that fractures tend to occur in the more brittle facies, for example, in tight sands and carbonates. In contrast, strain in shale is more likely to be accommodated by ductile flow. Hence, prior knowledge of bed thickness and facies architecture, calibrated to outcrops, are powerful constraints on the interpreted fracture distribution. Another important constraint is that

  15. Preliminary fracture analysis of the core pressure boundary tube for the Advanced Neutron Source Research Reactor

    Energy Technology Data Exchange (ETDEWEB)

    Schulz, K.C. [Univ. of Turabo, Gurabo, Puerto (Puerto Rico). College of Engineering; Yahr, G.T. [Oak Ridge National Lab., TN (United States)

    1995-08-01

    The outer core pressure boundary tube (CPBT) of the Advanced neutron Source (ANS) reactor being designed at Oak Ridge National Laboratory is currently specified as being composed of 6061-T6 aluminum. ASME Boiler and Pressure Vessel Code fracture analysis rules for nuclear components are based on the use of ferritic steels; the expressions, tables, charts and equations were all developed from tests and analyses conducted for ferritic steels. Because of the nature of the Code, design with thin aluminum requires analytical approaches that do not directly follow the Code. The intent of this report is to present a methodology comparable to the ASME Code for ensuring the prevention of nonductile fracture of the CPBT in the ANS reactor. 6061-T6 aluminum is known to be a relatively brittle material; the linear elastic fracture mechanics (LEFM) approach is utilized to determine allowable flaw sizes for the CPBT. A J-analysis following the procedure developed by the Electric Power Research Institute was conducted as a check; the results matched those for the LEFM analysis for the cases analyzed. Since 6061-T6 is known to embrittle when irradiated, the reduction in K{sub Q} due to irradiation is considered in the analysis. In anticipation of probable requirements regarding maximum allowable flaw size, a survey of nondestructive inspection capabilities is also presented. A discussion of probabilistic fracture mechanics approaches, principally Monte Carlo techniques, is included in this report as an introduction to what quantifying the probability of nonductile failure of the CPBT may entail.

  16. Characterization of Metacarpal Fractures in a Military Population.

    Science.gov (United States)

    Dichiera, Robert; Dunn, John; Bader, Julia; Bulken-Hoover, Jamie; Pallis, Mark

    2016-08-01

    The purpose of this study was to investigate the incidence and type of metacarpal (MC) fractures in a military population, and whether these fractures are related to age, military occupational specialty, aggression, or accidental injury. A retrospective record-based review was conducted at a single military center over a 5-year period. Service members with index finger through small finger MC fracture were identified. Data were collected utilizing Armed Forces Health Longitudinal Technology Application and electronic profile (e-profile) databases. Data collected included demographic information, mechanism of injury, nature of injury, total number of visits, and estimated time on physical restriction. 400 patients met inclusion criteria. Males accounted for 94% of the study population, 75% of fractures were of the small finger MC, 54% of patients were between 20 and 24 years, 90% were sustained by junior enlisted personnel, and most occurred by punching. Men aged service members and are often self-inflicted. As a result, these injuries account for time lost at work, reduced job performance, and decreased medical readiness. PMID:27483536

  17. Nano-iron Tracer Test for Characterizing Preferential Flow Path in Fractured Rock

    Science.gov (United States)

    Chia, Y.; Chuang, P. Y.

    2015-12-01

    Deterministic description of the discrete features interpreted from site characterization is desirable for developing a discrete fracture network conceptual model. It is often difficult, however, to delineate preferential flow path through a network of discrete fractures in the field. A preliminary cross-borehole nano-iron tracer test was conducted to characterize the preferential flow path in fractured shale bedrock at a hydrogeological research station. Prior to the test, heat-pulse flowmeter measurements were performed to detect permeable fracture zones at both the injection well and the observation well. While a few fracture zones are found permeable, most are not really permeable. Chemical reduction method was used to synthesize nano zero-valent iron particles with a diameter of 50~150 nm. The conductivity of nano-iron solution is about 3100 μs/cm. The recorded fluid conductivity shows the arrival of nano-iron solution in the observation well 11.5 minutes after it was released from the injection well. The magnetism of zero-valent iron enables it to be absorbed on magnet array designed to locate the depth of incoming tracer. We found nearly all of absorbed iron on the magnet array in the observation well were distributed near the most permeable fracture zone. The test results revealed a preferential flow path through a permeable fracture zone between the injection well and the observation well. The estimated hydraulic conductivity of the connected fracture is 2.2 × 10-3 m/s. This preliminary study indicated that nano-iron tracer test has the potential to characterize preferential flow path in fractured rock.

  18. Characterization of Hydraulic Fracture with Inflated Dislocation Moving Within a Semi-infinite Medium

    Institute of Scientific and Technical Information of China (English)

    OUYANG Zhi-hua; ELSWORTH Derek; LI Qiang

    2007-01-01

    Hydraulic fracturing is accompanied by a change in pore fluid pressure. As a result, this may be conveniently represented as inflated dislocation moving within a semi-infinite medium. Theory is developed to describe the pore pressures that build up around an inflated volumetric dislocation migrating within a saturated porous-elastic semi-infinite medium as analog to hydraulic fracturing emplacement. The solution is capable of evaluating the system behavior of both constant fluid pressure and zero flux surface conditions through application of a superposition. Characterization of horizontal moving dislocation processes is conducted as an application of these techniques. Where the mechanical and hydraulic parameters are defined, a priori, type curve matching of responses may be used to evaluate emplacement location uniquely. Pore pressure response elicited at a dilation, subject to pressure control is of interest in representing hydraulic fracturing where leak-off is an important component. The effect of hydraulic fracturing on fracture fluid pressure is evaluated in a poroelastic hydraulic fracture model utilizing dislocation theory. A minimum set of dimensionless parameters are defined that describe the system. Pore fluid pressures recorded during hydraulic fracturing of a well in the San Joaquin Valley of Central California is examined using the proposed model. The estimated geometry of the hydraulic fracture is matched with reasonable fidelity with the measured data.

  19. VSP [Vertical Seismic Profiling] and cross hole tomographic imaging for fracture characterization

    International Nuclear Information System (INIS)

    For the past several years LBL has been carrying out experiments at various fractured rock sites to determine the fundamental nature of the propagation of seismic waves in fractured media. These experiments have been utilizing high frequency (1000 to 10000 Hz.) signals in a cross-hole configuration at scales of several tens of meters. Three component sources and receivers are used to map fracture density, and orientation. The goal of the experiments has been to relate the seismological parameters to the hydrological parameters, if possible, in order to provide a more accurate description of a starting model for hydrological characterization. The work is ultimately aimed at the characterization and monitoring of the Yucca Mountain site for the storage of nuclear waste. In addition to these controlled experiments multicomponent VSP work has been carried out at several sites to determine fracture characteristics. The results to date indicate that both P-wave and S-wave can be used to map the location of fractures. In addition, fractures that are open and conductive are much more visible to seismic waves that non-conductive fractures. The results of these tests indicate direct use in an unsaturated environment. 12 refs., 10 figs

  20. The detection and characterization of natural fractures using P-wave reflection data, multicomponent VSP, borehole image logs and the in-situ stress field determination

    Energy Technology Data Exchange (ETDEWEB)

    Hoekstra, P. [Coleman Research Corp., Orlando, FL (United States)

    1995-04-01

    The objectives of this project are to detect and characterize fractures in a naturally fractured tight gas reservoir, using surface seismic methods, borehole imaging logs, and in-situ stress field data. Further, the project aims to evaluate the various seismic methods as to their effectiveness in characterizing the fractures, and to formulate the optimum employment of the seismic methods as regards fracture characterization.

  1. Advanced electron microscopy characterization of multimetallic nanoparticles

    Science.gov (United States)

    Khanal, Subarna Raj

    Research in noble metal nanoparticles has led to exciting progress in a versatile array of applications. For the purpose of better tailoring of nanoparticles activities and understanding the correlation between their structures and properties, control over the composition, shape, size and architecture of bimetallic and multimetallic nanomaterials plays an important role on revealing their new or enhanced functions for potentials application. Advance electron microscopy techniques were used to provide atomic scale insights into the structure-properties of different materials: PtPd, Au-Au3Cu, Cu-Pt, AgPd/Pt and AuCu/Pt nanoparticles. The objective of this work is to understand the physical and chemical properties of nanomaterials and describe synthesis, characterization, surface properties and growth mechanism of various bimetallic and multimetallic nanoparticles. The findings have provided us with novel and significant insights into the physical and chemical properties of noble metal nanoparticles. Different synthesis routes allowed us to synthesize bimetallic: Pt-Pd, Au-Au3Cu, Cu-Pt and trimetallic: AgPd/Pt, AuCu/Pt, core-shell and alloyed nanoparticles with monodispersed sizes, controlled shapes and tunable surface properties. For example, we have synthesized the polyhedral PtPd core-shell nanoparticles with octahedral, decahedral, and triangular plates. Decahedral PtPd core-shell structures are novel morphologies for this system. For the first time we fabricated that the Au core and Au3Cu alloyed shell nanoparticles passivated with CuS2 surface layers and characterized by Cs-corrected scanning transmission electron microscopy. The analysis of the high-resolution micrographs reveals that these nanoparticles have decahedral structure with shell periodicity, and that each of the particles is composed by Au core and Au3Cu ordered superlattice alloyed shell surrounded by CuS 2 surface layer. Additionally, we have described both experimental and theoretical methods of

  2. Fracture Mechanics Characterization of an AnisotropicGeomaterial

    OpenAIRE

    Cravero, Masantonio; Iabichino, Giorgio; Valente, Silvio; Fidelibus, Corrado; Barpi, Fabrizio

    2012-01-01

    Argillites are considered worldwide as potential host rock for high level radioactive waste given the low permeability and strong adsorption potential. However, the excavation of the galleries of a repository would produce a disturbed zone around the boundaries rich of new fractures which may enhance the conductivity of the rock along the gallery axis. Several mine-by experiments have been performed in underground rock labs to investi- gate the features of the disturbed zone. In Mont Terri UR...

  3. Advancing New 3D Seismic Interpretation Methods for Exploration and Development of Fractured Tight Gas Reservoirs

    Energy Technology Data Exchange (ETDEWEB)

    James Reeves

    2005-01-31

    In a study funded by the U.S. Department of Energy and GeoSpectrum, Inc., new P-wave 3D seismic interpretation methods to characterize fractured gas reservoirs are developed. A data driven exploratory approach is used to determine empirical relationships for reservoir properties. Fractures are predicted using seismic lineament mapping through a series of horizon and time slices in the reservoir zone. A seismic lineament is a linear feature seen in a slice through the seismic volume that has negligible vertical offset. We interpret that in regions of high seismic lineament density there is a greater likelihood of fractured reservoir. Seismic AVO attributes are developed to map brittle reservoir rock (low clay) and gas content. Brittle rocks are interpreted to be more fractured when seismic lineaments are present. The most important attribute developed in this study is the gas sensitive phase gradient (a new AVO attribute), as reservoir fractures may provide a plumbing system for both water and gas. Success is obtained when economic gas and oil discoveries are found. In a gas field previously plagued with poor drilling results, four new wells were spotted using the new methodology and recently drilled. The wells have estimated best of 12-months production indicators of 2106, 1652, 941, and 227 MCFGPD. The latter well was drilled in a region of swarming seismic lineaments but has poor gas sensitive phase gradient (AVO) and clay volume attributes. GeoSpectrum advised the unit operators that this location did not appear to have significant Lower Dakota gas before the well was drilled. The other three wells are considered good wells in this part of the basin and among the best wells in the area. These new drilling results have nearly doubled the gas production and the value of the field. The interpretation method is ready for commercialization and gas exploration and development. The new technology is adaptable to conventional lower cost 3D seismic surveys.

  4. PREFACE: International Symposium on Dynamic Deformation and Fracture of Advanced Materials (D2FAM 2013)

    Science.gov (United States)

    Silberschmidt, Vadim V.

    2013-07-01

    Intensification of manufacturing processes and expansion of usability envelopes of modern components and structures in many cases result in dynamic loading regimes that cannot be resented adequately employing quasi-static formulations of respective problems of solid mechanics. Specific features of dynamic deformation, damage and fracture processes are linked to various factors, most important among them being: a transient character of load application; complex scenarios of propagation, attenuation and reflection of stress waves in real materials, components and structures; strain-rate sensitivity of materials properties; various thermo-mechanical regimes. All these factors make both experimental characterisation and theoretical (analytical and numerical) analysis of dynamic deformation and fracture rather challenging; for instance, besides dealing with a spatial realisation of these processes, their evolution with time should be also accounted for. To meet these challenges, an International Symposium on Dynamic Deformation and Fracture of Advanced Materials D2FAM 2013 was held on 9-11 September 2013 in Loughborough, UK. Its aim was to bring together specialists in mechanics of materials, applied mathematics, physics, continuum mechanics, materials science as well as various areas of engineering to discuss advances in experimental and theoretical analysis, and numerical simulations of dynamic mechanical phenomena. Some 50 papers presented at the Symposium by researchers from 12 countries covered various topics including: high-strain-rate loading and deformation; dynamic fracture; impact and blast loading; high-speed penetration; impact fatigue; damping properties of advanced materials; thermomechanics of dynamic loading; stress waves in micro-structured materials; simulation of failure mechanisms and damage accumulation; processes in materials under dynamic loading; a response of components and structures to harsh environment. The materials discussed at D2FAM 2013

  5. Quantitative characterization of the fracture surface of Si single crystals by confocal microscopy

    Energy Technology Data Exchange (ETDEWEB)

    Xin, Y.B.; Hsia, K.J.; Lange, D.A. [Univ. of Illinois, Urbana, IL (United States)

    1995-12-01

    Experiments are conducted to study the dislocation nucleation conditions at the crack tip in {l_brace}110{r_brace}<110> oriented Si single crystals. Specimens with surface cracks are first statically loaded at elevated temperatures for a prolonged period of time to initiate and move dislocations away from the crack tip, then cooled down to room temperature and loaded to fracture to measure the fracture toughness. Fractographic analysis of the fracture surfaces is performed. Distinct wavy patterns on the fracture surface at the initial cleavage crack front are observed, which is attributed to the existence of local mixed mode 1/mode 3 stresses resulting from the inhomogeneous dislocation activity. Confocal microscopy is employed to quantify the fracture surface roughness. The results show that the increase of fracture toughness is directly associated with the increased area of the rough surface, which is characterized by the roughness number or the fractal dimension increment. The results also demonstrate that dislocation nucleation can occur only at discrete sites. The spacing between these dislocation nucleation sources is of the order of 1 {micro}m. A simple model is developed for the relationship between the fracture toughness and the surface roughness parameters, which is in good agreement with the experimental results.

  6. Experimental characterization and modelling of the alteration of fractured cement under CO2 storage conditions

    International Nuclear Information System (INIS)

    The main purpose of this thesis was to characterize and to model the hydrodynamic and thermochemical processes leading to the alteration of the wellbore cement materials under borehole conditions. Percolation experiments were performed on fractured cement samples under CO2 storage conditions (60 C and 10 MPa). Injection flow rate was dictated by the fracture aperture of each sample. CO2 enriched brine was flowed along the fracture aperture, and permeability changes as well as chemical evolution of major cations were continuously acquired during the experiment time. Reaction paths developed by the alteration of the cement were characterized using microtomography and ESEM images. The experiments conducted using samples presenting large fracture apertures during 5 h showed that permeability was maintained constant during the experiment time. Three reacted layers were displaying by the alteration of portlandite and CSH. Long term experiment (26 h) conducted with large initial fracture aperture showed a decrease of the permeability after 15 hours of CO2 exposure. Otherwise, experiments performed on samples presenting narrow apertures indicated the conversion of portlandite and CSH to calcite leading to the permeability reduction and the fracture clogging. Assemblages of phases and chemical changes were modelled using GEMS-PSI speciation code. We studied also using a coupled transport-reactive model the conditions leading to the cement alteration and the formation of associated layers. (author)

  7. Fracture characterization and discrimination criteria for karst and tectonic fractures in the Ellenburger Group, West Texas: Implications for reservoir and exploration models

    Energy Technology Data Exchange (ETDEWEB)

    Hoak, T.E. [Science Applications International Corp., Germantown, MD (United States)]|[Kestrel Geoscience, Littleton, CO (United States); Sundberg, K.R. [Phillips Petroleum Co., Bartlesville, OK (United States); Deyhim, P. [Oklahoma State Univ., Stillwater, OK (United States); Ortoleva, P. [Indiana Univ., Bloomington, IN (United States). Lab. for Computational Geodynamics

    1998-12-31

    In the Ellenburger Group fractured dolomite reservoirs of West Texas, it is extremely difficult to distinguish between multiple phases of karst-related fracturing, modifications to the karst system during burial, and overprinting tectonic fractures. From the analyses of drill core, the authors developed criteria to distinguish between karst and tectonic fractures. In addition, they have applied these criteria within the context of a detailed diagenetic cement history that allows them to further refine the fracture genesis and chronology. In these analyses, the authors evaluated the relationships between fracture intensity, morphologic attributes, host lithology, fracture cement, and oil-staining. From this analysis, they have been able to characterize variations in Ellenburger tectonic fracture intensity by separating these fractures from karst-related features. In general, the majority of fracturing in the Ellenburger is caused by karst-related fracturing although a considerable percentage is caused by tectonism. These findings underscore the importance of considering the complete geologic evolution of a karst reservoir during exploration and field development programs. The authors have been able to more precisely define the spatial significance of the fracture data sets by use of oriented core from Andector Field. They have also demonstrated the importance of these results for exploration and reservoir development programs in West Texas, and the potential to extrapolate these results around the globe. Given the historic interest in the large hydrocarbon reserves in West Texas carbonate reservoirs, results of this study will have tremendous implications for exploration and production strategies targeting vuggy, fractured carbonate systems not only in West Texas, but throughout the globe.

  8. Fracture characterization from near-offset VSP inversion

    Energy Technology Data Exchange (ETDEWEB)

    Horne, S. [British Geological Survey, Edinburgh (United Kingdom)]|[Univ. of Edinburgh (United Kingdom). Dept. of Geology and Geophysics; MacBeth, C. [British Geological Survey, Edinburgh (United Kingdom); Queen, J.; Rizer, W.; Cox, V. [Conoco, Inc., Ponca City, OK (United States)

    1997-01-01

    A global optimization method incorporating a ray-tracing scheme is used to invert observations of shear-wave splitting from two near-offset VSPs recorded at the Conoco Borehole Test Facility, Kay County, Oklahoma. Inversion results suggest that the seismic anisotropy is due to a non-vertical fracture system. This interpretation is constrained by the VSP acquisition geometry for which two sources are employed along near diametrically opposite azimuths about the well heads. A correlation is noted between the time-delay variations between the fast and slow split shear waves and the sandstone formations.

  9. Advances in fracture mechanics analyses of primary system performance under operating and accident conditions

    International Nuclear Information System (INIS)

    Safety research sponsored by the Nuclear Regulatory Commission, Division of Reactor Safety Research, has resulted in notable advances in several areas of importance in the safety evaluation of reactor primary systems under normal operations and accident situations. First, the methods of linear elastic fracture mechanics and of elastic plastic fracture mechanics have been validated for prediction of pressure vessel performance by the Intermediate Vessel Test program results at the Oak Ridge National Laboratory. The ability confidently to predict vessel performance under realistic service conditions has permitted development of the computer program OCTAVIA which computes failure curves for a range of flaw sizes in terms of pressure and temperature for specified presure vessel material at specific neutron fluence levels. It then considers the probability of occurrence of flaw sizes and magnitude of pressure during an operational, overpressurization transient and determines the probability of failure, for both individual flaw sizes and for the full spectrum. This advance has been verified by the confirmatory results of testing small thick-walled cylinders under thermal shock conditions in the Heavy Section Steel Technology program, and of warm prestressing tests at the US Navel Research Laboratory. Thirdly, the technology of crack arrest has reached a level wherein standardization of test specimens and testing methods is now possible and, indeed, is underway. (Auth.)

  10. Applicability of smaller than Charpy specimens for fracture toughness characterization with the VTT method

    International Nuclear Information System (INIS)

    The term fracture toughness usually refers to the linear elastic fracture resistance parameter KIC. In the case of structural steels, the estimation of KIC is limited to the lower shelf of toughness or require extremely large specimens. This specimen size requirement has been one major obstacle for applying fracture mechanics in structural integrity assessment outside aviation, nuclear and off-shore industries. During the last decade, a statistical data treatment methodology, based on a micro-mechanistic cleavage fracture model, combined with elastic plastic finite element analysis has enabled the fracture toughness to be characterized with small specimens in the ductile-to-brittle transition region. The methodology is known as the VTT method or the Master Curve procedure. The development has led to a new testing standard for fracture toughness testing of ferritic steels in the transition range. Here, the premises for the methodology are described and its validity range is discussed. Presently the methodology has been validated for as small as 10.10 mm2 bend specimens, but the use of even smaller specimens is under investigation. Specifically, results obtained with three different sub-Charpy specimen configurations are presented and discussed. (author)

  11. Characterization of Fractured Reservoirs Using a Combination of Downhole Pressure and Self-Potential Transient Data

    Directory of Open Access Journals (Sweden)

    Yuji Nishi

    2012-01-01

    Full Text Available In order to appraise the utility of self-potential (SP measurements to characterize fractured reservoirs, we carried out continuous SP monitoring using multi Ag-AgCl electrodes installed within two open holes at the Kamaishi Mine, Japan. The observed ratio of SP change to pressure change associated with fluid flow showed different behaviors between intact host rock and fractured rock regions. Characteristic behavior peculiar to fractured reservoirs, which is predicted from numerical simulations of electrokinetic phenomena in MINC (multiple interacting continua double-porosity media, was observed near the fractures. Semilog plots of the ratio of SP change to pressure change observed in one of the two wells show obvious transition from intermediate time increasing to late time stable trends, which indicate that the time required for pressure equilibration between the fracture and matrix regions is about 800 seconds. Fracture spacing was estimated to be a few meters assuming several micro-darcies (10-18 m2 of the matrix region permeability, which is consistent with geological and hydrological observations.

  12. Fractal characterization of fracture networks: An improved box-counting technique

    Science.gov (United States)

    Roy, Ankur; Perfect, Edmund; Dunne, William M.; McKay, Larry D.

    2007-12-01

    Box counting is widely used for characterizing fracture networks as fractals and estimating their fractal dimensions (D). If this analysis yields a power law distribution given by N ∝ r-D, where N is the number of boxes containing one or more fractures and r is the box size, then the network is considered to be fractal. However, researchers are divided in their opinion about which is the best box-counting algorithm to use, or whether fracture networks are indeed fractals. A synthetic fractal fracture network with a known D value was used to develop a new algorithm for the box-counting method that returns improved estimates of D. The method is based on identifying the lower limit of fractal behavior (rcutoff) using the condition ds/dr → 0, where s is the standard deviation from a linear regression equation fitted to log(N) versus log(r) with data for r sequentially excluded. A set of 7 nested fracture maps from the Hornelen Basin, Norway was used to test the improved method and demonstrate its accuracy for natural patterns. We also reanalyzed a suite of 17 fracture trace maps that had previously been evaluated for their fractal nature. The improved estimates of D for these maps ranged from 1.56 ± 0.02 to 1.79 ± 0.02, and were much greater than the original estimates. These higher D values imply a greater degree of fracture connectivity and thus increased propensity for fracture flow and the transport of miscible or immiscible chemicals.

  13. Application of small specimens to fracture mechanics characterization of irradiated pressure vessel steels

    International Nuclear Information System (INIS)

    In this study, precracked Charpy V-notch (PCVN) specimens were used to characterize the fracture toughness of unirradiated and irradiated reactor pressure vessel steels in the transition region by means of three-point static bending. Fracture toughness at cleavage instability was calculated in terms of elastic-plastic KJc values. A statistical size correction based upon weakest-link theory was performed. The concept of a master curve was applied to analyze fracture toughness properties. Initially, size-corrected PCVN data from A 533 grade B steel, designated HSST Plate O2, were used to position the master curve and a 5% tolerance bound for KJc data. By converting PCVN data to IT compact specimen equivalent KJc data, the same master curve and 5% tolerance bound curve were plotted against the Electric Power Research Institute valid linear-elastic KJc database and the ASME lower bound KIc curve. Comparison shows that the master curve positioned by testing several PCVN specimens describes very well the massive fracture toughness database of large specimens. These results give strong support to the validity of KJc with respect to KIc in general and to the applicability of PCVN specimens to measure fracture toughness of reactor vessel steels in particular. Finally, irradiated PCVN specimens of other materials were tested, and the results are compared to compact specimen data. The current results show that PCVNs demonstrate very good capacity for fracture toughness characterization of reactor pressure vessel steels. It provides an opportunity for direct measurement of fracture toughness of irradiated materials by means of precracking and testing Charpy specimens from surveillance capsules. However, size limits based on constraint theory restrict the operational test temperature range for KJc data from PCVN specimens. 13 refs., 8 figs., 1 tab

  14. Techniques for Source Zone and Plume Characterization of Tetrachloroethene in Fractured Limestone Aquifers

    DEFF Research Database (Denmark)

    Fjordbøge, Annika Sidelmann; Mosthaf, Klaus; Janniche, Gry S.;

    Characterization of chlorinated solvents in fractured limestone aquifers is essential for proper development of site specific conceptual models and subsequent risk assessment and remediation. High resolution characterization is challenged by the difficulties involved in collection of intact core...... samples as water flushing during drilling often results in extensive core losses, especially from zones with soft limestone in contact with flint beds. Field investigations with alternative characterization techniques have been carried out at two Danish sites with tetrachloroethene (PCE) contaminated...... fractured limestone aquifers. The two sites represent different scales (source and plume) and contaminant levels (DNAPL and dissolved). The scope of the investigations was to evaluate different techniques for characterization of the contaminant distribution in the limestone aquifers and to obtain...

  15. Advances on models, characterizations and applications

    CERN Document Server

    Balakrishnan, N; Gebizlioglu, O L

    2005-01-01

    PrefaceContributorsThe Shapes of the Probability Density, Hazard, and Reverse Hazard FunctionsMasaaki SibuyaStochastic Ordering of Risks, Influence of Dependence, and A.S. ConstructionsLudger RüschendorfThe q-Factorial Moments of Discrete q-Distributions and a Characterization of the Euler DistributionCh.A. Charalambides and N. PapadatosOn the Characterization of Distributions Through the Properties of Conditional Expectations of Order StatisticsI. Bairamov and O. GebizliogluCharacterization of the Exponential Distribution by Conditional Expectations of Generalized SpacingsErhard Cramer and Ud

  16. Electrical characterization of advanced gate dielectrics

    NARCIS (Netherlands)

    Degraeve, R.; Schmitz, J.; Pantisano, L.; Simoen, E.; Houssa, M.; Kaczer, B.; Groeseneken, G.; Baklanov, M.; Green, M.; Maex, K.

    2007-01-01

    The topic of thin films is an area of increasing importance in materials science, electrical engineering and applied solid state physics; with both research and industrial applications in microelectronics, computer manufacturing, and physical devices. Advanced, high-performance computers, high-defin

  17. Fracture strength characterization for 25 micron and 125 micron thick SOI-MEMS structures

    International Nuclear Information System (INIS)

    MEMS structural devices are often fabricated by bulk-micromachining using a deep reactive ion-etching process (DRIE) for silicon. DRIE creates the high aspect ratio silicon features used as sensors and actuators in MEMS devices. This paper characterizes fracture strength distributions for DRIE etched MEMS test structures with device layer thicknesses of 25 μm and 125 μm using pull-table style strength test structures. The 25 μm thick measurements offered a direct comparison with previous investigations; whereas, the 125 μm thick measurements are unique to this study. The fracture strength distributions measured for 125 μm thick specimens ranged to significantly lower values and had a narrower distribution compared to previous and current 25 μm thick device layer fracture strength distributions. scanning electron microscopy (SEM) and atomic force microscopy (AFM) were used to characterize and correlate surface roughness features with the observed fracture strength measurements. Characterization revealed that although both the 25 μm and 125 μm thick device layer structures predominantly exhibited scalloping sidewall morphology, the 125 μm thick structures transitioned to rougher curtaining sidewall morphology towards the bottom of the device layer. The difference in strength distributions is attributed to this increased roughness present in the curtaining region and on the bottom surfaces of thicker device layers. (paper)

  18. Innovations in the characterization of fractured rocks developed within the Stripa project

    International Nuclear Information System (INIS)

    This text deals with the hydrogeological work that has been carried out at Stripa Mine. First of all, the philosophy applied evolved through the years, and has finally been focused on a fractured rock approach. Second, it has been necessary to develop hydraulic testing methods - such as focused packer testing - and equipment; the key of the success of the equipment that was built, was that it was fully computer controlled and able to regulate water pressures quickly, reliably and accurately. In the end, the aim of the hydrogeological testing was to characterize both the small scale fracture network and the large scale major fracture zone which composed the site. (TEC). 13 refs., 5 figs

  19. Joint geophysical and flow inversion to characterize fracture networks in subsurface systems

    CERN Document Server

    Mudunuru, M K; Makedonska, N; Chen, T

    2016-01-01

    Subsurface applications including geothermal, geological carbon sequestration, oil and gas, etc., typically involve maximizing either the extraction of energy or the storage of fluids. Characterizing the subsurface is extremely complex due to heterogeneity and anisotropy. Due to this complexity, there are uncertainties in the subsurface parameters, which need to be estimated from multiple diverse as well as fragmented data streams. In this paper, we present a non-intrusive joint inversion framework, for integrating data from geophysical and flow sources to constraint subsurface Discrete Fracture Networks (DFN). In this approach, we first estimate bounds on the statistics for the DFN fracture orientations using microseismic data. These bounds are estimated through a combination of a focal mechanism (physics-based approach) and clustering analysis (statistical approach) of seismic data. Then, the fracture lengths are constrained based on the flow data. The efficacy of this multi-physics based joint inversion is...

  20. Laser characterization with advanced digital signal processing

    DEFF Research Database (Denmark)

    Piels, Molly; Tafur Monroy, Idelfonso; Zibar, Darko

    2015-01-01

    The use of machine learning techniques to characterize lasers with low output power is reviewed. Optimized phase tracking algorithms that can produce accurate noise spectra are discussed, and a method for inferring the amplitude noise spectrum and rate equation model of the laser under test is pr...

  1. Advanced Structural Characterization of Organic Thin Films

    DEFF Research Database (Denmark)

    Gu, Yun

    In this thesis, the structural characterizations of three organic film systems are described. Several X-ray based techniques have been utilized for the characterizations for different research goals. The structures of N,N',N-trioctyltriazatriangulenium (Oct3-TATA+) salts have been investigated...... by optical, surface and X-ray method. We describe the production of Langmuir-Blodgett film and how the absorption spectroscopy is a powerful tool to identify layer of monomer and dimer. X-ray refelctometry has been applied as a method for the study of the multilayer film and interface structure. A separation...... of small molecule and polymer layers is indicated by Flory- Huggins theory for the triisopropylsilylethynl pentacene (TIPS-PEN) and polystyrene blend films. In order to investigate the phase separated layers in the ink-jet printed films, we propose a method to measure diraction Bragg peaks by X...

  2. Characterizing Fractures in Geysers Geothermal Field by Micro-seismic Data, Using Soft Computing, Fractals, and Shear Wave Anisotropy

    Energy Technology Data Exchange (ETDEWEB)

    Aminzadeh, Fred [Univ. of Southern California, Los Angeles, CA (United States); Sammis, Charles [Univ. of Southern California, Los Angeles, CA (United States); Sahimi, Mohammad [Univ. of Southern California, Los Angeles, CA (United States); Okaya, David [Univ. of Southern California, Los Angeles, CA (United States)

    2015-04-30

    The ultimate objective of the project was to develop new methodologies to characterize the northwestern part of The Geysers geothermal reservoir (Sonoma County, California). The goal is to gain a better knowledge of the reservoir porosity, permeability, fracture size, fracture spacing, reservoir discontinuities (leaky barriers) and impermeable boundaries.

  3. Using radar tomography, tracer experiments and hydraulic data to characterize fractured rock flow systems

    Science.gov (United States)

    Day-Lewis, Frederick David

    Among the most pressing problems in hydrogeology is describing heterogeneity in fractured rock, where data are typically local and sparse, and permeability varies by orders of magnitude over short distances. This dissertation presents new approaches to characterize fractured rock groundwater flow systems using cross-well radar, tracer, and hydraulic experiments. The methods are demonstrated using data from the U.S. Geological Survey Fractured Rock Hydrology Research Site near Mirror Lake, New Hampshire. One underutilized source of information in characterization of fractured rock is hydraulic connection data. Wells connected by a high-permeability fracture zone tend to exhibit similar hydraulic responses during pumping or drilling. A simulated-annealing algorithm is presented to condition geostatistical simulations to inferred connections. The method is used to generate 3-D realizations of fracture-zone geometry at the Mirror Lake Site. Results indicate the likely extents of specific zones. Flow models based on realizations are calibrated to hydraulic data to estimate the hydraulic parameters of the fracture zones and surrounding bedrock. Another innovative source of information for characterization is time-lapse difference-attenuation radar tomography, which has been used to monitor the migration of electrically conductive saline tracers. A sequential-inversion methodology is presented and demonstrated for a synthetic example. The method uses space-time parameterization and regularization to account for changes in concentration that occur quickly relative to the collection of radar data. The time-lapse tomographic inversion method is applied to data from the Mirror Lake Site. Difference-attenuation tomography indicates the timing and spatial distribution of tracer transport in three planes that form a triangular prism. Tracer migration is focused along a preferential pathway. Comparison of the time-series of tomograms with the outlet tracer data suggests that much

  4. Correlation of microstructure and fracture toughness of advanced 9Cr/CrMoV dissimilarly welded joint

    Energy Technology Data Exchange (ETDEWEB)

    Guo, Qian [Shanghai Key Laboratory of Materials Laser Processing and Modification, School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240 (China); Lu, Fenggui, E-mail: Lfg119@sjtu.edu.cn [Shanghai Key Laboratory of Materials Laser Processing and Modification, School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240 (China); Liu, Xia [Shanghai Turbine Plant of Shanghai Electric Power Generation Equipment Co. Ltd., Shanghai 200240 (China); Yang, Renjie [Shanghai Turbine Works Company, Shanghai 200240 (China); Cui, Haichao [Shanghai Key Laboratory of Materials Laser Processing and Modification, School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240 (China); Gao, Yulai, E-mail: ylgao@shu.edu.cn [State Key Laboratory of Advanced Special Steels, Shanghai University, Shanghai 200072 (China)

    2015-06-25

    In this paper, the fracture toughness and the related microstructure characteristics of dissimilarly welded joint manufactured by advanced 9Cr and CrMoV steels were systematically investigated. The dissimilarly welded joint was fabricated by narrow gap submerged arc welding (NG-SAW) applying multi-layer and multi-pass technique. Fracture toughness, as one of the most important property to assess the reliability of welded joint, was studied for different regions including CrMoV base metal (CrMoV-BM), heat affected zone (HAZ) of CrMoV side (CrMoV-HAZ), weld metal (WM), heat affected zone of 9Cr side (9Cr-HAZ) and 9Cr base metal (9Cr-BM). It was found that the fracture toughness of CrMoV-BM, CrMoV-HAZ and WM was better than that of 9Cr-HAZ and 9Cr-BM. In order to illustrate these results, the microstructure of the whole welded joint was observed by optical microscope (OM), scanning electron microscope (SEM) and transmission electron microscope (TEM) detailedly. It was found that the fine high-temperature tempered martensite and bainite in WM, CrMoV-BM and CrMoV-HAZ contribute to the higher fracture toughness, while lower fracture toughness for 9Cr-BM and HAZ was caused by coarse tempered lath-martensite. Furthermore, the fracture morphology showed that ductile fracture occurred in WM and CrMoV side, while brittle fracture appeared in BM and HAZ of 9Cr side.

  5. Correlation of microstructure and fracture toughness of advanced 9Cr/CrMoV dissimilarly welded joint

    International Nuclear Information System (INIS)

    In this paper, the fracture toughness and the related microstructure characteristics of dissimilarly welded joint manufactured by advanced 9Cr and CrMoV steels were systematically investigated. The dissimilarly welded joint was fabricated by narrow gap submerged arc welding (NG-SAW) applying multi-layer and multi-pass technique. Fracture toughness, as one of the most important property to assess the reliability of welded joint, was studied for different regions including CrMoV base metal (CrMoV-BM), heat affected zone (HAZ) of CrMoV side (CrMoV-HAZ), weld metal (WM), heat affected zone of 9Cr side (9Cr-HAZ) and 9Cr base metal (9Cr-BM). It was found that the fracture toughness of CrMoV-BM, CrMoV-HAZ and WM was better than that of 9Cr-HAZ and 9Cr-BM. In order to illustrate these results, the microstructure of the whole welded joint was observed by optical microscope (OM), scanning electron microscope (SEM) and transmission electron microscope (TEM) detailedly. It was found that the fine high-temperature tempered martensite and bainite in WM, CrMoV-BM and CrMoV-HAZ contribute to the higher fracture toughness, while lower fracture toughness for 9Cr-BM and HAZ was caused by coarse tempered lath-martensite. Furthermore, the fracture morphology showed that ductile fracture occurred in WM and CrMoV side, while brittle fracture appeared in BM and HAZ of 9Cr side

  6. ADVANCED FRACTURING TECHNOLOGY FOR TIGHT GAS: AN EAST TEXAS FIELD DEMONSTRATION

    Energy Technology Data Exchange (ETDEWEB)

    Mukul M. Sharma

    2005-03-01

    The primary objective of this research was to improve completion and fracturing practices in gas reservoirs in marginal plays in the continental United States. The Bossier Play in East Texas, a very active tight gas play, was chosen as the site to develop and test the new strategies for completion and fracturing. Figure 1 provides a general location map for the Dowdy Ranch Field, where the wells involved in this study are located. The Bossier and other tight gas formations in the continental Unites States are marginal plays in that they become uneconomical at gas prices below $2.00 MCF. It was, therefore, imperative that completion and fracturing practices be optimized so that these gas wells remain economically attractive. The economic viability of this play is strongly dependent on the cost and effectiveness of the hydraulic fracturing used in its well completions. Water-fracs consisting of proppant pumped with un-gelled fluid is the type of stimulation used in many low permeability reservoirs in East Texas and throughout the United States. The use of low viscosity Newtonian fluids allows the creation of long narrow fractures in the reservoir, without the excessive height growth that is often seen with cross-linked fluids. These low viscosity fluids have poor proppant transport properties. Pressure transient tests run on several wells that have been water-fractured indicate a long effective fracture length with very low fracture conductivity even when large amounts of proppant are placed in the formation. A modification to the water-frac stimulation design was needed to transport proppant farther out into the fracture. This requires suspending the proppant until the fracture closes without generating excessive fracture height. A review of fracture diagnostic data collected from various wells in different areas (for conventional gel and water-fracs) suggests that effective propped lengths for the fracture treatments are sometimes significantly shorter than those

  7. On the analysis of a mixed mode bending sandwich specimen for debond fracture characterization

    OpenAIRE

    Quispitupa, Amilcar; Berggreen, Christian; Carlsson, Leif A.

    2009-01-01

    The mixed mode bending specimen originally developed for mixed mode delamination fracture characterization of unidirectional composites has been extended to the study of debond propagation in foam cored sandwich specimens. The compliance and strain energy release rate expressions for the mixed mode bending sandwich specimen are derived based on a superposition analysis of solutions for the double cantilever beam and cracked sandwich beam specimens by applying a proper kinematic relationship f...

  8. Characterization of the Microstructure, Fracture, and Mechanical Properties of Aluminum Alloys 7085-O and 7175-T7452 Hollow Cylinder Extrusions

    Science.gov (United States)

    Benoit, Samuel G.; Chalivendra, Vijaya B.; Rice, Matthew A.; Doleski, Robert F.

    2016-06-01

    Microstructural, tensile, and fracture characterizations of cylindrically forged forms of aluminum alloys AA7085-O and AA7175-T7452 were performed. Mechanical and fracture properties were investigated along radial, circumferential, and longitudinal directions to determine directional dependency. American Society for Testing and Materials (ASTM) test methods (ASTM E8-04 and ASTM E1820) were employed for both the tensile and fracture characterizations, respectively. The tensile and fracture properties were related to microstructure in each direction. The strength, elongation at break, and ultimate tensile strength of AA7085-O were higher than those of AA7175-T7452. AA7175-T7452 alloy failed in a brittle manner during fracture studies. AA7085-O outperformed AA7175-T7452 on fracture energy in all of the orientations studied. Smaller grain sizes on the planes normal to circumferential and longitudinal directions showed improvement in both elongation at break and fracture energy values compared to those of radial direction. Scanning electron microscopy images demonstrated cleavage fracture in AA7175-T7452 and transgranular fracture in AA7085-O.

  9. Geophysical methods for fracture characterization in and around potential sites for nuclear waste disposal

    International Nuclear Information System (INIS)

    Historically, geophysical methods have been used extensively to successfully explore the subsurface for petroleum, gas, mineral, and geothermal resources. Their application, however, for site characterization, and monitoring the performance of near surface waste sites or repositories has been somewhat limited. Presented here is an overview of the geophysical methods that could contribute to defining the subsurface heterogeneity and extrapolating point measurements at the surface and in boreholes to volumetric descriptions in a fractured rock. In addition to site characterization a significant application of geophysical methods may be in performance assessment and in monitoring the repository to determine if the performance is as expected

  10. Advanced NMR characterization of zeolite catalysts

    Science.gov (United States)

    Welsh, L. B.

    1985-04-01

    The program discussed in this report is a two-year two-phase joint UOP-University of Illinois study of the application of improved high resolution solid state nuclear magnetic resonance (NMR) techniques to the characterization of zeolite catalysts. During the first phase of this program very pure, and in some cases isotopically enriched faujasites will be prepared and studied by magic angle sample spinning NMR (MASS NMR) and variable engine sample spinning NMR (VASS NMR) on 500 and 360 MHz (proton frequency) NMR spectrometers. The NMR techniques that will be emphasized are the measurement and analysis of the (17)O NMR properties, (27)Al NMR intensity quantitation, and (27)Al and (29)Si NMR relaxation rates. During the second phase of this program these NMR techniques will be used to study the effects of impurity concentration, dealumination treatments and cation exchange on the NMR properties of faujasites. The initial emphasis of this program during Phase I is on the preparation and measurement of the NMR properties of (17)O enriched Na-Y faujasties.

  11. Ssismic Methodologies Applied To The Characterization Of Fractured Rock Massifs: Case Studies

    Science.gov (United States)

    Marti, D.; Carbonell, R.; Flecha, I.; Palomeras, I.; Font-Capo, J.; Vazquez-Sune, E.; Perez-Estaun, A.

    2007-05-01

    The detailed characterization of fractured media in the shallow subsurface is becoming important. The detailed knowledge of the fracture network is mandatory in any hydrogeological model to constrain the potential pathways for water circulation. The geophysical methodolgies can provide a detailed image of the fractured rock and also the 3D distribution of physical properties. Two case studies are discussed in this work. The characterization of fractures in a waste disposal site and, the design and construction of a subway tunnel. In the first case, a multiseismic experiment was carried out in an old abandoned uranium mine. 2D and 3D seismic experiments including VSP, surface seismic reflection and travel time seismic tomography provided a 3D image of the internal structure of a granitic massif for hydrogeological studies of the preferred paths for the migration of contaminants. The tectonic stability of the site was also addressed by means of seismic measurements. The joint interpretation of all the available data enabled the interpretation of the low velocity anomalies in the 3D seismic tomography image as the fragile fractures and the alteration associated to them. A 3D image of the geometry of the heterogeneous weathered surface layer was also obtained. This surface is controlled by the complex network of faults and dykes observed in the area. The second case study involves 2D and 3D seismic experiments to aid the horizontal drilling of tunnels for a new subway line in Barcelona (Spain). Seismic data acquisition in a densely populated city is very difficult. The street layout determines the geometry of the acquisition experiments. The instrumentation can not always be located on the surface projection of the tunnel trace, therefore, pseudo 3D acquisition is required, deploying the instrumentation were it is possible. Furthermore, the shallow subsurface features extremely heterogeneous "weathered" layer of variable thickness (building fundations, sewage system

  12. Comparison of fracture properties in SA508 Gr.3 and Gr.4N high strength low alloy steels for advanced pressure vessel materials

    International Nuclear Information System (INIS)

    Nuclear power systems are moving to a larger capacity or smaller modular type. In any either case, advanced pressure vessel materials with high strength and toughness are definitely needed for an optimization of the design and construction, as well as the long-term operation. In this paper, two candidate materials, both of which are within the current ASME specifications of SA508 steel forging, are compared from the view point of fracture resistance properties for a nuclear pressure vessel steel. The microstructure and mechanical properties of SA508 Gr.3 Cl.1, Cl.2, and Gr.4N steels were also characterized. The predominant microstructure of SA508 Gr.4N model alloy is tempered martensite, while SA508 Gr.3 Cl.1 and Cl.2 steels show a tempered upper bainitic structure. SA508 Gr. 4N model alloy showed the best strength and transition behavior among the three types of SA508 steel. SA508 Gr.3 Cl.2 steel has good strength and fracture toughness, but there is a decrease in the upper-self energy. The fracture resistance and fatigue crack growth rate of SA508 Gr.3 Cl.2 and Gr.4N steels were comparable to those of SA508 Gr.3 Cl.1 steel. In terms of mechanical properties, SA508 Gr.4N steel is a fascinating material for the pressure vessel application although it still needs verification on the aging behavior such as the irradiation embrittlement resistance

  13. Seismic geometric attribute analysis for fracture characterization: New methodologies and applications

    Science.gov (United States)

    Di, Haibin

    In 3D subsurface exploration, detection of faults and fractures from 3D seismic data is vital to robust structural and stratigraphic analysis in the subsurface, and great efforts have been made in the development and application of various seismic attributes (e.g. coherence, semblance, curvature, and flexure). However, the existing algorithms and workflows are not accurate and efficient enough for robust fracture detection, especially in naturally fractured reservoirs with complicated structural geometry and fracture network. My Ph.D. research is proposing the following scopes of work to enhance our capability and to help improve the resolution on fracture characterization and prediction. For discontinuity attribute, previous methods have difficulty highlighting subtle discontinuities from seismic data in cases where the local amplitude variation is non-zero mean. This study proposes implementing a gray-level transformation and the Canny edge detector for improved imaging of discontinuities. Specifically, the new process transforms seismic signals to be zero mean and helps amplify subtle discontinuities, leading to an enhanced visualization for structural and stratigraphic details. Applications to various 3D seismic datasets demonstrate that the new algorithm is superior to previous discontinuity-detection methods. Integrating both discontinuity magnitude and discontinuity azimuth helps better define channels, faults and fractures, than the traditional similarity, amplitude gradient and semblance attributes. For flexure attribute, the existing algorithm is computationally intensive and limited by the lateral resolution for steeply-dipping formations. This study proposes a new and robust volume-based algorithm that evaluate flexure attribute more accurately and effectively. The algorithms first volumetrically fit a cubic surface by using a diamond 13-node grid cell to seismic data, and then compute flexure using the spatial derivatives of the built surface. To avoid

  14. Measurement system for systematic hydrological characterization of unsaturated fractured welded tuff in a mined underground tunnel.

    Science.gov (United States)

    Cook, P J; Salve, R; Freifeld, B M; Tsang, Y T

    2003-01-01

    A field investigation of unsaturated flow through a lithophysal unit of fractured welded tuff containing lithophysal cavities has been initiated. To characterize flow in this spatially heterogeneous medium, a systematic approach has been developed to perform tests in boreholes drilled at regular intervals in an underground tunnel (drift). The purpose of the testing is to quantify the amounts of water seeping into the drift versus the amount of water moving around the drift when released into boreholes at many equidistant locations along the drift. In this paper, we describe the test equipment system that has been built for this purpose. Because the field-scale measurements--of liquid flow in the unsaturated, fractured rocks--require continuous testing for periods of days to weeks, the control of test equipment has been fully automated, allowing operation with no human presence at the field site. Preliminary results from the first set of tests indicate that, while the effects of evaporation on characterization of hydrological properties of the rock can be significant, these effects can be controlled and quantified. These tests give insight into the role of the cavities as potential storage during the initial transient flow prior to the breakthrough of water at the drift crown, as well as the role of connected fractures that provide the subsequent quasi-steady flow. In addition to the stated purpose of realizing the flow partitioning, the results yield values for the effective porosity in the pathways for liquid flow in the regions tested thus far. PMID:12873008

  15. An Integrated Approach to Characterizing Bypassed Oil in Heterogeneous and Fractured Reservoirs Using Partitioning Tracers

    Energy Technology Data Exchange (ETDEWEB)

    Akhil Datta-Gupta

    2005-08-01

    naturally fractured reservoirs with changing field conditions. This considerably broadens the applicability of the streamline-based analysis of tracer data and field production history for characterization of heterogeneous and fractured reservoirs.

  16. CHARACTERIZATION OF THE ADVANCED RADIOGRAPHIC CAPABILITY FRONT END ON NIF

    Energy Technology Data Exchange (ETDEWEB)

    Haefner, C; Heebner, J; Dawson, J; Fochs, S; Shverdin, M; Crane, J K; Kanz, V K; Halpin, J; Phan, H; Sigurdsson, R; Brewer, W; Britten, J; Brunton, G; Clark, W; Messerly, M J; Nissen, J D; Nguyen, H; Shaw, B; Hackel, R; Hermann, M; Tietbohl, G; Siders, C W; Barty, C J

    2009-07-15

    We have characterized the Advanced Radiographic Capability injection laser system and demonstrated that it meets performance requirements for upcoming National Ignition Facility fusion experiments. Pulse compression was achieved with a scaled down replica of the meter-scale grating ARC compressor and sub-ps pulse duration was demonstrated at the Joule-level.

  17. Characterization Of The Advanced Radiographic Capability Front End On NIF

    International Nuclear Information System (INIS)

    We have characterized the Advanced Radiographic Capability injection laser system and demonstrated that it meets performance requirements for upcoming National Ignition Facility fusion experiments. Pulse compression was achieved with a scaled down replica of the meter-scale grating ARC compressor and sub-ps pulse duration was demonstrated at the Joule-level

  18. Modeling of the fracture behavior of spot welds using advanced micro-mechanical damage models

    Science.gov (United States)

    Sommer, Silke

    2010-06-01

    This paper presents the modeling of deformation and fracture behavior of resistance spot welded joints in DP600 steel sheets. Spot welding is still the most commonly used joining technique in automotive engineering. In overloading situations like crash joints are often the weakest link in a structure. For those reasons, crash simulations need reliable and applicable tools to predict the load bearing capacity of spot welded components. Two series of component tests with different spot weld diameters have shown that the diameter of the weld nugget is the main influencing factor affecting fracture mode (interfacial or pull-out fracture), load bearing capacity and energy absorption. In order to find a correlation between nugget diameter, load bearing capacity and fracture mode, the spot welds are simulated with detailed finite element models containing base metal, heat affected zone and weld metal in lap-shear loading conditions. The change in fracture mode from interfacial to pull-out or peel-out fracture with growing nugget diameter under lap-shear loading was successfully modeled using the Gologanu-Leblond model in combination with the fracture criteria of Thomason and Embury. A small nugget diameter is identified to be the main cause for interfacial fracture. In good agreement with experimental observations, the calculated pull-out fracture initiates in the base metal at the boundary to the heat affected zone.

  19. Hydraulic Anisotropy Characterization Using Azimuthal Self Potential Gradient [ASPG]: Results from Pneumatic Fracturing of Tight Clay Soils

    Science.gov (United States)

    Slater, L.; Wishart, D.; Schnell, D.; Hermann, G.

    2008-12-01

    Recent studies have shown that bulk hydraulic anisotropy associated with fractures in fractured rock aquifers can be inferred from Azimuthal Self Potential Gradient (ASPG) measurements. This extremely simple technique involves measuring the self potential gradient as a function of azimuth with a pair of non polarizing electrodes connected to a voltmeter. The electrokinetic effect associated with the flow of fluids within fractures is the source of the ASPG signal. Fracture strike mapping at multiple sites has repeatedly demonstrated the effectiveness of the method at the field scale and indicated that the direction of flow can be determined from the polarity of relatively large ASPG signals. A laboratory study was conducted to determine whether ASPG could also be used to characterize the hydraulic anisotropy associated with the enhancement of permeability and porosity of tight unconsolidated soils (e.g. clays) as a result of pneumatic fracturing, a technique to improve the effectiveness of remediation efforts. Compressed kaolinite sediments were pneumatically fractured following industry procedures. The resulting fracture geometry was quantified from strike analysis of visible fractures combined with strike data from optical borehole televiewer (BHTV) imaging. ASPG measurements were then made during injection of a simulated remedial treatment (electrolyte/dye) under an applied gas pressure. Consistent with previous findings in fractured rock aquifers, ASPG lobes are well correlated with azimuths of high fracture strike density suggesting that the ASPG anisotropy is a proxy measure of hydraulic anisotropy created by the pneumatic fracturing. The magnitude of the ASPG signal scales linearly (linear correlation coefficients > 0.74) with the applied gas pressure gradient for any particular hydraulically-active fracture set and the positive lobe of the ASP anomaly denotes the flow direction within that fracture set. These findings demonstrate that applications of the

  20. An integrated methodology for sub-surface fracture characterization using microseismic data: A case study at the NW Geysers

    Science.gov (United States)

    Aminzadeh, Fred; Tafti, Tayeb A.; Maity, Debotyam

    2013-04-01

    Geothermal and unconventional hydrocarbon reservoirs are often characterized by low permeability and porosity. So, they are difficult to produce and require stimulation techniques, such as thermal shear deactivation and hydraulic fracturing. Fractures provide porosity for fluid storage and permeability for fluid movement and play an important role in production from this kind of reservoirs. Hence, characterization of fractures has become a vitally important consideration in every aspect of exploration, development and production so as to provide additional energy resources for the world. During the injection or production of fluid, induced seismicity (micro-seismic events) can be caused by reactivated shears created fractures or the natural fractures in shear zones and faults. Monitoring these events can help visualize fracture growth during injection stimulation. Although the locations of microseismic events can be a useful characterization tool and have been used by many authors, we go beyond these locations to characterize fractures more reliably. Tomographic inversion, fuzzy clustering, and shear wave splitting are three methods that can be applied to microseismic data to obtain reliable characteristics about fractured areas. In this article, we show how each method can help us in the characterization process. In addition, we demonstrate how they can be integrated with each other or with other data for a more holistic approach. The knowledge gained might be used to optimize drilling targets or stimulation jobs to reduce costs and maximize production. Some of the concepts discussed in this paper are general in nature, and may be more applicable to unconventional hydrocarbon reservoirs than the metamorphic and igneous reservoir rocks at The Geysers geothermal field.

  1. Fracture toughness master curve characterization of Linde 1092 weld metal for Beaver valley 1 reactor

    International Nuclear Information System (INIS)

    This report summarizes the test results obtained from the Korean contribution to the integrity assessment of low toughness Beaver Valley reactor vessel by characterizing the fracture toughness of Linde 1092 (No. 305414) weld metal. 10 PCVN specimens and 10 1T-CT specimens were tested in accordance with the ASTM E 1921-97 standard, 'Standard test method for determination of reference temperature, To, for ferritic steels in the transition range'. This results can also be useful for assessment of Linde 80 low toughness welds of Kori-1

  2. Fracture toughness master curve characterization of Linde 1092 weld metal for Beaver valley 1 reactor

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Bong Sang; Yang, Won Jon; Hong, Jun Hwa

    2000-12-01

    This report summarizes the test results obtained from the Korean contribution to the integrity assessment of low toughness Beaver Valley reactor vessel by characterizing the fracture toughness of Linde 1092 (No. 305414) weld metal. 10 PCVN specimens and 10 1T-CT specimens were tested in accordance with the ASTM E 1921-97 standard, 'Standard test method for determination of reference temperature, T{sub o}, for ferritic steels in the transition range'. This results can also be useful for assessment of Linde 80 low toughness welds of Kori-1.

  3. Applied velocity versus offset (VVO) to validated & characterized fracturing zone in intra Baturaja Formation, South Sumatera Basin

    Science.gov (United States)

    Mardiyan, Hilman; Rusli, Saifatur

    2016-01-01

    The velocity versus offset (VVO) as new geophysical method can be applied to detect some geological phenomenon, such as hydrocarbon trap, structural-fracture anomaly, facies changes, etc. The VVO method is data driven, based on the normal move out equation (NMO) and measuring the local event correlation between adjacent traces to get velocity gradient attributes which is derived from cross-plotting the velocity versus offset (VVO). This paper is describing applied VVO model that controlled by well data which indicated fracture from logs data, especially Resistivity Imager Logs or Formation Micro Imager (FMI). Images FMI logs data at Intra-Baturaja Carbonate Formation (BRF) in South Palembang Sub-basin (SPB), South Sumatera, shows vugs with fractures which orientation is roughly NNW-SSE. Meanwhile, the 2D NMO seismic gathers indicated those all as hockey stick at far offset. By applying VVO method, hockey stick can be identified and then used to validated, characterized and localized where the fracturing zone in intra-Baturaja Formation is. Laterally, VVO quantified as velocity gradient attribute which associated with geological model as the fracturing zone in study area. Characterization fracturing zone in Intra Baturaja Formation as geological lateral model by design is a challenging task for most exploration and production. In term of exploration where limited data is available, it can be used step ahead as carbonate fracture reservoir candidate in proven area and adjacent, especially in SPB South Sumatra.

  4. Fracture Characterization in Enhanced Geothermal Systems by Wellbore and Reservoir Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Horne, Roland N.; Li, Kewen; Alaskar, Mohammed; Ames, Morgan; Co, Carla; Juliusson, Egill; Magnusdottir, Lilja

    2012-06-30

    This report highlights the work that was done to characterize fractured geothermal reservoirs using production data. That includes methods that were developed to infer characteristic functions from production data and models that were designed to optimize reinjection scheduling into geothermal reservoirs, based on these characteristic functions. The characterization method provides a robust way of interpreting tracer and flow rate data from fractured reservoirs. The flow-rate data are used to infer the interwell connectivity, which describes how injected fluids are divided between producers in the reservoir. The tracer data are used to find the tracer kernel for each injector-producer connection. The tracer kernel describes the volume and dispersive properties of the interwell flow path. A combination of parametric and nonparametric regression methods were developed to estimate the tracer kernels for situations where data is collected at variable flow-rate or variable injected concentration conditions. The characteristic functions can be used to calibrate thermal transport models, which can in turn be used to predict the productivity of geothermal systems. This predictive model can be used to optimize injection scheduling in a geothermal reservoir, as is illustrated in this report.

  5. Hydrogeloogic characterization of fractured rock formations: A guide for groundwater remediators

    International Nuclear Information System (INIS)

    A field site was developed in the foothills of the Sierra Nevada, California to develop and test a multi-disciplinary approach to the characterization of ground water flow and transport in fractured rocks. Nine boreholes were drilled into the granitic bedrock, and a wide variety of new and traditional subsurface characterization tools were implemented. The hydrogeologic structure and properties of the field site were deduced by integrating results from the various geologic, geophysical, hydrologic, and other investigative methods. The findings of this work are synthesized into this report, which is structured in a guidebook format. The applications of the new and traditional technologies, suggestions on how best to use, integrate, and analyze field data, and comparisons of the shortcoming and benefits of the different methods are presented

  6. Hydrogeloogic characterization of fractured rock formations: A guide for groundwater remediators

    Energy Technology Data Exchange (ETDEWEB)

    Cohen, A.J.B.

    1995-10-01

    A field site was developed in the foothills of the Sierra Nevada, California to develop and test a multi-disciplinary approach to the characterization of ground water flow and transport in fractured rocks. Nine boreholes were drilled into the granitic bedrock, and a wide variety of new and traditional subsurface characterization tools were implemented. The hydrogeologic structure and properties of the field site were deduced by integrating results from the various geologic, geophysical, hydrologic, and other investigative methods. The findings of this work are synthesized into this report, which is structured in a guidebook format. The applications of the new and traditional technologies, suggestions on how best to use, integrate, and analyze field data, and comparisons of the shortcoming and benefits of the different methods are presented.

  7. Cross-borehole flow analysis to characterize fracture connections in the Melechov Granite, Bohemian-Moravian Highland, Czech Republic

    Science.gov (United States)

    Paillet, Frederick L.; Williams, John H.; Urik, Joseph; Lukes, Joseph; Kobr, Miroslav; Mares, Stanislav

    2012-01-01

    Application of the cross-borehole flow method, in which short pumping cycles in one borehole are used to induce time-transient flow in another borehole, demonstrated that a simple hydraulic model can characterize the fracture connections in the bedrock mass between the two boreholes. The analysis determines the properties of fracture connections rather than those of individual fractures intersecting a single borehole; the model contains a limited number of adjustable parameters so that any correlation between measured and simulated flow test data is significant. The test was conducted in two 200-m deep boreholes spaced 21 m apart in the Melechov Granite in the Bohemian-Moravian Highland, Czech Republic. Transient flow was measured at depth stations between the identified transmissive fractures in one of the boreholes during short-term pumping and recovery periods in the other borehole. Simulated flows, based on simple model geometries, closely matched the measured flows. The relative transmissivity and storage of the inferred fracture connections were corroborated by tracer testing. The results demonstrate that it is possible to assess the properties of a fracture flow network despite being restricted to making measurements in boreholes in which a local population of discrete fractures regulates the hydraulic communication with the larger-scale aquifer system.

