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Sample records for activation analysis determinacao

  1. Application of activation analysis for determination of some elements in cassiterite samples; Aplicacao da analise por ativacao para a determinacao de alguns elementos em amostras de cassiterita

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    Armelin, Maria Jose Aguirre

    1978-07-01

    This work consists in the development of an analytical method using activation by thermal neutrons for the determination of some minor elements and traces present in cassiterite (tin ore). This method was then applied to determine these elements in samples of cassiterite from different regions of Brazil. An analysis was made of the mineralogy characteristic of cassiterite as well as of the minerals most commonly associated with it. Four main types of interference were found to occur in the analysis by activation of trace elements in samples of cassiterite. The method involves the analysis without chemical separation for the determination of some elements and the analysis with chemical separation for the determination of other elements. The steps involved in both types of analysis are described. In the analysis with chemical separation the matrix element (tin) is separated by distillation in an H{sub 2}SO{sub 4}-HBr medium, after fusion of the ore with Na{sub 2}O{sub 2}. Arsine and antimony are determined in the distilled, whereas some lanthanide elements and uranium are determined in the distillation residue by separating them as a group by precipitation with lanthanum fluoride. A discussion on the precision, accuracy and sensibility of the method is also included. (author)

  2. Trace element determination study in human hair by neutron activation analysis; Estudo da determinacao de elementos traco em cabelos humanos pelo metodo de analise por ativacao com neutrons

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    Frazao, Selma Violato

    2008-07-01

    Human hair analysis studies have been subject of continuous interest due to the fact that they can be used as an important tool to evaluate trace element levels in the human body. These determinations have been carried out to use hair for environmental and occupational monitoring, to identify intoxication or poisoning by toxic metals, to assess nutritional status, to diagnose and to prevent diseases and in forensic sciences. Although hair analysis presents several advantages over other human tissue or fluid analyses, such as organ tissue, blood, urine and saliva, there are some controversies regarding the use of hair analysis data. These controversies arise from the fact that it is difficult to establish reliable reference values for trace elements in hair. The purpose of this study was to evaluate the factors that affect element concentrations in hair samples from a population considered healthy and residing in the Sao Paulo metropolitan area. The collected human head hair was cut in small pieces, washed, dried and analyzed by neutron activation analysis (NAA). Aliquots of hair samples and synthetic elemental standards were irradiated at the IEA-R1 nuclear research reactor for 16 h under a thermal neutron flux of about 5x10{sup 12} n cm{sup -2} s{sup -1} for As, Br, Ca, Co, Cr, Cs, Cu, Fe, K, La, Na, Sb, Sc, Se and Zn determinations. The induced gamma activities of the standards and samples were measured using a gamma ray spectrometer coupled to an hiperpure Ge detector. For quality control of the results, IAEA- 85 Human Hair and INCT-TL-1 Tea Leaves certified reference materials (CRMs) were analyzed. Results obtained in these CRMs presented for most of elements, good agreement with the values of the certificates (relative errors less than 10%) and good precision (variation coefficients less than 13.6%). Results of replicate hair sample analysis showed good reproducibility indicating homogeneity of the prepared sample. Results obtained in the analyses of dyed and

  3. Determination of uranium fission products interference factors in neutron activation analysis; Determinacao de fatores de interferencia de produtos de fissao de uranio na analise por ativacao neutronica

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    Ribeiro Junior, Ibere Souza

    2014-09-01

    Neutron activation analysis is a method used in the determination of several elements in different kinds of matrices. However, when the sample contains high U levels the problem of {sup 235}U fission interference occurs. A way to solve this problem is to perform the correction using the interference factor due to U fission for the radionuclides used on elemental analysis. In this study was determined the interference factor due to U fission for the radioisotopes {sup 141}Ce, {sup 143}Ce, {sup 140}La, {sup 99}Mo, {sup 147}Nd, {sup 153}Sm and {sup 95}Zr in the research nuclear reactor IEA-R1 on IPEN-CNEN/SP. These interference factors were determined experimentally, by irradiation of synthetic standards for 8 hours in a selected position in the reactor, and theoretically, determining the epithermal to neutron fluxes ratio in the same position where synthetic standards were irradiated and using reported nuclear parameters on the literature. The obtained interference factors were compared with values reported by other works. To evaluate the reliability of these factors they were applied in the analysis of studied elements in the certified reference materials NIST 8704 Buffalo River Sediment, IRMM BCR- 667 Estuarine Sediment e IAEA-SL-1 Lake Sediment. (author)

  4. Determination of essential elements in dietetic sample by neutron activation analysis; Determinacao de elementos essenciais em alimentos dieteticos pela tecnica de analise por ativacao com neutrons

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    Siquelli, Murilo V.; Maihara, Vera A. Maihara [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil). Lab. de Analise por Ativacao Neutronica]. E-mail: murilo_siquelli@hotmail.com; vmaihara@ipen.br

    2005-07-01

    In the last years there has been an increase of the dietetic product consumption by people who suffer from diabetes, heart disease and by people concerned about having a healthy life as well. Despite the increase of dietetic product presents in the diet of the Brazilian population, the use of these products is still controversial. The analysis of the nutritional composition of these products is becoming important because a great number of people is changing their traditional food by dietetic products. In the literature, there is no information about the inorganic composition, mainly related to the essential elements, in the dietetic products: diet and light . In this study are presented preliminary results of the concentrations of Br, Ca, Cr, Fe, Na and Zn determined by Instrumental Neutron Activation Analysis in aspartame, saccharin and cyclamate sodium , and stevia based sweetener samples. Gelatin samples, diet and light, were also analyzed. Methodology validation was done analyzing NIST reference materials Tea Leaves (INCT-TL-1) and Mixed Polish Herbs (INCT-MPH-2). (author)

  5. Essential and toxic element determination in edible mushrooms by neutron activation analysis; Determinacao de elementos essenciais e toxicos em cogumelos comestiveis por analise por ativacao com neutrons

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    Moura, Patricia Landim da Costa

    2008-07-01

    In this study concentrations of As, Br, Co, Cr, Cs, Fe, K, Na, Rb, Se and Zn were determined in edible mushrooms acquired from commercial establishments in the city of Sao Paulo and directly from Mogi das Cruzes, Suzano, Juquitiba and Mirandopolis producers. The analytical technique used for determining these elements in edible mushrooms was Instrumental Neutron Activation Analysis (INAA). Species of the Agaricus, Lentinus and Pleurotus genera were acquired during the period from November, 2006 to March, 2007. About 150 to 200 mg of freeze-dried mushrooms were irradiated in a neutron flux of 1012 cm{sup -2} s{sup -1} for 8 hours in the IEA-R1 nuclear research reactor at IPEN-CNEN-SP. In order to evaluate the precision and accuracy of the methodology, four reference materials: INCT-MPH-2 Mixed Polish Herbs and INCT-TL-1 Tea Leaves, NIST SRM 1577b Bovine Liver, and the material Mushroom from IAEA were analyzed. Results showed some variation in the element concentrations among the different genera. In some samples, arsenic was found but in low concentrations. Arsenic is probably derived from the contamination from pesticides used in the cultivation, in their the substrates where mushrooms uptake their nutrients. Although there are element concentration variations, mushrooms can still be considered a very rich nutritional source, mainly because of their low concentrations of Na, and due to the good source of K, Fe and Zn. (author)

  6. Determination of essential elements in edible seaweed by neutron activation analysis; Determinacao de elementos essenciais em algas marinhas comestiveis por analise por ativacao neutronica

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    Alves, Cassio Bessa Lima; Maihara, Vera Akiko, E-mail: cassio_man@hotmail.com, E-mail: vmaihara@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2013-07-01

    Comestible marine algae are gaining wider global trade, not only because of the taste but also the nutritional quality they present. They are rich in protein, fiber, vitamins and are excellent sources of essential elements due to their ability to absorb substances storing them in their bodies. its chemical composition varies according to the species, habitat, maturity and environmental conditions which are submitted. The method of Neutron Activation Analysis was used to determine the essential elements Cl, K, Mg, Mn and Na present in marine algae from different countries, which are sold in the city of Sao Paulo. A total of 6 samples of marine algae were analyzed, 4 species of Nori (Porphyra umbilicates) from China, Korea, Japan and USA; 1 of Hijiki (Hijikia fusiforme) species from Japan; and 1 species of Kombu (Laminaria sp.) of South Korea. To validate the methodology used was the reference material NIST SRM 1577b Bovine Liver. The concentrations range from 5265-1175 μg/g to CL; from 14413-90261 μg/g to K; from 3007-7091 μg/g to Mg; from 2,3-33,8 μg/g to Mn and from 5161-24973 μg/g to Na.

  7. Rare-earth and thorium in soil and manioc: determination using neutron activation analysis; Terras-raras e torio em solo e mandioca: determinacao por ativacao neutronica

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    Silva, Lucilene Guerra e [Minas Gerais Univ., Belo Horizonte, MG (Brazil). Faculdade de Farmacia; Menezes, Maria Angela de B.C.; Palmieri, Helena E.L. [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN), Belo Horizonte, MG (Brazil). Servico de Reator e Irradiacoes]. E-mail: menezes@cdtn.br; Nalini Junior, Herminio A. [Ouro Preto Univ., MG (Brazil). Dept. de Geologia; Jacimivic, Radojko [Instituto Josef Stefan, Liubliana (Slovenia). Dept. de Ciencias Ambientais

    2005-07-01

    This paper reports the elements rare-earth and Thorium determined in soil and manioc during an assessment carried out to evaluate the elemental concentration in several matrixes connected with the chain food. One site studied is in the Iron Quadrangle, Minas Gerais, Brazil, that presented mineral exploration activity in the past. Another site is without any mining activity and it is outside the Quadrangle. The objective was to evaluate the influence of a mining activity on the elemental concentration in the soil and manioc is grown around the mining area. The elemental determination was achieved by applying the k{sub 0}-instrumental Neutron Activation. (author)

  8. Simultaneous determination of minerals in different varieties of forage by neutron activation analysis; Analise por ativacao com neutrons aplicada para a determinacao simultanea de minerais em diferentes especies de forrageira

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    Armelin, Maria Jose A.; Piasentin, Ricardo M.; Souza, Marcos P. de [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil). Supervisao de Radioquimica; Cruvinel, Paulo E. [Empresa Brasileira de Pesquisa Agropecuaria, Sao Carlos, SP (Brazil). Centro Nacional de Pesquisa e Desenvolvimento de Instrumentacao Agropecuaria

    1996-07-01

    Six varieties of forages were analyzed by instrumental neutron activation analysis. The experimental conditions allowed the determination of Ca(5); K(%); Mg ({mu}g/g); Mn({mu}g/g); Ti({mu}g/g) and V(ng/g) in 30 minutes, approximately. The accuracy of the method was evaluated by means of reference material analysis. The precision of the results was lower than 10%, except for Ti and some cases for Na was near 20%. (author)

  9. Comparative study between the PIXE technique and neutron activation analysis for Zinc determination; Estudo comparativo entre a tecnica de inducao de raios X por particulas e analise por ativacao com neutrons na determinacao do metal pesado zinco

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    Cruvinel, Paulo Estevao; Crestana, Silvio [Empresa Brasileira de Pesquisa Agropecuaria, Sao Carlos, SP (Brazil). CNPDIA. E-mail: cruvinel@cnpdia.embrapa.br; Armelin, Maria Jose Aguirre [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil); Artaxo Netto, Paulo Eduardo [Sao Paulo Univ., SP (Brazil). Inst. de Fisica

    1997-07-01

    This work presents a comparative study between the PIXE, proton beams and neutron activation analysis (NAA) techniques, for determination of total zinc concentration. Particularly, soil samples from the Pindorama, Instituto Agronomico de Campinas, Sao Paulo State, Brazil, experimental station have been analysed and measuring the zinc contents in {mu}g/g. The results presented good correlation between the mentioned techniques. The PIXE and NAA analyses have been carried out by using the series S, 2.4 MeV proton beams Pelletron accelerator and the IPEN/CNEN-IEA-R1 reactor, both installed at the Sao Paulo - Brazil university.

  10. Drawing up of a procedure for vanadium determination in mussels using the neutron activation analysis method; Estabelecimento de procedimento para determinacao de vanadio em mexilhoes pelo metodo de analise por ativacao com neutrons

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    Seo, Daniele, E-mail: danyseo@uol.com.b [Universidade Presbiteriana Mackenzie, Sao Paulo, SP (Brazil). Centro de Ciencias Biologicas e da Saude; Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil); Vasconcellos, Marina B.A.; Saiki, Mitiko; Catharino, Marilia G.M.; Moreira, Edson G., E-mail: mbvascon@ipen.b, E-mail: mitiko@ipen.b, E-mail: mgcatharino@uol.com.b, E-mail: emoreira@ipen.b [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil); Sousa, Eduinetty C.P.M. de; Pereira, Camilo D.S., E-mail: edvinett@usp.b, E-mail: camilo.pereira@usp.b [Universidade de Sao Paulo (IO/USP), SP (Brazil). Inst. Oceanografico. Lab. de Ecotoxicologia Marinha

    2009-07-01

    This work establishes an adequate procedure for obtaining reliable results for determination of vanadium in mussels, leg by leg by the neutron activation analysis (NAA), viewing the posterior application on the bio monitoring the coastal pollution, particularly near the petroleum terminals.For the evaluation of result quality concerning to the quality of those results, the work analysed the reference material certification NIST SRM 1566b Oyster Tissue. The precision of the results were also analysed using repetitions of mussel samples collected at the coastal of northern Sao Paulo state, Brazil. The NAA procedure consisted of 200 mg of sample and a synthetic standard of vanadium during a period of 8 s and under a thermal neutron flux of 6.6 x 10{sup 12} n cm{sup -2} s{sup -1} at the pneumatic station 4 of the IEA-R1 nuclear reactor of IPEN-CNEN/SP. After a 3 min decay, the measurements of the gamma activities of the sample and the standard were done using a Ge hyper pure semi-conductor detector, connected to gamma ray multichannel analyser. The vanadium were determined by the measurement of the gamma activity of the {sup 52}V through the 1434.08 keV peak, and half-life time of 3.75 min. The concentration of V were calculated by the comparative method. The obtained results indicated the viability of the NAA procedure established for the determination of vanadium in mussels

  11. Determination of rare earth and uranium in reference biological materials certified by the method of neutron activation analysis; Determinacao de terras raras e de uranio em materiais biologicos de referencia certificados pelo metodo de analise por ativacao com neutrons

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    Pereira, Lais H.P.; Saiki, Mitiko, E-mail: laispaciulli@gmail.com, E-mail: mitiko@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2013-07-01

    The objective of this study was to evaluate the precision and accuracy of the determinations of Sc, La, Ce, Nd, Sm, Eu, Tb, Yb, Lu and U in certified reference materials (CRMs). To solve the problem of interference from fission products of U in the determination of lanthanides were obtained correction factors for this interference for {sup 140}La, {sup 141}Ce, {sup 143}Ce, {sup 153}Sm and {sup 147}Nd. The experimental procedure of Neutron Activation Analysis consisted of irradiating aliquots of each of the CRMs with synthetic standards of elements under thermal neutron flux of the IEA-R1 nuclear reactor, followed by gamma-ray spectrometry using a high-resolution hyperpurity GE detector. The analyzes of CRMs indicate good accuracy and precision of results, demonstrating the feasibility of applying of established procedure in NAA of elements studied in organic vegetable matrices.

  12. Application of neutron activation analysis for the determination of essential elements in egg samples; Aplicacao da analise por ativacao com neutrons para a determinacao de elementos essenciais em amostras de ovos

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    Gomes, Bruna G.; Maihara, Vera A.; Avegliano, Roseane P., E-mail: brunagabrielegomes@gmail.com, E-mail: vmaihara@ipen.br, E-mail: pagliaro@usp.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2013-07-01

    The eggs are among the twenty foods consumed by the population of the five major regions of Brazil. Among the types of eggs, there are differences in nutritional value, which can vary according to the food of the bird. This study evaluating the elements Cl, K, Mg, Mn and Na considered essential micronutrients in food, because they are fundamental in several metabolic processes necessary for the maintenance and training of the human body. We analyzed three types of eggs: egg whites, of the quail, and the colonial in cooked and raw form, using the Instrumental Neutron Activation Analysis method (INAA). The egg samples were lyophilized and pulverized before analysis. To validate the methodology, reference materials NIST RM 8415 Whole Egg Powder and NIST SRM 1567 Wheat Flour were analyzed. The samples, reference materials and standards of the elements were irradiated for 20 seconds under a thermal neutron flux of 6,6x10{sup 12} cm -2 s -1 in the nuclear research reactor IEA-R1 of IPEN-CNEN / SP. The results were consistent with the values of the Brazilian Table of Food Composition (TACO)

  13. Determination of essential and toxic elements in commercial baby foods by instrumental neutron activation analysis and atomic absorption spectrometry; Determinacao dos elementos essenciais e toxicos em alimentos comerciais infantis por analise por ativacao com neutrons e espectrometria de absorcao atomica

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    Vallinoto, Priscila

    2013-08-01

    The World Health Organization recommends that infants should be breast fed exclusively for at least six months after birth. After this period, it is recommended to start introducing complementary foods, in order to meet the child's nutritional, mineral and energy needs. Commercial food products for infants form an important part of the diet for many babies. Thus, it is very important that such food contains sufficient amounts of minerals. Inadequate complementary feeding is a major cause of high rates of infant malnutrition in developing countries. In this study, essential elements: Ca, Cl, Co, Cr, Fe, K, Mg, Mn, Na, Se and Zn and toxic elements: As, Cd, Hg levels were determined in twenty seven different commercial infant food product samples by Instrumental Neutron Activation Analysis (INAA) and Atomic Absorption Spectrometry (AAS). In order to validate both methodologies the reference material: INCT MPH-2 Mixed Polish Herbs and NIST - SRM 1577b Bovine Liver by INAA and NIST - SRM 1548th Typical Diet and NIST - SRM 1547 Peach Leaves by AAS were analyzed. The twenty seven baby food samples were acquired from Sao Paulo city supermarkets and stores. Essential and toxic elements were determined. Most of the essential element concentrations obtained were lower than the World Health Organization requirements, while concentrations of toxic elements were below the tolerable upper limit. These low essential element concentrations in these samples indicate that infants should not be fed only with commercial complementary foods. (author)

  14. Neutron activation analysis for determining of inorganic trace elements in by-products of soybean, cotton, corn, wheat, sorghum and rice; Aplicacao da analise por ativacao com neutrons para determinacao de elementos inorganicos em subprodutos da soja, algodao, milho, trigo, sorgo e arroz

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    Teruya, Carla M.; Armelin, Maria Jose [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil); Silva Filho, Jose Cleto [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil). Ciencias Animais; Silva, Aliomar G. [Empresa Brasileira de Pesquisa Agropecuaria (EMBRAPA), Sao Carlos, SP (Brazil). Centro de Pesquisa de Pecuaria do Sudeste

    1999-11-01

    In the present paper the instrumental neutron activation analysis was applied to determine some essential and toxic elements in six agroindustrial by-products utilized to feed animal. The accuracy of the method was evaluated by means of reference material analysis. In general, the precision of the method was lower than 10% and the accuracy near to 5%. (author) 7 refs., 1 tab.

  15. Determination of active oxygen content in rare earth peroxides; Determinacao de oxigenio ativo em peroxidos de terras raras

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    Queiroz, Carlos A.S.; Abrao, Alcidio

    1993-12-31

    The content of active oxygen in rare earth peroxides have been determined after the dissolution of the samples with hydrocloridic acid in the presence of potassium iodide. The free generated iodine is titrated with sodium thiosulfate using starch as indicator. The oxidation of iodide to the free iodine indicates the presence of a higher valence state rare earth oxide, until now specifically recognized for the oxides of cerium (Ce O{sub 2}), praseodymium (Pr{sub 6} O{sub 1}1) and terbium (TB{sub 4} O{sub 7}). recently the authors synthesized a new series of rare earth compounds, the peroxides. These new compounds were prepared by precipitating the rare earth elements complexed with carbonate ion by addition of hydrogen peroxide. the authors demonstrated that all rare earth elements, once solubilized by complexing with carbonate ion, are quantitatively precipitated as peroxide by addition of hydrogen peroxide. (author) 3 refs., 1 tab.

  16. Application of instrumental neutron activation analysis for determining As, Br, K, La, Mn, Na and Sm in samples of pine wood; Aplicacao da analise por ativacao neutronica instrumental para determinacao de As, Br, K, La, Mn, Na e Sm em amostras de madeiras de Pinus

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    Oliveira, Helder de; Fernandes, Elisabete A. de Nadai; Bacchi, Marcio Arruda; Tagliaferro, Fabio Sileno [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil); Sarries, Gabriel Adrian [Sao Paulo Univ., Piracicaba, SP (Brazil). Escola Superior de Agricultura Luiz de Queiroz

    1999-11-01

    Multi-elementary and considered non destructive, the neutron activation analysis is a technique that allows simultaneous and instrumental determination of several elements, becoming especially useful when it is fundamental the knowledge of the total chemical composition, as in the certification of reference materials, application in geochemistry, analyses of aerosols, determination of origin of materials, forensic analyzes and of environmental pollution. However, the dependence of reactors, or other neutrons sources, the generation of radioactive material and the time waiting needed for some determinations are the main barriers pointed int he application of that technique. The present work aimed at establishing the best conditions for the detection of elements of short half-life Br, K, La, Mn, Na and Sm in samples of wood of Pinus, because the reactor used is located distant of the laboratory where the measures of the induced radioactivity are made, to determine trace elements that possess half-lives smaller than two days. For such, suitable equations, using the Surface of Response technique in the SAS software, to minimize the uncertainties of detection of the photopeak function of the elementary concentration and as a decay time.(author) 6 refs., 3 figs., 11 tabs.

  17. Determination of Hg and other elements in fish and plant samples from Amazonic region, by neutron activation analysis; Determinacao de Hg e outros elementos de interesse em amostras de peixes e plantas da regiao amazonica, por analise por ativacao com neutrons

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    Favaro, Debora I.T.; Vasconcellos, Marina B.A. [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil). Supervisao de Radioquimica; Fostier, Anne Helene [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil). Lab. de Quimica Analitica

    1996-07-01

    In the present work the region of Serra do Navio, Amapa State, was chosen to asses the Hg contamination due to gold mining activities. As part of monitoring of this region, fishes and plants were collected and analysed by instrumental neutron activation (INAA). Through this method it was possible to determine the concentration of the elements: As, Ca, Cr, Co, Fe, Hg, Rb, Sb, Se and Zn in fishes and Ca, Co, Cr, Fe, Hg, La, Na, Rb, Sb, Sc, Se and Zn in plants. Mercury concentrations found in fishes ranged from 0.64 to 1.11 {mu}/g and from 0.83 to 0.15 {mu}g/g in plants. These results were compared with those obtained by the atomic absorption technique and they agreed well. The accuracy and precision of the INAA method were checked by means of analyses of reference materials. (author)

  18. Multielementar determination by neutron activation in sediment samples from Tartarugalzinho region, Amapa State, Brazil; Determinacao multielementar em amostras de sedimentos da regiao do Tartarugalzinho, Amapa, por ativacao neutronica

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    Neri, Maria C.; Favaro, Debora I.T.; Vasconcellos, Marina B.A. [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil); Oliveira, Sonia M.B. de; Melfi, Adolfo J. [Sao Paulo Univ., SP (Brazil). Inst. de Geociencias; Fostier, Anne H. [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil). Lab. de Quimica Analitica; Guimaraes, Jean R.D. [Universidade Federal, Rio de Janeiro, RJ (Brazil). Inst. de Biofisica; Forti, Maria C. [Instituto Nacional de Pesquisas Espaciais (INPE), Sao Jose dos Campos, SP (Brazil)

    1999-11-01

    In the present work, sediment samples collected in the Tartarugalzinho region, State of Amapa, were analyzed by instrumental neutron activation analysis. The concentration of the elements As, Ba, Br, Co, Cr, Cs, Fe, Na, Rb, Sc, Se, Ta, Th, U, Zn and Zr and the rare earth elements Ce, Eu, La, Lu, Nd, Sm, Tb and Yb could be determined. Analysis of the reference materials Buffalo River Sediment (NIST SRM 2704) and Soil 7 (IAEA) showed the accuracy and precision of the method. (author) 4 refs., 1 fig., 7 tabs.

  19. Determination of micro minerals in phosphorus source fed to animals by activation with neutrons; Determinacao de microminerais em fontes de fosforo fornecidas a animais por ativacao com neutrons

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    Armelin, Maria Jose A.; Mori, Clara S. [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil); Silva, Jose Cleto da [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil)

    1995-12-31

    Instrumental neutron activation analysis was applied to determine the elements Ca, Co, Cr, Cu, Eu, Fe, K, La, Mg, Mn, Na, P, Sb, Sc and Zn in four phosphatic supplementation samples. analysis of variance, Turkey`s and Sheffe`s test were applied to certify the homogeneity of the sub-samples (200 mg). In general, the precision of the method was lower than 15%. The phosphatic supplementation samples analyzed can be considered adequate to feed into animals in relation to mineral composition. (author). 5 refs., 2 tabs.

  20. Application of neutron activation analysis to the determination of total mercury and other elements of interest in soil and sediment samples from Serra do Navio and Vila Nova River Basin, Amapa, Brazil; Aplicacao do metodo de ativacao neutronica a determinacao do mercurio total e outros elementos de interesse em amostras de solo e sedimento da Serra do Navio e Bacia do Rio Vila Nova, Amapa

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    Goncalves, Cristina

    1997-07-01

    In this work it is presented a survey on total mercury determination by a radiochemical method in sediment and soil samples from two regions, in the state of Amapa: Serra do Navio (background area) and Vila Nova river basin (gold mining area). The method consisted in leaching of the irradiated samples with acqua regia in a Parr bomb, and heating in microwave oven, for one minute. Then the solvent extraction technique was applied, using bismuth diethyldithiocarbamate (Bi(DDC){sub 3}) as extractant agent. The organic phase, containing {sup 197}Hg and {sup 203}Hg radioisotopes, was measured in a gamma spectrometer with hyper pure Ge detector. This method eliminated the interference of the 279.54 keV photopeak of {sup 75}Se on 279.2 keV photopeak of {sup 203}Hg, besides improving counting statistics of both Hg radioisotopes. The elements As, Ba, Br, Ce, Co, Cr, Cs, Eu, Fe, Hf, Ho, K, La, Lu, Mg, Mn, Na, Nd, Rb, Sb, Sc, Se, Sm, Ta, Tb, Th, Ti, U, V, W, Yb, Zn and Zr were also determined by the instrumental neutron activation analysis. Two irradiation series were carried out to quantify these elements in soil and sediment samples; a short term irradiation allowed to evaluate Mg, Mn, Na, Ti and V levels, and by long term irradiation, the other elements were determined. Precision and accuracy of radiochemical procedure were verified by means of analysis of the reference materials Buffalo River Sediment and Lake Sediment, for sediments and GXR-5, for soils. For the instrumental analysis, the reference materials Buffalo River Sediment, Soil 7, JB-1 and Oyster Tissue were used. The samples were also submitted to X ray diffraction, in Instituto de Geoscience-USP, to observe mercury behaviour with mineralogy. Aluminium concentration was determined by X ray fluorescence method, in the Department of Materials, IPEN/CNEN-SP, making possible enrichment factor calculation so that mercurial contamination in the gold mining area (Vila Nova river basin) could be evaluated. The mercury

  1. Mineral water {sup 222} Rn activity decrease due to consumption habits; Determinacao do decrescimo da atividade de radonio-222 em aguas minerais simulando habitos de consumo

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    Cipriani, Moacir; Taddei, Maria Helena Tirollo; Silva, Nivaldo Carlos da [Comissao Nacional de Energia Nuclear (CNEN), Pocos de Caldas, MG (Brazil). Laboratorio

    2001-07-01

    Mineral waters from the Pocos de Caldas Plateau springs, an elevated region with high natural radioactivity, in the State of Minas Gerais, Brazil, have significant {sup 222} Rn concentration on site. The highest concentration in the waters are from: Fonte Villela - Aguas da Prata ({approx} 1000 Bql{sup -1}); Fonte Grande Hotel - Pocinhos do Rio Verde ({approx} 400 Brq{sup -1}) and Fonte CNEN Lab - Pocos de Caldas ({approx} 290 Bql{sup -1}). These waters are used by the population as drinking water and due to consumption habits, can lead to internal doses above accepted limits for the public. This work deals with the decrease of {sup 222} Rn activity in mineral waters fro two different popular consumption habits, and with the adult effective dose equivalent reduction due to water consumption habits. It has been found that the estimated dose based on the biokinetic Crawford-Brown model, can be one fourth of dose based on {sup 222} Rn activity on site. (author)

  2. Activation analysis

    International Nuclear Information System (INIS)

    The neutron activation analysis, which appears to be in limits for further advance, is the most suitable for providing information on the principal as well as the microcomponents in any sample of solid form. Then, instrumental activation analysis is capable of determination of far many elements in various samples. Principally on the neutron activation analysis, the following are described in literature survey from 1982 to middle 1984: bibliography, review, data collection, etc.; problems in spectral analysis and measurement; activation analysis with neutrons; charged particle and photo-nucleus reactions; chemical separation, isotopic dilution activation analysis; molecular activation analysis; standard materials; life and its relation samples; environmental, food, court trial and archaeological samples; space and earth sciences. (Mori, K.)

  3. Determination of trace elements in Mesozoic dykes of the Serra do Mar by neutron activation; Determinacao de elementos tracos em diques mesozoicos da Serra do Mar por meio de ativacao com neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Vicentini, Caio M.; Marques, Leila S., E-mail: caio.vicentini@usp.br, E-mail: leila@iag.usp.br [Universidade de Sao Paulo (IAG/USP), Sao Paulo, SP (Brazil). Instituto de Astronomia, Geofisica e Ciencias Atmosfericas; Figueiredo, Ana Maria G., E-mail: anamaria@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2013-07-01

    The analysis of trace elements such as rare earths, Th, U, Ta, Hf, Ba, Rb and Ba, is a very important tool for petrogenetic studies. In order to study these processes in dykes of Enxame Serra do Mar (Coast of Sao Paulo and Rio de Janeiro), belonging to the Parana Magmatic Province (PMP), one of the most significant provinces of continental basalts in the world, were perform analyzes by neutron activation in these dikes. The technique, employed in Centro de Reator de Pesquisa of the Instituto de Pesquisas Energeticas e Nucleares, provided concentrations of trace elements with accuracy levels of 10% and 9%, which are suitable for petrogenetic studies. Due to the low concentrations of the elements analyzed, the experimental routine sample preparation processes covered very careful to avoid contamination. The samples investigated can be divided into four groups: basic rocks (SiO{sub 2} <55%) with Ti / Y> 500; basic rocks with Ti / Y <500; intermediate rocks (55% 63%). Dikes of intermediate and acid composition only occur at the Sao Sebastiao Island and adjacent coastal region. The concentrations of major and minor elements, as well as the abundance patterns of rare earths and other incompatible elements of these more differentiated rocks, show significant similarities with the type of the volcanic Chapeco, suggesting similar genesis, in other worlds, including also processes of crustal contamination.

  4. In vivo determination of the {sup 99m}Tc-MDP incorporated activity in bone tissue; Determinacao in vivo da atividade incorporada de {sup 99m} Tc-MDP no tecido osseo

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Joseane Fonseca; Braga, Francisco J.H.N. [Sao Paulo Univ., Ribeirao Preto, SP (Brazil). Faculdade de Filosofia, Ciencias e Letras. Dept. de Fisica e Matematica; Dantas, Bernardo M.; Bertelli, Luiz [Instituto de Radioprotecao e Dosimetria (IRD), Rio de Janeiro, RJ (Brazil); Ghilardi Netto, Thomaz [Sao Paulo Univ., Ribeirao Preto, SP (Brazil). Faculdade de Medicina. Centro de Ciencias da Imagem e Fisica Medica

    1998-07-01

    For determining in vivo {sup 99m}Tc-MDP incorporated activity in bone tissue using a scintillation chamber as a image detection and acquisition system it is necessary the system calibration using an anthropomorphic physical simulator. The development of a tibia and fibula simulator in order to estimate bone tissue activity is presented. This procedure can be used either for workers monitoring or for the metabolic behavior of this radiopharmaceutical.

  5. Impregnation of 12-tungstophosphoric acid on silica - part I: determination of impregnation parameters, characterization and evaluation of catalytic activity; Impregnacao do acido 12-fosfotungstico em silica - parte I: determinacao de parametros de impregnacao, caracterizacao e avaliacao da atividade catalitica

    Energy Technology Data Exchange (ETDEWEB)

    Scroccaro, Karine Isabel; Tanobe, Valcineide Oliveira de Andrade; Cocco, Lilian Cristina; Yamamoto, Carlos Itsuo, E-mail: karineisabel@yahoo.com.br [Universidade Federal do Parana, Curitiba, PR (Brazil). Centro Politecnico. Dept. de Engenharia Quimica; Wypych, Fernando [Universidade Federal do Parana, Curitiba, PR (Brazil). Centro Politecnico. Dept. de Quimica

    2012-07-01

    Catalyst based on Kegging-type heteropolyacids (H{sub 3}PW{sub 12}O{sub 40} - HPA), supported on SiO{sub 2} (H{sub 3}PW), were prepared by the impregnation method under different thermal treatment conditions. The materials were characterized by different instrumental techniques and used as catalysts in the methyl esterification reactions of stearic acid. Using the catalyst with 15% of HPA, conversions higher than 60% were obtained after 2 h of reaction at 65 deg C. Recovery studies using hot-filtration with ethanol at 75 deg C showed satisfactory activity for two additional reaction cycles. (author)

  6. Determining internal movement costs at a warehouse using activity-based costing: offshore petroleum production application; Determinacao dos custos de movimentacao interna de um deposito utilizando a metodologia de custeio baseado em atividades: aplicacao a producao de petroleo offshore

    Energy Technology Data Exchange (ETDEWEB)

    Azevedo, Italo Ricardo Moreira de [Brasil Supply S.A., Vitoria, ES (Brazil); Leal, Jose Eugenio [Pontificia Univ. Catolica do Rio de Janeiro (PUC-Rio), RJ (Brazil)

    2004-07-01

    As from the flexibilization of the petroleum monopoly, which took place in the second half of the 1990's, the petroleum and gas sector in Brazil has undergone a series of changes that have directly impacted the commercial relations among the companies in the sector. The increases in operational efficiency and reduction of costs have become basic factors for the companies wishing to compete in this market. This paper presents a study whose objective is to map, model, and determine the costs involved in the process for internal movement in a warehouse used as logistics support to offshore petroleum production. Based on the description of the internal movement process for product storage, the main resources are identified. Then, a mathematical model based on Activity-Based Costing is draw up, in which the results generated comprise the values for internal movement costs for each type of product moved in the warehouse. (author)

  7. Absolute activity measurement and gamma-ray emission probability for decay of I-126; Medida absoluta da atividade e determinacao da taxa de emissao gama por decaimento do {sup 126} I

    Energy Technology Data Exchange (ETDEWEB)

    Fonseca, Katia Aparecida

    1997-07-01

    The accurate knowledge of the gamma-ray emission probability per decay of radionuclides is important in several applications. In the case of {sup 126} I, its importance lies mainly in fast neutron dosimetry as well as in the production of {sup 125} I where {sup 126} I appears as an impurity. In the present work the gamma-ray emission probabilities per decay for the 388 and 666-KeV transitions of {sup 126} I have been measured. This radionuclide was obtained by means of the {sup 127} I(n, 2n){sup 126} I reaction in a fast neutron flux at the IPEN 2 MW research reactor. The methodology for the primary standardization of {sup 126} I is described. For this purpose, two different coincidence systems were used due to the complex decay scheme of this radionuclide. The {beta}branch measurement was carried out in a 4 {pi}(PC){beta}-{gamma} coincidence system consisting of a proportional counter, coupled to a pair of 3'x3' Na I (Tl) crystal. The electron capture branch was measured in a X-{gamma} coincidence system using two NaI(Tl) crystals. The gamma-ray measurements were performed in a HPGe system, previously calibrated by means of standard sources supplied by the International Atomic Energy Agency. All the uncertainties evolved were treated rigorously, by means of covariance analysis. (author)

  8. Determination of total alpha and beta activity in water for human consumption by LSC(Liquid Scintillation Counter); Determinacao de atividades alfa e beta total em agua para consumo humano por LSC (Contador de Cintilacao Liquida))

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2013-07-01

    The Ordinance Brazilian of Ministry of Health (MS 2914/2011) establishes the standards for quality of water intended for human consumption, being limits values of 5.0 Bq/L for gross alpha, and 1.0 Bq/L for gross beta radioactivity. The liquid scintillation spectrometry (LSC) technique has been presented as an alternative to conventional procedure using gas flow proportional counter. The present work shows a review of the methods for determination of gross alpha and gross beta in water by using LSC. Between the factors that influence the accuracy and repeatability of the analytical results we can highlight: thermal preconcentration, type of the acid and calibration standard. A procedure was established and carried out to samples of the National Program of Intercomparison of Radionuclides in Environmental Samples for evaluation of its performance. The gross alpha and gross beta analysis in samples of the public water supplies in the Metropolitan Region of Goiania, state of Goias was carried out. The results are consistent with the guideline values form the Ministry of Health concerning radioactivity. (author)

  9. Analysis of oil content in sunflower seeds with nuclear magnetic ressonance and `SOXHLET` methods; Determinacao do teor de oleo em sementes de girassol pelos metodos de ressonancia magnetica nuclear e soxhlet

    Energy Technology Data Exchange (ETDEWEB)

    Ungaro, Maria Regina Goncalves [Instituto Agronomico de Campinas, SP (Brazil). Secao de Oleaginosas; Toledo, Nilva Maria Prestes de [Instituto Agronomico de Campinas, SP (Brazil). Secao Tecnica Experimental e Calculo; Teixeira, Joao Paulo Feijao [Instituto Agronomico de Campinas, SP (Brazil). Secao de Fitoquimica; Suassuna Filho, Jose [Universidade Estadual de Campinas (UNICAMP), Campinas, SP (Brazil). Dept.de Fisica

    1992-12-31

    Individual and group of seeds of some sunflower populations were utilized in order to evaluate the feasibility of oil content evaluations by the Nuclear Magnetic Resonance method (NMR). Correlation analysis with the extractive method (Soxhlet) was performed. The results showed that: the oil in the seeds behaved like a liquid in the NMR analysis; there was a high and positive correlation (r = 0,93) between NMR and Soxhlet; there was no correlation between seed weight and oil content; the observed variability in oil content among seeds of a plant were higher than between plants of a population; these values indicate the importance of making individual analysis of oil content by the NMR method for the sunflower breeding for oil content. (author) 7 refs., 2 figs., 4 tabs.

  10. Forensic activation analysis

    International Nuclear Information System (INIS)

    Basic principles of neutron activation analysis are outlined. Examples of its use in police science include analysis for gunshot residues, toxic element determinations and multielement comparisons. Advantages of neutron activation analysis over other techniques are described. (R.L.)

  11. Neutron Activation Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Corliss, William R.

    1968-01-01

    In activation analysis, a sample of an unknown material is first irradiated (activated) with nuclear particles. In practice these nuclear particles are almost always neutrons. The success of activation analysis depends upon nuclear reactions which are completely independent of an atom's chemical associations. The value of activation analysis as a research tool was recognized almost immediately upon the discovery of artificial radioactivity. This book discusses activation analysis experiments, applications and technical considerations.

  12. 13. seminar 'Activation analysis'

    International Nuclear Information System (INIS)

    Collection of the abstracts of contributions to the seminar covering broad ranges of application of activation analysis and improvements of systems and process steps. Most of them have been prepared separately for the energy data bases. (RB)

  13. Activation analysis in Greece

    International Nuclear Information System (INIS)

    A review of research and development on NAA as well as examples of applications of this method are presented, taken from work carried out over the last 21 years at the Radioanalytical Laboratory of the Department of Chemistry in the Greek Nuclear Research Center ''Demokritos''. Improved and faster radiochemical NAA methods have been developed for the determination of Au, Ni, Cl, As, Cu, U, Cr, Eu, Hg and Mo in several materials, for the simultaneous determination of Br and I; Mg, Sr and Ni; As and Cu; As, Sb and Hg; Mn, Sr and Ba; Cd and Zn; Se and As; Mo and Cr in biological materials. Instrumental NAA methods have also been developed for the determination of Ag, Cl and Na in lake waters, Al, Ca, Mg and V in wines, 7 trace elements in biological materials, 17 trace elements in sediments and 20 minor and trace elements in ceramics. A comprehensive computer program for routine activation analysis using Ge(Li) detectors have been worked out. A rather extended charged-particle activation analysis program is carried out for the last 10 years, including particle induced X-ray emission (PIXE) analysis, particle induced prompt gamma-ray emission analysis (PIGE), other nuclear reactions and proton activation analysis. A special neutron activation method, the delayed fission neutron counting method is used for the analysis of fissionable elements, as U, Th, Pu, in samples of the whole nuclear fuel cycle including geological, enriched and nuclear safeguards samples

  14. Forensic Activation Analysis

    International Nuclear Information System (INIS)

    The high sensitivity of high-flux (reactor) thermal-neutron activation analysis (NAA) for the detection and quantitative measurement of a large number of elements has led, in recent years, to a considerable degree of application of the method in the area of scientific crime investigation (criminalistics). Thus, in a Forensic Activation Analysis Bibliography recently compiled by the author, some 135 publications in this field are listed - and more are appearing quite rapidly. The nondestructive character of the purely-instrumental form of the method is an added advantage in forensic work, since evidence samples involved in actual criminal cases are not destroyed during analysis, but are preserved intact for possible presentation in court. Quite aside from, or in addition to, use in court, NAA results can be very helpful in the investigative stage of particular criminal cases. The ultra sensitivity of the method often enables one to analyze evidence specimens that are too tiny for meaningful analysis by more conventional elemental analysis methods. Also, this high sensitivity often enables one to characterize, or individualize, evidence specimens as to the possibility of common origin - via the principle of multi-element trace-constituent characterization

  15. Study on activation analysis

    International Nuclear Information System (INIS)

    High purity aluminum has been analyzed by neutron activation analysis. The determination of copper contents is aluminum has been used to evaluate its purity level. A new sensitive method has been developed by using graphite thermal column to reduce or eliminate the interference of 24Na which is generated from 27Al (n,α) 24Na reaction by fast neutron. Influence for activity of 24Na due to above reaction is found to be between 2.3 - 2.8 %. Copper contents in the high purity aluminum come out 0.542±0.084 ppm. In addition, contents of 23 other impurity elements (<0.1 - 0.01 ppm) are measured using general method after detection limit and optimum conditions are established. (author)

  16. Activation analysis in forensic studies

    International Nuclear Information System (INIS)

    Application of neutron activation analysis in forensics are grouped into 3 categories: firearms-discharge applications, elemental analysis of other nonbiological evidence materials (paint, other), and elemental analysis of biological evidence materials (multielemental analysis of hair, analysis of hair for As and Hg). 18 refs

  17. Determination of metals and rare earths in leach solution of phosphogypsum by instrumental neutron activation analysis (INAA); Determinacao de metais e terras raras em solucao lixiviada de fosfogesso por AANI

    Energy Technology Data Exchange (ETDEWEB)

    Costa, Gabriela J.L., E-mail: glcosta@ipen.br [Universidade Nove de Julho, Sao Paulo, SP (Brazil); Saueia, Catia H.R.; Mazzilli, Barbara P., E-mail: chsaueia@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2011-07-01

    The phosphogypsum is a sub-product of the fertilizer industries and is composed of the gypsum matrix (CaSO{sub 4}.2H{sub 2}O) which naturally contains high tenors of impurities such as 2P{sub O}5 and metals coming from the original phosphat rock. The Brazilian phosphogypsum and the various uses has been researched through his elementary and radiochemistry characterization. This work determine the metals (As, Ba, Co and Se) and rare earths (La, Ce, Sm, Eu, Tb and Lu) presents in samples of phosphogypsum leach solutions

  18. Analysis of Precision of Activation Analysis Method

    DEFF Research Database (Denmark)

    Heydorn, Kaj; Nørgaard, K.

    1973-01-01

    The precision of an activation-analysis method prescribes the estimation of the precision of a single analytical result. The adequacy of these estimates to account for the observed variation between duplicate results from the analysis of different samples and materials, is tested by the statistic T...

  19. Determination of scaling factors to estimate the radionuclide inventory in waste with low and intermediate-level activity from the IEA-R1 reactor; Determinacao de fatores de escala para estimativa do inventario de radionuclideos em rejeitos de media e baixa atividades do reator IEA-R1

    Energy Technology Data Exchange (ETDEWEB)

    Taddei, Maria Helena Tirollo

    2013-07-01

    Regulations regarding transfer and final disposal of radioactive waste require that the inventory of radionuclides for each container enclosing such waste must be estimated and declared. The regulatory limits are established as a function of the annual radiation doses that members of the public could be exposed to from the radioactive waste repository, which mainly depend on the activity concentration of radionuclides, given in Bq/g, found in each waste container. Most of the radionuclides that emit gamma-rays can have their activity concentrations determined straightforwardly by measurements carried out externally to the containers. However, radionuclides that emit exclusively alpha or beta particles, as well as gamma-rays or X-rays with low energy and low absolute emission intensity, or whose activity is very low among the radioactive waste, are generically designated as Difficult to Measure Nuclides (DTMs). The activity concentrations of these DTMs are determined by means of complex radiochemical procedures that involve isolating the chemical species being studied from the interference in the waste matrix. Moreover, samples must be collected from each container in order to perform the analyses inherent to the radiochemical procedures, which exposes operators to high levels of radiation and is very costly because of the large number of radioactive waste containers that need to be characterized at a nuclear facility. An alternative methodology to approach this problem consists in obtaining empirical correlations between some radionuclides that can be measured directly – such as {sup 60}Co and {sup 137}Cs, therefore designated as Key Nuclides (KNs) – and the DTMs. This methodology, denominated Scaling Factor, was applied in the scope of the present work in order to obtain Scaling Factors or Correlation Functions for the most important radioactive wastes with low and intermediate-activity level from the IEA-R1 nuclear research reactor. (author)

  20. Determination of {sup 234}U and {sup 238}U activity concentrations in groundwaters from three deep wells drilled in Itu Intrusive Suite (SP); Determinacao das concentracoes de atividade de {sup 234}U e {sup 238}U em aguas subterraneas de tres pocos perfurados em rochas da Suite Intrusiva de Itu (SP)

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Francisca de

    2006-07-01

    Activity concentrations of ({sup 234}U) and ({sup 238}U) were determined in groundwaters drawn from three deep wells drilled in rocks from Itu Intrusive Suite (SP), two located in Salto town (S and SY wells) and the other one in Itu (I well). Sampling was done from September, 2004 to December, 2005, and twelve samples of each well were collected monthly. For those determinations alpha spectrometry technique was used, providing high precision results, as shown by the very good agreement of the data obtained in the analyses of 23 duplicates. The waters from the three wells presented a considerable enrichment of {sup 234}U in relation to {sup 238}U, indicating an important radioactive disequilibrium of these isotopes. In well I, the activity concentrations of ({sup 238}U) varied from (1,06 +- 0,03) to (2,1+- 0,2) mBq/L and those of ({sup 234}U) spanned from (3,1 +- 0,2) to (6,0 +- 0,4) mBq/L, whereas ({sup 234}U/{sup 238}U) activity ratios did not present significant variation, during the sampling time interval, presenting an average of 2,8 +- 0,1. The S waters showed the lowest uranium concentrations and the largest diversity of ({sup 238}U) and ({sup 234}U) activity concentrations, which varied from (0,26 +- 0,02) to (1,07+- 0,08) mBq/L and from (1,8 +- 0,1) to (7,0 +- 0,5) mBq/L, respectively, and also presented variable ({sup 234}U/{sup 238}U) activity ratios, spanning from (2,79 +- 0,07) to (8,1+- 0,3). In SY well, ({sup 238}U) activities varied between (0,8 +- 0,1) and (4,2 +- 0,3) mBq/L and those ones of ({sup 234}U) from (14 +- 1) to (53 +- 4) mBq/L, whereas ({sup 234}U/{sup 238}U) ratios fell in the interval from 12,6 +- 0,3 to 18,3 +- 0,4, with the highest activities of both radioisotopes registered during the dry season and the lowest ones in the rainy time period. The ({sup 234}U/{sup 238}U) activity ratios, which were invariable during sampling period of well I, indicated the contribution of rainfall to recharge the aquifer. The observed correlation

  1. Use of cyclic voltammetry and electrochemical impedance spectroscopy for determination of active surface area of modified carbon-based electrodes; Uso da voltametria ciclica e da espectroscopia de impedancia eletroquimica na determinacao da area superficial ativa de eletrodos modificados a base de carbono

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Leticia Lopes de

    2011-07-01

    Carbon-based electrodes as well the ion exchange electrodes among others have been applied mainly in the treatment of industrial effluents and radioactive wastes. Carbon is also used in fuel cells as substrate for the electrocatalysts, having high surface area which surpasses its geometric area. The knowledge of the total active area is important for the determination of operating conditions of an electrochemical cell with respect to the currents to be applied (current density). In this study it was used two techniques to determine the electrochemical active surface area of glassy carbon, electrodes and ion exchange electrodes: cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS). The experiments were carried out with KNO{sub 3} 0.1 mol.L{sup -1} solutions in a three-electrode electrochemical cell: carbon-based working electrode, platinum auxiliary electrode and Ag/AgCl reference electrode. The glassy carbon and porous carbon electrodes with geometric areas of 3.14 x 10{sup -2} and 2.83 X 10{sup -1} cm{sup 2}, respectively, were used. The ion exchange electrode was prepared by mixing graphite, carbon, ion exchange resin and a binder, and this mixture was applied in three layers on carbon felt, using a geometric area of 1.0 cm{sup 2} during the experiments. The capacitance (Cd) of the materials was determined by EIS using Bode diagrams. The value of 172 {mu}F.cm{sup -2} found for the glassy carbon is consistent with the literature data ({approx} 200 {mu}F.cm'-{sup 2}). By VC, varying the scan rate from 0.2 to 2.0 mV.s-1, the capacitance CdS (S = active surface area) in the region of the electric double layer (EDL) of each material was determined. By EIS, the values of C{sub d}, 3.0 x 10{sup -5} {mu}F.cm'-{sup 2} and 11 x 10{sup 3} {mu}F.cm-2, were found for the porous carbon and ion exchange electrodes, respectively, which allowed the determination of active surface areas as 3.73 x 106 cm{sup 2} and 4.72 cm{sup 2}. To sum up, the

  2. Standardizing Activation Analysis: New Software for Photon Activation Analysis

    International Nuclear Information System (INIS)

    Photon Activation Analysis (PAA) of environmental, archaeological and industrial samples requires extensive data analysis that is susceptible to error. For the purpose of saving time, manpower and minimizing error, a computer program was designed, built and implemented using SQL, Access 2007 and asp.net technology to automate this process. Based on the peak information of the spectrum and assisted by its PAA library, the program automatically identifies elements in the samples and calculates their concentrations and respective uncertainties. The software also could be operated in browser/server mode, which gives the possibility to use it anywhere the internet is accessible. By switching the nuclide library and the related formula behind, the new software can be easily expanded to neutron activation analysis (NAA), charged particle activation analysis (CPAA) or proton-induced X-ray emission (PIXE). Implementation of this would standardize the analysis of nuclear activation data. Results from this software were compared to standard PAA analysis with excellent agreement. With minimum input from the user, the software has proven to be fast, user-friendly and reliable.

  3. Economical aspects and analysis for the determination of the economic viability of a gas microturbine operating as a electric power generation system; Analise e aspectos economicos para determinacao da viabilidade economica de uma microturbina a gas operando como sistema de geracao de energia eletrica

    Energy Technology Data Exchange (ETDEWEB)

    Venson, Giuliano Gardolinski [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil)]. E-mails: venson@ufmg.br; Barros, Jose Eduardo Mautone [Centro Federal de Educacao Tecnologica de Minas Gerais, Belo Horizonte, MG (Brazil)]. E-mail: mautone@des.cefetmg.br; Ayres, Naiara Pacheco [Grupo Irmaos Ayres S.A., Contagem, MG (Brazil)]. E-mail: pacheco@iasa.ind.br

    2006-07-01

    This paper presents the methodology used for the criteria determination of the economic viability of a gas microturbine in development the operating parallel to the central distribution network. The study intends to verify the influence of the acquisition cost, the specific cost of the operation and the financing rate applied to the microturbine related to the economic viability criteria. The criteria used are based on investment analysis analytical methods such as the return internal rate. For the development of the methodology the energy demand and consumption data of a medium size have been used.

  4. Electro-oxidative leaching of pitchblende for uranium determination by arsenazo III spectrophotometry using fluid injection analysis system; Lixiviacao eletro-oxidativa de pechblenda para determinacao de uranio por espectrofotometria com arsenazo III empregando um sistema de analises por injecao em fluxo

    Energy Technology Data Exchange (ETDEWEB)

    Sousa, Alvaro Serafim Ferreira de

    2006-07-01

    In this work two different electro dissolution cells were projected and tested in order to solubilize pitchblende minerals aiming to posterior on line association to a flow injection system for the spectrophotometric determination of uranium leachate. The influence of current density, time, temperature, the electrolyte concentration nature, and the particle suspension density, were studied. Hydrodynamic and chemical parameters effects were evaluated to establish the best efficiency of the flow injection analysis system and to receive samples pretreated by electro oxidative leaching for the uranium determination. Arsenazo III was used as a colorimetric reagent and parameters such as acidity and reagents concentration, carrier and reagent flow rates, injection volume, reactor and reduction column size were studied and optimized. The calibration curves have showed a linear behavior (R{sup 2} = 0.9996) between the concentration range of 0.05 and 2.0 mgL{sup -1}. A relative deviation standard of 5.5 % (at 0.1 mgL{sup -1}) and a detection limit of 0.02 mgL{sup -1} were obtained, as well an analytical throughput of 60 sample determinations per hour. In the association of the flow injected analysis system with the electro-dissolution cells, values up to 98 % were obtained for the uranium extraction. The developed methodology for the electrooxidative extraction and on line spectrophotometric uranium determination in pitchblende samples, showed agreement with the reference method (ICP-MS), with a deviation between the results of less than 3.5 %. The proposal system showed advantages in relation to the conventional technique, like: automation of all analytical process, less quantities and more swiftness in the sample dissolution, less volume and acid concentration and reduction of the matrix effect. (author)

  5. Charged-particle activation analysis

    International Nuclear Information System (INIS)

    The paper discusses the methodology and application of nuclear activation with ion beams (19 via 16O(3He,p)18F, 12C(3He,α)11C and 14N(p,α)11C respectively. Recently, triton activation has been shown to be inherently still superior to 3He activation for the determination of oxygen [16O(3H,n)18F]. Lithium, boron, carbon and sulphur can be detected rapidly, nondestructively and with high sensitivity (approximately 0.25ppm for Li and B) via ''quasi-prompt'' activation based on the detection of short-lived, high-energy beta emitters (10ms1H(7Li,n)7Be for example. Nondestructive multielement analysis: Proton activation has the inherent potential for meeting requirements of broad elemental coverage, sensitivity (ppm and sub-ppm range) and selectivity. Up to 30 elements have been determined in Al, Co, Ag, Nb, Rh, Ta and biological samples, using 12-MeV proton activation followed by gamma-ray spectrometry. These capabilities are further enhanced with the counting of X-ray emitters, 28 elements (269) and accuracy using proton activation. 204Pb/206Pb ratios can also be determined with a relative precision of a few per cent. Although charged-particle activation analysis is a well-established trace analysis technique, broad potential capabilities remain to be explored, e.g. those arising from ultrashort-lived nuclides, heavy ion interactions and the combination of delayed and prompt methods. (author)

  6. Automated activation-analysis system

    International Nuclear Information System (INIS)

    An automated delayed neutron counting and instrumental neutron activation analysis system has been developed at Los Alamos National Laboratory's Omega West Reactor (OWR) to analyze samples for uranium and 31 additional elements with a maximum throughput of 400 samples per day. The system and its mode of operation for a large reconnaissance survey are described

  7. Instrumentation in neutron activation analysis

    International Nuclear Information System (INIS)

    The rise of neutron activation analysis (NAA) as a tool in geochemical research has parallelled advances in detector, multi-channel analyzer, and computer technology. Micro-computers are now being integrated into NAA systems, and gamma-ray spectrometer instrumentation is evolving towards direct-reading systems. The investigator is faced with a wide range of possibilities and choices when equipping or re-equipping a laboratory. The geoscientist is provided with an overview of the available instrumentation and what soon may be feasible. (L.L.)

  8. Conference on instrumental activation analysis IAA 92

    International Nuclear Information System (INIS)

    The publication contains 26 abstracts primarily concerned with neutron activation analysis, although other analytical techniques based on X-ray fluorescence analysis, PIXE, PIGE, RBS are also included. Some contributions deal with aspects of quality practice and assurance in radioanalytical laboratories, with marketing of instrumental neutron activation analysis services, with hard- and software aspects of radiation detection, etc. (Z.S.)

  9. Instrumental neutron activation analysis - a routine method

    International Nuclear Information System (INIS)

    This thesis describes the way in which at IRI instrumental neutron activation analysis (INAA) has been developed into an automated system for routine analysis. The basis of this work are 20 publications describing the development of INAA since 1968. (Auth.)

  10. Analysis of HR activities in selected company

    OpenAIRE

    Jandová, Šárka

    2012-01-01

    The aim of this thesis is based on theoretical knowledge and analysis of the basic HR activities in the selected company to identify the strengths and weaknesses of the policies implemented personnel work. Then propose an effective ways of improving HR activities and employee satisfaction. Basic personal activities analyzed in this thesis are the adaptation, acquisition and selection of employees, performance management and staff appraisal, remuneration and training of staff. Analysis of pers...

  11. Conference on Instrumental Activation Analysis: IAA 89

    Science.gov (United States)

    Vobecky, M.; Obrusnik, I.

    1989-05-01

    The proceedings contain 40 abstracts of papers all of which have been incorporated in INIS. The papers were centred on the applications of radioanalytical methods, especially on neutron activation analysis, x ray fluorescence analysis, PIXE analysis and tracer techniques in biology, medicine and metallurgy, measuring instruments including microcomputers, and data processing methods.

