Refraction angle and edge visibility in X-ray diffraction enhanced imaging

International Nuclear Information System (INIS)

Chen Yu; Jia Quanjie; Li Gang; Wang Yuzhu; Xue Xianying; Jiang Xiaoming

2007-01-01

Diffraction-enhanced X-ray imaging could extract accurately the refraction angles of the sample, which is very important to increase the image contrast of low Z samples. In this paper, the DEI experiments with X-rays of different energies were performed both on wedge-shaped and rounded model samples. Refraction angles of the two samples were all obtained accurately, and the results agreed well with the calculations. Quantitative analyses based on Edge Visibility were performed for the wedge-shaped model sample. The results revealed that the calculated positions for the Best Edge Visibility of the slope with fixed refraction angle were calculable in good agreement with the experimental results. A quantitative research on the Edge Visibility of real tissues sample was carried out and the optimal condition for best contrast of DEI images were discussed. (authors)

Wide-angle display developments by computer graphics

Science.gov (United States)

Fetter, William A.

1989-01-01

Computer graphics can now expand its new subset, wide-angle projection, to be as significant a generic capability as computer graphics itself. Some prior work in computer graphics is presented which leads to an attractive further subset of wide-angle projection, called hemispheric projection, to be a major communication media. Hemispheric film systems have long been present and such computer graphics systems are in use in simulators. This is the leading edge of capabilities which should ultimately be as ubiquitous as CRTs (cathode-ray tubes). These assertions are not from degrees in science or only from a degree in graphic design, but in a history of computer graphics innovations, laying groundwork by demonstration. The author believes that it is timely to look at several development strategies, since hemispheric projection is now at a point comparable to the early stages of computer graphics, requiring similar patterns of development again.

JMFA2—a graphically interactive Java program that fits microfibril angle X-ray diffraction data

Science.gov (United States)

Steve P. Verrill; David E. Kretschmann; Victoria L. Herian

2006-01-01

X-ray diffraction techniques have the potential to decrease the time required to determine microfibril angles dramatically. In this paper, we discuss the latest version of a curve-fitting toll that permits us to reduce the time required to evaluate MFA X-ray diffraction patterns. Further, because this tool reflects the underlying physics more accurately than existing...

Wide-azimuth angle-domain imaging for anisotropic reverse-time migration

KAUST Repository

Sava, Paul C.; Alkhalifah, Tariq Ali

2011-01-01

Extended common-image-point gathers (CIP) constructed by wide-azimuth TI wave-equation migration contain all the necessary information for angle decomposition as a function of the reflection and azimuth angles at selected locations in the subsurface. The reflection and azimuth angles are derived from the extended images using analytic relations between the space-lag and time-lag extensions. This post-imaging decomposition requires only information which is already available at the time of migration, i.e. the model parameters and the tilt angles of the TI medium. The transformation amounts to a linear Radon transform applied to the CIPs obtained after the application of the extended imaging condition. If information about the reflector dip is available at the CIP locations, then only two components of the space-lag vectors are required, thus reducing computational cost and increasing the affordability of the method. This efficient angle decomposition method is suitable for wide-azimuth imaging in anisotropic media with arbitrary orientation of the symmetry plane. © 2011 Society of Exploration Geophysicists.

Steel research using neutron beam techniques. In-situ neutron diffraction, small-angle neutron scattering and residual stress analysis

International Nuclear Information System (INIS)

Sueyoshi, Hitoshi; Ishikawa, Nobuyuki; Yamada, Katsumi; Sato, Kaoru; Nakagaito, Tatsuya; Matsuda, Hiroshi; Arakaki, Yu; Tomota, Yo

2014-01-01

Recently, the neutron beam techniques have been applied for steel researches and industrial applications. In particular, the neutron diffraction is a powerful non-destructive method that can analyze phase transformation and residual stress inside the steel. The small-angle neutron scattering is also an effective method for the quantitative evaluation of microstructures inside the steel. In this study, in-situ neutron diffraction measurements during tensile test and heat treatment were conducted in order to investigate the deformation and transformation behaviors of TRIP steels. The small-angle neutron scattering measurements of TRIP steels were also conducted. Then, the neutron diffraction analysis was conducted on the high strength steel weld joint in order to investigate the effect of the residual stress distribution on the weld cracking. (author)

Application and development of non contact angle-wide viewing system in vitreous retinal surgery

Directory of Open Access Journals (Sweden)

Rong-Hua He

2016-07-01

Full Text Available Wide-angle viewing system as an important auxiliary device can clearly observe the whole fundus field of vision in vitreous surgery, which enable vitreoretinal surgery more efficient, safer and more effective. So it has very high application value in ophthalmologic operation. In this paper, we studied the development and application of wide-angle viewing system in vitreoretinal surgery in recent years, from which we summed up the advantage of non-contact wide-angle viewing system in clinical field, and pointed out the shortcomings. The ultimate goal is to make the non-contact wide-angle viewing system better applied in vitreous surgery.

Highly efficient and broadband wide-angle holography using patch-dipole nanoantenna reflectarrays.

Science.gov (United States)

Yifat, Yuval; Eitan, Michal; Iluz, Zeev; Hanein, Yael; Boag, Amir; Scheuer, Jacob

2014-05-14

We demonstrate wide-angle, broadband, and efficient reflection holography by utilizing coupled dipole-patch nanoantenna cells to impose an arbitrary phase profile on the reflected light. High-fidelity images were projected at angles of 45 and 20° with respect to the impinging light with efficiencies ranging between 40-50% over an optical bandwidth exceeding 180 nm. Excellent agreement with the theoretical predictions was found at a wide spectral range. The demonstration of such reflectarrays opens new avenues toward expanding the limits of large-angle holography.

Region of Interest Selection Interface for Wide-Angle Arthroscope

Directory of Open Access Journals (Sweden)

Jung Kyunghwa

2015-01-01

Full Text Available We have proposed a new interface for an wide-angle endoscope for solo surgery. The wide-angle arthroscopic view and magnified region of interest (ROI within the wide view were shown simultaneously. With a camera affixed to surgical instruments, the position of the ROI could be determined by manipulating the surgical instrument. Image features acquired by the A-KAZE approach were used to estimate the change of position of the surgical instrument by tracking the features every time the camera moved. We examined the accuracy of ROI selection using three different images, which were different-sized square arrays and tested phantom experiments. When the number of ROIs was twelve, the success rate was best, and the rate diminished as the size of ROIs decreased. The experimental results showed that the method of using a camera without additional sensors satisfied the appropriate accuracy required for ROI selection, and this interface was helpful in performing surgery with fewer assistants.

Electromagnetic Power Harvester Using Wide-Angle and Polarization-Insensitive Metasurfaces

Directory of Open Access Journals (Sweden)

Xuanming Zhang

2018-03-01

Full Text Available A new wide-angle and polarization-insensitive metasurface (MS instead of traditional antenna is built as the primary ambient energy harvester in this paper. The MS is a two-dimensional energy harvesting array that is composed of subwavelength electrical small ring resonator that is working at 2.5 GHz (LTE/WiFi. In the case of different polarization and incidence angles, we demonstrate the metasurface can achieve high harvesting efficiency of 90%. The fabricated prototype of 9 × 9 MS energy harvesting array is measured, and the experimental results validate that the proposed MS has a good performance more than 80% of energy harvesting efficiency for arbitrary polarization and wide-angle incident waves. The good agreement of the simulation with the experiment results verifies the practicability and effectiveness of the proposed MS structure, which will provide a new source of supply in wireless sensor networks (WSN.

Influence of multiple small-angle neutron scattering on diffraction peak broadening in ferritic steel

Czech Academy of Sciences Publication Activity Database

Woo, W.; Em, V.; Shin, E.; Mikula, Pavol; Ryukhtin, Vasyl

2015-01-01

Roč. 48, APR (2015), s. 350-356 ISSN 0021-8898 R&D Projects: GA ČR GB14-36566G; GA MŠk(CZ) LM2011019 Institutional support: RVO:61389005 Keywords : peak broadening * small-angle neutron scattering * neutron diffraction * magnetic domain Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 3.720, year: 2014

Investigations of time resolved x-ray wide-angle scattering and x-ray small-angle scattering at DESY

International Nuclear Information System (INIS)

Zachmann, H.G.; Gehrke, R.; Prieske, W.; Riekel, C.

1985-01-01

Instrumentation is described for the simultaneous wide-angle and small-angle x-ray scattering. The method was applied to the study of the isothermal crystallization of polyethylene terephthalates. In agreement with the classical theories of crystallization, the data showed that the density difference between the crystals and the non-crystalline regions does not change with time. The mechanisms of melting, recrystallization, and crystal thickening were investigated by small-angle x-ray scattering with stepwise changes and continuous changes of temperature using polyethylene terephthalate

Wide angle spectrometers for intermadiate energy electron accelerators

International Nuclear Information System (INIS)

Leconte, P.

1982-10-01

It is shown that improvements of the detector acceptances (in solid angle and momentum bite) is as important as increased duty cycle for coincidence experiments. To have a maximum efficiency and thus to reduce the cost of experiments, it is imperative to develop maximum solid angle systems. This implies an axial symmetry with respect to the incoming beam. At Saclay, we have investigated some of the properties of specific detectors covering up to 90% of 4π steradians for a high energy, 100% duty cycle electron accelerator. The techniques of wide angle spectrometers have already been explored on a large scale in high energy physics. However, in the case of charged particles, such detectors, compared to classical iron dipole spectrometers, present a smaller resolving power and a rather low background rejection. The choice of which of these two solutions is to be used depends on the conditions of the specific experiment

A high resolution position sensitive X-ray MWPC for small angle X-ray diffraction

International Nuclear Information System (INIS)

Bateman, J.E.; Connolly, J.F.; Stephenson, R.; Tappern, G.J.

1981-02-01

A small sealed-off delay line readout MWPC X-ray detector has been designed and built for small angle X-ray diffraction applications. Featuring a sensitive area of 100 mm x 25 mm it yields a spatial resolution of 0.13 mm (standard deviation) with a high rate capability and good quantum efficiency for copper K radiation. (author)

Two wide-angle imaging neutral-atom spectrometers

Energy Technology Data Exchange (ETDEWEB)

McComas, D.J.

1997-12-31

The Two Wide-angle Imaging Neutral-atom Spectrometers (TWINS) mission provides a new capability for stereoscopically imaging the magnetosphere. By imaging the charge exchange neutral atoms over a broad energy range (1 < E , {approximately} 100 keV) using two identical instruments on two widely-spaced high-altitude, high-inclination spacecraft, TWINS will enable the 3-dimensional visualization and the resolution of large scale structures and dynamics within the magnetosphere for the first time. These observations will provide a leap ahead in the understanding of the global aspects of the terrestrial magnetosphere and directly address a number of critical issues in the ``Sun-Earth Connections`` science theme of the NASA Office of Space Science.

Two wide-angle imaging neutral-atom spectrometers

International Nuclear Information System (INIS)

McComas, D.J.

1997-01-01

The Two Wide-angle Imaging Neutral-atom Spectrometers (TWINS) mission provides a new capability for stereoscopically imaging the magnetosphere. By imaging the charge exchange neutral atoms over a broad energy range (1 < E , ∼ 100 keV) using two identical instruments on two widely-spaced high-altitude, high-inclination spacecraft, TWINS will enable the 3-dimensional visualization and the resolution of large scale structures and dynamics within the magnetosphere for the first time. These observations will provide a leap ahead in the understanding of the global aspects of the terrestrial magnetosphere and directly address a number of critical issues in the ''Sun-Earth Connections'' science theme of the NASA Office of Space Science

The structure of formate on TiO{sub 2}(110) by scanned-energy and scanned-angle photoelectron diffraction

Energy Technology Data Exchange (ETDEWEB)

Thevuthasan, S.; Kim, Y.J.; Herman, G.S. [Pacific Northwest National Laboratory, Richland, WA (United States)] [and others

1997-04-01

There is a considerable interest in understanding the interaction of small organic molecules with oxide surfaces. The chemistry of formate interactions with TiO{sub 2}(110) has been investigated by several groups, but there is little information on the structure of the adsorbate/surface complex. Recently the authors combined high-energy x-ray photoelectron diffraction (XPD) measurements at PNNL with low-energy scanned-angle and scanned-energy photoelectron diffraction measurements at the ALS to investigate the structure of the formate ion on TiO{sub 2}(110) in detail. The high-energy XPD results reveal that formate binds through the oxygens in a bidentate fashion to Ti cation rows along the [001] direction with an O-C-O bond angle of about 126{degrees}. Low-energy photoelectron diffraction data, which is briefly described below, was used to identify the specific bonding geometry, including the bond length between the Ti cation and the oxygen in the formate.

Hybrid wide-angle viewing-endoscopic vitrectomy using a 3D visualization system

Directory of Open Access Journals (Sweden)

Kita M

2018-02-01

Full Text Available Mihori Kita, Yuki Mori, Sachiyo Hama Department of Ophthalmology, National Organization Kyoto Medical Center, Kyoto, Japan Purpose: To introduce a hybrid wide-angle viewing-endoscopic vitrectomy, which we have reported, using a 3D visualization system developed recently. Subjects and methods: We report a single center, retrospective, consecutive surgical case series of 113 eyes that underwent 25 G vitrectomy (rhegmatogenous retinal detachment or proliferative vitreoretinopathy, 49 eyes; epiretinal membrane, 18 eyes; proliferative diabetic retinopathy, 17 eyes; vitreous opacity or vitreous hemorrhage, 11 eyes; macular hole, 11 eyes; vitreomacular traction syndrome, 4 eyes; and luxation of intraocular lens, 3 eyes. Results: This system was successfully used to perform hybrid vitrectomy in the difficult cases, such as proliferative vitreoretinopathy and proliferative diabetic retinopathy. Conclusion: Hybrid wide-angle viewing-endoscopic vitrectomy using a 3D visualization system appears to be a valuable and promising method for managing various types of vitreoretinal disease. Keywords: 25 G vitrectomy, endoscope, wide-angle viewing system, 3D visualization system, hybrid

A three-dimensional wide-angle BPM for optical waveguide structures

Science.gov (United States)

Ma, Changbao; van Keuren, Edward

2007-01-01

Algorithms for effective modeling of optical propagation in three- dimensional waveguide structures are critical for the design of photonic devices. We present a three-dimensional (3-D) wide-angle beam propagation method (WA-BPM) using Hoekstra’s scheme. A sparse matrix algebraic equation is formed and solved using iterative methods. The applicability, accuracy and effectiveness of our method are demonstrated by applying it to simulations of wide-angle beam propagation, along with a technique for shifting the simulation window to reduce the dimension of the numerical equation and a threshold technique to further ensure its convergence. These techniques can ensure the implementation of iterative methods for waveguide structures by relaxing the convergence problem, which will further enable us to develop higher-order 3-D WA-BPMs based on Padé approximant operators.

Diamagneto-Dielectric Anisotropic Wide Angle Impedance Matching Layers for Active Phased Arrays

NARCIS (Netherlands)

Silvestri, F.; Cifola, L.; Gerini, G.

2016-01-01

In this paper, we present the full process of designing anisotropic metamaterial (MM) wide angle impedance matching (WAIM) layers. These layers are used to reduce the scan losses that occur in active phased arrays for large scanning angles. Numerical results are provided to show the improvement in

Diamagneto-dielectric anisotropic wide angle impedance matching layers for active phased arrays

NARCIS (Netherlands)

Silvestri, F.; Cifola, L.; Gerini, G.

2016-01-01

In this paper we present the full process of designing anisotropic metamaterial (MM) wide angle impedance matching (WAIM) layers. These layers are used to reduce the scan losses that occur in active phased arrays for large scanning angles. Numerical results are provided to show the improvement in

Effect of substrate material selection on polychromatic integral diffraction efficiency for multilayer diffractive optics in oblique incident situation

Science.gov (United States)

Zhang, Bo; Cui, Qingfeng; Piao, Mingxu

2018-05-01

The effect of substrate material selection for multilayer diffractive optical elements (MLDOEs) on polychromatic integral diffraction efficiency (PIDE) is studied in the oblique incident situation. A mathematical model of substrate material selection is proposed to obtain the high PIDE with large incident angle. The extended expression of the microstructure heights with consideration of incident angle is deduced to calculate the PIDE difference Δ η bar(λ) for different substrate material combinations. The smaller value of Δ η bar(λ) indicates the more optimal substrate material combination in a wide incident angle range. Based on the deduced mathematical model, different MLDOEs are analyzed in visible and infrared wavebands. The results show that the three-layer DOEs can be applied in larger incident angle situation than the double-layer DOEs in visible waveband. When the two substrate materials are the same, polycarbonate (PC) is more reasonable than poly(methyl methacrylate) (PMMA) as the middle filling optical material for the three-layer DOEs. In the infrared waveband, the PIDE decreases in the LWIR are obviously smaller than that in the MWIR for the same substrate material combination, and the PIDE cannot be calculated when the incident angle larger than critical angle. The analysis results can be used to guide the hybrid optical system design with MLDOEs.

Graded index and randomly oriented core-shell silicon nanowires for broadband and wide angle antireflection

Directory of Open Access Journals (Sweden)

P. Pignalosa

2011-09-01

Full Text Available Antireflection with broadband and wide angle properties is important for a wide range of applications on photovoltaic cells and display. The SiOx shell layer provides a natural antireflection from air to the Si core absorption layer. In this work, we have demonstrated the random core-shell silicon nanowires with both broadband (from 400nm to 900nm and wide angle (from normal incidence to 60º antireflection characteristics within AM1.5 solar spectrum. The graded index structure from the randomly oriented core-shell (Air/SiOx/Si nanowires may provide a potential avenue to realize a broadband and wide angle antireflection layer.

Wide-angle full-vector beam propagation method based on an alternating direction implicit preconditioner

Science.gov (United States)

Chui, Siu Lit; Lu, Ya Yan

2004-03-01

Wide-angle full-vector beam propagation methods (BPMs) for three-dimensional wave-guiding structures can be derived on the basis of rational approximants of a square root operator or its exponential (i.e., the one-way propagator). While the less accurate BPM based on the slowly varying envelope approximation can be efficiently solved by the alternating direction implicit (ADI) method, the wide-angle variants involve linear systems that are more difficult to handle. We present an efficient solver for these linear systems that is based on a Krylov subspace method with an ADI preconditioner. The resulting wide-angle full-vector BPM is used to simulate the propagation of wave fields in a Y branch and a taper.

Processing two-dimensional X-ray diffraction and small-angle scattering data in DAWN 2.

Science.gov (United States)

Filik, J; Ashton, A W; Chang, P C Y; Chater, P A; Day, S J; Drakopoulos, M; Gerring, M W; Hart, M L; Magdysyuk, O V; Michalik, S; Smith, A; Tang, C C; Terrill, N J; Wharmby, M T; Wilhelm, H

2017-06-01

A software package for the calibration and processing of powder X-ray diffraction and small-angle X-ray scattering data is presented. It provides a multitude of data processing and visualization tools as well as a command-line scripting interface for on-the-fly processing and the incorporation of complex data treatment tasks. Customizable processing chains permit the execution of many data processing steps to convert a single image or a batch of raw two-dimensional data into meaningful data and one-dimensional diffractograms. The processed data files contain the full data provenance of each process applied to the data. The calibration routines can run automatically even for high energies and also for large detector tilt angles. Some of the functionalities are highlighted by specific use cases.

Metasurface Enabled Wide-Angle Fourier Lens.

Science.gov (United States)

Liu, Wenwei; Li, Zhancheng; Cheng, Hua; Tang, Chengchun; Li, Junjie; Zhang, Shuang; Chen, Shuqi; Tian, Jianguo

2018-06-01

Fourier optics, the principle of using Fourier transformation to understand the functionalities of optical elements, lies at the heart of modern optics, and it has been widely applied to optical information processing, imaging, holography, etc. While a simple thin lens is capable of resolving Fourier components of an arbitrary optical wavefront, its operation is limited to near normal light incidence, i.e., the paraxial approximation, which puts a severe constraint on the resolvable Fourier domain. As a result, high-order Fourier components are lost, resulting in extinction of high-resolution information of an image. Other high numerical aperture Fourier lenses usually suffer from the bulky size and costly designs. Here, a dielectric metasurface consisting of high-aspect-ratio silicon waveguide array is demonstrated experimentally, which is capable of performing 1D Fourier transform for a large incident angle range and a broad operating bandwidth. Thus, the device significantly expands the operational Fourier space, benefitting from the large numerical aperture and negligible angular dispersion at large incident angles. The Fourier metasurface will not only facilitate efficient manipulation of spatial spectrum of free-space optical wavefront, but also be readily integrated into micro-optical platforms due to its compact size. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Recent advancements of wide-angle polarization analysis with 3He neutron spin filters

International Nuclear Information System (INIS)

Chen, W.C.; Gentile, T.R.; Ye, Q.; Kirchhoff, A.; Watson, S.M.; Rodriguez-Rivera, J.A.; Qiu, Y.; Broholm, C.

2016-01-01

Wide-angle polarization analysis with polarized 3 He based neutron spin filters (NSFs) has recently been employed on the Multi-Axis Crystal Spectrometer (MACS) at the National Institute of Standards and Technology Center for Neutron Research (NCNR). Over the past several years, the apparatus has undergone many upgrades to address the fundamental requirements for wide angle polarization analysis using spin exchange optical pumping based 3 He NSFs. In this paper, we report substantial improvements in the on-beam-line performance of the apparatus and progress toward routine user capability. We discuss new standard samples used for 3 He NSF characterization and the flipping ratio measurement on MACS. We further discuss the management of stray magnetic fields produced by operation of superconducting magnets on the MACS instrument, which can significantly reduce the 3 He polarization relaxation time. Finally, we present the results of recent development of horseshoe-shaped wide angle cells. (paper)

Wide-azimuth angle gathers for anisotropic wave-equation migration

KAUST Repository

Sava, Paul C.

2012-10-15

Extended common-image-point gathers (CIP) constructed by wide-azimuth TI wave-equation migration contain all the necessary information for angle decomposition as a function of the reflection and azimuth angles at selected locations in the subsurface. The aperture and azimuth angles are derived from the extended images using analytic relations between the space- and time-lag extensions using information which is already available at the time of migration, i.e. the anisotropic model parameters. CIPs are cheap to compute because they can be distributed in the image at the most relevant positions, as indicated by the geologic structure. If the reflector dip is known at the CIP locations, then the computational cost can be reduced by evaluating only two components of the space-lag vector. The transformation from extended images to angle gathers is a planar Radon transform which depends on the local medium parameters. This transformation allows us to separate all illumination directions for a given experiment, or between different experiments. We do not need to decompose the reconstructed wavefields or to choose the most energetic directions for decomposition. Applications of the method include illumination studies in complex areas where ray-based methods fail, and assuming that the subsurface illumination is sufficiently dense, the study of amplitude variation with aperture and azimuth angles. © 2012 European Association of Geoscientists & Engineers.

Wide-azimuth angle gathers for anisotropic wave-equation migration

KAUST Repository

Sava, Paul C.; Alkhalifah, Tariq Ali

2012-01-01

Extended common-image-point gathers (CIP) constructed by wide-azimuth TI wave-equation migration contain all the necessary information for angle decomposition as a function of the reflection and azimuth angles at selected locations in the subsurface. The aperture and azimuth angles are derived from the extended images using analytic relations between the space- and time-lag extensions using information which is already available at the time of migration, i.e. the anisotropic model parameters. CIPs are cheap to compute because they can be distributed in the image at the most relevant positions, as indicated by the geologic structure. If the reflector dip is known at the CIP locations, then the computational cost can be reduced by evaluating only two components of the space-lag vector. The transformation from extended images to angle gathers is a planar Radon transform which depends on the local medium parameters. This transformation allows us to separate all illumination directions for a given experiment, or between different experiments. We do not need to decompose the reconstructed wavefields or to choose the most energetic directions for decomposition. Applications of the method include illumination studies in complex areas where ray-based methods fail, and assuming that the subsurface illumination is sufficiently dense, the study of amplitude variation with aperture and azimuth angles. © 2012 European Association of Geoscientists & Engineers.

Asymmetric-cut variable-incident-angle monochromator.

Science.gov (United States)

Smither, R K; Graber, T J; Fernandez, P B; Mills, D M

2012-03-01

A novel asymmetric-cut variable-incident-angle monochromator was constructed and tested in 1997 at the Advanced Photon Source of Argonne National Laboratory. The monochromator was originally designed as a high heat load monochromator capable of handling 5-10 kW beams from a wiggler source. This was accomplished by spreading the x-ray beam out on the surface an asymmetric-cut crystal and by using liquid metal cooling of the first crystal. The monochromator turned out to be a highly versatile monochromator that could perform many different types of experiments. The monochromator consisted of two 18° asymmetrically cut Si crystals that could be rotated about 3 independent axes. The first stage (Φ) rotates the crystal around an axis perpendicular to the diffraction plane. This rotation changes the angle of the incident beam with the surface of the crystal without changing the Bragg angle. The second rotation (Ψ) is perpendicular to the first and is used to control the shape of the beam footprint on the crystal. The third rotation (Θ) controls the Bragg angle. Besides the high heat load application, the use of asymmetrically cut crystals allows one to increase or decrease the acceptance angle for crystal diffraction of a monochromatic x-ray beam and allows one to increase or decrease the wavelength bandwidth of the diffraction of a continuum source like a bending-magnet beam or a normal x-ray-tube source. When the monochromator is used in the doubly expanding mode, it is possible to expand the vertical size of the double-diffracted beam by a factor of 10-15. When this was combined with a bending magnet source, it was possible to generate an 8 keV area beam, 16 mm wide by 26 mm high with a uniform intensity and parallel to 1.2 arc sec that could be applied in imaging experiments.

Foucault imaging and small-angle electron diffraction in controlled external magnetic fields.

Science.gov (United States)

Nakajima, Hiroshi; Kotani, Atsuhiro; Harada, Ken; Ishii, Yui; Mori, Shigeo

2016-12-01

We report a method for acquiring Foucault images and small-angle electron diffraction patterns in external magnetic fields using a conventional transmission electron microscope without any modification. In the electron optical system that we have constructed, external magnetic fields parallel to the optical axis can be controlled using the objective lens pole piece under weak excitation conditions in the Foucault mode and the diffraction mode. We observe two ferromagnetic perovskite-type manganese oxides, La 0.7 Sr 0.3 MnO 3 (LSMO) and Nd 0.5 Sr 0.5 MnO 3 , in order to visualize magnetic domains and their magnetic responses to external magnetic fields. In rhombohedral-structured LSMO, pinning of magnetic domain walls at crystallographic twin boundaries was found to have a strong influence on the generation of new magnetic domains in external applied magnetic fields. © The Author 2016. Published by Oxford University Press on behalf of The Japanese Society of Microscopy. All rights reserved. For permissions, please e-mail: journals.permissions@oup.com.

Proton diffraction

International Nuclear Information System (INIS)

Den Besten, J.L.; Jamieson, D.N.; Allen, L.J.

1998-01-01

The Lindhard theory on ion channeling in crystals has been widely accepted throughout ion beam analysis for use in simulating such experiments. The simulations use a Monte Carlo method developed by Barret, which utilises the classical 'billiard ball' theory of ions 'bouncing' between planes or tubes of atoms in the crystal. This theory is not valid for 'thin' crystals where the planes or strings of atoms can no longer be assumed to be of infinite proportions. We propose that a theory similar to that used for high energy electron diffraction can be applied to MeV ions, especially protons, in thin crystals to simulate the intensities of transmission channeling and of RBS spectra. The diffraction theory is based on a Bloch wave solution of the Schroedinger equation for an ion passing through the periodic crystal potential. The widely used universal potential for proton-nucleus scattering is used to construct the crystal potential. Absorption due to thermal diffuse scattering is included. Experimental parameters such as convergence angle, beam tilt and scanning directions are considered in our calculations. Comparison between theory and experiment is encouraging and suggests that further work is justified. (authors)

Study on the wide-angle Michelson interferometer with large air gap.

Science.gov (United States)

Gao, Haiyang; Tang, Yuanhe; Hua, Dengxin; Liu, Hanchen

2011-10-10

A wide-angle Michelson interferometer with large air gap is proposed to effectively reduce the size of the glass arms and constraint on material. It provides a novel and practical instrument for ground based wind measurement of the upper atmosphere. The field widening conditions for the large air gap are calculated in theory. For the five spectral lines of 557.7 nm, 630.0 nm, 732.0 nm, 834.6 nm, and 865.7 nm, the optimal results under ideal condition are obtained with air gaps of 1.0 cm, 1.5 cm, and 2.0 cm, respectively. With the fixed optical path difference (OPD) of 7.495 cm, three pairs of glass arms are optimized. The pair with length of 1.5 cm for air gap, 5.765 cm for H-ZF12, and 2.956 cm for H-ZLaF54, has better effect of field widening than the other two pairs and its OPD variation is only within 0.30 wavelengths at incident angle of 3°. For developing a more practical wide-angle Michelson interferometer, the H-K9L glass with size of 4.445 cm is employed as the arm material of solid interferometer. The experiment for field of view of 3° is designed and the data processing and analysis for 60 images show the agreement between experimental results and theoretical simulation. The OPD variations are only within 0.27 wavelengths for image edge. The feasibility and practicality of the wide-angle Michelson interferometer with large air gap is proved by means of theory and experiment. © 2011 Optical Society of America

Note: An X-ray powder diffractometer with a wide scattering-angle range of 72° using asymmetrically positioned one-dimensional detectors

Energy Technology Data Exchange (ETDEWEB)

Katsuya, Yoshio; Tanaka, Masahiko [Synchrotron X-ray Station at SPring-8, National Institute for Materials Science (NIMS), 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan); Song, Chulho [Synchrotron X-ray Station at SPring-8, National Institute for Materials Science (NIMS), 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan); Global Research Center for Environment and Energy based Nanomaterials Science (GREEN), Lithium Air Battery Specially Promoted Research Team, NIMS, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan); Ito, Kimihiko; Kubo, Yoshimi [Global Research Center for Environment and Energy based Nanomaterials Science (GREEN), Lithium Air Battery Specially Promoted Research Team, NIMS, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan); Sakata, Osami, E-mail: SAKATA.Osami@nims.go.jp [Synchrotron X-ray Station at SPring-8, National Institute for Materials Science (NIMS), 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan); Global Research Center for Environment and Energy based Nanomaterials Science (GREEN), Lithium Air Battery Specially Promoted Research Team, NIMS, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan); Synchrotron X-ray Group, Quantum Beam Unit, NIMS, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan)

2016-01-15

An X-ray powder diffractometer has been developed for a time-resolved measurement without the requirement of a scattering angle (2θ) scan. Six one-dimensional detector modules are asymmetrically arranged in a vertical line at a designed distance of 286.5 mm. A detector module actually covers a diffraction angle of about 12° with an angular resolution of 0.01°. A diffracted intensity pattern is simultaneously recorded in a 2θ angular range from 1.63° to 74.37° in a “one shot” measurement. We tested the performance of the diffractometer with reference CeO{sub 2} powders and demonstrated diffraction measurements from an operating lithium-air battery.

Nondestructive hydrogen analysis of steam-oxidized Zircaloy-4 by wide-angle neutron scattering

Science.gov (United States)

Yan, Yong; Qian, Shuo; Garrison, Ben; Smith, Tyler; Kim, Peter

2018-04-01

A nondestructive neutron scattering method to precisely measure the hydrogen content in high-temperature steam-oxidized Zircaloy-4 cladding was developed. Zircaloy-4 cladding was used to produce hydrided specimens with hydrogen content up to ≈500 wppm. Following hydrogen charging, the hydrogen content of the hydrided specimens was measured using the vacuum hot extraction method, by which the samples with desired hydrogen concentrations were selected for the neutron study. The hydrided samples were then oxidized in steam up to ≈6.0 wt. % at 1100 °C. Optical microscopy shows that our hydriding procedure results in uniform distribution of circumferential hydrides across the wall thickness, and uniform oxide layers were formed on the sample surfaces by the steam oxidation. Small- and wide-angle neutron scattering were simultaneously performed to provide a quick (less than an hour per sample) measurement of the hydrogen content in various types of hydrided and oxidized Zircaloy-4. Our study demonstrates that the hydrogen in pre-oxidized Zircaloy-4 cladding can be measured very accurately by both small- and wide-angle neutron scattering. For steam-oxidized samples, the small-angle neutron scattering is contaminated with coherent scattering from additional structural features induced by the steam oxidation. However, the scattering intensity of the wide-angle neutron scattering increases proportionally with the hydrogen charged in the samples. The hydrogen content and wide-angle neutron scattering intensity are highly linearly correlated for the oxidized cladding samples examined in this work, and can be used to precisely determine the hydrogen content in steam-oxidized Zircaloy-4 samples. Hydrogen contents determined by neutron scattering of oxidation samples were also found to be consistent with the results of chemical analysis within acceptable margins for error.

Dielectric-based subwavelength metallic meanders for wide-angle band absorbers.

Science.gov (United States)

Shen, Su; Qiao, Wen; Ye, Yan; Zhou, Yun; Chen, Linsen

2015-01-26

We propose nano-meanders that can achieve wide-angle band absorption in visible regime. The nano-meander consists of a subwavelength dielectric grating covered by continuous ultra-thin Aluminum film (less than one tenth of the incident wavelength). The excited photonic resonant modes, such as cavity mode, surface plasmonic mode and Rayleigh-Wood anomaly, are discussed in detail. Nearly total resonant absorption due to funneling mechanism in the air nano-groove is almost invariant with large incident angle in transverse magnetic polarization. From both the structural geometry and the nanofabrication point of view, the light absorber has a very simple geometrical structure and it is easy to be integrated into complex photonic devices. The highly efficient angle-robust light absorber can be potential candidate for a range of passive and active photonic applications, including solar-energy harvesting as well as producing artificial colors on a large scale substrate.

A Microbeam Small-Angle X-ray Scattering Study on Enamel Crystallites in Subsurface Lesion

Energy Technology Data Exchange (ETDEWEB)

Yagi, N; Ohta, N; Matsuo, T [Japan Synchrotron Radiation Research Institute, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan); Tanaka, T; Terada, Y; Kamasaka, H; Kometani, T, E-mail: yagi@spring8.or.j [Ezaki Glico Co. Ltd., 4-6-5 Utajima, Nishiyodogawa-ku, Osaka 555-8502 (Japan)

2010-10-01

The early caries lesion in bovine tooth enamel was studied by two different X-ray diffraction systems at the SPring-8 third generation synchrotron radiation facility. Both allowed us simultaneous measurement of the small and large angle regions. The beam size was 6{mu}m at BL40XU and 50{mu}m at BL45XU. The small-angle scattering from voids in the hydroxyapatite crystallites and the wide-angle diffraction from the hydroxyapatite crystals were observed simultaneously. At BL40XU an X-ray image intensifier was used for the small-angle and a CMOS flatpanel detector for the large-angle region. At BL45XU, a large-area CCD detector was used to cover both regions. A linear microbeam scan at BL40XU showed a detailed distribution of voids and crystals and made it possible to examine the structural details in the lesion. The two-dimensional scan at BL45XU showed distribution of voids and crystals in a wider region in the enamel. The simultaneous small- and wide-angle measurement with a microbeam is a powerful tool to elucidate the mechanisms of demineralization and remineralization in the early caries lesion.

A Microbeam Small-Angle X-ray Scattering Study on Enamel Crystallites in Subsurface Lesion

International Nuclear Information System (INIS)

Yagi, N; Ohta, N; Matsuo, T; Tanaka, T; Terada, Y; Kamasaka, H; Kometani, T

2010-01-01

The early caries lesion in bovine tooth enamel was studied by two different X-ray diffraction systems at the SPring-8 third generation synchrotron radiation facility. Both allowed us simultaneous measurement of the small and large angle regions. The beam size was 6μm at BL40XU and 50μm at BL45XU. The small-angle scattering from voids in the hydroxyapatite crystallites and the wide-angle diffraction from the hydroxyapatite crystals were observed simultaneously. At BL40XU an X-ray image intensifier was used for the small-angle and a CMOS flatpanel detector for the large-angle region. At BL45XU, a large-area CCD detector was used to cover both regions. A linear microbeam scan at BL40XU showed a detailed distribution of voids and crystals and made it possible to examine the structural details in the lesion. The two-dimensional scan at BL45XU showed distribution of voids and crystals in a wider region in the enamel. The simultaneous small- and wide-angle measurement with a microbeam is a powerful tool to elucidate the mechanisms of demineralization and remineralization in the early caries lesion.

Wide-angle, polarization-insensitive and broadband absorber based on eight-fold symmetric SRRs metamaterial

Science.gov (United States)

Wu, Dong; Liu, Yumin; Yu, Zhongyuan; Chen, Lei; Ma, Rui; Li, Yutong; Li, Ruifang; Ye, Han

2016-12-01

In this paper, we propose a novel three dimensional metamaterial design with eight-fold rotational symmetry that shows a polarization-insensitive, wide-angle and broadband perfect absorption in the microwave band. By simulation, the polarization-insensitive absorption is over 90% between 26.9 GHz to 32.9 GHz, and the broadband absorption remains a good absorption performance to a wide incident angles for both TE and TM polarizations. The magnetic field distribution are investigated to interpret the physical mechanism of broadband absorption. The broadband absorption is based on overlapping the multiple magnetic resonances at the neighboring frequencies by coupling effects of multiple metallic split-ring resonators (SRRs). Moreover, it is demonstrate that the designed structure can be extended to other frequencies by scale down the size of the unit cell, such as the visible frequencies. The simulated results show that the absorption of the smaller absorber is above 90% in the frequency range from 467 THz to 765 THz(392-642 nm), which include orange to purple light in visible region(400-760nm). The wide-angle and polarization-insensitive stabilities of the smaller absorber is also demonstrated at visible region. The proposed work provides a new design of realization of a polarization-insensitive, wide-angle and broadband absorber ranging different frequency bands, and such a structure has potential application in the fields of solar cell, imaging and detection.

Glancing angle synchrotron X-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Cernik, R J [Daresbury Lab., Warrington, WA (United States)

1996-09-01

This paper describes in basic detail some of the techniques that can be used to study thin films and surfaces. These are all in the X-ray region and cover reflectivity, diffraction form polycrystalline films, textured films and single crystal films. Other effects such as fluorescence and diffuse scattering are mentioned but not discussed in detail. Two examples of the reflectivity from multilayers and the diffraction from iron oxide films are discussed. The advantages of the synchrotron for these studies is stressed and the experimental geometries that can be employed are described i detail. A brief bibliography is provided at the end to accompany this part of the 1996 Frascati school.

Glancing angle synchrotron X-ray diffraction

International Nuclear Information System (INIS)

Cernik, R.J.

1996-01-01

This paper describes in basic detail some of the techniques that can be used to study thin films and surfaces. These are all in the X-ray region and cover reflectivity, diffraction form polycrystalline films, textured films and single crystal films. Other effects such as fluorescence and diffuse scattering are mentioned but not discussed in detail. Two examples of the reflectivity from multilayers and the diffraction from iron oxide films are discussed. The advantages of the synchrotron for these studies is stressed and the experimental geometries that can be employed are described i detail. A brief bibliography is provided at the end to accompany this part of the 1996 Frascati school

Wide Angle Michelson Doppler Imaging Interferometer (WAMDII)

Science.gov (United States)

Roberts, B.

1986-01-01

The wide angle Michelson Doppler imaging interferometer (WAMDII) is a specialized type of optical Michelson interferometer working at sufficiently long path difference to measure Doppler shifts and to infer Doppler line widths of naturally occurring upper atmospheric Gaussian line emissions. The instrument is intended to measure vertical profiles of atmospheric winds and temperatures within the altitude range of 85 km to 300 km. The WAMDII consists of a Michelson interferometer followed by a camera lens and an 85 x 106 charge coupled device photodiode array. Narrow band filters in a filter wheel are used to isolate individual line emissions and the lens forms an image of the emitting region on the charge coupled device array.

Stratigraphic imaging of sub-basalt sediments using waveform tomography of wide-angle seismic data

Science.gov (United States)

Sain, K.; Gao, F.; Pratt, G.; Zelt, C. A.

2003-12-01

The oil industry is interested in imaging the fine structures of sedimentary formations masked below basalt flows for commercial exploration of hydrocarbons. Seismic exploration of sediments hidden below high-velocity basalt cover is a difficult problem because near-vertical reflection data are contaminated with multiples, converted waves and scattering noise generated by interbeds, breccia and vesicles within the basalt. The noise becomes less prominent as the source-receiver offset increases, and the signals carrying sub-surface information stand out at the wide-angle range. The tomography of first arrival traveltime data can provide little information about the underlying low-velocity sediments. Traveltime inversion of wide-angle seismic data including both first arrivals and identifiable wide-angle reflected phases has been an important tool in the delineation of the large-scale velocity structure of sub-basalt sediments, although it lacks the small-scale velocity details. Here we apply 2-D full-waveform inversion ("waveform tomography") to wide-angle seismic data with a view to extracting the small-scale stratigraphic features of sedimentary formations. Results from both synthetic data, generated for a realistic earth model, and field dataset from the basalt covered Saurashtra peninsula, India, will be presented. This approach has potential to delineate thin sedimentary layers hidden below thick basalt cover also, and may serve as a powerful tool to image sedimentary basins, where they are covered by high-velocity materials like basalts, salts, carbonates, etc. in various parts of the world.

Two wide-angle imaging neutral-atom spectrometers (TWINS)

International Nuclear Information System (INIS)

McComas, D.J.; Blake, B.; Burch, J.

1998-01-01

Two Wide-angle Imaging Neutral-atom Spectrometers (TWINS) is a revolutionary new mission designed to stereoscopically image the magnetosphere in charge exchange neutral atoms for the first time. The authors propose to fly two identical TWINS instruments as a mission of opportunity on two widely-spaced high-altitude, high-inclination US Government spacecraft. Because the spacecraft are funded independently, TWINS can provide a vast quantity of high priority science observations (as identified in an ongoing new missions concept study and the Sun-Earth Connections Roadmap) at a small fraction of the cost of a dedicated mission. Because stereo observations of the near-Earth space environs will provide a particularly graphic means for visualizing the magnetosphere in action, and because of the dedication and commitment of the investigator team to the principles of carrying space science to the broader audience, TWINS will also be an outstanding tool for public education and outreach

Portable mini-chamber for temperature dependent studies using small angle and wide angle x-ray scattering

Science.gov (United States)

Dev, Arun Singh; Kumar, Dileep; Potdar, Satish; Pandit, Pallavi; Roth, Stephan V.; Gupta, Ajay

2018-04-01

The present work describes the design and performance of a vacuum compatible portable mini chamber for temperature dependent GISAXS and GIWAXS studies of thin films and multilayer structures. The water cooled body of the chamber allows sample annealing up to 900 K using ultra high vacuum compatible (UHV) pyrolytic boron nitride heater, thus making it possible to study the temperature dependent evolution of structure and morphology of two-dimensional nanostructured materials. Due to its light weight and small size, the chamber is portable and can be accommodated at synchrotron facilities worldwide. A systematic illustration of the versatility of the chamber has been demonstrated at beamline P03, PETRA-III, DESY, Hamburg, Germany. Temperature dependent grazing incidence small angle x-ray scattering (GISAXS) and grazing incidence wide angle x-ray scattering (GIWAXS) measurements were performed on oblique angle deposited Co/Ag multilayer structure, which jointly revealed that the surface diffusion in Co columns in Co/Ag multilayer enhances by increasing temperature from RT to ˜573 K. This results in a morphology change from columnar tilted structure to densely packed morphological isotropic multilayer.

Predictors of Intraocular Pressure After Phacoemulsification in Primary Open-Angle Glaucoma Eyes with Wide Versus Narrower Angles (An American Ophthalmological Society Thesis).

Science.gov (United States)

Lin, Shan C; Masis, Marisse; Porco, Travis C; Pasquale, Louis R

2017-08-01

To assess if narrower-angle status and anterior segment optical coherence tomography (AS-OCT) parameters can predict intraocular pressure (IOP) drop in primary open-angle glaucoma (POAG) patients after cataract surgery. This was a prospective case series of consecutive cataract surgery patients with POAG and no peripheral anterior synechiae (PAS) using a standardized postoperative management protocol. Preoperatively, patients underwent gonioscopy and AS-OCT. The same glaucoma medication regimen was resumed by 1 month. Potential predictors of IOP reduction included narrower-angle status by gonioscopy and angle-opening distance (AOD500) as well as other AS-OCT parameters. Mixed-effects regression adjusted for use of both eyes and other potential confounders. We enrolled 66 eyes of 40 glaucoma patients. The IOP reduction at 1 year was 4.2±3 mm Hg (26%, P gonioscopy. By AOD500 classification, the narrower-angle group had 3.4±3 mm Hg (21%, P <.001) reduction vs 2.5±3 mm Hg (16%, P <.001) in the wide-angle group ( P =.031 for difference). When the entire cohort was assessed, iris thickness, iris area, and lens vault were correlated with increasing IOP reduction at 1 year ( P <.05 for all). In POAG eyes, cataract surgery lowered IOP to a greater degree in the narrower-angle group than in the wide-angle group, and parameters relating to iris thickness and area, as well as lens vault, were correlated with IOP reduction. These findings can guide ophthalmologists in their selection of cataract surgery as a potential management option.

New developments in the simultaneous measurement system of wide-angle and small-angle x-ray scatterings and vibrational spectra for the static and dynamic analyses of the hierarchical structures of polymer solids

International Nuclear Information System (INIS)

Tashiro, Kohji; Yamamoto, Hiroko; Yoshioka, Taiyo; Ninh, Tran Hai; Shimada, Shigeru; Nakatani, Takeshi; Iwamoto, Hiroyuki; Ohta, Noboru; Masunaga, Hiroyasu

2012-01-01

A simultaneous measurement system of wide-angle X-ray diffraction (WAXD), small-angle X-ray scattering (SAXS) and Raman or transmission-type infrared spectroscopy was developed by us. Its purposes is to clarify the static and dynamic structural changes of polymer materials subjected to the various external condition changes. Some examples described here include the study of the stretch-induced reorientation phenomenon of a-axially-oriented polyethylene, the study of structural change in photo-induced solid-state polymerization reaction of muconic acid ester monomer crystal, the study of the two-stage high-temperature phase transitions of aliphatic nylons, the study of stress-induced crystalline phase transition of an oriented poly(tetramethylene terephthalate) sample and its relation to the higher-order structural change, and the study of structural regularization process of poly(L-lactic acid) in the isothermal crystallization of the meso phase. These case studies in the clarification of hierarchical structural changes of polymer materials have proven that the simultaneous measurement systems can be useful to examine the structural changes in polymer systems. (author)

Small area analysis using micro-diffraction techniques

International Nuclear Information System (INIS)

Goehner, Raymond P.; Tissot, Ralph G. Jr.; Michael, Joseph R.

2000-01-01

An overall trend toward smaller electronic packages and devices makes it increasingly important and difficult to obtain meaningful diffraction information from small areas. X-ray micro-diffraction, electron back-scattered diffraction (EBSD) and Kossel are micro-diffraction techniques used for crystallographic analysis including texture, phase identification and strain measurements. X-ray micro-diffraction primarily is used for phase analysis and residual strain measurements. X-ray micro-diffraction primarily is used for phase analysis and residual strain measurements of areas between 10 microm to 100 microm. For areas this small glass capillary optics are used for producing a usable collimated x-ray beam. These optics are designed to reflect x-rays below the critical angle therefore allowing for larger solid acceptance angle at the x-ray source resulting in brighter smaller x-ray beams. The determination of residual strain using micro-diffraction techniques is very important to the semiconductor industry. Residual stresses have caused voiding of the interconnect metal which then destroys electrical continuity. Being able to determine the residual stress helps industry to predict failures from the aging effects of interconnects due to this stress voiding. Stress measurements would be impossible using a conventional x-ray diffractometer; however, utilizing a 30 microm glass capillary these small areas are readily assessable for analysis. Kossel produces a wide angle diffraction pattern from fluorescent x-rays generated in the sample by an e-beam in a SEM. This technique can yield very precise lattice parameters for determining strain. Fig. 2 shows a Kossel pattern from a Ni specimen. Phase analysis on small areas is also possible using an energy dispersive spectrometer (EBSD) and x-ray micro-diffraction techniques. EBSD has the advantage of allowing the user to observe the area of interest using the excellent imaging capabilities of the SEM. An EDS detector has been

Wide field and diffraction limited array camera for SIRTF

International Nuclear Information System (INIS)

Fazio, G.G.; Koch, D.G.; Melnick, G.J.

1986-01-01

The Infrared Array Camera for the Space Infrared Telescope Facility (SIRTF/IRAC) is capable of two-dimensional photometry in either a wide field or diffraction-limited mode over the wavelength interval from 2 to 30 microns. Three different two-dimensional direct readout (DRO) array detectors are being considered: Band 1-InSb or Si:In (2-5 microns) 128 x 128 pixels, Band 2-Si:Ga (5-18 microns) 64 x 64 pixels, and Band 3-Si:Sb (18-30 microns) 64 x 64 pixels. The hybrid DRO readout architecture has the advantages of low read noise, random pixel access with individual readout rates, and nondestructive readout. The scientific goals of IRAC are discussed, which are the basis for several important requirements and capabilities of the array camera: (1) diffraction-limited resolution from 2-30 microns, (2) use of the maximum unvignetted field of view of SIRTF, (3) simultaneous observations within the three infrared spectral bands, and (4) the capability for broad and narrow bandwidth spectral resolution. A strategy has been developed to minimize the total electronic and environmental noise sources to satisfy the scientific requirements. 7 references

Data handling for the wide-angle hall jet experiment

International Nuclear Information System (INIS)

Cassel, D.; Engelmann, R.; Gordon, H.; Grannis, P.; Mallik, U.; Meadows, B.; Morris, T.; Plano, R.; Saulys, A.; Stein, S.

1978-01-01

The data handling needs for a jet production experiment in the wide-angle hall are discussed. The several layers of triggering and a data acquisition system were designed, the configuration of the local intersection computer system was discussed, and the time required to analyze a typical event was estimated. It was concluded that the experiment does not appear to place unrealistic demands on detector technology. The slow trigger was believed to be the crucial aspect of the experiment. 15 figures, 1 tables

Solutions on a high-speed wide-angle zoom lens with aspheric surfaces

Science.gov (United States)

Yamanashi, Takanori

2012-10-01

Recent development in CMOS and digital camera technology has accelerated the business and market share of digital cinematography. In terms of optical design, this technology has increased the need to carefully consider pixel pitch and characteristics of the imager. When the field angle at the wide end, zoom ratio, and F-number are specified, choosing an appropriate zoom lens type is crucial. In addition, appropriate power distributions and lens configurations are required. At points near the wide end of a zoom lens, it is known that an aspheric surface is an effective means to correct off-axis aberrations. On the other hand, optical designers have to focus on manufacturability of aspheric surfaces and perform required analysis with respect to the surface shape. Centration errors aside, it is also important to know the sensitivity to aspheric shape errors and their effect on image quality. In this paper, wide angle cine zoom lens design examples are introduced and their main characteristics are described. Moreover, technical challenges are pointed out and solutions are proposed.

Geostationary Coastal and Air Pollution Events (GeoCAPE) Wide Angle Spectrometer (WAS)

Science.gov (United States)

Kotecki, Carl; Chu, Martha; Mannino, Antonio; Marx, Catherine Trout; Bowers, Gregory A.; Bolognese, Jeffrey A.; Matson, Elizabeth A.; McBirney, Thomas R.; Earle, Cleland P.; Choi, Michael K.;

Design considerations for a backlight with switchable viewing angles

Science.gov (United States)

Fujieda, Ichiro; Takagi, Yoshihiko; Rahadian, Fanny

2006-08-01

Small-sized liquid crystal displays are widely used for mobile applications such as cell phones. Electronic control of a viewing angle range is desired in order to maintain privacy for viewing in public as well as to provide wide viewing angles for solitary viewing. Conventionally, a polymer-dispersed liquid crystal (PDLC) panel is inserted between a backlight and a liquid crystal panel. The PDLC layer either transmits or scatters the light from the backlight, thus providing an electronic control of viewing angles. However, such a display system is obviously thick and expensive. Here, we propose to place an electronically-controlled, light-deflecting device between an LED and a light-guide of a backlight. For example, a liquid crystal lens is investigated for other applications and its focal length is controlled electronically. A liquid crystal phase grating either transmits or diffracts an incoming light depending on whether or not a periodic phase distribution is formed inside its liquid crystal layer. A bias applied to such a device will control the angular distribution of the light propagating inside a light-guide. Output couplers built in the light-guide extract the propagating light to outside. They can be V-shaped grooves, pyramids, or any other structures that can refract, reflect or diffract light. When any of such interactions occur, the output couplers translate the changes in the propagation angles into the angular distribution of the output light. Hence the viewing-angle characteristic can be switched. The designs of the output couplers and the LC devices are important for such a backlight system.

The use of new facility by means internal balance with sting support for wide range Angle of Attack aircraft

Science.gov (United States)

Subagyo; Daryanto, Yanto; Risnawan, Novan

2018-04-01

The development of facilities for the testing of wide range angle of attack aircraft in the wind tunnel at subsonic regime has done and implemented. Development required to meet the test at an angle of attack from -20 ° to 40 °. Testing the wide range angle of attack aircraft with a wide variation of the angle of attack become important needs. This can be done simply by using the sting support-equipped by internal balance to measure the forces and moments component aerodynamics. The results of development and use on the wide range angle of attack aircraft testing are aerodynamics characteristics in the form of the coefficient three components forces and the three components of the moment. A series of test aircraft was successfully carried out and the results are shown in the form of graphs of characteristic of aerodynamics at wind speed 70 m/s.

Ultra-broadband and wide-angle perfect absorber based on composite metal-semiconductor grating

Science.gov (United States)

Li, Xu; Wang, Zongpeng; Hou, Yumin

2018-01-01

In this letter, we present an ultra-broadband and wide-angle perfect absorber based on composite Ge-Ni grating. Near perfect absorption above 90% is achieved in a wide frequency range from 150 nm to 4200 nm, which covers almost the full spectrum of solar radiation. The absorption keeps robust in a wide range of incident angle from 0º to 60º. The upper triangle Ge grating works as an antireflection coating. The lower Ni grating works as a reflector and an effective energy trapper. The guided modes inside Ge grating are excited due to reflection of the lower Ni grating surface. In longer wavelength band, gap surface plasmons (GSPs) in the Ni grating are excited and couple with the guided modes inside the Ge grating. The coupled modes extend the perfect absorption band to the near-infrared region (150 nm-4200 nm). This design has potential application in photovoltaic devices and thermal emitters.

Wide-Angle Multistatic Synthetic Aperture Radar: Focused Image Formation and Aliasing Artifact Mitigation

National Research Council Canada - National Science Library

Luminati, Jonathan E

2005-01-01

...) imagery from a Radar Cross Section (RCS) chamber validates this approach. The second implementation problem stems from the large Doppler spread in the wide-angle scene, leading to severe aliasing problems...

Based on graphene tunable dual-band terahertz metamaterial absorber with wide-angle

Science.gov (United States)

Huang, Mulin; Cheng, Yongzhi; Cheng, Zhengze; Chen, Haoran; Mao, Xuesong; Gong, Rongzhou

2018-05-01

We present a wide-angle tunable dual-band terahertz (THz) metamaterial absorber (MMA) based on square graphene patch (SGP). This MMA is a simple periodic array, consisting of a dielectric substrate sandwiched with the SGP and a continuous metallic film. The designed MMA can achieve dual-band absorption by exciting fundamental and second higher-order resonance modes on SGP. The numerical simulations indicate that the absorption spectrum of the designed MMA is tuned from 0.85 THz to 1.01 THz, and from 2.84 THz to 3.37 THz when the chemical potential of the SGP is increasing from 0.4eV to 0.8eV. Moreover, it operates well in a wide-angle of the incident waves. The presented THz MMA based on the SGP could find some potential applications in optoelectronic related devices, such as sensor, emitter and wavelength selective radiators.

Ultrathin triple-band polarization-insensitive wide-angle compact metamaterial absorber

International Nuclear Information System (INIS)

Shang, Shuai; Yang, Shizhong; Tao, Lu; Yang, Lisheng; Cao, Hailin

2016-01-01

In this study, the design, realization, and characterization of an ultrathin triple-band polarization-insensitive wide-angle metamaterial absorber are reported. The metamaterial absorber comprises a periodic array of modified six-fold symmetric snowflake-shaped resonators with strip spiral line load, which is printed on a dielectric substrate backed by a metal ground plane. It is shown that the absorber exhibits three distinct near-unity absorption peaks, which are distributed across C, X, Ku bands, respectively. Owing to the six-fold symmetry, the absorber is insensitive to the polarization of the incident radiation. In addition, the absorber shows excellent absorption performance over wide oblique incident angles for both transverse electric and transverse magnetic polarizations. Simulated surface current and field distributions at the three absorption peaks are demonstrated to understand the absorption mechanism. Particularly, the absorption modes come from the fundamental and high-order dipole resonances. Furthermore, the experimental verification of the designed absorber is conducted, and the measured results are in reasonable agreement with the simulated ones. The proposed ultrathin (∼0.018λ 0 , λ 0 corresponding to the lowest peak absorption frequency) compact (0.168λ 0 ×0.168λ 0 corresponding to the area of a unit cell) absorber enables potential applications such as stealth technology, electromagnetic interference and spectrum identification.

Trans-palpebral illumination: an approach for wide-angle fundus photography without the need for pupil dilation

OpenAIRE

Toslak, Devrim; Thapa, Damber; Chen, Yanjun; Erol, Muhammet Kazim; Paul Chan, R. V.; Yao, Xincheng

2016-01-01

It is technically difficult to construct wide-angle fundus imaging devices due to the complexity of conventional transpupillary illumination and imaging mechanisms. We report here a new method, i.e., trans-palpebral illumination, for wide-angle fundus photography without the need for pupil dilation. By constructing a smartphone-based prototype imaging device, we demonstrated a 152° view in a single-shot image. The unique combination of low-cost smartphone design and automatic illumination opt...

HIFI - a dedicated HIgh-FIeld diffraction and spectroscopy instrument

International Nuclear Information System (INIS)

Steffens, P.; Enderle, M.; Boehm, M.; Roux, S.

2011-01-01

The outstanding scientific impact of single-crystal neutron diffraction and spectroscopy in steady state vertical magnetic fields up to 15 T (17 T without dilution fringe) is reflected in numerous high-profile publications. Magnetic fields 30 T - 35 T in vertical geometry allow to address enigmatic questions without equivalence at lower fields. The constraints implied by such magnetic fields demand a specially designed dedicated instrument. Since the vertical field geometry is crucial for single-crystal diffraction as well as spectroscopy, the solid angle of scattered neutrons is restricted, and a high-flux reactor is best suited to host a corresponding instrument. We propose a world-wide unique versatile instrument for diffraction and spectroscopy in vertical steady fields of 30 T. (authors)

Large deflection angle, high-power adaptive fiber optics collimator with preserved near-diffraction-limited beam quality.

Science.gov (United States)

Zhi, Dong; Ma, Yanxing; Chen, Zilun; Wang, Xiaolin; Zhou, Pu; Si, Lei

2016-05-15

We report on the development of a monolithic adaptive fiber optics collimator, with a large deflection angle and preserved near-diffraction-limited beam quality, that has been tested at a maximal output power at the 300 W level. Additionally, a new measurement method of beam quality (M2 factor) is developed. Experimental results show that the deflection angle of the collimated beam is in the range of 0-0.27 mrad in the X direction and 0-0.19 mrad in the Y direction. The effective working frequency of the device is about 710 Hz. By employing the new measurement method of the M2 factor, we calculate that the beam quality is Mx2=1.35 and My2=1.24, which is in agreement with the result from the beam propagation analyzer and is preserved well with the increasing output power.