  8. Characterization of freeze-fractured epithelial plasma membranes on nanometer scale with ToF-SIMS.

    Science.gov (United States)

    Draude, Felix; Körsgen, Martin; Pelster, Andreas; Schwerdtle, Tanja; Müthing, Johannes; Arlinghaus, Heinrich F

    2015-03-01

    Time-of-flight secondary ion mass spectrometry (ToF-SIMS) was used to characterize the freeze-fracturing process of human epithelial PANC-1 and UROtsa cells. For this purpose, phosphatidylcholine, sphingomyelin, phosphatidylethanolamine, and phosphatidylserine standard samples were investigated to find specific signals with both high specificity and signal intensity. The results were used to investigate single cells of subconfluent cell layers prepared with a special silicon wafer sandwich preparation technique. This freeze-fracturing technique strips cell membranes off the cells, isolating them on opposing silicon wafer substrates. Criteria were found for defining regions with stripped off cell membranes and, on the opposing wafer, complementary regions with the remaining cells. Measured ethanolamine/choline and serine/choline ratios in these regions clearly showed that in the freeze-fracturing process, the lipid bilayer of the plasma membrane is split along its central zone. Accordingly, only the outer lipid monolayer is stripped off the cell, while the inner lipid monolayer remains attached to the cell on the opposing wafer, thus allowing detailed analysis of a single lipid monolayer. Furthermore, it could be shown that using different washing procedures did not influence the transmembrane lipid distribution. Under optimized preparation conditions, it became feasible to detect lipids with a lateral resolution of approximately 100 nm. The data indicate that ToF-SIMS would be a very useful technique to study with very high lateral resolution changes in lipid composition caused, for example, by lipid storage diseases or pharmaceuticals that interfere with the lipid metabolism.

  9. The bedrock geology and fracture characterization of the Maynard quadrangle of eastern Massachusetts

    Science.gov (United States)

    Arvin, Tracey A.

    The bedrock geology of the Maynard quadrangle of east-central Massachusetts was examined through field and petrographic studies and mapped at a scale of 1:24,000. The quadrangle spans much of the Nashoba terrane and a small area of the Avalon terrane. Two stratigraphic units were defined in the Nashoba terrane: the Cambrian to Ordovician Marlboro Formation and the Ordovician Nashoba Formation. In addition, four igneous units were defined in the Nashoba terrane: the Silurian to Ordovician phases of the Andover Granite, the Silurian to Devonian Assabet Quartz Diorite, the Silurian to Devonian White Pond Diorites (new name), and the Mississippian Indian Head Hill Igneous Complex. In the Avalon terrane, one stratigraphic unit was defined as the Proterozoic Z Westboro Formation Mylonites, and one igneous unit was defined as the Proterozoic Z to Devonian Sudbury Valley Igneous Complex. Two major faults were identified: the intra-terrane Assabet River fault zone in the central part of the quadrangle, and the south-east Nashoba terrane bounding Bloody Bluff fault zone. Petrofabric studies on fault rocks in two areas indicated final motion in those areas: the sheared Marlboro Formation amphibolites indicated dextral transpressive NW over SE motion, and the Westboro Formation Mylonites indicated sinistral strike-slip motion. Fracture characterization of entire quadrangle where attributes (orientation, trace length, spacing, and termination) of fractures and joints were used to identify dominant sets of fractures that affect the transmissivity and storage of groundwater. Orientations of SW -- NE are dominant throughout the quadrangle and consistent with regional trend.

  10. Tensile fracture and thermal conductivity characterization of toughened epoxy/CNT nanocomposites

    Energy Technology Data Exchange (ETDEWEB)

    Balakrishnan, Anandh [School of Aerospace and Mechanical Engineering, University of Oklahoma, Norman, OK 73019 (United States); Saha, Mrinal C., E-mail: msaha@ou.edu [School of Aerospace and Mechanical Engineering, University of Oklahoma, Norman, OK 73019 (United States)

    2011-01-25

    Rubber toughened epoxy/CNT nanocomposites were manufactured at different weight percents between 0 and 1% of multiwall carbon nanotube (MWNT) using a high intensity ultrasonic liquid processor with a titanium probe. Mechanical properties of manufactured dog bone samples were measured in tension and the results indicated a maximum of 23% increase in the elastic modulus at 0.6% by weight of MWNT. However, the fracture strength showed a maximum decrease of about 11% as a function of increasing MWNT loading. Scanning Electron Microscopy (SEM) images from the neat samples revealed a distinct circular pit at the top left edge of the specimen with an overall tearing deformation causing the fracture paths. Comparatively, all nanocomposite samples on an average seemed to show a prominent brittle fracture with little or no evidence of circular pit formation. The amount of tearing deformation seemed to be enhanced in the nanocomposite specimens as compare to the neat ones. Finally, Transmission Electron Microscopy images indicated that different states of dispersion exist in all of the nanocomposite samples. The data showed that agglomeration of nanotubes increases as a function of weight percent. In addition to mechanical property characterization, thermal conductivity of all the samples was determined as a function of temperature between 30 deg. C and 100 deg. C using the 3{omega} method. The tested samples showed an almost 16% increase in thermal conductivity. The minimal enhancement in thermal conductivity has been analyzed from the standpoint of the Effective Medium Theory. Interfacial thermal resistances exhibit no order of magnitude changes explaining the conductivity results.

  11. GEOTECHNICAL/GEOCHEMICAL CHARACTERIZATION OF ADVANCED COAL PROCESS WASTE STREAMS

    Energy Technology Data Exchange (ETDEWEB)

    Edwin S. Olson; Charles J. Moretti

    1999-11-01

    Thirteen solid wastes, six coals and one unreacted sorbent produced from seven advanced coal utilization processes were characterized for task three of this project. The advanced processes from which samples were obtained included a gas-reburning sorbent injection process, a pressurized fluidized-bed coal combustion process, a coal-reburning process, a SO{sub x}, NO{sub x}, RO{sub x}, BOX process, an advanced flue desulfurization process, and an advanced coal cleaning process. The waste samples ranged from coarse materials, such as bottom ashes and spent bed materials, to fine materials such as fly ashes and cyclone ashes. Based on the results of the waste characterizations, an analysis of appropriate waste management practices for the advanced process wastes was done. The analysis indicated that using conventional waste management technology should be possible for disposal of all the advanced process wastes studied for task three. However, some wastes did possess properties that could present special problems for conventional waste management systems. Several task three wastes were self-hardening materials and one was self-heating. Self-hardening is caused by cementitious and pozzolanic reactions that occur when water is added to the waste. All of the self-hardening wastes setup slowly (in a matter of hours or days rather than minutes). Thus these wastes can still be handled with conventional management systems if care is taken not to allow them to setup in storage bins or transport vehicles. Waste self-heating is caused by the exothermic hydration of lime when the waste is mixed with conditioning water. If enough lime is present, the temperature of the waste will rise until steam is produced. It is recommended that self-heating wastes be conditioned in a controlled manner so that the heat will be safely dissipated before the material is transported to an ultimate disposal site. Waste utilization is important because an advanced process waste will not require

  12. Advanced Conceptual Models for Unsaturated and Two-Phase Flow in Fractured Rock

    Energy Technology Data Exchange (ETDEWEB)

    Harihar Rajaram; Robert J. Glass; Michael J. Nicholl; Thomas R. Wood

    2007-06-24

    The Department of Energy Environmental Management Program is faced with two major issues involving two-phase flow in fractured rock; specifically, transport of dissolved contaminants in the Vadose Zone, and the fate of Dense Nonaqueous Phase Liquids (DNAPLs) below the water table. Conceptual models currently used to address these problems do not correctly include the influence of the fractures, thus leading to erroneous predictions. Recent work has shown that it is crucial to understand the topology, or 'structure' of the fluid phases (air/water or water/DNAPL) within the subsurface.

  13. Recent Advances in the Molecular Characterization of Circulating Tumor Cells

    Energy Technology Data Exchange (ETDEWEB)

    Lowes, Lori E. [London Regional Cancer Program, London Health Sciences Centre, London, ON N6A 4L6 (Canada); Department of Anatomy and Cell Biology, Schulich School of Medicine and Dentistry, Western University, London, ON N6A 5C1 (Canada); Department of Oncology, Schulich School of Medicine and Dentistry, Western University, London, ON N6A 4L6 (Canada); Allan, Alison L., E-mail: alison.allan@lhsc.on.ca [London Regional Cancer Program, London Health Sciences Centre, London, ON N6A 4L6 (Canada); Department of Anatomy and Cell Biology, Schulich School of Medicine and Dentistry, Western University, London, ON N6A 5C1 (Canada); Department of Oncology, Schulich School of Medicine and Dentistry, Western University, London, ON N6A 4L6 (Canada); Lawson Health Research Institute, London, ON N6C 2R5 (Canada)

    2014-03-13

    Although circulating tumor cells (CTCs) were first observed over a century ago, lack of sensitive methodology precluded detailed study of these cells until recently. However, technological advances have now facilitated the identification, enumeration, and characterization of CTCs using a variety of methods. The majority of evidence supporting the use of CTCs in clinical decision-making has been related to enumeration using the CellSearch{sup ®} system and correlation with prognosis. Growing evidence also suggests that CTC monitoring can provide an early indication of patient treatment response based on comparison of CTC levels before and after therapy. However, perhaps the greatest potential that CTCs hold for oncology lies at the level of molecular characterization. Clinical treatment decisions may be more effective if they are based on molecular characteristics of metastatic cells rather than on those of the primary tumor alone. Molecular characterization of CTCs (which can be repeatedly isolated in a minimally invasive fashion) provides the opportunity for a “real-time liquid biopsy” that allows assessment of genetic drift, investigation of molecular disease evolution, and identification of actionable genomic characteristics. This review focuses on recent advances in this area, including approaches involving immunophenotyping, fluorescence in situ hybridization (FISH), multiplex RT-PCR, microarray, and genomic sequencing.

  14. An Integrated Approach to Characterizing Bypassed Oil in Heterogeneous and Fractured Reservoirs Using Partitioning Tracers

    Energy Technology Data Exchange (ETDEWEB)

    Akhil Datta-Gupta

    2006-08-01

    This report presents an efficient trajectory-based approach to integrate transient pressure data into high-resolution reservoir and aquifer models. The method involves alternating travel time and peak amplitude matching of pressure response using inverse modeling and is particularly well-suited for high resolution subsurface characterization using hydraulic tomography or pressure interference tests. Compared to travel time inversion only, our proposed approach results in a significantly improved match of the pressure response at the wells and also better estimates of subsurface properties. This is accomplished with very little increase in computational cost. Utilizing the concept of a ''diffusive'' time of flight derived from an asymptotic solution of the diffusivity equation, we develop analytical approaches to estimate the sensitivities for travel time and peak amplitude of pressure response to subsurface properties. The sensitivities are then used in an iterative least-squared minimization to match the pressure data. We illustrate our approach using synthetic and field examples. In the field application at a fractured limestone formation, the predominant fracture patterns emerging from the inversion are shown to be consistent with independent geophysical experiments and borehole data.

  15. Advanced airborne geophysics for site and watershed characterization and remediation

    Energy Technology Data Exchange (ETDEWEB)

    Brown, B.; Hodges, G. [Fugro Airborne Surveys, Mississauga, ON (Canada)

    2007-04-01

    Airborne geophysics systems now have the ability to make accurately map the conductivity of the earth's subsurface. This article provided details of various site characterization surveys conducted using helicopter electromagnetic (HEM) surveys. Recent improvements in computer software, the use of global positioning systems (GPS), lasers, and fiber optics have increased the ability of HEM systems to accurately map ground conditions. Airborne electromagnetic survey techniques were used to characterize the geological features and lithology of the Sulphur Bank Mercury Mine (SBMM) on the eastern shore of Clear Lake in California. Natural conduits for the movement of groundwater were identified. Data showed that acidic water and mercury from the mine were contaminating the lake. The data showed good agreement with results obtained from previous conventional geologic and hydrologic investigations. HEM surveys were also used to characterize conductive mine pools and groundwater plumes at areas in the eastern United States that contained abandoned surface and underground coal mines. HEM was used to delineate source areas and flow paths for acidic, metal-containing groundwater, and data obtained from the surveys were used to plan mitigation activities. The survey identified 11 mine pools, as well as flooded workings that had previously not been mapped. HEM surveys were also used to map water-bearing fractures in areas of crystalline bedrock in drought-ridden regions in Brazil. Information from the surveys was used to locate drill targets for water wells. A test survey was used to identify wellheads leaking methane in a privately-owned gas field in Wyoming. Five methane leakage plumes were detected as a result of the survey. HEM geophysical surveys have also been used to map conductivity variations due to changes in water salinity at the Biscayne aquifer in the Florida everglades. It was concluded that airborne and HEM surveys provide significant cost savings when

  16. Energy dissipation and contour integral characterizing fracture behavior of incremental plasticity

    Institute of Scientific and Technical Information of China (English)

    Qi-Lin He; Lin-Zhi Wu; Ming Li; Hong-Bo Chen

    2011-01-01

    Jep-integral is derived for characterizing the fracture behavior of elastic-plastic materials. The Jep-integral differs from Rice's J-integral in that the free energy density rather than the stress working density is employed to define energy-momentum tensor. The Jep-integral is proved to be path-dependent regardless of incremental plasticity and deformation plasticity. The Jep-integral possesses clearly clear physical meaning: (1) the value Jeptjp evaluated on the infinitely small contour surrounding the crack tip represents the crack tip energy dissipation; (2) when the global steadystate crack growth condition is approached, the value of Jepfar-ss calculated along the boundary contour equals to the sum of crack tip dissipation and bulk dissipation of plastic zone. The theoretical results are verified by simulating mode I crack problems.

  17. Unsaturated fractured rock characterization methods and data sets at the Apache Leap Tuff Site

    Energy Technology Data Exchange (ETDEWEB)

    Rasmussen, T.C.; Evans, D.D.; Sheets, P.J.; Blanford, J.H. [Arizona Univ., Tucson, AZ (USA). Dept. of Hydrology and Water Resources

    1990-08-01

    Performance assessment of high-level nuclear waste containment feasibility requires representative values of parameters as input, including parameter moments, distributional characteristics, and covariance structures between parameters. To meet this need, characterization methods and data sets for interstitial, hydraulic, pneumatic and thermal parameters for a slightly welded fractured tuff at the Apache Leap Tuff Site situated in central Arizona are reported in this document. The data sets include the influence of matric suction on measured parameters. Spatial variability is investigated by sampling along nine boreholes at regular distances. Laboratory parameter estimates for 105 core segments are provided, as well as field estimates centered on the intervals where the core segments were collected. Measurement uncertainty is estimated by repetitively testing control samples. 31 refs., 10 figs., 21 tabs.

  18. Unsaturated fractured rock characterization methods and data sets at the Apache Leap Tuff Site

    International Nuclear Information System (INIS)

    Performance assessment of high-level nuclear waste containment feasibility requires representative values of parameters as input, including parameter moments, distributional characteristics, and covariance structures between parameters. To meet this need, characterization methods and data sets for interstitial, hydraulic, pneumatic and thermal parameters for a slightly welded fractured tuff at the Apache Leap Tuff Site situated in central Arizona are reported in this document. The data sets include the influence of matric suction on measured parameters. Spatial variability is investigated by sampling along nine boreholes at regular distances. Laboratory parameter estimates for 105 core segments are provided, as well as field estimates centered on the intervals where the core segments were collected. Measurement uncertainty is estimated by repetitively testing control samples. 31 refs., 10 figs., 21 tabs

  19. Characterization and Quantification of Pneumatic Fracturing Effects at a Clay Till Site

    DEFF Research Database (Denmark)

    Christiansen, Camilla Maymann; Riis, Charlotte; Christensen, Stine Brok;

    2008-01-01

    Environmental fracturing offers assistance to remediation efforts at contaminated, low-permeability sites via creation of active fracture networks, and hence, reduction of mass transport limitations set by diffusion in low-permeability matrices. A pilot study of pneumatic fracturing, focusing...... on direct documentation of fracture propagation patterns and spacing, was performed at a typical basal clay till site. The study applied a novel package of documentation methods, including injection of five tracers with different characteristics (bromide, uvitex, fluorescein, rhodamine WT, and brilliant...

  20. CHARACTERIZATION OF IN-SITU STRESS AND PERMEABILITY IN FRACTURED RESERVOIRS

    Energy Technology Data Exchange (ETDEWEB)

    Daniel R. Burns; Nafi Toksoz

    2006-03-16

    Using a 3-D finite difference method with a rotated-staggered-grid (RSG) scheme we generated synthetic seismograms for a reservoir model consisting of three horizontal layers with the middle layer containing parallel, equally spaced fractures. By separating and analyzing the backscattered signals in the FK domain, we can obtain an estimate of the fracture spacing. The fracture spacing is estimated by taking one-half of the reciprocal of the dominant wavenumber of the backscattered energy in data acquired normal to the fractures. FK analysis for fracture spacing estimation was successfully applied to these model results, with particular focus on PS converted waves. The method was then tested on data from the Emilio Field. The estimated fracture spacing from the dominant wavenumber values in time windows at and below the reservoir level is 25-40m. A second approach for fracture spacing estimation is based on the observation that interference of forward and backscattered energy from fractures introduces notches in the frequency spectra of the scattered wavefield for data acquired normal to the fracture strike. The frequency of these notches is related to the spacing of the fractures. This Spectral Notch Method was also applied to the Emilio data, with the resulting range of fracture spacing estimates being 25-50m throughout the field. The dominant spacing fracture spacing estimate is about 30-40 m, which is very similar to the estimates obtained from the FK method.

  1. Multicomponent, three-dimensional seismic characterization of a fractured coalbed methane reservoir, Cedar Hill Field, San Juan County, New Mexico

    Energy Technology Data Exchange (ETDEWEB)

    Shuck, E.L.

    1993-01-01

    Methane is produced from fractured coalbed reservoirs at Cedar Hill field in the San Juan basin. Fracturing and local stress are critical to production due to the absence of matrix permeability in the coals. Knowledge of the direction of open fractures, the degree of fracturing, reservoir pressure and compartmentalization is required to understand the flow of fluids through the reservoir. A multicomponent 3-D seismic survey was acquired to aid in coalbed methane reservoir characterization. Coalbed reservoir heterogeneities, including isolated pressure cells, zones of increased fracture density, and variable fracture directions, have been identified through the analysis of the multicomponent data and integration with petro-physical and reservoir engineering studies. Strike-slip faults, which compartmentalize the reservoir, have been identified by structural interpretation of the 3-D P-wave seismic data. These faults form boundaries for pressure cells which have been identified by P-wave reflection amplitude anomalies. The analysis of polarizations, traveltimes, and reflection amplitudes from the shear-wave seismic data has allowed the identification of zones of variable fracture direction and fracture density. There is good agreement between stresses inferred from the structural interpretation and those indicated by the shear-wave polarizations. Reflection amplitudes have been calibrated to seismic velocities and reservoir pressures through the use of petrophysical data taken from core samples. Shear-wave anisotropy has been quantified over the reservoir zone using both traveltime and thin-bed reflection response with excellent agreement between the two methods. Crack densities computed from the anisotropy show two regions of high crack density, one coinciding with a sealed overpressured cell, and the other partially drained by a producing well. This indicates potential for monitoring the production of coalbed methane reservoirs using multicomponent seismology.

  2. Implementing ground surface deformation tools to characterize field-scale properties of a fractured aquifer during a short hydraulic test

    Science.gov (United States)

    Schuite, Jonathan; Longuevergne, Laurent; Bour, Olivier; Boudin, Frédérick; Durand, Stéphane

    2016-04-01

    In naturally fractured reservoirs, fluid flow is governed by the structural and hydromechanical properties of fracture networks or conductive fault zones. In order to ensure a sustained exploitation of resources or to assess the safety of underground storage, it is necessary to evaluate these properties. As they generally form highly heterogeneous and anisotropic reservoirs, fractured media may be well characterized by means of several complementary experimental methods or sounding techniques. In this framework, the observation of ground deformation has been proved useful to gain insight of a fractured reservoir's geometry and hydraulic properties. Commonly, large conductive structures like faults can be studied from surface deformation from satellite methods at monthly time scales, whereas meter scale fractures have to be examined under short-term in situ experiments using high accuracy intruments like tiltmeters or extensometers installed in boreholes or at the ground's surface. To the best of our knowledge, the feasability of a field scale (~ 100 m) characterization of a fractured reservoir with geodetic tools in a short term experiment has not yet been addressed. In the present study, we implement two complementary ground surface geodetic tools, namely tiltmetry and optical leveling, to monitor the deformation induced by a hydraulic recovery test at the Ploemeur hydrological observatory (France). Employing a simple purely elastic modeling approach, we show that the joint use of time constraining data (tilt) and spatially constraining data (vertical displacement) makes it possible to evaluate the geometry (dip, root depth and lateral extent) and the storativity of a hydraulically active fault zone, in good agreement with previous studies. Hence we demonstrate that the adequate use of two complementary ground surface deformation methods offer a rich insight of large conductive structure's properties using a single short term hydraulic load. Ground surface

  3. Fracture characterization of flysch formation by terrestrial digital photogrammetry: an example in the Antola Formation (upper Staffora Valley, Italy)

    Science.gov (United States)

    Meisina, Claudia; Menegoni, Niccolò; Perotti, Cesare

    2016-04-01

    Geomechanical characterization of flysch formations plays an important role for its implication in slope stability and fluids circulation, especially in Apenninic areas. The Antola Formation of Upper Cretaceous age crops out extensively in the Northern Apennines and provides an important case of study. It consists of turbiditic graded units of calcareous sandstones, sandstones, marlstones, and shales and is interpreted as a deep-sea basin plain deposit, with lateral facies variations which range from proximal, thick-bedded turbidities to distal turbidites that show predominantly thickening upward cycles and have a high percentage of shale. It is in general characterized by folds developed in absence of metamorphism and a usually high degree of fracturation. The presence of well developed fracture networks enhances circulation of fluid and therefore alteration of the less competent layers causing problems of slope stability. Fracture characterization of Antola Formation based on field survey is very time consuming and often limited by the insufficient availability and inaccessibility of outcrops. For this reason, terrestrial remote sensing and in particular terrestrial digital photogrammetry has been applied to investigate the geomechanical features of the formation in the upper Staffora Valley (Northern Italy). Digital photogrammetry allows to generate by Structure from Motion (SfM) technique a 3D point cloud that represents the Digital Outcrop Model (DOM). New technologies allow to associate appropriate texture to the point cloud from the images, in order to preserve important visual information. The analysis of several textured 3D DOMs allows to digitally acquire a large amount of data on discontinuities parameters such as orientation, spacing, aperture, persistence and filling, in order to better characterize the rock mass. Some tests performed by field survey data acquisition to validate the digitally collected data, gave positive results, showing differences

  4. Advanced Reservoir Characterization in the Antelope Shale to Establish the Viability of CO2 Enhanced Oil Recovery in California's Monterey Formation Siliceous Shales

    International Nuclear Information System (INIS)

    The primary objective of this research is to conduct advanced reservoir characterization and modeling studies in the Antelope Shale reservoir. Characterization studies will be used to determine the technical feasibility of implementing a CO2 enhanced oil recovery project in the Antelope Shale in Buena Vista Hills Field. The Buena Vista Hills pilot CO2 project will demonstrate the economic viability and widespread applicability of CO2 flooding in fractured siliceous shale reservoirs of the San Joaquin Valley. The research consists of four primary work processes: (1) Reservoir Matrix and Fluid Characterization; (2) Fracture characterization; (3) reservoir Modeling and Simulation; and (4) CO2 Pilot Flood and Evaluation. Work done in these areas is subdivided into two phases or budget periods. The first phase of the project will focus on the application of a variety of advanced reservoir characterization techniques to determine the production characteristics of the Antelope Shale reservoir. Reservoir models based on the results of the characterization work will be used to evaluate how the reservoir will respond to secondary recovery and EOR processes. The second phase of the project will include the implementation and evaluation of an advanced enhanced oil recovery (EOR) pilot in the United Anticline (West Dome) of the Buena Vista Hills Field

  5. CHARACTERIZATION OF IN-SITU STRESS AND PERMEABILITY IN FRACTURED RESERVOIRS

    Energy Technology Data Exchange (ETDEWEB)

    Daniel R. Burns; M. Nafi Toksoz

    2004-07-19

    Expanded details and additional results are presented on two methods for estimating fracture orientation and density in subsurface reservoirs from scattered seismic wavefield signals. In the first, fracture density is estimated from the wavenumber spectra of the integrated amplitudes of the scattered waves as a function of offset in pre-stack data. Spectral peaks correctly identified the 50m, 35m, and 25m fracture spacings from numerical model data using a 40Hz source wavelet. The second method, referred to as the Transfer Function-Scattering Index Method, is based upon observations from 3D finite difference modeling that regularly spaced, discrete vertical fractures impart a ringing coda-type signature to any seismic energy that is transmitted through or reflected off of them. This coda energy is greatest when the acquisition direction is parallel to the fractures, the seismic wavelengths are tuned to the fracture spacing, and when the fractures have low stiffness. The method uses surface seismic reflection traces to derive a transfer function, which quantifies the change in an apparent source wavelet propagating through a fractured interval. The transfer function for an interval with low scattering will be more spike-like and temporally compact. The transfer function for an interval with high scattering will ring and be less temporally compact. A Scattering Index is developed based on a time lag weighting of the transfer function. When a 3D survey is acquired with a full range of azimuths, the Scattering Index allows the identification of subsurface areas with high fracturing and the orientation (or strike) of those fractures. The method was calibrated with model data and then applied to field data from a fractured reservoir giving results that agree with known field measurements. As an aid to understanding the scattered wavefield seen in finite difference models, a series of simple point scatterers was used to create synthetic seismic shot records collected over

  6. Recent advances in the treatment of hip fractures in the elderly.

    Science.gov (United States)

    Rozell, Joshua C; Hasenauer, Mark; Donegan, Derek J; Neuman, Mark

    2016-01-01

    The treatment of hip fractures in the elderly represents a major public health priority and a source of ongoing debate among orthopaedic surgeons and anesthesiologists. Most of these injuries are treated with surgery in an expedient fashion. From the surgical perspective, there are certain special considerations in this population including osteoporosis, pre-existing arthritis, age, activity level, and overall health that contribute to the type of surgical fixation performed. Open reduction and internal fixation versus arthroplasty remain the two major categories of treatment. While the indications and treatment algorithms still remain controversial, the overall goal for these patients is early mobilization and prevention of morbidity and mortality. The use of preoperative, regional anesthesia has aided in this effort. The purpose of this review article is to examine the various treatment modalities for hip fractures in the elderly and discuss the most recent evidence in the face of a rapidly aging population. PMID:27547384

  7. Mask characterization for CDU budget breakdown in advanced EUV lithography

    Science.gov (United States)

    Nikolsky, Peter; Strolenberg, Chris; Nielsen, Rasmus; Nooitgedacht, Tjitte; Davydova, Natalia; Yang, Greg; Lee, Shawn; Park, Chang-Min; Kim, Insung; Yeo, Jeong-Ho

    2012-11-01

    As the ITRS Critical Dimension Uniformity (CDU) specification shrinks, semiconductor companies need to maintain a high yield of good wafers per day and a high performance (and hence market value) of finished products. This cannot be achieved without continuous analysis and improvement of on-product CDU as one of the main drivers for process control and optimization with better understanding of main contributors from the litho cluster: mask, process, metrology and scanner. In this paper we will demonstrate a study of mask CDU characterization and its impact on CDU Budget Breakdown (CDU BB) performed for an advanced EUV lithography with 1D and 2D feature cases. We will show that this CDU contributor is one of the main differentiators between well-known ArFi and new EUV CDU budgeting principles. We found that reticle contribution to intrafield CDU should be characterized in a specific way: mask absorber thickness fingerprints play a role comparable with reticle CDU in the total reticle part of the CDU budget. Wafer CD fingerprints, introduced by this contributor, may or may not compensate variations of mask CD's and hence influence on total mask impact on intrafield CDU at the wafer level. This will be shown on 1D and 2D feature examples in this paper. Also mask stack reflectivity variations should be taken into account: these fingerprints have visible impact on intrafield CDs at the wafer level and should be considered as another contributor to the reticle part of EUV CDU budget. We observed also MEEF-through-field fingerprints in the studied EUV cases. Variations of MEEF may also play a role for the total intrafield CDU and may be taken into account for EUV Lithography. We characterized MEEF-through-field for the reviewed features, the results to be discussed in our paper, but further analysis of this phenomenon is required. This comprehensive approach to characterization of the mask part of EUV CDU characterization delivers an accurate and integral CDU Budget

  8. Characterization of In-Situ Stress and Permeability in Fractured Reservoirs

    Energy Technology Data Exchange (ETDEWEB)

    Daniel R. Burns; M. Nafi Toksoz

    2006-06-30

    Fracture orientation and spacing are important parameters in reservoir development. This project resulted in the development and testing of a new method for estimating fracture orientation and two new methods for estimating fracture spacing from seismic data. The methods developed were successfully applied to field data from fractured carbonate reservoirs. Specific results include: the development a new method for estimating fracture orientation from scattered energy in seismic data; the development of two new methods for estimating fracture spacing from scattered energy in seismic data; the successful testing of these methods on numerical model data and field data from two fractured carbonate reservoirs; and the validation of fracture orientation results with borehole data from the two fields. Researchers developed a new method for determining the reflection and scattering characteristics of seismic energy from subsurface fractured formations. The method is based upon observations made from 3D finite difference modeling of the reflected and scattered seismic energy over discrete systems of vertical fractures. Regularly spaced, discrete vertical fractures impart a ringing coda type signature to seismic energy that is transmitted through or reflected off of them. This signature varies in amplitude and coherence as a function of several parameters including: (1) the difference in angle between the orientation of the fractures and the acquisition direction, (2) the fracture spacing, (3) the wavelength of the illuminating seismic energy, and (4) the compliance, or stiffness, of the fractures. This coda energy is the most coherent when the acquisition direction is parallel to the strike of the fractures. It has the largest amplitude when the seismic wavelengths are tuned to the fracture spacing, and when the fractures have low stiffness. The method uses surface seismic reflection traces to derive a transfer function that quantifies the change in the apparent source

  9. Verification and characterization of continuum behavior of fractured rock at AECL Underground Research Laboratory

    International Nuclear Information System (INIS)

    The purposes of this study are to determine when a fracture system behaves as a porous medium and what the corresponding permeability tensor is. A two-dimensional fracture system model is developed with density, size, orientation, and location of fractures in an impermeable matrix as random variables. Simulated flow tests through the models measure directional permeability, K/sub g/. Polar coordinate plots of 1/√K/sub g/, which are ellipses for equivalent anistropic homogeneous porous media, are graphed and best fit ellipses are calculated. Fracture length and areal density were varied such that fracture frequency was held constant. The examples showed the permeability increased with fracture length. The modeling techniques were applied to data from the Atomic Energy of Canada Ltd.'s Underground Research Laboratory facility in Manitoba, Canada by assuming the fracture pattern at the surface persists at depth. Well test data were used to estimate the aperture distribution by both correlating and not correlating the aperture with fracture length. The permeability of models with uncorrelated length and aperture were smaller than those for correlated models. A Monte Carlo type study showed that analysis of steady state packer tests consistently underestimate the mean aperture. Finally, a three-dimensional model in which fractures are discs randomly located in space, interactions between the fractures are line segments, and the solution of the steady state flow equations is based on image theory was discussed

  10. Integrating 3D seismic curvature and curvature gradient attributes for fracture characterization: Methodologies and interpretational implications

    Energy Technology Data Exchange (ETDEWEB)

    Gao, Dengliang

    2013-03-01

    In 3D seismic interpretation, curvature is a popular attribute that depicts the geometry of seismic reflectors and has been widely used to detect faults in the subsurface; however, it provides only part of the solutions to subsurface structure analysis. This study extends the curvature algorithm to a new curvature gradient algorithm, and integrates both algorithms for fracture detection using a 3D seismic test data set over Teapot Dome (Wyoming). In fractured reservoirs at Teapot Dome known to be formed by tectonic folding and faulting, curvature helps define the crestal portion of the reservoirs that is associated with strong seismic amplitude and high oil productivity. In contrast, curvature gradient helps better define the regional northwest-trending and the cross-regional northeast-trending lineaments that are associated with weak seismic amplitude and low oil productivity. In concert with previous reports from image logs, cores, and outcrops, the current study based on an integrated seismic curvature and curvature gradient analysis suggests that curvature might help define areas of enhanced potential to form tensile fractures, whereas curvature gradient might help define zones of enhanced potential to develop shear fractures. In certain fractured reservoirs such as at Teapot Dome where faulting and fault-related folding contribute dominantly to the formation and evolution of fractures, curvature and curvature gradient attributes can be potentially applied to differentiate fracture mode, to predict fracture intensity and orientation, to detect fracture volume and connectivity, and to model fracture networks.

  11. Geologic characterization of fractures as an aid to hydrologic modeling of the SCV block at the Stripa mine

    International Nuclear Information System (INIS)

    A series of hydrologic tests have been conducted at the Stripa research mine in Sweden to develop hydrologic characterization techniques for rock masses in which fractures form the primary flow paths. The structural studies reported here were conducted to aid in the hydrologic examination of a cubic block of granite with dimensions of 150 m on a side. This block (the SCV block) is located between the 310- and 460-m depth levels at the Stripa mine. This report describes and interprets the fracture system geology at Stripa as revealed in drift exposures, checks the interpretive model against borehole records and discusses the hydrologic implication of the model, and examines the likely effects of stress redistribution around a drift (the Validation drift) on inflow to the drift along a prominent fracture zone. (72 refs.) (au)

  12. Microstructure evolution in HAZ and suppression of Type IV fracture in advanced ferritic power plant steels

    International Nuclear Information System (INIS)

    The effect of boron and nitrogen on the microstructure evolution in heat affected zone (HAZ) of 9Cr steel during simulated heating and on the Type IV fracture in welded joints has been investigated at 650 oC. Gr.92 exhibits a significant decrease in time to rupture after thermal cycle to a peak temperature near AC3, while the creep life of Gr.92N, subjected to only normalizing but no tempering, and 9Cr-boron steel is substantially the same as that of the base metals. In Gr.92 after AC3 thermal cycle, very few precipitates are formed along PAGBs in the fine-grained microstructure. In the P92N and 9Cr-boron steel after AC3 heat cycle, on the other hand, not only PAGBs but also lath and block boundaries are covered by M23C6 carbides in the coarse-grained microstructure. It is concluded that the degradation in creep life in Gr.92 after the AC3 thermal cycle is not caused by grain refinement but that the reduction of boundary and sub-boundary hardening is the most important. Soluble boron is essential for the change in α/γ transformation behavior during heating and also for the suppression of Type IV fracture in welded joints. Newly alloy-designed 9Cr steel with 160 ppm boron and 85 ppm nitrogen exhibits much higher creep rupture strength of base metal than P92 and also no Type IV fracture in welded joints at 650 oC.

  13. Characterization of advanced polymethylmethacrylate (PMMA) targets for TNSA laser irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Torrisi, L., E-mail: Lorenzo.Torrisi@unime.it [Department of Physics and Earth Science, Messina University, V.le F.S. d’Alcontres 31, 98166 S. Agata, Messina (Italy); Cutroneo, M.; Semian, V. [Nuclear Physics Institute, ASCR, 250 68 Rez (Czech Republic); Ceccio, G. [Department of Physics and Earth Science, Messina University, V.le F.S. d’Alcontres 31, 98166 S. Agata, Messina (Italy)

    2015-10-01

    Highlights: • The manuscript presents the procedure to prepare thin advanced targets based on PMMA polymer in order to obtain high ion acceleration in laser-generated plasma. • The manuscript is original for the procedures of polymer preparation and preliminary techniques used. - Abstract: Characterization of advanced micrometric foils suitable for TNSA regime were performed using optical spectroscopy, microscopy and Nd:YAG low laser intensity. Micrometric acrylic beads were produced in polymethylmethacrylate foils through complex physical and technical procedures in order to enhance the absorption coefficient in the IR region. Moreover, Au nanoparticles were embedded in the polymer in order to induce surface plasmon resonance absorption and plasma electron density enhancement. The suitably prepared polymers were investigated at low laser intensity to have evidence of their capability to absorb IR wavelength radiations and promote enhancement of the plasma temperature and density. Results indicate that the high transparence of PMMA foils can be strongly reduced by the presences of the micrometric acrylic beads and that the obtainable laser-generated plasma improves the ion acceleration when high beads density and high Au nanoparticles concentrations are employed.

  14. Characterization of the Advanced Stirling Radioisotope Generator Engineering Unit 2

    Science.gov (United States)

    Lewandowski, Edward J.; Oriti, Salvatore M.; Schifer, Niholas A.

    2016-01-01

    Significant progress was made developing the Advanced Stirling Radioisotope Generator (ASRG) 140-W radioisotope power system. While the ASRG flight development project has ended, the hardware that was designed and built under the project is continuing to be tested to support future Stirling-based power system development. NASA Glenn Research Center recently completed the assembly of the ASRG Engineering Unit 2 (EU2). The ASRG EU2 consists of the first pair of Sunpower's Advanced Stirling Convertor E3 (ASC-E3) Stirling convertors mounted in an aluminum housing, and Lockheed Martin's Engineering Development Unit (EDU) 4 controller (a fourth-generation controller). The ASC-E3 convertors and Generator Housing Assembly (GHA) closely match the intended ASRG Qualification Unit flight design. A series of tests were conducted to characterize the EU2, its controller, and the convertors in the flight-like GHA. The GHA contained an argon cover gas for these tests. The tests included measurement of convertor, controller, and generator performance and efficiency; quantification of control authority of the controller; disturbance force measurement with varying piston phase and piston amplitude; and measurement of the effect of spacecraft direct current (DC) bus voltage on EU2 performance. The results of these tests are discussed and summarized, providing a basic understanding of EU2 characteristics and the performance and capability of the EDU 4 controller.

  15. Ratchetting behavior of advanced 9–12% chromium ferrite steel under creep–fatigue loadings: Fracture modes and dislocation patterns

    International Nuclear Information System (INIS)

    Highlights: ► Additional fatigue damage triggers the transition from ductility to brittle fracture. ► Dislocation disintegration is the main microstructural origin of premature breakdown. ► Additional fatigue damage can be ascribed to ratchetting formed in stress change. - Abstract: In order to reveal the physical mechanisms of ratchetting process under creep–fatigue loadings, following ratchetting tests in advanced 9–12% chromium ferrite steel, a study of associated fracture modes and dislocation patterns explored by scanning electron microscopy (SEM) and transmission electron microscopy (TEM) observations is presented in this paper. Two main domains were observed depending both on the peak hold time and on the stress ratio, in which the ratchetting deformation and failure mechanisms were different. These two damage domains correspond to two distinct creep–ratchetting interaction mechanisms. Particular attention was paid to the dependence of ratchetting damage behavior on the stability of dislocation substructure. In addition, an attempt is made to correlate the results of the microstructural investigations with the variations of internal stress.

  16. Fracture characterization at the Conoco Borehole Test Facility using shear-wave anisotropy

    Energy Technology Data Exchange (ETDEWEB)

    Horne, S.A. [Univ. of Edinburgh (United Kingdom); MacBeth, C.D.; Queen, J.; Rizer, W.D.

    1995-12-31

    Two multi-component near-offset VSP experiments are used, in conjunction with borehole data, to characterise the subsurface fracture system at the Conoco Borehole Test Facility, Oklahoma. Time delays between the fast and slow split shear-waves are observed to correlate with the heavily fractured sandstone formations. Inversion of the shear-wave splitting estimates is achieved using a Genetic Algorithm which incorporates an anisotropic ray tracing scheme. The inversion results suggest that the fracture orientation is sub-vertical. A method of determining fracture dip using an opposite azimuth VSP method is suggested.

  17. Experimental and computing strategies in advanced material characterization problems

    Science.gov (United States)

    Bolzon, G.

    2015-10-01

    The mechanical characterization of materials relies more and more often on sophisticated experimental methods that permit to acquire a large amount of data and, contemporarily, to reduce the invasiveness of the tests. This evolution accompanies the growing demand of non-destructive diagnostic tools that assess the safety level of components in use in structures and infrastructures, for instance in the strategic energy sector. Advanced material systems and properties that are not amenable to traditional techniques, for instance thin layered structures and their adhesion on the relevant substrates, can be also characterized by means of combined experimental-numerical tools elaborating data acquired by full-field measurement techniques. In this context, parameter identification procedures involve the repeated simulation of the laboratory or in situ tests by sophisticated and usually expensive non-linear analyses while, in some situation, reliable and accurate results would be required in real time. The effectiveness and the filtering capabilities of reduced models based on decomposition and interpolation techniques can be profitably used to meet these conflicting requirements. This communication intends to summarize some results recently achieved in this field by the author and her co-workers. The aim is to foster further interaction between engineering and mathematical communities.

  18. Experimental and computing strategies in advanced material characterization problems

    Energy Technology Data Exchange (ETDEWEB)

    Bolzon, G. [Department of Civil and Environmental Engineering, Politecnico di Milano, piazza Leonardo da Vinci 32, 20133 Milano, Italy gabriella.bolzon@polimi.it (Italy)

    2015-10-28

    The mechanical characterization of materials relies more and more often on sophisticated experimental methods that permit to acquire a large amount of data and, contemporarily, to reduce the invasiveness of the tests. This evolution accompanies the growing demand of non-destructive diagnostic tools that assess the safety level of components in use in structures and infrastructures, for instance in the strategic energy sector. Advanced material systems and properties that are not amenable to traditional techniques, for instance thin layered structures and their adhesion on the relevant substrates, can be also characterized by means of combined experimental-numerical tools elaborating data acquired by full-field measurement techniques. In this context, parameter identification procedures involve the repeated simulation of the laboratory or in situ tests by sophisticated and usually expensive non-linear analyses while, in some situation, reliable and accurate results would be required in real time. The effectiveness and the filtering capabilities of reduced models based on decomposition and interpolation techniques can be profitably used to meet these conflicting requirements. This communication intends to summarize some results recently achieved in this field by the author and her co-workers. The aim is to foster further interaction between engineering and mathematical communities.

  19. Fracture characterization by fusion of geophysical and geomechanical data: a case study from the Asmari reservoir, the Central Zagros fold-thrust belt

    International Nuclear Information System (INIS)

    Fractured reservoirs contain a large proportion of hydrocarbon reserves in the Middle East. In these types of reservoirs, a variety of fracture types and networks provide the required permeability for hydrocarbon storage and flow. Fractured reservoir characterization has been challenging to petroleum geoscientists and reservoir engineers in terms of developing new approaches in this direction. A variety of techniques have been developed in the literature to study the distribution and the impact of fracture pore types on reservoir characterization. However, such techniques are not suitable for subsurface cases where prediction of fractures become troublesome and each of the developed techniques has its own advantages and limitations. In this study, an integrated approach is proposed for fracture characterization by employing different sources of data including 3D seismic attributes, geomechanical parameters, unconventional logs (image log and nuclear magnetic response (NMR) log), velocity-deviation log (VDL), conventional well logs, and routine core analysis data. Based on the azimuths of horizontal principal stresses and natural fractures, location of the wells over the structure hanging wall is determined. Interpretation of the seismic profiles from the study area indicated a fault-related fold structure style with fault throws controlling the magnitude of curvature. Moreover, fracture distribution of the Asmari reservoir is predicted by using curvature attribute, geomechanical parameters and horizontal slices of VDL. It seems that fractures probably have a much higher distribution at zone 1 and zone 3 of the Asmari formation. (paper)

  20. Fracture characterization by fusion of geophysical and geomechanical data: a case study from the Asmari reservoir, the Central Zagros fold-thrust belt

    Science.gov (United States)

    Kosari, Ehsan; Ghareh-Cheloo, Sajjad; Kadkhodaie-Ilkhchi, Ali; Bahroudi, Abbas

    2015-02-01

    Fractured reservoirs contain a large proportion of hydrocarbon reserves in the Middle East. In these types of reservoirs, a variety of fracture types and networks provide the required permeability for hydrocarbon storage and flow. Fractured reservoir characterization has been challenging to petroleum geoscientists and reservoir engineers in terms of developing new approaches in this direction. A variety of techniques have been developed in the literature to study the distribution and the impact of fracture pore types on reservoir characterization. However, such techniques are not suitable for subsurface cases where prediction of fractures become troublesome and each of the developed techniques has its own advantages and limitations. In this study, an integrated approach is proposed for fracture characterization by employing different sources of data including 3D seismic attributes, geomechanical parameters, unconventional logs (image log and nuclear magnetic response (NMR) log), velocity-deviation log (VDL), conventional well logs, and routine core analysis data. Based on the azimuths of horizontal principal stresses and natural fractures, location of the wells over the structure hanging wall is determined. Interpretation of the seismic profiles from the study area indicated a fault-related fold structure style with fault throws controlling the magnitude of curvature. Moreover, fracture distribution of the Asmari reservoir is predicted by using curvature attribute, geomechanical parameters and horizontal slices of VDL. It seems that fractures probably have a much higher distribution at zone 1 and zone 3 of the Asmari formation.

  1. Tensile fracture characterization of braze joined copper-to-CFC coupon assemblies

    Science.gov (United States)

    Trester, P. W.; Valentine, P. G.; Johnson, W. R.; Chin, E.; Reis, E. E.; Colleraine, A. P.

    1996-10-01

    A vacuum brazing process was used to join a broad spectrum of carbon-fiber reinforced carbon matrix composite (CFC) materials, machined into cylindrical coupons, between coupons of oxygen-free copper, the braze alloy was a copper-base alloy which contained only low activation elements (Al, Si, and Ti) relative to a titanium baseline specification. This demonstration was of particular importance for plasma facing components (PFCs) under design for use in the Tokamak Physics Experiment (TPX); the braze investigation was conducted by General Atomics for the Princeton Plasma Physics Laboratory. A tensile test of each brazed assembly was conducted. The results from the braze processing, testing, and fracture characterization studies of this reporting support the use of CFC's of varied fiber architecture and matrix processing in PFC designs for TPX. Further, the copper braze alloy investigated is now considered to be a viable candidate for a low-activation bond design. The prediction of plasma disruption-induced loads on the PFCs in TPX requires that joint strength between CFC tiles and their copper substrate be considered in design analysis and CFC selection.

  2. Characterizing fractured reservoir by multicomponent reflection data and VSPs in the Paris basin

    Energy Technology Data Exchange (ETDEWEB)

    Li, Xiang-Yang; MacBeth, C.; Lefeuvre, F. [and others

    1995-12-31

    We process and interpret nine-component (9C, three component recordings of two horizontal and one vertical sources) surface seismic data and two nearby VSPs to characterize the fractured carbonate reservoir in the Dogger Formation in the Paris Basin. This is achieved by analysing differential changes in the various attributes of the vector wavefield: velocity ratios, polarizations, amplitudes and differential travel times. Careful processing is required to preserve and recover these attributes which have diagnostic anomalies associated with the Dogger formation. The interval shear-anisotropy within the Dogger shows an average of 4% with significant lateral variations, which might be interpreted as lateral changes in porosity and permeability. The differential shear-wave amplitude from the top of the Dogger shows an overall dimming. The shear-wave polarization section reveals detailed internal layering, up to six intervals, within the Dogger, which is not visible in the P-wave section. The information inferred from these wavefield attributes can be broadly correlated with the reservoir properties at the inter-well scale in Duval but with more detailed lateral variations.

  3. Characterization of fracture patterns and hygric properties for moisture flow modelling in cracked concrete

    DEFF Research Database (Denmark)

    Rouchier, Simon; Janssen, Hans; Rode, Carsten;

    2012-01-01

    Several years after their installation, building materials such as concrete present signs of ageing in the form of fractures covering a wide range of sizes, from microscopic to macroscopic cracks. All sizes of fractures can have a strong influence on heat and moisture flow in the building envelop...

  4. A synoptic approach to the seismic sensing of heterogeneous fractures: from geometric reconstruction to interfacial characterization

    CERN Document Server

    Pourahmadian, Fatemeh; Haddar, Houssem

    2016-01-01

    A non-iterative waveform sensing approach is proposed toward (i) geometric reconstruction of penetrable fractures, and (ii) quantitative identification of their heterogeneous contact condition by seismic i.e. elastic waves. To this end, the fracture support $\\Gamma$ (which may be non-planar and unconnected) is first recovered without prior knowledge of the interfacial condition by way of the recently established approaches to non-iterative waveform tomography of heterogeneous fractures, e.g. the methods of generalized linear sampling and topological sensitivity. Given suitable approximation $\\breve\\Gamma$ of the fracture geometry, the jump in the displacement field across $\\breve\\Gamma$ i.e. the fracture opening displacement (FOD) profile is computed from remote sensory data via a regularized inversion of the boundary integral representation mapping the FOD to remote observations of the scattered field. Thus obtained FOD is then used as input for solving the traction boundary integral equation on $\\breve\\Gamm...

  5. Mechanical characterization of a CO2 fractured reservoir by means of microseismicity induced by high pressure injection tests

    Science.gov (United States)

    De Simone, Silvia; Soler, Joaquim; Carrera, Jesus; Slooten, Luit Jan; Ortiz, Gema

    2014-05-01

    Reservoir characterization is an essential issue in geological storage of CO2 in Technological Development Plant (TDP). In particular, hydromechanical characterization of the caprock-reservoir system is crucial, in order to define the maximum suitable injection pressure and the in-situ mechanical properties. Thus, it is possible to conjecture the hydromechanical behavior of the system during CO2 injection. Microseismicity induced by fluid injection may be used as instruments to find out fractured reservoir properties. Indeed, the hydromechanical response is controlled by permeability (k), Young modulus (E) and Poisson ratio (ν). In caprock-reservoir systems, reservoir stiffness controls the stress transfer towards the caprock, where failure may occur. Therefore, the location of the microseismic hypocenters could give information on the reservoir stiffness. In this work we propose a simulation and calibration method of the microseismicity induced by high pressure fluid injection in a fractured reservoir. Coupled hydromechanical models are peformed. The methology is applied to a particular case study.

  6. Characterizing fractured plutonic rocks of the Canadian shield for deep geological disposal of Canada`s radioactive wastes

    Energy Technology Data Exchange (ETDEWEB)

    Lodha, G.S.; Davison, C.C.; Gascoyne, M. [Atomic Energy of Canada Ltd. , Pinawa, MB (Canada). Whiteshell Labs.

    1998-09-01

    Since 1978 AECL has been investigating plutonic rocks of the Canadian Shield as a potential medium for the disposal of Canada`s nuclear fuel waste. During the last two years this study has been continued as part of Ontario Hydro`s used fuel disposal program. Methods have been developed for characterizing the geotechnical conditions at the regional scale of the Canadian Shield as well as for characterizing conditions at the site scale and the very near-field scale needed for locating and designing disposal vault rooms and waste emplacement areas. The Whiteshell Research Area (WRA) and the Underground Research Laboratory (URL) in southeastern Manitoba have been extensively used to develop and demonstrate the different scales of characterization methods. At the regional scale, airborne magnetic and electromagnetic surveys combined with LANDSAT 5 and surface gravity survey data have been helpful in identifying boundaries of the plutonic rocks , overburden thicknesses, major lineaments that might be geological structures, lithological contacts and depths of the batholiths. Surface geological mapping of exposed rock outcrops, combined with surface VLF/EM, radar and seismic reflection surveys were useful in identifying the orientation and depth continuity of low-dipping fracture zones beneath rock outcrops to a depth of 500 to 1000 m. The surface time-domain EM method has provided encouraging results for identifying the depth of highly saline pore waters. The regional site scale investigations at the WRA included the drilling of twenty deep boreholes (> 500 m) at seven separate study areas. Geological core logging combined with borehole geophysical logging, TV/ATV logging, flowmeter logging and full waveform sonic logging in these boreholes helped to confirm the location of hydro geologically important fractures, orient cores and infer the relative permeability of some fracture zones. Single-hole radar and crosshole seismic tomography surveys were useful to establish the

  7. Advancing sensitivity analysis to precisely characterize temporal parameter dominance

    Science.gov (United States)

    Guse, Björn; Pfannerstill, Matthias; Strauch, Michael; Reusser, Dominik; Lüdtke, Stefan; Volk, Martin; Gupta, Hoshin; Fohrer, Nicola

    2016-04-01

    Parameter sensitivity analysis is a strategy for detecting dominant model parameters. A temporal sensitivity analysis calculates daily sensitivities of model parameters. This allows a precise characterization of temporal patterns of parameter dominance and an identification of the related discharge conditions. To achieve this goal, the diagnostic information as derived from the temporal parameter sensitivity is advanced by including discharge information in three steps. In a first step, the temporal dynamics are analyzed by means of daily time series of parameter sensitivities. As sensitivity analysis method, we used the Fourier Amplitude Sensitivity Test (FAST) applied directly onto the modelled discharge. Next, the daily sensitivities are analyzed in combination with the flow duration curve (FDC). Through this step, we determine whether high sensitivities of model parameters are related to specific discharges. Finally, parameter sensitivities are separately analyzed for five segments of the FDC and presented as monthly averaged sensitivities. In this way, seasonal patterns of dominant model parameter are provided for each FDC segment. For this methodical approach, we used two contrasting catchments (upland and lowland catchment) to illustrate how parameter dominances change seasonally in different catchments. For all of the FDC segments, the groundwater parameters are dominant in the lowland catchment, while in the upland catchment the controlling parameters change seasonally between parameters from different runoff components. The three methodical steps lead to clear temporal patterns, which represent the typical characteristics of the study catchments. Our methodical approach thus provides a clear idea of how the hydrological dynamics are controlled by model parameters for certain discharge magnitudes during the year. Overall, these three methodical steps precisely characterize model parameters and improve the understanding of process dynamics in hydrological

  8. CHARACTERIZATION OF IN-SITU STRESS AND PERMEABILITY IN FRACTURED RESERVOIRS

    Energy Technology Data Exchange (ETDEWEB)

    Daniel R. Burns; M. Nafi Toksoz

    2005-02-04

    Numerical modeling and field data tests are presented on the Transfer Function/Scattering Index Method for estimating fracture orientation and density in subsurface reservoirs from the ''coda'' or scattered energy in the seismic trace. Azimuthal stacks indicate that scattered energy is enhanced along the fracture strike direction. A transfer function method is used to more effectively indicate fracture orientation. The transfer function method, which involves a comparison of the seismic signature above and below a reservoir interval, effectively eliminates overburden effects and acquisition imprints in the analysis. The transfer function signature is simplified into a scattering index attribute value that gives fracture orientation and spatial variations of the fracture density within a field. The method is applied to two field data sets, a 3-D Ocean Bottom Cable (OBC) seismic data set from an offshore fractured carbonate reservoir in the Adriatic Sea and a 3-D seismic data set from an onshore fractured carbonate field in the Middle East. Scattering index values are computed in both fields at the reservoir level, and the results are compared to borehole breakout data and Formation MicroImager (FMI) logs in nearby wells. In both cases the scattering index results are in very good agreement with the well data. Field data tests and well validation will continue. In the area of technology transfer, we have made presentations of our results to industry groups at MIT technical review meetings, international technical conferences, industry workshops, and numerous exploration and production company visits.

  9. Burnout prediction using advance image analysis coal characterization techniques

    Energy Technology Data Exchange (ETDEWEB)

    Edward Lester; Dave Watts; Michael Cloke [University of Nottingham, Nottingham (United Kingdom). School of Chemical Environmental and Mining Engineering

    2003-07-01

    The link between petrographic composition and burnout has been investigated previously by the authors. However, these predictions were based on 'bulk' properties of the coal, including the proportion of each maceral or the reflectance of the macerals in the whole sample. Combustion studies relating burnout with microlithotype analysis, or similar, remain less common partly because the technique is more complex than maceral analysis. Despite this, it is likely that any burnout prediction based on petrographic characteristics will become more accurate if it includes information about the maceral associations and the size of each particle. Chars from 13 coals, 106-125 micron size fractions, were prepared using a Drop Tube Furnace (DTF) at 1300{degree}C and 200 millisecond and 1% Oxygen. These chars were then refired in the DTF at 1300{degree}C 5% oxygen and residence times of 200, 400 and 600 milliseconds. The progressive burnout of each char was compared with the characteristics of the initial coals. This paper presents an extension of previous studies in that it relates combustion behaviour to coals that have been characterized on a particle by particle basis using advanced image analysis techniques. 13 refs., 7 figs.

  10. High temperature material characterization and advanced materials development

    Energy Technology Data Exchange (ETDEWEB)

    Ryu, Woo Seog; Kim, D. H.; Kim, S. H. and others

    2005-03-15

    The study is to characterize the structural materials under the high temperature, one of the most significant environmental factors in nuclear systems. And advanced materials are developed for high temperature and/or low activation in neutron irradiation. Tensile, fatigue and creep properties have been carried out at high temperature to evaluate the mechanical degradation. Irradiation tests were performed using the HANARO. The optimum chemical composition and heat treatment condition were determined for nuclear grade 316NG stainless steel. Nitrogen, aluminum, and tungsten were added for increasing the creep rupture strength of FMS steel. The new heat treatment method was developed to form more stable precipitates. By applying the novel whiskering process, high density SiC/SiC composites with relative density above 90% could be obtained even in a shorter processing time than the conventional CVI process. Material integrated databases are established using data sheets. The databases of 6 kinds of material properties are accessible through the home page of KAERI material division.

  11. Nanocrystalline materials: recent advances in crystallographic characterization techniques

    Directory of Open Access Journals (Sweden)

    Emilie Ringe

    2014-11-01

    Full Text Available Most properties of nanocrystalline materials are shape-dependent, providing their exquisite tunability in optical, mechanical, electronic and catalytic properties. An example of the former is localized surface plasmon resonance (LSPR, the coherent oscillation of conduction electrons in metals that can be excited by the electric field of light; this resonance frequency is highly dependent on both the size and shape of a nanocrystal. An example of the latter is the marked difference in catalytic activity observed for different Pd nanoparticles. Such examples highlight the importance of particle shape in nanocrystalline materials and their practical applications. However, one may ask `how are nanoshapes created?', `how does the shape relate to the atomic packing and crystallography of the material?', `how can we control and characterize the external shape and crystal structure of such small nanocrystals?'. This feature article aims to give the reader an overview of important techniques, concepts and recent advances related to these questions. Nucleation, growth and how seed crystallography influences the final synthesis product are discussed, followed by shape prediction models based on seed crystallography and thermodynamic or kinetic parameters. The crystallographic implications of epitaxy and orientation in multilayered, core-shell nanoparticles are overviewed, and, finally, the development and implications of novel, spatially resolved analysis tools are discussed.

  12. Application of Advanced Master Curve Approaches to the EURO Fracture Toughness Data Set

    Energy Technology Data Exchange (ETDEWEB)

    Lucon, E.; Scibetta, M.

    2007-01-15

    The so-called EURO data set is the largest set ever assembled, consisting of fracture toughness results obtained in the ductile-to-brittle transition region. It was the outcome of a large EU sponsored project which involved ten European laboratories in the second half of the 90ies. Several post-project investigations have identified one of the blocks from which specimens were extracted (block SX9) as macroscopically inhomogeneous and significantly tougher than the remaining blocks. In this study, the variability of block SX9 has been investigated using the conventional Master Curve (MC) methodology and some recent MC extensions, namely the SINTAP lower tail, the single point estimation, the bi-modal Master Curve and the multi-modal Master Curve. The basic MC method is intended for macroscopically homogeneous ferritic steels only, and the alternative approaches have been developed for the investigation of inhomogeneous materials. Therefore, these methods can be used to study the behaviour of block SX9 within the EURO data set. It has been found that the bi-modal and multi-modal MC approaches are quite effective in detecting the anomaly represented by block SX9, but only when analyses are performed on data sets of comparable size.

  13. Characterization of fracture patterns and hygric properties for moisture flow modelling in cracked concrete

    OpenAIRE

    Rouchier, S.; Janssen, Hans; Rode, C; Woloszyn, M.; Foray, G.; Roux, J-J.

    2012-01-01

    International audience Several years after their installation, building materials such as concrete present signs of ageing in the form of fractures covering a wide range of sizes, from microscopic to macroscopic cracks. All sizes of fractures can have a strong influence on heat and moisture flow in the building envelope, but their distribution is difficult to predict due to the variety of environmental factors which cause them. This paper aims at applying experimental non-destructive techn...

  14. CHARACTERIZATION OF IN-SITU STRESS AND PERMEABILITY IN FRACTURED RESERVOIRS

    Energy Technology Data Exchange (ETDEWEB)

    Daniel R. Burns; M. Nafi Toksoz

    2005-08-01

    During the past six months we have adapted our 3-D elastic, anisotropic finite difference code by implementing the rotated staggered grid (RSG) method to more accurately represent large contrasts of elastic moduli between the fractures and surrounding formation, and applying the perfectly matched layer (PML) absorbing boundary condition to minimize boundary reflections. Two approaches for estimating fracture spacing from scattered seismic energy were developed. The first relates notches in the amplitude spectra of the scattered wavefield to the dominant fracture spacing that caused the scattering. The second uses conventional FK filtering to isolate the backscattered signals and then recovers an estimate of the fracture spacing from the dominant wavelength of those signals. Both methods were tested on synthetic data and then applied to the Emilio field data. The spectral notch method estimated the Emilio fracture spacing to be about 30 to 40 m, while the FK method found fracture spacing of about 48 to 53 m. We continue to work on two field data sets from fractured carbonate reservoirs provided by our industry sponsors--the offshore Emilio Field data (provided by ENIAGIP), and an onshore reservoir from the Middle East (provided by Shell). Calibration data in the form of well logs and previous fracture studies are available for both data sets. In previous reports we showed the spatial distribution fractures in the Emilio Field based on our calculated scattering index values. To improve these results we performed a map migration of all the scattering indices. The results of this migration process show a very strong correlation between the spatial distribution and orientation of our estimated fracture distribution and the fault system in the field. We observe that the scattering index clusters tend to congregate around the fault zones, particularly near multiple faults and at fault tips. We have also processed a swath of data from the second data set (the onshore

  15. Using advanced electron microscopy for the characterization of catalytic materials

    Science.gov (United States)

    Pyrz, William D.