  12. Neutron activation analysis of reference materials

    International Nuclear Information System (INIS)

    The importance is pointed out of neutron activation analysis in the preparation of reference materials, and studies are reported conducted recently by UJV. Instrumental neutron activation analysis has been used in testing homogeneity and in determining 28 elements in newly prepared reference standards of coal fly ash designated ENO, EOP and ECH. For accuracy testing, the same method was used in the analysis of NBS SRM-1633a Trace Elements in Coal Fly Ash and IAEA CRM Soil-5 and RM Soil-7. Radiochemical neutron activation analysis was used in determining Cd, Cu, Mn, Mo, and Zn in biological materials NBS SRM-1577 Bovine Liver, Bowen's Kale and in IAEA RM Milk Powder A-11 and Animal Muscle H-4. In all instances very good precision and accuracy of neutron activation analysis results were shown. (author)

  13. Neutron activation analysis of geochemical samples

    International Nuclear Information System (INIS)

    The present paper will describe the work done at the Technical Research Centre of Finland in developing methods for the large-scale activation analysis of samples for the geochemical prospecting of metals. The geochemical prospecting for uranium started in Finland in 1974 and consequently a manually operated device for the delayed neutron activation analysis of uranium was taken into use. During 1974 9000 samples were analyzed. The small capacity of the analyzer made it necessary to develop a completely automated analyzer which was taken into use in August 1975. Since then 20000-30000 samples have been analyzed annually the annual capacity being about 60000 samples when running seven hours per day. Multielemental instrumental neutron activation analysis is used for the analysis of more than 40 elements. Using instrumental epithermal neutron activation analysis 25-27 elements can be analyzed using one irradiation and 20 min measurement. During 1982 12000 samples were analyzed for mining companies and Geological Survey of Finland. The capacity is 600 samples per week. Besides these two analytical methods the analysis of lanthanoids is an important part of the work. 11 lanthanoids have been analyzed using instrumental neutron activation analysis. Radiochemical separation methods have been developed for several elements to improve the sensitivity of the analysis

  14. Applications of neutron activation analysis in industry

    International Nuclear Information System (INIS)

    Neutron activation analysis technique is discussed in brief. This technique is used for quality control of raw materials, process materials and finished products, as well as activities in research and development for the improvement of the products and new products. The uses of this technique in several experienced industries are mentioned (author)

  15. New studies in forensic neutron activation analysis

    International Nuclear Information System (INIS)

    Three recently completed studies in forensic neutron activation analysis are reported: a study of 0.22-caliber rimfire cartridge primers, a large-scale study of shotgun pellets, and a new 5-element procedure for the analysis of bullet-lead and shotgun-pellet samples. (author) 12 refs

  16. New studies in forensic neutron activation analysis

    International Nuclear Information System (INIS)

    Earlier studies in forensic neutron activation analysis are being extended in This Laboratory. Three of these new studies are reported here: 1) a study of 0.22-caliber rimfire cartridge primers, 2) a large-scale study of shotgun pellets, and 3) a new 5-element procedure for the analysis of bullet-lead and shotgun-pellet samples. (author)

  17. Computational Models for Analysis of Illicit Activities

    DEFF Research Database (Denmark)

    Nizamani, Sarwat

    Numerous illicit activities happen in our society, which, from time to time affect the population by harming individuals directly or indirectly. Researchers from different disciplines have contributed to developing strategies to analyze such activities, in order to help law enforcement agents dev...... population globally sensitive to specific world issues. The models discuss the dynamics of population in response to such issues. All the models presented in the thesis can be combined for a systematic analysis of illicit activities.......Numerous illicit activities happen in our society, which, from time to time affect the population by harming individuals directly or indirectly. Researchers from different disciplines have contributed to developing strategies to analyze such activities, in order to help law enforcement agents...... devise policies to minimize them. These activities include cybercrimes, terrorist attacks or violent actions in response to certain world issues. Beside such activities, there are several other related activities worth analyzing, for which computational models have been presented in this thesis...

  18. Evaluation of business activity using financial analysis

    OpenAIRE

    Kučerová, Martina

    2012-01-01

    Czech University of Life Sciences Prague Faculty of Economics and Management Department of Trade and Accounting Abstract of Diploma Thesis Evaluation of business activity using financial analysis Martina Kučerová © 2012 CULS in Prague Summary: The aim of this thesis is to apply methods of financial analysis on chosen business for its first three accounting periods 2009, 2010 and 2011. The thesis is further analysis of my bachelor thesis on to...

  19. Determination of methodology of automatic history matching; Determinacao de metodologia de ajuste automatizado de historico

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Jose Pedro Moura dos

    2000-01-01

    In management of hydrocarbon reservoirs the numeric simulation is a fundamental tool. The validation of a field model with production report is made through history matching which, many times, is done by trial and errors procedures consuming excessive computational time and human efforts. The objective of this work is to present a methodology for automation of the history matching using the program UNIPAR with the modules of parallel computing, sensibility analysis and optimization. Based on an example of an offshore field, analyses of the objective function (water production, oil production and average pressure of the reservoir) behavior were accomplished as function of the variations of reservoir parameters. It was verified that this behavior is very regular. After that, several adjustment situations were tested to define a procedure to be used for a history matching. (author) Ate aqui estao scanned.

  20. Human hair neutron activation analysis: analysis on population level, mapping

    International Nuclear Information System (INIS)

    Neutron activation analysis is an outstanding analytical method having very wide applications in various fields. Analysis of human hair within last decades mostly based on neutron activation analysis is a very attractive illustration of the application of nuclear analytical techniques. Very interesting question is how the elemental composition differs in different areas or cities. In this connection the present paper gives average data and maps of various localities in the vicinity of drying-out Aral Sea and of various industrial cities in Central Asia. (author)

  1. Neutron activation spectrometry and neutron activation analysis in analytical geochemistry

    International Nuclear Information System (INIS)

    The present report is to show the geochemists who are interested in neutron activation spectrometry (NAS) and neutron activation analysis (NAA) which analytical possibilities these methods offer him. As a review of these analytical possibilities, a lieterature compolation is given which is subdivided into two groups: 1) rock (basic, intermediary, acid, sediments, soils and nuds, diverse minerals, tectites, meteorites and lunar material). 2) ore (Al, Au, Be, Cr, Cu, Mn, Mo, Fe, Pb, Pt, Sn, Ti, W, Zn, Zr, U and phosphate ore, polymetallic ores, fluorite, monazite and diverse ores). The applied methods as well as the determinable elements in the given materials can be got from the tables. On the whole, the literature evaluation carried out makes it clear that neutron activation spectrometry is a very useful multi-element method for the analysis of rocks. The analysis of ores, however, is subjected to great limitations. As rock analysis is very frequently of importance in prospecting for ore deposits, the NAS proves to be extremely useful for this very field of application. (orig./LH)

  2. High-capacity neutron activation analysis facility

    International Nuclear Information System (INIS)

    A high-capacity neutron activation analysis facility, the Reactor Activation Facility, was designed and built and has been in operation for about a year at one of the Savannah River Plant's production reactors. The facility determines uranium and about 19 other elements in hydrogeochemical samples collected in the National Uranium Resource Evaluation program, which is sponsored and funded by the United States Department of Energy, Grand Junction Office. The facility has a demonstrated average analysis rate of over 10,000 samples per month, and a peak rate of over 16,000 samples per month. Uranium is determined by cyclic activation and delayed neutron counting of the U-235 fission products; other elements are determined from gamma-ray spectra recorded in subsequent irradiation, decay, and counting steps. The method relies on the absolute activation technique and is highly automated for round-the-clock unattended operation

  3. Activation analysis of air particulate matter

    International Nuclear Information System (INIS)

    This review on activation analysis of air particulate matter is an extended and updated version of a review given by the same authors in 1985. The main part is aimed at the analytical scheme and refers to rules and techniques for sampling, sample and standard preparation, irradiation and counting procedures, as well as data processing, - evaluation, and - presentation. Additional chapters deal with relative and monostandard methods, the use of activation analysis for atmosphere samples in various localities, and level of toxic and other elements in the atmosphere. The review contains 190 references. (RB)

  4. Design of Neutron Activation Analysis Laboratorium Room

    International Nuclear Information System (INIS)

    Base on the planning to increase of the research and service quality in the ''Neutron activation analysis'' (APN),the design of mentioned ''Neutron activation analysis laboratories room'' has been done in the multi purpose reactor G.A. Siwabessy. By the using the designed installation, the irradiation preparation and counting sample can be done. The design doing by determination of installation lay out and maximum particle contain in the air. The design installation required a unit of 1 HP blower, a unit of 1 HP split air condition and 2 units 1200 x 800 mm HEPA filter. This paper concluded that this design is feasible to fabricated

  5. Quality assurance in biomedical neutron activation analysis

    International Nuclear Information System (INIS)

    The summary report represents an attempt to identify some of the possible sources of error in in vitro neutron activation analysis of trace elements applied to specimens of biomedical origin and to advise on practical means to avoid them. The report is intended as guidance for all involved in analysis, including sample collection and preparation for analysis. All these recommendations constitute part of quality assurance which is here taken to encompass the two concepts - quality control and quality assessment. Quality control is the mechanism established to control errors, while quality assessment is the mechanism used to verify that the analytical procedure is operating within acceptable limits

  6. Prompt gamma-ray activation analysis (PGAA)

    Energy Technology Data Exchange (ETDEWEB)

    Kern, J. [Fribourg Univ. (Switzerland). Inst. de Physique

    1996-11-01

    The paper deals with a brief description of the principles of prompt gamma-ray activation analysis (PGAA), with the detection of gamma-rays, the PGAA project at SINQ and with the expected performances. 8 figs., 3 tabs., 10 refs.

  7. The Atomic Fingerprint: Neutron Activation Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Keisch, Bernard [Carnegie-Mellon University

    1972-01-01

    The nuclei of atoms are stable only when they contain certain numbers of neutrons and protons. Since nuclei can absorb additional neutrons, which in many cases results in the conversion of a stable nucleus to a radioactive one, neutron activation analysis is possible.

  8. Isotopic neutron sources for neutron activation analysis

    International Nuclear Information System (INIS)

    This User's Manual is an attempt to provide for teaching and training purposes, a series of well thought out demonstrative experiments in neutron activation analysis based on the utilization of an isotopic neutron source. In some cases, these ideas can be applied to solve practical analytical problems. 19 refs, figs and tabs

  9. Transforming Teacher Education, An Activity Theory Analysis

    Science.gov (United States)

    McNicholl, Jane; Blake, Allan

    2013-01-01

    This paper explores the work of teacher education in England and Scotland. It seeks to locate this work within conflicting sociocultural views of professional practice and academic work. Drawing on an activity theory framework that integrates the analysis of these seemingly contradictory discourses with a study of teacher educators' practical…

  10. Neutron activation analysis of Etruscan pottery

    International Nuclear Information System (INIS)

    Neutron activation analysis (NAA) has been widely used in archaeology for compositional analysis of pottery samples taken from sites of archaeological importance. Elemental profiles can determine the place of manufacture. At Cornell, samples from an Etruscan site near Siena, Italy, are being studied. The goal of this study is to compile a trace element concentration profile for a large number of samples. These profiles will be matched with an existing data bank in an attempt to understand the place of origin for these samples. The 500 kW TRIGA reactor at the Ward Laboratory is used to collect NAA data for these samples. Experiments were done to set a procedure for the neutron activation analysis with respect to sample preparation, selection of irradiation container, definition of activation and counting parameters and data reduction. Currently, we are able to analyze some 27 elements in samples of mass 500 mg with a single irradiation of 4 hours and two sequences of counting. Our sensitivity for many of the trace elements is better than 1 ppm by weight under the conditions chosen. In this talk, details of our procedure, including quality assurance as measured by NIST standard reference materials, will be discussed. In addition, preliminary results from data treatment using cluster analysis will be presented. (author)

  11. Analysis by neutron activation analysis a some ancient Dacian ceramics

    CERN Document Server

    Olariu, A

    1999-01-01

    Ancient Dacian ceramics, from three different establishments from Romanian territory have been analyzed by neutron activation analysis. A series of elements has been determined: Ba, Eu, K, La, Mn, Na, Sc, Sm. Ba is the element that could be considered to differentiate relatively the three groups of ceramics.

  12. Activity Analysis and Cost Analysis in Medical Schools.

    Science.gov (United States)

    Koehler, John E.; Slighton, Robert L.

    There is no unique answer to the question of what an ongoing program costs in medical schools. The estimates of program costs generated by classical methods of cost accounting are unsatisfactory because such accounting cannot deal with the joint production or joint cost problem. Activity analysis models aim at calculating the impact of alternative…

  13. Multiscale statistical analysis of coronal solar activity

    CERN Document Server

    Gamborino, Diana; Martinell, Julio J

    2016-01-01

    Multi-filter images from the solar corona are used to obtain temperature maps which are analyzed using techniques based on proper orthogonal decomposition (POD) in order to extract dynamical and structural information at various scales. Exploring active regions before and after a solar flare and comparing them with quiet regions we show that the multiscale behavior presents distinct statistical properties for each case that can be used to characterize the level of activity in a region. Information about the nature of heat transport is also be extracted from the analysis.

  14. Service activities of chemical analysis division

    International Nuclear Information System (INIS)

    Progress of the Division during the year of 1988 was described on the service activities for various R and D projects carrying out in the Institute, for the fuel fabrication and conversion plant, and for the post-irradiation examination facility. Relevant analytical methodologies developed for the chemical analysis of an irradiated fuel, safeguards chemical analysis, and pool water monitoring were included such as chromatographic separation of lanthanides, polarographic determination of dissolved oxygen in water, and automation on potentiometric titration of uranium. Some of the laboratory manuals revised were also included in this progress report. (Author)

  15. Nondestructive gamma activation analysis of mineral materials

    International Nuclear Information System (INIS)

    The basic problems are described related to the use of gamma activation analysis. The applicability was studied of instrumental gamma activation analysis (IGAA) in geology. A number of minerals, rocks, marine sediments and reference materials were studied. For irradiation a betatron and a microtron were used. The results show that IGAA allows the simultaneous determination of a number of trace elements at concentrations of tenths of ppm. The results are given of comparisons made of the analytical possibilities of microtron IGAA and reactor INAA in geology. Tables show the results of the application of IGAA, the main products and parameters of photoexcitation reactions and graphically represented are the gamma spectra of measured materials. (J.B.)

  16. KFUPM fast neutron activation analysis facility

    International Nuclear Information System (INIS)

    A newly established Fast Neutron Activation Analysis facility at the Energy Research Laboratory is described. The facility mainly consists of a fast neutron irradiation station and a gamma ray counting station. Both stations are connected by a fast pneumatic sample transfer system which transports the sample from the irradiation station to the counting station in a short time of 3 s. The fast neutron activation analysis facility has been tested by measuring the 27A(n, α)24Na and 115In(n, n')115mIn cross sections at 14.8 and 2.5 MeV neutron energies, respectively. Within the experimental uncertainties, the measured cross sections for these elements agree with the published values. (orig.)

  17. Analysis of an iodide radioimmunoassay for 11-deoxicortisol measurement; Analise de um radioimunoensaio iodado para determinacao de 11-deoxicortisol

    Energy Technology Data Exchange (ETDEWEB)

    Madeira, Joao Luiz de Oliveira; Bussmann, Luciane Zgoda; Lima-Valassi, Helena Panteliou; Mendonca, Berenice Bilharinho de, E-mail: joao.madeira@usp.br [Universidade de Sao Paulo (HCFM/USP), SP (Brazil). Hospital das Clinicas. Departamento de Clinica Medica

    2014-04-15

    Objective: our aim was to correlate 11-deoxycortisol levels obtained by two currently available techniques for 11-deoxycortisol measurement: radioimmunoassay, and high performance liquid chromatography followed by tandem mass spectrometry (MS/MS). The latter is the gold standard method for steroid hormone measurement. Materials and methods: we selected 88 samples and the results of these two methods were compared by Deming regression. Results: the analytical sensitivity of the RIA was 0.30 ng/mL, with inadequate linearity and inadequate precision profile (34% of the samples had a CV ≥ 20%). From the selected samples, 54 had measurable levels of 11-deoxycortisol in both methods and were used in the comparison. The comparison of RIA with LC-MS/MS showed an overestimation of the results by RIA. The correlation coefficient was 0.610; linear regression slope was 3.751; and the intercept was 0.145, indicating a poor correlation between the two methods. Conclusion: we concluded that 11-deoxycortisol measured by radioimmunoassay, despite a good analytical sensitivity, showed very low specificity, precluding its use as a reliable method for 11-deoxycortisol measurement. (author)

  18. Reactor neutron activation analysis of industrial materials

    International Nuclear Information System (INIS)

    The specific application of neutron activation analysis (n.a.a.) for industrial materials is demonstrated by the determination of impurities in BeO, Al, Si, Cu, Ge, GaP, GaAs, steel, and irradiated uranium. A group scheme gives an orientation about the possibilities of n.a.a. The use of different standards, methods for the measurement of low radioactivities and errors caused by recoil reaction and radiation stimulated diffusion are discussed. (author)

  19. Trace elements determination in ginseng and ginkgo biloba medicinal plants; Determinacao de elementos traco nos fitofarmacos ginseng e ginkgo biloba

    Energy Technology Data Exchange (ETDEWEB)

    Avino, Simone; Saiki, Mitiko; Fulfaro, Roberto [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil). Lab. de Analise por Ativacao Neutronica

    2002-07-01

    Determinations of trace elements in medicinal plants or in their extracts are of great interest since some elements are components of active constituents or they can affect the plant metabolism and consequently the formation of active constituents. In this work, inorganic components in medicinal drugs, Ginseng e Ginkgo Biloba provided from different laboratories, were analyzed by neutron activation analysis. Elements As, Br, Ca, Cl, Co Cr, Cs, Fe, K, La, Mg, Mn, Na, Rb, Sb, Sc, and Zn, were determined in these samples. Comparisons carried out between the results obtained for samples from different laboratories indicated distinct concentrations for several elements. These results may be attributed to the effect of soil composition and environmental conditions where these plants were cultivated. The precision and accuracy of the results were evaluated by analyzing reference materials Bowen's Kale from IUAPC and Cabbage from IAEA. (author)

  20. Activation Analysis and Public Health. Survey Paper

    International Nuclear Information System (INIS)

    The technique of activation analysis has useful and distinctive applications, not yet fully recognized or exploited, in public health. Three areas of usefulness may be recognized. 1. Industrial hygiene. Activation analysis offers a simple and efficient method for assessing and controlling occupational hazards associated with the handling of toxic materials, such as compounds of arsenic and of mercury. Examination of hair and nail samples, taken at six-monthly intervals, will yield a surprising amount of information regarding the influence on occupational exposure of individual variation in working habits, and inadequacy or non-observance of hygienic rules and other prescribed safety measures. 2. Epidemiology. The advantage conferred by activation analysis lies in the possibility of rapid and accurate estimation of trace element concentrations in small samples of tissue or other materials, such as can readily be obtained from population groups large enough to be statistically significant. Surveys of this kind have interesting potentialities in relation to dental caries, cancer, cirrhosis of the liver and heart disease. 3. Recognition of essential trace elements. Surveys of trace element concentrations suggest that the variability of tissue levels among members of a population is smaller for essential trace elements than for non-essential elements. It is possible also that tissue levels show a normal distribution for essential elements and a log-normal distribution for non-essential elements. (author)

  1. Neutron Activation analysis of waste water

    International Nuclear Information System (INIS)

    An instrumental neutron activation analysis for the simultaneous determination of chlorine, bromine, sodium, manganese, cobalt, copper, chromium, zinc, nickel, antimony and iron in waste water is described. They were determined in waste water samples under normal conditions by non-destructive neutron activation simultaneously using a suitable monostandard method. Standardized water samples were used and irradiated in polyethylene ampoules at a neutron flux of 1013 cm-2 s-1 for periods of 1 minute, 1 and 10 hours. A Ge hyperpure detector was used for your activity determination, with count times of 60, 180, 300 and 600 seconds. The obtained results show than the method can be utilized for the determination of this elements without realize anything previous treatment of the samples. (Author)

  2. Analysis of ayurvedic medicinal leaves by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Concentrations of 15 elements were determined in medicinally important ayurvedic medicinal leaves. Instrumental neutron activation analysis was employed for the determination of the elements viz. Na, K, Br, Sm, Cr, Zn, Th, Rb, Sr, Fe, La, Co, Ce, Cs and Eu. The samples were neutron irradiated at 100 kW TRIGA -Mainz nuclear reactor and the induced activities were measured by gamma ray spectrometry using an efficiency calibrated high resolution high purity germanium (HPGe) detector. The concentrations of these elements in the medicinal leaves and their medicinal importance are discussed. (author)

  3. Multielemental analysis of soils by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    The results of an instrumental neutron activation analysis of some elemental concentrations in different soil samples near the industrial areas at Tirupati, India, are reported. Altogether 14 elements, Sm, La, Cr, Co, Zn, Cs, Ce, Th, Rb, Na, K, Sr, Fe and Eu were determined. The samples were irradiated with neutrons at the 100 kW Triga - Mainz research reactor and the induced activities were measured by gamma-ray spectrometry using an efficiency calibrated high resolution high purity germanium (HPGe) detector in connection with a multichannel analyzer. The results are discussed. (author)

  4. Industrial applications of neutron activation analysis

    International Nuclear Information System (INIS)

    Neutron activation analysis has been widely used in the industry and over the years played a key role in the development of manufacturing process as well as monitoring of the process flow. In this context NAA has been utilized both in R and D, and in the factory as a flexible analytical tool. It has been used successfully in numerous industries including broad categories such as Chemical, Pharmaceutical, Mining, Photographic, Oil and Gas, Automobile, Defense, Semiconductor and Electronic industries. Dow Chemical owns and operates a research reactor for analytical measurements of samples generated in both R and D, and manufacturing area in its plant in Midland, Michigan. Although most industries do not have reactors on their campus but use an off site reactor regularly, and often have in-house neutron sources such as a 252Cf used primarily for NAA. In most industrial materials analysis laboratory NAA is part of a number of analytical techniques such as ICP-MS, AA, SIMS, FTIR, XRF, TXRF etc. Analysis of complex industrial samples may require data from each of these methods to provide a clear picture of the materials issues involved. With the improvement of classical analytical techniques, and the introduction of new techniques, e.g. TXRF, the role of NAA continues to be a key bench mark technique that provides accurate and reliable data. The strength of the NAA in bulk analysis is balanced by its weakness in providing surface sensitive or spatially resolved analysis as is required by many applications. (author)

  5. Scalable histopathological image analysis via active learning.

    Science.gov (United States)

    Zhu, Yan; Zhang, Shaoting; Liu, Wei; Metaxas, Dimitris N

    2014-01-01

    Training an effective and scalable system for medical image analysis usually requires a large amount of labeled data, which incurs a tremendous annotation burden for pathologists. Recent progress in active learning can alleviate this issue, leading to a great reduction on the labeling cost without sacrificing the predicting accuracy too much. However, most existing active learning methods disregard the "structured information" that may exist in medical images (e.g., data from individual patients), and make a simplifying assumption that unlabeled data is independently and identically distributed. Both may not be suitable for real-world medical images. In this paper, we propose a novel batch-mode active learning method which explores and leverages such structured information in annotations of medical images to enforce diversity among the selected data, therefore maximizing the information gain. We formulate the active learning problem as an adaptive submodular function maximization problem subject to a partition matroid constraint, and further present an efficient greedy algorithm to achieve a good solution with a theoretically proven bound. We demonstrate the efficacy of our algorithm on thousands of histopathological images of breast microscopic tissues. PMID:25320821

  6. Activation Analysis and Nuclear Research in Burma

    International Nuclear Information System (INIS)

    Research endeavours in the field of Nuclear Sciences in Burma appear to be concentrated in three main Institutions. These are the Chemistry and Physics Departments of the Rangoon Arts & Science University and the Union of Burma Applied Research Institute (UBARI). In view of possible forthcoming developments an expanded research programme, which is to be implemented on the basis of a five year plan, has been drawn up. Research topics included in this programme are predominantly of practical interest and aimed at a contribution by nuclear methods, in particular activation analysis, to the technological and industrial needs of the country

  7. Determination of the Antarctic region active margin basement by using integration of the information coming from the multichannel seismic analysis and the magnetometry; Determinacao do embasamento da margen ativa da regiao Antartica pela integracao de informacoes provenientes da sismica multicanal e da magnetometria

    Energy Technology Data Exchange (ETDEWEB)

    Torres, Luiz Carlos [Diretoria de Hidrografia e Navegacao, XX (Brazil); Gomes, Benedito Souza [PETROBRAS S.A., Rio de Janeiro, RJ (Brazil); Gamboa, Luiz Antonio P. [Universidade Federal Fluminense, Niteroi, RJ (Brazil)

    1999-07-01

    Geophysical measurements were carried out in the Western Margin of the Antarctic Peninsula and Bransfield Strait by the Brazilian Antarctic Program during the summers of 1987 and 1988. The present work, using a continued seismic multi channel and magnetometry data profile crossing the area, intends to present a two-dimensional model of the interface sediment/basement and contribute to the understanding of the complex geology verified in the studying area. By this model, the main provinces of the are (Deep Ocean, South Shetland Trench, Accretionary Prism, Volcanic Arc South Shetland Islands and Bransfield Basin) could be determined. The seismic and magnetic measurements information when superposed can attribute more consistencies to the interpreted basement; although each method has its particular resolution. This way, when the seismic interpretation was not possible due to complex structures disposition, magnetic measurements could offer good estimation about basement depth. The fit between both methods (seismic and magnetic measurements) was reasonable both on the oceanic basin and in the region of Bransfield Strait. The magnetometry, as as well seismic, was sensible to the dip of Drake Plate at South Shetland Trench and the Intrusive occurrence at Bransfield Basin axis. (author)

  8. Neutron activation analysis of human hair

    International Nuclear Information System (INIS)

    As a part of IAEA research project, ''Activation analysis of hair as an indicator of contamination of man by environmental trace element pollutants'', a survey was carried out to elucidate the levels of various trace element concentration in hair of local population in the Tokyo Metropolitan areas, by applying instrumental neutron activation analysis. A total of 202 scalp hair samples were collected from the inhabitants classified by sex and five age classes. Irradiation was made in the Rikkyo University 100 kW TRIGA MARK-II reactor. Using several combinations of irradiation time, cooling time and counting time, forty elements were determined. The relationship between several trace element contents in hair and such factors as sex, age class, hair treatment, smoking habit and dental treatment, was analyzed by using the method of multiple regression. It was shown that (1) Hair treatment had a predominant effect on the contents of bromine, magnesium and calcium in hair, (2) Aging and amoking contributed increasing mercury content in hair, and hair treatment acted reversely. (author)

  9. Activation Analysis in Forensic Science. Survey Paper

    International Nuclear Information System (INIS)

    Recently the unique features of the activation analysis method have been utilized to advantage to meet some specialized needs in the scientific investigation of crime. A review of the principal forensic activation analysis applications to biological materials to date indicates that they may be roughly classified as: (i) the detection and determination of residues of toxic materials in foodstuffs, human tissues, sera and excreta; (ii) the 'individualization' of hair, fibres, narcotics and drugs; and (iii) investigation of the transference of ballistic material to bone, cloth or paper. Analyses of these materials in some actual forensic investigations have been perfected to the point of acceptance in the law courts of several countries. Additional and broader areas of application are under development in a number of nuclear and forensic laboratories. (i) The determination of sub microgram quantities of phosphorus compounds, arsenic, mercury, selenium and thallium in specimens from post-mortem examinations and from living persons showing symptoms of toxicity has revealed certain ingestion of abnormal amount of toxic substances by comparison with similar specimens from healthy persons. In some cases, with tissues such as hair and nails, the time scale of the ingestion of arsenic or mercury has been revealed through the distribution of the deposited element with distance from the growing end or edge. (ii) A series of feasibility studies on the possibility of distinguishing similar materials through their characteristic trace-element patterns have resulted from observations of the wide range or variation in trace impurity content in specimens which come from different individuals or different natural sources. For example, extensive activation analyses for more than twenty elements in human head hair from many people have been carried out and a statistical analysis of the results indicate that activation hair comparisons in forensic investigations may be quite definitive

  10. Research Activities involving Radioactivation Analysis in Korea

    International Nuclear Information System (INIS)

    When the Triga Mark-II Research Reactor was installed at this institute in 1960, it was furnished with a pneumatic tube, a fume hood, and a laboratory bench for the purpose of developing the utilization of the research reactor in this country. This marked the commencement of research activity in radioactivation analysis in Korea. Since the output of the reactor was not sufficient enough to perform any sophisticated fundamental research work in nuclear science, radioactivation analysis was considered as one of the most promising means of utilising the reactor. Various requests for routine analysis of the trace elements contained in Korean mineral ores, archaeological materials, domestic industrial samples, native medicinal plants, and criminological samples had been filed at this institute. Fortunately, a well trained scientist and technician for the radioactivation work had been working at this division and hence these requests from the public had been well worked out to receive much recognition of scientists and engineers both in this country and overseas. A brief summary of the research work accomplished is presented in this paper and a brief outline of the routine analytical work is also described on the basis of local situations

  11. Neutron activation analysis of urinary calculi

    International Nuclear Information System (INIS)

    Urinary calculi resulting from disorders in the urinary system are mostly composed of uric acid, urates, calcium oxalate, alkaline earth phosphates (Ca and Mg), triple phosphate (magnesium ammonium phosphate), calcium carbonate, cystine, xanthine, and traces of proteins. The determination of these macro-constituents has been carried out by different analytical procedures. No attempts however, have been reported regarding the determination of trace elements in urinary stones, apart from that of Herring et al., who investigated the consumption of strontium by urolithiasis patients. The present work is a non-destructive neutron activation analysis of urinary calculi, to search the variation in concentration of certain trace elements with the chemical composition of the calculus

  12. Reactor neutron activation for multielemental analysis

    International Nuclear Information System (INIS)

    Neutron Activation Analysis using single comparator (K0 NAA method) has been used for obtaining multielemental profiles in a variety of matrices related to environment. Gold was used as the comparator. Neutron flux was characterised by determining f, the epithermal to thermal neutron flux ratio and cc, the deviation from ideal shape of the neutron spectrum. The f and a were determined in different irradiation positions in APSARA reactor, PCF position in CIRUS reactor and tray rod position in Dhruva reactor using both cadmium cut off and multi isotope detector methods. High resolution gamma ray spectrometry was used for radioactive assay of the activation products. This technique is being used for multielement analysis in a variety of matrices like lake sediments, sea nodules and crusts, minerals, leaves, cereals, pulses, leaves, water and soil. Elemental profiles of the sediments corresponding to different depths from Nainital lake were determined and used to understand the history of natural absorption/desorption pattern of the previous 160 years. Ferromanganese crusts from different locations of Indian Ocean were analysed with a view to studying the distribution of some trace elements along with Fe and Mn. Variation of Mn/Fe ratio was used to identify the nature of the crusts as hydrogenous or hydrothermal. Fe-rich and Fe-depleted nodules from Indian Ocean were analysed to understand the REE patterns and it is proposed that REE-Th associated minerals could be the potential Th contributors to the sea water and thus reached ferromanganese nodules. Dolomites (unaltered and altered), two types of serpentines and intrusive rock dolerite from the asbestos mines of Cuddapah basin were analysed for major, minor and trace elements. The elemental concentrations are used for distinguishing and characterising these minerals. From our investigations, it was concluded that both dolomite and dolerite contribute elements in the serpentinisation process. Chemical neutron

  13. Analysis of physical activities in Taekwondo Pumsae.

    Science.gov (United States)

    Lee, Sang-Bock; Cha, Eun-Jong; Lee, Tae-Soo

    2008-01-01

    Exercise is very important element for successful aging. Among many sports events, Korea is the suzerain of Taekwondo. When competing (Taekwondo Free Fighting) after learning Poomse as basic movements and inuring them, people compete with movements depending on situation. Among Poomses of Taekwondo, Taegeuk Poomse consists of very basic movements from 1 Jang to 8 Jang and they are for inuring to body. In order to prescribe Taegeuk Jang, which is the basic movement of Taekwondo that Korea is the suzerain, as an exercise for successful aging, it is necessary to analyze physical activity level of each Taegeuk Jang (From 1 Jang through 8 Jang) and suggest the same. Therefore, in this study, I analyzed physical activity level of each Jang of Taegeuk Poomse by attaching Armband made by Body Media Company on brachia and legs below knee of Taekwondo trainees. The result of the analysis of the whole momentum from Taegeuk 1 Jang to 8 Jang is as follows: First, the average absolute value of acceleration variation of vertical direction signal (L-MAD): 5.15. Second, the average absolute value of acceleration variation of horizontal direction signal (T-MAD): 3.44. Finally, the average of calorie consumption per minute (AEE/Min): 5.06 Cal. The obtained result corresponds to proper exercise condition for successful aging and it can be utilized as data for exercise prescription for the young and the old.

  14. Solar active regions: a nonparametric statistical analysis

    CERN Document Server

    Pelt, J; Tuominen, I

    2009-01-01

    The sunspots and other solar activity indicators tend to cluster on the surface of the Sun.These clusters very often occur at certain longitudes that persist in time.It is of general interest to find new and simple ways to characterize the observed distributions of different indicators and their behaviour in time. In the present work we use Greenwich sunspot data to evaluate statistical but not totally coherent stability of sunspot distribution along latitudes as well as longitudes. The aim was to obtain information on the longitudinal distribution of the underlying spot-generating mechanism rather than on the distribution and migration of sunspots or sunspot groups on the solar surface. Therefore only sunspot groups were included in the analysis, and only the time of their first appearance was used. We use simple nonparametric approach to reveal sunspot migration patterns and their persistency. Our analysis shows that regions where spots are generated tend to rotate differentially as the spots and spot group...

  15. Applications of neutron activation analysis technique

    International Nuclear Information System (INIS)

    The technique was developed as far back as 1936 by G. Hevesy and H. Levy for the analysis of Dy using an isotopic source. Approximately 40 elements can be analyzed by instrumental neutron activation analysis (INNA) technique with neutrons from a nuclear reactor. By applying radiochemical separation, the number of elements that can be analysed may be increased to almost 70. Compared with other analytical methods used in environmental and industrial research, NAA has some unique features. These are multi-element capability, rapidity, reproducibility of results, complementarity to other methods, freedom from analytical blank and independency of chemical state of elements. There are several types of neutron sources namely: nuclear reactors, accelerator-based and radioisotope-based sources, but nuclear reactors with high fluxes of neutrons from the fission of 235U give the most intense irradiation, and hence the highest available sensitivities for NAA. In this paper, the applications of NAA of socio-economic importance are discussed. The benefits of using NAA and related nuclear techniques for on-line applications in industrial process control are highlighted. A brief description of the NAA set-ups at CERT is enumerated. Finally, NAA is compared with other leading analytical techniques

  16. Activation analysis in Europe: present and future perspectives

    International Nuclear Information System (INIS)

    A survey is given of the present-day European contribution to activation analysis, covering neutron activation analysis (NAA), charged particle activation analysis (CPAA) and photon activation analysis (PAA). Attention is paid to the available irradiation facilities, in particular nuclear reactors, cyclotrons and Van de Graaff accelerators, and linear electron accelerators. Mention is made of progress in fundamental fields, but the attention is especially focussed on practical applications: environmental, geochemical/cosmochemical, biological/medical, and high-purity materials. Eventually, the role of activation analysis in research projects of the Commission of the European Communities (CEC) and in the Reference Materials program of the Community Bureau of Reference (BCR) is emphasized

  17. Operating cost analysis of anaesthesia: Activity based costing (ABC analysis

    Directory of Open Access Journals (Sweden)

    Majstorović Branislava M.

    2011-01-01

    Full Text Available Introduction. Cost of anaesthesiology represent defined measures to determine a precise profile of expenditure estimation of surgical treatment, which is important regarding planning of healthcare activities, prices and budget. Objective. In order to determine the actual value of anaestesiological services, we started with the analysis of activity based costing (ABC analysis. Methods. Retrospectively, in 2005 and 2006, we estimated the direct costs of anestesiological services (salaries, drugs, supplying materials and other: analyses and equipment. of the Institute of Anaesthesia and Resuscitation of the Clinical Centre of Serbia. The group included all anesthetized patients of both sexes and all ages. We compared direct costs with direct expenditure, “each cost object (service or unit” of the Republican Health-care Insurance. The Summary data of the Departments of Anaesthesia documented in the database of the Clinical Centre of Serbia. Numerical data were utilized and the numerical data were estimated and analyzed by computer programs Microsoft Office Excel 2003 and SPSS for Windows. We compared using the linear model of direct costs and unit costs of anaesthesiological services from the Costs List of the Republican Health-care Insurance. Results. Direct costs showed 40% of costs were spent on salaries, (32% on drugs and supplies, and 28% on other costs, such as analyses and equipment. The correlation of the direct costs of anaestesiological services showed a linear correlation with the unit costs of the Republican Healthcare Insurance. Conclusion. During surgery, costs of anaesthesia would increase by 10% the surgical treatment cost of patients. Regarding the actual costs of drugs and supplies, we do not see any possibility of costs reduction. Fixed elements of direct costs provide the possibility of rationalization of resources in anaesthesia.

  18. Inorganic constituents determination in medicinal plants and their extracts; Determinacao dos constituintes inorganicos em plantas medicinais e seus extratos

    Energy Technology Data Exchange (ETDEWEB)

    Francisconi, Lucilaine Silva

    2014-07-01

    Different types of therapies have been introduced as an alternative treatment to combat different types of human disorders. Among them, the use of herbal teas has been highlighted by the cost/benefit, easiness of acquisition and administration. The aim of this study was to determine the inorganic constituents, and evaluate the element concentrations of As, Ba, Br, Ca, Co, Cr, Cs, Fe, Hf, K, Mg. Mn, Na, Rb, Sb, Sc, Se, Ta, Th, Ti, U, V, Zn and Zr by neutron activation analysis; and Cd, Cu, Ni and Pb, by atomic emission spectrometry, with inductively coupled plasma source and Hg, by atomic absorption spectrometry, with cold vapor generation in medicinal plants and their extracts, whose marketing was recently regulated by National Health Surveillance Agency (ANVISA). The relevance of these analyses is justified by the need of contributing to the recommendation of such plants as sources of minerals in the diet and, also, to verify if their concentrations cam pose some harm to the organism. The techniques showed adequate sensitivity in determining the concentration for most of the elements. Toxic elements were found in concentration not harmful to the human body. The results, also, allowed possible to correlate the elemental concentration in the analyzed species, by the determination the correlation coefficients and applications of cluster analysis. From these results it was confirmers in the groups of elements, regarding the variation of the concentrations observed in some plants and their extracts. The elements that play important roles in the human metabolism were determined in concentrations that can help both, to avoid the lack of these elements in the organisms, from the diet, and in treatment of disease. (author)

  19. Analysis of human enamel and dentine by neutron activation analysis

    International Nuclear Information System (INIS)

    Determination of trace elements in dental tissues has been of great interest to study the correlation between element composition and caries as well as food habits of individuals. In the present study dentine and enamel samples from healthy individuals were analysed by neutron activation analysis. The teeth were provided form dental clinics, and they were previously washed using purified water and acetone. Then they were dried at 40 deg C and ground in a agate mortar. The samples and element standards were irradiated with thermal neutrons at the IEA-R1 nuclear reactor. Long irradiations of 8 h under thermal neutron flux of 5x1012 n cm-2 s-1 were used for Ca, Na, Sr and Zn determinations. In short irradiations of 15 s and under neutron flux of 1012 n cm-2 s-1 the elements Mg, Mn, Na e Sr were determined. The induced gamma activities of the samples and standards were measured using a hyperpure Ge detector coupled to a gamma ray spectrometer. Elemental concentrations were calculated by comparative method. Results obtained showed that Ca, Mg and Na are present in both tissues at the level of percentages and the elements Mn, Sr and Zn at the μg g-1 levels. For quality control of the results the certified reference materials NIST 1400 Bone Ash and NIST 1486 Bone Meal were analysed. (author)

  20. Determination of elements in blood of golden hamster by NAA; Determinacao de elementos em sangue de hamster dourado usando AAN

    Energy Technology Data Exchange (ETDEWEB)

    Aguiar, Rodrigo Oliveira de

    2009-07-01

    In the present study Neutron Activation Analysis technique has been used to determine, simultaneously, some element concentrations of clinical relevance in whole blood samples of golden hamster. The normal range for Br, Ca, Cl K, Mg, Na and S considering 2 {sigma} (Two Standard deviations) was 0.011 0.047 gL{sup -1} (Br); 0.11 0.35 gL{sup -1} (Ca); 2.11 3.75 gL{sup -1} (Cl); 1.35 2.79 gL{sup -1} (K), 0.026 0.090 gL{sup -1} (Mg), 1.03 2.51 gL{sup -1} (Na) e 0.97 2.01 gL{sup -1} (S). The knowledge of these limits became possible to perform clinical investigation in this animal model using whole blood. The comparison with the results from human being whole blood estimation (Hamster and human) became possible to check the similarities or physiologic differences, an important data for animal experimentation. (author)

  1. Activation analysis for the Ignitor tokamak

    International Nuclear Information System (INIS)

    The purpose of the Ignitor experiment is to produce DT plasma regimes where ignition can take place. From the neutronics point of view, after a first period of machine set up and tuning in aneutronic operation, a second phase of 2.5 MeV neutron production with pure deuterium plasmas at increasing density is anticipated. After that, a transition phase to increasing percentage of tritium will be followed by several years of operations with 50% of tritium leading to short but intense 14-MeV neutron emission. To deal with the concerns due to the strong neutron emission, a detailed description of the actual Ignitor machine is implemented in the MCNP-4B Monte Carlo code to calculate the neutron fluxes in all machine components, taking in account the streaming through the ports. These fluxes are then used as input for the FISPACT-97 code for the analysis of the activation at the end of life and at intermediate times for safety assessment purposes. The resulting dose rate outside the device is also studied. The results point out that remote handling is needed for repair/maintenance of inner components following the DD operations, and that the access in the hall near the device could be restricted from the beginning of DT operations. The requirements on additional shield are discussed

  2. Application of Data Mining methods in analysis of company's activity

    OpenAIRE

    Tyurina Dina N.

    2013-01-01

    The article considers expediency of application of Data Mining means along with traditional statistical methods of analysis of financial and economic activity of a company for revealing all possible factors that influence upon effectiveness of its functioning by means of solving clusterisation tasks. It shows main advantages of application of Data Mining means in analysis of company's activity. It offers an algorithm of conduction analysis of company's activity, which facilitates significant ...

  3. Selected industrial and environmental applications of neutron activation analysis

    International Nuclear Information System (INIS)

    A review of the applications of Instrumental Neutron Activation Analysis (INAA) in the industrial and environmental fields is given. Detection limits for different applications are also given. (author)

  4. Intruder Activity Analysis under Unreliable Sensor Networks

    Energy Technology Data Exchange (ETDEWEB)

    Tae-Sic Yoo; Humberto E. Garcia

    2007-09-01

    This paper addresses the problem of counting intruder activities within a monitored domain by a sensor network. The deployed sensors are unreliable. We characterize imperfect sensors with misdetection and false-alarm probabilities. We model intruder activities with Markov Chains. A set of Hidden Markov Models (HMM) models the imperfect sensors and intruder activities to be monitored. A novel sequential change detection/isolation algorithm is developed to detect and isolate a change from an HMM representing no intruder activity to another HMM representing some intruder activities. Procedures for estimating the entry time and the trace of intruder activities are developed. A domain monitoring example is given to illustrate the presented concepts and computational procedures.

  5. High-Throughput Analysis of Enzyme Activities

    Energy Technology Data Exchange (ETDEWEB)

    Lu, Guoxin [Iowa State Univ., Ames, IA (United States)

    2007-01-01

    High-throughput screening (HTS) techniques have been applied to many research fields nowadays. Robot microarray printing technique and automation microtiter handling technique allows HTS performing in both heterogeneous and homogeneous formats, with minimal sample required for each assay element. In this dissertation, new HTS techniques for enzyme activity analysis were developed. First, patterns of immobilized enzyme on nylon screen were detected by multiplexed capillary system. The imaging resolution is limited by the outer diameter of the capillaries. In order to get finer images, capillaries with smaller outer diameters can be used to form the imaging probe. Application of capillary electrophoresis allows separation of the product from the substrate in the reaction mixture, so that the product doesn't have to have different optical properties with the substrate. UV absorption detection allows almost universal detection for organic molecules. Thus, no modifications of either the substrate or the product molecules are necessary. This technique has the potential to be used in screening of local distribution variations of specific bio-molecules in a tissue or in screening of multiple immobilized catalysts. Another high-throughput screening technique is developed by directly monitoring the light intensity of the immobilized-catalyst surface using a scientific charge-coupled device (CCD). Briefly, the surface of enzyme microarray is focused onto a scientific CCD using an objective lens. By carefully choosing the detection wavelength, generation of product on an enzyme spot can be seen by the CCD. Analyzing the light intensity change over time on an enzyme spot can give information of reaction rate. The same microarray can be used for many times. Thus, high-throughput kinetic studies of hundreds of catalytic reactions are made possible. At last, we studied the fluorescence emission spectra of ADP and obtained the detection limits for ADP under three different

  6. Neutron activation analysis of wheat samples

    Energy Technology Data Exchange (ETDEWEB)

    Galinha, C. [CERENA-IST, Technical University of Lisbon, Av. Rovisco Pais 1, 1049-001 Lisboa (Portugal); Instituto Tecnoclogico e Nuclear, URSN, E.N. 10, 2686-953 Sacavem (Portugal); Anawar, H.M. [Instituto Tecnoclogico e Nuclear, URSN, E.N. 10, 2686-953 Sacavem (Portugal); Freitas, M.C., E-mail: cfreitas@itn.pt [Instituto Tecnoclogico e Nuclear, URSN, E.N. 10, 2686-953 Sacavem (Portugal); Pacheco, A.M.G. [CERENA-IST, Technical University of Lisbon, Av. Rovisco Pais 1, 1049-001 Lisboa (Portugal); Almeida-Silva, M. [Instituto Tecnoclogico e Nuclear, URSN, E.N. 10, 2686-953 Sacavem (Portugal); Coutinho, J.; Macas, B.; Almeida, A.S. [INRB/INIA-Elvas, National Institute of Biological Resources, Est. Gil Vaz, 7350-228 Elvas (Portugal)

    2011-11-15

    The deficiency of essential micronutrients and excess of toxic metals in cereals, an important food items for human nutrition, can cause public health risk. Therefore, before their consumption and adoption of soil supplementation, concentrations of essential micronutrients and metals in cereals should be monitored. This study collected soil and two varieties of wheat samples-Triticum aestivum L. (Jordao/bread wheat), and Triticum durum L. (Marialva/durum wheat) from Elvas area, Portugal and analyzed concentrations of As, Cr, Co, Fe, K, Na, Rb and Zn using Instrumental Neutron Activation Analysis (INAA) to focus on the risk of adverse public health issues. The low variability and moderate concentrations of metals in soils indicated a lower significant effect of environmental input on metal concentrations in agricultural soils. The Cr and Fe concentrations in soils that ranged from 93-117 and 26,400-31,300 mg/kg, respectively, were relatively high, but Zn concentration was very low (below detection limit <22 mg/kg) indicating that soils should be supplemented with Zn during cultivation. The concentrations of metals in roots and straw of both varieties of wheat decreased in the order of K>Fe>Na>Zn>Cr>Rb>As>Co. Concentrations of As, Co and Cr in root, straw and spike of both varieties were higher than the permissible limits with exception of a few samples. The concentrations of Zn in root, straw and spike were relatively low (4-30 mg/kg) indicating the deficiency of an essential micronutrient Zn in wheat cultivated in Portugal. The elemental transfer from soil to plant decreases with increasing growth of the plant. The concentrations of various metals in different parts of wheat followed the order: Root>Straw>Spike. A few root, straw and spike samples showed enrichment of metals, but the majority of the samples showed no enrichment. Potassium is enriched in all samples of root, straw and spike for both varieties of wheat. Relatively to the seed used for cultivation

  7. The Analysis of Activated Carbon Regeneration Technologies

    Institute of Scientific and Technical Information of China (English)

    姚芳

    2014-01-01

    A series of methods for activated carbon regeneration were briefly introduced.Such as thermal regeneration,chemical regeneration,biochemical regeneration,and newly supercritical fluid regeneration, electrochemical regeneration,light-catalyzed regeneration,and microwave radiation method,and the developing trend of activated carbon regeneration was predicted.

  8. Karyotype Analysis Activity: A Constructivist Learning Design

    Science.gov (United States)

    Ahmed, Noveera T.

    2015-01-01

    This classroom activity is based on a constructivist learning design and engages students in physically constructing a karyotype of three mock patients. Students then diagnose the chromosomal aneuploidy based on the karyotype, list the symptoms associated with the disorder, and discuss the implications of the diagnosis. This activity is targeted…

  9. Detailed Analysis of Motor Unit Activity

    DEFF Research Database (Denmark)

    Nikolic, Mile; Sørensen, John Aasted; Dahl, Kristian;

    1997-01-01

    System for decomposition of EMG signals intotheir constituent motor unit potentials and their firing patterns.The aim of the system is detailed analysis ofmotor unit variability.......System for decomposition of EMG signals intotheir constituent motor unit potentials and their firing patterns.The aim of the system is detailed analysis ofmotor unit variability....

  10. International conference activation analysis and its applications (ICAAA): abstracts

    International Nuclear Information System (INIS)

    International conference on the Activation Analysis and its Applications was hold in Beijing of China on October 15-19, 1990. It was organized and co-sponsored by Division of Activation Analysis and Radioanalysis, National Natural Science Foundation of China and China Nuclear Society, etc.. 159 pieces of Articles in the field were received in the conference, from many countries

  11. Trace Analysis of Ancient Gold Objects Using Radiochemical Neutron Activation

    CERN Document Server

    Olariu, A; Constantinescu, O; Badica, T; Popescu, I V; Besliu, C; Leahu, D; Olariu, Agata; Constantinescu, Mioara; Leahu, Doina

    1999-01-01

    Radiochemical neutron activation analysis has been applied to investigate the microelements in gold samples with archaeological importance. Chemical separation has allowed the determination of traces of Ir, Os, Sb, Zn, Co, Fe, Ni. Instrumental neutron activation analysis has been used for the determination of Cu.

  12. Development of educational program for neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Moon, Jong Hwa; Kim, Sun Ha; Ryel, Sung; Kang, Young Hwan; Lee, Kil Yong; Yeon, Yeon Yel; Cho, Seung Yeon

    2000-08-01

    This technical report is developed to apply an educational and training program for graduate student and analyst utilizing neutron activation analysis. The contents of guide book consists of five parts as follows; introduction, gamma-ray spectrometry and measurement statistics, its applications, to understand of comprehensive methodology and to utilize a relevant knowledge and information on neutron activation analysis.

  13. Development of educational program for neutron activation analysis

    International Nuclear Information System (INIS)

    This technical report is developed to apply an educational and training program for graduate student and analyst utilizing neutron activation analysis. The contents of guide book consists of five parts as follows; introduction, gamma-ray spectrometry and measurement statistics, its applications, to understand of comprehensive methodology and to utilize a relevant knowledge and information on neutron activation analysis

  14. Large sample neutron activation analysis of a ceramic vase

    OpenAIRE

    Stamatelatos, I.E.; Tzika, F.; Vasilopoulou, T.; Koster-Ammerlaan, M.J.J.

    2010-01-01

    Large Sample Neutron Activation Analysis (LSNAA) was applied to perform non-destructive elemental analysis of a ceramic vase. Appropriate neutron self-shielding and gamma ray detection efficiency calibration factors were derived using Monte Carlo code MCNP5. The results of LSNAA were compared against Instrumental Neutron Activation Analysis (INAA) results and a satisfactory agreement between the two methods was observed. The ratio of derived concentrations between the two methods was within 0...

  15. Teaching-Learning Activity Modeling Based on Data Analysis

    Directory of Open Access Journals (Sweden)

    Kyungrog Kim

    2015-03-01

    Full Text Available Numerous studies are currently being carried out on personalized services based on data analysis to find and provide valuable information about information overload. Furthermore, the number of studies on data analysis of teaching-learning activities for personalized services in the field of teaching-learning is increasing, too. This paper proposes a learning style recency-frequency-durability (LS-RFD model for quantified analysis on the level of activities of learners, to provide the elements of teaching-learning activities according to the learning style of the learner among various parameters for personalized service. This is to measure preferences as to teaching-learning activity according to recency, frequency and durability of such activities. Based on the results, user characteristics can be classified into groups for teaching-learning activity by categorizing the level of preference and activity of the learner.

  16. HPTLC Analysis, Antioxidant and Antigout Activity of Indian Plants

    OpenAIRE

    Nile, Shivraj Hariram; Park, Se Won

    2014-01-01

    The HPTLC analysis, antioxidant, and antigout activity of Asparagus racemosus, Withania somnifera, Vitex negundo, Plumbago zeylanica, Butea monosperma and Tephrosia purpurea extracts were investigated. The chemical fingerprinting were carried out by high performance thin layer chromatography (HPTLC), antioxidant activity by ABTS, DPPH, FRAP radical scavenging assays, and antiogout activity by cow milk xanthine oxidase. The HPTLC fingerprint qualitatively revealed predominant amount of flavono...

  17. Faculty Activity Analysis in the Universidad Tecnica Del Estado Campuses.

    Science.gov (United States)

    Karadima, Oscar

    An analysis of academic activities of college faculty at the eight campuses of Chile's Universidad Tecnica del Estado was conducted. Activities were grouped into seven categories: direct teaching, indirect teaching, research, community services, faculty development, academic administration, and other activities. Following the narrative…

  18. Insurer’s activity as object of economic analysis

    Directory of Open Access Journals (Sweden)

    O.O. Poplavskiy

    2015-12-01

    Full Text Available The article is devoted to the substantiation of theoretical fundamentals of insurer’s analysis and peculiarities of its implementation. The attention has been focused on the important role of economic analysis in economic science which is confirmed by its active use in research and practical orientation. The author summarizes the classification and principles of insurer’s activity analysis, supplements it with specific principles for insurer’s environment, publicity and risk-orientation which enable increasingly to take into account the peculiarities of insurance relations. The paper pays attention to the specification of elements of analysis and its key directions including the analysis of insurer’s financing, the analysis of insurance operations and the analysis of investment activity which will allow the effective functioning of risk management system.

  19. Introduction of Prompt Gamma Thermal Neutron Activation Analysis at CARR

    Institute of Scientific and Technical Information of China (English)

    WANG; Xing-hua; XIAO; Cai-jin; ZHANG; Gui-ying; YAO; Yong-gang; JIN; Xiang-chun; WANG; Ping-sheng; HUA; Long; NI; Bang-fa

    2013-01-01

    CARR will provide with maximal neutron flux in Asia,the third of the world.By using the high quality neutron beam and the advanced international experience,Prompt Gamma Neutron Activation Analysis(PGNAA)facility will be setup at high level.PGNAA on CARR will promote the development of nuclear analysis technology and improve Chinese status in the nuclear analysis field.

  20. Determination of viability of irradiated `pera` orange protoplasts; Determinacao da viabilidade de protoplastos irradiados de laranja pera

    Energy Technology Data Exchange (ETDEWEB)

    Cristofani, M. [Instituto Agronomico de Campinas, SP (Brazil); Mendes, B.J.; Tulmann Neto, A.; Ando, A. [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil)

    1993-12-31

    The viability of sweet orange protoplants, submitted to different dosages of gamma radiation, was studied to determine the lethal dose. The analysis suggested that the viability was inversely proportional to gamma radiation and the lethal dose was established. 14 refs., 1 fig., 2 tabs.

  1. Design professional activity analysis in design management

    Directory of Open Access Journals (Sweden)

    Claudia de Souza Libanio

    2013-08-01

    Full Text Available Design use perception, as an essential element for achieving competitive advantage, also suggests the need to manage the design activities in companies. However, a few is discussed about the activity of these design professionals who participate in this process, their roles, functions and competencies, including  their connections to a company and other involved sectors. This article aims to analyze, during the design management processes, the work relations of design professionals connected to organizations both internal and externally, in order to comprehend the structure and intervenient factors on the activity of these professionals, as well as the interactions with their main coworkers. The methodology was exploratory and qualitative, using in-depth interviews with three design professionals. Subsequently, the responses were analyzed allowing the comparison of these obtained data to the theoretical bases researched. Through this case study, it was possible to realize the aspects and the structure of the design professional activity, connected intern and externally to organizations, as well as its relations with the main coworkers.

  2. Microscopic Analysis of Activated Sludge. Training Manual.

    Science.gov (United States)

    Office of Water Program Operations (EPA), Cincinnati, OH. National Training and Operational Technology Center.

    This training manual presents material on the use of a compound microscope to analyze microscope communities, present in wastewater treatment processes, for operational control. Course topics include: sampling techniques, sample handling, laboratory analysis, identification of organisms, data interpretation, and use of the compound microscope.…

  3. Active Shape Analysis of Mandibular Growth

    DEFF Research Database (Denmark)

    Hilger, Klaus Baggesen; Larsen, Rasmus; Kreiborg, Sven;

    2003-01-01

    This work contains a clinical validation using biological landmarks of a Geometry Constrained Diffusion registration of mandibular surfaces. Canonical Correlations Analysis is extended to analyse 3D landmarks and the correlations are used as similarity measures for landmark clustering. A novel Ac...

  4. ANALYSIS OF ECOLOGICAL ACTIVITY OF PODLASIE PROVINCE

    OpenAIRE

    Agnieszka Kisło; Iwona Skoczko

    2014-01-01

    The beginning of the period where the impact of human activity took dangerous size is considered to be 40 years of the nineteenth century. Then the large-scale production of electricity increased production of metallurgical industry and transport development. Significant changes contributed to rapid population growth and urbanization and industrialization processes. Man by intensive exploitation reduces or completely exhausted most natural resources. This has resulted in the availability crit...

  5. Regulatory activities of government: analysis of determinants

    Directory of Open Access Journals (Sweden)

    Primož Pevcin

    2006-12-01

    Full Text Available International comparisons show that large cross-country differences exist in the overall macro extent of regulation of the economy. In this context, the main purpose of the article is to investigate, why such differences exist by identifying and empirically verifying the effect of various factors that could potentially shape those differences. Empirical analysis based on the sample of 32 developed and democratic countries revealed that almost 70 % of variation in the macro extent of regulation could be explained with 7 statistically significant explanatory variables. The econometric analysis revealed that the macro extent of regulation decreases with income inequality in society, with the level of economic development, with the sizeof economy, with the share of transfer spending in GDP and with the share of government employment in labour force. On the other hand, the extent of regulation is positively related to government ownership of enterprises and to presidential political regime

  6. Rapid radiochemical separations in neutron activation analysis

    International Nuclear Information System (INIS)

    Rapid radiochemical separation procedures based on the removal of metal ions by columns of C18-bonded silica gel after selective complexation are examined and the simplicity of the method demonstrated by its application to the determination of Mn, Cu and Zn in neutron-activated biological material. The method is rapid and reliable and readily adaptable in all radiochemical laboratories. An alternative separation procedure for selenium in blood plasma involving desalination and concentration of the selenium protein complex by gel filtration or ultrafiltration is briefly discussed. (author)

  7. Active vision in satellite scene analysis

    Science.gov (United States)

    Naillon, Martine

    1994-01-01

    In earth observation or planetary exploration it is necessary to have more and, more autonomous systems, able to adapt to unpredictable situations. This imposes the use, in artificial systems, of new concepts in cognition, based on the fact that perception should not be separated from recognition and decision making levels. This means that low level signal processing (perception level) should interact with symbolic and high level processing (decision level). This paper is going to describe the new concept of active vision, implemented in Distributed Artificial Intelligence by Dassault Aviation following a 'structuralist' principle. An application to spatial image interpretation is given, oriented toward flexible robotics.