Random Combinatorial Gradient Metasurface for Broadband, Wide-Angle and Polarization-Independent Diffusion Scattering.

Science.gov (United States)

Zhuang, Yaqiang; Wang, Guangming; Liang, Jiangang; Cai, Tong; Tang, Xiao-Lan; Guo, Tongfeng; Zhang, Qingfeng

2017-11-29

This paper proposes an easy, efficient strategy for designing broadband, wide-angle and polarization-independent diffusion metasurface for radar cross section (RCS) reduction. A dual-resonance unit cell, composed of a cross wire and cross loop (CWCL), is employed to enhance the phase bandwidth covering the 2π range. Both oblique-gradient and horizontal-gradient phase supercells are designed for illustration. The numerical results agree well with the theoretical ones. To significantly reduce backward scattering, the random combinatorial gradient metasurface (RCGM) is subsequently constructed by collecting eight supercells with randomly distributed gradient directions. The proposed metasurface features an enhanced specular RCS reduction performance and less design complexity compared to other candidates. Both simulated and measured results show that the proposed RCGM can significantly suppress RCS and exhibits broadband, wide-angle and polarization independence features.

Borehole radar diffraction tomography

Energy Technology Data Exchange (ETDEWEB)

Cho, Seong Jun; Kim, Jung Ho; Yi, Myeong Jong; Chung, Seung Hwan; Lee, Hee Il [Korea Institute of Geology Mining and Materials, Taejon (Korea, Republic of)

1997-12-01

Tomography is widely used as imaging method for determining subsurface structure. Among the reconstruction algorithms for tomographic imaging, travel time tomography is almost applied to imaging subsurface. But isolated small body comparable with the wavelength could not be well recognized by travel time tomography. Other tomographic method are need to improve the imaging process. In the study of this year, diffraction tomography was investigated. The theory for diffraction tomography is based on the 1st-order Born approximation. Multisource holography, which is similar to Kirchihoff migration, is compared with diffraction tomography. To improve 1st-order Born diffraction tomography, two kinds of filter designed from multisource holography and 2-D green function, respectively, applied on the reconstructed image. The algorithm was tested for the numerical modeling data of which algorithm consists of the analytic computation of radar signal in transmitter and receiver regions and 2-D FDM scheme for the propagation of electromagnetic waves in media. The air-filled cavity model to show a typical diffraction pattern was applied to diffraction tomography imaging, and the result shows accurate location and area of cavity. But the calculated object function is not well matched the real object function, because the air-filled cavity model is not satisfied week scattered inhomogeneity for 1st born approximation, and the error term is included in estimating source wavelet from received signals. In spite of the object function error, the diffraction tomography assist for interpretation of subsurface as if conducted with travel time tomography. And the fracture model was tested, 1st born diffraction tomographic image is poor because of limited view angle coverage and violation of week scatter assumption, but the filtered image resolve the fracture somewhat better. The tested diffraction tomography image confirms effectiveness of filter for enhancing resolution. (author). 14

Difference structures from time-resolved small-angle and wide-angle x-ray scattering

Science.gov (United States)

Nepal, Prakash; Saldin, D. K.

2018-05-01

Time-resolved small-angle x-ray scattering/wide-angle x-ray scattering (SAXS/WAXS) is capable of recovering difference structures directly from difference SAXS/WAXS curves. It does so by means of the theory described here because the structural changes in pump-probe detection in a typical time-resolved experiment are generally small enough to be confined to a single residue or group in close proximity which is identified by a method akin to the difference Fourier method of time-resolved crystallography. If it is assumed, as is usual with time-resolved structures, that the moved atoms lie within the residue, the 100-fold reduction in the search space (assuming a typical protein has about 100 residues) allows the exaction of the structure by a simulated annealing algorithm with a huge reduction in computing time and leads to a greater resolution by varying the positions of atoms only within that residue. This reduction in the number of potential moved atoms allows us to identify the actual motions of the individual atoms. In the case of a crystal, time-resolved calculations are normally performed using the difference Fourier method, which is, of course, not directly applicable to SAXS/WAXS. The method developed in this paper may be thought of as a substitute for that method which allows SAXS/WAXS (and hence disordered molecules) to also be used for time-resolved structural work.

Detection of Clinically Significant Retinopathy of Prematurity Using Wide-angle Digital Retinal Photography

Science.gov (United States)

Chiang, Michael F.; Melia, Michele; Buffenn, Angela N.; Lambert, Scott R.; Recchia, Franco M.; Simpson, Jennifer L.; Yang, Michael B.

2013-01-01

Objective To evaluate the accuracy of detecting clinically significant retinopathy of prematurity (ROP) using wide-angle digital retinal photography. Methods Literature searches of PubMed and the Cochrane Library databases were conducted last on December 7, 2010, and yielded 414 unique citations. The authors assessed these 414 citations and marked 82 that potentially met the inclusion criteria. These 82 studies were reviewed in full text; 28 studies met inclusion criteria. The authors extracted from these studies information about study design, interventions, outcomes, and study quality. After data abstraction, 18 were excluded for study deficiencies or because they were superseded by a more recent publication. The methodologist reviewed the remaining 10 studies and assigned ratings of evidence quality; 7 studies were rated level I evidence and 3 studies were rated level III evidence. Results There is level I evidence from ≥5 studies demonstrating that digital retinal photography has high accuracy for detection of clinically significant ROP. Level III studies have reported high accuracy, without any detectable complications, from real-world operational programs intended to detect clinically significant ROP through remote site interpretation of wide-angle retinal photographs. Conclusions Wide-angle digital retinal photography has the potential to complement standard ROP care. It may provide advantages through objective documentation of clinical examination findings, improved recognition of disease progression by comparing previous photographs, and the creation of image libraries for education and research. Financial Disclosure(s) Proprietary or commercial disclosure may be found after the references. PMID:22541632

A high resolution, high counting rate bidimensional, MWPC imaging detector for small angle X-ray diffraction studies

International Nuclear Information System (INIS)

Bateman, J.E.; Connolly, J.F.; Sawyer, E.C.; Stephenson, R.

1981-07-01

The performance is reported of a 200 mm x 200 mm X-ray imaging MWPC aimed at applications in small angle X-ray diffraction and scattering. With quantum energies of approximately 8 keV high spatial resolution (+- 0.5 mm x +- 0.14 mm) with a capability for data taking at >approximately 350 kHz is reported. The detection efficiency is approximately 75% and the detector operates as a sealed unit with a long lifetime. (author)

Rotation Estimation for Wide-Angle Inverse Synthetic Aperture Radar Imaging

Directory of Open Access Journals (Sweden)

Wei Zhou

2016-01-01

Full Text Available To present focused ISAR imaging results in the homogenous range and cross-range domain, an integrated scheme is proposed to estimate both the targets equivalent rotational velocity (RV and rotational center (RC. The RV estimation is improved by radial projection combined with keystone processing, and then the RC is estimated through image entropy minimization. Finally, delicate imaging results may be obtained for wide-angle scenarios. Experiment results are provided to demonstrate the effectiveness of the proposed method.

Jet disruption in wide-angle tailed radio galaxies

International Nuclear Information System (INIS)

Burns, J.O.; Norman, M.L.; Clarke, D.A.

1986-01-01

The mechanisms responsible for the bending of the jets and tails of wide-angle tailed (WAT) radio galaxies in clusters are investigated theoretically, with a focus on sharp bends and rapid jet disruption. Large (1 Mpc) and small (200 kpc) WATs are differentiated, and it is suggested that the jet-tail transition in large WATs is due to collisions between the jet and cool clouds of the intracluster medium (ICM). The transition in small WATs is attributed to the passage of the jet through a planar Mach disk perpendicular to the jet flow direction. Such a disk is shown in numerical simulations to form when there is a shocklike jump in ambient pressure at the ISM/ICM interface; the origins of such a jump are explored. 14 references

Preliminary small-angle X-ray scattering and X-ray diffraction studies of the BTB domain of lola protein from Drosophila melanogaster

Science.gov (United States)

Boyko, K. M.; Nikolaeva, A. Yu.; Kachalova, G. S.; Bonchuk, A. N.; Dorovatovskii, P. V.; Popov, V. O.

2017-11-01

The Drosophila genome has several dozens of transcription factors (TTK group) containing BTB domains assembled into octamers. The LOLA protein belongs to this family. The purification, crystallization, and preliminary X-ray diffraction and small-angle X-ray scattering (SAXS) studies of the BTB domain of this protein are reported. The crystallization conditions were found by the vapor-diffusion technique. A very low diffraction resolution (8.7 Å resolution) of the crystals was insufficient for the determination of the threedimensional structure of the BTB domain. The SAXS study demonstrated that the BTB domain of the LOLA protein exists as an octamer in solution.

A two-dimensional wide-angle proton spectrometer with improved angular resolution

International Nuclear Information System (INIS)

Yang, Su; Deng, Yanqing; Ge, Xulei; Fang, Yuan; Wei, Wenqing; Gao, Jian; Liu, Feng; Chen, Min; Liao, Guoqian; Li, Yutong; Zhao, Li; Ma, Yanyun

2017-01-01

We present an improvement design of a two-dimensional (2D) angular-resolved proton spectrometer for wide-angle measurement of proton beams from high-intensity laser-solid interactions. By using a 2D selective entrance pinhole array with different periods in orthogonal axes, the angular resolution along one dimension is improved by a factor of 6.7. This improvement provides the accessibility to detect the spatial fine structures of the proton energy spectrum.

A two-dimensional wide-angle proton spectrometer with improved angular resolution

Energy Technology Data Exchange (ETDEWEB)

Yang, Su [Key Laboratory for Laser Plasmas (Ministry of Education) and Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China); Collaborative Innovation Center of IFSA (CICIFSA), Shanghai Jiao Tong University, Shanghai 200240 (China); Deng, Yanqing [Key Laboratory for Laser Plasmas (Ministry of Education) and Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China); Collaborative Innovation Center of IFSA (CICIFSA), Shanghai Jiao Tong University, Shanghai 200240 (China); College of Science, National University of Defense Technology, Changsha 410073 (China); Ge, Xulei [Key Laboratory for Laser Plasmas (Ministry of Education) and Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China); Collaborative Innovation Center of IFSA (CICIFSA), Shanghai Jiao Tong University, Shanghai 200240 (China); State Key Laboratory of Surface Physics and Department of Physics, Fudan University, Shanghai 200433 (China); Fang, Yuan; Wei, Wenqing; Gao, Jian; Liu, Feng; Chen, Min [Key Laboratory for Laser Plasmas (Ministry of Education) and Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China); Collaborative Innovation Center of IFSA (CICIFSA), Shanghai Jiao Tong University, Shanghai 200240 (China); Liao, Guoqian; Li, Yutong [Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, Beijing 100190 (China); Collaborative Innovation Center of IFSA (CICIFSA), Shanghai Jiao Tong University, Shanghai 200240 (China); Zhao, Li [State Key Laboratory of Surface Physics and Department of Physics, Fudan University, Shanghai 200433 (China); Ma, Yanyun [College of Science, National University of Defense Technology, Changsha 410073 (China); Collaborative Innovation Center of IFSA (CICIFSA), Shanghai Jiao Tong University, Shanghai 200240 (China); and others

2017-07-11

We present an improvement design of a two-dimensional (2D) angular-resolved proton spectrometer for wide-angle measurement of proton beams from high-intensity laser-solid interactions. By using a 2D selective entrance pinhole array with different periods in orthogonal axes, the angular resolution along one dimension is improved by a factor of 6.7. This improvement provides the accessibility to detect the spatial fine structures of the proton energy spectrum.

Electro-optic diffraction grating tuned laser

International Nuclear Information System (INIS)

Hughes, R.S.

1975-01-01

An electro-optic diffraction grating tuned laser comprising a laser medium, output mirror, retro-reflective grating and an electro-optic diffraction grating beam deflector positioned between the laser medium and the reflective diffraction grating is described. An optional angle multiplier may be used between the electro-optic diffraction grating and the reflective grating. (auth)

Diffraction in nuclear scattering

International Nuclear Information System (INIS)

Wojciechowski, H.

1986-01-01

The elastic scattering amplitudes for charged and neutral particles have been decomposed into diffractive and refractive parts by splitting the nuclear elastic scattering matrix elements into components responsible for these effects. It has been shown that the pure geometrical diffractive effect which carries no information about the nuclear interaction is always predominant at forward angle of elastic angular distributions. This fact suggests that for strongly absorbed particles only elastic cross section at backward angles, i.e. the refractive cross section, can give us basic information about the central nuclear potential. 12 refs., 4 figs., 1 tab. (author)

Theory, design, and experimental verification of a reflectionless bianisotropic Huygens' metasurface for wide-angle refraction

Science.gov (United States)

Chen, Michael; Abdo-Sánchez, Elena; Epstein, Ariel; Eleftheriades, George V.

2018-03-01

Huygens' metasurfaces are electrically thin devices which allow arbitrary field transformations. Beam refraction is among the first demonstrations of realized metasurfaces. As previously shown for extreme-angle refraction, control over only the electric impedance and magnetic admittance of the Huygens' metasurface proved insufficient to produce the desired reflectionless field transformation. To maintain zero reflections for wide refraction angles, magnetoelectric coupling between the electric and magnetic response of the metasurface, leading to bianisotropy, can be introduced. In this paper, we report the theory, design, and experimental characterization of a reflectionless bianisotropic metasurface for extreme-angle refraction of a normally incident plane wave towards 71.8° at 20 GHz. The theory and design of three-layer asymmetric bianisotropic unit cells are discussed. The realized printed circuit board structure was tested via full-wave simulations as well as experimental characterization. To experimentally verify the prototype, two setups were used. A quasi-optical experiment was conducted to assess the specular reflections of the metasurface, while a far-field antenna measurement characterized its refraction nature. The measurements verify that the fabricated metasurface has negligible reflections and the majority of the scattered power is refracted to the desired Floquet mode. This provides an experimental demonstration of a reflectionless wide-angle refracting metasurface using a bianisotropic Huygens' metasurface at microwave frequencies.

Anisotropic light diffraction in crystals with a large acoustic-energy walk-off

Science.gov (United States)

Balakshy, V. I.; Voloshin, A. S.; Molchanov, V. Ya.

2014-11-01

The influence of energy walk-off in an acoustic beam on the characteristic of anisotropic Bragg diffraction of light has been investigated by the example of paratellurite crystal. The angular and frequency characteristics of acousto-optic diffraction have been calculated in wide ranges of ultrasound frequencies and Bragg angles using the modified Raman-Nath equations. It is shown that the walk-off of an acoustic beam may change (either widen or narrow) significantly the frequency and angular ranges. The calculation results have been experimentally checked on an acousto-optic cell made of 10.5°-cut paratellurite crystal.

Conversion of Natural Tannin to Hydrothermal and Graphene-Like Carbons Studied by Wide-Angle X-ray Scattering.

Science.gov (United States)

Jurkiewicz, Karolina; Hawełek, Łukasz; Balin, Katarzyna; Szade, Jacek; Braghiroli, Flavia L; Fierro, Vanessa; Celzard, Alain; Burian, Andrzej

2015-08-13

The atomic structure of carbon materials prepared from natural tannin by two different techniques, high-temperature pyrolysis and low-temperature hydrothermal carbonization, was studied by wide-angle X-ray scattering. The obtained diffraction data were converted to the real space representation in the form of pair distribution functions. The X-ray photoelectron spectroscopy measurements provided information about the chemical state of carbon in tannin-based materials that was used to construct final structural models of the investigated samples. The results of the experimental data in both reciprocal and real spaces were compared with computer simulations based on the PM7 semiempirical quantum chemical method. Using the collected detailed information, structural models of the tannin-based carbons were proposed. The characteristics of the investigated materials at the atomic level were discussed in relation to their preparation method. The rearrangement of the tannin molecular structure and its transformation to graphene-like structure was described. The structure of tannin-based carbons pyrolyzed at 900 °C exhibited coherently scattering domains about 20 Å in size, consisting of two defected atomic layers and resembling a graphene-like arrangement.

Angle-resolved photoemission extended fine structure

International Nuclear Information System (INIS)

Barton, J.J.

1985-03-01

Measurements of the Angle-Resolved Photoemission Extended Fine Structure (ARPEFS) from the S(1s) core level of a c(2 x 2)S/Ni(001) are analyzed to determine the spacing between the S overlayer and the first and second Ni layers. ARPEFS is a type of photoelectron diffraction measurement in which the photoelectron kinetic energy is swept typically from 100 to 600 eV. By using this wide range of intermediate energies we add high precision and theoretical simplification to the advantages of the photoelectron diffraction technique for determining surface structures. We report developments in the theory of photoelectron scattering in the intermediate energy range, measurement of the experimental photoemission spectra, their reduction to ARPEFS, and the surface structure determination from the ARPEFS by combined Fourier and multiple-scattering analyses. 202 refs., 67 figs., 2 tabs

25G compared with 20G vitrectomy under Resight non-contact wide-angle lenses for Terson syndrome.

Science.gov (United States)

Mao, Xinbang; You, Zhipeng

2017-08-01

The aim of the present study was to compare the effectiveness of 25G vitrectomy to standard 20G vitrectomy for treatment of Terson syndrome under Resight non-contact wide-angle lenses. This was a case-control study of 20 patients with Terson syndrome (study group) that underwent 25G vitrectomy under Resight non-contact wide-angle lenses, with those of 20 matched patients that underwent 20G vitrectomy (control group). Medical records were reviewed from between July 2011 and October 2013. Data included results of the Early Treatment Diabetic Retinopathy Study examination, ophthalmology B-scan ultrasonography and fundus photography. The mean age, follow-up time, the preoperative visual acuity of LogMAR and the preoperative intraocular pressure (IOP) were all comparable in the two groups (all P>0.05). There were statistically significant differences in postoperative visual acuity of LogMAR compared with preoperative visual acuity (Pcontact wide-angle lenses can achieve a significantly shorter operative time and lower post-operative IOP compared with 20G Vitrectomy.

Analysis of dislocation loops by means of large-angle convergent beam electron diffraction

CERN Document Server

Jäger, C; Morniroli, J P; Jäger, W

2002-01-01

Diffusion-induced dislocation loops in GaP and GaAs were analysed by means of large-angle convergent beam electron diffraction (LACBED) and conventional contrast methods of transmission electron microscopy. It is demonstrated that LACBED is perfectly suited for use in analysing dislocation loops. The method combines analyses of the dislocation-induced splitting of Bragg lines in a LACBED pattern for the determination of the Burgers vector with analyses of the loop contrast behaviour in transmission electron microscopy bright-field images during tilt experiments, from which the habit plane of the dislocation loop is determined. Perfect dislocation loops formed by condensation of interstitial atoms or vacancies were found, depending on the diffusion conditions. The loops possess left brace 110 right brace-habit planes and Burgers vectors parallel to (110). The LACBED method findings are compared with results of contrast analyses based on the so-called 'inside-outside' contrast of dislocation loops. Advantages o...

A wide angle view imaging diagnostic with all reflective, in-vessel optics at JET

Energy Technology Data Exchange (ETDEWEB)

Clever, M. [Institute of Energy and Climate Research – Plasma Physics, Forschungszentrum Jülich GmbH, Association EURATOM-FZJ, 52425 Jülich (Germany); Arnoux, G.; Balshaw, N. [Euratom/CCFE Fusion Association, Culham Science Centre, Abingdon, Oxon OX14 3DB (United Kingdom); Garcia-Sanchez, P. [Laboratorio Nacional de Fusion, Asociacion EURATOM-CIEMAT, Madrid (Spain); Patel, K. [Euratom/CCFE Fusion Association, Culham Science Centre, Abingdon, Oxon OX14 3DB (United Kingdom); Sergienko, G. [Institute of Energy and Climate Research – Plasma Physics, Forschungszentrum Jülich GmbH, Association EURATOM-FZJ, 52425 Jülich (Germany); Soler, D. [Winlight System, 135 rue Benjamin Franklin, ZA Saint Martin, F-84120 Pertuis (France); Stamp, M.F.; Williams, J.; Zastrow, K.-D. [Euratom/CCFE Fusion Association, Culham Science Centre, Abingdon, Oxon OX14 3DB (United Kingdom)

2013-10-15

Highlights: ► A new wide angle view camera system has been installed at JET. ► The system helps to protect the ITER-like wall plasma facing components from damage. ► The coverage of the vessel by camera observation systems was increased. ► The system comprises an in-vessel part with parabolic and flat mirrors. ► The required image quality for plasma monitoring and wall protection was delivered. -- Abstract: A new wide angle view camera system has been installed at JET in preparation for the ITER-like wall campaigns. It considerably increases the coverage of the vessel by camera observation systems and thereby helps to protect the – compared to carbon – more fragile plasma facing components from damage. The system comprises an in-vessel part with parabolic and flat mirrors and an ex-vessel part with beam splitters, lenses and cameras. The system delivered the image quality required for plasma monitoring and wall protection.

Honeywell's Compact, Wide-angle Uv-visible Imaging Sensor

Science.gov (United States)

Pledger, D.; Billing-Ross, J.

1993-01-01

Honeywell is currently developing the Earth Reference Attitude Determination System (ERADS). ERADS determines attitude by imaging the entire Earth's limb and a ring of the adjacent star field in the 2800-3000 A band of the ultraviolet. This is achieved through the use of a highly nonconventional optical system, an intensifier tube, and a mega-element CCD array. The optics image a 30 degree region in the center of the field, and an outer region typically from 128 to 148 degrees, which can be adjusted up to 180 degrees. Because of the design employed, the illumination at the outer edge of the field is only some 15 percent below that at the center, in contrast to the drastic rolloffs encountered in conventional wide-angle sensors. The outer diameter of the sensor is only 3 in; the volume and weight of the entire system, including processor, are 1000 cc and 6 kg, respectively.

WAMDII: The Wide Angle Michelson Doppler Imaging Interferometer

Science.gov (United States)

1992-01-01

As part of an effort to learn more about the upper atmosphere and how it is linked to the weather experienced each day, NASA and NRCC are jointly sponsoring the Wide Angle Michelson Doppler Imaging Interferometer (WAMDII) Mission. WAMDII will measure atmospheric temperature and wind speed in the upper atmosphere. In addition to providing data on the upper atmosphere, the wind speed and temperature readings WAMDII takes will also be highly useful in developing and updating computer simulated models of the upper atmosphere. These models are used in the design and testing of equipment and software for Shuttles, satellites, and reentry vehicles. In making its wind speed and temperature measurements, WAMDII examines the Earth's airglow, a faint photochemical luminescence caused by the influx of solar ultraviolet energy into the upper atmosphere. During periods of high solar flare activity, the amount of this UV energy entering the upper atmosphere increases, and this increase may effect airglow emissions.

X-ray diffraction investigation of spin reorientation in SmFe2

International Nuclear Information System (INIS)

Gaviko, V.S.; Korolyov, A.V.; Mushnikov, N.V.

1996-01-01

Spontaneous magnetoelastic crystal lattice distortions in the spin reorientation region of high magnetostrictive SmFe 2 have been investigated by X-ray diffraction in the temperature range 80-300 K. Comparison of experimental shapes of X-ray diffraction lines with calculated shapes shows that, in the region of the spin reorientation transition, a mixture of left angle 110 right angle and left angle 111 right angle phases rather than the angular left angle uuw right angle -type phase is realized. The temperature dependence of the relative volume content of left angle 110 right angle and left angle 111 right angle phases is determined using least-squares fitting. (orig.)

The influence of texture on the strain measured by diffraction

International Nuclear Information System (INIS)

Penning, P.; Brakman, C.M.

1988-01-01

Strain, as determined by diffraction techniques, is calculated from its constituents. First, the fraction of the crystals that have the proper orientation for diffraction. One degree of freedom is present: the angle of rotation φ 2 '' about the scattering vector that the diffracting crystals have in common. The proper orientations, expressed in Euler angles, lie on a line ('trace') in orientation space. The density along the trace is asserted to be known as a Fourier series in φ 2 ''. Second, the strain in the diffracting crystals. The simplest possible models are discussed: the Voigt and Reuss approximations. The symmetries of the crystal (m3 or m3m) and of the orientation distribution function (o.d.f.) are taken into account. The dilatation in spacing of the reflecting planes is found as a Fourier series in φ 2 '' also. Only the zeroth, first and second harmonic (including phase angles: five parameters) play a part. The diffraction strain is the average over the angle φ 2 '' of the dilatation, weighted with the product of the orientation density and the square of the structure factor. For each contributing trace, the corresponding Fourier coefficients have to be multiplied and added to obtain the diffraction strain. The symmetry of the diffraction pole figure is derived. (orig.)

5G antenna array with wide-angle beam steering and dual linear polarizations

KAUST Repository

Klionovski, Kirill

2017-10-25

In this paper, we present the design of a switched-beam antenna array at millimeter-wave frequencies for future 5G applications. The proposed antenna array is based on wideband patch antenna elements and a Butler matrix feed network. The patch antenna has a broad radiation pattern for wide-angle beam steering and allows the simultaneous operation with two orthogonal linear polarizations. A combination of two separated Butler matrices provides independent beam steering for both polarizations in the wide operating band. The antenna array has a simple multilayer construction, and it is made on a low-cost Rogers laminate.

5G antenna array with wide-angle beam steering and dual linear polarizations

KAUST Repository

Klionovski, Kirill; Shamim, Atif; Sharawi, Mohammad Said

2017-01-01

In this paper, we present the design of a switched-beam antenna array at millimeter-wave frequencies for future 5G applications. The proposed antenna array is based on wideband patch antenna elements and a Butler matrix feed network. The patch antenna has a broad radiation pattern for wide-angle beam steering and allows the simultaneous operation with two orthogonal linear polarizations. A combination of two separated Butler matrices provides independent beam steering for both polarizations in the wide operating band. The antenna array has a simple multilayer construction, and it is made on a low-cost Rogers laminate.

Automatic control unit for A neutron diffraction crystal spectrometer

Energy Technology Data Exchange (ETDEWEB)

Adib, M.; Abbas, Y.; Mostafa, M.; Hamouda, I.

1982-01-01

An automatic transistorized unit has been designed and constructed to control the operation of the double axis crystal spectrometer installed in front of one of the horizontal channels of the ET-RR-1 reactor. The function of the automatic unit is to store the diffracted neutrons at a certain angle with respect to the direction of the incident neutron beam in a selected channel of a 1024-multichannel analyzer for a certain preadjusted time period. AT the end of this time period the unit rotates the spectrometer's arm to another angle, selects the next channel of the MCA and provides the measurement of the diffracted neutron for the same time period. Such a sequence is repeated automatically over all angles required for the neutron diffraction pattern of the sample under investigation. As a result, the stored information at the MCA provides the neutron diffraction pattern as a function of channel number, where each channel corresponds to a certain scattering angle. The stored distribution at MCA can be obtained through the analyzer read out unit. The designed automatic unit has the possibility of providing the neutron diffraction pattern using a 6-digit scaler and a printer.

Monitoring the recrystallisation of amorphous xylitol using Raman spectroscopy and wide-angle X-ray scattering.

Science.gov (United States)

Palomäki, Emmi; Ahvenainen, Patrik; Ehlers, Henrik; Svedström, Kirsi; Huotari, Simo; Yliruusi, Jouko

2016-07-11

In this paper we present a fast model system for monitoring the recrystallization of quench-cooled amorphous xylitol using Raman spectroscopy and wide-angle X-ray scattering. The use of these two methods enables comparison between surface and bulk crystallization. Non-ordered mesoporous silica micro-particles were added to the system in order to alter the rate of crystallization of the amorphous xylitol. Raman measurements showed that adding silica to the system increased the rate of surface crystallization, while X-ray measurements showed that the rate of bulk crystallization decreased. Using this model system it is possible to measure fast changes, which occur in minutes or within a few hours. Raman-spectroscopy and wide-angle X-ray scattering were found to be complementary techniques when assessing surface and bulk crystallization of amorphous xylitol. Copyright © 2016 Elsevier B.V. All rights reserved.

Diamond-anvil cell for radial x-ray diffraction

International Nuclear Information System (INIS)

Chesnut, G N; Schiferl, D; Streetman, B D; Anderson, W W

2006-01-01

We have designed a new diamond-anvil cell capable of radial x-ray diffraction to pressures of a few hundred GPa. The diffraction geometry allows access to multiple angles of Ψ, which is the angle between each reciprocal lattice vector g(hkl) and the compression axis of the cell. At the 'magic angle', Ψ∼54.7 0 , the effects of deviatoric stresses on the interplanar spacings, d(hkl), are significantly reduced. Because the systematic errors, which are different for each d(hkl), are significantly reduced, the crystal structures and the derived equations of state can be determined reliably. At other values of Ψ, the effects of deviatoric stresses on the diffraction pattern could eventually be used to determine elastic constants

Metasurface-based angle-selective multichannel acoustic refractor

Science.gov (United States)

Liu, Bingyi; Jiang, Yongyuan

2018-05-01

We theoretically study the angle-selective refractions of an impedance-matched acoustic gradient-index metasurface, which is integrated with a rigid bar array of a deep subwavelength period. An interesting refraction order appears under the all-angle incidence despite the existence of a critical angle, and notably, the odevity of the phase-discretization level apparently selects the transmitted diffraction orders. We utilize the strategy of multilayered media design to realize a three-channel acoustic refractor, which shows good promise for constructing multifunctional diffractive acoustic elements for acoustic communication.

Doppler Aliasing Reduction in Wide-Angle Synthetic Aperture Radar Using Phase Modulated Random Stepped-Frequency Waveforms

National Research Council Canada - National Science Library

Hyatt, Andrew W

2006-01-01

...) waveforms in a Wide-Angle Synthetic Aperture Radar (WA-SAR) scenario. RSF waveforms have been demonstrated to have desirable properties which allow for cancelling of Doppler aliased scatterers in WA-SAR images...

Load transfer in bovine plexiform bone determined by synchrotron x-ray diffraction

International Nuclear Information System (INIS)

Akhtar, R.; Daymond, M.; Almer, J.; Mummery, P.; The Univ. of Manchester; Queen's Univ.

2008-01-01

High-energy synchrotron x-ray diffraction (XRD) has been used to quantify load transfer in bovine plexiform bone. By using both wide-angle and small-angle XRD, strains in the mineral as well as the collagen phase of bone were measured as a function of applied compressive stress. We suggest that a greater proportion of the load is borne by the more mineralized woven bone than the lamellar bone as the applied stress increases. With a further increase in stress, load is shed back to the lamellar regions until macroscopic failure occurs. The reported data fit well with reported mechanisms of microdamage accumulation in bovine plexiform bone

Rapid small-angle X-ray diffraction of a tonically contracting molluscan smooth muscle recorded with imaging plates

International Nuclear Information System (INIS)

Tajima, Y.; Okada, K.; Yoshida, O.; Seto, T.; Amemiya, Y.

1989-01-01

Small-angle X-ray diffraction patterns from the anterior byssus retractor muscles of Mytilus edulis contracting tonically in response to stimulation with acetylcholine were recorded in a 30 s exposure with synchrotron radiation and a high-sensitivity X-ray area detector called an imaging plate. The 190 A layer line from the thin filaments increased in intensity with increase in tonic tension up to 6x10 4 kg m -2 . Above this value, the layer-line intensity remained almost constant and comparable to that for a contracting skeletal muscle, indicating that the same structural changes of the thin filaments occur in both muscles. (orig.)

Small-angle and wide-angle X-ray scattering study on the bilayer structure of synthetic and bovine heart cardiolipins

International Nuclear Information System (INIS)

Takahashi, Hiroshi; Hayakawa, Tomohiro; Ito, Kazuki; Takata, Masaki; Kobayashi, Toshihide

2010-01-01

Cardiolipin (CL) is a membrane phospholipid containing four fatty acid chains. CL plays an important role in energy transformation in mitochondria. The disorder of CL biosynthesis is involved in a genetic disease, Barth syndrome. Alteration of fatty acid composition of CLs has been found in Barth syndrome patients, i.e., the decrease of unsaturated fatty acid chains. In this study, we investigated how the degree of saturation alters the structure of CL bilayers by using X-ray scattering. Bovine heart CL and two synthetic CLs were compared. Fatty acid compositions of these three CLs have different saturation. Small-angle X-ray scattering data showed that the decrease of the number of double bonds in the unsaturated fatty acid chains causes to thicken the CL bilayers. In addition, wide-angle X-ray scattering data suggested that the decrease reduces the degree of disorder of the hydrophobic region in a liquid crystalline phase. These results may be related to the dysfunction of mitochondria in Barth syndrome.

Small-angle and wide-angle X-ray scattering study on the bilayer structure of synthetic and bovine heart cardiolipins

Energy Technology Data Exchange (ETDEWEB)

Takahashi, Hiroshi [Biophysics Laboratory, Department of Chemistry and Chemical Biology, Gunma University, Maebashi, Gunma, 371-8510 (Japan); Hayakawa, Tomohiro [Life Science Laboratory, Advanced Materials Laboratories, Sony Corporation, Yushima, Bunkyo-ku, Tokyo, 113-8510 (Japan); Ito, Kazuki; Takata, Masaki [Structural Materials Science Laboratory, RIKEN SPring-8 Center, Sayo, Hyogo 679-5148 (Japan); Kobayashi, Toshihide, E-mail: htakahas@chem-bio.gunma-u.ac.j [Lipid Biology Laboratory, RIKEN, Wako, Saitama 351-0198 (Japan)

2010-10-01

Cardiolipin (CL) is a membrane phospholipid containing four fatty acid chains. CL plays an important role in energy transformation in mitochondria. The disorder of CL biosynthesis is involved in a genetic disease, Barth syndrome. Alteration of fatty acid composition of CLs has been found in Barth syndrome patients, i.e., the decrease of unsaturated fatty acid chains. In this study, we investigated how the degree of saturation alters the structure of CL bilayers by using X-ray scattering. Bovine heart CL and two synthetic CLs were compared. Fatty acid compositions of these three CLs have different saturation. Small-angle X-ray scattering data showed that the decrease of the number of double bonds in the unsaturated fatty acid chains causes to thicken the CL bilayers. In addition, wide-angle X-ray scattering data suggested that the decrease reduces the degree of disorder of the hydrophobic region in a liquid crystalline phase. These results may be related to the dysfunction of mitochondria in Barth syndrome.

Integration of least angle regression with empirical Bayes for multi-locus genome-wide association studies

Science.gov (United States)

Multi-locus genome-wide association studies has become the state-of-the-art procedure to identify quantitative trait loci (QTL) associated with traits simultaneously. However, implementation of multi-locus model is still difficult. In this study, we integrated least angle regression with empirical B...

Determination of low-field critical parameters of superconducting niobium by small-angle neutron diffraction

International Nuclear Information System (INIS)

Christen, D.K.; Spooner, S.; Thorel, P.; Kerchner, H.R.

1977-01-01

The perfect double-crystal small-angle diffraction technique enables measurement of scattering angles to within 0.3 arc sec. accuracy. At a wavelength of 2.55 A, this provides a resolution of 3 x 10 -6 A -1 in the scattering vector. This technique has been used to study the anisotropic behavior of the critical parameters B 0 and H/sub c1/, characteristic of the first-order magnetic phase transition which occurs in low-kappa type-II superconductors. Magnetic fields were applied parallel to several crystal axes of a large single-crystal sphere of pure niobium, resulting in well-defined flux-line lattices (FLL). Measurement of the FLL cell area in the intermediate mixed state field region gives the equilibrium flux density B 0 , which results from an attractive interaction between fluxoids. In addition, field variation of the scattered neutron intensity allows measurement of the transition field between the mixed state and intermediate mixed state. This transition field is related to the lower critical field H/sub c1/ and enables its determination to a precision 0.2%. Data at T = 4.3 K display a small anisotropic effect of about 2% in B 0 and 1% in H/sub c1/. Although orientation effects of this magnitude are difficult to resolve by bulk measurements, the neutron data are in accord with magnetization data. Observations regarding the temperature dependence of these parameters also will be presented, and comparisons made with current theoretical models

An automatic control unit for A neutron diffraction crystal spectrometer

International Nuclear Information System (INIS)

Adib, M.; Abbas, Y.; Mostafa, M.; Hamouda, I.

1982-01-01

An automatic transistorized unit has been designed and constructed to control the operation of the double axis crystal spectrometer installed in front of one of the horizontal channels of the ET-RR-1 reactor. The function of the automatic unit is to store the diffracted neutrons at a certain angle with respect to the direction of the incident neutron beam in a selected channel of a 1024-multichannel analyzer for a certain preadjusted time period. AT the end of this time period the unit rotates the spectrometer's arm to another angle, selects the next channel of the MCA and provides the measurement of the diffracted neutron for the same time period. Such a sequence is repeated automatically over all angles required for the neutron diffraction pattern of the sample under investigation. As a result, the stored information at the MCA provides the neutron diffraction pattern as a function of channel number, where each channel corresponds to a certain scattering angle. The stored distribution at MCA can be obtained through the analyzer read out unit. The designed automatic unit has the possibility of providing the neutron diffraction pattern using a 6-digit scaler and a printer

Analysis of dislocation loops by means of large-angle convergent beam electron diffraction

International Nuclear Information System (INIS)

Jaeger, Ch; Spiecker, E; Morniroli, J P; Jaeger, W

2002-01-01

Diffusion-induced dislocation loops in GaP and GaAs were analysed by means of large-angle convergent beam electron diffraction (LACBED) and conventional contrast methods of transmission electron microscopy. It is demonstrated that LACBED is perfectly suited for use in analysing dislocation loops. The method combines analyses of the dislocation-induced splitting of Bragg lines in a LACBED pattern for the determination of the Burgers vector with analyses of the loop contrast behaviour in transmission electron microscopy bright-field images during tilt experiments, from which the habit plane of the dislocation loop is determined. Perfect dislocation loops formed by condensation of interstitial atoms or vacancies were found, depending on the diffusion conditions. The loops possess {110}-habit planes and Burgers vectors parallel to (110). The LACBED method findings are compared with results of contrast analyses based on the so-called 'inside-outside' contrast of dislocation loops. Advantages of the LACBED method consist in the possibility of determining the complete Burgers vector of the dislocation loops and of an unambiguous and fast loop type analysis

Angle sensitive single photon avalanche diode

Energy Technology Data Exchange (ETDEWEB)

Lee, Changhyuk, E-mail: cl678@cornell.edu; Johnson, Ben, E-mail: bcj25@cornell.edu; Molnar, Alyosha, E-mail: am699@cornell.edu [Electrical and Computer Engineering, Cornell University, Ithaca, New York 14850 (United States)

2015-06-08

An ideal light sensor would provide exact information on intensity, timing, location, and angle of incoming photons. Single photon avalanche diodes (SPADs) provide such desired high (single photon) sensitivity with precise time information and can be implemented at a pixel-scale to form an array to extract spatial information. Furthermore, recent work has demonstrated photodiode-based structures (combined with micro-lenses or diffraction gratings) that are capable of encoding both spatial and angular information of incident light. In this letter, we describe the implementation of such a grating structure on SPADs to realize a pixel-scale angle-sensitive single photon avalanche diode (A-SPAD) built in a standard CMOS process. While the underlying SPAD structure provides high sensitivity, the time information of the two layers of diffraction gratings above offers angle-sensitivity. Such a unique combination of SPAD and diffraction gratings expands the sensing dimensions to pave a path towards lens-less 3-D imaging and light-field time-of-flight imaging.

Specific features of two diffraction schemes for a widely divergent X-ray beam

Energy Technology Data Exchange (ETDEWEB)

Avetyan, K. T.; Levonyan, L. V.; Semerjian, H. S.; Arakelyan, M. M., E-mail: marakelyan@ysu.am; Badalyan, O. M. [Yerevan State University (Armenia)

2015-03-15

We investigated the specific features of two diffraction schemes for a widely divergent X-ray beam that use a circular diaphragm 30–50 μm in diameter as a point source of characteristic radiation. In one of the schemes, the diaphragm was set in front of the crystal (the diaphragm-crystal (d-c) scheme); in the other, it was installed behind the crystal (the crystal-diaphragm (c-d) scheme). It was established that the diffraction image in the c-d scheme is a topographic map of the investigated crystal area. In the d-c scheme at L = 2l (l and L are the distances between the crystal and the diaphragm and between the photographic plate and the diaphragm, respectively), the branches of hyperbolas formed in this family of planes (hkl) by the characteristic K{sub α} and K{sub β} radiations, including higher order reflections, converge into one straight line. It is experimentally demonstrated that this convergence is very sensitive to structural inhomogeneities in the crystal under study.

Time-domain Brillouin scattering assisted by diffraction gratings

Science.gov (United States)

Matsuda, Osamu; Pezeril, Thomas; Chaban, Ievgeniia; Fujita, Kentaro; Gusev, Vitalyi

2018-02-01

Absorption of ultrashort laser pulses in a metallic grating deposited on a transparent sample launches coherent compression/dilatation acoustic pulses in directions of different orders of acoustic diffraction. Their propagation is detected by delayed laser pulses, which are also diffracted by the metallic grating, through the measurement of the transient intensity change of the first-order diffracted light. The obtained data contain multiple frequency components, which are interpreted by considering all possible angles for the Brillouin scattering of light achieved through multiplexing of the propagation directions of light and coherent sound by the metallic grating. The emitted acoustic field can be equivalently presented as a superposition of plane inhomogeneous acoustic waves, which constitute an acoustic diffraction grating for the probe light. Thus the obtained results can also be interpreted as a consequence of probe light diffraction by both metallic and acoustic gratings. The realized scheme of time-domain Brillouin scattering with metallic gratings operating in reflection mode provides access to wide range of acoustic frequencies from minimal to maximal possible values in a single experimental optical configuration for the directions of probe light incidence and scattered light detection. This is achieved by monitoring the backward and forward Brillouin scattering processes in parallel. Potential applications include measurements of the acoustic dispersion, simultaneous determination of sound velocity and optical refractive index, and evaluation of samples with a single direction of possible optical access.

Wide Angle of Incidence-Insensitive Polarization-Independent THz Metamaterial Absorber for Both TE and TM Mode Based on Plasmon Hybridizations

Directory of Open Access Journals (Sweden)

Xiu Tao Huang

2018-04-01

Full Text Available An ultra-wide-angle THz metamaterial absorber (MA utilizing sixteen-circular-sector (SCR resonator for both transverse electric (TE and transverse magnetic (TM mode is designed and investigated numerically. At normal incidence, the absorptivity of the proposed MA is higher than 93.7% at 9.05 THz for different polarization angles, due to the rotational symmetry structure of the unit cell. Under oblique incidence, the absorptivity can still exceed 90%, even when the incident angle is up to 70° for both TE and TM mode. Especially, the frequency variation in TE mode is less than 0.25% for different incident angles from 0° to 70°. The electric field (Ez distributions are used to explain the absorption mechanism. Numerical simulation results show that the high absorption with wide-angle independence stems from fundamental dipole resonance and gap surface plasmons. The broadband deep-infrared MA is also obtained by stacking three metal-dielectric layers. The designed MA has great potential in bolometric pixel elements, biomedical sensors, THz imaging, and solar cells.

Linear wide angle sun sensor for spinning satellites

Science.gov (United States)

Philip, M. P.; Kalakrishnan, B.; Jain, Y. K.

1983-08-01

A concept is developed which overcomes the defects of the nonlinearity of response and limitation in range exhibited by the V-slit, N-slit, and crossed slit sun sensors normally used for sun elevation angle measurements on spinning spacecraft. Two versions of sensors based on this concept which give a linear output and have a range of nearly + or - 90 deg of elevation angle are examined. Results are presented for the application of the twin slit version of the sun sensor in the three Indian satellites, Rohini, Apple, and Bhaskara II, which was successfully used for spin rate control and spin axis orientation control corrections as well as for sun elevation angle and spin period measurements.

Wide angle Compton scattering within the SCET factorization framework

International Nuclear Information System (INIS)

Kivel, N.

2016-01-01

Existing data for the electromagnetic proton form factors and for the cross section of the wide angle Compton scattering (WACS) show that the hard two-gluon exchange mechanism (collinear factorization) is still not applicable in the kinematical region where Mandelstam variables s ∼ -t ∼ -u are about a few GeV 2 . On the other hand these observables can be described in phenomenological models where spectator quarks are soft which assumes a large contribution due to the soft-overlap mechanism. It turns out that the simple QCD factorization picture is not complete and must also include the soft-overlap contribution which can be described as a certain matrix element in the soft collinear effective theory (SCET). Then the leading power contribution to WACS amplitude is described as a sum of the hard- and soft-spectator contributions. The existing experimental data allows one to check certain conclusions based on the assumption about dominant role of the soft-spectator mechanism. (author)

Rietveld refinement with time-of-flight powder diffraction data from pulsed neutron sources

International Nuclear Information System (INIS)

David, W.I.F.; Jorgensen, J.D.

1990-10-01

The recent development of accelerator-based pulsed neutron sources has led to the widespread use of the time-of-flight technique for neutron powder diffraction. The properties of the pulsed source make possible unusually high resolution over a wide range of d spacings, high count rates, and the ability to collect complete data at fixed scattering angles. The peak shape and other instrument characteristics can be accurately modelled, which make Rietveld refinement possible for complex structures. In this paper we briefly review the development of the Rietveld method for time-of-flight diffraction data from pulsed neutron sources and discuss the latest developments in high resolution instrumentation and advanced Rietveld analysis methods. 50 refs., 12 figs., 14 tabs

The refractive-index correction in powder diffraction

International Nuclear Information System (INIS)

Hart, M.; Parrish, W.; Bellotto, M.; Lim, G.S.

1988-01-01

Throughout the history of powder diffraction practice there has been uncertainty about whether or not a refractive-index correction should be made to Bragg's law. High-precision Bragg-angle measurements have been performed with synchrotron radiation on SRM-640 silicon powders at glancing angles; it is found that little or no correction is necessary for the usual 2θ angle range. (orig.)

The GPD H and spin correlations in wide-angle Compton scattering

Energy Technology Data Exchange (ETDEWEB)

Kroll, P. [Universitaet Wuppertal, Fachbereich Physik, Wuppertal (Germany)

2017-06-15

Wide-angle Compton scattering (WACS) is discussed within the handbag approach in which the amplitudes are given by products of hard subprocess amplitudes and form factors, specific to Compton scattering, which represent 1/x-moments of generalized parton distributions (GPDs). The quality of our present knowledge of these form factors and of the underlying GPDs is examined. As will be discussed in some detail the form factor R{sub A} and the underlying GPD H are poorly known. It is argued that future data on the spin correlations A{sub LL} and/or K{sub LL} will allow for an extraction of R{sub A} which can be used to constrain the large -t behavior of H. (orig.)

Duality in diffraction dissociations

International Nuclear Information System (INIS)

Santoro, Alberto.

1977-01-01

Diffractive dissociations (aN→a*πN) are naturally explained and a model that accounts for the three-variable correlation (mass-transfer-Jackson angle correlation) is presented. This model takes into account the three possible exchanges: t (pion), u(a*) and s(a) channel exchanger. The physical consequences of the model are: a strong mass-slope correlation due to the zeros of the amplitude, a factorization of diffractive dissociations (factorization of the Pomeron), the possibility of extending this model to double diffractive dissociation and diffraction by nuclei. This model was applied to the NN→NπN reaction. Using the usual parameters of the Deck model, a comparison is made with experiments for all available distributions. the strong slope of the peak at 1400 MeV is naturally explained [fr

Diamond beamline I07: a beamline for surface and interface diffraction.

Science.gov (United States)

Nicklin, Chris; Arnold, Tom; Rawle, Jonathan; Warne, Adam

2016-09-01

Beamline I07 at Diamond Light Source is dedicated to the study of the structure of surfaces and interfaces for a wide range of sample types, from soft matter to ultrahigh vacuum. The beamline operates in the energy range 8-30 keV and has two endstations. The first houses a 2+3 diffractometer, which acts as a versatile platform for grazing-incidence techniques including surface X-ray diffraction, grazing-incidence small- (and wide-) angle X-ray scattering, X-ray reflectivity and grazing-incidence X-ray diffraction. A method for deflecting the X-rays (a double-crystal deflector) has been designed and incorporated into this endstation, extending the surfaces that can be studied to include structures formed on liquid surfaces or at liquid-liquid interfaces. The second experimental hutch contains a similar diffractometer with a large environmental chamber mounted on it, dedicated to in situ ultrahigh-vacuum studies. It houses a range of complementary surface science equipment including a scanning tunnelling microscope, low-energy electron diffraction and X-ray photoelectron spectroscopy ensuring that correlations between the different techniques can be performed on the same sample, in the same chamber. This endstation allows accurate determination of well ordered structures, measurement of growth behaviour during molecular beam epitaxy and has also been used to measure coherent X-ray diffraction from nanoparticles during alloying.

Wide angle view of MOCR activity during STS-3 mission

Science.gov (United States)

1982-01-01

Wide angle view of Mission Operation Control Room (MOCR) activity during Day 2 of STS-3 mission. This view shows many of th consoles, tracking map, and Eidophor-controlled data screens. Flight controllers in the foreground are (l.r.) R. John Rector and Chares L. Dumie. They are seated at the EECOM console. The 'thermodillo' contraption, used by flight controllers to indicate the Shuttle's position in relation to the sun for various tests, can be seen at right (28732); closeup view of the 'thermodillo'. The position of the armadillo's tail indicates position of the orbiter in relation to sun (28733); Mission Specialist/Astronaut Sally K. Ride, STS-3 orbit team spacecraft communicator (CAPCOM), talks to flight director during mission control center activity. Mission Specialist/Astronaut George D. Nelson, backup orbit team CAPCOM, watches the monitor at his console (28734).

Correlations in the hadronic double diffractive dissociation

International Nuclear Information System (INIS)

Goldegol, Alexandre.

1991-05-01

A given reaction of double diffractive dissociation is studied based on the three-component Deck Model. The correlations among the diffractive slope, the effective mass of the dissociated particle sub-system and the dissociation angle in the Gottfried-Jackson are studied based in this model. 9 refs, 19 figs

Interdiffusion in nanometer-scale multilayers investigated by in situ low-angle x-ray diffraction

Science.gov (United States)

Wang, Wei-Hua; Bai, Hai Yang; Zhang, Ming; Zhao, J. H.; Zhang, X. Y.; Wang, W. K.

1999-04-01

An in situ low-angle x-ray diffraction technique is used to investigate interdiffusion phenomena in various metal-metal and metal-amorphous Si nanometer-scale compositionally modulated multilayers (ML's). The temperature-dependent interdiffusivities are obtained by accurately monitoring the decay of the first-order modulation peak as a function of annealing time. Activation enthalpies and preexponential factors for the interdiffusion in the Fe-Ti, Ag-Bi, Fe-Mo, Mo-Si, Ni-Si, Nb-Si, and Ag-Si ML's are determined. Activation enthalpies and preexponential factors for the interdiffusion in the ML's are very small compared with that in amorphous alloys and crystalline solids. The relation between the atomic-size difference and interdiffusion in the ML's are investigated. The observed interdiffusion characteristics are compared with that in amorphous alloys and crystalline α-Zr, α-Ti, and Si. The experimental results suggest that a collective atomic-jumping mechanism govern the interdiffusion in the ML's, the collective proposal involving 8-15 atoms moving between extended nonequilibrium defects by thermal activation. The role of the interdiffusion in the solid-state reaction in the ML's is also discussed.

Angle change of the parent arteries after stent-assisted coil embolization of wide-necked intracranial bifurcation aneurysms

International Nuclear Information System (INIS)

Cho, W.-S.; Kang, H.-S.; Kim, J.E.; Kwon, O.-K.; Oh, C.W.; Cho, Y.D.; Han, M.H.

2014-01-01

Aim: To investigate the angle changes of the parent arteries after stent-assisted coil embolization of wide-necked intracranial bifurcation aneurysms. Materials and methods: The adjacent parent arterial angles before and after stent-assisted coil embolization were measured in 38 patients with aneurysms of the anterior communicating artery (ACoAA) and 41 patients with bifurcation aneurysms of the middle cerebral artery (MCABA). Variables were analysed in relation to the angle changes. Results: Vascular angles of the parent arteries significantly increased by 27.8° (±18.5°) immediately after stent-assisted coil embolization in 79 cases (p < 0.001), with 25.7° (±14.8°) in ACoAA and 29.7° (±21.4°) in MCABA, respectively. In 51 (64.6%) cases with follow-up angiography (mean interval 13.5 ± 4.1 months), vascular angles increased by 27.2° (±17.1°) immediately after treatment and further increased by 20.7° (±14.3°) at the last follow-up (all p < 0.001). More acute pre-stent angles of the parent arteries correlated with greater post-stent angle changes (p = 0.006). Younger age tended to be inversely related to post-stent angle changes (p = 0.091). Conclusion: Stent placement during coil embolization induced significant changes in the aneurysm–parent artery relationship. Further study is needed to elicit the association between angle change of the parent arteries and aneurysmal stability after coil embolization

Assessment of firing conditions in old fired-clay bricks. The contribution of X-ray powder diffraction with the Rietveld method and small angle neutron scattering

Czech Academy of Sciences Publication Activity Database

Viani, Alberto; Sotiriadis, Konstantinos; Len, A.; Šašek, Petr; Ševčík, Radek

2016-01-01

Roč. 116, June (2016), s. 33-43 ISSN 1044-5803 R&D Projects: GA MŠk(CZ) LO1219 Keywords : fired- clay brick * Rietveld method * small angle neutron scattering * X-ray diffraction * firing temperature Subject RIV: AL - Art, Architecture, Cultural Heritage Impact factor: 2.714, year: 2016 http://www.sciencedirect.com/science/article/pii/S1044580316300870

Wide-band all-angle acoustic self-collimation by rectangular sonic crystals with elliptical bases

International Nuclear Information System (INIS)

Cicek, Ahmet; Kaya, Olgun Adem; Ulug, Bulent

2011-01-01

Self-collimation of acoustic waves in the whole angular range of ±90 0 in the second and third bands of a two-dimensional rectangular sonic crystal with elliptical basis is demonstrated by examining the band structure and equifrequency contours. 70% and 77% of the second and third bands are available for wide-band all-angle self-collimation spanning a bandwidth of approximately 29% and 25% of the central frequencies of the all-angle self-collimation frequency ranges, respectively. Self-collimation of waves over large distances with a small divergence of beam width in the transverse direction is demonstrated through computations based on the finite element method. The second and third bands available for self-collimation are seen to vary linearly in the vast mid-range where a small group velocity dispersion prevents temporal divergence of waves with different frequencies.

Theory of hard diffraction and rapidity gaps

International Nuclear Information System (INIS)

Del Duca, V.

1995-06-01

In this talk we review the models describing the hard diffractive production of jets or more generally high-mass states in presence of rapidity gaps in hadron-hadron and lepton-hadron collisions. By rapidity gaps we mean regions on the lego plot in (pseudo)-rapidity and azimuthal angle where no hadrons are produced, between the jet(s) and an elastically scattered hadron (single hard diffraction) or between two jets (double hard diffraction). (orig.)

Posterior Vitreous Detachment as Observed by Wide-Angle OCT Imaging.

Science.gov (United States)

Tsukahara, Mayuka; Mori, Keiko; Gehlbach, Peter L; Mori, Keisuke

2018-04-06

Posterior vitreous detachment (PVD) plays an important role in vitreoretinal interface disorders. Historically, observations of PVD using OCT have been limited to the macular region. The purpose of this study is to image the wide-angle vitreoretinal interface after PVD in normal subjects using montaged OCT images. An observational cross-sectional study. A total of 144 healthy eyes of 98 normal subjects aged 21 to 95 years (51.4±22.0 [mean ± standard deviation]). Montaged images of horizontal and vertical OCT scans through the fovea were obtained in each subject. Montaged OCT images. By using wide-angle OCT, we imaged the vitreoretinal interface from the macula to the periphery. PVD was classified into 5 stages: stage 0, no PVD (2 eyes, both aged 21 years); stage 1, peripheral PVD limited to paramacular to peripheral zones (88 eyes, mean age 38.9±16.2 years, mean ± standard deviation); stage 2, perifoveal PVD extending to the periphery (12 eyes, mean age 67.9±8.4 years); stage 3, peripapillary PVD with persistent vitreopapillary adhesion alone (7 eyes, mean age 70.9±11.9 years); stage 4, complete PVD (35 eyes, mean age 75.1±10.1 years). All stage 1 PVDs (100%) were observed in the paramacular to peripheral region where the vitreous gel adheres directly to the cortical vitreous and retinal surface. After progression to stage 2 PVD, the area of PVD extends posteriorly to the perifovea and anteriorly to the periphery. Vitreoschisis was observed in 41.2% at PVD initiation (stage 1a). Whereas prior work suggests that PVD originates in the perifoveal region and after the sixth decade, our observations demonstrate that (1) PVD first appears even in the third decade of life and gradually appears more extensively throughout life; (2) more than 40% of eyes without fundus diseases at their PVD initiation are associated with vitreoschisis; and (3) PVD is first noted primarily in the paramacular-peripheral region where vitreous gel adheres to the retinal surface and is

Scleral Buckling Using a Non-contact Wide-Angle Viewing System with a 25-Gauge Chandelier Endoilluminator.

Science.gov (United States)

Jo, Jaehyuck; Moon, Byung Gil; Lee, Joo Yong

2017-12-01

To report the outcome of scleral buckling using a non-contact wide-angle viewing system with a 25-gauge chandelier endoilluminator. Retrospective analyses of medical records were performed for 17 eyes of 16 patients with primary rhegmatogenous retinal detachment (RRD) without proliferative vitreoretinopathy who had undergone conventional scleral buckling with cryoretinopexy using the combination of a non-contact wide-angle viewing system and chandelier endoillumination. The patients were eight males and five females with a mean age of 26.8 ± 10.2 (range, 11 to 47) years. The mean follow-up period was 7.3 ± 3.1 months. Baseline best-corrected visual acuity was 0.23 ± 0.28 logarithm of the minimum angle of resolution units. Best-corrected visual acuity at the final visit showed improvement (0.20 ± 0.25 logarithm of the minimum angle of resolution units), but the improvement was not statistically significant (p = 0.722). As a surgery-related complication, there was vitreous loss at the end of surgery in one eye. As a postoperative complication, increased intraocular pressure (four cases) and herpes simplex epithelial keratitis (one case) were controlled postoperatively with eye drops. One case of persistent RRD after primary surgery needed additional vitrectomy, and the retina was postoperatively attached. Scleral buckling with chandelier illumination as a surgical technique for RRD has the advantages of relieving the surgeon's neck pain from prolonged use of the indirect ophthalmoscope and sharing the surgical procedure with another surgical team member. In addition, fine retinal breaks that are hard to identify using an indirect ophthalmoscope can be easily found under the microscope by direct endoillumination. © 2017 The Korean Ophthalmological Society

Purification, crystallization, small-angle X-ray scattering and preliminary X-ray diffraction analysis of the SH2 domain of the Csk-homologous kinase

International Nuclear Information System (INIS)

Gunn, Natalie J.; Gorman, Michael A.; Dobson, Renwick C. J.; Parker, Michael W.; Mulhern, Terrence D.