    Catalysis will continue to be vitally important to the advancement and sustainability of industrialized societies. Unfortunately, the petroleum-based resources that currently fuel the energy and consumer product needs of an advancing society are becoming increasingly difficult and expensive to extract as supplies diminish and the quality of sources degrade. Therefore, the development of sustainable energy sources and the improvement of the carbon efficiency of existing chemical processes are critical. Further challenges require that these initiatives are accomplished in an environmentally friendly fashion since the effects of carbon-based emissions are proving to be a serious threat to global climate stability. In this dissertation, materials being developed for sustainable energy and process improvement initiatives are studied. Our approach is to use materials characterization, namely advanced electron microscopy, to analyze the targeted systems at the nano- or Angstrom-scale with the goal of developing useful relationships between structure, composition, crystalline order, morphology, and catalytic performance. One area of interest is the complex Mo-V-M-O (M=Te, Sb, Ta, Nb) oxide system currently being developed for the selective oxidation/ammoxidation of propane to acrylic acid or acrylonitrile, respectively. Currently, the production of acrylic acid and acrylonitrile rely on propylene-based processes, yet significant cost savings could be realized if the olefin-based feeds could be replaced by paraffin-based ones. The major challenge preventing this feedstock replacement is the development of a suitable paraffin-activating catalyst. Currently, the best candidate is the Mo-V-Nb-Te-O complex oxide catalyst that is composed of two majority phases that are commonly referred to as M1 and M2. However, there is a limited understanding of the roles of each component with respect to how they contribute to catalyst stability and the reaction mechanism. Aberration

  16. Advanced materials characterization based on full field deformation measurements

    Science.gov (United States)

    Carpentier, A. Paige

    Accurate stress-strain constitutive properties are essential for understanding the complex deformation and failure mechanisms for materials with highly anisotropic mechanical properties. Among such materials, glass-fiber- and carbon-fiber-reinforced polymer--matrix composites play a critical role in advanced structural designs. The large number of different methods and specimen types currently required to generate three-dimensional allowables for structural design slows down the material characterization. Also, some of the material constitutive properties are never measured due to the prohibitive cost of the specimens needed. This work shows that simple short-beam shear (SBS) specimens are well-suited for measurement of multiple constitutive properties for composite materials and that can enable a major shift toward accurate material characterization. The material characterization is based on the digital image correlation (DIC) full-field deformation measurement. The full-field-deformation measurement enables additional flexibility for assessment of stress--strain relations, compared to the conventional strain gages. Complex strain distributions, including strong gradients, can be captured. Such flexibility enables simpler test-specimen design and reduces the number of different specimen types required for assessment of stress--strain constitutive behavior. Two key elements show advantage of using DIC in the SBS tests. First, tensile, compressive, and shear stress--strain relations are measured in a single experiment. Second, a counter-intuitive feasibility of closed-form stress and modulus models, normally applicable to long beams, is demonstrated for short-beam specimens. The modulus and stress--strain data are presented for glass/epoxy and carbon/epoxy material systems. The applicability of the developed method to static, fatigue, and impact load rates is also demonstrated. In a practical method to determine stress-strain constitutive relations, the stress

  17. Characterization of plasticity and fracture of shell casing of lithium-ion cylindrical battery

    Science.gov (United States)

    Zhang, Xiaowei; Wierzbicki, Tomasz

    2015-04-01

    Most of the literature on lithium-ion battery cells is concerned with modeling of jellyroll with little attention to properties of shell casing. However, shell casing provides substantial strength and fracture resistance under mechanical loading and therefore must be an important part of modeling of lithium-ion batteries. The paper reports on a comprehensive test program on commercially available empty shell casing of 18650 lithium-ion cylindrical cells. Part of the tests was used to determine plastic and fracture properties from sub-size specimens cut from lateral part of the cans. The other part served to validate plasticity and fracture models under various loading conditions. The associated flow rule was used to simulate plasticity behavior and Modified Mohr-Coulomb (MMC) fracture model was adopted to predict crack initiation and propagation of shell casing. Simulation results confirmed that present plasticity and fracture models could predict global plastic behavior of the cells under different loading conditions. The jellyroll model with volumetric hardening was introduced to compare the performance of empty shell casing, bare jellyroll and complete battery cell. It was shown that in many loading situations, for example, three point bending of the cylindrical cells, the metallic shell casing provides most of mechanical resistance.

  18. Semi-automatic characterization of fractured rock masses using 3D point clouds: discontinuity orientation, spacing and SMR geomechanical classification

    Science.gov (United States)

    Riquelme, Adrian; Tomas, Roberto; Abellan, Antonio; Cano, Miguel; Jaboyedoff, Michel

    2015-04-01

    Investigation of fractured rock masses for different geological applications (e.g. fractured reservoir exploitation, rock slope instability, rock engineering, etc.) requires a deep geometric understanding of the discontinuity sets affecting rock exposures. Recent advances in 3D data acquisition using photogrammetric and/or LiDAR techniques currently allow a quick and an accurate characterization of rock mass discontinuities. This contribution presents a methodology for: (a) use of 3D point clouds for the identification and analysis of planar surfaces outcropping in a rocky slope; (b) calculation of the spacing between different discontinuity sets; (c) semi-automatic calculation of the parameters that play a capital role in the Slope Mass Rating geomechanical classification. As for the part a) (discontinuity orientation), our proposal identifies and defines the algebraic equations of the different discontinuity sets of the rock slope surface by applying an analysis based on a neighbouring points coplanarity test. Additionally, the procedure finds principal orientations by Kernel Density Estimation and identifies clusters (Riquelme et al., 2014). As a result of this analysis, each point is classified with a discontinuity set and with an outcrop plane (cluster). Regarding the part b) (discontinuity spacing) our proposal utilises the previously classified point cloud to investigate how different outcropping planes are linked in space. Discontinuity spacing is calculated for each pair of linked clusters within the same discontinuity set, and then spacing values are analysed calculating their statistic values. Finally, as for the part c) the previous results are used to calculate parameters F_1, F2 and F3 of the Slope Mass Rating geomechanical classification. This analysis is carried out for each discontinuity set using their respective orientation extracted in part a). The open access tool SMRTool (Riquelme et al., 2014) is then used to calculate F1 to F3 correction

  19. Characterization of short-fibre reinforced thermoplastics for fracture fixation devices.

    Science.gov (United States)

    Brown, S A; Hastings, R S; Mason, J J; Moet, A

    1990-10-01

    This study focuses on determining the effects of clinically relevant procedures on the flexural and fracture toughness properties of three short-fibre thermoplastic composites for potential application as fracture fixation devices. The procedures included sterilization, heat contouring and saline soaking. The three materials tested were polysulphone, polybutylene terephthalate and polyetheretherketone, all reinforced with 30% short carbon fibres. The polysulphone composite showed significant degradation in mechanical properties due to saline soaking. The polybutylene terephthalate exhibited significant degradation of mechanical properties following both contouring and saline soaking. The polyetheretherketone composite, however, exhibited no degradation in mechanical properties. The results demonstrated that flexion and fracture toughness testing were effective for determining the response of the composites to different applied conditions and demonstrated the stability of polyetheretherketone subjected to these treatments. Scanning electron microscopy demonstrated the most effective fibre-matrix bonding to be in the polyetheretherketone.

  20. An example of using oil-production induced microseismicity in characterizing a naturally fractured reservoir

    Energy Technology Data Exchange (ETDEWEB)

    Rutledge, J.T.; Phillips, W.S. [Nambe Geophysical, Inc., Santa Fe, NM (United States); Schuessler, B.K.; Anderson, D.W. [Los Alamos National Lab., NM (United States)

    1996-06-01

    Microseismic monitoring was conducted using downhole geophone tools deployed in the Seventy-Six oil field, Clinton County, Kentucky. Over a 7-month monitoring period, 3237 microearthquakes were detected during primary oil production; no injection operations were conducted. Gross changes in production rate correlate with microearthquake event rate with event rate lagging production-rate changes by about 2 weeks. Hypocenters and first-motion data have revealed low-angle, thrust fracture zones above and below the currently drained depth interval. Production history, well logs and drill tests indicate the seismically-active fractures are previously drained intervals that have subsequently recovered to hydrostatic pressure via brine invasion. The microseismic data have revealed, for the first time, the importance of the low-angle fractures in the storage and production of oil in the study area. The seismic behavior is consistent with poroelastic models that predict slight increases in compressive stress above and below currently drained volumes.

  1. Fracture characterization in patterned thin films by cross-sectional nanoindentation

    Energy Technology Data Exchange (ETDEWEB)

    Ocana, I. [CEIT and TECNUN (University of Navarra), P. Manuel Lardizabal 15, 20018 San Sebastian (Spain); Molina-Aldareguia, J.M. [CEIT and TECNUN (University of Navarra), P. Manuel Lardizabal 15, 20018 San Sebastian (Spain); Gonzalez, D. [CEIT and TECNUN (University of Navarra), P. Manuel Lardizabal 15, 20018 San Sebastian (Spain); Elizalde, M.R. [CEIT and TECNUN (University of Navarra), P. Manuel Lardizabal 15, 20018 San Sebastian (Spain)]. E-mail: relizalde@ceit.es; Sanchez, J.M. [CEIT and TECNUN (University of Navarra), P. Manuel Lardizabal 15, 20018 San Sebastian (Spain); Martinez-Esnaola, J.M. [CEIT and TECNUN (University of Navarra), P. Manuel Lardizabal 15, 20018 San Sebastian (Spain); Gil Sevillano, J. [CEIT and TECNUN (University of Navarra), P. Manuel Lardizabal 15, 20018 San Sebastian (Spain); Scherban, T.. E-mail: Tracey_Scherban@Hotmail.com; Pantuso, D. [Logic Technology Development, Intel Corporation, Hillsboro, OR 97124 (United States); Sun, B. [Logic Technology Development, Intel Corporation, Hillsboro, OR 97124 (United States); Xu, G. [Logic Technology Development, Intel Corporation, Hillsboro, OR 97124 (United States); Miner, B. [Logic Technology Development, Intel Corporation, Hillsboro, OR 97124 (United States); He, J. [Logic Technology Development, Intel Corporation, Hillsboro, OR 97124 (United States); Maiz, J. [Logic Technology Development, Intel Corporation, Hillsboro, OR 97124 (United States)

    2006-08-15

    A testing technique based on cross-sectional nanoindentation has been used to assess the mechanical reliability of interconnect structures. A Berkovich indenter was used to initiate fracture in a silicon substrate and cracks propagated through the structure. To better control crack growth and to convert the problem into two dimensions, a trench parallel to the indentation surface was previously machined using a focused ion beam. The crack lengths obtained for different material systems in the interconnect structure correlate well with the fracture energies measured for the same materials in blanket films. Finite element model simulations incorporating cohesive elements have been used to model the fracture processes and to explain the different cracking behaviour observed.

  2. 大庆外围油田储层裂缝综合描述技术%COMPREHENSIVE CHARACTERIZING TECHNIQUE OF THE RESERVOIR FRACTURES IN DAQING PERIPHERAL OILFIELDS

    Institute of Scientific and Technical Information of China (English)

    孙淑艳; 刘益嘉; 刘迪

    2012-01-01

    大庆外围油田以低、特低渗透储层为主,天然裂缝比较发育.针对储层裂缝对油田注水开发效果影响较大的问题,通过分析研究外围油田裂缝监测数据资料,深入开展了储层裂缝表征、预测及综合描述方法研究,研究了双重介质储层裂缝建模方法,形成了一套完整的低孔低渗储层裂缝定量描述方法,建立了裂缝网络模型及双重介质模型,实现了裂缝几何模型与等效介质模型转换,初步解决了储层裂缝地质建模技术难题.其研究成果在油田开发中得到广泛应用,取得较好的开发效果和经济效益,对非均质裂缝型油田精细开发调整具有重要指导意义.%Daqing peripheral oilfields are mainly characterized by low-permeability & ultra-low-permeability reservoirs and well-developed natural fractures. In the light of the issue of serious influences of the reservoir fractures on the performances of oilfield water flooding, with the help of the analyses and studies on the monitored data of the fractures, the method researches on the fracture characterization, forecast and comprehensive describing method are deeply carried out, and moreover the dual- porosity media fracture modeling approach is studied, thus a set of complete quantified characterizing method of low-porosity and low-permeability reservoir fractures is established, the fracture network model and dual-porosity media model are built, so the geometric model of the fractures can be converted into equivalent media model, finally the technical problems of the geological modeling for the reservoir fractures is generally solved. The study achievements have extensively applied in the oilfield development and the much better social and economical effects have been acquired. In a word, the achievements have possessed important guiding significance for the fine development adjustment of heterogeneous fractured oilfields. characterization of reservoir fracture; fracture forecast

  3. High Temperature Materials Characterization and Advanced Materials Development

    International Nuclear Information System (INIS)

    The project has been carried out for 2 years in stage III in order to achieve the final goals of performance verification of the developed materials, after successful development of the advanced high temperature material technologies for 3 years in Stage II. The mechanical and thermal properties of the advanced materials, which were developed during Stage II, were evaluated at high temperatures, and the modification of the advanced materials were performed. Moreover, a database management system was established using user-friendly knowledge-base scheme to complete the integrated-information material database in KAERI material division

  4. APPLICATION OF RESERVOIR CHARACTERIZATION AND ADVANCED TECHNOLOGY TO IMPROVE RECOVERY AND ECONOMICS IN A LOWER QUALITY SHALLOW SHELF SAN ANDRES RESERVOIR

    International Nuclear Information System (INIS)

    The Class 2 Project at West Welch was designed to demonstrate the use of advanced technologies to enhance the economics of improved oil recovery (IOR) projects in lower quality Shallow Shelf Carbonate (SSC) reservoirs, resulting in recovery of additional oil that would otherwise be left in the reservoir at project abandonment. Accurate reservoir description is critical to the effective evaluation and efficient design of IOR projects in the heterogeneous SSC reservoirs. Therefore, the majority of Budget Period 1 was devoted to reservoir characterization. Technologies being demonstrated include: (1) Advanced petrophysics; (2) Three-dimensional (3-D) seismic; (3) Crosswell bore tomography; (4) Advanced reservoir simulation; (5) Carbon dioxide (CO2) stimulation treatments; (6) Hydraulic fracturing design and monitoring; and (7) Mobility control agents

  5. APPLICATION OF RESERVOIR CHARACTERIZATION AND ADVANCED TECHNOLOGY TO IMPROVE RECOVERY AND ECONOMICS IN A LOWER QUALITY SHALLOW SHELF SAN ANDRES RESERVOIR

    Energy Technology Data Exchange (ETDEWEB)

    T. Scott Hickman; James J. Justice

    2001-06-16

    The Class 2 Project at West Welch was designed to demonstrate the use of advanced technologies to enhance the economics of improved oil recovery (IOR) projects in lower quality Shallow Shelf Carbonate (SSC) reservoirs, resulting in recovery of additional oil that would otherwise be left in the reservoir at project abandonment. Accurate reservoir description is critical to the effective evaluation and efficient design of IOR projects in the heterogeneous SSC reservoirs. Therefore, the majority of Budget Period 1 was devoted to reservoir characterization. Technologies being demonstrated include: (1) Advanced petrophysics; (2) Three-dimensional (3-D) seismic; (3) Crosswell bore tomography; (4) Advanced reservoir simulation; (5) Carbon dioxide (CO{sub 2}) stimulation treatments; (6) Hydraulic fracturing design and monitoring; and (7) Mobility control agents.

  6. Hydro-geophysical characterization for groundwater resources potential of fractured limestone reservoirs in Amdoun Monts (North-western Tunisia)

    Science.gov (United States)

    Redhaounia, Belgacem; Bédir, Mourad; Gabtni, Hakim; Batobo, Ountsche Ilondo; Dhaoui, Mohamed; Chabaane, Achref; Khomsi, Sami

    2016-05-01

    This study has led to the identification of the Upper Cretaceous and Lower Eocene (Abiod, Boudabbous/El Gueria Formations) fractured and karstic aquifers in the Amdoun region (Northwestern Tunisia). Geological information (litho-stratigraphy and fractures network study) and geophysical (gravity, wells analysis, seismic reflection, Electrical Resistivity Tomography (ERT)) investigations performed in the area have highlighted, with some detail, images of structures of carbonate aquifers near anticline flanks and along perched synclines. Some factors such as fracture intensity, karsts evolution and structural position have an important influence on the hydrologic productivity of Abiod and Boudabbous/El Gueria reservoirs. Different methodologies were used to characterize the geological and hydro-geological perched aquifers and produce the 3D geo-electrical model of near surface karstic features and cavities of the carbonate limestone in the Aïn Sallem site. This study integrates the geological and geophysical information available and can serve as a representative example in the description of the most important hydraulic reserves in the North-western Tunisia.

  7. Characterization of injection wells in a fractured reservoir using PTS logs, Steamboat Hills Geothermal Field, Nevada, USA

    Energy Technology Data Exchange (ETDEWEB)

    Goranson, Colin; Combs, Jim

    1995-01-26

    The Steamboat Hills Geothermal Field in northwestern Nevada, about 15 km south of Reno, is a shallow (150m to 825m) moderate temperature (155 C to 168 C) liquid-dominated geothermal reservoir situated in highly-fractured granodiorite. Three injection wells were drilled and completed in granodiorite to dispose of spent geothermal fluids from the Steamboat II and III power plants (a 30 MW air-cooled binary-type facility). Injection wells were targeted to depths below 300m to inject spent fluids below producing fractures. First, quasi-static downhole pressure-temperature-spinner (PTS) logs were obtained. Then, the three wells were injection-tested using fluids between 80 C and 106 C at rates from 70 kg/s to 200 kg/s. PTS logs were run both up and down the wells during these injection tests. These PTS surveys have delineated the subsurface fracture zones which will accept fluid. The relative injectivity of the wells was also established. Shut-in interzonal flow within the wells was identified and characterized.

  8. The application of vertical seismic profiling and cross-hole tomographic imaging for fracture characterization at Yucca Mountain

    Energy Technology Data Exchange (ETDEWEB)

    Majer, E.L.; Peterson, J.E.; Tura, M.A.; McEvilly, T.V.

    1990-01-01

    In order to obtain the necessary characterization for the storage of nuclear waste, much higher resolution of the features likely to affect the transport of radionuclides will be required than is normally achieved in conventional surface seismic reflection used in the exploration and characterization of petroleum and geothermal resources. Because fractures represent a significant mechanical anomaly seismic methods using are being investigated as a means to image and characterize the subsurface. Because of inherent limitations in applying the seismic methods solely from the surface, state-of-the-art borehole methods are being investigated to provide high resolution definition within the repository block. Therefore, Vertical Seismic Profiling (VSP) and cross-hole methods are being developed to obtain maximum resolution of the features that will possible affect the transport of fluids. Presented here will be the methods being developed, the strategy being pursued, and the rational for using VSP and crosshole methods at Yucca Mountain. The approach is intended to be an integrated method involving improvements in data acquisition, processing, and interpretation as well as improvements in the fundamental understanding of seismic wave propagation in fractured rock. 33 refs., 4 figs.

  9. The application of vertical seismic profiling and cross-hole tomographic imaging for fracture characterization at Yucca Mountain

    International Nuclear Information System (INIS)

    In order to obtain the necessary characterization for the storage of nuclear waste, much higher resolution of the features likely to affect the transport of radionuclides will be required than is normally achieved in conventional surface seismic reflection used in the exploration and characterization of petroleum and geothermal resources. Because fractures represent a significant mechanical anomaly seismic methods using are being investigated as a means to image and characterize the subsurface. Because of inherent limitations in applying the seismic methods solely from the surface, state-of-the-art borehole methods are being investigated to provide high resolution definition within the repository block. Therefore, Vertical Seismic Profiling (VSP) and cross-hole methods are being developed to obtain maximum resolution of the features that will possible affect the transport of fluids. Presented here will be the methods being developed, the strategy being pursued, and the rational for using VSP and crosshole methods at Yucca Mountain. The approach is intended to be an integrated method involving improvements in data acquisition, processing, and interpretation as well as improvements in the fundamental understanding of seismic wave propagation in fractured rock. 33 refs., 4 figs

  10. Face/core interface fracture characterization of mixed mode bending sandwich specimens

    DEFF Research Database (Denmark)

    Quispitupa, Amilcar; Berggreen, Christian; Carlsson, L.A.

    2011-01-01

    and PVC H45, H100 and H250 foam core materials were evaluated. A methodology to perform precracking on fracture specimens in order to achieve a sharp and representative crack front is outlined. The mixed mode loading was controlled in the mixed mode bending (MMB) test rig by changing the loading...

  11. Critical cleavage fracture stress characterization of A508 nuclear pressure vessel steels

    International Nuclear Information System (INIS)

    The critical cleavage fracture stress of SA508 Gr.4N and SA508 Gr.3 low alloy reactor pressure vessel (RPV) steels was studied through the combination of experiments and finite element method (FEM) analysis. The results showed that the value of the local cleavage fracture stress, σF, of SA508 Gr.4N steel was significantly higher than that of SA508 Gr.3 steel. Detailed microstructural analysis was carried out using FEGSEM which revealed much smaller grains, finer and more homogenous carbide particles formed in SA508 Gr.4N steel. Compared with the SA508 Gr.3 steel currently used in the nuclear industry, the SA508 Gr.4N steel possesses higher strength and notch toughness as well as improved cleavage fracture behavior, and is considered a better candidate RPV steel for the next generation nuclear reactors. - Highlights: • Critical cleavage fracture stress was calculated through experiments and FEM. • Effects of both grain and carbide particle sizes on σF were discussed. • The SA508 Gr.4N steel is a better candidate for the next generation nuclear reactors

  12. Face/core mixed mode debond fracture toughness characterization using the modified TSD test method

    DEFF Research Database (Denmark)

    Berggreen, Christian; Quispitupa, Amilcar; Costache, Andrei;

    2014-01-01

    The modified tilted sandwich debond (TSD) test method is used to examine face/core debond fracture toughness of sandwich specimens with glass/polyester face sheets and PVC H45 and H100 foam cores over a large range of mode-mixities. The modification was achieved by reinforcing the loaded face she...

  13. Preferential flow characterization in fractured aquifer by injecting dissolved oxygen in boreholes

    Science.gov (United States)

    Vurro, Michele; Donnaloia, Mietta; Masciopinto, Costantino; Pennetta, Luigi; Robbins, Gary; Vitale, Sarah

    2016-04-01

    A new approach to identify contributing fractures and wellbore flow in fractured and karst aquifers is presented. It is time efficient, low cost and based on a benign tracer: the dissolved oxygen (DO). The method was already applied by other scientists to test fractured crystalline rock wells. The DO method consists in elevating water DO concentration in a borehole by bubbling air at assigned water depths using a porous polypropylene tube (bubbler) connected to a compressed air tank with tubing. After the aeration, the resulting profile should be a linear increase in DO with depth due to the effects of water pressure on oxygen solubility. Any changes in the DO profile will be then observed when water flows into and through the well. DO dilution can be used to locate inflowing fractures and to define active flow zones in wells. If there is no change in the DO profile, a "dead zones" in the well is present, that is to say no flow is taking place or can be identified. The DO tests in this work have been carried out in the industrial area of Bari, at the experimental station, constituted by five wells drilled at the CNR-IRSA. The wells penetrate karstic limestone. Results show enhanced flow through at depths between 32 and 37 meters below the water level: DO concentrations decrease until they reach values close to 0 mg/l. DO curves show also the presence of inflowing fractures, as testified by the decrease in the DO concentrations due to the effects of water dilution, at depths of 4 and 9 meters (below the water table) in the north well, at 4 and 10 meters in the central well, and at 30 meters in the south well. The benefits of utilizing DO as a tracer include ease of accessibility, low cost and time-efficiency as well as non-toxic nature of the tracer and no impact on flow conditions.

  14. CHARACTERIZATION OF IN-SITU STRESS AND PERMEABILITY IN FRACTURED RESERVOIRS

    Energy Technology Data Exchange (ETDEWEB)

    Daniel R. Burns; M. Nafi Toksoz

    2002-12-31

    We have extended a three-dimensional finite difference elastic wave propagation model previously developed at the Massachusetts Institute of Technology (MIT) Earth Resources Laboratory (ERL) for modeling and analyzing the effect of fractures on seismic waves. The code has been translated into C language and parallelized [using message passing interface (MPI)] to allow for larger models to be run on Linux PC computer clusters. We have also obtained another 3-D code from Lawrence Berkeley Laboratory, which we will use for verification of our ERL code results and also to run discrete fracture models. Testing of both codes is underway. We are working on a new finite difference model of borehole wave propagation for stressed formations. This code includes coordinate stretching to provide stable, variable grid sizes that will allow us to model the thin fluid annulus layers in borehole problems, especially for acoustic logging while drilling (LWD) applications. We are also extending our analysis routines for the inversion of flexural wave dispersion measurements for in situ stress estimates. Initial results on synthetic and limited field data are promising for a method to invert cross dipole data for the rotation angle and stress state simultaneously. A meeting is being scheduled between MIT and Shell Oil Company scientists to look at data from a fractured carbonate reservoir that may be made available to the project. The Focus/Disco seismic processing system from Paradigm Geophysical has been installed at ERL for field data analysis and as a platform for new analysis modules. We have begun to evaluate the flow properties of discrete fracture distributions through a simple 2D numerical model. Initial results illustrate how fluid flow pathways are very sensitive to variations in the geometry and apertures of fracture network.

  15. Advancing Analytical Methods for Characterization of Anionic Carbohydrate Biopolymers

    OpenAIRE

    Langeslay, Derek Joseph

    2013-01-01

    The focus of this dissertation is on the development of improved analytical methods for the characterization of anionic carbohydrate biopolymers. Our goal is to extract important information from complex mixtures of heterogeneous polysaccharides by characterizing their substituent oligosaccharides in terms of monosaccharide composition and primary and secondary structure. This work focuses on the application of two major analytical platforms: spectroscopy and chromatography. The development ...

  16. Method development and strategy for the characterization of complexly faulted and fractured rhyolitic tuffs, Yucca Mountain, Nevada

    Energy Technology Data Exchange (ETDEWEB)

    Karasaki, K. [Lawrence Berkeley Lab., CA (United States); Galloway, D. [Geological Survey, Sacramento, CA (United States)

    1991-06-01

    The planned high-level nuclear waste repository at Yucca Mountain, Nevada, would exist in unsaturated, fractured welded tuff. One possible contaminant pathway to the accessible environment is transport by groundwater infiltrating to the water table and flowing through the saturated zone. Therefore, an effort to characterize the hydrology of the saturated zone is being undertaken in parallel with that of the unsaturated zone. As a part of the saturated zone investigation, there wells-UE-25c{number_sign}1, UE-25c{number_sign}2, and UE-25c{number_sign}3 (hereafter called the c-holes)-were drilled to study hydraulic and transport properties of rock formations underlying the planned waste repository. The location of the c-holes is such that the formations penetrated in the unsaturated zone occur at similar depths and with similar thicknesses as at the planned repository site. In characterizing a highly heterogeneous flow system, several issues emerge. (1) The characterization strategy should allow for the virtual impossibility to enumerate and characterize all heterogeneities. (2) The methodology to characterize the heterogeneous flow system at the scale of the well tests needs to be established. (3) Tools need to be developed for scaling up the information obtained at the well-test scale to the larger scale of the site. In the present paper, the characterization strategy and the methods under development are discussed with the focus on the design and analysis of the field experiments at the c-holes.

  17. Characterization of fractures and flow zones in a contaminated crystalline-rock aquifer in the Tylerville section of Haddam, Connecticut

    Science.gov (United States)

    Johnson, Carole D.; Kiel, Kristal F.; Joesten, Peter K.; Pappas, Katherine L.

    2016-10-04

    The U.S. Geological Survey, in cooperation with the Connecticut Department of Energy and Environmental Protection, investigated the characteristics of the bedrock aquifer in the Tylerville section of Haddam, Connecticut, from June to August 2014. As part of this investigation, geophysical logs were collected from six water-supply wells and were analyzed to (1) identify well construction, (2) determine the rock type and orientation of the foliation and layering of the rock, (3) characterize the depth and orientation of fractures, (4) evaluate fluid properties of the water in the well, and (5) determine the relative transmissivity and head of discrete fractures or fracture zones. The logs included the following: caliper, electromagnetic induction, gamma, acoustic and (or) optical televiewer, heat-pulse flowmeter under ambient and pumped conditions, hydraulic head data, fluid electrical conductivity and temperature under postpumping conditions, and borehole-radar reflection collected in single-hole mode. In a seventh borehole, a former water-supply well, only caliper, fluid electrical conductivty, and temperature logs were collected, because of a constriction in the borehole.This report includes a description of the methods used to collect and process the borehole geophysical data, the description of the data collected in each of the wells, and a comparison of the results collected in all of the wells. The data are presented in plots of the borehole geophysical logs, tables, and figures. Collectively these data provide valuable characterizations that can be used to improve or inform site conceptual models of groundwater flow in the study area.

  18. Electromagnetic characterization of fractured rock for geological disposal studies of spent nuclear fuel

    Energy Technology Data Exchange (ETDEWEB)

    Eloranta, E. [Radiation and Nuclear Safety Authority, Helsinki (Finland); Ermutlu, M. [Nokia Research Center, Helsinki (Finland); Flykt, M.; Lindell, I.; Nikoskinen, K.; Sihvola, A. [Helsinki Univ. of Technology, Espoo (Finland). Electromagnetics Lab.

    1998-04-01

    In the report, the results of a joint research project carried out in 1991-1997 by the Finnish Radiation and Nuclear Safety Authority (STUK) and the Electromagnetics Laboratory of the Helsinki University of Technology are presented. The main purpose was to create computational models for electric potential responses when the medium is anisotropic and is bounded by a perfect magnetic conductor, a perfect electric conductor, and an anisotropic impedance surface. Furthermore, the geometry of two anisotropic half spaces and a layered medium were considered. The solutions of the problems were made using image theory. For modeling the electric potential in anisotropic medium with inhomogeneities, an integral equation was formulated. Also a wedge structure was treated as an extension to the traditional two parallel plate model of fracture geometry. The equivalentization of fracturing with anisotropy is a research area that still continues that still continues 46 refs. The publication contains also fourteen previous publications by authors

  19. Characterization and prevention of formation damage for fractured carbonate reservoir formations with low permeability

    Institute of Scientific and Technical Information of China (English)

    Shu Yong; Yan Jienian

    2008-01-01

    Stress sensitivity and water blocking in fractured carbonate reservoir formations with low permeability were determined as the main potential damage mechanisms during drilling and completion operations in the ancient buried hill Ordovician reservoirs in the Tarim Basin. Geological structure,lithology, porosity, permeability and mineral components all affect the potential for formation damage.The experimental results showed that the permeability loss was 83.8%-98.6% caused by stress sensitivity,and was 27.9%-48.1% caused by water blocking. Based on the experimental results, several main conclusions concerning stress sensitivity can be drawn as follows: the lower the core permeability and the smaller the core fracture width, the higher the stress sensitivity. Also, stress sensitivity results in lag effect for both permeability recovery and fracture closure. Aimed at the mechanisms of formation damage, a modified low-damage mixed metal hydroxide (MMH) drilling fluid system was developed,which was mainly composed of low-fluorescence shale control agent, filtration control agent, lowfluorescence lubricant and surfactant. The results of experimental evaluation and field test showed that the newly-developed drilling fluid and engineering techniques provided could dramatically increase the return permeability (over 85%) of core samples. This drilling fluid had such advantages as good rheological and lubricating properties, high temperature stability, and low filtration rate (API filtration less than 5 ml after aging at 120 ℃ for 4 hours). Therefore, fractured carbonate formations with low permeability could be protected effectively when drilling with the newly-developed drilling fluid.Meanwhile, field test showed that both penetration rate and bore stability were improved and the soaking time of the drilling fluid with formation was sharply shortened, indicating that the modified MMH drilling fluid could meet the requirements of drilling engineering and geology.

  20. AN INTEGRATED APPROACH TO CHARACTERIZING BYPASSED OIL IN HETEROGENEOUS AND FRACTURED RESERVOIRS USING PARTITIONING TRACERS

    Energy Technology Data Exchange (ETDEWEB)

    Akhil Datta-Gupta

    2004-08-01

    We explore the use of efficient streamline-based simulation approaches for modeling and analysis partitioning interwell tracer tests in heterogeneous and fractured hydrocarbon reservoirs. The streamline approach is generalized to model water injection in naturally fractured reservoirs through the use of a dual media approach. The fractures and matrix are treated as separate continua that are connected through a transfer function, as in conventional finite difference simulators for modeling fractured systems. A detailed comparison with a commercial finite difference simulator shows very good agreement. Furthermore, an examination of the scaling behavior of the computation time indicates that the streamline approach is likely to result in significant savings for large-scale field applications. We also propose a novel approach to history matching finite-difference models that combines the advantage of the streamline models with the versatility of finite-difference simulation. In our approach, we utilize the streamline-derived sensitivities to facilitate history matching during finite-difference simulation. The use of finite-difference model allows us to account for detailed process physics and compressibility effects. The approach is very fast and avoids much of the subjective judgments and time-consuming trial-and-errors associated with manual history matching. We demonstrate the power and utility of our approach using a synthetic example and two field examples. Finally, we discuss several alternative ways of using partitioning interwell tracer tests (PITTs) in oil fields for the calculation of oil saturation, swept pore volume and sweep efficiency, and assess the accuracy of such tests under a variety of reservoir conditions.

  1. Tiltmeters as Tools for Characterizing Geometrical and Hydrodynamical Properties of Fractured Crystalline Aquifers and Fault Zones

    Science.gov (United States)

    Schuite, J.; Longuevergne, L.; Bour, O.; Lavenant, N.; Boudin, F.

    2014-12-01

    In many geological reservoirs, open fractures or fault zones generally induce high spatial variability of hydrodynamical properties and shape the main deep-seated flow paths. It is of crucial interest to determine their structure and properties in order to achieve a sound and sustained exploitation of resources or to estimate the risk of failure of any underground storage. Tiltmeters have emerged as new tools to observe deformation generated by groundwater flow. As such instruments are highly sensitive to pressure gradients, they are perfectly suited for monitoring channelized flow in connected fractures and fault zones. Hence, they provide a unique insight of these reservoirs' geometry and dynamics over broad time scales. Here we demonstrate that continuous tilt data from surface long baseline tiltmeters (LBT) can be used alone to evaluate the general functioning of a fractured hardrock system and estimate the hydraulic properties of its main conductive features. The study is applied to the pumping site of Ploemeur observatory (Brittany, France) which is well documented and instrumented, and therefore forms a convenient setting for introducing LBT as tools for fractured media hydrology. On the short term, tilt signals are strongly correlated with pumping cycles and associated head level changes in well-connected boreholes. Besides, when pumps are stopped the maximal tilt direction is systematically perpendicular to a subvertical fault zone whose azimuth of strike has thereby been refined down to degree precision. By using a semi-analytical model of deformation, we establish the link between tilt and pressure change during pumping interruptions which then allows for hydraulic properties estimation from tilt measurements only. Finally, we validate our results with previous estimates obtained from other studies and discuss the orientation of future work that could enhance these estimates.

  2. Determination of cleavage planes and fracture characterization of Ni-based single crystal superalloys

    Science.gov (United States)

    Merrill, John M.; Wilcox, Roy C.

    1992-01-01

    The room temperature fracture behavior of the Ge Rene N-4, CMSX-2, and CMSX-4C single crystal Ni-based superalloys was studied. All crystals were grown along the (001) direction and tensile tested in both helium and hydrogen atmospheres. A stereoscopic technique developed for use with a scanning electron microscope was applied to determine cleavage planes. Planar gamma(') morphologies also were examined to help determine cleavage planes. Helium charged specimens failed on a number of planes including the (111), (110), and (320). In most cases planes of the (111)-type initiated at the notch region and became smaller and smaller as they moved in radially. Tensile strengths in helium averaged 1000 MPa higher than that of the hydrogen charged specimens. Specimens tested in hydrogen generally failed on (100)-type planes originating from the notch region. This (100) region comprised 60 to 80 percent of the total fracture surface on most samples and appeared as large flat planes perpendicular to the growth direction of the crystal. The interior regions contained (100)-type planes as well as (321), (320), (210), and (111)-types. Hydrogen charged specimens also showed a high percentage of large cracks oriented at 90 deg to one another, indicative of the (100)-type fracture. The Ge Rene N4 and the CMSX-4C samples contained 3-5 percent gamma/gamma(') eutectic, while the CMSX-2 samples had little or no gamma/gamma(') eutectic. The relationship between gamma/gamma(') eutectic and the fracture surface has not been fully determined, but it is thought that the gamma/gamma(') eutectic may serve as a possible trapping site for hydrogen.

  3. ADVANCED CHARACTERIZATION OF FRACTURED RESERVOIRS IN CARBONATE ROCKS: THE MICHIGAN BASIN

    Energy Technology Data Exchange (ETDEWEB)

    James R. Wood; William B. Harrison

    2001-04-01

    Among the accomplishments of this past reporting period are obtaining a complete landgrid for the State of Michigan and the digital processing of the high and medium resolution DEM files. We can now extract lineations from the DEMs automatically using machine algorithms. One tentative result that may be very significant is that we may be seeing manifestations of buried structures in the DEM data. We are looking at a set of extracted lineations in the northern lower peninsula that appear to follow the trend of the pinnacle reefs (Silurian) which had relief approaching 300 feet but are now buried to greater than 3000 feet. We have also extracted the dolomite alteration data from all fields and can show that this is mainly confined to the basin center. It may be related to the paleo-rift suggested by the paleomagnetic and gravity data. As reported last time, the acquisition of a 3D seismic dataset over Stoney Point Field from Marathon Oil Company, is complete and attention is being devoted to incorporating the data into the project database and utilizing it. The surface lineation study is focusing on Stoney Point Field using the high-resolution DEM data and plotting of subsurface formation top data for the main reservoir, the Trenton (Ordovician) Formation. The fault pattern at Stoney Point is well documented by Marathon and we are looking for any manifestations on the surface. The main project database is now about as complete as it will be for this project. The main goals have been met, although the scanning of the paper records will have to continue beyond the scheduled end of the project due to the sheer number of records and the increased donations of data from companies as word spread of the project. One of the unanticipated benefits of the project has been the cooperation of gas and oil companies that are or were active in the Michigan Basin in donating material to the project. Both Michigan Tech and Western Michigan continue to receive donations at an accelerating pace. The data management software developed to handle the data, Atlas, is scheduled to undergo a 3rd revision before the project ends. The goals are to streamline access to the data by improving the display and add several new features, including the ability to turn the landgrid on and off. We may also be able to include the capability to calculate or recalculate footage calls as well. We discovered the reason that some of the 1/24,000 USGS DEM (Digital Elevation Models) for the State of Michigan contain high levels of noise and are making one last attempt to acquire a set of good files before the project ends. This will greatly improve the large-scale map (48 inches x 84 inches) that has been constructed by mosaicking of the high-resolution files. This map shows excellent ground surface detail and has drawn much comment and requests for copies at the venues where it has been displayed. Although it was generated for mapping of surface lineations the map has other uses, particularly analysis of the glacial drift in Michigan.

  4. Petrological mineralogical and geochemical characterization of the granitoids and fracture fillings developed in Ratones Mines (Spain)

    International Nuclear Information System (INIS)

    The petrological, mineralogical and geochemical characterisation of the granitoids and fracture fillings developed in the Ratones Mine (Caceres, Spain) has been done in order to understand rock-water interaction processes which control water geochemical parameters. Special interest has been devoted to the analysis and interpretation of REE patterns in the solid phase (granitoids and fracture fillings) because they constitute geochemical tracers in water-rock interaction process. Moreover, REE are considered as actinide analogues. In order to characterise the solid phase (granitoids and fracture fillings) several investigation scales (system, outcrop, whole rock, mineral and geochemical components) have been considered and different types of samples have been analysed. These factors control the methodological approach used in this investigation. The analytical methods we have used in this investigation are microscope, qualitative and semi-quantitative methods (XRD, SEM,EDAX) and quantitative methods (ICP-MS, XRF, EM, LAM-IC-MS). The bulk of the granitoids located around the Ratones Mine Belongs to the alkaline feldspar granite-sienogranite lihotype and they show a peraluminous and subalkaline pattern. From the mineralogical point of view, they are composed by quartz, K-feldspar (Or>90%), showing sericitation, moscovitization and turmolinization altherations, alkaline plagioclase (An-=-3%), usually altered to sericite, saussirite and less frequently affected by moscovitization processes, Fe-Al biotite, frequently affected by chloritization processes and sometimes replaced by muscovite, and finally muscovite (>2% celadonite and <4% paragonite) both of primary and secondary origin. The differences observed between the different lithotypes are related with the modal proportion of the principal minerals,with the presence or absence of certain accessory minerals ( turmaline, cordierite), with specific textural patterns, grain size and also with the richness in specific

  5. Characterization of thermal tracer tests and heat exchanges in fractured media

    Science.gov (United States)

    de La Bernardie, Jérôme; Bour, Olivier; Guihéneuf, Nicolas; Chatton, Eliot; Labasque, Thierry; Longuevergne, Laurent; Le Lay, Hugo; Koch, Florian; Gerard, Marie-Françoise; Lavenant, Nicolas; Le Borgne, Tanguy

    2016-04-01

    Geothermal energy is a renewable energy source particularly attractive due to associated low greenhouse gas emission rates. Crystalline rocks are in general considered of poor interest for geothermal applications at shallow depths (< 100m), because of the low permeability of the medium. In some cases, fractures may enhance permeability, but thermal energy storage at these shallow depths is still remaining very challenging because of the low storativity of the medium. Within this framework, the purpose of this study is to test the possibility of efficient thermal energy storage in shallow fractured rocks with a single well semi open loop heat exchanger (standing column well). For doing so, several heat tracer tests have been achieved along a borehole between two connected fractures. The heat tracer tests have been achieved at the experimental site of Ploemeur (H+ observatory network). The tracer tests consist in monitoring the temperature in the upper fracture while injecting hot water in the deeper one thanks to a field boiler. For such an experimental setup, the main difficulty to interpret the data comes from the requirement for separating the temperature advective signal of the tracer test (temperature recovery) from the heat increase due to injection of hot water through the borehole which induces heat losses all along the injection tube in the water column. For doing so, in addition to a double straddle packer used for isolating the injection chamber, the particularity of the experimental set up is the use of fiber optic distributed temperature sensing (FO-DTS); an innovative technology which allows spatial and temporal monitoring of the temperature all along the well. Thanks to this tool, we were able to estimate heat increases coming from diffusion along the injection tube which is found much lower than localized temperature increases resulting from tracer test recovery. With local temperatures probes, separating both effects would not have been feasible. We

  6. Materials characterization and fracture mechanics of a space grade dielectric silicone insulation

    Science.gov (United States)

    Abdel-Latif, A. I.; Tweedie, A. T.

    1982-01-01

    The present investigation is concerned with the DC 93-500 high voltage silicone insulation material employed to pot the gun and the collector end of a traveling wave tube (TWT) used on the Landsat D Satellite. The fracture mechanics behavior of the silicone resin was evaluated by measuring the slow crack velocity as a function of the opening mode of the stress intensity factor at +25 and -10 C, taking into account various uniaxial discrete strain values. It was found that the silicone resins slow crack growth is faster than that for a high voltage insulation polyurethane material at the same stress intensity factor value and room temperature.

  7. Characterization of an injectable, degradable polymer for mechanical stabilization of mandibular fractures.

    Science.gov (United States)

    Henslee, Allan M; Yoon, Diana M; Lu, Benjamin Y; Yu, Joseph; Arango, Andrew A; Marruffo, Liann P; Seng, Luke; Anver, Tamir D; Ather, Hunaiza; Nair, Manitha B; Piper, Sean O; Demian, Nagi; Wong, Mark E K; Kasper, F Kurtis; Mikos, Antonios G

    2015-04-01

    This study investigated the use of injectable poly(propylene fumarate) (PPF) formulations for mandibular fracture stabilization applications. A full factorial design with main effects analysis was employed to evaluate the effects of the PPF:N-vinyl pyrrolidone (NVP, crosslinking agent) ratio and dimethyl toluidine (DMT, accelerator) concentration on key physicochemical properties including setting time, maximum temperature, mechanical properties, sol fraction, and swelling ratio. Additionally, the effects of formulation crosslinking time on the mechanical and swelling properties were investigated. The results showed that increasing the PPF:NVP ratio from 3:1 to 4:1 or decreasing the DMT concentration from 0.05 to 0.01 v/w % significantly decreased all mechanical properties as well as significantly increased the sol fraction and swelling ratio. Also, increasing the crosslinking time at 37°C from 1 to 7 days significantly increased all mechanical properties and decreased both the sol fraction and swelling ratio. This study further showed that the flexural stiffness of ex vivo stabilized rabbit mandibles increased from 1.7 ± 0.3 N/mm with a traditional mini-plate fixator to 14.5 ± 4.1 N/mm for the 4:1 (0.05 v/w % DMT) PPF formulation at day 1. Overall, the formulations tested in this study were found to have properties suitable for potential further consideration in mandibular fracture fixation applications. PMID:24934595

  8. Characterizing a fractured aquifer in Mexico using geological attributes related to open-pit groundwater

    Science.gov (United States)

    Herrera, Enrique; Garfias, Jaime

    2013-09-01

    A multivariable analysis of the Rock Quality Designation ( RQD) and its relation with the hydraulic conductivity of 17 dewatering wells in an open-pit mine (central Mexico) is presented as a tool for groundwater exploration in fractured aquifers. A solid model was constructed with the RQD data using three sizes for each grid cell and four interpolation methods. The inverse-distance method with a small grid gives the best results. The resulting RQD solid model was used to locate 22 pilot holes, on which an air-lift test was performed as a qualitative assessment of their usefulness. The results showed a lower water production (1.8 l/s) in shale that has low alteration, whereas in highly altered shale, breccias, and intrusive rock, the flow rate was 3.9 l/s. This implies an important relationship between the pilot-hole performance, the lithology, and the rock alteration, but it was also found that some fractures or faults, which cannot be detected clearly by the RQD, play an important role in the hydrodynamics of the aquifer. In conclusion, it is necessary to consider all available factors that can help to identify the hydrodynamic behavior of the aquifer because using only RQD data can lead to errors in prospecting for groundwater.

  9. Characterization of an injectable, degradable polymer for mechanical stabilization of mandibular fractures.

    Science.gov (United States)

    Henslee, Allan M; Yoon, Diana M; Lu, Benjamin Y; Yu, Joseph; Arango, Andrew A; Marruffo, Liann P; Seng, Luke; Anver, Tamir D; Ather, Hunaiza; Nair, Manitha B; Piper, Sean O; Demian, Nagi; Wong, Mark E K; Kasper, F Kurtis; Mikos, Antonios G

    2015-04-01

    This study investigated the use of injectable poly(propylene fumarate) (PPF) formulations for mandibular fracture stabilization applications. A full factorial design with main effects analysis was employed to evaluate the effects of the PPF:N-vinyl pyrrolidone (NVP, crosslinking agent) ratio and dimethyl toluidine (DMT, accelerator) concentration on key physicochemical properties including setting time, maximum temperature, mechanical properties, sol fraction, and swelling ratio. Additionally, the effects of formulation crosslinking time on the mechanical and swelling properties were investigated. The results showed that increasing the PPF:NVP ratio from 3:1 to 4:1 or decreasing the DMT concentration from 0.05 to 0.01 v/w % significantly decreased all mechanical properties as well as significantly increased the sol fraction and swelling ratio. Also, increasing the crosslinking time at 37°C from 1 to 7 days significantly increased all mechanical properties and decreased both the sol fraction and swelling ratio. This study further showed that the flexural stiffness of ex vivo stabilized rabbit mandibles increased from 1.7 ± 0.3 N/mm with a traditional mini-plate fixator to 14.5 ± 4.1 N/mm for the 4:1 (0.05 v/w % DMT) PPF formulation at day 1. Overall, the formulations tested in this study were found to have properties suitable for potential further consideration in mandibular fracture fixation applications.

  10. Advanced composites characterization with x-ray technologies

    Energy Technology Data Exchange (ETDEWEB)

    Baaklini, G.Y. [National Aeronautics and Space Administration, Cleveland, OH (United States). Lewis Research Center

    1993-12-31

    Recognizing the critical need to advance new composites for the aeronautics and aerospace industries, the author is focusing on advanced test methods that are vital to successful modeling and manufacturing of future generations of high temperature and durable composite materials. These newly developed composites are necessary to reduce propulsion cost and weight, to improve performance and reliability, and to address longer-term national strategic thrusts for sustaining global preeminence in high speed air transport and in high performance military aircraft. Radiography during mechanical testing and intermittent x-ray computed tomography (CT) interrogation were found to be viable nondestructive test methods for understanding damage progression and mechanical behavior of laminated ceramic matrix composite (CMC) systems such as SiC/RBSN and metal matrix composite (MMC) systems such as SiC/Ti based composites. Pretest, in-situ, and post-test radiography provided a greater understanding of CMC mechanical behavior, a verification of related experimental procedures, and validation of related analytical models. CT identified manufacturing problems, guided machining of components to final dimensions, and lead structural and design engineers to realistic component-life-prediction models. The technology needs were defined for the x-ray modalities that were investigated in this paper.

  11. Optical design and characterization of an advanced computational imaging system

    Science.gov (United States)

    Shepard, R. Hamilton; Fernandez-Cull, Christy; Raskar, Ramesh; Shi, Boxin; Barsi, Christopher; Zhao, Hang

    2014-09-01

    We describe an advanced computational imaging system with an optical architecture that enables simultaneous and dynamic pupil-plane and image-plane coding accommodating several task-specific applications. We assess the optical requirement trades associated with custom and commercial-off-the-shelf (COTS) optics and converge on the development of two low-cost and robust COTS testbeds. The first is a coded-aperture programmable pixel imager employing a digital micromirror device (DMD) for image plane per-pixel oversampling and spatial super-resolution experiments. The second is a simultaneous pupil-encoded and time-encoded imager employing a DMD for pupil apodization or a deformable mirror for wavefront coding experiments. These two testbeds are built to leverage two MIT Lincoln Laboratory focal plane arrays - an orthogonal transfer CCD with non-uniform pixel sampling and on-chip dithering and a digital readout integrated circuit (DROIC) with advanced on-chip per-pixel processing capabilities. This paper discusses the derivation of optical component requirements, optical design metrics, and performance analyses for the two testbeds built.

  12. An Integrated Approach to Characterizing Bypassed Oil in Heterogeneous and Fractured Reservoirs Using Partitioning Tracers. Annual Report

    International Nuclear Information System (INIS)

    This report presents an efficient trajectory-based approach to integrate transient pressure data into high-resolution reservoir and aquifer models. The method involves alternating travel time and peak amplitude matching of pressure response using inverse modeling and is particularly well-suited for high resolution subsurface characterization using hydraulic tomography or pressure interference tests. Compared to travel time inversion only, our proposed approach results in a significantly improved match of the pressure response at the wells and also better estimates of subsurface properties. This is accomplished with very little increase in computational cost. Utilizing the concept of a ''diffusive'' time of flight derived from an asymptotic solution of the diffusivity equation, we develop analytical approaches to estimate the sensitivities for travel time and peak amplitude of pressure response to subsurface properties. The sensitivities are then used in an iterative least-squared minimization to match the pressure data. We illustrate our approach using synthetic and field examples. In the field application at a fractured limestone formation, the predominant fracture patterns emerging from the inversion are shown to be consistent with independent geophysical experiments and borehole data

  13. Characterization of the role of heterogeneous advection and diffusion on transport in weathered and fractured granite

    Science.gov (United States)

    Guihéneuf, N.; Boisson, A.; Bour, O.; Le Borgne, T.; Marechal, J.; Nigon, B.; Wajiddudin, M.; Ahmed, S.

    2013-12-01

    The prediction of transport in weathered and fractured rocks is critical as it represents the primary control of contaminant transfer from the subsurface in many parts of the world. This is the case in Southern India, where the subsurface is composed mainly of weathered and fractured granite and where the overexploitation of the groundwater resource since the 70's has led to high water table depletion and strong groundwater quality deterioration. One key issue for modelling transport in such systems is to quantify the respective role of advective heterogeneities and matrix diffusion, which can both lead to strongly non Fickian transport properties. We investigate this question by analysing tracer test experiments performed under different flow configurations at a fractured granite experimental site located in Andhra Pradesh (India). We performed both convergent and push-pull tracer tests within the same fracture and at different scales. Three convergent tracer tests were performed with a solution of fluorescein for different pumping rate and for different distances between injection and pumping boreholes: 6, 30 and 41 meters. To evaluate diffusive process, we performed two long-duration push-pull tests (push time of 3 hours) with a solution of two conservative tracers of different diffusion coefficient (fluorescein and sodium chloride). We performed also six others push-pull tests with only fluorescein but for a variable push times of 14 min and 55 min with or without resting time of about 60 min. The late-time behaviour on the breakthrough curves (BTCs) obtained for all convergent tracer tests showed a power-law slope of -2. Two of them showed an inflexion in the BTCs suggesting the existence of two independent flow paths and thus a highly channelized flow. The long-duration push-pull tests showed similar late-time behaviour with a power-law slope of -2.2 for both tracers. The six others push-pull tests showed a variation of power-law exponent from -3 to -2

  14. Advances in characterizing ubiquitylation sites by mass spectrometry

    DEFF Research Database (Denmark)

    Sylvestersen, K.B.; Young, C.; Nielsen, M.L.

    2013-01-01

    The attachment of one or more ubiquitin moieties to proteins plays a central regulatory mechanism in eukaryotic cells. Protein ubiquitylation regulates numerous cellular processes, including protein degradation, signal transduction, DNA repair and cell division. The characterization of ubiquityla......The attachment of one or more ubiquitin moieties to proteins plays a central regulatory mechanism in eukaryotic cells. Protein ubiquitylation regulates numerous cellular processes, including protein degradation, signal transduction, DNA repair and cell division. The characterization......-scale identification of ubiquitylation sites by peptide-level enrichment strategies. The discovery that ubiquitylation is a widespread modification similar to phosphorylation and acetylation suggests cross-talk may also occur at the post translational modification level. © 2012 Elsevier Ltd....

  15. Synthesis and characterization of new polymeric materials for advanced applications

    OpenAIRE

    Sanna, Roberta

    2014-01-01

    The main aim of this thesis was to synthesize and characterize new kinds of polymeric nanocomposite materials, including stimuli responsive hydrogels, organic-inorganic interpenetrating polymer networks, polyacrylates and polyurethanes. Specifically, this work was divided in two main threads: in the first one, electric field-, ionic force-, pH- and thermo-responsive hydrogels were prepared, whose thermal and mechanical properties, as well as the swelling behavior were strongly improved by the...

  16. Multispectral and hyperspectral advanced characterization of soldier's camouflage equipment

    Science.gov (United States)

    Lagueux, Philippe; Kastek, Mariusz; Chamberland, Martin; PiÄ tkowski, Tadeusz; Farley, Vincent; Dulski, Rafał; Trzaskawka, Piotr

    2013-10-01

    The requirements for soldier camouflage in the context of modern warfare are becoming more complex and challenging given the emergence of novel infrared sensors. There is a pressing need for the development of adapted fabrics and soldier camouflage devices to provide efficient camouflage in both the visible and infrared spectral ranges. The Military University of Technology has conducted an intensive project to develop new materials and fabrics to further improve the camouflage efficiency of soldiers. The developed materials shall feature visible and infrared properties that make these unique and adapted to various military context needs. This paper presents the details of an advanced measurement campaign of those unique materials where the correlation between multispectral and hyperspectral infrared measurements is performed.

  17. Characterization of UMT2013 Performance on Advanced Architectures

    Energy Technology Data Exchange (ETDEWEB)

    Howell, Louis [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

    2014-12-31

    This paper presents part of a larger effort to make detailed assessments of several proxy applications on various advanced architectures, with the eventual goal of extending these assessments to codes of programmatic interest running more realistic simulations. The focus here is on UMT2013, a proxy implementation of deterministic transport for unstructured meshes. I present weak and strong MPI scaling results and studies of OpenMP efficiency on the Sequoia BG/Q system at LLNL, with comparison against similar tests on an Intel Sandy Bridge TLCC2 system. The hardware counters on BG/Q provide detailed information on many aspects of on-node performance, while information from the mpiP tool gives insight into the reasons for the differing scaling behavior on these two different architectures. Preliminary tests that exploit NVRAM as extended memory on an Ivy Bridge machine designed for “Big Data” applications are also included.

  18. Laser-driven spall experiments in ductile materials in order to characterize Johnson fracture model constants

    International Nuclear Information System (INIS)

    We describe laser-driven spall experiments on aluminum, tantalum, steel and gold targets. The free-surface velocity is measured by using a VISAR diagnostic and is compared with numerical simulations at early spallation stage based on the Johnson fracture model. For each material, we first launch one-dimensional simulations with different values of the model parameters and determine the ones which reproduce correctly the experimental data. Then we use two-dimensional simulations to take into account spatial inhomogeneity of the loading pressure over the laser spot. We show non planar ejected spalls which are in agreement with experimental results. We finally study the fragmentation of thin targets and show differences in material behavior for steel in comparison to gold, tantalum and aluminum. (authors)

  19. Three dimensional characterization and capture zone analysis of a dipping tabular fractured bedrock aquifer

    International Nuclear Information System (INIS)

    In order to improve the effectiveness of an existing groundwater recovery and treatment system at a manufacturing site in eastern Pennsylvania, an analysis of groundwater flow within fractured bedrock of the Triassic Brunswick Formation was conducted using water quality, lithologic and hydrologic data, compiled at the site over a period of 13 years. Groundwater quality data, collected from on-site monitoring wells and offsite wells, indicate that a plume of dissolved phase volatile organic compounds originates on the site and has migrated off-site. Groundwater pumping test data from different areas of the site and from three discrete bedrock zones, as well as, the performance of the existing groundwater treatment system indicate: the groundwater system in the bedrock at the site can be conceptualized as a series of tabular aquifers (brittle fractured beds) separated by finer grained, more ductile aquitards which control flow between aquifers. The hydrologic units within the site bedrock have the same orientation as the geologic beds at the site. The development of groundwater flow maps, corrected for anisotropy, which utilize the cone of depression from the existing recovery well, coupled with the geohydrologic model of the site, allowed the development of a modified multiple well groundwater recovery system which will provide control of groundwater sufficient to capture the on-site contamination. The findings of the study demonstrate that the understanding of the geology of the bedrock aquifer and the hydrologic properties of the different geologic units at the site was critical to the design of an effective groundwater recovery system which considers both the anisotropy of the bedrock and the presence of aquitards within the bedrock

  20. Characterization of fracture behavior of zirconium alloys for fuel rod cladding of nuclear power plant in the post-quench stage of a LOCA (Loss of Coolant Accident)

    International Nuclear Information System (INIS)

    In order to guarantee the integrity of nuclear fuel rod cladding, it is necessary for EDF to characterize the ductility of cladding after a Loss of Coolant Accident (LOCA). The thesis is about the characterization of the fracture behavior of cold-worked stress-relieved Zircaloy-4 claddings which have undergone LOCA conditions simulated in laboratory by a high temperature oxidation followed by a cooling. The high temperature oxidation is carried out at 1100 C and 1200 C with different times, which leads to different oxidation levels varying from 3% to 30% ECR (Equivalent Cladding Reacted). The high temperature oxidation is followed by two types of cooling: water quench and air cooling. The oxidized claddings contain two fragile layers - the outer zirconium oxide ZrO2 layer and the middle a(O) layer, and a layer which can have residual ductility - the inner ex-β layer. Characterizations by means of optical microscopy, electron probe micro analysis and nano-indentation have been carried out on the oxidized claddings. A correlation between the oxygen concentration and the nano-hardness and the Young's modulus has been proposed.The Expansion Due to Compression (EDC) test has been developed with an instrumentation of stereo digital image correlation, and then used to characterize the mechanical behavior of the oxidized claddings. The behavior of the oxidized claddings has been studied via macroscopic EDC test curves and observations of fractured or pre-deformed test samples. A fracture scenario of the oxidized claddings has been proposed. The fracture scenario has then been validated via EDC tests on oxidized claddings whose ZrO2 and a(O) layers have been removed, and via finite element modeling of EDC tests. Moreover, a fracture criterion has been established. The mechanical behavior modeling and the proposed fracture criterion have been validated by modeling of ring compression test. (author)

  1. Thermal Characterization of Nanostructures and Advanced Engineered Materials

    Science.gov (United States)

    Goyal, Vivek Kumar

    to heat-sinking units. This dissertation presents results of the experimental investigation and theoretical interpretation of thermal transport in the advanced engineered materials, which include thin films for thermal management of nanoscale devices, nanostructured superlattices as promising candidates for high-efficiency thermoelectric materials, and improved TIMs with graphene and metal particles as fillers providing enhanced thermal conductivity. The advanced engineered materials studied include chemical vapor deposition (CVD) grown ultrananocrystalline diamond (UNCD) and microcrystalline diamond (MCD) films on Si substrates, directly integrated nanocrystalline diamond (NCD) films on GaN, free-standing polycrystalline graphene (PCG) films, graphene oxide (GOx) films, and "pseudo-superlattices" of the mechanically exfoliated Bi2Te3 topological insulator films, and thermal interface materials (TIMs) with graphene fillers.