  8. A statistical analysis of electrical cerebral activity

    International Nuclear Information System (INIS)

    The aim of this work was to study the statistical properties of the amplitude of the electroencephalographic signal. The experimental method is described (implantation of electrodes, acquisition and treatment of data). The program of the mathematical analysis is given (calculation of probability density functions, study of stationarity) and the validity of the tests discussed. The results concerned ten rabbits. Trips of EEG were sampled during 40 s. with very short intervals (500 μs). The probability density functions established for different brain structures (especially the dorsal hippocampus) and areas, were compared during sleep, arousal and visual stimulus. Using a Χ2 test, it was found that the Gaussian distribution assumption was rejected in 96.7 per cent of the cases. For a given physiological state, there was no mathematical reason to reject the assumption of stationarity (in 96 per cent of the cases). (author)

  9. Mathematical analysis of complex cellular activity

    CERN Document Server

    Bertram, Richard; Teka, Wondimu; Vo, Theodore; Wechselberger, Martin; Kirk, Vivien; Sneyd, James

    2015-01-01

    This book contains two review articles on mathematical physiology that deal with closely related topics but were written and can be read independently. The first article reviews the basic theory of calcium oscillations (common to almost all cell types), including spatio-temporal behaviors such as waves. The second article uses, and expands on, much of this basic theory to show how the interaction of cytosolic calcium oscillators with membrane ion channels can result in highly complex patterns of electrical spiking. Through these examples one can see clearly how multiple oscillatory processes interact within a cell, and how mathematical methods can be used to understand such interactions better. The two reviews provide excellent examples of how mathematics and physiology can learn from each other, and work jointly towards a better understanding of complex cellular processes. Review 1: Richard Bertram, Joel Tabak, Wondimu Teka, Theodore Vo, Martin Wechselberger: Geometric Singular Perturbation Analysis of Burst...

  10. Diagnosis of mucoviscidosis by neutron activation analysis. Part 1

    International Nuclear Information System (INIS)

    Symptoms pathology, incidence, and gravity of the inherent syndrome called mucoviscidosis, or cystic fibrosis are described in this Part I. The analytical methods used for its diagnosis, both the conventional chemical ones and by neutron activation analysis are also summarised. Finally, an analytical method to study the incidence of mucoviscidosis in Brazil is presented. This , essentially, consists in bromine determination, in fingernails, by resonance neutron activation analysis. (author)

  11. Evaluation of methods for wax determination in crude oil; Avaliacao de metodos de determinacao de parafinas em petroleo

    Energy Technology Data Exchange (ETDEWEB)

    Dias, Julio Cesar M.; Silva, Maria do Socorro A.J. da; Vasconcellos, Rosa C.U. [PETROBRAS S.A., Rio de Janeiro, RJ (Brazil). Centro de Pesquisas; Tamanqueira, Juliana B. [Fundacao Gorceix, Ouro Preto, MG (Brazil)

    2008-07-01

    Determining the wax content of crude oil is of great importance for petroleum industry, especially for production, storage and transportation of crude oils. Many different methodologies of wax determining are available in the technical literature. However, the selection of the most suitable method must be in accordance with the aim of the analysis and observing the specificities of each technique. The purpose of this work was to determine the performance of different techniques of wax determining applied to characterization of precipitation properties of waxy compounds in crude oils. Twelve samples of crude oils proceeding from the main Brazilian oil producing sedimentary basins were selected for this study. These samples were analyzed by three important analytical techniques of wax determining: precipitation by cooled solvent; liquid chromatography with precipitation by cooled solvent; and liquid chromatography followed by gas chromatography. Differential scanning calorimetry data related to the wax crystallization in these oils were used as parameters of validation. The results obtained in this study indicate that the liquid chromatography followed by gas chromatography method has the best performance for wax determining in crude oils. (author)

  12. Determination of radioactive materials in granite used as ornamental rocks; Determinacao de materiais radioativos em granitos utilizados como rochas ornamentais

    Energy Technology Data Exchange (ETDEWEB)

    Salas, Humberto Terrazas; Barbosa, Joao Batista Santos; Murta, Clecio Campi; Rocha, Francisco de Assis [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN), Belo Horizonte, MG (Brazil)). E-mail: salasht@urano.cdtn.br; Nalini Junior, Herminio Arias; Mendes, Julio Cesar [Ouro Preto Univ., MG (Brazil). Escola de Minas. Dept. de Geologia

    2000-07-01

    For environment quality control, either in a global or regional perspective, the determination of the radioactivity present in the minerals of rocks must be included. This control is carried out through specific analysis, applied to all geological materials used in civil architecture design and other applications (e.g. artistic). To date, the radioactivity of rocks has not been specifically studied, from which an adequate and comprehensive systematics is applied, in order to determine the radioactive minerals and their corresponding alterations. In Brazil, the industry of ornamental rocks is continually increasing at high rates, with a growing variety of rocks being commercialized locally as well as abroad. To a certain extent, the technical characterization of these rocks, through standard procedures defined by standardization institutions, is already available worldwide. However, among the petrographic properties specified for these rocks, minor or accessory minerals (less than 1%) are not adequately determined and detected. Among these components are radioactive minerals and, occasionally, carriers of precious metals, rare earths and other economically important minerals. (author)

  13. Prompt Gamma-Ray Neutron Activation Analysis (PGNAA) for Elemental Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Robin P. Gardner

    2006-04-11

    This research project was to improve the prompt gamma-ray neutron activation analysis (PGNAA) measurement approach for bulk analysis, oil well logging, and small sample thermal enutron bean applications.

  14. ANALYSIS OF ECOLOGICAL ACTIVITY OF PODLASIE PROVINCE

    Directory of Open Access Journals (Sweden)

    Agnieszka Kisło

    2014-01-01

    Full Text Available The beginning of the period where the impact of human activity took dangerous size is considered to be 40 years of the nineteenth century. Then the large-scale production of electricity increased production of metallurgical industry and transport development. Significant changes contributed to rapid population growth and urbanization and industrialization processes. Man by intensive exploitation reduces or completely exhausted most natural resources. This has resulted in the availability criterion, which is distinguished by inexhaustible and exhaustible resources. Exhaustible resources may include solar, wind, energy, ocean currents and the energy of the Earth. Exhaustible resources, however, are the elements of nature that as a result of the operation can be completely depleted or destroyed. These resources include: water, soil, plant world, animal world natural resources. The greater the intensity of acquiring human resources, the faster will be the depleted. There is also a very important division of exhaustible resources: non-renewable resources, renewable and very difficult reproducible (living areas. Non-renewable resources are mainly minerals, such as iron ore, crude oil, coal, sulfur, natural gas, useful stones, limestone, salt, and many other minerals. After extraction resources are processed, and the bed from which they were extracted can no longer be used. It is different from renewable resources; they are characterized by the fact that over time they are reconstituted, although, for this to happen balance of the environment through the rational use must be maintained. These resources include, among others, soil, water, flora and fauna, as well as atmospheric air.

  15. Analysis of supercooling activities of surfactants.

    Science.gov (United States)

    Kuwabara, Chikako; Terauchi, Ryuji; Tochigi, Hiroshi; Takaoka, Hisao; Arakawa, Keita; Fujikawa, Seizo

    2014-08-01

    Supercooling-promoting activities (SCAs) of 25 kinds of surfactants including non-ionic, anionic, cationic and amphoteric types were examined in solutions (buffered Milli-Q water, BMQW) containing the ice nucleation bacterium (INB) Erwinia ananas, silver iodide (AgI) or BMQW alone, which unintentionally contained unidentified ice nucleators, by a droplet freezing assay. Most of the surfactants exhibited SCA in solutions containing AgI but not in solutions containing the INB E. ananas or BMQW alone. SCAs of many surfactants in solutions containing AgI were very high compared with those of previously reported supercooling-promoting substances. Cationic surfactants, hexadecyltrimethylammonium bromide (C16TAB) and hexadecyltrimethylammonium chloride (C16TAC), at concentrations of 0.01% (w/v) exhibited SCA of 11.8 °C, which is the highest SCA so far reported. These surfactants also showed high SCAs at very low concentrations in solutions containing AgI. C16TAB exhibited SCA of 5.7 °C at a concentration of 0.0005% (w/v). PMID:24792543

  16. Spatiotemporal Data Mining, Analysis, and Visualization of Human Activity Data

    Science.gov (United States)

    Li, Xun

    2012-01-01

    This dissertation addresses the research challenge of developing efficient new methods for discovering useful patterns and knowledge in large volumes of electronically collected spatiotemporal activity data. I propose to analyze three types of such spatiotemporal activity data in a methodological framework that integrates spatial analysis, data…

  17. Applying an Activity System to Online Collaborative Group Work Analysis

    Science.gov (United States)

    Choi, Hyungshin; Kang, Myunghee

    2010-01-01

    This study determines whether an activity system provides a systematic framework to analyse collaborative group work. Using an activity system as a unit of analysis, the research examined learner behaviours, conflicting factors and facilitating factors while students engaged in collaborative work via asynchronous computer-mediated communication.…

  18. Performance analysis of active schedules in identical parallel machine

    Institute of Scientific and Technical Information of China (English)

    Changjun WANG; Yugeng XI

    2007-01-01

    Active schedule is one of the most basic and popular concepts in production scheduling research. For identical parallel machine scheduling with jobs' dynamic arrivals, the tight performance bounds of active schedules under the measurement of four popular objectives are respectively given in this paper. Similar analysis method and conclusions can be generalized to static identical parallel machine and single machine scheduling problem.

  19. Project-Based Language Learning: An Activity Theory Analysis

    Science.gov (United States)

    Gibbes, Marina; Carson, Lorna

    2014-01-01

    This paper reports on an investigation of project-based language learning (PBLL) in a university language programme. Learner reflections of project work were analysed through Activity Theory, where tool-mediated activity is understood as the central unit of analysis for human interaction. Data were categorised according to the components of human…

  20. Applied research of environmental monitoring using instrumental neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Young Sam; Moon, Jong Hwa; Chung, Young Ju

    1997-08-01

    This technical report is written as a guide book for applied research of environmental monitoring using Instrumental Neutron Activation Analysis. The contents are as followings; sampling and sample preparation as a airborne particulate matter, analytical methodologies, data evaluation and interpretation, basic statistical methods of data analysis applied in environmental pollution studies. (author). 23 refs., 7 tabs., 9 figs.

  1. Supply and demand analysis of leisure activities in selected region

    OpenAIRE

    Helcl, Petr

    2014-01-01

    The Thesis on the topic "Supply and demand analysis of leisure activities in the region," focuses on the forms of spending free time in the selected region. The theoretical part deals with the study of scientific publications focusing on leisure and leisure education. The economic concepts are examined to define the work, factors affecting leisure adults and content of leisure activities and leisure educational activities. The legal system of the Czech Republic defining the possibilities of a...

  2. Neutron activation analysis for environmental sample in Thailand

    Energy Technology Data Exchange (ETDEWEB)

    Busamongkol, Arporn; Nouchpramool, Sunun; Bunprapob, Supamatthree [Office of Atomic Energy for Peace, Bangkok (Thailand); Sumitra, Tatchai [Chulalongkorn Univ., Dept. of Nuclear Technology, Bangkok (Thailand)

    2003-03-01

    Neutron Activation Analysis has been applied for the trace elements analysis in environmental samples. Thirty three samples of airborne particulate were collected every week at Ongkharak Nuclear Research Center (ONRC) during the period of June 1998 to March 1999. The Ti, I, Mg, Na, V, K, Cl, Al, Mn, Ca, As, Sm, Sb, Br, La, Ce, Th, Cr, Cs, Sc, Rb, Fe, Zn and Co were analyzed by Neutron Activation Analysis utilizing 2 MW TRIGA MARK III research reactor. The certified reference materials 1632a and 1633a from National Bureau of Standard were select as standard. (author)

  3. Determination of essential elements in formulas commercialized at the Sao Paulo state, Brazil; Determinacao de elementos essenciais em formulas infantis comercializadas em Sao Paulo-Brasil

    Energy Technology Data Exchange (ETDEWEB)

    Campos, Vinicius Dias; Vallinoto, Priscila; Maihara, Vera Akiko, E-mail: pvallinoto@ipen.br, E-mail: vmaihara@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2011-07-01

    This paper intends to determine the concentration of elements, presents in the infant formulas, by using the Neutron Activation Analysis for verification if the quantity is not exceeding the toxicity limit, and if the concentration of each element is correct as presented on the label of each packaging

  4. Activation analysis in the environment: Science and technology

    International Nuclear Information System (INIS)

    Science is disciplined curiosity. Activation analysis was created more than 50 yr ago by Hevesy's curiosity and Levi's experimental skill. Technology is the exploitation of machines and materials for the fulfillment of human needs or wants. The early history of neutron activation analysis (NAA) was greatly influenced by military requirements. Since then the technique has found applications in many disciplines, including materials science, medicine, archaeology, geochemistry, agriculture, and forensic science. More recently, neutron activation analysts, responding to increasing public interest and concern, have made distinctive contributions to the study of environmental problems. Activation analysis, though it uses some procedures derived from physics, is essentially a chemical technique. The chemical study of the environment may be reviewed under many headings; three are discussed here: 1. occupational medicine 2. health of the general public 3. environmental pollution

  5. Cytotoxic activity and phytochemical analysis of Arum palaestinum Boiss

    Institute of Scientific and Technical Information of China (English)

    Mai Mohammed Farid; Sameh Reda Hussein; Lamiaa Fawzy Ibrahim; Mohammed Ali El Desouky; Amr Mohammed Elsayed; Ahmad Ali El Oqlah; Mahmoud Mohammed Saker

    2015-01-01

    Objective:To evaluate the in vitro cytotoxic activity of the fractionated extract as well as isolated compounds of Arum palaestinum Boiss. (A. palaestinum) (black calla lily), and to identify the volatile components which may be responsible for the potential antitumor activity. Methods: A. palaestinum was collected from its natural habitats and subjected to phytochemical analysis for separation of pure compounds. In vitro cytotoxic activity was investigated against four human carcinoma cell lines Hep2, HeLa, HepG2 and MCF7 for the fractionated extract and isolated compounds. While, the diethyl ether fraction was subjected to GC–MS analysis as it exhibited the most potent cytotoxic effect to evaluate the active constituents responsible for the cytotoxic activities. Results:Four flavonoid compounds were isolated (luteolin, chrysoeriol, isoorientin, isovitexin) from the diethyl ether and ethyl acetate. The extracts and the pure isolated compounds showed a significant high antiproliferative activity against all investigated cell lines. The GC–MS analysis revealed the separation and identification of 15 compounds representing 95.01%of the extract and belonging to different groups of chemical compounds. Conclusions:The present study is considered to be the first report on the cytotoxic activities carried out on different selected fractions and pure compounds of A. palaestinum to provide evidences for its strong antitumor activities. In addition, chrysoeriol and isovitexin compounds were isolated for the first time from the studied taxa.

  6. Cytotoxic activity and phytochemical analysis of Arum palaestinum Boiss.

    Institute of Scientific and Technical Information of China (English)

    Mai; Mohammed; Farid; Sameh; Reda; Hussein; Lamiaa; Fawzy; Ibrahim; Mohammed; Ali; El; Desouky; Amr; Mohammed; Elsayed; Ahmad; Ali; El; Oqlah; Mahmoud; Mohammed; Saker

    2015-01-01

    Objective: To evaluate the in vitro cytotoxic activity of the fractionated extract as well as isolated compounds of Arum palaestinum Boiss.(A. palaestinum)(black calla lily), and to identify the volatile components which may be responsible for the potential antitumor activity.Methods: A. palaestinum was collected from its natural habitats and subjected to phytochemical analysis for separation of pure compounds. In vitro cytotoxic activity was investigated against four human carcinoma cell lines Hep2, He La, Hep G2 and MCF7 for the fractionated extract and isolated compounds. While, the diethyl ether fraction was subjected to GC–MS analysis as it exhibited the most potent cytotoxic effect to evaluate the active constituents responsible for the cytotoxic activities.Results: Four flavonoid compounds were isolated(luteolin, chrysoeriol, isoorientin,isovitexin) from the diethyl ether and ethyl acetate. The extracts and the pure isolated compounds showed a significant high antiproliferative activity against all investigated cell lines. The GC–MS analysis revealed the separation and identification of 15 compounds representing 95.01% of the extract and belonging to different groups of chemical compounds.Conclusions: The present study is considered to be the first report on the cytotoxic activities carried out on different selected fractions and pure compounds of A. palaestinum to provide evidences for its strong antitumor activities. In addition,chrysoeriol and isovitexin compounds were isolated for the first time from the studied taxa.

  7. MODEL OF ACTIVITY OF THE ENTERPRISE AS MODEL OF ACTIVITY OF THE HUMAN: SEARCH ANALYSIS

    Directory of Open Access Journals (Sweden)

    Ruslan Flerovich Vildanov

    2014-09-01

    Full Text Available Actualized demand of manufactury company's efficiency from the point of quality charachteristics. Reveal unbreakable connection of man and organisation, on example of the comparative analysis of man's and manufacture company's activities. Studing models of company's and men's activities in order to reveal similarity. In order of their implementation to the economics assumes opportunity of using scientific methods, which use for studying functions, vital activities and behavior of the men.

  8. A package for gamma-ray spectrum analysis and routine neutron activation analysis

    Indian Academy of Sciences (India)

    M E Medhat; A Abdel-Hafiez; Z Awaad; M A Ali

    2005-08-01

    A package for gamma spectrum analysis (PGSA) was developed using object oriented Borland C++ design for MS-windows. This package consists of five programs which can be used for gamma-ray spectrum analysis and routine neutron activation analysis. The advantages of PGSA are its simple algorithms and its need for only minimum amount of input information.

  9. Analysis of nuclear activity of ten polar ring galaxies

    CERN Document Server

    Freitas-Lemes, P; Dors, O L; Faúndez-Abans, M

    2013-01-01

    The accumulation of mass from the interaction process that forms the polar ring galaxies is a factor that favors the conditions necessary to trigger nonthermal nuclear activities.. This fact encouraged the chemical analysis of ten polar ring galaxies. In order to verify the presence of an active nucleus in these galaxias, we built diagnostic diagrams using lines H{\\beta}, [OIII], [HI], H{\\alpha}, [NII], and [SII] and classified the type of nuclear activity. For galaxies that do not show shock, the parameters N2 and O3N2 were also determined. From this sample, we identified seven galaxies with an active nucleus and three that behave as HII regions. One galaxy with an active nucleus was classified as Seyfert. Although our data do not provide a statistically significant sample, we can speculate that polar ring galaxies are a setting conducive to trigger non-thermal nuclear activities.

  10. Methodology for determination of activity of radionuclides by gamma spectrometry; Metodologia para determinacao da atividade de radionuclideos por sistema de espectrometria gama

    Energy Technology Data Exchange (ETDEWEB)

    Fragoso, Maria da Conceicao de Farias; Oliveira, Victor Rogerio S. de; Oliveira, Mercia L.; Lima, Fernando Roberto de Andrade, E-mail: mariacc05@gmail.com [Centro Regional de Ciencias Nucleares do Nordeste (CRCN-NE/CNEN-NE), Recife, PE (Brazil)

    2014-07-01

    Due to the growth in the number of procedures that make use of the positron emission tomography (PET), there is a need for standard solutions for the calibration of the systems used for the measurement of the PET radiopharmaceutical (activimeter) in radiopharmacies and in nuclear medicine services. Among the existing alternatives for the standardization of radioactive sources, the method known as gamma spectrometry is widely used for short-lived radionuclides. The purpose of this study was to implement the methodology for standardization of the {sup 18}F solutions by gamma spectrometry at the Regional Center for Nuclear Sciences of the Northeast (CRCN-NE/CNEN-NE), Brazil. (author)

  11. Determination of the crust thickness in the active margin of the Antarctic region; Determinacao da estrutura crustal na margem ativa da regiao antartica

    Energy Technology Data Exchange (ETDEWEB)

    Torres, Luiz Carlos; Gamboa, Luiz Antonio Pierantoni [Universidade Federal Fluminense, Niteroi, RJ (Brazil). Lagemar; Gomes, Benedito Souza [PETROBRAS, Rio de Janeiro, RJ (Brazil)

    1997-07-01

    Seismic multichannel, gravity and magnetometry measurements were carried out in the region of West coast of the Antarctic Peninsula, Bransfield Strait, South Shetland Islands and South Shetland Trench, by Brazilian Antarctic Program during the summers of 1987 and 1988. The present work, using a continue seismic and gravity and gravity data profile crossing the area, intends to present a two-dimensional model of the crust thickness in this region. By this model, the Moho discontinuity would lie at a depth of 14.5 km below the axis of the Bransfield trough. This anomalous behaviour in addition to compressional processes identified in the accretionary prism and trench, was interpreted as an evidence of the continued opening of the Bransfield basin. (author)

  12. Status Report on the Neutron Activation Analysis Activities in the Philippines

    International Nuclear Information System (INIS)

    The Philippines has a one megawatt open-pool type nuclear research reactor which is presently utilized in the conduct of nuclear research and development activities. The reactor is operated by the Philippine Atomic Research Center, the research arm of the Philippine Atomic Energy Commission. The reactor is presently utilized in the production of some radioisotopes, nuclear physics experiments and neutron activation analysis. For activation analysis the facilities available include the two 2 inch pneumatic tubes and a 2-inch central core dry-pipe. Although the reactor has been operative since 1963 it was only in the latter part of 1966 that a neutron activation analysis group was organized and almost immediately the training of personnel and setting up of a radiochemical laboratory and nucleonic counting assembly were initiated. Today, the counting system include a 100 channel analyzer with a 3 x 3 inch Nal(Tl) crystal

  13. Survey on Neutron Activation Analysis Activities at the Dalat Nuclear Research Centre

    International Nuclear Information System (INIS)

    The Dalat Nuclear Research Centre (D.N.R.C.) during the past few years has been involved in conducting an activation analysis service. Work has been carried out in collaboration with other organizations. However, no rigid research programme of our own has been established and thus the Radiochemistry Division of the D.N.R.C. has no personnel and special facilities permanently engaged in this field. The equipment and facilities used are shared with other activities within the Division and the whole Centre. The activities in neutron activation analysis at the D.N.R.C. are sporadically revived by requests for analysis. Up to now, such analyses have been performed free of charge. Most of the work was carried out on biological materials such as vegetables, raw natural rubber (RES smoked sheets of different qualities, crepes and dried rubber films obtained from concentrated natural latex) from hevea tree leaves from various clones

  14. Performance Analysis for Dispensing Mechanism of Active Code

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    The dispensing mechanism of active code is a key technology in an active network. Conventional capsule and programmable switch approaches have their own shortcomings. The DCCAN(distributed code caching for active network) mechanism presented in this paper overcomes these shortcomings. In this paper, capsule and programmable switch approaches are introduced, and their shortcomings are analyzed. The principle of the DCCAN mechanism is described. The theory analysis in transmit width based on the DCCAN mechanism and capsule approach are described. The theory analysis shows that the DCCAN mechanism has many good characteristics and can improve the efficiency of an active network. Key factors which affect the transmit width based on the DCCAN mechanism are discussed. The using condition of the DCCAN mechanism is also discussed.

  15. Visual Analysis of Biological Activity Data with Scaffold Hunter.

    Science.gov (United States)

    Klein, Karsten; Koch, Oliver; Kriege, Nils; Mutzel, Petra; Schäfer, Till

    2013-12-01

    The growing interest in chemogenomics approaches over the last years has led to an increasing amount of data regarding chemical and the corresponding biological activity space. The resulting data, collected in either in-house or public databases, need to be analyzed efficiently to speed-up the increasingly difficult task of drug discovery. Unfortunately, the discovery of new chemical entities or new targets for known drugs ('drug repurposing') is not suitable to a fully automated analysis or a simple drill down process. Visual interactive interfaces that allow to explore chemical space in a systematic manner and facilitate analytical reasoning can help to overcome these problems. Scaffold Hunter is a tool for the visual analysis of chemical compound databases that provides integrated visualization and analysis of biological activity data and fosters the interactive exploration of data imported from a variety of sources. We describe the features and illustrate the use by means of an exemplary analysis workflow.

  16. Neutron Activation Analysis for investigation of elemental composition of Amarantus

    International Nuclear Information System (INIS)

    In this work instrumental neutron activation analysis is applied for the characterization of the elemental composition of Amaranthus seeds, known in the prehistorical period, a tropical plant with promising nutritional and economic value. The characterization is enriched by the results of radiochemical neutron activation analysis for cobalt, molybdenum and uranium content. The comparison of the results, for three sorts of edible flour, commercially available: Soya Flour, Corn Bean Flour and Amaranthus Flour, is presented. The validation of the analytical methods used was carried out on the basis of participation in the interlaboratory comparison organized by the INCT (INCT-TL-1, INCT-MPH-2) and by NIST (SRM 1575a). (author)

  17. Xenon diffusion studies with prompt gamma activation analysis

    International Nuclear Information System (INIS)

    Developing a better understanding of xenon transport through porous systems is critical to predicting how this gas will enter the atmosphere after a below ground nuclear weapons test. Radioxenon monitoring is a vital part of the Comprehensive Nuclear-Test-Ban Treaty (CTBT) International Monitoring System. This work details the development of prompt gamma activation analysis for measuring the diffusion rates of xenon and argon gases through a porous medium. The University of Texas at Austin maintains a prompt gamma activation analysis facility with a peak neutron flux of ∼ 1.5 x 107 cm-2 s-1 and a beam diameter of 1 cm. Due to the relatively large prompt gamma cross sections of many stable xenon isotopes at thermal and sub-thermal neutron energies, prompt gamma activation analysis is a suitable technique for in situ non-destructive analysis of natural xenon. A test chamber has been designed and constructed to utilize prompt gamma activation analysis to measure xenon and argon diffusion through geological materials (e.g., sand, soil, etc.). Initial experiments have been conducted to determine the detection limits for stable gas measurements. The results from these experiments will be utilized to benchmark parts of a xenon transport model that is being used to determine diffusion coefficients for xenon and argon. (author)

  18. DNQAA program to be used in activation analysis

    International Nuclear Information System (INIS)

    The concentrations of the analysed elements were calculated by the program, based on the instrumental technique of analysis by activation. The DNQAA corrects due to the radioactive decay and to the neutron flow variation or carried particles and too the error propagation involved in the analysis. It is written in ORACL to be used in the ORTEC 6240-42 system. (L.M.J.)

  19. Instrumental Neuron Activation Analysis for certification of stainless steel materials

    International Nuclear Information System (INIS)

    The use of Instrumental Neuron Activation Analysis (INAA) may contribute to improve the certification of the materials, especially in the case of minor and trace elements. In presented paper the INAA method of analysis of stainless steel materials has been elaborated. The obtained results were compared with those of common analytical techniques. The presented results show the usefulness of the INAA method for the certification of CRMs for the iron and steel industry

  20. Structural Analysis Extended with Active Fault Isolation - Methods and Algorithms

    DEFF Research Database (Denmark)

    Gelso, Esteban R.; Blanke, Mogens

    2009-01-01

    Isolability of faults is a key issue in fault diagnosis whether the aim is maintenance or active fault-tolerant control. It is often encountered that while faults are detectable, they are only group-wise isolable from a usual diagnostic point of view. However, active injection of test signals on...... system inputs can considerably enhance fault isolability. This paper investigates this possibility of active fault isolation from a structural point of view. While such extension of the structural analysis approach was suggested earlier, algorithms and case studies were needed to explore this theory. The...

  1. Cluster analysis of activity-time series in motor learning

    DEFF Research Database (Denmark)

    Balslev, Daniela; Nielsen, Finn Årup; Frutiger, Sally A.;

    2002-01-01

    Neuroimaging studies of learning focus on brain areas where the activity changes as a function of time. To circumvent the difficult problem of model selection, we used a data-driven analytic tool, cluster analysis, which extracts representative temporal and spatial patterns from the voxel...... practice-related activity in a fronto-parieto-cerebellar network, in agreement with previous studies of motor learning. These voxels were separated from a group of voxels showing an unspecific time-effect and another group of voxels, whose activation was an artifact from smoothing. Hum. Brain Mapping 15...

  2. Cluster analysis of activity-time series in motor learning

    DEFF Research Database (Denmark)

    Balslev, Daniela; Nielsen, Finn Å; Futiger, Sally A;

    2002-01-01

    Neuroimaging studies of learning focus on brain areas where the activity changes as a function of time. To circumvent the difficult problem of model selection, we used a data-driven analytic tool, cluster analysis, which extracts representative temporal and spatial patterns from the voxel...... practice-related activity in a fronto-parieto-cerebellar network, in agreement with previous studies of motor learning. These voxels were separated from a group of voxels showing an unspecific time-effect and another group of voxels, whose activation was an artifact from smoothing...

  3. IN VITRO ANALYSIS OF MIGRATION ACTIVITY OF ENCEPHALYTOGENIC T CEL

    Directory of Open Access Journals (Sweden)

    M. A. Nosov

    2010-01-01

    Full Text Available Experimental autoimmune encephalomyelitis in an adoptive transfer model is caused by injecting animal with activated T cells specific for a CNS antigen, e.g., basic myelin protein. Development of autimmune inflammation in such a model is connected with changed functional stateof encephalytogenic (EG T cells in the coure of disease progression, as reflected by changes in their activation, proliferation and motility levels. Present work describes an original technique allowing for in vitro analysis of encephalytogenic T cell motility, and studying effects of certain compomemts of extracellular matrix upon migration and functional activities of EG T cells.

  4. Aerosol and air pollution study by neutron activation analysis

    International Nuclear Information System (INIS)

    Thermal neutron activation analysis technique was used in air pollution and aerosol elemental content and size distribution investigations. Air pollution samples were collected on Whatman 41 paper filters which were activated along with known quantities of standards in a flux of approximately 1013 nxcm-2xs-1. The activity of the samples was measured with a 40 cm3 Ge(Li) detector and analyzed with the computer program JANE, which identified the isotopes and found their quantities by normalization with the standard measurement results. Correlation between the various elements, in particular those belonging to dust from the desert and those considered typical urban air pollution, is investigated. (author)

  5. Nondestructive multielemental analysis of ancient roman pottery using photon activation analysis techniques

    International Nuclear Information System (INIS)

    Several analytical methods were tested for the multiparameter-analysis of ancient roman pottery in order to elaborate a procedure for their identification. Main constituents, minor and trace-elements have been analyzed by high-energy photon activation analysis, followed by high resolution gamma spectroscopy. The environmental influence on the concentrations of the minor constituents and trace elements during deposition of the sherds in the soil has been examined. A comparison has been made between analysis data of ancient pottery obtained by photon activation analysis, X-ray fluorescence analysis and 14 MeV neutron activation analysis. Tables are given on the time dependence of the trace elements. The numerical data are summarized in several diagrams. (T.G.)

  6. Analysis by Neutron activation of the Calakmul jadeite mask

    International Nuclear Information System (INIS)

    It is very important to know the elemental composition of archaeological materials with the purpose to find relations that allow to establish their origin standards. the origin and present localization of pre hispanic archaeological pieces can lead to the determination of commercial routes and of technology transfer among different ancient cultures. In the present work it has been realized a systematic analysis using the Instrumental neutron activation analysis technique of three samples obtained from Calakmul jadeite mask, tomb I, that in addition to give a composition of constituent and trace elements detected by this technique it has leaded to establish an applicable methodology to the routine analysis of ceramics of historical interest. (Author)

  7. Statistical analysis of acoustic wave parameters near active regions

    CERN Document Server

    Soares, M Cristina Rabello; Scherrer, Philip H

    2016-01-01

    In order to quantify the influence of magnetic fields on acoustic mode parameters and flows in and around active regions, we analyse the differences in the parameters in magnetically quiet regions nearby an active region (which we call `nearby regions'), compared with those of quiet regions at the same disc locations for which there are no neighboring active regions. We also compare the mode parameters in active regions with those in comparably located quiet regions. Our analysis is based on ring diagram analysis of all active regions observed by HMI during almost five years. We find that the frequency at which the mode amplitude changes from attenuation to amplification in the quiet nearby regions is around 4.2 mHz, in contrast to the active regions, for which it is about 5.1 mHz. This amplitude enhancement (the `acoustic halo effect') is as large as that observed in the active regions, and has a very weak dependence on the wave propagation direction. The mode energy difference in nearby regions also changes...

  8. Statistical Analysis of Acoustic Wave Parameters Near Solar Active Regions

    Science.gov (United States)

    Rabello-Soares, M. Cristina; Bogart, Richard S.; Scherrer, Philip H.

    2016-08-01

    In order to quantify the influence of magnetic fields on acoustic mode parameters and flows in and around active regions, we analyze the differences in the parameters in magnetically quiet regions nearby an active region (which we call “nearby regions”), compared with those of quiet regions at the same disk locations for which there are no neighboring active regions. We also compare the mode parameters in active regions with those in comparably located quiet regions. Our analysis is based on ring-diagram analysis of all active regions observed by the Helioseismic and Magnetic Imager (HMI) during almost five years. We find that the frequency at which the mode amplitude changes from attenuation to amplification in the quiet nearby regions is around 4.2 mHz, in contrast to the active regions, for which it is about 5.1 mHz. This amplitude enhacement (the “acoustic halo effect”) is as large as that observed in the active regions, and has a very weak dependence on the wave propagation direction. The mode energy difference in nearby regions also changes from a deficit to an excess at around 4.2 mHz, but averages to zero over all modes. The frequency difference in nearby regions increases with increasing frequency until a point at which the frequency shifts turn over sharply, as in active regions. However, this turnover occurs around 4.9 mHz, which is significantly below the acoustic cutoff frequency. Inverting the horizontal flow parameters in the direction of the neigboring active regions, we find flows that are consistent with a model of the thermal energy flow being blocked directly below the active region.

  9. Application of prompt gamma-ray activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Park, Kwang Won; Moon, Jong Hwa; Kim, Sun Ha; Baek, Sung Ryel [Korea Atomic Energy Research Institute, Taejeon (Korea)

    2002-03-01

    This technical report is written for the promotion to utilization of prompt gamma-ray activation analysis facility to be installed in HANARO reactor. It is described for a practical aspects including experiment and equipments, methodology, current status of the research and development and its applications. 102 refs., 32 figs., 25 tabs. (Author)

  10. Making Sense of Total VET Activity: An Initial Market Analysis

    Science.gov (United States)

    National Centre for Vocational Education Research (NCVER), 2016

    2016-01-01

    Following the successful first national publication of total vocational education and training (VET) activity and presentation of various informative data products, NCVER has continued to undertake further analysis of the submitted data. This paper is the first in a suite of the National Centre for Vocational Education Research (NCVER) authored…

  11. Neutron activation analysis - an aid to forensic science

    International Nuclear Information System (INIS)

    Forensic Science is oriented towards the examination of evidence specimens, collected from a scene of crime in order to establish the link between the criminal and the crime. This science therefore has a profound role to play in criminal justice delivery system. The importance of neutron activation analysis (NAA) as a specialised technique to aid crime investigation has emerged and has been recognised

  12. Instrumental neutron activation analysis of some ayurvedic medicines: Pt. 1

    Energy Technology Data Exchange (ETDEWEB)

    Rajurkar, N.S.; Vinchurkar, M.S. (Poona Univ., Pune (India). Dept. of Chemistry)

    1992-12-01

    Several medicines have been manufactured and prescribed to overcome mineral deficiencies in the human body. Such medicines are mixtures of several components. The present work is undertaken to analyze various Ayurvedic medicines, mainly of herbal origin and used for different purposes, for their elemental contents, by neutron activation analysis. (author).

  13. Neutron activation analysis of final molasses from the sugar industry

    International Nuclear Information System (INIS)

    Molasses samples from 74 factories were analyzed by neutron activation analysis. The concentration values of the 35 elements was determined. The toxicity and the influence of the presence of theses elements in sugar loss in the molasses and fermentative process is discussed

  14. Development of HANARO Activation Analysis System and Utilization Technology

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Y. S.; Moon, J. H.; Cho, H. J. (and others)

    2007-06-15

    1. Establishment of evaluation system using a data for a neutron activation analysis : Improvement of NAA measurement system and its identification, Development of combined data evaluation code of NAA/PGAA, International technical cooperation project 2. Development of technique for a industrial application of high precision gamma nuclide spectroscopic analysis : Analytical quality control, Development of industrial application techniques and its identification 3. Industrial application research for a prompt gamma-ray activation analysis : Improvement of Compton suppression counting system (PGAA), Development of applied technology using a PGAA system 4. Establishment of NAA user supporting system and KOLAS management : Development and validation of KOLAS/ISO accreditation testing and identification method, Cooperation researches for a industrial application, Establishment of integrated user analytical supporting system, Accomplishment of sample irradiation facility.

  15. Development of HANARO Activation Analysis System and Utilization Technology

    International Nuclear Information System (INIS)

    1. Establishment of evaluation system using a data for a neutron activation analysis : Improvement of NAA measurement system and its identification, Development of combined data evaluation code of NAA/PGAA, International technical cooperation project 2. Development of technique for a industrial application of high precision gamma nuclide spectroscopic analysis : Analytical quality control, Development of industrial application techniques and its identification 3. Industrial application research for a prompt gamma-ray activation analysis : Improvement of Compton suppression counting system (PGAA), Development of applied technology using a PGAA system 4. Establishment of NAA user supporting system and KOLAS management : Development and validation of KOLAS/ISO accreditation testing and identification method, Cooperation researches for a industrial application, Establishment of integrated user analytical supporting system, Accomplishment of sample irradiation facility

  16. Use of activation analysis of hair in environmental protection

    International Nuclear Information System (INIS)

    Human hair is very suitable for use in environmental control monitoring because trace elements concentrate in it at higher levels than in most other organs. Unlike in other biological materials, the trace element contents in hair can be determined by instrumental neutron activation analysis (INAA), as the interference by 24Na can be eliminated by appropriate washing of hair, e.g., using the procedure recommended by IAEA. The methods of sampling, washing and sample analysis using INAA and neutron activation analysis with radiochemical separation are described including the recommended way of the presentation of results. The results are presented of analyses for trace elements in hair from both little and highly polluted areas. (Ha)

  17. Artifact suppression and analysis of brain activities with electroencephalography signals

    Institute of Scientific and Technical Information of China (English)

    Md. Rashed-Al-Mahfuz; Md. Rabiul Islam; Keikichi Hirose; Md. Khademul Islam Molla

    2013-01-01

    Brain-computer interface is a communication system that connects the brain with computer (or other devices) but is not dependent on the normal output of the brain (i.e., peripheral nerve and muscle). Electro-oculogram is a dominant artifact which has a significant negative influence on further analysis of real electroencephalography data. This paper presented a data adaptive technique for artifact suppression and brain wave extraction from electroencephalography signals to detect regional brain activities. Empirical mode decomposition based adaptive thresholding approach was employed here to suppress the electro-oculogram artifact. Fractional Gaussian noise was used to determine the threshold level derived from the analysis data without any training. The purified electroencephalography signal was composed of the brain waves also called rhythmic components which represent the brain activities. The rhythmic components were extracted from each electroencephalography channel using adaptive wiener filter with the original scale. The regional brain activities were mapped on the basis of the spatial distribution of rhythmic components, and the results showed that different regions of the brain are activated in response to different stimuli. This research analyzed the activities of a single rhythmic component, alpha with respect to different motor imaginations. The experimental results showed that the proposed method is very efficient in artifact suppression and identifying individual motor imagery based on the activities of alpha component.

  18. Analysis of Some Egyptian Cosmetic Samples by Fast Neutron Activation Analysis

    CERN Document Server

    Medhat, M E; Fayez-Hassan, M

    2001-01-01

    A description of D-T neutron generator (NG) is presented. This generator can be used for fast neutron activation analysis applied to determine some selected elements, especially light elements, in different materials. In our work, the concentration of the elements Na, Mg, Al, Si, K, Cl, Ca and Fe, were determined in two domestic brands of face powder by using 14 MeV neutron activation analysis.

  19. PHYTOCHEMICAL ANALYSIS AND ANTIMICROBIAL ACTIVITY OF CASIA OCCIDENTALIS (L

    Directory of Open Access Journals (Sweden)

    Venkanna Lunavath

    2013-02-01

    Full Text Available The trend of using natural products has increased and the active plant extracts are frequently screened for new drug discoveries. The present study deals with the screening of Casia occidentalis leaves for their antimicrobial activity against various strains of bacteria. Plant Cassia occidentalis belongs to family Caesalpiniaceae, is a diffuse offensively odorous under shrub. Casia occidentalis were shade dried, powered and was extracted using solvents Methanol. The antimicrobial activity test performed by the disc diffusion method. Preliminary phytochemical analysis of the plant extracts fractions of HXF, CTF, CFF and AQF showed the presence of carbohydrates, amino acids, phytosterols, fixed oils and phenolic compounds. The AQF fraction of C. occidentalis showed high activity across pseudomonas aeuruginosa and staphylococcus aureus bacteria. The present study indicates the potential usefulness of Casia occidentalis leaves in the treatment of various diseases caused by micro-organisms.

  20. Recent developments in environmental research using neutron activation analysis

    International Nuclear Information System (INIS)

    In studies of the origin and fates of trace elements, it is advantageous to be able to analyze samples for a wide spectrum of elements with a high sensitivity and accuracy. This condition is best satisfied with instrumental neutron activation analysis (INAA), since it is one of the most sensitive, selective, and reliable multielement analysis techniques available. In spite of these advantages in environmental studies, use of the technique has been generally limited to aerosol and source material analysis. Over the last few years, the trace analysis and radiochemistry group at the Massachusetts Institute of Technology's Nuclear Reactor Laboratory has applied INAA to various environmental samples for methodology development and/or to provide more information on some important environmental processes. Some examples of these studies are provided in this paper

  1. Multifractal detrended fluctuation analysis of optogenetic modulation of neural activity

    Science.gov (United States)

    Kumar, S.; Gu, L.; Ghosh, N.; Mohanty, S. K.

    2013-02-01

    Here, we introduce a computational procedure to examine whether optogenetically activated neuronal firing recordings could be characterized as multifractal series. Optogenetics is emerging as a valuable experimental tool and a promising approach for studying a variety of neurological disorders in animal models. The spiking patterns from cortical region of the brain of optogenetically-stimulated transgenic mice were analyzed using a sophisticated fluctuation analysis method known as multifractal detrended fluctuation analysis (MFDFA). We observed that the optogenetically-stimulated neural firings are consistent with a multifractal process. Further, we used MFDFA to monitor the effect of chemically induced pain (formalin injection) and optogenetic treatment used to relieve the pain. In this case, dramatic changes in parameters characterizing a multifractal series were observed. Both the generalized Hurst exponent and width of singularity spectrum effectively differentiates the neural activities during control and pain induction phases. The quantitative nature of the analysis equips us with better measures to quantify pain. Further, it provided a measure for effectiveness of the optogenetic stimulation in inhibiting pain. MFDFA-analysis of spiking data from other deep regions of the brain also turned out to be multifractal in nature, with subtle differences in the parameters during pain-induction by formalin injection and inhibition by optogenetic stimulation. Characterization of neuronal firing patterns using MFDFA will lead to better understanding of neuronal response to optogenetic activation and overall circuitry involved in the process.

  2. Development and validation of I-activation analysis code

    International Nuclear Information System (INIS)

    I-Activation Analysis Code (IAAC) is a nuclear depletion code which solves coupled Bateman equations for radioactive-transmutation and growth-decay system for large numbers of isotopes to get time evolution of decay products and nuclear activity. It is currently being developed primarily for neutron activation and radiation waste analysis, as a part of the code development activities. The code functions by separating long and short-lived isotopes and then uses the well-known matrix exponential method to quickly solve a large system of coupled, linear, first-order ordinary differential equations with constant coefficients for long-lived isotopes. This method allows a faster treatment of complex decay and transmutation schemes. The short-lived isotopes are solved using approximated decay-chain method. FENDL 3.0 neutron activation files are used for data library. Separate set of code modules are designed to read, decode, convert and condense the continuous-energy ACE formatted data into 175 VITAMIN-J energy groups. The new compiled library that includes half-lives and neutron absorption cross sections is then used as input source for nuclear data. The code is readily suitable for calculations pertaining to nuclear transmutation, activation and decay studies in mainly fusion applications and activation analyses. Details of the code and its primary validation performed for various test cases and material compositions, largely related to current ITER project specific neutronic and radiation analyses will be presented. The nuclear activity calculations are validated against FISPACT, available under EASY code system. (author)

  3. Aspects of precision and accuracy in neutron activation analysis

    International Nuclear Information System (INIS)

    Analytical results without systematic errors and with accurately known random errors are normally distributed around their true values. Such results may be produced by means of neutron activation analysis both with and without radiochemical separation. When all sources of random variation are known a priori, their effect may be combined with the Poisson statistics characteristic of the counting process, and the standard deviation of a single analytical result may be estimated. The various steps of a complete neutron activation analytical procedure are therefore studied in detail with respect to determining their contribution to the overall variability of the final result. Verification of the estimated standard deviation is carried out by demonstrating the absence of significant unknown random errors through analysing, in replicate, samples covering the range of concentrations and matrices anticipated in actual use. Agreement between the estimated and the observed variability of replicate results is then tested by a simple statistic T based on the chi-square distribution. It is found that results from neutron activation analysis on biological samples can be brought into statistical control. In routine application of methods in statistical control the same statistical test may be used for quality control when some of the actual samples are analysed in duplicate. This analysis of precision serves to detect unknown or unexpected sources of variation of the analytical results, and both random and systematic errors have been discovered in practical trace element investigations in different areas of research. Particularly, at the ultratrace level of concentration where there are few or no standard reference materials for ascertaining the accuracy of results, the proposed quality control based on the analysis of precision combined with neutron activation analysis with radiochemical separation, with an a priori precision independent of the level of concentration, becomes a

  4. Offgas Analysis and Pyrolysis Mechanism of Activated Carbon from Bamboo Sawdust by Chemical Activation With KOH

    Institute of Scientific and Technical Information of China (English)

    TIAN Yong; LIU Ping; WANG Xiufang; ZHONG Guoying; CHEN Guanke

    2011-01-01

    Bamboo sawdust was used as the precursor for the multipurpose use of waste.Offgases released during the activation process of bamboo by KOH were investigated quantitatively and qualitatively by a gas analyzer. TG/DTG curves during the pyrolysis process with different impregnation weight ratios (KOH to bamboo) were obtained by a thermogravimetric analyzer. Pyrolysis mechanism of bamboo was proposed. The results showed that the offgases were composed of CO, NO,SO2 and hydrocarbon with the concentration of 1 372, 37, 86, 215 mg/L, respectively. Thermogravimetric analysis indicated that the pyrolytic process mainly experienced two steps. The first was the low temperature activation step (lower than 300 ℃), which was the pre-activation and induction period.The second was the high temperature activation step(higher than 550 ℃), which was a radial activation followed by pore production. The second process was the key to control the pore distribution of the final product.

  5. Study of the determination of copper by substoichiometric isotopic dilution analysis; Estudo da determinacao de cobre por analise por diluicao isotopica subestequiometrica

    Energy Technology Data Exchange (ETDEWEB)

    Souza Faquim, Elaine de

    1994-12-31

    The tracer {sup 64} Cu having a half-life of 12,8 h produced by the irradiation of {sup 63} Cu with thermal neutron was separated by substoichiometric extraction of Cu(II) with dithizone in carbon tetrachloride. An aliquot of the organic layer was measured on a {gamma}-ray spectrometer consisting of a Na I(Tl) well-type detector and associated electronics. The influence of hydrochloric, sulfuric and nitric acids and the equilibrium time were studied. The reproducibility of the substoichiometric extraction was checked using increasing amounts of tracer {sup 64} Cu. The precision and accuracy of the method were tested using reference materials. After establishing the best analytical conditions, the method was applied to the determination of copper at trace levels in solid samples of diet, wheat flour and in liquid samples, like wine and beer. (author). 57 refs., 3 figs., 7 tabs.

  6. Analysis of alternatives for immobilized low activity waste disposal

    Energy Technology Data Exchange (ETDEWEB)

    Burbank, D.A.

    1997-10-28

    This report presents a study of alternative disposal system architectures and implementation strategies to provide onsite near-surface disposal capacity to receive the immobilized low-activity waste produced by the private vendors. The analysis shows that a flexible unit strategy that provides a suite of design solutions tailored to the characteristics of the immobilized low-activity waste will provide a disposal system that best meets the program goals of reducing the environmental, health, and safety impacts; meeting the schedule milestones; and minimizing the life-cycle cost of the program.

  7. Analysis of alternatives for immobilized low-activity waste disposal

    International Nuclear Information System (INIS)

    This report presents a study of alternative disposal system architectures and implementation strategies to provide onsite near-surface disposal capacity to receive the immobilized low-activity waste produced by the private vendors. The analysis shows that a flexible unit strategy that provides a suite of design solutions tailored to the characteristics of the immobilized low-activity waste will provide a disposal system that best meets the program goals of reducing the environmental, health, and safety impacts; meeting the schedule milestones; and minimizing the life-cycle cost of the program

  8. Teaching chemistry with neutron activation analysis at Dalhousie University

    International Nuclear Information System (INIS)

    The Dalhousie University SLOWPOKE-2 Reactor (DUSR) has been operating since July 1976 and has proven to be an invaluable tool in many teaching programs. These reactors are inherently safe and are designed to serve teaching and research needs of the universities, research centers, hospitals, etc. Since the DUSR has been, from its inception, associated with the Trace Analysis Research Centre, which is the Analytical Chemistry Division of the Department of Chemistry, the main thrust of its use continues to be in the field of nuclear analytical chemistry. Both teaching and research programs involve trace element analysis by neutron activation

  9. Active Greens : An Analysis of the Determinants of Green Party Members' Activism in Environmental Movements

    NARCIS (Netherlands)

    Botetzagias, Iosif; van Schuur, Wijbrandt

    2012-01-01

    This article investigates green party members' activism in the environmental movement and tests how a number of predictors, theoretically suggested in the past yet rarely empirically tested, can account for it. The authors' analysis is based on an extensive data set of members of 15 green parties in

  10. Some Applications of Fast Neutron Activation Analysis of Oxygen

    Energy Technology Data Exchange (ETDEWEB)

    Owrang, Farshid

    2003-07-01

    illustrated how the activated water would propagate along that pipe. C) Combustion products. In order to investigate the oxidation in combustion products (deposits), the total amount of oxygen in the deposits collected from combustion chambers of a modern gasoline engine was measured, using cyclic fast neutron activation analysis (FNAA). As a compartment, the organic compounds containing oxygen were identified using {sup 13}C solid-state nuclear magnetic resonance (NMR) spectroscopy. The results of FNAA showed that the amount of oxygen in deposits varies depending on where the deposits have been formed. {sup 13}C NMR has showed that the carbon backbone of the deposits exists as highly oxidized poly aromatics and/or graphitic structure. D) On-line fast neutron activation analysis. On-line neutron activation analysis was used to detect the amount of oxygen in bulk liquids. The method was optimised for on-line detection of oxygen in rapeseed oil. The goal was to develop a non-intrusive method for measurement of the total amount of oxygen in oil during combustion/oxidation.

  11. Adult active transport in the Netherlands: an analysis of its contribution to physical activity requirements.

    Directory of Open Access Journals (Sweden)

    Elliot Fishman

    Full Text Available Modern, urban lifestyles have engineered physical activity out of everyday life and this presents a major threat to human health. The Netherlands is a world leader in active travel, particularly cycling, but little research has sought to quantify the cumulative amount of physical activity through everyday walking and cycling.Using data collected as part of the Dutch National Travel Survey (2010 - 2012, this paper determines the degree to which Dutch walking and cycling contributes to meeting minimum level of physical activity of 150 minutes of moderate intensity aerobic activity throughout the week. The sample includes 74,465 individuals who recorded at least some travel on the day surveyed. As physical activity benefits are cumulative, all walking and cycling trips are analysed, including those to and from public transport. These trips are then converted into an established measure of physical activity intensity, known as metabolic equivalents of tasks. Multivariate Tobit regression models were performed on a range of socio-demographic, transport resources, urban form and meteorological characteristics.The results reveal that Dutch men and women participate in 24 and 28 minutes of daily physical activity through walking and cycling, which is 41% and 55% more than the minimum recommended level. It should be noted however that some 57% of the entire sample failed to record any walking or cycling, and an investigation of this particular group serves as an important topic of future research. Active transport was positively related with age, income, bicycle ownership, urban density and air temperature. Car ownership had a strong negative relationship with physically active travel.The results of this analysis demonstrate the significance of active transport to counter the emerging issue of sedentary lifestyle disease. The Dutch experience provides other countries with a highly relevant case study in the creation of environments and cultures that

  12. Analysis of medicinal plant extracts by neutron activation method

    International Nuclear Information System (INIS)

    This dissertation has presented the results from analysis of medicinal plant extracts using neutron activation method. Instrumental neutron activation analysis was applied to the determination of the elements Al, Br, Ca, Ce, Cl, Cr, Cs, Fe, K, La, Mg, Mn, Na, Rb, Sb, Sc and Zn in medicinal extracts obtained from Achyrolcline satureoides DC, Casearia sylvestris, Centella asiatica, Citrus aurantium L., Solano lycocarpum, Solidago microglossa, Stryphnondedron barbatiman and Zingiber officinale R. plants. The elements Hg and Se were determined using radiochemical separation by means of retention of Se in HMD inorganic exchanger and solvent extraction of Hg by bismuth diethyl-dithiocarbamate solution. Precision and accuracy of the results have been evaluated by analysing reference materials. The therapeutic action of some elements found in plant extracts analyzed was briefly discussed

  13. Molecular activation analysis for organo-halogen contaminants in yogurt

    International Nuclear Information System (INIS)

    The concentrations of total halogen (TX), extractable organo-halogen (EOX), extractable persistent organo-halogen (EPOX), organo-chlorine pesticides (OCPs) and polychlorinated biphenyls (PCBs) in 18 different yogurt specimens of 14 brands from Beijing, Tianjin, Shanghai, Guangzhou and Shijiazhuang were determined by epithermal neutron activation analysis (ENAA), molecular activation analysis (MAA) and GC-Mass Spectrometry (GC-MS), respectively. The results indicated that the halogen in yogurt mainly existed as inorganic species and non-extractable organo-halogen compounds. About 1/3 to 1/4 of EOX was EPOX. Further, EOCl and EPOCl were the main organo-halogen species in yogurt. The average concentration of the unknown organo-chlorine was 96% of the EPOCl. HCHs and DDTs were still the main contaminants of OCPs in the yogurt of interest. Also, PCB202, PCB103 and PCB208 were the main contaminants of PCBs. (authors)

  14. Applied research and development of neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Moon, Jong Hwa; Kim, Sun Ha; Baek, Sung Ryel; Kim, Young Gi; Jung, Hwan Sung; Park, Kwang Won; Kang, Sang Hun; Lim, Jong Myoung

    2003-05-01

    The aims of this project are to establish the quality control system of Neutron Activation Analysis(NAA) due to increase of industrial needs for standard analytical method and to prepare and identify the standard operation procedure of NAA through practical testing for different analytical items. R and D implementations of analytical quality system using neutron irradiation facility and gamma-ray measurement system and automation of NAA facility in HANARO research reactor are as following ; 1) Establishment of NAA quality control system for the maintenance of best measurement capability and the promotion of utilization of HANARO research reactor 2) Improvement of analytical sensitivity for industrial applied technologies and establishment of certified standard procedures 3) Standardization and development of Prompt Gamma-ray Activation Analysis (PGAA) technology.

  15. Applied research and development of neutron activation analysis

    International Nuclear Information System (INIS)

    The aims of this project are to establish the quality control system of Neutron Activation Analysis(NAA) due to increase of industrial needs for standard analytical method and to prepare and identify the standard operation procedure of NAA through practical testing for different analytical items. R and D implementations of analytical quality system using neutron irradiation facility and gamma-ray measurement system and automation of NAA facility in HANARO research reactor are as following ; 1) Establishment of NAA quality control system for the maintenance of best measurement capability and the promotion of utilization of HANARO research reactor 2) Improvement of analytical sensitivity for industrial applied technologies and establishment of certified standard procedures 3) Standardization and development of Prompt Gamma-ray Activation Analysis (PGAA) technology

  16. Practical aspects of operating a neutron activation analysis laboratory

    International Nuclear Information System (INIS)

    This book is intended to advise in everyday practical problems related to operating a neutron activation analysis (NAA) laboratory. It gives answers to questions like ''what to use NAA for'', ''how to find relevant research problems'', ''how to find users for the technique'', ''how to estimate the cost of the analysis and how to finance the work'', ''how to organize the work in a rational way'' and ''how to perform the quality control''. It gives advice in choosing staff, equipment, and consumables and how to design facilities and procedures according to need and available resources. Potential applications of economic or environmental importance, reactor facilities, counting and measuring equipment of the lab, cooperation with other analytical groups and competitiveness of NAA are discussed by experienced analysts. The compiled 8 tables of data useful for neutron activation analysts are a valuable asset for research labs as well as industrial quality control units. Refs, figs and tabs

  17. Software for a measuring facility for activation analysis

    International Nuclear Information System (INIS)

    A software package has been developed for an APPLE P.C. The programs are intended to control an automated measuring station for photon activation analysis at GELINA, the linear accelerator of C.B.N.M. at Geel (Belgium). They allow to set-up a measuring scheme, to execute it under computer control, to accumulate and store 2 K-spectra using a built-in ADC and to output the results as listings, plots or evaluated reports

  18. Design and analysis of an active power factor correction circuit

    OpenAIRE

    Zhou, Zhen

    1989-01-01

    The design of an active-unity power factor correction circuit with variable-hysteresis control for off-line dc-to-dc switching power supplies is described. Design equations relating the boost inductor current ripple to the circuit components selection and circuit performance arc discussed. A computer-aided design program (CADO) is developed to give the optimal circuit components selection. A 500 watt, 300 volt experimental circuit is built to verify the simulation and analysis ...