2011-01-01

The Src-homology 2 (SH2) domain of Csk-family protein tyrosine kinases acts as a conformational switch to regulate their catalytic activity, which in turn promotes the inhibition of their proto-oncogenic targets, the Src-family kinases. Here, the expression, purification, small-angle X-ray scattering and preliminary diffraction analysis of the SH2 domain of the Csk-homologous kinase is reported. The C-terminal Src kinase (Csk) and Csk-homologous kinase (CHK) are endogenous inhibitors of the proto-oncogenic Src family of protein tyrosine kinases (SFKs). Phosphotyrosyl peptide binding to their Src-homology 2 (SH2) domains activates Csk and CHK, enhancing their ability to suppress SFK signalling; however, the detailed mechanistic basis of this activation event is unclear. The CHK SH2 was expressed in Escherichia coli and the purified protein was characterized as monomeric by synchrotron small-angle X-ray scattering in-line with size-exclusion chromatography. The CHK SH2 crystallized in 0.2 M sodium bromide, 0.1 M bis-Tris propane pH 6.5 and 20% polyethylene glycol 3350 and the best crystals diffracted to ∼1.6 Å resolution. The crystals belonged to space group P2, with unit-cell parameters a = 25.8, b = 34.6, c = 63.2 Å, β = 99.4°

A 2D MWPC area detector for use with synchrotron X-radiation at the Daresbury Laboratory for small angle diffraction and scattering

International Nuclear Information System (INIS)

Helliwell, J.R.; Hughes, G.; Przybylski, M.M.; Ridley, P.A.; Sumner, I.; Bateman, J.E.; Connolly, J.F.; Stephenson, R.

1982-01-01

A 2D multiwire proportional chamber area detector is being developed to provide a real time data acquisition system for small angle scattering and diffraction experiments with synchrotron X-radiation at the Daresbury synchrotron radiation source (SRS). The chamber has a circular aperture, 200 mm diameter with an anode and cathode wire pitch of 1 mm; a front cathode-anode spacing of 6 mm and a 6 mm spacing between anode and rear cathode. A 1 mm thick front beryllium window and a rear aluminium cover plate with indium seals provide a gas-tight system. Previous experiments with a similar chamber design allowed continual use of the chamber for up to 2 years without refill. A digitising time of 2 μs is expected based on a 260 mm delay line and Lecroy TDC linked to a mass semiconductor memory of 512 x 256 elements. The experiment will be controlled by a PDP 11/04 computer with 28 K memory interfaced to a CAMAC create with 64 K fast access CAMAC memory. The system should be relatively easy to use with good order to order resolution and reasonable rate for small angle diffraction and scattering experiments on biological systems. Evaluation of the set-up for protein crystallography is planned though a TV based image intensifier (Enraf-Nonius) is preferred for this application at the SRS. (orig.)

Wide-angle X-ray scattering study of heat-treated PEEK and PEEK composite

Science.gov (United States)

Cebe, Peggy; Lowry, Lynn; Chung, Shirley Y.; Yavrouian, Andre; Gupta, Amitava

1987-01-01

Samples of poly(etheretherketone) (PEEK) neat resin and APC-2 carbon fiber composite were subjected to various heat treatments, and the effect of quenching and annealing treatments was studied by wide-angle X-ray scattering. It is found that high-temperature treatments may introduce disorder into neat resin and composite PEEK when followed by rapid cooling. The disorder is metastable and can revert to ordered state when the material is heated above its glass transition temperature and then cooled slowly. The disorder may result from residual thermal stresses.

Diffracted X-ray tracking for monitoring intramolecular motion in individual protein molecules using broad band X-ray

Energy Technology Data Exchange (ETDEWEB)

Ichiyanagi, Kouhei; Sasaki, Yuji C. [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan); Japan Science and Technology Agency, CREST, CREST, Sasaki-Team, 609 Kiban Building, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8561 (Japan); Sekiguchi, Hiroshi; Hoshino, Masato; Kajiwara, Kentaro; Senba, Yasunori; Ohashi, Haruhiko; Ohta, Noboru [Japan Synchrotron Radiation Research Institute, SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan); Hoshisashi, Kentaro; Jae-won, Chang; Tokue, Maki; Matsushita, Yufuku [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan); Nishijima, Masaki; Inoue, Yoshihisa [Department of Applied Chemistry and Office for University-Industry Collaboration, Osaka University, 2-1 Yamadaoka, Suita, Osaka 565-0871 (Japan); Yagi, Naoto [Japan Science and Technology Agency, CREST, CREST, Sasaki-Team, 609 Kiban Building, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8561 (Japan); Japan Synchrotron Radiation Research Institute, SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan)

2013-10-15

Diffracted X-ray tracking (DXT) enables the tilting and twisting motions of single protein molecules to be monitored with micro- to milliradian resolution using a highly brilliant X-ray source with a wide energy bandwidth. We have developed a technique to monitor single molecules using gold nanocrystals attached to individual protein molecules using the BL28B2 beamline at SPring-8. In this paper we present the installation of a single toroidal X-ray mirror at BL28B2 to focus X-rays in an energy range of 10–20 keV (△E/E = 82% for an X-ray with a wide energy bandwidth). With this beamline we tracked diffraction spots from gold nanocrystals over a wide angle range than that using quasi-monochromatic X-rays. Application of the wide angle DXT technique to biological systems enabled us to observe the on-site motions of single protein molecules that have been functionalized in vivo. We further extend the capability of DXT by observing the fractional tilting and twisting motions of inner proteins under various conditions. As a proof of this methodology and to determine instrumental performance the intramolecular motions of a human serum albumin complex with 2-anthracenecarboxylic acid was investigated using the BL28B2 beamline. The random tilting and twisting intramolecular motions are shown to be directly linked to the movement of individual protein molecules in the buffer solution.

EVALUATION OF THE QUALITY OF ACTION CAMERAS WITH WIDE-ANGLE LENSES IN UAV PHOTOGRAMMETRY

OpenAIRE

Hastedt, H.; Ekkel, T.; Luhmann, T.

2016-01-01

The application of light-weight cameras in UAV photogrammetry is required due to restrictions in payload. In general, consumer cameras with normal lens type are applied to a UAV system. The availability of action cameras, like the GoPro Hero4 Black, including a wide-angle lens (fish-eye lens) offers new perspectives in UAV projects. With these investigations, different calibration procedures for fish-eye lenses are evaluated in order to quantify their accuracy potential in UAV photogrammetry....

Theory of hard diffraction and rapidity gaps

International Nuclear Information System (INIS)

Del Duca, V.

1996-01-01

In this talk we review the models describing the hard diffractive production of jets or more generally high-mass states in presence of rapidity gaps in hadron-hadron and lepton-hadron collisions. By rapidity gaps we mean regions on the lego plot in (pseudo)-rapidity and azimuthal angle where no hadrons are produced, between the jet(s) and an elastically scattered hadron (single hard diffraction) or between two jets (double hard diffraction). copyright 1996 American Institute of Physics

Piezo activated mode tracking system for widely tunable mode-hop-free external cavity mid-IR semiconductor lasers

Science.gov (United States)

Wysocki, Gerard (Inventor); Tittel, Frank K. (Inventor); Curl, Robert F. (Inventor)

2010-01-01

A widely tunable, mode-hop-free semiconductor laser operating in the mid-IR comprises a QCL laser chip having an effective QCL cavity length, a diffraction grating defining a grating angle and an external cavity length with respect to said chip, and means for controlling the QCL cavity length, the external cavity length, and the grating angle. The laser of claim 1 wherein said chip may be tuned over a range of frequencies even in the absence of an anti-reflective coating. The diffraction grating is controllably pivotable and translatable relative to said chip and the effective QCL cavity length can be adjusted by varying the injection current to the chip. The laser can be used for high resolution spectroscopic applications and multi species trace-gas detection. Mode-hopping is avoided by controlling the effective QCL cavity length, the external cavity length, and the grating angle so as to replicate a virtual pivot point.

Diffraction at TOTEM

OpenAIRE

Antchev, G.; Aspell, P.; Avati, V.; Bagliesi, M.G.; Berardi, V.; Berretti, M.; Bottigli, U.; Bozzo, M.; Brucken, E.; Buzzo, A.; Cafagna, F.; Calicchio, M.; Catanesi, M.G.; Catastini, P.L.; Cecchi, R.

2008-01-01

The TOTEM experiment at the LHC measures the total proton-proton cross section with the luminosity-independent method and the elastic proton-proton cross-section over a wide |t|-range. It also performs a comprehensive study of diffraction, spanning from cross-section measurements of individual diffractive processes to the analysis of their event topologies. Hard diffraction will be studied in collaboration with CMS taking advantage of the large common rapidity coverage for charged and neutral...

Stress induced modulation of magnetic domain diffraction of single crystalline yttrium iron garnet

Science.gov (United States)

Mito, Shinichiro; Yoshihara, Yuki; Takagi, Hiroyuki; Inoue, Mitsuteru

2018-05-01

Stress induced modulation of the diffraction angle and efficiency of the light reflected from a stripe-domain magnetic garnet was demonstrated. The spacing of the magnetic domain was changed using the inverse magnetostriction effect. The sample structure was a piezo actuator/Al reflection layer/magnetic garnet substrate. A diffraction angle between the 0th and 1st ordered light was changed from 9.12 deg. to 10.20 deg. This result indicates that the domain spacing was changed from 3.3 μm to 3.0 μm. The change of the diffraction angle was irreversible for the voltage. However, reversible, linear and continuous change of the diffraction efficiency was observed. These results could be applicable for a voltage-driven optical solid state light deflector with low power consumption and high switching speed.

Optimization of nonimaging focusing heliostat in dynamic correction of astigmatism for a wide range of incident angles.

Science.gov (United States)

Chong, Kok-Keong

2010-05-15

To overcome astigmatism has always been a great challenge in designing a heliostat capable of focusing the sunlight on a small receiver throughout the year. In this Letter, a nonimaging focusing heliostat with a dynamic adjustment of facet mirrors in a group manner has been analyzed for optimizing the astigmatic correction in a wide range of incident angles. This what is to the author's knowledge a new heliostat is not only designed to serve the purpose of concentrating sunlight to several hundreds of suns, but also to significantly reduce the variation of the solar flux distribution with the incident angle.

The design and q resolution of the small and wide angle neutron scattering instrument (TAIKAN) in J-PARC

International Nuclear Information System (INIS)

Takata, Shin-ichi; Suzuki, Jun-ichi; Shinohara, Takenao; Oku, Takayuki; Tominaga, Taiki; Nakatani, Takeshi; Inamura, Yasuhiro; Suzuya, Kentaro; Aizawa, Kazuya; Arai, Masatoshi; Ohishi, Kazuki; Iwase, Hiroki; Ito, Takayoshi; Otomo, Toshiya; Sugiyama, Masaaki

2015-01-01

The small and wide angle neutron scattering instrument (TAIKAN) is designed to cover the wide q range of 0.005 0.3 Å"-"1 with the other banks. The q resolution was compared with the values experimentally obtained from the widths of Bragg peaks of a standard sample, silver behenate. The results of the experiment were consistent with the theory. It was confirmed that TAIKAN was completed as was expected. (author)

Crystallization behavior of polyethylene on silicon wafers in solution casting processes traced by time-resolved measurements of synchrotron grazing-incidence small-angle and wide-angle X-ray scattering

International Nuclear Information System (INIS)

Sasaki, S; Masunaga, H; Takata, M; Itou, K; Tashiro, K; Okuda, H; Takahara, A

2009-01-01

Crystallization behavior of polyethylene (PE) on silicon wafers in solution casting processes has been successfully traced by time-resolved grazing-incidence small-angle and wide-angle X-ray scattering (GISWAXS) measurements utilizing synchrotron radiation. A p-xylene solution of PE kept at ca. 343 K was dropped on a silicon wafer at ca. 298 K. While the p-xylene evaporated naturally from the dropped solution sample, PE chains crystallized to be a thin film. Raman spectral measurements were performed simultaneously with the GISWAXS measurements to evaluate quantitatively the p-xylene the dropped solution contained. Grazing-incidence wide-angle X-ray scattering (GIWAXS) patterns indicated nucleation and crystal growth in the dropped solution and the following as-cast film. GIWAXS and Raman spectral data revealed that crystallization of PE was enhanced after complete evaporation of the p-xylene from the dropped solution. The [110] and [200] directions of the orthorhombic PE crystal became relatively parallel to the wafer surface with time, which implied that the flat-on lamellae with respect to the wafer surface were mainly formed in the as-cast film. On the other hand, grazing-incidence small-angle X-ray scattering (GISAXS) patterns implied formation of isolated lamellae in the dropped solution. The lamellae and amorphous might alternatively be stacked in the preferred direction perpendicular to the wafer surface. The synchrotron GISWAXS experimental method could be applied for kinetic study on hierarchical structure of polymer thin films.

Diffraction at TOTEM

OpenAIRE

Giani, S; Niewiadomski, H; Antchev, G; Aspell, P; Avati, V; Bagliesi, M G; Berardi, V; Berretti, M; Besta, M; Bozzo, M; Brücken, E; Buzzo, A; Cafagna, F; Calicchio, M; Catanesi, M G

2010-01-01

The primary objective of the TOTEM experiment at the LHC is the measurement of the total proton-proton cross section with the luminosity-independent method and the study of elastic proton-proton cross-section over a wide |t|-range. In addition TOTEM also performs a comprehensive study of diffraction, spanning from cross-section measurements of individual diffractive processes to the analysis of their event topologies. Hard diffraction will be studied in collaboration with CMS taking advantage...

Low angle X-ray scattering

International Nuclear Information System (INIS)

Torrianni, I.L.

1983-01-01

The theoretical and experimental problems appearing in diffraction experiments at very low angles by several kinds of materials are discussed. The importance of synchrotron radiation in such problems is shown. (L.C.) [pt

Influence of microfibril angle on the thermal and dynamic-mechanical properties of Acacia Mangium wood using X-ray diffraction and dynamics-mechanical test

International Nuclear Information System (INIS)

Tabet, T.A.; Julynnie Wajir; Fauziah Abdul Aziz

2009-01-01

The term microfibril angle, MFA in wood science refers to the angle between the direction of the helical windings of cellulose microfibrils in the secondary cell wall, S 2 layer of fibers and tracheids and the long axis of the cell. In this study, the mean MFA of the cell walls were determined for thin samples of thickness 200.0 μm from pith and outwards, for eight ages of Acacia Mangium wood. The determination of MFA was based on a diffraction pattern arising from cellulose crystal planes of the type 002 generated by x-ray diffraction and recorded using an electronic detector. The results show an inversely relationship between MFA and age of tree in Acacia mangium wood. MFA decreased from 26.13 degree at age 3 year-old to 0.20 degree at tree of age 15 year-old for the pith region. The most significant drop occurred from 16.14 degree at age 7 year-old to 11.30 degree at age 9 year-old. an inversely relationship between MFA and storage modulus E ' was evidence in Acacia mangium at age 10 year-old. The results showed that about 76.22 % variation of loss modulus E was attributed to the MFA, while about 66.4 % of the variation of glass transition T g was explained by MFA under the same experimental conditions. (author)

Diffraction tomography for plasma refractive index measurements

International Nuclear Information System (INIS)

Howard, J.; Nazikian, R.; Sharp, L.E.

1989-01-01

Measurement of the properties of probing beams of coherent electromagnetic radiation yields essential information about the line of sight integrated plasma refractive index. Presented is a scalar diffraction treatment of forward angle scattering plasma diagnostics based on the diffraction projection theorem first presented by E. Wolf in 1969. New results are obtained for near field scattering from probing Gaussian beams and it is demonstrated that the effects of diffraction need to be addressed for tomographic inversion of near field scattering and interferometry data. 33 refs., 10 figs

Theory of magnetic neutron small-angle scattering using the dynamical theory of diffraction instead of the Born approximation. I

International Nuclear Information System (INIS)

Schaerpf, O.

1978-01-01

Two ways are given for solving the problem of the dependence of the refraction on the direction of magnetization on both sides of the refractive boundary, one applying the Halpern magnetic scattering vector, the other applying the dynamical theory of diffraction. They lead to different results. Experimental investigation of refraction by magnetic boundaries shows no dependence of the angle of deflection on the relative angles of magnetization in adjacent domains. This behaviour is only described correctly by the dynamical theory, which far from Laue reflections leads to a treatment by the Schoedinger equation with a spin-dependent potential dependent on the average continuous homogenous magnetic induction, both for the law of refraction and for the precession of the spin. The results of this treatment are discussed as a consequence of the behaviour of the spin of the neutrons. This gives some insight about how and why, with refraction, the intensities of the direct and deflected beams depend on the magnetization directions in adjacent domains. The dynamical theory also shows that the Halpern magnetic scattering vector applies only with Laue or Bragg reflections and not with transmission far from those reflections. (Auth.)

X-ray diffraction and NMR data for the study of the location of idebenone and idebenol in model membranes

Directory of Open Access Journals (Sweden)

Victoria Gómez-Murcia

2016-06-01

Full Text Available Here we present some of our data about the interaction of idebenone and idebenol with dipalmitoyl-phosphatidylcholine (DPPC. In particular, we include data of small angle X-ray diffraction (SAXD and wide angle X-ray diffraction experiments, obtention of electronic profiles of the membranes, 2H-NMR and 31P-NMR, as part of the research article: “Both idebenone and idebenol are localized near the lipid-water interface of the membrane and increase its fluidity” (Gomez-Murcia et al., 2016 [1]. These data were obtained from model membranes that included different proportions of idebenone and idebenol, at temperatures both above and below of the gel to fluid phase. The X-ray experiments were carried out by using a modified Kratky compact camera (MBraun-Graz-Optical Systems, Graz Austria, incorporating two coupled linear position sensitive detectors. The NMR data were collected from a a Bruker Avance 600 instrument.

Diffraction enhanced imaging: a simple model

International Nuclear Information System (INIS)

Zhu Peiping; Yuan Qingxi; Huang Wanxia; Wang Junyue; Shu Hang; Chen Bo; Liu Yijin; Li Enrong; Wu Ziyu

2006-01-01

Based on pinhole imaging and conventional x-ray projection imaging, a more general DEI (diffraction enhanced imaging) equation is derived using simple concepts in this paper. Not only can the new DEI equation explain all the same problems as with the DEI equation proposed by Chapman, but also some problems that cannot be explained with the old DEI equation, such as the noise background caused by small angle scattering diffracted by the analyser

Diffraction enhanced imaging: a simple model

Energy Technology Data Exchange (ETDEWEB)

Zhu Peiping; Yuan Qingxi; Huang Wanxia; Wang Junyue; Shu Hang; Chen Bo; Liu Yijin; Li Enrong; Wu Ziyu [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049 (China)

2006-10-07

Based on pinhole imaging and conventional x-ray projection imaging, a more general DEI (diffraction enhanced imaging) equation is derived using simple concepts in this paper. Not only can the new DEI equation explain all the same problems as with the DEI equation proposed by Chapman, but also some problems that cannot be explained with the old DEI equation, such as the noise background caused by small angle scattering diffracted by the analyser.

Computational design for a wide-angle cermet-based solar selective absorber for high temperature applications

International Nuclear Information System (INIS)

Sakurai, Atsushi; Tanikawa, Hiroya; Yamada, Makoto

2014-01-01

The purpose of this study is to computationally design a wide-angle cermet-based solar selective absorber for high temperature applications by using a characteristic matrix method and a genetic algorithm. The present study investigates a solar selective absorber with tungsten–silica (W–SiO 2 ) cermet. Multilayer structures of 1, 2, 3, and 4 layers and a wide range of metal volume fractions are optimized. The predicted radiative properties show good solar performance, i.e., thermal emittances, especially beyond 2 μm, are quite low, in contrast, solar absorptance levels are successfully high with wide angular range, so that solar photons are effectively absorbed and infrared radiative heat loss can be decreased. -- Highlights: • Electromagnetic simulation of radiative properties by characteristic matrix method. • Optimization for multilayered W–SiO 2 cermet-based absorber by a Genetic Algorithm. • We propose a successfully high solar performance of solar selective absorber

Vectorial diffraction properties of THz vortex Bessel beams.

Science.gov (United States)

Wu, Zhen; Wang, Xinke; Sun, Wenfeng; Feng, Shengfei; Han, Peng; Ye, Jiasheng; Yu, Yue; Zhang, Yan

2018-01-22

A vortex Bessel beam combines the merits of an optical vortex and a Bessel beam, including a spiral wave front and a non-diffractive feature, which has immense application potentials in optical trapping, optical fabrication, optical communications, and so on. Here, linearly and circularly polarized vortex Bessel beams in the terahertz (THz) frequency range are generated by utilizing a THz quarter wave plate, a spiral phase plate, and Teflon axicons with different opening angles. Taking advantage of a THz focal-plane imaging system, vectorial diffraction properties of the THz vortex Bessel beams are comprehensively characterized and discussed, including the transverse (Ex, Ey) and longitudinal (Ez) polarization components. The experimental phenomena are accurately simulated by adopting the vectorial Rayleigh diffraction integral. By varying the opening angle of the axicon, the characteristic parameters of these THz vortex Bessel beams are exhibited and compared, including the light spot size, the diffraction-free range, and the phase evolution process. This work provides the precise experimental and theoretical bases for the comprehension and application of a THz vortex Bessel beam.

Agreement between image grading of conventional (45°) and ultra wide-angle (200°) digital images in the macula in the Reykjavik eye study.

Science.gov (United States)

Csutak, A; Lengyel, I; Jonasson, F; Leung, I; Geirsdottir, A; Xing, W; Peto, T

2010-10-01

To establish the agreement between image grading of conventional (45°) and ultra wide-angle (200°) digital images in the macula. In 2008, the 12-year follow-up was conducted on 573 participants of the Reykjavik Eye Study. This study included the use of the Optos P200C AF ultra wide-angle laser scanning ophthalmoscope alongside Zeiss FF 450 conventional digital fundus camera on 121 eyes with or without age-related macular degeneration using the International Classification System. Of these eyes, detailed grading was carried out on five cases each with hard drusen, geographic atrophy and chorioretinal neovascularisation, and six cases of soft drusen. Exact agreement and κ-statistics were calculated. Comparison of the conventional and ultra wide-angle images in the macula showed an overall 96.43% agreement (κ=0.93) with no disagreement at end-stage disease; although in one eye chorioretinal neovascularisation was graded as drusenoid pigment epithelial detachment. Of patients with drusen only, the exact agreement was 96.1%. The detailed grading showed no clinically significant disagreement between the conventional 45° and 200° images. On the basis of our results, there is a good agreement between grading conventional and ultra wide-angle images in the macula.

Quasi-Bragg diffraction of atoms

NARCIS (Netherlands)

Domen, K.F.E.M.; Jansen, M.A.H.M.; Leeuwen, van K.A.H.

2006-01-01

We report on a novel atomic beamsplitter. It combines the advantages of Bragg scattering (transfer possible into a single, very high diffraction order due to adiabatic conservation of ‘transverse kinetic energy’) with the convenience of tuning the splitting angle simply by adjusting a magnetic

Colour-singlet exchange and tests of models of diffractive DIS

International Nuclear Information System (INIS)

Williams, J.C.

2000-03-01

Diffractive deep-inelastic scattering events observed at the HERA electron-proton collider are interpreted as an interaction involving a virtual photon scattering off a colour-singlet state within the proton. Models which attempt to describe the colour-singlet exchanged in diffractive interactions range from the purely phenomenological Donnachie-Landshoff form factor approach to the QCD-motivated gluon-exchange models and the scalar-pomeron model. It is important to find ways to test these models. In this thesis colour-singlet exchange models of diffractive DIS are compared with cross section and structure function data from the H1 detector. H1 select diffractive data by requiring there to be a large angle between the forward proton direction and any other significant detector activity. This pseudo-rapidity gap cut extracts colour-singlet exchange events from the standard DIS data sample. For a wide range of the parameter space covered by the HERA experiments, however, the pseudo-rapidity gap cuts restrict the final-state phase space available for diffractive scattering. One consequence is that pseudo-rapidity gap cuts can be used to select diffractive events in which the colour-singlet only couples to off-shell partons. To leading order in the strong coupling constant, the diffractive final state consists of a quark-antiquark pair. Higher-order events include diffractive production of quark-antiquark-gluon states. In the region where pseudo-rapidity gap cuts restrict the accessible phase space, the cuts reject low transverse momentum quark-antiquark diffractive events. Pseudo-rapidity gap data selection cuts also allow selection of an enhanced 3-jet data sample. The structure function and transverse momentum distribution data can be described by either a two-gluon model or by the Donnachie-Landshoff model, both models requiring a significant contribution from quark-antiquark-gluon diffractive final states to fit the full kinematic range of the diffractive data

Characterization of thin-film multilayers using magnetization curves and modeling of low-angle X-ray diffraction data

Energy Technology Data Exchange (ETDEWEB)

Lane, M. [Emory & Henry College, VA (United States); Chaiken, A.; Michel, R.P. [Lawrence Livermore National Lab., CA (United States)

1994-12-01

We have characterized thin-film multilayers grown by ion-beam sputtering using magnetization curves and modeling of low-angle x-ray diffraction data. In our films, we use ferromagnetic layer = Co, Fe, and NiFe and spacer layer = Si, Ge, FeSi{sub 2}, and CoSi{sub 2}. We have studied the effects of (1) deposition conditions; (2) thickness of layers; (3) different layer materials; and (4) annealing. We find higher magnetization in films grown at 1000V rather than 500V and in films with spacer layers of 50{angstrom} rather than 100{angstrom}. We find higher coercivity in films with cobalt grown on germanium rather than silicon, metal grown on gold underlayers rather than on glass substrates, and when using thinner spacer layers. Finally, modeling reveals that films grown with disilicide layers are more thermally stable than films grown with silicon spacer layers.

A gas microstrip wide angle X-ray detector for application in synchrotron radiation experiments

CERN Document Server

Bateman, J E; Derbyshire, G E; Duxbury, D M; Lipp, J; Mir, J A; Simmons, J E; Spill, E J; Stephenson, R; Dobson, B R; Farrow, R C; Helsby, W I; Mutikainen, R; Suni, I

2002-01-01

The Gas Microstrip Detector has counting rate capabilities several orders of magnitude higher than conventional wire proportional counters while providing the same (or better) energy resolution for X-rays. In addition the geometric flexibility provided by the lithographic process combined with the self-supporting properties of the substrate offers many exciting possibilities for X-ray detectors, particularly for the demanding experiments carried out on Synchrotron Radiation Sources. Using experience obtained in designing detectors for Particle Physics we have developed a detector for Wide Angle X-ray Scattering studies. The detector has a fan geometry which makes possible a gas detector with high detection efficiency, sub-millimetre spatial resolution and good energy resolution over a wide range of X-ray energy. The detector is described together with results of experiments carried out at the Daresbury Laboratory Synchrotron Radiation Source.

Concept development for the ITER equatorial port visible/infrared wide angle viewing system

International Nuclear Information System (INIS)

Reichle, R.; Beaumont, B.; Boilson, D.; Bouhamou, R.; Direz, M.-F.; Encheva, A.; Henderson, M.; Kazarian, F.; Lamalle, Ph.; Lisgo, S.; Mitteau, R.; Patel, K. M.; Pitcher, C. S.; Pitts, R. A.; Prakash, A.; Raffray, R.; Schunke, B.; Snipes, J.; Diaz, A. Suarez; Udintsev, V. S.

2012-01-01

The ITER equatorial port visible/infrared wide angle viewing system concept is developed from the measurement requirements. The proposed solution situates 4 viewing systems in the equatorial ports 3, 9, 12, and 17 with 4 views each (looking at the upper target, the inner divertor, and tangentially left and right). This gives sufficient coverage. The spatial resolution of the divertor system is 2 times higher than the other views. For compensation of vacuum-vessel movements, an optical hinge concept is proposed. Compactness and low neutron streaming is achieved by orienting port plug doglegs horizontally. Calibration methods, risks, and R and D topics are outlined.

Super-broadband non-diffraction guiding modes in photonic crystals with elliptical rods

Energy Technology Data Exchange (ETDEWEB)

Liang, W Y; Wang, T B; Yin, C P; Dong, J W; Leng, F C; Wang, H Z, E-mail: stswhz@mail.sysu.edu.c [State Key Laboratory of Optoelectronic Materials and Technologies, Zhongshan (Sun Yat-Sen) University, Guangzhou 510275 (China)

2010-02-24

Non-diffraction guiding modes covering the full broad band of a photonic crystal with elliptical rods for TM mode are reported in this paper. All such modes can be used to effectively guide electromagnetic waves since they have near-zero group velocity components along the {Gamma}X' direction. In the fourth dispersion surface of the photonic crystal, the two wide flat regions spanning the first Brillouin zone possess unique properties: one dimension corresponds to a broad band, while the other corresponds to full incident angles of 0-90{sup 0}. These properties have many potential applications; as an example, here a broadband all-angle supercollimation with a bandwidth of 169 nm around 1550 nm is demonstrated. For the inverted structure of elliptical holes in a dielectric, similar results can be achieved over 140 nm around 1550 nm for TE mode.

An upgrade beamline for combined wide, small and ultra small-angle x-ray scattering at the ESRF

Energy Technology Data Exchange (ETDEWEB)

Van Vaerenbergh, Pierre; Léonardon, Joachim; Sztucki, Michael; Boesecke, Peter; Gorini, Jacques; Claustre, Laurent; Sever, Franc; Morse, John; Narayanan, Theyencheri [ESRF - The European Synchrotron, F-38043 Grenoble (France)

2016-07-27

This contribution presents the main design features of the upgraded beamline ID02 (TRUSAXS). The beamline combines different small-angle X-ray scattering techniques in one unique instrument. The key component of this instrument is an evacuated (5×10{sup −3} mbar) stainless steel detector tube of length 34 m and diameter 2 m. Three different detectors (Rayonix MX170, Pilatus 300 K and FReLoN 4M) are housed inside a motorized wagon which travels along a rail system with very low parasitic lateral movements (± 0.3 mm). This system allows automatically changing the sample-to-detector distance from about 1 m to 31 m and selecting the desired detector. In addition, a wide angle detector (Rayonix LX170) is installed just above the entrance cone of the tube for optional wide-angle X-ray scattering measurements. The beamstop system enables monitoring of the X-ray beam intensity in addition to blocking the primary beam, and automated insertion of selected masks behind the primary beamstop. The focusing optics and collimation system permit to cover a scattering vector (q) range of 0.002 nm{sup −1} ≤ q ≤ 50 nm{sup −1} with one unique setting using 0.1 nm X-ray wavelength for moderate flux (5×10{sup 12} photons/sec). However, for higher flux (6x10{sup 13} photons/sec) or higher resolution (minimum q < 0.001 nm{sup −1}), focusing and collimation, respectively need to be varied. For a sample-to-detector distance of 31 m and 0.1 nm wavelength, two dimensional ultra small-angle X-ray scattering patterns can be recorded down to q≈0.001 nm{sup −1} with far superior quality as compared to one dimensional profiles obtained with a Bonse-Hart instrument.

Space resolved x-ray diffraction measurements of the supercooled state of polymers

International Nuclear Information System (INIS)

Asano, Tsutomu; Yoshida, Shinya; Nishida, Akira; Mina, M.F.

2002-01-01

In order to measure an ordering process of polymers, the supercooled state near the crystallizing surface was observed by a space resolved X-ray diffraction method at Photon Factory (PF). Using temperature slope crystallization, low density polyethylene and even-number paraffins were examined during crystallization from the melt state. The results indicate that polyethylene shows a sharp b-axis orientation where the lamellar normal and crystalline c-axis are perpendicular to the temperature slope. The crystalline lamellae are well-developed with lamellar thickness of 180 A. The supercooled melt state just above the crystallizing plane shows some diffraction in the small angle region without any crystalline reflection in the wide angle. This fact suggests that a long-range ordering (lamellar structure) appears prior to the short-range one (crystalline structure). The in-situ crystallizing surface was observed by an optical microscope connected to a TV system. The crystallizing surface of even-number paraffins moves to upwards in the temperature slope. In-situ X-ray measurements at PF revealed that the crystalline c-axis and lamellar normal of the even number paraffins are parallel to the temperature slope. From these results, the crystalline ordering and the surface movement of even number paraffins are explained using special nucleation mechanism including a screw dislocation. (author)

A hands-free region-of-interest selection interface for solo surgery with a wide-angle endoscope: preclinical proof of concept.

Science.gov (United States)

Jung, Kyunghwa; Choi, Hyunseok; Hong, Hanpyo; Adikrishna, Arnold; Jeon, In-Ho; Hong, Jaesung

2017-02-01

A hands-free region-of-interest (ROI) selection interface is proposed for solo surgery using a wide-angle endoscope. A wide-angle endoscope provides images with a larger field of view than a conventional endoscope. With an appropriate selection interface for a ROI, surgeons can also obtain a detailed local view as if they moved a conventional endoscope in a specific position and direction. To manipulate the endoscope without releasing the surgical instrument in hand, a mini-camera is attached to the instrument, and the images taken by the attached camera are analyzed. When a surgeon moves the instrument, the instrument orientation is calculated by an image processing. Surgeons can select the ROI with this instrument movement after switching from 'task mode' to 'selection mode.' The accelerated KAZE algorithm is used to track the features of the camera images once the instrument is moved. Both the wide-angle and detailed local views are displayed simultaneously, and a surgeon can move the local view area by moving the mini-camera attached to the surgical instrument. Local view selection for a solo surgery was performed without releasing the instrument. The accuracy of camera pose estimation was not significantly different between camera resolutions, but it was significantly different between background camera images with different numbers of features (P solo surgeries without a camera assistant.

Variable angle asymmetric cut monochromator

International Nuclear Information System (INIS)

Smither, R.K.; Fernandez, P.B.

1993-09-01

A variable incident angle, asymmetric cut, double crystal monochromator was tested for use on beamlines at the Advanced Photon Source (APS). For both undulator and wiggler beams the monochromator can expand area of footprint of beam on surface of the crystals to 50 times the area of incident beam; this will reduce the slope errors by a factor of 2500. The asymmetric cut allows one to increase the acceptance angle for incident radiation and obtain a better match to the opening angle of the incident beam. This can increase intensity of the diffracted beam by a factor of 2 to 5 and can make the beam more monochromatic, as well. The monochromator consists of two matched, asymmetric cut (18 degrees), silicon crystals mounted so that they can be rotated about three independent axes. Rotation around the first axis controls the Bragg angle. The second rotation axis is perpendicular to the diffraction planes and controls the increase of the area of the footprint of the beam on the crystal surface. Rotation around the third axis controls the angle between the surface of the crystal and the wider, horizontal axis for the beam and can make the footprint a rectangle with a minimum. length for this area. The asymmetric cut is 18 degrees for the matched pair of crystals, which allows one to expand the footprint area by a factor of 50 for Bragg angles up to 19.15 degrees (6 keV for Si[111] planes). This monochromator, with proper cooling, will be useful for analyzing the high intensity x-ray beams produced by both undulators and wigglers at the APS

Surface and interface strains studied by x-ray diffraction

International Nuclear Information System (INIS)

Akimoto, Koichi; Emoto, Takashi; Ichimiya, Ayahiko

1998-01-01

The authors have developed a technique of X-ray diffraction in order to measure strain fields near semiconductor surface and interface. The diffraction geometry is using the extremely asymmetric Bragg-case bulk reflection of a small incident angle to the surface and a large angle exiting from the surface. The incident angle of the X-rays is set near critical angle of total reflection by tuning X-ray energy of synchrotron radiation at the Photon Factory, Japan. For thermally grown-silicon oxide/Si(100) interface, the X-ray intensity of the silicon substrate 311 reflection has been measured. From comparison of the full width at half maxima (FWHM) of X-ray rocking curves of various thickness of silicon oxides, it has been revealed that silicon substrate lattice is highly strained in the thin (less than about 5 nm) silicon oxide/silicon system. In order to know the original silicon surface strain, the authors have also performed the same kind of measurements in the ultra-high vacuum chamber. A clean Si(111) 7x7 surface gives sharper X-ray diffraction peak than that of the native oxide/Si(111) system. From these measurements, it is concluded that the thin silicon oxide film itself gives strong strain fields to the silicon substrates, which may be the reason of the existence of the structural transition layer at the silicon oxide/Si interface

Beam steering for virtual/augmented reality displays with a cycloidal diffractive waveplate.

Science.gov (United States)

Chen, Haiwei; Weng, Yishi; Xu, Daming; Tabiryan, Nelson V; Wu, Shin-Tson

2016-04-04

We proposed a switchable beam steering device with cycloidal diffractive waveplate (CDW) for eye tracking in a virtual reality (VR) or augmented reality (AR) display system. Such a CDW diffracts the incident circularly polarized light to the first order with over 95% efficiency. To convert the input linearly polarized light to right-handed or left-handed circular polarization, we developed a broadband polarization switch consisting of a twisted nematic liquid crystal cell and an achromatic quarter-wave retardation film. By cascading 2-3 CDWs together, multiple diffraction angles can be achieved. To suppress the color dispersion, we proposed two approaches to obtain the same diffraction angle for red, green, and blue LEDs-based full color displays. Our device exhibits several advantages, such as high diffraction efficiency, fast response time, low power consumption, and low cost. It holds promise for the emerging VR/AR displays.

Influence of preferred orientation of minerals in the mineralogical identification process by X-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Silva, Amanda Luzia da; Oliveira, Arno H. de [Universidade Federal de Minas Gerais (DEN/UFMG), Belo Horizonte, MG (Brazil). Dept. de Engenharia Nuclear; Fernandes, Maria Lourdes Souza, E-mail: lourdesfernandes@ufmg.b [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil). Inst. de GeoCiencias. Centro de Pesquisa Professor Manoel Teixeira da Costa

2011-07-01

The X-ray diffraction corresponds to one of the main techniques for characterization of microstructures in crystalline materials, widely used in the identification of minerals in samples of geological materials. Some minerals have a property called preferred orientation which corresponds to the orientation tendency of the crystals of ground minerals to orient themselves in certain directions according to a preferred crystallographic plane. This property affects the analysis by X-ray diffraction and this fact can generates erroneous results in the characterization. The purpose of this study is to identify the negative influence of the preferred orientation of a mineral in the generation of diffraction patterns obtained in the X-ray diffraction analysis. For this, a sample of muscovite, a mineral of mica group, was prepared by two different methods: the frontal method and the back loading method. In the analysis using the frontal method there was displacement of the XRD pattern in the abscissa axis, where it was observed changes in interplanar distance and angle 2{theta} values, which are essential information for characterization and identification of a mineral. In the analysis using the back loading method, the generated XRD pattern showed no displacement in the axis of abscissas and showed interplanar distance and angle 2{theta} values closer to the real values for the muscovite. The results showed that one can only make improvements to the process of sample preparation minimizing the effect of preferred orientation in the analysis. There is no need to change conditions of diffractometer measurements. (author)

Influence of preferred orientation of minerals in the mineralogical identification process by X-ray diffraction

International Nuclear Information System (INIS)

Silva, Amanda Luzia da; Oliveira, Arno H. de; Fernandes, Maria Lourdes Souza

2011-01-01

The X-ray diffraction corresponds to one of the main techniques for characterization of microstructures in crystalline materials, widely used in the identification of minerals in samples of geological materials. Some minerals have a property called preferred orientation which corresponds to the orientation tendency of the crystals of ground minerals to orient themselves in certain directions according to a preferred crystallographic plane. This property affects the analysis by X-ray diffraction and this fact can generates erroneous results in the characterization. The purpose of this study is to identify the negative influence of the preferred orientation of a mineral in the generation of diffraction patterns obtained in the X-ray diffraction analysis. For this, a sample of muscovite, a mineral of mica group, was prepared by two different methods: the frontal method and the back loading method. In the analysis using the frontal method there was displacement of the XRD pattern in the abscissa axis, where it was observed changes in interplanar distance and angle 2θ values, which are essential information for characterization and identification of a mineral. In the analysis using the back loading method, the generated XRD pattern showed no displacement in the axis of abscissas and showed interplanar distance and angle 2θ values closer to the real values for the muscovite. The results showed that one can only make improvements to the process of sample preparation minimizing the effect of preferred orientation in the analysis. There is no need to change conditions of diffractometer measurements. (author)

Photoelectron diffraction and holography: Present status and future prospects

Energy Technology Data Exchange (ETDEWEB)

Fadley, C.S. [California Univ., Davis, CA (United States). Dept. of Physics]|[Lawrence Berkeley Lab., CA (United States); Thevuthasan, S. [California Univ., Davis, CA (United States). Dept. of Physics; Kaduwela, A.P. [Lawrence Berkeley Lab., CA (United States)] [and others

1993-07-01

Photoelectron diffraction and photoelectron holography, a newly developed variant of it, can provide a rich range of information concerning surface structure. These methods are sensitive to atomic type, chemical state, and spin state. The theoretical prediction of diffraction patterns is also well developed at both the single scattering and multiple scattering levels, and quantitative fits of experiment to theory can lead to structures with accuracies in the {plus_minus}0.03 {Angstrom} range. Direct structural information can also be derived from forward scattering in scanned-angle measurements at higher energies, path length differences contained in scanned-energy data at lower energies, and holographic inversions of data sets spanning some region in angle and energy space. Diffraction can also affect average photoelectron emission depths. Circular dichroism in core-level emission can be fruitfully interpreted in terms of photoelectron diffraction theory, as can measurements with spin-resolved core-spectra, and studies of surface magnetic structures and phase transitions should be possible with these methods. Synchrotron radiation is a key element of fully utilizing these techniques.

Development of high-speed and wide-angle visible observation diagnostics on Experimental Advanced Superconducting Tokamak using catadioptric optics

International Nuclear Information System (INIS)

Yang, J. H.; Hu, L. Q.; Zang, Q.; Han, X. F.; Shao, C. Q.; Sun, T. F.; Chen, H.; Wang, T. F.; Li, F. J.; Hu, A. L.; Yang, X. F.

2013-01-01

A new wide-angle endoscope for visible light observation on the Experimental Advanced Superconducting Tokamak (EAST) has been recently developed. The head section of the optical system is based on a mirror reflection design that is similar to the International Thermonuclear Experimental Reactor-like wide-angle observation diagnostic on the Joint European Torus. However, the optical system design has been simplified and improved. As a result, the global transmittance of the system is as high as 79.6% in the wavelength range from 380 to 780 nm, and the spatial resolution is <5 mm for the full depth of field (4000 mm). The optical system also has a large relative aperture (1:2.4) and can be applied in high-speed camera diagnostics. As an important diagnostic tool, the optical system has been installed on the HT-7 (Hefei Tokamak-7) for its final experimental campaign, and the experiments confirmed that it can be applied to the investigation of transient processes in plasma, such as ELMy eruptions in H-mode, on EAST

The Scherrer equation and the dynamical theory of X-ray diffraction.

Science.gov (United States)

Muniz, Francisco Tiago Leitão; Miranda, Marcus Aurélio Ribeiro; Morilla Dos Santos, Cássio; Sasaki, José Marcos

2016-05-01

The Scherrer equation is a widely used tool to determine the crystallite size of polycrystalline samples. However, it is not clear if one can apply it to large crystallite sizes because its derivation is based on the kinematical theory of X-ray diffraction. For large and perfect crystals, it is more appropriate to use the dynamical theory of X-ray diffraction. Because of the appearance of polycrystalline materials with a high degree of crystalline perfection and large sizes, it is the authors' belief that it is important to establish the crystallite size limit for which the Scherrer equation can be applied. In this work, the diffraction peak profiles are calculated using the dynamical theory of X-ray diffraction for several Bragg reflections and crystallite sizes for Si, LaB6 and CeO2. The full width at half-maximum is then extracted and the crystallite size is computed using the Scherrer equation. It is shown that for crystals with linear absorption coefficients below 2117.3 cm(-1) the Scherrer equation is valid for crystallites with sizes up to 600 nm. It is also shown that as the size increases only the peaks at higher 2θ angles give good results, and if one uses peaks with 2θ > 60° the limit for use of the Scherrer equation would go up to 1 µm.

Wideband metamaterial array with polarization-independent and wide incident angle for harvesting ambient electromagnetic energy and wireless power transfer

Science.gov (United States)

Zhong, Hui-Teng; Yang, Xue-Xia; Song, Xing-Tang; Guo, Zhen-Yue; Yu, Fan

2017-11-01

In this work, we introduced the design, demonstration, and discussion of a wideband metamaterial array with polarization-independent and wide-angle for harvesting ambient electromagnetic (EM) energy and wireless power transfer. The array consists of unit cells with one square ring and four metal bars. In comparison to the published metamaterial arrays for harvesting EM energy or wireless transfer, this design had the wide operation bandwidth with the HPBW (Half Power Band Width) of 110% (6.2 GHz-21.4 GHz), which overcomes the narrow-band operation induced by the resonance characteristic of the metamaterial. On the normal incidence, the simulated maximum harvesting efficiency was 96% and the HPBW was 110% for the random polarization wave. As the incident angle increases to 45°, the maximum efficiency remained higher than 88% and the HPBW remained higher than 83% for the random polarization wave. Furthermore, the experimental verification of the designed metamaterial array was conducted, and the measured results were in reasonable agreement with the simulated ones.

Structural refinement and extraction of hydrogen atomic positions in polyoxymethylene crystal based on the first successful measurements of 2-dimensional high-energy synchrotron X-ray diffraction and wide-angle neutron diffraction patterns of hydrogenated and deuterated species

International Nuclear Information System (INIS)

Tashiro, Kohji; Hanesaka, Makoto; Ohhara, Takashi; Kurihara, Kazuo; Tamada, Taro; Kuroki, Ryota; Fujiwara, Satoru; Ozeki, Tomoji; Kitano, Toshiaki; Nishu, Takashi; Tanaka, Ichiro; Niimura, Nobuo

2007-01-01

2-Dimensional X-ray and neutron diffraction patterns have been successfully measured for deuterated and hydrogenated polyoxymethylene (POM) samples obtained by γ-ray induced solid-state polymerization reaction. More than 700 reflections were collected from the X-ray diffraction data at -150degC by utilizing a high-energy synchrotron X-ray beam at SPring-8, Japan, from which the crystal structure of POM has been refined thoroughly including the extraction of hydrogen atomic positions at clearly seen in the difference Fourier synthesis map. As the first trial the nonuniform (9/5) helical model was analyzed with the reliability factor (R factor) 6.9%. The structural analysis was made also using the X-ray reflections of about 400 observed at room temperature (R 8.8%), and the thermal parameters of constituent atoms were compared between the low and high temperatures to discuss the librational thermal motion of the chains. The 2-dimensional neutron diffraction data, collected for the deuterated and hydrogenated POM samples using an imaging plate system specifically built-up for neutron scattering experiment, have allowed us to pick up the D and H atomic positions clearly in the Fourier synthesis maps. Another possible model, (29/16) helix, which was proposed by several researches, has been also investigated on the basis of the X-ray diffraction data at -150degC. The direct method succeeded in extracting this (29/16) model straightforwardly. The R factor was 8.6%, essentially the same as that of (9/5) helical model. This means that the comparison of the diffraction intensity between the data collected from the full-rotation X-ray diffraction pattern and the intensity calculated for both the (9/5) and (29/16) models cannot be used for the unique determination of the superiority of the model, (9/5) or (29/16) helix. However, we have found the existence of 001 and 002 reflections which give the longer repeating period 55.7 A. Besides there observed a series of meridional

Peculiarities of section topograms for the multiple diffraction of X rays

Energy Technology Data Exchange (ETDEWEB)

Kohn, V. G., E-mail: kohnvict@yandex.ru [National Research Centre “Kurchatov Institute” (Russian Federation); Smirnova, I. A. [Russian Academy of Sciences, Institute of Solid State Physics (Russian Federation)

2016-07-15

The distortion of interference fringes on the section topograms of single crystal due to the multiple diffraction of X rays has been investigated. The cases of the 220 and 400 reflections in a silicon crystal in the form of a plate with a surface oriented normally to the [001] direction are considered both theoretically and experimentally. The same section topogram exhibits five cases of multiple diffraction at small azimuthal angles for the 400 reflection and MoK{sub α} radiation, while the topogram for the 220 reflection demonstrates two cases of multiple diffraction. All these cases correspond to different combinations of reciprocal lattice vectors. Exact theoretical calculations of section topograms for the aforementioned cases of multiple diffraction have been performed for the first time. The section topograms exhibit two different distortion regions. The distortions in the central region of the structure are fairly complex and depend strongly on the azimuthal angle. In the tails of the multiple diffraction region, there is a shift of two-beam interference fringes, which can be observed even with a laboratory X-ray source.

X-ray diffraction and chemical bonding

International Nuclear Information System (INIS)

Bats, J.W.

1976-01-01

Chemical bonds are investigated in sulfamic acid (H 3 N-SO 3 ), sodium sulfonlate dihydrate (H 2 NC 6 H 4 SO 3 Na.2H 2 O), 2,5-dimercaptothiadiazole (HS-C 2 N 2 S-SH), sodium cyanide dihydrate (NaCN.2H 2 O), sodium thiocyanate (NaSCN) and ammonium thiocyanate (NH 4 SCN) by X-ray diffraction, and if necessary completed with neutron diffraction. Crystal structures and electron densities are determined together with bond length and angles. Also the effects of thermal motion are discussed

Reflection color filters of the three primary colors with wide viewing angles using common-thickness silicon subwavelength gratings.

Science.gov (United States)

Kanamori, Yoshiaki; Ozaki, Toshikazu; Hane, Kazuhiro

2014-10-20

We fabricated reflection color filters of the three primary colors with wide viewing angles using silicon two-dimensional subwavelength gratings on the same quartz substrate. The grating periods were 400, 340, and 300 nm for red, green, and blue filters, respectively. All of the color filters had the same grating thickness of 100 nm, which enabled simple fabrication of a color filter array. Reflected colors from the red, green, and blue filters under s-polarized white-light irradiation appeared in the respective colors at incident angles from 0 to 50°. By rigorous coupled-wave analysis, the dimensions of each color filter were designed, and the calculated reflectivity was compared with the measured reflectivity.

X-ray diffraction study of surface-layer structure in parallel grazing rays

International Nuclear Information System (INIS)

Shtypulyak, N.I.; Yakimov, I.I.; Litvintsev, V.V.

1989-01-01

An x-ray diffraction method is described for study of thin polycrystalline and amorphous films and surface layers in an extremely asymmetrical diffraction system in parallel grazing rays using a DRON-3.0 diffractometer. The minimum grazing angles correspond to diffraction under conditions of total external reflection and a layer depth of ∼ 2.5-8 nm

First observation of new effects at the set-up for searching for a neutron electric dipole moment by a crystal-diffraction method

CERN Document Server

Fedorov, V V; Semenikhin, S Y; Voronin, V V

2002-01-01

First observation of new effects was carried out using the set-up created for searching for a neutron electric dipole moment (EDM) by a crystal-diffraction method. For the first time the neutron dynamical Laue diffraction for the Bragg angles close to a right angle (up to 87 ) was studied, using the direct diffraction beam and a thick (propor to 3.5-cm) crystal. The effect of an essential time delay of diffracting neutrons inside the crystal for Bragg angles close to 90 was experimentally observed, using a time-of-flight method. The phenomenon of neutron-beam depolarization was first experimentally observed for the case of Laue diffraction in a noncentrosymmetric alpha-quartz crystal. It is experimentally proved that the interplanar electric field, affecting a neutron in a crystal, maintains its value up to Bragg angles equal to 87 . These results confirm the opportunity to increase by more than an order of magnitude the sensitivity of the method to the neutron EDM, using the diffraction angles close to 90 , ...

Angular criterion for distinguishing between Fraunhofer and Fresnel diffraction

International Nuclear Information System (INIS)

Medina, Francisco F.; Garcia-Sucerquia, Jorge; Castaneda, Roman; Matteucci, Giorgio

2003-03-01

The distinction between Fresnel and Fraunhofer diffraction is a crucial condition for the accurate analysis of diffracting structures. In this paper we propose a criterion based on the angle subtended by the first zero of the diffraction pattern from the center of the diffracting aperture. The determination of the zero of the diffraction pattern is the crucial point for assuring the precision of the criterion. It mainly depends on the dynamical range of the detector. Therefore, the applicability of adequate thresholds for different detector types is discussed. The criterion is also generalized by expressing it in terms of the number of Fresnel zones delimited by the aperture. Simulations are reported for illustrating the feasibility of the criterion. (author)

Low cost and thin metasurface for ultra wide band and wide angle polarization insensitive radar cross section reduction

Science.gov (United States)

Ameri, Edris; Esmaeli, Seyed Hassan; Sedighy, Seyed Hassan

2018-05-01

A planar low cost and thin metasurface is proposed to achieve ultra-wideband radar cross section (RCS) reduction with stable performance with respect to polarization and incident angles. This metasurface is composed of two different artificial magnetic conductor unit cells arranged in a chessboard like configuration. These unit cells have a Jerusalem cross pattern with different thicknesses, which results in wideband out-phase reflection and RCS reduction, consequently. The designed metasurface reduces RCS more than 10-dB from 13.6 GHz to 45.5 GHz (108% bandwidth) and more than 20-dB RCS from 15.2 GHz to 43.6 GHz (96.6%). Moreover, the 10-dB RCS reduction bandwidth is very stable (more than 107%) for both TE and TM polarizations. The good agreement between simulations and measurement results proves the design, properly. The ultra-wide bandwidth, low cost, low profile, and stable performance of this metasurface prove its high capability compared with the state-of-the-art references.

Powder diffraction

Energy Technology Data Exchange (ETDEWEB)

Hart, M.

1995-12-31

the importance of x-ray powder diffraction as an analytical tool for phase identification of materials was first pointed out by Debye and Scherrer in Germany and, quite independently, by Hull in the US. Three distinct periods of evolution lead to ubiquitous application in many fields of science and technology. In the first period, until the mid-1940`s, applications were and developed covering broad categories of materials including inorganic materials, minerals, ceramics, metals, alloys, organic materials and polymers. During this formative period, the concept of quantitative phase analysis was demonstrated. In the second period there followed the blossoming of technology and commercial instruments became widely used. The history is well summarized by Parrish and by Langford and Loueer. By 1980 there were probably 10,000 powder diffractometers in routine use, making it the most widely used of all x-ray crystallographic instruments. In the third, present, period data bases became firmly established and sophisticated pattern fitting and recognition software made many aspects of powder diffraction analysis routine. High resolution, tunable powder diffractometers were developed at sources of synchrotron radiation. The tunability of the spectrum made it possible to exploit all the subtleties of x-ray spectroscopy in diffraction experiments.

Powder diffraction

International Nuclear Information System (INIS)

Hart, M.

1995-01-01

The importance of x-ray powder diffraction as an analytical tool for phase identification of materials was first pointed out by Debye and Scherrer in Germany and, quite independently, by Hull in the US. Three distinct periods of evolution lead to ubiquitous application in many fields of science and technology. In the first period, until the mid-1940's, applications were and developed covering broad categories of materials including inorganic materials, minerals, ceramics, metals, alloys, organic materials and polymers. During this formative period, the concept of quantitative phase analysis was demonstrated. In the second period there followed the blossoming of technology and commercial instruments became widely used. The history is well summarized by Parrish and by Langford and Loueer. By 1980 there were probably 10,000 powder diffractometers in routine use, making it the most widely used of all x-ray crystallographic instruments. In the third, present, period data bases became firmly established and sophisticated pattern fitting and recognition software made many aspects of powder diffraction analysis routine. High resolution, tunable powder diffractometers were developed at sources of synchrotron radiation. The tunability of the spectrum made it possible to exploit all the subtleties of x-ray spectroscopy in diffraction experiments

DISCOVERY OF AN EXTREMELY WIDE-ANGLE BIPOLAR OUTFLOW IN AFGL 5142

Energy Technology Data Exchange (ETDEWEB)

Liu, Tie; Kim, Kee-Tae; Lee, Chang-Won; Cho, Se-Hyung [Korea Astronomy and Space Science Institute 776, Daedeokdae-ro, Yuseong-gu, Daejeon, 305-348 (Korea, Republic of); Zhang, Qizhou [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States); Wu, Yuefang [Department of Astronomy, Peking University, Beijing 100871 (China); Goldsmith, Paul F. [Jet Propulsion Laboratory, California Institute of Technology, 4800 Oak Grove Drive, Pasadena, CA 91109 (United States); Li, Di [National Astronomical Observatories, Chinese Academy of Science, A20 Datun Road, Chaoyang District, Beijing 100012 (China); Liu, Sheng-Yuan; Chen, Huei-Ru [Institute of Astronomy and Astrophysics, Academia Sinica, Taipei, Taiwan (China); Tatematsu, Ken’ichi [National Astronomical Observatory of Japan, 2-21-1 Osawa, Mitaka, Tokyo 181-8588 (Japan); Wang, Ke [European Southern Observatory, Karl-Schwarzschild-Str. 2, D-85748 Garching bei München (Germany); Lee, Jeong-Eun [School of Space Research, Kyung Hee University, Yongin-Si, Gyeonggi-Do 446-701 (Korea, Republic of); Qin, Sheng-Li [Department of Astronomy, Yunnan University, and Key Laboratory of Astroparticle Physics of Yunnan Province, Kunming 650091 (China); Mardones, Diego, E-mail: liutiepku@gmail.com [Departamento de Astronomía, Universidad de Chile, Casilla 36-D, Santiago (Chile)

2016-06-10

Most bipolar outflows are associated with individual young stellar objects and have small opening angles. Here we report the discovery of an extremely wide-angle (∼180°) bipolar outflow (“EWBO”) in a cluster forming region AFGL 5142 from low-velocity emission of the HCN (3–2) and HCO{sup +} (3–2) lines. This bipolar outflow is along a north-west to south-east direction with a line of sight flow velocity of about 3 km s{sup −1} and is spatially connected to the high-velocity jet-like outflows. It seems to be a collection of low-velocity material entrained by the high-velocity outflows due to momentum feedback. The total ejected mass and mass loss rate due to both high-velocity jet-like outflows and the “EWBO” are ∼24.5 M {sub ⊙} and ∼1.7 × 10{sup −3} M {sub ⊙} yr{sup −1}, respectively. Global collapse of the clump is revealed by the “blue profile” in the HCO{sup +} (1–0) line. A hierarchical network of filaments was identified in NH{sub 3} (1, 1) emission. Clear velocity gradients of the order of 10 km s{sup −1} pc{sup −1} are found along filaments, indicating gas inflow along the filaments. The sum of the accretion rate along filaments and mass infall rate along the line of sight is ∼3.1 × 10{sup −3} M {sub ⊙} yr{sup −1}, which exceeds the total mass loss rate, indicating that the central cluster is probably still gaining mass. The central cluster is highly fragmented and 22 condensations are identified in 1.1 mm continuum emission. The fragmentation process seems to be determined by thermal pressure and turbulence. The magnetic field may not play an important role in fragmentation.