  2. Hydrogeophysical characterization of transport processes in fractured rock by combining push-pull and single-hole ground penetrating radar experiments

    Science.gov (United States)

    Shakas, Alexis; Linde, Niklas; Baron, Ludovic; Bochet, Olivier; Bour, Olivier; Le Borgne, Tanguy

    2016-02-01

    The in situ characterization of transport processes in fractured media is particularly challenging due to the considerable spatial uncertainty on tracer pathways and dominant controlling processes, such as dispersion, channeling, trapping, matrix diffusion, ambient and density driven flows. We attempted to reduce this uncertainty by coupling push-pull tracer experiments with single-hole ground penetrating radar (GPR) time-lapse imaging. The experiments involved different injection fractures, chaser volumes and resting times, and were performed at the fractured rock research site of Ploemeur in France (H+ network, hplus.ore.fr/en). For the GPR acquisitions, we used both fixed and moving antenna setups in a borehole that was isolated with a flexible liner. During the fixed-antenna experiment, time-varying GPR reflections allowed us to track the spatial and temporal dynamics of the tracer during the push-pull experiment. During the moving antenna experiments, we clearly imaged the dominant fractures in which tracer transport took place, fractures in which the tracer was trapped for longer time periods, and the spatial extent of the tracer distribution (up to 8 m) at different times. This demonstrated the existence of strongly channelized flow in the first few meters and radial flow at greater distances. By varying the resting time of a given experiment, we identified regions affected by density-driven and ambient flow. These experiments open up new perspectives for coupled hydrogeophysical inversion aimed at understanding transport phenomena in fractured rock formations.

  3. Site characterization and validation - measurement of flowrate, solute velocities and aperture variation in natural fractures as a function of normal and shear stress, stage 3

    International Nuclear Information System (INIS)

    Laboratory tests have been completed on natural fracture planes in three, 200 mm diameter, cores, to determine the effect of changes in normal and shear stress on fracture permeability and porosity. In each core, a single fracture plane was oriented parallel to the core axis and the flow and tracer tests were completed under linear flow boundary conditions. At the completion of the full stressflow test cycle, the fracture plane was impregnated with resin and, after the resin had hardened, the fracture plane was sectioned and the structure of the pore space characterized. The test data showed that there is linear relationship between the logarithm of flowrate and the logarithm of normal stress. For shear tests on the two main samples, which were conducted at shear stresses less than the peak shear strength, the flowrates decreased slightly with increase in shear displacement. The porosities determined from the resin data and the fluid velocities determined from the tracer tests show that the volume of fluid in the fracture plane is much greater than that predicted using equivalent smooth parallel plate model. (authors)

  4. Effects of simplifying fracture network representation on inert chemical migration in fracture-controlled aquifers

    Science.gov (United States)

    Wellman, T.P.; Shapiro, A.M.; Hill, M.C.

    2009-01-01

    While it is widely recognized that highly permeable 'large-scale' fractures dominate chemical migration in many fractured aquifers, recent studies suggest that the pervasive 'small-scale' fracturing once considered of less significance can be equally important for characterizing the spatial extent and residence time associated with transport processes. A detailed examination of chemical migration through fracture-controlled aquifers is used to advance this conceptual understanding. The influence of fracture structure is evaluated by quantifying the effects to transport caused by a systematic removal of fractures from three-dimensional discrete fracture models whose attributes are derived from geologic and hydrologic conditions at multiple field sites. Results indicate that the effects to transport caused by network simplification are sensitive to the fracture network characteristics, degree of network simplification, and plume travel distance, but primarily in an indirect sense since correlation to individual attributes is limited. Transport processes can be 'enhanced' or 'restricted' from network simplification meaning that the elimination of fractures may increase or decrease mass migration, mean travel time, dispersion, and tailing of the concentration plume. The results demonstrate why, for instance, chemical migration may not follow the classic advection-dispersion equation where dispersion approximates the effect of the ignored geologic structure as a strictly additive process to the mean flow. The analyses further reveal that the prediction error caused by fracture network simplification is reduced by at least 50% using the median estimate from an ensemble of simplified fracture network models, and that the error from network simplification is at least 70% less than the stochastic variability from multiple realizations. Copyright 2009 by the American Geophysical Union.

  5. Advanced Branching Control and Characterization of Inorganic Semiconducting Nanocrystals

    Energy Technology Data Exchange (ETDEWEB)

    Hughes, Steven Michael [Univ. of California, Berkeley, CA (United States)

    2007-01-01

    The ability to finely tune the size and shape of inorganic semiconducting nanocrystals is an area of great interest, as the more control one has, the more applications will be possible for their use. The first two basic shapes develped in nanocrystals were the sphere and the anistropic nanorod. the II_VI materials being used such as Cadmium Selenide (CdSe) and Cadmium Telluride (CdTe), exhibit polytypism, which allows them to form in either the hexagonally packed wurtzite or cubically packed zinc blende crystalline phase. The nanorods are wurtzite with the length of the rod growing along the c-axis. As this grows, stacking faults may form, which are layers of zinc blende in the otherwise wurtzite crystal. Using this polytypism, though, the first generation of branched crystals were developed in the form of the CdTe tetrapod. This is a nanocrystal that nucleates in the zincblend form, creating a tetrahedral core, on which four wurtzite arms are grown. This structure opened up the possibility of even more complex shapes and applications. This disseration investigates the advancement of branching control and further understanding the materials polytypism in the form of the stacking faults in nanorods.

  6. Microstructural and mechanical characterization of laser deposited advanced materials

    Science.gov (United States)

    Sistla, Harihar Rakshit

    Additive manufacturing in the form of laser deposition is a unique way to manufacture near net shape metallic components from advanced materials. Rapid solidification facilitates the extension of solid solubility, compositional flexibility and decrease in micro-segregation in the melt among other advantages. The current work investigates the employment of laser deposition to fabricate the following: 1. Functionally gradient materials: This allows grading dissimilar materials compositionally to tailor specific properties of both these materials into a single component. Specific compositions of the candidate materials (SS 316, Inconel 625 and Ti64) were blended and deposited to study the brittle intermetallics reported in these systems. 2. High entropy alloys: These are multi- component alloys with equiatomic compositions of 5 or more elements. The ratio of Al to Ni was decreased to observe the transition of solid solution from a BCC to an FCC crystal structure in the AlFeCoCrNi system. 3. Structurally amorphous alloys: Zr-based metallic glasses have been reported to have high glass forming ability. These alloys have been laser deposited so as to rapidly cool them from the melt into an amorphous state. Microstructural analysis and X-ray diffraction were used to study the phase formation, and hardness was measured to estimate the mechanical properties.

  7. Advances in the analysis and characterization of DLC coatings

    Energy Technology Data Exchange (ETDEWEB)

    Bellido-Gonzalez, V.; Hampshire, J.; Jones, A.H.S.; Allen, T.J.; Witts, J.; Teer, D.G.; Pierret, B. [Teer Coatings Ltd., Hartlebury Trading Estate, Worcestershire (United Kingdom)

    1998-01-01

    A series of new DLC coatings have been produced by magnetron sputtering using standard in-house equipment. Different tests have been carried out for the analysis and characterization of the coatings. By combining ball cratering with pin-on-disc, standard scratch and multiscratch tests, interesting information has been obtained (failure mechanism, wear properties, etc.). In addition, in combination with ball cratering, a novel method has been developed for the assessment of the refractive index of transparent and semi-transparent DLC films. In the pin-on-disc and multiscratch tests, the conductivity of the film was used to follow the wear progression (DLC has a relatively low electrical conductivity). This device can show local failures produced in the coating (indicated by an increase of film conductivity) which normally remains undetected in a frictional record. (orig.) 14 refs.

  8. Wetlands Assessment for site characterization, Advanced Neutron Source (ANS)

    Energy Technology Data Exchange (ETDEWEB)

    Wade, M.C.; Socolof, M.L. [Oak Ridge National Lab., TN (United States). Energy Div.; Rosensteel, B.; Awl, D. [JAYCOR, Vienna, VA (United States)

    1994-10-01

    This Wetlands Assessment has been prepared in accordance with the Department of Energy`s (DOE) Code of Federal Regulations (CFR) 10 CFR 1022, Compliance with Floodplain/Wetlands Environmental Review Requirements, which established the policy and procedure for implementing Executive Order 11990, Protection of Wetlands. The proposed action is to conduct characterization activities in or near wetlands at the ANS site. The proposed action will covered under a Categorical Exclusion, therefore this assessment is being prepared as a separate document [10 CFR 1022.12(c)]. The purpose of this Wetlands Assessment is to fulfill the requirements of 10 CFR 1022.12(a) by describing the project, discussing the effects of the proposed action upon the wetlands, and considering alternatives to the proposed action.

  9. Wetlands Assessment for site characterization, Advanced Neutron Source (ANS)

    International Nuclear Information System (INIS)

    This Wetlands Assessment has been prepared in accordance with the Department of Energy's (DOE) Code of Federal Regulations (CFR) 10 CFR 1022, Compliance with Floodplain/Wetlands Environmental Review Requirements, which established the policy and procedure for implementing Executive Order 11990, Protection of Wetlands. The proposed action is to conduct characterization activities in or near wetlands at the ANS site. The proposed action will covered under a Categorical Exclusion, therefore this assessment is being prepared as a separate document [10 CFR 1022.12(c)]. The purpose of this Wetlands Assessment is to fulfill the requirements of 10 CFR 1022.12(a) by describing the project, discussing the effects of the proposed action upon the wetlands, and considering alternatives to the proposed action

  10. An Integrated Approach to Characterizing Bypassed Oil in Heterogeneous and Fractured Reservoirs Using Partitioning Tracers

    Energy Technology Data Exchange (ETDEWEB)

    Akhil Datta-Gupta

    2006-12-31

    We explore the use of efficient streamline-based simulation approaches for modeling partitioning interwell tracer tests in hydrocarbon reservoirs. Specifically, we utilize the unique features of streamline models to develop an efficient approach for interpretation and history matching of field tracer response. A critical aspect here is the underdetermined and highly ill-posed nature of the associated inverse problems. We have investigated the relative merits of the traditional history matching ('amplitude inversion') and a novel travel time inversion in terms of robustness of the method and convergence behavior of the solution. We show that the traditional amplitude inversion is orders of magnitude more non-linear and the solution here is likely to get trapped in local minimum, leading to inadequate history match. The proposed travel time inversion is shown to be extremely efficient and robust for practical field applications. The streamline approach is generalized to model water injection in naturally fractured reservoirs through the use of a dual media approach. The fractures and matrix are treated as separate continua that are connected through a transfer function, as in conventional finite difference simulators for modeling fractured systems. A detailed comparison with a commercial finite difference simulator shows very good agreement. Furthermore, an examination of the scaling behavior of the computation time indicates that the streamline approach is likely to result in significant savings for large-scale field applications. We also propose a novel approach to history matching finite-difference models that combines the advantage of the streamline models with the versatility of finite-difference simulation. In our approach, we utilize the streamline-derived sensitivities to facilitate history matching during finite-difference simulation. The use of finite-difference model allows us to account for detailed process physics and compressibility effects

  11. Development and characterization of advanced electron beam resists

    Science.gov (United States)

    Agrawal, Ankur

    Over the past twenty years, the amount of research and development work for electron beam resists has seriously lagged that performed for optical resists. This has been due mainly to the relatively low volume use of electron beam lithography for production purposes. However, as electron beam lithography is now becoming the primary solution for achieving future critical dimension requirements in mask making and appears to be a promising NGL technology, interest in electron beam resist development has increased in recent years. The primary issue in electron beam resist design centers around finding a single resist system that combines the required sensitivity and etch resistance that is needed to enable high volume production. In this work, the primary goal was to explore the development of a novel two-component non-chemically amplified electron beam resist material for high keV (>10 keV) patterning for mask-making with: (1) high contrast, (2) high sensitivity, (3) high resolution, and, (4) high etch resistance. Poly (2-methyl-1-pentene co 2-ethoxyethyl-methallyl ether sulfone) was used as a polymeric e-beam sensitive material conjunction with a series of commercial novolac resins to formulate electron beam resists. These two-component resists have been termed sulfone-novolac system (SNS) resists. The approach used in this project is to develop a suite of experimental tools and simulation models that can be used to aid in the rational design, formulation, and characterization of new electron beam resists. The main tasks that have been addressed are: (1) development of the electron beam resist characterization tool set, (2) understanding the fundamental material behavior of a non-chemically amplified polysulfone-novolac (SNS) e-beam resist for next generation mask making, (3) lithographic process development and optimization for the SNS resists, (4) evaluation of the lithographic performance of the SNS resists using the optimized processing conditions, and (5) develop

  12. Grouting design based on characterization of the fractured rock. Presentation and demonstration of a methodology

    International Nuclear Information System (INIS)

    The design methodology presented in this document is based on an approach that considers the individual fractures. The observations and analyses made during production enable the design to adapt to the encountered conditions. The document is based on previously published material and overview flow charts are used to show the different steps. Parts of or the full methodology has been applied for a number of tunneling experiments and projects. SKB projects in the Aespoe tunnel include a pillar experiment and pre-grouting of a 70 meter long tunnel (TASQ). Further, for Hallandsas railway tunnel (Skaane south Sweden), a field pre-grouting experiment and design and post-grouting of a section of 133 meters have been made. For the Nygard railway tunnel (north of Goeteborg, Sweden), design and grouting of a section of 86 meters (pre-grouting) and 60 meters (post-grouting) have been performed. Finally, grouting work at the Tornskog tunnel (Stockholm, Sweden) included design and grouting along a 100 meter long section of one of the two tunnel tubes. Of importance to consider when doing a design and evaluating the result are: - The identification of the extent of the grouting needed based on inflow requirements and estimates of tunnel inflow before grouting. - The selection of grout and performance of grouting materials including penetration ability and length. The penetration length is important for the fan geometry design. - The ungrouted compared to the grouted and excavated rock mass conditions: estimates of tunnel inflow and (if available) measured inflows after grouting and excavation. Identify if possible explanations for deviations. For the Hallandsas, Nygard and Tornskog tunnel sections, the use of a Pareto distribution and the estimate of tunnel inflow identified a need for sealing small aperture fractures (< 50 - 100 μm) to meet the inflow requirements. The tunneling projects show that using the hydraulic aperture as a basis for selection of grout is a good

  13. Fracture and vein characterization of a crystalline basement reservoir, central Yemen

    Science.gov (United States)

    Veeningen, R.; Grasemann, B.; Decker, K.; Bischoff, R.; Rice, A. H. N.

    2012-04-01

    The country of Yemen is located in the south-western part of the Arabian plate. The Pan-African basement found in western and central Yemen is highly deformed during the Proterozoic eon and is part of the Arabian-Nubian shield ANS (670-540Ma). This ANS is a result of the amalgamation of high-grade gneiss terranes and low-grade island arcs. The development of an extensive horst-and-graben system related to the breakup of Gondwana in the Mesozoic, has reactivated the Pan-African basement along NW-SE trending normal faults. As a result, younger Meosozoic marls, sandstones, clastics and limestones are unconformably overlying the basement. Some of these formations act as a source and/or reservoir for hydrocarbons. Due to fracturing of the basement, hydrocarbons have migrated horizontally into the basement, causing the crystalline basement to be a potential hydrocarbon reservoir. Unfortunately, little is known about the Pan-African basement in Central Yemen and due its potential as a reservoir, the deformation and oil migration history (with a main focus on the fracturing and veining history) of the basement is investigated in high detail. Representative samples are taken from 2 different wells from the Habban Field reservoir, located approximately 320 ESE of Sana'a. These samples are analysed using e.g. the Optical Microscope, SEM, EDX and CL, but also by doing Rb-Sr age dating, isotope analysis and fluid inclusion analysis. In well 1, the only lithology present is an altered gneiss with relative large (<5 cm diameter) multi-mineralic veins. In well 3, quartzite (top), gneiss (middle) and quartz porphyry's (middle) are intruded by a so called "younger" granitoid body (592.6±4.1Ma). All lithologies record polyphase systems of mineral veins. Pyrite and saddle dolomite in these veins have euhedral shapes, which means that they have grown in open cavities. Calcite is the youngest mineral in these veins, closing the vein and aborting the fluid flow. Fluid inclusions inside

  14. Advancements in waste water characterization through NMR spectroscopy: review.

    Science.gov (United States)

    Alves Filho, Elenilson G; Alexandre e Silva, Lorena M; Ferreira, Antonio G

    2015-09-01

    There are numerous organic pollutants that lead to several types of ecosystem damage and threaten human health. Wastewater treatment plants are responsible for the removal of natural and anthropogenic pollutants from the sewage, and because of this function, they play an important role in the protection of human health and the environment. Nuclear magnetic resonance (NMR) has proven to be a valuable analytical tool as a result of its versatility in characterizing both overall chemical composition as well as individual species in a wide range of mixtures. In addition, NMR can provide physical information (rigidity, dynamics, etc.) as well as permit in depth quantification. Hyphenation with other techniques such as liquid chromatography, solid phase extraction and mass spectrometry creates unprecedented capabilities for the identification of novel and unknown chemical species. Thus, NMR is widely used in the study of different components of wastewater, such as complex organic matter (fulvic and humic acids), sludge and wastewater. This review article summarizes the NMR spectroscopy methods applied in studies of organic pollutants from wastewater to provide an exhaustive review of the literature as well as a guide for readers interested in this topic. PMID:25280056

  15. Advanced optical measurements for characterizing photophysical properties of single nanoparticles.

    Energy Technology Data Exchange (ETDEWEB)

    Polsky, Ronen; Davis, Ryan W.; Arango, Dulce C.; Brozik, Susan Marie; Wheeler, David Roger

    2009-09-01

    Formation of complex nanomaterials would ideally involve single-pot reaction conditions with one reactive site per nanoparticle, resulting in a high yield of incrementally modified or oriented structures. Many studies in nanoparticle functionalization have sought to generate highly uniform nanoparticles with tailorable surface chemistry necessary to produce such conjugates, with limited success. In order to overcome these limitations, we have modified commercially available nanoparticles with multiple potential reaction sites for conjugation with single ssDNAs, proteins, and small unilamellar vesicles. These approaches combined heterobifunctional and biochemical template chemistries with single molecule optical methods for improved control of nanomaterial functionalization. Several interesting analytical results have been achieved by leveraging techniques unique to SNL, and provide multiple paths for future improvements for multiplex nanoparticle synthesis and characterization. Hyperspectral imaging has proven especially useful for assaying substrate immobilized fluorescent particles. In dynamic environments, temporal correlation spectroscopies have been employed for tracking changes in diffusion/hydrodynamic radii, particle size distributions, and identifying mobile versus immobile sample fractions at unbounded dilution. Finally, Raman fingerprinting of biological conjugates has been enabled by resonant signal enhancement provided by intimate interactions with nanoparticles and composite nanoshells.

  16. Quantifying Fracture Heterogeneity in Different Domains of Folded Carbonate Rocks to Improve Fractured Reservoir Analog Fluid Flow Models

    NARCIS (Netherlands)

    Bisdom, K.; Bertotti, G.; Gauthier, B.D.M.; Hardebol, N.J.

    2013-01-01

    Fluid flow in carbonate reservoirs is largely controlled by multiscale fracture networks. Significant variations of fracture network porosity and permeability are caused by the 3D heterogeneity of the fracture network characteristics, such as intensity, orientation and size. Characterizing fracture

  17. Recent advances in processing and characterization of edgeless detectors

    Science.gov (United States)

    Wu, X.; Kalliopuska, J.; Eränen, S.; Virolainen, T.

    2012-02-01

    During past five years VTT has actively developed edgeless detector fabrication process. The straightforward and high yield process relies on ion-implantation to activate the edges of the detector. A recent fabrication process was performed at VTT to provide p-on-n edgeless detectors. The layout contained DC- and AC-coupled strip detector and pixel detectors for Medipix/Timepix readouts. The fabricated detector thicknesses were 50, 100 and 150 μm. Electrical characterization was done for 5 × 5 mm2 edgeless diodes on wafer level. All measured electrical parameters showed a dramatic dependence on the diode thickness. Leakage current was measured below 10 nA/cm2 at full depletion. Calculation using a theoretical approximation indicates the diode surface generation current of less than 300 pA. The breakdown voltages were measured to be above 140 V and increased as a function of diode thickness. Reverse bias of 10 V is enough to fully deplete designed edgeless diodes. Leakage current dependence of temperature was investigated for both p-on-n and previous n-on-n edgeless detectors and results show that the leakage current doubles for every 8.5 degree Celsius rise in temperature. TCAD device simulations reveal that breakdown occurs at the lateral p-n junction where the electric field reaches its highest value. Thick edgeless diodes have wider bulk space that allows electric potential to drop and causes smaller curvature of the equipotential lines. This releases the accumulation of electric field at the corner of anode and increases the breakdown voltage. A good match of the simulated and the measured capacitance-voltage curves enables identification of proper parameters used in the simulation.

  18. Structural level characterization of base oils using advanced analytical techniques

    KAUST Repository

    Hourani, Nadim

    2015-05-21

    Base oils, blended for finished lubricant formulations, are classified by the American Petroleum Institute into five groups, viz., groups I-V. Groups I-III consist of petroleum based hydrocarbons whereas groups IV and V are made of synthetic polymers. In the present study, five base oil samples belonging to groups I and III were extensively characterized using high performance liquid chromatography (HPLC), comprehensive two-dimensional gas chromatography (GC×GC), and Fourier transform ion cyclotron resonance mass spectrometry (FT-ICR MS) equipped with atmospheric pressure chemical ionization (APCI) and atmospheric pressure photoionization (APPI) sources. First, the capabilities and limitations of each analytical technique were evaluated, and then the availed information was combined to reveal compositional details on the base oil samples studied. HPLC showed the overwhelming presence of saturated over aromatic compounds in all five base oils. A similar trend was further corroborated using GC×GC, which yielded semiquantitative information on the compound classes present in the samples and provided further details on the carbon number distributions within these classes. In addition to chromatography methods, FT-ICR MS supplemented the compositional information on the base oil samples by resolving the aromatics compounds into alkyl- and naphtheno-subtituted families. APCI proved more effective for the ionization of the highly saturated base oil components compared to APPI. Furthermore, for the detailed information on hydrocarbon molecules FT-ICR MS revealed the presence of saturated and aromatic sulfur species in all base oil samples. The results presented herein offer a unique perspective into the detailed molecular structure of base oils typically used to formulate lubricants. © 2015 American Chemical Society.

  19. CHARACTERIZATION OF THE FRACTURE WORK FOR DUCTILE FILM UNDERGOING THE MICRO-SCRATCH

    Institute of Scientific and Technical Information of China (English)

    魏悦广; 赵满洪; 唐山

    2002-01-01

    The interface adhesion strength (or interface toughness) of a thinfilm/substrate system is often assessed by the micro-scratch test. For a brittle filmmaterial, the interface adhesion strength is easily obtained through measuring thescratch driving forces. However, to measure the interface adhesion strength (or in-terface toughness) for a metal thin film material (the ductile material) by the micro-scratch test is very difficult, because intense plastic deformation is involved and theproblem is a three-dimensional elastic-plastic one. In the present research, usinga double-cohesive zone model, the failure characteristics of the thin film/substratesystem can be described and further simulated. For a steady-state scratching pro-cess, a three-dimensional elastic-plastic finite element method based on the doublecohesive zone model is developed and adopted, and the steady-state fracture workof the total system is calculated. The parameter relations between the horizontaldriving forces (or energy release rate of the scratching process) and the separationstrength of thin film/substrate interface, and the material shear strength, as well asthe material parameters are developed. Furthermore, a scratch experiment for theAl/Si film/substrate system is carried out and the failure mechanisms are explored.Finally, the prediction results are applied to a scratch experiment for the Pt/NiOmaterial system given in the literature.

  20. Characterization of Fatty Acid Composition in Bone Marrow Fluid From Postmenopausal Women: Modification After Hip Fracture.

    Science.gov (United States)

    Miranda, Melissa; Pino, Ana María; Fuenzalida, Karen; Rosen, Clifford J; Seitz, Germán; Rodríguez, J Pablo

    2016-10-01

    Bone marrow adipose tissue (BMAT) is associated with low bone mass, although the functional consequences for skeletal maintenance of increased BMAT are currently unclear. BMAT might have a role in systemic energy metabolism, and could be an energy source as well as an endocrine organ for neighboring bone cells, releasing cytokines, adipokines and free fatty acids into the bone marrow microenvironment. The aim of the present report was to compare the fatty acid composition in the bone marrow supernatant fluid (BMSF) and blood plasma of postmenopausal women women (65-80 years old). BMSF was obtained after spinning the aspirated bone marrow samples; donors were classified as control, osteopenic or osteoporotic after dual-energy X-ray absorptiometry. Total lipids from human bone marrow fluid and plasma were extracted, converted to the corresponding methyl esters, and finally analyzed by a gas chromatographer coupled with a mass spectrometer. Results showed that fatty acid composition in BMSF was dynamic and distinct from blood plasma, implying significance in the locally produced lipids. The fatty acid composition in the BMSF was enriched in saturated fatty acid and decreased in unsaturated fatty acids as compared to blood plasma, but this relationship switched in women who suffered a hip fracture. On the other hand, there was no relationship between BMSF and bone mineral density. In conclusion, lipid composition of BMSF is distinct from the circulatory compartment, most likely reflecting the energy needs of the marrow compartment. J. Cell. Biochem. 117: 2370-2376, 2016. © 2016 Wiley Periodicals, Inc.

  1. Advances in acrylic-alkyd hybrid synthesis and characterization

    Science.gov (United States)

    Dziczkowski, Jamie

    2008-10-01

    performance. Reversible-addition fragmentation polymerization techniques were employed to create a new class of acrylic-alkyd hybrid materials. Medium and long oil alkyds made from the monoglyceride process using soybean oil, glycerol, and phthalic anhydride were modified with a RAFT chain transfer agent. The alkyd macro-RAFT agents were reached by end-capping a medium oil soya-based alkyd with a carboxy-functional trithiocarbonate. The alkyd macro-RAFT agents were then used to create acrylic-alkyd block structures by polymerizing different acrylic monomers, including both acrylates and methacrylates in the presence of the macro-RAFT agent and 2, 2'-azobisisobutyronitrile (AIBN). Co-acrylic segments were reached by complete polymerization of one monomer followed by the addition of a second monomer and additional free radical initiator. The alkyds, macro-RAFT agents and, acrylic-alkyd blocks were characterized by size-exclusion chromatography (SEC), FTIR, and 1H-NMR. Pseudo-first-order kinetics behavior and conversion vs. molecular weight plots show that the RAFT-mediated reaction afforded a more controlled process for the synthesis of acrylated-alkyd materials. Preliminary coatings tests showed that material properties of acrylated-alkyds achieved by RAFT polymerization exhibit good overall coatings properties including adhesion, gloss, hardness, and impact resistance.

  2. Characterization and evaluation of sites for deep geological disposal of radioactive waste in fractured rocks. Proceedings

    International Nuclear Information System (INIS)

    The third Aespoe International Seminar was organised by SKB to assess the state of the art in characterisation and evaluation of sites for deep geological disposal of radioactive waste in fractured rocks. Site characterisation and evaluation are important elements for determining the site suitability and long-term safety of a geological repository for radioactive waste disposal. Characterisation work also provides vital information for the design of the underground facility and the engineered barrier system that will contain the waste. The aim of the seminar was to provide a comprehensive assessment of the current know-how on this topic based on world-wide experience from more than 20 years of characterisation and evaluation work. The seminar, which was held at the Aespoe Hard Rock Laboratory was attended by 72 scientists from 10 different countries. The program was divided into four sessions of which two were run in parallel. A total of 38 oral and 5 poster presentations were given at the seminar. The presentations gave a comprehensive summary of recently completed and current work on site characterisation, modelling and application in performance assessments. The results presented at the seminar generally show that significant progress has been made in this field during the last decade. New characterisation techniques have become available, strategies for site investigations have developed further, and model concepts and codes have reached new levels of refinement. Data obtained from site characterisation have also successfully been applied in several site specific performance assessments. The seminar clearly showed that there is a solid scientific basis for assessing the suitability of sites for actual repositories based on currently available site characterisation technology and modelling capabilities. Separate abstracts have been prepared for 38 of the presentations

  3. Characterization and evaluation of sites for deep geological disposal of radioactive waste in fractured rocks. Proceedings

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1998-09-01

    The third Aespoe International Seminar was organised by SKB to assess the state of the art in characterisation and evaluation of sites for deep geological disposal of radioactive waste in fractured rocks. Site characterisation and evaluation are important elements for determining the site suitability and long-term safety of a geological repository for radioactive waste disposal. Characterisation work also provides vital information for the design of the underground facility and the engineered barrier system that will contain the waste. The aim of the seminar was to provide a comprehensive assessment of the current know-how on this topic based on world-wide experience from more than 20 years of characterisation and evaluation work. The seminar, which was held at the Aespoe Hard Rock Laboratory was attended by 72 scientists from 10 different countries. The program was divided into four sessions of which two were run in parallel. A total of 38 oral and 5 poster presentations were given at the seminar. The presentations gave a comprehensive summary of recently completed and current work on site characterisation, modelling and application in performance assessments. The results presented at the seminar generally show that significant progress has been made in this field during the last decade. New characterisation techniques have become available, strategies for site investigations have developed further, and model concepts and codes have reached new levels of refinement. Data obtained from site characterisation have also successfully been applied in several site specific performance assessments. The seminar clearly showed that there is a solid scientific basis for assessing the suitability of sites for actual repositories based on currently available site characterisation technology and modelling capabilities. Separate abstracts have been prepared for 38 of the presentations

  4. Application of reservoir characterization and advanced technology to improve recovery and economics in a lower quality shallow shelf carbonate reservoir. End of budget period report, August 3, 1994--December 31, 1996

    Energy Technology Data Exchange (ETDEWEB)

    Taylor, A.R.; Hinterlong, G.; Watts, G.; Justice, J.; Brown, K.; Hickman, T.S.

    1997-12-01

    The Oxy West Welch project is designed to demonstrate how the use of advanced technology can improve the economics of miscible CO{sub 2} injection projects in a lower quality shallow shelf carbonate reservoir. The research and design phase primarily involves advanced reservoir characterization and accelerating the production response. The demonstration phase will implement the reservoir management plan based on an optimum miscible CO{sub 2} flood as designed in the initial phase. During Budget Period 1, work was completed on the CO{sub 2} stimulation treatments and the hydraulic fracture design. Analysis of the CO{sub 2} stimulation treatment provided a methodology for predicting results. The hydraulic fracture treatment proved up both the fracture design approach a and the use of passive seismic for mapping the fracture wing orientation. Although the 3-D seismic interpretation is still being integrated into the geologic model and interpretation of borehole seismic is still underway, the simulator has been enhanced to the point of giving good waterflood history matches. The simulator-forecasted results for an optimal designed miscible CO{sub 2} flood in the demonstration area gave sufficient economics to justify continuation of the project into Budget Period 2.

  5. Advanced approaches to characterize the human intestinal microbiota by computational meta-analysis

    NARCIS (Netherlands)

    Nikkilä, J.; Vos, de W.M.

    2010-01-01

    GOALS: We describe advanced approaches for the computational meta-analysis of a collection of independent studies, including over 1000 phylogenetic array datasets, as a means to characterize the variability of human intestinal microbiota. BACKGROUND: The human intestinal microbiota is a complex micr

  6. Amplitude inversion of fast and slow converted waves for fracture characterization of the Montney Formation in Pouce Coupe field, Alberta, Canada

    Science.gov (United States)

    MacFarlane, Tyler L.

    The Montney Formation of western Canada is one of the largest economically viable gas resource plays in North America with reserves of 449TCF. As an unconventional tight gas play, the well development costs are high due to the hydraulic stimulations necessary for economic success. The Pouce Coupe research project is a multidisciplinary collaboration between the Reservoir Characterization Project (RCP) and Talisman Energy Inc. with the objective of understanding the reservoir to enable the optimization of well placement and completion design. The work in this thesis focuses on identifying the natural fractures in the reservoir that act as the delivery systems for hydrocarbon flow to the wellbore. Characterization of the Montney Formation at Pouce Coupe is based on time-lapse multicomponent seismic surveys that were acquired before and after the hydraulic stimulation of two horizontal wells. Since shear-wave velocities and amplitudes of the PS-waves are known to be sensitive to near-vertical fractures, I utilize isotropic simultaneous seismic inversions on azimuthally-sectored PS1 and PS2 data sets to obtain measurements of the fast and slow shear-velocities. Specifically, I analyze two orthogonal azimuths that are parallel and perpendicular to the strike of the dominant fracture system in the field. These volumes are used to approximate the shear-wave splitting parameter (gamma(s*)) that is closely related to crack density. Since crack density has a significant impact on defining the percolation zone, the work presented in this thesis provides information that can be utilized to reduce uncertainty in the reservoirs fracture model. Isotropic AVO inversion of azimuthally limited PS-waves demonstrates sufficient sensitivity to detect contrast between the anisotropic elastic properties of the reservoir and is capable of identifying regions with high crack density. This is supported by integration with spinner production logs, hydraulic stimulation history of the field

  7. Experimental and Numerical Study on the Cracked Chevron Notched Semi-Circular Bend Method for Characterizing the Mode I Fracture Toughness of Rocks

    Science.gov (United States)

    Wei, Ming-Dong; Dai, Feng; Xu, Nu-Wen; Liu, Jian-Feng; Xu, Yuan

    2016-05-01

    The cracked chevron notched semi-circular bending (CCNSCB) method for measuring the mode I fracture toughness of rocks combines the merits (e.g., avoidance of tedious pre-cracking of notch tips, ease of sample preparation and loading accommodation) of both methods suggested by the International Society for Rock Mechanics, which are the cracked chevron notched Brazilian disc (CCNBD) method and the notched semi-circular bend (NSCB) method. However, the limited availability of the critical dimensionless stress intensity factor (SIF) values severely hinders the widespread usage of the CCNSCB method. In this study, the critical SIFs are determined for a wide range of CCNSCB specimen geometries via three-dimensional finite element analysis. A relatively large support span in the three point bending configuration was considered because the fracture of the CCNSCB specimen in that situation is finely restricted in the notch ligament, which has been commonly assumed for mode I fracture toughness measurements using chevron notched rock specimens. Both CCNSCB and NSCB tests were conducted to measure the fracture toughness of two different rock types; for each rock type, the two methods produce similar toughness values. Given the reported experimental results, the CCNSCB method can be reliable for characterizing the mode I fracture toughness of rocks.

  8. Pre- and post-stimulation characterization of geothermal well GRT-1, Rittershoffen, France: insights from acoustic image logs of hard fractured rock

    Science.gov (United States)

    Vidal, Jeanne; Genter, Albert; Schmittbuhl, Jean

    2016-05-01

    Geothermal well GRT-1 (Rittershoffen, Alsace) was drilled in 2012. Its open-hole section (extending down to a depth of 2.6 km) penetrated fractured sandstones and granite. In 2013, the well was subjected to Thermal, Chemical and Hydraulic (TCH) stimulation, which improved the injectivity index five-fold. The goal of the study was to assess the impact of the stimulation by comparing pre- and post-stimulation logs and well-logging (temperature [T] log) and mud-logging data. This comparison revealed modifications of almost all the natural fractures. However, not all of these fractures are associated with permeability enhancement, and the post-stimulation T logs are important for characterizing this enhancement. Chemical alteration due to mechanical erosion at the tops and bottoms of the fractures was observed in the sandstones. These zones display indications of very small new permeability after the TCH stimulation. Because a major fault zone caved extensively where it crosses the borehole, it was not imaged in the acoustic logs. However, this originally permeable zone was enhanced as demonstrated by the T logs. Based on the natural injectivity of this fault zone, hydraulic erosion and thermal microcracking of its internal quartz veins are associated with this permeability enhancement. Although local changes in the borehole wall observed in the acoustic images cannot be directly linked to the improved injectivity index, the comparison of the acoustic image logs allows for identification of fracture zones impacted by the TCH stimulation.

  9. Pre- and post-stimulation characterization of geothermal well GRT-1, Rittershoffen, France: insights from acoustic image logs of hard fractured rock

    Science.gov (United States)

    Vidal, Jeanne; Genter, Albert; Schmittbuhl, Jean

    2016-08-01

    Geothermal well GRT-1 (Rittershoffen, Alsace) was drilled in 2012. Its open-hole section (extending down to a depth of 2.6 km) penetrated fractured sandstones and granite. In 2013, the well was subjected to Thermal, Chemical and Hydraulic (TCH) stimulation, which improved the injectivity index fivefold. The goal of the study was to assess the impact of the stimulation by comparing pre- and post-stimulation well-logging (acoustic and temperature [T] logs) and mud-logging data. This comparison revealed modifications of almost all the natural fractures. However, not all of these fractures are associated with permeability enhancement, and the post-stimulation T logs are important for characterizing this enhancement. Chemical alteration due to mechanical erosion at the tops and bottoms of the fractures was observed in the sandstones. These zones display indications of very small new permeability after the TCH stimulation. Because a major fault zone caved extensively where it crosses the borehole, it was not imaged in the acoustic logs. However, this originally permeable zone was enhanced as demonstrated by the T logs. Based on the natural injectivity of this fault zone, hydraulic erosion and thermal microcracking of its internal quartz veins are associated with this permeability enhancement. Although local changes in the borehole wall observed in the acoustic images cannot be directly linked to the improved injectivity index, the comparison of the acoustic image logs allows for identification of fracture zones impacted by the TCH stimulation.

  10. Characterization of the mechanisms controlling the permeability changes of fractured cements flowed through by CO2-rich brine.

    Science.gov (United States)

    Abdoulghafour, H; Luquot, L; Gouze, P

    2013-09-17

    Experiments were conducted to assess the potential impact of fractured well-cement degradation on leakage rate. Permeability was monitored while CO2-enriched reservoir-equilibrated brine was flowed at constant rate through a single fracture in a class G cement core under conditions mimicking geologic sequestration environments (temperature 60 °C, pressure 10 MPa). The results demonstrate that, at least for the conditions used in the experiment, an initial leakage in a 42 μm aperture fracture (permeability = 1.5 × 10(-10) m(2)) can be self-mitigated due to the decrease of the fracture hydraulic aperture after about 15 h. This decrease results from the development of continuous highly hydrated amorphous Si-rich alteration products at the edge of the fracture and the dense carbonation of the bulk cement that mitigate the penetration of the alteration front. PMID:23937192

  11. Characterization and simulation of an exhumed fractured petroleum reservoir. Final report, March 18, 1996--September 30, 1998

    Energy Technology Data Exchange (ETDEWEB)

    Forster, C.B.; Nielson, D.L.; Deo, M.

    1998-12-01

    An exhumed fractured reservoir located near Alligator Ridge in central Nevada provides the basis for developing and testing different approaches for simulating fractured petroleum reservoirs. The fractured analog reservoir comprises a 90 m thickness of silty limestone and shaly interbeds within the Devonian Pilot Shale. A period of regional compression followed by ongoing basin and range extension has created faults and fractures that, in tern, have controlled the migration of both oil and gold ore-forming fluids. Open pit gold mines provide access for observing oil seepage, collecting the detailed fracture data needed to map variations in fracture intensity near faults, build discrete fracture network models and create equivalent permeability structures. Fault trace patterns mapped at the ground surface provide a foundation for creating synthetic fault trace maps using a stochastic procedure conditioned by the outcrop data. Conventional simulations of petroleum production from a 900 by 900 m sub-domain within the reservoir analog illustrate the possible influence of faults and fractures on production. The consequences of incorporating the impact of different stress states (e.g., extension, compression or lithostatic) are also explored. Simulating multiphase fluid flow using a discrete fracture, finite element simulator illustrates how faults acting as conduits might be poorly represented by the upscaling procedures used to assign equivalent permeability values within reservoir models. The parallelized reservoir simulators developed during this project provide a vehicle to evaluate when it might be necessary to incorporate very fine scale grid networks in conventional reservoir simulators or to use finely gridded discrete fracture reservoir simulators.

  12. A New Method to Infer Advancement of Saline Front in Coastal Groundwater Systems by 3D: The Case of Bari (Southern Italy Fractured Aquifer

    Directory of Open Access Journals (Sweden)

    Costantino Masciopinto

    2016-02-01

    Full Text Available A new method to study 3D saline front advancement in coastal fractured aquifers has been presented. Field groundwater salinity was measured in boreholes of the Bari (Southern Italy coastal aquifer with depth below water table. Then, the Ghyben-Herzberg freshwater/saltwater (50% sharp interface and saline front position were determined by model simulations of the freshwater flow in groundwater. Afterward, the best-fit procedure between groundwater salinity measurements, at assigned water depth of 1.0 m in boreholes, and distances of each borehole from the modelled freshwater/saltwater saline front was used to convert each position (x, y in groundwater to the water salinity concentration at depth of 1.0 m. Moreover, a second best-fit procedure was applied to the salinity measurements in boreholes with depth z. These results provided a grid file (x, y, z, salinity suitable for plotting the actual Bari aquifer salinity by 3D maps. Subsequently, in order to assess effects of pumping on the saltwater-freshwater transition zone in the coastal aquifer, the Navier-Stokes (N-S equations were applied to study transient density-driven flow and salt mass transport into freshwater of a single fracture. The rate of seawater/freshwater interface advancement given by the N-S solution was used to define the progression of saline front in Bari groundwater, starting from the actual salinity 3D map. The impact of pumping of 335 L·s−1 during the transition period of 112.8 days was easily highlighted on 3D salinity maps of Bari aquifer.

  13. Role of the advanced microstructures characterization in modeling of mechanical properties of AHSS steels

    Energy Technology Data Exchange (ETDEWEB)

    Radwański, Krzysztof, E-mail: kradwanski@imz.pl; Wrożyna, Andrzej, E-mail: awrozyna@imz.pl; Kuziak, Roman, E-mail: rkuziak@imz.pl

    2015-07-15

    Detailed knowledge of the fraction, morphology and chemical composition of phase constituents and their effect on the mechanical properties play a crucial role in understanding of the mechanisms influencing the properties of Advanced High Strength Steels (AHSS). On the other hand, the most important microstructural features of these steels are characterized by different size, starting from the nano- and ending on the microscale. Therefore, a detailed characterization of the AHSS microstructure must involve many methods capable of tracing the microstructure at different scale levels. The paper presents selected capabilities of advanced analytical techniques, in combination with conventional light optical microscopy (LOM), for quantitative characterization of the microstructure developed in AHSS steels during thermomechanical processing or continuous annealing. The material used for the investigation comprised the samples of DP steel sheet produced at the industrial scale. Special emphasis was focused on the capabilities of the Field Emission Gun Scanning Electron Microscopy (FEG SEM) combined with EBSD of microstructural characterization. The significance of accurate microstructure characterization for the modeling of mechanical properties of AHSS steels was demonstrated for the case of numerical calculation of the stress–strain curve in the standard tensile test. The work results indicate that such an engineering approach is useful for prediction of material properties.

  14. Characterization of plasma-induced phenol advanced oxidation process in a DBD reactor

    OpenAIRE

    Marotta, E.; Ceriani, E.; Shapoval, V.; Schiorlin, M.; Ceretta, C.; Rea, M.; Paradisi, C.

    2011-01-01

    Abstract Using phenol as a model organic pollutant we studied and characterized an innovative advanced oxidation process in water using a prototype dielectric barrier discharge (DBD) reactor in which electrical discharges are produced in the air above the water surface. Phenol is decomposed quite efficiently in this reactor operated at room temperature and atmospheric pressure. The process selectivity to form CO2 is, however, to be improved since a large fraction of the treated org...

  15. Development of a Prototype Photoacoustic Microscope and Spectroscope and Advanced Semiconductor Material Characterization

    OpenAIRE

    Xu, L.

    2012-01-01

    The thesis can be divided into two parts. In the first part of my thesis, I present the design, construction and test results of a prototype gas-cell Photoacoustic (PA) Spectrometer and Microscope. It is a low cost, non-contact technique, which can be used to characterize semiconductor band-gap structures and subsurface defects. It requires no liquid coupling and no sample surface preparation in advance. The instrument development includes the optical system design, mechani...

  16. A multidimensional horizontal-loop controlled-source electromagnetic inversion method and its use to characterize heterogeneity in aquiferous fractured crystalline rocks

    Science.gov (United States)

    Sasaki, Yutaka; Meju, Max A.

    2006-07-01

    The controlled-source dual horizontal-loop harmonic electromagnetic (HLEM) profiling method is well suited to the problem of investigating fracture zones in crystalline rocks but there are still limitations in the way that experimental data are currently interpreted-the use of 1-D data inversion leads to inaccurate determination of geological structure. To allow accurate characterization of zones of fractured rock especially underneath heterogeneous overburden, we have developed an efficient 2.5-D regularized inversion method for reconstructing subsurface electrical resistivity distributions from multifrequency HLEM data, with the forward problem solved in 3-D using a staggered-grid finite-difference method. The inversion method is validated using a synthetic example and practical data sets from four borehole sites in a granitic terrain in northeast Brazil. An appraisal of our results for sites with boreholes sited using conventional data analysis procedures shows that we can distinguish between optimally located productive wells in fracture-zone lineaments and those with diminished yields in weathered layer with no major underlying fracture zones. We suggest that 2.5-D inversion can aid in developing better strategies for sustainable groundwater resource development in the basement terrains.

  17. SACRAL FRACTURES

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    Objective. To delineate the clinical spectrum and treatment choice of sacral fractures.Methods. In this series, 39 sacral fractures were retrospectively reviewed and classified utilizing Denis′ classification. There were 21 Zone Ⅰ fractures, 6 Zone Ⅱ fractures and 12 Zone Ⅲ fractures. Neurological deficits were present in seven patients. Thirty seven patients were treated conservatively and two underwent surgical management.Results.Thirty eight patients were followed up for three months to 19 years. Thirty three have recovered, four improved, and one remained disabled.Conclusion.The treatment of sacral fractures requires assessment of pelvic stability and existing nerve injury. The patients with pelvic ring instability and neurological deficits should be treated with fracture reduction and stability reconstruction. When the patients with pelvic fracture are complicated with neurological deficits, sacral fracture should be first suspected. Once the diagnosis of sacral fracture is made, fracture reduction should be indicated. Conservative treatment usually permits satisfactory results.

  18. Characterization of fracture reservoirs using static and dynamic data: From sonic and 3D seismic to permeability distribution

    Energy Technology Data Exchange (ETDEWEB)

    Parra, J.O.; Hackett, C.L.; Brown, R.L.; Collier, H.A.; Datta-Gupta, A.

    1998-10-01

    To characterize the Buena Vista Hills field, the authors have implemented methods of modeling, processing and interpretation. The modeling methods are based on deterministic and stochastic solutions. Deterministic solutions were developed in Phase 1 and applied in Phase 2 to simulate acoustic responses of laminated reservoirs. Specifically, the simulations were aimed at implementing processing techniques to correct P-wave and S-wave velocity logs for scattering effects caused by thin layering. The authors are also including a summary of the theory and the processing steps of this new method for predicting intrinsic dispersion and attenuation in Section 2. Since the objective for correcting velocity scattering effects is to predict intrinsic dispersion from velocity data, they are presenting an application to illustrate how to relate permeability anisotropy with intrinsic dispersion. Also, the theoretical solution for calculating full waveform dipole sonic that was developed in Phase 1 was applied to simulate dipole responses at different azimuthal source orientations. The results will be used to interpret the effects of anisotropy associated with the presence of vertical fractures at Buena Vista Hills. The results of the integration of core, well logs, and geology of Buena Vista Hills is also given in Section 2. The results of this integration will be considered as the input model for the inversion technique for processing production data. Section 3 summarizes accomplishments. In Section 4 the authors present a summary of the technology transfer and promotion efforts associated with this project. In the last section, they address the work to be done in the next six months and future work by applying the processing, modeling and inversion techniques developed in Phases 1 and 2 of this project.

  19. Application of reservoir characterization and advanced technology to improve recovery and economics in a lower quality shallow shelf San Andres Reservoir. Quarterly Report for the period: 1 April - 30 June 2001

    International Nuclear Information System (INIS)

    The Class 2 Project at West Welch was designed to demonstrate the use of advanced technologies to enhance the economics of improved oil recovery (IOR) projects in lower quality Shallow Shelf Carbonate (SSC) reservoirs, resulting in recovery of additional oil that would otherwise be left in the reservoir at project abandonment. Accurate reservoir description is critical to the effective evaluation and efficient design of IOR projects in the heterogeneous SSC reservoirs. Therefore, the majority of Budget Period 1 was devoted to reservoir characterization. Technologies being demonstrated include: (1) Advanced petrophysics; (2) Three-dimensional (3-D) seismic; (3) Crosswell bore tomography; (4) Advanced reservoir simulation; (5) Carbon dioxide (CO2) stimulation treatments; (6) Hydraulic fracturing design and monitoring; and (7) Mobility control agents

  20. Characterization of triboluminescent enhanced discontinuous glass–fiber composite beams for micro-damage detection and fracture assessment

    International Nuclear Information System (INIS)

    This work reports the micro-emissions of triboluminescent (TL) concentrated composites and their evaluation at the onset of damage and crack propagation. Unreinforced vinyl ester resin and discontinuous glass–fiber reinforced non-prismatic beams were fabricated incorporating 10 wt% concentration of a highly triboluminescent material (ZnS:Mn). Triboluminescent observations were seen in both two- and three-phase composite systems throughout the failure loading-cycle. Results indicate emissions occur at various intensities corresponding to initial notch-length and imminent micro-matrix fracture. The fracturing or deformation energy was estimated by an experimental method of the J-integral analysis [1], where a lower threshold for excitation was found to be approximately less than 0.5 J m−2, below its respective critical composite fracture energy (~3 and 7 J m−2). Initiation of micro-cracks was observed for reinforced samples and were subjected to three-point bend tests in lieu of the multiple signatures of the transient signal response. - Highlights: • We examined triboluminescence of reinforced and unreinforced beams. • The addition of J-integral fracture analysis indicates low energy excitation. • Excitation is related to matrix fracture in unreinforced samples. • Excitation is related to micro-matrix fracture and potential fiber failure

  1. Master curve characterization of the fracture toughness behavior in SA508 Gr.4N low alloy steels

    Science.gov (United States)

    Lee, Ki-Hyoung; Kim, Min-Chul; Lee, Bong-Sang; Wee, Dang-Moon

    2010-08-01

    The fracture toughness properties of the tempered martensitic SA508 Gr.4N Ni-Mo-Cr low alloy steel for reactor pressure vessels were investigated by using the master curve concept. These results were compared to those of the bainitic SA508 Gr.3 Mn-Mo-Ni low alloy steel, which is a commercial RPV material. The fracture toughness tests were conducted by 3-point bending with pre-cracked charpy (PCVN) specimens according to the ASTM E1921-09c standard method. The temperature dependency of the fracture toughness was steeper than those predicted by the standard master curve, while the bainitic SA508 Gr.3 steel fitted well with the standard prediction. In order to properly evaluate the fracture toughness of the Gr.4N steels, the exponential coefficient of the master curve equation was changed and the modified curve was applied to the fracture toughness test results of model alloys that have various chemical compositions. It was found that the modified curve provided a better description for the overall fracture toughness behavior and adequate T0 determination for the tempered martensitic SA508 Gr.4N steels.

  2. Characterization of the Young’s modulus, residual stress and fracture strength of Cu–Sn–In thin films using combinatorial deposition and micro-cantilevers

    International Nuclear Information System (INIS)

    Microcantilevers coupled with combinatorial deposition were used to characterize the Young’s modulus, residual stress and fracture strength of Cu–Sn–In thin films over a broad range of compositions. Measurement inaccuracies due to cantilever non-idealities were corrected using finite element simulations and deflection measurements at multiple locations. η–phase with a composition Cu53Sn25In22 was discovered to have the highest fracture strength and therefore has potential in thin film solder bonding applications. This study provides a database for the mechanical properties of a wide range of Cu–Sn–In alloys. Moreover, the techniques developed in this study provide a highly efficient approach to finding an intermetallic compound composition with the most desired mechanical properties. (paper)

  3. Battery Separator Characterization and Evaluation Procedures for NASA's Advanced Lithium-Ion Batteries

    Science.gov (United States)

    Baldwin, Richard S.; Bennet, William R.; Wong, Eunice K.; Lewton, MaryBeth R.; Harris, Megan K.

    2010-01-01

    To address the future performance and safety requirements for the electrical energy storage technologies that will enhance and enable future NASA manned aerospace missions, advanced rechargeable, lithium-ion battery technology development is being pursued within the scope of the NASA Exploration Technology Development Program s (ETDP's) Energy Storage Project. A critical cell-level component of a lithium-ion battery which significantly impacts both overall electrochemical performance and safety is the porous separator that is sandwiched between the two active cell electrodes. To support the selection of the optimal cell separator material(s) for the advanced battery technology and chemistries under development, laboratory characterization and screening procedures were established to assess and compare separator material-level attributes and associated separator performance characteristics.

  4. Microstructure and fracture mode of a martensitic stainless steel steam turbine blade characterized via scanning auger microscopy and potentiodynamic polarization

    International Nuclear Information System (INIS)

    The microstructure, the fracture and the resistance to pitting corrosion, in a10−2M (NaCl + Na2SO4) solution, of steam turbine blades, made of martensitic stainless steel (12% Cr), were analysed prior and after their utilization (during about 100 000 hours). The unused blades display an inter-granular fracture mode whereas a trans-granular one emerges in used blades. The SAM analysis of the fractured surfaces reveals that this change is concomitant with carbon and chromium redistribution from the grain boundaries to the grain interior. The potentiodynamic polarization curves and the SEM-EDS analysis of the pitting sites show that the used blades are less susceptible to pitting corrosion than the unused ones. These results are interpreted as a further qualitative evidence of an evolution of the microstructure leading to the formation of new precipitates

  5. Fractured Petroleum Reservoirs

    Energy Technology Data Exchange (ETDEWEB)

    Firoozabadi, Dr. Abbas

    2000-01-18

    In this report the results of experiments of water injection in fractured porous media comprising a number of water-wet matrix blocks are reported for the first time. The blocks experience an advancing fracture-water level (FWL). Immersion-type experiments are performed for comparison; the dominant recovery mechanism changed from co-current to counter-current imbibition when the boundary conditions changed from advancing FWL to immersion-type. Single block experiments of co-current and counter-current imbibition was performed and co-current imbibition leads to more efficient recovery was found.

  6. Quantitative ultrasound characterization of locally advanced breast cancer by estimation of its scatterer properties

    Energy Technology Data Exchange (ETDEWEB)

    Tadayyon, Hadi [Physical Sciences, Sunnybrook Research Institute, Sunnybrook Health Sciences Centre, Toronto, Ontario M4N 3M5 (Canada); Department of Medical Biophysics, Faculty of Medicine, University of Toronto, Toronto, Ontario M5G 2M9 (Canada); Sadeghi-Naini, Ali; Czarnota, Gregory, E-mail: Gregory.Czarnota@sunnybrook.ca [Physical Sciences, Sunnybrook Research Institute, Sunnybrook Health Sciences Centre, Toronto, Ontario M4N 3M5 (Canada); Department of Medical Biophysics, Faculty of Medicine, University of Toronto, Toronto, Ontario M5G 2M9 (Canada); Department of Radiation Oncology, Odette Cancer Centre, Sunnybrook Health Sciences Centre, Toronto, Ontario M4N 3M5 (Canada); Department of Radiation Oncology, Faculty of Medicine, University of Toronto, Toronto, Ontario M5T 1P5 (Canada); Wirtzfeld, Lauren [Department of Physics, Ryerson University, Toronto, Ontario M5B 2K3 (Canada); Wright, Frances C. [Division of Surgical Oncology, Sunnybrook Health Sciences Centre, Toronto, Ontario M4N 3M5 (Canada)

    2014-01-15

    Purpose: Tumor grading is an important part of breast cancer diagnosis and currently requires biopsy as its standard. Here, the authors investigate quantitative ultrasound parameters in locally advanced breast cancers that can potentially separate tumors from normal breast tissue and differentiate tumor grades. Methods: Ultrasound images and radiofrequency data from 42 locally advanced breast cancer patients were acquired and analyzed. Parameters related to the linear regression of the power spectrum—midband fit, slope, and 0-MHz-intercept—were determined from breast tumors and normal breast tissues. Mean scatterer spacing was estimated from the spectral autocorrelation, and the effective scatterer diameter and effective acoustic concentration were estimated from the Gaussian form factor. Parametric maps of each quantitative ultrasound parameter were constructed from the gated radiofrequency segments in tumor and normal tissue regions of interest. In addition to the mean values of the parametric maps, higher order statistical features, computed from gray-level co-occurrence matrices were also determined and used for characterization. Finally, linear and quadratic discriminant analyses were performed using combinations of quantitative ultrasound parameters to classify breast tissues. Results: Quantitative ultrasound parameters were found to be statistically different between tumor and normal tissue (p < 0.05). The combination of effective acoustic concentration and mean scatterer spacing could separate tumor from normal tissue with 82% accuracy, while the addition of effective scatterer diameter to the combination did not provide significant improvement (83% accuracy). Furthermore, the two advanced parameters, including effective scatterer diameter and mean scatterer spacing, were found to be statistically differentiating among grade I, II, and III tumors (p = 0.014 for scatterer spacing, p = 0.035 for effective scatterer diameter). The separation of the tumor

  7. Quantitative ultrasound characterization of locally advanced breast cancer by estimation of its scatterer properties

    International Nuclear Information System (INIS)

    Purpose: Tumor grading is an important part of breast cancer diagnosis and currently requires biopsy as its standard. Here, the authors investigate quantitative ultrasound parameters in locally advanced breast cancers that can potentially separate tumors from normal breast tissue and differentiate tumor grades. Methods: Ultrasound images and radiofrequency data from 42 locally advanced breast cancer patients were acquired and analyzed. Parameters related to the linear regression of the power spectrum—midband fit, slope, and 0-MHz-intercept—were determined from breast tumors and normal breast tissues. Mean scatterer spacing was estimated from the spectral autocorrelation, and the effective scatterer diameter and effective acoustic concentration were estimated from the Gaussian form factor. Parametric maps of each quantitative ultrasound parameter were constructed from the gated radiofrequency segments in tumor and normal tissue regions of interest. In addition to the mean values of the parametric maps, higher order statistical features, computed from gray-level co-occurrence matrices were also determined and used for characterization. Finally, linear and quadratic discriminant analyses were performed using combinations of quantitative ultrasound parameters to classify breast tissues. Results: Quantitative ultrasound parameters were found to be statistically different between tumor and normal tissue (p < 0.05). The combination of effective acoustic concentration and mean scatterer spacing could separate tumor from normal tissue with 82% accuracy, while the addition of effective scatterer diameter to the combination did not provide significant improvement (83% accuracy). Furthermore, the two advanced parameters, including effective scatterer diameter and mean scatterer spacing, were found to be statistically differentiating among grade I, II, and III tumors (p = 0.014 for scatterer spacing, p = 0.035 for effective scatterer diameter). The separation of the tumor

  8. Mineralogical, Chemical, and Isotopic Characterization of Fracture-Coating Minerals in Borehole Samples from Western Pahute Mesa and Oasis Valley, Nevada

    Energy Technology Data Exchange (ETDEWEB)

    Benedict, F C; Rose, T P; Zhou, X

    2000-09-01

    This report summarizes the results of a mineralogical and geochemical investigation of fracture-coating phases obtained from archived borehole core and cuttings samples from the western Pahute Mesa-Oasis Valley region. The objective is to provide data needed to validate UGTA flow and transport models for this region. Fracture-lining minerals were characterized using micrographic techniques (SEM-EDS), and selected calcite samples were analyzed for their stable isotope ({sup 13}C/{sup 12}C and {sup 18}O/{sup 16}O) and rare earth element (REE) abundances. The main conclusions are as follows: (1) The distribution of fracture-lining mineral phases is a function of primary rock type, the style and degree of syn-depositional alteration, effects of post-depositional hydrothermal alteration, and fracture location relative to recharge waters (in the unsaturated zone) or through going groundwater (in the saturated zone). (2) Fracture-lining minerals within the welded tuff aquifers (principally the Timber Mountain and Paintbrush Tuffs) are characterized by the assemblage calcite + chalcedony + Fe- and Mn-oxyhydroxides + mixed illite/smectite (in approximate decreasing order of abundance). The predominant mode of host rock alteration is quartzofeldspathic. (3) Interbedded rhyolitic lava flow aquifers are characterized by the fracture-lining assemblage chalcedony + mixed illite/smectite + Fe- and Mn-oxyhydroxides {+-} calcite {+-} quartz {+-} K-feldspar (in approximate decreasing order of abundance). These include lava flow aquifers from the Thirsty Canyon, Beatty Wash, Paintbrush, and Quartz Mountain groups. The predominant mode of host rock alteration is quartzofeldspathic. (4) Fracture-lining zeolite minerals are abundant only within one of the basaltic lava flow aquifers (Trachyte of Ribbon Cliff) where they occur with chalcedony + calcite + clay minerals. (5) Stable isotope analyses ({sup 13}C/{sup 12}C and {sup 18}O/{sup 16}O) of secondary calcite samples were used to

  9. Characterization by notched and precracked Charpy tests of the in-service degradation of RPV steel fracture toughness

    Energy Technology Data Exchange (ETDEWEB)

    Fabry, A.