  19. Multielement determination in soil extracts by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Forest Swiss soils from 39 locations, each sampled at three depths, were extracted with a buffered solution of pH 4.65 containing EDTA. Nearly 30 elements were determined by instrumental neutron activation analysis. The results obtained are discussed in terms of efficiency of the extractant, precision and accuracy. Summarized results are presented for the quantity fractions of the extracted elements. (author) 18 refs.; 4 figs.; 3 tabs

  20. Analysis of volcanic activity patterns using MODIS thermal alerts

    OpenAIRE

    Rothery, Dave A.; Coppola, Diego; Saunders, Charlotte

    2005-01-01

    We investigate eruptive activity by analysis of thermal-alert data from the MODIS (Moderate Resolution Imaging Spectrometer) thermal infrared satellite instrument, detected by the MODVOLC (MODIS Volcano alert) algorithm. These data are openly available on a website, and easy to use. We show how such data can plug major gaps in the conventional monitoring record of volcanoes in an otherwise generally poorly-documented region (Melanesia), including: characterising the mechanism of lava effusion...

  1. Instrumental Neutron Activation Analysis Technique using Subsecond Radionuclides

    DEFF Research Database (Denmark)

    Nielsen, H.K.; Schmidt, J.O.

    1987-01-01

    The fast irradiation facility Mach-1 installed at the Danish DR 3 reactor has been used in boron determinations by means of Instrumental Neutron Activation Analysis using12B with 20-ms half-life. The performance characteristics of the system are presented and boron determinations of NBS standard...... reference materials as well as fertilizer materials are compared by literature value and spectrophotometric measurements, respectively. In both cases good agreement is obtained....

  2. Gold determination in massive samples by neutron activation analysis

    CERN Document Server

    Broglio, Eduardo

    2015-01-01

    This work presents the characteristics of the Neutron Activation Analysis (NAA) in the determination of gold in voluminous mineral samples using a linear particle accelerator (Linac) as source of irradiation. The used volumes are one or two orders of magnitude higher than the ones that can be used in nuclear research reactor, which is the source usually used to determine through the NAA. This study was encouraged by a specific legal requirement to determine the gold law in a small Patagonian gold deposit.

  3. Diagnostic Application of Absolute Neutron Activation Analysis in Hematology

    Energy Technology Data Exchange (ETDEWEB)

    Zamboni, C.B.; Oliveira, L.C.; Dalaqua, L. Jr.

    2004-10-03

    The Absolute Neutron Activation Analysis (ANAA) technique was used to determine element concentrations of Cl and Na in blood of healthy group (male and female blood donators), select from Blood Banks at Sao Paulo city, to provide information which can help in diagnosis of patients. This study permitted to perform a discussion about the advantages and limitations of using this nuclear methodology in hematological examinations.

  4. Genetic analysis of lipolytic activities in Thermus thermophilus HB27.

    Science.gov (United States)

    Leis, Benedikt; Angelov, Angel; Li, Haijuan; Liebl, Wolfgang

    2014-12-10

    The extremely thermophilic bacterium Thermus thermophilus HB27 displays lipolytic activity for the hydrolysis of triglycerides. In this study we performed a mutational in vivo analysis of esterases and lipases that confer growth on tributyrin. We interrupted 10 ORFs suspected to encode lipolytic enzymes. Two chromosomal loci were identified that resulted in reduced hydrolysis capabilities against tributyrin and various para-nitrophenyl acyl esters. By implementation of a convenient new one-step method which abstains from the use of selectable markers, a mutant strain with multiple scar-less deletions was constructed by sequentially deleting ORFs TT_C1787, TT_C0340, TT_C0341 and TT_C0904. The quadruple deletion mutant of T. thermophilus exhibited significantly lower lipolytic activity (approximately 25% residual activity compared to wild type strain) over a broad range of fatty acyl esters and had lost the ability to grow on agar plates containing tributyrin as the sole carbon source. Furthermore, we were able to determine the impact of each gene disruption on the lipolytic activity profile in this model organism and show that the esterase activity in T. thermophilus HB27 is due to a concerted action of several hydrolases having different substrate preferences and activities. The esterase-less T. thermophilus multi-deletion mutant from this study can be used as a screening and expression host for esterase genes from thermophiles or metagenomes. PMID:25102235

  5. Genetic analysis of lipolytic activities in Thermus thermophilus HB27.

    Science.gov (United States)

    Leis, Benedikt; Angelov, Angel; Li, Haijuan; Liebl, Wolfgang

    2014-12-10

    The extremely thermophilic bacterium Thermus thermophilus HB27 displays lipolytic activity for the hydrolysis of triglycerides. In this study we performed a mutational in vivo analysis of esterases and lipases that confer growth on tributyrin. We interrupted 10 ORFs suspected to encode lipolytic enzymes. Two chromosomal loci were identified that resulted in reduced hydrolysis capabilities against tributyrin and various para-nitrophenyl acyl esters. By implementation of a convenient new one-step method which abstains from the use of selectable markers, a mutant strain with multiple scar-less deletions was constructed by sequentially deleting ORFs TT_C1787, TT_C0340, TT_C0341 and TT_C0904. The quadruple deletion mutant of T. thermophilus exhibited significantly lower lipolytic activity (approximately 25% residual activity compared to wild type strain) over a broad range of fatty acyl esters and had lost the ability to grow on agar plates containing tributyrin as the sole carbon source. Furthermore, we were able to determine the impact of each gene disruption on the lipolytic activity profile in this model organism and show that the esterase activity in T. thermophilus HB27 is due to a concerted action of several hydrolases having different substrate preferences and activities. The esterase-less T. thermophilus multi-deletion mutant from this study can be used as a screening and expression host for esterase genes from thermophiles or metagenomes.

  6. Active Desiccant-Based Preconditioning Market Analysis and Product Development

    Energy Technology Data Exchange (ETDEWEB)

    Fischer, J.

    2001-01-11

    The Phase 1 report (ORNL/Sub/94-SVO44/1), completed earlier in this program, involved a comprehensive field survey and market analysis comparing various specialized outdoor air handling units. This initial investigation included conventional cooling and reheat, conventional cooling with sensible recovery, total energy recovery systems (passive desiccant technology) and various active desiccant systems. The report concluded that several markets do promise a significant sales opportunity for a Climate Changer-based active desiccant system offering. (Climate Changer is a registered trademark of Trane Company.) This initial market analysis defined the wants and needs of the end customers (design engineers and building owners), which, along with subsequent information included in this report, have been used to guide the determination of the most promising active desiccant system configurations. This Phase 2 report begins with a summary of a more thorough investigation of those specific markets identified as most promising for active desiccant systems. Table 1 estimates the annual sales potential for a cost-effective product line of active desiccant systems, such as that built from Climate Changer modules. The Product Development Strategy section describes the active desiccant system configurations chosen to best fit the needs of the marketplace while minimizing system options. Key design objectives based on market research are listed in this report for these active desiccant systems. Corresponding performance goals for the dehumidification wheel required to meet the overall system design objectives are also defined. The Performance Modeling section describes the strategy used by SEMCO to design the dehumidification wheels integrated into the prototype systems currently being tested as part of the U.S. Department of Energy's Advanced Desiccant Technology Program. Actual performance data from wheel testing was used to revise the system performance and energy analysis

  7. A description of the BNL active surface analysis facility

    International Nuclear Information System (INIS)

    Berkeley Nuclear Laboratories has a responsibility for the assessment of radioactive specimens arising both from post irradiation examination of power reactor components and structures and experimental programmes concerned with fission and activation product transport. Existing analytical facilities have been extended with the commissioning of an active surface analysis instrument (XSAM 800pci, Kratos Analytical). Surface analysis involves the characterisation of the outer few atomic layers of a solid surface/interface whose chemical composition and electronic structure will probably be different from the bulk. The new instrument consists three interconnected chambers positioned in series; comprising of a high vacuum sample introduction chamber, an ultra-high vacuum sample treatment/fracture chamber and an ultra-high vacuum sample analysis chamber. The sample analysis chamber contains the electron, X-ray and ion-guns and the electron and ion detectors necessary for performing X-ray photoelectron spectroscopy, scanning Auger microscopy and secondary-ion mass spectroscopy. The chamber also contains a high stability manipulator to enable sub-micron imaging of specimens to be achieved and provide sample heating and cooling between - 180 and 6000C. (author)

  8. Enhancement of research reactor utilization for neutron activation analysis

    International Nuclear Information System (INIS)

    Analytical Chemistry Division has been utilising NAA for the past 4 decades for trace analysis of a number of materials. Some of the procedures developed recently for the trace element determination of high purity hi-tech and nuclear pure materials, geological, environmental and forensic samples by radiochemical neutron activation analysis (RNAA) are discussed here. Nearly complete characterization of high purity (>4N) As and Ga is possible by the procedures developed which are simple, rapid and elegant and can be used easily for the process samples. It is to be emphasised that though the INAA is simple and being widely followed, the RNAA alone can address the problems of analysis for elements present at ultra trace levels in many matrices. (author)

  9. Behavioural activation for depression; an update of meta-analysis of effectiveness and sub group analysis.

    Directory of Open Access Journals (Sweden)

    David Ekers

    Full Text Available BACKGROUND: Depression is a common, disabling condition for which psychological treatments are recommended. Behavioural activation has attracted increased interest in recent years. It has been over 5 years since our meta-analyses summarised the evidence supporting and this systematic review updates those findings and examines moderators of treatment effect. METHOD: Randomised trials of behavioural activation for depression versus controls or anti-depressant medication were identified using electronic database searches, previous reviews and reference lists. Data on symptom level and study level moderators were extracted and analysed using meta-analysis, sub-group analysis and meta-regression respectively. RESULTS: Twenty six randomised controlled trials including 1524 subjects were included in this meta-analysis. A random effects meta-analysis of symptom level post treatment showed behavioural activation to be superior to controls (SMD -0.74 CI -0.91 to -0.56, k = 25, N = 1088 and medication (SMD -0.42 CI -0.83 to-0.00, k = 4, N = 283. Study quality was low in the majority of studies and follow- up time periods short. There was no indication of publication bias and subgroup analysis showed limited association between moderators and effect size. CONCLUSIONS: The results in this meta-analysis support and strengthen the evidence base indicating Behavioural Activation is an effective treatment for depression. Further high quality research with longer term follow-up is needed to strengthen the evidence base.

  10. Provenience studies using neutron activation analysis: the role of standardization

    International Nuclear Information System (INIS)

    This paper covers the historical background of chemical analysis of archaeological artifacts which dates back to 1790 to the first application of neutron activation analysis to archaeological ceramics and goes on to elaborate on the present day status of neutron activation analysis in provenience studies, and the role of standardization. In principle, the concentrations of elements in a neutron-activated specimen can be calculated from an exact knowledge of neutron flux, its intensity, duration and spectral (energy) distribution, plus an exact gamma ray count calibrated for efficiency, corrected for branching rates, etc. However, in practice it is far easier to compare one's unknown to a standard of known or assumed composition. The practice has been for different laboratories to use different standards. With analyses being run in the thousands throughout the world, a great benefit would be derived if analyses could be exchanged among all users and/or generators of data. The emphasis of this paper is on interlaboratory comparability of ceramic data; how far are we from it, what has been proposed in the past to achieve this goal, and what is being proposed. All of this may be summarized under the general heading of Analytical Quality Control - i.e., how to achieve precise and accurate analysis. The author proposes that anyone wishing to analyze archaeological ceramics should simply use his own standard, but attempt to calibrate that standard as nearly as possible to absolute (i.e., accurate) concentration values. The relationship of Analytical Quality Control to provenience location is also examined

  11. Current status of neutron activation analysis in HANARO Research Reactor

    International Nuclear Information System (INIS)

    The facilities for neutron activation analysis in the HANARO (Hi-flux Advanced Neutron Application Research Reactor) are described and the main applications of NAA (Neutron Activation Analysis) are reviewed. The sample irradiation tube, automatic and manual pneumatic transfer system were installed at three irradiation holes of HANARO at the end of 1995. The performance of the NAA facility was examined to identify the characteristics of the tube transfer system, irradiation sites and custom-made polyethylene irradiation capsule. The available thermal neutron fluxes at irradiation sites are in the range of 3 x 1013 - 1 x 1014 n/cm2·s and cadmium ratios are in 15 - 250. For an automatic sample changer for gamma-ray counting, a domestic product was designed and manufactured. An integrated computer program (Labview) to analyse the content was developed. In 2001, PGNAA (Prompt Gamma Neutron Activation Analysis) facility has been installed using a diffracted neutron beam of ST1. NAA has been applied in the trace component analysis of nuclear, geological, biological, environmental and high purity materials, and various polymers for research and development. The improvement of analytical procedures and establishment of an analytical quality control and assurance system were studied. Applied research and development for the environment, industry and human health by NAA and its standardization were carried out. For the application of the KOLAS (Korea Laboratory Accreditation Scheme), evaluation of measurement uncertainty and proficiency testing of reference materials were performed. Also to verify the reliability and to validate analytical results, intercomparison studies between laboratories were carried out. (author)

  12. Current status of neutron activation analysis in HANARO Research Reactor

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Moon, Jong Hwa; Sohn, Jae Min [Korea Atomic Energy Research Institute, Daejeon (Korea)

    2003-03-01

    The facilities for neutron activation analysis in the HANARO (Hi-flux Advanced Neutron Application Research Reactor) are described and the main applications of NAA (Neutron Activation Analysis) are reviewed. The sample irradiation tube, automatic and manual pneumatic transfer system were installed at three irradiation holes of HANARO at the end of 1995. The performance of the NAA facility was examined to identify the characteristics of the tube transfer system, irradiation sites and custom-made polyethylene irradiation capsule. The available thermal neutron fluxes at irradiation sites are in the range of 3 x 10{sup 13} - 1 x 10{sup 14} n/cm{sup 2}{center_dot}s and cadmium ratios are in 15 - 250. For an automatic sample changer for gamma-ray counting, a domestic product was designed and manufactured. An integrated computer program (Labview) to analyse the content was developed. In 2001, PGNAA (Prompt Gamma Neutron Activation Analysis) facility has been installed using a diffracted neutron beam of ST1. NAA has been applied in the trace component analysis of nuclear, geological, biological, environmental and high purity materials, and various polymers for research and development. The improvement of analytical procedures and establishment of an analytical quality control and assurance system were studied. Applied research and development for the environment, industry and human health by NAA and its standardization were carried out. For the application of the KOLAS (Korea Laboratory Accreditation Scheme), evaluation of measurement uncertainty and proficiency testing of reference materials were performed. Also to verify the reliability and to validate analytical results, intercomparison studies between laboratories were carried out. (author)

  13. Image patch analysis of sunspots and active regions. I. Intrinsic dimension and correlation analysis

    CERN Document Server

    Moon, Kevin R; Delouille, Veronique; De Visscher, Ruben; Watson, Fraser; Hero, Alfred O

    2015-01-01

    Complexity of an active region is related to its flare-productivity. Mount Wilson or McIntosh sunspot classifications measure such complexity but in a categorical way, and may therefore not use all the information present in the observations. Moreover, such categorical schemes hinder a systematic study of an active region's evolution for example. We propose fine-scale quantitative descriptors for an active region's complexity and relate them to the Mount Wilson classification. We analyze the local correlation structure within continuum and magnetogram data, as well as the cross-correlation between continuum and magnetogram data. We compute the intrinsic dimension, partial correlation, and canonical correlation analysis (CCA) of image patches of continuum and magnetogram active region images taken from the SOHO-MDI instrument. We use masks of sunspots derived from continuum as well as larger masks of magnetic active regions derived from the magnetogram to analyze separately the core part of an active region fr...

  14. Activation Analysis of Biological Samples of Forensic Interest

    International Nuclear Information System (INIS)

    In forensic (crime investigation) studies, samples of a biological origin are frequently used as evidence. Often it is necessary to compare one sample (associated with a victim or the scene of a crime) with another sample of the same general type (associated with a suspect in some way). The purpose of such comparisons is to establish, if possible, that - to a high degree of probability - the two samples have a common origin. Typically, all available relevant methods of comparison are utilized in such cases by the criminalist: microscopic examination; X-ray diffraction; infra-red, visible, and ultra-violet spectrometry; and various methods of elemental analysis. The forensic applications of high-flux thermal-neutron activation analysis (NAA) have shown great promise and are attracting considerable attention. The authors' laboratory has been engaged in such forensic NAA research and development studies for the past five years. (It also operates a non-profit Forensic Activation Analysis Service, available to all law enforcement agencies, for the NAA comparison of evidence samples involved in actual criminal cases. Samples from many actual cases have been thus examined.) In the United States, NAA results have now been successfully presented in court in some 20 actual cases. Some of the evidence-type materials of interest are non-biological; others are biological. Only the latter will be discussed in this paper. The principal evidence-type materials of a biological nature that have been examined in this laboratory by high-flux thermal-NAA to date are the following: hair, blood, faeces, urine, fingernails, skin, wood, tobacco, whisky, green plants, and marijuana. (In addition, a number of these evidence-type materials have also been studied in this laboratory by high-flux photonuclear activation analysis (PNAA); attention in this paper will be largely devoted to the thermal-NAA forensic studies.) The main topics to be reported upon in this paper are: (1) limits of

  15. Fast-neutron activation analysis of light elements

    International Nuclear Information System (INIS)

    Full text: The determination of lithium, carbon, oxygen, nitrogen and other light chemical elements in various modern materials in microgram level is of importance for analytical science. As it is well-known, a thermal neutron activation of C, H, N, and O produces negligible γ-ray activity. 13C (n, γ) 14C and 2H (n, γ) 3H reactions produce very small activities of the non- γ- emitters 3H and 14C, and the 19O (n, γ)19O and 15N(n, γ)16N reactions give very short lived 19O (27 sec) and 16N (7.1 sec). All of these reactions have extremely low thermal neutron cross sections. Therefore a major advantage of the instrumental neutron activation analysis (INAA) is the determination of trace elements in biological, medical and environmental materials. For this reason the above mentioned problems are solved with use of some variants of nuclear analytical techniques based on application of charged particle accelerators. However, there are several non-traditional reactor activation analysis techniques to solve such problems which have been developed and applied in various fields of semiconductor industry, biology, geology. In recent years these techniques were named as the nuclear reactor based charged particles activation analysis (NRCPAA). We distinguished two possible applications of a nuclear reactor as charged particles source. During last years the capabilities of the NRCPAA were investigated intensively and some our results were applied to determine light elements contents [1,2]. The recoil protons are produced as the result of (n, p) elastic and inelastic scattering interaction of fast neutrons with nucleus of light elements, for example, hydrogen. These protons are applied for the development of proton activation analysis for the determination of large concentrations of Li, B and O. The non-destructive activation analysis with use of 14-MeV fast neutrons (FNAA) is the most suitable method for analysis of N, P and Si. FNAA was applied for determination of nitrogen

  16. Activity optimization method in SPECT: A comparison with ROC analysis

    Institute of Scientific and Technical Information of China (English)

    D(I)AZ Marlén Pérez; RIZO Oscar Díaz; D(I)AZ Adlin López; APARICIO Eric Estévez; D(I)AZ Reinaldo Roque

    2006-01-01

    A discriminant method for optimizing activity in nuclear medicine studies is validated by comparison with ROC performed with a cardiac phantom. Three different lesions (L1, L2 and L3) were placed in the myocardium-wall by pairs for each SPECT. Three activities (84, 37 or 18.5 MBq) of 99mTc were used as background. Linear discriminant analysis was used to select the parameters that characterize image quality among the measured variables in the images [(Background-to-Lesion (B/Li) and Signal-to-Noise (Si/N) ratio s)]. Two clusters with different image quality (P=0.021) were obtained. The ratios B/L1, B/L2 and B/L3are the parameters used to construct the function with 100% of cases correctly classified into the clusters. The value of 37 MBq was the lowest tested activity for which good results for the B/Li ratios were obtained. The result coincides with the applied ROC-analysis (r=0.89).

  17. Elemental analysis of rain- and fresh water by neutron activation analysis

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Analysis of rain-and fresh water for trace constituents is a manda tory part of environmental monitoring. This text gives a survey of neutron activation analysis (NAA) within the framework of current environmental water research pro grammes, based on the practice developed in co-operation with the Dutch Energy Research Centre at Petten (ECN). While the procedures reported in literature cover about thirty five elements, our routine procedures of instrumental neutron activation analysis (INAA) is limited to ten to fifteen elements. The use of some dedicated ra diochemical separations (RNAA) adds another six, some of which are speciated as well. Current contributions of NAA to water analysis center on determination and speciation of anionic trace elements, notably Br, I, As. and Se, on the assay of some ultra traces like Ag, Au and Hg and on validation.

  18. Instrumental neutron activation analysis of sectioned hair strands for arsenic

    Energy Technology Data Exchange (ETDEWEB)

    Guinn, V.P. [Univ. of Maryland, College Park, MD (United States)

    1996-12-31

    Instrumental neutron activation analysis (INAA) is a valuable and proven method for the quantitative analysis of sectioned human head hair specimens for arsenic - and, if arsenic is found to be present at high concentrations, the approximate times when it was ingested. Reactor-flux thermal-neutron activation of the hair samples produces 26.3-h {sup 76}As, which is then detected by germanium gamma-ray spectrometry, measuring the 559.1-keV gamma-ray peak of {sup 76}As. Even normal levels of arsenic in hair, in the range of <1 ppm up to a few parts per million of arsenic can be measured - and the far higher levels associated with large internal doses of arsenic, levels approaching or exceeding 100 ppm arsenic, are readily and accurately measurable. However, all phases of forensic investigations of possible chronic (or in some cases, acute) arsenic poisoning are important, i.e., not just the analysis phase. All of these phases are discussed in this paper, based on the author`s experience and the experience of others, in criminal cases. Cases of chronic arsenic poisoning often reveal a series of two to four doses, perhaps a few months apart, with increasing doses.

  19. Activities of the neutron activation analysis laboratory of the radiochemistry division of IPEN - CNEN/SP

    International Nuclear Information System (INIS)

    Neutron activation analysis (NAA) is one of the relevant applications of nuclear research reactors. Due to the high neutron fluxes available in these reactors, an excellent sensitivity of analysis is attained for many elements. NAA is one of the most sensitive, precise and accurate analytical methods for trace element determination. NAA has been one of the main activities of the Radiochemistry Division of IPEN, since the beginning of the operation of the nuclear reactor IEA-R1. Most of the effort was devoted to research work, aimed to improvements in the method as well as to its applications to several kinds of matrixes (geological, biological, metallic, environmental, forensic). Besides, analytical services were also offered, to the CNEN, to industries, universities, mining companies and research institutes. In the present paper, a review is made of the research work being developed presently at the Radiochesmitry Division of IPEN. A discussion is also made of the planned expansion of the analytical services offered

  20. Automated absolute activation analysis with californium-252 sources

    Energy Technology Data Exchange (ETDEWEB)

    MacMurdo, K.W.; Bowman, W.W.

    1978-09-01

    A 100-mg /sup 252/Cf neutron activation analysis facility is used routinely at the Savannah River Laboratory for multielement analysis of many solid and liquid samples. An absolute analysis technique converts counting data directly to elemental concentration without the use of classical comparative standards and flux monitors. With the totally automated pneumatic sample transfer system, cyclic irradiation-decay-count regimes can be pre-selected for up to 40 samples, and samples can be analyzed with the facility unattended. An automatic data control system starts and stops a high-resolution gamma-ray spectrometer and/or a delayed-neutron detector; the system also stores data and controls output modes. Gamma ray data are reduced by three main programs in the IBM 360/195 computer: the 4096-channel spectrum and pertinent experimental timing, counting, and sample data are stored on magnetic tape; the spectrum is then reduced to a list of significant photopeak energies, integrated areas, and their associated statistical errors; and the third program assigns gamma ray photopeaks to the appropriate neutron activation product(s) by comparing photopeak energies to tabulated gamma ray energies. Photopeak areas are then converted to elemental concentration by using experimental timing and sample data, calculated elemental neutron capture rates, absolute detector efficiencies, and absolute spectroscopic decay data. Calculational procedures have been developed so that fissile material can be analyzed by cyclic neutron activation and delayed-neutron counting procedures. These calculations are based on a 6 half-life group model of delayed neutron emission; calculations include corrections for delayed neutron interference from /sup 17/O. Detection sensitivities of < or = 400 ppB for natural uranium and 8 ppB (< or = 0.5 (nCi/g)) for /sup 239/Pu were demonstrated with 15-g samples at a throughput of up to 140 per day. Over 40 elements can be detected at the sub-ppM level.

  1. Neutron activation analysis of medieval and early modern times ceramics

    International Nuclear Information System (INIS)

    Provenience studies of medieval and early modern times ceramics from the Eastern Danube area of Austria have been performed by instrumental neutron activation analysis. All sherds examined were selected from pottery which was specially charactrized by pottery marks ('Cross Potent', 'Crossmark within a circle', 'Latin Cross', 'Cross Paty'). With respect to the chemical composition five different pottery groups could be evaluated by cluster analysis. Archaeological results: The'Cross Patent' was used by different potter's workshops whereas the 'Crossmark within a circle' was more likely restricted to one manufacture entre. The distribution of the 'Latin Cross' and The 'Cross Paty' over all five clusters indicated the usage of clay from different deposits. The assignment of the 'Cross Paty' exclusively to the area of Passau could be disproved. (Author)

  2. Neutron activation analysis for monitoring northern terrestrial ecosystems

    International Nuclear Information System (INIS)

    New experimental data have been obtained on heavy metal and rare-earth element concentrations in environmental objects, namely pine needles and soils, caused by atmospheric pollution in different regions of the Kola Peninsula. The investigation was performed with the use of epithermal neutron activation analysis at the IBR-2 fast pulsed reactor. The analysis of nearly 40 element distributions in pine needles and soils from the studied geographical points testifies of a strong contamination source - the nickel smelting complex in Monchegorsk. The contamination levels for Ni, Co, Cr, Se, and others are also high and may be hazardous for this region population because some of these elements are carcinogenic. 6 refs., 1 fig., 2 tabs

  3. Analysis of innovation activity of Slovak and Czech enterprises

    Directory of Open Access Journals (Sweden)

    Emília Spišáková

    2011-04-01

    Full Text Available European innovation scoreboard is used to monitor and compare the innovation performance of European countries, according to which was the Slovak Republic, together with two other V4 countries, i.e. Hungary and Poland, at the time of last available data from this area, classified into the last, fourth group of countries named “catching-up countries”. These countries were characterized by the lack of innovation activity, which was well below the EU 27 average. From the V4 countries, Czech Republic achieved the best results, belongs to “moderate innovators” and is the most close to the European average. At a present time all four countries are included in a group of moderate innovators. The innovation performance of whole country is particularly influenced by innovation activities of enterprises operating in this country. For this reason, the article deals with the detailed analysis of innovative activity of enterprises by their size and sector of their operation in Czech and Slovak Republic, and also deals with the cooperation of enterprises in these activities in terms of the type of partner and the countries of their interaction.

  4. Neutron Activation Analysis of Pre-Columbian Pottery in Venezuela

    International Nuclear Information System (INIS)

    Pre-Hispanic pottery figurines from north-central Venezuela islands and mainland were analysed by neutron activation analysis (INAA and PGAA) at the Budapest Research to establish their provenience. In order to classify the samples of figurines, characteristic molecular and atomic components were determined. Several mass ratios were calculated for significant classification of the object of two origins. Results shed light on the origin of island figurines and suggest specific areas of their production on the mainland, contributing to better understanding of late pre-Hispanic migration patterns in the southeastern Caribbean region

  5. Technique for particle flow measuring in activation analysis

    International Nuclear Information System (INIS)

    The invention is refered to the methods of measuring particle flow in nuclear-physical methods of substance composition monitoring. The purpose of the invention is to simplify the process of particle flux measurement and improve the accuracy of analysis. To do this, ''clean'' foil is located behind the monitor, when irradiating ''thin'' monitor, located in front of the sample, and measuring induced radioactivity of radionuclide, produced from the monitor basic element. The value oa particle flow is assessed according to activity of radionuclide nuclei, introduced from monitor into the foil, due to nuclear transformation energy. Monitor thickness should exceed the maximal path of radionuclide nuclei in monitor substance. 1 fig

  6. Analysis of graphic representations of activity theory in international journals

    Directory of Open Access Journals (Sweden)

    Marco André Mazzarotto

    2016-05-01

    Full Text Available Activity theory is a relevant framework for the Design field, and their graphic representations are cognitive artifacts that aid the understanding, use and communication of this theory. However, there is a lack of consistency around the graphics and labels used in these representations. Based on this, the aim of this study was to identify, analyze and evaluate these differences and propose a representation that aims to be more suitable for the theory. For this, uses as method a literature review based on Engeström (2001 and its three generations of visual models, combined with graphical analysis of representations collected in a hundred papers from international journals.

  7. Investigation of a medieval sword using photon activation analysis

    International Nuclear Information System (INIS)

    An ancient sword was examined for indications of forgery or, if authentic, any later processing or changes, e.g. replacement of parts of the weapon. Radiochemical as well as non-destructive analyses using high energy photon activation were used as analytical techniques. Metal parts of the hilt were analysed radiochemically and instrumentally whereas the blade was analysed non-destructively. Metallurgical investigations (hardness measurements, microstructure analysis) performed in parallel are also briefly described. No evidence of non-authenticity was found, which agrees well with the results of stylistical and weapon-scientific investigation carried out by an expert of ancient weaponry. (author) 20 refs.; 1 fig.; 2 tabs

  8. Control of pneumatic transfer system for neutron activation analysis

    International Nuclear Information System (INIS)

    Pneumatic transfer system(PTS) is one of the facilities to be used in irradiation of target materials for neutron activation analysis(NAA) in the research reactor. There are two systems the manual and the automatic system in PTS of HANARO research reactor. The pneumatic transfer system consists of many devices, sends and loads the capsules from NAA laboratory into three holes in the reflector tank of reactor and retrieves irradiated capsules after irradiation. This report describes the part's design, control system and the operation procedures. All the algorithm described in the text will be used for maintenance and upgrading

  9. Failure Mode and Effect Analysis of Active Magnetic Bearings

    Directory of Open Access Journals (Sweden)

    K.P. Lijesh

    2016-03-01

    Full Text Available In the present research work Failure Mode and Effect Analysis (FMEA of an Active Magnetic Bearing (AMB has been presented. Various possible failures modes of AMBs and the corresponding effects of those failures on performance of AMBs have been identified. The identified failure modes of AMBs will facilitate designer to incorporate necessary design features that would prevent the occurrence of the failure. The severity, occurrence and detection of the failures modes are determined based on a rating scale of 1 to 5 to quantify the Risk Priority Number (RPN of the failure modes. The methods to eliminate or reduce the high-risk-failure modes are proposed.

  10. Elemental characterization of Brazilian beans using neutron activation analysis

    International Nuclear Information System (INIS)

    Beans are important for many developing countries as a source of protein and mineral nutrients. Here, ten commercial types of Brazilian beans, from the species Phaseolus vulgaris (common beans) and Vigna unguiculata (cowpeas), were analyzed by neutron activation analysis for the determination of Br, Ca, Co, Cs, Fe, K, Mo, Na, Rb, Sc and Zn. There were statistical differences (p/0.05) amongst the commercial types, except for Br, Rb and Sc. In general, non-essential elements showed high variability, indicating that the origin of beans had a strong influence on the mass fraction of such elements. (author)

  11. Determination of mercury in dentists through Neutron activation analysis

    International Nuclear Information System (INIS)

    It was determined the mercury levels in urine through Neutron activation analysis to 25 dentists who have been exposed to mercury by several time periods, because of the routine manipulations of amalgams. The determined concentrations of mercury were less to 10 μ g Hg/l of urine. The results were founded inside the safety limits reported in the literature. The mercury levels in the dentists are associated with a wide variety of factors that contribute to their exposure as: number of years of dental practice, number of amalgams manipulated between others. (Author)

  12. Fractal analysis of granular activated carbons using isotherm data

    Energy Technology Data Exchange (ETDEWEB)

    Khalili, N.R.; Pan, M. [Illinois Institute of Technology, Chicago, IL (United States). Dept. of Chemical and Environmental Engineering; Sandi, G. [Argonne National Lab., IL (United States)

    1997-08-01

    Utilization of adsorption on solid surfaces was exercised for the first time in 1785. Practical application of unactivated carbon filters, and powdered carbon were first demonstrated in the American water treatment plant, and a municipal treatment plant in New Jersey, in 1883 and 1930, respectively. The use of activated carbon became widespread in the next few decades. At present, adsorption on carbons has a wide spread application in water treatment and removal of taste, odor, removal of synthetic organic chemicals, color-forming organics, and desinfection by-products and their naturally occurring precursors. This paper presents an analysis of the surface fractal dimension and adsorption capacity of a group of carbons.

  13. Activation analysis of particulates emitted from aircraft jet engines

    International Nuclear Information System (INIS)

    Particulate matter in emission gas from aircraft jet engines was subjected to instrumental neutron activation analysis and the compositions of trace elements, such as Na, Al, Cl, Sc, V, Cr, Mn, Fe, Co, Cu, Zn, Br, Sb and Th were determined. For comparison, airborne dust samples collected in and around the airport and a soot sample collected in a jet nozzle were also analyzed. The analytical results obtained involve some ambiguous points mainly resulting from the imperfect sampling method. The analytical sensitivity was insufficient because of the too small amount of collected samples. These should be improved in future studies. (auth.)

  14. Activation Analysis. Proceedings of an Informal Study Group Meeting

    International Nuclear Information System (INIS)

    As part of its programme to promote the exchange of information relating to nuclear science and technology, the International Atomic Energy Agency convened in Bangkok, Thailand, from 6-8 July 1970, an informal meeting to discuss the topic of Activation Analysis. The meeting was attended by participants drawn from the following countries: Australia, Burma, Ceylon, Republic of China, India, Indonesia, Prance, Japan, Republic of Korea, New Zealand, Philippines, Singapore, Thailand, United States of America and Vietnam. The proceedings consist of the contributions presented at the meeting with minor editorial changes

  15. Control of pneumatic transfer system for neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Jung, H. S.; Chung, Y. S.; Wu, J. S.; Kim, H. K.; Choi, Y. S.; Kim, S. H.; Moon, J. H.; Baek, S. Y

    2000-06-01

    Pneumatic transfer system(PTS) is one of the facilities to be used in irradiation of target materials for neutron activation analysis(NAA) in the research reactor. There are two systems the manual and the automatic system in PTS of HANARO research reactor. The pneumatic transfer system consists of many devices, sends and loads the capsules from NAA laboratory into three holes in the reflector tank of reactor and retrieves irradiated capsules after irradiation. This report describes the part's design, control system and the operation procedures. All the algorithm described in the text will be used for maintenance and upgrading.

  16. Practical applications of activation analysis and other nuclear techniques

    International Nuclear Information System (INIS)

    Neeutron activation analysis (NAA) is a versatile, sensitive multielement, usually nondestructive analytical technique used to determine elemental concentrations in a variety of materials. Samples are irradiated with neutrons in a nuclear reactor, removed, and for the nondestructive technique, the induced radioactivity measured. This measurement of γ rays emitted from specific radionuclides makes possible the quantitative determination of elements present. The method is described, advantages and disadvantages listed and a number of examples of its use given. Two other nuclear methods, particle induced x-ray emission and synchrotron produced x-ray fluorescence are also briefly discussed

  17. CMS dashboard for monitoring of the user analysis activities

    Science.gov (United States)

    Karavakis, Edward; Andreeva, Julia; Maier, Gerhild; Khan, Akram

    2012-12-01

    The CMS Virtual Organisation (VO) uses various fully distributed job submission methods and execution backends. The CMS jobs are processed on several middleware platforms such as the gLite, the ARC and the OSG. Up to 200,000 CMS jobs are submitted daily to the Worldwide LHC Computing Grid (WLCG) infrastructure and this number is steadily growing. These mentioned factors increase the complexity of the monitoring of the user analysis activities within the CMS VO. Reliable monitoring is an aspect of particular importance; it is a vital factor for the overall improvement of the quality of the CMS VO infrastructure.

  18. Multi-element study in aluminium by activation analysis technique

    International Nuclear Information System (INIS)

    The instrumental activation analysis is a technique relatively quickly that help to know the elemental composition of materials. It is used mainly in the trace elements determination but in the case of major elements it is necessary to make some considerations as the different nuclear reactions carried out due to the neutron flux is a mixture of thermal and fast neutrons. This could be interpreted for the presence and or erroneous quantification about some elements. In this work, is described the way in which was analyzed a container piece with approximately a 85% of aluminium. The elements Zn, Mn, Sb, Ga, Cu, Cl and Sm were determined. (Author)

  19. Neutron activation analysis of hair from breast cancer patients

    International Nuclear Information System (INIS)

    Hair samples from breast cancer patients were collected at the same time as tumour and normal tissues obtained during mastectomy, in order to determine elemental concentrations and investigate whether hair can act as an epidemiological monitor of the disease. Instrumental neutron activation analysis was used and concentrations for Na, Mg, S, Cl, Ca, Mn, Cu, Zn, Br, I, Sb, Ba, Au and Hg in the hair samples measured. No strong correlations were found between the concentrations of Cl, Cu, Zn and Br in hair and those in tumour tissues and in normal tissues. The level of Zn in the patients hair is low and that of Ca very high

  20. Toxicogenomic analysis of pharmacological active coumarins isolated from Calophyllum brasiliense.

    Science.gov (United States)

    Gomez-Verjan, J C; Estrella-Parra, E A; Gonzalez-Sanchez, I; Rivero-Segura, N A; Vazquez-Martinez, R; Magos-Guerrero, G; Mendoza-Villanueva, D; Cerbón-Cervantes, M A; Reyes-Chilpa, R

    2015-12-01

    Calophyllum brasiliense (Calophyllaceae) is a tropical rain forest tree, mainly distributed in South and Central America. It is an important source of bioactive natural products like, for instance soulatrolide, and mammea type coumarins. Soulatrolide is a tetracyclic dipyranocoumarins and a potent inhibitor of HIV-1 reverse transcriptase and Mycobacterium tuberculosis. Mammea A/BA and A/BB coumarins, pure or as a mixture, are highly active against several leukemia cell lines, Trypanosoma cruzi and Leishmania amazonensis. In the present work, a toxicogenomic analysis of Soulatrolide and Mammea A/BA + A/BB (3:1) mixture was performed in order to validate the toxicological potential of this type of compounds. Soulatrolide or mixture of mammea A/BA + A/BB (3:1) was administered orally to male mice (CD-1) at dose of 100 mg/kg/daily, for 1 week. After this time, mice were sacrificed, and RNA extracted from the liver of treated animals. Transcriptomic analysis was performed using Affymetrix Mouse Gene 1.0 ST Array. Robust microarray analysis (RMA) and two way ANOVA test revealed for mammea mixture treatment 46 genes upregulated and 72 downregulated genes; meanwhile, for soulatrolide 665 were upregulated and 1077 downregulated genes. Enrichment analysis for such genes revealed that in both type of treatments genetic expression were mainly involved in drug metabolism. Overall results indicate a safety profile. The microarray data complies with MIAME guidelines and are deposited in GEO under accession number GSE72755.

  1. Toxicogenomic analysis of pharmacological active coumarins isolated from Calophyllum brasiliense

    Directory of Open Access Journals (Sweden)

    J.C. Gomez-Verjan

    2015-12-01

    Full Text Available Calophyllum brasiliense (Calophyllaceae is a tropical rain forest tree, mainly distributed in South and Central America. It is an important source of bioactive natural products like, for instance soulatrolide, and mammea type coumarins. Soulatrolide is a tetracyclic dipyranocoumarins and a potent inhibitor of HIV-1 reverse transcriptase and Mycobacterium tuberculosis. Mammea A/BA and A/BB coumarins, pure or as a mixture, are highly active against several leukemia cell lines, Trypanosoma cruzi and Leishmania amazonensis. In the present work, a toxicogenomic analysis of Soulatrolide and Mammea A/BA + A/BB (3:1 mixture was performed in order to validate the toxicological potential of this type of compounds. Soulatrolide or mixture of mammea A/BA + A/BB (3:1 was administered orally to male mice (CD-1 at dose of 100 mg/kg/daily, for 1 week. After this time, mice were sacrificed, and RNA extracted from the liver of treated animals. Transcriptomic analysis was performed using Affymetrix Mouse Gene 1.0 ST Array. Robust microarray analysis (RMA and two way ANOVA test revealed for mammea mixture treatment 46 genes upregulated and 72 downregulated genes; meanwhile, for soulatrolide 665 were upregulated and 1077 downregulated genes. Enrichment analysis for such genes revealed that in both type of treatments genetic expression were mainly involved in drug metabolism. Overall results indicate a safety profile. The microarray data complies with MIAME guidelines and are deposited in GEO under accession number GSE72755.

  2. Analysis of large samples by neutron activation analysis. Quality assurance aspects

    International Nuclear Information System (INIS)

    The need for quality assurance in large sample instrumental neutron activation analysis (INAA) requires the development of unconventional methods of quality control. Certified reference materials are not available at the 1-5 kg scale; moreover, inhomogeneities which might affect the accuracy of the real sample analysis would not be reflected in the analysis of a reference material or in-house control sample even when available. Model studies indicate that inhomogeneities with strong gamma ray absorbing properties have the largest effect on the accuracy of the concentrations. The occurrence of these inhomogeneities may be derived from gamma spectrum analysis. Other opportunities for quality assurance are with the calculated estimates of the parameters describing neutron and gamma ray self-attenuation, and eventually through direct assessment after homogenization of the large sample, subsampling and conventional analysis. (author)

  3. Automatization of the neutron activation analysis method in the nuclear analysis laboratory

    International Nuclear Information System (INIS)

    In the present paper the work done to automatice the Neutron Activation Analysis technic with a neutron generator is described. An interface between an IBM compatible microcomputer and the equipment in use to make this kind of measurement was developed. including the specialized software for this system

  4. The monostandard method in thermal neutron activation analysis

    International Nuclear Information System (INIS)

    A simple method is described for instrumental multielement thermal neutron activation analysis using a monostandard. For geological and air dust samples, iron is used as a comparator, while sodium has advantages for biological materials. To test the capabilities of this method, the values of the effective cross sections of the 23 elements determined were evaluated in a reactor site with an almost pure thermal neutron flux of about 9 x 1012 n x cm-2 x sec-1 and an epithermal neutron contribution of less than 0,03%. The obtained values were found to agree mostly well with the literature best values of thermal neutron cross sections. The results of an analysis by activation in the same site agree well with the relative method using multielement standard and for several standard reference materials with certified element contents. A comparison of the element contents obtained by the monostandard and relative methods together with corresponding precisions and accuracies is given. A brief survey of the monostandard method is presented. (orig.)

  5. Extravehicular Activity System Sizing Analysis Tool (EVAS_SAT)

    Science.gov (United States)

    Brown, Cheryl B.; Conger, Bruce C.; Miranda, Bruno M.; Bue, Grant C.; Rouen, Michael N.

    2007-01-01

    An effort was initiated by NASA/JSC in 2001 to develop an Extravehicular Activity System Sizing Analysis Tool (EVAS_SAT) for the sizing of Extravehicular Activity System (EVAS) architecture and studies. Its intent was to support space suit development efforts and to aid in conceptual designs for future human exploration missions. Its basis was the Life Support Options Performance Program (LSOPP), a spacesuit and portable life support system (PLSS) sizing program developed for NASA/JSC circa 1990. EVAS_SAT estimates the mass, power, and volume characteristics for user-defined EVAS architectures, including Suit Systems, Airlock Systems, Tools and Translation Aids, and Vehicle Support equipment. The tool has undergone annual changes and has been updated as new data have become available. Certain sizing algorithms have been developed based on industry standards, while others are based on the LSOPP sizing routines. The sizing algorithms used by EVAS_SAT are preliminary. Because EVAS_SAT was designed for use by members of the EVA community, subsystem familiarity on the part of the intended user group and in the analysis of results is assumed. The current EVAS_SAT is operated within Microsoft Excel 2003 using a Visual Basic interface system.

  6. Quality Assurance and Control in Laboratory using Neutron Activation Analysis

    International Nuclear Information System (INIS)

    In accordance with the increment of international trade associated with the worldwide globalization, the importance of quality assurance and control for the commodity produced from one's own country has been stressed. ISO (International Organization for Standards) defines quality control as 'the operational techniques and activities that are used to fulfill the requirements for quality'. Since 1996, the HANARO research reactor in the Korea Atomic Energy Research Institute has been operated thereafter initial critical operation on April 1995. Neutron activation analysis system and applied techniques which is one of a nuclear analytical technologies using reactor neutrons has been developed for user's supporting and the establishment of the quality system for a measurement and analysis, testing and inspection was implemented successfully. On the basis of the qualified NAA system, the test and measurement of more than 1500 samples which is requested from 30 organizations including industrial companies, universities and institutes carried out in NAA laboratory annually. Moreover, as the goal of mutual recognition agreement (MRA) which can be removed a technical barrier in international trade, the objectivity and the confidence of analytical quality in NAA laboratory became established through the installation of international accreditation system by implementing analytical quality system in accordance with international standards in 2001. The aim of the report was to summarize the technical management of introduction, methods and the results for a quality control and assurance which should be performed in NAA technique using the HANARO research reactor. The report will help building up effective quality control strategy in the future

  7. Activation analysis of Turkish and Canadian clays and Turkish pottery

    International Nuclear Information System (INIS)

    Activation analysis of Canadian and Turkish clays showed that Cs, Th, Sc, Hf, Ta and Co were the most useful elements to study in order to obtain a differentiation by multivariate analysis. The same elements were used to study a variety of Turkish potsherds. It was found that Roman and Byzantine pottery from Yalincak, and Phrygian pottery from Great Tumulus and Tumulus 2 were most probably made from local clay beds. Phrygian pottery from Yalincak shows a tendency to form a small sub-group. However, there are a large number of outliers. No such grouping was found with the Bronze Age pottery analyzed. About 100 mg of sample were weighed into quartz ampoules. A standard pottery was used as a reference in the measurements. Samples were irradiated for a period of 24 hours. The first activity measurements were made a week after the irradiation. The measurement lasted 4000 seconds. A 30 cm3 Ge(Li) detector was coupled to a 4096-channel pulse-height analyzer. The data were recorded on magnetic tapes which were then computer-processed to calculate the peak areas using the program GAMMANAL. Tabulated data on more than 150 samples are given. (T.G.)

  8. Neutron activation analysis and atomic absorption spectrophotometry for the analysis of fresh, pasteurised and powder milk

    Energy Technology Data Exchange (ETDEWEB)

    Wasim, M.; Rehman, S.; Arif, M.; Fatima, I.; Zaidi, J.H. [Pakistan Inst. of Nuclear Science and Technology, Islamabad (Pakistan). Chemistry Div.

    2012-07-01

    This study shows the application of semi-absolute k{sub 0} instrumental neutron activation analysis (k{sub 0}-INAA), epithermal neutron activation analysis (ENAA) and atomic absorption spectrophotometry (AAS) for the determination of 21 elements (Br, Ca, Cl, Co, Cr, Cs, Cu, Fe, Hf, I, K, Mg, Mn, Na, Ni, P, Pb, Rb, Sc Sr, and Zn) in different types of milk samples. The ENAA was required for the determination of iodine, AAS for Cu, Ni and Pb and the rest of the elements were measured by k{sub 0}-INAA. Thirteen elements (Br, Ca, Cl, Cs, Cu, Fe, K, Mg, Na, P, Rb, Sr and Zn) were identified in all milk samples. Ni was detected in eleven and Pb in two samples. Concentrations of most of the elements were within the ranges of the world reported data. The data was further explored by principal component analysis to find relationships between samples and elements. (orig.)

  9. Modeling and experimental vibration analysis of nanomechanical cantilever active probes

    International Nuclear Information System (INIS)

    Nanomechanical cantilever (NMC) active probes have recently received increased attention in a variety of nanoscale sensing and measurement applications. Current modeling practices call for a uniform cantilever beam without considering the intentional jump discontinuities associated with the piezoelectric layer attachment and the NMC cross-sectional step. This paper presents a comprehensive modeling framework for modal characterization and dynamic response analysis of NMC active probes with geometrical discontinuities. The entire length of the NMC is divided into three segments of uniform beams followed by applying appropriate continuity conditions. The characteristics matrix equation is then used to solve for system natural frequencies and mode shapes. Using an equivalent electromechanical moment of a piezoelectric layer, forced motion analysis of the system is carried out. An experimental setup consisting of a commercial NMC active probe from Veeco and a state-of-the-art microsystem analyzer, the MSA-400 from Polytec, is developed to verify the theoretical developments proposed here. Using a parameter estimation technique based on minimizing the modeling error, optimal values of system parameters are identified. Mode shapes and the modal frequency response of the system for the first three modes determined from the proposed model are compared with those obtained from the experiment and commonly used theory for uniform beams. Results indicate that the uniform beam model fails to accurately predict the actual system response, especially in multiple-mode operation, while the proposed discontinuous beam model demonstrates good agreement with the experimental data. Such detailed and accurate modeling framework can lead to significant enhancement in the sensitivity of piezoelectric-based NMC sensors for use in variety of sensing and imaging applications

  10. Applications of short-lived activation products in neutron activation analysis of bio-environmental specimens

    International Nuclear Information System (INIS)

    This report discusses the advantages and disadvantages, special techniques, and actual and potential applications of neutron activation analysis (NAA) utilizing short-lived neutron-induced products, with special reference to the analysis of samples of biological and environmental origin. Attention is devoted mainly to products having half-lives in roughly the range of 10 milliseconds to 60 seconds, but with some discussion of the usefulness of even shorter-lived species, and ones with half-lives as long as a few minutes. Important aspects of the analytical methodology include sample preparation, irradiation/transfer systems, activity measurements, data processing and analytical quality assurance. It is concluded that several trace elements can be determined in bio-environmental samples (as well as in samples of industrial, geochemical and other origin). In particular, this method provides analytical possibilities for several elements (e.g. B, F, Li and V) that are difficult to determine in some matrices at trace levels by any other technique. These conclusions are illustrated in an annex by results of calculations in which the applicability of the techniques to the analysis of several biological and environmental reference materials is evaluated by means of an advance computer prediction program. The report concludes with an annotated bibliography of relevant publications (including abstracts, where available) taken from the INIS database. (author)

  11. The role of neutron activation analysis in nutritional biomonitoring programs

    International Nuclear Information System (INIS)

    Nutritional biomonitoring is a multidisciplinary task and an integral part of a more general bioenvironmental surveillance. In its comprehensive form, it is a combination of biological, environmental, and nutrient monitoring activities. Nutrient monitoring evaluates the input of essential nutrients required to maintain vital bodily functions; this includes vigilance over extreme fluctuations of nutrient intake in relation to the recommended dietary allowances and estimated safe and adequate daily dietary intakes and adherence to the goals of provisional tolerance limits. Environmental monitoring assesses the external human exposure via ambient pathways, namely, air, water, soil, food, etc. Biological monitoring quantifies a toxic agent and its metabolites in representative biologic specimens of an exposed organ to identify health effects. In practice, coordinating all three components of a nutritional biomonitoring program is complex, expensive, and tedious. Experience gained from the US National Health and Nutrition Examination Surveys demonstrates the problems involved. By far the most critical challenge faced here is the question of analytical quality control, particularly when trace element determinations are involved. Yet, measures to ensure reliability of analytical data are mandatory, and there are no short-cuts to this requirement. The purpose of this presentation is to elucidate the potential of neutron activation analysis (NAA) in nutritional biomonitoring activities

  12. Recurrence Plot Analysis Of Mo odle Platform Users’ Activity

    Directory of Open Access Journals (Sweden)

    Jaros ł aw Kilon

    2010-12-01

    Full Text Available The Learning Management System (LMS records activity of many users: students, teachers and administration workers. The e-learning system is a virtual place where thousands of dynamical systems (users communicate each others. These communication leads to changes of users’ activities. The users (human behaviour is nonlinear (Sulis et al., 1995, therefore we can say that LMS is a virtual pl atform of interaction of nonlinear dynamical systems (Ignatowska et al., 2005; Ignatowska et al., 2008. In case of LMS system the number of logs of each user is one of the m easures of his activity. The dynamics of changes of logs to LMS have been analyzed in the paper using the recurrence plot method. The analyses carried out in the paper have shown that recurrence plots are useful in exploring e-learning system dynamics. The comparison between the results of e-learning courses evaluation made by students and RP analysis allow us to withdraw the following conclusion: the increase of complexity and difficulty of the course causes the increase of RR coefficient.

  13. PHYTOCHEMICAL ANALYSIS AND ANTIBACTERIAL ACTIVITY OF KEDROSTIS FOETIDISSIMA (JACQ. COGN.

    Directory of Open Access Journals (Sweden)

    Vasantha K

    2012-01-01

    Full Text Available Hexane, petroleum ether, chloroform, acetone and methanol extracts of leaf, stem and tuber of Kedrostis foetidissima were tested for qualitative and quantitative phytochemical analysis. The results of K. foetidissima leaf extracts revealed the presence of flavonoids and steroids in all extracts studied. Flavonoids, tannins, triterpenoids, phenols, steroids, glycosides and cardiac glycosides are present in the chloroform, methanol and acetone extracts while saponin were detected only in methanol and acetone extract. The various extracts were evaluated for antibacterial activities. Antibacterial activities of the extracts against Staphylococcus aureus, Escherichia coli, Klebsiella pneumoniae, Serratia marcescens and Pseudomonas aeruginosa were investigated by using disc diffusion method. It was observed that, chloroform, acetone and methanol extracts of leaf, stem and tuber of Kedrostis foetidissima showed activity against the entire tested gram positive and gram negative bacterial strains. Inhibitory effect of 100% concentration of petroleum ether and hexane extract was observed against Serratia marcesense (7.05; 4.00mm, Staphylococcus aureus (5.67; 6.83mm, Escherichia coli (4.93; 4.40mm and Pseudomonas aeruginosa (2.15; 3.50mm. Hence, this plant can be used to discover bioactive natural products that may serve as leads in the development of new pharmaceuticals that address unmet therapeutic use.

  14. Dictionary learning and sparse recovery for electrodermal activity analysis

    Science.gov (United States)

    Kelsey, Malia; Dallal, Ahmed; Eldeeb, Safaa; Akcakaya, Murat; Kleckner, Ian; Gerard, Christophe; Quigley, Karen S.; Goodwin, Matthew S.

    2016-05-01

    Measures of electrodermal activity (EDA) have advanced research in a wide variety of areas including psychophysiology; however, the majority of this research is typically undertaken in laboratory settings. To extend the ecological validity of laboratory assessments, researchers are taking advantage of advances in wireless biosensors to gather EDA data in ambulatory settings, such as in school classrooms. While measuring EDA in naturalistic contexts may enhance ecological validity, it also introduces analytical challenges that current techniques cannot address. One limitation is the limited efficiency and automation of analysis techniques. Many groups either analyze their data by hand, reviewing each individual record, or use computationally inefficient software that limits timely analysis of large data sets. To address this limitation, we developed a method to accurately and automatically identify SCRs using curve fitting methods. Curve fitting has been shown to improve the accuracy of SCR amplitude and location estimations, but have not yet been used to reduce computational complexity. In this paper, sparse recovery and dictionary learning methods are combined to improve computational efficiency of analysis and decrease run time, while maintaining a high degree of accuracy in detecting SCRs. Here, a dictionary is first created using curve fitting methods for a standard SCR shape. Then, orthogonal matching pursuit (OMP) is used to detect SCRs within a dataset using the dictionary to complete sparse recovery. Evaluation of our method, including a comparison to for speed and accuracy with existing software, showed an accuracy of 80% and a reduced run time.

  15. A provenance study of coffee by photon activation analysis

    International Nuclear Information System (INIS)

    Photon activation analysis (PAA) is a multi-elemental radioanalytical technique in trace elements analysis with high accuracy and precision. Researchers at the Idaho accelerator center performed PAA analysis on coffee samples from several locations around the world as an initial step in assessing the relationship between trace elements in illicit drugs and the soils in which they were grown. The preliminary results show coffees from different locations have different concentrations of trace elements. In the three cases where we have soil samples, the matrices of elements in the coffee samples are closely related to the matrices of the elements of the local soil samples. The majority of trace elemental content is similar to that of the local soil sample in which the coffee is planted. It may be that coffee assimilates numerous elements from the soil where it is grown in similar ratios as is found in the soil. Thus, it is conceivable that the elemental content could serve as 'fingerprint' to trace the origins of the coffee. To verify our analytical results we applied X-ray fluorescence (XRF) methods as well. Our PAA results are consistent with XRF experimental data. The future of tracing the origin of illicit drugs with the PAA technique is promising. (author)

  16. Antioxidant activity of Costa Rican propolis: a multivariate analysis approach

    International Nuclear Information System (INIS)

    Propolis is produced by Apis mellifera bees from resins of plants that are found around the apiary. The chemical composition is highly variable and Costa Rica has reported without studies of characterization to define the types of propolis in the country. 119 samples were collected from beekeeping areas of the country. The spectrum of 1H-NMR and its antioxidant activity against DPPH radical were measured. The spectra have been divided into 243 blocks of 0,04 ppm and processed with the Minitab software for multivariate analysis. 99 of the samples collected were used for construction of models for the valuation of the predictive ability of the model have been used coefficients of determination (R2) of prediction by the software and the remaining 20 samples. The existence of three types of propolis with chemically different metabolomes were determined by principal component analysis (PCA). A prediction model was constructed by analysis of partial least squares (PLS). The prediction model has allowed to classify a propolis according to the level of antioxidant activity (AAO), high (type I and II) or low (type III) from the spectrum of 1H-NMR. The R2 has been 0.88 and R2 prediction of 0, 718 for new samples. The nconiferyl benzoate of group I and nemorosone of the group II as two discriminated antioxidants among the groups I and II were isolated and high concentration levels of these compounds have been differentiated with respect to type III. This has allowed the construction of a linear discriminant model with a success rate of 100% for the samples used for formulation and 92,9 for the prediction of different samples. The classification systems could be applied to the standardization of the quality of propolis from Costa Rica for future medicinal or cosmetic applications that take advantage of its antioxidant properties. Also, the methylated derivative has isolated and identified of the nconiferyl benzoate thereof propolis than was obtained his counterpart

  17. The analysis and reconciliation of students' rebuttals in argumentation activities

    Science.gov (United States)

    Lin, Yu-Ren; Hung, Jeng-Fung

    2016-01-01

    The present study investigated the guidance provided by science teachers to resolve conflicts during socioscientific issue-based argumentation activities. A graphical representation (GR) was developed as a tool to code and analyze the dialogue interaction process. Through the GR and qualitative analysis, we identified three types of dialogue reconciling strategies. The first one consists of teacher management, in which the teacher temporarily maintains the right to speak when students get mired in an emotional rebuttal situation. The second strategy involves the use of qualifiers to identify the strengths and weaknesses of an opposing argument. The third strategy consists of providing students with guidance to keep both parties (i.e. the students taking, respectively, the affirmative and negative positions) on the same discussion topic and can be used to assist teachers with forming broad questions that prompt students to conduct deeper discussions. These reconciling strategies were beneficial in that they helped students to argue in a more reflective way.