Far-field divergence of a vectorial plane wave diffracted by a circular aperture from the vectorial structure

International Nuclear Information System (INIS)

Zhou Guo-Quan

2011-01-01

Based on the vectorial structure of an electromagnetic wave, the analytical and concise expressions for the TE and TM terms of a vectorial plane wave diffracted by a circular aperture are derived in the far-field. The expressions of the energy flux distributions of the TE term, the TM term and the diffracted plane wave are also presented. The ratios of the power of the TE and TM terms to that of the diffracted plane wave are examined in the far-field. In addition, the far-field divergence angles of the TE term, the TM term and the diffracted plane wave, which are related to the energy flux distribution, are investigated. The different energy flux distributions of the TE and TM terms result in the discrepancy of their divergence angles. The influences of the linearly polarized angle and the radius of the circular aperture on the far-field divergence angles of the TE term, the TM term and the diffracted plane wave are discussed in detail. This research may promote the recognition of the optical propagation through a circular aperture. (electromagnetism, optics, acoustics, heat transfer, classical mechanics, and fluid dynamics)

Diffraction at TOTEM

CERN Document Server

Giani, S; Antchev, G; Aspell, P; Avati, V; Bagliesi, M G; Berardi, V; Berretti, M; Besta, M; Bozzo, M; Brücken, E; Buzzo, A; Cafagna, F; Calicchio, M; Catanesi, M G; Cecchi, R; Ciocci, M A; Dadel, P; Deile, M; Dimovasili, E; Eggert, K; Eremin, V; Ferro, F; Fiergolski, A; García, F; Greco, V; Grzanka, L; Heino, J; Hildén, T; Kaspar, J; Kopal, J; Kundrát, V; Kurvinen, K; Lami, S; Latino, G; Lauhakangas, R; Leszko, R; Lippmaa, E; Lokajícek, M; Lo Vetere, M; Lucas Rodriguez, F; Macrí, M; Magazzù, G; Meucci, M; Minutoli, S; Notarnicola, G; Oliveri, E; Oljemark, F; Orava, R; Oriunno, M; Österberg, K; Pedreschi, E; Petäjäjärvi, J; Prochazka, J; Quinto, M; Radermacher, E; Radicioni, E; Ravotti, F; Rella, G; Robutti, E; Ropelewski, L; Rostkowski, M; Ruggiero, G; Rummel, A; Saarikko, H; Sanguinetti, G; Santroni, A; Scribano, A; Sette, G; Snoeys, W; Spinella, F; Ster, A; Taylor, C; Trummal, A; Turini, N; Whitmore, J; Wu, J; Zalewski, M

2010-01-01

The primary objective of the TOTEM experiment at the LHC is the measurement of the total proton-proton cross section with the luminosity-independent method and the study of elastic proton-proton cross-section over a wide |t|-range. In addition TOTEM also performs a comprehensive study of diffraction, spanning from cross-section measurements of individual diffractive processes to the analysis of their event topologies. Hard diffraction will be studied in collaboration with CMS taking advantage of the large common rapidity coverage for charged and neutral particle detection and the large variety of trigger possibilities even at large luminosities. TOTEM will take data under all LHC beam conditions including standard high luminosity runs to maximise its physics reach. This contribution describes the main features of the TOTEM diffractive physics programme including measurements to be made in the early LHC runs.

DMSO-induced dehydration of DPPC membranes studied by x-ray diffraction, small angle neutron scattering and calorimetry

International Nuclear Information System (INIS)

Kiselev, M.A.; Kiselev, A.M.; Lesieur, P.; Grabielle-Madelmond, C.; Ollivon, M.

1998-01-01

The properties of dimethyl sulfoxide (DMSO), a cryoprotector well known for its biological and therapeutic applications, were investigated on lipid membranes by x-ray diffraction, differential scanning calorimetry (DSC) and small angle neutron scattering (SANS). The DSC study of water freezing and melting of ice was performed in the ternary system which consists of 1,2-dipalmitoyl-sn-glycero-3-phosphatidylcholine (DPPC)/DMSO/water system. The influence of DMSO on the DPPC membrane structure was established in the excess of solvent in the region of DMSO mole fraction from 0.0 to 1.0. The methods applied demonstrated the differences in the membrane structure in three sub-regions of DMSO mole fraction (X DMSO ) from 0.0 to 0.3 for the first, from 0.3 to 0.9 for the second, and from 0.9 to 1.0 for the third sub-region. The results for 0.0 ≤ X DMSO ≤ 0.3 can be explained in the framework of DMSO-induced dehydration of intermembrane space

Light scattering by red blood cells in ektacytometry: Fraunhofer versus anomalous diffraction

NARCIS (Netherlands)

Streekstra, G. J.; Hoekstra, A. G.; Nijhof, E. J.; Heethaar, R. M.

1993-01-01

In the present literature on ektacytometry, small angle light scattering by ellipsoidal red blood cells is commonly approximated by Fraunhofer diffraction. Calculations on a sphere with the size and relative refractive index of a red cell, however, show that Fraunhofer diffraction deviates

Membrane structure: neutron diffraction and small angle scattering studies

International Nuclear Information System (INIS)

Zaccai, G.

1985-01-01

The author considers a molecule in a beam of radiation of wavelength lambda. Two extreme ways are shown in which on can have many identical molecules in a sample: a crystal in which they are related to each other by the symmetry of a lattice, and complete disorder in which there is no correlation between molecules. The detailed crystallographic analysis of isomorphous replacement is examined. Neutron diffraction experiments with specific deuteration are performed to characterize interactions of cholesterol with lipid bilayers. Retinal rod outer segment disk membranes and the purple membrane of H. halobium are examined

Photoelectron diffraction k-space volumes of the c(2x2) Mn/Ni(100) structure

Energy Technology Data Exchange (ETDEWEB)

Banerjee, S.; Denlinger, J.; Chen, X. [Univ. of Wisconsin, Milwaukee, WI (United States)] [and others

1997-04-01

Traditionally, x-ray photoelectron diffraction (XPD) studies have either been done by scanning the diffraction angle for fixed kinetic energy (ADPD), or scanning the kinetic energy at fixed exit angle (EDPD). Both of these methods collect subsets of the full diffraction pattern, or volume, which is the intensity of photoemission as a function of momentum direction and magnitude. With the high density available at the Spectromicroscopy Facility (BL 7.0) {open_quotes}ultraESCA{close_quotes} station, the authors are able to completely characterize the photoelectron diffraction patterns of surface structures, up to several hundred electron volts kinetic energy. This large diffraction `volume` can then be analyzed in many ways. The k-space volume contains as a subset the energy dependent photoelectron diffraction spectra along all emission angles. It also contains individual, hemispherical, diffraction patterns at specific kinetic energies. Other `cuts` through the data set are also possible, revealing new ways of viewing photoelectron diffraction data, and potentially new information about the surface structure being studied. In this article the authors report a brief summary of a structural study being done on the c(2x2) Mn/Ni(100) surface alloy. This system is interesting for both structural and magnetic reasons. Magnetically, the Mn/Ni(100) surface alloy exhibits parallel coupling of the Mn and Ni moments, which is opposite to the reported coupling for the bulk, disordered, alloy. Structurally, the Mn atoms are believed to lie well above the surface plane.

Diffraction radiation from relativistic particles

CERN Document Server

Potylitsyn, Alexander Petrovich; Strikhanov, Mikhail Nikolaevich; Tishchenko, Alexey Alexandrovich

2010-01-01

This book deals with diffraction radiation, which implies the boundary problems of electromagnetic radiation theory. Diffraction radiation is generated when a charged particle moves in a vacuum near a target edge. Diffraction radiation of non-relativistic particles is widely used to design intense emitters in the cm wavelength range. Diffraction radiation from relativistic charged particles is important for noninvasive beam diagnostics and design of free electron lasers based on Smith-Purcell radiation which is diffraction radiation from periodic structures. Different analytical models of diffraction radiation and results of recent experimental studies are presented in this book. The book may also serve as guide to classical electrodynamics applications in beam physics and electrodynamics. It can be of great use for young researchers to develop skills and for experienced scientists to obtain new results.

Diffraction radiation from relativistic particles

International Nuclear Information System (INIS)

Potylitsyn, Alexander Petrovich; Ryazanov, Mikhail Ivanovich; Strikhanov, Mikhail Nikolaevich; Tishchenko, Alexey Alexandrovich

2010-01-01

This book deals with diffraction radiation, which implies the boundary problems of electromagnetic radiation theory. Diffraction radiation is generated when a charged particle moves in a vacuum near a target edge. Diffraction radiation of non-relativistic particles is widely used to design intense emitters in the cm wavelength range. Diffraction radiation from relativistic charged particles is important for noninvasive beam diagnostics and design of free electron lasers based on Smith-Purcell radiation which is diffraction radiation from periodic structures. Different analytical models of diffraction radiation and results of recent experimental studies are presented in this book. The book may also serve as guide to classical electrodynamics applications in beam physics and electrodynamics. It can be of great use for young researchers to develop skills and for experienced scientists to obtain new results. (orig.)

Scalable, "Dip-and-Dry" Fabrication of a Wide-Angle Plasmonic Selective Absorber for High-Efficiency Solar-Thermal Energy Conversion.

Science.gov (United States)

Mandal, Jyotirmoy; Wang, Derek; Overvig, Adam C; Shi, Norman N; Paley, Daniel; Zangiabadi, Amirali; Cheng, Qian; Barmak, Katayun; Yu, Nanfang; Yang, Yuan

2017-11-01

A galvanic-displacement-reaction-based, room-temperature "dip-and-dry" technique is demonstrated for fabricating selectively solar-absorbing plasmonic-nanoparticle-coated foils (PNFs). The technique, which allows for facile tuning of the PNFs' spectral reflectance to suit different radiative and thermal environments, yields PNFs which exhibit excellent, wide-angle solar absorptance (0.96 at 15°, to 0.97 at 35°, to 0.79 at 80°), and low hemispherical thermal emittance (0.10) without the aid of antireflection coatings. The thermal emittance is on par with those of notable selective solar absorbers (SSAs) in the literature, while the wide-angle solar absorptance surpasses those of previously reported SSAs with comparable optical selectivities. In addition, the PNFs show promising mechanical and thermal stabilities at temperatures of up to 200 °C. Along with the performance of the PNFs, the simplicity, inexpensiveness, and environmental friendliness of the "dip-and-dry" technique makes it an appealing alternative to current methods for fabricating selective solar absorbers. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

System description and analysis. Part 1: Feasibility study for helicopter/VTOL wide-angle simulation image generation display system

Science.gov (United States)

1977-01-01

A preliminary design for a helicopter/VSTOL wide angle simulator image generation display system is studied. The visual system is to become part of a simulator capability to support Army aviation systems research and development within the near term. As required for the Army to simulate a wide range of aircraft characteristics, versatility and ease of changing cockpit configurations were primary considerations of the study. Due to the Army's interest in low altitude flight and descents into and landing in constrained areas, particular emphasis is given to wide field of view, resolution, brightness, contrast, and color. The visual display study includes a preliminary design, demonstrated feasibility of advanced concepts, and a plan for subsequent detail design and development. Analysis and tradeoff considerations for various visual system elements are outlined and discussed.

Broadband and wide-angle distributed Bragg reflectors based on amorphous germanium films by glancing angle deposition.

Science.gov (United States)

Leem, Jung Woo; Yu, Jae Su

2012-08-27

We fabricated the distributed Bragg reflectors (DBRs) with amorphous germanium (a-Ge) films consisted of the same materials at a center wavelength (λc) of 1.33 μm by the glancing angle deposition. Their optical reflectance properties were investigated in the infrared wavelength region of 1-1.9 μm at incident light angles (θ inc) of 8-70°, together with the theoretical analysis using a rigorous coupled-wave analysis simulation. The two alternating a-Ge films at the incident vapor flux angles of 0 and 75° were formed as the high and low refractive index materials, respectively. The a-Ge DBR with only 5 periods exhibited a normalized stop bandwidth (∆λ/λ c) of ~24.1%, maintaining high reflectance (R) values of > 99%. Even at a high θ inc of 70°, the ∆λ/λ c was ~21.9%, maintaining R values of > 85%. The a-Ge DBR with good uniformity was obtained over the area of a 2 inch Si wafer. The calculated reflectance results showed a similar tendency to the measured data.

Models for electromagnetic scattering from the sea at extremely low grazing angles

Science.gov (United States)

Wetzel, Lewis B.

1987-12-01

The present state of understanding in the field of low-grazing-angle sea scatter is reviewed and extended. The important concept of shadowing is approached from the point of view of diffraction theory, and limits in wind speed and radar frequency are found for the application of shadowing theories based on geometrical optics. The implications of shadowing function based on illumination thresholding are shown to compare favorably with a variety of experimental results. Scattering from the exposed surface peaks is treated by a composite-surface Bragg model, and by wedge models using both physical optics and the method of equivalent currents. Curiously, the scattering levels predicted by these widely different approximations are all in fairly good agreement with experimental values for moderately low grazing angles (about 5 deg), with the physical optics wedge model being superior at 1 deg. A new scattering feature, the slosh, is introduced, with scattering behavior that resembles the temporal and polarization dependence of observed low angle returns from calm water. The plume model of scattering from breaking waves (from earlier work) is discussed as a source of high-intensity Sea Spikes. It is emphasized that the prediction of low angle scattering from the sea will require considerably more information about the shape, size, and distribution of the actual scattering features.

Design and experimental tests of a novel neutron spin analyzer for wide angle spin echo spectrometers

Energy Technology Data Exchange (ETDEWEB)

Fouquet, Peter; Farago, Bela; Andersen, Ken H.; Bentley, Phillip M.; Pastrello, Gilles; Sutton, Iain; Thaveron, Eric; Thomas, Frederic [Institut Laue-Langevin, BP 156, F-38042 Grenoble Cedex 9 (France); Moskvin, Evgeny [Helmholtzzentrum Berlin, Glienicker Strasse 100, D-14109 Berlin (Germany); Pappas, Catherine [Helmholtzzentrum Berlin, Glienicker Strasse 100, D-14109 Berlin (Germany); Faculty of Applied Sciences, Delft University of Technology, Mekelweg 15, 2629 JB Delft (Netherlands)

2009-09-15

This paper describes the design and experimental tests of a novel neutron spin analyzer optimized for wide angle spin echo spectrometers. The new design is based on nonremanent magnetic supermirrors, which are magnetized by vertical magnetic fields created by NdFeB high field permanent magnets. The solution presented here gives stable performance at moderate costs in contrast to designs invoking remanent supermirrors. In the experimental part of this paper we demonstrate that the new design performs well in terms of polarization, transmission, and that high quality neutron spin echo spectra can be measured.

Crustal structure of the North Iberian continental margin from seismic refraction/wide-angle reflection profiles

Science.gov (United States)

Ruiz, M.; Díaz, J.; Pedreira, D.; Gallart, J.; Pulgar, J. A.

2017-10-01

The structure and geodynamics of the southern margin of the Bay of Biscay have been investigated from a set of 11 multichannel seismic reflection profiles, recorded also at wide angle offsets in an onshore-offshore network of 24 OBS/OBH and 46 land sites. This contribution focuses on the analysis of the wide-angle reflection/refraction data along representative profiles. The results document strong lateral variations of the crustal structure along the margin and provide an extensive test of the crustal models previously proposed for the northern part of the Iberian Peninsula. Offshore, the crust has a typical continental structure in the eastern tip of the bay, which disappears smoothly towards the NW to reach crustal thickness close to 10 km at the edge of the studied area ( 45°N, 6°W). The analysis of the velocity-depth profiles, altogether with additional information provided by the multichannel seismic data and magnetic surveys, led to the conclusion that the crust in this part of the bay should be interpreted as transitional from continental to oceanic. Typical oceanic crust has not been imaged in the investigated area. Onshore, the new results are in good agreement with previous results and document the indentation of the Bay of Biscay crust into the Iberian crust, forcing its subduction to the North. The interpreted profiles show that the extent of the southward indentation is not uniform, with an Alpine root less developed in the central and western sector of the Basque-Cantabrian Basin. N-S to NE-SW transfer structures seem to control those variations in the indentation degree.

Corner diffraction coefficients for the quarter plane

DEFF Research Database (Denmark)

Hansen, Thorkild B.

1991-01-01

that the corner current for the right-angled corner, illuminated from a forward direction, consists mainly of two edge waves propagating along the edges forming the corner. Analytical expressions for these edge wave currents are constructed from the numerical results. A corner diffracted field is calculated...

Flexible and conformable broadband metamaterial absorber with wide-angle and polarization stability for radar application

Science.gov (United States)

Chen, Huijie; Yang, Xiaoqing; Wu, Shiyue; Zhang, Di; Xiao, Hui; Huang, Kama; Zhu, Zhanxia; Yuan, Jianping

2018-01-01

In this work, a type of flexible, broadband electromagnetic microwave absorber is designed, fabricated and experimentally characterized. The absorber is composed of lumped resistors loaded frequency selective surface which is mounted on flexible substrate using silicone rubber and in turn backed by copper film. The simulated results show that an effective absorption (over 90%) bandwidth spans from 7.6 to 18.3 GHz, which covers both X (8-12 GHz) and Ku (12-18 GHz) bands, namely a 82.6% fraction bandwidth. And the bandwidth performs a good absorption response by varying the incident angle up to 60° for both TE and TM polarization. Moreover, the flexibility of the substrate enables the absorber conformably to bend and attach to cylinders of various radius without breakdown of the absorber. The designed structure has been fabricated and measured for both planar and conformable cases, and absorption responses show a good agreement of the broadband absorption feature with the simulated ones. This work has demonstrated specifically that proposed structure provides polarization-insensitive, wide-angle, flexible and conformable wideband absorption, which extends the absorber’s application to practical radar cross section reductions for radars and warships.

DNA hydration studied by neutron fiber diffraction

Energy Technology Data Exchange (ETDEWEB)

Fuller, W.; Forsyth, V.T.; Mahendrasingam, A.; Langan, P.; Pigram, W.J. [Keele Univ. (United Kingdom)] [and others

1994-12-31

The development of neutron high angle fiber diffraction to investigate the location of water around the deoxyribonucleic acid (DNA) double-helix is described. The power of the technique is illustrated by its application to the D and A conformations of DNA using the single crystal diffractometer, D19, at the Institute Laue-Langevin, Grenoble and the time of flight diffractometer, SXD, at the Rutherford Appleton ISIS Spallation Neutron Source. These studies show the existence of bound water closely associated with the DNA. The patterns of hydration in these two DNA conformations are quite distinct and are compared to those observed in X-ray single crystal studies of two-stranded oligodeoxynucleotides. Information on the location of water around the DNA double-helix from the neutron fiber diffraction studies is combined with that on the location of alkali metal cations from complementary X-ray high angle fiber diffraction studies at the Daresbury Laboratory SRS using synchrotron radiation. These analyses emphasize the importance of viewing DNA, water and ions as a single system with specific interactions between the three components and provide a basis for understanding the effect of changes in the concentration of water and ions in inducing conformations] transitions in the DNA double-helix.

DNA hydration studied by neutron fiber diffraction

International Nuclear Information System (INIS)

Fuller, W.; Forsyth, V.T.; Mahendrasingam, A.; Langan, P.; Pigram, W.J.

1994-01-01

The development of neutron high angle fiber diffraction to investigate the location of water around the deoxyribonucleic acid (DNA) double-helix is described. The power of the technique is illustrated by its application to the D and A conformations of DNA using the single crystal diffractometer, D19, at the Institute Laue-Langevin, Grenoble and the time of flight diffractometer, SXD, at the Rutherford Appleton ISIS Spallation Neutron Source. These studies show the existence of bound water closely associated with the DNA. The patterns of hydration in these two DNA conformations are quite distinct and are compared to those observed in X-ray single crystal studies of two-stranded oligodeoxynucleotides. Information on the location of water around the DNA double-helix from the neutron fiber diffraction studies is combined with that on the location of alkali metal cations from complementary X-ray high angle fiber diffraction studies at the Daresbury Laboratory SRS using synchrotron radiation. These analyses emphasize the importance of viewing DNA, water and ions as a single system with specific interactions between the three components and provide a basis for understanding the effect of changes in the concentration of water and ions in inducing conformations] transitions in the DNA double-helix

Details of 1π sr wide acceptance angle electrostatic lens for electron energy and two-dimensional angular distribution analysis combined with real space imaging

International Nuclear Information System (INIS)

Tóth, László; Matsuda, Hiroyuki; Matsui, Fumihiko; Goto, Kentaro; Daimon, Hiroshi

2012-01-01

We propose a new 1π sr Wide Acceptance Angle Electrostatic Lens (WAAEL), which works as a photoemission electron microscope (PEEM), a highly sensitive display-type electron energy and two-dimensional angular distribution analyzer. It can display two-dimensional angular distributions of charged particles within the acceptance angle of ±60° that is much larger than the largest acceptance angle range so far and comparable to the display-type spherical mirror analyzer developed by Daimon et al. . It has good focusing capabilities with 5-times magnification and 27(4) μm lateral-resolution. The relative energy resolution is typically from 2 to 5×10 -3 depending on the diameter of energy aperture and the emission area on the sample. Although, the lateral resolution of the presented lens is far from those are available nowadays, but this is the first working model that can form images using charged particles collected from 1π sr wide acceptance angle. The realization of such lens system is one of the first possible steps towards reaching the field of imaging type atomic resolution electron microscopy Feynman et al. Here some preliminary results are shown.

Diffraction at TOTEM

CERN Document Server

Antchev, G.; Avati, V.; Bagliesi, M.G.; Berardi, V.; Berretti, M.; Bottigli, U.; Bozzo, M.; Brucken, E.; Buzzo, A.; Cafagna, F.; Calicchio, M.; Catanesi, M.G.; Catastini, P.L.; Cecchi, R.; Ciocci, M.A.; Deile, M.; Dimovasili, E.; Eggert, K.; Eremin, V.; Ferro, F.; Garcia, F.; Giani, S.; Greco, V.; Heino, J.; Hilden, T.; Kaspar, J.; Kopal, J.; Kundrat, V.; Kurvinen, K.; Lami, S.; Latino, G.; Lauhakangas, R.; Lippmaa, E.; Lokajicek, M.; Lo Vetere, M.; Lucas Rodriguez, F.; Macri, M.; Magazzu, G.; Meucci, M.; Minutoli, S.; Niewiadomski, H.; Noschis, E.; Notarnicola, G.; Oliveri, E.; Oljemark, F.; Orava, R.; Oriunno, M.; Osterberg, K.; Palazzi, P.; Pedreschi, E.; Petajajarvi, J.; Quinto, M.; Radermacher, E.; Radicioni, E.; Ravotti, F.; Rella, G.; Robutti, E.; Ropelewski, L.; Ruggiero, G.; Rummel, A.; Saarikko, H.; Sanguinetti, G.; Santroni, A.; Scribano, A.; Sette, G.; Snoeys, W.; Spinella, F.; Squillacioti, P.; Ster, A.; Taylor, C.; Trummal, A.; Turini, N.; Whitmore, J.; Wu, J.

2009-01-01

The TOTEM experiment at the LHC measures the total proton-proton cross section with the luminosity-independent method and the elastic proton-proton cross-section over a wide |t|-range. It also performs a comprehensive study of diffraction, spanning from cross-section measurements of individual diffractive processes to the analysis of their event topologies. Hard diffraction will be studied in collaboration with CMS taking advantage of the large common rapidity coverage for charged and neutral particle detection and the large variety of trigger possibilities even at large luminosities. TOTEM will take data under all LHC beam conditions including standard high luminosity runs to maximize its physics reach. This contribution describes the main features of the TOTEM physics programme including measurements to be made in the early LHC runs. In addition, a novel scheme to extend the diffractive proton acceptance for high luminosity runs by installing proton detectors at IP3 is described.

Diffraction contrast imaging using virtual apertures

International Nuclear Information System (INIS)

Gammer, Christoph; Burak Ozdol, V.; Liebscher, Christian H.; Minor, Andrew M.

2015-01-01

Two methods on how to obtain the full diffraction information from a sample region and the associated reconstruction of images or diffraction patterns using virtual apertures are demonstrated. In a STEM-based approach, diffraction patterns are recorded for each beam position using a small probe convergence angle. Similarly, a tilt series of TEM dark-field images is acquired. The resulting datasets allow the reconstruction of either electron diffraction patterns, or bright-, dark- or annular dark-field images using virtual apertures. The experimental procedures of both methods are presented in the paper and are applied to a precipitation strengthened and creep deformed ferritic alloy with a complex microstructure. The reconstructed virtual images are compared with conventional TEM images. The major advantage is that arbitrarily shaped virtual apertures generated with image processing software can be designed without facing any physical limitations. In addition, any virtual detector that is specifically designed according to the underlying crystal structure can be created to optimize image contrast. - Highlights: • A dataset containing all structural information of a given position is recorded. • The dataset allows reconstruction of virtual diffraction patterns or images. • Specific virtual apertures are designed to image precipitates in a complex alloy. • Virtual diffraction patterns from arbitrarily small regions can be established. • Using STEM diffraction to record the dataset is more efficient than TEM dark-field

Neutron Larmor diffraction measurements for materials science

International Nuclear Information System (INIS)

Repper, J.; Keller, T.; Hofmann, M.; Krempaszky, C.; Petry, W.; Werner, E.

2010-01-01

Neutron Larmor diffraction (LD) is a high-resolution diffraction technique based on the Larmor precession of polarized neutrons. In contrast to conventional diffraction, LD does not depend on the accurate measurement of Bragg angles, and thus the resolution is independent of the beam collimation and monochromaticity. At present, a relative resolution for the determination of the crystal lattice spacing d of Δd/d∼10 -6 is achieved, i.e. at least one order of magnitude superior to conventional neutron or X-ray techniques. This work is a first step to explore the application of LD to high-resolution problems in the analysis of residual stresses, where both the accurate measurement of absolute d values and the possibility of measuring type II and III stresses may provide additional information beyond those accessible by conventional diffraction techniques. Data obtained from Inconel 718 samples are presented.

Neutron Larmor diffraction measurements for materials science

Energy Technology Data Exchange (ETDEWEB)

Repper, J., E-mail: julia_repper@web.de [Forschungsneutronenquelle Heinz Maier-Leibnitz (FRM II), TU Muenchen, 85747 Garching (Germany); Keller, T. [Max-Planck-Institut fuer Festkoerperforschung, 70569 Stuttgart (Germany)] [Forschungsneutronenquelle Heinz Maier-Leibnitz (FRM II), TU Muenchen, 85747 Garching (Germany); Hofmann, M. [Forschungsneutronenquelle Heinz Maier-Leibnitz (FRM II), TU Muenchen, 85747 Garching (Germany); Krempaszky, C. [Christian-Doppler-Labor fuer Werkstoffmechanik von Hochleistungslegierungen, TU Muenchen, 85747 Garching (Germany); Petry, W. [Forschungsneutronenquelle Heinz Maier-Leibnitz (FRM II), TU Muenchen, 85747 Garching (Germany); Werner, E. [Lehrstuhl fuer Werkstoffkunde und Werkstoffmechanik, TU Muenchen, 85747 Garching (Germany)

2010-05-15

Neutron Larmor diffraction (LD) is a high-resolution diffraction technique based on the Larmor precession of polarized neutrons. In contrast to conventional diffraction, LD does not depend on the accurate measurement of Bragg angles, and thus the resolution is independent of the beam collimation and monochromaticity. At present, a relative resolution for the determination of the crystal lattice spacing d of {Delta}d/d{approx}10{sup -6} is achieved, i.e. at least one order of magnitude superior to conventional neutron or X-ray techniques. This work is a first step to explore the application of LD to high-resolution problems in the analysis of residual stresses, where both the accurate measurement of absolute d values and the possibility of measuring type II and III stresses may provide additional information beyond those accessible by conventional diffraction techniques. Data obtained from Inconel 718 samples are presented.

submitter Digital Image Correlation of 2D X-ray Powder Diffraction Data for Lattice Strain Evaluation

CERN Document Server

Zhang, Hongjia; Salvati, Enrico; Daisenberger, Dominik; Lunt, Alexander J G; Fong, Kai Soon; Song, Xu; Korsunsky, Alexander M

2018-01-01

High energy 2D X-ray powder diffraction experiments are widely used for lattice strain measurement. The 2D to 1D conversion of diffraction patterns is a necessary step used to prepare the data for full pattern refinement, but is inefficient when only peak centre position information is required for lattice strain evaluation. The multi-step conversion process is likely to lead to increased errors associated with the ‘caking’ (radial binning) or fitting procedures. A new method is proposed here that relies on direct Digital Image Correlation analysis of 2D X-ray powder diffraction patterns (XRD-DIC, for short). As an example of using XRD-DIC, residual strain values along the central line in a Mg AZ31B alloy bar after 3-point bending are calculated by using both XRD-DIC and the conventional ‘caking’ with fitting procedures. Comparison of the results for strain values in different azimuthal angles demonstrates excellent agreement between the two methods. The principal strains and directions are calculated...

X-ray diffraction

International Nuclear Information System (INIS)

Vries, J.L. de.

1976-01-01

The seventh edition of Philips' Review of literature on X-ray diffraction begins with a list of conference proceedings on the subject, organised by the Philips' organisation at regular intervals in various European countries. This is followed by a list of bulletins. The bibliography is divided according to the equipment (cameras, diffractometers, monochromators) and its applications. The applications are subdivided into sections for high/low temperature and pressure, effects due to the equipment, small angle scattering and a part for stress, texture and phase analyses of metals and quantitative analysis of minerals

Burgers Vector Analysis of Vertical Dislocations in Ge Crystals by Large-Angle Convergent Beam Electron Diffraction.

Science.gov (United States)

Groiss, Heiko; Glaser, Martin; Marzegalli, Anna; Isa, Fabio; Isella, Giovanni; Miglio, Leo; Schäffler, Friedrich

2015-06-01

By transmission electron microscopy with extended Burgers vector analyses, we demonstrate the edge and screw character of vertical dislocations (VDs) in novel SiGe heterostructures. The investigated pillar-shaped Ge epilayers on prepatterned Si(001) substrates are an attempt to avoid the high defect densities of lattice mismatched heteroepitaxy. The Ge pillars are almost completely strain-relaxed and essentially defect-free, except for the rather unexpected VDs. We investigated both pillar-shaped and unstructured Ge epilayers grown either by molecular beam epitaxy or by chemical vapor deposition to derive a general picture of the underlying dislocation mechanisms. For the Burgers vector analysis we used a combination of dark field imaging and large-angle convergent beam electron diffraction (LACBED). With LACBED simulations we identify ideally suited zeroth and second order Laue zone Bragg lines for an unambiguous determination of the three-dimensional Burgers vectors. By analyzing dislocation reactions we confirm the origin of the observed types of VDs, which can be efficiently distinguished by LACBED. The screw type VDs are formed by a reaction of perfect 60° dislocations, whereas the edge types are sessile dislocations that can be formed by cross-slips and climbing processes. The understanding of these origins allows us to suggest strategies to avoid VDs.

Impact of large field angles on the requirements for deformable mirror in imaging satellites

Science.gov (United States)

Kim, Jae Jun; Mueller, Mark; Martinez, Ty; Agrawal, Brij

2018-04-01

For certain imaging satellite missions, a large aperture with wide field-of-view is needed. In order to achieve diffraction limited performance, the mirror surface Root Mean Square (RMS) error has to be less than 0.05 waves. In the case of visible light, it has to be less than 30 nm. This requirement is difficult to meet as the large aperture will need to be segmented in order to fit inside a launch vehicle shroud. To reduce this requirement and to compensate for the residual wavefront error, Micro-Electro-Mechanical System (MEMS) deformable mirrors can be considered in the aft optics of the optical system. MEMS deformable mirrors are affordable and consume low power, but are small in size. Due to the major reduction in pupil size for the deformable mirror, the effective field angle is magnified by the diameter ratio of the primary and deformable mirror. For wide field of view imaging, the required deformable mirror correction is field angle dependant, impacting the required parameters of a deformable mirror such as size, number of actuators, and actuator stroke. In this paper, a representative telescope and deformable mirror system model is developed and the deformable mirror correction is simulated to study the impact of the large field angles in correcting a wavefront error using a deformable mirror in the aft optics.

DMSO-induced dehydration of DPPC membranes studied by x-ray diffraction, small angle neutron scattering and calorimetry

Energy Technology Data Exchange (ETDEWEB)

Kiselev, M A; Kiselev, A M [Frank Laboratory of Neutron Physics, Joint Institute for Nuclear Research, Dubna (Russian Federation); Lesieur, P [LURE, Universite Paris-Sud, Bat. 209-D, F91405 Orsay cedex, (France); Grabielle-Madelmond, C; Ollivon, M [Physico-Chimie des systemes polyphases, URA 1218 du CNRS, Faculte de Pharmacie, tour B, F-92296, Chatenay Malabry (France)

1998-12-01

The properties of dimethyl sulfoxide (DMSO), a cryoprotector well known for its biological and therapeutic applications, were investigated on lipid membranes by x-ray diffraction, differential scanning calorimetry (DSC) and small angle neutron scattering (SANS). The DSC study of water freezing and melting of ice was performed in the ternary system which consists of 1,2-dipalmitoyl-sn-glycero-3-phosphatidylcholine (DPPC)/DMSO/water system. The influence of DMSO on the DPPC membrane structure was established in the excess of solvent in the region of DMSO mole fraction from 0.0 to 1.0. The methods applied demonstrated the differences in the membrane structure in three sub-regions of DMSO mole fraction (X{sub DMSO}) from 0.0 to 0.3 for the first, from 0.3 to 0.9 for the second, and from 0.9 to 1.0 for the third sub-region. The results for 0.0 {<=} X{sub DMSO} {<=} 0.3 can be explained in the framework of DMSO-induced dehydration of intermembrane space 11 refs., 7 figs. Submitted to the Conference `ISSRNS`98`, 15-20 Jun 1998, Ustron-Jaszowiec, Poland

Understanding nucleic acid structural changes by comparing wide-angle x-ray scattering (WAXS) experiments to molecular dynamics simulations

Energy Technology Data Exchange (ETDEWEB)

Pabit, Suzette A.; Katz, Andrea M.; Pollack, Lois [School of Applied and Engineering Physics, Cornell University, Ithaca, New York 14853 (United States); Tolokh, Igor S. [Department of Computer Science, Virginia Tech, Blacksburg, Virginia 24061 (United States); Drozdetski, Aleksander [Department of Physics, Virginia Tech, Blacksburg, Virginia 24061 (United States); Baker, Nathan [Pacific Northwest National Laboratory, Richland, Washington 99352 (United States); Onufriev, Alexey V. [Department of Computer Science, Virginia Tech, Blacksburg, Virginia 24061 (United States); Department of Physics, Virginia Tech, Blacksburg, Virginia 24061 (United States)

2016-05-28

Wide-angle x-ray scattering (WAXS) is emerging as a powerful tool for increasing the resolution of solution structure measurements of biomolecules. Compared to its better known complement, small angle x-ray scattering (SAXS), WAXS targets higher scattering angles and can enhance structural studies of molecules by accessing finer details of solution structures. Although the extension from SAXS to WAXS is easy to implement experimentally, the computational tools required to fully harness the power of WAXS are still under development. Currently, WAXS is employed to study structural changes and ligand binding in proteins; however, the methods are not as fully developed for nucleic acids. Here, we show how WAXS can qualitatively characterize nucleic acid structures as well as the small but significant structural changes driven by the addition of multivalent ions. We show the potential of WAXS to test all-atom molecular dynamics (MD) simulations and to provide insight into understanding how the trivalent ion cobalt(III) hexammine (CoHex) affects the structure of RNA and DNA helices. We find that MD simulations capture the RNA structural change that occurs due to addition of CoHex.

Identifying low and high density amorphous phases during zeolite amorphisation using small and wide angle X-ray scattering

International Nuclear Information System (INIS)

Meneau, F.; Greaves, G.N.

2005-01-01

In situ experiments following the thermal amorphisation of zeolites reveal massive increases in small angle X-ray scattering (SAXS), persisting well beyond the stage where wide angle X-ray scattering (WAXS) can detect that any crystalline phase is present. This heterogeneity in the amorphised phase is attributed to the transition from a low density amorphous phase (LDA) to a high density amorphous phase (HDA) at the glass transition. The fractions of zeolite, LDA and HDA phases obtained from SAXS analysis are discussed in the context of non-linear changes detected in 29 Si solid state NMR during zeolite amorphisation. Whilst the HDA phase is chemically disordered, the LDA phase exhibits much of the Al-Si ordering present in the starting zeolite. These findings are considered in the context of perfect glasses predicted to occur when super strong liquids are supercooled

Efficient Terahertz Wide-Angle NUFFT-Based Inverse Synthetic Aperture Imaging Considering Spherical Wavefront

Directory of Open Access Journals (Sweden)

Jingkun Gao

2016-12-01

Full Text Available An efficient wide-angle inverse synthetic aperture imaging method considering the spherical wavefront effects and suitable for the terahertz band is presented. Firstly, the echo signal model under spherical wave assumption is established, and the detailed wavefront curvature compensation method accelerated by 1D fast Fourier transform (FFT is discussed. Then, to speed up the reconstruction procedure, the fast Gaussian gridding (FGG-based nonuniform FFT (NUFFT is employed to focus the image. Finally, proof-of-principle experiments are carried out and the results are compared with the ones obtained by the convolution back-projection (CBP algorithm. The results demonstrate the effectiveness and the efficiency of the presented method. This imaging method can be directly used in the field of nondestructive detection and can also be used to provide a solution for the calculation of the far-field RCSs (Radar Cross Section of targets in the terahertz regime.

Accuracy and efficiency considerations for wide-angle wavefield extrapolators and scattering operators

Science.gov (United States)

Thomson, C. J.

2005-10-01

Several observations are made concerning the numerical implementation of wide-angle one-way wave equations, using for illustration scalar waves obeying the Helmholtz equation in two space dimensions. This simple case permits clear identification of a sequence of physically motivated approximations of use when the mathematically exact pseudo-differential operator (PSDO) one-way method is applied. As intuition suggests, these approximations largely depend on the medium gradients in the direction transverse to the main propagation direction. A key point is that narrow-angle approximations are to be avoided in the interests of accuracy. Another key consideration stems from the fact that the so-called `standard-ordering' PSDO indicates how lateral interpolation of the velocity structure can significantly reduce computational costs associated with the Fourier or plane-wave synthesis lying at the heart of the calculations. A third important point is that the PSDO theory shows what approximations are necessary in order to generate an exponential one-way propagator for the laterally varying case, representing the intuitive extension of classical integral-transform solutions for a laterally homogeneous medium. This exponential propagator permits larger forward stepsizes. Numerical comparisons with Helmholtz (i.e. full) wave-equation finite-difference solutions are presented for various canonical problems. These include propagation along an interfacial gradient, the effects of a compact inclusion and the formation of extended transmitted and backscattered wave trains by model roughness. The ideas extend to the 3-D, generally anisotropic case and to multiple scattering by invariant embedding. It is concluded that the method is very competitive, striking a new balance between simplifying approximations and computational labour. Complicated wave-scattering effects are retained without the need for expensive global solutions, providing a robust and flexible modelling tool.

Stress measurements by multi-reflection grazing-incidence X-ray diffraction method (MGIXD) using different radiation wavelengths and different incident angles

International Nuclear Information System (INIS)

Marciszko, Marianna; Baczmański, Andrzej; Braham, Chedly; Wróbel, Mirosław; Wroński, Sebastian; Cios, Grzegorz

2017-01-01

The presented study introduces the development of the multi-reflection grazing-incidence X-ray diffraction method (MGIXD) for residual stress determination. The proposed new methodology is aimed at obtaining more reliable experimental data and increasing the depth of non-destructive stress determination below the sample surface. To verify proposed method measurements were performed on a classical X-ray diffractometer (Cu Kα radiation) and using synchrotron radiation (three different wavelengths: λ = 1.2527 Å, λ = 1.5419 Å and λ = 1.7512 Å). The Al2017 alloy subjected to three different surface treatments was investigated in this study. The obtained results showed that the proposed development of MGIXD method, in which not only different incident angles but also different wavelengths of X-ray are used, can be successfully applied for residual stress determination, especially when stress gradients are present in the sample.

Combined in situ small and wide angle X-ray scattering studies of TiO2 nano-particle annealing to 1023 K

DEFF Research Database (Denmark)

Kehres, Jan; Andreasen, Jens Wenzel; Krebs, Frederik C

2010-01-01

Combined in situ small- and wide-angle X-ray scattering (SAXS/WAXS) studies were performed in a recently developed laboratory setup to investigate the dynamical properties of dry oleic acid-capped titanium dioxide nanorods during annealing in an inert gas stream in a temperature interval of 298-1...

Fabrication of multi-focal microlens array on curved surface for wide-angle camera module

Science.gov (United States)

Pan, Jun-Gu; Su, Guo-Dung J.

2017-08-01

In this paper, we present a wide-angle and compact camera module that consists of microlens array with different focal lengths on curved surface. The design integrates the principle of an insect's compound eye and the human eye. It contains a curved hexagonal microlens array and a spherical lens. Compared with normal mobile phone cameras which usually need no less than four lenses, but our proposed system only uses one lens. Furthermore, the thickness of our proposed system is only 2.08 mm and diagonal full field of view is about 100 degrees. In order to make the critical microlens array, we used the inkjet printing to control the surface shape of each microlens for achieving different focal lengths and use replication method to form curved hexagonal microlens array.

Single-Crystal Diffraction from Two-Dimensional Block Copolymer Arrays

International Nuclear Information System (INIS)

Stein, G. E.; Kramer, E. J.; Li, X.; Wang, J.

2007-01-01

The structure of oriented 2D block copolymer single crystals is characterized by grazing-incidence small-angle x-ray diffraction, demonstrating long-range sixfold orientational order. From line shape analysis of the higher-order Bragg diffraction peaks, we determine that translational order decays algebraically with a decay exponent η=0.2, consistent with the Kosterlitz-Thouless-Halperin-Nelson-Young theory for a 2D crystal with a shear modulus μ=2x10 -4 N/m

X-ray diffraction microtomography using synchrotron radiation

CERN Document Server

Barroso, R C; Jesus, E F O; Oliveira, L F

2001-01-01

The X-ray diffraction computed tomography technique is based on the interference phenomena of the coherent scatter. For low-momentum transfer, it is most probable that the scattering interaction will be coherent. A selective discrimination of a given element in a scanned specimen can be realized by fixing the Bragg angle which produces an interference peak and then, to carry out the computed tomography in the standard mode. The image reconstructed exalts the presence of this element with respect to other ones in a sample. This work reports the feasibility of a non-destructive synchrotron radiation X-ray diffraction imaging technique. This research was performed at the X-ray Diffraction beam line of the National Synchrotron Light Laboratory (LNLS) in Brazil. The coherent scattering properties of different tissue and bone substitute materials were evaluated. Furthermore, diffraction patterns of some polycrystalline solids were studied due to industrial and environmental human exposure to these metals. The obtai...

Correlations in the hadronic double diffractive dissociation; Correlacoes na dupla dissociacao difrativa hadronica

Energy Technology Data Exchange (ETDEWEB)

Goldegol, Alexandre

1991-05-01

A given reaction of double diffractive dissociation is studied based on the three-component Deck Model. The correlations among the diffractive slope, the effective mass of the dissociated particle sub-system and the dissociation angle in the Gottfried-Jackson are studied based in this model. 9 refs, 19 figs.

The paediatric Bohler's angle and crucial angle of Gissane: a case series

Directory of Open Access Journals (Sweden)

Crawford Haemish A

2011-01-01

Full Text Available Abstract Background Bohler's angle and the crucial angle of Gissane can be used to assess calcaneal fractures. While the normal adult values of these angles are widely known, the normal paediatric values have not yet been established. Our aim is to investigate Bohler's angle and the crucial angle of Gissane in a paediatric population and establish normal paediatric reference values. Method We measured Bohler's angle and the crucial angle of Gissane using normal plain ankle radiographs of 763 patients from birth to 14 years of age completed over a five year period from July 2003 to June 2008. Results In our paediatric study group, the mean Bohler's angle was 35.2 degrees and the mean crucial angle of Gissane was 111.3 degrees. In an adult comparison group, the mean Bohler's angle was 39.2 degrees and the mean crucial angle of Gissane was 113.8 degrees. The differences in Bohler's angle and the crucial angle of Gissane between these two groups were statistically significant. Conclusion We have presented the normal values of Bohler's angle and the crucial angle of Gissane in a paediatric population. These values may provide a useful comparison to assist with the management of the paediatric calcaneal fracture.

Introducing a standard method for experimental determination of the solvent response in laser pump, x-ray probe time-resolved wide-angle x-ray scattering experiments on systems in solution

DEFF Research Database (Denmark)

Kjær, Kasper Skov; Brandt van Driel, Tim; Kehres, Jan

2013-01-01

In time-resolved laser pump, X-ray probe wide-angle X-ray scattering experiments on systems in solution the structural response of the system is accompanied by a solvent response. The solvent response is caused by reorganization of the bulk solvent following the laser pump event, and in order...... response-the solvent term-experimentally when applying laser pump, X-ray probe time-resolved wide-angle X-ray scattering. The solvent term describes difference scattering arising from the structural response of the solvent to changes in the hydrodynamic parameters: pressure, temperature and density. We...... is demonstrated to exhibit first order behaviour with respect to the amount of energy deposited in the solution. We introduce a standardized method for recording solvent responses in laser pump, X-ray probe time-resolved X-ray wide-angle scattering experiments by using dye mediated solvent heating. Furthermore...

Diffraction of a Gaussian laser beam by a straight edge leading to the formation of optical vortices and elliptical diffraction fringes

Science.gov (United States)

Zeylikovich, Iosif; Nikitin, Aleksandr

2018-04-01

The diffraction of a Gaussian laser beam by a straight edge has been studied theoretically and experimentally for many years. In this paper, we have experimentally observed for the first time the formation of the cusped caustic (for the Fresnel number F ≈ 100) in the shadow region of the straight edge, with the cusp placed near the center of the circular laser beam(λ = 0 . 65 μm) overlapped with the elliptical diffraction fringes. These fringes are originated at the region near the cusp of the caustic where light intensity is zero and the wave phase is singular (the optical vortex). We interpret observed diffraction fringes as a result of interference between the helical wave created by the optical vortex and cylindrical wave diffracted at the straight edge. We have theoretically revealed that the number of high contrast diffraction fringes observable in a shadow region is determined by the square of the diffracted angles in the range of spatial frequencies of the scattered light field in excellent agreement with experiments. The extra phase singularities with opposite charges are also observed along the shadow boundary as the fork-like diffraction fringes.

Experimental investigation of Popper’s proposed ghost-diffraction experiment

Science.gov (United States)

Bolduc, Eliot; Karimi, Ebrahim; Piché, Kevin; Leach, Jonathan; Boyd, Robert W.

2017-10-01

In an effort to challenge the Copenhagen interpretation of quantum mechanics, Karl Popper proposed an experiment involving spatially separated entangled particles. In this experiment, one of the particles passes through a very narrow slit, and thereby its position becomes well-defined. This particle therefore diffracts into a large divergence angle; this effect can be understood as a consequence of the Heisenberg uncertainty principle. Popper further argued that its entangled partner would become comparably localized in position, and that, according to his understanding of the Copenhagen interpretation of quantum mechanics, the ‘mere knowledge’ of the position of this particle would cause it also to diffract into a large divergence angle. Popper recognized that such behavior could violate the principle of causality in that the slit could be removed and the partner particle would be expected to respond instantaneously. Popper thus concluded that it was most likely the case that, in an actual experiment, the partner photon would not undergo increased diffractive spreading and thus that the Copenhagen interpretation is incorrect. Here, we report and analyze the results of an implementation of Popper’s proposal. We find that the partner beam does not undergo increased diffractive spreading. Our work helps to clarify the issues raised in Popper’s proposal, and it provides further insight into the nature of entanglement and its relation to the uncertainty principle as applied to correlated particles.

Wide-angle ITER-prototype tangential infrared and visible viewing system for DIII-D

Energy Technology Data Exchange (ETDEWEB)

Lasnier, C. J., E-mail: lasnier@LLNL.gov; Allen, S. L.; Ellis, R. E.; Fenstermacher, M. E.; McLean, A. G.; Meyer, W. H.; Morris, K.; Seppala, L. G. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94551-0808 (United States); Crabtree, K. [College of Optics, University of Arizona, Tucson, Arizona 85721 (United States); Van Zeeland, M. A. [General Atomics, P.O. Box 85608, San Diego, California 92186-5608 (United States)

2014-11-15

An imaging system with a wide-angle tangential view of the full poloidal cross-section of the tokamak in simultaneous infrared and visible light has been installed on DIII-D. The optical train includes three polished stainless steel mirrors in vacuum, which view the tokamak through an aperture in the first mirror, similar to the design concept proposed for ITER. A dichroic beam splitter outside the vacuum separates visible and infrared (IR) light. Spatial calibration is accomplished by warping a CAD-rendered image to align with landmarks in a data image. The IR camera provides scrape-off layer heat flux profile deposition features in diverted and inner-wall-limited plasmas, such as heat flux reduction in pumped radiative divertor shots. Demonstration of the system to date includes observation of fast-ion losses to the outer wall during neutral beam injection, and shows reduced peak wall heat loading with disruption mitigation by injection of a massive gas puff.

Diffraction by an immersed elastic wedge

CERN Document Server

Croisille, Jean-Pierre

1999-01-01

This monograph presents the mathematical description and numerical computation of the high-frequency diffracted wave by an immersed elastic wave with normal incidence. The mathematical analysis is based on the explicit description of the principal symbol of the pseudo-differential operator connected with the coupled linear problem elasticity/fluid by the wedge interface. This description is subsequently used to derive an accurate numerical computation of diffraction diagrams for different incoming waves in the fluid, and for different wedge angles. The method can be applied to any problem of coupled waves by a wedge interface. This work is of interest for any researcher concerned with high frequency wave scattering, especially mathematicians, acousticians, engineers.

Diffraction imaging and velocity analysis using oriented velocity continuation

KAUST Repository

Decker, Luke

2014-08-05

We perform seismic diffraction imaging and velocity analysis by separating diffractions from specular reflections and decomposing them into slope components. We image slope components using extrapolation in migration velocity in time-space-slope coordinates. The extrapolation is described by a convection-type partial differential equation and implemented efficiently in the Fourier domain. Synthetic and field data experiments show that the proposed algorithm is able to detect accurate time-migration velocities by automatically measuring the flatness of events in dip-angle gathers.

Hard diffraction and deep inelastic scattering

International Nuclear Information System (INIS)

Bjorken, J.D.

1994-04-01

Since the advent of hard-collision physics, the study of diffractive processes - shadow physics - has been less prominent than before. However, there is now a renewed interest in the subject, especially in that aspect which synthesizes the short-distance, hard-collision phenomena with the classical physics of large rapidity-gaps. This is especially stimulated by the recent data on deep-inelastic scattering from HERA, as well as the theoretical work which relates to it. The word diffraction is sometimes used by high-energy physicists in a loose way. The author defines this term to mean: A diffractive process occurs if and only if there is a large rapidity gap in the produced-particle phase space which is not exponentially suppressed. Here a rapidity gap means essentially no hadrons produced into the rapidity gap (which operates in the open-quotes legoclose quotes phase-space of pseudo-rapidity and azimuthal angle). And non-exponential suppression implies that the cross-section for creating a gap with width Δη does not have a power-law decrease with increasing subenergy s=e Δη , but behaves at most like some power of pseudorapidity Δη∼log(s). The term hard diffraction shall simply refer to those diffractive process which have jets in the final-state phase-space

Multiple scattering in grazing-incidence X-ray diffraction: impact on lattice-constant determination in thin films

Energy Technology Data Exchange (ETDEWEB)

Resel, Roland, E-mail: roland.resel@tugraz.at; Bainschab, Markus; Pichler, Alexander [Graz University of Technology, Graz (Austria); Dingemans, Theo [Delft University of Technology, Delft (Netherlands); Simbrunner, Clemens [Johannes Kepler University, Linz (Austria); University of Bremen, Bremen (Germany); Stangl, Julian [Johannes Kepler University, Linz (Austria); Salzmann, Ingo [Humboldt University, Berlin (Germany)

2016-04-20

The use of grazing-incidence X-ray diffraction to determine the crystal structure from thin films requires accurate positions of Bragg peaks. Refraction effects and multiple scattering events have to be corrected or minimized. Dynamical scattering effects are observed in grazing-incidence X-ray diffraction experiments using an organic thin film of 2,2′:6′,2′′-ternaphthalene grown on oxidized silicon as substrate. Here, a splitting of all Bragg peaks in the out-of-plane direction (z-direction) has been observed, the magnitude of which depends both on the incidence angle of the primary beam and the out-of-plane angle of the scattered beam. The incident angle was varied between 0.09° and 0.25° for synchrotron radiation of 10.5 keV. This study reveals comparable intensities of the split peaks with a maximum for incidence angles close to the critical angle of total external reflection of the substrate. This observation is rationalized by two different scattering pathways resulting in diffraction peaks at different positions at the detector. In order to minimize the splitting, the data suggest either using incident angles well below the critical angle of total reflection or angles well above, which sufficiently attenuates the contributions from the second scattering path. This study highlights that the refraction of X-rays in (organic) thin films has to be corrected accordingly to allow for the determination of peak positions with sufficient accuracy. Based thereon, a reliable determination of the lattice constants becomes feasible, which is required for crystallographic structure solutions from thin films.

X-ray diffraction and mechanical properties studies on Kevlar-49 fibres

International Nuclear Information System (INIS)

Abdo, S. M.

1988-01-01

The thesis deals with the effect of annealing in the temperature range 150-500 degrees celsius, and long-term ageing (1-150 days) at 150 degrees celsius, on the structure and mechanical properties of Kevlar-49 fibres. Wide-angle x-ray diffraction techniques were used to characterize quantitatively the structure in terms of crystallinity, crystallite size and orientation. The mechanical properties were characterized in terms of initial Young's modulus, tensile strength, and elongation at break. Thermogravimetric analysis was performed to determine the loss in weight after annealing. Differential Thermal Analysis (DTA) scan was performed to determine the 'peak melting point' of the untreated Kevlar-49 fibres. The surface topography, fracture behaviour and microfibrillar character of Kevlar-49 were studied in a scanning electron microscope. 52 refs., 30 figs., 6 tabs. (A.M.H.)

Digital Image Correlation of 2D X-ray Powder Diffraction Data for Lattice Strain Evaluation

Science.gov (United States)

Zhang, Hongjia; Sui, Tan; Daisenberger, Dominik; Fong, Kai Soon

2018-01-01

High energy 2D X-ray powder diffraction experiments are widely used for lattice strain measurement. The 2D to 1D conversion of diffraction patterns is a necessary step used to prepare the data for full pattern refinement, but is inefficient when only peak centre position information is required for lattice strain evaluation. The multi-step conversion process is likely to lead to increased errors associated with the ‘caking’ (radial binning) or fitting procedures. A new method is proposed here that relies on direct Digital Image Correlation analysis of 2D X-ray powder diffraction patterns (XRD-DIC, for short). As an example of using XRD-DIC, residual strain values along the central line in a Mg AZ31B alloy bar after 3-point bending are calculated by using both XRD-DIC and the conventional ‘caking’ with fitting procedures. Comparison of the results for strain values in different azimuthal angles demonstrates excellent agreement between the two methods. The principal strains and directions are calculated using multiple direction strain data, leading to full in-plane strain evaluation. It is therefore concluded that XRD-DIC provides a reliable and robust method for strain evaluation from 2D powder diffraction data. The XRD-DIC approach simplifies the analysis process by skipping 2D to 1D conversion, and opens new possibilities for robust 2D powder diffraction data analysis for full in-plane strain evaluation. PMID:29543728

Digital Image Correlation of 2D X-ray Powder Diffraction Data for Lattice Strain Evaluation

Directory of Open Access Journals (Sweden)

Hongjia Zhang

2018-03-01

Full Text Available High energy 2D X-ray powder diffraction experiments are widely used for lattice strain measurement. The 2D to 1D conversion of diffraction patterns is a necessary step used to prepare the data for full pattern refinement, but is inefficient when only peak centre position information is required for lattice strain evaluation. The multi-step conversion process is likely to lead to increased errors associated with the ‘caking’ (radial binning or fitting procedures. A new method is proposed here that relies on direct Digital Image Correlation analysis of 2D X-ray powder diffraction patterns (XRD-DIC, for short. As an example of using XRD-DIC, residual strain values along the central line in a Mg AZ31B alloy bar after 3-point bending are calculated by using both XRD-DIC and the conventional ‘caking’ with fitting procedures. Comparison of the results for strain values in different azimuthal angles demonstrates excellent agreement between the two methods. The principal strains and directions are calculated using multiple direction strain data, leading to full in-plane strain evaluation. It is therefore concluded that XRD-DIC provides a reliable and robust method for strain evaluation from 2D powder diffraction data. The XRD-DIC approach simplifies the analysis process by skipping 2D to 1D conversion, and opens new possibilities for robust 2D powder diffraction data analysis for full in-plane strain evaluation.

A credit card verifier structure using diffraction and spectroscopy concepts

Science.gov (United States)

Sumriddetchkajorn, Sarun; Intaravanne, Yuttana

2008-04-01

We propose and experimentally demonstrate an angle-multiplexing based optical structure for verifying a credit card. Our key idea comes from the fact that the fine detail of the embossed hologram stamped on the credit card is hard to duplicate and therefore its key color features can be used for distinguishing between the real and counterfeit ones. As the embossed hologram is a diffractive optical element, we choose to shine one at a time a number of broadband lightsources, each at different incident angle, on the embossed hologram of the credit card in such a way that different color spectra per incident angle beam is diffracted and separated in space. In this way, the number of pixels of each color plane is investigated. Then we apply a feed forward back propagation neural network configuration to separate the counterfeit credit card from the real one. Our experimental demonstration using two off-the-shelf broadband white light emitting diodes, one digital camera, a 3-layer neural network, and a notebook computer can identify all 69 counterfeit credit cards from eight real credit cards.

Wide-angle imaging LIDAR (WAIL): a ground-based instrument for monitoring the thickness and density of optically thick clouds

International Nuclear Information System (INIS)

Love, Steven P.; Davis, A.B.; Rohde, C.A.; Ho, Cheng

2001-01-01

Traditional lidar provides little information on dense clouds beyond the range to their base (ceilometry), due to their extreme opacity. At most optical wavelengths, however, laser photons are not absorbed but merely scattered out of the beam, and thus eventually escape the cloud via multiple scattering, producing distinctive extended space- and time-dependent patterns which are, in essence, the cloud's radiative Green functions. These Green functions, essentially 'movies' of the time evolution of the spatial distribution of escaping light, are the primary data products of a new type of lidar: Wide Angle Imaging Lidar (WAIL). WAIL data can be used to infer both optical depth and physical thickness of clouds, and hence the cloud liquid water content. The instrumental challenge is to accommodate a radiance field varying over many orders of magnitude and changing over widely varying time-scales. Our implementation uses a high-speed microchannel plate/crossed delay line imaging detector system with a 60-degree full-angle field of view, and a 532 nm doubled Nd:YAG laser. Nighttime field experiments testing various solutions to this problem show excellent agreement with diffusion theory, and retrievals yield plausible values for the optical and geometrical parameters of the observed cloud decks.

Active probing of cloud multiple scattering, optical depth, vertical thickness, and liquid water content using wide-angle imaging lidar

Science.gov (United States)

Love, Steven P.; Davis, Anthony B.; Rohde, Charles A.; Tellier, Larry; Ho, Cheng

2002-09-01

At most optical wavelengths, laser light in a cloud lidar experiment is not absorbed but merely scattered out of the beam, eventually escaping the cloud via multiple scattering. There is much information available in this light scattered far from the input beam, information ignored by traditional 'on-beam' lidar. Monitoring these off-beam returns in a fully space- and time-resolved manner is the essence of our unique instrument, Wide Angle Imaging Lidar (WAIL). In effect, WAIL produces wide-field (60-degree full-angle) 'movies' of the scattering process and records the cloud's radiative Green functions. A direct data product of WAIL is the distribution of photon path lengths resulting from multiple scattering in the cloud. Following insights from diffusion theory, we can use the measured Green functions to infer the physical thickness and optical depth of the cloud layer, and, from there, estimate the volume-averaged liquid water content. WAIL is notable in that it is applicable to optically thick clouds, a regime in which traditional lidar is reduced to ceilometry. Here we present recent WAIL data on various clouds and discuss the extension of WAIL to full diurnal monitoring by means of an ultra-narrow magneto-optic atomic line filter for daytime measurements.