    1997-01-01

    The current engineering and regulatory practice to estimate fracture toughness safety margins for nuclear reactor pressure vessels (RPVs) relies heavily on the CVN impact test. Techniques to estimate in-service toughness degradation directly using a variety of precracked specimens are under development worldwide. Emphasis is on their miniaturization. In the nuclear context, it is essential to address many issues such as representativity of the surveillance programs with respect to the vessel in terms of materials and environment, transferability of test results to the structure (constraint and size effects), lower bound toughness certification, creadibility relative to trends of exising databases. An enhanced RPV surveillance strategy in under development in Belgium. It combines state-of-the-art micromechanical and damage modelling to the evaluation of CVN load-deflection signals, tensile stress-strain curves and slow-bend tests of reconstituted precracked Charpy specimens. A probabilistic micromechanical model has been established for static and dynamic transgranular cleavage initiation fracture toughness in the ductile-brittle transition temperature range. This model allows to project toughness bounds for any steel embrittlement condition from the corresponding CVN and static tensile properties, using a single scaling factor defined by imposing agreement with toughness tests in a single condition. The outstanding finding incorporated by this toughness transfer model is that the microcleavage fracture stress is affected by temperature in the ductile-brittle transition and that this influence is strongly correlated to the flow stress: this explains the shape of the K{sub Ic}n K{sub Id} temperature curves as well as the actual magnitude of the strain rate and irradiation effects. Furthermore, CVN crack arrest loads and fracture appearance are also taken advantage of in order to estimate K{sub Ia} degradation. Finally, the CVN-tensile load-temperature diagram

  10. Root fractures

    DEFF Research Database (Denmark)

    Andreasen, Jens Ove; Christensen, Søren Steno Ahrensburg; Tsilingaridis, Georgios

    2012-01-01

    The purpose of this study was to analyze tooth loss after root fractures and to assess the influence of the type of healing and the location of the root fracture. Furthermore, the actual cause of tooth loss was analyzed.......The purpose of this study was to analyze tooth loss after root fractures and to assess the influence of the type of healing and the location of the root fracture. Furthermore, the actual cause of tooth loss was analyzed....

  11. Prospective study of ankle and foot fractures in elderly women

    Directory of Open Access Journals (Sweden)

    Yadagiri Surender Rao

    2015-01-01

    Full Text Available The epidemiology of ankle fractures in old people is changing as time passes on. The incidence of ankle fractures increases with advancing age. The study conducted was among a rural popula-tion which comprised of 68 women (32 women with ankle fractures & 36 women with foot fractures. Patients studied were in the age group more than 50 years. The study highlights the etiological & risk factors for fractures of ankle & foot. The commonest ankle fracture was the lateral malleolar fracture & the commonest foot fracture was the 5th Metatarsal fracture. Diabetes is a risk factor which increases the occurrence of ankle and foot injuries.

  12. Differential oxidative status and immune characterization of the early and advanced stages of human breast cancer.

    Science.gov (United States)

    Panis, C; Victorino, V J; Herrera, A C S A; Freitas, L F; De Rossi, T; Campos, F C; Simão, A N Colado; Barbosa, D S; Pinge-Filho, P; Cecchini, R; Cecchini, A L

    2012-06-01

    Breast cancer is the malignant neoplasia with the highest incidence in women worldwide. Chronic oxidative stress and inflammation have been indicated as major mediators during carcinogenesis and cancer progression. Human studies have not considered the complexity of tumor biology during the stages of cancer advance, limiting their clinical application. The purpose of this study was to characterize systemic oxidative stress and immune response parameters in early (ED; TNM I and II) and advanced disease (AD; TNM III and IV) of patients diagnosed with infiltrative ductal carcinoma breast cancer. Oxidative stress parameters were evaluated by plasmatic lipoperoxidation, carbonyl content, thiobarbituric reactive substances (TBARS), nitric oxide levels (NO), total radical antioxidant parameter (TRAP), superoxide dismutase, and catalase activities and GSH levels. Immune evaluation was determined by TNF-α, IL-1β, IL-12, and IL-10 levels and leukocytes oxidative burst evaluation by chemiluminescence. Tissue damage analysis included heart (total CK and CKMB), liver (AST, ALT, GGT), and renal (creatinine, urea, and uric acid) plasmatic markers. C-reactive protein (CRP) and iron metabolism were also evaluated. Analysis of the results verified different oxidative stress statuses occur at distinct cancer stages. ED was characterized by reduction in catalase, 8-isoprostanes, and GSH levels, with enhanced lipid peroxidation and TBARS levels. AD exhibited more pronounced oxidative status, with reduction in catalase activity and TRAP, intense lipid peroxidation and high levels of NO, TBARs, and carbonyl content. ED patients presented a Th2 immune pattern, while AD exhibited Th1 status. CRP levels and ferritin were increased in both stages of disease. Leukocytes burst impairment was observed in both the groups. Plasma iron levels were significantly elevated in AD. The data obtained indicated that oxidative stress enhancement and immune response impairment may be necessary to ensure

  13. Advanced glycation end product ligands for the receptor for advanced glycation end products: Biochemical characterization and formation kinetics

    NARCIS (Netherlands)

    Valencia, J.V.; Weldon, S.C.; Quinn, D.; Kiers, G.H.; Groot, J. de; TeKoppele, J.M.; Hughes, T.E.

    2004-01-01

    Advanced glycation end products (AGEs) accumulate with age and at an accelerated rate in diabetes. AGEs bind cell-surface receptors including the receptor for advanced glycation end products (RAGE). The dependence of RAGE binding on specific biochemical characteristics of AGEs is currently unknown.

  14. US Geological Survey Committee for the Advancement of Science in the Yucca Mountain Project symposium on {open_quotes}Fractures, Hydrology, and Yucca Mountain{close_quotes}: Abstracts and summary

    Energy Technology Data Exchange (ETDEWEB)

    Gomberg, J. [ed.

    1991-12-31

    The principal objective of this symposium is to review the available information on fractured/faulted terrains in terms of a coherent hydrogeologic model of ground-water fluid flow and transport, particularly as it pertains to the Yucca Mountain region. This review addresses the influence and significance of fractures on ground-water flow and the transport of conservative-species solutes within the context of the hydrogeologic setting of the Yucca Mountain area. The relations between fluid flow and fractured or faulted host rock are examined integrally from information on geologic, seismologic, hydrologic, and geomechanical properties of the system. The development of new hydrogeologic approaches that incorporate information from this integrated database are contrasted with more standard approaches toward understanding flow in fractured reservoirs. Ground-water flow in both the unsaturated zone and the saturated zone are considered. The application of various models of flow is addressed, examples include porous-media equivalent and discontinuum fracture-network models. Data and interpretations from the Yucca Mountain area are presented to establish a context for information exchange. The symposium includes discussions relevant to technical considerations for characterizing the Yucca Mountain area hydrogeology. On the basis of these discussions, CASY has compiled this document in order to formally summarize the proceedings and communicate recommendations for future directions of research and investigation.

  15. Thermal transport in a coupled sinusoidal fracture-matrix system

    OpenAIRE

    N.Natarajan,; Suresh Kumar, G.

    2010-01-01

    In this study, the behavior of thermal fronts along the fracture is studied in a coupled fracture-matrix system with sinusoidal fracture geometry. Cold water is injected into the fracture, which advances gradually extracting heat from the adjacent reservoir matrix. The heat conduction into the rock-matrix is assumed to be one dimensionalperpendicular to the rock fracture. Constant temperature water is injected into the fracture and the behavior of thermal fronts for various thermal conductivi...

  16. Characterization of Tubing from Advanced ODS alloy (FCRD-NFA1)

    Energy Technology Data Exchange (ETDEWEB)

    Maloy, Stuart Andrew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Aydogan, Eda [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Anderoglu, Osman [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Lavender, Curt [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Anderson, Iver [Ames Lab., Ames, IA (United States); Rieken, Joel [Ames Lab., Ames, IA (United States); Lewandowski, John [Case Western Reserve Univ., Cleveland, OH (United States); Hoelzer, Dave [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Odette, George R. [Univ. of California, Santa Barbara, CA (United States)

    2016-09-20

    Fabrication methods are being developed and tested for producing fuel clad tubing of the advanced ODS 14YWT and FCRD-NFA1 ferritic alloys. Three fabrication methods were based on plastically deforming a machined thick wall tube sample of the ODS alloys by pilgering, hydrostatic extrusion or drawing to decrease the outer diameter and wall thickness and increase the length of the final tube. The fourth fabrication method consisted of the additive manufacturing approach involving solid-state spray deposition (SSSD) of ball milled and annealed powder of 14YWT for producing thin wall tubes. The details of these fabrication methods are described in ORNL/TM-2015/499 “Status of producing 5 inch long clad tubing of ODS ferritic alloys.” Of the four fabrication methods, two methods were successful at producing tubing for further characterization: production of tubing by High velocity oxy-fuel spray forming and production of tubing using high temperature hydrostatic extrusion. The characterization described in the following report shows through neutron diffraction the texture produced during extrusion while maintaining the beneficial oxide dispersion. Future work will center on extending these processes to producing longer tubing for characterization and irradiation testing.

  17. The Use of Acoustic Emission to Characterize Fracture Behavior During Vickers Indentation of HVOF Thermally Sprayed WC-Co Coatings

    Science.gov (United States)

    Faisal, N. H.; Steel, J. A.; Ahmed, R.; Reuben, R. L.

    2009-12-01

    This paper describes how acoustic emission (AE) measurements can be used to supplement the mechanical information available from an indentation test. It examines the extent to which AE data can be used to replace time-consuming surface crack measurement data for the assessment of fracture toughness of brittle materials. AE is known to be sensitive to fracture events and so it was expected that features derived from the AE data may provide information on the processes (microscale and macroscale fracture events and densification) occurring during indentation. AE data were acquired during indentation tests on samples of a WC-12%Co coating of nominal thickness 300 μm at a variety of indentation loads. The raw AE signals were reduced to three stages and three features per stage, giving nine possible indicators per indentation. Each indicator was compared with the crack profile, measured both conventionally and using a profiling method which gives the total surface crack length around the indent. A selection of the indents was also sectioned in order to make some observations on the subsurface damage. It has been found that reproducible AE signals are generated during indentation involving three distinct stages, associated, respectively, with nonradial cracking, commencement of radial cracking, and continued descent of the indenter. It has been shown that AE can give at least as good a measure of cracking processes during indentation as is possible using crack measurement after indentation.

  18. Synthesis and characterization of inorganic nanostructured materials for advanced energy storage

    Science.gov (United States)

    Xie, Jin

    The performance of advanced energy storage devices is intimately connected to the designs of electrodes. To enable significant developments in this research field, we need detailed information and knowledge about how the functions and performances of the electrodes depend on their chemical compositions, dimensions, morphologies, and surface properties. This thesis presents my successes in synthesizing and characterizing electrode materials for advanced electrochemical energy storage devices, with much attention given to understanding the operation and fading mechanism of battery electrodes, as well as methods to improve their performances and stabilities. This dissertation is presented within the framework of two energy storage technologies: lithium ion batteries and lithium oxygen batteries. The energy density of lithium ion batteries is determined by the density of electrode materials and their lithium storage capabilities. To improve the overall energy densities of lithium ion batteries, silicon has been proposed to replace lithium intercalation compounds in the battery anodes. However, with a ~400% volume expansion upon fully lithiation, silicon-based anodes face serious capacity degradation in battery operation. To overcome this challenge, heteronanostructure-based Si/TiSi2 were designed and synthesized as anode materials for lithium ion batteries with long cycling life. The performance and morphology relationship was also carefully studied through comparing one-dimensional and two-dimensional heteronanostructure-based silicon anodes. Lithium oxygen batteries, on the other hand, are devices based on lithium conversion chemistries and they offer higher energy densities compared to lithium ion batteries. However, existing carbon based electrodes in lithium oxygen batteries only allow for battery operation with limited capacity, poor stability and low round-trip efficiency. The degradation of electrolytes and carbon electrodes have been found to both contribute

  19. Combining geoelectrical and advanced lysimeter methods to characterize heterogeneous flow and transport under unsaturated transient conditions

    Science.gov (United States)

    Wehrer, M.; Skowronski, J.; Binley, A. M.; Slater, L. D.

    2013-12-01

    Our ability to predict flow and transport processes in the unsaturated critical zone is considerably limited by two characteristics: heterogeneity of flow and transience of boundary conditions. The causes of heterogeneous - or preferential - flow and transport are fairly well understood, yet the characterization and quantification of such processes in natural profiles remains challenging. This is due to current methods of observation, such as staining and isotope tracers, being unable to observe multiple events on the same profile and offering limited spatial information. In our study we demonstrate an approach to characterize preferential flow and transport processes applying a combination of geoelectrical methods and advanced lysimeter techniques. On an agricultural soil profile, which was transferred undisturbed into a lysimeter container, we applied systematically varied input flow boundary conditions, resembling natural precipitation events. We simultaneously measured the breakthrough of a conservative tracer. Flow and transport in the soil column were observed using electrical resistivity tomography (ERT), tensiometers, water content probes and a multicompartment suction plate (MSP). These techniques allowed a direct ground-truthing of soil moisture and pore fluid resistivity changes estimated noninvasively using ERT. We were able to image both the advancing infiltration front and the advancing tracer front using time lapse ERT. Water content changes associated with the advancing infiltration front dominated over pore fluid conductivity changes during short term precipitation events. Conversely, long term displacement of the solute front was monitored during periods of constant water content in between infiltration events. We observed preferential flow phenomena through ERT and through the MSP, which agreed in general terms. The preferential flow fraction was observed to be independent of precipitation rate. This suggests the presence of a fingering process

  20. Characterization of Radium and Radon Isotopes in Hydraulic Fracturing Flowback Fluid and Gas from the Marcellus Shale

    Science.gov (United States)

    Bardsley, A.

    2015-12-01

    High volume hydraulic fracturing of unconventional deposits has expanded rapidly over the past decade in the US, with much attention focused on the Marcellus Shale gas reservoir in the northeastern US. We use naturally occurring radium isotopes and 222Rn to explore changes in formation characteristics as a result of hydraulic fracturing. Gas and produced waters were analyzed from time series samples collected soon after hydraulic fracturing at three Marcellus Shale well sites in the Appalachian Basin, USA. Analyses of δ18O, Cl- , and 226Ra in flowback fluid are consistent with two end member mixing between injected slick water and formation brine. All three tracers indicate that the ratio of injected water to formation brine declines with time across both time series. Cl- concentration (max ~1.5-2.2 M) and 226Ra activity (max ~165-250 Bq/Kg) in flowback fluid are comparable at all three sites. There are differences evident in the stable isotopic composition (δ18O & δD) of injected slick water across the three sites, but all appear to mix with formation brine of similar isotopic composition. On a plot of water isotopes, δ18O in formation brine-dominated fluid is enriched by ~3-4 permille relative to the Global Meteoric Water Line, indicating oxygen exchange with shale. The ratio of 223Ra/226Ra and 228Ra/226Ra in produced waters is quite low relative to shale samples analyzed. This indicates that most of the 226Ra in the formation brine must be sourced from shale weathering or dissolution rather than emanation due to alpha recoil from the rock surface. During the first week of flowback, ratios of short lived isotopes 223Ra and 224Ra to longer lived radium isotopes change modestly, suggesting rock surface area per unit of produced water volume did not change substantially. For one well, longer term gas samples were collected. The 222Rn/methane ratio in produced gas from this site declines with time and may represent a decrease in the brine to gas ratio in the

  1. Biofilm development in a hotspot of mixing between shallow and deep groundwater in a fractured aquifer: field evidence from joint flow, chemical and microbiological characterization

    Science.gov (United States)

    Bochet, Olivier; Le Borgne, Tanguy; Pédrot, Mathieu; Labasque, Thierry; Lavenant, Nicolas; Petton, Christophe; Dufresne, Alexis; Ben Maamar, Sarah; Chatton, Eliot; De la Bernardie, Jérôme; Aquilina, Luc

    2015-04-01

    Biofilm development in a hotspot of mixing between shallow and deep groundwater in a fractured aquifer: field evidence from joint flow, chemical and microbiological characterization Olivier Bochet1, Tanguy Le Borgne1, Mathieu Pédrot1, Thierry Labasque1, Nicolas Lavenant1, Christophe Petton1, Alexis Dufresne2,Sarah Ben Maamar1-2, Eliot Chatton1, Jérôme de la Bernardie1, Luc Aquilina1 1: Géosciences Rennes, CNRS UMR 6118, Université de Rennes 1, Campus de Beaulieu bât 14B, Rennes, France 2: Ecobio, CNRS UMR 6553, Université de Rennes 1, Campus de Beaulieu, bât 14, Rennes, France Biofilms play a major role in controlling the fluxes and reactivity of chemical species transported in hydrological systems. Their development can have either positive impacts on groundwater quality (e.g. attenuation of contaminants under natural or stimulated conditions), or possible negative effects on subsurface operations (e.g. bio-clogging of geothermal dipoles or artificial recharge systems). Micro-organisms require both electron donors and electron acceptors for cellular growth, proliferation and maintenance of their metabolic functions. The mechanisms controlling these reactions derive from the interactions occurring at the micro-scale that depend on mineral compositions, the biota of subsurface environment, but also fluid mixing, which determines the local concentrations of nutriments, electron donors and electron acceptors. Hence, mixing zones between oxygen and nutriment rich shallow groundwater and mineralized deep groundwater are often considered as potential hotspots of microbial activity, although relatively few field data document flow distributions, transport properties, chemical gradients and micro-organisms distributions across these mixing interfaces. Here we investigate the origin of a localized biofilm development observed in the fractured granite aquifer at the Ploemeur observatory (H+ network hplus.ore.fr).This biofilm composed of ferro-oxidizing bacteria is

  2. Recent Advances in Cloning and Characterization of Disease Resistance Genes in Rice

    Institute of Scientific and Technical Information of China (English)

    Liang-Ying Dai; Xiong-Lun Liu; Ying-Hui Xiao; Guo-Liang Wang

    2007-01-01

    Rice diseases caused by fungi, bacteria and viruses are one of the major constraints for sustainable rice (Oryza sativa L.) production worldwide. The use of resistant cultivars is considered the most economical and effective method to control rice diseases. In the last decade, a dozen resistance genes against the fungal pathogen Magnaporthe grisea and the bacterial pathogen Xanthomonas oryzae pv. oryzae have been cloned. Approximately half of them encode nuclear binding site (NBS) and leucine rich repeat (LRR)-containing proteins, the most common type of cloned plant resistance genes. Interestingly, four of them encode novel proteins which have not been identified in other plant species, suggesting that unique mechanisms might be involved in rice defense responses. This review summarizes the recent advances in cloning and characterization of disease resistance genes in rice and presents future perspectives for in-depth molecular analysis of the function and evolution of rice resistance genes and their interaction with avirulence genes in pathogens.

  3. Advanced Technology Large-Aperture Space Telescope (ATLAST): Characterizing Habitable Worlds

    CERN Document Server

    Postman, M; Krist, J; Stapelfeldt, K; Brown, R; Oegerle, W; Lo, A; Clampin, M; Soummer, R; Wiseman, J; Mountain, M

    2009-01-01

    The Advanced Technology Large Aperture Space Telescope (ATLAST) is a set of mission concepts for the next generation UV-Optical-Near Infrared space telescope with an aperture size of 8 to 16 meters. ATLAST, using an internal coronagraph or an external occulter, can characterize the atmosphere and surface of an Earth-sized exoplanet in the Habitable Zone of long-lived stars at distances up to ~45 pc, including its rotation rate, climate, and habitability. ATLAST will also allow us to glean information on the nature of the dominant surface features, changes in cloud cover and climate, and, potentially, seasonal variations in surface vegetation. ATLAST will be able to visit up to 200 stars in 5 years, at least three times each, depending on the technique used for starlight suppression and the telescope aperture. More frequent visits can be made for interesting systems.

  4. Advances in Multi-Pixel Photon Counter technology: First characterization results

    Science.gov (United States)

    Bonanno, G.; Marano, D.; Romeo, G.; Garozzo, S.; Grillo, A.; Timpanaro, M. C.; Catalano, O.; Giarrusso, S.; Impiombato, D.; La Rosa, G.; Sottile, G.

    2016-01-01

    Due to the recent advances in silicon photomultiplier technology, new types of Silicon Photomultiplier (SiPM), also named Multi-Pixel Photon Counter (MPPC) detectors have become recently available, demonstrating superior performance in terms of their most important electrical and optical parameters. This paper presents the latest characterization results of the novel Low Cross-Talk (LCT) MPPC families from Hamamatsu, where a noticeable fill-factor enhancement and cross-talk reduction is achieved. In addition, the newly adopted resin coating has been proven to yield improved photon detection capabilities in the 280-320 nm spectral range, making the new LCT MPPCs particularly suitable for emerging applications like Cherenkov Telescope Array, and Astroparticle Physics.

  5. On the Use of Accelerated Test Methods for Characterization of Advanced Composite Materials

    Science.gov (United States)

    Gates, Thomas S.

    2003-01-01

    A rational approach to the problem of accelerated testing for material characterization of advanced polymer matrix composites is discussed. The experimental and analytical methods provided should be viewed as a set of tools useful in the screening of material systems for long-term engineering properties in aerospace applications. Consideration is given to long-term exposure in extreme environments that include elevated temperature, reduced temperature, moisture, oxygen, and mechanical load. Analytical formulations useful for predictive models that are based on the principles of time-based superposition are presented. The need for reproducible mechanisms, indicator properties, and real-time data are outlined as well as the methodologies for determining specific aging mechanisms.

  6. A comparison of conventional and advanced ultrasonic inspection techniques in the characterization of TMC materials

    Science.gov (United States)

    Holland, Mark R.; Handley, Scott M.; Miller, James G.; Reighard, Mark K.

    1992-01-01

    Results obtained with a conventional ultrasonic inspection technique as well as those obtained with more advanced ultrasonic NDE methods in the characterization of an 8-ply quasi-isotropic titanium matrix composite (TMC) specimen are presented. Images obtained from a conventional ultrasonic inspection of TMC material are compared with those obtained using more sophisticated ultrasonic inspection methods. It is suggested that the latter techniques are able to provide quantitative images of TMC material. They are able to reveal the same potential defect indications while simultaneously providing more quantitative information concerning the material's inherent properties. Band-limited signal loss and slope-of-attenuation images provide quantitative data on the inherent material characteristics and defects in TMC.

  7. Perfusion CT in patients with advanced bronchial carcinomas: a novel chance for characterization and treatment monitoring?

    International Nuclear Information System (INIS)

    Advanced bronchial carcinomas by means of perfusion and peak enhancement using dynamic contrast-enhanced multislice CT are characterized. Twenty-four patients with advanced bronchial carcinoma were examined. During breathhold, after injection of a contrast-medium (CM), 25 scans were performed (1 scan/s) at a fixed table position. Density-time curves were evaluated from regions of interest of the whole tumor and high- and low-enhancing tumor areas. Perfusion and peak enhancement were calculated using the maximum-slope method of Miles and compared with size, localization (central or peripheral) and histology. Perfusion of large tumors (>50 cm3) averaged over both the whole tumor (P=0.001) and the highest enhancing area (P=0.003) was significantly lower than that of smaller ones. Independent of size, central carcinomas had a significantly (P=0.04) lower perfusion (mean 27.9 ml/min/100 g) than peripheral ones (mean 66.5 ml/min/100 g). In contrast, peak enhancement of central and peripheral carcinomas was not significantly different. Between non-small-cell lung cancers and small-cell lung cancers, no significant differences were observed in both parameters. In seven tumors, density increase after CM administration started earlier than in the aorta, indicating considerable blood supply from pulmonary vessels. Tumor perfusion was dependent on tumor size and localization, but not on histology. Furthermore, perfusion CT disclosed blood supply from both pulmonary and/or bronchial vessels in some tumors. (orig.)

  8. Advanced Characterization of Molecular Interactions in TALSPEAK-like Separations Systems

    Energy Technology Data Exchange (ETDEWEB)

    Nash, Kenneth [Washington State Univ., Pullman, WA (United States); Guelis, Artem [Argonne National Lab. (ANL), Argonne, IL (United States); Lumetta, Gregg J. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Sinkov, Sergey [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

    2015-10-21

    Combining unit operations in advanced aqueous reprocessing schemes brings obvious process compactness advantages, but at the same time greater complexity in process design and operation. Unraveling these interactions requires increasingly sophisticated analytical tools and unique approaches for adequate analysis and characterization that probe molecular scale interactions. Conventional slope analysis methods of solvent extraction are too indirect to provide much insight into such interactions. This project proposed the development and verification of several analytical tools based on studies of TALSPEAK-like aqueous processes. As such, the chemistry of trivalent fission product lanthanides, americium, curium, plutonium, neptunium and uranium figure prominently in these studies. As the project was executed, the primary focus fell upon the chemistry or trivalent lanthanides and actinides. The intent of the investigation was to compare and contrast the results from these various complementary techniques/studies to provide a stronger basis for predicting the performance of extractant/diluent mixtures as media for metal ion separations. As many/most of these techniques require the presence of metal ions at elevated concentrations, it was expected that these studies would take this investigation into the realm of patterns of supramolecular organization of metal complexes and extractants in concentrated aqueous/organic media. We expected to advance knowledge of the processes that enable and limit solvent extraction reactions as a result of the application of fundamental chemical principles to explaining interactions in complex media.

  9. Advanced reservoir characterization for improved oil recovery in a New Mexico Delaware basin project

    Energy Technology Data Exchange (ETDEWEB)

    Martin, F.D.; Kendall, R.P.; Whitney, E.M. [Dave Martin and Associates, Inc., Socorro, NM (United States)] [and others

    1997-08-01

    The Nash Draw Brushy Canyon Pool in Eddy County, New Mexico is a field demonstration site in the Department of Energy Class III program. The basic problem at the Nash Draw Pool is the low recovery typically observed in similar Delaware fields. By comparing a control area using standard infill drilling techniques to a pilot area developed using advanced reservoir characterization methods, the goal of the project is to demonstrate that advanced technology can significantly improve oil recovery. During the first year of the project, four new producing wells were drilled, serving as data acquisition wells. Vertical seismic profiles and a 3-D seismic survey were acquired to assist in interwell correlations and facies prediction. Limited surface access at the Nash Draw Pool, caused by proximity of underground potash mining and surface playa lakes, limits development with conventional drilling. Combinations of vertical and horizontal wells combined with selective completions are being evaluated to optimize production performance. Based on the production response of similar Delaware fields, pressure maintenance is a likely requirement at the Nash Draw Pool. A detailed reservoir model of pilot area was developed, and enhanced recovery options, including waterflooding, lean gas, and carbon dioxide injection, are being evaluated.

  10. Recent Advances in Characterization of Lignin Polymer by Solution-State Nuclear Magnetic Resonance (NMR Methodology

    Directory of Open Access Journals (Sweden)

    Run-Cang Sun

    2013-01-01

    Full Text Available The demand for efficient utilization of biomass induces a detailed analysis of the fundamental chemical structures of biomass, especially the complex structures of lignin polymers, which have long been recognized for their negative impact on biorefinery. Traditionally, it has been attempted to reveal the complicated and heterogeneous structure of lignin by a series of chemical analyses, such as thioacidolysis (TA, nitrobenzene oxidation (NBO, and derivatization followed by reductive cleavage (DFRC. Recent advances in nuclear magnetic resonance (NMR technology undoubtedly have made solution-state NMR become the most widely used technique in structural characterization of lignin due to its versatility in illustrating structural features and structural transformations of lignin polymers. As one of the most promising diagnostic tools, NMR provides unambiguous evidence for specific structures as well as quantitative structural information. The recent advances in two-dimensional solution-state NMR techniques for structural analysis of lignin in isolated and whole cell wall states (in situ, as well as their applications are reviewed.

  11. New Generation of High Resolution Ultrasonic Imaging Technique for Advanced Material Characterization: Review

    Science.gov (United States)

    Maev, R. Gr.

    The role of non-destructive material characterization and NDT is changing at a rapid rate, continuing to evolve alongside the dramatic development of novel techniques based on the principles of high-resolution imaging. The modern use of advanced optical, thermal, ultrasonic, laser-ultrasound, acoustic emission, vibration, electro-magnetic, and X-ray techniques, etc., as well as refined measurement and signal/data processing devices, allows for continuous generation of on-line information. As a result real-time process monitoring can be achieved, leading to the more effective and efficient control of numerous processes, greatly improving manufacturing as a whole. Indeed, concurrent quality inspection has become an attainable reality. With the advent of new materials for use in various structures, joints, and parts, however, innovative applications of modern NDT imaging techniques are necessary to monitor as many stages of manufacturing as possible. Simply put, intelligent advance manufacturing is impossible without actively integrating modern non-destructive evaluation into the production system.

  12. Hip fracture - discharge

    Science.gov (United States)

    Inter-trochanteric fracture repair - discharge; Subtrochanteric fracture repair - discharge; Femoral neck fracture repair - discharge; Trochanteric fracture repair - discharge; Hip pinning surgery - discharge

  13. Open reduction and internal fixation of proximal humerus fractures.

    Science.gov (United States)

    Drosdowech, Darren S; Faber, Kenneth J; Athwal, George S

    2008-10-01

    Open reduction of proximal humeral fractures has the advantage of providing direct control over each fracture fragment and permitting anatomic reduction and fixation with advanced devices. Modern fixed-angle locking plates designed specifically for proximal humerus fractures have allowed the expansion of surgical indications permitting surgeons to address more complicated fractures. Advanced preoperative imaging and fluoroscopy allow a better understanding of fracture patterns and permit the surgeon to use this knowledge intraoperatively. Research is required to further validate fracture classification systems, to develop surgical guidelines for decision making, and to compare the outcomes of the various treatments options for proximal humerus fractures.

  14. Sub-seafloor acoustic characterization of seamounts near the Ogasawara Fracture Zone in the western Pacific using chirp (3-7 kHz) subbottom profiles

    Science.gov (United States)

    Lee, Tae-Gook; Hein, James R.; Lee, Kiehwa; Moon, Jai-Woon; Ko, Young-Tak

    2005-10-01

    A detailed analysis of chirp (3-7 kHz) subbottom profiles and bathymetry was performed on data collected from seamounts near the Ogasawara Fracture Zone (OFZ) in the western Pacific. The OFZ, which is a 150 km wide rift zone showing 600 km of right-lateral movement in a NW-SE direction, is unique among the fracture zones of the Pacific in that it includes many old seamounts (e.g., Magellan Seamounts and seamounts on Dutton Ridge). Sub-seafloor acoustic echoes on the seamounts are classified into nine specific types based on the nature and continuity of the echoes, subbottom structure, and morphology of the seafloor: (1) distinct echoes (types I-1, I-2, I-3), (2) indistinct echoes (types II-1, II-2, II-3), and (3) hyperbolic echoes (types III-1, III-2, III-3). Type I-2 pelagic sediments, characterized by thin and intermittent coverage, were probably deposited in topographically sheltered areas when bottom currents were strong, whereas type I-1 pelagic sediments accumulated during continuous and widespread sedimentation. Development of seamount flank rift zones in the OFZ may have been influenced by preexisting structures in the transform fracture zone at the time of volcanism, whereas those on Ita Mai Tai seamount in the Pigafetta Basin originated solely by edifice-building processes. Flank rift zones that formed by dike intrusions and eruptions played an important role in mass wasting. Mass-wasting processes included block faulting or block slides around the summit margin, sliding/slumping, debris flows, and turbidites, which may have been triggered by faulting, volcanism, dike injection, and weathering during various stages in the evolution of the seamounts.

  15. Contemporary Management of Infected Mandibular Fractures

    OpenAIRE

    Alpert, Brian; Kushner, George M.; Tiwana, Paul S.

    2008-01-01

    The treatment of infected mandibular fractures has advanced rather dramatically over the past 50 years. Immobilization with maxillomandibular fixation and/or splints, removal of diseased teeth in the fracture line, external fixation, use of antibiotics, debridement, and rigid internal fixation has played a role in management. Perhaps the most important advance was the realization that infected fractures also result from moving fragments and nonvital bone, not just bacteria. Controlling moveme...

  16. Mask characterization for critical dimension uniformity budget breakdown in advanced extreme ultraviolet lithography

    Science.gov (United States)

    Nikolsky, Peter; Strolenberg, Chris; Nielsen, Rasmus; Nooitgedacht, Tjitte; Davydova, Natalia; Yang, Greg; Lee, Shawn; Park, Chang-Min; Kim, Insung; Yeo, Jeong-Ho

    2013-04-01

    As the International Technology Roadmap for Semiconductors critical dimension uniformity (CDU) specification shrinks, semiconductor companies need to maintain a high yield of good wafers per day and high performance (and hence market value) of finished products. This cannot be achieved without continuous analysis and improvement of on-product CDU as one of the main drivers for process control and optimization with better understanding of main contributors from the litho cluster: mask, process, metrology and scanner. We will demonstrate a study of mask CDU characterization and its impact on CDU Budget Breakdown (CDU BB) performed for advanced extreme ultraviolet (EUV) lithography with 1D (dense lines) and 2D (dense contacts) feature cases. We will show that this CDU contributor is one of the main differentiators between well-known ArFi and new EUV CDU budgeting principles. We found that reticle contribution to intrafield CDU should be characterized in a specific way: mask absorber thickness fingerprints play a role comparable with reticle CDU in the total reticle part of the CDU budget. Wafer CD fingerprints, introduced by this contributor, may or may not compensate variations of mask CDs and hence influence on total mask impact on intrafield CDU at the wafer level. This will be shown on 1D and 2D feature examples. Mask stack reflectivity variations should also be taken into account: these fingerprints have visible impact on intrafield CDs at the wafer level and should be considered as another contributor to the reticle part of EUV CDU budget. We also observed mask error enhancement factor (MEEF) through field fingerprints in the studied EUV cases. Variations of MEEF may play a role towards the total intrafield CDU and may need to be taken into account for EUV lithography. We characterized MEEF-through-field for the reviewed features, with results herein, but further analysis of this phenomenon is required. This comprehensive approach to quantifying the mask part of

  17. Ductile damage Cam-Clay plasticity and fracture modeling of shale based on nano-characterization experiment

    Science.gov (United States)

    Bennett, K. C.; Borja, R. I.

    2015-12-01

    A finite strain ductile damage formulation of Modified Cam-Clay (MCC) plasticity has been developed in order to model the observed elastoplastic behavior of shale at nano- to micro-scales. Nano-indentation combined with both 2D and 3D imaging was performed on a sample of Woodford shale. Significant plastic deformation was observed in the nano-indentation testing, and nano-scale resolution FIB-SEM imaging of the post-indented regions has revealed that the plastic deformation is accompanied by extensive micro-fracture of the shale's highly heterogeneous micro-structure. A spatial tensor that is similar to Eshelby's energy momentum tensor is shown to be energy conjugate to the plastic velocity gradient under large inelastic volume strain. These results are cast in MCC framework drawing on the concept of continuum damage. The resulting formulation provides a connection between density (porosity), elastic (and plastic) moduli, and micro damage/healing. Nonlinear finite element modeling is used for implementation of the constitutive model in simulation of both laboratory-scale and nano- to micro-scale experiments. The results show that the model is able to predict the inception and propagation of micro-fractures around inhomogeneities, as well as capture the resulting behavior observed at the much larger laboratory scale.

  18. Unstable Pelvic Fractures Associated with Femoral Shaft Fractures: A Retrospective Analysis

    Directory of Open Access Journals (Sweden)

    Chun-Liang Wu

    2013-04-01

    Full Text Available Background: Both pelvic fractures and femoral shaft fractures are caused by high-energy injuries. When unstable pelvic fractures and femoral shaft fractures occur concomitantly, the optimal treatment method is controversial. The aim of this study was to establish a reasonable principle for treating such complicated injuries. Methods: Forty patients sustaining unstable pelvic fractures and concomitant femoral shaft fractures were treated in a 7-year period. The initial management of the fractures was started at the emergency service according to the Advanced Trauma Life Support protocol. Unstable pelvic fractures were wrapped by cloth sheets and femoral shaft fractures were immobilized with a splint. Angiography was performed on patients with unstable hemodynamic status. The definitive treatment for combined fractures was performed after stabilizing the hemodynamics. Closed nailing was used for femoral shaft fractures, and pelvic fractures were treated with various techniques. Results: The mortality rate was 12.5% (5/40 during admission. Thirty-three patients were followed up for an average of 32 months (range, 12-76 months. There were 33 cases of unstable pelvic fractures and 36 instances of femoral shaft fractures. The union rate for pelvic fractures was 100% (33/33, while femoral shaft fractures had a 94.4% (34/36 union rate. The average healing time was 3.3 months (range, 1.6-8.1 months and 4.1 months (range, 2.5-18.2 months for pelvic and femoral shaft fractures, respectively. After fracture, 34 hips (94% achieved a satisfactory result in the Harris hip score and 30 knees (83% achieved a satisfactory result in the Mize knee score. Conclusions: Stabilization of the hemodynamics in patients with combined fractures should be the first aim. Angiography to stop arterial bleeding in the pelvis is often life-saving. The definitive treatment for combined fractures, such as pelvic fractures and femoral shaft fractures, should wait until hemodynamics

  19. Subtrochanteric fractures in bisphosphonate-naive patients

    DEFF Research Database (Denmark)

    Adachi, Jonathan D; Lyles, Kenneth; Boonen, Steven;

    2011-01-01

    Our purpose was to characterize the risks of osteoporosis-related subtrochanteric fractures in bisphosphonate-naive individuals. Baseline characteristics of patients enrolled in the HORIZON-Recurrent Fracture Trial with a study-qualifying hip fracture were examined, comparing those who sustained ...

  20. PREFACE: Symposium 1: Advanced Structure Analysis and Characterization of Ceramic Materials

    Science.gov (United States)

    Yashima, Masatomo

    2011-05-01

    Preface to Symposium 1 (Advanced Structure Analysis and Characterization of Ceramic Materials) of the International Congress of Ceramics III, held 14-18 November 2010 in Osaka, Japan Remarkable developments have been made recently in the structural analysis and characterization of inorganic crystalline and amorphous materials, such as x-ray, neutron, synchrotron and electron diffraction, x-ray/neutron scattering, IR/Raman scattering, NMR, XAFS, first-principle calculations, computer simulations, Rietveld analysis, the maximum-entropy method, in situ measurements at high temperatures/pressures and electron/nuclear density analysis. These techniques enable scientists to study not only static and long-range periodic structures but also dynamic and short-/intermediate-range structures. Multi-scale characterization from the electron to micrometer levels is becoming increasingly important as a means of understanding phenomena at the interfaces, grain boundaries and surfaces of ceramic materials. This symposium has discussed the structures and structure/property relationships of various ceramic materials (electro, magnetic and optical ceramics; energy and environment related ceramics; bio-ceramics; ceramics for reliability secure society; traditional ceramics) through 38 oral presentations including 8 invited lectures and 49 posters. Best poster awards were given to six excellent poster presentations (Y-C Chen, Tokyo Institute of Technology; C-Y Chung, Tohoku University; T Stawski, University of Twente; Y Hirano, Nagoya Institute of Technology; B Bittova, Charles University Prague; Y Onodera, Kyoto University). I have enjoyed working with my friends in the ICC3 conference. I would like to express special thanks to other organizers: Professor Scott T Misture, Alfred University, USA, Professor Xiaolong Chen, Institute of Physics, CAS, China, Professor Takashi Ida, Nagoya Institute of Technology, Japan, Professor Isao Tanaka, Kyoto University, Japan. I also acknowledge the

  1. New C2 synchondrosal fracture classification system

    Energy Technology Data Exchange (ETDEWEB)

    Rusin, Jerome A.; Ruess, Lynne [Department of Radiology, Nationwide Children' s Hospital, Columbus, OH (United States); The Ohio State University College of Medicine and Public Health, Columbus, OH (United States); Daulton, Robert S. [Department of Radiology, Nationwide Children' s Hospital, Columbus, OH (United States)

    2015-06-15

    Excessive cervical flexion-extension accompanying mild to severe impact injuries can lead to C2 synchondrosal fractures in young children. To characterize and classify C2 synchondrosal fracture patterns. We retrospectively reviewed imaging and medical records of children who were treated for cervical spine fractures at our institution between 1995 and 2014. We reviewed all fractures involving the five central C2 synchondroses with regard to patient demographics, mechanism of injury, fracture pattern, associated fractures and other injuries, treatment plans and outcome. Fourteen children had fractures involving the central C2 synchondroses. There were nine boys and five girls, all younger than 6 years. We found four distinct fracture patterns. Eleven complete fractures were further divided into four subtypes (a, b, c and d) based on degree of anterior displacement of the odontoid segment and presence of distraction. Nine of these 11 children had fractures through both odontoneural synchondroses and the odontocentral synchondrosis; one had fractures involving both neurocentral synchondroses and the odontoneural synchondrosis; one had fractures through bilateral odontoneural and bilateral neurocentral synchondroses. Three children had incomplete fractures, defined as a fracture through a single odontoneural synchondrosis with or without partial extension into either the odontocentral or the adjacent neurocentral synchondroses. All complete fractures were displaced or angulated. Four had associated spinal cord injury, including two contusions (subtype c fractures) and two fatal transections (subtype d fractures). Most children were treated with primary halo stabilization. Subtype c fractures required surgical fixation. We describe four patterns of central C2 synchondrosal fractures, including two unique patterns that have not been reported. We propose a classification system to distinguish these fractures and aid in treatment planning. (orig.)

  2. Multi-isotope (carbon and chlorine) analysis for fingerprinting and site characterization at a fractured bedrock aquifer contaminated by chlorinated ethenes

    Energy Technology Data Exchange (ETDEWEB)

    Palau, Jordi, E-mail: jordi.palau@unine.ch [Departament de Cristal.lografia, Mineralogia i Dipòsits Minerals, Facultat de Geologia, Universitat de Barcelona, Martí i Franquès, s/n 08028 Barcelona (Spain); Marchesi, Massimo [Departament de Cristal.lografia, Mineralogia i Dipòsits Minerals, Facultat de Geologia, Universitat de Barcelona, Martí i Franquès, s/n 08028 Barcelona (Spain); Department of Earth and Environmental Sciences, University of Waterloo, Waterloo, Ontario N2L 3G1 (Canada); Chambon, Julie C.C. [Department of Environmental Engineering, Technical University of Denmark, 2800 Lyngby (Denmark); Aravena, Ramon [Department of Earth and Environmental Sciences, University of Waterloo, Waterloo, Ontario N2L 3G1 (Canada); Canals, Àngels [Departament de Cristal.lografia, Mineralogia i Dipòsits Minerals, Facultat de Geologia, Universitat de Barcelona, Martí i Franquès, s/n 08028 Barcelona (Spain); Binning, Philip J.; Bjerg, Poul L. [Department of Environmental Engineering, Technical University of Denmark, 2800 Lyngby (Denmark); Otero, Neus; Soler, Albert [Departament de Cristal.lografia, Mineralogia i Dipòsits Minerals, Facultat de Geologia, Universitat de Barcelona, Martí i Franquès, s/n 08028 Barcelona (Spain)

    2014-03-01

    The use of compound specific multi-isotope approach (C and Cl) in the characterization of a chlorinated ethenes contaminated fractured aquifer allows the identification of several sources and contaminant plumes, as well as the occurrence of biodegradation and mixing processes. The study site is located in Spain with contamination resulting in groundwater concentrations of up to 50 mg/L of trichloroethene (TCE), the most abundant chlorinated ethene, and 7 mg/L of tetrachloroethene (PCE). The potential sources of contamination including abandoned barrels, an underground tank, and a disposal lagoon, showed a wide range in δ{sup 13}C values from − 15.6 to − 40.5‰ for TCE and from − 18.5 to − 32.4‰ for PCE, allowing the use of isotope fingerprinting for tracing of the origin and migration of these contaminants in the aquifer. In contrast, there is no difference between the δ{sup 37}Cl values for TCE in the contaminant sources, ranging from + 0.53 to + 0.66‰. Variations of δ{sup 37}Cl and δ{sup 13}C in the different contaminant plumes were used to investigate the role of biodegradation in groundwater. Moreover, the isotopic data were incorporated into a reactive transport model for determination of whether the isotope pattern observed downstream from the tank's source could be explained by the simultaneous effect of mixing and biodegradation. The results demonstrate that a multi-isotope approach is a valuable tool for characterization of complex sites such as fractured bedrock aquifer contaminated by multiple sources, providing important information which can be used by consultants and site managers to prioritize and design more successful remediation strategies. - Highlights: • Origin and fate of CAHs in groundwater by means of multi CSIA ({sup 13}C,{sup 35}Cl) survey • Innovative/new approach tested in a fractured bedrock site • Differentiation of distinct CAH sources • Biodegradation and source mixing recognition in the aquifer.

  3. Hydraulic fracture propagation modeling and data-based fracture identification

    Science.gov (United States)

    Zhou, Jing

    Successful shale gas and tight oil production is enabled by the engineering innovation of horizontal drilling and hydraulic fracturing. Hydraulically induced fractures will most likely deviate from the bi-wing planar pattern and generate complex fracture networks due to mechanical interactions and reservoir heterogeneity, both of which render the conventional fracture simulators insufficient to characterize the fractured reservoir. Moreover, in reservoirs with ultra-low permeability, the natural fractures are widely distributed, which will result in hydraulic fractures branching and merging at the interface and consequently lead to the creation of more complex fracture networks. Thus, developing a reliable hydraulic fracturing simulator, including both mechanical interaction and fluid flow, is critical in maximizing hydrocarbon recovery and optimizing fracture/well design and completion strategy in multistage horizontal wells. A novel fully coupled reservoir flow and geomechanics model based on the dual-lattice system is developed to simulate multiple nonplanar fractures' propagation in both homogeneous and heterogeneous reservoirs with or without pre-existing natural fractures. Initiation, growth, and coalescence of the microcracks will lead to the generation of macroscopic fractures, which is explicitly mimicked by failure and removal of bonds between particles from the discrete element network. This physics-based modeling approach leads to realistic fracture patterns without using the empirical rock failure and fracture propagation criteria required in conventional continuum methods. Based on this model, a sensitivity study is performed to investigate the effects of perforation spacing, in-situ stress anisotropy, rock properties (Young's modulus, Poisson's ratio, and compressive strength), fluid properties, and natural fracture properties on hydraulic fracture propagation. In addition, since reservoirs are buried thousands of feet below the surface, the

  4. Design, Fabrication, and Characterization of Carbon Nanotube Field Emission Devices for Advanced Applications

    Science.gov (United States)

    Radauscher, Erich Justin

    Carbon nanotubes (CNTs) have recently emerged as promising candidates for electron field emission (FE) cathodes in integrated FE devices. These nanostructured carbon materials possess exceptional properties and their synthesis can be thoroughly controlled. Their integration into advanced electronic devices, including not only FE cathodes, but sensors, energy storage devices, and circuit components, has seen rapid growth in recent years. The results of the studies presented here demonstrate that the CNT field emitter is an excellent candidate for next generation vacuum microelectronics and related electron emission devices in several advanced applications. The work presented in this study addresses determining factors that currently confine the performance and application of CNT-FE devices. Characterization studies and improvements to the FE properties of CNTs, along with Micro-Electro-Mechanical Systems (MEMS) design and fabrication, were utilized in achieving these goals. Important performance limiting parameters, including emitter lifetime and failure from poor substrate adhesion, are examined. The compatibility and integration of CNT emitters with the governing MEMS substrate (i.e., polycrystalline silicon), and its impact on these performance limiting parameters, are reported. CNT growth mechanisms and kinetics were investigated and compared to silicon (100) to improve the design of CNT emitter integrated MEMS based electronic devices, specifically in vacuum microelectronic device (VMD) applications. Improved growth allowed for design and development of novel cold-cathode FE devices utilizing CNT field emitters. A chemical ionization (CI) source based on a CNT-FE electron source was developed and evaluated in a commercial desktop mass spectrometer for explosives trace detection. This work demonstrated the first reported use of a CNT-based ion source capable of collecting CI mass spectra. The CNT-FE source demonstrated low power requirements, pulsing

  5. Fracture Mechanics

    CERN Document Server

    Zehnder, Alan T

    2012-01-01

    Fracture mechanics is a vast and growing field. This book develops the basic elements needed for both fracture research and engineering practice. The emphasis is on continuum mechanics models for energy flows and crack-tip stress- and deformation fields in elastic and elastic-plastic materials. In addition to a brief discussion of computational fracture methods, the text includes practical sections on fracture criteria, fracture toughness testing, and methods for measuring stress intensity factors and energy release rates. Class-tested at Cornell, this book is designed for students, researchers and practitioners interested in understanding and contributing to a diverse and vital field of knowledge. Alan Zehnder joined the faculty at Cornell University in 1988. Since then he has served in a number of leadership roles including Chair of the Department of Theoretical and Applied Mechanics, and Director of the Sibley School of Mechanical and Aerospace Engineering.  He teaches applied mechanics and his research t...

  6. Characterization of geolocation accuracy of Suomi NPP Advanced Technology Microwave Sounder measurements

    Science.gov (United States)

    Han, Yang; Weng, Fuzhong; Zou, Xiaolei; Yang, Hu; Scott, Deron

    2016-05-01

    The Advanced Technology Microwave Sounder (ATMS) onboard Suomi National Polar-orbiting Partnership satellite has 22 channels at frequencies ranging from 23 to 183 GHz for probing the atmospheric temperature and moisture under all weather conditions. As part of the ATMS calibration and validation activities, the geolocation accuracy of ATMS data must be well characterized and documented. In this study, the coastline crossing method (CCM) and the land-sea fraction method (LFM) are utilized to characterize and quantify the ATMS geolocation accuracy. The CCM is based on the inflection points of the ATMS window channel measurements across the coastlines, whereas the LFM collocates the ATMS window channel data with high-resolution land-sea mask data sets. Since the ATMS measurements provide five pairs of latitude and longitude data for K, Ka, V, W, and G bands, respectively, the window channels 1, 2, 3, 16, and 17 from each of these five bands are chosen for assessing the overall geolocation accuracy. ATMS geolocation errors estimated from both methods are generally consistent from 40 cases in June 2014. The ATMS along-track (cross-track) errors at nadir are within ±4.2 km (±1.2 km) for K/Ka, ±2.6 km (±2.7 km) for V bands, and ±1.2 km (±0.6 km) at W and G bands, respectively. At the W band, the geolocation errors derived from both algorithms are probably less reliable due to a reduced contrast of brightness temperatures in coastal areas. These estimated ATMS along-track and cross-track geolocation errors are well within the uncertainty requirements for all bands.

  7. [Hip Fracture--Epidemiology, Management and Liaison Service. Risk factor for hip fracture].

    Science.gov (United States)

    Fujiwara, Saeko

    2015-04-01

    Many risk factors have been identified for hip fracture, including female, advanced age, osteoporosis, previous fractures, low body weight or low body mass index, alcohol drinking, smoking, family history of fractures, use of glucocorticoid, factors related to falls, and bone strength. The factors related to falls are number of fall, frail, post stroke, paralysis, muscle weakness, anti-anxiety drugs, anti-depression drugs, and sedatives. Dementia and respiratory disease and others have been reported to be risk factors for secondary hip fracture.

  8. Mining the Advanced Spectral Library (ASTRAL): Characterizing Winds of Evolved M-Stars

    Science.gov (United States)

    Nielsen, Krister E.; Carpenter, K. G.; Kober, G. V.; Cheng, K.; Ayres, T. R.; Harper, G.

    2013-01-01

    The HST/STIS treasury program Advanced Spectral Library (ASTRAL) enables investigations of the character and dynamics of the wind and chromosphere of cool stars, using high quality spectral data. This paper present the analysis of the outflowing winds of the M3.4 giant Gamma Cru and the M2Iab supergiant Alpha Ori. The outer atmospheres of these objects show strong evidence for significant inhomogeneity in their thermal and kinematic structure, and are in general not well understood. The wind features are characterized by a strong chromospheric emission suppressed by a overlying wind absorption, for many transitions producing a double peak feature. The relative strengths and wavelength shifts between the absorption and emission components of the lines reflect the acceleration of the wind from the base of the chromosphere, as the self-absorption is due to the overlying wind absorption, whose velocity relative to the chromosphere varies with height and thus line opacity. The wind profiles are sensitive to the wind opacity, turbulence and flow velocity, and hence favorable to analyze with the Sobolev source function with Exact Integration of the transfer equation (SEI) code. This paper will show a velocity and intensity analysis of the wind profiles and modeling with the SEI code to derive an improved set of wind parameters, primarily, for Gamma Cru.

  9. Characterization techniques for the high-brightness particle beams of the Advanced Photon Source (APS)

    Energy Technology Data Exchange (ETDEWEB)

    Lumpkin, A.H.

    1993-08-01

    The Advanced Photon Source (APS) will be a third-generation synchrotron radiation (SR) user facility in the hard x-ray regime (10--100 keV). The design objectives for the 7-GeV storage ring include a positron beam natural emittance of 8 {times} 10{sup {minus}9} m-rad at an average current of 100 mA. Proposed methods for measuring the transverse and longitudinal profiles will be described. Additionally, a research and development effort using an rf gun as a low-emittance source of electrons for injection into the 200- to 650-MeV linac subsystem is underway. This latter system is projected to produce electron beams with a normalized, rms emittance of {approximately}2 {pi} mm-mrad at peak currents of near one hundred amps. This interesting characterization problem will also be briefly discussed. The combination of both source types within one laboratory facility will stimulate the development of diagnostic techniques in these parameter spaces.

  10. Advanced Compatibility Characterization Of AF-M315E With Spacecraft Propulsion System Materials Project

    Science.gov (United States)

    McClure, Mark B.; Greene, Benjamin

    2014-01-01

    All spacecraft require propulsion systems for thrust and maneuvering. Propulsion systems can be chemical, nuclear, electrical, cold gas or combinations thereof. Chemical propulsion has proven to be the most reliable technology since the deployment of launch vehicles. Performance, storability, and handling are three important aspects of liquid chemical propulsion. Bipropellant systems require a fuel and an oxidizer for propulsion, but monopropellants only require a fuel and a catalyst for propulsion and are therefore simpler and lighter. Hydrazine is the state of the art propellant for monopropellant systems, but has drawbacks because it is highly hazardous to human health, which requires extensive care in handling, complex ground ops due to safety and environmental considerations, and lengthy turnaround times for reusable spacecraft. All users of hydrazine monopropellant must contend with these issues and their associated costs. The development of a new monopropellant, intended to replace hydrazine, has been in progress for years. This project will apply advanced techniques to characterize the engineering properties of materials used in AF-M315E propulsion systems after propellant exposure. AF-M315E monopropellant has been selected HQ's Green Propellant Infusion Mission (GPIM) to replace toxic hydrazine for improved performance and reduce safety and health issues that will shorten reusable spacecraft turn-around time. In addition, this project will fundamentally strengthen JSC's core competency to evaluate, use and infuse liquid propellant systems.

  11. X-Ray microprobe characterization of materials: the case for undulators on advanced storage rings

    International Nuclear Information System (INIS)

    The unique properties of X-rays offer many advantages over electrons and other charged particles for the microcharacterization of materials. X-rays are more efficient in exciting characteristic X-ray fluorescence and produce higher fluorescent signals to backgrounds than obtained with electrons. Detectable limits for X-rays are a few parts per billion and are 10-3 to 10-5 less than obtained with electrons. Energy deposition in the sample by X-rays is 10-3 to 10-4 less than for electrons for the same detectable concentration. High-brightness storage rings, especially in the 6 GeV class with undulators, will be approximately 103 brighter in the X-ray energy range from 5 keV to 35 keV than existing storage rings and provide for X-ray microprobes that are as bright as the most advanced electron probes. Such X-ray microprobes will produce unprecedented low levels of detection in diffraction, EXAFS, Auger, and photoelectron spectoscopies for both chemical characterization and elemental identification. These major improvements in microcharacterization capabilities will be wide-ranging ramifications not only in materials science but also in physics, chemistry, geochemistry, biology, and medicine

  12. Application of advanced radiographic imaging techniques for characterizing low level nuclear waste

    International Nuclear Information System (INIS)

    BIR is currently investigating the use of two advanced x-ray imaging techniques for characterizing containers of solidified nuclear waste. These techniques, digital radiography (DR) and computed tomography (CT), are performed by computerized imaging systems that can automatically inspect containers using a set of imaging parameters chosen by the operator. Both inspection techniques can be performed by the same imaging system. The inspection result is a computer image, or series of images, that can be manipulated by the operator to show a wide variety of features within the inspected object. For the inspections performed so far, we have used the ACTIS CT/DR system that BIR designed and built for NASA's Marshall Space Flight Center. The inspections are being performed as part of a continuing Phase I/Phase II SBIR program for the U.S. Department of Energy. This paper discusses inspections performed on three types of waste containers: (1) a simulated waste drum imaged in Phase 1; (2) 55 gallon drums of assorted waste items supplied by the DOE'S EG and G Rocky Flats plant and by Westinghouse Hanford; and (3) several containers of glass used for solidifying radioactive substances, supplied by the DOE'S Westinghouse Savannah River site. The Phase II work also includes investigating dual energy CT imaging and designing a mechanically simplified ACTIS system and mobile trailer specifically for waste inspection. (author)

  13. Preparation and characterization of an advanced collagen aggregate from porcine acellular dermal matrix.

    Science.gov (United States)

    Liu, Xinhua; Dan, Nianhua; Dan, Weihua

    2016-07-01

    The objective of this study was to extract and characterize an advanced collagen aggregate (Ag-col) from porcine acellular dermal matrix (pADM). Based on histological examination, scanning electron microscopy (SEM) and atomic force microscope (AFM), Ag-col was composed of the D-periodic cross-striated collagen fibrils and thick collagen fiber bundles with uneven diameters and non-orientated arrangement. Fourier transform infrared (FTIR) spectra of pADM, Ag-col and Col were similar and revealed the presence of the triple helix. Circular dichroism (CD) analysis exhibited a slightly higher content of α-helix but inappreciably less amount of random coil structure in Ag-col compared to Col. Moreover, imino acid contents of pADM, Ag-col and Col were 222.43, 218.30 and 190.01 residues/1000 residues, respectively. From zeta potential analysis, a net charge of zero was found at pH 6.45 and 6.11 for Ag-col and Col, respectively. Differential scanning calorimetry (DSC) study suggested that the Td of Ag-col was 20°C higher than that of Col as expected, and dynamic mechanical analysis (DMA) indicated that Ag-col possessed a higher storage modulus but similar loss factor compared to Col. Therefore, the collagen aggregate from pADM could serve as a better alternative source of collagens for further applications in food and biological industries. PMID:27039117

  14. Characterization of the Edge Crack Torsion (ECT) Test for Mode III Fracture Toughness Measurement of Laminated Composites

    Science.gov (United States)

    Ratcliffe, James G.

    2004-01-01

    The edge crack torsion (ECT) test is designed to initiate mode III delamination growth in composite laminates. The test has undergone several design changes during its development. The objective of this paper was to determine the suitability of the current ECT test design a mode III fracture test. To this end, ECT tests were conducted on specimens manufactured from IM7/8552 and S2/8552 tape laminates. Three-dimensional finite element analyses were performed. The analysis results were used to calculate the distribution of mode I, mode II, and mode III strain energy release rate along the delamination front. The results indicated that mode IIIdominated delamination growth would be initiated from the specimen center. However, in specimens of both material types, the measured values of GIIIc exhibited significant dependence on delamination length. Load-displacement response of the specimens exhibited significant deviation from linearity before specimen failure. X-radiographs of a sample of specimens revealed that damage was initiated in the specimens prior to failure. Further inspection of the failure surfaces is required to identify the damage and determine that mode III delamination is initiated in the specimens.

  15. External fixation in contemporary fracture management

    OpenAIRE

    McCoy, G. F.; Orr, J. F.; Templeton, J.

    1987-01-01

    Important advances have been made within the last two decades in the field of fracture management. The development of the AO internal fixation system and the advances in cast bracing techniques are but two of the improvements worthy of mention. It is, however, in the field of external fixation of fractures that the greatest advances have been made. This paper traces the history of external fixation up to the present day and discusses, with examples, the application of external fixation in the...