  18. Computer-aided Symbolic Analysis for the Active Network

    Institute of Scientific and Technical Information of China (English)

    徐望人; 徐静波

    2004-01-01

    The totally coded method (TCM) reveal the same law which governing the gain calculating for signal flow graph as Mason formula does. This algorithm is carried out merely in the domain of code operation. Based on pure code algorithm, it is more efficiency because any figure searching is no longer necessary. The code-series (CS), which are organized from node association table, have the holo-information nature, so that both the content and the sign of each gain-term can be determined via the coded method. The principle of this method is obvious and it is suited for computer programming. The capability of the computer-aided analysis for the active network, such as operation amplifier network, can be enhanced.

  19. Semiautomatic exchanger of samples for carry out neutron activation analysis

    International Nuclear Information System (INIS)

    In this paper the design methodology and implementation of a semiautomatic exchanger of samples for the Analysis Laboratory by Neutron Activation of the Reactor department is presented. Taking into account the antecedents, the necessities of improvement are described, as well as the equipment that previously contained the Laboratory. The project of the semiautomatic exchanger of samples was developed at Instituto Nacional de Investigaciones Nucleares, with its own technology to increase independence from commercial equipment. Each element of the semiautomatic exchanger of samples is described both in the design phase as construction. The achieved results are positive and encouraging for the fulfillment of the proposed objective that is to increase the capacity of the Laboratory. (Author)

  20. Structural analysis and immunostimulatory activity of glycopeptides from Paecilomyces sinensis.

    Science.gov (United States)

    Zhu, Zhen-Yuan; Meng, Meng; Sun, Huiqing; Li, Yang; Yu, Na; Zhang, Yong-Min

    2016-03-01

    The parasitic fungus, Paecilomyces sinensis, is used to produce Cordyceps materials as a succedaneum of natural Cordyceps sinensis (C. sinensis) in China. In this work, a glycopeptide (CPS-II) was isolated and purified from Paecilomyces sinensis. The result of HPLC indicated that CPS-II was a glycopeptide. The estimated average molecular weight of CPS-II was 2 × 10(6) Da. FTIR, methylation, periodate oxidation, Smith degradation, (1)H NMR, (13)C NMR and CD were used for its structural analysis. The glycopeptide CPS-II was mainly composed of (1 → 3), (1 → 4) connected glucose and galactose as the backbone, there are (1 → 2,3,6) connected glucose, (1 → 3,6) connected mannose, and (1 → 6) connected galactose. Cell proliferation assay and morphological observations indicated that in a certain range of concentrations and time, CPS-II can significantly improve the proliferation activity of RAW264.7 cells. PMID:26912165

  1. Analysis of Heat Transfer in Actively Cooled Compound Gun Barrel

    Institute of Scientific and Technical Information of China (English)

    WU Bin; XIA Wei

    2005-01-01

    when a gun fires, a large amount of heat is brought in the barrel. Erosion/wear and security problems(self ignition of the propellant) associated with this high thermal energy have to be solved owing to the use of higher combustion gas temperature for improved cannon performance and firing at the sustained high rates. Barrel cooling technologies are the effective measures for addressing this issue. In view of the importance of having knowledge of the heat flux, an approach to calculate heat flux based on measurements was presented and validated. The calculated heat flux is used as the inner boundary condition for modeling heat transfer in a 155 mm mid-wall cooled compound gun barrel. Theoretical analysis and simulated results show that natural air cooling is dramatically slower than the forced liquid mid-wall cooling, accordingly wear life of actively cooled barrel is increased and barrel overheating is prevented.

  2. NIRS-BASED CORTICAL ACTIVATION ANALYSIS BY TEMPORAL CROSS CORRELATION

    Directory of Open Access Journals (Sweden)

    Raul Fernandez-Rojas

    2016-02-01

    Full Text Available In this study we present a method of signal processing to determine dominant channels in near infrared spectroscopy (NIRS. To compare measuring channels and identify delays between them, cross correlation is computed. Furthermore, to find out possible dominant channels, a visual inspection was performed. The outcomes demonstrated that the visual inspection exhibited evoked-related activations in the primary somatosensory cortex (S1 after stimulation which is consistent with comparable studies and the cross correlation study discovered dominant channels on both cerebral hemispheres. The analysis also showed a relationship between dominant channels and adjacent channels. For that reason, our results present a new method to identify dominant regions in the cerebral cortex using near-infrared spectroscopy. These findings have also implications in the decrease of channels by eliminating irrelevant channels for the experiment.

  3. Handbook of nuclear data for neutron activation analysis. Vol. I

    International Nuclear Information System (INIS)

    The first part of a two-volume book which is meant for experimentalists working in instrumental activation analysis and related fields, such as nuclear metrology, materials testing and environmental studies. The volume describes the basic processes of gamma-ray interaction with matter as well as the important phenomena affecting gamma-ray spectra formation in semiconductor spectrometers. A brief account is also given of computation methods commonly employed for spectra evaluation. The results rather than detailed derivations are stressed. A great deal of material si divided into five chapters and nine appendices. The inclusion of many tables of significant spectroscopic data should make the text a useful handbook for those dealing with multi-channel gamma-ray spectra. (author) 26 figs., 82 tabs., 334 refs

  4. Quantitative analysis on tectonic deformation of active rupture zones

    Institute of Scientific and Technical Information of China (English)

    JIANG Zai-sen; NIU An-fu; WANG Min; LI Kai-wu; FANG Ying; ZHANG Xi; ZHANG Xiao-liang

    2005-01-01

    Based on the regional GPS data of high spatial resolution, we present a method of quantitative analysis on the tectonic deformation of active rupture zones in order to predict the location of forthcoming major earthquakes. Firstly we divide the main fault area into certain deformation units, then derive the geometric deformation and relative dislocation parameters of each unit and finally estimate quantitatively the slip and strain rates in each segment of the rupture zone. Furthermore, by comparing the consistency of deformation in all segments of the whole rupture zone, we can determine the possible anomalous segments as well as their properties and amplitudes. In analyzing the eastern boundaries of Sichuan-Yunnan block with the GPS velocity data for the period of 1991~2001, we have discovered that the Mianning-Ningnan-Dongchuan segment on the Zemuhe-Xiaojiang fault zone is relatively locked and the left-lateral shear strain rate here is higher.

  5. The Application of Neutron Activation Analysis in Thailand

    International Nuclear Information System (INIS)

    The technique of neutron activation analysis was introduced at the OAEP about 5 years ago. Since that time, it has become a useful technique for the determination. in particular, of certain trace inorganic elements in biological samples in this country. Scientists here have been working in close co-operation with those in other Government laboratories to meet the requirements of their studies. At present, a high resolution solid state gamma-ray detector is lacking in our laboratory. The results of the work to be described briefly were thus mainly carried out utilising our research reactor as the neutron source and multi-channel analysers together with the technique of radiochemical separation. In some cases, the non-destructive method was found feasible

  6. Neutron activation analysis of organohalogens in Chinese human hair

    International Nuclear Information System (INIS)

    To effectively extract organohalogens from human hair, two factors, the extracting time and hair length on the extraction efficiency of organohalogens were studied by neutron activation analysis (NAA) and gas chromatograph-electron capture detector (GC-ECD), respectively. Furthermore, the concentrations of extractable organohalogens (EOX) and extractable persistent organohalogens (EPOX) in hair samples from angioma and control babies were also measured by the established method. The results indicated that the optimal Soxhlet-extraction time for EOX and EPOX in hair was from 8 to 11 hours, and the extraction efficiencies for organochlorine pesticides in hair were in the order of powder >2 mm>5 mm. Also, the mean levels of EOCl and EPOCl in hair of the angioma babies were significantly higher than those in the control babies (PEOClEPOCl<0.05), which implied the possible relationship between the environmental pollution and angioma. (author)

  7. Instrumental neutron activation analysis of fly ash, aerosols and hair

    International Nuclear Information System (INIS)

    Samples of coal, slag, emissions retained on the separating devices, fly ash, aerosols and hair taken in the area of coal-fired power plant were analyzed by means of instrumental neutron activation analysis. 13 to 23 elements were determined in the samples. The data obtained for emissions and aerosols were further evaluated by calculation of enrichment factors, correlation coefficients and by the ratio matching method. The concentrations of elements determined in the hair of the exposed group were compared with data of control and so called ''out control'' groups as well as with recent data found for hair in other countries. It can be seen from the results that arsenic is the most serious pollutant in the area. (author)

  8. Instrumental neutron activation analysis of the hair of metallurgical workers

    International Nuclear Information System (INIS)

    Hair samples were collected from 20 metallurgical workers (10 males and 10 females) and from 59 control subjects (32 males and 27 females), whose jobs do not indicate a specific occupational exposure. The concentrations of ten minor and trace elements (Al, Co, Cu, Fe, Mg, Mn, Sb, Se, V and Zn) were determined by instrumental neutron activation analysis (INAA). The statistical data distributions, the sex and age influences in these elemental concentrations and the average values obtained for the control group were compared with published data. The effect of occupational exposure to the metallic elements was reflected in elemental compositon of hair by significant higher concentration levels of Al, Co, Cu, Fe, Mg, Mn, Sb, V and Zn in the hair of the exposed group, when compared with the control group. (author)

  9. Tool for automated method design in activation analysis

    International Nuclear Information System (INIS)

    A computational approach to the optimization of the adjustable parameters of nuclear activation analysis has been developed for use in comprehensive method design calculations. An estimate of sample composition is used to predict the gamma-ray spectra to be expected for given sets of values of experimental parameters. These spectra are used to evaluate responses such as detection limits and measurement precision for application to optimization by the simplex method. This technique has been successfully implemented for the simultaneous determination of sample size and irradiation, decay and counting times by the optimization of either detection limit or precision. Both single-element and multielement determinations can be designed with the aid of these calculations. The combination of advance prediction and simplex optimization is both flexible and efficient and produces numerical results suitable for use in further computations

  10. Toenail elemental analysis of Korean young adults by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    The element contents in toenail clippings of healthy Korean young adults were measured using an instrumental neutron activation analysis. The average contents of elements such as Na, K, Cl, Ca, Fe, Se, and Zn are 449, 474, 1024, 1677, 66, 0.7 and 94 mg/kg in men, whereas those contents in women respectively 332, 476, 836, 1097, 66, 0.8 and 104 mg/kg. The correlation analysis of toenail elements with chronic disease risks showed positive associations between Na and serum HDL-cholesterol, blood pressure, and negative associations between Se and Hs-CRP, between Zn and hemoglobin level. (author)

  11. Detailed analysis of the promoter activity of an attenuated lentivirus.

    Science.gov (United States)

    Blatti-Cardinaux, Laure; Sanjosé, Leticia; Zahno, Marie-Luise; Zanoni, Reto; Reina, Ramses; Bertoni, Giuseppe

    2016-07-01

    In spite of an eradication campaign that eliminated clinical cases of caprine arthritis encephalitis virus-induced arthritis in the Swiss goat population, seroconversions are still observed. In the affected flocks, viruses belonging mainly to the small ruminant lentivirus A4 subtype are regularly isolated. These viruses are considered attenuated, except in the mammary gland, where high viral loads and histopathological lesions have been observed. We previously characterized and sequenced such field isolates, detecting several potentially attenuating mutations in their LTR. Here we present a detailed analysis of the promoter activity of these genetic elements, which was comparable to those of virulent isolates. An AP-1 binding site was shown to be crucial for promoter activity in reporter gene assays and also in the context of a replicating molecular clone. Other sites, such as AML(vis) and a conserved E-box, appeared to be less crucial. Analysis of a unique AP-4 site showed a clear discrepancy between results obtained with reporter gene assays and those with mutated viruses. Within the limits of this in vitro study, we did not find evidence pointing to the LTR as the genetic correlate of attenuation for these viruses. Finally, the limited replication of SRLV A4 in mammary cell culture could not explain the suggested mammary tropism. In contrast, and in view of the abundance of macrophages in the mammary gland, it is the striking replication capacity of SRLV A4 in these cells, unaffected by all LTR mutations tested, which may explain the apparent mammary tropism of these viruses. PMID:27114068

  12. Quantifying cortical activity during general anesthesia using wavelet analysis.

    Science.gov (United States)

    Zikov, Tatjana; Bibian, Stéphane; Dumont, Guy A; Huzmezan, Mihai; Ries, Craig R

    2006-04-01

    This paper reports on a novel method for quantifying the cortical activity of a patient during general anesthesia as a surrogate measure of the patient's level of consciousness. The proposed technique is based on the analysis of a single-channel (frontal) electroencephalogram (EEG) signal using stationary wavelet transform (SWT). The wavelet coefficients calculated from the EEG are pooled into a statistical representation, which is then compared to two well-defined states: the awake state with normal EEG activity, and the isoelectric state with maximal cortical depression. The resulting index, referred to as the wavelet-based anesthetic value for central nervous system monitoring (WAV(CNS)), quantifies the depth of consciousness between these two extremes. To validate the proposed technique, we present a clinical study which explores the advantages of the WAV(CNS) in comparison with the BIS monitor (Aspect Medical Systems, MA), currently a reference in consciousness monitoring. Results show that the WAV(CNS) and BIS are well correlated (r = 0.969) during periods of steady-state despite fundamental algorithmic differences. However, in terms of dynamic behavior, the WAV(CNS) offers faster tracking of transitory changes at induction and emergence, with an average lead of 15-30 s. Furthermore, and conversely to the BIS, the WAV(CNS) regains its preinduction baseline value when patients are responding to verbal command after emergence from anesthesia. We conclude that the proposed analysis technique is an attractive alternative to BIS monitoring. In addition, we show that the WAV(CNS) dynamics can be modeled as a linear time invariant transfer function. This index is, therefore, well suited for use as a feedback sensor in advisory systems, closed-loop control schemes, and for the identification of the pharmacodynamic models of anesthetic drugs.

  13. Quality Assurance and Control in Laboratory using Neutron Activation Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Y. S.; Moon, J. H.; Sun, G. M.; Kim, S. H.; Baek, S. Y.; Lim, J. M.; Kim, H. R

    2007-01-15

    In accordance with the increment of international trade associated with the worldwide globalization, the importance of quality assurance and control for the commodity produced from one's own country has been stressed. ISO (International Organization for Standards) defines quality control as 'the operational techniques and activities that are used to fulfill the requirements for quality'. Since 1996, the HANARO research reactor in the Korea Atomic Energy Research Institute has been operated thereafter initial critical operation on April 1995. Neutron activation analysis system and applied techniques which is one of a nuclear analytical technologies using reactor neutrons has been developed for user's supporting and the establishment of the quality system for a measurement and analysis, testing and inspection was implemented successfully. On the basis of the qualified NAA system, the test and measurement of more than 1500 samples which is requested from 30 organizations including industrial companies, universities and institutes carried out in NAA laboratory annually. Moreover, as the goal of mutual recognition agreement (MRA) which can be removed a technical barrier in international trade, the objectivity and the confidence of analytical quality in NAA laboratory became established through the installation of international accreditation system by implementing analytical quality system in accordance with international standards in 2001. The aim of the report was to summarize the technical management of introduction, methods and the results for a quality control and assurance which should be performed in NAA technique using the HANARO research reactor. The report will help building up effective quality control strategy in the future.

  14. ANALYSIS OF AN ELECTROSTRICTIVE STACK ACTUATORFOR ACTIVE TRAILING EDGE FLAPS

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    Helicopter is a complex dynamic system with many rotating components. The rotor blades operate in a highly complex aerodynamic environment. The vibratory hub load, which is caused by cyclic variation of centrifugal and aerodynamic load of the rotating blades in flight, is transmitted to the fuselage, resulting in serious vibration and noise of the structure. It is one of the most important exciting sources in helicopters.  There has long been a desire to reduce helicopter vibration and to improve its performance. Control schemes adopted so far can be classified as either passive or active control technologies. The passive technologies include optimization of rotor hub, blade and the fuselage, hub or blade mounted passive vibration absorbers and anti-resonant vibration isolators. One of the major disadvantages with passive technologies is that they are designed to provide maximum vibration reduction at a specific frequency; therefore, their performance is degraded significantly with changes in the operating conditions of the rotor system.  With the development of computer science and active control technology, increasing efforts have been devoted to active control technologies to benefit helicopter vibration suppression in recent years. Earlier studies include Higher Harmonic Control (HHC)[1] and Individual Blade Control (IBC)[2], which is aimed to reduce the vibratory blade load by oscillating the blade in pitch motion using hydraulic actuators. It is successful in suppressing the vibration of the fuselage; however, its application is limited by serious energy consumption.  To overcome these difficulties, a new concept in helicopter vibration control is the smart rotor system. In this scheme, actuators are embedded in composite blades. They are used to activate the trailing edge flaps in higher harmonic pitch motion to adjust the lift force actively. Under the regulation of a control system, the vibratory hub load can be counteracted actively at

  15. Analysis of umayyad islamic silver coins (Dirhams) by using instrumental neutron activation analysis

    Institute of Scientific and Technical Information of China (English)

    1999-01-01

    Islamic silver coins (Dirhams) running the period between 107 to 126 Hijri (726-743AD), which belong to the Umayyad Empire period, 41-132 hijri (661-750AD), were selected for analysis by using instrumentalneutron activation analysis techniques.During this period (105-126H),(724-743AD), the Caliph Hisham Eben Abdlemalek ruled the Umayyad Empire.Dirhams were irradiated in a reactor neutron activation facility.Levels of various elements viz.Cu, Ag and Au were estimated.It was found that the average silver concentration, the baseconstituent of the Dirham, was about 88wt%.Correlation between thecomposition of Dirhams and the historical implications was discussed.

  16. Active contour model based on force field analysis

    Institute of Scientific and Technical Information of China (English)

    HOU Zhi-qiang; HAN Chong-zhao

    2006-01-01

    The traditional snake initial contour should be close to the true boundary of an object of interest in an image;otherwise,an incorrect result will be obtained.Next,active contours have difficulties progressing into boundary concavities.Moreover,the traditional snake as well as almost all of its improved methods can be easily obtained from the local minimum because snake models are nonconvex.An active contour model based on force field analysis (FFA),namely,FFA snake model,is presented in this paper.Based on analyzing force distribution rules of the distance potential force field,a standard is introduced here to distinguish the false one from contour points.The result is not considered as the final solution when the snake energy is minimal.Furthermore,estimation and calculation should be made according to the established standard;only then can the result be considered final.Thus,the snake is prevented from running into the local minimum.The simulation results show that the FFA snake model has a large capture range and can move a snake into the boundary concavities,and that it is able to obtain the object of interest's contour precisely.Compared with the gradient vector flow snake,this new model has a low computational cost.

  17. Mercury mass measurement in fluorescent lamps via neutron activation analysis

    Science.gov (United States)

    Viererbl, L.; Vinš, M.; Lahodová, Z.; Fuksa, A.; Kučera, J.; Koleška, M.; Voljanskij, A.

    2015-11-01

    Mercury is an essential component of fluorescent lamps. Not all fluorescent lamps are recycled, resulting in contamination of the environment with toxic mercury, making measurement of the mercury mass used in fluorescent lamps important. Mercury mass measurement of lamps via instrumental neutron activation analysis (NAA) was tested under various conditions in the LVR-15 research reactor. Fluorescent lamps were irradiated in different positions in vertical irradiation channels and a horizontal channel in neutron fields with total fluence rates from 3×108 cm-2 s-1 to 1014 cm-2 s-1. The 202Hg(n,γ)203Hg nuclear reaction was used for mercury mass evaluation. Activities of 203Hg and others induced radionuclides were measured via gamma spectrometry with an HPGe detector at various times after irradiation. Standards containing an Hg2Cl2 compound were used to determine mercury mass. Problems arise from the presence of elements with a large effective cross section in luminescent material (europium, antimony and gadolinium) and glass (boron). The paper describes optimization of the NAA procedure in the LVR-15 research reactor with particular attention to influence of neutron self-absorption in fluorescent lamps.

  18. Trace elements in coloured opals using neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    McOrist, G.D.; Smallwood, A. [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia)

    1996-12-31

    Neutron activation analysis (NAA) is a technique particularly suited to analysing opals since it is non-destructive and the silica matrix of opals is not prone to significant activation. It was used to determine the concentration of trace elements in 50 samples of orange, yellow, green, blue and pink opals as well as 18 samples of colourless opals taken from a number of recognised fields in Australia, Peru, Mexico and USA. The results were then evaluated to determine if a relationship existed between trace element content and opal colour. The mean concentration of most of the elements found in orange, yellow and colourless opals were similar with few exceptions. This indicated that, for these samples, colour is not related to the trace elements present. However, the trace element profile of the green, pink and blue opals was found to be significantly different with each colour having a much higher concentration of certain trace elements when compared with all other opals analysed. 7 refs.

  19. Neutron activation analysis: a powerful tool in provenance investigations

    International Nuclear Information System (INIS)

    It is well known that neutron activation analysis (NAA), both instrumental and destructive, allows the simultaneous determination of a number of elements, mostly trace elements, with high levels of precision and accuracy. These peculiar properties of NAA are very useful when applied to provenance studies, i.e. to the identification of the origin of raw materials with which artifacts had been manufactured in ancient times. Data reduction by statistical procedures, especially multivariate analysis techniques, provides a statistical 'fingerprint' of investigated materials, both raw materials and archaeological artifacts, that, upon comparison, allows the identification of the provenance of prime matters used for artifact manufacturing. Thus information on quarries and flows exploitation in the antiquity, on technological raw materials processing, on trade routes and about the circulation of fakes, can be obtained. In the present paper two case studies are reported. The first one deals with the identification of the provenance of clay used to make ceramic materials, mostly bricks and tiles, recovered from the excavation of a Roman 'villa' in Lomello (Roman name Laumellum) and of Roman settlings in Casteggio (Roman name Clastidium). Both sites are located in the Province of Pavia in areas called Lomellina and Oltrepo respectively. The second one investigates the origin of the white marble used to build medieval arks, Carolingian age, located in the church of San Felice, now property of the University of Pavia. Experimental set-up, analytical results and data reduction procedures are presented and discussed. (author)

  20. Carbon Dioxide Information Analysis Center: FY 1992 activities

    Energy Technology Data Exchange (ETDEWEB)

    Cushman, R.M. [Oak Ridge National Lab., TN (United States). Carbon Dioxide Information Analysis Center; Stoss, F.W. [Tennessee Univ., Knoxville, TN (United States). Energy, Environment and Resources Center

    1993-03-01

    During the course of a fiscal year, Oak Ridge National Laboratory`s Carbon Dioxide Information Analysis Center (CDIAC) distributes thousands of specialty publications-numeric data packages (NDPs), computer model packages (CMPs), technical reports, public communication publications, newsletters, article reprints, and reference books-in response to requests for information related to global environmental issues, primarily those pertaining to climate change. CDIACs staff also provides technical responses to specific inquiries related to carbon dioxide (CO{sub 2}), other trace gases, and climate. Hundreds of referrals to other researchers, policy analysts, information specialists, or organizations are also facilitated by CDIAC`s staff. This report provides an account of the activities accomplished by CDIAC during the period October 1, 1991 to September 30, 1992. An organizational overview of CDIAC and its staff is supplemented by a detailed description of inquiries received and CDIAC`s response to those inquiries. As analysis and description of the preparation and distribution of numeric data packages, computer model packages, technical reports, newsletters, fact sheets, specialty publications, and reprints is provided. Comments and descriptions of CDIAC`s information management systems, professional networking, and special bilateral agreements are also described.

  1. Carbon Dioxide Information Analysis Center: FY 1991 activities

    Energy Technology Data Exchange (ETDEWEB)

    Cushman, R.M.; Stoss, F.W.

    1992-06-01

    During the course of a fiscal year, Oak Ridge National Laboratory`s Carbon Dioxide Information Analysis Center (CDIAC) distributes thousands of specially publications-numeric data packages (NDPs), computer model packages (CMPs), technical reports, public communication publications, newsletters, article reprints, and reference books-in response to requests for information related to global environmental issues, primarily those pertaining to climate change. CDIAC`s staff also provides technical responses to specific inquiries related to carbon dioxide (CO{sub 2}), other trace gases, and climate. Hundreds of referrals to other researchers, policy analysts, information specialists, or organizations are also facilitated by CDIAC`s staff. This report provides an account of the activities accomplished by CDIAC during the period October 1, 1990 to September 30, 1991. An organizational overview of CDIAC and its staff is supplemented by a detailed description of inquiries received and CDIAC`s response to those inquiries. An analysis and description of the preparation and distribution of numeric data packages, computer model packages, technical reports, newsletters, factsheets, specially publications, and reprints is provided. Comments and descriptions of CDIAC`s information management systems, professional networking, and special bilateral agreements are also described.

  2. Carbon Dioxide Information Analysis Center: FY 1991 activities

    Energy Technology Data Exchange (ETDEWEB)

    Cushman, R.M.; Stoss, F.W.

    1992-06-01

    During the course of a fiscal year, Oak Ridge National Laboratory's Carbon Dioxide Information Analysis Center (CDIAC) distributes thousands of specially publications-numeric data packages (NDPs), computer model packages (CMPs), technical reports, public communication publications, newsletters, article reprints, and reference books-in response to requests for information related to global environmental issues, primarily those pertaining to climate change. CDIAC's staff also provides technical responses to specific inquiries related to carbon dioxide (CO{sub 2}), other trace gases, and climate. Hundreds of referrals to other researchers, policy analysts, information specialists, or organizations are also facilitated by CDIAC's staff. This report provides an account of the activities accomplished by CDIAC during the period October 1, 1990 to September 30, 1991. An organizational overview of CDIAC and its staff is supplemented by a detailed description of inquiries received and CDIAC's response to those inquiries. An analysis and description of the preparation and distribution of numeric data packages, computer model packages, technical reports, newsletters, factsheets, specially publications, and reprints is provided. Comments and descriptions of CDIAC's information management systems, professional networking, and special bilateral agreements are also described.

  3. IDENTIFICATION OF CRITICAL SSCM ACTIVITIES THROUGH CONFIRMATORY FACTOR ANALYSIS

    Directory of Open Access Journals (Sweden)

    V. Narasimham

    2013-06-01

    Full Text Available As a developing country, economic and environmental performance has to be balanced in India. Green supply chain management (GSCM is emerging as an important proactive approach for Indian enterprises for improving environmental performance of processes and products in accordance with the requirements of environmental regulations. This study examines the consistency approaches by confirmatory factor analysis that determines the construct validity, convergent validity,construct reliability and internal consistency of the items of Sustainable supply chain management (SSCM requirements. This study examines the consistency approaches by Confirmatory factor analysis that determines the adoption and implementation of Sustainable supply chain management activities in small & medium scale industries. The requirements include Management commitment, customer coordination, sustainable design & production, green procurement and eco logistics for sustainable supply chains. This study suggested that the five factor model with eighteen items of the sustainable supply chain design had a good fit. Further, the study showed a valid and reliable measurement to identify critical items among the requirements of sustainable supply chains.

  4. Rescaled range (R/S) analysis on seismic activity parameters

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    The rescaled range (R/S) analysis, proposed by Hurst, is a newstatistical method. Being different from traditional statistical method, R/S analysis can provide the information of maximum fluctuation (range) of statistical parame-ters. At present paper, several modern instrumental earthquake catalogues in different spatial scale, temporal scale, and with different seismic activity background are studied, and R/S method is used to analyze the variation of range of seismic parameters such as earthquake frequency, and earthquake time interval. For different seismic parameters, the ratio of range to standard deviation - R/S is a power law function of the length of time, and the exponent H of power law is always greater than 0.5. As we know, H=0.5 is the characteristics of all ideal random processes. Our results indicate that earthquake series is not an ideal Poisson process, on the contrary, the earth-quake as a phenomenon bears dual characteristics of randomicity and regularity, and the greater H departs from 0.5, the more regularity the time series will show, and vice versa. With time scale changing, one can give the conserva-tive estimate of the fluctuation, which might occur in a relatively long time scale, only by using the limited and known time records.

  5. Coincidence Prompt Gamma-Ray Neutron Activation Analysis

    Energy Technology Data Exchange (ETDEWEB)

    R.P. gandner; C.W. Mayo; W.A. Metwally; W. Zhang; W. Guo; A. Shehata

    2002-11-10

    The normal prompt gamma-ray neutron activation analysis for either bulk or small beam samples inherently has a small signal-to-noise (S/N) ratio due primarily to the neutron source being present while the sample signal is being obtained. Coincidence counting offers the possibility of greatly reducing or eliminating the noise generated by the neutron source. The present report presents our results to date on implementing the coincidence counting PGNAA approach. We conclude that coincidence PGNAA yields: (1) a larger signal-to-noise (S/N) ratio, (2) more information (and therefore better accuracy) from essentially the same experiment when sophisticated coincidence electronics are used that can yield singles and coincidences simultaneously, and (3) a reduced (one or two orders of magnitude) signal from essentially the same experiment. In future work we will concentrate on: (1) modifying the existing CEARPGS Monte Carlo code to incorporate coincidence counting, (2) obtaining coincidence schemes for 18 or 20 of the common elements in coal and cement, and (3) optimizing the design of a PGNAA coincidence system for the bulk analysis of coal.

  6. Cosmetics chemical composition characterization by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Brazil is in the third position in the world's cosmetics market. It is an expanding and growing market where new products and manufacturing processes are in a constant and steady expansion. Therefore, it is mandatory that the composition of the products is well known in order to guarantee safety and quality of daily used cosmetics. The Brazilian National Health Surveillance Agency (ANVISA) has issued a resolution, RDC No. 48, March 16, 2006, which defines a 'List of Substances which can not be used in personal hygiene products, cosmetics and perfumes'. In this work, samples of locally manufactured and imported cosmetics (lipsticks, eye shadows, etc.) were analyzed using the Instrumental Neutron Activation Analysis technique. The samples were irradiated in the TRIGA IPR-R1 reactor of the Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN), on a 100kW thermal power, with a thermal neutron fluence rate about 8x1011ncm-2s-1. The analysis has detected the chemical elements Br, Ba, Ga, Na, K, Sc, Fe, Cr, Zn, Sm, W, La, Rb, Cs, Ta, Ge, Co, U, Ti, V, Cl, Al, Mn and Cu. The concentrations of these elements are on a range from 5 to 3000μg.g-1. Some chemical elements observed in samples (Cl, Br, Cr, U) are included at ANVISA prohibitive list. (author)

  7. Image patch analysis of sunspots and active regions. I. Intrinsic dimension and correlation analysis

    Science.gov (United States)

    Moon, Kevin R.; Li, Jimmy J.; Delouille, Véronique; De Visscher, Ruben; Watson, Fraser; Hero, Alfred O.

    2016-01-01

    Context. The flare productivity of an active region is observed to be related to its spatial complexity. Mount Wilson or McIntosh sunspot classifications measure such complexity but in a categorical way, and may therefore not use all the information present in the observations. Moreover, such categorical schemes hinder a systematic study of an active region's evolution for example. Aims: We propose fine-scale quantitative descriptors for an active region's complexity and relate them to the Mount Wilson classification. We analyze the local correlation structure within continuum and magnetogram data, as well as the cross-correlation between continuum and magnetogram data. Methods: We compute the intrinsic dimension, partial correlation, and canonical correlation analysis (CCA) of image patches of continuum and magnetogram active region images taken from the SOHO-MDI instrument. We use masks of sunspots derived from continuum as well as larger masks of magnetic active regions derived from magnetogram to analyze separately the core part of an active region from its surrounding part. Results: We find relationships between the complexity of an active region as measured by its Mount Wilson classification and the intrinsic dimension of its image patches. Partial correlation patterns exhibit approximately a third-order Markov structure. CCA reveals different patterns of correlation between continuum and magnetogram within the sunspots and in the region surrounding the sunspots. Conclusions: Intrinsic dimension has the potential to distinguish simple from complex active regions. These results also pave the way for patch-based dictionary learning with a view toward automatic clustering of active regions.

  8. Thermal analysis of activated carbons modified with silver metavanadate

    Energy Technology Data Exchange (ETDEWEB)

    Goscianska, Joanna; Nowicki, Piotr; Nowak, Izabela [Faculty of Chemistry, Adam Mickiewicz University in Poznan, Grunwaldzka 6, 60-780 Poznan (Poland); Pietrzak, Robert, E-mail: pietrob@amu.edu.pl [Faculty of Chemistry, Adam Mickiewicz University in Poznan, Grunwaldzka 6, 60-780 Poznan (Poland)

    2012-08-10

    Highlights: Black-Right-Pointing-Pointer Preparation of the activated carbons from waste materials as new supports for AgVO{sub 3}. Black-Right-Pointing-Pointer Decomposition of AgVO{sub 3} to V{sub 2}O{sub 5} and Ag{sup 0} for the samples 1 and 3 wt.% Ag-V is observed. Black-Right-Pointing-Pointer Samples containing 5 wt.% Ag-V decompose to vanadyl species as intermediate compounds. - Abstract: The effect of silver metavanadate doping on physicochemical properties and thermal behaviour of the activated carbons obtained from waste materials was investigated. The carbonaceous supports were subjected to carbonisation at 400 or 600 Degree-Sign C. The samples carbonised at 600 Degree-Sign C have much more developed surface area and porous structure than the analogous samples obtained at 400 Degree-Sign C. Impregnation of activated carbons with silver metavanadate leads to a decrease in their surface area and pore volume. According to thermal analysis (TG, DTG) in the samples containing 1 and 3 wt.% of silver metavanadate, AgVO{sub 3} is fully decomposed to do vanadium oxide and Ag, with no intermediate products, while in the samples containing 5 wt.% AgVO{sub 3}, this salt is decomposed to vanadyl species as intermediate compounds at 350 Degree-Sign C before the formation of V{sub 2}O{sub 5} at 500 Degree-Sign C. Moreover, in all samples impregnated with silver metavanadate the nanoparticles of silver undergo crystallisation leading to reduction of Ag{sup +} ions from the vanadium salt to Ag{sup 0}.

  9. Analysis by neutron activation analysis a some ancient ceramics from Romanian territories

    CERN Document Server

    Olariu, A

    1999-01-01

    In this paper we have analyzed samples of Neolithic ceramics from Cucuteni-Scanteia - Vaslui county and Neolithic and Dacian ceramics from Magurele - Bucharest, by the method of neutron activation analysis. The following elements have been observed: Fe, K, La, Mn, Na, Sc and Sm. It has been noticed a relative and a slight clusterization of the analyzed items on the ratios of concentrations Na/Mn, La/Sc and La/Sm.

  10. Neutron activation analysis as applied to instrumental analysis of trace elements from seawater

    International Nuclear Information System (INIS)

    Particulate matter collected from the coastal area delimited by the mouth of the river Volturno and the Sabaudia lake has been analyzed by instrumental neutron activation analysis for its content of twenty-two trace elements. The results for surface water and bottom water are reported separately, thus evidencing the effect of sampling depth on the concentration of many elements. The necessity of accurately 'cleaning' the filters before use is stressed

  11. Neutron activation analysis as analytical tool of environmental issue

    International Nuclear Information System (INIS)

    Neutron activation analysis (NAA) ia applicable to the sample of wide range of research fields, such as material science, biology, geochemistry and so on. However, respecting the advantages of NAA, a sample with small amounts or a precious sample is the most suitable samples for NAA, because NAA is capable of trace analysis and non-destructive determination. In this paper, among these fields, NAA of atmospheric particulate matter (PM) sample is discussed emphasizing on the use of obtained data as an analytical tool of environmental issue. Concentration of PM in air is usually very low, and it is not easy to get vast amount of sample even using a high volume air sampling devise. Therefore, high sensitive NAA is suitable to determine elements in PM samples. Main components of PM is crust oriented silicate, and so on in rural/remote area, and carbonic materials and heavy metals are concentrated in PM in urban area, because of automobile exhaust and other anthropogenic emission source. Elemental pattern of PM reflects a condition of air around the monitoring site. Trends of air pollution can be traced by periodical monitoring of PM by NAA method. Elemental concentrations in air change by season. For example, crustal elements increase in dry season, and sea salts components increase their concentration when wind direction from sea is dominant. Elements that emitted from anthropogenic sources are mainly contained in fine portion of PM, and increase their concentration during winter season, when emission from heating system is high and air is stable. For further analysis and understanding of environmental issues, indicator elements for various emission sources, and elemental concentration ratios of some environmental samples and source portion assignment techniques are useful. (author)

  12. Highly sensitive index of sympathetic activity based on time-frequency spectral analysis of electrodermal activity.

    Science.gov (United States)

    Posada-Quintero, Hugo F; Florian, John P; Orjuela-Cañón, Álvaro D; Chon, Ki H

    2016-09-01

    Time-domain indices of electrodermal activity (EDA) have been used as a marker of sympathetic tone. However, they often show high variation between subjects and low consistency, which has precluded their general use as a marker of sympathetic tone. To examine whether power spectral density analysis of EDA can provide more consistent results, we recently performed a variety of sympathetic tone-evoking experiments (43). We found significant increase in the spectral power in the frequency range of 0.045 to 0.25 Hz when sympathetic tone-evoking stimuli were induced. The sympathetic tone assessed by the power spectral density of EDA was found to have lower variation and more sensitivity for certain, but not all, stimuli compared with the time-domain analysis of EDA. We surmise that this lack of sensitivity in certain sympathetic tone-inducing conditions with time-invariant spectral analysis of EDA may lie in its inability to characterize time-varying dynamics of the sympathetic tone. To overcome the disadvantages of time-domain and time-invariant power spectral indices of EDA, we developed a highly sensitive index of sympathetic tone, based on time-frequency analysis of EDA signals. Its efficacy was tested using experiments designed to elicit sympathetic dynamics. Twelve subjects underwent four tests known to elicit sympathetic tone arousal: cold pressor, tilt table, stand test, and the Stroop task. We hypothesize that a more sensitive measure of sympathetic control can be developed using time-varying spectral analysis. Variable frequency complex demodulation, a recently developed technique for time-frequency analysis, was used to obtain spectral amplitudes associated with EDA. We found that the time-varying spectral frequency band 0.08-0.24 Hz was most responsive to stimulation. Spectral power for frequencies higher than 0.24 Hz were determined to be not related to the sympathetic dynamics because they comprised less than 5% of the total power. The mean value of time

  13. Highly sensitive index of sympathetic activity based on time-frequency spectral analysis of electrodermal activity.

    Science.gov (United States)

    Posada-Quintero, Hugo F; Florian, John P; Orjuela-Cañón, Álvaro D; Chon, Ki H

    2016-09-01

    Time-domain indices of electrodermal activity (EDA) have been used as a marker of sympathetic tone. However, they often show high variation between subjects and low consistency, which has precluded their general use as a marker of sympathetic tone. To examine whether power spectral density analysis of EDA can provide more consistent results, we recently performed a variety of sympathetic tone-evoking experiments (43). We found significant increase in the spectral power in the frequency range of 0.045 to 0.25 Hz when sympathetic tone-evoking stimuli were induced. The sympathetic tone assessed by the power spectral density of EDA was found to have lower variation and more sensitivity for certain, but not all, stimuli compared with the time-domain analysis of EDA. We surmise that this lack of sensitivity in certain sympathetic tone-inducing conditions with time-invariant spectral analysis of EDA may lie in its inability to characterize time-varying dynamics of the sympathetic tone. To overcome the disadvantages of time-domain and time-invariant power spectral indices of EDA, we developed a highly sensitive index of sympathetic tone, based on time-frequency analysis of EDA signals. Its efficacy was tested using experiments designed to elicit sympathetic dynamics. Twelve subjects underwent four tests known to elicit sympathetic tone arousal: cold pressor, tilt table, stand test, and the Stroop task. We hypothesize that a more sensitive measure of sympathetic control can be developed using time-varying spectral analysis. Variable frequency complex demodulation, a recently developed technique for time-frequency analysis, was used to obtain spectral amplitudes associated with EDA. We found that the time-varying spectral frequency band 0.08-0.24 Hz was most responsive to stimulation. Spectral power for frequencies higher than 0.24 Hz were determined to be not related to the sympathetic dynamics because they comprised less than 5% of the total power. The mean value of time

  14. Current studies of biological materials using instrumental and radiochemical neutron activation analysis

    International Nuclear Information System (INIS)

    Instrumental neutron activation analysis still remains the preferred option when analysing the trace element distribution in a wide rage of materials by neutron activation analysis. However, when lower limits of detection are required or major interferences reduce the effectiveness of this technique, radiochemical neutron activation analysis is applied. This paper examines the current use of both methods and the development of rapid radiochemical techniques for analysis of the biological materials, hair, cow's milk, human's milk, milk powder, blood and blood serum

  15. Using robust statistics to improve neutron activation analysis results

    Energy Technology Data Exchange (ETDEWEB)

    Zahn, Guilherme S.; Genezini, Frederico A.; Ticianelli, Regina B.; Figueiredo, Ana Maria G., E-mail: gzahn@ipen.b [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil). Centro do Reator de Pesquisas

    2011-07-01

    Neutron activation analysis (NAA) is an analytical technique where an unknown sample is submitted to a neutron flux in a nuclear reactor, and its elemental composition is calculated by measuring the induced activity produced. By using the relative NAA method, one or more well-characterized samples (usually certified reference materials - CRMs) are irradiated together with the unknown ones, and the concentration of each element is then calculated by comparing the areas of the gamma ray peaks related to that element. When two or more CRMs are used as reference, the concentration of each element can be determined by several different ways, either using more than one gamma ray peak for that element (when available), or using the results obtained in the comparison with each CRM. Therefore, determining the best estimate for the concentration of each element in the sample can be a delicate issue. In this work, samples from three CRMs were irradiated together and the elemental concentration in one of them was calculated using the other two as reference. Two sets of peaks were analyzed for each element: a smaller set containing only the literature-recommended gamma-ray peaks and a larger one containing all peaks related to that element that could be quantified in the gamma-ray spectra; the most recommended transition was also used as a benchmark. The resulting data for each element was then reduced using up to five different statistical approaches: the usual (and not robust) unweighted and weighted means, together with three robust means: the Limitation of Relative Statistical Weight, Normalized Residuals and Rajeval. The resulting concentration values were then compared to the certified value for each element, allowing for discussion on both the performance of each statistical tool and on the best choice of peaks for each element. (author)

  16. Medical application of in vivo neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Cohn, S.H.; Ellis, K.J.; Vartsky, D.; Zanzi, I.; Aloia, J.F.

    1978-01-01

    The clinical usefulness of total body neutron activation analysis (TBNAA) was clearly established at an IAEA panel meeting in Vienna in 1972. It is best demonstrated by the studies involving the measurement of total-body calcium. This measurement provides data useful for the diagnosis and management of metabolic bone disorders. It should be emphasized, however, that while most of the applications to date have involved calcium and phosphorus, the measurement of sodium, chlorine and nitrogen also appear to be useful clinically. Total-body calcium measurements utilizing TBNAA have been used in studies of osteoporosis to establish absolute and relative deficits of calcium in patients with this disease in comparison to a normal contrast population. Changes in total-body calcium (skeletal mass) have also been useful for quantitating the efficacy of various therapies in osteoporosis. Serial measurements over periods of years provide long-term balance data by direct measurement with a higher precision (+- 2%) than is possible by the use of any other technique. In the renal osteodystrophy observed in patients with renal failure, disorders of both calcium and phosphorus, as well as electrolyte disturbances, have been studied. The measure of total-body levels of these elements gives the clinician useful data upon which to design dialysis therapy. The measurement of bone changes in endocrine dysfunction has been studied, particularly in patients with thyroid and parathyroid disorders. In parathyroidectomy, the measurement of total-body calcium, post-operatively, can indicate the degree of bone resorption. Skeletal metabolism and body composition in acromegaly and Cushing's disease have also been investigated by TBNAA. Levels of cadmium in liver and kidney have also been measured in-vivo by prompt-gamma neutron activation and associated with hypertension, emphysema and cigarette smoking.

  17. Medical application of in vivo neutron activation analysis

    International Nuclear Information System (INIS)

    The clinical usefulness of total body neutron activation analysis (TBNAA) was clearly established at an IAEA panel meeting in Vienna in 1972. It is best demonstrated by the studies involving the measurement of total-body calcium. This measurement provides data useful for the diagnosis and management of metabolic bone disorders. It should be emphasized, however, that while most of the applications to date have involved calcium and phosphorus, the measurement of sodium, chlorine and nitrogen also appear to be useful clinically. Total-body calcium measurements utilizing TBNAA have been used in studies of osteoporosis to establish absolute and relative deficits of calcium in patients with this disease in comparison to a normal contrast population. Changes in total-body calcium (skeletal mass) have also been useful for quantitating the efficacy of various therapies in osteoporosis. Serial measurements over periods of years provide long-term balance data by direct measurement with a higher precision (+- 2%) than is possible by the use of any other technique. In the renal osteodystrophy observed in patients with renal failure, disorders of both calcium and phosphorus, as well as electrolyte disturbances, have been studied. The measure of total-body levels of these elements gives the clinician useful data upon which to design dialysis therapy. The measurement of bone changes in endocrine dysfunction has been studied, particularly in patients with thyroid and parathyroid disorders. In parathyroidectomy, the measurement of total-body calcium, post-operatively, can indicate the degree of bone resorption. Skeletal metabolism and body composition in acromegaly and Cushing's disease have also been investigated by TBNAA. Levels of cadmium in liver and kidney have also been measured in-vivo by prompt-gamma neutron activation and associated with hypertension, emphysema and cigarette smoking

  18. Predictive Analysis of Landslide Activity Using Remote Sensing Data

    Science.gov (United States)

    Markuzon, N.; Regan, J.; Slesnick, C.

    2012-12-01

    Landslides are historically one of the most damaging geohazard phenomena in terms of death tolls and socio-economic losses. Therefore, understanding the underlying causes of landslides and how environmental phenomena affect their frequency and severity is of critical importance. Of specific importance for mitigating future damage is increasing our understanding of how climate change will affect landslide severity, occurrence rates, and damage. We are developing data driven models aimed at predicting landslide activity. The models learn multi-dimensional weather and geophysical patterns associated with historical landslides and estimate location-dependent probabilities for landslides under current or future weather and geophysical conditions. Our approach uses machine learning algorithms capable of determining non-linear associations between dependent variables and landslide occurrence without requiring detailed knowledge of geomorphology. Our primary goal in year one of the project is to evaluate the predictive capabilities of data mining models in application to landslide activity, and to analyze if the approach will discover previously unknown variables and/or relationships important to landslide occurrence, frequency or severity. The models include remote sensing and ground-based data, including weather, landcover, slope, elevation and drainage information as well as urbanization data. The historical landslide dataset we used to build our preliminary models was compiled from City of Seattle landslide files, United States Geological Survey reports, newspaper articles, and a verified subset of the Seattle Landslide Database that consists of all reported landslides within Seattle, WA, between 1948 and 1999. Most of the landslides analyzed to-date are shallow. Using statistical analysis and unsupervised clustering methods we have thus far identified subsets of weather conditions that lead to a significantly higher landslide probability, and have developed

  19. A software architectural framework specification for neutron activation analysis

    International Nuclear Information System (INIS)

    Neutron Activation Analysis (NAA) is a sensitive multi-element nuclear analytical technique that has been routinely applied by research reactor (RR) facilities to environmental, nutritional, health related, geological and geochemical studies. As RR facilities face calls to increase their research output and impact, with existing or reducing budgets, automation of NAA offers a possible solution. However, automation has many challenges, not the least of which is a lack of system architecture standards to establish acceptable mechanisms for the various hardware/software and software/software interactions among data acquisition systems, specialised hardware such as sample changers, sample loaders, and data processing modules. This lack of standardization often results in automation hardware and software being incompatible with existing system components, in a facility looking to automate its NAA operations. This limits the availability of automation to a few RR facilities with adequate budgets or in-house engineering resources. What is needed is a modern open system architecture for NAA, that provides the required set of functionalities. This paper describes such an 'architectural framework' (OpenNAA), and portions of a reference implementation. As an example of the benefits, calculations indicate that applying this architecture to the compilation and QA steps associated with the analysis of 35 elements in 140 samples, with 14 SRM's, can reduce the time required by over 80 %. The adoption of open standards in the nuclear industry has been very successful over the years in promoting interchangeability and maximising the lifetime and output of nuclear measurement systems. OpenNAA will provide similar benefits within the NAA application space, safeguarding user investments in their current system, while providing a solid path for development into the future. (author)

  20. A simple and fast method for the determination of active ingredient in antiperspirant cosmetics by neutron activation analysis

    International Nuclear Information System (INIS)

    Antiperspirant cosmetics are tested for their active ingredient (aluminium chlorohydroxide) by conventional analytical techniques. Aluminium has been determined by instrumental neutron activation analysis in all antiperspirant products and package forms available in the Greek market in order to develop a simple and fast method for quantization. The results show that neutron activation analysis could be established as an official method for the determination of active ingredient in antiperspirant cosmetics. The proposed method is compared with the existing official methods and an alternative sampling method for aerosol package is presented. (author)

  1. Segmentation of visitors to shopping centers based on their activities through factor analysis and cluster analysis

    Directory of Open Access Journals (Sweden)

    reza soleymani-damaneh

    2013-08-01

    Full Text Available Knowing customers of shopping centers contributes greatly to increase profits of these centers. Segmentation of the customers is one of the most effective means of knowing the customers. The purpose of this study was to present a segmentation of the customers based on their activities in the shopping centers. The participants were 157 visitors to Milad-e-Noor Shopping Center who were required to answer the questions in the questionnaire. Data were analyzed in three steps. Through the use of factor analysis, in the first step, the number of variables was reduced to the four factors of entertainment activities, planned shopping, shopping information gathering and unplanned shopping. These factors were then inserted into K-mean cluster analysis and, in the second step and the visitors were divided into 4 segments on the basis of their activity as following: traditionalists, shopping center enthusiasts, wandering customers, and entertainment seekers. In the third step, the demographic and behavioral variables were investigated in the identified clusters. Considering the variables of age, academic status and accompanying persons in shopping centers, these clusters were significantly different. In respect to variables of sex, marital status, the length of presence in the shopping centers, occupations and monthly salary they were recognized as homogenous, however.

  2. Inorganic constituents in herbal medicine by neutron activation analysis

    International Nuclear Information System (INIS)

    The demand for herbal medicines is growing worldwide. The expansion of interest has required the standardization of the sector with implementation and constant review of technical standards for production and marketing of these medicines in order to ensure the safe use, therapeutic efficacy and quality of the products. According to data from the World Health Organization, approximately 80% of world population has resorted to the benefits of certain herbs with therapeutic action popularly recognized. Despite the vast flora and the extensive use of medicinal plants by the population, it is a consensus that scientific studies on the subject are insufficiency. Therefore, it is necessary to stimulate such studies in view of the importance of the results of both individual and social field. The determination of major, minor and trace elements and the research of metabolic processes and their impacts on human health are of great importance due to the growth of environmental pollution that directly affects the plants and therefore the phytotherapics. Therefore, the objective of this work was to determine the content of inorganic constituents in herbal medicine: moisture, total ash and the elements As, Ba, Br, Ca, Cs, Co, Cr, Fe, Hf, K, Na, Rb, Sb, Sc, Se, Ta, Th, U, Zn and Zr by neutron activation analysis in order to verify the quality of the products. It was observed that the elemental concentrations varied in a wide range from plant to plant and elements with higher concentrations were Ba, Fe, Cr and Zn. (author)

  3. Elementary concentration of Peruibe black mud by neutron activation analysis

    International Nuclear Information System (INIS)

    The Peruibe Black Mud is used in therapies such as psoriasis, peripheral dermatitis, acne, seborrehea, myalgia arthritis and rheumatic non-articular processes. This material is characterized by is fine organic matter particles, sulphate reducing bacteria and a high content of potential reduction ions. Although this material is particles, sulphate reducing bacteria and a high content of potential reduction ions. Although this material is considered natural, it may not be free of possible adverse health effects, like toxic chemical elements, when used for therapeutic purposes. In the therapeutic treatments involving clays, clays are used in mud form also called peloids, obtained by maturation process. Five in natura and three maturated Black Mud samples were collected in Peruibe city, Sao Paulo State, Brazil. To investigate the distribution of major, trace and rare earth elements in the in natura and maturated clays that constitute the Peruibe Black Mud, neutron activation analysis (NAA) was used. A comparison between in natura and maturated mud shows that major, trace and rare earth elements follow the same order in both types. Generally, the concentrations in the maturated mud are slightly lower than in natura mud. Enrichment on the upper continental crust could be observed for the elements As, Br, Sb and Se, in these types of mud. (author)

  4. Environmental and Economic Analysis of Thermal Active Building System

    Directory of Open Access Journals (Sweden)

    Paulo Fabiano Reis Lessa

    2016-05-01

    Full Text Available This paper is regarding one promising technological solution – which is so called Thermal Active Building Systems (TABS –for one of the most critical problems both in environmental and economic aspects, which is the raising energy consumption. Buildings are the principal application target of the solution once that population spends most part of their time inside them. Therefore, more energy is required to supply an increasingly demand in lighting, air conditioning, heating, electronic devices and so on. In this context, TABS emerge like a possible solution. To ensure the system efficiency or, in other words, prove its viability, it will be applied an environmental management tool (SWOT Analysis weighting all the pros and comparing with its drawbacks, based on previous experiences in implantation of such system, available in literature. A basic theoretical background, which is extremely important to a better comprehension of the system, covering both engineering and environmental management areas, is presented on this paper. Results shown that TABS are efficient mechanisms in the reduction of power consumption, committed with sustainable development, and which worth the investments in a Life Cycle Cost evaluation

  5. Essential trace elements in edible mushrooms by Neutron Activation Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Moura, Patricia L.C.; Maihara, Vera A.; Castro, Lilian P. de [Instituto de Pesquisa e Energetica e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)]. E-mail: patricialandim@ig.com.br; vmaihara@ipen.br; lilian.Pavanelli@terra.com.br; Figueira, Rubens C.L. [Universidade Cruzeiro do Sul, Sao Paulo, SP (Brazil)]. E-mail: figueiraru@yahoo.com.br

    2007-07-01

    Mushrooms are excellent nutritional sources since they provide proteins, fibers and mineral, such as K, P, Fe. They have also been the focus of medical research. In Brazil mushrooms are not consumed in large quantities by the general population since people know little about the nutritional and medicinal benefits that mushrooms offer. Hence, this study intends to contribute to a better understanding of the essential element content in edible mushrooms, which are currently commercialized in Sao Paulo state. Br Fe, K, Na and Zn concentrations were determined by Instrumental Neutron Activation Analysis in the following mushroom species: Shitake (Lentinus edodes), Shimeji (Pleurotus ssp), Paris Champignon (Agaricus bisporus), Hiratake ( Pleurotus ssp) and Eringue (Pleurotus Eryngu. The mushroom samples were acquired from commercial establishments in the city of Sao Paulo and directly from the producers. Essential element contents in mushrooms varied between Br 0.03 to 4.1 mg/kg; Fe 20 to 267 mg/kg; K 1.2 to 5.3 g/kg, Na 10 to 582 mg/kg and Zn 60 to 120 mg/kg. The results confirm that mushrooms can be considered a good source of K, Fe and Zn. The low Na level is a good nutritional benefit for the consumer. (author)

  6. Design and Analysis of a Multiscale Active Queue Management Scheme

    Institute of Scientific and Technical Information of China (English)

    Qi-Jin Ji; Yong-Qiang Dong

    2006-01-01

    Since Internet is dominated by TCP-based applications, active queue management (AQM) is considered as an effective way for congestion control. However, most AQM schemes suffer obvious performance degradation with dynamic traffic. Extensive measurements found that Internet traffic is extremely bursty and possibly self-similar. We propose in this paper a new AQM scheme called multiscale controller (MSC) based on the understanding of traffic burstiness in multiple time scale. Different from most of other AQM schemes, MSC combines rate-based and queue-based control in two time scales. While the rate-based dropping on burst level (large time scales) determines the packet drop aggressiveness and is responsible for low and stable queuing delay, good robustness and responsiveness, the queue-based modulation of the packet drop probability on packet level (small time scales) will bring low loss and high throughput. Stability analysis is performed based on a fluid-flow model of the TCP/MSC congestion control system and simulation results show that MSC outperforms many of the current AQM schemes.

  7. Analysis of competitive activity of qualified handball players

    Directory of Open Access Journals (Sweden)

    Tyshchenko V. A.

    2013-02-01

    Full Text Available The results of competition activity of leading masculine handball commands are considered on Olympiad-2012 on the basis of estimation of efficiency of throws on a gate. Protocols of games are studied. Viewing of the videotape recordings of matches and analysis of reports of complex scientific groups which worked on Olympiad is conducted. The results of estimation of efficiency of throws of ball on a gate, executed from different positions are got. It is set that for 8 conducted games olympic champions (France, executed 363 throws on a gate (on the average 45,38 throws for a game, hammered in 229 goal (28,63 goal for a game and attained the greatest effectiveness - 63%. It is set that efficiency of throws of handball commands is expressly up-diffused in a descending order, in obedience to busy on Olympiad places. Directions the correction of the programs of preparation of skilled handballers and control of their implementation are offered for the collapsible command of Ukraine.

  8. ANALYSIS OF OPPORTUNITIES In CRM Marketing activities airlines

    OpenAIRE

    С.В. ПЕТРОВСЬКА

    2013-01-01

    Тhe analysis of possibilities of application of CRM or Customer Relationship Management is conducted in marketing activity of airlines. It is retained that traditional approaches which are used in CRM require a substantial improvement. Проведено аналіз можливостей застосування CRM чи Customer Relationship Management у маркетинговій діяльності авіакомпаній. Показано, що традиційні підходи, що застосовуються у CRM, вимагають істотного вдосконалювання....

  9. Exergy Analysis of Human Respiration Under Physical Activity

    Directory of Open Access Journals (Sweden)

    Jurandir Itizo Yanagihara

    2010-09-01

    Full Text Available

    This paper presents an exergy analysis of the human body under physical activity. A model of the respiratory system and a model of the thermal system were used for this purpose. These models consider heat and mass transfers in lungs, tissues and blood. Each component of these models is represented by a uniform compartment governed by equations for diffusion, convection, O2 consumption, CO2/heat generation and heat and mass transfer with the environment. The models allow the calculation of the exergy destruction in the lung and tissues, and the contribution of each entropy generation mechanism in the total generation. Furthermore, a discussion is proposed regarding the efficiency of the human body under physical exercise.