Active probing of cloud multiple scattering, optical depth, vertical thickness, and liquid water content using wide-angle imaging LIDAR

International Nuclear Information System (INIS)

Love, Steven P.; Davis, Anthony B.; Rohde, Charles A.; Tellier, Larry L.; Ho, Cheng

2002-01-01

At most optical wavelengths, laser light in a cloud lidar experiment is not absorbed but merely scattered out of the beam, eventually escaping the cloud via multiple scattering. There is much information available in this light scattered far from the input beam, information ignored by traditional 'on-beam' lidar. Monitoring these off-beam returns in a fully space- and time-resolved manner is the essence of our unique instrument, Wide Angle Imaging Lidar (WAIL). In effect, WAIL produces wide-field (60-degree full-angle) 'movies' of the scattering process and records the cloud's radiative Green functions. A direct data product of WAIL is the distribution of photon path lengths resulting from multiple scattering in the cloud. Following insights from diffusion theory, we can use the measured Green functions to infer the physical thickness and optical depth of the cloud layer, and, from there, estimate the volume-averaged liquid water content. WAIL is notable in that it is applicable to optically thick clouds, a regime in which traditional lidar is reduced to ceilometry. Here we present recent WAIL data oti various clouds and discuss the extension of WAIL to full diurnal monitoring by means of an ultra-narrow magneto-optic atomic line filter for daytime measurements.

Seismic structure from multi-channel seismic reflection and wide-angle data of Transect 0E in the Southern Gulf of California

Science.gov (United States)

Paramo, P.; Holbrook, W.; Brown, H.; Lizarralde, D.; Fletcher, J.; Umhoefer, P.; Kent, G.; Harding, A.; Gonzalez, A.; Axen, G.

2005-12-01

We present a velocity model from wide-angle data along with coincident prestack depth migration sections from seismic reflection data collected in the southern Gulf of California. Transect 0E runs NE to SW from the hills of Sierra Madre in mainland Mexico near Mazatlan to approximately 115 km into Gulf of California waters. Wide-angle data were recorded by 9 ocean bottom seismometers, deployed by the R/V New Horizon and 10 Reftek seismometers located along onshore extension of the transect. The average spacing for the OBS and Refteks is ~12 km and shots were fired from the R/V Maurice Ewing at 150 m intervals. Transect 0E crosses what it is believed to be extended continental crust and lies in the initial direction of extension characteristic of the proto-gulf. Preliminary results from the velocity model show upper crustal velocities of 6.1-6.3 km/s and lower crustal velocities of 6.7-7.0 km/s along the entire transect. Seismic velocities and crustal thicknesses observed along transect 0E are characteristic of non-volcanic margins.

X-ray diffraction patterns and diffracted intensity of Kα spectral lines of He-like ions

Science.gov (United States)

Goyal, Arun; Khatri, Indu; Singh, A. K.; Sharma, Rinku; Mohan, Man

2017-09-01

In the present paper, we have calculated fine-structure energy levels related to the configurations 1s2s, 1s2p, 1s3s and 1s3p by employing GRASP2K code. We have also computed radiative data for transitions from 1s2p 1 P1o, 1s2p 3 P2o, 1s2p 3 P1o and 1s2s 3S1 to the ground state 1s2. We have made comparisons of our presented energy levels and transition wavelengths with available results compiled by NIST and good agreement is achieved. We have also provided X-ray diffraction (XRD) patterns of Kα spectral lines, namely w, x, y and z of Cu XXVIII, Kr XXXV and Mo with diffraction angle and maximum diffracted intensity which is not published elsewhere in the literature. We believe that our presented results may be beneficial in determination of the order parameter, X-ray crystallography, solid-state drug analysis, forensic science, geological and medical applications.

X-ray diffraction evidence for myelin disorder in brain from humans with Alzheimer's disease.

Science.gov (United States)

Chia, L S; Thompson, J E; Moscarello, M A

1984-09-05

Wide-angle X-ray diffraction studies revealed that the lipid phase transition temperature of myelin from brain tissue of humans with Alzheimer's disease was about 12 degrees C lower than that of normal age-matched controls, indicating differences in the physical organization of the myelin lipid bilayer. Elevated levels of malondialdehyde and conjugated diene were found in brain tissue from humans with Alzheimer's disease, indicating an increased amount of lipid peroxidation over the controls. An increase in myelin disorder and in lipid peroxidation can both be correlated with aging in human brain, but the changes in myelin from humans with Alzheimer's disease are more pronounced than in normal aging. These changes might represent severe or accelerated aging.

Diffraction of polarized light on periodic structures

International Nuclear Information System (INIS)

Bukanina, V; Divakov, D; Tyutyunnik, A; Hohlov, A

2012-01-01

Periodic structures as photonic crystals are widely used in modern laser devices, communication technologies and for creating various beam splitters and filters. Diffraction gratings are applied for creating 3D television sets, DVD and Blu-ray drives and reflective structures (Berkley mirror). It is important to simulate diffraction on such structures to design optical systems with predetermined properties based on photonic crystals and diffraction gratings. Methods of simulating diffraction on periodic structures uses theory of Floquet-Bloch and rigorous coupled-wave analysis (RCWA). Current work is dedicated to analysis of photonic band gaps and simulating diffraction on one-dimensional binary diffraction grating using RCWA. The Maxwell's equations for isotropic media and constitutive relations based on the cgs system were used as a model.

Note: Optimization of magnifying a polarization angle with Littrow layout blazed gratings.

Science.gov (United States)

Sasao, H; Arakawa, H; Imazawa, R; Kawano, Y; Itami, K; Kubo, H

2017-03-01

Magnification of a polarization angle with Littrow layout gratings has been developed. High magnification with a factor of 7.7 using two gratings in Littrow layout was experimentally proved. The magnification range was investigated by calculation at a wavelength of 10.6 μm. The method can be applied for a high magnification factor >30. Larger groove numbers and smaller blaze angles are suitable for the large magnification. Statistical fluctuation of the diffracted polarization angle is compared with that of the incident polarization angle.

Determination of surface tension coefficient of liquids by diffraction of light on capillary waves

International Nuclear Information System (INIS)

Nikolić, D; Nešić, Lj

2012-01-01

This paper describes a simple technique for determining the coefficient of the surface tension of liquids, based on laser light diffraction on capillary waves. Capillary waves of given frequency are created by an exciter needle acting on the surface of liquid and represent a reflective diffraction grating, the constant of which (the wavelength of capillary waves) can be determined based on a known incidence angle of light (grazing angle). We obtain the coefficient of the surface tension of liquids by applying the dispersion relation for capillary waves and analyze the difficulties that arise when setting up and conducting the experiment in detail. (paper)

Classical system underlying a diffracting quantum billiard

Indian Academy of Sciences (India)

Manan Jain

2018-01-05

Jan 5, 2018 ... Wave equation; rays; quantum chaos. PACS Nos 03.65.Ge; 05.45.Mt; 42.25.Fx. 1. Introduction. Diffraction [1] is a complex wave phenomenon which manifests classically and quantum mechanically. Among a wide range of systems where diffraction becomes important, there is an interesting situation of.

Small-angle scattering studies of the fully hydrated phospholipid DPPC

Energy Technology Data Exchange (ETDEWEB)

Mason, P.C.; Gaulin, B.D. [Department of Physics and Astronomy, McMaster University, Hamilton, Ontario, L8S 4M1 (CANADA); Epand, R.M. [Department of Biochemistry, McMaster University, Hamilton, Ontario, L8N 3Z5 (CANADA); Wignall, G.D.; Lin, J.S. [Center for Small-Angle Scattering Research, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831 (United States)

1999-01-01

Small-angle neutron and x-ray scattering studies have been carried out on fully hydrated dipalmitoylphosphatidylcholine (DPPC) multilamellar vesicles. This system is known to exhibit two distinct ripple (P{sub {beta}{sup {prime}}}) phases, which depend on sample history, at temperatures intermediate to its high-temperature liquid crystalline (L{sub {alpha}}), phase, and its low-temperature gel (L{sub {beta}{sup {prime}}}), phase. On cooling from the L{sub {alpha}} phase, the P{sub {beta}{sup {prime}}} phase displays a complex multipeak diffraction pattern that differs significantly from the diffraction pattern seen in the P{sub {beta}{sup {prime}}} phase obtained on warming from the L{sub {beta}{sup {prime}}} phase. Examining the P{sub {beta}{sup {prime}}} phase on cooling using small-angle neutron scattering and x-ray diffraction techniques leads to the conclusion that this phase is characterized by a long wavelength ripple ({lambda}{sub r}{approximately}330thinsp{Angstrom}) and a highly monoclinic unit cell ({gamma}{approximately}125{degree}). As the P{sub {beta}{sup {prime}}} phase is traversed in temperature, the ripple wavelength changes significantly while the monoclinicity remains unchanged. Ripples from the P{sub {beta}{sup {prime}}} phase are seen to persist into the L{sub {beta}{sup {prime}}} phase on cooling, leading to increased small-angle scattering characteristic of a disordered stacking of the lamellae. {copyright} {ital 1999} {ital The American Physical Society}

Elastic wave diffraction by infinite wedges

Energy Technology Data Exchange (ETDEWEB)

Fradkin, Larissa; Zernov, Victor [Sound Mathematics Ltd., Cambridge CB4 2AS (United Kingdom); Gautesen, Arthur [Mathematics Department, Iowa State University and Ames Laboratory (United States); Darmon, Michel, E-mail: l.fradkin@soundmathematics.com [CEA-LIST, CEA-Saclay, 91191 Gif-sur-Yvette (France)

2011-01-01

We compare two recently developed semi-analytical approaches to the classical problem of diffraction by an elastic two dimensional wedge, one based on the reciprocity principle and Fourier Transform and another, on the representations of the elastodynamic potentials in the form of Sommerfeld Integrals. At present, in their common region of validity, the approaches are complementary, one working better than the other at some isolated angles of incidence.

Lattice strain measurements on sandstones under load using neutron diffraction

Science.gov (United States)

Frischbutter, A.; Neov, D.; Scheffzük, Ch.; Vrána, M.; Walther, K.

2000-11-01

Neutron diffraction methods (both time-of-flight- and angle-dispersive diffraction) are applied to intracrystalline strain measurements on geological samples undergoing uniaxial increasing compressional load. The experiments were carried out on Cretaceous sandstones from the Elbezone (East Germany), consisting of >95% quartz which are bedded but without crystallographic preferred orientation of quartz. From the stress-strain relation the Young's modulus for our quartz sample was determined to be (72.2±2.9) GPa using results of the neutron time-of-flight method. The influence of different kinds of bedding in sandstones (laminated and convolute bedding) could be determined. We observed differences of factor 2 (convolute bedding) and 3 (laminated bedding) for the elastic stiffness, determined with angle dispersive neutron diffraction (crystallographic strain) and with strain gauges (mechanical strain). The data indicate which geological conditions may influence the stress-strain behaviour of geological materials. The influence of bedding on the stress-strain behaviour of a laminated bedded sandstone was indicated by direct residual stress measurements using neutron time-of-flight diffraction. The measurements were carried out six days after unloading the sample. Residual strain was measured for three positions from the centre to the periphery and within two radial directions of the cylinder. We observed that residual strain changes from extension to compression in a different manner for two perpendicular directions of the bedding plane.

Atomic quasi-Bragg-diffraction in a magnetic field

NARCIS (Netherlands)

Domen, K.F.E.M.; Jansen, M.A.H.M.; Dijk, van W.; Leeuwen, van K.A.H.

2009-01-01

We report on a technique to split an at. beam coherently with an easily adjustable splitting angle. In our expt. metastable helium atoms in the |{1s2s}3S1 M=1 state diffract from a polarization gradient light field formed by counterpropagating .sigma.+ and .sigma.- polarized laser beams in the

Structural evolution of regenerated silk fibroin under shear: Combined wide- and small-angle x-ray scattering experiments using synchrotron radiation

International Nuclear Information System (INIS)

Rossle, Manfred; Panine, Pierre; Urban, Volker S.; Riekel, Christine

2004-01-01

The structural evolution of regenerated Bombyx mori silk fibroin during shearing with a Couette cell has been studied in situ by synchrotron radiation small- and wide-angle x-ray scattering techniques. An elongation of fibroin molecules was observed with increasing shear rate, followed by an aggregation phase. The aggregates were found to be amorphous with β-conformation according to infrared spectroscopy. Scanning x-ray microdiffraction with a 5 (micro)m beam on aggregated material, which had solidified in air, showed silk II reflections and a material with equatorial reflections close to the silk I structure reflections, but with strong differences in reflection intensities. This silk I type material shows up to two low-angle peaks suggesting the presence of water molecules that might be intercalated between hydrogen-bonded sheets.

Structural evolution of regenerated silk fibroin under shear: Combined wide- and small-angle x-ray scattering experiments using synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Rossle, Manfred [European Molecular Biology Laboratory (EMBL), France; Panine, Pierre [European Synchrotron Radiation Facility (ESRF); Urban, Volker S [ORNL; Riekel, Christine [European Synchrotron Radiation Facility (ESRF)

2004-04-01

The structural evolution of regenerated Bombyx mori silk fibroin during shearing with a Couette cell has been studied in situ by synchrotron radiation small- and wide-angle x-ray scattering techniques. An elongation of fibroin molecules was observed with increasing shear rate, followed by an aggregation phase. The aggregates were found to be amorphous with {beta}-conformation according to infrared spectroscopy. Scanning x-ray microdiffraction with a 5 {micro}m beam on aggregated material, which had solidified in air, showed silk II reflections and a material with equatorial reflections close to the silk I structure reflections, but with strong differences in reflection intensities. This silk I type material shows up to two low-angle peaks suggesting the presence of water molecules that might be intercalated between hydrogen-bonded sheets.

Watching Nanoparticles Form: An In Situ (Small-/Wide-Angle X-ray Scattering/Total Scattering) Study of the Growth of Yttria-Stabilised Zirconia in Supercritical Fluids

DEFF Research Database (Denmark)

Tyrsted, Christoffer; Pauw, Brian; Jensen, Kirsten Marie Ørnsbjerg

2012-01-01

Understanding nanoparticle formation reactions requires multitechnique in situ characterisation, since no single characterisation technique provides adequate information. Here, the first combined small-angle X-ray scattering (SAXS)/wide-angle X-ray scattering (WAXS)/total-scattering study of nano...... of nanoparticle formation is presented. We report on the formation and growth of yttria-stabilised zirconia (YSZ) under the extreme conditions of supercritical methanol for particles with Y2O3 equivalent molar fractions of 0, 4, 8, 12 and 25%....

Global search in photoelectron diffraction structure determination using genetic algorithms

Energy Technology Data Exchange (ETDEWEB)

Viana, M L [Departamento de Fisica, Icex, UFMG, Belo Horizonte, Minas Gerais (Brazil); Muino, R Diez [Donostia International Physics Center DIPC, Paseo Manuel de Lardizabal 4, 20018 San Sebastian (Spain); Soares, E A [Departamento de Fisica, Icex, UFMG, Belo Horizonte, Minas Gerais (Brazil); Hove, M A Van [Department of Physics and Materials Science, City University of Hong Kong, Hong Kong (China); Carvalho, V E de [Departamento de Fisica, Icex, UFMG, Belo Horizonte, Minas Gerais (Brazil)

2007-11-07

Photoelectron diffraction (PED) is an experimental technique widely used to perform structural determinations of solid surfaces. Similarly to low-energy electron diffraction (LEED), structural determination by PED requires a fitting procedure between the experimental intensities and theoretical results obtained through simulations. Multiple scattering has been shown to be an effective approach for making such simulations. The quality of the fit can be quantified through the so-called R-factor. Therefore, the fitting procedure is, indeed, an R-factor minimization problem. However, the topography of the R-factor as a function of the structural and non-structural surface parameters to be determined is complex, and the task of finding the global minimum becomes tough, particularly for complex structures in which many parameters have to be adjusted. In this work we investigate the applicability of the genetic algorithm (GA) global optimization method to this problem. The GA is based on the evolution of species, and makes use of concepts such as crossover, elitism and mutation to perform the search. We show results of its application in the structural determination of three different systems: the Cu(111) surface through the use of energy-scanned experimental curves; the Ag(110)-c(2 x 2)-Sb system, in which a theory-theory fit was performed; and the Ag(111) surface for which angle-scanned experimental curves were used. We conclude that the GA is a highly efficient method to search for global minima in the optimization of the parameters that best fit the experimental photoelectron diffraction intensities to the theoretical ones.

From the Atlas to the Rif a Crustal seismic image across Morocco: The SIMA & RIFSEIS control source wide-angle seismic reflection data

Science.gov (United States)

Carbonell, Ramon; Ayarza, Puy; Gallart, Josep; Diaz, Jordi; Harnafi, Mimoun; Levander, Alan; Teixell, Antonio

2014-05-01

The velocity structure of the crust and the geometry of the Moho across Morocco has been the main target of two recently acquired wide-angle seismic reflection transects. One is the SIMA experiment which provided seismic constraints beneath the Atlas Mountains and the second has been the RIFSEIS experiment which sampled the RIF orogen. Jointly these controlled source wide-angle seismic reflection data results in an almost 700 km, seismic profile going from the the Sahara craton across the High and Middle Atlas and Rif Mountain till the Gibraltar-Arc (Alboran). Current work on the interpretation of the seismic data-set is based on forward modeling, ray-tracing, as well as low fold wide-angle stacking. The data has resulted in a detailed crustal structure and velocity model for the Atlas Mountains and a 700 km transect revealing the irregular topography of the Moho beneath these two mountain orogens. Results indicate that the High Atlas features a moderate crustal thickness and that shortening is resolved at depth through a crustal root where the Saharan crust under-thrusts below the Moroccan crust, defining a lower crust imbrication which locally places the Moho boundary at, approximately, 40 km depth. The P-wave velocity model is characterized, in averaged, by relatively low velocities. These low deep crustal velocities together with other geophysical observables such as: conductivity estimates derived from Mt measurements; moderate Bouguer gravity anomaly; surface exposures of recent alkaline volcanics; lead the interpretation to propose that partial melts are currently emplaced in the deep crustal levels and in the upper mantle. The Moho discontinuity defines a crust which is in average relatively thin beneath the Atlas which is almost a 4000 m high orogenic belt. The resulting model supports existence of mantle upwelling as a possible mechanism that contributes, significantly, to maintain the High Atlas topography.

High precision refractometry based on Fresnel diffraction from phase plates.

Science.gov (United States)

Tavassoly, M Taghi; Naraghi, Roxana Rezvani; Nahal, Arashmid; Hassani, Khosrow

2012-05-01

When a transparent plane-parallel plate is illuminated at a boundary region by a monochromatic parallel beam of light, Fresnel diffraction occurs because of the abrupt change in phase imposed by the finite change in refractive index at the plate boundary. The visibility of the diffraction fringes varies periodically with changes in incident angle. The visibility period depends on the plate thickness and the refractive indices of the plate and the surrounding medium. Plotting the phase change versus incident angle or counting the visibility repetition in an incident-angle interval provides, for a given plate thickness, the refractive index of the plate very accurately. It is shown here that the refractive index of a plate can be determined without knowing the plate thickness. Therefore, the technique can be utilized for measuring plate thickness with high precision. In addition, by installing a plate with known refractive index in a rectangular cell filled with a liquid and following the described procedures, the refractive index of the liquid is obtained. The technique is applied to measure the refractive indices of a glass slide, distilled water, and ethanol. The potential and merits of the technique are also discussed.

Future directions in high-pressure neutron diffraction

Science.gov (United States)

Guthrie, M.

2015-04-01

The ability to manipulate structure and properties using pressure has been well known for many centuries. Diffraction provides the unique ability to observe these structural changes in fine detail on lengthscales spanning atomic to nanometre dimensions. Amongst the broad suite of diffraction tools available today, neutrons provide unique capabilities of fundamental importance. However, to date, the growth of neutron diffraction under extremes of pressure has been limited by the weakness of available sources. In recent years, substantial government investments have led to the construction of a new generation of neutron sources while existing facilities have been revitalized by upgrades. The timely convergence of these bright facilities with new pressure-cell technologies suggests that the field of high-pressure (HP) neutron science is on the cusp of substantial growth. Here, the history of HP neutron research is examined with the hope of gleaning an accurate prediction of where some of these revolutionary capabilities will lead in the near future. In particular, a dramatic expansion of current pressure-temperature range is likely, with corresponding increased scope for extreme-conditions science with neutron diffraction. This increase in coverage will be matched with improvements in data quality. Furthermore, we can also expect broad new capabilities beyond diffraction, including in neutron imaging, small angle scattering and inelastic spectroscopy.

Bio-Inspired Wide-Angle Broad-Spectrum Cylindrical Lens Based on Reflections from Micro-Mirror Array on a Cylindrical Elastomeric Membrane

Directory of Open Access Journals (Sweden)

Chi-Chieh Huang

2014-06-01

Full Text Available We present a wide-angle, broad-spectrum cylindrical lens based on reflections from an array of three-dimensional, high-aspect-ratio micro-mirrors fabricated on a cylindrical elastomeric substrate, functionally inspired by natural reflecting superposition compound eyes. Our device can perform one-dimensional focusing and beam-shaping comparable to conventional refraction-based cylindrical lenses, while avoiding chromatic aberration. The focal length of our cylindrical lens is 1.035 mm, suitable for micro-optical systems. Moreover, it demonstrates a wide field of view of 152° without distortion, as well as modest spherical aberrations. Our work could be applied to diverse applications including laser diode collimation, barcode scanning, holography, digital projection display, microlens arrays, and optical microscopy.

X-ray diffraction 2 - diffraction principles

International Nuclear Information System (INIS)

O'Connor, B.

1999-01-01

Full text: The computation of powder diffraction intensities is based on the principle that the powder pattern comprises the summation of the intensity contributions from each of the crystallites (or single crystals) in the material. Therefore, it is of value for powder diffractionists to appreciate the form of the expression for calculating single crystal diffraction pattern intensities. This knowledge is especially important for Rietveld analysis practitioners in terms of the (i) mathematics of the method and (ii) retrieving single crystal structure data from the literature. We consider the integrated intensity from a small single crystal being rotated at velocity ω through the Bragg angle θ for reflection (hkl).... I(hkl) = [l o /ω]. [e 4 /m 2 c 4 ]. [λ 3 δV F(hkl) 2 /υ 2 ].[(1+cos 2 2θ)/2sin2θ] where e, m and c are the usual fundamental constants; λ is the x-ray wavelength, δV is the crystallite volume; F(hkl) is the structure factor; υ is the unit cell volume; and (1+cos 2 θ)/2sin2θ] is the Lorentz-polarisation factor for an unpolarised incident beam. The expression does not include a contribution for extinction. The influence of factors λ, δV, F(hkl) and υ on the intensities should be appreciated by powder diffractionists, especially the structure factor, F(hkl), which is responsible for the fingerprint nature of diffraction patterns, such as the rise and fall of intensity from peak to peak. The structure factor expression represents the summation of the scattered waves from each of the j scattering centres (i e atoms) in the unit cell: F(hkl) Σ f j exp[2πi (h.x j +k.y i +l. z i )] T j . Symbol f is the scattering factor (representing the atom-type scattering efficiency); (x, y, z) are the fractional position coordinates of atom j within the unit cell; and T is the thermal vibration factor for the atom given by: T j = 8π 2 2 > sin 2 θ/λ 2 with 2 > being the mean-square vibration amplitude of the atom (assumed to be isotropic). The

A study on displacement of crystalline diffraction peaks in electron-beam irradiated filter paper cellulose

International Nuclear Information System (INIS)

Zhou Ruimin; Xiang Qun; Song Jing

1997-01-01

It is found that the crystalline diffraction angles of the electron-beam irradiated filter paper cellulose shift regularly when the irradiation dose is increased. The experiments indicate that the molecules between crystalline area and amorphous area in the filter paper cellulose will be degraded by the irradiation and the cellulose molecules in the surface of crystal will come off, thus the microcrystalline dimension will be reduced and the diffraction angle will become smaller. The fact that intensity of the 002 peak for filter paper samples decreases gradually with the increasing storage time can be attributed to the post-irradiation effect

An Autonomous Data Reduction Pipeline for Wide Angle EO Systems

Science.gov (United States)

Privett, G.; George, S.; Feline, W.; Ash, A.; Routledge, G.

The UK’s National Space and Security Policy states that the identification of potential on-orbit collisions and re-entry warning over the UK is of high importance, and is driving requirements for indigenous Space Situational Awareness (SSA) systems. To meet these requirements options are being examined, including the creation of a distributed network of simple, low cost commercial–off-the-shelf electro-optical sensors to support survey work and catalogue maintenance. This paper outlines work at Dstl examining whether data obtained using readily-deployable equipment could significantly enhance UK SSA capability and support cross-cueing between multiple deployed systems. To effectively exploit data from this distributed sensor architecture, a data handling system is required to autonomously detect satellite trails in a manner that pragmatically handles highly variable target intensities, periodicity and rates of apparent motion. The processing and collection strategies must be tailored to specific mission sets to ensure effective detections of platforms as diverse as stable geostationary satellites and low altitude CubeSats. Data captured during the Automated Transfer Vehicle-5 (ATV-5) de-orbit trial and images captured of a rocket body break up and a deployed deorbit sail have been employed to inform the development of a prototype processing pipeline for autonomous on-site processing. The approach taken employs tools such as Astrometry.Net and DAOPHOT from the astronomical community, together with image processing and orbit determination software developed inhouse by Dstl. Interim results from the automated analysis of data collected from wide angle sensors are described, together with the current perceived limitations of the proposed system and our plans for future development.

NIST/Sandia/ICDD Electron Diffraction Database: A Database for Phase Identification by Electron Diffraction.

Science.gov (United States)

Carr, M J; Chambers, W F; Melgaard, D; Himes, V L; Stalick, J K; Mighell, A D

1989-01-01

A new database containing crystallographic and chemical information designed especially for application to electron diffraction search/match and related problems has been developed. The new database was derived from two well-established x-ray diffraction databases, the JCPDS Powder Diffraction File and NBS CRYSTAL DATA, and incorporates 2 years of experience with an earlier version. It contains 71,142 entries, with space group and unit cell data for 59,612 of those. Unit cell and space group information were used, where available, to calculate patterns consisting of all allowed reflections with d -spacings greater than 0.8 A for ~ 59,000 of the entries. Calculated patterns are used in the database in preference to experimental x-ray data when both are available, since experimental x-ray data sometimes omits high d -spacing data which falls at low diffraction angles. Intensity data are not given when calculated spacings are used. A search scheme using chemistry and r -spacing (reciprocal d -spacing) has been developed. Other potentially searchable data in this new database include space group, Pearson symbol, unit cell edge lengths, reduced cell edge length, and reduced cell volume. Compound and/or mineral names, formulas, and journal references are included in the output, as well as pointers to corresponding entries in NBS CRYSTAL DATA and the Powder Diffraction File where more complete information may be obtained. Atom positions are not given. Rudimentary search software has been written to implement a chemistry and r -spacing bit map search. With typical data, a full search through ~ 71,000 compounds takes 10~20 seconds on a PDP 11/23-RL02 system.

Atomic structure of large angle grain boundaries determined by quantitative X-ray diffraction techniques

International Nuclear Information System (INIS)

Fitzsimmons, M.R.; Sass, S.L.

1988-01-01

Quantitative X-ray diffraction techniques have been used to determine the atomic structure of the Σ = 5 and 13 [001] twist boundaries in Au with a resolution of 0.09 Angstrom or better. The reciprocal lattices of these boundaries were mapped out using synchrotron radiation. The atomic structures were obtained by testing model structures against the intensity observations with a chi square analysis. The boundary structure were modeled using polyhedra, including octahedra, special configurations of tetrahedra and Archimedian anti-prisms, interwoven together by the boundary symmetry. The results of this work point to the possibility of obtaining general rules for grain boundary structure based on X-ray diffraction observations that give the atomic positions with high resolution

The double Brewster angle effect

Science.gov (United States)

Thirion-Lefevre, Laetitia; Guinvarc'h, Régis

2018-01-01

The Double Brewster angle effect (DBE) is an extension of the Brewster angle to double reflection on two orthogonal dielectric surfaces. It results from the combination of two pseudo-Brewster angles occurring in complementary incidence angles domains. It can be observed for a large range of incidence angles provided that double bounces mechanism is present. As a consequence of this effect, we show that the reflection coefficient at VV polarization can be at least 10 dB lower than the reflection coefficient at HH polarization over a wide range of incidence angle - typically from 20 to 70∘. It is experimentally demonstrated using a Synthetic Aperture Radar (SAR) image that this effect can be seen on buildings and forests. For large buildings, the difference can reach more than 20 dB. xml:lang="fr"

Natural quasy-periodic binary structure with focusing property in near field diffraction pattern.

Science.gov (United States)

Mihailescu, Mona

2010-06-07

A naturally-inspired phase-only diffractive optical element with a circular symmetry given by a quasi-periodic structure of the phyllotaxis type is presented in this paper. It is generated starting with the characteristic parametric equations which are optimal for the golden angle interval. For some ideal geometrical parameters, the diffracted intensity distribution in near-field has a central closed ring with almost zero intensity inside. Its radius and intensity values depend on the geometry or non-binary phase distribution superposed onto the phyllotaxis geometry. Along propagation axis, the transverse diffraction patterns from the binary-phase diffractive structure exhibit a self-focusing behavior and a rotational motion.

On Babinet's principle and diffraction associated with an arbitrary particle.

Science.gov (United States)

Sun, Bingqiang; Yang, Ping; Kattawar, George W; Mishchenko, Michael I

2017-12-01

Babinet's principle is widely used to compute the diffraction by a particle. However, the diffraction by a 3-D object is not totally the same as that simulated with Babinet's principle. This Letter uses a surface integral equation to exactly formulate the diffraction by an arbitrary particle and illustrate the condition for the applicability of Babinet's principle. The present results may serve to close the debate on the diffraction formalism.

Fast parallel diffractive multi-beam femtosecond laser surface micro-structuring

Energy Technology Data Exchange (ETDEWEB)

Zheng Kuang, E-mail: z.kuang@liv.ac.uk [Laser Group, Department of Engineering, University of Liverpool, Brodie Building, Liverpool L69 3GQ (United Kingdom); Dun Liu; Perrie, Walter; Edwardson, Stuart; Sharp, Martin; Fearon, Eamonn; Dearden, Geoff; Watkins, Ken [Laser Group, Department of Engineering, University of Liverpool, Brodie Building, Liverpool L69 3GQ (United Kingdom)

2009-04-15

Fast parallel femtosecond laser surface micro-structuring is demonstrated using a spatial light modulator (SLM). The Gratings and Lenses algorithm, which is simple and computationally fast, is used to calculate computer generated holograms (CGHs) producing diffractive multiple beams for the parallel processing. The results show that the finite laser bandwidth can significantly alter the intensity distribution of diffracted beams at higher angles resulting in elongated hole shapes. In addition, by synchronisation of applied CGHs and the scanning system, true 3D micro-structures are created on Ti6Al4V.

Design and fabrication of directional diffractive device on glass substrate for multiview holographic 3D display

Science.gov (United States)

Su, Yanfeng; Cai, Zhijian; Liu, Quan; Zou, Wenlong; Guo, Peiliang; Wu, Jianhong

2018-01-01

Multiview holographic 3D display based on the nano-grating patterned directional diffractive device can provide 3D images with high resolution and wide viewing angle, which has attracted considerable attention. However, the current directional diffractive device fabricated on the photoresist is vulnerable to damage, which will lead to the short service life of the device. In this paper, we propose a directional diffractive device on glass substrate to increase its service life. In the design process, the period and the orientation of the nano-grating at each pixel are carefully calculated accordingly by the predefined position of the viewing zone, and the groove parameters are designed by analyzing the diffraction efficiency of the nano-grating pixel on glass substrate. In the experiment, a 4-view photoresist directional diffractive device with a full coverage of pixelated nano-grating arrays is efficiently fabricated by using an ultraviolet continuously variable spatial frequency lithography system, and then the nano-grating patterns on the photoresist are transferred to the glass substrate by combining the ion beam etching and the reactive ion beam etching for controlling the groove parameters precisely. The properties of the etched glass device are measured under the illumination of a collimated laser beam with a wavelength of 532nm. The experimental results demonstrate that the light utilization efficiency is improved and optimized in comparison with the photoresist device. Furthermore, the fabricated device on glass substrate is easier to be replicated and of better durability and practicability, which shows great potential in the commercial applications of 3D display terminal.

Fusion bonding of Si wafers investigated by x ray diffraction

DEFF Research Database (Denmark)

Weichel, Steen; Grey, Francois; Rasmussen, Kurt

2000-01-01

The interface structure of bonded Si(001) wafers with twist angle 6.5 degrees is studied as a function of annealing temperature. An ordered structure is observed in x-ray diffraction by monitoring a satellite reflection due to the periodic modulation near the interface, which results from...

Examination of the ''Ultra-wide-angle compton camera'' in Fukushima

International Nuclear Information System (INIS)

Takeda, Shin'ichiro; Watanabe, Shin; Takahashi, Tadayuki

2012-01-01

Japan Aerospace Exploration Agency (JAXA) has made the camera in the title, which can visualize radioactive substances emitting gamma ray in a wide-angle view of almost 180 degrees (hemisphere) and this paper explains its technological details and actual examination in Iitatemura Village, Fukushima Prefecture. The camera has a detector module consisting from 5-laminated structure of 2 layers of Si-double-sided strip detector (Si-DSD) and 3 layers of CdTe-DSD at 4 mm pitch, and their device size and electrode pitch are made the same, which enables the detector tray and analog application specific integrated circuit (ASIC) usable to communize the read-out circuits and for economical reduction. Two modules are placed side by side for increasing sensitivity and car-loaded to operate at -5 degree for the examination. The CdTe-DSD has actually Pt cathode and Al anode (Pt/CdTe/Al) for reduction of electric leaking and increase of energy resolution for 137 Cs gamma ray (662 keV). Data from the detector are digital pulse height values, which are then converted to the hit information of the detected position and energy. The hit event due to photoelectric absorption peak in CdTe originated from Compton scattering in Si is selected to be back-projected on the celestial hemisphere, leading to the torus depending on the direction of the gamma ray, of which accumulation results in specifying the position of the source. At the Village of 2-3 mcSv/h of ambient dose environment, locally accumulated radioactive substances (30 mcSv/h) are successfully visualized. With use of soft gamma ray detector in ASTRO-H satellite under development in JAXA, the improved camera can be more sensitive and may be useful in such a case as de-contamination to monitor its results in real time. (T.T.)

Some simple ideas on x-ray reflection and grazing-incidence diffraction from thin surfactant films

DEFF Research Database (Denmark)

Kjær, K.

1994-01-01

For Langmuir films of long linear amphiphilic molecules at the air-water interface, grazing-incidence diffraction data resolved in terms of both the horizontal and vertical components of the scattering angle can be evaluated to a fair level of detail by means of a slide rule. Specular reflection ...... data require more sophisticated means although some rules of thumb can be formulated.......For Langmuir films of long linear amphiphilic molecules at the air-water interface, grazing-incidence diffraction data resolved in terms of both the horizontal and vertical components of the scattering angle can be evaluated to a fair level of detail by means of a slide rule. Specular reflection...

Automated high pressure cell for pressure jump x-ray diffraction.

Science.gov (United States)

Brooks, Nicholas J; Gauthe, Beatrice L L E; Terrill, Nick J; Rogers, Sarah E; Templer, Richard H; Ces, Oscar; Seddon, John M

2010-06-01

A high pressure cell for small and wide-angle x-ray diffraction measurements of soft condensed matter samples has been developed, incorporating a fully automated pressure generating network. The system allows both static and pressure jump measurements in the range of 0.1-500 MPa. Pressure jumps can be performed as quickly as 5 ms, both with increasing and decreasing pressures. Pressure is generated by a motorized high pressure pump, and the system is controlled remotely via a graphical user interface to allow operation by a broad user base, many of whom may have little previous experience of high pressure technology. Samples are loaded through a dedicated port allowing the x-ray windows to remain in place throughout an experiment; this facilitates accurate subtraction of background scattering. The system has been designed specifically for use at beamline I22 at the Diamond Light Source, United Kingdom, and has been fully integrated with the I22 beamline control systems.

Automated high pressure cell for pressure jump x-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Brooks, Nicholas J.; Gauthe, Beatrice L. L. E.; Templer, Richard H.; Ces, Oscar; Seddon, John M. [Department of Chemistry, Imperial College London, South Kensington Campus, London SW7 2AZ (United Kingdom); Terrill, Nick J. [Diamond Light Source, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0DE (United Kingdom); Rogers, Sarah E. [ISIS, Rutherford Appleton Laboratory, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0QX (United Kingdom)

2010-06-15

A high pressure cell for small and wide-angle x-ray diffraction measurements of soft condensed matter samples has been developed, incorporating a fully automated pressure generating network. The system allows both static and pressure jump measurements in the range of 0.1-500 MPa. Pressure jumps can be performed as quickly as 5 ms, both with increasing and decreasing pressures. Pressure is generated by a motorized high pressure pump, and the system is controlled remotely via a graphical user interface to allow operation by a broad user base, many of whom may have little previous experience of high pressure technology. Samples are loaded through a dedicated port allowing the x-ray windows to remain in place throughout an experiment; this facilitates accurate subtraction of background scattering. The system has been designed specifically for use at beamline I22 at the Diamond Light Source, United Kingdom, and has been fully integrated with the I22 beamline control systems.

Automated high pressure cell for pressure jump x-ray diffraction

International Nuclear Information System (INIS)

Brooks, Nicholas J.; Gauthe, Beatrice L. L. E.; Templer, Richard H.; Ces, Oscar; Seddon, John M.; Terrill, Nick J.; Rogers, Sarah E.

2010-01-01

A high pressure cell for small and wide-angle x-ray diffraction measurements of soft condensed matter samples has been developed, incorporating a fully automated pressure generating network. The system allows both static and pressure jump measurements in the range of 0.1-500 MPa. Pressure jumps can be performed as quickly as 5 ms, both with increasing and decreasing pressures. Pressure is generated by a motorized high pressure pump, and the system is controlled remotely via a graphical user interface to allow operation by a broad user base, many of whom may have little previous experience of high pressure technology. Samples are loaded through a dedicated port allowing the x-ray windows to remain in place throughout an experiment; this facilitates accurate subtraction of background scattering. The system has been designed specifically for use at beamline I22 at the Diamond Light Source, United Kingdom, and has been fully integrated with the I22 beamline control systems.

The atomic scale structure of CXV carbon: wide-angle x-ray scattering and modeling studies.

Science.gov (United States)

Hawelek, L; Brodka, A; Dore, J C; Honkimaki, V; Burian, A

2013-11-13

The disordered structure of commercially available CXV activated carbon produced from finely powdered wood-based carbon has been studied using the wide-angle x-ray scattering technique, molecular dynamics and density functional theory simulations. The x-ray scattering data has been converted to the real space representation in the form of the pair correlation function via the Fourier transform. Geometry optimizations using classical molecular dynamics based on the reactive empirical bond order potential and density functional theory at the B3LYP/6-31g* level have been performed to generate nanoscale models of CXV carbon consistent with the experimental data. The final model of the structure comprises four chain-like and buckled graphitic layers containing a small percentage of four-fold coordinated atoms (sp(3) defects) in each layer. The presence of non-hexagonal rings in the atomic arrangement has been also considered.

Depth distribution of chemical phase concentration determined by grazing incidence X-ray diffraction

International Nuclear Information System (INIS)

Novak, P.; Ballo, P.; Dobrocka, E.; Vallo, M.; Lalinsky, T.

2013-01-01

Grazing incidence geometry is widely used in X-ray diffraction analysis of thin films. Penetration depth of radiation can be easily changed by an appropriate selection of the angle of incidence α that enables obtaining information from different depths of the sample. This depth can be decreased up to a nanometer scale by approaching the critical angle α_c for total external reflection. This method therefore provides an efficient tool for the analysis of depth distribution of various structural properties, such as the crystallite size, the amorphous fraction, stress or the concentration of chemical phase. However, absorption of the radiation can be characterized by an average attenuation coefficient μ a special care has to be paid to the last property. Variation of chemical phase concentration with depth usually results in depth dependence on the attenuation coefficient. In this contribution a method for determination of depth distribution of a chemical phase is outlined. The method correctly takes into account the depth variation of the attenuation coefficient. The method is tested on thin oxidized Ir layers. The aim of this paper is a comparison two simple model cases with the experimental results. (authors)

Transport cross section for small-angle scattering

International Nuclear Information System (INIS)

D'yakonov, M.I.; Khaetskii, A.V.

1991-01-01

Classical mechanics is valid for describing potential scattering under the conditions (1) λ much-lt α and (2) U much-gt ℎυ/α, where λ is the de Broglie wavelength, α is the characteristic size of the scatterer, U is the characteristic value of the potential energy, and υ is the velocity of the scattered particle. The second of these conditions means that the typical value of the classical scattering angle is far larger than the diffraction angle λ/α. In this paper the authors show that this second condition need not hold in a derivation of the transport cross section. In other words, provided that the condition λ much-lt α holds, it is always possible to calculate the transport cross section from the expressions of classical mechanics, even in the region U approx-lt ℎυ/α, where the scattering is diffractive,and the differential cross section is greatly different from the classical cross section. The transport cross section is found from the classical expression even in the anticlassical case U much-lt ℎυ/α, where the Born approximation can be used

Diagnostic performance of digital breast tomosynthesis with a wide scan angle compared to full-field digital mammography for the detection and characterization of microcalcifications

International Nuclear Information System (INIS)

Clauser, Paola; Nagl, Georg; Helbich, Thomas H.; Pinker-Domenig, Katja; Weber, Michael; Kapetas, Panagiotis; Bernathova, Maria; Baltzer, Pascal A.T.

2016-01-01

Highlights: • Wide scan-angle DBT alone shows a high detection rate for microcalcifications. • DBT and FFDM can characterize microcalcifications at a comparable level. • Characterization is influenced by reader and by lesion type (benign vs malignant). • DBT might be used as a stand-alone technique for the assessment of microcalcifications. - Abstract: Objectives: To assess the diagnostic performance of digital breast tomosynthesis (DBT), with a wide scan-angle, compared to full-field digital mammography (FFDM), for the detection and characterization of microcalcifications. Methods: IRB approval was obtained for this retrospective study. We selected 150 FFDM and DBT (50 benign and 50 malignant histologically verified microcalcifications, 50 cases classified as BI-RADS 1). Four radiologists evaluated, in separate sessions and blinded to patients’ history and histology, the presence of microcalcifications. Cases with microcalcifications were assessed for visibility, characteristics, and grade of suspicion using BI-RADS categories. Detection rate and diagnostic performance were calculated. Visibility, lesions’ characteristics and reading time were analysed. Results: Detection rate and visibility were good for both FFDM and DBT, without intra-reader differences (P = 0.510). Inter-reader differences were detected (P < 0.018). Only two lesions were not detected by any reader on either FFDM or DBT. Diagnostic performance with DBT was as good as that of FFDM, but a significant inter-reader difference was found (P = 0.041). High inter-reader variability in the use of the descriptors was found. Reading time for DBT was almost twice that for FFDM (44 and 25 s, respectively). Conclusion: Wide scan-angle DBT enabled the detection and characterization of microcalcifications with no significant differences from FFDM. Inter-reader variability was seen.

Diagnostic performance of digital breast tomosynthesis with a wide scan angle compared to full-field digital mammography for the detection and characterization of microcalcifications

Energy Technology Data Exchange (ETDEWEB)

Clauser, Paola, E-mail: paola.clauser@meduniwien.ac.at [Department of Biomedical Imaging and Image-Guided Therapy, Division of Molecular and Gender Imaging, Medical University of Vienna, Waehringer Guertel 18-20, 1090 Vienna (Austria); Nagl, Georg [Department for Radiology and Interventional Radiology, Landesklinikum Horn, Spitalgasse 10, 3580 Horn (Austria); Helbich, Thomas H., E-mail: thomas.helbich@meduniwien.ac.at [Department of Biomedical Imaging and Image-Guided Therapy, Division of Molecular and Gender Imaging, Medical University of Vienna, Waehringer Guertel 18-20, 1090 Vienna (Austria); Pinker-Domenig, Katja [Department of Biomedical Imaging and Image-Guided Therapy, Division of Molecular and Gender Imaging, Medical University of Vienna, Waehringer Guertel 18-20, 1090 Vienna (Austria); Weber, Michael [Department of Biomedical Imaging and Image-Guided Therapy, Division of General and Pediatric Radiology, Medical University of Vienna, Waehringer Guertel 18-20, 1090 Vienna (Austria); Kapetas, Panagiotis; Bernathova, Maria; Baltzer, Pascal A.T. [Department of Biomedical Imaging and Image-Guided Therapy, Division of Molecular and Gender Imaging, Medical University of Vienna, Waehringer Guertel 18-20, 1090 Vienna (Austria)

2016-12-15

Highlights: • Wide scan-angle DBT alone shows a high detection rate for microcalcifications. • DBT and FFDM can characterize microcalcifications at a comparable level. • Characterization is influenced by reader and by lesion type (benign vs malignant). • DBT might be used as a stand-alone technique for the assessment of microcalcifications. - Abstract: Objectives: To assess the diagnostic performance of digital breast tomosynthesis (DBT), with a wide scan-angle, compared to full-field digital mammography (FFDM), for the detection and characterization of microcalcifications. Methods: IRB approval was obtained for this retrospective study. We selected 150 FFDM and DBT (50 benign and 50 malignant histologically verified microcalcifications, 50 cases classified as BI-RADS 1). Four radiologists evaluated, in separate sessions and blinded to patients’ history and histology, the presence of microcalcifications. Cases with microcalcifications were assessed for visibility, characteristics, and grade of suspicion using BI-RADS categories. Detection rate and diagnostic performance were calculated. Visibility, lesions’ characteristics and reading time were analysed. Results: Detection rate and visibility were good for both FFDM and DBT, without intra-reader differences (P = 0.510). Inter-reader differences were detected (P < 0.018). Only two lesions were not detected by any reader on either FFDM or DBT. Diagnostic performance with DBT was as good as that of FFDM, but a significant inter-reader difference was found (P = 0.041). High inter-reader variability in the use of the descriptors was found. Reading time for DBT was almost twice that for FFDM (44 and 25 s, respectively). Conclusion: Wide scan-angle DBT enabled the detection and characterization of microcalcifications with no significant differences from FFDM. Inter-reader variability was seen.

Constraining variable density of ice shelves using wide-angle radar measurements

Science.gov (United States)

Drews, Reinhard; Brown, Joel; Matsuoka, Kenichi; Witrant, Emmanuel; Philippe, Morgane; Hubbard, Bryn; Pattyn, Frank

2016-04-01

The thickness of ice shelves, a basic parameter for mass balance estimates, is typically inferred using hydrostatic equilibrium, for which knowledge of the depth-averaged density is essential. The densification from snow to ice depends on a number of local factors (e.g., temperature and surface mass balance) causing spatial and temporal variations in density-depth profiles. However, direct measurements of firn density are sparse, requiring substantial logistical effort. Here, we infer density from radio-wave propagation speed using ground-based wide-angle radar data sets (10 MHz) collected at five sites on Roi Baudouin Ice Shelf (RBIS), Dronning Maud Land, Antarctica. We reconstruct depth to internal reflectors, local ice thickness, and firn-air content using a novel algorithm that includes traveltime inversion and ray tracing with a prescribed shape of the depth-density relationship. For the particular case of an ice-shelf channel, where ice thickness and surface slope change substantially over a few kilometers, the radar data suggest that firn inside the channel is about 5 % denser than outside the channel. Although this density difference is at the detection limit of the radar, it is consistent with a similar density anomaly reconstructed from optical televiewing, which reveals that the firn inside the channel is 4.7 % denser than that outside the channel. Hydrostatic ice thickness calculations used for determining basal melt rates should account for the denser firn in ice-shelf channels. The radar method presented here is robust and can easily be adapted to different radar frequencies and data-acquisition geometries.

SoftWAXS: a computational tool for modeling wide-angle X-ray solution scattering from biomolecules.

Science.gov (United States)

Bardhan, Jaydeep; Park, Sanghyun; Makowski, Lee

2009-10-01

This paper describes a computational approach to estimating wide-angle X-ray solution scattering (WAXS) from proteins, which has been implemented in a computer program called SoftWAXS. The accuracy and efficiency of SoftWAXS are analyzed for analytically solvable model problems as well as for proteins. Key features of the approach include a numerical procedure for performing the required spherical averaging and explicit representation of the solute-solvent boundary and the surface of the hydration layer. These features allow the Fourier transform of the excluded volume and hydration layer to be computed directly and with high accuracy. This approach will allow future investigation of different treatments of the electron density in the hydration shell. Numerical results illustrate the differences between this approach to modeling the excluded volume and a widely used model that treats the excluded-volume function as a sum of Gaussians representing the individual atomic excluded volumes. Comparison of the results obtained here with those from explicit-solvent molecular dynamics clarifies shortcomings inherent to the representation of solvent as a time-averaged electron-density profile. In addition, an assessment is made of how the calculated scattering patterns depend on input parameters such as the solute-atom radii, the width of the hydration shell and the hydration-layer contrast. These results suggest that obtaining predictive calculations of high-resolution WAXS patterns may require sophisticated treatments of solvent.

Accurate electron channeling contrast analysis of a low angle sub-grain boundary

International Nuclear Information System (INIS)

Mansour, H.; Crimp, M.A.; Gey, N.; Maloufi, N.

2015-01-01

High resolution selected area channeling pattern (HR-SACP) assisted accurate electron channeling contrast imaging (A-ECCI) was used to unambiguously characterize the structure of a low angle grain boundary in an interstitial-free-steel. The boundary dislocations were characterized using TEM-style contrast analysis. The boundary was determined to be tilt in nature with a misorientation angle of 0.13° consistent with the HR-SACP measurements. The results were verified using high accuracy electron backscatter diffraction (EBSD), confirming the approach as a discriminating tool for assessing low angle boundaries

Technical Note: An investigation of polarity effects for wide-angle free-air chambers

Energy Technology Data Exchange (ETDEWEB)

Shen, H., E-mail: Hong.Shen@nrc-cnrc.gc.ca; Ross, C. K. [Ionizing Radiation Standards, National Research Council, Ottawa, Ontario K1A 0R6 (Canada); Culberson, W. S. [Department of Medical Physics, University of Wisconsin-Madison, Madison, Wisconsin 53705 (United States)

2016-07-15

Purpose: Wide-angle free-air chambers (WAFACs) are used as primary standard measurement devices for establishing the air-kerma strength of low-energy, low-dose rate brachytherapy seeds. The National Research Council of Canada (NRC) is commissioning a primary standard wide-angle free-air chamber (NRC WAFAC) to serve the calibration needs of Canadian clients. The University of Wisconsin has developed a similar variable-aperture free-air chamber (UW VAFAC) to be used as a research tool. As part of the NRC commissioning, measurements were carried out for both polarities of the applied bias voltage and the resulting effects were observed to be very large. Similar effects were identified with the UW VAFAC. The authors describe the measurements carried out to determine the underlying causes of the polarity effect and the approach used to eliminate it. Methods: The NRC WAFAC is based on the WAFAC design developed at the National Institute of Standards and Technology in the USA. Charge measurements for {sup 125}I and {sup 241}Am sources were carried out for both negative and positive polarities on the NRC WAFAC and UW VAFAC. Two aperture sizes were also investigated with the UW VAFAC. In addition, measurements on the NRC WAFAC were carried out with a small bias between the collecting electrode and the shield foil at the downstream end of the chamber. To mitigate all of the polarity effects, the downstream surface of the collecting electrode was covered with a thin layer of graphite on both the NRC and UW chambers. Results: Both chamber designs showed a difference of more than 30 % between the charge collected with positive and negative bias voltages for the smallest electrode separation. It was shown for the NRC WAFAC that charge could be collected in the small gap downstream of the collecting volume by applying a voltage between the shield foil and the collecting electrode, even though an insulating foil (Mylar or polyimide film) separated the conducting surface from the

Technical Note: An investigation of polarity effects for wide-angle free-air chambers

International Nuclear Information System (INIS)

Shen, H.; Ross, C. K.; Culberson, W. S.

2016-01-01

Purpose: Wide-angle free-air chambers (WAFACs) are used as primary standard measurement devices for establishing the air-kerma strength of low-energy, low-dose rate brachytherapy seeds. The National Research Council of Canada (NRC) is commissioning a primary standard wide-angle free-air chamber (NRC WAFAC) to serve the calibration needs of Canadian clients. The University of Wisconsin has developed a similar variable-aperture free-air chamber (UW VAFAC) to be used as a research tool. As part of the NRC commissioning, measurements were carried out for both polarities of the applied bias voltage and the resulting effects were observed to be very large. Similar effects were identified with the UW VAFAC. The authors describe the measurements carried out to determine the underlying causes of the polarity effect and the approach used to eliminate it. Methods: The NRC WAFAC is based on the WAFAC design developed at the National Institute of Standards and Technology in the USA. Charge measurements for 125 I and 241 Am sources were carried out for both negative and positive polarities on the NRC WAFAC and UW VAFAC. Two aperture sizes were also investigated with the UW VAFAC. In addition, measurements on the NRC WAFAC were carried out with a small bias between the collecting electrode and the shield foil at the downstream end of the chamber. To mitigate all of the polarity effects, the downstream surface of the collecting electrode was covered with a thin layer of graphite on both the NRC and UW chambers. Results: Both chamber designs showed a difference of more than 30 % between the charge collected with positive and negative bias voltages for the smallest electrode separation. It was shown for the NRC WAFAC that charge could be collected in the small gap downstream of the collecting volume by applying a voltage between the shield foil and the collecting electrode, even though an insulating foil (Mylar or polyimide film) separated the conducting surface from the small gap

A study of the formation of amorphous calcium phosphate and hydroxyapatite on melt quenched Bioglass using surface sensitive shallow angle X-ray diffraction.

Science.gov (United States)

Martin, R A; Twyman, H; Qiu, D; Knowles, J C; Newport, R J

2009-04-01

Melt quenched silicate glasses containing calcium, phosphorous and alkali metals have the ability to promote bone regeneration and to fuse to living bone. These glasses, including 45S5 Bioglass((R)) [(CaO)(26.9)(Na(2)O)(24.4)(SiO(2))(46.1)(P(2)O(5))(2.6)], are routinely used as clinical implants. Consequently there have been numerous studies on the structure of these glasses using conventional diffraction techniques. These studies have provided important information on the atomic structure of Bioglass((R)) but are of course intrinsically limited in the sense that they probe the bulk material and cannot be as sensitive to thin layers of near-surface dissolution/growth. The present study therefore uses surface sensitive shallow angle X-ray diffraction to study the formation of amorphous calcium phosphate and hydroxyapatite on Bioglass((R)) samples, pre-reacted in simulated body fluid (SBF). Unreacted Bioglass((R)) is dominated by a broad amorphous feature around 2.2 A(-1) which is characteristic of sodium calcium silicate glass. After reacting Bioglass((R)) in SBF a second broad amorphous feature evolves ~1.6 A(-1) which is attributed to amorphous calcium phosphate. This feature is evident for samples after only 4 h reacting in SBF and by 8 h the amorphous feature becomes comparable in magnitude to the background signal of the bulk Bioglass((R)). Bragg peaks characteristic of hydroxyapatite form after 1-3 days of reacting in SBF.

Measurable position-sensitive wide-angle interference effects of single photons radiated by a nitrogen-vacancy center in diamond

International Nuclear Information System (INIS)

Sandor Varro

2014-01-01

Single-photon wide-angle interference phenomena have been studied theoretically for glass-diamond-oil (air) layered structures. As a single optical radiator, one NV-center has been assumed close to the upper surface of a diamond plate, and it was represented by a Hertzian dipole of arbitrary orientation. It has been shown that the far-field interference pattern (of 3/5 or 100% visibility) is sensitive to the vertical position of the NV-center, to that extent that ∼2 nm difference in distance from the upper surface of the diamond results in ∼0.01 degree shift of the pattern, which should be a measurable effect. (author)

Innovative diffraction gratings for high-resolution resonant inelastic soft x-ray scattering spectroscopy

International Nuclear Information System (INIS)

Voronov, D.L.; Warwick, T.; Gullikson, E. M.; Salmassi, F.; Padmore, H. A.

2016-01-01

High-resolution Resonant Inelastic X-ray Scattering (RIXS) requires diffraction gratings with very exacting characteristics. The gratings should provide both very high dispersion and high efficiency which are conflicting requirements and extremely challenging to satisfy in the soft x-ray region for a traditional grazing incidence geometry. To achieve high dispersion one should increase the groove density of a grating; this however results in a diffraction angle beyond the critical angle range and results in drastic efficiency loss. The problem can be solved by use of multilayer coated blazed gratings (MBG). In this work we have investigated the diffraction characteristics of MBGs via numerical simulations and have developed a procedure for optimization of grating design for a multiplexed high resolution imaging spectrometer for RIXS spectroscopy to be built in sector 6 at the Advanced Light Source (ALS). We found that highest diffraction efficiency can be achieved for gratings optimized for 4"t"h or 5"t"h order operation. Fabrication of such gratings is an extremely challenging technological problem. We present a first experimental prototype of these gratings and report its performance. High order and high line density gratings have the potential to be a revolutionary new optical element that should have great impact in the area of soft x-ray RIXS.

Correction of X-ray diffraction profiles in linear-type PSPC by position factor

International Nuclear Information System (INIS)

Takahashi, Toshio

1992-01-01

PSPC (Position Sensitive Proportional Counter) makes it possible to obtain one-dimentional diffraction profiles without mechanical scanning. In a linear-type PSPC, the obtained profiles need correcting, because the position factor influences the intensity of the diffracted X-ray beam and the counting rate at each position on PSPC. The distances from the specimen are not the same at the center and at the edge of the detector, and the intensity decreases at the edge because of radiation and absorption. The counting rate varies with the incident angle of the diffracted beam at each position on PSPC. The position factor f i at channel i of the multichannel-analyser is given by f i = cos 4 α i ·exp{-μR(1/cosα i -1)} where R is the distance between the specimen and the center of PSPC, μ is the linear absorption coefficient and α i is the incident angle of the diffracted beam at channel i. The background profiles of silica gel powder were measured with CrKα and CuKα. The parameters of the model function were fitted to the profiles by the non-linear least squares method. The agreement between these parameters and the calculated values shows that the position factor can correct the measured profiles properly. (author)

Sunda-Banda Arc Transition: Marine Wide-Angle Seismic Modeling

Science.gov (United States)

Shulgin, A.; Planert, L.; Kopp, H.; Mueller, C.; Lueschen, E.; Engels, M.; Flueh, E.; Djajadihardja, Y.; Sindbad Working Group, T

2008-12-01

The Sunda-Banda Arc transition is the region of active convergence and collision of the Indo-Australian and Eurasian Plates. The style of subduction changes from an oceanic-island arc subduction to a continental- island arc collision. The character of the incoming plate varies from the rough topography of the Roo Rise, to the smooth seafloor of the Abyssal Plain off Bali, Sumbawa. Forearc structures include well-developed forearc basins and an accretionary prism/outer forearc high of variable size and shape. To quantify the variability of structure of the lower plate and the effects on the upper plate a refraction seismic survey was carried during cruise SO190-2. A total of 245 ocean bottom seismometers were deployed along 1020 nm of wide-angle seismic profiles in four major north-south oriented corridors. To assess the velocity structure we used a tomographic method which jointly inverts for refracted and reflected phases. The sedimentary layers of the models, obtained by the analysis of high-resolution MCS data (see Lueschen et al), were incorporated into the starting model. The obtained models exhibit strong changes of the incoming oceanic crust for the different portions of the margin: The westernmost profile off eastern Java shows a crustal thickness of more than 15 km, most likely related to the presence of an oceanic plateau. Profiles off Lombok reveal an oceanic crust of 8-9 km average thickness in the Argo Abyssal Plain. Crustal and upper mantle velocities are slightly decreased within an area of about 50-60 km seaward of the trench, indicating fracturing and related serpentinization due to bending of the oceanic crust and associated normal faulting. The outer forearc high is characterized by velocities of 2.5-5.5 km/s. For the Lombok Basin, the profiles show a sedimentary infill of up to 3.5 km thick and typical sediment velocities of 1.75-3.0 km/s. A reflector at 16 km depth and velocity values of 7.4-7.8 km/s beneath it suggest the presence of a shallow

Characterization of diffraction gratings by use of a tabletop soft-x-ray laser

International Nuclear Information System (INIS)

Seminario, Max; Rocca, Jorge J.; Depine, Ricardo A.; Bach, Benny; Bach, Bernie

2001-01-01

We have demonstrated the use of a high-repetition-rate 46.9-mm tabletop laser to characterize diffraction gratings designed for grazing-incidence operation in the soft-x-ray spectral region. The efficiencies for various diffraction orders were measured as a function of angle of incidence and compared with the results of model simulations. This measurement technique provides benchmarks with which to improve electromagnetic codes used in the design of soft-x-ray diffraction gratings. The results illustrate the potential of compact tabletop soft-x-ray lasers for use as a new tool for characterization of short-wavelength optics at the manufacturer's site

Relationship between electrical properties and crystallization of indium oxide thin films using ex-situ grazing-incidence wide-angle x-ray scattering

Science.gov (United States)

González, G. B.; Okasinski, J. S.; Buchholz, D. B.; Boesso, J.; Almer, J. D.; Zeng, L.; Bedzyk, M. J.; Chang, R. P. H.