  16. Mechanical properties of fracture zones

    International Nuclear Information System (INIS)

    Available data on mechanical characteristics of fracture zones are compiled and discussed. The aim is to improve the basis for adequate representation of fracture zones in geomechanical models. The sources of data researched are primarily borehole investigations and case studies in rock engineering, involving observations of fracture zones subjected to artificial load change. Boreholes only yield local information about the components of fracture zones, i.e. intact rock, fractures and various low-strength materials. Difficulties are therefore encountered in evaluating morphological and mechanical properties of fracture zones from borehole data. Although often thought of as macroscopically planar features, available field data consistently show that fracture zones are characterized by geometrical irregularities such as thickness variations, surface undulation and jogs. These irregularities prevail on all scales. As a result, fracture zones are on all scales characterized by large, in-plane variation of strength- and deformational properties. This has important mechanical consequences in terms of non-uniform stress transfer and complex mechanisms of shear deformation. Field evidence for these findings, in particular results from the underground research laboratory in Canada and from studies of induced fault slip in deep mines, is summarized and discussed. 79 refs

  17. Advanced characterization of MIMAS MOX fuel microstructure to quantify the HBS formation

    Energy Technology Data Exchange (ETDEWEB)

    Bouloré, Antoine, E-mail: antoine.boulore@cea.fr [CEA, DEN, DEC Fuel Research Department, Cadarache, F13108 Saint-Paul-lez-Durance (France); Aufore, Laurence; Federici, Eric [CEA, DEN, DEC Fuel Research Department, Cadarache, F13108 Saint-Paul-lez-Durance (France); Blanpain, Patrick [AREVA NP SAS, 10 rue Juliette Récamier, F-69456 Lyon (France); Blachier, Rémi [EDF, SEPTEN, 12-14 Av. Dutrievoz, F-69628 Villeurbanne (France)

    2015-01-15

    Highlights: • An advanced characterization of MIMAS MOX fuel based only on fresh fuel pellet characterization. • A probabilistic approach to model the High Burnup Structure formation in oxide fuels. • Validation of the method by comparing to experimental data obtained on fuel irradiated in the Halden reactor. - Abstract: Fission gas behaviour in accidental situations is closely related to the location of fission gas before the accident. More precisely, most of the fission gas in intergranular position is released during the accident and HBS zones contribute a lot to this intergranular quantity. So a methodology to characterize the HBS zones a priori from examination of unirradiated pellet has been developed at CEA. Characterization of plutonium distribution in MIMAS MOX fresh fuel pellets can be performed by image analysis on 1 mm{sup 2} X-ray mappings of plutonium acquired using Electron Probe Micro Analysis (EPMA). The specific software developed to describe the fuel using Pu X-ray mapping (ANACONDA) has been improved in order to simulate the fission products (FP) production and recoil during a given irradiation of the fuel, taking into account the evolution of the plutonium due to neutron irradiation. This simulation results from calculations with our fuel performance code ALCYONE combined with image processing. The final result is a mapping of local burn-up, but also the distribution of the relative FP concentration as a function of the local burn-up. A validation of this simulation process has been done by comparing the simulated mapping of neodymium to one measured on the same fuel batch after irradiation. Using previous studies of mechanisms for HBS formation, a probabilistic criterion for HBS formation has been proposed, based on the EPMA measurements of the decrease of the xenon signal as a function of the local burn-up. Combining the simulated FP cartography with this probabilistic HBS formation criterion, it is possible to calculate the surface

  18. Characterization of Tubing from Advanced ODS alloy (FCRD-NFA1)

    Energy Technology Data Exchange (ETDEWEB)

    Maloy, Stuart Andrew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Aydogan, Eda [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Anderoglu, Osman [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Lavender, Curt [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Anderson, Iver [Ames Lab., Ames, IA (United States); Rieken, Joel [Ames Lab., Ames, IA (United States); Lewandowski, John [Case Western Reserve Univ., Cleveland, OH (United States); Hoelzer, Dave [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Odette, George R. [Univ. of California, Santa Barbara, CA (United States)

    2016-09-20

    Fabrication methods are being developed and tested for producing fuel clad tubing of the advanced ODS 14YWT and FCRD-NFA1 ferritic alloys. Three fabrication methods were based on plastically deforming a machined thick-wall tube sample of the ODS alloys by pilgering, hydrostatic extrusion or drawing to decrease the outer diameter and wall thickness and increase the length of the final tube. The fourth fabrication method consisted of the additive manufacturing approach involving solid-state spray deposition (SSSD) of ball milled and annealed powder of 14YWT for producing thin-wall tubes. Of the four fabrication methods, two methods were successful at producing tubing for further characterization: production of tubing by high-velocity oxy-fuel spray forming and production of tubing using high-temperature hydrostatic extrusion. The characterization described shows through neutron diffraction the texture produced during extrusion while maintaining the beneficial oxide dispersion. In this research, the parameters for innovative thermal spray deposition and hot extrusion processing methods have been developed to produce the final nanostructured ferritic alloy (NFA) tubes having approximately 0.5 mm wall thickness. Effect of different processing routes on texture and grain boundary characteristics has been investigated. It was found that hydrostatic extrusion results in combination of plane strain and shear deformations which generate rolling textures of α- and γ-fibers on {001}<110> and {111}<110> together with a shear texture of ζ-fiber on {011}<211> and {011}<011>. On the other hand, multi-step plane strain deformation in cross directions leads to a strong rolling textures of θ- and ε-fiber on {001}<110> together with weak γ-fiber on {111}<112>. Even though the amount of the equivalent strain is similar, shear deformation leads to much lower texture indexes compared to the plane strain deformations. Moreover, while 50% of hot rolling brings about a large number of

  19. CCS Acceptability: Social Site Characterization and Advancing Awareness at Prospective Storage Sites in Poland and Scotland

    Directory of Open Access Journals (Sweden)

    Brunsting Suzanne

    2015-04-01

    Full Text Available This paper summarizes the work on the social dimension conducted within the EU FP7 SiteChar project. The most important aim of the research was to advance public awareness and draw lessons for successful public engagement activities when developing a CO2 storage permit application. To this end, social site characterization (e.g. representative surveys and public participation activities (focus conference were conducted at two prospective Carbon Capture and Storage (CCS sites: an onshore site in Poland and an offshore site in Scotland. The research consisted of four steps over a time period of 1.5 year, from early 2011 to mid-2012. The first step consisted of four related qualitative and quantitative research activities to provide a social characterization of the areas: desk research, stakeholder interviews, media analyses, and a survey among representative samples of the local community. The aim was to identify: stakeholders or interested parties; factors that may drive their perceptions of and attitudes towards CCS. Results were used to as input for the second step, in which a new format for public engagement named ‘focus conferences’ was tested at both sites involving a small sample of the local community. The third step consisted of making available generic as well as site-specific information to the general and local public, by: setting up a bilingual set of information pages on the project website suitable for a lay audience; organizing information meetings at both sites that were open to all who took interest. The fourth step consisted of a second survey among a new representative sample of the local community. The survey was largely identical to the survey in step 1 to enable the monitoring of changes in awareness, knowledge and opinions over time. Results provide insight in the way local CCS plans may be perceived by the local stakeholders, how this can be reliably assessed at early stage without raising unnecessary concerns, and how

  20. CCS acceptability: social site characterization and advancing awareness at prospective storage sites in Poland and Scotland

    International Nuclear Information System (INIS)

    This paper summarizes the work on the social dimension conducted within the EU FP7 SiteChar project. The most important aim of the research was to advance public awareness and draw lessons for successful public engagement activities when developing a CO2 storage permit application. To this end, social site characterization (e.g. representative surveys) and public participation activities (focus conference) were conducted at two prospective Carbon Capture and Storage (CCS) sites: an onshore site in Poland and an offshore site in Scotland. The research consisted of four steps over a time period of 1.5 year, from early 2011 to mid-2012. The first step consisted of four related qualitative and quantitative research activities to provide a social characterization of the areas: desk research, stakeholder interviews, media analyses, and a survey among representative samples of the local community. The aim was to identify: - stakeholders or interested parties; - factors that may drive their perceptions of and attitudes towards CCS. Results were used to as input for the second step, in which a new format for public engagement named 'focus conferences' was tested at both sites involving a small sample of the local community. The third step consisted of making available generic as well as site-specific information to the general and local public, by: - setting up a bilingual set of information pages on the project web site suitable for a lay audience; - organizing information meetings at both sites that were open to all who took interest. The fourth step consisted of a second survey among a new representative sample of the local community. The survey was largely identical to the survey in step 1 to enable the monitoring of changes in awareness, knowledge and opinions over time. Results provide insight in the way local CCS plans may be perceived by the local stakeholders, how this can be reliably assessed at early stage without raising unnecessary concerns, and how

  1. Chemical characterization of emissions from advanced technology light-duty vehicles

    Science.gov (United States)

    Graham, Lisa

    Results of detailed emissions measurements of seven 2000 model year advanced technology vehicles are reported. Six of the seven vehicles were imported from Europe and Japan and are not yet available for sale in Canada. Three of the vehicles were with direct injection diesel (DDI) technology, three with gasoline direct injection (GDI) technology and one vehicle was a gasoline-electric hybrid. It is expected that vehicles with these technologies will be forming a larger fraction of the Canadian light-duty vehicle fleet in the coming years in response to requirements to reduce greenhouse gas emissions from the transportation sector in support of Canada's ratification of the Kyoto Protocol; and as a result of improving fuel quality (most notably reducing the sulphur content of both diesel and gasoline). It is therefore important to understand the potential impacts on air quality of such changes in the composition of the vehicle fleet. The emissions from these vehicles were characterized over four test cycles representing different driving conditions. Samples of the exhaust were collected for determining methane, non-methane hydrocarbons and carbonyl compounds for the purposes of comparing ozone-forming potential of the emissions. Although these vehicles were not certified to Canadian emissions standards as tested, all vehicles met the then current Tier 1 emission standards, except for one diesel vehicle which did not meet the particulate matter (PM) standard. The DDI vehicles had the highest NO X emissions, the highest specific reactivity and the highest ozone-forming potential of the vehicles tested. When compared to conventional gasoline vehicles, the ozone-forming potential was equivalent. The GDI vehicles had lower NO X emissions, lower specific reactivity and lower ozone-forming potential than the conventional gasoline vehicles. Both the diesel and GDI vehicles had higher PM emissions than the conventional gasoline vehicles. The gasoline-electric hybrid vehicle

  2. Characterization of a linear device developed for research on advanced plasma imaging and dynamics

    International Nuclear Information System (INIS)

    Within the scope of long term research on imaging diagnostics for steady-state plasmas and understanding of edge plasma physics through diagnostics with conventional spectroscopic methods, we have constructed a linear electron cyclotron resonance (ECR) plasma device named Research on Advanced Plasma Imaging and Dynamics (RAPID). It has a variety of axial magnetic field profiles provided by eight water-cooled magnetic coils and two dc power supplies. The positions of the magnetic coils are freely adjustable along the axial direction and the power supplies can be operated with many combinations of electrical wiring to the coils. Here, a 6 kW 2.45 GHz magnetron is used to produce steady-state hydrogen, helium, and argon plasmas with central magnetic fields of 875 and/or 437.5 G (second harmonic). In order to achieve the highest possible plasma performance within the limited input parameters, wall conditioning experiments were carried out. Chamber bake-out was achieved with heating coils that were wound covering the vessel, and long-pulse electron cyclotron heating discharge cleaning was also followed after 4 days of bake-out. A uniform bake-out temperature (150 deg. C) was achieved by wrapping the vessel in high temperature thermal insulation textile and by controlling the heating coil current using a digital control system. The partial pressure changes were observed using a residual gas analyzer, and a total system pressure of 5x10-8 Torr was finally reached. Diagnostic systems including a millimeter-wave interferometer, a high resolution survey spectrometer, a Langmuir probe, and an ultrasoft x-ray detector were used to provide the evidence that the plasma performance was improved as we desired. In this work, we present characterization of the RAPID device for various system conditions and configurations.

  3. Biologically active collagen-based scaffolds: advances in processing and characterization.

    Science.gov (United States)

    Yannas, I V; Tzeranis, D S; Harley, B A; So, P T C

    2010-04-28

    A small number of type I collagen-glycosaminoglycan scaffolds (collagen-GAG scaffolds; CGSs) have unusual biological activity consisting primarily in inducing partial regeneration of organs in the adult mammal. Two of these are currently in use in a variety of clinical settings. CGSs appear to induce regeneration by blocking the adult healing response, following trauma, consisting of wound contraction and scar formation. Several structural determinants of biological activity have been identified, including ligands for binding of fibroblasts to the collagen surface, the mean pore size (which affects ligand density) and the degradation rate (which affects the duration of the wound contraction-blocking activity by the scaffold). Processing variables that affect these determinants include the kinetics of swelling of collagen fibres in acetic acid, freezing of the collagen-GAG suspension and cross-linking of the freeze-dried scaffold. Recent developments in the processing of CGSs include fabrication of scaffolds that are paucidisperse in pore size, scaffolds with gradients in physicochemical properties (and therefore biological activity) and scaffolds that incorporate a mineral component. Advances in the characterization of the pore structure of CGSs have been made using confocal and nonlinear optical microscopy (NLOM). The mechanical behaviour of CGSs, as well as the resistance to degradative enzymes, have been studied. Following seeding with cells (typically fibroblasts), contractile forces in the range 26-450 nN per cell are generated by the cells, leading to buckling of scaffold struts. Ongoing studies of cell-seeded CGSs with NLOM have shown an advantage over the use of confocal microscopy due to the ability of the former method to image the CGS surfaces without staining (which alters its surface ligands), reduced cell photodamage, reduced fluorophore photobleaching and the ability to image deeper inside the scaffold. PMID:20308118

  4. Characterization of mechanical properties of aluminized coatings in advanced gas turbine blades using a small punch method

    Energy Technology Data Exchange (ETDEWEB)

    Sugita, Y.; Ito, M. [Chuba Electric Power Co., Nagoya (Japan). Electric Power R and D Center; Sakurai, S. [Hitachi Ltd. (Japan). Mechanical Engineering Research Lab.; Bloomer, T.E.; Kameda, J. [Ames Lab., IA (United States)]|[Iowa State Univ., Ames, IA (United States). Center for Advanced Technology Development

    1997-04-01

    Advanced technologies of superalloy casting and coatings enable one to enhance the performance of combined cycle gas turbines for electric power generation by increasing the firing temperature. This paper describes examination of the microstructure/composition and mechanical properties (22--950 C) in aluminized CoCrAlY coatings of advanced gas turbine blades using scanning Auger microprobe and a small punch (SP) testing method. Aluminized coatings consisted of layered structure divided into four regimes: (1) Al enriched and Cr depleted region, (2) Al and Cr graded region, (3) fine grained microstructure with a mixture of Al and Cr enriched phases and (4) Ni/Co interdiffusion zone adjacent to the interface. SP specimens were prepared in order that the specimen surface would be located in the various coating regions. SP tests indicated strong dependence of the fracture properties on the various coatings regimes. Coatings 1 and 2 with very high microhardness showed much easier formation of brittle cracks in a wide temperature range, compared to coatings 3 and 4 although the coating 2 had ductility improvement at 950 C. The coating 3 had lower room temperature ductility than the coating 4. However, the ductility in the coating 3 exceeded that in the region 4 above 730 C due to a precipitous ductility increase. The integrity of aluminized coatings while in-service is discussed in light of the variation of the low cycle fatigue life as well as the ductility in the layered structure.

  5. Fracture toughness of irradiated stainless steel alloys

    International Nuclear Information System (INIS)

    The postirradiation fracture toughness responses of Types 316 and 304 stainless steel (SS) wrought products, cast CF8 SS and Type 308 SS weld deposit were characterized at 4270C using J/sub R/-curve techniques. Fast-neutron irradiation of these alloys caused an order of magnitude reduction in J/sub c/ and two orders of magnitude reduction in tearing modulus at neutron exposures above 10 dpa, where radiation-induced losses in toughness appeared to saturate. Saturation J/sub c/ values for the wrought materials ranged from 28 to 31 kJ/m2; the weld exhibited a saturation level of 11 kJ/m2. Maximum allowable flaw sizes for highly irradiated stainless steel components stressed to 90% of the unirradiated yield strength are on the order of 3 cm for the wrought material and 1 cm for the weld. Electron fractographic examination revealed that irradiation displacement damage brought about a transition from ductile microvoid coalescence to channel fracture, associated with local separation along planar deformation bands. The lower saturation toughness value for the weld relative to that for the wrought products was attributed to local failure of ferrite particles ahead of the advancing crack which prematurely initiated channel fracture

  6. Fractures in infants and toddlers with rickets

    Energy Technology Data Exchange (ETDEWEB)

    Chapman, Teresa; Done, Stephen [Seattle Children' s Hospital, Department of Radiology, Seattle, WA (United States); Sugar, Naomi; Feldman, Kenneth [Seattle Children' s Hospital, Children' s Protection Program, Seattle, WA (United States); Marasigan, Joanne; Wambold, Nicolle [University of Washington, College of Arts and Sciences, Seattle, WA (United States)

    2010-07-15

    Rickets affects young infants and toddlers. However, there is a paucity of literature regarding the types of fractures that occur in rachitic patients. To evaluate the age of patients at which radiographically evident rickets occurs, and to characterize the age incidence and fractures that are observed in infants and toddlers with radiographically evident rickets. A retrospective study of children younger than 24 months was performed. Clinical data and radiographs were reviewed. Radiographs obtained within 1 month of the diagnosis were evaluated for the presence or absence of osteopenia, presence or absence of fraying-cupping, and presence and characterization of fractures. After exclusion criteria were applied, 45 children were included in the study. Children with rickets evident by radiograph were in the age range of 2-24 months. Fractures were present in 17.5% of the study group, exclusively in mobile infants and toddlers. Fracture types included transverse long bone fractures, anterior and anterior-lateral rib fractures, and metaphyseal fractures. All fractures occurred exclusively in patients with severe, overtly evident rickets. Fractures occur in older infants and toddlers with overt rickets and can be seen by radiograph. Fractures do not resemble high-risk non-accidental trauma fractures. (orig.)

  7. The Functional Potential of Microbial Communities in Hydraulic Fracturing Source Water and Produced Water from Natural Gas Extraction Characterized by Metagenomic Sequencing

    OpenAIRE

    Arvind Murali Mohan; Bibby, Kyle J.; Daniel Lipus; Richard W Hammack; Gregory, Kelvin B.

    2014-01-01

    Microbial activity in produced water from hydraulic fracturing operations can lead to undesired environmental impacts and increase gas production costs. However, the metabolic profile of these microbial communities is not well understood. Here, for the first time, we present results from a shotgun metagenome of microbial communities in both hydraulic fracturing source water and wastewater produced by hydraulic fracturing. Taxonomic analyses showed an increase in anaerobic/facultative anaerobi...

  8. Increasing Heavy Oil Reserves in the Wilmington Oil Field Through Advanced Reservoir Characterization and Thermal Production Technologies, Class III

    Energy Technology Data Exchange (ETDEWEB)

    City of Long Beach; Tidelands Oil Production Company; University of Southern California; David K. Davies and Associates

    2002-09-30

    The objective of this project was to increase the recoverable heavy oil reserves within sections of the Wilmington Oil Field, near Long Beach, California through the testing and application of advanced reservoir characterization and thermal production technologies. It was hoped that the successful application of these technologies would result in their implementation throughout the Wilmington Field and, through technology transfer, will be extended to increase the recoverable oil reserves in other slope and basin clastic (SBC) reservoirs.

  9. Increasing Heavy Oil Reserves in the Wilmington Oil Field Through Advanced Reservoir Characterization and Thermal Production Technologies, Class III

    Energy Technology Data Exchange (ETDEWEB)

    City of Long Beach; Tidelands Oil Production Company; University of Southern California; David K. Davies and Associates

    2002-09-30

    The objective of this project was to increase the recoverable heavy oil reserves within sections of the Wilmington Oil Field, near Long Beach, California through the testing and application of advanced reservoir characterization and thermal production technologies. The successful application of these technologies would result in expanding their implementation throughout the Wilmington Field and, through technology transfer, to other slope and basin clastic (SBC) reservoirs.

  10. Locking plates in proximal humerus fractures.

    Science.gov (United States)

    Strohm, P C; Helwig, P; Konrad, G; Südkamp, N P

    2007-12-01

    It is well known that proximal humerus fractures are among the three most frequent fracture types. Epidemiological invetsigations show that in people elder than 60 years the fracture of the proximal humerus is more frequent than fractures of the hip region (17). Over the last decades several techniques have been applied for treatment of proximal humerus fractures. Widely accepted is the initiation of a conservative treatment regimen for undisplaced fractures, however, the standard treatment for displaced fractures, especially three and four part fractures, is still the center of scientific debate. Many different implants have been tested and investigated, thus demonstrating lack of sufficient results. Over the last years the development of angle stable, locking implants started and clinical studies demonstrated encouraging results. In our clinic the locking proximal humerus plate and the PHILOS plate advanced to the implant of choice for treatment of displaced proximal humerus fractures. There are still cases of implant failure and humerus head necrosis, but most of these complications were caused by the fracture type and not an implant specific problem. However the overall results with these new implants are encouraging. Key words: locking plates, proximal humerus fracture, humerus, humerus fracture, PHILOS, PHP.

  11. Developing Advanced Seismic Imaging Methods For Characterizing the Fault Zone Structure

    Science.gov (United States)

    Zhang, Haijiang

    2015-04-01

    Here I present a series of recent developments on seismic imaging of fault zone structure. The goals of these advanced methods are to better determine the physical properties (including seismic velocity, attenuation, and anisotropy) around the fault zone and its boundaries. In order to accurately determine the seismic velocity structure of the fault zone, we have recently developed a wavelet-based double-difference seismic tomography method, in which the wavelet coefficients of the velocity model, rather than the model itself, are solved using both the absolute and differential arrival times. This method takes advantage of the multiscale nature of the velocity model and the multiscale wavelet representation property. Because of the velocity model is sparse in the wavelet domain, a sparsity constraint is applied to tomographic inversion. Compared to conventional tomography methods, the new method is both data- and model-adaptive, and thus can better resolve the fault zone structure. In addition to seismic velocity property of the fault zone, seismic anisotropy and attenuation properties are also important to characterize the fault zone structure. For this reason, we developed the seismic anisotropy tomography method to image the three-dimensional anisotropy strength model of the fault zone using shear wave splitting delay times between fast and slow shear waves. The applications to the San Andreas fault around Parkfield, California and north Anatolian fault in Turkey will be shown. To better constrain the seismic attenuation structure, we developed a new seismic attenuation tomography method using measured t* values for first arrival body waves, in which the structures of attenuation and velocity models are similar through the cross-gradient constraint. Seismic tomography can, however, only resolve the smooth variations in elastic properties in Earth's interior. To image structure at length scales smaller than what can be resolved tomographically, including

  12. Modeling 3D Fracture Network in Carbonate NFR: Contribution from an Analogue Dataset, the Cante Perdrix Quarry, Calvisson, SE France

    NARCIS (Netherlands)

    Gauthier, B.D.M.; Bisdom, K.; Bertotti, G.

    2012-01-01

    The full 3D characterization of fracture networks is a key issue in naturally fractured reservoir modeling. Fracture geometry (e.g., orientation, size, spacing), fracture scale (e.g., bed-confined fractures, fracture corridors), lateral and vertical variations, need to be defined from limited, gener

  13. Multi-isotope (carbon and chlorine) analysis for fingerprinting and site characterization at a fractured bedrock aquifer contaminated by chlorinated ethenes

    DEFF Research Database (Denmark)

    Palau, Jordi; Marchesi, Massimo; Chambon, Julie Claire Claudia;

    2014-01-01

    The use of compound specific multi-isotope approach (C and Cl) in the characterization of a chlorinated ethenes contaminated fractured aquifer allows the identification of several sources and contaminant plumes, as well as the occurrence of biodegradation and mixing processes. The study site......, showed a wide range in δ13C values from − 15.6 to − 40.5‰ for TCE and from − 18.5 to − 32.4‰ for PCE, allowing the use of isotope fingerprinting for tracing of the origin and migration of these contaminants in the aquifer. In contrast, there is no difference between the δ37Cl values for TCE...... in the contaminant sources, ranging from + 0.53 to + 0.66‰. Variations of δ37Cl and δ13C in the different contaminant plumes were used to investigate the role of biodegradation in groundwater. Moreover, the isotopic data were incorporated into a reactive transport model for determination of whether the isotope...

  14. Modelling water table drawdown and recovery during tunnel excavation in fractured rock: estimating environmental impacts and characterizing uncertainties in a heterogeneous domain

    Science.gov (United States)

    Sege, J.; Li, Y.; Chang, C. F.; Chen, J.; Chen, Z.; Rubin, Y.; Li, X.; Hehua, Z.; Wang, C.; Osorio-Murillo, C. A.

    2015-12-01

    This study will develop a numerical model to characterize the perturbation of local groundwater systems by underground tunnel construction. Tunnels and other underground spaces act as conduits that remove water from the surrounding aquifer, and may lead to drawdown of the water table. Significant declines in water table elevation can cause environmental impacts by altering root zone soil moisture and changing inflows to surface waters. Currently, it is common to use analytical solutions to estimate groundwater fluxes through tunnel walls. However, these solutions often neglect spatial and temporal heterogeneity in aquifer parameters and system stresses. Some heterogeneous parameters, such as fracture densities, can significantly affect tunnel inflows. This study will focus on numerical approaches that incorporate heterogeneity across a range of scales. Time-dependent simulations will be undertaken to compute drawdown at various stages of excavation, and to model water table recovery after low-conductivity liners are applied to the tunnel walls. This approach will assist planners in anticipating environmental impacts to local surface waters and vegetation, and in computing the amount of tunnel inflow reduction required to meet environmental targets. The authors will also focus on managing uncertainty in model parameters. For greater planning applicability, extremes of a priori parameter ranges will be explored in order to anticipate best- and worst-case scenarios. For calibration and verification purposes, the model will be applied to a completed tunnel project in Mount Mingtang, China, where tunnel inflows were recorded throughout the construction process.

  15. Galeazzi fracture.

    Science.gov (United States)

    Atesok, Kivanc I; Jupiter, Jesse B; Weiss, Arnold-Peter C

    2011-10-01

    Galeazzi fracture is a fracture of the radial diaphysis with disruption at the distal radioulnar joint (DRUJ). Typically, the mechanism of injury is forceful axial loading and torsion of the forearm. Diagnosis is established on radiographic evaluation. Underdiagnosis is common because disruption of the ligamentous restraints of the DRUJ may be overlooked. Nonsurgical management with anatomic reduction and immobilization in a long-arm cast has been successful in children. In adults, nonsurgical treatment typically fails because of deforming forces acting on the distal radius and DRUJ. Open reduction and internal fixation is the preferred surgical option. Anatomic reduction and rigid fixation should be followed by intraoperative assessment of the DRUJ. Further intraoperative interventions are based on the reducibility and postreduction stability of the DRUJ. Misdiagnosis or inadequate management of Galeazzi fracture may result in disabling complications, such as DRUJ instability, malunion, limited forearm range of motion, chronic wrist pain, and osteoarthritis.

  16. Capillary fracture of soft gels

    OpenAIRE

    Bostwick, Joshua B.; Daniels, Karen E.

    2013-01-01

    A liquid droplet resting on a soft gel substrate can deform that substrate to the point of material failure, whereby fractures develop on the gel surface that propagate outwards from the contact-line in a starburst pattern. In this paper, we characterize i) the initiation process in which the number of arms in the starburst is controlled by the ratio of surface tension contrast to the gel's elastic modulus and ii) the propagation dynamics showing that once fractures are initiated they propaga...

  17. [Recent progress in orthopaedic managements of osteoporosis-related fractures].

    Science.gov (United States)

    Yamamoto, Seizo

    2011-07-01

    Recent progress in orthopaedic treatment of osteoporosis-related fractures was reviewed. In the treatment of femoral neck fractures, impacted or nondisplaced type is treated by three cannulated cancellous pins. Displaced type of femoral neck fracture is treated by bipolar prosthesis. Results of femoral neck fractures are influenced by the complications of each patients. Osteoporotic spine fractures are commonly healed within 2 or 3 months. Spinal compression with paraparesis or paraplegia is unusual complication in burst type of spine fractures. Surgical decompression, bone grafting and stabilization with instrumentation can result in some correction of deformity and neurogenic recovery. Distal radius fractures are common fractures in the eldery. Recently advances includes external fixation and plate fixation for the comminuted fractures in the distal radius. Treatments of osteoporosis-related fractures are still difficult problems to be resolved. PMID:21774371

  18. Fracture Blisters

    Directory of Open Access Journals (Sweden)

    Uebbing, Claire M

    2011-02-01

    Full Text Available Fracture blisters are a relatively uncommon complication of fractures in locations of the body, such as the ankle, wrist elbow and foot, where skin adheres tightly to bone with little subcutaneous fat cushioning. The blister that results resembles that of a second degree burn.These blisters significantly alter treatment, making it difficult to splint or cast and often overlying ideal surgical incision sites. Review of the literature reveals no consensus on management; however, most authors agree on early treatment prior to blister formation or delay until blister resolution before attempting surgical correction or stabilization. [West J Emerg Med. 2011;12(1;131-133.

  19. Fracture of brittle solids

    CERN Document Server

    Lawn, Brian

    1993-01-01

    This is an advanced text for higher degree materials science students and researchers concerned with the strength of highly brittle covalent-ionic solids, principally ceramics. It is a reconstructed and greatly expanded edition of a book first published in 1975. The book presents a unified continuum, microstructural and atomistic treatment of modern day fracture mechanics from a materials perspective. Particular attention is directed to the basic elements of bonding and microstructure that govern the intrinsic toughness of ceramics. These elements hold the key to the future of ceramics as high-technology materials--to make brittle solids strong, we must first understand what makes them weak. The underlying theme of the book is the fundamental Griffith energy-balance concept of crack propagation. The early chapters develop fracture mechanics from the traditional continuum perspective, with attention to linear and nonlinear crack-tip fields, equilibrium and non-equilibrium crack states. It then describes the at...

  20. Multi-Site Application of the Geomechanical Approach for Natural Fracture Exploration

    Energy Technology Data Exchange (ETDEWEB)

    R. L. Billingsley; V. Kuuskraa

    2006-03-31

    In order to predict the nature and distribution of natural fracturing, Advanced Resources Inc. (ARI) incorporated concepts of rock mechanics, geologic history, and local geology into a geomechanical approach for natural fracture prediction within mildly deformed, tight (low-permeability) gas reservoirs. Under the auspices of this project, ARI utilized and refined this approach in tight gas reservoir characterization and exploratory activities in three basins: the Piceance, Wind River and the Anadarko. The primary focus of this report is the knowledge gained on natural fractural prediction along with practical applications for enhancing gas recovery and commerciality. Of importance to tight formation gas production are two broad categories of natural fractures: (1) shear related natural fractures and (2) extensional (opening mode) natural fractures. While arising from different origins this natural fracture type differentiation based on morphology is sometimes inter related. Predicting fracture distribution successfully is largely a function of collecting and understanding the available relevant data in conjunction with a methodology appropriate to the fracture origin. Initially ARI envisioned the geomechanical approach to natural fracture prediction as the use of elastic rock mechanics methods to project the nature and distribution of natural fracturing within mildly deformed, tight (low permeability) gas reservoirs. Technical issues and inconsistencies during the project prompted re-evaluation of these initial assumptions. ARI's philosophy for the geomechanical tools was one of heuristic development through field site testing and iterative enhancements to make it a better tool. The technology and underlying concepts were refined considerably during the course of the project. As with any new tool, there was a substantial learning curve. Through a heuristic approach, addressing these discoveries with additional software and concepts resulted in a stronger set

  1. Melt fracture revisited

    Energy Technology Data Exchange (ETDEWEB)

    Greenberg, J. M.

    2003-07-16

    In a previous paper the author and Demay advanced a model to explain the melt fracture instability observed when molten linear polymer melts are extruded in a capillary rheometer operating under the controlled condition that the inlet flow rate was held constant. The model postulated that the melts were a slightly compressible viscous fluid and allowed for slipping of the melt at the wall. The novel feature of that model was the use of an empirical switch law which governed the amount of wall slip. The model successfully accounted for the oscillatory behavior of the exit flow rate, typically referred to as the melt fracture instability, but did not simultaneously yield the fine scale spatial oscillations in the melt typically referred to as shark skin. In this note a new model is advanced which simultaneously explains the melt fracture instability and shark skin phenomena. The model postulates that the polymer is a slightly compressible linearly viscous fluid but assumes no slip boundary conditions at the capillary wall. In simple shear the shear stress {tau}and strain rate d are assumed to be related by d = F{tau} where F ranges between F{sub 2} and F{sub 1} > F{sub 2}. A strain rate dependent yield function is introduced and this function governs whether F evolves towards F{sub 2} or F{sub 1}. This model accounts for the empirical observation that at high shears polymers align and slide more easily than at low shears and explains both the melt fracture and shark skin phenomena.

  2. Fracture source

    Directory of Open Access Journals (Sweden)

    2003-07-01

    Full Text Available The fracture properties of many different types of fibers are covered in a timely new book that will prove to be a tremendous source of information and references for researchers in the wide and diverse field of fibers and composites, says Bill Clegg.

  3. Heterogeneous reactive transport under unsaturated transient conditions characterized by 3D electrical resistivity tomography and advanced lysimeter methods

    Science.gov (United States)

    Wehrer, Markus; Slater, Lee

    2015-04-01

    Our ability to predict flow and transport processes in the unsaturated critical zone is considerably limited by two characteristics: heterogeneity of flow and transience of boundary conditions. The causes of heterogeneous flow and transport are fairly well understood, yet the characterization and quantification of such processes in natural profiles remains challenging. This is due to current methods of observation, such as staining and isotope tracers, being unable to observe multiple events on the same profile and offering limited spatial information. In our study we demonstrate an approach to characterize preferential flow and transport processes applying a combination of geoelectrical methods and advanced lysimeter techniques. On an agricultural soil profile, which was transferred undisturbed into a lysimeter container, we systematically applied a variety of input flow boundary conditions, resembling natural precipitation events. We measured breakthroughs of a conservative tracer and of nitrate, originating from the application of a slow release fertilizer and serving as a reactive tracer. Flow and transport in the soil column were observed using electrical resistivity tomography (ERT), tensiometers, water content probes and a multicompartment suction plate (MSP). These techniques allowed a direct validation of water content dynamics and tracer breakthrough under transient boundary conditions characterized noninvasively by ERT. We were able to image the advancing infiltration front and the advancing front of tracer and nitrate using time lapse ERT. Water content changes associated with the advancing infiltration front dominated over pore fluid conductivity changes during short term precipitation events. Conversely, long-term displacement of the solute fronts was monitored during periods of constant water content in between infiltration events. We observed preferential flow phenomena through ERT and through the MSP, which agreed in general terms. The preferential

  4. Mesoscale Characterization of Coupled Hydromechanical Behavior of a Fractured Porous Slope in Response to Free Water-Surface Movement

    Energy Technology Data Exchange (ETDEWEB)

    Rutqvist, Jonny; Guglielmi, Y.; Cappa, F.; Rutqvist, J.; Tsang, C.-F.; Thoraval, A.

    2008-05-15

    the high-permeability zones. The periodicity and magnitude of free water-surface movements cause 10 to 20% variations in those local stress/strain accumulations related to the contrasting HM behavior for high and low-permeable elements of the slope. Finally, surface-tilt monitoring coupled with internal localized pressure/deformation measurements appears to be a promising method for characterizing the HM properties and behavior of a slope, and for detecting its progressive destabilization.

  5. INCREASING HEAVY OIL RESERVES IN THE WILMINGTON OIL FIELD THROUGH ADVANCED RESERVOIR CHARACTERIZATION AND THERMAL PRODUCTION TECHNOLOGIES

    Energy Technology Data Exchange (ETDEWEB)

    Scott Hara

    2001-06-27

    The objective of this project is to increase the recoverable heavy oil reserves within sections of the Wilmington Oil Field, near Long Beach, California through the testing and application of advanced reservoir characterization and thermal production technologies. The successful application of these technologies will result in expanding their implementation throughout the Wilmington Field and, through technology transfer, to other slope and basin clastic (SBC) reservoirs. The existing steamflood in the Tar zone of Fault Block II-A (Tar II-A) has been relatively inefficient because of several producibility problems which are common in SBC reservoirs: inadequate characterization of the heterogeneous turbidite sands, high permeability thief zones, low gravity oil and non-uniform distribution of the remaining oil. This has resulted in poor sweep efficiency, high steam-oil ratios, and early steam breakthrough. Operational problems related to steam breakthrough, high reservoir pressure, and unconsolidated sands have caused premature well and downhole equipment failures. In aggregate, these reservoir and operational constraints have resulted in increased operating costs and decreased recoverable reserves. A suite of advanced reservoir characterization and thermal production technologies are being applied during the project to improve oil recovery and reduce operating costs.

  6. Microwave dynamic large signal waveform characterization of advanced InGaP HBT for power amplifiers

    Energy Technology Data Exchange (ETDEWEB)

    Zhao Lixin; Jin Zhi; Liu Xinyu, E-mail: zhaolixin@ime.ac.c [Institute of Microelectronics, Chinese Academy of Sciences, Beijing 100029 (China)

    2009-12-15

    In wireless mobile communications and wireless local area networks (WLAN), advanced InGaP HBT with power amplifiers are key components. In this paper, the microwave large signal dynamic waveform characteristics of an advanced InGaP HBT are investigated experimentally for 5.8 GHz power amplifier applications. The microwave large signal waveform distortions at various input power levels, especially at large signal level, are investigated and the reasons are analyzed. The output power saturation is also explained. These analyses will be useful for power amplifier designs. (semiconductor devices)

  7. Microwave dynamic large signal waveform characterization of advanced InGaP HBT for power amplifiers

    Institute of Scientific and Technical Information of China (English)

    Zhao Lixin; Jin Zhi; Liu Xinyu

    2009-01-01

    In wireless mobile communications and wireless local area networks (WLAN), advanced lnGaP HBT with power amplifiers are key components. In this paper, the microwave large signal dynamic waveform characteristics of an advanced InGaP HBT are investigated experimentally for 5.8 GHz power amplifier applications. The microwave large signal waveform distortions at various input power levels, especially at large signal level, are investigated and the reasons are analyzed. The output power saturation is also explained. These analyses will be useful for power amplifier designs.

  8. Application of Reservoir Characterization and Advanced Technology to Improve Recovery and Economics in a Lower Quality Shallow Shelf Carbonate Reservoir, Class II

    Energy Technology Data Exchange (ETDEWEB)

    Hickman, T. Scott; Justice, James J.; Egg, Rebecca

    2001-08-07

    The Oxy operated Class 2 Project at West Welch Project is designed to demonstrate how the use of advanced technology can improve the economics of miscible CO2 injection projects in lower quality Shallow Shelf Carbonate reservoirs. The research and design phase (Budget Period 1) primarily involved advanced reservoir demonstration characterization. The current demonstration phase (Budget Period 2) is the implementation of the reservoir management plan for an optimum miscible CO2 flood design based on the reservoir characterization.

  9. A Comprehensive Microfluidics Device Construction and Characterization Module for the Advanced Undergraduate Analytical Chemistry Laboratory

    Science.gov (United States)

    Piunno, Paul A. E.; Zetina, Adrian; Chu, Norman; Tavares, Anthony J.; Noor, M. Omair; Petryayeva, Eleonora; Uddayasankar, Uvaraj; Veglio, Andrew

    2014-01-01

    An advanced analytical chemistry undergraduate laboratory module on microfluidics that spans 4 weeks (4 h per week) is presented. The laboratory module focuses on comprehensive experiential learning of microfluidic device fabrication and the core characteristics of microfluidic devices as they pertain to fluid flow and the manipulation of samples.…

  10. An Empirical Grounded Theory Approach to Characterizing Advanced Mathematical Thinking in College Calculus

    Science.gov (United States)

    Nabb, Keith A.

    2013-01-01

    The research literature has made calls for greater coherence and consistency with regard to the meaning and use of the term advanced mathematical thinking (AMT) in mathematics education (Artigue, Batanero, & Kent, 2007; Selden & Selden, 2005). Educators and researchers agree that students should be engaged in AMT but it is unclear…

  11. Increasing Heavy Oil Reserves in the Wilmington Oil Field Through Advanced Reservoir Characterization and Thermal Production Technologies

    Energy Technology Data Exchange (ETDEWEB)

    Scott Hara

    1998-03-03

    The project involves improving thermal recovery techniques in a slope and basin clastic (SBC) reservoir in the Wilmington field, Los Angeles Co., Calif. using advanced reservoir characterization and thermal production technologies. The existing steamflood in the Tar zone of Fault Block (FB) II-A has been relatively inefficient because of several producibility problems which are common in SBC reservoirs. Inadequate characterization of the heterogeneous turbidite sands, high permeability thief zones, low gravity oil, and nonuniform distribution of remaining oil have all contributed to poor sweep efficiency, high steam-oil ratios, and early steam breakthrough. Operational problems related to steam breakthrough, high reservoir pressure, and unconsolidated formation sands have caused premature well and downhole equipment failures. In aggregate, these reservoir and operational constraints have resulted in increased operating costs and decreased recoverable reserves. The advanced technologies to be applied include: (1) Develop three-dimensional (3-D) deterministic and stochastic geologic models. (2) Develop 3-D deterministic and stochastic thermal reservoir simulation models to aid in reservoir management and subsequent development work. (3) Develop computerized 3-D visualizations of the geologic and reservoir simulation models to aid in analysis. (4) Perform detailed study on the geochemical interactions between the steam and the formation rock and fluids. (5) Pilot steam injection and production via four new horizontal wells (2 producers and 2 injectors). (6) Hot water alternating steam (WAS) drive pilot in the existing steam drive area to improve thermal efficiency. (7) Installing a 2100 foot insulated, subsurface harbor channel crossing to supply steam to an island location. (8) Test a novel alkaline steam completion technique to control well sanding problems and fluid entry profiles. (9) Advanced reservoir management through computer-aided access to production and

  12. Increasing Heavy Oil Reserves in the Wilmington Oil Field Through Advanced Reservoir Characterization and Thermal Production Technologies

    Energy Technology Data Exchange (ETDEWEB)

    Scott Hara

    1997-08-08

    The project involves improving thermal recovery techniques in a slope and basin clastic (SBC) reservoir in the Wilmington field, Los Angeles Co., Calif. using advanced reservoir characterization and thermal production technologies. The existing steamflood in the Tar zone of Fault Block (FB) II-A has been relatively inefficient because of several producibility problems which are common in SBC reservoirs. Inadequate characterization of the heterogeneous turbidite sands, high permeability thief zones, low gravity oil, and nonuniform distribution of remaining oil have all contributed to poor sweep efficiency, high steam-oil ratios, and early steam breakthrough. Operational problems related to steam breakthrough, high reservoir pressure, and unconsolidated formation sands have caused premature well and downhole equipment failures. In aggregate, these reservoir and operational constraints have resulted in increased operating costs and decreased recoverable reserves. The advanced technologies to be applied include: (1) Develop three-dimensional (3-D) deterministic and stochastic geologic models. (2) Develop 3-D deterministic and stochastic thermal reservoir simulation models to aid in reservoir management and subsequent development work. (3) Develop computerized 3-D visualizations of the geologic and reservoir simulation models to aid in analysis. (4) Perform detailed study on the geochemical interactions between the steam and the formation rock and fluids. (5) Pilot steam injection and production via four new horizontal wells (2 producers and 2 injectors). (6) Hot water alternating steam (WAS) drive pilot in the existing steam drive area to improve thermal efficiency. (7) Installing a 2100 foot insulated, subsurface harbor channel crossing to supply steam to an island location. (8) Test a novel alkaline steam completion technique to control well sanding problems and fluid entry profiles. (9) Advanced reservoir management through computer-aided access to production and

  13. Conducting Reflective, Hands-On Research with Advanced Characterization Instruments: A High-Level Undergraduate Practical Exploring Solid-State Polymorphism

    Science.gov (United States)

    Coles, S. J.; Mapp, L. K.

    2016-01-01

    An undergraduate practical exercise has been designed to provide hands-on, instrument-based experience of advanced characterization techniques. A research experience approach is taken, centered around the concept of solid-state polymorphism, which requires a detailed knowledge of molecular and crystal structure to be gained by advanced analytical…

  14. The functional potential of microbial communities in hydraulic fracturing source water and produced water from natural gas extraction characterized by metagenomic sequencing.

    Directory of Open Access Journals (Sweden)

    Arvind Murali Mohan

    Full Text Available Microbial activity in produced water from hydraulic fracturing operations can lead to undesired environmental impacts and increase gas production costs. However, the metabolic profile of these microbial communities is not well understood. Here, for the first time, we present results from a shotgun metagenome of microbial communities in both hydraulic fracturing source water and wastewater produced by hydraulic fracturing. Taxonomic analyses showed an increase in anaerobic/facultative anaerobic classes related to Clostridia, Gammaproteobacteria, Bacteroidia and Epsilonproteobacteria in produced water as compared to predominantly aerobic Alphaproteobacteria in the fracturing source water. The metabolic profile revealed a relative increase in genes responsible for carbohydrate metabolism, respiration, sporulation and dormancy, iron acquisition and metabolism, stress response and sulfur metabolism in the produced water samples. These results suggest that microbial communities in produced water have an increased genetic ability to handle stress, which has significant implications for produced water management, such as disinfection.

  15. Intelligent fracture creation for shale gas development

    KAUST Repository

    Douglas, Craig C.

    2011-05-14

    Shale gas represents a major fraction of the proven reserves of natural gas in the United States and a collection of other countries. Higher gas prices and the need for cleaner fuels provides motivation for commercializing shale gas deposits even though the cost is substantially higher than traditional gas deposits. Recent advances in horizontal drilling and multistage hydraulic fracturing, which dramatically lower costs of developing shale gas fields, are key to renewed interest in shale gas deposits. Hydraulically induced fractures are quite complex in shale gas reservoirs. Massive, multistage, multiple cluster treatments lead to fractures that interact with existing fractures (whether natural or induced earlier). A dynamic approach to the fracturing process so that the resulting network of reservoirs is known during the drilling and fracturing process is economically enticing. The process needs to be automatic and done in faster than real-time in order to be useful to the drilling crews.

  16. Recent trends in fracture and damage mechanics

    CERN Document Server

    Zybell, Lutz

    2016-01-01

    This book covers a wide range of topics in fracture and damage mechanics. It presents historical perspectives as well as recent innovative developments, presented by peer reviewed contributions from internationally acknowledged authors.  The volume deals with the modeling of fracture and damage in smart materials, current industrial applications of fracture mechanics, and it explores advances in fracture testing methods. In addition, readers will discover trends in the field of local approach to fracture and approaches using analytical mechanics. Scholars in the fields of materials science, engineering and computational science will value this volume which is dedicated to Meinhard Kuna on the occasion of his 65th birthday in 2015. This book incorporates the proceedings of an international symposium that was organized to honor Meinhard Kuna’s contributions to the field of theoretical and applied fracture and damage mechanics.

  17. The Relationship between Mid-face Fractures and Brain Injuries

    OpenAIRE

    Khalighi Sigaroudi A.; Vadiati Saberi B.; Yousefzadeh Chabok Sh.

    2012-01-01

    Statement of Problem: Although advances in technology have led to improvements in man’s life in different aspects, statistics show that the incidence of fractures is increasing in different regions of the body. Recent studies show that midface fractures are strongly associated with patient's death. The exact relationship between different types of facial fractures and brain injuries is still controversial. Purpose: To evaluate individuals with midface fractures from different causes and deter...

  18. Combined Tibial Tubercle Avulsion Fracture and Patellar Avulsion Fracture: An Unusual Variant in an Adolescent Patient.

    Science.gov (United States)

    Stepanovich, Matthew T; Slakey, Joseph B

    2016-01-01

    Traumatic extensor dysfunction of the knee in children is a rare injury, with the majority resulting from tibial tubercle avulsion fracture or patellar sleeve fracture. We report a rare case of combined patellar avulsion fracture and tibial tubercle fracture. With open anatomic reduction, both injuries were successfully treated. While many variations of tibial tubercle fracture have been reported, the authors believe this to be the first report in the English-language literature of this particular combined injury to the knee extensor mechanism in an adolescent. Advanced imaging with computed tomography provided vital information to aid with operative planning, especially since the majority of the unossified tubercle was not seen on plain radiographs, and all fracture fragments were originally believed to be from the tibial tubercle. Computed tomography distinguished the patellar fracture from the tibial tubercle fragments, verifying preoperatively the complexity of the injury. PMID:26761925

  19. The Advancement of Public Awareness, Concerning TRU Waste Characterization, Using a Virtual Document

    Energy Technology Data Exchange (ETDEWEB)

    West, T. B.; Burns, T. P.; Estill, W. G.; Riggs, M. J.; Taggart, D. P.; Punjak, W. A.

    2002-02-28

    Building public trust and confidence through openness is a goal of the DOE Carlsbad Field Office for the Waste Isolation Pilot Plant (WIPP). The objective of the virtual document described in this paper is to give the public an overview of the waste characterization steps, an understanding of how waste characterization instrumentation works, and the type and amount of data generated from a batch of drums. The document is intended to be published on a web page and/or distributed at public meetings on CDs. Users may gain as much information as they desire regarding the transuranic (TRU) waste characterization program, starting at the highest level requirements (drivers) and progressing to more and more detail regarding how the requirements are met. Included are links to: drivers (which include laws, permits and DOE Orders); various characterization steps required for transportation and disposal under WIPP's Hazardous Waste Facility Permit; physical/chemical basis for each characterization method; types of data produced; and quality assurance process that accompanies each measurement. Examples of each type of characterization method in use across the DOE complex are included. The original skeleton of the document was constructed in a PowerPoint presentation and included descriptions of each section of the waste characterization program. This original document had a brief overview of Acceptable Knowledge, Non-Destructive Examination, Non-Destructive Assay, Small Quantity sites, and the National Certification Team. A student intern was assigned the project of converting the document to a virtual format and to discuss each subject in depth. The resulting product is a fully functional virtual document that works in a web browser and functions like a web page. All documents that were referenced, linked to, or associated, are included on the virtual document's CD. WIPP has been engaged in a variety of Hazardous Waste Facility Permit modification activities. During

  20. Evolution of a mining induced fracture network in the overburden strata of an inclined coal seam

    Institute of Scientific and Technical Information of China (English)

    Wei; Xiujun; Gao; Mingzhong; Lv; Youchang; Shi; Xiangchao; Gao; Hailian; Zhou; Hongwei

    2012-01-01

    The geological conditions of the Pingdingshan coal mining group were used to construct a physical model used to study the distribution and evolution of mining induced cracks in the overburden strata.Digital graphics technology and fractal theory are introduced to characterize the distribution and growth of the mining induced fractures in the overburden strata of an inclined coal seam.A relationship between fractal dimension of the fracture network and the pressure in the overburden strata is suggested.Mining induced fractures spread dynamically to the mining face and up into the roof as the length of advance increases.Moreover,the fractal dimension of the fracture network increases with increased mining length,in general,but decreases during a period from overburden strata separation until the main roof collapses.It is a1so shown that overburden strata pressure plays an important role in the evolution of mining induced fractures and that the fractal dimension of the fractures increases with the pressure of the overburden.

  1. Evolution of a mining induced fracture network in the overburden strata of an inclined coal seam

    Institute of Scientific and Technical Information of China (English)

    Wei Xiujun; Gao Mingzhong; Lv Youchang; Shi Xiangchao; Gao Hailian; Zhou Hongwei

    2012-01-01

    The geological conditions of the Pingdingshan coal mining group were used to construct a physical model used to study the distribution and evolution of mining induced cracks in the overburden strata.Digital graphics technology and fractal theory are introduced to characterize the distribution and growth of the mining induced fractures in the overburden strata of an inclined coal seam.A relationship between fractal dimension of the fracture network and the pressure in the overburden strata is suggested.Mining induced fractures spread dynamically to the mining face and up into the roof as the length of advance increases.Moreover,the fractal dimension of the fracture network increases with increased mining length,in general,but decreases during a period from overburden strata separation until the main roof collapses.it is also shown that overburden strata pressure plays an important role in the evolution of mining induced fractures and that the fractal dimension of the fractures increases with the pressure of the overburden.

  2. The advancement of public awareness, concerning TRU waste characterization, using a virtual document.

    Energy Technology Data Exchange (ETDEWEB)

    West, T. B. (Thomas B.); Burns, T. P. (Timothy P.); Estill, W. G. (Wesley G.); Riggs, M. J. (Matt J.); Taggart, Daniel P.; Punjak, W. A. (Wayne A.)

    2002-01-01

    Building public trust and confidence through openness is a goal of the DOE Carlsbad Field Office for the Waste Isolation Pilot Plant (WIPP). The objective of the virtual document described in this paper is to give the public an overview of the waste characterization steps, an understanding of how waste characterization instrumentation works, and the type and amount of data generated from a batch of drums. The document is intended to be published on a web page andlor distributed at public meetings on CDs. Users may gain as much information as they desire regarding the transuranic (TRU) waste characterization program, starting at the highest level requirements (drivers) and progressing to more and more detail regarding how the requirements are met. Included are links to: (1) drivers (which include laws, permits and DOE Orders) (2) various characterization steps required for transportation and disposal under WIPP's Hazardous Waste Facility Permit (3) physical/chemical basis for each characterization method (4) types of data produced (5) quality assurance process that accompanies each measurement

  3. Laboratory characterization of advanced SO/sub 2/ control by-products: Spray dryer wastes: Final report

    Energy Technology Data Exchange (ETDEWEB)

    Thompson, C.M.; Achord, R.D.; Blythe, G.M.

    1988-05-01

    This report on the solid waste characterization of spray dryer wastes is the first in a series of five advanced SO/sub 2/ control waste characterization reports resulting from Task 2 of Research Project 2708-1. Task 2, Solid Waste Characterization, involved a detailed characterization of solid waste products based on literature and property determinations. The chemical, physical, engineering, and leaching properties of spray dryer wastes will be used to support the evaluation of waste management design and operation and potential utilization in Tasks 3 and 4 of this project. Results indicate that spray dryer wastes, although varied in chemical composition, can be handled in conventional collection, transportation, and storage systems designed for fly ash. These waste management systems will require designs that are capable of handling larger volumes and masses of dry waste materials. Chemical differences between spray dryer wastes and fly ash are greater than the physical and engineering property differences. Spray dryer wastes were nonhazardous and could be disposed in landfills. Utilization of spray dryer wastes as mineral admixture in Portland cement concrete and blended cements might be limited by chemical compositional requirements specified for reuse.

  4. Multidetector Computed Tomography of Cervical Spine Fractures in Ankylosing Spondylitis

    Energy Technology Data Exchange (ETDEWEB)

    Koivikko, M.P.; Kiuru, M.J.; Koskinen, S.K. [Helsinki Univ. Central Hospital, Toeoeloe Trauma Center (Finland). Dept. of Radiology

    2004-11-01

    Purpose: To analyze multidetector computed tomography (MDCT) cervical spine findings in trauma patients with advanced ankylosing spondylitis (AS). Material and Methods: Using PACS, 2282 cervical spine MDCT examinations requested by emergency room physicians were found during a period of 3 years. Of these patients, 18 (16 M, aged 41-87, mean 57 years) had advanced AS. Primary imaging included radiography in 12 and MRI in 11 patients. Results: MDCT detected one facet joint subluxation and 31 fractures in 17 patients: 14 transverse fractures, 8 spinous process fractures, 2 Jefferson's fractures, 1 type I and 2 type II odontoid process fractures, and 1 each: atlanto-occipital joint fracture and C2 laminar fracture plus isolated transverse process and facet joint fractures. Radiographs detected 48% and MRI 60% of the fractures. MRI detected all transverse and odontoid fractures, demonstrating spinal cord abnormalities in 72%. Conclusion: MDCT is superior to plain radiographs or MRI, showing significantly more injuries and yielding more information on fracture morphology. MRI is valuable, however, in evaluating the spinal cord and soft-tissue injuries. Fractures in advanced AS often show an abnormal orientation and are frequently associated with spinal cord injuries. In these patients, for any suspected cervical spine injuries, MDCT is therefore the imaging modality of choice.

  5. NATO Advanced Study Institute on Scanning Probe Microscopy : Characterization, Nanofabrication and Device Application of Functional Materials

    CERN Document Server

    Vilarinho, Paula Maria; Kingon, Angus; Scanning Probe Microscopy : Characterization, Nanofabrication and Device Application of Functional Materials

    2005-01-01

    As the characteristic dimensions of electronic devices continue to shrink, the ability to characterize their electronic properties at the nanometer scale has come to be of outstanding importance. In this sense, Scanning Probe Microscopy (SPM) is becoming an indispensable tool, playing a key role in nanoscience and nanotechnology. SPM is opening new opportunities to measure semiconductor electronic properties with unprecedented spatial resolution. SPM is being successfully applied for nanoscale characterization of ferroelectric thin films. In the area of functional molecular materials it is being used as a probe to contact molecular structures in order to characterize their electrical properties, as a manipulator to assemble nanoparticles and nanotubes into simple devices, and as a tool to pattern molecular nanostructures. This book provides in-depth information on new and emerging applications of SPM to the field of materials science, namely in the areas of characterisation, device application and nanofabrica...

  6. Light Water Reactor Sustainability Program Risk Informed Safety Margin Characterization (RISMC) Advanced Test Reactor Demonstration Case Study

    Energy Technology Data Exchange (ETDEWEB)

    Curtis Smith; David Schwieder; Cherie Phelan; Anh Bui; Paul Bayless

    2012-08-01

    Safety is central to the design, licensing, operation, and economics of Nuclear Power Plants (NPPs). Consequently, the ability to better characterize and quantify safety margin holds the key to improved decision making about LWR design, operation, and plant life extension. A systematic approach to characterization of safety margins and the subsequent margins management options represents a vital input to the licensee and regulatory analysis and decision making that will be involved. The purpose of the RISMC Pathway R&D is to support plant decisions for risk-informed margins management with the aim to improve economics, reliability, and sustain safety of current NPPs. Goals of the RISMC Pathway are twofold: (1) Develop and demonstrate a risk-assessment method coupled to safety margin quantification that can be used by NPP decision makers as part of their margin recovery strategies. (2) Create an advanced “RISMC toolkit” that enables more accurate representation of NPP safety margin. This report describes the RISMC methodology demonstration where the Advanced Test Reactor (ATR) was used as a test-bed for purposes of determining safety margins. As part of the demonstration, we describe how both the thermal-hydraulics and probabilistic safety calculations are integrated and used to quantify margin management strategies.

  7. GeLCMS for in-depth protein characterization and advanced analysis of proteomes

    DEFF Research Database (Denmark)

    Lundby, Alicia; Olsen, Jesper V

    2011-01-01

    In recent years the array of mass spectrometry (MS) applications to address questions in molecular and cellular biology has greatly expanded and continues to grow. Modern mass spectrometers allow for identification, characterization, as well as quantification of protein compositions and their mod...

  8. INCREASING HEAVY OIL RESERVES IN THE WILMINGTON OIL FIELD THROUGH ADVANCED RESERVOIR CHARACTERIZATION AND THERMAL PRODUCTION TECHNOLOGIES

    Energy Technology Data Exchange (ETDEWEB)

    Unknown

    2001-08-08

    The objective of this project is to increase the recoverable heavy oil reserves within sections of the Wilmington Oil Field, near Long Beach, California, through the testing and application of advanced reservoir characterization and thermal production technologies. The hope is that successful application of these technologies will result in their implementation throughout the Wilmington Field and, through technology transfer, will be extended to increase the recoverable oil reserves in other slope and basin clastic (SBC) reservoirs. The existing steamflood in the Tar zone of Fault Block II-A (Tar II-A) has been relatively inefficient because of several producibility problems which are common in SBC reservoirs: inadequate characterization of the heterogeneous turbidite sands, high permeability thief zones, low gravity oil and non-uniform distribution of the remaining oil. This has resulted in poor sweep efficiency, high steam-oil ratios, and early steam breakthrough. Operational problems related to steam breakthrough, high reservoir pressure, and unconsolidated sands have caused premature well and downhole equipment failures. In aggregate, these reservoir and operational constraints have resulted in increased operating costs and decreased recoverable reserves. A suite of advanced reservoir characterization and thermal production technologies are being applied during the project to improve oil recovery and reduce operating costs, including: (1) Development of three-dimensional (3-D) deterministic and stochastic reservoir simulation models--thermal or otherwise--to aid in reservoir management of the steamflood and post-steamflood phases and subsequent development work. (2) Development of computerized 3-D visualizations of the geologic and reservoir simulation models to aid reservoir surveillance and operations. (3) Perform detailed studies of the geochemical interactions between the steam and the formation rock and fluids. (4) Testing and proposed application of a

  9. Characterization of transient noise in Advanced LIGO relevant to gravitational wave signal GW150914

    CERN Document Server

    ,

    2016-01-01

    On September 14, 2015, a gravitational wave signal from a coalescing black hole binary system was observed by the Advanced LIGO detectors. This paper describes the transient noise backgrounds used to determine the significance of the event (designated GW150914) and presents the results of investigations into potential correlated or uncorrelated sources of transient noise in the detectors around the time of the event. The detectors were operating nominally at the time of GW150914. We have ruled out environmental influences and non-Gaussian instrument noise at either LIGO detector as the cause of the observed gravitational wave signal.