  10. Inorganic constituents in herbal medicine by neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Goncalves, Rodolfo D.M.R.; Francisconi, Lucilaine S.; Silva, Paulo S.C. da, E-mail: pscsilva@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN- SP), Sao Paulo, SP (Brazil)

    2011-07-01

    The demand for herbal medicines is growing worldwide. The expansion of interest has required the standardization of the sector with implementation and constant review of technical standards for production and marketing of these medicines in order to ensure the safe use, therapeutic efficacy and quality of the products. According to data from the World Health Organization, approximately 80% of world population has resorted to the benefits of certain herbs with therapeutic action popularly recognized. Despite the vast flora and the extensive use of medicinal plants by the population, it is a consensus that scientific studies on the subject are insufficiency. Therefore, it is necessary to stimulate such studies in view of the importance of the results of both individual and social field. The determination of major, minor and trace elements and the research of metabolic processes and their impacts on human health are of great importance due to the growth of environmental pollution that directly affects the plants and therefore the phytotherapics. Therefore, the objective of this work was to determine the content of inorganic constituents in herbal medicine: moisture, total ash and the elements As, Ba, Br, Ca, Cs, Co, Cr, Fe, Hf, K, Na, Rb, Sb, Sc, Se, Ta, Th, U, Zn and Zr by neutron activation analysis in order to verify the quality of the products. It was observed that the elemental concentrations varied in a wide range from plant to plant and elements with higher concentrations were Ba, Fe, Cr and Zn. (author)

  11. Environmental risk analysis for offshore oil and gas activities

    Energy Technology Data Exchange (ETDEWEB)

    Brude, Odd Willy; Aspholm, Ole O.; Rudberg, Anders [Det Norske Veritas (Brazil)

    2008-07-01

    Offshore oil and gas activities always have a risk for environmental impact due to potential accidental releases of oil and gas. The environmental risk can be calculated as a combination of the frequency of such accidents to occur and their environmental consequences in terms of environmental damage to habitats or populations. A method for conducting environmental risk analysis has been in use in Norwegian offshore waters for a decade, with a continuously refinement of methodology over the past years. This paper outlines the principles in the MIRA method and gives examples and discussions regarding use in different environmental compartments. The risk assessment starts with identification of oil spill scenarios with frequencies of potential release rates and spill durations. The next step is to model the oil drift for each accidental oil spill scenario. Drift and fate of oil is modeled probabilistic. Based on the oil spill scenarios and their probability of oil pollution, the potential environmental damage is quantified for each scenario. The endpoint of environmental damage is reduction of a population and the resulting recovery time (in years) for various species and habitats. Environmental risk levels are then evaluated against the operating companies' environmental acceptance criteria. (author)

  12. Low-cost activation analysis at small research reactors

    CERN Document Server

    Westphal, G P; Lemmel, H; Niedermaier, M R; Joestl, K; Schröder, P; Böck, H H; Schachner, H; Klapfer, E

    2003-01-01

    A software implementation of a loss-free counting multichannel analyzer, storing immediately into the multimegabyte memory of a low-cost 486 or Pentium type PC, enables the real-time control of a rabbit system as well as the collection of up to 1000 pairs of simultaneously recorded loss-corrected and non-corrected spectra of 16 k channels each, in a true sequence without time gaps in between, at throughput rates of up to 200 kc/s. Intended for activation analysis of short-lived isomeric transitions, the system renders possible peak to background optimizations and separations of lines with different half-lives without an a priori knowledge of sample composition by summing up appropriate numbers of spectra over appropriate intervals of time. By automatically adapting the noise filtering time to individual pulse intervals, the Preloaded Digital Filter (PLDF) combines low- to medium-rate resolutions comparable to those of high-quality Gaussian amplifiers with throughput rates of up to 100 kc/s, and high-rate reso...

  13. Calculation of Raman optical activity spectra for vibrational analysis.

    Science.gov (United States)

    Mutter, Shaun T; Zielinski, François; Popelier, Paul L A; Blanch, Ewan W

    2015-05-01

    By looking back on the history of Raman Optical Activity (ROA), the present article shows that the success of this analytical technique was for a long time hindered, paradoxically, by the deep level of detail and wealth of structural information it can provide. Basic principles of the underlying theory are discussed, to illustrate the technique's sensitivity due to its physical origins in the delicate response of molecular vibrations to electromagnetic properties. Following a short review of significant advances in the application of ROA by UK researchers, we dedicate two extensive sections to the technical and theoretical difficulties that were overcome to eventually provide predictive power to computational simulations in terms of ROA spectral calculation. In the last sections, we focus on a new modelling strategy that has been successful in coping with the dramatic impact of solvent effects on ROA analyses. This work emphasises the role of complementarity between experiment and theory for analysing the conformations and dynamics of biomolecules, so providing new perspectives for methodological improvements and molecular modelling development. For the latter, an example of a next-generation force-field for more accurate simulations and analysis of molecular behaviour is presented. By improving the accuracy of computational modelling, the analytical capabilities of ROA spectroscopy will be further developed so generating new insights into the complex behaviour of molecules.

  14. Elementary concentration of Peruibe black mud by neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Torrecilha, Jefferson K.; Ponciano, Ricardo; Silva, Paulo S.C da, E-mail: jeffkoy@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN-CNEN/SP), Sao Paulo, SP (Brazil)

    2013-07-01

    The Peruibe Black Mud is used in therapies such as psoriasis, peripheral dermatitis, acne, seborrehea, myalgia arthritis and rheumatic non-articular processes. This material is characterized by is fine organic matter particles, sulphate reducing bacteria and a high content of potential reduction ions. Although this material is particles, sulphate reducing bacteria and a high content of potential reduction ions. Although this material is considered natural, it may not be free of possible adverse health effects, like toxic chemical elements, when used for therapeutic purposes. In the therapeutic treatments involving clays, clays are used in mud form also called peloids, obtained by maturation process. Five in natura and three maturated Black Mud samples were collected in Peruibe city, Sao Paulo State, Brazil. To investigate the distribution of major, trace and rare earth elements in the in natura and maturated clays that constitute the Peruibe Black Mud, neutron activation analysis (NAA) was used. A comparison between in natura and maturated mud shows that major, trace and rare earth elements follow the same order in both types. Generally, the concentrations in the maturated mud are slightly lower than in natura mud. Enrichment on the upper continental crust could be observed for the elements As, Br, Sb and Se, in these types of mud. (author)

  15. Neutron activation analysis of lipsticks using gamma-ray spectrometry

    International Nuclear Information System (INIS)

    Neutron activation analysis with gamma-ray spectrometry was used to measure the concentrations of various elements in lipsticks of popular Indian and foreign brands. The aim of the present work was to study the possibility of existence of trace elements in samples of lipsticks (the ingredients of which are mostly organic in nature) and to see whether trace elements could distinguish lipsticks of different Indian and foreign brands from the forensic point of view apart from their inter-se differentiation. In the different samples of lipsticks that were analysed the following elements were detected: Au, Ba, Br, Ca, Cs, Fe, Na, Ru, Sb, Sc, Ta, Yb, Zn, Rb and Se. It was found that inter-se differentiation of lipsticks was possible on the basis of concentrations of trace elements and their profile. Concentration of bromine in samples of lipsticks identified lipsticks of different Indian brands. Samples of lipsticks of Indian and foreign brands could be differentiated on the basis of concentrations of cesium, antimony and scandium which were found to be higher in foreign brands as compared to those in Indian brands. (authors)

  16. Residual Chromium in Leather by Instrumental Neutron Activation Analysis

    Directory of Open Access Journals (Sweden)

    S. Okoh

    2012-01-01

    Full Text Available Problem statement: Most tanning processes employ the use of chromium sulphate. For chromium tanned leather, finished products may contain high amount of residual chromium. This may pose some health hazards, since chromium is known to be toxic at elevated concentration. This justifies the need for the study. Approach: Various samples of leather were collected from a tannery, a leather crafts market, a leather dump site and from local tanners all in Kano, Nigeria in 2009. The samples were irradiated for 6 h in the inner site of the Nigerian Research Reactor (NIRR-1 at a flux of 5×1011 ncm-2 sec-1. Results: After evaluating the spectrum, the mean results for chromium in the samples were determined as 2.33±0.3, 2.23±0.3 and 2.93±0.4% for samples from the tannery, leather crafts market and leather dump sites respectively. Chromium concentration in samples collected from local tanners who use tannins from Acacia nilotica as tanning agent was below the detection limit of Instrumental Neutron Activation Analysis (INAA technique used in the study. Conclusion: Although, the concentrations of chromium in the analysed samples were not much higher than what were obtained in literature, they may be enough to sensitize the population that is allergic to chromium.

  17. Analysis for toxic elements in food and drinking water in Thailand by neutron activation analysis

    International Nuclear Information System (INIS)

    This paper presents the results of a research aimed at the determination of several trace elements in foodstuffs and water in Thailand. The project included the development of adequate analytical procedures for the determination of As, Cd, Cu and Zn by ion exchange chromatography; Hg and Se by a direct combustion technique; Br, Co, Fe and Mn by instrumental neutron activation analysis (INAA); Pb by flame atomic absorption spectrophotometry; and As, Co, Mn, Sb, U, V, Zn, and Cr in water samples by pre-concentration on activated carbon followed by INAA. The samples analyzed comprised various kinds of vegetables, meat, poultry, beans and peas, various species of rice, fish, shellfish and other marine products. Natural and tap water samples were collected at several locations in twenty-nice provinces in Southern, Northern, North-Eastern and Central parts of Thailand. (author). 16 refs, 1 fig., 49 tabs

  18. Non-destructive analysis of ancient Egyptian vitreous materials by neutron activation analysis

    International Nuclear Information System (INIS)

    Chemical compositions of ancient Egyptian glass are one of the key information for identifying the location of the original material for production. The ordinary chemical analysis is however restricted because variable remains can not be destroyed. Thus sensitive analytical method in non-destructive manner is required. The neutron activation analysis was used in this research and the content of Ca, Cl, Al and Mn were found in ancient Egyptian glass and peak area of them were compared with those in the sand samples taken from several areas around Egypt because sand was thought as the raw material of such glasses. As a result, we found three different patterns in chemical compositions in the surrounding sand samples and we expect this pattern might be a good indicator of location of raw sand material. (author)

  19. Analysis of elements present in beers and brewing waters by neutron activation analysis

    International Nuclear Information System (INIS)

    Neutron activation analysis (NAA) was used for determination of Si, Na, K, Ca, Sc, V, Cr, Mn, Fe, Co, Zn, Rb, Cs, and La in Czech beers and brewing waters. The Si concentration in beer determined by the reaction 29Si(n,p)29Al with fast neutrons confirmed that beer is an important Si source in human diet. Determination of other trace elements by NAA with the whole spectrum of reactor neutrons aimed at the feasibility of identification of Gambrinus beers brewed in various breweries. The elements Ca and V appeared to be the best candidates for this purpose. The concentrations of elements determined by NAA were also compared with the recommended daily element intake for humans. The accuracy of the method was proved by analysis of reference materials, specifically NIST SRM 2704 Buffalo River Sediment, NIST SRM 1633b Coal Fly Ash, and NIST SRM 1515 Apple Leaves. (author)

  20. Elemental analysis of soil and hair sample by instrumental neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Quraishi, Shamshad Begum; Moon, Jong Hwa; Kim, Sun Ha; Baek, Sung Yeoil; Kang, Sang Hoon; Lim, Jong Myoung; Cho, Hyun Je; Kim, Young Jin

    2004-03-01

    Myanmar soil sample was analyzed by using the instrumental neutron activation analysis. The elemental concentrations in the sample, altogether 34 elements, Al As, Ba, Ce, Co, Cr, Cs, Eu, Fe, Ga, Gd, Hf, Ir, K, La, Lu, Mn, Na, Nd, Rb, Sb, Sc, Se, Sm, Th, Ti, V, Yb, Zn and Zr were determined. The concentration of 17 elements (Al, Au, Br, Ca, Cl, Cr, Cu, Co, Fe, Hg, K, Na, Mn, Mg, Sb, Se, Zn) in human hair samples were determined by INAA For quality control of analytical method, certified reference material was used.

  1. Multielement analysis of Nigerian chewing sticks by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    In Nigeria, various parts of various species of native plants have long been used for dental hygiene, with reportedly considerable effectiveness. These materials are known as 'chewing sticks'. This study was an effort to ascertain whether any unusual trace element concentrations might be present in Nigerian chewing sticks. Results are presented for 17 elements (Na, Mg, Al, Cl, K, Ca, Sc, V, Mn, Fe, Co, Zn, Br, Cs, La, Sm, Au) detected and measured in 12 species of such plants, via instrumental thermal-neutron activation analysis. (author)

  2. Elemental analysis of soil and hair sample by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Myanmar soil sample was analyzed by using the instrumental neutron activation analysis. The elemental concentrations in the sample, altogether 34 elements, Al As, Ba, Ce, Co, Cr, Cs, Eu, Fe, Ga, Gd, Hf, Ir, K, La, Lu, Mn, Na, Nd, Rb, Sb, Sc, Se, Sm, Th, Ti, V, Yb, Zn and Zr were determined. The concentration of 17 elements (Al, Au, Br, Ca, Cl, Cr, Cu, Co, Fe, Hg, K, Na, Mn, Mg, Sb, Se, Zn) in human hair samples were determined by INAA For quality control of analytical method, certified reference material was used

  3. Analysis of consumed fish species by neutron activation analysis in six Asian countries

    International Nuclear Information System (INIS)

    Fish were selected as a common target sample for a collaborative study of FNCA (Forum for Nuclear Cooperation in Asia)-NAA (neutron activation analysis) project in 2011. Six Asian countries took part in this work. Fish samples were purchased from commercial markets and prepared by following an agreed protocol. Toxic and essential elements in the prepared samples were determined by NAA. The concentration levels of As, Hg in many fish samples have higher values than the regulation ones. The fish contamination by heavy metals should be monitored continuously for human health. (author)

  4. Analysis of gold and silver concentration on gold mining tailings by neutron activation analysis

    International Nuclear Information System (INIS)

    Full text: Instrumental neutron-activation analysis without radiochemical separation is one of most applicable and often used methods to analyze the concentration of gold, silver and other rare and noble metals in gold ores. This method is not suitable for analyzing low concentration of gold and silver in gold mining tailings due to rather high concentration of some elements. Samples are dissolved by boiling in a mixture of concentrated hydrochloric and nitric acids to extract gold and silver into the solution. Chemical yield of gold and silver after dissolution of the sample and further chromatographic separation is between 92 and 95 percent respectively

  5. Applications of neutron activation analysis in agriculture of Uzbekistan

    International Nuclear Information System (INIS)

    Full text: Soil is one of the main components of biosphere, which is subject to Man's economic activity from year to year. Unfortunately, during last 50-60years it became an object of the chemization (the treatment of crop by poison chemicals and the usage of mineral fertilizers).Thus, definite pre-conditions are created to migrate to substances applied along the soil horizon. These substances fall into organism of Man and animals through soil-contacting media: plants, air, water. In this respect the instrumental neutron-activation techniques which allows determination of about 40 chemical elements in soils and other objects of environment, with detection limit equal to 0.001-10.0mg/kg and not more than 30% uncertainty, are provided with the Ge -detector (the Canberra firm). The report discusses some metrological points of INAA concerning the objects of environment, in particular, the influence of space-time non-uniformity of chemical element distributions on the reliability of analysis results. The elaborated techniques make it possible to: - establish the elemental composition of soils, cotton, natural waters, mineral fertilizers, aerosol dust of near land layer of various climatic zones of Uzbekistan, including the airs around the Aral sea. - study of the interrelation between the soil elemental composition and the chemism in the evolution of pathological processes - find the correlation between the cotton returns and Mn contents in soils and to elaborate on this base a new way to value the presown grain quality - choose the wall material of ancient monuments of a region, which were not strongly subjected to ecological impact, as standards to monitor the background of chemical elements in soils - value the ecologically agrochemical conditions of soils for main cotton-sawing zones of Uzbekistan - perform a large scale mapping of soils to find the Mn contents and to elaborate the technology of introduction of Mn - containing microfertilizers - estimate the

  6. An Analysis of the Literacy Activities Provided by Preschool Teachers

    OpenAIRE

    Erdoğan, Tolga; Altınkaynak, Şenay Özen; Erdoğan, Özge

    2013-01-01

     The aim of the study is to analyze the views of preschool teachers’ about literacy activities. In order to identify which literacy activities are used by the teachers, semi-structured interviews were carried out. The findings of the study indicate that preschool teachers participated in the study sufficiently give place in their instruction to the activities towards the development of the writing skill. However, it is also found that the activities in regard to the development of skills such...

  7. Analysis of activities for learning computer science unplugged

    OpenAIRE

    Zaviršek, Manca

    2013-01-01

    In following thesis I delve into activities for learning computer science unplugged available at Vidra website. Some activities are analyzed on the basis of learning objectives of Slovenian primary school curriculum for computer science and ACM K-12 Computer Science Curriculum. The main objective of this thesis is to estimate how much the activities match both curriculums. Within the thesis I analyze the goals of those activities in correlation to revised Bloom's taxonomy. By means...

  8. Establishment and application of the cyclic neutron activation analysis method on mini-reactor

    International Nuclear Information System (INIS)

    Background: Instrument neutron activation analysis is a nondestructive analytic method. Some elements after irradiation produce short half-life radio-nuclides (<60 s), and others produce both long-lived and short-lived nuclides. For these short-lived nuclides, the single measurement has big error. Purpose: In order to reduce the error, cyclic neutron activation analysis can be used to improve the sensitivity. Methods: A device was designed to be connected to the sample transporter, detector and irradiation pipeline in the reactor, which can automatically control the irradiation time and counting time. According to the nuclear parameters of certain elements, irradiation time and counting time and cycle times were determined by experiment. Cyclic activation analysis method was established at the mini-reactor. Results: This paper studied cyclic activation analysis conditions of 17 kinds of element, and applied to the determination of actual samples. Cyclic epithermal neutron activation analysis (CENAA) method was discussed too. By the analysis of national standard reference materials, the reliability of this method was confirmed. Conclusion: Cyclic neutron activation analysis (CNAA) is an effective analytic method for only short life nuclide elements. For both short and long lived nuclides of elements, the cyclic activation analysis method can make the analytical cycle shorten, from a few days or several weeks to within a few minutes. Cyclic activation analysis has the advantages of high sensitivity, and its precision and accuracy are better than single short irradiation activation analysis. (authors)

  9. Epithermal Neutron Activation Analysis of the Asian Herbal Plants

    International Nuclear Information System (INIS)

    Asian medicinal herbs Chrysanthemum (Spiraea aquilegifolia Pall.) and Red Sandalwood (Pterocarpus Santalinus) are widely used in folk and Ayurvedic medicine for healing and preventing some diseases. The modern medical science has proved that the Chrysanthemum (Spiraea aquilegifolia Pall.) possesses the following functions: reducing blood press, dispelling cancer cell, coronary artery's expanding and bacteriostating and Red Sandalwood (Pterocarpus Santalinus) is recommended against headache, toothache, skin diseases, vomiting and sometimes it is taken for treatment of diabetes. Species of Chrysanthemums were collected in the north-eastern and central Mongolia, and the Red Sandalwood powder was imported from India. Samples of Chrysanthemums (branches, flowers and leaves)(0.5 g) and red sandalwood powder (0.5 g) were subjected to the multi-element instrumental neutron activation analysis using epithermal neutrons (ENAA) at the IBR-2 reactor, Frank Laboratory of Neutron Physics (FLNP) JINR, Dubna. A total of 41 elements (Na, Mg, Al, Cl, K, Ca, Sc, V, Cr, Mn, Fe, Co, Ni, Zn, As, Se, Br, Rb, Sr, Zr, Mo, Cd, Cs, Ba, La, Hf, Ta, W, Sb, Au, Hg, Ce, Nd, Sm, Eu, Tb, Dy, Yb, Th, U, Lu) were determined. For the first time such a large group of elements was determined in the herbal plants used in Mongolia. The quality control of the analytical results was provided by using certified reference material Bowen Cabbage. The results obtained are compared to the ''Reference plant? data (B. Markert, 1992) and interpreted in terms of excess of such elements as Se, Cr, Ca, Fe, Ni, Mo, and rare earth elements.

  10. Epithermal Neutron Activation Analysis of the Asian Herbal Plants

    Science.gov (United States)

    Baljinnyam, N.; Jugder, B.; Norov, N.; Frontasyeva, M. V.; Ostrovnaya, T. M.; Pavlov, S. S.

    2011-06-01

    Asian medicinal herbs Chrysanthemum (Spiraea aquilegifolia Pall.) and Red Sandalwood (Pterocarpus Santalinus) are widely used in folk and Ayurvedic medicine for healing and preventing some diseases. The modern medical science has proved that the Chrysanthemum (Spiraea aquilegifolia Pall.) possesses the following functions: reducing blood press, dispelling cancer cell, coronary artery's expanding and bacteriostating and Red Sandalwood (Pterocarpus Santalinus) is recommended against headache, toothache, skin diseases, vomiting and sometimes it is taken for treatment of diabetes. Species of Chrysanthemums were collected in the north-eastern and central Mongolia, and the Red Sandalwood powder was imported from India. Samples of Chrysanthemums (branches, flowers and leaves) (0.5 g) and red sandalwood powder (0.5 g) were subjected to the multi-element instrumental neutron activation analysis using epithermal neutrons (ENAA) at the IBR-2 reactor, Frank Laboratory of Neutron Physics (FLNP) JINR, Dubna. A total of 41 elements (Na, Mg, Al, Cl, K, Ca, Sc, V, Cr, Mn, Fe, Co, Ni, Zn, As, Se, Br, Rb, Sr, Zr, Mo, Cd, Cs, Ba, La, Hf, Ta, W, Sb, Au, Hg, Ce, Nd, Sm, Eu, Tb, Dy, Yb, Th, U, Lu) were determined. For the first time such a large group of elements was determined in the herbal plants used in Mongolia. The quality control of the analytical results was provided by using certified reference material Bowen Cabbage. The results obtained are compared to the "Reference plant» data (B. Markert, 1992) and interpreted in terms of excess of such elements as Se, Cr, Ca, Fe, Ni, Mo, and rare earth elements.

  11. Activation analysis of mercury in head hair of dentists

    International Nuclear Information System (INIS)

    Mercury contents in head hair of 58 dentists, working at the hospital of Nihon University School of Dentistry, were determined using neutron activation analysis. The values ranged from 2.47 ppm to 13.7 ppm. The frequency distribution of the mercury contents increased steeply at about 2 ppm to the maximum of 4 -- 5 ppm, and decreased to about 11 ppm, its distribution pattern followed a log-normal one with a median of 5.46 ppm. The dentists were divided into two groups and the mercury contents in head hair of them were compared with each other. The arithmetic and geometric means of the values for dentists who handled amalgam in dental practice were 5.66 ppm (SD +- 1.80) and 5.40 ppm (SD x/ 1.36), while those for the dentists who did not handle amalgam in dental practice were 5.96 ppm (SD +- 2.82) and 5.38 ppm (SD x/ 1.59). The values of them agreed well with each other. The arithmetic mean for all dentists was 5.79 ppm (SD +- 2.28) and the geometric mean of them was 5.40 ppm (SD x/ 1.46). They were much lower than the values reported by Suzuki, Miyazawa or Sairenji, et al. in the past year, and they agreed well to those for normal Japanese men with the same age. Therefore it is concluded that proper mercury handling might be established in the dental office. (author)

  12. Recent applications of neutron activation analysis in Korea

    International Nuclear Information System (INIS)

    There are two purposes in this research; first aim is to promote the use of neutron activation analysis (NAA) as a utilization of nuclear research reactor in the field of air pollution studies through a routine and long-term monitoring. Other is to improve NAA with an experimental simplicity, high accuracy, excellent flexibility with respect to irradiation and counting conditions. For the study on air pollution, airborne particulate matter (APM) for the fine (< 2.5 μm EAD) and coarse particle (2.5-10 μm EAD) fractions were collected using the Gent stacked filter unit low volume sampler and two types of Nuclepore polycarbonate filters. Air samples were collected at two regions (suburban and industrial site of Daejeon city in the Republic of Korea) from January to December 2002. Mass concentration and elemental black carbon of APM were measured and the concentration of 25 elements were determined by Instrumental NAA. Analytical quality control is carried out using three certified reference materials (CRM). The monitoring data were treated statistically to assess air pollution source and source apportionment. The results obtained from this project can be used to investigate source identification and apportionment and its trends, and to establish a more cost-effective method for national air quality management. Preliminary experiment for application of ko-standardization method has been carried out to determine the reactor neutron spectrum parameters, i.e.a and f-values as the main factors of irradiation quality at NAA no.1 irradiation hole on HANARO research reactor, to determine peak detection efficiency for the HP Ge(EG and G ORTEC, GEM 35185) detector for the use in the ko-experiments and to compare the measured concentration results with the certified values of some CRMs applying the experimentally determined ko-parameters. (author)

  13. Proximate analysis for determination of micropores in granulated activated carbon

    Energy Technology Data Exchange (ETDEWEB)

    Berman, Ya. G.; Nikolaev, V.B.; Shepelev, A.N.

    1987-02-01

    A method is discussed for determining the specific micropore volume of granulated activated carbon used for water treatment in Soviet coking plants. Toluene molecules with a diameter of 0.67 nm are sorbed by activated carbon with micropore diameter ranging from 0.7 to 1.4 nm. Therefore, sorptive properties of activated carbon in relation to toluene supply information on micropore volume in carbon. A formula which describes this relation is derived. The method for determining micropore volume on the basis of toluene adsorption was tested using 8 types of activated carbon produced from coal and petroleum. Types of activated carbon characterized by the highest adsorption were selected. 1 ref.

  14. Elaboration of procedure for analysis of industrial and economic activities: the experience of LUKoil petroleum company

    International Nuclear Information System (INIS)

    The research and engineering centre within LUKoil company for economic studies has elaborated a method permitting analysis of production and economic activities of the LUKOIL petroleum production complex. The method envisages the following trends of analysis: general assessment of production and economic activities, analysis of basic production assets, manpower and wages use, net cost of marketable products, the state of finances, as well as specific features in analyzing the activities undertaken by joint ventures

  15. Elemental analysis of granite by instrumental neutron activation analysis (INAA) and X-ray fluorescence analysis (XRF)

    Energy Technology Data Exchange (ETDEWEB)

    El-Taher, A., E-mail: Atef_Eltaher@hotmail.com [Physics Department, Faculty of Science, Al-Azher University, Assuit 71452 (Egypt); Physics Department, Faculty of Science, Qassium University, Buraydah 51452 (Saudi Arabia)

    2012-01-15

    The instrumental neutron activation analysis technique (INAA) was used for qualitative and quantitative analysis of granite samples collected from four locations in the Aswan area in South Egypt. The samples were prepared together with their standards and simultaneously irradiated in a neutron flux of 7 Multiplication-Sign 10{sup 11} n/cm{sup 2} s in the TRIGA Mainz research reactor. Gamma-ray spectra from an hyper-pure germanium detector were analyzed. The present study provides the basic data of elemental concentrations of granite rocks. The following elements have been determined Na, Mg, K, Fe, Mn, Sc, Cr, Ti, Co, Zn, Ga, Rb, Zr, Nb, Sn, Ba, Cs, La, Ce, Nd, Sm, Eu, Yb, Lu, Hf, Ta, Th and U. The X-ray fluorescence (XRF) was used for comparison and to detect elements, which can be detected only by XRF such as F, S, Cl, Co, Cu, Mo, Ni, Pb, Se and V. The data presented here are our contribution to understanding the elemental composition of the granite rocks. Because there are no existing databases for the elemental analysis of granite, our results are a start to establishing a database for the Egyptian granite. It is hoped that the data presented here will be useful to those dealing with geochemistry, granite chemistry and related fields. - Highlights: Black-Right-Pointing-Pointer Instrumental neutron activation analysis technique (INAA) was used for qualitative and quantitative analysis of granite. Black-Right-Pointing-Pointer The samples were prepared together with their standards and simultaneously irradiated in a neutron flux of 7 Multiplication-Sign 10{sup 11} n/cm{sup 2} s in the TRIGA Mainz research reactor. Black-Right-Pointing-Pointer Following elements have been determined Na, Mg, K, Fe, Mn, Sc, Cr, Ti, Co, Zn, Ga, Rb, Zr, Nb, Sn, Ba, Cs, La, Ce, Nd, Sm, Eu, Yb, Lu, Hf, Ta, Th and U.

  16. Determination of copper in some Myanmar indigenous medicines by neutron activation analysis

    International Nuclear Information System (INIS)

    Copper was determined in two Myanmar indigenous medicines by neutron activation analysis using an Am(Be) radionuclide neutron source. The activity of 511 keV peak of the 64Cu was measured. (author) 2 refs.; 2 tabs

  17. The affect of industrial activities on zinc in alluvial Egyptian soil determined using neutron activation analysis

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Thirty-two surface (0-20 cm) soil samples were collected from different locations in Egypt representing non-polluted,moderately and highly polluted soils.The aim of this study was to evaluate total Zn content in alluvial soils of Nile Delta in Egypt by using the delayed neutron activation analysis technique (DNAA),in the irradiation facilities of the first Egyptian research reactor (ET-RR-1).The gamma-ray spectra were recorded with a hyper pure germanium detection system.The well resolved gamma-ray peak at 1116.0 kev was efficiently used for 65Zn content determination.Zn content in non-polluted soil samples ranged between 74.1 and 103.8 ppm with an average of 98.5 + 5.1 ppm.Zn content in moderately polluted soils ranged between 136.0 and 232.5 ppm with an average of 180.1 + 32.6 ppm.The highest Zn levels ranging from 240.0 and 733.0 ppm with an average of 410.3 + 54.4 ppm,were observed in soil samples collected from,either highly polluted agricultural soils exposed to prolonged irrigation with industrial wastewater or surface soil samples from industrial sites.

  18. A NOVEL GRAPH MODEL FOR E-MAIL FORENSICS: EVIDENCE ACTIVITY ANALYSIS GRAPH

    Directory of Open Access Journals (Sweden)

    Sridhar Neralla

    2013-10-01

    Full Text Available This work puts forward a novel technique for evidence analysis that assist cyber forensics expert for analyzing cyber crime episode in an effective manner. Novelty in Evidence Activity Analysis Graph is reflection of activities involved in the cyber crime that are represented as nodes along with stylometric analysis. In this pieceof work email based cyber crime incident is considered for study and that incident is represented in Evidence Activity Analysis Graph to fix the suspect. Comparisons between various graphs that are used in cyber forensics were also discussed in this paper. This model establishes relationships between various activities that were happened in the cyber crime.

  19. Chronic electromyographic analysis of circadian locomotor activity in crayfish.

    Science.gov (United States)

    Tomina, Yusuke; Kibayashi, Akihiro; Yoshii, Taishi; Takahata, Masakazu

    2013-07-15

    Animals generally exhibit circadian rhythms of locomotor activity. They initiate locomotor behavior not only reflexively in response to external stimuli but also spontaneously in the absence of any specific stimulus. The neuronal mechanisms underlying circadian locomotor activity can, therefore, be based on the rhythmic changes in either reflexive efficacy or endogenous activity. In crayfish Procambarus clarkii, it can be determined by analyzing electromyographic (EMG) patterns of walking legs whether the walking behavior is initiated reflexively or spontaneously. In this study, we examined quantitatively the leg muscle activity that underlies the locomotor behavior showing circadian rhythms in crayfish. We newly developed a chronic EMG recording system that allowed the animal to freely behave under a tethered condition for more than 10 days. In the LD condition in which the animals exhibited LD entrainment, the rhythmic burst activity of leg muscles for stepping behavior was preceded by non-rhythmic tonic activation that lasted for 1323±488ms when the animal initiated walking. In DD and LL free-running conditions, the pre-burst activation lasted for 1779±31 and 1517±39ms respectively. In the mechanical stimulus-evoked walking, the pre-burst activation ended within 79±6ms. These data suggest that periodic changes in the crayfish locomotor activity under the condition of LD entrainment or free-running are based on activity changes in the spontaneous initiation mechanism of walking behavior rather than those in the sensori-motor pathway connecting mechanoreceptors with leg movements.

  20. Planosol soil sample size for computerized tomography measurement of physical parameters; Tamanho de amostras para a determinacao de parametros fisicos em Planossolo por tomografia computadorizada

    Energy Technology Data Exchange (ETDEWEB)

    Pedrotti, Alceu [Sergipe Univ., Sao Cristovao, SE (Brazil). Dept. de Engenharia Agronomica]. E-mail: apedroti@ufs.br; Pauletto, Antonio [Universidade Federal de Pelotas, RS (Brazil). Faculdade de Agronomia Eliseu Maciel. Dept. de Solos; Crestana, Silvio; Cruvinel, Paulo Estevao; Vaz, Carlos Manoel Pedro; Naime, Joao de Mendonca; Silva, Alvaro Macedo da [Empresa Brasileira de Pesquisa Agropecuaria, Sao Carlos, SP (Brazil). Instrumentacao Agropecuaria

    2003-12-01

    Computerized tomography (CT) is an important tool in Soil Science for noninvasive measurement of density and water content of soil samples. This work aims to describe the aspects of sample size adequacy for Planosol (Albaqualf) and to evaluate procedures for statistical analysis, using a CT scanner with a {sup 241} Am source. Density errors attributed to the equipment are 0.051 and 0.046 Mg m{sup -3} for horizons A and B, respectively. The theoretical value for sample thickness for the Planosol, using this equipment, is 4.0 cm for the horizons A and B. The ideal thickness of samples is approximately 6.0 cm, being smaller for samples of the horizon B in relation to A. Alternatives for the improvement of the efficiency analysis and the reliability of the results obtained by CT are also discussed, and indicate good precision and adaptability of the application of this technology in Planosol (Albaqualf) studies. (author)

  1. Image patch analysis of sunspots and active regions

    Directory of Open Access Journals (Sweden)

    Moon Kevin R.

    2016-01-01

    Full Text Available Context. Separating active regions that are quiet from potentially eruptive ones is a key issue in Space Weather applications. Traditional classification schemes such as Mount Wilson and McIntosh have been effective in relating an active region large scale magnetic configuration to its ability to produce eruptive events. However, their qualitative nature prevents systematic studies of an active region’s evolution for example. Aims. We introduce a new clustering of active regions that is based on the local geometry observed in Line of Sight magnetogram and continuum images. Methods. We use a reduced-dimension representation of an active region that is obtained by factoring the corresponding data matrix comprised of local image patches. Two factorizations can be compared via the definition of appropriate metrics on the resulting factors. The distances obtained from these metrics are then used to cluster the active regions. Results. We find that these metrics result in natural clusterings of active regions. The clusterings are related to large scale descriptors of an active region such as its size, its local magnetic field distribution, and its complexity as measured by the Mount Wilson classification scheme. We also find that including data focused on the neutral line of an active region can result in an increased correspondence between our clustering results and other active region descriptors such as the Mount Wilson classifications and the R-value. Conclusions. Matrix factorization of image patches is a promising new way of characterizing active regions. We provide some recommendations for which metrics, matrix factorization techniques, and regions of interest to use to study active regions.

  2. Determination of mechanical damage from wells under oil and gas flow condition; Determinacao de dano mecanico em pocos sob condicao de escoamento de oleo e gas

    Energy Technology Data Exchange (ETDEWEB)

    Marques, J. B.D. [PETROBRAS S.A., Rio de Janeiro, RJ (Brazil); Trevisan, O. V. [Universidade Estadual de Campinas (UNICAMP), SP (Brazil)

    2008-07-01

    The well bore effect is one of the most difficult variables obtained from well test analysis under two-phase condition. The presence of the gas in a well inserted in reservoir, which operates under gas drive solution, hinders the development of the analytical model to determine the mechanical damage. It is one of the reasons of the using the single phase well test analysis methodologies become suitable to the multiphase cases. The determination of the well bore effect is justified; therefore it is possible to work over in the well in order to determinate the real potential productive. The main objective of this work is to reevaluate a method of determination of the mechanical damage gotten from a well test under two-phase condition. In this work a simplified model of reservoir simulation is constructed in a commercial simulator in order to validate the methodology. The refinement of the blocks near to the well adopted in the simulation is a good representation of the well mechanical damage which occurs in a homogeneous reservoir. The types of well test analysis used in this work are two: drawdown and buildup test. The results gotten for this methodology, as will be shown, are excellent quality and the model of simulation presented here can be used for other analytical methods studies in order to determinate the mechanical damage or other variable of the reservoir. (author)

  3. ACTIVITY ANALYSIS WITH HIDDEN MARKOV MODEL FOR AMBIENT ASSISTED LIVING

    Directory of Open Access Journals (Sweden)

    Dietmar Bruckner

    2012-06-01

    Full Text Available In an Ambient Assisted Living (AAL project the activities of the user will be analyzed. The raw data is from a motion detector. Through data processing the huge amount of dynamic raw data was translated to state data. With hidden Markov model, forward algorithm to analyze these state data the daily activity model of the user was built. Thirdly by comparing the model with observed activity sequences, and finding out the similarities between them, defined the best adapt routine in the model. Furthermore an activity routine net was built and used to compare with the hidden Markov model.

  4. Safety- and Risk Analysis Activities in Chemical Industry in Europe

    Energy Technology Data Exchange (ETDEWEB)

    Kozine, Igor; Duijm, Nijs Jan; Lauridsen Kurt [Risoe National Laboratory, Roskilde (Denmark). Systems Analysis Department

    2001-07-01

    The current paper gives an overview of the legislation and the methods used in safety and risk management in the chemical industry within Europe and in particular within the European Union. The paper is based on a report that has been written for the SOS-1 project under the Nordic nuclear safety research (NKS). Safety- and risk-related matters in the process industry, in particular, in chemical, within the EU are subject to consideration at three levels: (1) EU legislation, (2) European/intemational standardisation, and (3) socio-economic analysis. EC Directives define the 'essential requirements', e.g., protection of health and safety, that must be fulfilled when goods are placed on the market or some industry is put into operation. The European standards bodies (CEN, CENELEC and ETSI) have the task of establishing the corresponding technical specifications, meeting the essential requirements of the Directives, compliance with which will provide a presumption of conformity with the essential requirements. Such specifications are referred to as 'harmonised standards'. Compliance with harmonised standards remains voluntary, and manufacturers are free to choose any other technical solution that provides compliance with the essential requirements. This view is stated in the 'New Approach' to technical harmonisation and standardisation (details can be found on the web page: http://europe.eu.int/comm/enterprise/newapproach/standardization/index .html). Standardisation as well as the regulation of technical risks is increasingly being undertaken at European or international level. The European legislator limits its role to the affirmation of overall objectives, and leaves it to the economic players to draw up the technical procedures and standards to specify in detail the ways and means of attaining them. Many countries have introduced requirements that new legislation and/or administrative regulations be subject to socio-economic analysis

  5. An ecosystem analysis of the activated sludge microbial community.

    Science.gov (United States)

    Yiannakopoulou, Trissevyene V

    2010-01-01

    This study was undertaken (i) to investigate the interactions of the activated sludge microbial community in a chemostat with the "environment", such as the substrate composition and variations, (ii) to investigate how these interactions affect the quality of the treated effluent and (iii) to determine the limits or applicability conditions to the indicators and to the prediction potential of the treated effluent quality. This work presents (a) the experimental results obtained from a reactor fed municipal wastewater (Data Set2-DS2) concerning the reactor's operating conditions and the microbial community of the sludge (b) comparisons between DS2 and an older Data Set (DS1) obtained when the reactor was fed synthetic substrate, all other experimental conditions being identical, and (c) simulation results and sensitivity analyses of two model runs (R1 and R2, corresponding to DS1 and DS2). The first trophic level (P(1)) of the DS2 microbial community consisted of bacteria, the second trophic level (P(2)) of bacteria-eating protozoa, rotifers and nematodes and the third trophic level (P(3)) of carnivorous protozoa and arthropods. Rotifers were an important constituent of the DS2 microbial community. The DS1 and DS1 communities differed in total size, trophic level sizes and species composition. Correlations between the major microbial groups of DS2 community and either loading rates or effluent quality attributes were generally low, but the correlation of bacteria with SVI and ammonia in the effluent was better. Also, the ratio of rotifers to protozoa in P(2) was correlated to BOD in the effluent. The results of this work indicate that predictions of the treated effluent quality based only on protozoa may not be safe. Sensitivity analysis of R2 run indicate that, when variation in Y and K(d) biokinetic coefficients of the sludge are combined with fluctuations in composition and quality of municipal wastewater entering the reactor, then sufficient significant

  6. Committed effective dose determination in cereal flours by gamma-ray spectrometry; Determinacao das doses efetivas por ingestao de farinhas de cereais atraves da espectrometria de raios gama

    Energy Technology Data Exchange (ETDEWEB)

    Scheibel, Viviane

    2006-07-01

    The health impact from radionuclides ingestion of foodstuffs was evaluated by the committed effective doses determined in commercial samples of South-Brazilian cereal flours (soy, wheat, corn, manioc, rye, oat, barley and rice flour). The radioactivity traces of {sup 228}Th, {sup 228}Ra, {sup 226}Ra, {sup 40}K, {sup 7}Be and {sup 137}Cs were measured by gamma-ray spectrometry employing a 66% relative efficiency HPGe detector. The energy resolution for the 1332.46 keV line of {sup 60}Co was 2.03 keV. The committed effective doses were calculated with the activities analyzed in the present flour samples, the foodstuff rates of consumption (Brazilian Institute of Geography and Statistics) and the ingestion dose coefficients (International Commission of Radiological Protection). The reliability median activities were verified with {chi}{sup 2} tests, assuring the fittings quality. The highest concentration levels of {sup 228}Th and {sup 40}K were 3.5 {+-} 0.4 and 1469 {+-} 17 Bq.kg{sup -1} for soy flour, respectively, with 95% of confidence level. The lower limit of detection for {sup 137}Cs ranged from 0.04 to 0.4 Bq.kg{sup -1}. The highest committed effective dose was 0.36 {mu}Sv.y{sup -1} for {sup 228}Ra in manioc flour (adults). All committed effective doses determined at the present work were lower than the UNSCEAR limits of 140 {mu}Sv.y{sup -1} and much lower than the ICRP (1991) limits of 1 mSv.y{sup -1}, for general public. There are few literature references for natural and artificial radionuclides in foodstuffs and mainly for committed effective doses. This work brings the barley flour data, which is not present at the literature and {sup 7}Be data which is not encountered in foodstuffs at the literature, besides all the other flours data information about activities and committed effective doses. (author)

  7. Active tourism as a tourist mode in expansion. Analysis of the supply of active tourism in Spain

    Directory of Open Access Journals (Sweden)

    Noelia Araújo Vila

    2012-06-01

    Full Text Available Parallel to the social and economic situation, where the experience economy is a reality, new tourist typologies are emerging in line with this demand experiential. Tourists are looking for sensations and emotions, so tourism sector has diversified its offer adapting to this desire. Active tourism appears, mode belonging to a larger field, nature tourism, a booming tourist type today by the increase of tourists interested in its activities. Therefore, this paper takes from this concept to below detail the types that are part of it, and finally it does an analysis of the active tourism offer of the Spanish territory, territory that is appropriate for this type of activity.

  8. Evolution & Phylogenetic Analysis: Classroom Activities for Investigating Molecular & Morphological Concepts

    Science.gov (United States)

    Franklin, Wilfred A.

    2010-01-01

    In a flexible multisession laboratory, students investigate concepts of phylogenetic analysis at both the molecular and the morphological level. Students finish by conducting their own analysis on a collection of skeletons representing the major phyla of vertebrates, a collection of primate skulls, or a collection of hominid skulls.

  9. Multi-element analysis of the obese subject by in vivo neutron activation analysis

    International Nuclear Information System (INIS)

    The Leeds facility for in vivo neutron activation analysis has been modified and calibrated for the simultaneous measurement of nitrogen, potassium, sodium, chlorine, phosphorus and calcium in obese patients weighing up to 210 kg. The effects of body size and shape were incorporated into the calibration by measuring 14 anthropomorphic phantoms of known composition representing individual patients being treated for obesity. The phantoms were constructed from tissue substitutes representing lean skeletal and adipose tissues, arranged to simulate the distributions of the corresponding tissues within the patients, as visualised by CT scanning. The precision of the method, determined by measuring a single phantom ten times over a period of ten weeks, is between two and three per cent for all elements except calcium, for which it is 11.3%. Accuracy is estimated to be similar to precision. The procedure has been used to study changes in body composition of patients undergoing therapeutic starvation. (author)

  10. The path of obsidian at the Tajin region. Origin analysis through Neutron Activation Analysis

    International Nuclear Information System (INIS)

    The task of contemporary archaeology is extended every day; new techniques and new instruments have been incorporating to those tools which the archaeologist has in order to achieve a better approach to his study object. The archaeology had been exploring in the physical chemical sciences with the purpose to obtain information beyond the traditional methodologies and so obtaining more and best data. The sudden advance in the knowledge of the basic particles which make up the matter can be applied to these archaeological studies too. Archaeology takes part of the new possibilities which nuclear physics offers in the study of materials such as ceramics, clays, metal alloys, native metals and practically some lithological source. In Latin America the neutron activation analysis was used first for the characterization and determination of the ceramics origin. Some regions have been better studied from the point of view of obsidian exploitation and consumption, such is the case of El Tajin and Oaxaca region in Mexico. (Author)

  11. Analysis of some egyptian cosmetic samples by using fast neutron activation analysis

    International Nuclear Information System (INIS)

    A description of our neutron generator (NG) facility for neutron activation analysis is presented. As an example, the concentration of Na, Mg, Al, Si, K, Cl, Ca and Fe elements were determined in two domestic brands of face powder by using a beam of 14 MeV neutrons. An empirical expression for detector efficiency in terms of incident gamma ray energy and the source-detector distance has been obtained for a hyper pure germanium detector (HPGe) using different standard point sources. The comparison of the calculated efficiencies and the measured values in the energy range from 59.5 to 1332.2 keV and for source-to-detector distances of 5-30 cm show the agreement between the calculated values and the measured experimental values

  12. Multielement analysis of environmental reference materials by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Concentrations of trace elements in environmental reference materials prepared by the National Institute for Environmental Studies, Japan (NIES) and by the National Institute of Standards and Technology, USA (NIST) were determined by instrumental neutron activation analysis (INAA). NIES CRM No. 5 Human Hair, No. 6 Mussel, No. 7 Tea Leaves, No. 8 Vehicle Exhaust Particulates, No. 9 Sargasso and No. 10 Rice Flour-unpolished samples (ca. 150 - 1200 mg) and NIST SRM 1632a Bituminous Coal, SRM 1635 Sub-bituminous Coal and SRM 1633a Coal Fly Ash samples (ca. 10 - 150 mg) were irradiated at the Musashi Institute of Technology Research Reactor (MITRR). Concentrations of 28 - 52 elements in these NIES and NIST environmental reference materials were determined by two irradiation methods and four γ-ray counting methods. The determined values were in good agreement with the NIES and NIST certified values. (author)

  13. Trace Element Analysis of Human Lung Tissue by Neutron Activation and Instrumental Analysis

    International Nuclear Information System (INIS)

    The measurement of trace elements in tissues in the ppm to pp109 range requires very careful and specialized techniques both in the sample acquisition and in subsequent analysis. Many of the trace elements which are present in human tissues are at lower concentrations than those in super-pure chemical reagents; also, an acid rinse of typical laboratory glassware may contain as much of some trace elements as the tissue sample being studied. An analytical technique based on neutron activation for the measurement of trace elements in tissues has been developed which requires a minimum of pre-irradiation handling followed by the direct measurement of the activation products on a multidimensional or a solid-state gammaray spectrometer. This technique has been applied to a study of trace elements in human lung tissue. Lung tissue contains not only the tissue-bound elements but also those which have been deposited in the cells of the pulmonary alveoli through inhalation. The method permits the direct measurement of 15 trace elements. The analysis of lung tissues thus provides information on the integrated trace element deposition resulting during the life of an individual. The concentrations of several of these including Fe, Br, P, Se, Ag, Zn, Cs, Co, Sc, U and Sb have been measured in several autopsy and biopsy samples of both normal and diseased tissues from several subjects with known case histories. The variations in the observed trace element compositions are presented and considered in terms of the occupational and medical history of the subject. (author)

  14. Adult active transport in the Netherlands: An analysis of its contribution to physical activity requirements

    NARCIS (Netherlands)

    Fishman, E; Böcker, L; Helbich, M

    2015-01-01

    Modern, urban lifestyles have engineered physical activity out of everyday life and this presents a major threat to human health. The Netherlands is a world leader in active travel, particularly cycling, but little research has sought to quantify the cumulative amount of physical activity through ev

  15. Analysis of Essential Elements for Plants Growth Using Instrumental Neutron Activation Analysis

    Directory of Open Access Journals (Sweden)

    R. L. Njinga

    2013-01-01

    Full Text Available In this study, a total of ten essential elements for plants growth in the Guinea savanna region of Niger State in Northern Nigeria have been identified in the soils using instrumental neutron activation analysis. The experimental results show good agreement with certified or literature values within the agreed percentage range of ±2.35% to ±8.69%. However, the concentration distributions of the ten identified elements in the soil samples within the studied area for plants growth revealed the following: Fe (123.4 ppm, Mn (2100.7 ppm, K (5544.3 ppm, Al (54752.4 ppm, Ti (3082.9 ppm, Ca (4635 ppm, V (54.3 ppm, Na (857.5 ppm, Mg (13924.1 ppm, and Dy (12.1 ppm. A further analysis of the two fundamental soil physical parameters for healthy growth of some common crops like egusimelon, groundnut, rice, yams, soybeans, cassava, and potato analyzed in this work revealed a pH range of 4.0 pH–8.0 pH and a temperature range of 28.0°C to 29.3°C, which are optimal for plant nutrients availability in the soils within the study area.

  16. Determination of volatiles produced during radiation processing in food and medicinal herbs; Determinacao de volateis produzidos durante o processamento por radiacao em ervas alimenticias e medicinais

    Energy Technology Data Exchange (ETDEWEB)

    Salum, Debora Christina

    2008-07-01

    In order to protect food from pathogenic microorganisms as well as to increase its shelf life while keeping sensorial properties (e.g. odor and taste), once the latter are one of the main properties required by spice buyers, it is necessary to analyze volatile formation from irradiation of medicinal and food herbs. The aim of the present study was to analyze volatile formation from Co irradiation of Laurus Cinnamomum, Piper Nigrum, Origanum Vulgare and Myristica Fragans. Possible changes on the odor of these herbs are evaluated by characterizing different radiation doses and effects on sensorial properties in order to allow better application of irradiation technology. l he samples have been irradiated in plastic packages by making use of a {sup 60}Co Gamma irradiator. Irradiation doses of 0, 5, 10, 15, 20 and 25kGy have been tested. For the analysis of the samples, SPME has been applied, while for the analysis of volatile compounds, CG/MS. Spice irradiation has promoted mostly decrease in volatile compounds when doses of 5, 10, 15, 20 and 25kGy were used. For Laurus cinnamomum, the irradiation decreased volatile by nearly 56% and 89.5% respectively, comparing to volatile from a sample which has not been previously irradiated. Differently from other spices analyzed, irradiation on Myristica Fragans has increased volatile compounds except for 4-terpineol. The miristicine (toxic substance when in large quantities, commonly mentioned as narcotic) has increased by nearly 80%. For Origanum Vulgare and Piper Nigrum, significant decrease in volatile compounds have been found, mainly when it comes to 25 kGy irradiation. In general, results indicate loss of sensorial quality of spices. (author)

  17. Study of the elemental composition of Chenopodium Quinoa Willd by fast neutron activation analysis and X ray fluorescence analysis

    International Nuclear Information System (INIS)

    By means of x-ray fluorescence and fast neutron activation analysis the nitrogen content has been determined in samples of roots, stems, leaf, flowers and grains from Quinua (Chenopodium Quinoa Willd), which was previously treated with fertilizer

  18. Study on the methods for analysis of the chemical poison in canister by neutron activity

    International Nuclear Information System (INIS)

    The method that is used to analyse the poison gases in canister by neutron activity is proposed. Through theory analysis and experimental measurement, the feasibility for analysis of the poison gases in a canister by neutron activity has been demonstrated, and it is proved that the method itself do not result in radioactive problem to use again the canister. (authors)

  19. Instrumental neutron activation analysis of carbonatites from Panda Hill and Oldoinyo-Lengai, Tanzania

    International Nuclear Information System (INIS)

    Twenty nine (major and trace) elements including nine rare earth elements (REE) in African carbonatite samples were determined by instrumental neutron activation analysis (INAA). The geochemical behavior of trace elements in carbonatites, especially REE pattern (chondrite normalized), and the efficiency of neutron activation analysis compared to other methods are discussed in this study. (author)

  20. Teaching Tip: Using Activity Diagrams to Model Systems Analysis Techniques: Teaching What We Preach

    Science.gov (United States)

    Lending, Diane; May, Jeffrey

    2013-01-01

    Activity diagrams are used in Systems Analysis and Design classes as a visual tool to model the business processes of "as-is" and "to-be" systems. This paper presents the idea of using these same activity diagrams in the classroom to model the actual processes (practices and techniques) of Systems Analysis and Design. This tip…

  1. Application of neutron activation analysis system in Xi'an pulsed reactor

    CERN Document Server

    Zhang Wen Shou; Yu Qi

    2002-01-01

    Neutron Activation Analysis System in Xi'an Pulsed Reactor is consist of rabbit fast radiation system and experiment measurement system. The functions of neutron activation analysis are introduced. Based on the radiation system. A set of automatic data handling and experiment simulating system are built. The reliability of data handling and experiment simulating system had been verified by experiment

  2. Analysis and modeling of container terminal handling activities

    OpenAIRE

    Armando CARTENÌ; Luca, Stefano de

    2010-01-01

    Although the technical literature contains numerous efforts to simulate container terminal performance, little attention has been paid to setting up, calibrating and validating models for handling equipment activities. This paper presents results from the estimation of activity duration concerning three different types of handling equipment: mobile harbor cranes, gantry cranes and reach stackers. Two estimation approaches (sample means vs. random variables) were investigated with respect to d...

  3. IN VITRO ANALYSIS OF MIGRATION ACTIVITY OF ENCEPHALYTOGENIC T CEL

    OpenAIRE

    M. A. Nosov; E. A. Korneva

    2014-01-01

    Experimental autoimmune encephalomyelitis in an adoptive transfer model is caused by injecting animal with activated T cells specific for a CNS antigen, e.g., basic myelin protein. Development of autimmune inflammation in such a model is connected with changed functional stateof encephalytogenic (EG) T cells in the coure of disease progression, as reflected by changes in their activation, proliferation and motility levels. Present work describes an original technique allowing for in vitro ana...

  4. Phytochemical analysis and in vitro antioxidant activity of Uncaria gambir

    Directory of Open Access Journals (Sweden)

    Mohd Amir

    2012-01-01

    Full Text Available The present research work was carried out to evaluate the antioxidant potential and antiradical property of methanolic extract of Uncaria gambir. Antioxidant and radical scavenging activity were determined by using different in vitro assays including reducing power assay, superoxide anion scavenging activity assay, hydroxyl radical scavenging activity assay, nitric oxide scavenging activity assay, DPPH free radical scavenging assay and hydrogen peroxide method. Preliminary phytochemical screening revealed that the extract of U. gambir possesses flavonoids, alkaloids and phenolic materials. In the present investigation, quantitative estimation of flavonoids content and phenolic content was also carried out by colorimetric methods, using aluminium chloride and Folin-Ciocalteu reagent method, respectively, to establish relationship between antioxidant activity and total phenolics and flavonoid contents. The total phenolic and flavonoid contents were found to be 18.37±2.79 mg gallic acid equivalents (GAE/g dry weight and 5.82±2.23 mg rutin equivalents (RE/g dry weight, respectively. The extract showed significant antioxidant activity in a dose-dependent manner in all the assays. The IC 50 values of all parameters were determined. Ascorbic acid was used as standard. The results obtained in the present study indicated that U. gambir extract could be a potential source of natural antioxidant.

  5. Development of Distinction Method of Production Area of Ginsengs by Using a Neutron Activation Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Young Jin; Chung, Yong Sam; Sun, Gwang Min; Lee, Yu Na; Yoo, Sang Ho [KAERI, Daejeon (Korea, Republic of)

    2010-05-15

    Distinction of production area of Korean ginsengs has been tried by using neutron activation techniques such as an instrumental neutron activation analysis (INAA) and a prompt gamma activation analysis (PGAA). A distribution of elements has varied according to the part of plant clue to the difference of enrichment effect and influence from a soil where the plants have been grown. So correlation study between plants and soil has been an Issue. In this study, the distribution of trace elements within a Korean ginseng was investigated by using an instrumental neutron activation analysis

  6. Elemental analysis of granite by instrumental neutron activation analysis (INAA) and X-ray fluorescence analysis (XRF).