2017-05-01

Grazing-incidence, wide-angle x-ray scattering measurements were conducted on indium oxide thin films grown on silica substrates via pulsed laser deposition. Growth temperatures (TG) in this study ranged from -50 °C to 600 °C, in order to investigate the thermal effects on the film structure and its spatial homogeneity, as well as their relationship to electrical properties. Films grown below room temperature were amorphous, while films prepared at TG = 25 °C and above crystallized in the cubic bixbyite structure, and their crystalline fraction increased with deposition temperature. The electrical conductivity (σ) and electrical mobility (μ) were strongly enhanced at low deposition temperatures. For TG = 25 °C and 50 °C, a strong ⟨100⟩ preferred orientation (texture) occurred, but it decreased as the deposition temperature, and consequential crystallinity, increased. Higher variations in texture coefficients and in lattice parameters were measured at the film surface compared to the interior of the film, indicating strong microstructural gradients. At low crystallinity, the in-plane lattice spacing expanded, while the out-of-plane spacing contracted, and those values merged at TG = 400 °C, where high μ was measured. This directional difference in lattice spacing, or deviatoric strain, was linear as a function of both deposition temperature and the degree of crystallinity. The crystalline sample with TG = 100 °C had the lowest mobility, as well as film diffraction peaks which split into doublets. The deviatoric strains from these doublet peaks differ by a factor of four, supporting the presence of both a microstructure and strain gradient in this film. More isotropic films exhibit larger μ values, indicating that the microstructure directly correlates with electrical properties. These results provide valuable insights that can help to improve the desirable properties of indium oxide, as well as other transparent conducting oxides.

Orphan Basin crustal structure from a dense wide-angle seismic profile - Tomographic inversion

Science.gov (United States)

Watremez, Louise; Lau, K. W. Helen; Nedimović, Mladen R.; Louden, Keith E.; Karner, Garry D.

2014-05-01

Orphan Basin is located on the eastern margin of Canada, offshore of Newfoundland and East of Flemish Cap. It is an aborted continental rift formed by multiple episodes of rifting. The crustal structure across the basin has been determined by an earlier refraction study using 15 instruments on a 550 km long line. It shows that the continental crust was extended over an unusually wide region but did not break apart. The crustal structure of the basin thus documents stages in the formation of a magma-poor rifted margin up to crustal breakup. The OBWAVE (Orphan Basin Wide-Angle Velocity Experiment) survey was carried out to image crustal structures across the basin and better understand the processes of formation of this margin. The spacing of the 89 recording stations varies from 3 to 5 km along this 500-km-long line, which was acquired along a pre-existing reflection line. The highest resolution section corresponds to the part of the profile where the crust was expected to be the thinnest. We present the results from a joint tomography inversion of first and Moho reflected arrival times. The high data density allows us to define crustal structures with greater detail than for typical studies and to improve the understanding of the processes leading to the extreme stretching of continental crust. The final model was computed following a detailed parametric study to determine the optimal parameters controlling the ray-tracing and the inversion processes. The final model shows very good resolution. In particular, Monte Carlo standard deviations of crustal velocities and Moho depths are generally Orphan Basin is the result of rifting of a non-homogeneous Avalon terrane where the lower crust is primarily ductile.

Study of the local structure of binary surfaces by electron diffraction (XPS, LEED)

OpenAIRE

Gereová, Katarína

2006-01-01

Study of local structure of binary surface with usage of ultra-thin film of cerium deposited on a Pd (111) single-crystal surface is presented. X-ray photoelectron spectroscopy and diffraction (XPS, XPD), angle resolved UV photoemission spectroscopy (ARUPS) and low energy electron diffraction (LEED) was used for our investigations. LEED and X-ray excited photoemission intensities results represent a surface-geometrical structure. As well, mapping of ultra-violet photoelectron intensities as a...

Probing multi-scale mechanical damage in connective tissues using X-ray diffraction.

Science.gov (United States)

Bianchi, Fabio; Hofmann, Felix; Smith, Andrew J; Thompson, Mark S

2016-11-01

The accumulation of microstructural collagen damage following repetitive loading is linked to painful and debilitating tendon injuries. As a hierarchical, semi-crystalline material, collagen mechanics can be studied using X-ray diffraction. The aim of the study was to describe multi-structural changes in tendon collagen following controlled plastic damage (5% permanent strain). We used small angle X-ray scattering (SAXS) to interrogate the spacing of collagen molecules within a fibril, and wide angle X-ray scattering (WAXS) to measure molecular strains under macroscopic loading. Simultaneous recordings of SAXS and WAXS patterns, together with whole-tissue strain in physiologically hydrated rat-tail tendons were made during increments of in situ tensile loading. Results showed that while tissue level modulus was unchanged, fibril modulus decreased significantly, and molecular modulus significantly increased. Further, analysis of higher order SAXS peaks suggested structural changes in the gap and overlap regions, possibly localising the damage to molecular cross-links. Our results provide new insight into the fundamental damage processes at work in collagenous tissues and point to new directions for their mitigation and repair. This article reports the first in situ loading synchrotron studies on mechanical damage in collagenous tissues. We provide new insight into the nano- and micro-structural mechanisms of damage processes. Pre-damaged tendons showed differential alteration of moduli at macro, micro and nano-scales as measured using X-ray scattering techniques. Detailed analysis of higher order diffraction peaks suggested damage is localised to molecular cross-links. The results are consistent with previous X-ray scattering studies of tendons and also with recent thermal stability studies on damaged material. Detailed understanding of damage mechanisms is essential in the development of new therapies promoting tissue repair. Copyright © 2016 Acta Materialia Inc

The spectral combination characteristic of grating and the bi-grating diffraction imaging effect

Institute of Scientific and Technical Information of China (English)

2007-01-01

This paper reports on a new property of grating, namely spectral combination, and on bi-grating diffraction imaging that is based on spectral combination. The spectral combination characteristic of a grating is the capability of combining multiple light beams of different wavelengths incident from specific angles into a single beam. The bi-grating diffraction imaging is the formation of the image of an object with two gratings: the first grating disperses the multi-color light beams from the object and the second combines the dispersed light beams to form the image. We gave the conditions necessary for obtaining the spectral combination. We also presented the equations that relate the two gratings’ spatial frequencies, diffraction orders and positions necessary for obtaining the bi-grating diffraction imaging.

Novel tendencies in developing small-angle neutron scattering methods for studying the structure of biological macromolecules

International Nuclear Information System (INIS)

Serdyuk, I.

1995-01-01

In recent 20 years thermal neutron scattering has been acknowledged an important instrument for structural studies in molecular biology. The methods of neutron diffraction of high resolution, which are not discussed in this paper, have already permitted to obtain a detailed representation of the course of proteolytic reactions and have arisen a number of new problems connected with the localization of water molecules and the H-D exchange. The methods of low resolution widely used due to a relative simplicity of the experiment have been successfully applied for both solving structural problems per se and investigating the changes in the structure when macromolecules perform their biological functions. The most promising are novel experimental approaches: the triple isotopic substitution method and the method of spin dynamic polarization. These methods ensure solving structural problems at a higher resolution than the dimensions of the macromolecules studied. Installation of new experimental instruments makes neutron measurements more accessible, and development of direct methods for interpretation of experimental data using the apparatus of spherical harmonics opens new possibilities for small-angle neutron scattering making it a necessary element for interpretation of diffraction data of monocrystals of intricate biological macromolecules. The paper presents a brief account of the tendencies in theoretical development and practical use of small-angle scattering for studying biological macromolecules. Special attention is given to the studies carried out in the Laboratory of Neutron Physics on a unique pulse IBR-2 reactor. (author) 14 refs

Kinoform design with an optimal-rotation-angle method.

Science.gov (United States)

Bengtsson, J

1994-10-10

Kinoforms (i.e., computer-generated phase holograms) are designed with a new algorithm, the optimalrotation- angle method, in the paraxial domain. This is a direct Fourier method (i.e., no inverse transform is performed) in which the height of the kinoform relief in each discrete point is chosen so that the diffraction efficiency is increased. The optimal-rotation-angle algorithm has a straightforward geometrical interpretation. It yields excellent results close to, or better than, those obtained with other state-of-the-art methods. The optimal-rotation-angle algorithm can easily be modified to take different restraints into account; as an example, phase-swing-restricted kinoforms, which distribute the light into a number of equally bright spots (so called fan-outs), were designed. The phase-swing restriction lowers the efficiency, but the uniformity can still be made almost perfect.

Nonuniform fast Fourier transform method for numerical diffraction simulation on tilted planes.

Science.gov (United States)

Xiao, Yu; Tang, Xiahui; Qin, Yingxiong; Peng, Hao; Wang, Wei; Zhong, Lijing

2016-10-01

The method, based on the rotation of the angular spectrum in the frequency domain, is generally used for the diffraction simulation between the tilted planes. Due to the rotation of the angular spectrum, the interval between the sampling points in the Fourier domain is not even. For the conventional fast Fourier transform (FFT)-based methods, a spectrum interpolation is needed to get the approximate sampling value on the equidistant sampling points. However, due to the numerical error caused by the spectrum interpolation, the calculation accuracy degrades very quickly as the rotation angle increases. Here, the diffraction propagation between the tilted planes is transformed into a problem about the discrete Fourier transform on the uneven sampling points, which can be evaluated effectively and precisely through the nonuniform fast Fourier transform method (NUFFT). The most important advantage of this method is that the conventional spectrum interpolation is avoided and the high calculation accuracy can be guaranteed for different rotation angles, even when the rotation angle is close to π/2. Also, its calculation efficiency is comparable with that of the conventional FFT-based methods. Numerical examples as well as a discussion about the calculation accuracy and the sampling method are presented.

A CMOS active pixel sensor system for laboratory- based x-ray diffraction studies of biological tissue

International Nuclear Information System (INIS)

Bohndiek, Sarah E; Cook, Emily J; Arvanitis, Costas D; Olivo, Alessandro; Royle, Gary J; Clark, Andy T; Prydderch, Mark L; Turchetta, Renato; Speller, Robert D

2008-01-01

X-ray diffraction studies give material-specific information about biological tissue. Ideally, a large area, low noise, wide dynamic range digital x-ray detector is required for laboratory-based x-ray diffraction studies. The goal of this work is to introduce a novel imaging technology, the CMOS active pixel sensor (APS) that has the potential to fulfil all these requirements, and demonstrate its feasibility for coherent scatter imaging. A prototype CMOS APS has been included in an x-ray diffraction demonstration system. An industrial x-ray source with appropriate beam filtration is used to perform angle dispersive x-ray diffraction (ADXRD). Optimization of the experimental set-up is detailed including collimator options and detector operating parameters. Scatter signatures are measured for 11 different materials, covering three medical applications: breast cancer diagnosis, kidney stone identification and bone mineral density calculations. Scatter signatures are also recorded for three mixed samples of known composition. Results are verified using two independent models for predicting the APS scatter signature: (1) a linear systems model of the APS and (2) a linear superposition integral combining known monochromatic scatter signatures with the input polychromatic spectrum used in this case. Cross validation of experimental, modelled and literature results proves that APS are able to record biologically relevant scatter signatures. Coherent scatter signatures are sensitive to multiple materials present in a sample and provide a means to quantify composition. In the future, production of a bespoke APS imager for x-ray diffraction studies could enable simultaneous collection of the transmitted beam and scattered radiation in a laboratory-based coherent scatter system, making clinical transfer of the technique attainable

Wide-angle light-trapping electrode for photovoltaic cells.

Science.gov (United States)

Omelyanovich, Mikhail M; Simovski, Constantin R

2017-10-01

In this Letter, we experimentally show that a submicron layer of a transparent conducting oxide that may serve a top electrode of a photovoltaic cell based on amorphous silicon when properly patterned by notches becomes an efficient light-trapping structure. This is so for amorphous silicon thin-film solar cells with properly chosen thicknesses of the active layers (p-i-n structure with optimal thicknesses of intrinsic and doped layers). The nanopatterned layer of transparent conducting oxide reduces both the light reflectance from the photovoltaic cell and transmittance through the photovoltaic layers for normal incidence and for all incidence angles. We explain the physical mechanism of our light-trapping effect, prove that this mechanism is realized in our structure, and show that the nanopatterning is achievable in a rather easy and affordable way that makes our method of solar cell enhancement attractive for industrial adaptations.

Purification, crystallization, small-angle X-ray scattering and preliminary X-ray diffraction analysis of the SH2 domain of the Csk-homologous kinase.

Science.gov (United States)

Gunn, Natalie J; Gorman, Michael A; Dobson, Renwick C J; Parker, Michael W; Mulhern, Terrence D

2011-03-01

The C-terminal Src kinase (Csk) and Csk-homologous kinase (CHK) are endogenous inhibitors of the proto-oncogenic Src family of protein tyrosine kinases (SFKs). Phosphotyrosyl peptide binding to their Src-homology 2 (SH2) domains activates Csk and CHK, enhancing their ability to suppress SFK signalling; however, the detailed mechanistic basis of this activation event is unclear. The CHK SH2 was expressed in Escherichia coli and the purified protein was characterized as monomeric by synchrotron small-angle X-ray scattering in-line with size-exclusion chromatography. The CHK SH2 crystallized in 0.2 M sodium bromide, 0.1 M bis-Tris propane pH 6.5 and 20% polyethylene glycol 3350 and the best crystals diffracted to ∼1.6 Å resolution. The crystals belonged to space group P2, with unit-cell parameters a=25.8, b=34.6, c=63.2 Å, β=99.4°.

Detailed Analysis of Amplitude and Slope Diffraction Coefficients for knife-edge structure in S-UTD-CH Model

Directory of Open Access Journals (Sweden)

Eray Arik

2017-03-01

Full Text Available In urban, rural and indoor applications, diffraction mechanism is very important to predict the field strength and calculate the coverage accurately. The diffraction mechanism takes place on NLOS (non-line-of-sight cases like rooftop, vertex, corner, edge and sharp surfaces. S-UTD-CH model computes three type of electromagnetic wave incidence such as direct, reflected and diffracted waves, respectively. As obstacles in diffraction geometry are in the same or closer height, contribution of the diffraction mechanism is dominant. To predict the diffracted fields accurately, amplitude and slope diffraction coefficients and the derivative of these coefficients have to be taken correctly. In this paper, all the derivations about diffraction coefficients are made for knife edge type structures and extensive simulations are performed in order to analyze the amplitude and diffraction coefficients. In plane angle diffraction, contributions of amplitude and slope diffraction coefficient are maxima.

Studies in small angle scattering techniques

International Nuclear Information System (INIS)

Moellenbach, K.

1980-03-01

Small angle scattering of neutrons, X-rays and γ-rays are found among the spectroscopic methods developed in the recent years. Although these techniques differ from each other in many respects, e.g. radiation sources and technical equipment needed, their power to resolve physical phenomena and areas of application can be discussed in a general scheme. Selected examples are given illustrating the use of specific technical methods. Jahn-Teller driven structural phase transitions in Rare Earth zircons were studied with neutron scattering as well as small angle γ-ray diffraction. The study of neutron scattering from formations of magnetic domains in the Ising ferromagnet LiTbF 4 is a second example. Both these examples represent more than experimental test cases since the theoretical interpretations of the data obtained are discussed as well. As a last example the use of small angle scattering methods for the study of molecular biological samples is discussed. In particular the experimental procedures used in connection with scattering from aqueous solutions of proteins and protein complexes are given. (Auth.)

New software to model energy dispersive X-ray diffraction in polycrystalline materials

Energy Technology Data Exchange (ETDEWEB)

Ghammraoui, B., E-mail: bahaa.ghammraoui@cea.fr [CEA-Leti, MINATEC Campus, 17 rue des Martyrs, F 38054 Grenoble, Cedex 9 (France); Tabary, J. [CEA-Leti, MINATEC Campus, 17 rue des Martyrs, F 38054 Grenoble, Cedex 9 (France); Pouget, S. [CEA-INAC Sciences de la matieres, 17 rue des Martyrs, F 38054 Grenoble, Cedex 9 (France); Paulus, C.; Moulin, V.; Verger, L. [CEA-Leti, MINATEC Campus, 17 rue des Martyrs, F 38054 Grenoble, Cedex 9 (France); Duvauchelle, Ph. [CNDRI-Insa Lyon, Universite de Lyon, F-69621, Villeurbanne Cedex (France)

2012-02-01

Detection of illicit materials, such as explosives or drugs, within mixed samples is a major issue, both for general security and as part of forensic analyses. In this paper, we describe a new code simulating energy dispersive X-ray diffraction patterns in polycrystalline materials. This program, SinFullscat, models diffraction of any object in any diffractometer system taking all physical phenomena, including amorphous background, into account. Many system parameters can be tuned: geometry, collimators (slit and cylindrical), sample properties, X-ray source and detector energy resolution. Good agreement between simulations and experimental data was obtained. Simulations using explosive materials indicated that parameters such as the diffraction angle or the energy resolution of the detector have a significant impact on the diffraction signature of the material inspected. This software will be a convenient tool to test many diffractometer configurations, providing information on the one that best restores the spectral diffraction signature of the materials of interest.

The peak in neutron powder diffraction

International Nuclear Information System (INIS)

Laar, B. van; Yelon, W.B.

1984-01-01

For the application of Rietveld profile analysis to neutron powder diffraction data a precise knowledge of the peak profile, in both shape and position, is required. The method now in use employs a Gaussian shaped profile with a semi-empirical asymmetry correction for low-angle peaks. The integrated intensity is taken to be proportional to the classical Lorentz factor calculated for the X-ray case. In this paper an exact expression is given for the peak profile based upon the geometrical dimensions of the diffractometer. It is shown that the asymmetry of observed peaks is well reproduced by this expression. The angular displacement of the experimental profile with respect to the nominal Bragg angle value is larger than expected. Values for the correction to the classical Lorentz factor for the integrated intensity are given. The exact peak profile expression has been incorporated into a Rietveld profile analysis refinement program. (Auth.)

Reconstruction of Stress and Composition Profiles from X-ray Diffraction Experiments - How to Avoid Ghost Stresses?

DEFF Research Database (Denmark)

Christiansen, Thomas; Somers, Marcel A.J.

2004-01-01

On evaluating lattice strain-depth or stress-depth profiles with X-ray diffraction, the variation of the information depth while combining various tilt angles,psi, in combination with lattice spacing gradients leads to artefacts,so-called ghost or fictitious stresses. X-ray diffraction lattice...... method for the evaluation of stress/strain and composition profiles, while minimising the risk for ghost stresses....

Enhancement of diffraction efficiency of laminar-type diffraction gratings overcoated with diamond-like carbon (DLC) in soft x-ray region

Energy Technology Data Exchange (ETDEWEB)

Koike, Masato, E-mail: koike.masato@jaea.go.jp; Imazono, Takashi [Quantum Beam Science Center, Japan Atomic Energy Agency, 8-1-7 Umemidai, Kizugawa, Kyoto 619-0215 Japan (Japan); Nagano, Tetsuya; Sasai, Hiroyuki; Oue, Yuki; Yonezawa, Zeno; Kuramoto, Satoshi [Device Dept., Shimadzu Corp., 1Nishinokyo-Kuwabara-cho, Nakagyo-ku, Kyoto 604-8511 Japan (Japan); Terauchi, Masami [Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai 980-8577 Japan (Japan); Takahashi, Hideyuki [Science Equipment Sales Dept., JEOL Ltd., 2-1-1 Ohtemachi, Chiyoda-ku, Tokyo 100-0004 Japan (Japan); Notoya, Satoshi; Murano, Takanori [SA Business Unit, JEOL Ltd., 3-1-2 Musashino, Akishima, Tokyo 196-8558 Japan (Japan)

2016-07-27

Boron is the critical trace element in the production of high quality steel, creating a great demand for an efficient detection method of the B-K emission band at around 6.76 nm. To meet this demand we made a simulation study and obtained a practical method to improve the diffraction efficiency of metal-coated laminar-type gratings for a grazing incidence flat-field spectrograph by overcoating a sufficiently transparent high-density material. In the simulation the diffraction efficiency in a spectral region of 3.5-8.5 nm was computed for several combinations of overcoating materials and coating metals, with various thicknesses of the overcoating layer. The result obtained are: (1) the best overcoating material is high-density diamond-like carbon (DLC) having a density of 3.1 g/cm{sup 3}, (2) its optimum thickness is 24 nm at an angle of incidence of 87.0°, and (3) with this thickness the first-order diffraction efficiency is expected to reach 29.7 %, which well exceeds 15.6 % for Ni-coated (or 14.1 % for Au-coated) grating.

Crustal structure of the Murray Ridge, northwest Indian Ocean, from wide-angle seismic data

Science.gov (United States)

Minshull, T. A.; Edwards, R. A.; Flueh, E. R.

2015-07-01

The Murray Ridge/Dalrymple Trough system forms the boundary between the Indian and Arabian plates in the northern Arabian Sea. Geodetic constraints from the surrounding continents suggest that this plate boundary is undergoing oblique extension at a rate of a few millimetres per year. We present wide-angle seismic data that constrains the composition of the Ridge and of adjacent lithosphere beneath the Indus Fan. We infer that Murray Ridge, like the adjacent Dalrymple Trough, is underlain by continental crust, while a thin crustal section beneath the Indus Fan represents thinned continental crust or exhumed serpentinized mantle that forms part of a magma-poor rifted margin. Changes in crustal structure across the Murray Ridge and Dalrymple Trough can explain short-wavelength gravity anomalies, but a long-wavelength anomaly must be attributed to deeper density contrasts that may result from a large age contrast across the plate boundary. The origin of this fragment of continental crust remains enigmatic, but the presence of basement fabrics to the south that are roughly parallel to Murray Ridge suggests that it separated from the India/Seychelles/Madagascar block by extension during early breakup of Gondwana.

Experimental and theoretical investigations of diffraction enhanced imaging

International Nuclear Information System (INIS)

Wang Junyue; Zhu Peiping; Yuan Qingxi; Huang Wanxia; Shu Hang; Chen Bo; Li Enrong; Liu Yijin; Hu Tiandou; Wu Ziyu

2007-01-01

This contribution investigates the effect on the imaging contrast of the small angle scattering and of the rocking curve in the entire angular range. We show that based on the small angle scattering properties, the reflectivity of the crystal analyzer and the rocking curve of the monochromator-analyzer, in a diffraction enhanced imaging (DEI) experimental setup the contrast of the image collected at the top of the rocking curve is always higher than that of the apparent absorption image. Moreover, our experimental data confirm that the quality of a refraction image is superior to a refraction-like image. In order to understand the observed behavior we introduce and discuss the contribution of a new term in the classical DEI equation

Experimental and theoretical investigations of diffraction enhanced imaging

Energy Technology Data Exchange (ETDEWEB)

Wang Junyue [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049 (China); Graduate University of the Chinese Academy of Sciences, Beijing 100049 (China); Zhu Peiping [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049 (China)], E-mail: zhupp@ihep.ac.cn; Yuan Qingxi; Huang Wanxia [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049 (China); Shu Hang [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049 (China); Graduate University of the Chinese Academy of Sciences, Beijing 100049 (China); Chen Bo [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049 (China); Li Enrong [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049 (China); Graduate University of the Chinese Academy of Sciences, Beijing 100049 (China); Liu Yijin; Hu Tiandou; Wu Ziyu [Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049 (China)

2007-09-21

This contribution investigates the effect on the imaging contrast of the small angle scattering and of the rocking curve in the entire angular range. We show that based on the small angle scattering properties, the reflectivity of the crystal analyzer and the rocking curve of the monochromator-analyzer, in a diffraction enhanced imaging (DEI) experimental setup the contrast of the image collected at the top of the rocking curve is always higher than that of the apparent absorption image. Moreover, our experimental data confirm that the quality of a refraction image is superior to a refraction-like image. In order to understand the observed behavior we introduce and discuss the contribution of a new term in the classical DEI equation.

Low energy positron diffraction from Cu(111): Importance of surface loss processes at large angles of incidence

International Nuclear Information System (INIS)

Lessor, D.L.; Duke, C.B.; Lippel, P.H.; Brandes, G.R.; Canter, K.F.; Horsky, T.N.

1990-10-01

Intensities of positrons specularly diffracted from Cu(111) were measured at the Brandeis positron beam facility and analyzed in the energy range 8eV i = 4eV. At lower energies strong energy dependences occur associated both with multiple elastic scattering phenomena within atomic layers of Cu parallel to the surface and with the thresholds of inelastic channels (e.g., plasmon creation). Use of the free electron calculation of V i shows that energy dependence of inelastic processes is necessary to obtain a satisfactory description of the absolute magnitude of the diffracted intensities below E = 50eV. Detailed comparison of the calculated and observed diffraction intensities reveals the necessity of incorporating surface loss processes explicitly into the model in order to achieve a quantitative description of the measured intensities for E 40 degree. 30 refs., 5 figs., 1 tab

O2 atmospheric band measurements with WINDII: Performance of a narrow band filter/wide angle Michelson combination in space

International Nuclear Information System (INIS)

Ward, W.E.; Hersom, C.H.; Tai, C.C.; Gault, W.A.; Shepherd, G.G.; Solheim, B.H.

1994-01-01

Among the emissions viewed by the Wind Imaging Interferometer (WINDII) on the Upper Atmosphere Research Satellite (UARS) are selected lines in the (0-0) transition of the O2 atmospheric band. These lines are viewed simultaneously using a narrow band filter/wide-angle Michelson interferometer combination. The narrow band filter is used to separate the lines on the CCD (spectral-spatial scanning) and the Michelson used to modulate the emissions so that winds and rotational temperatures may be measured from the Doppler shifts and relative intensities of the lines. In this report this technique will be outlined and the on-orbit behavior since launch summarized

A controllable viewing angle LCD with an optically isotropic liquid crystal

International Nuclear Information System (INIS)

Kim, Min Su; Lim, Young Jin; Yoon, Sukin; Kang, Shin-Woong; Lee, Seung Hee; Kim, Miyoung; Wu, Shin-Tson

2010-01-01

An optically isotropic liquid crystal (LC) such as a blue phase LC or an optically isotropic nano-structured LC exhibits a very wide viewing angle because the induced birefringence is along the in-plane electric field. Utilizing such a material, we propose a liquid crystal display (LCD) whose viewing angle can be switched from wide view to narrow view using only one panel. In the device, each pixel is divided into two parts: a major pixel and a sub-pixel. The main pixels display the images while the sub-pixels control the viewing angle. In the main pixels, birefringence is induced by horizontal electric fields through inter-digital electrodes leading to a wide viewing angle, while in the sub-pixels, birefringence is induced by the vertical electric field so that phase retardation occurs only at oblique angles. As a result, the dark state (or contrast ratio) of the entire pixel can be controlled by the voltage of the sub-pixels. Such a switchable viewing angle LCD is attractive for protecting personal privacy.

The incidence angle influence on the structure of secondary-emission characteristics of single crystals

International Nuclear Information System (INIS)

Gasanov, E.R.; Aliyev, B.Z.

2012-01-01

Full text : The dependences of Wand MO single crystals in different atom planes have been studied in this work. It is revealed that maximums are added to each dependency and also minimums of first and second degree. This fact is explained by diffraction dynamic theory. It is established that electron diffraction oriented not perpendicularly to crystal surface is the reason of appearance of second order structure on studied secondary-emission characteristics. In the present work being the continuation and development of SEE investigations of high-melting metal single crystals begun earlier by authors, the structure dependence of SEE main characteristics of angle has been studied. This angle has been chosen because as it is mentioned before the bad repeatability in different experiments for it is observed

Assessment of firing conditions in old fired-clay bricks: The contribution of X-ray powder diffraction with the Rietveld method and small angle neutron scattering

Energy Technology Data Exchange (ETDEWEB)

Viani, Alberto, E-mail: viani@itam.cas.cz [Institute of Theoretical and Applied Mechanics AS CR, Centre of Excellence Telč, Batelovská 485, CZ-58856 Telč (Czech Republic); Sotiriadis, Konstantinos [Institute of Theoretical and Applied Mechanics AS CR, Centre of Excellence Telč, Batelovská 485, CZ-58856 Telč (Czech Republic); Len, Adél [Wigner Research Centre for Physics HAS, Konkoly-Thege 29-33, 1121 Budapest (Hungary); Šašek, Petr; Ševčík, Radek [Institute of Theoretical and Applied Mechanics AS CR, Centre of Excellence Telč, Batelovská 485, CZ-58856 Telč (Czech Republic)

2016-06-15

Full characterization of fired-clay bricks is crucial for the improvement of process variables in manufacturing and, in case of old bricks, for restoration/replacement purposes. To this aim, five bricks produced in a plant in Czech Republic in the past have been investigated with a combination of analytical techniques in order to derive information on the firing process. An additional old brick from another brickyard was also used to study the influence of different raw materials on sample microstructure. The potential of X-ray diffraction with the Rietveld method and small angle neutron scattering technique has been exploited to describe the phase transformations taking place during firing and characterize the brick microstructure. Unit-cell parameter of spinel and amount of hematite are proposed as indicators of the maximum firing temperature, although for the latter, limited to bricks produced from the same raw material. The fractal quality of the surface area of pores obtained from small angle neutron scattering is also suggested as a method to distinguish between bricks produced from different raw clays. - Highlights: • Rietveld method helps in describing microstructure and physical properties of bricks. • XRPD derived cell parameter of spinel is proposed as an indicator of firing temperature. • SANS effectively describes brick micro and nanostructure, including closed porosity. • Fractal quality of pore surface is proposed as ‘fingerprint’ of brick manufacturing.

The current status of small-angle x-ray scattering beamline at Diamond Light Source

International Nuclear Information System (INIS)

Inoue, Katsuaki; Doutch, James; Terrill, Nick

2013-01-01

The small-angle X-ray scattering (SAXS) covers the major disciplines of biology, chemistry and physics delivering structural and dynamic information in nanoscience, mesoscopic architectures, supramolecular structures, and nucleation/growth of crystals. SAXS is also proving to be important in archaeological, environmental, and conservation sciences, and has further indicated its ability to span wide-ranging scientific disciplines. Thus, strong needs for SAXS studies are increasing significantly in a broad range of scientific fields year by year. Based on such a background, the demand for high throughput SAXS experiments is increasing. At the synchrotron facility, Diamond Light Source, one SAXS beamline, Non-crystalline diffraction I22 is now operational and highly automated throughput small-angle X-ray scattering (HATSAXS) beamline B21 is now under construction. I22 is the Undulator beamline and wide varieties of experiments, including time-resolved experiments are attempted. Based on the concept of HATSAXS, the key feature of B21 will focuses on the automation of end-station equipment. A automated sample changer has been purchased for solution SAXS measurements on biomolecules. A robotic-arm-type automated sample changer that is capable of handling several kinds of samples in material science is also being constructed. B21 is expected to successfully provide all users highly automated throughput measurements with the highest possible reliability and accuracy. Construction of this beamline will end in the second half of 2012, and will be open for users in the early summer of 2013 after commissioning. (author)

Wide-angle NSE and TOF the spectrometer SPAN at BENSC

CERN Document Server

Pappas, C; Kischnik, R; Mezei, F

2002-01-01

The cylindrical symmetry of the magnetic field configuration of SPAN allows for simultaneous neutron spin echo (NSE) measurements over the whole range of scattering angles accessible by a spectrometer. The open construction also allows for time-of-flight (TOF) measurements, which can be performed under the same conditions as NSE, in particular with polarization analysis. TOF and NSE spectra are then directly comparable with each other, without any adjustable parameters, covering a dynamic range of more than four orders of magnitude at a single wavelength. (orig.)

Wide-angle NSE and TOF: the spectrometer SPAN at BENSC

International Nuclear Information System (INIS)

Pappas, C.; Triolo, A.; Kischnik, R.; Mezei, F.

2002-01-01

The cylindrical symmetry of the magnetic field configuration of SPAN allows for simultaneous neutron spin echo (NSE) measurements over the whole range of scattering angles accessible by a spectrometer. The open construction also allows for time-of-flight (TOF) measurements, which can be performed under the same conditions as NSE, in particular with polarization analysis. TOF and NSE spectra are then directly comparable with each other, without any adjustable parameters, covering a dynamic range of more than four orders of magnitude at a single wavelength. (orig.)

Crystalline phase of sodium germanate system determined by x-ray diffraction and 23Na magic angle spinning nuclear magnetic resonance

International Nuclear Information System (INIS)

Hussin, R.; Holland, D.; Dupree, R.

2000-01-01

Crystalline products of sodium germanate glasses system with composition from 10 mol% to 50 mol% Na 2 O have been investigated using 23 Na magic angle spinning (MAS) nuclear magnetic resonance (NMR) spectroscopy and x-ray diffraction (XRD). Fitting of the 23 Na NMR spectra of the crystalline phases concerning different crystallographically sodium atom in sodium germanate system are reasonably reproducible as observed by the spectra obtained. The line shape simulations of the 23 Na NMR spectra yielded NMR quadrupolar parameters such as nuclear quadrupole coupling constants (C Q ), asymmetry parameters (η), and isotropic chemical shifts (δ i ). 23 Na NMR isotropic chemical shift may also provide further information on the structural environment of the sodium atom. A simple correlation between structure and NMR parameters to be tested can be used to probe the structure of sodium germanate glasses. The experimental 23 Na chemical shifts correlate well with an empirical shift parameter based on the total oxygen-cation bond valence and Na-O distances of all oxygen atoms in the first coordination sphere of the sodium cation. In this study the different phases in the sodium germanate system were identified. These results show that 23 Na NMR can provide examples of the types of structural information for sodium germanate system. (Author)

Lattice-parameter-difference measurement of heteroepitaxial structures by means of extremely asymmetrical Bragg diffraction

International Nuclear Information System (INIS)

Pietsch, U.; Borchard, W.

1987-01-01

The sensitivity of measurements of the lattice-parameter difference in monocrystalline heterostructures can be enhanced by use of an extremely asymmetrical diffraction geometry. If the angle of incidence is somewhat higher than the critical angle for total external reflection, the Bragg peak is shifted from the position calculated by kinematic theory. The amount of shift depends on the angle of incidence as well as on the mass density of the material used. For heteroepitaxial structures both the layer and the substrate peaks are shifted but by different amounts. Therefore it becomes possible to characterize layers of totally lattice-matched structures also. (orig.)

Full-color, large area, transmissive holograms enabled by multi-level diffractive optics.

Science.gov (United States)

Mohammad, Nabil; Meem, Monjurul; Wan, Xiaowen; Menon, Rajesh

2017-07-19

We show that multi-level diffractive microstructures can enable broadband, on-axis transmissive holograms that can project complex full-color images, which are invariant to viewing angle. Compared to alternatives like metaholograms, diffractive holograms utilize much larger minimum features (>10 µm), much smaller aspect ratios (30 mm ×30 mm). We designed, fabricated and characterized holograms that encode various full-color images. Our devices demonstrate absolute transmission efficiencies of >86% across the visible spectrum from 405 nm to 633 nm (peak value of about 92%), and excellent color fidelity. Furthermore, these devices do not exhibit polarization dependence. Finally, we emphasize that our devices exhibit negligible absorption and are phase-only holograms with high diffraction efficiency.

Diffraction and angular momentum effects in semiclassical atomic scattering theory

International Nuclear Information System (INIS)

Russek, A.

1979-01-01

The semiclassical scattering theory of Mott and Massey and Ford and Wheeler is here extended to multichannel scattering as occurs at a crossing or pseudocrossing of the transient molecule formed by the colliding atoms. The generalized theory incorporates both interference and diffraction phenomena, but the emphasis in this work is on diffraction. For small-angle scattering, diffraction effects become broader, not narrower, as the collision energy increases: ΔbΔtau > or = h[E/sub inc//(2m)]/sup 1/2/ relates the uncertainties in impact parameter b and reduced scattering angle tau = E/sub inc/theta, and determines the range in b required to resolve a structure in the deflection function of height Δtau. In the kilovolt range of collision energies, the effects of local maxima and minima in the deflection function are washed out, and the Airy-function approximation of Ford and Wheeler is inappropriate to describe the differential cross section. More generally, it is shown that at keV collision energies the stationary-phase approximation, heretofore essential in the reduction to the semiclassical limit, breaks down in the vicinity of a level crossing. An approximate theorem is proposed which remains valid in this region and elsewhere reduces to the standard stationary-phase approximation. Several illustrative examples are considered. A separate development treats the effect on the differential scattering cross section of a change in electronic angular momentum when electronic excitation occurs

Measurement of the spatial resolution of wide-pitch silicon strip detectors with large incident angle

International Nuclear Information System (INIS)

Kawasaki, T.; Hazumi, M.; Nagashima, Y.

1996-01-01

As a part of R ampersand D for the BELLE experiment at KEK-B, we measured the spatial resolution of silicon strip detectors for particles with incident angles ranging from 0 degrees to 75 degrees. These detectors have strips with pitches of 50, 125 and 250 μm on the ohmic side. We have obtained the incident angle dependence which agreed well with a Monte Carlo simulation. The resolution was found to be 11 μm for normal incidence with a pitch of 50 μm, and 29 μm for incident angle of 75 degrees with a pitch of 250μm

Neutron diffraction on polymorphic phases of phospholipids

International Nuclear Information System (INIS)

Adachi, Tomohiro; Furusaka, Michihiro; Otomo, Toshiya; Hatta, Ichiro

2001-01-01

Small angle neutron diffraction experiments were performed in DPPC and DPPC/cholesterol systems. We investigated the DPPC-d62 bilayers without cholesterol and the DPPC-d75 bilayers with 5 and 15 mol% cholesterol. For DPPC-d62 systems, in the gel and fluid phase, the reflections up to third order from lamellar structure were observed. Scattering length density profiles of these systems were generated. They show that the packing density of hydrocarbon chain in gel phase is higher than in fluid phase. We show that the neutron diffraction experiment is effective on observing the packing and the scattering length density of the hydrocarbon chain. On the other hand, for DPPC-d75/cholesterol systems, only the reflection from the ripple structure was observed. It shows that cholesterol is periodically localized in accordance with ripple structure forming a periodic bandlike structure parallel to a ridge of the ripple structure. (author)

Selected-area diffraction and spectroscopy in LEEM and PEEM

International Nuclear Information System (INIS)

Tromp, R.M.

2012-01-01

This paper addresses the effects of spherical and chromatic aberration of the objective lens, as well as chromatic dispersion of magnetic prism arrays, on the ability to perform selected area Low Energy Electron Diffraction, as well as (Angle Resolved) Photo Electron Spectroscopy experiments in today's advanced cathode lens microscopy instruments. -- Highlights: ► Aberrations of the cathode lens affect SA diffraction and spectroscopy experiments in LEEM/PEEM. ► In LEEM the problem can be overcome by inserting the SA aperture in the illuminating path. ► In PEEM for selected areas smaller than 2–4 μm aberration correction becomes a necessity. ► Chromatic dispersion in the magnetic prism array commonly can be neglected in most cases.

ELECTROMAGNETIC SCATTERING AND ANTENNA TECHNOLOGY (EMSAT) Task Order 0003: Design of a Circularly Polarized, 20 60 GHZ Active Phased Array for Wide Angle Scanning

Science.gov (United States)

2017-08-08

previously published linear -to-circular polarizers. This is because the first sheet has a low inductance in the -direction, which acts as a wire-grid...GHZ Active Phased Array for Wide Angle Scanning Carl R. Pfeiffer Defense Engineering Corporation Boris Tomasic Multispectral Sensing and...GRANT NUMBER 5c. PROGRAM ELEMENT NUMBER 62204F/61102F 6. AUTHOR(S) Carl R. Pfeiffer (Defense Engineering Corporation) Boris Tomasic (AFRL

Prospects of diffractive physics with the ATLAS forward detectors

CERN Document Server

Lopez Paz, Ivan; The ATLAS collaboration

2017-01-01

The ATLAS Forward Proton (AFP) detector provides measurements of the momentum and emission angle of very forward protons. This enables the observation and measurement of a range of processes where one or both protons remain intact. Such processes are associated with elastic and diffractive scattering. In this talk, we give on overview of the technical details of the AFP, its current status as well as its associated physics program.

Viewing angle switching of patterned vertical alignment liquid crystal display

International Nuclear Information System (INIS)

Lim, Young Jin; Jeong, Eun; Chin, Mi Hyung; Lee, Seung Hee; Ji, Seunghoon; Lee, Gi-Dong

2008-01-01

Viewing angle control of a patterned vertical alignment (PVA) liquid crystal display using only one panel is investigated. In conventional PVA modes, a vertically aligned liquid crystal (LC) director tilts down in four directions making 45 deg. with respect to crossed polarizers to exhibit a wide viewing angle. In the viewing angle control device, one pixel was divided into two sub-pixels such that the LC director in the main pixel is controlled to be tilted down in multiple directions making an angle with the polarizer, playing the role of main display with the wide viewing angle, while the LC director in the sub-pixel is controlled to be tilted down to the polarizer axis, playing the role of sub-pixel to the viewing angle control for the narrow viewing angle. Using sub-pixel control, light leakage or any type of information such as characters and image can be generated in oblique viewing directions without distorting the image quality in the normal direction, which will prevent others from peeping at the displayed image by overlapping the displayed image with the made image

Characterization of white poplar and eucalyptus after ionic liquid pretreatment as a function of biomass loading using X-ray diffraction and small angle neutron scattering

Energy Technology Data Exchange (ETDEWEB)

Yuan, Xueming [Beijing Univ. of Chemical Technology (China); Duan, Yonghao [Beijing Univ. of Chemical Technology (China); He, Lilin [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Singh, Seema [Sandia National Lab. (SNL-CA), Livermore, CA (United States); Joint BioEnergy Inst. (JBEI), Emeryville, CA (United States); Simmons, Blake [Joint BioEnergy Inst. (JBEI), Emeryville, CA (United States); Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Cheng, Gang [Beijing Univ. of Chemical Technology (China); Joint BioEnergy Inst. (JBEI), Emeryville, CA (United States); Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)

2017-02-08

A systematic study was done to understand interactions among biomass loading during ionic liquid (IL) pretreatment, biomass type and biomass structures. White poplar and eucalyptus samples were pretreated using 1-ethyl-3-methylimidazolium acetate (EmimOAc) at 110 °C for 3 h at biomass loadings of 5, 10, 15, 20 and 25 wt%. All of the samples were chemically characterized and tested for enzymatic hydrolysis. Physical structures including biomass crystallinity and porosity were measured by X-ray diffraction (XRD) and small angle neutron scattering (SANS), respectively. SANS detected pores of radii ranging from ~25 to 625 Å, enabling assessment of contributions of pores with different sizes to increased porosity after pretreatment. Contrasting dependences of sugar conversion on white poplar and eucalyptus as a function of biomass loading were observed and cellulose crystalline structure was found to play an important role.

ENDIX. A computer program to simulate energy dispersive X-ray and synchrotron powder diffraction diagrams

International Nuclear Information System (INIS)

Hovestreydt, E.; Karlsruhe Univ.; Parthe, E.; Benedict, U.

1987-01-01

A Fortran 77 computer program is described which allows the simulation of energy dispersive X-ray and synchrotron powder diffraction diagrams. The input consists of structural data (space group, unit cell dimensions, atomic positional and displacement parameters) and information on the experimental conditions (chosen Bragg angle, type of X-ray tube and applied voltage or operating power of synchrotron radiation source). The output consists of the normalized intensities of the diffraction lines, listed by increasing energy (in keV), and of an optional intensity-energy plot. The intensities are calculated with due consideration of the wave-length dependence of both the anomalous dispersion and the absorption coefficients. For a better agreement between observed and calculated spectra provision is made to optionally superimpose, on the calculated diffraction line spectrum, all additional lines such as fluorescence and emission lines and escape peaks. The different effects which have been considered in the simulation are discussed in some detail. A sample calculation of the energy dispersive powder diffraction pattern of UPt 3 (Ni 3 Sn structure type) is given. Warning: the user of ENDIX should be aware that for a successful application it is necessary to adapt the program to correspond to the actual experimental conditions. Even then, due to the only approximately known values of certain functions, the agreement between observed and calculated intensities will not be as good as for angle dispersive diffraction methods

Application of new synchrotron powder diffraction techniques to anomalous scattering from glasses

International Nuclear Information System (INIS)

Beno, M.A.; Knapp, G.S.; Armand, P.; Price, D.L.; Saboungi, M.

1995-01-01

We have applied two synchrotron powder diffraction techniques to the measurement of high quality anomalous scattering diffraction data for amorphous materials. One of these methods, which uses a curved perfect crystal analyzer to simultaneously diffract multiple powder lines into a position sensitive detector has been shown to possess high resolution, low background, and very high counting rates. This data measurement technique provides excellent energy resolution while minimizing systematic errors resulting from detector nonlinearity. Anomalous scattering data for a Cesium Germanate glass collected using this technique will be presented. The second powder diffraction technique uses a flat analyzer crystal to deflect multiple diffraction lines out of the equatorial plane. Calculations show that this method possesses sufficient energy resolution for anomalous scattering experiments when a perfect crystal analyzer is used and is experimentally much simpler. Future studies will make use of a rapid sample changer allowing the scattering from the sample and a standard material (a material not containing the anomalous scatterer) to be measured alternately at each angle, reducing systematic errors due to beam instability or sample misalignment

Neutron diffraction and NQR study of the intermediate turn angle phase formed during AFI to AFII recording in YBa2Cu3-xAlxO6+#delta#

DEFF Research Database (Denmark)

Brecht, E.; Schmahl, W.W.; Fuess, H.

1997-01-01

The reordering mechanism from the antiferromagnetic phase AFI to the antiferromagnetic phase AFII in an oxygen-deficient YBa2Cu2.94Al0.06O6+delta single crystal with an oxygen content delta=0.18 in the Cu(1) layer has been studied by neutron diffraction and nuclear quadrupole resonance (NQR......). The crystal orders magnetically from the paramagnetic state to the antiferromagnetic AFI state at the Neel temperature T-N=403 K with an empirical critical exponent of beta = 0.26. Reordering to the antiferromagnetic AFII state sets in at T-2 = 12 K. In both the AFI and AFII phases the ordered magnetic...... as a function of temperature. This result indicates unequivocally that the AFIAFII reordering takes place via a noncollinear intermediate turn angle phase AFI+II....

Computer programs for unit-cell determination in electron diffraction experiments

International Nuclear Information System (INIS)

Li, X.Z.

2005-01-01

A set of computer programs for unit-cell determination from an electron diffraction tilt series and pattern indexing has been developed on the basis of several well-established algorithms. In this approach, a reduced direct primitive cell is first determined from experimental data, in the means time, the measurement errors of the tilt angles are checked and minimized. The derived primitive cell is then checked for possible higher lattice symmetry and transformed into a proper conventional cell. Finally a least-squares refinement procedure is adopted to generate optimum lattice parameters on the basis of the lengths of basic reflections in each diffraction pattern and the indices of these reflections. Examples are given to show the usage of the programs

Interphase microstress measurements in IN 718 by cold neutron diffraction

Energy Technology Data Exchange (ETDEWEB)

Repper, J.; Link, P.; Hofmann, M.; Petry, W. [TU Muenchen, Forschungsneutronenquelle Heinz Maier-Leibnitz (FRM II), Garching (Germany); Krempaszky, C. [TU Muenchen, Christian-Doppler-Labor fuer Werkstoffmechanik von Hochleistungslegierungen, Garching (Germany); Werner, E. [TU Muenchen, Lehrstuhl fuer Werkstoffkunde und Werkstoffmechanik, Garching (Germany)

2010-06-15

Thermal neutron diffraction is an important and reliable method for the investigation of microscopic stresses. The measurement of Bragg reflections caused by phases of small volume fractions, however, is often intricate due to low intensities and overlapping peaks. The wavelength range of cold neutrons allows to shift the Bragg reflections to larger scattering angles resulting in an increase of relative distances between Bragg reflections. The high resolution of cold neutron diffraction technique is demonstrated by in-situ load tests in which selected Bragg reflections caused by precipitates with small volume fractions in the precipitation strengthened alloy IN 718 are observed. The accumulated microstrains show marked differences in dependence of the precipitated phases within the matrix phase. (orig.)

Experimental coherent X-ray diffractive imaging: capabilities and limitations of the technique

International Nuclear Information System (INIS)

Schropp, Andreas

2008-08-01

The investigations pursued during this work were focused on the testing of the applicability of the coherent X-ray diffractive imaging(CXDI)-method in the hard X-ray regime and different measurements were carried out at photon energies between 7 keV and 10 keV. The samples investigated were lithographically prepared two-dimensional gold structures with a size ranging from 3 μm to 10 μm as well as a cluster of gold spheres with a lateral extension of about 3.5 μm. Continuous diffraction patterns were recorded in small angle scattering geometry. In some of the measurements a scattering signal up to the edge of the detector could be measured which corresponds to a lateral resolution of about 30 nm. For certain samples it was possible to reconstruct the object from the measured diffraction data. Since the scattered intensity of non-periodic objects is weak at large scattering angles, the available photon flux is finally the main limitation of the method with regard to the achievable resolution. The experimental data were used to get an estimate of photon flux required for sub-nanometer resolution. The ptychographic iterative phase retrieval algorithm proposed by J. M. Rodenburg et al. (2004) was implemented and tested on simulated diffraction data. Additionally, a genetic algorithm has been developed and implemented for phase retrieval. This algorithm is very different from state-of-the-art algorithms and allows to introduce further experimentally important parameters such as a certain illumination function and partial coherence of the X-ray light. (orig.)

High-energy X-ray diffraction studies of disordered materials

International Nuclear Information System (INIS)

Kohara, Shinji; Suzuya, Kentaro

2003-01-01

With the arrival of the latest generation of synchrotron sources and the introduction of advanced insertion devices (wigglers and undulators), the high-energy (E≥50 keV) X-ray diffraction technique has become feasible, leading to new approaches in the quantitative study of the structure of disordered materials. High-energy X-ray diffraction has several advantages: higher resolution in real space due to a wide range of scattering vector Q, smaller correction terms (especially the absorption correction), reduction of truncation errors, the feasibility of running under extreme environments, including high-temperatures and high-pressures, and the ability to make direct comparisons between X-ray and neutron diffraction data. Recently, high-energy X-ray diffraction data have been combined with neutron diffraction data from a pulsed source to provide more detailed and reliable structural information than that hitherto available

EVALUATION OF THE QUALITY OF ACTION CAMERAS WITH WIDE-ANGLE LENSES IN UAV PHOTOGRAMMETRY

Directory of Open Access Journals (Sweden)

H. Hastedt

2016-06-01

Full Text Available The application of light-weight cameras in UAV photogrammetry is required due to restrictions in payload. In general, consumer cameras with normal lens type are applied to a UAV system. The availability of action cameras, like the GoPro Hero4 Black, including a wide-angle lens (fish-eye lens offers new perspectives in UAV projects. With these investigations, different calibration procedures for fish-eye lenses are evaluated in order to quantify their accuracy potential in UAV photogrammetry. Herewith the GoPro Hero4 is evaluated using different acquisition modes. It is investigated to which extent the standard calibration approaches in OpenCV or Agisoft PhotoScan/Lens can be applied to the evaluation processes in UAV photogrammetry. Therefore different calibration setups and processing procedures are assessed and discussed. Additionally a pre-correction of the initial distortion by GoPro Studio and its application to the photogrammetric purposes will be evaluated. An experimental setup with a set of control points and a prospective flight scenario is chosen to evaluate the processing results using Agisoft PhotoScan. Herewith it is analysed to which extent a pre-calibration and pre-correction of a GoPro Hero4 will reinforce the reliability and accuracy of a flight scenario.

Evaluation of the Quality of Action Cameras with Wide-Angle Lenses in Uav Photogrammetry

Science.gov (United States)

Hastedt, H.; Ekkel, T.; Luhmann, T.

2016-06-01

The application of light-weight cameras in UAV photogrammetry is required due to restrictions in payload. In general, consumer cameras with normal lens type are applied to a UAV system. The availability of action cameras, like the GoPro Hero4 Black, including a wide-angle lens (fish-eye lens) offers new perspectives in UAV projects. With these investigations, different calibration procedures for fish-eye lenses are evaluated in order to quantify their accuracy potential in UAV photogrammetry. Herewith the GoPro Hero4 is evaluated using different acquisition modes. It is investigated to which extent the standard calibration approaches in OpenCV or Agisoft PhotoScan/Lens can be applied to the evaluation processes in UAV photogrammetry. Therefore different calibration setups and processing procedures are assessed and discussed. Additionally a pre-correction of the initial distortion by GoPro Studio and its application to the photogrammetric purposes will be evaluated. An experimental setup with a set of control points and a prospective flight scenario is chosen to evaluate the processing results using Agisoft PhotoScan. Herewith it is analysed to which extent a pre-calibration and pre-correction of a GoPro Hero4 will reinforce the reliability and accuracy of a flight scenario.

Geometrical characterization of micro-optical cylindrical lens arrays using angular resolved diffraction

DEFF Research Database (Denmark)

Iversen, Theis Faber Quist; Hanson, Steen Grüner

2010-01-01

been shown (Iversen et al 2009 J. Opt. A: Pure Appl. Opt. 11 054014 (6pp), B¨uttner and Zeitner 2002 Appl. Opt. 41 6841 8) that the average radius of curvature of an MLA structure can be extracted by observing the far-field diffraction pattern intensity distribution obtained from illumination....... By scanning the angle of incidence of the coherent illumination and simultaneously observing the diffracted intensity, information about the grating period and the radius of curvature can be extracted. The method is implemented with emphasis on further development for compact, high-speed dedicated systems. We...

On the theory of diffraction of Maxwellian atomic beams by solid surfaces

International Nuclear Information System (INIS)

Goodman, F.O.

1976-01-01

In the context of diffraction of Maxwellian (thermal) atomic beams by solid surfaces, the usual assumption that the angular position of the maximum in a diffracted beam corresponds to the diffraction angle of atoms with the most probable de Broglie wavelength is examined, and compared with other possible criteria and with the correct result. It is concluded that, although this criterion may be the best simple one available, it is certainly bad in some situations; the reasons why, and the conditions under which, it is expected to be good are discussed. Also, it is shown that considerable care must be taken when shapes of diffracted beams and when angular positions of their maxima are calculated, because certain physical effects (which are always present) may change these shapes and positions in unexpected ways. The theory is compared with two sets of relatively modern experimental data, one set for which the fit is good, and another set for which a fit is impossible

A structural view of Pd model catalysts : high-pressure surface X-Ray diffraction

NARCIS (Netherlands)

Rijn, Richard van

2012-01-01

This thesis describes the development of a combined high-pressure/ultrahigh-vacuum flow reactor for the study of model catalysts by means of surface x-ray diffraction and grazing incidence small angle scattering. The system was used to measure a stability diagram for the different oxide phases

Ninety Years of Powder Diffraction: from Birth to Maturity

International Nuclear Information System (INIS)

Paszkowicz, W.

2006-01-01

The expression ''powder diffraction '' denotes the phenomenon of diffraction of any electromagnetic waves or particles on polycrystalline (powdered, bulk or thin film) materials which is used in a wide variety experimental settings. The X-ray powder-diffraction method was devised and developed during the First World War (1916) by a Dutch/Swiss team, Peter Debye and Paul Scherrer, in Goettingen, Germany, and independently, marginally later, by an American, Albert W. Hull in Schenectady, USA. The birth of powder diffraction came four years after the discovery of the phenomenon of single-crystal diffraction made in 1912 by Walther Friedrich, Paul Knipping and Max Laue in Munich and developed from 1912/1913 by William Henry Bragg (father) and William Lawrence Bragg (son), and later by many others. Powder diffraction became a milestone towards an understanding of the nature of materials, especially of those which cannot be prepared in the form of suitable single crystals, and permitted rapid progress in solid state physics and chemistry. The events leading to the discovery of powder-diffraction phenomenon are briefly reviewed. The importance of synchrotron powder diffraction studies, which have developed since 1980s, is emphasised. (author)

Precession electron diffraction for SiC grain boundary characterization in unirradiated TRISO fuel

International Nuclear Information System (INIS)

Lillo, T.M.; Rooyen, I.J. van; Wu, Y.Q.

2016-01-01

Highlights: • SiC grain orientation determined by TEM-based precession electron diffraction. • Orientation data improved with increasing TEM sample thickness. • Fraction of low angle grain boundaries lower from PED data than EBSD data. • Fractions of high angle and CSL-related boundaries similar to EBSD data. - Abstract: Precession electron diffraction (PED), a transmission electron microscopy-based technique, has been evaluated for the suitability for evaluating grain boundary character in the SiC layer of tristructural isotropic (TRISO) fuel. This work reports the effect of transmission electron microscope (TEM) lamella thickness on the quality of data and establishes a baseline comparison to SiC grain boundary characteristics, in an unirradiated TRISO particle, determined previously using a conventional electron backscatter diffraction (EBSD) scanning electron microscope (SEM)-based technique. In general, it was determined that the lamella thickness produced using the standard focused ion beam (FIB) fabrication process (∼80 nm), is sufficient to provide reliable PED measurements, although thicker lamellae (∼120 nm) were found to produce higher quality orientation data. Also, analysis of SiC grain boundary character from the TEM-based PED data showed a much lower fraction of low-angle grain boundaries compared to SEM-based EBSD data from the SiC layer of a TRISO-coated particle made using the same fabrication parameters and a SiC layer deposited at a slightly lower temperature from a surrogate TRISO particle. However, the fractions of high-angle and coincident site lattice (CSL)-related grain boundaries determined by PED are similar to those found using SEM-based EBSD. Since the grain size of the SiC layer of TRSIO fuel can be as small as 250 nm (Kirchhofer et al., 2013), depending on the fabrication parameters, and since grain boundary fission product precipitates in irradiated TRISO fuel can be nano-sized, the TEM-based PED orientation data

Feedback by AGN Jets and Wide-angle Winds on a Galactic Scale

Energy Technology Data Exchange (ETDEWEB)

Dugan, Zachary; Silk, Joseph [The Johns Hopkins University Department of Physics and Astronomy, Bloomberg Center for Physics and Astronomy, Room 366, 3400 N. Charles Street, Baltimore, MD 21218 (United States); Gaibler, Volker [Universität Heidelberg, Zentrum für Astronomie, Institut für Theoretische Astrophysik, Albert-Ueberle-Str. 2, D-69120 Heidelberg (Germany)

2017-07-20

To investigate the differences in mechanical feedback from radio-loud and radio-quiet active galactic nuclei on the host galaxy, we perform 3D AMR hydrodynamic simulations of wide-angle, radio-quiet winds with different inclinations on a single, massive, gas-rich disk galaxy at a redshift of 2–3. We compare our results to hydrodynamic simulations of the same galaxy but with a jet. The jet has an inclination of 0° (perpendicular to the galactic plane), and the winds have inclinations of 0°, 45°, and 90°. We analyze the impact on the host’s gas, star formation, and circumgalactic medium. We find that jet feedback is energy-driven and wind feedback is momentum-driven. In all the simulations, the jet or wind creates a cavity mostly devoid of dense gas in the nuclear region where star formation is then quenched, but we find strong positive feedback in all the simulations at radii greater than 3 kpc. All four simulations have similar SFRs and stellar velocities with large radial and vertical components. However, the wind at an inclination of 90° creates the highest density regions through ram pressure and generates the highest rates of star formation due to its ongoing strong interaction with the dense gas of the galactic plane. With increased wind inclination, we find greater asymmetry in gas distribution and resulting star formation. Our model generates an expanding ring of triggered star formation with typical velocities of the order of 1/3 of the circular velocity, superimposed on the older stellar population. This should result in a potentially detectable blue asymmetry in stellar absorption features at kiloparsec scales.