  10. Site characterization and validation - Final report

    International Nuclear Information System (INIS)

    The central aims of the Site Characterization and Validation (SCV) project were to develop and apply; * an advanced site characterization methodology and * a methodology to validate the models used to describe groundwater flow and transport in fractured rock. The basic experiment within the SCV project was to predict the distribution of water flow and tracer transport through a volume of rock, before and after excavation of a sub-horizontal drift, and to compare these predictions with actual field measurements. A structured approach was developed to combine site characterization data into a geological and hydrogeological conceptual model of a site. The conceptual model was based on a binary description where the rock mass was divided into 'fracture zones' and 'averagely fractured rock'. This designation into categories was based on a Fracture Zone Index (FZI) derived from principal component analysis of single borehole data. The FZI was used to identify the location of fracture zones in the boreholes and the extent of the zones between the boreholes was obtained form remote sensing data (radar and seismics). The consistency of the geometric model thus defined, and its significance to the flow system, was verified by cross-hole hydraulic testing. The conceptual model of the SCV site contained three major and four minor fractures zones which were the principal hydraulic conduits at the site. The location and extent of the fracture zones were included explicitly in the flow and transport models. Four different numerical modelling approaches were pursued within the project; one porous medium approach, two discrete fracture approaches, and an equivalent discontinuum approach. A series of tracer tests was also included in the prediction-validation exercise. (120 refs.) (au)

  11. Coupled Fracture and Flow in Shale in Hydraulic Fracturing

    Science.gov (United States)

    Carey, J. W.; Mori, H.; Viswanathan, H.

    2014-12-01

    Production of hydrocarbon from shale requires creation and maintenance of fracture permeability in an otherwise impermeable shale matrix. In this study, we use a combination of triaxial coreflood experiments and x-ray tomography characterization to investigate the fracture-permeability behavior of Utica shale at in situ reservoir conditions (25-50 oC and 35-120 bars). Initially impermeable shale core was placed between flat anvils (compression) or between split anvils (pure shear) and loaded until failure in the triaxial device. Permeability was monitored continuously during this process. Significant deformation (>1%) was required to generate a transmissive fracture system. Permeability generally peaked at the point of a distinct failure event and then dropped by a factor of 2-6 when the system returned to hydrostatic failure. Permeability was very small in compression experiments (conformed to Forscheimer's law. The coupled deformation and flow behavior of Utica shale, particularly the large deformation required to initiate flow, indicates the probable importance of activation of existing fractures in hydraulic fracturing and that these fractures can have adequate permeability for the production of hydrocarbon.

  12. Influence of fracture heterogeneity and wing length on the response of vertically fractured wells

    Energy Technology Data Exchange (ETDEWEB)

    Bennett, C.O.; Raghavan, R.; Reynolds, A.C.; Rosato, N.D.

    1983-04-01

    A finite-conductivity vertical fracture intersecting a well produced at a constant rate or at a constant pressure is considered. The pressure (or rate) response is obtained from a numerical model. Two aspects of this problem are considered: variable fracture conductivity and unequal fracture wing lengths. The first part of this paper examines the influence of fracture conductivity on the well response. In practice, the fracture conductivity is a decreasing function of distance from the wellbore. If the fracture conductivity decreases monotonically with distance from the wellbore, then at late times the variable fracture conductivity solutions behave like a constant-conductivity fracture, with conductivity equal to the arithmetic average of the conductivity. At early times the response is identical to that of a constant-conductivity fracture, corresponding to the highest conductivity of the fracture. For the variable fracture conductivity case, the bilinear flow period characterized by a one-quarter slope line may be obscured. Thus, analysis of short-time data can be difficult. The authors also consider situations where the fracture conductivity does not decrease monotonically with distance. The response for these cases is discussed in detail. The second part of the paper examines the effect of unequal wing lengths on the pressure response.

  13. Influence of fracture heterogeneity and wing length on the response of vertically fractured wells

    Energy Technology Data Exchange (ETDEWEB)

    Bennett, C.O.; Raghavan, R.; Reynolds, A.C.; Rosato, N.D.

    1983-04-01

    A finite-conductivity vertical fracture intersecting a well produced at a constant rate or at a constant pressure is considered. The pressure (or rate) response is obtained from a numerical model. Two aspects of this problem are considered: variable fracture conductivity and unequal fracture wing lengths. The first part of this paper examines the influence of fracture conductivity on the well response. In practice, the fracture conductivity is a decreasing function of distance from the wellbore. If the fracture conductivity decreases monotonically with distance from the wellbore, then at late times the variable fracture conductivity solutions behave like a constant-conductivity fracture, with conductivity equal to the arithmetic average of the conductivity. At early times the response is identical to that of a constant-conductivity fracture, corresponding to the highest conductivity of the fracture. For the variable fracture conductivity case, the bilinear flow period characterized by a one-quarter slope line may be obscured. Thus, analysis of short-time data can be difficult. The authors also consider situations where the fracture conductivity does not decrease monotonically with distance. The response for these cases is discussed in detail. The second part of the paper examines the effect of unequal wing lengths on the pressure response. The authors delineate conditions under which the effect of wing length on the response will become dominant. They discuss the influence of wing length on both early- and long-time data.

  14. Application of Reservoir Characterization and Advanced Technology to Improve Recovery and Economics in a Lower Quality Shallow Shelf Carbonate Reservoir

    Energy Technology Data Exchange (ETDEWEB)

    Rebecca Egg

    2002-09-30

    The OXY-operated Class 2 Project at West Welch is designed to demonstrate how the use of advanced technology can improve the economics of miscible CO{sub 2} injection projects in lower quality Shallow Shelf Carbonate reservoirs. The research and design phase (Budget Period 1) primarily involved advanced reservoir characterization. The current demonstration phase (Budget Period 2) is the implementation of the reservoir management plan for an optimum miscible CO{sub 2} flood design based on the reservoir characterization. Although Budget Period 1 for the Project officially ended 12/31/96, reservoir characterization and simulation work continued during the Budget Period 2. During the fifth and sixth annual reporting periods (8/3/98-8/2/00) covered by this report, work continued on interpretation of the cross well seismic data to create porosity and permeability profiles which were distributed into the reservoir geostatistically. The initial interwell seismic CO{sub 2} monitor survey was conducted, the acquired data processed and interpretation started. Only limited well work and facility construction was conducted in the project area. The CO{sub 2} injection initiated in October 1997 was continued, although the operator had to modify the operating plan in response to low injection rates, well performance and changes in CO{sub 2} supply. CO{sub 2} injection was focused in a smaller area to increase the reservoir processing rate. By the end of the reporting period three producers had shown sustained oil rate increases and ten wells had experienced gas (CO{sub 2}) breakthrough.

  15. Naturally fractured tight gas: Gas reservoir detection optimization. Quarterly report, January 1--March 31, 1997

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1997-12-31

    Economically viable natural gas production from the low permeability Mesaverde Formation in the Piceance Basin, Colorado requires the presence of an intense set of open natural fractures. Establishing the regional presence and specific location of such natural fractures is the highest priority exploration goal in the Piceance and other western US tight, gas-centered basins. Recently, Advanced Resources International, Inc. (ARI) completed a field program at Rulison Field, Piceance Basin, to test and demonstrate the use of advanced seismic methods to locate and characterize natural fractures. This project began with a comprehensive review of the tectonic history, state of stress and fracture genesis of the basin. A high resolution aeromagnetic survey, interpreted satellite and SLAR imagery, and 400 line miles of 2-D seismic provided the foundation for the structural interpretation. The central feature of the program was the 4.5 square mile multi-azimuth 3-D seismic P-wave survey to locate natural fracture anomalies. The interpreted seismic attributes are being tested against a control data set of 27 wells. Additional wells are currently being drilled at Rulison, on close 40 acre spacings, to establish the productivity from the seismically observed fracture anomalies. A similar regional prospecting and seismic program is being considered for another part of the basin. The preliminary results indicate that detailed mapping of fault geometries and use of azimuthally defined seismic attributes exhibit close correlation with high productivity gas wells. The performance of the ten new wells, being drilled in the seismic grid in late 1996 and early 1997, will help demonstrate the reliability of this natural fracture detection and mapping technology.

  16. Advanced robotics technology applied to mixed waste characterization, sorting and treatment

    International Nuclear Information System (INIS)

    There are over one million cubic meters of radioactively contaminated hazardous waste, known as mixed waste, stored at Department of Energy facilities. Researchers at Lawrence Livermore National Laboratory (LLNL) are developing methods to safely and efficiently treat this type of waste. LLNL has automated and demonstrated a means of segregating items in a mixed waste stream. This capability incorporates robotics and automation with advanced multi-sensor information for autonomous and teleoperational handling of mixed waste items with previously unknown characteristics. The first phase of remote waste stream handling was item singulation; the ability to remove individual items of heterogeneous waste directly from a drum, box, bin, or pile. Once objects were singulated, additional multi-sensory information was used for object classification and segregation. In addition, autonomous and teleoperational surface cleaning and decontamination of homogeneous metals has been demonstrated in processing mixed waste streams. The LLNL waste stream demonstration includes advanced technology such as object classification algorithms, identification of various metal types using active and passive gamma scans and RF signatures, and improved teleoperational and autonomous grasping of waste objects. The workcell control program used an off-line programming system as a server to perform both simulation control as well as actual hardware control of the workcell. This paper will discuss the motivation for remote mixed waste stream handling, the overall workcell layout, sensor specifications, workcell supervisory control, 3D vision based automated grasp planning and object classification algorithms

  17. Advanced robotics technology applied to mixed waste characterization, sorting and treatment

    Energy Technology Data Exchange (ETDEWEB)

    Wilhelmsen, K.; Hurd, R.; Grasz, E.

    1994-04-01

    There are over one million cubic meters of radioactively contaminated hazardous waste, known as mixed waste, stored at Department of Energy facilities. Researchers at Lawrence Livermore National Laboratory (LLNL) are developing methods to safely and efficiently treat this type of waste. LLNL has automated and demonstrated a means of segregating items in a mixed waste stream. This capability incorporates robotics and automation with advanced multi-sensor information for autonomous and teleoperational handling of mixed waste items with previously unknown characteristics. The first phase of remote waste stream handling was item singulation; the ability to remove individual items of heterogeneous waste directly from a drum, box, bin, or pile. Once objects were singulated, additional multi-sensory information was used for object classification and segregation. In addition, autonomous and teleoperational surface cleaning and decontamination of homogeneous metals has been demonstrated in processing mixed waste streams. The LLNL waste stream demonstration includes advanced technology such as object classification algorithms, identification of various metal types using active and passive gamma scans and RF signatures, and improved teleoperational and autonomous grasping of waste objects. The workcell control program used an off-line programming system as a server to perform both simulation control as well as actual hardware control of the workcell. This paper will discuss the motivation for remote mixed waste stream handling, the overall workcell layout, sensor specifications, workcell supervisory control, 3D vision based automated grasp planning and object classification algorithms.

  18. Advanced characterizations of austenitic oxide dispersion-strengthened (ODS) steels for high-temperature reactor applications

    Science.gov (United States)

    Miao, Yinbin

    Future advanced nuclear systems involve higher operation temperatures, intenser neutron flux, and more aggressive coolants, calling for structural materials with excellent performances in multiple aspects. Embedded with densely and dispersedly distributed oxide nanoparticles that are capable of not only pinning dislocations but also trapping radiation-induced defects, oxide dispersion-strengthened (ODS) steels provide excellence in mechanical strength, creep resistance, and radiation tolerance. In order to develop ODS steels with qualifications required by advanced nuclear applications, it is important to understand the fundamental mechanisms of the enhancement of ODS steels in mechanical properties. In this dissertation, a series of austenitic ODS stainless steels were investigated by coordinated state-of-the-art techniques. A series of different precipitate phases, including multiple Y-Ti-O, Y-Al-O, and Y-Ti-Hf-O complex oxides, were observed to form during mechanical alloying. Small precipitates are likely to have coherent or cubic-on-cubic orientation relationships with the matrix, allowing the dislocation to shear through. The Orowan looping mechanism is the dominant particle-dislocation interaction mode as the temperature is low, whereas the shearing mechanism and the Hirsch mechanism are also observed. Interactions between the particles and the dislocations result in the load-partitioning phenomenon. Smaller particles were found to have the stronger loading-partitioning effect. More importantly, the load-partitioning of large size particles are marginal at elevated temperatures, while the small size particles remain sustaining higher load, explaining the excellent high temperature mechanical performance of ODS steels.

  19. Etat de l'art en fracturation hydraulique State-Of-The-Art in Hydraulic Fracturing

    Directory of Open Access Journals (Sweden)

    Bouteca M.

    2006-11-01

    Full Text Available Cet article est un abrégé des connaissances de base sur la mécanique de la fracturation hydraulique (éléments de mécanique de la rupture, pression de fracturation et pression de fermeture, sur l'avancement actuel des travaux de modélisation de la propagation de fracture classés par type d'approche mécanique (bidimensionnelle, pseudotridimensionnelle, tridimensionnelle et par méthode de résolution (analytique, numérique, sur les propriétés des fluides de fracturation et des agents de soutènement. Deux chapitres à caractère plus pratique sont consacrés à la préparation et à la mise en oeuvre de la fracturation hydraulique ainsi qu'à l'évaluation des résultats de la fracturation hydraulique en termes de perméabilité, dimensions et direction de fracture. This article is an abridged review of basic knowledge about the mechanics of hydraulic fracturing (fracture mechanics, fracturing pressure and closure pressure, about recent advances in the modeling of fracture propagation classified by type of mechanical approach (two-dimensional, pseudo-three-dimensional, three-dimensional and by method of solution (analytic, numeric, and about the properties of fracturing fluids and propping agents. Two chapters having a more practical nature are devoted to the preparation and implementation of hydraulic fracturing as well as to the evaluation of hydraulic-fracturing results in terms of permeability and fracture sizes and direction.

  20. Advanced robotics handling and controls applied to Mixed Waste characterization, segregation and treatment

    International Nuclear Information System (INIS)

    At Lawrence Livermore National Laboratory under the Mixed Waste Operations program of the Department of Energy Robotic Technology Development Program (RTDP), a key emphasis is developing a total solution to the problem of characterizing, handling and treating complex and potentially unknown mixed waste objects. LLNL has been successful at looking at the problem from a system perspective and addressing some of the key issues including non-destructive evaluation of the waste stream prior to the materials entering the handling workcell, the level of automated material handling required for effective processing of the waste stream objects (both autonomous and tele-operational), and the required intelligent robotic control to carry out the characterization, segregation, and waste treating processes. These technologies were integrated and demonstrated in a prototypical surface decontamination workcell this past year

  1. Advanced in situ multi-scale characterization of hardness of carbon-fiber-reinforced plastic

    Science.gov (United States)

    Wang, Hongxin; Masuda, Hideki; Kitazawa, Hideaki; Onishi, Keiko; Kawai, Masamichi; Fujita, Daisuke

    2016-10-01

    In situ multi-scale characterization of hardness of carbon-fiber-reinforced plastic (CFRP) is demonstrated by a traditional hardness tester, instrumented indentation tester and atomic-force-microscope (AFM)-based nanoindentation. In particular, due to the large residual indentation and nonuniform distribution of the microscale carbon fibers, the Vickers hardness could not be calculated by the traditional hardness tester. In addition, the clear residual microindentation could not be formed on the CFRP by instrumented indentation tester because of the large tip half angle of the Berkovich indenter. Therefore, an efficient technique for characterizing the true nanoscale hardness of CFRP was proposed and evaluated. The local hardness of the carbon fibers or plastic matrix on the nanoscale did not vary with nanoindentation location. The Vickers hardnesses of the carbon fiber and plastic matrix determined by AFM-based nanoindentation were 340 ± 30 and 40 ± 2 kgf/mm2, respectively.

  2. RESIDUES FROM COAL CONVERSION AND UTILIZATION: ADVANCED MINERALOGICAL CHARACTERIZATION AND DISPOSED BYPRODUCT DIAGENESIS

    Energy Technology Data Exchange (ETDEWEB)

    Gregory J. McCarthy; Dean G. Grier

    1998-09-01

    The goals of the project are two-fold: (1) to upgrade semi-quantitative X-ray diffraction (QXRD) methods presently used in analyzing complex coal combustion by-product (CCB) systems, with the quantitative Rietveld method, and (2) to apply this method to a set of by-product materials that have been disposed or utilized for a long period (5 years or more) in contact with the natural environment, to further study the nature of CCB diagenesis. The project is organized into three tasks to accomplish these two goals: (1) thorough characterization of a set of previously analyzed disposed by-product materials, (2) development of a set of CCB-specific protocols for Rietveld QXRD, and (3) characterization of an additional set of disposed CCB materials, including application of the protocols for Rietveld QXRD developed in Task 2.

  3. RESIDUES FROM COAL CONVERSION AND UTILIZATION: ADVANCED MINERALOGICAL CHARACTERIZATION AND DISPOSED BYPRODUCT DIAGENESIS

    Energy Technology Data Exchange (ETDEWEB)

    Gregory J. McCarthy; Dean G. Grier

    1998-03-01

    The goals of the project are two-fold: (1) to upgrade semi-quantitative X-ray diffraction (QXRD) methods presently used in analyzing complex coal combustion by-product (CCB) systems, with the quantitative Rietveld method, and (2) to apply this method to a set of by-product materials that have been disposed or utilized for a long period (5 years or more) in contact with the natural environment, to further study the nature of CCB diagenesis. The project is organized into three tasks to accomplish these two goals: (1) thorough characterization of a set of previously analyzed disposed by-product materials, (2) development of a set of CCB-specific protocols for Rietveld QXRD, and (3) characterization of an additional set of disposed CCB materials, including application of the protocols for Rietveld QXRD developed in Task 2.

  4. Turbine blade wear and damage. An overview of advanced characterization techniques

    Energy Technology Data Exchange (ETDEWEB)

    Schlobohm, Jochen; Li, Yinan; Kaestner, Markus; Poesch, Andreas; Reithmeier, Eduard [Hannover Univ. (Germany). Inst. fuer Mess- und Regelungstechnik; Bruchwald, Oliver; Frackowiak, Wojciech; Reimche, Wilfried; Maier, Hans Juergen [Hannover Univ. (Germany). Inst. fuer Werkstoffkunde

    2016-07-01

    This paper gives an overview of four measurement techniques that allow to extensively characterize the status of a worn turbine blade. In addition to the measurement of geometry and surface properties, the condition of the two protective coatings needs to be monitored. Fringe projection was used to detect and quantify geometric variances. The technique was improved using newly developed algorithms like inverse fringe projection. A Michelson interferometer was employed to further analyze areas with geometric defects and characterize the surface morphology of the blade. Pulsed high frequency induction thermography enabled the scanning of the blade for small cracks at or close to the surface. High frequency eddy current testing was used to determine the protective layers status and their thickness.

  5. Identification and characterization of hydrologic properties of fractured tuff using hydraulic and tracer tests, test well USW H-4, Yucca Mountain, Nye County, Nevada

    International Nuclear Information System (INIS)

    Test well USW H-4, located on the eastern edge of Yucca Mountain, Nye County, Nevada, penetrates volcanic tuffs through which water moves primarily along fractures. Data, collected from hydrologic and tracer tests and an acoustic-televiewer log, were used to quantify intrawell-bore flow directions and rates, permeability distribution, fracture porosity, and orientations of the hydraulic-conductivity ellipsoid for the test well. Borehole temperature data collected during a pumping test were used to identify 33 locations at which water was entering the hole. These results correlated well with results from radioactive-tracer surveys and packer tests of isolated intervals. Iodine-131 was used as a tracer under nonpumping conditions to study flow within the borehole, and to identify fractures that produced or accepted water. Water within the borehole was moving down from above and up from below toward the interval between 2500 and 3070 feet. Inflow and outflow were detected in the two most permeable zones in the borehole; however, the nondetection of it in the other test intervals may have resulted from monitoring periods that were too short. In the uppermost permeable zone, water moved down from above 2365 feet and exited the borehole between 2365 to 2375 feet; freshwater entered the borehole between 2380 and 2385 feet and moved downward. The probable shape and orientation of the hydraulic-conductivity ellipsoid were calculated from fracture frequency and orientation data. The plane containing the two larger principal axes of the ellipsoid strikes approximately north 230 east and is nearly vertical. These two axes are approximately the same magnitude and are five to seven times larger than the smallest axis. Fracture porosity is about 10-4 to 10-3, as estimated from the cubic law for hydraulic conductivity of fractures. 13 refs., 7 figs., 4 tabs

  6. Multi scaling in fracture surfaces morphology

    International Nuclear Information System (INIS)

    Full Text:Things fall apart via the propagation of cracks whose paths leave complex patterns behind. These fracture paths were shown to exhibit remarkable scaling properties that can be described by self-affine fractal geometry. In this framework, the fracture morphology is characterized by a single roughness exponent. We show, by analyzing higher order structure functions, that in 1+1 dimensions the fracture paths are actually multi scaling graphs, ruling out a the conjecture that two dimensional fracture belongs to the universality class of directed polymers in random media. We develop a model of two dimensional quasi-static fracture, based on the method of iterated conformal mappings for stochastic growth, reproducing the essential features of experimental fracture surfaces morphology

  7. Capillary fracture of soft gels

    Science.gov (United States)

    Bostwick, Joshua B.; Daniels, Karen E.

    2013-10-01

    A liquid droplet resting on a soft gel substrate can deform that substrate to the point of material failure, whereby fractures develop on the gel surface that propagate outwards from the contact line in a starburst pattern. In this paper, we characterize (i) the initiation process, in which the number of arms in the starburst is controlled by the ratio of the surface tension contrast to the gel's elastic modulus, and (ii) the propagation dynamics showing that once fractures are initiated they propagate with a universal power law L∝t3/4. We develop a model for crack initiation by treating the gel as a linear elastic solid and computing the deformations within the substrate from the liquid-solid wetting forces. The elastic solution shows that both the location and the magnitude of the wetting forces are critical in providing a quantitative prediction for the number of fractures and, hence, an interpretation of the initiation of capillary fractures. This solution also reveals that the depth of the gel is an important factor in the fracture process, as it can help mitigate large surface tractions; this finding is confirmed with experiments. We then develop a model for crack propagation by considering the transport of an inviscid fluid into the fracture tip of an incompressible material and find that a simple energy-conservation argument can explain the observed material-independent power law. We compare predictions for both linear elastic and neo-Hookean solids, finding that the latter better explains the observed exponent.

  8. Confocal microscopy-fracture reconstruction and finite element modeling characterization of local cleavage toughness in a ferritic/martensitic steel in subsized Charpy V-notch impact tests

    International Nuclear Information System (INIS)

    The confocal microscopy (CM)-fracture reconstruction (FR) method, coupled with scanning electron microscopy (SEM) fractography, was used to measure the critical notch deformation conditions at cleavage initiation for two subsized Charpy V-notch (CVN) specimen geometries of Japan ferritic/martensitic steel (JFMS). A new method was developed to permit FR of notched specimens. Three-dimensional finite element analysis (FEA) simulations of the notch and specimen deformation were used to estimate values of critical micro-cleavage fracture stress, σ*, and critical stressed area, A*. Since σ*-A* is independent of size and geometry, it provides a fundamental local measure of cleavage toughness

  9. Experimental validation of microseismic emissions from a controlled hydraulic fracture in a synthetic layered medium

    Science.gov (United States)

    Roundtree, Russell

    A controlled hydraulic fracture experiment was performed on two medium sized (11" x 11" x 15") synthetic layered blocks of low permeability, low porosity Lyons sandstone sandwiched between cement. The purpose of the research was to better understand and characterize the fracture evolution as the fracture tip impinged upon the layer boundaries between the well bonded layers. It is also one of the first documented uses of passive microseismic used in a laboratory environment to characterize hydraulic fracturing. A relatively low viscosity fluid of 1000 centipoise, compared to properly scaled previous work (Casas 2005, and Athavale 2007), was pumped at a constant rate of 10 mL/minute through a steel cased hole landed and isolated in the sandstone layer. Efforts were made to contain the hydraulic fracture within the confines of the rock specimen to retain the created hydraulic fracture geometry. Two identical samples and treatment schedules were created and differed only in the monitoring system used to characterize the microseismic activity during the fracture treatment. The first block had eight embedded P-wave transducers placed in the sandstone layer to record the passive microseismic emissions and localize the location and time of the acoustic event. The second block had six compressional wave transducers and twelve shear wave transducers embedded in the sandstone layer of the block. The intention was to record and process the seismic data using conventional P-wave to S-wave difference timing techniques well known in industry. While this goal ultimately not possible due to the geometry of the receiver placements and the limitations of the Vallene acquisition processing software, the data received and the events localized from the 18 transducer test were of much higher numbers and quality than on the eight transducer test. This experiment proved conclusively that passive seismic emission recording can yield positive results in the laboratory. Just as in the field

  10. Oxy-Combustion Environment Characterization: Fire- and Steam-Side Corrosion in Advanced Combustion

    Energy Technology Data Exchange (ETDEWEB)

    G. R. Holcomb; J. Tylczak; G. H. Meier; B. S. Lutz; N. M. Yanar; F. S. Pettit; J. Zhu; A. Wise; D. E. Laughlin; S. Sridhar

    2012-09-25

    Oxy-fuel combustion is burning a fuel in oxygen rather than air. The low nitrogen flue gas that results is relatively easy to capture CO{sub 2} from for reuse or sequestration. Corrosion issues associated with the environment change (replacement of much of the N{sub 2} with CO{sub 2} and higher sulfur levels) from air- to oxy-firing were examined. Alloys studied included model Fe-Cr alloys and commercial ferritic steels, austenitic steels, and nickel base superalloys. The corrosion behavior is described in terms of corrosion rates, scale morphologies, and scale/ash interactions for the different environmental conditions. Additionally, the progress towards laboratory oxidation tests in advanced ultra-supercritical steam is updated.

  11. The Design and Characterization of Wideband Spline-profiled Feedhorns for Advanced Actpol

    Science.gov (United States)

    Simon, Sara M.; Austermann, Jason; Beall, James A.; Choi, Steve K.; Coughlin, Kevin P.; Duff, Shannon M.; Gallardo, Patricio A.; Henderson, Shawn W.; Hills, Felicity B.; Ho, Shuay-Pwu Patty; Hubmayr, Johannes; Josaitis, Alec; Koopman, Brian J.; McMahon, Jeff J.; Nati, Federico; Newburgh, Laura; Niemack, Michael D.; Salatino, Maria; Schillaci, Alessandro; Wollack, Edward J.

    2016-01-01

    Advanced ACTPol (AdvACT) is an upgraded camera for the Atacama Cosmology Telescope (ACT) that will measure the cosmic microwave background in temperature and polarization over a wide range of angular scales and five frequency bands from 28-230 GHz. AdvACT will employ four arrays of feedhorn-coupled, polarization- sensitive multichroic detectors. To accommodate the higher pixel packing densities necessary to achieve Ad- vACTs sensitivity goals, we have developed and optimized wideband spline-profiled feedhorns for the AdvACT multichroic arrays that maximize coupling efficiency while carefully controlling polarization systematics. We present the design, fabrication, and testing of wideband spline-profiled feedhorns for the multichroic arrays of AdvACT.

  12. Cryogenic helium gas circulation system for advanced characterization of superconducting cables and other devices

    Science.gov (United States)

    Pamidi, Sastry; Kim, Chul Han; Kim, Jae-Ho; Crook, Danny; Dale, Steinar

    2012-04-01

    A versatile cryogenic test bed, based on circulating cryogenic helium gas, has been designed, fabricated, and installed at the Florida State University Center for Advanced Power Systems (FSU-CAPS). The test bed is being used to understand the benefits of integrating the cryogenic systems of multiple superconducting power devices. The helium circulation system operates with four sets of cryocooler and heat exchanger combinations. The maximum operating pressure of the system is 2.1 MPa. The efficacy of helium circulation systems in cooling superconducting power devices is evaluated using a 30-m-long simulated superconducting cable in a flexible cryostat. Experiments were conducted at various mass flow rates and a variety of heat load profiles. A 1-D thermal model was developed to understand the effect of the gas flow parameters on the thermal gradients along the cable. Experimental results are in close agreement with the results from the thermal model.

  13. Advanced reservoir characterization in the Antelope Shale to establish the viability of CO2 enhanced oil recovery in California`s Monterey Formation siliceous shales. Annual report, February 7, 1997--February 6, 1998

    Energy Technology Data Exchange (ETDEWEB)

    Morea, M.F.

    1998-06-01

    The primary objective of this research is to conduct advanced reservoir characterization and modeling studies in the Antelope Shale reservoir. Characterization studies will be used to determine the technical feasibility of implementing a CO{sub 2} enhanced oil recovery project in the antelope Shale in Buena Vista Hills Field. The proposed pilot consists of four existing producers on 20 acre spacing with a new 10 acre infill well drilled as the pilot CO{sub 2} injector. Most of the reservoir characterization during Phase 1 of the project will be performed using data collected in the pilot pattern wells. During this period the following tasks have been completed: laboratory wettability; specific permeability; mercury porosimetry; acoustic anisotropy; rock mechanics analysis; core description; fracture analysis; digital image analysis; mineralogical analysis; hydraulic flow unit analysis; petrographic and confocal thin section analysis; oil geochemical fingerprinting; production logging; carbon/oxygen logging; complex lithologic log analysis; NMR T2 processing; dipole shear wave anisotropy logging; shear wave vertical seismic profile processing; structural mapping; and regional tectonic synthesis. Noteworthy technological successes for this reporting period include: (1) first (ever) high resolution, crosswell reflection images of SJV sediments; (2) first successful application of the TomoSeis acquisition system in siliceous shales; (3) first detailed reservoir characterization of SJV siliceous shales; (4) first mineral based saturation algorithm for SJV siliceous shales, and (5) first CO{sub 2} coreflood experiments for siliceous shale. Preliminary results from the CO{sub 2} coreflood experiments (2,500 psi) suggest that significant oil is being produced from the siliceous shale.

  14. Isolation and characterization of canine advanced preantral and early antral follicles.

    Science.gov (United States)

    Durrant, B S; Pratt, N C; Russ, K D; Bolamba, D

    1998-04-01

    This study was designed to develop preantral follicle isolation and classification protocols for the domestic dog as a model for endangered canids. Ovary donors were grouped by age, size, breed purity, ovary weight and ovary status. Ovaries were randomly assigned to 1 of 3 digestion protocols: A) digestion and follicle isolation on the day of spaying; B) storage at 4 degrees C for 18 to 24 h prior to digestion and follicle isolation; C) digestion on the day of spaying, then incubation at 4 degrees C for 18 h prior to follicle isolation. Minced tissue was placed in a collagenase/DNase solution at 37 degrees C for 1 h. Follicles were classified by oocyte size and opaqueness and by size and appearance of the granulosa cell layers. Preantral follicles contained small, pale oocytes. Preantral follicles containing grown oocytes with dense cytoplasmic lipid were designated as advanced preantral. Only advanced preantral and early antral follicles were examined and classified further. Group 1 follicles had incomplete or absent granulosa layers, Group 2 follicles had several intact granulosa layers, while Group 3 were vesicular (early antral) follicles. Misshapen or pale grown oocytes were classified as degenerated. The percentage of intact germinal vesicles (GV) was recorded for each Group. Digestion Protocol B produced the lowest percentage of degenerated follicles (P < 0.01). Prepubertal donors had fewer (P < 0.01) follicles in each Group and more (P < 0.001) degenerated follicles than older bitches. Larger ovaries yielded the highest total number of follicles (P < 0.05). Ovary status did not affect follicle yield. Oocytes from Group 1 follicles had fewer intact GVs than those from Group 2 or Group 3 (P < 0.0001). These findings provide an opportunity for quantitative studies of the factors regulating folliculogenesis in the domestic dog as a model for endangered canids. PMID:10732100

  15. Characterization and mapping of a new male sterility mutant of anther advanced dehiscence (t) in rice

    Institute of Scientific and Technical Information of China (English)

    Yi Zhang; Yunfeng Li; Jian Zhang; Fucheng Shen; Yuanxin Huang; Zhiwei Wu

    2008-01-01

    Anther dehiscence is very important for pollen maturation and release.The mutants of anther dehiscence in rice (Oryza sativa L.) arefew,and related research remains poor.A male sterility mutant of anther dehiscence in advance,add(t),has been found in Minghui 63 and its sterility is not sensitive to thermo-photo.To learn the character of sterilization and the function of the add(t) gene,the morphological and cytological studies on the anther and pollen,the ability of the pistil being fertilized,inheritance of the mutant,and mapping of add(t)gene have been conducted.The anther size is normal but the color is white in the mutant against the natural yellow in the wild-type.The pollen is malformed,unstained,and small in the KI-I2 solution.The anther dehiscence is in advance at the bicellular pollen stage.A crossing test indicated that the grain setting ratio of the add(t) is significantly lower than that of the CMS line 2085A.The ability of the pistil being fertilized is most probably decreased by the add(t) gene.The male sterility is controlled by a single recessive gene of add(t).This gene is mapped between the markers of R02004 (InDel) and RM300 (SSR) on chromosome 2,and the genetic distance from the add(t) gene to these markers is 0.78 cM and 4.66 cM,respectively.

  16. Fabrication and characterization of anisotropic nanofiber scaffolds for advanced drug delivery systems

    Directory of Open Access Journals (Sweden)

    Jalani G

    2014-05-01

    Full Text Available Ghulam Jalani,* Chan Woo Jung,* Jae Sang Lee, Dong Woo Lim Department of Bionano Engineering, College of Engineering Sciences, Hanyang University, Education Research Industry Cluster at Ansan Campus, Ansan, South Korea*These authors contributed equally to this workAbstract: Stimuli-responsive, polymer-based nanostructures with anisotropic compartments are of great interest as advanced materials because they are capable of switching their shape via environmentally-triggered conformational changes, while maintaining discrete compartments. In this study, a new class of stimuli-responsive, anisotropic nanofiber scaffolds with physically and chemically distinct compartments was prepared via electrohydrodynamic cojetting with side-by-side needle geometry. These nanofibers have a thermally responsive, physically-crosslinked compartment, and a chemically-crosslinked compartment at the nanoscale. The thermally responsive compartment is composed of physically crosslinkable poly(N-isopropylacrylamide poly(NIPAM copolymers, and poly(NIPAM-co-stearyl acrylate poly(NIPAM-co-SA, while the thermally-unresponsive compartment is composed of polyethylene glycol dimethacrylates. The two distinct compartments were physically crosslinked by the hydrophobic interaction of the stearyl chains of poly(NIPAM-co-SA or chemically stabilized via ultraviolet irradiation, and were swollen in physiologically relevant buffers due to their hydrophilic polymer networks. Bicompartmental nanofibers with the physically-crosslinked network of the poly(NIPAM-co-SA compartment showed a thermally-triggered shape change due to thermally-induced aggregation of poly(NIPAM-co-SA. Furthermore, when bovine serum albumin and dexamethasone phosphate were separately loaded into each compartment, the bicompartmental nanofibers with anisotropic actuation exhibited decoupled, controlled release profiles of both drugs in response to a temperature. A new class of multicompartmental nanofibers could be

  17. INCREASING HEAVY OIL RESERVES IN THE WILMINGTON OIL FIELD THROUGH ADVANCED RESERVOIR CHARACTERIZATION AND THERMAL PRODUCTION TECHNOLOGIES

    Energy Technology Data Exchange (ETDEWEB)

    Scott Hara

    2004-03-05

    The overall objective of this project is to increase heavy oil reserves in slope and basin clastic (SBC) reservoirs through the application of advanced reservoir characterization and thermal production technologies. The project involves improving thermal recovery techniques in the Tar Zone of Fault Blocks II-A and V (Tar II-A and Tar V) of the Wilmington Field in Los Angeles County, near Long Beach, California. A primary objective is to transfer technology which can be applied in other heavy oil formations of the Wilmington Field and other SBC reservoirs, including those under waterflood. The thermal recovery operations in the Tar II-A and Tar V have been relatively inefficient because of several producibility problems which are common in SBC reservoirs. Inadequate characterization of the heterogeneous turbidite sands, high permeability thief zones, low gravity oil, and nonuniform distribution of remaining oil have all contributed to poor sweep efficiency, high steam-oil ratios, and early steam breakthrough. Operational problems related to steam breakthrough, high reservoir pressure, and unconsolidated formation sands have caused premature well and downhole equipment failures. In aggregate, these reservoir and operational constraints have resulted in increased operating costs and decreased recoverable reserves. The advanced technologies to be applied include: (1) Develop three-dimensional (3-D) deterministic and stochastic geologic models. (2) Develop 3-D deterministic and stochastic thermal reservoir simulation models to aid in reservoir management and subsequent development work. (3) Develop computerized 3-D visualizations of the geologic and reservoir simulation models to aid in analysis. (4) Perform detailed study on the geochemical interactions between the steam and the formation rock and fluids. (5) Pilot steam injection and production via four new horizontal wells (2 producers and 2 injectors). (6) Hot water alternating steam (WAS) drive pilot in the

  18. INCREASING HEAVY OIL RESERVES IN THE WILMINGTON OIL FIELD THROUGH ADVANCED RESERVOIR CHARACTERIZATION AND THERMAL PRODUCTION TECHNOLOGIES

    Energy Technology Data Exchange (ETDEWEB)

    Scott Hara

    2003-06-04

    The overall objective of this project is to increase heavy oil reserves in slope and basin clastic (SBC) reservoirs through the application of advanced reservoir characterization and thermal production technologies. The project involves improving thermal recovery techniques in the Tar Zone of Fault Blocks II-A and V (Tar II-A and Tar V) of the Wilmington Field in Los Angeles County, near Long Beach, California. A primary objective is to transfer technology which can be applied in other heavy oil formations of the Wilmington Field and other SBC reservoirs, including those under waterflood. The thermal recovery operations in the Tar II-A and Tar V have been relatively inefficient because of several producibility problems which are common in SBC reservoirs. Inadequate characterization of the heterogeneous turbidite sands, high permeability thief zones, low gravity oil, and nonuniform distribution of remaining oil have all contributed to poor sweep efficiency, high steam-oil ratios, and early steam breakthrough. Operational problems related to steam breakthrough, high reservoir pressure, and unconsolidated formation sands have caused premature well and downhole equipment failures. In aggregate, these reservoir and operational constraints have resulted in increased operating costs and decreased recoverable reserves. The advanced technologies to be applied include: (1) Develop three-dimensional (3-D) deterministic and stochastic geologic models. (2) Develop 3-D deterministic and stochastic thermal reservoir simulation models to aid in reservoir management and subsequent development work. (3) Develop computerized 3-D visualizations of the geologic and reservoir simulation models to aid in analysis. (4) Perform detailed study on the geochemical interactions between the steam and the formation rock and fluids. (5) Pilot steam injection and production via four new horizontal wells (2 producers and 2 injectors). (6) Hot water alternating steam (WAS) drive pilot in the

  19. INCREASING HEAVY OIL RESERVES IN THE WILMINGTON OIL FIELD THROUGH ADVANCED RESERVOIR CHARACTERIZATION AND THERMAL PRODUCTION TECHNOLOGIES

    Energy Technology Data Exchange (ETDEWEB)

    Scott Hara

    2003-09-04

    The overall objective of this project is to increase heavy oil reserves in slope and basin clastic (SBC) reservoirs through the application of advanced reservoir characterization and thermal production technologies. The project involves improving thermal recovery techniques in the Tar Zone of Fault Blocks II-A and V (Tar II-A and Tar V) of the Wilmington Field in Los Angeles County, near Long Beach, California. A primary objective is to transfer technology which can be applied in other heavy oil formations of the Wilmington Field and other SBC reservoirs, including those under waterflood. The thermal recovery operations in the Tar II-A and Tar V have been relatively inefficient because of several producibility problems which are common in SBC reservoirs. Inadequate characterization of the heterogeneous turbidite sands, high permeability thief zones, low gravity oil, and nonuniform distribution of remaining oil have all contributed to poor sweep efficiency, high steam-oil ratios, and early steam breakthrough. Operational problems related to steam breakthrough, high reservoir pressure, and unconsolidated formation sands have caused premature well and downhole equipment failures. In aggregate, these reservoir and operational constraints have resulted in increased operating costs and decreased recoverable reserves. The advanced technologies to be applied include: (1) Develop three-dimensional (3-D) deterministic and stochastic geologic models. (2) Develop 3-D deterministic and stochastic thermal reservoir simulation models to aid in reservoir management and subsequent development work. (3) Develop computerized 3-D visualizations of the geologic and reservoir simulation models to aid in analysis. (4) Perform detailed study on the geochemical interactions between the steam and the formation rock and fluids. (5) Pilot steam injection and production via four new horizontal wells (2 producers and 2 injectors). (6) Hot water alternating steam (WAS) drive pilot in the

  20. Fracture Toughness Evaluation of Kori-1 RPV Beltline Weld for a Long-Term Operation

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Bong-Sang; Kim, Min-Chul; Ahn, Sang-Bok; Kim, Byung-Chul; Hong, Jun-Hwa [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2007-07-01

    Irradiation embrittlement of RPV (reactor pressure vessel) material is the most important aging issue for a long-term operation of nuclear power plants. KORI unit 1, which is the first PWR in Korea, is approaching its initial licensing life of 30 years. In order to operate the reactor for another 10 years and more, it should be demonstrated that the irradiation embrittlement of the reactor will be adequately managed by ensuring that the fracture toughness properties have a certain level of the safety margin. The current regulation requires Charpy V-notch impact data through conventional surveillance tests. It is based on the assumption that Charpy impact test results are well correlated with the fracture toughness properties of many engineering steels. However, Charpy V-notch impact data may not be adequate to estimate the fracture toughness of certain materials, such as Linde 80 welds. During the last decade, a tremendous number of fracture toughness data on many RPV steels have been produced in accordance with the new standard test method, the so-called master curve method. ASTM E1921 represents a revolutionary advance in characterizing fracture toughness of RPV steels, since it permits establishing the ductile to brittle transition portion of the fracture toughness curve with direct measurements on a relatively small number of relatively small specimens, such as pre-cracked Charpy specimens. Actual fracture toughness data from many different RPV steels revealed that the Charpy test estimations are generally conservative with the exception of a few cases. Recent regulation codes in USA permit the master curve fracture toughness methodology in evaluating an irradiation embrittlement of commercial nuclear reactor vessels.

  1. Electro-hydraulic forming of advanced high-strength steels: Deformation and microstructural characterization

    Energy Technology Data Exchange (ETDEWEB)

    Rohatgi, Aashish; Stephens, Elizabeth V.; Edwards, Danny J.; Smith, Mark T.; Davies, Richard W.

    2012-06-08

    This conference manuscript describes mechanical and microstructural characterization of steel sheets that were deformed via the electro-hydraulic forming technique. The manuscripts shows the importance of the experimental technique developed at PNNL in the sense that the deformation history information enabled by this technique is not obtainable through existing conventional approaches. Additionally, strain-rate effects on texture development during sheet-forming at high-rates are described. Thus, we have demonstrated that it is now possible to correlate deformation history with microstructural development during high-rate forming, a capability that is unique to PNNL.

  2. Fracture mechanics solution of confined water progressive intrusion height of mining fracture floor

    Institute of Scientific and Technical Information of China (English)

    Lu Haifeng; Yao Duoxi; Shen Dan; Cao Jiyang

    2015-01-01

    In order to obtain the value of confined water progressive intrusion height of mining fracture floor, the analysis equation was deduced based on the fracture extension theory of the fracture mechanics. Further-more, the influence of some parameters (e.g., advancing distance of working face, water pressure, initial fracture length and its angle) on confined water progressive intrusion height were analyzed. The results indicate that tension-shearing fracture of floor is extended more easily than compression-shearing frac-ture under the same conditions. When floor fracture dip angle is less than 90?, tension-shearing extension occurs more easily on the left edge of the goaf. If fracture dip angle is larger than 90?, it occurs more easily on the right edge of the goaf. The longer the advancing distance of working face is, the greater initial frac-ture length goes; or the larger water pressure is, the greater possibility of tension-shearing extension occurs. The confined water progressive intrusion height reaches the maximum on the edge of the goaf. Field in situ test is consistent with the theoretical analysis result.

  3. Advanced imaging as a novel approach to the characterization of membranes for microfiltration applications

    Science.gov (United States)

    Marroquin, Milagro

    The primary objectives of my dissertation were to design, develop and implement novel confocal microscopy imaging protocols for the characterization of membranes and highlight opportunities to obtain reliable and cutting-edge information of microfiltration membrane morphology and fouling processes. After a comprehensive introduction and review of confocal microscopy in membrane applications (Chapter 1), the first part of this dissertation (Chapter 2) details my work on membrane morphology characterization by confocal laser scanning microscopy (CLSM) and the implementation of my newly developed CLSM cross-sectional imaging protocol. Depth-of-penetration limits were identified to be approximately 24 microns and 7-8 microns for mixed cellulose ester and polyethersulfone membranes, respectively, making it impossible to image about 70% of the membrane bulk. The development and implementation of my cross-sectional CLSM method enabled the imaging of the entire membrane cross-section. Porosities of symmetric and asymmetric membranes with nominal pore sizes in the range 0.65-8.0 microns were quantified at different depths and yielded porosity values in the 50-60% range. It is my hope and expectation that the characterization strategy developed in this part of the work will enable future studies of different membrane materials and applications by confocal microscopy. After demonstrating how cross-sectional CLSM could be used to fully characterize membrane morphologies and porosities, I applied it to the characterization of fouling occurring in polyethersulfone microfiltration membranes during the processing of solutions containing proteins and polysaccharides (Chapter 3). Through CLSM imaging, it was determined where proteins and polysaccharides deposit throughout polymeric microfiltration membranes when a fluid containing these materials is filtered. CLSM enabled evaluation of the location and extent of fouling by individual components (protein: casein and polysaccharide

  4. CURBSIDE CONSULTATION IN FRACTURE MANAGEMENT: 49 CLINICAL QUESTIONS

    Directory of Open Access Journals (Sweden)

    Walter W. Virkus

    2008-12-01

    displaced bimalleolar fracture in insulin dependant middle aged woman; Man-agement of calcaneal fractures; Fixation technic for a displaced talar neck fracture in a patient in ER; Indica-tions for surgical treatment of metatarsal fractures; Bone grafting in acute fractures; Management of a nonunion of plated midshaft tibia fracture; Management of a child with a twisted ankle and normal x-rays; Assessment of com-partment syndrome in foot.The Section III is about “GENERAL FRACTURE CARE” including: Management of multiple orthopedic injuries and damage control orthopedics; Bone stimula-tion in nonunion; Indications for locking plates; Fractures requiring anatomic reduction.AUDIENCE: Mainly trauma fellows and practicing or-thopedists are the targeted audience of the book, but not only the basic knowledge for the orthopedic residents but also the expert advices for complicated and controversial cases pointing experienced surgeons widen the spectrum of audience. Also non-physician personnel may benefit the basic knowledge from brief answers given in a casual format.ASSESMENT: “Curbside Consultation in Fracture Man-agement:49 Clinical Questions” offering practical, brief, evidence based answers to frequently asked questions especially those have been often left controversial related with the treatment of fractures of upper and lower extrem-ity, pelvic fractures is a useful resource mainly for resi-dents, fellows and junior orthopedists. Casual format that mimics a “curbside” dialog of colleagues and also the rich illustrations by images and diagrams makes the advanced knowledge in the text easier to understand and learn. Questions are carefully chosen from a wide spectrum of subjects related to fracture management to form a unique reference including high and low energy trauma fractures, pediatric fractures, fractures in elderly, multiple orthope-dic injury, and general fracture care. Assessment of frac-tures and diagnostic approach, postoperative care and

  5. Structural characterization of the fracture systems in the porcelanites: Comparing data from the Monterey Formation in California USA and the Sap Bon Formation in Central Thailand

    Science.gov (United States)

    Kanjanapayont, Pitsanupong; Aydin, Atilla; Wongseekaew, Kanitsorn; Maneelok, Wichanee

    2016-09-01

    The fractures in the porcelanites from the Monterey Formation in California USA and the Sap Bon Formation in Central Thailand were documented for a comparative study of their modes, distribution, and their relationship to other structures such as folds and bedding planes. Both formations consist in thinly bedded stiff units that are prone to folding, flexural slip, and cross-bedding brittle fracturing under compression. There are two assemblages in the porcelanites. The first assemblage includes commonly vertical high-angle opening mode fractures, left-lateral strike-slip faults, normal faults, and thrust faults. The second one is sub-horizontal fractures which are associated with folds, bedding slip, and thrusts faults in both Monterey and Sap Bon formations. The structural architectures of these rocks and the associated groups of structures are remarkably similar in terms of both opening and shearing modes and their relationships with the bedding due to their depositional architecture and the compressional tectonic regimes, in spite of the fact that the two locations are more than ten thousand kilometers apart and have very different ages of deformation.

  6. Use of fracture filling mineral assemblages for characterizing water-rock interactions during exhumation of an accretionary complex: An example from the Shimanto Belt, southern Kyushu Japan

    Science.gov (United States)

    Ono, Takuya; Yoshida, Hidekazu; Metcalfe, Richard

    2016-06-01

    Various fracture filling minerals and secondary minerals in fracture walls were formed by fluid-rock interaction during the exhumation of the Palaeogene Shimanto Belt of Kyushu, Japan, which is located in an accretionary complex. Each mineral formed under favourable geological conditions and can be used to estimate the conditions of accretion and formation of the related rock sequences. Petrographic observations, mineralogical and geochemical analyses were made on fracture filling minerals and secondary minerals from boreholes of ca. 140 m depth, drilled in the Shimanto Belt. Results reveal that the secondary minerals were formed in three major stages distinguished by the sequential textural relationships of the minerals and the interpreted environment of mineral formation. Filling mineral assemblages show that the studied rock formation has been subducted to a depth of several km and the temperature reached was ca. 200-300 °C. After the subduction, the rock formation was uplifted and surface acidic water penetrated up to 80 m beneath the present ground surface. The acid water dissolved calcite fracture filling minerals to form the present groundwater flow-paths, which allowed recent wall rock alteration to occur. The results shown here imply that filling mineral assemblages can be an effective tool to evaluate the environmental changes during exhumation of an accretionary complex.

  7. Characterization and Suppression of the Electromagnetic Interference Induced Phase Shift in the JLab FEL Photo - Injector Advanced Drive Laser System

    Energy Technology Data Exchange (ETDEWEB)

    F. G. Wilson, D. Sexton, S. Zhang

    2011-09-01

    The drive laser for the photo-cathode gun used in the JLab Free Electron Laser (FEL) facility had been experiencing various phase shifts on the order of tens of degrees (>20{sup o} at 1497 MHz or >40ps) when changing the Advanced Drive Laser (ADL) [2][3][4] micro-pulse frequencies. These phase shifts introduced multiple complications when trying to setup the accelerator for operation, ultimately inhibiting the robustness and overall performance of the FEL. Through rigorous phase measurements and systematic characterizations, we determined that the phase shifts could be attributed to electromagnetic interference (EMI) coupling into the ADL phase control loop, and subsequently resolved the issue of phase shift to within tenths of a degree (<0.5{sup o} at 1497 MHz or <1ps). The diagnostic method developed and the knowledge gained through the entire process will prove to be invaluable for future designs of similar systems.

  8. Design and characterization of a 32-channel heterodyne radiometer for electron cyclotron emission measurements on experimental advanced superconducting tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Han, X.; Liu, X.; Liu, Y., E-mail: liuyong@ipp.ac.cn; Li, E. Z.; Hu, L. Q.; Gao, X. [Institution of Plasma Physics, Chinese Academy of Sciences, P. O. Box 1126, Hefei, Anhui 230031 (China); Domier, C. W.; Luhmann, N. C. [Department of Electrical and Computer Engineering, University of California, Davis, California 95616 (United States)

    2014-07-15

    A 32-channel heterodyne radiometer has been developed for the measurement of electron cyclotron emission (ECE) on the experimental advanced superconducting tokamak (EAST). This system collects X-mode ECE radiation spanning a frequency range of 104–168 GHz, where the frequency coverage corresponds to a full radial coverage for the case with a toroidal magnetic field of 2.3 T. The frequency range is equally spaced every 2 GHz from 105.1 to 167.1 GHz with an RF bandwidth of ∼500 MHz and the video bandwidth can be switched among 50, 100, 200, and 400 kHz. Design objectives and characterization of the system are presented in this paper. Preliminary results for plasma operation are also presented.

  9. Fractal patterns of fractures in granites

    Science.gov (United States)

    Velde, B.; Dubois, J.; Moore, D.; Touchard, G.

    1991-01-01

    Fractal measurements using the Cantor's dust method in a linear one-dimensional analysis mode were made on the fracture patterns revealed on two-dimensional, planar surfaces in four granites. This method allows one to conclude that: 1. (1)|The fracture systems seen on two-dimensional surfaces in granites are consistent with the part of fractal theory that predicts a repetition of patterns on different scales of observation, self similarity. Fractal analysis gives essentially the same values of D on the scale of kilometres, metres and centimetres (five orders of magnitude) using mapped, surface fracture patterns in a Sierra Nevada granite batholith (Mt. Abbot quadrangle, Calif.). 2. (2)|Fractures show the same fractal values at different depths in a given batholith. Mapped fractures (main stage ore veins) at three mining levels (over a 700 m depth interval) of the Boulder batholith, Butte, Mont. show the same fractal values although the fracture disposition appears to be different at different levels. 3. (3)|Different sets of fracture planes in a granite batholith, Central France, and in experimental deformation can have different fractal values. In these examples shear and tension modes have the same fractal values while compressional fractures follow a different fractal mode of failure. The composite fracture patterns are also fractal but with a different, median, fractal value compared to the individual values for the fracture plane sets. These observations indicate that the fractal method can possibly be used to distinguish fractures of different origins in a complex system. It is concluded that granites fracture in a fractal manner which can be followed at many scales. It appears that fracture planes of different origins can be characterized using linear fractal analysis. ?? 1991.

  10. Advanced x-ray spectrometric techniques for characterization of nuclear materials: An overview of recent laboratory activities

    Science.gov (United States)

    Misra, N. L.

    2014-11-01

    Advancements in x-ray spectrometric techniques at different stages have made this technique suitable for characterization of nuclear materials with respect to trace/major element determinations and compositional uniformity studies. The two important features of total reflection x-ray fluorescence spectrometry: 1) requirement of very small amount of sample in ng level 2) multielement analytical capability, in addition to other features, make this technique very much suitable to nuclear materials characterization as most of the nuclear materials are radioactive and the radioactive waste generated and radiation hazards to the operator are minimum when such low amount of sample is used. Similarly advanced features of energy dispersive x-ray fluorescence e.g. better geometry for high flux, reduction in background due to application of radiation filters have made the measurements of samples sealed inside thin alkathene/PVC covers possible with good sensitivity. This approach avoids putting the instrument inside a glove box for measuring radioactive samples and makes the operation/maintenance of the instrument and analysis of the samples possible in easy and fast manner. This approach has been used for major element determinations in mixed uranium-plutonium samples. Similarly μ-XRF with brilliant and micro-focused excitation sources can be used for compositional uniformity study of reactor fuel pellets. A μ-XRF study using synchrotron light source has been made to assess the compositional uniformity of mixed uranium-thorium oxide pellets produced by different processes. This approach is simple as it does not involve any sample preparation and is non-destructive. A brief summary of such activities carried out in our laboratory in past as well as ongoing and planned for the future have been discussed in the present manuscript.

  11. Characterization of Proxy Application Performance on Advanced Architectures. UMT2013, MCB, AMG2013

    Energy Technology Data Exchange (ETDEWEB)

    Howell, Louis H. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Gunney, Brian T. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Bhatele, Abhinav [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

    2015-10-09

    Three codes were tested at LLNL as part of a Tri-Lab effort to make detailed assessments of several proxy applications on various advanced architectures, with the eventual goal of extending these assessments to codes of programmatic interest running more realistic simulations. Teams from Sandia and Los Alamos tested proxy apps of their own. The focus in this report is on the LLNL codes UMT2013, MCB, and AMG2013. We present weak and strong MPI scaling results and studies of OpenMP efficiency on a large BG/Q system at LLNL, with comparison against similar tests on an Intel Sandy Bridge TLCC2 system. The hardware counters on BG/Q provide detailed information on many aspects of on-node performance, while information from the mpiP tool gives insight into the reasons for the differing scaling behavior on these two different architectures. Results from three more speculative tests are also included: one that exploits NVRAM as extended memory, one that studies performance under a power bound, and one that illustrates the effects of changing the torus network mapping on BG/Q.

  12. Characterization of aquatic humic substances to DBPs formation in advanced treatment processes for conventionally treated water.

    Science.gov (United States)

    Kim, Hyun-Chul; Yu, Myong-Jin

    2007-05-01

    An advanced water treatment demonstration plant consisted of ozone/granular activated carbon processes was operated to study feasibility of the processes. Natural organic matter (NOM) from raw and process waters at the demonstration plant was isolated into humic and non-humic fractions by physicochemical fractionation method to investigate characteristics of humic fraction (i.e., humic substances, HS) as a predominant haloform reactant. Ozone did not significantly oxidize the carboxylic fraction (from 39.1 to 35.9%), while GAC removed some of the carboxylic fraction (from 35.9 to 29.1%). Formation potential of trihalomethanes (THMs) as compared to haloacetic acids formation potential (HAAFP) was highly influenced by HS. Higher yields of THMs resulted from chlorination of HS with a higher phenolic content and phenolic fraction in the HS gradually decreased from 60.5% to 15.8% through the water treatment. The structural and functional changes of HS were identified by elemental, Fourier-transform infrared (FT-IR) and proton nuclear magnetic resonance ((1)H NMR) analyses, and these results were mutually consistent. The functional distribution data obtained by using A-21 resin could be used to support the interpretation of data obtained from the spectroscopic analyses. Decreases in ratio of UV absorbance at 253 nm and 203 nm (A(253)/A(203)) and DBPFPs/DOC showed consistent trends, therefore, A(253)/A(203) ratio may be a good indicator for the disinfection by-product formation potentials (DBPFPs).

  13. On Advanced Estimation Techniques for Exoplanet Detection and Characterization using Ground-Based Coronagraphs

    Science.gov (United States)

    Lawson, Peter R.; Frazin, Richard; Barrett, Harrison; Caucci, Luca; Devaney, Nicholas; Furenlid, Lars; Gladysz, Szymon; Guyon, Olivier; Krist, John; Maire, Jerome; Marois, Christian; Mawet, Dimitri; Mouillet, David; Mugnier, Laurent; Perrin, Marshall; Poyneer, Lisa; Pueyo, Laurent; Savransky, Dmitry; Soummer, Remi

    2012-01-01

    The direct imaging of planets around nearby stars is exceedingly difficult. Only about 14 exoplanets have been imaged to date that have masses less than 13 times that of Jupiter. The next generation of planet-finding coronagraphs, including VLT-SPHERE, the Gemini Planet Imager, Palomar P1640, and Subaru HiCIAO have predicted contrast performance of roughly a thousand times less than would be needed to detect Earth-like planets. In this paper we review the state of the art in exoplanet imaging, most notably the method of Locally Optimized Combination of Images (LOCI), and we investigate the potential of improving the detectability of faint exoplanets through the use of advanced statistical methods based on the concepts of the ideal observer and the Hotelling observer. We provide a formal comparison of techniques through a blind data challenge and evaluate performance using the Receiver Operating Characteristic (ROC) and Localization ROC (LROC) curves. We place particular emphasis on the understanding and modeling of realistic sources of measurement noise in ground-based AO-corrected coronagraphs. The work reported in this paper is the result of interactions between the co-authors during a week-long workshop on exoplanet imaging that was held in Squaw Valley, California, in March of 2012.

  14. Chronic Spontaneous Urticaria Is Characterized by Lower Serum Advanced Glycation End-Products

    Directory of Open Access Journals (Sweden)

    Alicja Grzanka

    2014-01-01

    Full Text Available Background. Chronic spontaneous urticaria (CSU is associated with activation of acute phase response. On the other hand, it is known that systemic inflammation may lead to increased formation of advanced glycation end-products (AGEs, associated with pathogenesis of various diseases. Aim. We aim to test whether chronic inflammation manifested by activated acute phase response may provide a mechanism for increased serum AGEs concentration in CSU. Methods. Concentrations of AGEs were measured spectrofluorimetrically in serum of CSU patients and the healthy subjects. Results. Serum AGEs and albumin concentrations in CSU patients were significantly lower as compared with the healthy subjects. Serum CRP concentration was significantly higher in patients with CSU than in the controls. Significant positive correlation was observed between AGEs and albumin concentrations in the subjects. Conclusions. CSU is not associated with increased circulating AGEs concentrations, despite the enhanced systemic inflammatory response. Paradoxical decrease of serum AGEs concentrations is probably a reflection of lower concentration of “negative acute phase proteins” such as albumin.

  15. Reactor Physics Scoping and Characterization Study on Implementation of TRIGA Fuel in the Advanced Test Reactor

    Energy Technology Data Exchange (ETDEWEB)

    Jennifer Lyons; Wade R. Marcum; Mark D. DeHart; Sean R. Morrell

    2014-01-01

    The Advanced Test Reactor (ATR), under the Reduced Enrichment for Research and Test Reactors (RERTR) Program and the Global Threat Reduction Initiative (GTRI), is conducting feasibility studies for the conversion of its fuel from a highly enriched uranium (HEU) composition to a low enriched uranium (LEU) composition. These studies have considered a wide variety of LEU plate-type fuels to replace the current HEU fuel. Continuing to investigate potential alternatives to the present HEU fuel form, this study presents a preliminary analysis of TRIGA® fuel within the current ATR fuel envelopes and compares it to the functional requirements delineated by the Naval Reactors Program, which includes: greater than 4.8E+14 fissions/s/g of 235U, a fast to thermal neutron flux ratio that is less than 5% deviation of its current value, a constant cycle power within the corner lobes, and an operational cycle length of 56 days at 120 MW. Other parameters outside those put forth by the Naval Reactors Program which are investigated herein include axial and radial power profiles, effective delayed neutron fraction, and mean neutron generation time.