    Science.gov (United States)

    El-Taher, A

    2012-01-01

    The instrumental neutron activation analysis technique (INAA) was used for qualitative and quantitative analysis of granite samples collected from four locations in the Aswan area in South Egypt. The samples were prepared together with their standards and simultaneously irradiated in a neutron flux of 7×10(11)n/cm(2)s in the TRIGA Mainz research reactor. Gamma-ray spectra from an hyper-pure germanium detector were analyzed. The present study provides the basic data of elemental concentrations of granite rocks. The following elements have been determined Na, Mg, K, Fe, Mn, Sc, Cr, Ti, Co, Zn, Ga, Rb, Zr, Nb, Sn, Ba, Cs, La, Ce, Nd, Sm, Eu, Yb, Lu, Hf, Ta, Th and U. The X-ray fluorescence (XRF) was used for comparison and to detect elements, which can be detected only by XRF such as F, S, Cl, Co, Cu, Mo, Ni, Pb, Se and V. The data presented here are our contribution to understanding the elemental composition of the granite rocks. Because there are no existing databases for the elemental analysis of granite, our results are a start to establishing a database for the Egyptian granite. It is hoped that the data presented here will be useful to those dealing with geochemistry, granite chemistry and related fields. PMID:21992845

  7. Determination of {sup 210}Pb and {sup 210}Po in cigarette tobacco; Determinacao de {sup 210}Pb e {sup 210}Po em tabaco de cigarros nacionais

    Energy Technology Data Exchange (ETDEWEB)

    Peres, Ana Claudia

    1999-07-01

    Cigarette smoking is one of the important pathways that could contribute to enhance the radiation dose to man, due to the relatively large concentrations of {sup 210}Pb and {sup 210}Po found in tobacco leaves. In this work, concentrations of these two radionuclides were determined in eight of the most commercialized cigarette brands produced in Brazil. The samples analyzed were bought randomly in the market. The {sup 210}Pb was determined by counting the beta activity of the {sup 210}Bi in a gas flow proportional detector, after radiochemical separation and precipitation of the PbCr0{sub 4}. The {sup 210}Po was determined by alpha spectrometry, using a surface barrier detector, after radiochemical separation and spontaneous deposition of Po in copper disk. The results showed concentrations ranging from 11,9 to 30,2 mBq per gram of dry tobacco for {sup 210}Pb and from 10,9 to 27,4 mBq per gram of dry tobacco for {sup 210}Po. (author)

  8. QSAR analysis on Spodoptera litura antifeedant activities for flavone derivatives

    Energy Technology Data Exchange (ETDEWEB)

    Duchowicz, Pablo R., E-mail: pabloducho@gmail.com [Instituto de Investigaciones Fisicoquimicas Teoricas y Aplicadas INIFTA (UNLP, CCT La Plata-CONICET), Diag. 113 y 64, Sucursal 4, C.C. 16, 1900 La Plata (Argentina); Goodarzi, Mohammad [Instituto de Investigaciones Fisicoquimicas Teoricas y Aplicadas INIFTA (UNLP, CCT La Plata-CONICET), Diag. 113 y 64, Sucursal 4, C.C. 16, 1900 La Plata (Argentina); Ocsachoque, Marco A. [Centro de Investigacion y Desarrollo en Ciencias Aplicadas ' Dr. J. J. Ronco' (CINDECA), Departamento de Quimica, Facultad de Ciencias Exactas, UNLP-CONICET. Calle 47 No 257, B1900AJK La Plata (Argentina); Romanelli, Gustavo P. [Centro de Investigacion y Desarrollo en Ciencias Aplicadas ' Dr. J. J. Ronco' (CINDECA), Departamento de Quimica, Facultad de Ciencias Exactas, UNLP-CONICET. Calle 47 No 257, B1900AJK La Plata (Argentina); Catedra de Quimica Organica, Facultad de Ciencias Agrarias y Forestales, UNLP. Calles 60 y 119, B1904AAN La Plata (Argentina); Ortiz, Erlinda del V. [Facultad de Tecnologia y Ciencias Aplicadas, Universidad Nacional de Catamarca, Av. Maximio Victoria 55, (4700), Catamarca (Argentina); Autino, Juan C.; Bennardi, Daniel O.; Ruiz, Diego M. [Catedra de Quimica Organica, Facultad de Ciencias Agrarias y Forestales, UNLP. Calles 60 y 119, B1904AAN La Plata (Argentina); Castro, Eduardo A. [Instituto de Investigaciones Fisicoquimicas Teoricas y Aplicadas INIFTA (UNLP, CCT La Plata-CONICET), Diag. 113 y 64, Sucursal 4, C.C. 16, 1900 La Plata (Argentina)

    2009-12-20

    We establish useful models that relate experimentally measured biological activities of compounds to their molecular structure. The pED{sub 50} feeding inhibition on Spodoptera litura species exhibited by aurones, chromones, 3-coumarones and flavones is analyzed in this work through the hypothesis encompassed in the Quantitative Structure-Activity Relationships (QSAR) Theory. This constitutes a first necessary computationally based step during the design of more bio-friendly repellents that could lead to insights for improving the insecticidal activities of the investigated compounds. After optimizing the molecular structure of each furane and pyrane benzoderivative with the semiempirical molecular orbitals method PM3, more than a thousand of constitutional, topological, geometrical and electronic descriptors are calculated and multiparametric linear regression models are established on the antifeedant potencies. The feature selection method employed in this study is the Replacement Method, which has proven to be successful in previous analyzes. We establish the QSAR both for the complete molecular set of compounds and also for each chemical class, so that acceptably describing the variation of the inhibitory activities from the knowledge of their structure and thus achieving useful predictive results. The main interest of developing trustful QSAR models is that these enable the prediction of compounds having no experimentally measured activities for any reason. Therefore, the structure-activity relationships are further employed for investigating the antifeedant activity on previously synthesized 2-,7-substituted benzopyranes, which do not pose any measured values on the biological expression. One of them, 2-({alpha}-naphtyl)-4H-1-benzopyran-4-one, results in a promising structure to be experimentally analyzed as it has predicted pED{sub 50} = 1.162.

  9. How much locomotive activity is needed for an active physical activity level: analysis of total step counts

    Directory of Open Access Journals (Sweden)

    Ohkawara Kazunori

    2011-11-01

    Full Text Available Abstract Background Although physical activity recommendations for public health have focused on locomotive activity such as walking and running, it is uncertain how much these activities contribute to overall physical activity level (PAL. The purpose of the present study was to determine the contribution of locomotive activity to PAL using total step counts measured in a calorimeter study. Methods PAL, calculated as total energy expenditure divided by basal metabolic rate, was evaluated in 11 adult men using three different conditions for 24-hour human calorimeter measurements: a low-activity day (L-day targeted at a low active level of PAL (1.45, and a high-frequency moderate activity day (M-day or a high-frequency vigorous activity day (V-day targeted at an active level of PAL (1.75. These subjects were permitted only light activities except prescribed activities. In a separate group of 41 adults, free-living PAL was evaluated using doubly-labeled water (DLW. In both experiments, step counts per day were also measured using an accelerometer. Results In the human calorimeter study, PAL and step counts were 1.42 ± 0.10 and 8,973 ± 543 steps/d (L-day, 1.82 ± 0.14 and 29,588 ± 1,126 steps/d (M-day, and 1.74 ± 0.15 and 23,755 ± 1,038 steps/d (V-day, respectively. In the DLW study, PAL and step counts were 1.73 ± 0.15 and 10,022 ± 2,605 steps/d, and there was no significant relationship between PAL and daily step counts. Conclusions These results indicate that an enormous number of steps are needed for an active level of PAL if individuals extend physical activity-induced energy expenditure by only locomotive activity. Therefore, non-locomotive activity such as household activity should also play a significant role in increasing PAL under free-living conditions.

  10. Adult active transport in the Netherlands: An analysis of its contribution to physical activity requirements

    OpenAIRE

    Elliot Fishman; Lars Böcker; Marco Helbich

    2015-01-01

    Introduction Modern, urban lifestyles have engineered physical activity out of everyday life and this presents a major threat to human health. The Netherlands is a world leader in active travel, particularly cycling, but little research has sought to quantify the cumulative amount of physical activity through everyday walking and cycling. Methods Using data collected as part of the Dutch National Travel Survey (2010 – 2012), this paper determines the degree to which Dutch walking and cycling ...

  11. Trace analysis measurements in high-purity aluminium by means of radiochemical neutron and proton activation analysis

    International Nuclear Information System (INIS)

    The aim of the study consisted in the development of efficient radiochemical composite processes and activation methods for the multi-element determination of traces within the lower ng range in high-purity aluminium. More than 50 elements were determined with the help of activation with reactor neutrons; the selective separation of matrix activity (adsorption with hydrated antimony pentoxide) led to a noticeable improvement of detectability, as compared with instrumental neutron activation analysis. Further improvements were achieved with the help of radiochemical group separations in ion exchangers or with the help of the selective separation of the pure beta-emitting elements. Over 20 elements up to high atomic numbers were determined by means of activating 13 MeV protons and 23 Me protons. In this connection, improvements of the detection limit by as a factor of 10 were achieved with radiochemical separation techniques, as compared with pure instrumental proton activation analysis. (RB)

  12. A Social Network Analysis Approach to Detecting Suspicious Online Financial Activities

    Science.gov (United States)

    Tang, Lei; Barbier, Geoffrey; Liu, Huan; Zhang, Jianping

    Social network analysis techniques can be applied to help detect financial crimes. We discuss the relationship between detecting financial crimes and the social web, and use select case studies to illustrate the potential for applying social network analysis techniques. With the increasing use of online financing services and online financial activities, it becomes more challenging to find suspicious activities among massive numbers of normal and legal activities.

  13. Determination and environmental estimation of NORMs in marine sediment environment of offshore platforms; Determinacao e avaliacao ambiental de NORMs em sedimento marinho entorno de plataformas offshore

    Energy Technology Data Exchange (ETDEWEB)

    Vegueria, Sergio F. Jerez, E-mail: sfjerez@vm.uff.br [Universidade Federal Fluminense (UFF), Niteroi, RJ (Brazil). Departamento de Quimica Analitica; Godoy, Jose M., E-mail: rccampos@puc-rio.br, E-mail: jmgodoy@puc-rio.br [Instituto de Radioprotecao e Dosimetria (IRD/CNEN-RJ), Rio de Janeiro, RJ (Brazil)

    2013-07-01

    The natural radioactive materials (NORM known as) are found in the earth's crust, and during the process of production of oil and gas are concentrated in the produced water and the fouling (scale) pipes used for extraction. The production of oil and gas from produced water comes, comprising: forming water (water naturally present in the well ); injection water , usually sea water previously injected into the well to maintaining the pressure while the oil is removed; and water condensed in some cases of gas production. A high radioactivity of {sup 226}Ra (natural grade of {sup 238}U) and {sup 228}Ra (from the natural series of {sup 232}Th) is detected in produced water due to the high solubility of radio in formation water as uranium and thorium, which are insoluble in this medium, remain the rock matrix. The study was conducted in the area of offshore oil production in the state of Rio de January and included the determination of uranium, {sup 226}Ra, {sup 210}Pb and {sup 228}Ra in marine sediment near the points of discharge of produced water from oil platforms. After the pre-treatment and digestion of samples, the determination of the natural uranium was performed on a mass spectrometer with inductively coupled plasma (ICP -MS). The activities of {sup 226}Ra and {sup 228}Ra were determined by high resolution gamma spectrometry through {sup 214}Bi and {sup 228}Ac , respectively. And in the case of {sup 210}Pb, a correction was made for self-absorption employing an external source of this radionuclide. The results showed that there is no impact in sediments in the vicinity of the studied platforms.

  14. Chemical Analysis and Biological Activity of Jordanian Chamomile Extracts

    Directory of Open Access Journals (Sweden)

    Nawal Hassan Al Bahtiti

    2012-02-01

    Full Text Available The Jordanian chamomile (Matricaria chamomilla has been researched more thoroughly to evaluate its useful properties. It is investigated and found that Jordanian chamomile is rich in phenolic compounds, with beneficial biological activities. By applying the most promising HPLC method, the content of total phenolics in methanolic extract was determined according to the Folin-Clocalteu procedure, and was found (GAE>20 mg/g. The flavonoid types were found as flavones and flavonolos.The minimum inhibitory concentration values for methanolic extracts of Jordanian chamomile were determined for different kinds of bacteria. The extracts have activity against Staphylococcus aurous, candida albicans, Esherichia Coli, Betula pubescens and Pinus sylvestris. The activity has been observed to be due to the tannins and a pigenin present in the extract. To utilize these significant sources of natural compounds, further characterization of phenolic composition is needed.

  15. Flipping the Audience Script: An Activity That Integrates Research and Audience Analysis

    Science.gov (United States)

    Lam, Chris; Hannah, Mark A.

    2016-01-01

    This article describes a flipped classroom activity that requires students to integrate research and audience analysis. The activity uses Twitter as a data source. In the activity, students identify a sample, collect customer tweets, and analyze the language of the tweets in an effort to construct knowledge about an audience's values, needs, and…

  16. Activation and afterheat analysis for CH HCSB TBM

    Institute of Scientific and Technical Information of China (English)

    CHEN Zhi; FENG Kai-ming; ZHANG Guo-shu; YUAN Tao

    2006-01-01

    With an activation calculation code FDKR and decay chain data library AF-DCDLIB, the radioactivity,afterheat decay and Biological Hazard Potential (BHP) from activation products have been analyzed in the CH HCSB TBM. The calculation results show that the total radioactivity inventory, heat decay and BHP are 2.10×1016Bq、5.06×10-3 MW、68.6 km3·(Kw)-1,respectively, at shutdown after a continuous irradiation over 0.53 years with 500 MW fusion power.It shows that there isn't seriously environmental safety issue in the TBM.

  17. Use of radioactive methods for determination of uranium, neptunium, plutonium, americium and curium isotopes in waste radioactive; Utilizacao de metodos radioanaliticos para determinacao de isotopos de uranio, netunio, plutonio, americio e curio em rejeitos radioativos

    Energy Technology Data Exchange (ETDEWEB)

    Geraldo, Bianca

    2012-07-01

    Activated charcoal is a common type of radioactive waste that contains high concentrations of fission and activation products. The management of this waste includes its characterization aiming the determination and quantification of the specific radionuclides including those known as Difficult-to-Measure Radionuclides (RDM). The analysis of the RDM's generally involves complex radiochemical analysis for purification and separation of the radionuclides, which are expensive and time-consuming. The objective of this work was to define a methodology for sequential analysis of the isotopes of uranium, neptunium, plutonium, americium and curium present in a type of radioactive waste, evaluating chemical yield, analysis of time spent, amount of secondary waste generated and cost. Three methodologies were compared and validated that employ ion exchange (TI+EC), extraction chromatography (EC) and extraction with polymers (ECP). The waste chosen was the activated charcoal from the purification system of primary circuit water cooling the reactor IEA-R1. The charcoal samples were dissolved by acid digestion followed by purification and separation of isotopes with ion exchange resins, extraction and chromatographic extraction polymers. Isotopes were analyzed on an alpha spectrometer, equipped with surface barrier detectors. The chemical yields were satisfactory for the methods TI+EC and EC. ECP method was comparable with those methods only for uranium. Statistical analysis as well the analysis of time spent, amount of secondary waste generated and cost revealed that EC method is the most effective for identifying and quantifying U, Np, Pu, Am and Cm present in charcoal. (author)

  18. Oneiric activity in schizophrenia: textual analysis of dream reports.

    Science.gov (United States)

    Zanasi, Marco; Calisti, Fabrizio; Di Lorenzo, Giorgio; Valerio, Giulia; Siracusano, Alberto

    2011-06-01

    This work evaluated the structure of dreams in people affected by schizophrenia. The verbal reports of 123 schizophrenic patients were compared with 123 dream reports from a control group. In accordance with the Jungian conceptualization of, dreams as texts, dream reports were assessed using textual analysis processing techniques. Significant differences were found in textual parameters, showing that the dreams reports of schizophrenic patients differ from those of the control group. It is thus possible that schizophrenia probably underlies changes in the oneiric production and dream reports. This work confirms the value of textual analysis in the study of oneiric material. PMID:20472473

  19. Carbon analysis in CdTe by nuclear activation

    Science.gov (United States)

    Chibani, H.; Stoquert, J. P.; Hage-Ali, M.; Koebel, J. M.; Abdesselam, M.; Siffert, P.

    1991-06-01

    We describe the capabilities of the nuclear reaction 12C(d, n) 13Nlimit→β +13C the measurement of absolute concentrations of C in CdTe by the charged particle activation (CPA) method. This technique is used to determine the segregation coefficient of C introduced as an impurity in CdTe.

  20. Human Activity Recognition as Time-Series Analysis

    Directory of Open Access Journals (Sweden)

    Hyesuk Kim

    2015-01-01

    Full Text Available We propose a system that can recognize daily human activities with a Kinect-style depth camera. Our system utilizes a set of view-invariant features and the hidden state conditional random field (HCRF model to recognize human activities from the 3D body pose stream provided by MS Kinect API or OpenNI. Many high-level daily activities can be regarded as having a hierarchical structure where multiple subactivities are performed sequentially or iteratively. In order to model effectively these high-level daily activities, we utilized a multiclass HCRF model, which is a kind of probabilistic graphical models. In addition, in order to get view-invariant, but more informative features, we extract joint angles from the subject’s skeleton model and then perform the feature transformation to obtain three different types of features regarding motion, structure, and hand positions. Through various experiments using two different datasets, KAD-30 and CAD-60, the high performance of our system is verified.

  1. Determination of rhenium in molybdenite by neutron-activation analysis.

    Science.gov (United States)

    Terada, K; Yoshimura, Y; Osaki, S; Kiba, T

    1967-01-01

    A neutron-activation method is described for the determination of rhenium in molybdenite. Radiochemical separation by a carrier technique was carried out very rapidly by means of successive liquid-liquid extraction processes. The recovery of rhenium, which was determined by a spectrophotometric method, was about 93%. About 10 samples could be analysed within 6 hr in parallel runs. PMID:18960067

  2. Proteomic analysis of macrophage activated with salmonella lipopolysaccharide

    Science.gov (United States)

    Macrophages play pivotal role in immunity. They are activated by many pathogen derived molecules such as lipopolysaccharides (LPS) which trigger the production of various proteins and peptides that drive and resolve inflammation. There are numerous studies on the effect of LPS at the genome level bu...

  3. EXTRACTION, ANALYSIS AND BIOLOGICAL ACTIVITIES OF A FAMILY OF DITERPENES

    OpenAIRE

    Emmanuelle Villedieu; Emilie Destandau; Chantal Pichon; Sabine Berteina-Raboin

    2011-01-01

    Our study deals with a diterpenoid lactone family isolated from Andrographis paniculata. Our work was to perform extraction method, HPLC analysis and purification starting from commercial products. It led to the isolation of several pure compounds. Then, we investigated the effect of these molecules and the crude extracts towards immunostimulation.

  4. Instrumental neutron activation analysis of roots and juice of carrot

    International Nuclear Information System (INIS)

    The results are presented of the determination of the contents of Na, Br, Ca, Ba, Fe, Zn, Co, Cr, Sb and Ni. The results of the analysis are in agreement with the usually given concentrations of the elements determined in identical or similar materials. The amount of monitored elements passing from the raw materials into juices was calculated. (J.B.)

  5. EXTRACTION, ANALYSIS AND BIOLOGICAL ACTIVITIES OF A FAMILY OF DITERPENES

    Directory of Open Access Journals (Sweden)

    Emmanuelle Villedieu

    2011-09-01

    Full Text Available Our study deals with a diterpenoid lactone family isolated from Andrographis paniculata. Our work was to perform extraction method, HPLC analysis and purification starting from commercial products. It led to the isolation of several pure compounds. Then, we investigated the effect of these molecules and the crude extracts towards immunostimulation.

  6. Analysis of Flavonoids in Rhamnus davurica and Its Antiproliferative Activities

    Directory of Open Access Journals (Sweden)

    Guilin Chen

    2016-09-01

    Full Text Available Rhamnus davurica Pall. (R. davurica has been used as a traditional medicinal herb for many years in China and abroad. It has been well documented as a rich source of flavonoids with diversified structures, which in turn results in far-ranging biological activities, such as anti-inflammation, anticancer, antibacterial and antioxidant activities. In order to further correlate their anticancer potentials with the phytochemical components, the fingerprint profile of R. davurica herb from Dongbei was firstly investigated using HPLC-ESI-MS/MS. Thirty two peaks were detected and identified, 14 of which were found in R. davurica for the first time in this work. Furthermore, a total of 23 peaks were resolved as flavonoids, which are the major components found in R. davurica. Meanwhile, the antiproliferative activities against human cancer cells of HT-29 and SGC-7901 in vitro exhibited distinct inhibitory effects with IC50 values at 24.96 ± 0.74 and 89.53 ± 4.11 μg/mL, respectively. Finally, the general toxicity against L-O2 cells displayed a much higher IC50 at 229.19 ± 8.52 μg/mL, which suggested very low or no toxicity on hepatic cell viability. The current study revealed for the first time the correlations between the flavonoids of R. davurica with their antiproliferative activities, which indicated that the fingerprint profile of flavonoids and their anticancer activities could provide valuable information on the quality control for herbal medicines and their derived natural remedies from this valuable medicinal plant.

  7. Phytochemical Analysis and Biological Activities of Cola nitida Bark

    Directory of Open Access Journals (Sweden)

    Durand Dah-Nouvlessounon

    2015-01-01

    Full Text Available Kola nut is chewed in many West African cultures and is used ceremonially. The aim of this study is to investigate some biological effects of Cola nitida’s bark after phytochemical screening. The bark was collected, dried, and then powdered for the phytochemical screening and extractions. Ethanol and ethyl acetate extracts of C. nitida were used in this study. The antibacterial activity was tested on ten reference strains and 28 meat isolated Staphylococcus strains by disc diffusion method. The antifungal activity of three fungal strains was determined on the Potato-Dextrose Agar medium mixed with the appropriate extract. The antioxidant activity was determined by DPPH and ABTS methods. Our data revealed the presence of various potent phytochemicals. For the reference and meat isolated strains, the inhibitory diameter zone was from 17.5±0.7 mm (C. albicans to 9.5±0.7 mm (P. vulgaris. The MIC ranged from 0.312 mg/mL to 5.000 mg/mL and the MBC from 0.625 mg/mL to >20 mg/mL. The highest antifungal activity was observed with F. verticillioides and the lowest one with P. citrinum. The two extracts have an excellent reducing free radical activity. The killing effect of A. salina larvae was perceptible at 1.04 mg/mL. The purified extracts of Cola nitida’s bark can be used to hold meat products and also like phytomedicine.

  8. Analytical strategies for uranium determination in natural water and industrial effluents samples; Estrategias analiticas para determinacao de uranio em amostras de aguas e efluentes industriais

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Juracir Silva

    2011-07-01

    minimize reagent consumption, as well as waste generation. A linear response was observed from 5.0 to 150.0 {mu}g L{sup -1}, with a detection limit, RSD, and sampling rate estimated as 1.3 {mu}g L{sup -1} (99.7% confidence level), 0.7% (n = 20), and 40 determinations per hour, respectively. The consumption of arsenazo 111 was reduced in 1250-fold in comparison to a procedure with preconcentration in solid phase. The accuracy of the methods was confirmed by analysis of two laboratory reference materials. In addition, an effluent sample was analyzed by inductively coupled plasma mass spectrometry (ICP-MS), and the observed recovery was satisfactory. The developed methods were applied to the determination of uranium in river, well and drinking water and industrial effluent collected from uranium-producing mine in Caetite city, Brazil. The results for uranium in drinking water samples from Caetite city were below the limit of quantification of methods, except for well water (17.0 +- 0.8 mg L{sup -1}) and a river water collected near of the mine (9.6 +- 0.8 mg L{sup -1}). (author)

  9. Does birth weight influence physical activity in youth? A combined analysis of four studies using objectively measured physical activity

    DEFF Research Database (Denmark)

    Ridgway, Charlotte L; Brage, Søren; Sharp, Stephen J;

    2011-01-01

    activity and sedentary time. This study uses combined analysis of three European cohorts and one from South America (n = 4,170). Birth weight was measured or parentally reported. Height and weight were measured and used to calculate Body Mass Index (BMI). PA was objectively measured using accelerometry...

  10. Functional analysis of Ficolin-3 mediated complement activation

    DEFF Research Database (Denmark)

    Hein, Estrid; Honoré, Christian; Skjoedt, Mikkel-Ole;

    2010-01-01

    Ficolin-3 mediated complement activation that could be applicable for research and clinical use. Bovine serum albumin (BSA) was acetylated (acBSA) and chosen as a solid phase ligand for Ficolins in microtiter wells. Binding of Ficolins on acBSA was evaluated, as was functional complement activation...... assessed by C4, C3 and terminal complement complex (TCC) deposition. Serum Ficolin-3 bound to acBSA in a calcium dependent manner, while only minimal binding of Ficolin-2 and no binding of Ficolin-1 were observed. No binding to normal BSA was seen for any of the Ficolins. Serum C4, C3 and TCC deposition...... on acBSA were dependent only on Ficolin-3 in appropriate serum dilutions. Deposition of down stream complement components correlated highly significantly with the serum concentration of Ficolin-3 but not with Ficolin-2 in healthy donors. To make the assay robust for clinical use a chemical compound...

  11. Legal and technical analysis of the activities involving radiation applications

    International Nuclear Information System (INIS)

    Activities related to radiation applications have been worldwide target of studies concerning biology, medicine, sociology, psychology and law, since prediction of the possible risks and harms associated with the use of radiation, depends on probabilities not easy to quantify, mainly in the most common low-dose situations. In Brazil, legislation generated in the last forty years did not match evolution of the scientific domains related above. This way, more recent rules not rarely conflict with older regulations, without revoking them. (author)

  12. Genetic analysis of beta1 integrin "activation motifs" in mice

    DEFF Research Database (Denmark)

    Czuchra, Aleksandra; Meyer, Hannelore; Legate, Kyle R;

    2006-01-01

    /beta tails, leading to tail separation and integrin activation. We analyzed mice in which we mutated the tyrosines of the beta1 tail and the membrane-proximal aspartic acid required for the salt bridge. Tyrosine-to-alanine substitutions abolished beta1 integrin functions and led to a beta1 integrin...... and the membrane-proximal salt bridge between alpha and beta1 tails have no apparent function under physiological conditions in vivo....

  13. Analysis of NOAA particle data and correlations to seismic activity

    OpenAIRE

    C. Fidani; Battiston, R.

    2008-01-01

    A decade of NOAA-15 particle flux data offers an opportunity to test claims of correlations between seismic activity and effects on the ionosphere. Over the last two decades, potentially interesting observations in the ionosphere-magnetosphere transition region have been investigated. Specifically these consists of anomalous particle fluxes detected by several space experiments and correlated with the earthquake occurrence. These particle fluxes are characterised by anomalous short-term and s...

  14. Neutron activation analysis in the investigation of pseudomonas to mercury

    International Nuclear Information System (INIS)

    The aim of this work was to investigate the resistance to mercury in Pseudomonas. The measurements were performed by using neutron activation technique. The TRIGA MARK 1-IPE-R1 reactor was used as the irradiation facility, and the nuclide Hg202 as target element. The experimental results showed that cultures of Pseudomonas during the logarithmic growing phase, have a significant volatilization of the Hg, while during the stationary phase, they absorb and retain this metal. (author)

  15. Structural Analysis of Polysaccharide from Cladonia furcatar and Its Activities

    Institute of Scientific and Technical Information of China (English)

    CHEN Qian; LIN Xin; CAI YuJun; LI ZhiXiao

    2001-01-01

    @@ Cladonia furcatar is a member of the lichens genus Cladonia. Japanese scientific researchers [1] made a great achievement in selecting lichens as anticancer agent and polysaccharides are generally considered to be their main bioactive constituents. Recently, Iacomini et al[2] have investigated the members of the genus Cladonia, a mannose-containing polysaccharide was isolated from Cladoniafurcatar. We now report the new chemical structure of polysaccharide from Cladoniafurcatar and its activities.

  16. Abstracts from the conference on instrumental activation analysis IAA 90

    International Nuclear Information System (INIS)

    The publication contains abstracts of 19 contributions presented at the conference, all of which fall within the INIS subject scope. The coverage of the conference was very wide, from the determination of vanadium in biological material through instrumental problems of gamma spectrometry through the determination of radioactive impurities to industrial problems such as the evaluation of the effect of surface finishing of internal combustion engines surface-activated by charged particles. (P.A.)

  17. Structural Analysis of Polysaccharide from Cladonia furcatar and Its Activities

    Institute of Scientific and Technical Information of China (English)

    CHEN; Qian

    2001-01-01

    Cladonia furcatar is a member of the lichens genus Cladonia. Japanese scientific researchers [1] made a great achievement in selecting lichens as anticancer agent and polysaccharides are generally considered to be their main bioactive constituents. Recently, Iacomini et al[2] have investigated the members of the genus Cladonia, a mannose-containing polysaccharide was isolated from Cladoniafurcatar. We now report the new chemical structure of polysaccharide from Cladoniafurcatar and its activities.  ……

  18. Analysis of a Constellation Lab Cooperative Learning Activity

    Science.gov (United States)

    Gauthier, A. J.

    2001-12-01

    A cooperative learning activity was designed for use in the undergraduate laboratory course Introduction to Astronomical Observation. This group exercise enhances the student's learning of constellations and will hopefully increase retention of the material throughout the semester. It also serves as an "ice-breaker" during the first week of lab, promoting student involvement and vested interest in the course. To gain some insight into the student mind, a survey was conducted to evaluate the usefulness and overall opinion of this method. The students who completed the survey had previously been enrolled in a pre-requisite astronomy course that also required a constellation lab. In this previous course they "learned" the constellations from an instructor and a flashlight beam, studied them on their own, and then promptly took a quiz. Both methods are analyzed from an instructional designer's point of view and suggestions for future activities are presented. The preliminary results and accompanying activity will be discussed in poster and hand-out medium.

  19. Metaproteomic analysis reveals microbial metabolic activities in the deep ocean

    Science.gov (United States)

    Wang, Da-Zhi; Xie, Zhang-Xian; Zhang, Shu-Feng; Wang, Ming-Hua; Zhang, Hao; Kong, Ling-Fen; Lin, Lin

    2016-04-01

    The deep sea is the largest habitat on earth and holds many and varied microbial life forms. However, little is known about their metabolic activities in the deep ocean. Here, we characterized protein profiles of particulate (>0.22 μm) and dissolved (between 10 kDa and 0.22 μm) fractions collected from the deep South China Sea using a shotgun proteomic approach. SAR324, Alteromonadales and SAR11 were the most abundant groups, while Prasinophyte contributed most to eukaryotes and cyanophage to viruses. The dominant heterotrophic activity was evidenced by the abundant transporters (33%). Proteins participating in nitrification, methanogenesis, methyltrophy and CO2 fixation were detected. Notably, the predominance of unique cellular proteins in dissolved fraction suggested the presence of membrane structures. Moreover, the detection of translation proteins related to phytoplankton indicated that other process rather than sinking particles might be the downward export of living cells. Our study implied that novel extracellular activities and the interaction of deep water with its overlying water could be crucial to the microbial world of deep sea.

  20. In Silico Antitubercular Activity Analysis of Benzofuran and Naphthofuran Derivatives

    Directory of Open Access Journals (Sweden)

    Prashantha Karunakar

    2014-01-01

    Full Text Available For the human health, Mycobacterium tuberculosis (MTB is the deadliest enemy since decades due to its multidrug resistant strains. During latent stage of tuberculosis infection, MTB consumes nitrate as the alternate mechanism of respiration in the absence of oxygen, thus increasing its survival and virulence. NarL is a nitrate/nitrite response transcriptional regulatory protein of two-component signal transduction system which regulates nitrate reductase and formate dehydrogenase for MTB adaptation to anaerobic condition. Phosphorylation by sensor kinase (NarX is the primary mechanism behind the activation of NarL although many response regulators get activated by small molecule phospho-donors in the absence of sensor kinase. Using in silico approach, the molecular docking of benzofuran and naphthofuran derivatives and dynamic study of benzofuran derivative were performed. It was observed that compound Ethyl 5-bromo-3-ethoxycarbonylamino-1-benzofuran-2-carboxylate could be stabilized at the active site for over 10 ns of simulation. Here we suggest that derivatives of benzofuran moiety can lead to developing novel antituberculosis drugs.

  1. Activated sludge morphology characterization through an image analysis procedure

    Directory of Open Access Journals (Sweden)

    Y. G. Perez

    2006-09-01

    Full Text Available This work deals with the development of a digital image analysis procedure to characterize microbial flocs obtained in three different WWTP: a bench-scale Sequencing Batch Reactor (SBR dealing with phenol and nitrogen biological removal, a municipal treatment unit (Ilha do Governador, Rio de Janeiro, Brazil and an industrial wastewater treatment plant (Ciba - Estrada do Colégio, Rio de Janeiro, Brazil. The developed procedure permits to obtain its morphological parameters like equivalent diameter, compactness, roundness and porosity properties as well as the fractal dimension. This procedure was validated and lead to identify the major relationships between the analysed morphological parameters. A minimum of 300 flocs should be included in the image analysis and a significant influence of the sample dilution step on the mean size of the flocs was verified. The porosity parameter positively correlated with the fractal dimension of microbial aggregates indicating the that highly porous flocs are very irregular.

  2. Computers in activation analysis and gamma-ray spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Carpenter, B. S.; D' Agostino, M. D.; Yule, H. P. [eds.

    1979-01-01

    Seventy-three papers are included under the following session headings: analytical and mathematical methods for data analysis; software systems for ..gamma..-ray and x-ray spectrometry; ..gamma..-ray spectra treatment, peak evaluation; least squares; IAEA intercomparison of methods for processing spectra; computer and calculator utilization in spectrometer systems; and applications in safeguards, fuel scanning, and environmental monitoring. Separate abstracts were prepared for 72 of those papers. (DLC)

  3. Neutron activation analysis for the archaeometric study of Catamarca pottery

    International Nuclear Information System (INIS)

    Samples of pottery and raw materials from the Puna and the mesothermal valleys regions were irradiated in the RA-3 reactor for 5 hours and 22 elements (As, Ba, Ce, Co, Cr, Cs, Eu, Fe, Gd, Hf, La, Lu, Nd, Rb, Sb, Sc, Sm, Ta, Tb, Th, U and Yb) were determined by instrumental analysis, 37 days after the irradiation. The results allow drawing conclusions on the production and distribution of the pottery in the region. (authors)

  4. Mathematical analysis techniques for modeling the space network activities

    Science.gov (United States)

    Foster, Lisa M.

    1992-01-01

    The objective of the present work was to explore and identify mathematical analysis techniques, and in particular, the use of linear programming. This topic was then applied to the Tracking and Data Relay Satellite System (TDRSS) in order to understand the space network better. Finally, a small scale version of the system was modeled, variables were identified, data was gathered, and comparisons were made between actual and theoretical data.

  5. Artifact suppression and analysis of brain activities with electroencephalography signals

    OpenAIRE

    Rashed-Al-Mahfuz, Md.; Islam, Md. Rabiul; Hirose, Keikichi; Molla, Md. Khademul Islam

    2013-01-01

    Brain-computer interface is a communication system that connects the brain with computer (or other devices) but is not dependent on the normal output of the brain (i.e., peripheral nerve and muscle). Electro-oculogram is a dominant artifact which has a significant negative influence on further analysis of real electroencephalography data. This paper presented a data adaptive technique for artifact suppression and brain wave extraction from electroencephalography signals to detect regional bra...

  6. TENDENCY OF IMPROVEMENT ANALYSIS OF VENTURE ACTIVITY FOR MANAGEMENT DECISIONS

    Directory of Open Access Journals (Sweden)

    G.Yu. Iakovetс

    2015-03-01

    Full Text Available The questions concerning the definition of current trends and prospects of venture financing new innovative enterprises as one of the most effective and alternative, but with a high degree of risk financing sources of the entity. The features of venture financing that is different from other sources of business financing, as well as income from investments of venture capital can greatly exceed the volume of investments, but at the same time such financing risks are significant, so it all makes it necessary to build an effective system of venture capital investments in the workplace. In the course of the study also revealed problems of analysis and minimization of risks in the performance of venture financing of innovative enterprises. Defining characteristics analysis and risk assessment of venture financing helps to find ways to minimize and systematization, avoidance and prevention of risks in the performance of venture capital. The study also identified the major areas of improvement analysis of venture capital for management decisions.

  7. Study on bioavailability of zinc for children's diet by using activable isotopic tracer 70Zn and neutron activation analysis techniques

    International Nuclear Information System (INIS)

    Bioavailability of zinc for three groups (low amount of diet zinc, balance amount of diet zinc and high amount of diet zinc) of children's diet is studied by using activable isotopic tracer 70Zn and neutron activation analysis techniques. The results indicate that the fractional absorption of zinc from balance diet zinc group is the highest, up to 33.9%. A procedure of pre-irradiation concentration zinc for fecal samples using anion exchanger is developed, and the enriched 70Zn with isotopic abundance of 18.3% is used for tracer. The mass ratios between 70Zn and 68Zn or 64Zn and their contents between natural zinc and enriched zinc are used to calculate the bioavailability of zinc. Instrumental neutron activation analysis of 64Zn of each original fecal samples and pre-irradiation concentrated zinc samples are used to normalize the chemical yield in order to reduce the uncertainty during the chemical separation procedure

  8. Structural interpretation of activity cliffs revealed by systematic analysis of structure-activity relationships in analog series.

    Science.gov (United States)

    Sisay, Mihiret T; Peltason, Lisa; Bajorath, Jürgen

    2009-10-01

    Discontinuity in structure-activity relationships (SARs) is caused by so-called activity cliffs and represents one of the major caveats in SAR modeling and lead optimization. At activity cliffs, small structural modifications of compounds lead to substantial differences in potency that are essentially unpredictable using quantitative structure-activity relationship (QSAR) methods. In order to better understand SAR discontinuity at the molecular level of detail, we have analyzed different compound series in combinatorial analog graphs and determined substitution patterns that introduce activity cliffs of varying magnitude. So identified SAR determinants were then analyzed on the basis of complex crystal structures to enable a structural interpretation of SAR discontinuity and underlying activity cliffs. In some instances, SAR discontinuity detected within analog series could be well rationalized on the basis of structural data, whereas in others a structural explanation was not possible. This reflects the intrinsic complexity of small molecule SARs and suggests that the analysis of short-range receptor-ligand interactions seen in X-ray structures is insufficient to comprehensively account for SAR discontinuity. However, in other cases, SAR information extracted from ligands was incomplete but could be deduced taking X-ray data into account. Thus, taken together, these findings illustrate the complementarity of ligand-based SAR analysis and structural information. PMID:19761254

  9. Seismic Activity in the Gulf of Mexico: a Preliminary Analysis

    Science.gov (United States)

    Franco, S. I.; Canet, C.; Iglesias, A.; Valdes-Gonzales, C. M.

    2013-05-01

    The southwestern corner of Gulf of Mexico (around the northern Isthmus of Tehuantepec) is exposed to an intense deep (> 100 km) seismic activity caused by the subduction of the Cocos plate. Aside from this, the gulf has been considered as a zone of low or no-seismicity. However, a sparse shallow seismic activity is observed across the Gulf of Mexico; some of these earthquakes have been strongly felt (e.g. 23/05/2007 and 10/09/2006), and the Jaltipan, 1959 earthquake caused fatalities and severe destruction in central and southern Veracruz. In this work we analyze 5 relevant earthquakes that occurred since 2001. At the central Gulf of Mexico focal mechanisms show inverse faults oriented approximately NW-SE with dip near 45 degrees, suggesting a link to sediment loading and/or to salt tectonics. On the other hand, in the southwestern corner of the gulf we analyzed some clear examples of strike-slip faults and activity probably related to the Veracruz Fault. One anomalous earthquake, recorded in 2007 in the western margin of the gulf, shows a strike-slip mechanism indicating a transform regime probably related with the East Mexican Fault. The recent improvement of the Mexican Seismological broadband network have allowed to record small earthquakes distributed in and around the Gulf of Mexico. Although the intermediate and large earthquakes in the region are infrequent, the historic evidence indicates that the magnitudes could reach Mw~6.4. This fact could be taken in consideration to reassess the seismic hazard for oil and industrial infrastructure in the region.

  10. Activation analysis for different structural alloys considered for ITER

    International Nuclear Information System (INIS)

    Activation calculations have been made for the austentic steel 316SS, the ferritic alloy HT-9, the titanium alloy Ti6A14V, and the vanadium alloy V5Cr5Ti in a liquid metal (Na) design suggested recently for ITER. The calculations show that the vanadium alloy has the minimum short and long-term radioactivity and BHP. It also has the minimum decay heat at all the time. The titanium alloy has less radioactivity than the austenitic and this ferritic alloys. However, the decay heat of this alloy could exceed that of the conventional alloys

  11. BUSINESS ANALYSIS OF THE ACTIVITY SC COMPLEX ASTORIA SRL

    Directory of Open Access Journals (Sweden)

    CLAUDIU VALENTIN NITU

    2010-01-01

    Full Text Available A firm is competitive if it can produce high quality products and services and lowercosts than its competitors and internationally. Ability to compete is to do better than firms in thesame industry in terms of sales, market share and profitability, capacity to achieve its strategicconduct, defined as the set of actions undertaken to influence the market, finally leading toincreased profits. The European Union said that the product or service quality at a competitiveprice. It is associated with all activities related to quality management, quality assurance andquality control, certification and accreditation, standardization, etc.

  12. An empirical analysis of the training activities of firms

    Directory of Open Access Journals (Sweden)

    Edit Hadhazi Barizsne

    2013-07-01

    Full Text Available The purpose of the current study is to search for a link between the characteristics of firms’ training activities and the characteristics of the organisations themselves. The validity of our hypothesis is examined on the basis of structured interviews. On the basis of the data we can state that the growth in the increase in the number of employees and the innovative nature of technology used have been accompanied by a parallel growth in the training behaviour of firms. In our study we attempt to study in detail the influence that the stage the firm is at on its life cycle curve has on the training provided to employees.

  13. Gender Analysis of Children’s Activities in Pakistan

    OpenAIRE

    Rana Ejaz Ali Khan

    2008-01-01

    This paper estimates gender differences in children’s time allocation among four ordered options. It analyses the sample of boys and girls separately through a series of probit models using primary data. We compare the socio-economic determinants of boys’ and girls’ activities. The results suggest that boys are more likely to go to school as compared to girls with the increase in their age. The provision of schooling as an instrument to decrease child labour and home-care would affect boys mo...

  14. Culture phenomenon analysis on the forest tour activity of China

    Institute of Scientific and Technical Information of China (English)

    Jiang Minjin

    2006-01-01

    This paper analyzes culture and forest culture, the intension of culture and forest culture, combines the understanding of the main cultural factor with the forest tour activity of China, analyzes the compatible phenomenon of Chinese forest culture and traditional culture, and explores culture of forest tourist site containing the meaning in forest tour. The author thinks the tour of forest culture which will be the important component of forest tour in forest culture,This paper puts forward simple questions existing in exploitation and advantage of forest tour culture, and proposes some countermeasures.

  15. Functional analysis of Ficolin-3 mediated complement activation

    DEFF Research Database (Denmark)

    Hein, Estrid; Honoré, Christian Le Fèvre; Skjoedt, Mikkel-Ole;

    2010-01-01

    assessed by C4, C3 and terminal complement complex (TCC) deposition. Serum Ficolin-3 bound to acBSA in a calcium dependent manner, while only minimal binding of Ficolin-2 and no binding of Ficolin-1 were observed. No binding to normal BSA was seen for any of the Ficolins. Serum C4, C3 and TCC deposition...... was applied to the samples that inhibited interference from the classical pathway due to the presence of anti-BSA antibodies in some sera. We describe a novel functional method for measuring complement activation mediated by Ficolin-3 in human serum up to the formation of TCC. The assay provides...

  16. Circadian patterns of Wikipedia editorial activity: a demographic analysis.

    Directory of Open Access Journals (Sweden)

    Taha Yasseri

    Full Text Available Wikipedia (WP as a collaborative, dynamical system of humans is an appropriate subject of social studies. Each single action of the members of this society, i.e., editors, is well recorded and accessible. Using the cumulative data of 34 Wikipedias in different languages, we try to characterize and find the universalities and differences in temporal activity patterns of editors. Based on this data, we estimate the geographical distribution of editors for each WP in the globe. Furthermore we also clarify the differences among different groups of WPs, which originate in the variance of cultural and social features of the communities of editors.

  17. Circadian patterns of Wikipedia editorial activity: A demographic analysis

    CERN Document Server

    Yasseri, Taha; Kerétsz, János

    2011-01-01

    Wikipedia (WP) as a collaborative, dynamical system of humans is an appropriate subject of social studies. Each single action of the members of this society, i.e. editors, is well recorded and accessible. Using the cumulative data of 34 Wikipedias in different languages, we try to characterize and find the universalities and differences in temporal activity patterns of editors. Based on this data, we estimate the geographical distribution of editors for each WP in the globe. Furthermore we also clarify the differences among different groups of WPs, which originate in the variance of cultural and social features of the communities of editors.

  18. Charismatic leadership and entrepreneurial activity: An empirical analysis

    Directory of Open Access Journals (Sweden)

    Stefan van Hemmen

    2013-10-01

    Full Text Available Entrepreneurship literature frequently identifies entrepreneurs as possessing a charismatic personality. Charisma is broadly defined as a combination of the talent to foresee market opportunities and the ability to motivate other people in the materialization of these opportunities. Business organizations also provide the context for developing skills and knowledge, which is particularly valuable for potential entrepreneurs who identify business opportunities. Using a sample of 41 countries, we show that higher rates of charismatic leadership at the country level are positively associated with entrepreneurial activity. This outcome suggests that both business-oriented and educational organizations that promote charismatic leadership play a significant role in the development of entrepreneurial incubators.

  19. Tensor analysis methods for activity characterization in spatiotemporal data

    Energy Technology Data Exchange (ETDEWEB)

    Haass, Michael Joseph; Van Benthem, Mark Hilary; Ochoa, Edward M

    2014-03-01

    Tensor (multiway array) factorization and decomposition offers unique advantages for activity characterization in spatio-temporal datasets because these methods are compatible with sparse matrices and maintain multiway structure that is otherwise lost in collapsing for regular matrix factorization. This report describes our research as part of the PANTHER LDRD Grand Challenge to develop a foundational basis of mathematical techniques and visualizations that enable unsophisticated users (e.g. users who are not steeped in the mathematical details of matrix algebra and mulitway computations) to discover hidden patterns in large spatiotemporal data sets.

  20. Neutron activation analysis of final molasses from cuban sugar industry

    International Nuclear Information System (INIS)

    Thermal and epithermal non-destructive activation analyses have been performed on samples of final molasses from 14 different sugar factories , covering the most important regions in Cuba. From the first measurement after irradiation at the Triga Mark reactor (VTT), the concentration of more than 15 elements is reported. The almost constant elemental composition shows that they can be used equally for different purposes as animal foodstuff and for the manufacture of biotechnological products. This work is part of a research project developed in order to establish a complete characterization of Cuban sugar molasses. (author). 7 refs., 2 tabs

  1. Statistical analysis on activation and photo-bleaching of step-wise multi-photon activation fluorescence of melanin

    Science.gov (United States)

    Gu, Zetong; Lai, Zhenhua; Zhang, Xi; Yin, Jihao; DiMarzio, Charles A.

    2015-03-01

    Melanin is regarded as the most enigmatic pigments/biopolymers found in most organisms. We have shown previously that melanin goes through a step-wise multi-photon absorption process after the fluorescence has been activated with high laser intensity. No melanin step-wise multi-photon activation fluorescence (SMPAF) can be obtained without the activation process. The step-wise multi-photon activation fluorescence has been observed to require less laser power than what would be expected from a non-linear optical process. In this paper, we examined the power dependence of the activation process of melanin SMPAF at 830nm and 920nm wavelengths. We have conducted research using varying the laser power to activate the melanin in a point-scanning mode for multi-photon microscopy. We recorded the fluorescence signals and position. A sequence of experiments indicates the relationship of activation to power, energy and time so that we can optimize the power level. Also we explored regional analysis of melanin to study the spatial relationship in SMPAF and define three types of regions which exhibit differences in the activation process.

  2. Recent Activities of Tsukuba Correlator/Analysis Center

    Science.gov (United States)

    Kokado, K.; Kurihara, S.; Kawabata, R.; Nozawa, K.

    2012-12-01

    The Geospatial Information Authority of Japan (GSI) has been a member of IVS and taken charge of a Network Station and an IVS Correlator since 1998. In addition, GSI became an IVS Operational Analysis Center in January 2010.The Tsukuba Correlator takes charge of correlation work for approximately 100 IVS-INT02 (INT2) sessions and 10 Japanese domestic sessions every year. In 2011, the number of INT2 sessions dramatically increased, because INT2 sessions were observed twice a day during the weekend from April 2011 to January 2012 due to the change in position of the Tsukuba 32-m antenna by the 2011 earthquake off the Pacific coast of Tohoku. The role of the Tsukuba VLBI Analysis Center is to produce ultra-rapid dUT1 measurements, sessions with the goal of obtaining a dUT1 solution within 30 minutes after the end of the observation session. The data processing system at the Tsukuba Correlator and Analysis Center was dramatically improved to achieve rapid data processing. It enabled us to shorten the data processing time to one-sixth and to process the IVS VLBI data in near real-time. In 2011, we processed the ultra-rapid dUT1 measurements with the Onsala or Wettzell stations from INT2 sessions or IVS 24-hour sessions, such as R1, RD or T2 sessions. The most successful sessions for ultra-rapid dUT1 measurement was the CONT11 sessions which were a campaign of 15 days of continuous VLBI sessions. During these sessions, we succeeded in estimating continuous dUT1 solutions in near real-time for 15 days.

  3. Analysis of natural neutron flux in a seismically active zone

    Directory of Open Access Journals (Sweden)

    V. F. Ostapenko

    2003-01-01

    Full Text Available In a seismically active zone in the near Almaty area (Kazakhstan since 1996 observations of variations of a natural neutron flux have been conducted. Sometimes the neutron flux rises sharply within the one-hour interval in comparison with the background. It occurs on the eve of activation of seismic processes. Increase of the neutron flux level had taken place from 1 h to 10 days prior to earthquakes. It is also indicated a tendency of growth of the anomaly level in accordance with the growth of energetic class of the subsequent earthquake. A character of connection between the neutron flux and earthquakes is still not clear. It is proposed that the neutron flux anomalies caused by variations of cosmic radiation intensity under action of fluxes of solar material, which is burst into interplanetary space (solar wind during solar flares. Energy of the solar wind transferred to Earth puts into action a trigger mechanism of the process of initiation of earthquakes at those places where conditions have already been prepared for them. The neutron flux anomalies can be used as substantial additional information for classical geophysical methods of short-term earthquake prediction.

  4. A quantitative analysis of contractility in active cytoskeletal protein networks.

    Science.gov (United States)

    Bendix, Poul M; Koenderink, Gijsje H; Cuvelier, Damien; Dogic, Zvonimir; Koeleman, Bernard N; Brieher, William M; Field, Christine M; Mahadevan, L; Weitz, David A

    2008-04-15

    Cells actively produce contractile forces for a variety of processes including cytokinesis and motility. Contractility is known to rely on myosin II motors which convert chemical energy from ATP hydrolysis into forces on actin filaments. However, the basic physical principles of cell contractility remain poorly understood. We reconstitute contractility in a simplified model system of purified F-actin, muscle myosin II motors, and alpha-actinin cross-linkers. We show that contractility occurs above a threshold motor concentration and within a window of cross-linker concentrations. We also quantify the pore size of the bundled networks and find contractility to occur at a critical distance between the bundles. We propose a simple mechanism of contraction based on myosin filaments pulling neighboring bundles together into an aggregated structure. Observations of this reconstituted system in both bulk and low-dimensional geometries show that the contracting gels pull on and deform their surface with a contractile force of approximately 1 microN, or approximately 100 pN per F-actin bundle. Cytoplasmic extracts contracting in identical environments show a similar behavior and dependence on myosin as the reconstituted system. Our results suggest that cellular contractility can be sensitively regulated by tuning the (local) activity of molecular motors and the cross-linker density and binding affinity. PMID:18192374

  5. Phytochemical analysis and gastroprotective activity of an olive leaf extract

    Directory of Open Access Journals (Sweden)

    IVANA ARSIĆ

    2009-04-01

    Full Text Available Some medicinal features of olive leaf have been known for centuries. It has been traditionally used as an antimicrobial and to prevent and treat diabetes mellitus and heart disease. Whether olive leaf, a natural antioxidant, influences the gastric defense mechanism and exhibits gastroprotection against experimentally-induced gastric lesions remains unknown. In this study, the content of total phenols, total flavonoids and tannins in olive leaf extract (OLE were determined. Seven phenolic compounds were identified and quantified (oleuropein, caffeic acid, luteolin, luteolin-7-O-glucoside, apigenin-7-O-glucoside, quercetin, and chryseriol. Furthermore, the protective activity of the OLE in gastric mucosal injury induced by a corrosive concentration of ethanol was investigated. In relation to the control group, pretreatment with OLE (40, 80 and 120 mg kg-1 significantly (p < 0.001 attenuated the gastric lesions induced by absolute ethanol. The protective effect of the OLE was similar to that obtained with a reference drug, ranitidine. The results obtained indicate that OLE possesses significant gastroprotective activity, and that the presence of compounds with antioxidative properties would probably explain this effect.

  6. Neutron activation analysis: nuclear interference from iron in manganese

    International Nuclear Information System (INIS)

    In the present work, the contribution of iron was verified in the analysis of manganese through the reaction of interference by fast neutron. The irradiation of the samples was accomplished in the channel IC-40 of the rotary rack of the TRIGA MARK I IPR-R1 research reactor, located at Nuclear Technology Development Centre/Brazilian Commission for Nuclear Energy, CDTN/CNEN. In this irradiation device, the average thermal neutron flux is 6.69 x 1011 neutron cm-2 s-1 and fast neutron flux is 7.37 x 1010 neutron cm-2 s-1. Manganese was determined through 56Mn induced by thermal neutron flux according to the reaction 55Mn(n, γ)56Mn. In the analysis of manganese, the contribution of iron was investigated according to the reaction of interference 56Fe(n, p)56Mn produced by the fast neutron. It was verified that the contribution of 1 g of iron is 20 μg of manganese. (author)

  7. CORRELATIVE ANALYSIS OF COSMIC RAY INTENSITY AND SOLAR ACTIVITY PARAMETERS

    Directory of Open Access Journals (Sweden)

    M. ROY

    2014-02-01

    Full Text Available Incoming cosmic ray shows significant intensity modulation in association with different solar geo parameters during their passage through heliosphere. Cosmic ray intensity is found anticorrelated with solar activity parameters. Using pressure corrected data of Mcmurdo neutron monitor, modulation of cosmic ray is analyzed covering solar cycles 21, 22, 23 and 24 (from 1976 to 2013. Negative and high correlations are obtained with some time lag for most of the solar parameters. Difference in shapes of hysteresis curves CRI~SSN, CRI~SRF. CRI~CI and CRI~FI for odd and even cycles pointed out that different mechanisms convection and diffusion are the dominating factors to drift cosmic ray particles.

  8. Clinical applications of in vivo neutron-activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Cohn, S.H.

    1982-01-01

    In vivo neutron activation has opened a new era of both clinical diagnosis and therapy evaluation, and investigation into and modelling of body composition. The techniques are new, but it is already clear that considerable strides can be made in increasing accuracy and precision, increasing the number of elements susceptible to measurement, enhancing uniformity, and reducing the dose required for the measurement. The work presently underway will yield significant data on a variety of environmental contaminants such as Cd. Compositional studies are determining the level of vital constituents such as nitrogen and potassium in both normal subjects and in patients with a variety of metabolic disorders. Therapeutic programs can be assessed while in progress.

  9. In-vivo neutron activation analysis: principles and clinical applications

    Energy Technology Data Exchange (ETDEWEB)

    Cohn, S.H.

    1982-01-01

    In vivo neutron activation has opened a new era of both clinical diagnosis and therapy evaluation, and investigation into and modelling of body composition. The techniques are new, but it is already clear that considerable strides can be made in increasing accuracy and precision, increasing the number of elements susceptible to measurement, enhancing uniformity, and reducing the dose required for the measurement. The work presently underway will yield significant data on a variety of environmental contaminants such as Cd. Compositional studies are determining the level of vital constituents such as nitrogen and potassium in both normal subjects and in patients with a variety of metabolic disorders. Therapeutic programs can be assessed while in progress. It seems likely that by the end of this century there will have been significant progress with this research tool, and exciting insights obtained into the nature and dynamics of human body composition.

  10. Neutron activation analysis of stable elements in marine algae

    International Nuclear Information System (INIS)

    The nuclear industry has grown during the last decades and continuing growth is predicted. Although considerable efforts are being made to minimize the release of the increasing amounts of radioactive wastes into marine environment, it is evident that the potential for radioactive contamination will continue to grow. The purposes of marine environment monitoring around nuclear facilities are to verify that they are functioning as it was designed and to detect the unplanned releases of radioactive contaminants. To provide a sufficient assessment with biological indicators of 60Co and 137Cs, most significant radionuclides in waste effluents released with nuclear power station, the concentration of stable elements in the Sargassum and other algae were surveyed with thermal neutron activation method. The results were followed: 1) The concentration of Mn, As, Zn, and Co were seem to be higher in the sargassum than in other algae. 2) The concentration of Co and Cs were higher in S. thunbergit than in other Sargassum. (author)

  11. Clinical applications of in vivo neutron-activation analysis

    International Nuclear Information System (INIS)

    In vivo neutron activation has opened a new era of both clinical diagnosis and therapy evaluation, and investigation into and modelling of body composition. The techniques are new, but it is already clear that considerable strides can be made in increasing accuracy and precision, increasing the number of elements susceptible to measurement, enhancing uniformity, and reducing the dose required for the measurement. The work presently underway will yield significant data on a variety of environmental contaminants such as Cd. Compositional studies are determining the level of vital constituents such as nitrogen and potassium in both normal subjects and in patients with a variety of metabolic disorders. Therapeutic programs can be assessed while in progress

  12. Numerical modeling and analysis of the active magnetic regenerator

    DEFF Research Database (Denmark)

    Nielsen, Kaspar Kirstein

    In this thesis the active magnetic regenerator (AMR) is analyzed using various numerical tools and experimental devices. A 2-dimensional transient numerical model of the AMR is developed and implemented and it is used to investigate the in uence of a range of parameters on the performance...... expressed as temperature span versus cooling power is mapped as a function of the central parameters. Since regenerators built of several magnetic materials distinguished by their respective magnetic transition temperatures are reported to perform better than single-material AMRs this concept has been...... investigated using the numerical AMR model. The results show indeed that the performance may be enhanced signicantly and it may thus be concluded that the performance of the AMR is dependent on a vast number of parameters (material composition, magnetic eld source, regenerator geometry, regenerator eciency...

  13. Performance analysis of a rotary active magnetic refrigerator

    DEFF Research Database (Denmark)

    Lozano, Jaime; Engelbrecht, Kurt; Bahl, Christian R.H.;

    2013-01-01

    Performance results for a novel rotary active magnetic regenerator (AMR) and detailed numerical model of it are presented. The experimental device consists of 24 regenerators packed with gadolinium (Gd) spheres rotating inside a four-pole permanent magnet with magnetic field of 1.24T. A parametric...... study of the temperature span, cooling power, coefficient of performance (COP) and efficiency of the system was carried out over a range of different hot reservoir temperatures, volumetric flow rates and cooling powers. Detailed modeling of the AMR using a 1D model was performed and compared......-equivalent cooling power (ExQ), and the overall second law efficiency, η2nd. Losses mapping indicated that friction and thermal leakage to the ambient are the most important contributors to the reduction of the system performance. Based on modeling results, improvements on the flow distributor design and reduction...