Dye and pigment-free structural colors and angle-insensitive spectrum filters

Energy Technology Data Exchange (ETDEWEB)

Guo, Lingjie Jay; Hollowell, Andrew E.; Wu, Yi-Kuei

2017-01-17

Optical spectrum filtering devices displaying minimal angle dependence or angle insensitivity are provided. The filter comprises a localized plasmonic nanoresonator assembly having a metal material layer defining at least one nanogroove and a dielectric material disposed adjacent to the metal material layer. The dielectric material is disposed within the nanogroove(s). The localized plasmonic nanoresonator assembly is configured to funnel and absorb a portion of an electromagnetic spectrum in the at least one nanogroove via localized plasmonic resonance to generate a filtered output having a predetermined range of wavelengths that displays angle insensitivity. Thus, flexible, high efficiency angle independent color filters having very small diffraction limits are provided that are particularly suitable for use as pixels for various display devices or for use in anti-counterfeiting and cryptography applications. The structures can also be used for colored print applications and the elements can be rendered as pigment-like particles.

Trapezoidal diffraction grating beam splitters in single crystal diamond

Science.gov (United States)

Kiss, Marcell; Graziosi, Teodoro; Quack, Niels

2018-02-01

Single Crystal Diamond has been recognized as a prime material for optical components in high power applications due to low absorption and high thermal conductivity. However, diamond microstructuring remains challenging. Here, we report on the fabrication and characterization of optical diffraction gratings exhibiting a symmetric trapezoidal profile etched into a single crystal diamond substrate. The optimized grating geometry diffracts the transmitted optical power into precisely defined proportions, performing as an effective beam splitter. We fabricate our gratings in commercially available single crystal CVD diamond plates (2.6mm x 2.6mm x 0.3mm). Using a sputter deposited hard mask and patterning by contact lithography, the diamond is etched in an inductively coupled oxygen plasma with zero platen power. The etch process effectively reveals the characteristic {111} diamond crystal planes, creating a precisely defined angled (54.7°) profile. SEM and AFM measurements of the fabricated gratings evidence the trapezoidal shape with a pitch of 3.82μm, depth of 170 nm and duty cycle of 35.5%. Optical characterization is performed in transmission using a 650nm laser source perpendicular to the sample. The recorded transmitted optical power as function of detector rotation angle shows a distribution of 21.1% in the 0th order and 23.6% in each +/-1st order (16.1% reflected, 16.6% in higher orders). To our knowledge, this is the first demonstration of diffraction gratings with trapezoidal profile in single crystal diamond. The fabrication process will enable beam splitter gratings of custom defined optical power distribution profiles, while antireflection coatings can increase the efficiency.

Small-angle neutron-scattering studies of the magnetic phase diagram of MnSi

DEFF Research Database (Denmark)

Harris, P.; Lebech, B.; Hae Seop Shim

1995-01-01

The antiferromagnetic order of MnSi has been studied as function of temperature and applied magnetic field using small-angle neutron scattering. The results were analyzed using the three-dimensional resolution function and the scattering cross-section to model the diffraction data. Physical...

Measurement system for diffraction efficiency of convex gratings

Science.gov (United States)

Liu, Peng; Chen, Xin-hua; Zhou, Jian-kang; Zhao, Zhi-cheng; Liu, Quan; Luo, Chao; Wang, Xiao-feng; Tang, Min-xue; Shen, Wei-min

2017-08-01

A measurement system for diffraction efficiency of convex gratings is designed. The measurement system mainly includes four components as a light source, a front system, a dispersing system that contains a convex grating, and a detector. Based on the definition and measuring principle of diffraction efficiency, the optical scheme of the measurement system is analyzed and the design result is given. Then, in order to validate the feasibility of the designed system, the measurement system is set up and the diffraction efficiency of a convex grating with the aperture of 35 mm, the curvature-radius of 72mm, the blazed angle of 6.4°, the grating period of 2.5μm and the working waveband of 400nm-900nm is tested. Based on GUM (Guide to the Expression of Uncertainty in Measurement), the uncertainties in the measuring results are evaluated. The measured diffraction efficiency data are compared to the theoretical ones, which are calculated based on the grating groove parameters got by an atomic force microscope and Rigorous Couple Wave Analysis, and the reliability of the measurement system is illustrated. Finally, the measurement performance of the system is analyzed and tested. The results show that, the testing accuracy, the testing stability and the testing repeatability are 2.5%, 0.085% and 3.5% , respectively.

Time-of-flight diffraction at pulsed neutron sources: An introduction to the symposium

International Nuclear Information System (INIS)

Jorgensen, J.D.

1994-01-01

In the 25 years since the first low-power demonstration experiments, pulsed neutron sources have become as productive as reactor sources for many types of diffraction experiments. The pulsed neutron sources presently operating in the United States, England, and Japan offer state of the art instruments for powder and single crystal diffraction, small angle scattering, and such specialized techniques as grazing-incidence neutron reflection, as well as quasielastic and inelastic scattering. In this symposium, speakers review the latest advances in diffraction instrumentation for pulsed neutron sources and give examples of some of the important science presently being done. In this introduction to the symposium, I briefly define the basic principles of pulsed neutron sources, review their development, comment in general terms on the development of time-of-flight diffraction instrumentation for these sources, and project how this field will develop in the next ten years

Suppressing Ghost Diffraction in E-Beam-Written Gratings

Science.gov (United States)

Wilson, Daniel; Backlund, Johan

2009-01-01

A modified scheme for electron-beam (E-beam) writing used in the fabrication of convex or concave diffraction gratings makes it possible to suppress the ghost diffraction heretofore exhibited by such gratings. Ghost diffraction is a spurious component of diffraction caused by a spurious component of grating periodicity as described below. The ghost diffraction orders appear between the main diffraction orders and are typically more intense than is the diffuse scattering from the grating. At such high intensity, ghost diffraction is the dominant source of degradation of grating performance. The pattern of a convex or concave grating is established by electron-beam writing in a resist material coating a substrate that has the desired convex or concave shape. Unfortunately, as a result of the characteristics of electrostatic deflectors used to control the electron beam, it is possible to expose only a small field - typically between 0.5 and 1.0 mm wide - at a given fixed position of the electron gun relative to the substrate. To make a grating larger than the field size, it is necessary to move the substrate to make it possible to write fields centered at different positions, so that the larger area is synthesized by "stitching" the exposed fields.

AFM, SEM and in situ RHEED study of Cu texture evolution on amorphous carbon by oblique angle vapor deposition

International Nuclear Information System (INIS)

Tang, F.; Gaire, C.; Ye, D.-X.; Karabacak, T.; Lu, T.-M.; Wang, G.-C.

2005-01-01

The evolution of the crystal orientation of a Cu film grown on an amorphous carbon substrate without intentional heating under 75±6 deg. oblique angle vapor deposition was investigated ex-situ by atomic force microscopy (AFM) and scanning electron microscopy (SEM), and in-situ by reflection high-energy electron diffraction (RHEED). At the initial stage of growth ( ∼100 nm thick) the diffraction pattern started to break symmetrically from the middle of the (111) and (200) rings representing the absence of (111) and (200) planes parallel to the substrate. However, after this transition stage, at the thickness of ∼410 nm, the intensity distribution of diffraction patterns appeared asymmetric about the middle of the rings, which is interpreted as the appearance of a tilted (111) texture. Finally the diffraction patterns developed into separated short arcs and showed only a II-O (two-orientation) texture. By comparing RHEED patterns with the SEM and AFM images of the final film, we argue that the tilted columns having tilted (111) top faces dominate in the later stage of growth. Furthermore, considering the geometry of crystals and shadowing effects, we argue that the vertices of columns having the highest growth velocity normal to the substrate and therefore receiving the maximum flux will dominate the film growth and determine the tilt angle of the texture and the preference of the azimuthal angle orientation

Structure determination of AgPO3 and (AgPO3)0.5(AgI)0.5 glasses by neutron diffraction and small angle neutron scattering

International Nuclear Information System (INIS)

Tachez, M.; Mercier, R.; Malugani, J.P.; Chieux, P.

1987-01-01

Neutron diffraction and small angle neutron scattering (SANS) were performed on AgPO 3 and (AgPO 3 ) 0.5 (AgI) 0.5 glasses. AgPO 3 glass is made up of long chains of PO 4 tetrahedra joined together by Ag atoms. When silver iodide is added, the radial distribution function shows a large peak at 2.83 A, due to Ag-I interactions. AgI does not modify the network forming unit. The existence of small clusters is confirmed by analysing the coordination number of Ag-I pairs obtained by subtracting the experimental structure function of the AgPO 3 glass from that of the corresponding AgI-doped glasses. A rough estimation of their size is given by SANS experiments. Not all the AgI pairs are involved in AgI cluster units. The compatibility of the results obtained with recent structural investigations by non diffractometric techniques is examined. 23 refs.; 5 figs.; 3 tabs

Photoemission in case of a strongly asymmetric X-ray dinamic diffraction

International Nuclear Information System (INIS)

Kruglov, M.V.; Sazontov, E.A.; Solomin, I.K.

1985-01-01

Possibility has been studied of utilizing strongly asymmet-- ric reflections, in particular in case when the reflected wave slips at a small angle along the surface, for investigating the structural violations of the surface crystal layers. Angular dependence extrinsic photoeffect (ADEP) in the region of X-ray incedence angles close to the Bragg diffraction angle was studied in this paper conformably to crystals with a distorted surface layer. Measurements were conducted with ideal germanium crystals using CuKsub(α) radiation reflections (220) and silicon crystals using CrKsub(α) radiation reflections (22O). It is shown that, in investigating deformed surface layers with low thichkness and large variation of interplanar space, as compared to the basic crystal matric, application of strongly asymmetric reflections anables to increase the sensitivity and information content of the method of abnormal ADEP

Tolerance analysis on diffraction efficiency and polychromatic integral diffraction efficiency for harmonic diffractive optics

Science.gov (United States)

Shan, Mao

2016-10-01

In this dissertation, the mathematical model of effect of manufacturing errors including microstructure relative height error and relative width error on diffraction efficiency for the harmonic diffractive optical elements (HDEs) is set up. According to the expression of the phase delay and diffraction efficiency of the HDEs, the expression of diffraction efficiency of refraction and diffractive optical element with the microstructure height and periodic width errors in fabrication process is presented in this paper. Furthermore, the effect of manufacturing errors on diffraction efficiency for the harmonic diffractive optical elements is studied, and diffraction efficiency change is analyzed as the relative microstructure height-error in the same and in the opposite sign as well as relative width-error in the same and in the opposite sign. Example including infrared wavelength with materials GE has been discussed in this paper. Two kinds of manufacturing errors applied in 3.7 4.3um middle infrared and 8.7-11.5um far infrared optical system which results in diffraction efficiency and PIDE of HDEs are studied. The analysis results can be used for manufacturing error control in micro-structure height and periodic width. Results can be used for HDEs processing.

High-energy coherent terahertz radiation emitted by wide-angle electron beams from a laser-wakefield accelerator

Science.gov (United States)

Yang, Xue; Brunetti, Enrico; Jaroszynski, Dino A.

2018-04-01

High-charge electron beams produced by laser-wakefield accelerators are potentially novel, scalable sources of high-power terahertz radiation suitable for applications requiring high-intensity fields. When an intense laser pulse propagates in underdense plasma, it can generate femtosecond duration, self-injected picocoulomb electron bunches that accelerate on-axis to energies from 10s of MeV to several GeV, depending on laser intensity and plasma density. The process leading to the formation of the accelerating structure also generates non-injected, sub-picosecond duration, 1–2 MeV nanocoulomb electron beams emitted obliquely into a hollow cone around the laser propagation axis. These wide-angle beams are stable and depend weakly on laser and plasma parameters. Here we perform simulations to characterise the coherent transition radiation emitted by these beams if passed through a thin metal foil, or directly at the plasma–vacuum interface, showing that coherent terahertz radiation with 10s μJ to mJ-level energy can be produced with an optical to terahertz conversion efficiency up to 10‑4–10‑3.

Solving crystal structures from neutron diffraction data

International Nuclear Information System (INIS)

Wilson, C.C.

1987-07-01

In order to pursue crystal structure determination using neutron diffraction data, and given the wide experience available of solving structures using X-ray data, the codes used in X-ray structural analysis should be adapted to the different requirements of a neutron experiment. Modifications have been made to a direct methods program MITHRIL and to a Patterson methods program PATMET to incorporate into these the features of neutron rather than X-ray diffraction. While to date these modifications have been fairly straightforward and many sophistications remain to be exploited, results obtained from the neutron versions of both programs are promising. (author)

Odd-order o.d.f. expansion coefficient determination. Case of diffraction strain measurements on cubic materials under macrostress loading

International Nuclear Information System (INIS)

Brakman, C.M.

1985-01-01

Diffraction intensity pole figures are often used for the determination of orientation distribution function (o.d.f.) expansion coefficients. The intensity can be seen as a convolution of the o.d.f. times unity with respect to one rotation angle (about the direction of measurement). The 'normal' polycrystalline diffraction experiment only yields the even-order o.d.f. coefficients. The experiment itself imposes a centre of inversion even upon non-centrosymmetric crystals. Crystals may exhibit a centre of inversion themselves. The hkl and anti hanti kanti l contributions to the intensity are indistinguishable then owing to the centre of inversion. As a consequence, the odd-order coefficients cannot be determined. The mean value of a general physical property determined by means of diffraction can be taken as a convolution of the o.d.f. times the single-crystal value of the physical property with respect to the rotation angle mentioned before. The dependency of the physical property on the rotation angle leads to more information being extracted from the o.d.f. in the property's mean-value pole figure. Then, all o.d.f. coefficients may be present in the mean value, i.e. the measurement. Consequently, diffraction-line-shift strain pole figures exhibit even- and odd-order o.d.f. coefficients, present or induced centres of inversion notwithstanding. If the dependency of the single-crystal strain on the rotation angle is known no model of elastic polycrystal coupling is needed. However, this does not occur in practice. The present state of the art does not allow the Kroener model to be used for textured materials. In this paper the Reuss model is used. If the (applied) macrostresses are known, the o.d.f. coefficients can be obtained from the formulae presented. (orig.)

Crystallographic structures of absorbates and neutron diffraction

International Nuclear Information System (INIS)

Marti, C.; Thorel, P.

1975-01-01

The advantage of neutron diffraction is that it is possible to work at any pressure and therefore to study an adsorbant-adsorbate couple within a wide pressure and temperature range and at thermodynamic equilibrium. Nitrogen adsorbed on graphite and CF 4 adsorbed on graphite were measured [fr

Short-range order in Fe-based metallic glasses: Wide-angle X-ray scattering studies

International Nuclear Information System (INIS)

Babilas, Rafał; Hawełek, Łukasz; Burian, Andrzej

2014-01-01

The local atomic structure of the Fe 80 B 20 , Fe 70 Nb 10 B 20 and Fe 62 Nb 8 B 30 glasses prepared in the form of ribbons has been studied by wide-angle X-ray scattering. Structural information about the amorphous ribbons has been derived from analysis of the radial distribution functions using the least-squares curve-fitting method. The obtained structural parameters indicate that Fe–Fe, Fe–B, Fe–Nb and Nb–B contributions are involved in the near-neighbor coordination spheres. The possible similarities of the local atomic arrangement in the investigated glasses and the crystalline Fe 3 B, Fe 23 B 6 and bcc Fe structures are also discussed. - Graphical abstract: Pair distribution functions (a) and best-fit model and experimental radial distribution functions for Fe 80 B 20 (b), Fe 70 Nb 10 B 20 (c) and Fe 62 Nb 8 B 30 (d) metallic glasses. - Highlights: • The short-range ordering in the Fe-based metallic glasses is presented. • The results of RDF function have been analyzed using the least-squares method. • The Fe–Fe, Fe–B, Fe–Nb or Nb–B contributions are involved in coordination spheres. • The structural unit is distorted triangular prism containing B, Fe or Nb atoms. • Similarities of atomic arrangement in glassy and crystalline structures are discussed

Microstructural parameters in 8 MeV Electron irradiated Bombyx mori silk fibers by wide-angle X-ray scattering studies (WAXS)

International Nuclear Information System (INIS)

Halabhavi, Sangappa

2009-01-01

The present work looks into the microstructural modification in Bombyx mori silk fibers, induced by electron irradiation. The irradiation process was performed in air at room temperature by use of 8 MeV electron accelerators at different doses: 0, 25, 50, 75 and 100 kGy respectively. Irradiation of polymer can be used to crosslink or degrade the desired component or to fixate the polymer morphology. The changes in microstructural parameters in these natural polymer fibers have been studied using wide angle X-ray scattering (WAXS) method. The crystal imperfection parameters such as crystallite size , lattice strain (g in %) and enthalpy (a * ) have been determined by line profile analysis (LPA) using Fourier method of Warren. Exponential, Lognormal and Reinhold functions for the column length distributions have been used for the determination of these parameters. The goodness of the fit and the consistency of these results suggest that the exponential distribution gives much better results, even though lognormal distribution has been widely used to estimate the similar stacking faults in metal oxide compounds. (author)

Microstructural Parameters in 8 MeV Electron-Irradiated BOMBYX MORI Silk Fibers by Wide-ANGLE X-Ray Scattering Studies (waxs)

Science.gov (United States)

Sangappa, Asha, S.; Sanjeev, Ganesh; Subramanya, G.; Parameswara, P.; Somashekar, R.

2010-01-01

The present work looks into the microstructural modification in electron irradiated Bombyx mori P31 silk fibers. The irradiation process was performed in air at room temperature using 8 MeV electron accelerator at different doses: 0, 25, 50 and 100 kGy. Irradiation of polymer is used to cross-link or degrade the desired component or to fix the polymer morphology. The changes in microstructural parameters in these natural polymer fibers have been computed using wide angle X-ray scattering (WAXS) data and employing line profile analysis (LPA) using Fourier transform technique of Warren. Exponential, Lognormal and Reinhold functions for the column length distributions have been used for the determination of crystal size, lattice strain and enthalpy parameters.

Quantitative angle-insensitive flow measurement using relative standard deviation OCT.

Science.gov (United States)

Zhu, Jiang; Zhang, Buyun; Qi, Li; Wang, Ling; Yang, Qiang; Zhu, Zhuqing; Huo, Tiancheng; Chen, Zhongping

2017-10-30

Incorporating different data processing methods, optical coherence tomography (OCT) has the ability for high-resolution angiography and quantitative flow velocity measurements. However, OCT angiography cannot provide quantitative information of flow velocities, and the velocity measurement based on Doppler OCT requires the determination of Doppler angles, which is a challenge in a complex vascular network. In this study, we report on a relative standard deviation OCT (RSD-OCT) method which provides both vascular network mapping and quantitative information for flow velocities within a wide range of Doppler angles. The RSD values are angle-insensitive within a wide range of angles, and a nearly linear relationship was found between the RSD values and the flow velocities. The RSD-OCT measurement in a rat cortex shows that it can quantify the blood flow velocities as well as map the vascular network in vivo .

Atomic scattering in the diffraction limit: electron transfer in keV Li+-Na(3s, 3p) collisions

International Nuclear Information System (INIS)

Poel, M van der; Nielsen, C V; Rybaltover, M; Nielsen, S E; Machholm, M; Andersen, N

2002-01-01

We measure angle differential cross sections (DCS) in Li + + Na → Li + Na + electron transfer collisions in the 2.7-24 keV energy range. We do this with a newly constructed apparatus which combines the experimental technique of cold target recoil ion momentum spectroscopy with a laser-cooled target. This setup yields a momentum resolution of 0.12 au, an order of magnitude better angular resolution than previous measurements on this system. This enables us to clearly resolve Fraunhofer-type diffraction patterns in the angle DCS. In particular, the angular width of the ring structure is given by the ratio of the de Broglie wavelength λ dB = 150 fm at a velocity v = 0.20 au and the effective atomic diameter for electron capture 2R = 20 au. Parallel AO and MO semiclassical coupled-channel calculations of the Na(3s, 3p) → Li(2s, 2p) state-to-state collision amplitudes have been performed, and quantum scattering amplitudes are derived by the eikonal method. The resulting angle-differential electron transfer cross sections and their diffraction patterns agree with the experimental level-to-level results over most scattering angles in the energy range

Exact solution for four-order acousto-optic Bragg diffraction with arbitrary initial conditions.

Science.gov (United States)

Pieper, Ron; Koslover, Deborah; Poon, Ting-Chung

2009-03-01

An exact solution to the four-order acousto-optic (AO) Bragg diffraction problem with arbitrary initial conditions compatible with exact Bragg angle incident light is developed. The solution, obtained by solving a 4th-order differential equation, is formalized into a transition matrix operator predicting diffracted light orders at the exit of the AO cell in terms of the same diffracted light orders at the entrance. It is shown that the transition matrix is unitary and that this unitary matrix condition is sufficient to guarantee energy conservation. A comparison of analytical solutions with numerical predictions validates the formalism. Although not directly related to the approach used to obtain the solution, it was discovered that all four generated eigenvalues from the four-order AO differential matrix operator are expressed simply in terms of Euclid's Divine Proportion.

Crustal Deformation In the Northwestern Margin of the South China Sea: Results From Wide-angle Seismic Modeling

Science.gov (United States)

Huang, H.; Klingelhoefer, F.

2017-12-01

The South China Sea (SCS) has undergone episodic spreading during the Cenozoic Era. The long-term extension has shaped the continental margins of the SCS, leading to a progressive breakup of the lithosphere. Separated blocks and rift troughs, as controlled by tectonic stretching, contains key information about the deforming mechanism of the crust. In this work, we present a P-wave velocity model of a wide-angle seismic profile OBS2013-1 which passes through the NW margin of the SCS. Modeling of 25 ocean bottom seismometers (OBS) data revealed a detailed crustal structure and shallow complexities along the profile (Figure 1). The crust thins symmetrically across the Xisha Trough, from more than 20 km on flanks to 10 km in the central valley where the sediments thickens over 5 km; A volcano is situated on top of the centre basement high where the Moho drops slightly. At the distal margin around the Zhongsha Trough, the upper crust was detached and accordingly made the middle crust exhumed in a narrow area ( 20 km wide). Meanwhile, materials from the lower crust rises asymmetrically, increasing the crustal velocity by 0.3 km/s and may also giving rise to volcanisms along the hanging side. A 40 km wide hyper-stretched crust (with thickness of 5 km) was identified next to the Zhongsha Trough and covered by overflowing magma and post-rift sediments on the top. These observations argue for a depth-related and asymmetrically extension of the crust, including (1) detachment fault controls the deformation of the upper crust, leading to exhumation of the middle crust and asymmetrically rising of the lower crust, (2) The region adjacent to the exhumation region and with highly thinned crust can be considered as extinct OCT due to magma-starved supplying.

Anomalously-dense firn in an ice-shelf channel revealed by wide-angle radar

Science.gov (United States)

Drews, R.; Brown, J.; Matsuoka, K.; Witrant, E.; Philippe, M.; Hubbard, B.; Pattyn, F.

2015-10-01

The thickness of ice shelves, a basic parameter for mass balance estimates, is typically inferred using hydrostatic equilibrium for which knowledge of the depth-averaged density is essential. The densification from snow to ice depends on a number of local factors (e.g. temperature and surface mass balance) causing spatial and temporal variations in density-depth profiles. However, direct measurements of firn density are sparse, requiring substantial logistical effort. Here, we infer density from radio-wave propagation speed using ground-based wide-angle radar datasets (10 MHz) collected at five sites on Roi Baudouin Ice Shelf (RBIS), Dronning Maud Land, Antarctica. Using a novel algorithm including traveltime inversion and raytracing with a prescribed shape of the depth-density relationship, we show that the depth to internal reflectors, the local ice thickness and depth-averaged densities can reliably be reconstructed. For the particular case of an ice-shelf channel, where ice thickness and surface slope change substantially over a few kilometers, the radar data suggests that firn inside the channel is about 5 % denser than outside the channel. Although this density difference is at the detection limit of the radar, it is consistent with a similar density anomaly reconstructed from optical televiewing, which reveals 10 % denser firn inside compared to outside the channel. The denser firn in the ice-shelf channel should be accounted for when using the hydrostatic ice thickness for determining basal melt rates. The radar method presented here is robust and can easily be adapted to different radar frequencies and data-acquisition geometries.

The ITER Equatorial Visible/Infra-Red Wide Angle Viewing System: Status of design and R&D

Energy Technology Data Exchange (ETDEWEB)

Salasca, Sophie, E-mail: sophie.salasca@cea.fr [CEA, IRFM, F-13108 Saint-Paul-lez-Durance (France); Aumeunier, Marie-Helene; Benoit, Fabrice; Cantone, Bruno; Corre, Yann; Delchambre, Elise; Ferlet, Marc; Gauthier, Eric; Guillon, Christophe; Houtte, Didier van; Keller, Delphine; Labasse, Florence; Larroque, Sebastien; Loarer, Thierry; Micolon, Frederic; Peluso, Bertrand; Proust, Maxime [CEA, IRFM, F-13108 Saint-Paul-lez-Durance (France); Blanchet, David; Peneliau, Yannick [CEA, DEN/DER, F-13108 Saint-Paul-lez-Durance (France); Alonso, Javier [CIEMAT, Avda. Complutense, 40, Madrid 28040 (Spain); and others

2015-10-15

Highlights: • The status of Equatorial Visible/Infra-Red Wide Angle Viewing System is presented. • An assessment of measurement parameters relevant for machine protection has been done. • Remaining uncertainties will be clarified during the System Level Design (SLD). • WAVS design is not considered mature enough to launch prototypes of subcomponents. • Mandatory prototypes and qualification tests are already identified. • Next stage (SLD) will enable to do trade-offs and address pending design issues. - Abstract: The Equatorial Visible/Infra-Red Wide Angle Viewing System (WAVS) is one of the ITER key diagnostics owing to its role in machine investment protection through the monitoring of Plasma Facing Components (PFCs) by Infra-Red thermography and visible imaging. Foreseen to be installed in 4 equatorial port plugs to maximize the coverage of divertor, first wall, heating antennas and upper strike zone, the WAVS will likely be composed of 15 lines of sight and 15 optical systems transferring the light along several meters from the PFCs through the port plug and interspace up to detectors located in the port cell. After a conceptual design phase led by ITER Organization, the design is being further developed through a Framework Partnership Agreement signed between the European Domestic Agency, Fusion for Energy, and a consortium gathering CEA, CIEMAT (with INTA as third party) and Bertin Technologies company. The next design step is the System Level Design (SLD) which will enable to consolidate the WAVS specifications as well as the performance realistically achievable (taking into account ITER and project constraints). The SLD has been preceded by a preparatory phase aiming at clarifying the WAVS functions and identifying critical prototyping. The outcomes of this preparatory phase are reported in this paper. First a review by the consortium of the WAVS measurement specifications is presented, for the purpose of a clearer separation of measurement

Industrial applications of neutron diffraction

International Nuclear Information System (INIS)

Felcher, G.P.

1989-01-01

Neutron diffraction (or, to be more general, neutron scattering) is a most versatile and universal tool, which has been widely employed to probe the structure, the dynamics and the magnetism of condensed matter. Traditionally used for fundamental research in solid state physics, this technique more recently has been applied to problems of immediate industrial interest, as illustrated in examples covering the main fields of endeavour. 14 refs., 14 figs

Study on guided-mode resonance characteristic of multilayer dielectric grating with broadband and wide using-angle

International Nuclear Information System (INIS)

Jian-Peng, Wang; Yun-Xia, Jin; Jian-Yong, Ma; Jian-Da, Shao; Zheng-Xiu, Fan

2010-01-01

Guided-mode resonance in a diffraction band of multilayer dielectric gratings may lead to a catastrophic result in laser system, especially in the ultrashort pulse laser system, so the inhibition of guided-mode resonance is very important. In this paper the characteristics of guided-mode resonance in multilayer dielectric grating are studied with the aim of better understanding the physical process of guided-mode resonance and designing a broadband multilayer dielectric grating with no guided-mode resonance. By employing waveguide theory, all guided-wave modes appearing in multilayer dielectric grating are found, and the incident conditions, separately, corresponding to each guided-wave mode are also obtained. The electric field enhancement in multilayer dielectric grating is shown obviously. Furthermore, from the detailed analyses on the guided-mode resonance conditions, it is found that the reduction of the grating period would effectively avoid the appearing of guided-mode resonance. And the expressions for calculating maximum periods, which ensure that no guided-mode resonance occurs in the requiring broad angle or wavelength range, are first reported. The above results calculated by waveguide theory and Fourier mode method are compared with each other, and they are coincident completely. Moreover, the method that relies on waveguide theory is more helpful for understanding the guided-mode resonance excited process and analyzing how each parameter affects the characteristic of guided-mode resonance. Therefore, the effects of multilayer dielectric grating parameters, such as period, fill factor, thickness of grating layer, et al., on the guided-mode resonance characteristic are discussed in detail based on waveguide theory, and some meaningful results are obtained. (classical areas of phenomenology)

Effects of Rayleigh damping, friction and rate-dependency on 3D residual stress simulation of angled shot peening

International Nuclear Information System (INIS)

Kim, Taehyung; Lee, Hyungyil; Hyun, Hong Chul; Jung, Sunghwan

2013-01-01

Highlights: ► We propose a 3D FE model to study peening residual stress involving angled shots. ► The FE model set with plastic shot are found to best match the X-ray diffraction data. ► The model provides 3D multi-shot impact FE solution with various incidence angles. - Abstract: In this study, we propose a 3D finite element (FE) model to study shot peening involving angled shots. Using the FE model for angled shot peening, we examine relationships with the residual stress introduced by shot peening of the factors such as the Rayleigh damping in the material, dynamic friction, and the rate dependency of the material and systematically integrate them with the FE model. The FE model is set with rigid shot, elastic shot, and plastic shot respectively. Plastic deformation of the shot is also explored with the FE model. The FE model is applied to study angled multi-shots. The FE results are verified with experimental data using X-ray diffraction (XRD). The FE model set with plastic shot are found to best match the XRD results validating accuracy of the 3D FE model properly integrated with the factors and plastically deformable shot ball. The proposed model will serve to simulate actual shot peening cases, which generally involve multi-shots with various incidence angles

Versatile application of indirect Fourier transformation to structure factor analysis: from X-ray diffraction of molecular liquids to small angle scattering of protein solutions.

Science.gov (United States)

Fukasawa, Toshiko; Sato, Takaaki

2011-02-28

We highlight versatile applicability of a structure-factor indirect Fourier transformation (IFT) technique, hereafter called SQ-IFT. The original IFT aims at the pair distance distribution function, p(r), of colloidal particles from small angle scattering of X-rays (SAXS) and neutrons (SANS), allowing the conversion of the experimental form factor, P(q), into a more intuitive real-space spatial autocorrelation function. Instead, SQ-IFT is an interaction potential model-free approach to the 'effective' or 'experimental' structure factor to yield the pair correlation functions (PCFs), g(r), of colloidal dispersions like globular protein solutions for small-angle scattering data as well as the radial distribution functions (RDFs) of molecular liquids in liquid diffraction (LD) experiments. We show that SQ-IFT yields accurate RDFs of liquid H(2)O and monohydric alcohol reflecting their local intermolecular structures, in which q-weighted structure function, qH(q), conventionally utilized in many LD studies out of necessity of performing direct Fourier transformation, is no longer required. We also show that SQ-IFT applied to theoretically calculated structure factors for uncharged and charged colloidal dispersions almost perfectly reproduces g(r) obtained as a solution of the Ornstein-Zernike (OZ) equation. We further demonstrate the relevance of SQ-IFT in its practical applications, using SANS effective structure factors of lysozyme solutions reported in recent literatures which revealed the equilibrium cluster formation due to coexisting long range electrostatic repulsion and short range attraction between the proteins. Finally, we present SAXS experiments on human serum albumin (HSA) at different ionic strength and protein concentration, in which we discuss the real space picture of spatial distributions of the proteins via the interaction potential model-free route.

Production of exclusive dijets in diffractive deep inelastic scattering at HERA

Energy Technology Data Exchange (ETDEWEB)

Abramowicz, H.; Gueta, O.; Kananov, S.; Levy, A.; Stern, A. [Tel Aviv University, Raymond and Beverly Sackler Faculty of Exact Sciences, School of Physics, Tel Aviv (Israel); Abt, I.; Caldwell, A.; Schmidke, W.B.; Verbytskyi, A. [Max-Planck-Institut fuer Physik, Munich (Germany); Adamczyk, L.; Gach, G.; Guzik, M.; Kisielewska, D.; Przybycien, M. [AGH-University of Science and Technology, Faculty of Physics and Applied Computer Science, Krakow (Poland); Adamus, M.; Tymieniecka, T. [National Centre for Nuclear Research, Warsaw (Poland); Antonelli, S. [University, Bologna (Italy); INFN Bologna, Bologna (Italy); Aushev, V. [National Academy of Sciences, Institute for Nuclear Research, Kiev (Ukraine); National Taras Shevchenko University of Kyiv, Department of Nuclear Physics, Kiev (Ukraine); Aushev, Y.; Iudin, A.; Kadenko, I.; Kondrashova, N.; Kononenko, O.; Onishchuk, Yu.; Shevchenko, R.; Shkola, O.; Trofymov, A.; Viazlo, O.; Zakharchuk, N. [National Taras Shevchenko University of Kyiv, Department of Nuclear Physics, Kiev (Ukraine); Behnke, O.; Behrens, U.; Borras, K.; Ciesielski, R.; Dolinska, G.; Geiser, A.; Gizhko, A.; Grebenyuk, J.; Gregor, I.; Hain, W.; Januschek, F.; Klein, U.; Korol, I.; Koetz, U.; Kowalski, H.; Kuprash, O.; Libov, V.; Lisovyi, M.; Lobodzinska, E.; Loehr, B.; Lontkovskyi, D.; Makarenko, I.; Malka, J.; Myronenko, V.; Notz, D.; Roloff, P.; Rubinsky, I.; Schneekloth, U.; Schoerner-Sadenius, T.; Stefaniuk, N.; Szuba, J.; Turkot, O.; Wichmann, K.; Wolf, G.; Zenaiev, O. [Deutsches Elektronen-Synchrotron DESY, Hamburg (Germany); Bertolin, A.; Dusini, S.; Longhin, A.; Stanco, L. [INFN Padova, Padua (Italy); Bloch, I. [Deutsches Elektronen-Synchrotron DESY, Zeuthen (Germany); Boos, E.G.; Pokrovskiy, N.S.; Zhautykov, B.O. [Institute of Physics and Technology of Ministry of Education and Science of Kazakhstan, Almaty (Kazakhstan); Brock, I.; Mergelmeyer, S.; Paul, E. [Physikalisches Institut der Universitaet Bonn, Bonn (Germany); Brook, N.H.; Wing, M. [University College London, Physics and Astronomy Department, London (United Kingdom); Brugnera, R.; Garfagnini, A.; Limentani, S. [Dipartimento di Fisica e Astronomia, Univ., Padua (Italy); INFN, Padua (Italy); Bruni, A.; Corradi, M. [INFN Bologna, Bologna (Italy); Bussey, P.J.; Saxon, D.H.; Skillicorn, I.O. [University of Glasgow, School of Physics and Astronomy, Glasgow (United Kingdom); Capua, M.; Schioppa, M.; Tassi, E. [Calabria University, Physics Department, Cosenza (Italy); INFN, Cosenza (Italy); Catterall, C.D. [York University, Department of Physics, Ontario (Canada); Chwastowski, J.; Figiel, J.; Krupa, B.; Stopa, P.; Zawiejski, L. [Polish Academy of Sciences, The Henryk Niewodniczanski Institute of Nuclear Physics, Krakow (Poland); Ciborowski, J.; Grzelak, G.; Nowak, R.J.; Perlanski, W.; Tomaszewska, J.; Zarnecki, A.F. [University of Warsaw, Faculty of Physics, Warsaw (Poland); Cooper-Sarkar, A.M.; Devenish, R.C.E.; Walczak, R. [University of Oxford, Department of Physics, Oxford (United Kingdom); Corriveau, F. [McGill University, Department of Physics, Montreal, Quebec (Canada); Dementiev, R.K.; Gladilin, L.K.; Golubkov, Yu.A.; Korzhavina, I.A.; Levchenko, B.B.; Lukina, O.Yu.; Shcheglova, L.M.; Zotkin, D.S. [Lomonosov Moscow State University, Skobeltsyn Institute of Nuclear Physics, Moscow (Russian Federation); Foster, B.; Gallo, E.; Klanner, R.; Kovalchuk, N.; Lohrmann, E.; Sztuk-Dambietz, J.; Szuba, D.; Turcato, M. [Hamburg University, Institute of Experimental Physics, Hamburg (Germany); Hochman, D.; Karshon, U. [Weizmann Institute, Department of Particle Physics and Astrophysics, Rehovot (Israel); Hori, R.; Nagano, K.; Tokushuku, K.; Yamada, S.; Yamazaki, Y. [Institute of Particle and Nuclear Studies, KEK, Tsukuba (Japan); Ibrahim, Z.A.; Jomhari, N.Z.; Mohamad Idris, F.; Mohammad Nasir, N.; Wan Abdullah, W.A.T. [Universiti Malaya, National Centre for Particle Physics, Kuala Lumpur (Malaysia); Iga, Y. [Polytechnic University, Tokyo (Japan); Ishitsuka, M.; Kuze, M.; Nobe, T. [Tokyo Institute of Technology, Department of Physics, Tokyo (JP); Kaur, M.; Kaur, P.; Singh, I. [Panjab University, Department of Physics, Chandigarh (IN); Kotanski, A.; Slominski, W. [Jagellonian University, Department of Physics, Krakow (PL); Ruspa, M. [Universita del Piemonte Orientale, Novara (IT); INFN, Turin (IT); Shyrma, Yu.; Zhmak, N. [National Academy of Sciences, Institute for Nuclear Research, Kiev (UA); Solano, A. [Universita di Torino (IT); INFN, Turin (IT); Tsurugai, T. [Meiji Gakuin University, Faculty of General Education, Yokohama (JP); Collaboration: ZEUS Collaboration

2016-01-15

Production of exclusive dijets in diffractive deep inelastic e{sup ±}p scattering has been measured with the ZEUS detector atHERAusing an integrated luminosity of 372 pb{sup -1}. The measurement was performed for γ* - p centre-of-mass energies in the range 90 < W < 250 GeV and for photon virtualities Q{sup 2} > 25 GeV{sup 2}. Energy flows around the jet axis are presented. The cross section is presented as a function of β and φ, where β = x/x{sub P}, x is the Bjorken variable and x{sub P} is the proton fractional longitudinal momentum loss. The angle φ is defined by the γ*-dijet plane and the γ*-e{sup ±} plane in the rest frame of the diffractive final state. The φ cross section is measured in bins of β. The results are compared to predictions from models based on different assumptions about the nature of the diffractive exchange. (orig.)

Production of exclusive dijets in diffractive deep inelastic scattering at HERA

International Nuclear Information System (INIS)

Abramowicz, H.; Abt, I.; Adamczyk, L.

2015-05-01

Production of exclusive dijets in diffractive deep inelastic e ± p scattering has been measured with the ZEUS detector at HERA using an integrated luminosity of 372 pb -1 . The measurement was performed for γ * -p centre-of-mass energies in the range 9025 GeV 2 . Energy and transverse-energy flows around the jet axis are presented. The cross section is presented as a function of β and φ, where β=x/x P , x is the Bjorken variable and x P is the proton fractional longitudinal momentum loss. The angle φ is defined by the γ * -dijet plane and the γ * -e ± plane in the rest frame of the diffractive final state. The φ cross section is measured in bins of β. The results are compared to predictions from models based on different assumptions about the nature of the diffractive exchange.

Understanding deformation with high angular resolution electron backscatter diffraction (HR-EBSD)

Science.gov (United States)

Britton, T. B.; Hickey, J. L. R.

2018-01-01

High angular resolution electron backscatter diffraction (HR-EBSD) affords an increase in angular resolution, as compared to ‘conventional’ Hough transform based EBSD, of two orders of magnitude, enabling measurements of relative misorientations of 1 x 10-4 rads (~ 0.006°) and changes in (deviatoric) lattice strain with a precision of 1 x 10-4. This is achieved through direct comparison of two or more diffraction patterns using sophisticated cross-correlation based image analysis routines. Image shifts between zone axes in the two-correlated diffraction pattern are measured with sub-pixel precision and this realises the ability to measure changes in interplanar angles and lattice orientation with a high degree of sensitivity. These shifts are linked to strains and lattice rotations through simple geometry. In this manuscript, we outline the basis of the technique and two case studies that highlight its potential to tackle real materials science challenges, such as deformation patterning in polycrystalline alloys.

Production of exclusive dijets in diffractive deep inelastic scattering at HERA

International Nuclear Information System (INIS)

Abramowicz, H.; Gueta, O.; Kananov, S.; Levy, A.; Stern, A.; Abt, I.; Caldwell, A.; Schmidke, W.B.; Verbytskyi, A.; Adamczyk, L.; Gach, G.; Guzik, M.; Kisielewska, D.; Przybycien, M.; Adamus, M.; Tymieniecka, T.; Antonelli, S.; Aushev, V.; Aushev, Y.; Iudin, A.; Kadenko, I.; Kondrashova, N.; Kononenko, O.; Onishchuk, Yu.; Shevchenko, R.; Shkola, O.; Trofymov, A.; Viazlo, O.; Zakharchuk, N.; Behnke, O.; Behrens, U.; Borras, K.; Ciesielski, R.; Dolinska, G.; Geiser, A.; Gizhko, A.; Grebenyuk, J.; Gregor, I.; Hain, W.; Januschek, F.; Klein, U.; Korol, I.; Koetz, U.; Kowalski, H.; Kuprash, O.; Libov, V.; Lisovyi, M.; Lobodzinska, E.; Loehr, B.; Lontkovskyi, D.; Makarenko, I.; Malka, J.; Myronenko, V.; Notz, D.; Roloff, P.; Rubinsky, I.; Schneekloth, U.; Schoerner-Sadenius, T.; Stefaniuk, N.; Szuba, J.; Turkot, O.; Wichmann, K.; Wolf, G.; Zenaiev, O.; Bertolin, A.; Dusini, S.; Longhin, A.; Stanco, L.; Bloch, I.; Boos, E.G.; Pokrovskiy, N.S.; Zhautykov, B.O.; Brock, I.; Mergelmeyer, S.; Paul, E.; Brook, N.H.; Wing, M.; Brugnera, R.; Garfagnini, A.; Limentani, S.; Bruni, A.; Corradi, M.; Bussey, P.J.; Saxon, D.H.; Skillicorn, I.O.; Capua, M.; Schioppa, M.; Tassi, E.; Catterall, C.D.; Chwastowski, J.; Figiel, J.; Krupa, B.; Stopa, P.; Zawiejski, L.; Ciborowski, J.; Grzelak, G.; Nowak, R.J.; Perlanski, W.; Tomaszewska, J.; Zarnecki, A.F.; Cooper-Sarkar, A.M.; Devenish, R.C.E.; Walczak, R.; Corriveau, F.; Dementiev, R.K.; Gladilin, L.K.; Golubkov, Yu.A.; Korzhavina, I.A.; Levchenko, B.B.; Lukina, O.Yu.; Shcheglova, L.M.; Zotkin, D.S.; Foster, B.; Gallo, E.; Klanner, R.; Kovalchuk, N.; Lohrmann, E.; Sztuk-Dambietz, J.; Szuba, D.; Turcato, M.; Hochman, D.; Karshon, U.; Hori, R.; Nagano, K.; Tokushuku, K.; Yamada, S.; Yamazaki, Y.; Ibrahim, Z.A.; Jomhari, N.Z.; Mohamad Idris, F.; Mohammad Nasir, N.; Wan Abdullah, W.A.T.; Iga, Y.; Ishitsuka, M.; Kuze, M.; Nobe, T.; Kaur, M.; Kaur, P.; Singh, I.; Kotanski, A.; Slominski, W.; Ruspa, M.; Shyrma, Yu.; Zhmak, N.; Solano, A.; Tsurugai, T.

2016-01-01

Production of exclusive dijets in diffractive deep inelastic e ± p scattering has been measured with the ZEUS detector atHERAusing an integrated luminosity of 372 pb -1 . The measurement was performed for γ* - p centre-of-mass energies in the range 90 < W < 250 GeV and for photon virtualities Q 2 > 25 GeV 2 . Energy flows around the jet axis are presented. The cross section is presented as a function of β and φ, where β = x/x P , x is the Bjorken variable and x P is the proton fractional longitudinal momentum loss. The angle φ is defined by the γ*-dijet plane and the γ*-e ± plane in the rest frame of the diffractive final state. The φ cross section is measured in bins of β. The results are compared to predictions from models based on different assumptions about the nature of the diffractive exchange. (orig.)

Linear systems formulation of scattering theory for rough surfaces with arbitrary incident and scattering angles.

Science.gov (United States)

Krywonos, Andrey; Harvey, James E; Choi, Narak

2011-06-01

Scattering effects from microtopographic surface roughness are merely nonparaxial diffraction phenomena resulting from random phase variations in the reflected or transmitted wavefront. Rayleigh-Rice, Beckmann-Kirchhoff. or Harvey-Shack surface scatter theories are commonly used to predict surface scatter effects. Smooth-surface and/or paraxial approximations have severely limited the range of applicability of each of the above theoretical treatments. A recent linear systems formulation of nonparaxial scalar diffraction theory applied to surface scatter phenomena resulted first in an empirically modified Beckmann-Kirchhoff surface scatter model, then a generalized Harvey-Shack theory that produces accurate results for rougher surfaces than the Rayleigh-Rice theory and for larger incident and scattered angles than the classical Beckmann-Kirchhoff and the original Harvey-Shack theories. These new developments simplify the analysis and understanding of nonintuitive scattering behavior from rough surfaces illuminated at arbitrary incident angles.

Single shot diffraction of picosecond 8.7-keV x-ray pulses

Directory of Open Access Journals (Sweden)

F. H. O’Shea

2012-02-01

Full Text Available We demonstrate multiphoton, single shot diffraction images of x rays produced by inverse Compton scattering a high-power CO_{2} laser from a relativistic electron beam, creating a pulse of 8.7 keV x rays. The tightly focused, relatively high peak brightness electron beam and high photon density from the 2 J CO_{2} laser yielded 6×10^{7} x-ray photons over the full opening angle in a single shot. Single shot x-ray diffraction is performed by passing the x rays though a vertical slit and on to a flat silicon (111 crystal. 10^{2} diffracted photons were detected. The spectrum of the detected x rays is compared to simulation. The diffraction and detection of 10^{2} x rays is a key step to a more efficient time resolved diagnostic in which the number of observed x rays might reach 10^{4}; enabling a unique, flexible x-ray source as a sub-ps resolution diagnostic for studying the evolution of chemical reactions, lattice deformation and melting, and magnetism.

Holographic diffraction gratings as laser radiation protection filters

International Nuclear Information System (INIS)

Pantelic, D.; Pantelic, G.

2006-01-01

Holographic volume diffraction gratings are used as attenuation filters, due to their selective spectral transmission. They can be tailored to reflect or transmit narrow spectral ranges by adjusting spatial frequency of Bragg grating in carefully chosen photosensitive materials, like silver-halide emulsion or di-chromated gelatin layers. If properly recorded and chemically processed, resulting gratings can significantly attenuate light at wavelengths corresponding to various laser spectral lines. Thus, they can be used as filters in laser protection goggles. We analyze the characteristics of Bragg gratings necessary to obtain high attenuation coefficients. Also, their angular selectivity is taken into account and corresponding experimental conditions are investigated. Although di-chromated gelatin seems to be almost ideal material, due to its almost 100% diffraction efficiency, environmental stability is poor (degradation under humid environment), thus making its practical usage difficult. Thus, we have analyzed alternative materials like di-chromated pullulan, which is stable under normal environmental conditions (without drop in diffraction efficiency after prolonged exposure to humidity). Pullulan is polymer (polysaccharide) of biologic origin produced by certain bacteria. If doped with chromium ions it becomes photosensitive, enabling recording of diffraction gratings with spatial frequency of more than 3000 lines/mm. Material is chemically processed by mixture of isopropyl alcohol and water. Both thick and thin layers can be produced by gravity settling. Spectral properties of resulting gratings are analyzed, showing that they can significantly attenuate laser light of particular wavelength, depending of grating period and its slant angle. (authors)

Effects of pressure and temperature on pore structure of ceramic synthesized from rice husk: A small angle neutron scattering investigation

Energy Technology Data Exchange (ETDEWEB)

Raut Dessai, R., E-mail: reshooin@yahoo.com [Department of Physics, Goa University, Taleigao Plateau, Goa 403 206 (India); Desa, J.A.E. [Department of Physics, Goa University, Taleigao Plateau, Goa 403 206 (India); Sen, D.; Mazumder, S. [Solid State Physics Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400 085 (India)

2013-07-05

Highlights: ► A porous ceramic has been prepared from silica obtained from rice husk. ► The ceramic has a hierarchical pore structure from micrometric to nano-metric. ► Small Angle Neutron Scattering data indicate nano-pore connectivity to micro-pores. ► Pore morphology can be tuned by compaction pressure and sintering temperature. -- Abstract: Ceramic powder has been synthesized from rice husk as the source of silica. In order to probe the evolution of its hierarchical mesoscopic and microscopic porous structure, the ceramic powder was compacted at different pressures and was sintered at different temperatures. A glassy ceramic to crystalline transition under thermal treatment (up to 1000 °C) was revealed by X-ray diffraction. Existence of pores in two widely separated length scales was indicated by small angle neutron scattering with the smaller ones having mass fractal arrangement. Although no significant change in small pore structure under thermal effect was indicated, a significant modification of the same has been revealed by small angle neutron scattering at different compaction pressures. Connectivity between the pores was ascertained from scattering experiments on the ceramic compact impregnated with heavy water. Scanning electron microscopy shows the microstructure to undergo appreciable coalescence of micrometric ceramic particles for sintering temperature and pressure changes.

Wide-Area Assessment of Aperiodic Small Signal Rotor Angle Stability in Real-Time

DEFF Research Database (Denmark)

Jóhannsson, Hjörtur; Nielsen, Arne Hejde; Østergaard, Jacob

2014-01-01

in rotor angle and a loss of synchronism, referred to as aperiodic small signal instability. The paper provides the theoretical background of the method and an analytical assessment criterion. Furthermore, a mathematical mapping of the generators' operating points that enables informative visualization...

X-ray and neutron diffraction studies of crystallinity in hydroxyapatite coatings.

Science.gov (United States)

Girardin, E; Millet, P; Lodini, A

2000-02-01

To standardize industrial implant production and make comparisons between different experimental results, we have to be able to quantify the crystallinity of hydroxyapatite. Methods of measuring crystallinity ratio were developed for various HA samples before and after plasma spraying. The first series of methods uses X-ray diffraction. The advantage of these methods is that X-ray diffraction equipment is used widely in science and industry. In the second series, a neutron diffraction method is developed and the results recorded are similar to those obtained by the modified X-ray diffraction methods. The advantage of neutron diffraction is the ability to obtain measurements deep inside a component. It is a nondestructive method, owing to the very low absorption of neutrons in most materials. Copyright 2000 John Wiley & Sons, Inc.

Spectroscopic and X-ray Diffraction Study of Structural Disorder in Cryomilled and Amorphous Griseofulvin

International Nuclear Information System (INIS)

Zarow, A.; Zhou, B.; Wang, X.; Pinal, R.; Iqbal, Z.

2011-01-01

Structural disorder induced by cryogenic milling and by heating to the amorphous phase in the active pharmaceutical ingredient Griseofulvin has been studied using Raman spectroscopy, X-ray powder diffraction (XRPD), and fluorescence spectroscopy. A broad, exciting-frequency-independent scattering background in the Raman spectra and changes in intensities and splitting of some of the Raman lines due to lattice and molecular modes have been observed. In the cryomilled samples this strong background is deconvoluted into two components: one due to lattice disorder induced by cryomilling and the other due to Mie scattering from nanosized crystallites. A single-component background scattering attributed to lattice disorder is seen in the Raman spectrum of the amorphous sample. Fluorescence measurements showed an intrinsic fluorescence signal in as-received Griseofulvin that does not correspond to the inelastic background in the Raman spectra and, moreover, decreases in intensity upon cryomilling, thus excluding an assignment of the Raman background intensity to impurity- or molecular-defect-induced fluorescence. Wide-angle XRPD measurements on cryomilled Griseofulvin shows a broad two-component background consistent with the background-scattering component in the Raman data associated with lattice disorder, but at longer correlation lengths. Persistence of this disorder to even longer lengths is evident in small-angle synchrotron XRPD data on micronized Griseofulvin taken as a function of temperature from the crystalline to the amorphous phase.

Spatial and spectral image distortions caused by diffraction of an ordinary polarised light beam by an ultrasonic wave

Energy Technology Data Exchange (ETDEWEB)

Machikhin, A S; Pozhar, V E [Scientific and Technological Centre of Unique Instrumentation, Russian Academy of Sciences, Moscow (Russian Federation)

2015-02-28

We consider the problem of determining the spatial and spectral image distortions arising from anisotropic diffraction by ultrasonic waves in crystals with ordinary polarised light (o → e). By neglecting the small-birefringence approximation, we obtain analytical solutions that describe the dependence of the diffraction angles and wave mismatch on the acousto-optic (AO) interaction geometry and crystal parameters. The formulas derived allow one to calculate and analyse the magnitude of diffraction-induced spatial and spectral image distortions and to identify the main types of distortions: chromatic compression and trapezoidal deformation. A comparison of the values of these distortions in the diffraction of ordinary and extraordinary polarised light shows that they are almost equal in magnitude and opposite in signs, so that consistent diffraction (o → e → o or e → o → e) in two identical AO cells rotated through 180° in the plane of diffraction can compensate for these distortions. (diffraction of radiation)

The bent crystal diffraction spectrometer at the BR2 reactor in Mol

Science.gov (United States)

Kaerts, E.; Jacobs, L.; Vandenput, G.; Van Assche, P. H. M.

1988-05-01

The DuMond-type bent crystal diffraction spectrometer installed at the BR2 reactor in Mol is presented. The spectrometer is mainly designed to study nuclear γ-transitions following thermal neutron capture. It covers the energy interval 25 ≦ Eγ ≦ 1500 keV. Instead of the traditionally used quartz crystals, a highly perfect silicium crystal is chosen as analysing crystal. Diffraction occurs from the (220) plane. The "quasi-mosaic" width, introduced by bending the crystal, is as small as 0.2″. The integrated reflecting power R of the bent crystal stays constant up to 1.5 MeV in first, 680 keV in second and 300 keV in third diffraction order. For higher photon energies, only an E-1 energy dependence is observed in second and third diffraction order. Consequently, besides improving the energy resolution, the use of these silicium crystals substantially increases the spectrometer efficiency and extends the high energy limit of bent crystal diffraction spectrometers. The diffraction angles are measured with a symmetrical interferometer system which covers an angular range of -6° to +6° with a precision of about 0.01″. Minimum diffraction line widths of 0.9″ have been measured, corresponding to an energy resolution ΔE = 1.35 × 10 -6E2n-1 keV -1. The dominant contribution to the observed line widths arises from the finite extent of the source.

A time-focusing Fourier chopper time-of-flight diffractometer for large scattering angles

International Nuclear Information System (INIS)

Heinonen, R.; Hiismaeki, P.; Piirto, A.; Poeyry, H.; Tiitta, A.

1975-01-01

A high-resolution time-of-flight diffractometer utilizing time focusing principles in conjunction with a Fourier chopper is under construction at Otaniemi. The design is an improved version of a test facility which has been used for single-crystal and powder diffraction studies with promising results. A polychromatic neutron beam from a radial beam tube of the FiR 1 reactor, collimated to dia. 70 mm, is modulated by a Fourier chopper (dia. 400 mm) which is placed inside a massive boron-loaded particle board shielding of 900 mm wall thickness. A thin flat sample (5 mm x dia. 80 mm typically) is mounted on a turntable at a distance of 4 m from the chopper, and the diffracted neutrons are counted by a scintillation detector at 4 m distance from the sample. The scattering angle 2theta can be chosen between 90deg and 160deg to cover Bragg angles from 45deg up to 80deg. The angle between the chopper disc and the incident beam direction as well as the angle of the detector surface relative to the diffracted beam can be adjusted between 45deg and 90deg in order to accomplish time-focusing. In our set-up, with equal flight paths from chopper to sample and from sample to detector, the time-focusing conditions are fulfilled when the chopper and the detector are parallel to the sample-plane. The time-of-flight spectrum of the scattered neutrons is measured by the reverse time-of-flight method in which, instead of neutrons, one essentially records the modulation function of the chopper during constant periods preceding each detected neutron. With a Fourier chopper whose speed is varied in a suitable way, the method is equivalent to the conventional Fourier method but the spectrum is obtained directly without any off-line calculations. The new diffractometer is operated automatically by a Super Nova computer which not only accumulates the synthetized diffraction pattern but also controls the chopper speed according to the modulation frequency sweep chosen by the user to obtain a

Analytical Electron Diffraction from Iii-V and II-Vi Semiconductors

Science.gov (United States)

Spellward, Paul

Available from UMI in association with The British Library. This thesis describes the development and evaluation of a number of new TEM-based techniques for the measurement of composition in ternary III-V and II-VI semiconductors. New methods of polarity determination in binary and ternary compounds are also presented. The theory of high energy electron diffraction is outlined, with particular emphasis on zone axis diffraction from well-defined strings. An account of TEM microstructural studies of Cd_{rm x}Hg _{rm 1-x}Te and CdTe epitaxial layers, which provided the impetus for developing the diffraction-based analytical techniques, is given. The wide range of TEM-based compositional determination techniques is described. The use of HOLZ deficiency lines to infer composition from a lattice parameter measurement is evaluated. In the case of Cd_{ rm x}Hg_{rm 1-x}Te, it is found to be inferior to other techniques developed. Studies of dynamical aspects of HOLZ diffraction can yield information about the dispersion surface from which a measure of composition may be obtained. This technique is evaluated for Al_{rm x}Ga_{rm 1-x} As, in which it is found to be of some use, and for Cd_{rm x}Hg _{rm 1-x}Te, in which the large Debye-Waller factor associated with mercury in discovered to render the method of little value. A number of critical voltages may be measured in medium voltage TEMs. The (111) zone axis critical voltage of Cd_{rm x}Hg _{rm 1-x}Te is found to vary significantly with x and forms the basis of an accurate technique for composition measurement in that ternary compound. Other critical voltage phenomena are investigated. In Al _{rm x}Ga_ {rm 1-x}As and other light ternaries, a non-systematic critical voltage is found to vary with x, providing a good indicator of composition. Critical voltage measurements may be made by conventional CBED or by various other techniques, which may also simultaneously yield information on the spatial variation of composition. The

Microarcsecond relative astrometry from the ground with a diffractive pupil

Energy Technology Data Exchange (ETDEWEB)

Ammons, S M; Bendek, E; Guyon, O

2011-09-08

The practical use of astrometry to detect exoplanets via the reflex motion of the parent star depends critically on the elimination of systematic floors in imaging systems. In the diffractive pupil technique proposed for space-based detection of exo-earths, extended diffraction spikes generated by a dotted primary mirror are referenced against a wide-field grid of background stars to calibrate changing optical distortion and achieve microarcsecond astrometric precision on bright targets (Guyon et al. 2010). We describe applications of this concept to ground-based uncrowded astrometry using a diffractive, monopupil telescope and a wide-field camera to image as many as {approx}4000 background reference stars. Final relative astrometric precision is limited by differential tip/tilt jitter caused by high altitude layers of turbulence. A diffractive 3-meter telescope is capable of reaching {approx}35 {micro}as relative astrometric error per coordinate perpendicular to the zenith vector in three hours on a bright target star (I < 10) in fields of moderate stellar density ({approx}40 stars arcmin{sup -2} with I < 23). Smaller diffractive apertures (D < 1 m) can achieve 100-200 {micro}as performance with the same stellar density and exposure time and a large telescope (6.5-10 m) could achieve as low as 10 {micro}as, nearly an order of magnitude better than current space-based facilities. The diffractive pupil enables the use of larger fields of view through calibration of changing optical distortion as well as brighter target stars (V < 6) by preventing star saturation. Permitting the sky to naturally roll to average signals over many thousands of pixels can mitigate the effects of detector imperfections.