  16. Recent Advances on Multi-Parameter Flow Cytometry to Characterize Antimicrobial Treatments.

    Science.gov (United States)

    Léonard, Lucie; Bouarab Chibane, Lynda; Ouled Bouhedda, Balkis; Degraeve, Pascal; Oulahal, Nadia

    2016-01-01

    The investigation on antimicrobial mechanisms is a challenging and crucial issue in the fields of food or clinical microbiology, as it constitutes a prerequisite to the development of new antimicrobial processes or compounds, as well as to anticipate phenomenon of microbial resistance. Nowadays it is accepted that a cells population exposed to a stress can cause the appearance of different cell populations and in particular sub-lethally compromised cells which could be defined as viable but non-culturable (VBNC). Recent advances on flow cytometry (FCM) and especially on multi-parameter flow cytometry (MP-FCM) provide the opportunity to obtain high-speed information at real time on damage at single-cell level. This review gathers MP-FCM methodologies based on individual and simultaneous staining of microbial cells employed to investigate their physiological state following different physical and chemical antimicrobial treatments. Special attention will be paid to recent studies exploiting the possibility to corroborate MP-FCM results with additional techniques (plate counting, microscopy, spectroscopy, molecular biology techniques, membrane modeling) in order to elucidate the antimicrobial mechanism of action of a given antimicrobial treatment or compound. The combination of MP-FCM methodologies with these additional methods is namely a promising and increasingly used approach to give further insight in differences in microbial sub-population evolutions in response to antimicrobial treatments. PMID:27551279

  17. Structural Characterization of Advanced Composite Tow-Steered Shells with Large Cutouts

    Science.gov (United States)

    Wu, K. Chauncey; Turpin, Jason D.; Gardner, Nathaniel W.; Stanford, Bret K.; Martin, Robert A.

    2015-01-01

    The structural performance of two advanced composite tow-steered shells with large cutouts, manufactured using an automated fiber placement system, is assessed using both experimental and analytical methods. The fiber orientation angles of the shells vary continuously around their circumference from +/- 10 degrees on the crown and keel, to +/- 45 degrees on the sides. The raised surface features on one shell result from application of all 24 tows during each fiber placement system pass, while the second shell uses the tow drop/add capability of the system to achieve a more uniform wall thickness. These unstiffened shells, both without and with small cutouts, were previously tested in axial compression and buckled elastically. In this study, a single unreinforced cutout, scaled to represent a cargo door on a commercial aircraft, is machined into one side of each shell. The prebuckling axial stiffnesses and bifurcation buckling loads of these shells with large cutouts are also computed using linear finite element structural analyses for preliminary comparisons with test data. During testing, large displacements are observed around the large cutouts, but the shells maintain an average of 91 percent of the axial stiffness, and also carry 85 percent of the buckling loads, when compared to the pristine shells without cutouts. These relatively small reductions indicate that there is great potential for using tow steering to mitigate the adverse effects of large cutouts on the overall structural performance.

  18. Buried explosive hazard characterization using advanced magnetic and electromagnetic induction sensors

    Science.gov (United States)

    Miller, Jonathan S.; Schultz, Gregory; Shah, Vishal

    2013-06-01

    Advanced electromagnetic induction arrays that feature high sensitivity wideband magnetic field and electromagnetic induction receivers provide significant capability enhancement to landmine, unexploded ordnance, and buried explosives detection applications. Specifically, arrays that are easily and quickly configured for integration with a variety of ground vehicles and mobile platforms offer improved safety and efficiency to personnel conducting detection operations including route clearance, explosive ordnance disposal, and humanitarian demining missions. We present experimental results for explosives detection sensor concepts that incorporate both magnetic and electromagnetic modalities. Key technology components include a multi-frequency continuous wave EMI transmitter, multi-axis induction coil receivers, and a high sensitivity chip scale atomic magnetometer. The use of multi-frequency transmitters provides excitation of metal encased threats as well as low conductivity non-metallic explosive constituents. The integration of a radio frequency tunable atomic magnetometer receiver adds increased sensitivity to lower frequency components of the electromagnetic response. This added sensitivity provides greater capability for detecting deeply buried targets. We evaluate the requirements for incorporating these sensor modalities in forward mounted ground vehicle operations. Specifically, the ability to detect target features in near real-time is critical to non-overpass modes. We consider the requirements for incorporating these sensor technologies in a system that enables detection of a broad range of explosive threats that include both metallic and non-metallic components.

  19. Reactor Physics Scoping and Characterization Study on Implementation of TRIGA Fuel in the Advanced Test Reactor

    International Nuclear Information System (INIS)

    The Advanced Test Reactor (ATR), under the Reduced Enrichment for Research and Test Reactors (RERTR) Program and the Global Threat Reduction Initiative (GTRI), is conducting feasibility studies for the conversion of its fuel from a highly enriched uranium (HEU) composition to a low enriched uranium (LEU) composition. These studies have considered a wide variety of LEU plate-type fuels to replace the current HEU fuel. Continuing to investigate potential alternatives to the present HEU fuel form, this study presents a preliminary analysis of TRIGA® fuel within the current ATR fuel envelopes and compares it to the functional requirements delineated by the Naval Reactors Program, which includes: greater than 4.8E+14 fissions/s/g of 235U, a fast to thermal neutron flux ratio that is less than 5% deviation of its current value, a constant cycle power within the corner lobes, and an operational cycle length of 56 days at 120 MW. Other parameters outside those put forth by the Naval Reactors Program which are investigated herein include axial and radial power profiles, effective delayed neutron fraction, and mean neutron generation time.

  20. Accurate Characterization of Winter Precipitation Using Multi-Angle Snowflake Camera, Visual Hull, Advanced Scattering Methods and Polarimetric Radar

    Directory of Open Access Journals (Sweden)

    Branislav M. Notaroš

    2016-06-01

    Full Text Available This article proposes and presents a novel approach to the characterization of winter precipitation and modeling of radar observables through a synergistic use of advanced optical disdrometers for microphysical and geometrical measurements of ice and snow particles (in particular, a multi-angle snowflake camera—MASC, image processing methodology, advanced method-of-moments scattering computations, and state-of-the-art polarimetric radars. The article also describes the newly built and established MASCRAD (MASC + Radar in-situ measurement site, under the umbrella of CSU-CHILL Radar, as well as the MASCRAD project and 2014/2015 winter campaign. We apply a visual hull method to reconstruct 3D shapes of ice particles based on high-resolution MASC images, and perform “particle-by-particle” scattering computations to obtain polarimetric radar observables. The article also presents and discusses selected illustrative observation data, results, and analyses for three cases with widely-differing meteorological settings that involve contrasting hydrometeor forms. Illustrative results of scattering calculations based on MASC images captured during these events, in comparison with radar data, as well as selected comparative studies of snow habits from MASC, 2D video-disdrometer, and CHILL radar data, are presented, along with the analysis of microphysical characteristics of particles. In the longer term, this work has potential to significantly improve the radar-based quantitative winter-precipitation estimation.

  1. Characterization and evaluation of fracture-cavity type carbonate reservoir in the western part of Northern Tarim uplift%塔北隆起西部缝洞型碳酸盐岩储层表征与评价

    Institute of Scientific and Technical Information of China (English)

    张军林; 田世澄; 郑多明

    2014-01-01

    Fracture-cavity type carbonatite reservoir has strong dimensional anisotropism, and hence reservoir characterization and eval-uation are very difficult. The plateau facies carbonatite fracture-cavity reservoir is stably developed in Middle Ordovician strata in west-ern W block of northern Tarim uplift. Utilizing paleo-geographic coordinate transform, logging reservoir analysis and sensibility attribu-tor analysis of the fracture-cavity type carbonatite reservoir, the authors studied the reservoir facies. Based on reservoir facies research and utilizing stochastic method, the authors built the dual porosity model for fracture-cavity reservoir, and characterized the carbonatite reservoir. Finally, in combination with AVO inversion and reservoir characterization, the carbonatite reservoir was evaluated. It is proved that the reservoir pattern in the study area is mainly of the fracture and cavity type, with fractures acting both as hydrocarbon ac-cumulation space and as the factor for the formation of cavity. AFE ( Automatic Fault Extraction) and wave classification attribution were sensitive to the fracture and cavity type reservoir. With increasing oil saturation, AVO of the reservoir became more obvious. The fluid prediction method based on pre-stack AVO inversion could reasonably forecast oil province of carbonnate reservoir.%缝洞型碳酸盐岩储层存在强烈的空间非均质性,储层表征与评价难度极大。塔北隆起西部W区块奥陶系中统顶部发育稳定的台地相碳酸盐岩缝洞型储层。应用古地理坐标转换构造建模技术、测井储层分析方法,并结合缝洞型储层地震属性进行储层相研究,以储层相分析成果为基础建立双孔隙度模型,对缝洞型储层进行定量表征,最后结合AVO流体预测,进行综合评价。研究表明:该区碳酸盐岩储层类型主要为裂缝型、裂缝孔洞型,裂缝既是储集空间又是孔洞形成的诱导因素;本征值裂缝属性

  2. Characterization of failure modes in deep UV and deep green LEDs utilizing advanced semiconductor localization techniques.

    Energy Technology Data Exchange (ETDEWEB)

    Tangyunyong, Paiboon; Miller, Mary A.; Cole, Edward Isaac, Jr.

    2012-03-01

    We present the results of a two-year early career LDRD that focused on defect localization in deep green and deep ultraviolet (UV) light-emitting diodes (LEDs). We describe the laser-based techniques (TIVA/LIVA) used to localize the defects and interpret data acquired. We also describe a defect screening method based on a quick electrical measurement to determine whether defects should be present in the LEDs. We then describe the stress conditions that caused the devices to fail and how the TIVA/LIVA techniques were used to monitor the defect signals as the devices degraded and failed. We also describe the correlation between the initial defects and final degraded or failed state of the devices. Finally we show characterization results of the devices in the failed conditions and present preliminary theories as to why the devices failed for both the InGaN (green) and AlGaN (UV) LEDs.

  3. Creep-fatigue evaluation and damage characterization for structural materials of advanced fast breeder reactor

    International Nuclear Information System (INIS)

    Creep-fatigue (Creep fatigue and fatigue) tests of Mod. 9Cr-1Mo steel have been performed by varying stress holding time at 550degC. Creep-fatigue properties are affected by stress holding, and strain rate increases with increasing stress holding time. In Vickers hardness measurements Vickers hardness of creep fatigue damaged specimen is larger than that of fatigue damaged specimen. In magnetic characterization the saturated magnetic flux density and permeability of creep fatigue damaged specimens are larger than those of fatigue damaged specimen. And in MFM observation the standard deviation value of creep fatigue damaged specimen is larger than that of fatigue damaged specimen. By TEM observation, the effect of stress holing time on these creep-fatigue properties can be explained by the difference of dislocation structures. (author)

  4. Experimental and finite element analysis of fracture criterion in general yielding fracture mechanics

    Indian Academy of Sciences (India)

    D M Kulkarni; Ravi Prakash; A N Kumar

    2002-12-01

    Efforts made over the last three decades to understand the fracture behaviour of structural materials in elastic and elasto-plastic fracture mechanics are numerous, whereas investigations related to fracture behaviour of materials in thin sheets or general yielding fracture regimes are limited in number. Engineering simulative tests are being used to characterize formability and drawability of sheet metals. However, these tests do not assure consistency in quality of sheet metal products. The prevention of failure in stressed structural components currently requires fracture mechanics based design parameters like critical load, critical crack-tip opening displacement or fracture toughness. The present attempt would aim to fulfill this gap and generate more information thereby increased understanding on fracture behaviour of sheet metals. In the present investigation, using a recently developed technique for determining fracture criteria in sheet metals, results are generated on critical CTOD and fracture toughness. Finite element analysis was performed to support the results on various fracture parameters. The differences are within 1 to 4%. At the end it is concluded that magnitude of critical CTOD and/or critical load can be used as a fracture criterion for thin sheets.

  5. On-line Optimization-Based Simulators for Fractured and Non-fractured Reservoirs

    Energy Technology Data Exchange (ETDEWEB)

    Milind D. Deo

    2005-08-31

    Oil field development is a multi-million dollar business. Reservoir simulation is often used to guide the field management and development process. Reservoir characterization and geologic modeling tools have become increasingly sophisticated. As a result the geologic models produced are complex. Most reservoirs are fractured to a certain extent. The new geologic characterization methods are making it possible to map features such as faults and fractures, field-wide. Significant progress has been made in being able to predict properties of the faults and of the fractured zones. Traditionally, finite difference methods have been employed in discretizing the domains created by geologic means. For complex geometries, finite-element methods of discretization may be more suitable. Since reservoir simulation is a mature science, some of the advances in numerical methods (linear, nonlinear solvers and parallel computing) have not been fully realized in the implementation of most of the simulators. The purpose of this project was to address some of these issues. {sm_bullet} One of the goals of this project was to develop a series of finite-element simulators to handle problems of complex geometry, including systems containing faults and fractures. {sm_bullet} The idea was to incorporate the most modern computing tools; use of modular object-oriented computer languages, the most sophisticated linear and nonlinear solvers, parallel computing methods and good visualization tools. {sm_bullet} One of the tasks of the project was also to demonstrate the construction of fractures and faults in a reservoir using the available data and to assign properties to these features. {sm_bullet} Once the reservoir model is in place, it is desirable to find the operating conditions, which would provide the best reservoir performance. This can be accomplished by utilization optimization tools and coupling them with reservoir simulation. Optimization-based reservoir simulation was one of the

  6. Characterizing the influence of stress-induced microcracks on the laboratory strength and fracture development in brittle rocks using a finite-discrete element method-micro discrete fracture network FDEM-μDFN approach

    Directory of Open Access Journals (Sweden)

    Pooya Hamdi

    2015-12-01

    Full Text Available Heterogeneity is an inherent component of rock and may be present in different forms including mineral heterogeneity, geometrical heterogeneity, weak grain boundaries and micro-defects. Microcracks are usually observed in crystalline rocks in two forms: natural and stress-induced; the amount of stress-induced microcracking increases with depth and in-situ stress. Laboratory results indicate that the physical properties of rocks such as strength, deformability, P-wave velocity and permeability are influenced by increase in microcrack intensity. In this study, the finite-discrete element method (FDEM is used to model microcrack heterogeneity by introducing into a model sample sets of microcracks using the proposed micro discrete fracture network (μDFN approach. The characteristics of the microcracks required to create μDFN models are obtained through image analyses of thin sections of Lac du Bonnet granite adopted from published literature. A suite of two-dimensional laboratory tests including uniaxial, triaxial compression and Brazilian tests is simulated and the results are compared with laboratory data. The FDEM-μDFN models indicate that micro-heterogeneity has a profound influence on both the mechanical behavior and resultant fracture pattern. An increase in the microcrack intensity leads to a reduction in the strength of the sample and changes the character of the rock strength envelope. Spalling and axial splitting dominate the failure mode at low confinement while shear failure is the dominant failure mode at high confinement. Numerical results from simulated compression tests show that microcracking reduces the cohesive component of strength alone, and the frictional strength component remains unaffected. Results from simulated Brazilian tests show that the tensile strength is influenced by the presence of microcracks, with a reduction in tensile strength as microcrack intensity increases. The importance of microcrack heterogeneity in

  7. Nanotechnology for treating osteoporotic vertebral fractures

    Science.gov (United States)

    Gao, Chunxia; Wei, Donglei; Yang, Huilin; Chen, Tao; Yang, Lei

    2015-01-01

    Osteoporosis is a serious public health problem affecting hundreds of millions of aged people worldwide, with severe consequences including vertebral fractures that are associated with significant morbidity and mortality. To augment or treat osteoporotic vertebral fractures, a number of surgical approaches including minimally invasive vertebroplasty and kyphoplasty have been developed. However, these approaches face problems and difficulties with efficacy and long-term stability. Recent advances and progress in nanotechnology are opening up new opportunities to improve the surgical procedures for treating osteoporotic vertebral fractures. This article reviews the improvements enabled by new nanomaterials and focuses on new injectable biomaterials like bone cements and surgical instruments for treating vertebral fractures. This article also provides an introduction to osteoporotic vertebral fractures and current clinical treatments, along with the rationale and efficacy of utilizing nanomaterials to modify and improve biomaterials or instruments. In addition, perspectives on future trends with injectable bone cements and surgical instruments enhanced by nanotechnology are provided. PMID:26316746

  8. Contemporary Management of Infected Mandibular Fractures

    Science.gov (United States)

    Alpert, Brian; Kushner, George M.; Tiwana, Paul S.

    2008-01-01

    The treatment of infected mandibular fractures has advanced rather dramatically over the past 50 years. Immobilization with maxillomandibular fixation and/or splints, removal of diseased teeth in the fracture line, external fixation, use of antibiotics, debridement, and rigid internal fixation has played a role in management. Perhaps the most important advance was the realization that infected fractures also result from moving fragments and nonvital bone, not just bacteria. Controlling movement and eliminating the dead bone allowed body defenses to also eliminate bacteria. The next logical step in the evolution of treatment was primary bone grafting of the resulting defect following application of rigid internal fixation and debridement of the dead bone. We offer our results with this treatment in 21 infected fractures, 20 of which achieved primary union. PMID:22110786

  9. Scale-Dependent Fracture-Matrix Interactions and Their Impact on Radionuclide Transport: Development of efficient particle-tracking methods

    Energy Technology Data Exchange (ETDEWEB)

    Rajaram, Harihar [University of Colorado, Boulder; Brutz, Michael [University of Colorado, Boulder; Klein, Dylan R [University of Colorado, Boulder; Mallikamas, Wasin [University of Colorado, Boulder

    2014-09-18

    Matrix Diffusion and Adsorption within a rock matrix are important mechanisms for retarding transport of radionuclides in fractured rock. Due to computational limitations and difficulties in characterizing complex subsurface systems, diffusive exchange between a fracture network and surrounding rock matrix is often modeled using simplified conceptual representations. There is significant uncertainty in “effective” parameters used in these models, such as the “effective matrix diffusivity”. Often, these parameters are estimated by fitting sparse breakthrough data, and estimated values fall outside meaningful ranges, because simplified interpretive models do not consider complex three-dimensional flow. There is limited understanding of the relationship between the effective parameters and rock mass characteristics including network structure and matrix properties. There is also evidence for an apparent scale-dependence in “effective matrix diffusion” coefficients. These observations raise questions on whether fracture-matrix interaction parameters estimated from small-scale tracer tests can be used for predicting radionuclide fate and transport at the scale of DOE field sites. High-resolution three-dimensional Discrete-Fracture-Network-Matrix (DFNM) models based on well-defined local scale transport equations can help to address some of these questions. Due to tremendous advances in computational technology over the last 10 years, DFNM modeling in relatively large domains is now feasible. The overarching objective of our research is to use DFNM modeling to improve fundamental understanding of how effective parameters in conceptual models are related to fracture network structure and matrix properties. An advanced three-dimensional DFNM model is being developed, which combines upscaled particle-tracking algorithms for fracture-matrix interaction and a parallel fracture-network flow simulator. The particle-tracking algorithms allow complexity in flow fields

  10. Advanced Characterization of Soil Organic Matter Using Ultra High Resolution Mass Spectrometry

    Science.gov (United States)

    Tfaily, M. M.; Chu, R.; Tolic, N.; Roscioli, K.; Robinson, E. R.; Paša-Tolić, L.; Hess, N. J.

    2014-12-01

    The focus on ecosystem stress and climate change is currently relevant as researchers and policymakers strive to understand the feedbacks between soil C dynamics and climate change. Successful development of molecular profiles that link soil microbiology with soil carbon (C) to ascertain soil vulnerability and resilience to climate change would have great impact on assessments of soil ecosystems in response to climate change. Additionally, better understanding of the dynamics of soil organic matter (SOM) plays a central role to climate modeling, and fate and transport of carbon. The use of ultra-high resolution mass spectrometry (UHR MS) has enabled the examination of molecules, directly from mixtures, with ultrahigh mass resolution and sub-ppm mass accuracy. In this study, EMSL's extensive expertise and capabilities in UHR MS proteomics were leveraged to develop extraction protocols for the characterization of carbon compounds in SOM, thereby providing the chemical and structural detail needed to develop mechanistic descriptions of soil carbon flow processes. Our experiments have allowed us to identify thousands of individual compounds in complex soil mixtures with a wide range of C content representing diverse ecosystems within the USA. The yield of the chemical extraction was dependent on (1) the type of solvent used and its polarity, (2) sample-to-solvent ratios and (3) the chemical and physical nature of the samples including their origins. Hexane, a non-polar organic solvent, was efficient in extracting lipid-like compounds regardless of soil origin or organic carbon %. For samples with high organic carbon %, acetonitrile extracted a wide range of compounds characterized with high O/C ratios, identified as polyphenolic compounds that were not observed with methanol extraction. Soils extracted with pyridine showed a similar molecular distribution to those extracted by methanol. Solvent extraction followed by UHR MS is a promising tool to understand the

  11. Increasing Heavy Oil Reserves in the Wilmington Oil Field through Advanced Reservoir Characterization and Thermal Production Technologies

    Energy Technology Data Exchange (ETDEWEB)

    City of Long Beach; David K.Davies and Associates; Tidelands Oil Production Company; University of Southern California

    1999-06-25

    The objective of this project is to increase the recoverable heavy oil reserves within sections of the Wilmington Oil Field, near Long Beach, California. This is realized through the testing and application of advanced reservoir characterization and thermal production technologies. It is hoped that the successful application of these technologies will result in their implementation throughout the Wilmington Field and through technology transfer, will be extended to increase the recoverable oil reserves in other slope and basin clastic (SBC) reservoirs. The existing steamflood in the Tar zone of Fault Block (FB) II-A has been relatively insufficient because of several producability problems which are common in SBC reservoir; inadequate characterization of the heterogeneous turbidite sands, high permeability thief zones, low gravity oil and non-uniform distribution of the remaining oil. This has resulted in poor sweep efficiency, high steam-oil ratios, and early breakthrough. Operational problems related to steam breakthrough, high reservoir pressure, and unconsolidated sands have caused premature well and downhole equipment failures. In aggregate, these reservoir and operational constraints have resulted in increased operating costs and decreased recoverable reserves.

  12. a Fractal Network Model for Fractured Porous Media

    Science.gov (United States)

    Xu, Peng; Li, Cuihong; Qiu, Shuxia; Sasmito, Agus Pulung

    2016-04-01

    The transport properties and mechanisms of fractured porous media are very important for oil and gas reservoir engineering, hydraulics, environmental science, chemical engineering, etc. In this paper, a fractal dual-porosity model is developed to estimate the equivalent hydraulic properties of fractured porous media, where a fractal tree-like network model is used to characterize the fracture system according to its fractal scaling laws and topological structures. The analytical expressions for the effective permeability of fracture system and fractured porous media, tortuosity, fracture density and fraction are derived. The proposed fractal model has been validated by comparisons with available experimental data and numerical simulation. It has been shown that fractal dimensions for fracture length and aperture have significant effect on the equivalent hydraulic properties of fractured porous media. The effective permeability of fracture system can be increased with the increase of fractal dimensions for fracture length and aperture, while it can be remarkably lowered by introducing tortuosity at large branching angle. Also, a scaling law between the fracture density and fractal dimension for fracture length has been found, where the scaling exponent depends on the fracture number. The present fractal dual-porosity model may shed light on the transport physics of fractured porous media and provide theoretical basis for oil and gas exploitation, underground water, nuclear waste disposal and geothermal energy extraction as well as chemical engineering, etc.

  13. Advanced Nanoscale Characterization of Cement Based Materials Using X-Ray Synchrotron Radiation: A Review

    KAUST Repository

    Chae, Sejung R.

    2013-05-22

    We report various synchrotron radiation laboratory based techniques used to characterize cement based materials in nanometer scale. High resolution X-ray transmission imaging combined with a rotational axis allows for rendering of samples in three dimensions revealing volumetric details. Scanning transmission X-ray microscope combines high spatial resolution imaging with high spectral resolution of the incident beam to reveal X-ray absorption near edge structure variations in the material nanostructure. Microdiffraction scans the surface of a sample to map its high order reflection or crystallographic variations with a micron-sized incident beam. High pressure X-ray diffraction measures compressibility of pure phase materials. Unique results of studies using the above tools are discussed-a study of pores, connectivity, and morphology of a 2,000 year old concrete using nanotomography; detection of localized and varying silicate chain depolymerization in Al-substituted tobermorite, and quantification of monosulfate distribution in tricalcium aluminate hydration using scanning transmission X-ray microscopy; detection and mapping of hydration products in high volume fly ash paste using microdiffraction; and determination of mechanical properties of various AFm phases using high pressure X-ray diffraction. © 2013 The Author(s).

  14. Development and characterization of advanced 9Cr ferritic/martensitic steels for fission and fusion reactors

    Energy Technology Data Exchange (ETDEWEB)

    Saroja, S., E-mail: saroja@igcar.gov.in [Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102, Tamil Nadu (India); Dasgupta, A.; Divakar, R.; Raju, S.; Mohandas, E.; Vijayalakshmi, M. [Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102, Tamil Nadu (India); Bhanu Sankara Rao, K. [School of Engineering Sciences, University of Hyderabad, Hyderabad (India); Raj, Baldev [Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102, Tamil Nadu (India)

    2011-02-15

    This paper presents the results on the physical metallurgy studies in 9Cr Oxide Dispersion Strengthened (ODS) and Reduced Activation Ferritic/Martensitic (RAFM) steels. Yttria strengthened ODS alloy was synthesized through several stages, like mechanical milling of alloy powders and yttria, canning and consolidation by hot extrusion. During characterization of the ODS alloy, it was observed that yttria particles possessed an affinity for Ti, a small amount of which was also helpful in refining the dispersoid particles containing mixed Y and Ti oxides. The particle size and their distribution in the ferrite matrix, were studied using Analytical and High Resolution Electron Microscopy at various stages. The results showed a distribution of Y{sub 2}O{sub 3} particles predominantly in the size range of 5-20 nm. A Reduced Activation Ferritic/Martensitic steel has also been developed with the replacement of Mo and Nb by W and Ta with strict control on the tramp and trace elements (Mo, Nb, B, Cu, Ni, Al, Co, Ti). The transformation temperatures (A{sub c1}, A{sub c3} and M{sub s}) for this steel have been determined and the transformation behavior of the high temperature austenite phase has been studied. The complete phase domain diagram has been generated which is required for optimization of the processing and fabrication schedules for the steel.

  15. Advances in Chemical and Structural Characterization of Concretion with Implications for Modeling Marine Corrosion

    Science.gov (United States)

    Johnson, Donald L.; DeAngelis, Robert J.; Medlin, Dana J.; Carr, James D.; Conlin, David L.

    2014-05-01

    The Weins number model and concretion equivalent corrosion rate methodology were developed as potential minimum-impact, cost-effective techniques to determine corrosion damage on submerged steel structures. To apply the full potential of these technologies, a detailed chemical and structural characterization of the concretion (hard biofouling) that transforms into iron bearing minerals is required. The fractions of existing compounds and the quantitative chemistries are difficult to determine from x-ray diffraction. Environmental scanning electron microscopy was used to present chemical compositions by means of energy-dispersive spectroscopy (EDS). EDS demonstrates the chemical data in mapping format or in point or selected area chemistries. Selected-area EDS data collection at precise locations is presented in terms of atomic percent. The mechanism of formation and distribution of the iron-bearing mineral species at specific locations will be presented. Based on water retention measurements, porosity in terms of void volume varies from 15 v/o to 30 v/o (vol.%). The void path displayed by scanning electron microscopy imaging illustrates the tortuous path by which oxygen migrates in the water phase within the concretion from seaside to metalside.

  16. Advanced Development and Characterization of DEA Amine-Polysulfone/Polyvinylacetate Blend Membranes

    Directory of Open Access Journals (Sweden)

    Asim Mushtaq

    2014-09-01

    Full Text Available Membrane technology effectively separates CO2 from CH4 and has been practiced for many years but requires membranes with high selectivity and permeability. Different approaches are employed to improve membrane performance and it is soon possible to develop a blended polymeric membrane that separates high pressure gas streams at the point of processing pressure. However, glassy polymers suffer a lack of permeability causing their performance to drop as an upper bound trade-off but highly selective and rubbery polymers have high permeability with low selectivity. As an amine solution is capable of purifying naturally acidic gas, blending glassy, rubbery polymers with amines-specifically, polysulfone and polyvinyl acetate with diethanol amine in dimethyl acetamide as solvent-we developed flat sheet membranes with desirable properties. As it is now possible to acquire amine-polymer blends with more desirable properties by mixing with a miscible polymer, it is essential to observe factors that affect the polymer's miscibility with amines. Hence, we also analyzed the effects of blend ratios on different properties. Blended membranes of different ratios were synthesized and their functional groups were characterized by Fourier Transformed Infra-Red spectroscopy (FTIR. We then employed Thermal Gravimetric Analysis (TGA to describe weight loss and Field Emission Scanning Electron Microscopy (FESEM to determine respective morphologies.

  17. Magnetoresistance mobility characterization in advanced FD-SOI n-MOSFETs

    Science.gov (United States)

    Shin, Minju; Shi, Ming; Mouis, Mireille; Cros, Antoine; Josse, Emmanuel; Mukhopadhyay, Sutirha; Piot, Benjamin; Kim, Gyu-Tae; Ghibaudo, Gérard

    2015-01-01

    In this work, we applied the magnetoresistance (MR) characterization technique on n-type FD-SOI devices from a 14 nm-node technology. A notable advantage of MR is that it can probe the sub-threshold region, where Coulomb scattering influence is unscreened, while classical methods are validated to the strong inversion regime. At first, we discuss the influence of series resistance depending on gate bias, gate stack and temperature in this technology. Secondly, for long channel devices, we show that Coulomb scattering plays no significant role below threshold voltage at room temperature, in spite of the presence of a high-k/metal gate stack. MR-mobility (μMR) measurements were also performed in interface coupling conditions in order to further assess the role of the high-k/metal gate stack on transport properties and to analyze back bias induced mobility variations, depending on temperature range. Finally, the comparative study of low field effective mobility (μ0) and μMR shows that critical gate length of mobility degradation can be overestimated by using μ0 at low temperature due to a lack of ability of Y-function method to capture unscreened Coulomb scattering.

  18. Advances in Adipose-Derived Stem Cells Isolation, Characterization, and Application in Regenerative Tissue Engineering.

    Science.gov (United States)

    Wankhade, Umesh D; Shen, Michael; Kolhe, Ravindra; Fulzele, Sadanand

    2016-01-01

    Obesity is a complex, multifactorial disease that has been extensively researched in recent times. Obesity is characterized by excess deposition of adipose tissue in response to surplus energy. Despite the negative connotations of adipose tissue (AT), it serves as a critical endocrine organ. Adipose tissue is a source of several adipokines and cytokines which have been deemed important for both normal metabolic function and disease formation. The discoveries of metabolically active brown AT in adult humans and adipose tissue derived stem cells (ADSC) have been key findings in the past decade with potential therapeutic implications. ADSCs represent an enticing pool of multipotent adult stem cells because of their noncontroversial nature, relative abundance, ease of isolation, and expandability. A decade and a half since the discovery of ADSCs, the scientific community is still working to uncover their therapeutic potential in a wide range of diseases. In this review, we provide an overview of the recent developments in the field of ADSCs and examine their potential use in transplantation and cell-based therapies for the regeneration of diseased organs and systems. We also hope to provide perspective on how to best utilize this readily available, powerful pool of stem cells in the future.

  19. Advanced Mass Spectrometric Methods for the Rapid and Quantitative Characterization of Proteomes

    Directory of Open Access Journals (Sweden)

    Richard D. Smith

    2006-04-01

    Full Text Available Progress is reviewed towards the development of a global strategy that aims to extend the sensitivity, dynamic range, comprehensiveness and throughput of proteomic measurements based upon the use of high performance separations and mass spectrometry. The approach uses high accuracy mass measurements from Fourier transform ion cyclotron resonance mass spectrometry (FTICR to validate peptide ‘accurate mass tags’ (AMTs produced by global protein enzymatic digestions for a specific organism, tissue or cell type from ‘potential mass tags’ tentatively identified using conventional tandem mass spectrometry (MS/MS. This provides the basis for subsequent measurements without the need for MS/ MS. High resolution capillary liquid chromatography separations combined with high sensitivity, and high resolution accurate FTICR measurements are shown to be capable of characterizing peptide mixtures of more than 105 components. The strategy has been initially demonstrated using the microorganisms Saccharomyces cerevisiae and Deinococcus radiodurans. Advantages of the approach include the high confidence of protein identification, its broad proteome coverage, high sensitivity, and the capability for stableisotope labeling methods for precise relative protein abundance measurements.

  20. A Metagenomic Advance for the Cloning and Characterization of a Cellulase from Red Rice Crop Residues.

    Science.gov (United States)

    Meneses, Carlos; Silva, Bruna; Medeiros, Betsy; Serrato, Rodrigo; Johnston-Monje, David

    2016-01-01

    Many naturally-occurring cellulolytic microorganisms are not readily cultivable, demanding a culture-independent approach in order to study their cellulolytic genes. Metagenomics involves the isolation of DNA from environmental sources and can be used to identify enzymes with biotechnological potential from uncultured microbes. In this study, a gene encoding an endoglucanase was cloned from red rice crop residues using a metagenomic strategy. The amino acid identity between this gene and its closest published counterparts is lower than 70%. The endoglucanase was named EglaRR01 and was biochemically characterized. This recombinant protein showed activity on carboxymethylcellulose, indicating that EglaRR01 is an endoactive lytic enzyme. The enzymatic activity was optimal at a pH of 6.8 and at a temperature of 30 °C. Ethanol production from this recombinant enzyme was also analyzed on EglaRR01 crop residues, and resulted in conversion of cellulose from red rice into simple sugars which were further fermented by Saccharomyces cerevisiae to produce ethanol after seven days. Ethanol yield in this study was approximately 8 g/L. The gene found herein shows strong potential for use in ethanol production from cellulosic biomass (second generation ethanol). PMID:27347917

  1. Preparation and characterization of B4C coatings for advanced research light sources.

    Science.gov (United States)

    Störmer, Michael; Siewert, Frank; Sinn, Harald

    2016-01-01

    X-ray optical elements are required for beam transport at the current and upcoming free-electron lasers and synchrotron sources. An X-ray mirror is a combination of a substrate and a coating. The demand for large mirrors with single layers consisting of light or heavy elements has increased during the last few decades; surface finishing technology is currently able to process mirror lengths up to 1 m with microroughness at the sub-nanometre level. Additionally, thin-film fabrication is able to deposit a suitable single-layer material, such as boron carbide (B4C), some tens of nanometres thick. After deposition, the mirror should provide excellent X-ray optical properties with respect to coating thickness errors, microroughness values and slope errors; thereby enabling the mirror to transport the X-ray beam with high reflectivity, high beam flux and an undistorted wavefront to an experimental station. At the European XFEL, the technical specifications of the future mirrors are extraordinarily challenging. The acceptable shape error of the mirrors is below 2 nm along the whole length of 1 m. At the Helmholtz-Zentrum Geesthacht (HZG), amorphous layers of boron carbide with thicknesses in the range 30-60 nm were fabricated using the HZG sputtering facility, which is able to cover areas up to 1500 mm long by 120 mm wide in one step using rectangular B4C sputtering targets. The available deposition area is suitable for the specified X-ray mirror dimensions of upcoming advanced research light sources such as the European XFEL. The coatings produced were investigated by means of X-ray reflectometry and interference microscopy. The experimental results for the B4C layers are discussed according to thickness uniformity, density, microroughness and thermal stability. The variation of layer thickness in the tangential and sagittal directions was investigated in order to estimate the achieved level of uniformity over the whole deposition area, which is considerably

  2. Preparation and characterization of B4C coatings for advanced research light sources

    Science.gov (United States)

    Störmer, Michael; Siewert, Frank; Sinn, Harald

    2016-01-01

    X-ray optical elements are required for beam transport at the current and upcoming free-electron lasers and synchrotron sources. An X-ray mirror is a combination of a substrate and a coating. The demand for large mirrors with single layers consisting of light or heavy elements has increased during the last few decades; surface finishing technology is currently able to process mirror lengths up to 1 m with microroughness at the sub-nanometre level. Additionally, thin-film fabrication is able to deposit a suitable single-layer material, such as boron carbide (B4C), some tens of nanometres thick. After deposition, the mirror should provide excellent X-ray optical properties with respect to coating thickness errors, microroughness values and slope errors; thereby enabling the mirror to transport the X-ray beam with high reflectivity, high beam flux and an undistorted wavefront to an experimental station. At the European XFEL, the technical specifications of the future mirrors are extraordinarily challenging. The acceptable shape error of the mirrors is below 2 nm along the whole length of 1 m. At the Helmholtz-Zentrum Geesthacht (HZG), amorphous layers of boron carbide with thicknesses in the range 30–60 nm were fabricated using the HZG sputtering facility, which is able to cover areas up to 1500 mm long by 120 mm wide in one step using rectangular B4C sputtering targets. The available deposition area is suitable for the specified X-ray mirror dimensions of upcoming advanced research light sources such as the European XFEL. The coatings produced were investigated by means of X-ray reflectometry and interference microscopy. The experimental results for the B4C layers are discussed according to thickness uniformity, density, microroughness and thermal stability. The variation of layer thickness in the tangential and sagittal directions was investigated in order to estimate the achieved level of uniformity over the whole deposition area, which is

  3. Advanced x-ray spectrometric techniques for characterization of nuclear materials: An overview of recent laboratory activities

    Energy Technology Data Exchange (ETDEWEB)

    Misra, N.L., E-mail: nlmisra@barc.gov.in

    2014-11-01

    Advancements in x-ray spectrometric techniques at different stages have made this technique suitable for characterization of nuclear materials with respect to trace/major element determinations and compositional uniformity studies. The two important features of total reflection x-ray fluorescence spectrometry: 1) requirement of very small amount of sample in ng level 2) multielement analytical capability, in addition to other features, make this technique very much suitable to nuclear materials characterization as most of the nuclear materials are radioactive and the radioactive waste generated and radiation hazards to the operator are minimum when such low amount of sample is used. Similarly advanced features of energy dispersive x-ray fluorescence e.g. better geometry for high flux, reduction in background due to application of radiation filters have made the measurements of samples sealed inside thin alkathene/PVC covers possible with good sensitivity. This approach avoids putting the instrument inside a glove box for measuring radioactive samples and makes the operation/maintenance of the instrument and analysis of the samples possible in easy and fast manner. This approach has been used for major element determinations in mixed uranium–plutonium samples. Similarly μ-XRF with brilliant and micro-focused excitation sources can be used for compositional uniformity study of reactor fuel pellets. A μ-XRF study using synchrotron light source has been made to assess the compositional uniformity of mixed uranium–thorium oxide pellets produced by different processes. This approach is simple as it does not involve any sample preparation and is non-destructive. A brief summary of such activities carried out in our laboratory in past as well as ongoing and planned for the future have been discussed in the present manuscript. - Highlights: • Advantages of TXRF characterization of nuclear materials are described. • The sample amount required/analytical radioactive

  4. Fractures in multiple sclerosis

    DEFF Research Database (Denmark)

    Stenager, E; Jensen, K

    1991-01-01

    In a cross-sectional study of 299 MS patients 22 have had fractures and of these 17 after onset of MS. The fractures most frequently involved the femoral neck and trochanter (41%). Three patients had had more than one fracture. Only 1 patient had osteoporosis. The percentage of fractures increase...

  5. Advances in EBSD and EBSD/EDS integration for the characterization of mineralogical samples

    Science.gov (United States)

    Palasse, L.; Goran, D.; Schwager, T.

    2013-12-01

    Electron BackScatter Diffraction (EBSD) is a well-known powerful technique for petrofabric studies using Scanning Electron Microscope. By assessing the quantitative microstructural information, i.e. crystallographic orientation data, it allows a large variety of applications: understanding the deformation mechanisms, seismic properties, metamorphic processes; and more recently, performing phase identification and discrimination when combined with Energy Dispersive X-Ray Spectroscopy (EDS). However, it is known that for multiphase mineralogical samples, the information delivered either by EBSD or by EDS alone is not enough to successfully distinguish the present phases. Typical examples for EBSD related indexing issues are phases creating similar patterns; and for EDS technique alone, phases with similar chemical composition like calcite and aragonite, quartz and cristobalite. Recent software and hardware developments have significantly improved the data quality as well as the efficiency/productivity. This presentation aims to reveal the latest development in data processing that has transformed the combination of the two complementary techniques into a powerful tool for characterizing multiphase materials. Through geosciences application examples, we will present the advantages brought by this new approach which uses the quantified EDS results and EBSP to identify the correct phase, reducing the need of data cleaning, and without spending extra time at the SEM. We will also demonstrate how powerful EBSD indexing algorithm can overcome the limitation from sample preparation, with some examples of high hit rate achieved on polyphase mineralogical specimen and even on shock-metamorphosed minerals. Last but not least, recent developments also enable the investigation of nanostructured materials in the scanning electron microscope (SEM) by Transmission Kikuchi Diffraction (TKD). Through some mineralogical applications, we will demonstrate the high spatial resolution

  6. Assessment of fracture risk

    Energy Technology Data Exchange (ETDEWEB)

    Kanis, John A. [WHO Collaborating Centre for Metabolic Bone Diseases, University of Sheffield Medical School, Beech Hill Road, Sheffield S10 2RX (United Kingdom)], E-mail: w.j.pontefract@sheffield.ac.uk; Johansson, Helena; Oden, Anders [WHO Collaborating Centre for Metabolic Bone Diseases, University of Sheffield Medical School, Beech Hill Road, Sheffield S10 2RX (United Kingdom); McCloskey, Eugene V. [WHO Collaborating Centre for Metabolic Bone Diseases, University of Sheffield Medical School, Beech Hill Road, Sheffield S10 2RX (United Kingdom); Osteoporosis Centre, Northern General Hospital, Sheffield (United Kingdom)

    2009-09-15

    Fractures are a common complication of osteoporosis. Although osteoporosis is defined by bone mineral density at the femoral neck, other sites and validated techniques can be used for fracture prediction. Several clinical risk factors contribute to fracture risk independently of BMD. These include age, prior fragility fracture, smoking, excess alcohol, family history of hip fracture, rheumatoid arthritis and the use of oral glucocorticoids. These risk factors in conjunction with BMD can be integrated to provide estimates of fracture probability using the FRAX tool. Fracture probability rather than BMD alone can be used to fashion strategies for the assessment and treatment of osteoporosis.

  7. Confocal microscopy-fracture reconstruction and finite element modeling characterization of local cleavage toughness in a ferritic/martensitic steel in subsized Charpy V-notch impact tests

    Energy Technology Data Exchange (ETDEWEB)

    Yamamoto, T. E-mail: yamataku@fusion.imr.tohoku.ac.jp; Odette, G.R.; Lucas, G.E.; Matsui, H

    2000-12-01

    The confocal microscopy (CM)-fracture reconstruction (FR) method, coupled with scanning electron microscopy (SEM) fractography, was used to measure the critical notch deformation conditions at cleavage initiation for two subsized Charpy V-notch (CVN) specimen geometries of Japan ferritic/martensitic steel (JFMS). A new method was developed to permit FR of notched specimens. Three-dimensional finite element analysis (FEA) simulations of the notch and specimen deformation were used to estimate values of critical micro-cleavage fracture stress, {sigma}{sup *}, and critical stressed area, A{sup *}. Since {sigma}{sup *}-A{sup *} is independent of size and geometry, it provides a fundamental local measure of cleavage toughness.

  8. Preparation and characterization of B{sub 4}C coatings for advanced research light sources

    Energy Technology Data Exchange (ETDEWEB)

    Störmer, Michael, E-mail: michael.stoermer@hzg.de [Helmholtz-Zentrum Geesthacht, Max-Planck-Strasse 1, D-21502 Geesthacht (Germany); Siewert, Frank [Helmholtz-Zentrum Berlin, Albert-Einstein-Strasse 15, 12489 Berlin (Germany); Sinn, Harald [European XFEL GmbH, Albert-Einstein-Ring 19, 22761 Hamburg (Germany)

    2016-01-01

    The challenging specifications for long X-ray mirrors for upcoming free-electron lasers can be achieved, especially for maintaining below 2 nm peak-to-valley shape error along the optical aperture of approximately 1 m-long mirrors. X-ray optical elements are required for beam transport at the current and upcoming free-electron lasers and synchrotron sources. An X-ray mirror is a combination of a substrate and a coating. The demand for large mirrors with single layers consisting of light or heavy elements has increased during the last few decades; surface finishing technology is currently able to process mirror lengths up to 1 m with microroughness at the sub-nanometre level. Additionally, thin-film fabrication is able to deposit a suitable single-layer material, such as boron carbide (B{sub 4}C), some tens of nanometres thick. After deposition, the mirror should provide excellent X-ray optical properties with respect to coating thickness errors, microroughness values and slope errors; thereby enabling the mirror to transport the X-ray beam with high reflectivity, high beam flux and an undistorted wavefront to an experimental station. At the European XFEL, the technical specifications of the future mirrors are extraordinarily challenging. The acceptable shape error of the mirrors is below 2 nm along the whole length of 1 m. At the Helmholtz-Zentrum Geesthacht (HZG), amorphous layers of boron carbide with thicknesses in the range 30–60 nm were fabricated using the HZG sputtering facility, which is able to cover areas up to 1500 mm long by 120 mm wide in one step using rectangular B{sub 4}C sputtering targets. The available deposition area is suitable for the specified X-ray mirror dimensions of upcoming advanced research light sources such as the European XFEL. The coatings produced were investigated by means of X-ray reflectometry and interference microscopy. The experimental results for the B{sub 4}C layers are discussed according to thickness uniformity, density

  9. Ash chemistry in MSW incineration plants: Advanced characterization and thermodynamic considerations

    Energy Technology Data Exchange (ETDEWEB)

    Frandsen, Flemming J.; Laursen, Karin; Arvelakis, S. (and others)

    2004-07-15

    A number of ash samples where collected at four Danish municipal solid waste incineration (MSWI) plants. Samples of bottom ash/slag, 2nd-3rd pass ashes and ESP/E-filter ash were collected at the plants. The ashes were analyzed by a number of standard chemical analyses, and a number of advanced analytical techniques. The wet chemical analyses of the different ash fractions revealed that residual ash is formed on the grate by interaction of the main ash forming elements, Al, Ca, Fe and Si. Some of this ash is entrained from the grate and carried with the flue gas along the flue gas duct, where volatile species of K, Na, Pb, Zn, Cl and S starts to condense heterogeneously on the fly ash, thereby causing a dilution of the main ash forming elements. When compared plant-by-plant, the ash chemical analyses showed that the plant with the highest S-content in the fly ash is the one with the most often operational problems in relation to deposition, while a high Cl-content is indicative of a high corrosive potential. An existing Computer Controlled Scanning Electron Microscopy (CCSEM) algorithm was extended with chemical classes covering Pb- and Zn-rich phases. This has made it possible also to analyze MSW-derived ashes by use of CCSEM. Representative samples of 2nd-3rd pass and ESP/E-filter ashes from the four plants have been analyzed by Quantitative X-Ray Diffraction (QXRD) analysis. Only a few crystalline phases were identified: KCl, NaCl, CaSO{sub 4}, SiO{sub 2} and CaCO{sub 3} being the main ones. No crystalline phases containing Pb or Zn were identified by QXRD. A comparison between CCSEM and QXRD revealed the expected surface nature of the CCSEM analysis. Samples of 2nd-3rd pass and ESP/E-filter ash from the four plants where investigated for melting behavior in the Simultaneous Thermal Analyzer (STA). It was shown that it is possible to quantify the melting behavior of these ashes, and that the melting goes on in two steps (salts followed by silicates/oxides). The

  10. Simulated evolution of fractures and fracture networks subject to thermal cooling: A coupled discrete element and heat conduction model

    Energy Technology Data Exchange (ETDEWEB)

    Huang, Hai; Plummer, Mitchell; Podgorney, Robert

    2013-02-01

    Advancement of EGS requires improved prediction of fracture development and growth during reservoir stimulation and long-term operation. This, in turn, requires better understanding of the dynamics of the strongly coupled thermo-hydro-mechanical (THM) processes within fractured rocks. We have developed a physically based rock deformation and fracture propagation simulator by using a quasi-static discrete element model (DEM) to model mechanical rock deformation and fracture propagation induced by thermal stress and fluid pressure changes. We also developed a network model to simulate fluid flow and heat transport in both fractures and porous rock. In this paper, we describe results of simulations in which the DEM model and network flow & heat transport model are coupled together to provide realistic simulation of the changes of apertures and permeability of fractures and fracture networks induced by thermal cooling and fluid pressure changes within fractures. Various processes, such as Stokes flow in low velocity pores, convection-dominated heat transport in fractures, heat exchange between fluid-filled fractures and solid rock, heat conduction through low-permeability matrices and associated mechanical deformations are all incorporated into the coupled model. The effects of confining stresses, developing thermal stress and injection pressure on the permeability evolution of fracture and fracture networks are systematically investigated. Results are summarized in terms of implications for the development and evolution of fracture distribution during hydrofracturing and thermal stimulation for EGS.

  11. A closer look at the fracture toughness of ferritic/martensitic steels

    Science.gov (United States)

    Lucon, Enrico

    2007-08-01

    SCK·CEN has characterized the mechanical properties of several ferritic/martensitic steels, both unirradiated and irradiated. Fracture toughness has been evaluated using Charpy impact and fracture mechanics tests. Two safety-related features have emerged: (a) the applicability of the master curve approach (ASTM E1921-05) appears questionable; and (b) irradiation embrittlement is systematically larger when quantified in terms of quasi-static fracture toughness than when measured from Charpy tests. Both issues are examined in detail and possible interpretations are proposed; potential improvements given by the application of more advanced fracture toughness analysis methodologies are discussed. In order to clarify whether the Charpy/fracture toughness difference in embrittlement is due to loading rate effects, dynamic toughness tests have been performed in the unirradiated condition and for two irradiation doses (0.3 and 1.6 dpa). The corresponding dynamic T0 shifts have been compared with the shifts of Charpy and master curve quasi-static transition temperatures. Other possible contributions are examined and discussed.

  12. A prediction scheme of the static fracture strength of MEMS structures based on the characterization of damage distribution on a processed surface

    International Nuclear Information System (INIS)

    This paper presents a scheme for predicting the strength of MEMS structures patterned into arbitrary shapes by deep reactive ion etching of a silicon wafer. The scheme is based on the inhomogeneous defect distribution on the etched surfaces. Single-crystal silicon specimens with different shapes were subjected to four-point bending tests with monotonically increasing load. The distributions of the fracture strength were described using two-parameter Weibull statistics, where the two parameters are defined as functions of the etching depth representing the inhomogeneity of the damage on the etched surface in the direction perpendicular to the wafer. In order to estimate the distribution of the local strength determined by the local level of damage, the etched surfaces of specimens without a notch were tested in three different bending directions corresponding to three different stress distributions, and three different strength levels were given due to surface roughness conditions caused by the non-uniformity of the etching process. The estimated values of the parameters were used to estimate the fracture strength of four types of notched specimens with different notch tip radii. The results of comparison between the distributions of predicted strengths and experimental data showed that the fracture strength of arbitrarily shaped structures is predictable on the basis of the information obtained from specimens without notch, by taking into account the characteristics of etched surface, i.e. the inhomogeneous damage. (paper)

  13. Splinting of Longitudinal Fracture: An Innovative Approach

    Directory of Open Access Journals (Sweden)

    Rashmi Bansal

    2016-01-01

    Full Text Available Trauma may result in craze lines on the enamel surface, one or more fractured cusps of posterior teeth, cracked tooth syndrome, splitting of posterior teeth, and vertical fracture of root. Out of these, management of some fractures is of great challenge and such teeth are generally recommended for extraction. Literature search reveals attempts to manage such fractures by full cast crown, orthodontic wires, and so forth, in which consideration was given to extracoronal splinting only. However, due to advancement in materials and technologies, intracoronal splinting can be achieved as well. In this case report, longitudinal fractures in tooth #27, tooth #37, and tooth #46 had occurred. In #27, fracture line was running mesiodistally involving the pulpal floor resulting in a split tooth. In teeth 37 and 46, fractures of the mesiobuccal cusp and mesiolingual cusp were observed, respectively. They were restored with cast gold inlay and full cast crown, respectively. Longitudinal fracture of 27 was treated with an innovative approach using intracanal reinforced composite with Ribbond, external reinforcement with an orthodontic band, and full cast metal crown to splint the split tooth.

  14. Splinting of Longitudinal Fracture: An Innovative Approach

    Science.gov (United States)

    Bansal, Rashmi; Chowdhary, Priyanka; Gurtu, Anuraag; Mehrotra, Nakul; Kishore, Abhinav

    2016-01-01

    Trauma may result in craze lines on the enamel surface, one or more fractured cusps of posterior teeth, cracked tooth syndrome, splitting of posterior teeth, and vertical fracture of root. Out of these, management of some fractures is of great challenge and such teeth are generally recommended for extraction. Literature search reveals attempts to manage such fractures by full cast crown, orthodontic wires, and so forth, in which consideration was given to extracoronal splinting only. However, due to advancement in materials and technologies, intracoronal splinting can be achieved as well. In this case report, longitudinal fractures in tooth #27, tooth #37, and tooth #46 had occurred. In #27, fracture line was running mesiodistally involving the pulpal floor resulting in a split tooth. In teeth 37 and 46, fractures of the mesiobuccal cusp and mesiolingual cusp were observed, respectively. They were restored with cast gold inlay and full cast crown, respectively. Longitudinal fracture of 27 was treated with an innovative approach using intracanal reinforced composite with Ribbond, external reinforcement with an orthodontic band, and full cast metal crown to splint the split tooth. PMID:27247808

  15. Lower extremity stress fractures in the military.

    Science.gov (United States)

    Jacobs, Jeremy M; Cameron, Kenneth L; Bojescul, John A

    2014-10-01

    Stress fractures of the lower extremities are common among the military population and, more specifically, military recruits who partake in basic training. Both intrinsic and extrinsic factors play a role in the development of these injuries, and it is important to identify those individuals at risk early in their military careers. Some of these factors are modifiable, so they may become preventable injuries. It is important to reiterate that one stress fracture places the soldier at risk for future stress fractures; but the first injury should not be reason enough for separation from the military, as literature would support no long-term deficits from properly treated stress fractures. Early in the process, radiographic analysis is typically normal; continued pain may warrant advanced imaging, such as scintigraphy or MRI. Most stress fractures that are caught early are amendable to nonoperative management consisting of a period of immobilization and NWB followed by progressive rehabilitation to preinjury levels. Complete or displaced fractures may require operative intervention as do tension-sided FNSF. Improving dietary and preaccession physical fitness levels may play a role in reducing the incidence of stress fractures in the active-duty military population. It is important to keep in mind when evaluating soldiers and athletes who present with activity-related pain that stress fractures are not uncommon and should be given significant consideration.

  16. Advanced Computational Approaches for Characterizing Stochastic Cellular Responses to Low Dose, Low Dose Rate Exposures

    Energy Technology Data Exchange (ETDEWEB)

    Scott, Bobby, R., Ph.D.

    2003-06-27

    OAK - B135 This project final report summarizes modeling research conducted in the U.S. Department of Energy (DOE), Low Dose Radiation Research Program at the Lovelace Respiratory Research Institute from October 1998 through June 2003. The modeling research described involves critically evaluating the validity of the linear nonthreshold (LNT) risk model as it relates to stochastic effects induced in cells by low doses of ionizing radiation and genotoxic chemicals. The LNT model plays a central role in low-dose risk assessment for humans. With the LNT model, any radiation (or genotoxic chemical) exposure is assumed to increase one¡¯s risk of cancer. Based on the LNT model, others have predicted tens of thousands of cancer deaths related to environmental exposure to radioactive material from nuclear accidents (e.g., Chernobyl) and fallout from nuclear weapons testing. Our research has focused on developing biologically based models that explain the shape of dose-response curves for low-dose radiation and genotoxic chemical-induced stochastic effects in cells. Understanding the shape of the dose-response curve for radiation and genotoxic chemical-induced stochastic effects in cells helps to better understand the shape of the dose-response curve for cancer induction in humans. We have used a modeling approach that facilitated model revisions over time, allowing for timely incorporation of new knowledge gained related to the biological basis for low-dose-induced stochastic effects in cells. Both deleterious (e.g., genomic instability, mutations, and neoplastic transformation) and protective (e.g., DNA repair and apoptosis) effects have been included in our modeling. Our most advanced model, NEOTRANS2, involves differing levels of genomic instability. Persistent genomic instability is presumed to be associated with nonspecific, nonlethal mutations and to increase both the risk for neoplastic transformation and for cancer occurrence. Our research results, based on

  17. Fracture Analysis of Particulate Reinforced Metal Matrix Composites

    Science.gov (United States)

    Min, James B.; Cornie, James A.

    2013-01-01

    A fracture analysis of highly loaded particulate reinforced composites was performed using laser moire interferometry to measure the displacements within the plastic zone at the tip of an advancing crack. Ten castings were made of five different particulate reinforcement-aluminum alloy combinations. Each casting included net-shape specimens which were used for the evaluation of fracture toughness, tensile properties, and flexure properties resulting in an extensive materials properties data. Measured fracture toughness range from 14.1 MPa for an alumina reinforced 356 aluminum alloy to 23.9 MPa for a silicon carbide reinforced 2214 aluminum alloy. For the combination of these K(sub Ic) values and the measured tensile strengths, the compact tension specimens were too thin to yield true plane strain K(sub Ic) values. All materials exhibited brittle behavior characterized by very small tensile ductility suggesting that successful application of these materials requires that the design stresses be below the elastic limit. Probabilistic design principles similar to those used with ceramics are recommended when using these materials. Such principles would include the use of experimentally determined design allowables. In the absence of thorough testing, a design allowable stress of 60 percent of the measured ultimate tensile stress is recommended.

  18. Naturally fractured tight gas reservoir detection optimization

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1998-11-30

    The work plan for October 1, 1997 to September 30, 1998 consisted of investigation of a number of topical areas. These topical areas were reported in four quarterly status reports, which were submitted to DOE earlier. These topical areas are reviewed in this volume. The topical areas covered during the year were: (1) Development of preliminary tests of a production method for determining areas of natural fracturing. Advanced Resources has demonstrated that such a relationship exists in the southern Piceance basin tight gas play. Natural fracture clusters are genetically related to stress concentrations (also called stress perturbations) associated with local deformation such a faulting. The mechanical explanation of this phenomenon is that deformation generally initiates at regions where the local stress field is elevated beyond the regional. (2) Regional structural and geologic analysis of the Greater Green River Basin (GGRB). Application of techniques developed and demonstrated during earlier phases of the project for sweet-spot delineation were demonstrated in a relatively new and underexplored play: tight gas from continuous-typeUpper Cretaceous reservoirs of the Greater Green River Basin (GGRB). The effort included data acquisition/processing, base map generation, geophysical and remote sensing analysis and the integration of these data and analyses. (3) Examination of the Table Rock field area in the northern Washakie Basin of the Greater Green River Basin. This effort was performed in support of Union Pacific Resources- and DOE-planned horizontal drilling efforts. The effort comprised acquisition of necessary seismic data and depth-conversion, mapping of major fault geometry, and analysis of displacement vectors, and the development of the natural fracture prediction. (4) Greater Green River Basin Partitioning. Building on fundamental fracture characterization work and prior work performed under this contract, namely structural analysis using satellite and

  19. Accurate Characterization of Winter Precipitation Using In-Situ Instrumentation, CSU-CHILL Radar, and Advanced Scattering Methods

    Science.gov (United States)

    Newman, A. J.; Notaros, B. M.; Bringi, V. N.; Kleinkort, C.; Huang, G. J.; Kennedy, P.; Thurai, M.

    2015-12-01

    We present a novel approach to remote sensing and characterization of winter precipitation and modeling of radar observables through a synergistic use of advanced in-situ instrumentation for microphysical and geometrical measurements of ice and snow particles, image processing methodology to reconstruct complex particle three-dimensional (3D) shapes, computational electromagnetics to analyze realistic precipitation scattering, and state-of-the-art polarimetric radar. Our in-situ measurement site at the Easton Valley View Airport, La Salle, Colorado, shown in the figure, consists of two advanced optical imaging disdrometers within a 2/3-scaled double fence intercomparison reference wind shield, and also includes PLUVIO snow measuring gauge, VAISALA weather station, and collocated NCAR GPS advanced upper-air system sounding system. Our primary radar is the CSU-CHILL radar, with a dual-offset Gregorian antenna featuring very high polarization purity and excellent side-lobe performance in any plane, and the in-situ instrumentation site being very conveniently located at a range of 12.92 km from the radar. A multi-angle snowflake camera (MASC) is used to capture multiple different high-resolution views of an ice particle in free-fall, along with its fall speed. We apply a visual hull geometrical method for reconstruction of 3D shapes of particles based on the images collected by the MASC, and convert these shapes into models for computational electromagnetic scattering analysis, using a higher order method of moments. A two-dimensional video disdrometer (2DVD), collocated with the MASC, provides 2D contours of a hydrometeor, along with the fall speed and other important parameters. We use the fall speed from the MASC and the 2DVD, along with state parameters measured at the Easton site, to estimate the particle mass (Böhm's method), and then the dielectric constant of particles, based on a Maxwell-Garnet formula. By calculation of the "particle-by-particle" scattering

  20. N