  14. Human hair identification by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Nondestructive neutron activation technique was used to analyze 17 elements (Al, As, Au, Ba, Br, Cl, Cu, Hg, I, K, Mg, Mn, Na, Sb, Sr, V and Zn) in 75 human hair samples in 5 different locations, respectively, from 15 glassware workers. The analytical results were treated further statistically to find the elemental distribution among different human hairs and to identify the individual's hair. The identifying probability of one's hair by the comparison of elemental concentrations is found to be 104-106 times higher from the same person's than from any other person's. The standard deviation of the elemental concentrations of samples taken from 5 different locations of one person is about 5 time smaller than the standard deviation for individual's hair. These data support the possibility of using NAA of hair for human hair identification. (author)

  15. Online Nonparametric Bayesian Activity Mining and Analysis From Surveillance Video.

    Science.gov (United States)

    Bastani, Vahid; Marcenaro, Lucio; Regazzoni, Carlo S

    2016-05-01

    A method for online incremental mining of activity patterns from the surveillance video stream is presented in this paper. The framework consists of a learning block in which Dirichlet process mixture model is employed for the incremental clustering of trajectories. Stochastic trajectory pattern models are formed using the Gaussian process regression of the corresponding flow functions. Moreover, a sequential Monte Carlo method based on Rao-Blackwellized particle filter is proposed for tracking and online classification as well as the detection of abnormality during the observation of an object. Experimental results on real surveillance video data are provided to show the performance of the proposed algorithm in different tasks of trajectory clustering, classification, and abnormality detection. PMID:26978823

  16. Applied research and development of neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Moon, Jong Hwa; Kim, Sun Ha; Bak, Sung Ryel; Park, Yong Chul; Kim, Young Ki; Chung, Hwan Sung; Park, Kwang Won; Kang, Sang Hun

    2000-05-01

    This report is written for results of research and development as follows : improvement of neutron irradiation facilities, counting system and development of automation system and capsules for NAA in HANARO ; improvement of analytical procedures and establishment of analytical quality control and assurance system; applied research and development of environment, industry and human health and its standardization. For identification and standardization of analytical method, environmental biological samples and polymer are analyzed and uncertainity of measurement are estimated. Also data intercomparison and proficency test were performed. Using airborne particulate matter chosen as a environmental indicators, trace elemental concentrations of sample collected at urban and rural site are determined and then the calculation of statistics and the factor analysis are carried out for investigation of emission source. International cooperation research project was carried out for utilization of nuclear techniques.

  17. Application of thermal analysis techniques in activated carbon production

    Science.gov (United States)

    Donnals, G.L.; DeBarr, J.A.; Rostam-Abadi, M.; Lizzio, A.A.; Brady, T.A.

    1996-01-01

    Thermal analysis techniques have been used at the ISGS as an aid in the development and characterization of carbon adsorbents. Promising adsorbents from fly ash, tires, and Illinois coals have been produced for various applications. Process conditions determined in the preparation of gram quantities of carbons were used as guides in the preparation of larger samples. TG techniques developed to characterize the carbon adsorbents included the measurement of the kinetics of SO2 adsorption, the performance of rapid proximate analyses, and the determination of equilibrium methane adsorption capacities. Thermal regeneration of carbons was assessed by TG to predict the life cycle of carbon adsorbents in different applications. TPD was used to determine the nature of surface functional groups and their effect on a carbon's adsorption properties.

  18. Application of neutron activation analysis to the study of diabetes

    International Nuclear Information System (INIS)

    INAA was a very convenient method for hair analysis. The preliminary results of our clinical study of elemental composition of hair from patients with insulin - requiring diabetes have proved again that scalp hair is a significant health status indicator. We found statistically significant changes of the concentrations of some essential and non-essential elements in the hair of diabetic patients, which may be related with the metabolic disorders specific for the disease. Future studies will need to provide more information on the possible role of some elements in diabetes. Also we intend to broaden the scope of the investigation to many elements and to other types of diabetes, in order to validate the results and the conclusions. (author)

  19. Muscle networks: Connectivity analysis of EMG activity during postural control

    Science.gov (United States)

    Boonstra, Tjeerd W.; Danna-Dos-Santos, Alessander; Xie, Hong-Bo; Roerdink, Melvyn; Stins, John F.; Breakspear, Michael

    2015-12-01

    Understanding the mechanisms that reduce the many degrees of freedom in the musculoskeletal system remains an outstanding challenge. Muscle synergies reduce the dimensionality and hence simplify the control problem. How this is achieved is not yet known. Here we use network theory to assess the coordination between multiple muscles and to elucidate the neural implementation of muscle synergies. We performed connectivity analysis of surface EMG from ten leg muscles to extract the muscle networks while human participants were standing upright in four different conditions. We observed widespread connectivity between muscles at multiple distinct frequency bands. The network topology differed significantly between frequencies and between conditions. These findings demonstrate how muscle networks can be used to investigate the neural circuitry of motor coordination. The presence of disparate muscle networks across frequencies suggests that the neuromuscular system is organized into a multiplex network allowing for parallel and hierarchical control structures.

  20. Neutron activation analysis of Urartian pottery from eastern Anatolia

    International Nuclear Information System (INIS)

    A total of 275 pottery and clay samples from Urartian period sites in eastern Anatolia were analyzed by INAA. The pottery sample originates primarily from the fortress and Outer Town at Ayanis and also includes samples from nearby sites in the Lake Van basin. A small sample of pottery from Bastam, a contemporary Urartian fortress in northwest Iran, and Kef Kalesi, a site on the north shore of Lake Van were also analyzed. Ten distinct compositional groups were identified during the course of the analysis suggesting that pottery was produced at multiple locations throughout the Urartian kingdom. In addition to identifying multiple production locales, the long-distance movement of pottery from the sites of Kef Kalesi and Bastam into the Van Basin and the movement of pottery from Ayanis to Bastam were documented. (author)

  1. Computerized Stokes analysis of optically active polymer films

    CERN Document Server

    Georgiev, Georgi

    2010-01-01

    Optics labs are an integral part of the advanced curriculum for physics majors. Students majoring in other disciplines, like chemistry, biology or engineering rarely have the opportunity to learn about the most recent optical techniques and mathematical representation used in today’s science and industry optics. Stokes analysis of polarization of light is one of those methods that are increasingly necessary but are seldom taught outside advanced physics or optics classes that are limited to physics majors. On the other hand biology and chemistry majors already use matrix and polarization techniques in the labs for their specialty, which makes the transition to matrix calculations seamless. Since most of the students in those majors postpone their enrollment in physics, most of the registered in those classes are juniors and seniors, enabling them to handle those techniques. We chose to study polymer samples to aid students majoring in other disciplines, especially chemistry and engineering, with understa...

  2. Systems Studies Department FY 78 activity report. Volume 2. Systems analysis. [Sandia Laboratories, Livermore

    Energy Technology Data Exchange (ETDEWEB)

    Gold, T.S.

    1979-02-01

    The Systems Studies Department at Sandia Laboratories Livermore (SLL) has two primary responsibilities: to provide computational and mathematical services and to perform systems analysis studies. This document (Volume 2) describes the FY Systems Analysis highlights. The description is an unclassified overview of activities and is not complete or exhaustive. The objective of the systems analysis activities is to evaluate the relative value of alternative concepts and systems. SLL systems analysis activities reflect Sandia Laboratory programs and in 1978 consisted of study efforts in three areas: national security: evaluations of strategic, theater, and navy nuclear weapons issues; energy technology: particularly in support of Sandia's solar thermal programs; and nuclear fuel cycle physical security: a special project conducted for the Nuclear Regulatory Commission. Highlights of these activities are described in the following sections. 7 figures. (RWR)

  3. Determination of cadmium in water samples by co-precipitation and neutron activation analysis

    International Nuclear Information System (INIS)

    For the determination of cadmium in sea water, a neutron activation analysis method involving a preconcentration step has been developed. Preconcentration is achieved by co-precipitation of cadmium dibenzyldithiocarbamate with phenolphthalein. The precipitate is collected on 0.45 μm membrane filters and cadmium is determined by instrumental neutron activation analysis. A 115mCd radio tracer was used to establish optimum conditions and to evaluate the chemical yield. (author) 14 refs.; 1 fig. ; 2 tabs

  4. Software for neutron activation analysis at reactor IBR-2, FLNP, JINR

    CERN Document Server

    Zlokazov, V B

    2004-01-01

    A Delphi program suite, developed for processing gamma-spectra of induced activity of nuclei, obtained from the neutron activation measurements at the reactor IBR-2, FLNF, JINR, is reported. This suite contains components, intended for carrying out all the operations of the analysis cycle, starling with a data acquisition program for gamma -spectrometers Gamma (written in C++ Builder) and including Delphi programs for steps of the analysis. (6 refs).

  5. Multielemental analysis of mineral nutrients in Nagpur Santra (Citrus reticulata Blanco) leaves by thermal neutron activation analysis

    International Nuclear Information System (INIS)

    Mn, Zn, Cu, Na, K, Fe and P have been determined in the Nagpur Santra (Citrus reticulata Blanco) leaves by thermal neutron activation analysis. The irradiated sample was dissolved in aqua regia in the presence of carriers. The β and/or γ activities of the purified elements were measured after radiochemical separations involving solvent extraction and precipitation. The values obtained for the elements are comparable to those reported in literature for Indian citrus leaves. (author)

  6. Use of research reactors for neutron activation analysis. Report of an advisory group meeting

    International Nuclear Information System (INIS)

    Neutron activation analysis (NAA) is an analytical technique based on the measurement of characteristic radiation from radionuclides formed directly or indirectly by neutron irradiation of the material of interest. In the last three decades, neutron activation analysis has been found to be extremely useful in the determination of trace and minor elements in many disciplines. These include environmental analysis applications, nutritional and health related studies, geological as well as material sciences. The most suitable source of neutrons for NAA is a research reactor. There are several application fields in which NAA has a superior position compared to other analytical methods, and there are good prospects in developing countries for long term growth. Therefore, the IAEA is making concerted efforts to promote neutron activation analysis and at the same time to assist developing Member States in better utilization of their research reactors. The purpose of the meeting was to discuss the benefits and the role of NAA in applications and research areas that may contribute towards improving utilization of research reactors. The participants focused on five specific topics: (1) Current trends in NAA; (2) The role of NAA compared to other methods of chemical analysis; (3) How to increase the number of NAA users through interaction with industries, research institutes, universities and medical institutions; (4) How to reduce costs and to maintain quality and reliability; (5) NAA using low power research reactors. Neutron activation analysis in its various forms is still active and there are good prospects in developing countries for long-term growth. This can be achieved by a more effective use of existing irradiation and counting facilities, a better end-user focus, and perhaps marginal improvements in equipment and techniques. Therefore, it is recommended that the Member States provide financial and other assistance to enhance the effectiveness of their laboratories

  7. Analysis of Research in Physical Activities of Slovenian Basic School Children in Recent Years

    Directory of Open Access Journals (Sweden)

    Klavdija Strniša

    2015-06-01

    Full Text Available Nowadays, physical activity is an extremely important segment of a healthy lifestyle not only for children but also for adults. Technological advances allow us to reach our goals with much less physical effort than was required of the individual in the past. Additionally, the fast pace of life and an increasingly sedentary lifestyle also contribute to reduced physical activity among the population. Analysis of published scientific articles in the field of physical activity among basic school students includes 15 research studies. They were included regardless of the origin of the publication and citation frequency. It can be seen that the most common segment of research in children’s physical activity is the gender perspective. Researchers are further interested in the effects of age, educational success, BMI, place of residence, frequency and time spent in physical activity, education and physical activity of parents, as well as the level of organization (organized / unorganized activity. Therefore it can be concluded that children’s physical activities are influenced by external and internal factors. Analysis of published research has shown that physical activity depends upon many internal and external factors. A higher level of physical activity is often detected with boys and children in urban areas, compared to rural ones. Physically active parents have physically more active children. A higher proportion of interviewed basic school students was found to participate in organized forms of exercise in comparison to the unorganized ones.

  8. Activation analysis of copper in foodstuffs after their partial destruction

    International Nuclear Information System (INIS)

    The samples analyzed (0.1 to 0.8 g) and the standards were irradiated for 24 hours with thermal neutrons (2x1012 n/cm2s), the ampoules were opened 2 hours after irradiation, 1 mg of non-active Cu carrier was added and the samples were mineralized for about 15 to 20 mins at 600 degC. The ash was leached with 5 ml of hot 10% HCl and following neutralization with ammonia and dilution with 20 ml of 10-3 M HCl, 10 ml of an α-benzoineoxime (2 g), pyridine (100 ml) and chloroform (900 ml) mixture was extracted at pH>=2. The extract was used for measuring radioactivity (6 hours after irradiation) and for spectrophotometric determination of the separation yield by the reverse IDA method (600 nm). The least measurable amount was 10-9 g, the standard deviation +-3.5%, the simultaneous processing of 20 samples took about 3 hours. With this method the results have higher values than with nonradiometric procedures burdened with a systematic error due to Cu losses. (M.K.)

  9. Tangram solved? Prefrontal cortex activation analysis during geometric problem solving.

    Science.gov (United States)

    Ayaz, Hasan; Shewokis, Patricia A; Izzetoğlu, Meltem; Çakır, Murat P; Onaral, Banu

    2012-01-01

    Recent neuroimaging studies have implicated prefrontal and parietal cortices for mathematical problem solving. Mental arithmetic tasks have been used extensively to study neural correlates of mathematical reasoning. In the present study we used geometric problem sets (tangram tasks) that require executive planning and visuospatial reasoning without any linguistic representation interference. We used portable optical brain imaging (functional near infrared spectroscopy--fNIR) to monitor hemodynamic changes within anterior prefrontal cortex during tangram tasks. Twelve healthy subjects were asked to solve a series of computerized tangram puzzles and control tasks that required same geometric shape manipulation without problem solving. Total hemoglobin (HbT) concentration changes indicated a significant increase during tangram problem solving in the right hemisphere. Moreover, HbT changes during failed trials (when no solution found) were significantly higher compared to successful trials. These preliminary results suggest that fNIR can be used to assess cortical activation changes induced by geometric problem solving. Since fNIR is safe, wearable and can be used in ecologically valid environments such as classrooms, this neuroimaging tool may help to improve and optimize learning in educational settings. PMID:23366983

  10. Screening and antibacterial activity analysis of some important medicinal plants

    Directory of Open Access Journals (Sweden)

    G. Senthilmurugan Viji

    2013-02-01

    Full Text Available The screening and study of five different plant specimens belonging to different families for phytochemical constituents was performed using generally accepted laboratory technique for qualitative determinations. The constituents screened were saponins, combined anthraquinones, terpenoids, flavonoids, carotenoids, steroids, xantho proteins, couramins, alkaloids, quinones, vitamin C. The distribution of these constituents in the plant specimens were assessed and compared. The medicinal plant studied were Acalypha indica, Camellia sinensis, Plectranthus amboinicus, Curcuma longa, Rauvolfia tetraphylla. All the plant speciemens were found to contain terpenoids, xantho proteins, couramins and vitamin C. They also contain Saponins (except Curcuma longa, Combined anthroquinones (except Acalypha indica, Camellia sinensis, Curcuma longa flavonoids (except Acalypha indica, Camellia sinensis, Carotenoids (except Acalypha indica, Curcuma longa, and steroids (except Plectranthus amboinicus, Rauvolfia tetraphylla Quinones were found in one out of the five specimens. Some of the medicinal plant seemed to have potential as source of useful drugs. Though the one percent extracts of all the plants showed some degree of antimicrobial activity, it was significant in Acalypha indica, Camellia sinensis, Plectranthus amboinicus, Curcuma longa, and Rauvolfia tetraphylla. The extract of Camellia sinensis and Acalypha indica was most effective against Enterobacter faecalis (ZI = 3 cm and ZI = 1.7cm and Camellia sinensis and Acalypha indica was most effective against Staphylococcus aureus (ZI = 2.1 cm.

  11. Shielding analysis for industrial package: focusing on dry active waste

    International Nuclear Information System (INIS)

    In this study, maximum exposure rate at DAW(Dry Active Waste) drum surface which is satisfying regulation limit was calculated for conceptual design of IP(Industrial Package). DAW can be classified as combustible and non-combustible waste and the calculation was conducted for single and mixed radionuclide for each type of waste. In case of combustible waste that mixed radionuclide is uniformly distributed, the maximum exposure rates at drum surface were 3.60E-01, 8.85E-01 and 1.27E+01 mSv/hr for IP Type 1, 2-a and 2-b, respectively. and 3.60E-01, 8.85E-01, 1.27E+01 mSv/hr for single radionuclide(Co-60). In case of non-combustible waste that mixed radionuclide is uniformly distributed, the maximum exposure rates at drum surface were 7.14E-01, 1.83E+00, 2.69E+01 mSv/hr for IP Type 1, 2-a and 2-b, respectively. and 7.13E-01, 1.81E-01, 2.62E+01 mSv/hr for single radionuclide(Co-60), Through this study, the maximum amount of DAW can be transported by IP was suggested as maximum exposure rate at drum surface and the calculation for the other types of waste will be conducted

  12. Neutron activation analysis of airborne thorium liberated during welding operations

    Energy Technology Data Exchange (ETDEWEB)

    Glasgow, D.C.; Robinson, L.; Janjovic, J.T.

    1996-02-01

    Typically, reactive metals such as aluminum are welded using a thoriated tungsten welding electrode which is attached to a source of argon gas such that the local atmosphere around the weld is inert. The metal is heated by the arc formed between the electrode and the grounded component to be welded. During this process, some of the electrode is vaporized in the arc and is potentially liberated to the surrounding air. This situation may result in a hazardous airborne thorium level. Because the electrode is consumed during welding, the electrode tip must be repeatedly dressed by grinding the tip to a fine point so that the optimal welding conditions are maintained. These grinding activities may also release thorium to the air. Data generated in the 1950s suggested that these electrodes posed no significant health hazard and seemed to justify their exemption from licensing requirements for source material. Since that time, other studies have been performed and present conflicting results as to the level of risk. Values both above and below the health protection limit in use in the United States, have been reported in the literature recently. This study is being undertaken to provide additional data which may be useful in evaluating both the chemical toxicity risk and radiological dose assessment criteria associated with thoriated tungsten welding operations.

  13. Research progress in nonlinear analysis of heart electric activities

    Institute of Scientific and Technical Information of China (English)

    2006-01-01

    Nonlinear science research is a hot point in the world. It has deepened our cognition of determinism and randomicity, simplicity and complexity, noise and order and it will profoundly influence the progress of the study of natural science, including life science.Life is the most complex nonlinear system and heart is the core of lifecycle system. In the late more than 20 years, nonlinear research on heart electric activities has made much headway. The commonly used parameters are based on chaos and fractal theory, such as correlation dimension, Lyapunov exponent, Kolmogorov entropy and multifractal singularity spectrum. This paper summarizes the commonly used methods in the nonlinear study of heart electric signal. Then, considering the shortages of the above traditional nonlinear parameters, we mainly introduce the results on short-term heart rate variability (HRV) signal (500 R-R intervals) and HFECG signal (1-2s). Finally, we point out it is worthwhile to put emphasis on the study of the sensitive nonlinearity parameters of short-term heart electric signal and their dynamic character and clinical effectivity.

  14. Learning Multiscale Active Facial Patches for Expression Analysis.

    Science.gov (United States)

    Zhong, Lin; Liu, Qingshan; Yang, Peng; Huang, Junzhou; Metaxas, Dimitris N

    2015-08-01

    In this paper, we present a new idea to analyze facial expression by exploring some common and specific information among different expressions. Inspired by the observation that only a few facial parts are active in expression disclosure (e.g., around mouth, eye), we try to discover the common and specific patches which are important to discriminate all the expressions and only a particular expression, respectively. A two-stage multitask sparse learning (MTSL) framework is proposed to efficiently locate those discriminative patches. In the first stage MTSL, expression recognition tasks are combined to located common patches. Each of the tasks aims to find dominant patches for each expression. Secondly, two related tasks, facial expression recognition and face verification tasks, are coupled to learn specific facial patches for individual expression. The two-stage patch learning is performed on patches sampled by multiscale strategy. Extensive experiments validate the existence and significance of common and specific patches. Utilizing these learned patches, we achieve superior performances on expression recognition compared to the state-of-the-arts. PMID:25291808

  15. Elemental analysis of airborne particulate by using thermal and epithermal neutron activation

    International Nuclear Information System (INIS)

    Thermal neutron activation analysis was used to determine Al, Br, Ca, Cl, Mn, Na, V, and Ti concentrations, whereas epithermal neutron activation analysis was used to determine Cu, I and Si concentrations. Counting by Compton suppression both in thermal neutron activation and epithermal neutron activation analysis showed the significantly different on detection limit of element compare with normal counting system. It revealed counting by Compton suppression gave better result. The enrichment factor of elements indicated that V and Mn were enriched in several fine particulate samples. Ca, Si and Na were not enriched, whereas Br, I and Cl were enriched in fine airborne particulate or in coarse one. It was found that Cl and Na did not have correlation, while Br and I showed the same enrichment the same enrichment trend and high correlation (0,9). It means that Br and I were from the same pollutant source. It could concluded that the thermal neutron and epithermal neutron activations analysis combined with counting by Compton suppression could enhance sensitivity of analysis of elemental air bone particulate that was very useful in air pollution study. Key words : activation analysis, thermal neutron, epithermal neutron, Compton

  16. The persistence of equatorial spread F - an analysis on seasonal, solar activity and geomagnetic activity aspects

    Science.gov (United States)

    Sreeja, V.; Devasia, C. V.; Ravindran, Sudha; Sridharan, R.

    2009-02-01

    The persistence (duration) of Equatorial Spread F (ESF), which has significant impact on communication systems, is addressed. Its behavior during different seasons and geomagnetic activity levels under the solar maximum (2001) and minimum (2006) conditions, is reported using the data from the magnetic equatorial location of Trivandrum (8.5° N; 77° E; dip 0.5° N) in India. The study reveals that the persistence of the irregularities can be estimated to a reasonable extent by knowing the post sunset F region vertical drift velocity (Vz) and the magnetic activity index Kp. Any sort of advance information on the possible persistence of the ionospheric irregularities responsible for ESF is important for understanding the scintillation morphology, and the results which form the first step in this direction are presented and discussed.

  17. Elemental analysis using instrumental neutron activation analysis and inductively coupled plasma atomic emission spectrometry: a comparative study

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Choi, Kwang Soon; Moon, Jong Hwa; Kim, Sun Ha; Lim, Jong Myoung; Kim, Young Jin [KAERI, Taejon (Korea, Republic of); Quraishi, Shamshad Begum [Bangladesh Atomic Energy Commission, Dhaka (Bangladesh)

    2003-05-01

    Elemental analyses for certified reference materials were carried out using instrumental neutron activation analysis and inductively coupled plasma-atomic emission spectrometry. Five Certified Reference Materials (CRM) were selected for the study on comparative analysis of environmental samples. The CRM are Soil (NIST SRM 2709), Coal fly ash (NIST SRM 1633a), urban dust (NIST SRM 1649a) and air particulate on filter media (NIST SRM 2783 and human hair (GBW 09101)

  18. Elemental analysis using instrumental neutron activation analysis and inductively coupled plasma atomic emission spectrometry: a comparative study

    International Nuclear Information System (INIS)

    Elemental analyses for certified reference materials were carried out using instrumental neutron activation analysis and inductively coupled plasma-atomic emission spectrometry. Five Certified Reference Materials (CRM) were selected for the study on comparative analysis of environmental samples. The CRM are Soil (NIST SRM 2709), Coal fly ash (NIST SRM 1633a), urban dust (NIST SRM 1649a) and air particulate on filter media (NIST SRM 2783 and human hair (GBW 09101)

  19. ISO Guest Observer Data Analysis and LWS Instrument Team Activities

    Science.gov (United States)

    Smith, Howard

    2001-01-01

    The following is an interim annual report. Dr. Smith is currently on an extended TDY to the Istituto di Fisica dello Spazio Interplanetario (IFSI) at the Consilio Nazionale delle Richerche (CNR) in Rome, Italy, where he has been working on a related NASA grant in support of analysis of Infrared Space Observatory (ISO) data on star formation in Ultra Luminous Infrared Galaxies and our galaxy. Work emphasizes development of metal mesh grids for use in spacecraft, and the design and fabrication of test elements by the Naval Research Laboratory, Washington D.C. Work has progressed well, but slowly, on that program due to the departure of a key engineer. NASA has been advised of the delay, and granted a no-cost extension, whereby SAO has authorized a delay in the final report from NRL. Nevertheless NRL has continued to make progress. Two papers have been submitted to refereed journals related to this program, and a new design for mesh operating in the 20-40 micron region has been developed. Meetings continue through the summer on these items. A new technical scientist has been made a job offer and hopefully will be on board NRL shortly, although most of the present grant work is already completed. A more complete report, with copies of the submitted papers, designs, and other measures of progress, will be submitted to NASA in September when Dr. Smith returns from his current TDY.

  20. Recent developments of prompt gamma activation analysis at Budapest

    International Nuclear Information System (INIS)

    The PGAA facility at the Budapest Research Reactor has been continually upgraded and developed since its start-up in 1996, as a result of which its performance has improved considerably. The installation of the cold neutron source, the partial change to supermirror neutron guides and their realignment increased the flux by almost two orders of magnitude. The data acquisition has been modernized as well; digital spectrometers were tested and implemented in novel forms of gamma-ray spectrum collection. This year a higher-efficiency HPGe detector and a new data acquisition module were put into operation. Most recently all the neutron guides were changed to supermirror-coated ones to further increase the neutron flux. The improved evaluation software makes possible a more reliable elemental analysis of the samples. In this progress report these developments are critically reviewed. The characteristics of the latest system are also described. It is the first time that a set of new partial gamma-ray production cross sections are presented, which are based on the new intensity values of 14N(n,γ)15N calibration standard. (author)

  1. Classroom management styles: an analysis from the teaching activities

    Directory of Open Access Journals (Sweden)

    Ana Lúcia Pereira Baccon,

    2015-07-01

    Full Text Available This paper analyzes and interprets the action of high school Physics teachers in the classroom. Based on the definitions given by Gauthier (1998 and Tardif (2002, we elaborated reports about action of teachers, seeking to describe how they performed class and content management in their classes. Each report was constructed from interviews and recordings of classes of three Physics teachers from public schools in Londrina, Paraná, Brazil. The reports were later interpreted through an analysis tool that considers the management of the subject and management of the class as a managing relation with wisdom (CHARLOT, 2000 in a didactic system (CHEVALLARD, 2005. As a result, we point out that the management styles of the three teachers, whose classes were analyzed in this paper, correspond approximately to three management styles: focused on the content of the subject (gS, focused on the teaching practiced by the teacher (gP or focused on students’ learning (gE. Thus, teachers may have three different general types of classroom management.

  2. Facilitating neuronal connectivity analysis of evoked responses by exposing local activity with principal component analysis preprocessing: simulation of evoked MEG.

    Science.gov (United States)

    Gao, Lin; Zhang, Tongsheng; Wang, Jue; Stephen, Julia

    2013-04-01

    When connectivity analysis is carried out for event related EEG and MEG, the presence of strong spatial correlations from spontaneous activity in background may mask the local neuronal evoked activity and lead to spurious connections. In this paper, we hypothesized PCA decomposition could be used to diminish the background activity and further improve the performance of connectivity analysis in event related experiments. The idea was tested using simulation, where we found that for the 306-channel Elekta Neuromag system, the first 4 PCs represent the dominant background activity, and the source connectivity pattern after preprocessing is consistent with the true connectivity pattern designed in the simulation. Improving signal to noise of the evoked responses by discarding the first few PCs demonstrates increased coherences at major physiological frequency bands when removing the first few PCs. Furthermore, the evoked information was maintained after PCA preprocessing. In conclusion, it is demonstrated that the first few PCs represent background activity, and PCA decomposition can be employed to remove it to expose the evoked activity for the channels under investigation. Therefore, PCA can be applied as a preprocessing approach to improve neuronal connectivity analysis for event related data.

  3. Effectiveness of Physical Activity Interventions for Preschoolers: A Meta-Analysis

    Science.gov (United States)

    Gordon, Elliott S.; Tucker, Patricia; Burke, Shauna M.; Carron, Albert V.

    2013-01-01

    Purpose: The purpose of the meta-analysis was to examine the effectiveness of physical activity interventions on physical activity participation among preschoolers. A secondary purpose was to investigate the influence of several possible moderator variables (e.g., intervention length, location, leadership, type) on moderate-to-vigorous physical…

  4. Conversion Matrix Analysis of GaAs HEMT Active Gilbert Cell Mixers

    DEFF Research Database (Denmark)

    Jiang, Chenhui; Johansen, Tom Keinicke; Krozer, Viktor

    2006-01-01

    In this paper, the nonlinear model of the GaAs HEMT active Gilbert cell mixer is investigated. Based on the model, the conversion gain expression of active Gilbert cell mixers is derived theoretically by using conversion matrix analysis method. The expression is verified by harmonic balance...

  5. In Vitro Antimicrobial Bioassays, DPPH Radical Scavenging Activity, and FTIR Spectroscopy Analysis of Heliotropium bacciferum

    OpenAIRE

    Ahmad, Sohail; AbdEl-Salam, Naser M.; Ullah, Riaz

    2016-01-01

    The present study deals with the antimicrobial, antioxidant, and functional group analysis of Heliotropium bacciferum extracts. Disc diffusion susceptibility method was followed for antimicrobial assessment. Noteworthy antimicrobial activities were recorded by various plant extracts against antibiotic resistant microorganisms. Plant flower extracts antioxidant activity was investigated against 2, 2-diphenyl-1-picryl hydrazyl radical by ultraviolet spectrophotometer (517 nm). Plant extracts di...

  6. Determination of gold in some Myanmar indigenous medicines by neutron activation analysis

    International Nuclear Information System (INIS)

    Gold has been determined in two Myanmar indigenous medicines TMF 14 (Devaauthada), TMF 15 (Shwe Thwe Say) by neutron activation analysis using an Am(Be) radionuclide neutron source. The activity of 411 keV of the 198Au has been measured. (author). 2 refs., 1 fig., 1 tab

  7. Simultaneous Determination of Arsenic, Manganese, and Selenium in Biological Materials by Neutron-Activation Analysis

    DEFF Research Database (Denmark)

    Heydorn, Kaj; Damsgaard, Else

    1973-01-01

    A new method was developed for the simultaneous determination of arsenic, manganese, and selenium in biological material by thermal-neutron activation analysis. The use of 81 mSe as indicator for selenium permitted a reduction of activation time to 1 hr for a 1 g sample, and the possibility of loss...

  8. 30 CFR 280.30 - What activities will not require environmental analysis?

    Science.gov (United States)

    2010-07-01

    ... Obligations Under This Part Environmental Issues § 280.30 What activities will not require environmental... 30 Mineral Resources 2 2010-07-01 2010-07-01 false What activities will not require environmental... environmental impact and will normally be categorically excluded from additional environmental analysis....

  9. Cultural-Historical Activity Theory and Domain Analysis: Metatheoretical Implications for Information Science

    Science.gov (United States)

    Wang, Lin

    2013-01-01

    Background: Cultural-historical activity theory is an important theory in modern psychology. In recent years, it has drawn more attention from related disciplines including information science. Argument: This paper argues that activity theory and domain analysis which uses the theory as one of its bases could bring about some important…

  10. Seeing, Believing, and Learning to Be Skeptical: Supporting Language Learning through Advertising Analysis Activities

    Science.gov (United States)

    Hobbs, Renee; He, Haixia; Robbgrieco, Michael

    2015-01-01

    This study documents how a high school ESL teacher working with new immigrants ages 14-20 supported the development of their critical thinking and English language skills by using advertising analysis activities. The article examines the use of key critical questions for analyzing media messages and documents instructional activities designed to…

  11. QSAR analysis of antitumor activities of 3,4-ethylenedioxythiphene derivatives

    Science.gov (United States)

    Rastija, Vesna; Bajić, Miroslav; Stolić, Ivana; Krstulović, Luka; Jukić, Marijana; Glavaš-Obrovac, Ljubica

    2015-12-01

    QSAR analysis was performed for the antitumor activity of 27 derivatives of 3,4-ethylenedioxythiophene against six carcinoma cell lines. The best models were obtained with surface area (SAG) in combination with lipohilicity (log P) as descriptors. Results have shown that molecules with smaller solvent accessible surface area and higher lipophilicy should have higher biological activity against carcinoma cell.

  12. Application of ABCD Formalism in Theoretical and Experimental Analysis of Actively Modelocked Fiber Laser

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Time domain ABCD matrix formalism is a useful model for analyzing the characteristics of actively modelocked fiber laser. Based on this model and given more consideration on the influences of optical fiber dispersion and optical fiber nonlinearity, the laser characteristic of actively modelocked fiber laser is analyzed, and the comparision of the theoretical analysis results with experimental ones is given.

  13. Comparing Effects of Different Writing Activities on Reading Comprehension: A Meta-Analysis

    Science.gov (United States)

    Hebert, Michael; Simpson, Amy; Graham, Steve

    2013-01-01

    The purposes of this review were to determine: (1) if different writing activities were more effective than others in improving students' reading comprehension, and (2) if obtained differences among writing activities was related to how reading comprehension was measured? Meta-analysis was used to examine these questions across studies involving…

  14. Determination of activable isotopic tracers of zinc by neutron activation analysis for study of bioavailability of zinc

    International Nuclear Information System (INIS)

    A procedure of pre-irradiation concentration of zinc in fecal samples using anion exchanger was developed for the study of the bioavailability of zinc by neutron activation analysis. The mass ratios between 70Zn and 68Zn, or 64Zn and their contents between natural zinc and enriched zinc are used to calculate the bioavailability of zinc when the abundance of the isotope 70Zn is not high enough. (author) 9 refs.; 1 fig.; 2 tabs

  15. Neutron activation analysis (NAA), radioisotope production via neutron activation (PNA) and fission product gas-jet (GJA)

    Energy Technology Data Exchange (ETDEWEB)

    Gaeggeler, H.W. [Paul Scherrer Inst. (PSI), Villigen (Switzerland)

    1996-11-01

    Three different non-diffractive applications of neutrons are outlined, neutron activation analysis, production of radionuclides, mostly for medical applications, and production of short-lived fission nuclides with a so-called gas-jet. It is shown that all three devices may be incorporated into one single insert at SINQ due to their different requests with respect to thermal neutron flux. Some applications of these three facilities are summarized. (author) 3 figs., 1 tab., 8 refs.

  16. A Multi-Wavelength Analysis of Active Regions and Sunspots by Comparison of Automated Detection Algorithms

    OpenAIRE

    Verbeeck, Cis; Higgins, Paul A.; Colak, Tufan; Watson, Fraser T.; Delouille, Veronique; Mampaey, Benjamin; Qahwaji, Rami

    2011-01-01

    Since the Solar Dynamics Observatory (SDO) began recording ~ 1 TB of data per day, there has been an increased need to automatically extract features and events for further analysis. Here we compare the overall detection performance, correlations between extracted properties, and usability for feature tracking of four solar feature-detection algorithms: the Solar Monitor Active Region Tracker (SMART) detects active regions in line-of-sight magnetograms; the Automated Solar Activity Prediction...

  17. Using wildlife activity and antibiotic resistance analysis to model bacterial water quality in coastal ponds

    OpenAIRE

    Pullaro, Thomas C.; Pan, Wei; Chiovarou, Erica D.; Daugomah, James W.; Shea, Norman R.; Siewicki, Thomas C.

    2009-01-01

    Models that help predict fecal coliform bacteria (FCB) levels in environmental waters can be important tools for resource managers. In this study, we used animal activity along with antibiotic resistance analysis (ARA), land cover, and other variables to build models that predict bacteria levels in coastal ponds that discharge into an estuary. Photographic wildlife monitoring was used to estimate terrestrial and aquatic wildlife activity prior to sampling. Increased duck activity was an impor...

  18. Optimization in Activation Analysis by Means of Epithermal Neutrons. Determination of Molybdenum in Steel

    International Nuclear Information System (INIS)

    Optimization in activation analysis by means of selective activation with epithermal neutrons is discussed. This method was applied to the determination of molybdenum in a steel alloy without recourse to radiochemical separations. The sensitivity for this determination is estimated to be 10 ppm. With the common form of activation by means of thermal neutrons, the sensitivity would be about one-tenth of this. The sensitivity estimations are based on evaluation of the photo peak ratios of Mo-99/Fe-59

  19. COMPILATION OF ACTIVE FAULT DATA IN PORTUGAL FOR USE IN SEISMIC HAZARD ANALYSIS

    OpenAIRE

    Nemser, E.S.; Cabral, J.; Terrinha, P.; Vilanova, S.; Besana-Ostman, G.M.; Bezzeghoud, M.; Borges, J. F.; Brum da Silveira, A.; Carvalho, J.; R.P. Dias; P. M. Figueiredo; Fonseca, J.; Lopes, F.C.; J. Madeira; L. Matias

    2010-01-01

    To estimate where future earthquakes are likely to occur, it is essential to combine information about past earthquakes with knowledge about the location and seismogenic properties of active faults. For this reason, robust probabilistic seismic hazard analysis (PSHA) integrates seismicity and active fault data. Existing seismic hazard assessments for Portugal rely exclusively on seismicity data and do not incorporate data on active faults. Project SHARE (Seismic Hazard Harmonization in Europe...

  20. Simple and direct determination of active ingredients in drugs by neutron activation analysis

    International Nuclear Information System (INIS)

    The increasing number of drugs in the market and the need for their control requires new, simple, fast and accurate analytical methods. Iodine, iron, manganese, silver and sodium were determined by INAA in various pharmaceutical formulations, representing capsules, injectables, powders for injection, solutions and tablets. From the results it appears that NAA could be used as an official method for the determination of iron, manganese and silver in pharmaceutical products, in which these elements are present as active ingredients, as well as for the control of the concentration limits for iodine and sodium. (author)

  1. The technical analysis of the stock exchange and physics: Japanese candlesticks for solar activity

    Science.gov (United States)

    Dineva, C.; Atanasov, V.

    2013-09-01

    In this article, we use the Japanese candlesticks, a method popular in the technical analysis of the Stock/Forex markets and apply it to a variable in physics-the solar activity. This method is invented and used exclusively for economic analysis and its application to a physical problem produced unexpected results. We found that the Japanese candlesticks are convenient tool in the analysis of the variables in the physics of the Sun. Based on our observations, we differentiated a new cycle in the solar activity.

  2. Promotion of physical activity in the European region: content analysis of 27 national policy documents

    DEFF Research Database (Denmark)

    Daugbjerg, Signe B; Kahlmeier, Sonja; Racioppi, Francesca;

    2009-01-01

    search methods, 49 national policy documents on physical activity promotion were identified. An analysis grid covering key features was developed for the analysis of the 27 documents published in English. RESULTS: Analysis showed that many general recommendations for policy developments are being....... Population groups most in need such as people with low levels of physical activity were rarely specifically targeted. Most policies emphasized the importance of an evaluation. However, only about half of them indicated a related intention or requirement. CONCLUSION: In recent years there has been...

  3. Biofac, a microbiological multimedia tool to perform the analysis of activated sludge

    International Nuclear Information System (INIS)

    The composition and structure of the macrobiotic that is part of the active sludge, its temporal evolution, and the analysis of the macroscopic and microscopic characteristics of it are a source of information of great help in making decisions for plant operators. Lack of training and access to specific information linked to the missing standardization of analysis processes hinder the implementation and interpretation of them. Using a multimedia tool in DVD, Facsa has developed the Biofac, an application in which it is documented and illustrated the most relevant aspects that allow the user to perform the analysis of activated sludge. (Author)

  4. Comparison of Activation Analysis Codes between CINDER'90 and ORIGEN-S

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Jeong Dong; Choi, Hong Yeop; Lee, Yong Deok; Kim, Hodong [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2014-05-15

    A Slowing Down Time Spectrometer (SDTS) system is the most feasible technology among the non-destructive techniques to directly analyze the content of isotopic fissile material. SDTS is necessary to a source neutron for inducing isotopic fissile fission. The source neutron is produced between the electron beam and a metal target by an (e,γ)(γ,n) reaction in the target. The target is required to have a high intensity neutron source through a proper target design. The status of activation on the designed target is analyzed through the activation code. Also, an activation evaluation of the material of the shielding facilities for SDTS system is required. The radioactivity intensity and kind of nuclides are measured through an activation analysis. ORIGEN-S and CINDER'90 codes are an activation code and are used in combination with the MCNPX code. ORIGEN-S code interprets a problem as one point about target. It cannot describe the geometry. CINDER'90 code can describe a 3D-geometry, and the result of CINDER'90 has high reliability when using a multi-group library. In this research, CINDER'90 was introduced as an activation analysis code and compared with the ORIGEN-S code. An activation analysis was conducted on the materials of the designed target. The ORIGEN-S and CINDER'90 code simulation results are provided for a selection of the activation analysis code. A Slowing Down Time Spectrometer (SDTS) system is a highly efficient technique in a nuclear material analysis. An activation analysis on the shielding and target material was required for the SDTS system. The activation results of CINDER'90 and ORIGEN-S codes were similar or different according to the nuclides because the cross section library of the codes is different. In utilizing the code, CINDER'90 code is more convenient than ORIGEN-S. It can describe the 3D-geometry, and therefore the activation information can be obtained by one simulation. The results of the activation

  5. Health-care district management information system plan: Review of operations analysis activities during calendar year 1975 and plan for continued research and analysis activities

    Science.gov (United States)

    Nielson, G. J.; Stevenson, W. G.

    1976-01-01

    Operations research activities developed to identify the information required to manage both the efficiency and effectiveness of the Veterans Administration (VA) health services as these services relate to individual patient care are reported. The clinical concerns and management functions that determine this information requirement are discussed conceptually. Investigations of existing VA data for useful management information are recorded, and a diagnostic index is provided. The age-specific characteristics of diseases and lengths of stay are explored, and recommendations for future analysis activities are articulated. The effect of the introduction of new technology to health care is also discussed.

  6. Research in the fields of radiochemistry and activation analysis using the LENA TRIGA nuclear plant

    International Nuclear Information System (INIS)

    In the past two years most of the research effort at the Radiochemistry Laboratory and National Research Council Centre for Radiochemistry and Activation Analysis has been devoted to research and development of activation analysis using the TRIGA Mark II LENA reactor of the University of Pavia. Pile neutrons have been used both in steady state and pulse mode, in the determination of oxygen in non ferrous materials. Neutron activation has been applied to the determination of some atmospheric particulate pollutants. Another field, in which activation analysis has been applied, is forensic research. Methods have been developed for the determination of antimony, barium and copper in gunpowder residues. By using inorganic materials such as molybdenum dibromide, zinc ferrocyanide and cadmium metal in granular form it was possible to set up simple chemical procedures in the activation analysis of trace amounts of noble metals in metallic matrices (high purity nickel and copper), geochemical materials (rocks and meteorites) and biological materials (orchard leaves). Neutron activation analysis was also used to investigate on the extraction of the platinum group metals from iodide and thiocyanate solutions at low concentrations

  7. A new approach to analysis of relationships between 137Cs activity concentrations in forest soil horizons

    International Nuclear Information System (INIS)

    The measurements results of 137Cs activity concentrations in forest soil profiles are discussed. In studies some simplifications were considered. First of them concerns disregarding of soil subtype in data analysis. However initially this parameter was considered in data analysis, it was finally ignored. The second assumption drops information about specific soil horizon. Description of 137Cs accumulation is based on relationships between its relative activity concentrations in soil layers. The model formulation was based on the results of exploratory data analysis of the relative 137Cs activity concentrations. In studies the methods designed for compositional data analysis were used. The results of analysis showed that the relationships between the relative activity concentrations of 137Cs in soil layers, due to their nature, might be divided into two groups. The first of them concerns layers located close to soil surface. The relative activity concentrations of 137Cs in these layers are proportional to each other, and distribution mechanism of cesium within them has the characteristics of the process leading to thermodynamic equilibrium. The second group is related to layers that are located deeper. The calculation results suggest lack of thermodynamic equilibrium between these layers and layers situated above. Utilization of a linear model for description of changes in relative activity concentrations of 137Cs in deeper layers supposes that these changes occur much slower than in layers lying above. (author)

  8. Using visual information analysis to explore complex patterns in the activity of designers

    DEFF Research Database (Denmark)

    Cash, Philip; Stanković, Tino; Štorga, Mario

    2014-01-01

    The analysis of complex interlinked datasets poses a significant problem for design researchers. This is addressed by proposing an information visualisation method for analysing patterns of design activity, qualitatively and quantitatively, with respect to time. This method visualises the tempora......The analysis of complex interlinked datasets poses a significant problem for design researchers. This is addressed by proposing an information visualisation method for analysing patterns of design activity, qualitatively and quantitatively, with respect to time. This method visualises...... to a fully realised example of information seeking activity. The core contribution of the proposed method is in supporting the analysis of activity with respect to both macro and micro level temporal interactions between variables....

  9. WWER Expert System for Fuel Failure Analysis Using Data on Primary Coolant Activity

    International Nuclear Information System (INIS)

    The computer expert system for fuel failure analysis of WWER during operation is presented. The diagnostics is based on the measurement of specific activity of reference nuclides in reactor primary coolant and application of a computer code for the data interpretation. The data analysis includes an evaluation of tramp uranium mass in reactor core, detection of failures by iodine and caesium spikes, evaluation of burnup of defective fuel. Evaluation of defective fuel burnup was carried out by applying the relation of caesium nuclides activity in spikes and relations of activities of gaseous fission products for steady state operational conditions. The method of burnup evaluation of defective fuel by use of fission gas activity is presented in detail. The neural-network analysis is performed for determination of failed fuel rod number and defect size. Results of the expert system application are illustrated for several fuel campaigns on operating WWER NPPs. (authors)

  10. Mediation analysis of the relationship between institutional research activity and patient survival

    DEFF Research Database (Denmark)

    Rochon, Justine; du Bois, Andreas; Lange, Theis

    2014-01-01

    mediated through either optimal surgery or chemotherapy. Taken together, about 26% of the beneficial effect of research activity was mediated through the proposed pathways. CONCLUSIONS: Mediation analysis allows proceeding from the question "Does it work?" to the question "How does it work?" In particular......BACKGROUND: Recent studies have suggested that patients treated in research-active institutions have better outcomes than patients treated in research-inactive institutions. However, little attention has been paid to explaining such effects, probably because techniques for mediation analysis...... existing so far have not been applicable to survival data. METHODS: We investigated the underlying mechanisms using a recently developed method for mediation analysis of survival data. Our analysis of the effect of research activity on patient survival was based on 352 patients who had been diagnosed...

  11. Comparative study of destructive and non-destructive methods in the activation analysis of rocks

    International Nuclear Information System (INIS)

    A comparative study between non-destructive thermal neutron activation analysis and activation analysis with radiochemical group separation is made Both methods are applied to the determination of trace elements minor and major elements in rocks. The treatment of the rocks, with special reference to the problems related to grinding and contamination by foreign elements is described. The choice of standards for multielement trace activation analysis is discussed. Two types of computer programs for the evalution of data obtained through Ge-li detector counting are used. All the phases of the destructive and non destructive analysis are described. In the destructive analysis, an adaptation of the group separation scheme developed by Morrison et al for the activation analysis of geological samples is made. The changes introduced make the radiochemical separation simpler and more rapid. Both destructive and non destructive methods are tested by means of the analysis of the United States Geological Survey standard rock AGV-1, which has been analysed by many authors. The same procedure is then applied to some alcaline rocks taken from the apatite mine of Jacupiranga, in the State of Sao Paulo, Brazil. The knowledge of the trace element concentration in these rocks is important for geochemical studies. A detailed study of the possible interferences encountered in the neutron activation analysis of these rocks is made, considering the interferences due to major activities, and to the proximity of the several gamma ray energies of the radioisotopes produced. Finally, the comparative study between the two methods is presented, using statistical tests for the quantitative evalution of results. (Author)

  12. Analysis and Design of Wide-Band SiGe HBT Active Mixers

    DEFF Research Database (Denmark)

    Johansen, Tom Keinicke; Krozer, Viktor; Vidkjær, Jens

    2005-01-01

    The frequency response of SiGe HBT active mixers based on the Gilbert cell topology is analyzed theoretically. The time-varying operation of the active mixer is taken into account by applying conversion matrix analysis. The main bandwidth-limiting mechanisms experienced in SiGe HBT active mixers...... performing frequency conversion of wide-band signals is discussed. The analysis is verified by computer simulations using a realistic high-frequency large-signal SiGe HBT model. An active mixer design based on the Gilbert cell topology modified for wide-band operation using emitter degenerated...... transconductance stage and shunt feedback load stage is discussed. Experimental results are given for an active mixer implemented in a 0.8-μm 35-GHz fT SiGe HBT BiCMOS process....

  13. Analysis of primer independent phosphorylase activity in potato plants: high levels of activity in sink organs and sucrose-dependent activity in cultured stem explants.

    Science.gov (United States)

    Moreno, S; Tandecarz, J S

    1996-07-01

    One isoform of potato (Solanum tuberosum L., cv. Spunta), type L phosphorylase (EC 2.4.1.1), exhibiting primer independent activity appears to be tuber-specific. However, this activity can also be modulated by exogenous sucrose in storage as well as in non-storage organs. Primer independent phosphorylase (PIPh) activity in microtubers and shoots of in vitro plantlets was found to be much higher than in tubers and shoots of soil-grown plants. Detached leaves of soil-grown plants showed an increase in PIPh activity as well when incubated in sucrose-containing Murashige-Skoog (MS) medium. This increase was always accompanied by a rise in starch content. The presence of metabolizable carbohydrates in the growth or incubation medium are likely to be responsible for the observed rise in PIPh activity. In vitro microtubers and micropropagated plantlet organs (shoots and roots) exhibited a correlation between measurable PIPh activity and presence of enzyme protein, as judged by Western blot analysis using anti-potato tuber type L phosphorylase antibody. Therefore, in addition, to be developmentally regulated (tuber-specific accumulation), PIPh activity associated with the tuber type L isoform might be under a form of metabolic regulation. PMID:8832093

  14. Structure-Activity Analysis of Gram-positive Bacterium-producing Lasso Peptides with Anti-mycobacterial Activity

    Science.gov (United States)

    Inokoshi, Junji; Koyama, Nobuhiro; Miyake, Midori; Shimizu, Yuji; Tomoda, Hiroshi

    2016-07-01

    Lariatin A, an 18-residue lasso peptide encoded by the five-gene cluster larABCDE, displays potent and selective anti-mycobacterial activity. The structural feature is an N-terminal macrolactam ring, through which the C-terminal passed to form the rigid lariat-protoknot structure. In the present study, we established a convergent expression system by the strategy in which larA mutant gene-carrying plasmids were transformed into larA-deficient Rhodococcus jostii, and generated 36 lariatin variants of the precursor protein LarA to investigate the biosynthesis and the structure-activity relationships. The mutational analysis revealed that four amino acid residues (Gly1, Arg7, Glu8, and Trp9) in lariatin A are essential for the maturation and production in the biosynthetic machinery. Furthermore, the study on structure-activity relationships demonstrated that Tyr6, Gly11, and Asn14 are responsible for the anti-mycobacterial activity, and the residues at positions 15, 16 and 18 in lariatin A are critical for enhancing the activity. This study will not only provide a useful platform for genetically engineering Gram-positive bacterium-producing lasso peptides, but also an important foundation to rationally design more promising drug candidates for combatting tuberculosis.

  15. Chromatographic finger print analysis and lysosomal membrane stabilisation activity of active fraction of Alstonia scholaris leaf extract in arthritic rats

    Directory of Open Access Journals (Sweden)

    Swapnil Goyal

    2014-01-01

    Full Text Available Object: The present study was aimed to assess the anti-arthritic activity of chloroform fraction of Alstonia scholaris leaf extract against Freund′s complete adjuvant (FCA-induced arthritis in rats. Materials and Methods: The anti-inflammatory activity of various fractions of ethanolic extract of Alstonia scholaris at concentration of 100 mg/kg was studied using the carrageenan-induced inflammatory models. The chloroform fraction shows significant anti-inflammatory activity. The chloroform fraction was further studied for anti-arthritic activity and HPTLC fingerprint analysis. For anti-arthritic activity, the active chloroform fraction was administered at the concentrations of 50 and 100 mg/kg body weight. The effect of chloroform fraction on liver ALP, ACP and LDH levels of lysosomal enzymes of FCA arthritic animals were studied. Indomethacin and prednisolone (10 mg/kg was used as standard. HPTLC studies were carried out using CAMAG HPTLC system equipped with linomat IV applicator, TLC scanner; Reprostar 3 and WIN CATS-4 software were used. Results: The chloroform fraction at 100 mg/kg, showed maximum inhibition (34.16% of inflammation induced by carrageenan. In FCA-induced arthritis, the chloroform fraction showed a highly significant reduction in paw volume (50 mg/kg-72.71%; 100 mg/kg-74.35%. The levels of lysosomal enzymes were significantly decreased in the chloroform fraction-treated groups. Conclusion: The possible mechanism of action of the chloroform fraction of Alstonia scholaris leaf extract may be through its stabilising action on lysosomal membranes. Future studies will provide new insights into the anti-arthritic activity of Alstonia scholaris and isolation of compound from it may eventually lead to development of a new class of anti-arthritic agent.

  16. [Activity and cost analysis in surgical pathology. Experience of a French university laboratory using the activity-based costing method].

    Science.gov (United States)

    Bellocq, J P; Biron, N; Kessler, S; Penaud, M; Faujour, V; Ospel, J; Supper, E; Barthel, A; Roussel, J F; Méchine-Neuville, A; Marcellin, L; Lang-Avérous, G; Chenard, M P

    2001-06-01

    Good self-knowledge enables us to have a well- reasoned adaptation to our environment. Starting from this precept based on simple common sense, activity and cost analysis, when applied to medical departments in a university hospital setting, represents a necessary phase in their scientific progression and in the continuation of their university vocation. This is all the more true given the present climate of economic and organizational restructuring of medical facilities. This paper relates the experience of a French surgical pathology department which was assessed for cost effectiveness using the Activity-Based Costing (ABC) method in 1999. This method, which originated in the business world and of which the general concepts are presented here, has given us a keener understanding of the diverse processes involved, their costs and how these costs are arrived at. Moreover, this method has identified the proportion of costs imputable to diagnostic work and of those linked to work specific to a university hospital, in particular teaching and research and development. The results can then be used for a clearer analysis of the figures required by prescribers and health care funding agencies, and, within the department, to enhance perception of work carried out by the entire staff in order to initiate a new type of management centered on activity (Activity-Based Management). Adaptable to any medical department, whatever its organizational structure, independent of the significance of any given code letter and regardless of the rating method used to grade activities, the ABC method also allows for comparisons between structures of a similar nature. The thoughts it inspires on economic performance must take into account the rules of good medical practice, the imperatives of quality assurance, the need for "breathing space" which are indispensable to research and a humanist conception of working relations.

  17. [Activity and cost analysis in surgical pathology. Experience of a French university laboratory using the activity-based costing method].

    Science.gov (United States)

    Bellocq, J P; Biron, N; Kessler, S; Penaud, M; Faujour, V; Ospel, J; Supper, E; Barthel, A; Roussel, J F; Méchine-Neuville, A; Marcellin, L; Lang-Avérous, G; Chenard, M P

    2001-06-01

    Good self-knowledge enables us to have a well- reasoned adaptation to our environment. Starting from this precept based on simple common sense, activity and cost analysis, when applied to medical departments in a university hospital setting, represents a necessary phase in their scientific progression and in the continuation of their university vocation. This is all the more true given the present climate of economic and organizational restructuring of medical facilities. This paper relates the experience of a French surgical pathology department which was assessed for cost effectiveness using the Activity-Based Costing (ABC) method in 1999. This method, which originated in the business world and of which the general concepts are presented here, has given us a keener understanding of the diverse processes involved, their costs and how these costs are arrived at. Moreover, this method has identified the proportion of costs imputable to diagnostic work and of those linked to work specific to a university hospital, in particular teaching and research and development. The results can then be used for a clearer analysis of the figures required by prescribers and health care funding agencies, and, within the department, to enhance perception of work carried out by the entire staff in order to initiate a new type of management centered on activity (Activity-Based Management). Adaptable to any medical department, whatever its organizational structure, independent of the significance of any given code letter and regardless of the rating method used to grade activities, the ABC method also allows for comparisons between structures of a similar nature. The thoughts it inspires on economic performance must take into account the rules of good medical practice, the imperatives of quality assurance, the need for "breathing space" which are indispensable to research and a humanist conception of working relations. PMID:11468559

  18. Real-time fMRI-based activation analysis and stimulus control

    Science.gov (United States)

    Moench, Tobias; Hollmann, Maurice; Bernarding, Johannes

    2007-03-01

    The real-time analysis of brain activation using functional MRI data offers a wide range of new experiments such as investigating self-regulation or learning strategies. However, besides special data acquisition and real-time data analysing techniques such examination requires dynamic and adaptive stimulus paradigms and self-optimising MRI-sequences. This paper presents an approach that enables the unified handling of parameters influencing the different software systems involved in the acquisition and analysing process. By developing a custom-made Experiment Description Language (EDL) this concept is used for a fast and flexible software environment which treats aspects like extraction and analysis of activation as well as the modification of the stimulus presentation. We describe how extracted real-time activation is subsequently evaluated by comparing activation patterns to previous acquired templates representing activated regions of interest for different predefined conditions. According to those results the stimulus presentation is adapted. The results showed that the developed system in combination with EDL is able to reliably detect and evaluate activation patterns in real-time. With a processing time for data analysis of about one second the approach is only limited by the natural time course of the hemodynamic response function of the brain activation.

  19. Physical activity in adolescents: analysis of the social influence of parents and friends

    Directory of Open Access Journals (Sweden)

    Luanna Alexandra Cheng

    2014-01-01

    Full Text Available OBJECTIVE: To analyze the association between physical activity and social support from parents and friends on the physical activity level among adolescents. METHODS: Data from 2,361 adolescents (56.6% females; mean age 16.4; SD = 1.2, from public and private high schools were analyzed. The physical activity level of the adolescents, parents, and friends were measured through a questionnaire. Parents' and friends' support and self-efficacy were measured using two previously tested scales. Data analysis was performed usingthe structural equation modeling in IBM(r SPSS(r AmosTM 20.0. RESULTS: Physical activity of friends was directly associated with physical activity level of adolescents. Physical activity of the father was associated with their sons, and the physical activity of mother was associated with their daughters. An indirect association was identified between the physical activity of parents and friends with physical activity level of the adolescents, mediated by social support. Social support was directly associated with physical activity in adolescents of both genders and indirectly mediated by self-efficacy. CONCLUSIONS: Parents and friends have a social influence on adolescents' level of physical activity through the mechanism of behavior modeling or through social support, mediated by self-efficacy.

  20. Phytochemical Analysis and Invitro Antiarthritic Activities of Whole Plant of Hybanthus enneaspermus

    Directory of Open Access Journals (Sweden)

    S. Umamaheswari

    2016-03-01

    Full Text Available The aim of the present study is to phytochemical analysis and invitro antiarthritic activities of whole plant of Hybanthus enneaspermus. The ethanolic extract of the plant was subjected to qualitative analysis for the presence of phytochemical substances. The invitro anti arthritic activity was determined by measuring the percentage of inhibition of protein denaturation. The phytochemical analysis showed the presence of alkaloids, flavonoids, tannins, terpenoids, saponins, steroids and reducing sugars. The antiarthritic activity was determined by protein inhibition assay. The percentage protection was found to be 64.6 % for extract and 91.2% (Diclofenac sodium. The IC50 value for the extract was found to 512.6 µg/ml and for the standard it was found to be 172.82 µg/ml.