Genome-wide linkage scan for primary open angle glaucoma: influences of ancestry and age at diagnosis.

Directory of Open Access Journals (Sweden)

Kristy R Crooks

Full Text Available Primary open-angle glaucoma (POAG is the most common form of glaucoma and one of the leading causes of vision loss worldwide. The genetic etiology of POAG is complex and poorly understood. The purpose of this work is to identify genomic regions of interest linked to POAG. This study is the largest genetic linkage study of POAG performed to date: genomic DNA samples from 786 subjects (538 Caucasian ancestry, 248 African ancestry were genotyped using either the Illumina GoldenGate Linkage 4 Panel or the Illumina Infinium Human Linkage-12 Panel. A total of 5233 SNPs was analyzed in 134 multiplex POAG families (89 Caucasian ancestry, 45 African ancestry. Parametric and non-parametric linkage analyses were performed on the overall dataset and within race-specific datasets (Caucasian ancestry and African ancestry. Ordered subset analysis was used to stratify the data on the basis of age of glaucoma diagnosis. Novel linkage regions were identified on chromosomes 1 and 20, and two previously described loci-GLC1D on chromosome 8 and GLC1I on chromosome 15--were replicated. These data will prove valuable in the context of interpreting results from genome-wide association studies for POAG.

Study of caprine bones after moist and dry heat processes by X-ray diffraction

International Nuclear Information System (INIS)

Barbosa, Caroline M.; Azeredo, Soraia R.; Lopes, Ricardo T.; Souza, Sheila M.F.M de

2013-01-01

Bone tissue is a biological material composed of hydroxyapatite (HAp) and collagen matrix. The bone X-ray diffraction (XRD) pattern presents characteristics of the hydroxyapatite crystallography planes. This paper presents the characterization by X-ray diffraction of caprine bone powder pattern and the comparison of this pattern with moist or dry heat cooked bone patterns. The parameters chosen to characterize the X-ray diffraction peaks were: angular position (2θ), full width at half maximumt (FWHM), and relative intensity (I rel ). The X-ray diffraction patterns were obtained with a Shimadzu XRD-6000 diffractometer. The caprine bone XRD pattern revealed a significant correlation of several crystallographic parameters (lattice data) with hydroxyapatite. The profiles of the three bone types analyzed presented differences. The study showed as small angular displacement (decrease of the 2θ angle) of some peaks was observed after moist and dry heat cooking processes. The characterization of bone tissue aimed to contribute to future analysis in the field of archeology. (author)

Study of caprine bones after moist and dry heat processes by X-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Barbosa, Caroline M., E-mail: carolmattosb@yahoo.com.br [Instituto de Arqueologia Brasileira (IAB), Belford Roxo, RJ (Brazil); Azeredo, Soraia R.; Lopes, Ricardo T., E-mail: soraia@lin.ufrj.br [Coordenacao dos Programas de Pos-Graduacao em Engenharia (COPPE/LIN/UFRJ), Rio de Janeiro, RJ (Brazil). Laboratorio de Instrumentacao Nuclear; Souza, Sheila M.F.M de, E-mail: sferraz@ensp.fiocruz.br [Fundacao Oswaldo Cruz (ENSP/FIOCRUZ), Rio de Janeiro, RJ (Brazil). Escola Nacional de Saude Publica Sergio Arouca

2013-07-01

Bone tissue is a biological material composed of hydroxyapatite (HAp) and collagen matrix. The bone X-ray diffraction (XRD) pattern presents characteristics of the hydroxyapatite crystallography planes. This paper presents the characterization by X-ray diffraction of caprine bone powder pattern and the comparison of this pattern with moist or dry heat cooked bone patterns. The parameters chosen to characterize the X-ray diffraction peaks were: angular position (2θ), full width at half maximumt (FWHM), and relative intensity (I{sub rel}). The X-ray diffraction patterns were obtained with a Shimadzu XRD-6000 diffractometer. The caprine bone XRD pattern revealed a significant correlation of several crystallographic parameters (lattice data) with hydroxyapatite. The profiles of the three bone types analyzed presented differences. The study showed as small angular displacement (decrease of the 2θ angle) of some peaks was observed after moist and dry heat cooking processes. The characterization of bone tissue aimed to contribute to future analysis in the field of archeology. (author)

Low-kilovolt coherent electron diffractive imaging instrument based on a single-atom electron source

Energy Technology Data Exchange (ETDEWEB)

Lin, Chun-Yueh [Department of Physics, National Taiwan University, Taipei 10617, Taiwan (China); Chang, Wei-Tse; Chen, Yi-Sheng; Hwu, En-Te; Chang, Chia-Seng; Hwang, Ing-Shouh, E-mail: ishwang@phys.sinica.edu.tw [Institute of Physics, Academia Sinica, Nankang, Taipei 11529, Taiwan (China); Hsu, Wei-Hao [Department of Materials Science and Engineering, National Tsing Hua University, Hsinchu 30013, Taiwan (China)

2016-03-15

In this work, a transmission-type, low-kilovolt coherent electron diffractive imaging instrument was constructed. It comprised a single-atom field emitter, a triple-element electrostatic lens, a sample holder, and a retractable delay line detector to record the diffraction patterns at different positions behind the sample. It was designed to image materials thinner than 3 nm. The authors analyzed the asymmetric triple-element electrostatic lens for focusing the electron beams and achieved a focused beam spot of 87 nm on the sample plane at the electron energy of 2 kV. High-angle coherent diffraction patterns of a suspended graphene sample corresponding to (0.62 Å){sup −1} were recorded. This work demonstrated the potential of coherent diffractive imaging of thin two-dimensional materials, biological molecules, and nano-objects at a voltage between 1 and 10 kV. The ultimate goal of this instrument is to achieve atomic resolution of these materials with high contrast and little radiation damage.

Dynamic grazing incidence fast atom diffraction during molecular beam epitaxial growth of GaAs

Energy Technology Data Exchange (ETDEWEB)

Atkinson, P., E-mail: atkinson@insp.jussieu.fr; Eddrief, M. [Sorbonne Universités, UPMC Univ. Paris 06, UMR 7588, INSP, F-75005 Paris (France); CNRS, UMR 7588, Institut des NanoSciences de Paris, 4 place Jussieu, F-75005 Paris (France); Etgens, V. H. [CNRS, UMR 7588, Institut des NanoSciences de Paris, 4 place Jussieu, F-75005 Paris (France); VeDeCom-Université Versailles Saint-Quentin en Yvelines, Versailles (France); Khemliche, H., E-mail: hocine.khemliche@u-psud.fr; Debiossac, M.; Mulier, M.; Lalmi, B.; Roncin, P. [ISMO UMR8214 CNRS-Université Paris-Sud, Orsay F-91400 (France); Momeni, A. [ISMO UMR8214 CNRS-Université Paris-Sud, Orsay F-91400 (France); Univ. Cergy Pontoise, F-95031 Cergy (France)

2014-07-14

A Grazing Incidence Fast Atom Diffraction (GIFAD) system has been mounted on a commercial molecular beam epitaxy chamber and used to monitor GaAs growth in real-time. In contrast to the conventionally used Reflection High Energy Electron Diffraction, all the GIFAD diffraction orders oscillate in phase, with the change in intensity related to diffuse scattering at step edges. We show that the scattered intensity integrated over the Laue circle is a robust method to monitor the periodic change in surface roughness during layer-by-layer growth, with oscillation phase and amplitude independent of incidence angle and crystal orientation. When there is a change in surface reconstruction at the start of growth, GIFAD intensity oscillations show that there is a corresponding delay in the onset of layer-by-layer growth. In addition, changes in the relative intensity of different diffraction orders have been observed during growth showing that GIFAD has the potential to provide insight into the preferential adatom attachment sites on the surface reconstruction during growth.

Accurate measurement of the orientation relationship of lath martensite and bainite by electron backscatter diffraction analysis

International Nuclear Information System (INIS)

Miyamoto, G.; Takayama, N.; Furuhara, T.

2009-01-01

A new method to determine the orientation relationship between martensite and bainite with the parent austenite is developed based on electron backscatter diffraction analysis. This method can determine the orientation relationship accurately without the presence of retained austenite, and is applicable to lath martensite and bainite in low-alloyed carbon steels. The angles between close-packed directions are about 3 o for lath martensite regardless of the carbon content, while the angles between close-packed planes become smaller with increasing carbon content.

2D Spin-Dependent Diffraction of Electrons From Periodical Chains of Nanomagnets

Directory of Open Access Journals (Sweden)

Teshome Senbeta

2012-03-01

Full Text Available The scattering of the unpolarized beams of electrons by nanomagnets in the vicinity of some scattering angles leads to complete spin polarized electrons. This result is obtained with the help of the perturbation theory. The dipole-dipole interaction between the magnetic moment of the nanomagnet and the magnetic moment of electron is treated as perturbation. This interaction is not spherically symmetric. Rather it depends on the electron spin variables. It in turn results in spinor character of the scattering amplitudes. Due to the smallness of the magnetic interactions, the scattering length of this process is very small to be proved experimentally. To enhance the relevant scattering lengths, we considered the diffraction of unpolarized beams of electrons by linear chains of nanomagnets. By tuning the distance between the scatterers it is possible to obtain the diffraction maximum of the scattered electrons at scattering angles which corresponds to complete spin polarization of electrons. It is shown that the total differential scattering length is proportional to N2 (N is a number of scatterers. Even small number of nanomagnets in the chain helps to obtain experimentally visible enhancement of spin polarization of the scattered electrons.

Evanescent Properties of Optical Diffraction from 2-Dimensional Hexagonal Photonic Crystals and Their Sensor Applications.

Science.gov (United States)

Liao, Yu-Yang; Chen, Yung-Tsan; Chen, Chien-Chun; Huang, Jian-Jang

2018-04-03

The sensitivity of traditional diffraction grating sensors is limited by the spatial resolution of the measurement setup. Thus, a large space is required to improve sensor performance. Here, we demonstrate a compact hexagonal photonic crystal (PhC) optical sensor with high sensitivity. PhCs are able to diffract optical beams to various angles in azimuthal space. The critical wavelength that satisfies the phase matching or becomes evanescent was used to benchmark the refractive index of a target analyte applied on a PhC sensor. Using a glucose solution as an example, our sensor demonstrated very high sensitivity and a low limit of detection. This shows that the diffraction mechanism of hexagonal photonic crystals can be used for sensors when compact size is a concern.

Tectonic History and Deep Structure of the Demerara Plateau from Combined Wide-Angle and Reflection Seismic Data and Plate Kinematic Reconstructions

Science.gov (United States)

Klingelhoefer, F.; Museur, T.; Roest, W. R.; Graindorge, D.; Chauvet, F.; Loncke, L.; Basile, C.; Poetisi, E.; Deverchere, J.; Lebrun, J. F.; Perrot, J.; Heuret, A.

2017-12-01

Many transform margins have associated intermediate depth marginal plateaus, which are commonly located between two oceanic basins. The Demerara plateau is located offshore Surinam and French Guiana. Plate kinematic reconstructions show that the plateau is located between the central and equatorial Atlantic in a position conjugate to the Guinean Plateau. In the fall of 2016, the MARGATS cruise acquired geophysical data along the 400 km wide Demerara plateau. The main objective of the cruise was to image the deep structure of the Demerara plateau and to study its tectonic history. A set of 4 combined wide-angle and reflection seismic profiles was acquired along the plateau, using 80 ocean-bottom seismometers, a 3 km long seismic streamer and a 8000 cu inch tuned airgun array. Forward modelling of the wide-angle seismic data on a profile, located in the eastern part of the plateau and oriented in a NE-SW direction, images the crustal structure of the plateau, the transition zone and the neighbouring crust of oceanic origin, up to a depth of 40 km. The plateau itself is characterised by a crust of 30 km thickness, subdivided into three distinct layers. However, the velocities and velocity gradients do not fit typical continental crust, with a lower crustal layer showing untypically high velocities and an upper layer having a steep velocity gradient. From this model we propose that the lowermost layer is probably formed from volcanic underplated material and that the upper crustal layer likely consists of the corresponding extrusive volcanic material, forming thick seaward-dipping reflector sequences on the plateau. A basement high is imaged at the foot of the slope and forms the ocean-continent transition zone. Further oceanward, a 5-6 km thick crust is imaged with velocities and velocity gradients corresponding to a thin oceanic crust. A compilation of magnetic data from the MARGATS and 3 previous cruises shows a high amplitude magnetic anomaly along the northern

MUSIC - Multifunctional stereo imaging camera system for wide angle and high resolution stereo and color observations on the Mars-94 mission

Science.gov (United States)

Oertel, D.; Jahn, H.; Sandau, R.; Walter, I.; Driescher, H.

1990-10-01

Objectives of the multifunctional stereo imaging camera (MUSIC) system to be deployed on the Soviet Mars-94 mission are outlined. A high-resolution stereo camera (HRSC) and wide-angle opto-electronic stereo scanner (WAOSS) are combined in terms of hardware, software, technology aspects, and solutions. Both HRSC and WAOSS are push-button instruments containing a single optical system and focal plates with several parallel CCD line sensors. Emphasis is placed on the MUSIC system's stereo capability, its design, mass memory, and data compression. A 1-Gbit memory is divided into two parts: 80 percent for HRSC and 20 percent for WAOSS, while the selected on-line compression strategy is based on macropixel coding and real-time transform coding.

Suspended DNA structural characterization by TEM diffraction

KAUST Repository

Marini, Monica

2017-12-01

In this work, micro-fabrication, super-hydrophobic properties and a physiologically compatible preparation step are combined and tailored to obtain background free biological samples to be investigated by Transmission Electron Microscopy (TEM) diffraction technique. The validation was performed evaluating a well-known parameter such as the DNA interbases value. The diffraction spacing measured is in good agreement with those obtained by HRTEM direct metrology and by traditional X-Ray diffraction. This approach addresses single molecule studies in a simplified and reproducible straightforward way with respect to more conventional and widely used techniques. In addition, it overcomes the need of long and elaborated samples preparations: the sample is in its physiological environment and the HRTEM data acquisition occurs without any background interference, coating, staining or additional manipulation. The congruence in the results reported in this paper makes the application of this approach extremely promising towards those molecules for which crystallization remains a hurdle, such as cell membrane proteins and fibrillar proteins.

Diffractive elements performance in chromatic confocal microscopy

International Nuclear Information System (INIS)

Garzon, J; Duque, D; Alean, A; Toledo, M; Meneses, J; Gharbi, T

2011-01-01

The Confocal Laser Scanning Microscopy (CLSM) has been widely used in the semiconductor industry and biomedicine because of its depth discrimination capability. Subsequent to this technique has been developed in recent years Chromatic Confocal Microscopy. This method retains the same principle of confocal and offers the added advantage of removing the axial movement of the moving system. This advantage is usually accomplished with an optical element that generates a longitudinal chromatic aberration and a coding system that relates the axial position of each point of the sample with the wavelength that is focused on each. The present paper shows the performance of compact chromatic confocal microscope when some different diffractive elements are used for generation of longitudinal chromatic aberration. Diffractive elements, according to the process and manufacturing parameters, may have different diffraction efficiency and focus a specific wavelength in a specific focal position. The performance assessment is carried out with various light sources which exhibit an incoherent behaviour and a broad spectral width.

Suspended DNA structural characterization by TEM diffraction

KAUST Repository

Marini, Monica; Allione, Marco; Lopatin, Sergei; Moretti, Manola; Giugni, Andrea; Torre, Bruno; Di Fabrizio, Enzo M.

2017-01-01

In this work, micro-fabrication, super-hydrophobic properties and a physiologically compatible preparation step are combined and tailored to obtain background free biological samples to be investigated by Transmission Electron Microscopy (TEM) diffraction technique. The validation was performed evaluating a well-known parameter such as the DNA interbases value. The diffraction spacing measured is in good agreement with those obtained by HRTEM direct metrology and by traditional X-Ray diffraction. This approach addresses single molecule studies in a simplified and reproducible straightforward way with respect to more conventional and widely used techniques. In addition, it overcomes the need of long and elaborated samples preparations: the sample is in its physiological environment and the HRTEM data acquisition occurs without any background interference, coating, staining or additional manipulation. The congruence in the results reported in this paper makes the application of this approach extremely promising towards those molecules for which crystallization remains a hurdle, such as cell membrane proteins and fibrillar proteins.

Measuring the nematic order of suspensions of colloidal fd virus by x-ray diffraction and optical birefringence

International Nuclear Information System (INIS)

Purdy, Kirstin R.; Dogic, Zvonimir; Fraden, Seth; Ruehm, Adrian; Lurio, Lawrence; Mochrie, Simon G. J.

2003-01-01

The orientational distribution function of the nematic phase of suspensions of the semiflexible rodlike virus fd is measured by x-ray diffraction as a function of concentration and ionic strength. X-ray diffraction from a single-domain nematic phase of fd is influenced by interparticle correlations at low angle, while only intraparticle scatter contributes at high angle. Consequently, the angular distribution of the scattered intensity arises from only the single-particle orientational distribution function at high angle but it also includes spatial and orientational correlations at low angle. Experimental measurements of the orientational distribution function from both the interparticle (structure factor) and intraparticle (form factor) scattering were made to test whether the correlations present in interparticle scatter influence the measurement of the single-particle orientational distribution function. It was found that the two types of scatter yield consistent values for the nematic order parameter. It was also found that x-ray diffraction is insensitive to the orientational distribution function's precise form, and the measured angular intensity distribution is described equally well by both Onsager's trial function and a Gaussian. At high ionic strength, the order parameter S of the nematic phase coexisting with the isotropic phase approaches theoretical predictions for long semiflexible rods S=0.55, but deviations from theory increase with decreasing ionic strength. The concentration dependence of the nematic order parameter also better agrees with theoretical predictions at high ionic strength indicating that electrostatic interactions have a measurable effect on the nematic order parameter. The x-ray order parameters are shown to be proportional to the measured birefringence, and the saturation birefringence of fd is determined enabling a simple, inexpensive way to measure the order parameter. Additionally, the spatial ordering of nematic fd was probed

Crustal structure variations along the NW-African continental margin: a comparison of new and existing models from wide angle and reflection seismic data

Science.gov (United States)

Biari, Y.; Klingelhoefer, F.; Sahabi, M.; Aslanian, D.; Philippe, S.; Louden, K. E.; Berglar, K.; Moulin, M.; Mehdi, K.; Graindorge, D.; Evain, M.; Benabellouahed, M.; Reichert, C. J.

2014-12-01

Deep seismic data represent a key to understand the geometry and mechanism of continental rifting. The passive continental margin of NW-Africa is one of the oldest on earth, formed during the Upper Triassic-Lower Liassic rifting of the central Atlantic Ocean over 200 Ma. We present new and existing wide-angle and reflection seismic data from three study regions along the margin located in the North Moroccan salt basin, on the central continental margin offshore Safi and in the south, offshore Dakhla. In each of the study areas several combined wide-angle and reflection seismic profiles perpendicular and parallel to the margin have been acquired and forward modelled using comparable methods. The thickness of unthinned continental crust decreases from 36 km in the North to about 27 km in the South. In the North Moroccan Basin continental crust thins from originally 36 km to about 8 km in a 150 km wide zone. The basin itself is underlain by highly thinned continental crust. Offshore safi thinning of the continental crust is confined to a 130 km wide zone with no neighboring sedimentary basin underlain by continental crust. In both areas the zone of crustal thinning is characterised by the presence of large blocks and abundant salt diapirs. In the south crustal thinning is more rapid in a zone of 90 km and asymmetric with the upper crust thinning more closely to the continent than the lower crust, probably due to depth-dependent stretching and the presence of the precambrian Reguibat Ridge on land. Oceanic crust is characterised by a thickness of 7-8 km along the complete margin. Relatively high velocities of up to 7.5 km/s have been imaged between magnetic anomalies S1 and M25, and are probably related to changes in the spreading velocities at the time of the Kimmeridgian/Tithonian plate reorganisation. Volcanic activity seems to be confined to the region next to the Canary Islands, and is thus not related to the initial opening of the oceanic, which was related to no

A honeycomb-like three-dimensional metamaterial absorber via super-wideband and wide-angle performances at millimeter wave and low THz frequencies

Science.gov (United States)

Vahidi, Alireza; Rajabalipanah, Hamid; Abdolali, Ali; Cheldavi, Ahmad

2018-04-01

Achieving wideband absorption via three-dimensional (3D) metamaterials has revealed as a new emerging innovative field of research, especially in recent years. Here, a novel 3D metamaterial absorber (MA) having a sixfold symmetry is designed which consists of periodic resistive honeycomb-like units. The proposed 3D MA exhibits a strong absorptivity above 90% in the widest bandwidth ever reported to the authors' knowledge from 50 to 460 GHz (the bandwidth ratio larger than 1:9), covering both millimeter wave and low -terahertz spectra. To understand the physical mechanism of absorption, the electric field and surface current distributions, the power loss density as well as the deteriorating effects of the high-order Floquet modes are monitored and discussed. As a distinctive feature in comparison to the similar 3D MAs, our engineered absorber provides multiple resonances, contributing to further broadening of the operating bandwidth. In addition, it is shown that the honeycomb-like MA retains its polarization-insensitive absorption in a wide range of incident wave angles and polarization angles. Due to flexibility of the design, these superior performances can be simply extended to terahertz, infrared and visible frequencies, potentially leading to many promising applications in imaging, sensing, and camouflage technology.

Biological imaging by soft X-ray diffraction microscopy

Science.gov (United States)

Shapiro, David

We have developed a microscope for soft x-ray diffraction imaging of dry or frozen hydrated biological specimens. This lensless imaging system does not suffer from the resolution or specimen thickness limitations that other short wavelength microscopes experience. The microscope, currently situated at beamline 9.0.1 of the Advanced Light Source, can collect diffraction data to 12 nm resolution with 750 eV photons and 17 nm resolution with 520 eV photons. The specimen can be rotated with a precision goniometer through an angle of 160 degrees allowing for the collection of nearly complete three-dimensional diffraction data. The microscope is fully computer controlled through a graphical user interface and a scripting language automates the collection of both two-dimensional and three-dimensional data. Diffraction data from a freeze-dried dwarf yeast cell, Saccharomyces cerevisiae carrying the CLN3-1 mutation, was collected to 12 run resolution from 8 specimen orientations spanning a total rotation of 8 degrees. The diffraction data was phased using the difference map algorithm and the reconstructions provide real space images of the cell to 30 nm resolution from each of the orientations. The agreement of the different reconstructions provides confidence in the recovered, and previously unknown, structure and indicates the three dimensionality of the cell. This work represents the first imaging of the natural complex refractive contrast from a whole unstained cell by the diffraction microscopy method and has achieved a resolution superior to lens based x-ray tomographic reconstructions of similar specimens. Studies of the effects of exposure to large radiation doses were also carried out. It was determined that the freeze-dried cell suffers from an initial collapse, which is followed by a uniform, but slow, shrinkage. This structural damage to the cell is not accompanied by a diminished ability to see small features in the specimen. Preliminary measurements on frozen

New calculations of cross-sections and charge asymmetries for lepton pair production and wide angle Bhabha scattering in e+e- collisions near the Z-peak

Science.gov (United States)

Field, J. H.

1994-03-01

A new event generator for lepton pair production and wide angle Bhabha scattering, BHAGENE3, is presented. Both electroweak and higher order (beyond O(α) QED corrections are included. Comparisons are made with results from the programs, based on the structure function formalism, ALIBABA, TOPAZ0 and ZFITTER. For the case of the final states l+l-γγ ( l = e, μ, τ) BHAGENE3 results are compared with those of Monte Carlo generators that use the exact O( α2) amplitudes.

Measurement of 3D refractive index distribution by optical diffraction tomography

Science.gov (United States)

Chi, Weining; Wang, Dayong; Wang, Yunxin; Zhao, Jie; Rong, Lu; Yuan, Yuanyuan

2018-01-01

Optical Diffraction Tomography (ODT), as a novel 3D imaging technique, can obtain a 3D refractive index (RI) distribution to reveal the important optical properties of transparent samples. According to the theory of ODT, an optical diffraction tomography setup is built based on the Mach-Zehnder interferometer. The propagation direction of object beam is controlled by a 2D translation stage, and 121 holograms based on different illumination angles are recorded by a Charge-coupled Device (CCD). In order to prove the validity and accuracy of the ODT, the 3D RI profile of microsphere with a known RI is firstly measured. An iterative constraint algorithm is employed to improve the imaging accuracy effectively. The 3D morphology and average RI of the microsphere are consistent with that of the actual situation, and the RI error is less than 0.0033. Then, an optical element fabricated by laser with a non-uniform RI is taken as the sample. Its 3D RI profile is obtained by the optical diffraction tomography system.

X-ray diffraction study of the structure of detonation nanodiamonds

International Nuclear Information System (INIS)

Ozerin, A. N.; Kurkin, T. S.; Ozerina, L. A.; Dolmatov, V. Yu.

2008-01-01

The spatial structure of aggregates formed by detonation nanodiamonds is investigated using the wide-angle and small-angle X-ray scattering techniques. The effective sizes of crystallites and the crystallite size distribution function are determined. The shape of scattering aggregates is restored from the small-angle X-ray scattering data. An analysis of the results obtained allowed the conclusion that the nanodiamond aggregates have an extended spatial structure composed of nine to ten clusters, each involving four to five crystallites with a crystal lattice of the diamond type

Detecting blind building façades from highly overlapping wide angle aerial imagery

Science.gov (United States)

Burochin, Jean-Pascal; Vallet, Bruno; Brédif, Mathieu; Mallet, Clément; Brosset, Thomas; Paparoditis, Nicolas

2014-10-01

This paper deals with the identification of blind building façades, i.e. façades which have no openings, in wide angle aerial images with a decimeter pixel size, acquired by nadir looking cameras. This blindness characterization is in general crucial for real estate estimation and has, at least in France, a particular importance on the evaluation of legal permission of constructing on a parcel due to local urban planning schemes. We assume that we have at our disposal an aerial survey with a relatively high stereo overlap along-track and across-track and a 3D city model of LoD 1, that can have been generated with the input images. The 3D model is textured with the aerial imagery by taking into account the 3D occlusions and by selecting for each façade the best available resolution texture seeing the whole façade. We then parse all 3D façades textures by looking for evidence of openings (windows or doors). This evidence is characterized by a comprehensive set of basic radiometric and geometrical features. The blindness prognostic is then elaborated through an (SVM) supervised classification. Despite the relatively low resolution of the images, we reach a classification accuracy of around 85% on decimeter resolution imagery with 60 × 40 % stereo overlap. On the one hand, we show that the results are very sensitive to the texturing resampling process and to vegetation presence on façade textures. On the other hand, the most relevant features for our classification framework are related to texture uniformity and horizontal aspect and to the maximal contrast of the opening detections. We conclude that standard aerial imagery used to build 3D city models can also be exploited to some extent and at no additional cost for facade blindness characterisation.

Determination of interplanar distances starting from diffraction spectra for the Cyber computer of the ININ

International Nuclear Information System (INIS)

Macias B, L.R.

1991-04-01

To identify a compound by means of diffraction it is required to obtain it spectrum or diffractogram that it is not more than a graphic I/I o vs. 2 θ. Since this analysis type is carried out on samples of glasses, it is expected that when impacting the radiation on the sample and to vary the angles θ and 2 θ, and when being completed the Bragg law, constructive interference it exists among all the radiation beams that emerge of the sample and take place the diffraction. In this work the diffractogram is identified by means of a graph equipment (x,t) that directly obtains the graphic I/I o vs. 2 θ and in this it has to be carried out angular measurement of the present peaks and later on with the data 2 θ i it was proceeds to compare with the totally identified patterns as the contents in the Powder Diffraction File of the Joint Committee on Powder Diffraction Standards (JCPDS). (Author)

Diffraction theory

NARCIS (Netherlands)

Bouwkamp, C.J.

1954-01-01

A critical review is presented of recent progress in classical diffraction theory. Both scalar and electromagnetic problems are discussed. The report may serve as an introduction to general diffraction theory although the main emphasis is on diffraction by plane obstacles. Various modifications of

New Insights into the Relationship Between Network Structure and Strain Induced Crystallization in Unvolcanized Natural Rubber by Synchrotron X-ray Diffraction

International Nuclear Information System (INIS)

Toki, S.; Hsiao, B.; Amnuaypornsri, S.; Sakdapipanich, J.

2009-01-01

The relationship between the network structure and strain-induced crystallization in un-vulcanized as well as vulcanized natural rubbers (NR) and synthetic poly-isoprene rubbers (IR) was investigated via synchrotron wide-angle X-ray diffraction (WAXD) technique. It was found that the presence of a naturally occurring network structure formed by natural components in un-vulcanized NR significantly facilitates strain-induced crystallization and enhances modulus and tensile strength. The stress-strain relation in vulcanized NR is due to the combined effect of chemical and naturally occurring networks. The weakness of naturally occurring network against stress and temperature suggests that vulcanized NR has additional relaxation mechanism due to naturally occurring network. The superior mechanical properties in NR compared with IR are mainly due to the existence of naturally occurring network structure.

Setup for in situ X-ray diffraction studies of thin film growth by magnetron sputtering

CERN Document Server

Ellmer, K; Weiss, V; Rossner, H

2001-01-01

A novel method is described for the in situ-investigation of nucleation and growth of thin films during magnetron sputtering. Energy dispersive X-ray diffraction with synchrotron light is used for the structural analysis during film growth. An in situ-magnetron sputtering chamber was constructed and installed at a synchrotron radiation beam line with a bending magnet. The white synchrotron light (1-70 keV) passes the sputtering chamber through Kapton windows and hits one of the substrates on a four-fold sample holder. The diffracted beam, observed under a fixed diffraction angle between 3 deg. and 10 deg., is energy analyzed by a high purity Ge-detector. The in situ-EDXRD setup is demonstrated for the growth of tin-doped indium oxide (ITO) films prepared by reactive magnetron sputtering from a metallic target.

An electrically driven terahertz metamaterial diffractive modulator with more than 20 dB of dynamic range

International Nuclear Information System (INIS)

Karl, N.; Reichel, K.; Mendis, R.; Mittleman, D. M.; Chen, H.-T.; Taylor, A. J.; Brener, I.; Benz, A.; Reno, J. L.

2014-01-01

We design and experimentally demonstrate a switchable diffraction grating for terahertz modulation based on planar active metamaterials, where a Schottky gate structure is implemented to tune the metamaterial resonances in real-time via the application of an external voltage bias. The diffraction grating is formed by grouping the active split-ring resonators into an array of independent columns with alternate columns biased. We observe off-axis diffraction over a wide frequency band in contrast to the narrow-band resonances, which permits operation of the device as a relatively high-speed, wide-bandwidth, high-contrast modulator, with more than 20 dB of dynamic range

X-ray Diffraction Study of Arsenopyrite at High Pressure

Energy Technology Data Exchange (ETDEWEB)

D Fan; M Ma; W Zhou; S Wei; Z Chen; H Xie

2011-12-31

The high-pressure X-ray diffraction study of a natural arsenopyrite was investigated up to 28.2 GPa using in situ angle-dispersive X-ray diffraction and a diamond anvil cell at National Synchrotron Light Source, Brookhaven National Laboratory. The 16:3:1 methanol-ethanol-water mixture was used as a pressure-transmitting medium. Pressures were measured using the ruby-fluorescence method. No phase change has been observed up to 28.2 GPa. The isothermal equation of state (EOS) was determined. The values of K{sub 0}, and K'{sub 0} refined with a third-order Birch-Murnaghan EOS are K{sub 0} = 123(9) GPa, and K'{sub 0} = 5.2(8). Furthermore, we confirm that the linear compressibilities ({beta}) along a, b and c directions of arsenopyrite is elastically isotropic ({beta}{sub a} = 6.82 x 10{sup -4}, {beta}{sub b} = 6.17 x 10{sup -4} and {beta}{sub c} = 6.57 x 10{sup -4} GPa{sup -1}).

A novel approach to electron data background treatment in an online wide-angle spectrometer for laser-accelerated ion and electron bunches

Science.gov (United States)

Lindner, F. H.; Bin, J. H.; Englbrecht, F.; Haffa, D.; Bolton, P. R.; Gao, Y.; Hartmann, J.; Hilz, P.; Kreuzer, C.; Ostermayr, T. M.; Rösch, T. F.; Speicher, M.; Parodi, K.; Thirolf, P. G.; Schreiber, J.

2018-01-01

Laser-based ion acceleration is driven by electrical fields emerging when target electrons absorb laser energy and consecutively leave the target material. A direct correlation between these electrons and the accelerated ions is thus to be expected and predicted by theoretical models. We report on a modified wide-angle spectrometer, allowing the simultaneous characterization of angularly resolved energy distributions of both ions and electrons. Equipped with online pixel detectors, the RadEye1 detectors, the investigation of this correlation gets attainable on a single shot basis. In addition to first insights, we present a novel approach for reliably extracting the primary electron energy distribution from the interfering secondary radiation background. This proves vitally important for quantitative extraction of average electron energies (temperatures) and emitted total charge.

Unitarized model of inclusive and diffractive DIS with Q2 evolution

International Nuclear Information System (INIS)

Armesto, Nestor; Salgado, Carlos A.; Tywoniuk, Konrad; Kaidalov, Alexei B.

2010-01-01

We discuss the interplay of low-x physics and QCD scaling violations by extending the unified approach describing inclusive structure functions and diffractive production in γ*p interactions proposed in previous papers to large values of Q 2 . We describe the procedure of extracting, from the nonperturbative model, initial conditions for the QCD evolution that respect unitarity. Assuming Regge factorization of the diffractive structure function, a similar procedure is proposed for the calculation of hard diffraction. The results are in good agreement with experimental data on the proton structure function F 2 and the most recent data on the reduced diffractive cross section, x P σ r D(3) . Predictions for both F 2 and F L are presented in a wide kinematical range and compared to calculations within high-energy QCD.

Accessing the diffracted wavefield by coherent subtraction

Science.gov (United States)

Schwarz, Benjamin; Gajewski, Dirk

2017-10-01

Diffractions have unique properties which are still rarely exploited in common practice. Aside from containing subwavelength information on the scattering geometry or indicating small-scale structural complexity, they provide superior illumination compared to reflections. While diffraction occurs arguably on all scales and in most realistic media, the respective signatures typically have low amplitudes and are likely to be masked by more prominent wavefield components. It has been widely observed that automated stacking acts as a directional filter favouring the most coherent arrivals. In contrast to other works, which commonly aim at steering the summation operator towards fainter contributions, we utilize this directional selection to coherently approximate the most dominant arrivals and subtract them from the data. Supported by additional filter functions which can be derived from wave front attributes gained during the stacking procedure, this strategy allows for a fully data-driven recovery of faint diffractions and makes them accessible for further processing. A complex single-channel field data example recorded in the Aegean sea near Santorini illustrates that the diffracted background wavefield is surprisingly rich and despite the absence of a high channel count can still be detected and characterized, suggesting a variety of applications in industry and academia.

Wide-Field Imaging Using Nitrogen Vacancies

Science.gov (United States)

Englund, Dirk Robert (Inventor); Trusheim, Matthew Edwin (Inventor)

2017-01-01

Nitrogen vacancies in bulk diamonds and nanodiamonds can be used to sense temperature, pressure, electromagnetic fields, and pH. Unfortunately, conventional sensing techniques use gated detection and confocal imaging, limiting the measurement sensitivity and precluding wide-field imaging. Conversely, the present sensing techniques do not require gated detection or confocal imaging and can therefore be used to image temperature, pressure, electromagnetic fields, and pH over wide fields of view. In some cases, wide-field imaging supports spatial localization of the NVs to precisions at or below the diffraction limit. Moreover, the measurement range can extend over extremely wide dynamic range at very high sensitivity.

Diffractive interference optical analyzer (DiOPTER)

Science.gov (United States)

Sasikumar, Harish; Prasad, Vishnu; Pal, Parama; Varma, Manoj M.

2016-03-01

This report demonstrates a method for high-resolution refractometric measurements using, what we have termed as, a Diffractive Interference Optical Analyzer (DiOpter). The setup consists of a laser, polarizer, a transparent diffraction grating and Si-photodetectors. The sensor is based on the differential response of diffracted orders to bulk refractive index changes. In these setups, the differential read-out of the diffracted orders suppresses signal drifts and enables time-resolved determination of refractive index changes in the sample cell. A remarkable feature of this device is that under appropriate conditions, the measurement sensitivity of the sensor can be enhanced by more than two orders of magnitude due to interference between multiply reflected diffracted orders. A noise-equivalent limit of detection (LoD) of 6x10-7 RIU was achieved in glass. This work focuses on devices with integrated sample well, made on low-cost PDMS. As the detection methodology is experimentally straightforward, it can be used across a wide array of applications, ranging from detecting changes in surface adsorbates via binding reactions to estimating refractive index (and hence concentration) variations in bulk samples. An exciting prospect of this technique is the potential integration of this device to smartphones using a simple interface based on transmission mode configuration. In a transmission configuration, we were able to achieve an LoD of 4x10-4 RIU which is sufficient to explore several applications in food quality testing and related fields. We are envisioning the future of this platform as a personal handheld optical analyzer for applications ranging from environmental sensing to healthcare and quality testing of food products.

Grazing incidence diffraction anomalous fine structure of self-assembled semiconductor nanostructures

International Nuclear Information System (INIS)

Grenier, S.; Letoublon, A.; Proietti, M.G.; Renevier, H.; Gonzalez, L.; Garcia, J.M.; Priester, C.; Garcia, J.

2003-01-01

We have studied self-organized quantum wires of InAs, grown by molecular beam epitaxy onto a InP(0 0 1) substrate, by means of grazing incidence diffraction anomalous fine structure (DAFS). The equivalent quantum wires thickness is 2.5 monolayers. We measured the (4 4 0) and (4 2 0) GIDAFS spectra, at the As K-edge, keeping the incidence and exit angles close to the InP critical angle. The analysis of both the smooth and oscillatory contributions of the DAFS spectrum, provide valuable information about composition and strain inside the quantum wires and close to the interface. We also show preliminary results on InAs wires encapsulated by a 40 A thick InP capping layer, suggesting the DAFS capability of probing different iso-strain regions of the wires

[Study of selegiline and related compounds with x-ray diffraction].

Science.gov (United States)

Simon, K; Böcskei, Z; Török, Z

1992-09-01

Selegiline and its parent compounds were studied by X-ray diffraction. It was established that the racemates of primary and secondary amines (p-fluoro-amphetamine, methamphetamine, p-fluoro-methamphetamine) hydrochloride do not form racemic compounds but crystalline as conglomerates, at the same time tertiary amines like selegiline and p-fluoro-selegiline hydrochlorides do. The crystalline structure of five enantiomeric hydrochlorides were determined, the CPhe-C-C-N torsion angle is anti-periplanar in all cases but in p-fluoro-amphetamine where it is gauche.

Rainbow and Fresnel diffraction effects in the heavy ion scattering

International Nuclear Information System (INIS)

Salvadori, M.C.B.S.

1984-01-01

A detailed theoretical analysis of the heavy-ion elastic scattering differential cross section, using the uniform semiclassical approximation of Berry in the sharp cut-off limit is presented. A decomposition of the cross section into four physically well-defined components is used in the analysis. The aim of the analysis is to explore the possibility of distinguishing at the cross-section level, between a pure raibow or Fresnel diffraction nature of the heavy-ion elastic scattering at above-barrier energies and not too large angles. (Author) [pt

Nanoporous active carbons at ambient conditions: a comparative study using X-ray scattering and diffraction, Raman spectroscopy and N2 adsorption

Science.gov (United States)

Shiryaev, A. A.; Voloshchuk, A. M.; Volkov, V. V.; Averin, A. A.; Artamonova, S. D.

2017-05-01

Furfural-derived sorbents and activated carbonaceous fibers were studied using Small- and Wide-angle X-ray scattering (SWAXS), X-ray diffraction and multiwavelength Raman spectroscopy after storage at ambient conditions. Correlations between structural features with degree of activation and with sorption parameters are observed for samples obtained from a common precursor and differing in duration of activation. However, the correlations are not necessarily applicable to the carbons obtained from different precursors. Using two independent approaches we show that treatment of SWAXS results should be performed with careful analysis of applicability of the Porod law to the sample under study. In general case of a pore with rough/corrugated surface deviations from the Porod law may became significant and reflect structure of the pore-carbon interface. Ignorance of these features may invalidate extraction of closed porosity values. In most cases the pore-matrix interface in the studied samples is not atomically sharp, but is characterized by 1D or 2D fluctuations of electronic density responsible for deviations from the Porod law. Intensity of the pores-related small-angle scattering correlates positively with SBET values obtained from N2 adsorption.

Nanoporous active carbons at ambient conditions: a comparative study using X-ray scattering and diffraction, Raman spectroscopy and N2 adsorption

International Nuclear Information System (INIS)

Shiryaev, A A; Voloshchuk, A M; Averin, A A; Artamonova, S D.; Volkov, V V

2017-01-01

Furfural-derived sorbents and activated carbonaceous fibers were studied using Small- and Wide-angle X-ray scattering (SWAXS), X-ray diffraction and multiwavelength Raman spectroscopy after storage at ambient conditions. Correlations between structural features with degree of activation and with sorption parameters are observed for samples obtained from a common precursor and differing in duration of activation. However, the correlations are not necessarily applicable to the carbons obtained from different precursors. Using two independent approaches we show that treatment of SWAXS results should be performed with careful analysis of applicability of the Porod law to the sample under study. In general case of a pore with rough/corrugated surface deviations from the Porod law may became significant and reflect structure of the pore-carbon interface. Ignorance of these features may invalidate extraction of closed porosity values. In most cases the pore-matrix interface in the studied samples is not atomically sharp, but is characterized by 1D or 2D fluctuations of electronic density responsible for deviations from the Porod law. Intensity of the pores-related small-angle scattering correlates positively with S BET values obtained from N 2 adsorption. (paper)

Study of the temperature rise induced by a focusing transducer with a wide aperture angle on biological tissue containing ribs

International Nuclear Information System (INIS)

Wang Xin; Lin Jiexing; Liu Xiaozhou; Liu Jiehui; Gong Xiufen

2016-01-01

We used the spheroidal beam equation to calculate the sound field created by focusing a transducer with a wide aperture angle to obtain the heat deposition, and then we used the Pennes bioheat equation to calculate the temperature field in biological tissue with ribs and to ascertain the effects of rib parameters on the temperature field. The results show that the location and the gap width between the ribs have a great influence on the axial and radial temperature rise of multilayer biological tissue. With a decreasing gap width, the location of the maximum temperature rise moves forward; as the ribs are closer to the transducer surface, the sound energy that passes through the gap between the ribs at the focus decreases, the maximum temperature rise decreases, and the location of the maximum temperature rise moves forward with the ribs. (paper)

A mobile system for a comprehensive online-characterization of nanoparticle aggregates based on wide-angle light scattering and laser-induced incandescence

Energy Technology Data Exchange (ETDEWEB)

Huber, Franz J. T.; Will, Stefan, E-mail: stefan.will@fau.de [Lehrstuhl für Technische Thermodynamik (LTT), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Erlangen 91058 (Germany); Erlangen Graduate School in Advanced Optical Technologies (SAOT), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Erlangen 91052 (Germany); Cluster of Excellence Engineering of Advanced Materials (EAM), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Erlangen 91052 (Germany); Altenhoff, Michael [Lehrstuhl für Technische Thermodynamik (LTT), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Erlangen 91058 (Germany); Erlangen Graduate School in Advanced Optical Technologies (SAOT), Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Erlangen 91052 (Germany)

2016-05-15

A mobile demonstrator for the comprehensive online-characterization of gas-borne nanoparticle aggregates is presented. Two optical measurement techniques are combined, both utilizing a pulsed Nd:YAG laser as light source. Aggregate size and fractal dimension are measured by Wide-Angle Light Scattering (WALS). An ellipsoidal mirror images elastically scattered light from scattering angles between 10° and 165° onto a CCD-camera chip resulting in an almost complete scattering diagram with high angular resolution. Primary particle size and volume fraction are measured by time-resolved Laser-Induced Incandescence (TiRe-LII). Here, particles are heated up to about 3000 K by the short laser pulse, the enhanced thermal radiation signal is detected with gated photomultiplier tubes. Analysis of the signal decay time and maximum LII-signal allows for the determination of primary particle diameter and volume fraction. The performance of the system is demonstrated by combined measurements on soot nanoparticle aggregates from a soot aerosol generator. Particle and aggregate sizes are varied by using different equivalence ratios of the combustion in the generator. Soot volume fraction can be adjusted by different levels of dilution with air. Online-measurements were carried out demonstrating the favorable performance of the system and the potential for industrial applications such as process control and product development. The particle properties obtained are confirmed through transmission electron microscopy analysis on representative samples.

A mobile system for a comprehensive online-characterization of nanoparticle aggregates based on wide-angle light scattering and laser-induced incandescence

International Nuclear Information System (INIS)

Huber, Franz J. T.; Will, Stefan; Altenhoff, Michael

2016-01-01

A mobile demonstrator for the comprehensive online-characterization of gas-borne nanoparticle aggregates is presented. Two optical measurement techniques are combined, both utilizing a pulsed Nd:YAG laser as light source. Aggregate size and fractal dimension are measured by Wide-Angle Light Scattering (WALS). An ellipsoidal mirror images elastically scattered light from scattering angles between 10° and 165° onto a CCD-camera chip resulting in an almost complete scattering diagram with high angular resolution. Primary particle size and volume fraction are measured by time-resolved Laser-Induced Incandescence (TiRe-LII). Here, particles are heated up to about 3000 K by the short laser pulse, the enhanced thermal radiation signal is detected with gated photomultiplier tubes. Analysis of the signal decay time and maximum LII-signal allows for the determination of primary particle diameter and volume fraction. The performance of the system is demonstrated by combined measurements on soot nanoparticle aggregates from a soot aerosol generator. Particle and aggregate sizes are varied by using different equivalence ratios of the combustion in the generator. Soot volume fraction can be adjusted by different levels of dilution with air. Online-measurements were carried out demonstrating the favorable performance of the system and the potential for industrial applications such as process control and product development. The particle properties obtained are confirmed through transmission electron microscopy analysis on representative samples.

Fluorinert as a pressure-transmitting medium for high-pressure diffraction studies

International Nuclear Information System (INIS)

Varga, Tamas; Wilkinson, Angus P.; Angel, Ross J.

2003-01-01

Fluorinert is a liquid pressure-transmitting medium that is widely used in high-pressure diffraction work. A systematic study of five different fluorinerts was carried out using single-crystal x-ray diffraction in a diamond-anvil cell in order to determine the pressure range over which they provide a hydrostatic stress state to the sample. It was found that none of the fluorinerts studied can be considered hydrostatic above 1.2 GPa, a lower pressure than reported previously

Deep seismic transect across the Tonankai earthquake area obtained from the onshore- offshore wide-angle seismic study

Science.gov (United States)

Nakanishi, A.; Obana, K.; Kodaira, S.; Miura, S.; Fujie, G.; Ito, A.; Sato, T.; Park, J.; Kaneda, Y.; Ito, K.; Iwasaki, T.

2008-12-01

In the Nankai Trough subduction seismogenic zone, M8-class great earthquake area can be divided into three segments; they are source regions of the Nankai, Tonankai and presumed Tokai earthquakes. The Nankai and Tonankai earthquakes had often occurred simultaneously, and caused a great event. Hypocenters of these great earthquakes were usually located off the cape Shiono, Kii Peninsula, and the rupture propagated westwards and eastwards, respectively. To obtain the deep structure of the down-dip limit of around the Nankai Trough seismogenic zone, the segment boundary and first break area off the Kii Peninsula, the onshore-offshore wide-angle seismic studies was conducted in the western and eastern part of the Kii Peninsula and their offshore area in 2004 and 2006, respectively. The result of the seismic study in 2004 is mainly shown here. Structural images along the onshore and offshore profiles have already been separately obtained. In this study, an onshore-offshore integrated image of the western part of the Kii Peninsula, ~400km in a total length, is obtained from first arrival tomography and traveltime mapping of reflection phases by combining dataset of 13 land explosions, 2269 land stations, 36 OBSs and 1806 offshore airgun shots. The subduction angle of the Philippine Sea plate (PSP) gradually increases landward up to ~20-25 degree. Beneath the onshore part, the subducting PSP is estimated at ~5km shallower than that previously derived from seismicity. Low frequency earthquakes (identified and picked by Japan Meteorological Agency) are relocated around the plate interface of the subducting PSP by using the deep seismic transect obtained in this study. The offshore research is part of 'Structure research on plate dynamics of the presumed rupture zone of the Tonankai-Nankai Earthquakes' funded by Ministry of Education, Culture, Sports, Science and Technology (MEXT). The onshore research carried by the Kyoto University is part of 'Special Project for

Method for Measurement of Multi-Degrees-of-Freedom Motion Parameters Based on Polydimethylsiloxane Cross-Coupling Diffraction Gratings

Science.gov (United States)

Duan, Junping; Zhu, Qiang; Qian, Kun; Guo, Hao; Zhang, Binzhen

2017-08-01

This work presents a multi-degrees-of-freedom motion parameter measurement method based on the use of cross-coupling diffraction gratings that were prepared on the two sides of a polydimethylsiloxane (PDMS) substrate using oxygen plasma processing technology. The laser beam that travels pass the cross-coupling optical grating would be diffracted into a two-dimensional spot array. The displacement and the gap size of the spot-array were functions of the movement of the laser source, as explained by the Fraunhofer diffraction effect. A 480 × 640 pixel charge-coupled device (CCD) was used to acquire images of the two-dimensional spot-array in real time. A proposed algorithm was then used to obtain the motion parameters. Using this method and the CCD described above, the resolutions of the displacement and the deflection angle were 0.18 μm and 0.0075 rad, respectively. Additionally, a CCD with a higher pixel count could improve the resolutions of the displacement and the deflection angle to sub-nanometer and micro-radian scales, respectively. Finally, the dynamic positions of hovering rotorcraft have been tracked and checked using the proposed method, which can be used to correct the craft's position and provide a method for aircraft stabilization in the sky.

Modeling the Radar Return of Powerlines Using an Incremental Length Diffraction Coefficient Approach

Science.gov (United States)

Macdonald, Douglas

A method for modeling the signal from cables and powerlines in Synthetic Aperture Radar (SAR) imagery is presented. Powerline detection using radar is an active area of research. Accurately identifing the location of powerlines in a scene can be used to aid pilots of low flying aircraft in collision avoidance, or map the electrical infrastructure of an area. The focus of this research was on the forward modeling problem of generating the powerline SAR signal from first principles. Previous work on simulating SAR imagery involved methods that ranged from efficient but insufficiently accurate, depending on the application, to more exact but computationally complex. A brief survey of the numerous ways to model the scattering of electromagnetic radiation is provided. A popular tool that uses the geometric optics approximation for modeling imagery for remote sensing applications across a wide range of modalities is the Digitial Imaging and Remote Sensing Image Generation (DIRSIG) tool. This research shows the way in which DIRSIG generates the SAR phase history is unique compared to other methods used. In particular, DIRSIG uses the geometric optics approximation for the scattering of electromagnetic radiation and builds the phase history in the time domain on a pulse-by-pulse basis. This enables an efficient generation of the phase history of complex scenes. The drawback to this method is the inability to account for diffraction. Since the characteristic diameter of many communication cables and powerlines is on the order of the wavelength of the incident radiation, diffraction is the dominant mechanism by which the radiation gets scattered for these targets. Comparison of DIRSIG imagery to field data shows good scene-wide qualitative agreement as well as Rayleigh distributed noise in the amplitude data, as expected for coherent imaging with speckle. A closer inspection of the Radar Cross Sections of canonical targets such as trihedrals and dihedrals, however, shows

The CCP14 for single crystal and powder diffraction

International Nuclear Information System (INIS)

Cranswick, L.M.D.

1999-01-01

Full text: The Collaborative Computation Project Number 14 for Single Crystal and Powder Diffraction (CCP14) is continuing in its objective to provide freely available software and resources for the powder diffraction and crystallographic community. Using the Internet and World Wide Web, we are presently compiling software and web resources, creating tutorials and help files. It also endeavours to encourage and provide resources to assist program authors with developing their software. The CCP14 presently has its web-site at and a mirror at (at CSIRO, Melbourne, Australia). Auto web-mirroring is being implemented to allow users to obtain software and access to resources in a more time effective manner. For people in countries isolated from the Internet, the CCP14 on CD-ROM can be snail mailed on request. This is in the form of a Virtual World Wide Web/Virtual Internet; in the same vein as the existing Crystallographic Nexus CD-ROM. Copyright (1999) Australian X-ray Analytical Association Inc

Expression, purification and preliminary diffraction studies of CmlS

International Nuclear Information System (INIS)

Latimer, Ryan; Podzelinska, Kateryna; Soares, Alexei; Bhattacharya, Anupam; Vining, Leo C.; Jia, Zongchao; Zechel, David L.

2009-01-01

CmlS from S. venezuelae is a flavin-dependent halogenase that is involved in the biosynthesis of the widely used antibiotic chloramphenicol. Here, the crystallization of CmlS and analysis of the initial diffraction data are reported. CmlS, a flavin-dependent halogenase (FDH) present in the chloramphenicol-biosynthetic pathway in Streptomyces venezuelae, directs the dichlorination of an acetyl group. The reaction mechanism of CmlS is of considerable interest as it will help to explain how the FDH family can halogenate a wide range of substrates through a common mechanism. The protein has been recombinantly expressed in Escherichia coli and purified to homogeneity. The hanging-drop vapour-diffusion method was used to produce crystals that were suitable for X-ray diffraction. Data were collected to 2.0 Å resolution. The crystal belonged to space group C2, with unit-cell parameters a = 208.1, b = 57.7, c = 59.9 Å, β = 97.5°

Standard test method for verifying the alignment of X-Ray diffraction instrumentation for residual stress measurement

CERN Document Server

American Society for Testing and Materials. Philadelphia

2010-01-01

1.1 This test method covers the preparation and use of a flat stress-free test specimen for the purpose of checking the systematic error caused by instrument misalignment or sample positioning in X-ray diffraction residual stress measurement, or both. 1.2 This test method is applicable to apparatus intended for X-ray diffraction macroscopic residual stress measurement in polycrystalline samples employing measurement of a diffraction peak position in the high-back reflection region, and in which the θ, 2θ, and ψ rotation axes can be made to coincide (see Fig. 1). 1.3 This test method describes the use of iron powder which has been investigated in round-robin studies for the purpose of verifying the alignment of instrumentation intended for stress measurement in ferritic or martensitic steels. To verify instrument alignment prior to stress measurement in other metallic alloys and ceramics, powder having the same or lower diffraction angle as the material to be measured should be prepared in similar fashion...

Three-dimensional nanostructure determination from a large diffraction data set recorded using scanning electron nanodiffraction

Directory of Open Access Journals (Sweden)

Yifei Meng

2016-09-01

Full Text Available A diffraction-based technique is developed for the determination of three-dimensional nanostructures. The technique employs high-resolution and low-dose scanning electron nanodiffraction (SEND to acquire three-dimensional diffraction patterns, with the help of a special sample holder for large-angle rotation. Grains are identified in three-dimensional space based on crystal orientation and on reconstructed dark-field images from the recorded diffraction patterns. Application to a nanocrystalline TiN thin film shows that the three-dimensional morphology of columnar TiN grains of tens of nanometres in diameter can be reconstructed using an algebraic iterative algorithm under specified prior conditions, together with their crystallographic orientations. The principles can be extended to multiphase nanocrystalline materials as well. Thus, the tomographic SEND technique provides an effective and adaptive way of determining three-dimensional nanostructures.

Blazed vector gratings fabricated using photosensitive polymer liquid crystals and control of polarization diffraction

Science.gov (United States)

Ono, Hiroshi; Kuzuwata, Mitsuru; Sasaki, Tomoyuki; Noda, Kohei; Kawatsuki, Nobuhiro

2014-03-01

The blazed vector grating possessing antisymmetric distributions of the birefringence were fabricated by exposing the line-focused linearly polarized ultraviolet light on the photosensitive polymer liquid crystals. The polarization states of the diffraction beams can be highly and widely controlled by designing the blazed structures, and the diffraction properties were well-explained by Jones calculus.

Prospect for application of compact accelerator-based neutron source to neutron engineering diffraction

Energy Technology Data Exchange (ETDEWEB)

Ikeda, Yoshimasa, E-mail: yoshimasa.ikeda@riken.jp [Center for Advanced Photonics, RIKEN, Wako, Saitama 351-0198 (Japan); Taketani, Atsushi; Takamura, Masato; Sunaga, Hideyuki [Center for Advanced Photonics, RIKEN, Wako, Saitama 351-0198 (Japan); Kumagai, Masayoshi [Faculty of Engineering, Tokyo City University, Setagaya, Tokyo 158-8857 (Japan); Oba, Yojiro [Research Reactor Institute, Kyoto University, Kumatori, Osaka 590-0494 (Japan); Otake, Yoshie [Center for Advanced Photonics, RIKEN, Wako, Saitama 351-0198 (Japan); Suzuki, Hiroshi [Materials Sciences Research Center, Japan Atomic Energy Agency, Tokai, Ibaraki 319-1195 (Japan)

2016-10-11

A compact accelerator-based neutron source has been lately discussed on engineering applications such as transmission imaging and small angle scattering as well as reflectometry. However, nobody considers using it for neutron diffraction experiment because of its low neutron flux. In this study, therefore, the neutron diffraction experiments are carried out using Riken Accelerator-driven Compact Neutron Source (RANS), to clarify the capability of the compact neutron source for neutron engineering diffraction. The diffraction pattern from a ferritic steel was successfully measured by suitable arrangement of the optical system to reduce the background noise, and it was confirmed that the recognizable diffraction pattern can be measured by a large sampling volume with 10 mm in cubic for an acceptable measurement time, i.e. 10 min. The minimum resolution of the 110 reflection for RANS is approximately 2.5% at 8 μs of the proton pulse width, which is insufficient to perform the strain measurement by neutron diffraction. The moderation time width at the wavelength corresponding to the 110 reflection is estimated to be approximately 30 μs, which is the most dominant factor to determine the resolution. Therefore, refinements of the moderator system to decrease the moderation time by decreasing a thickness of the moderator or by applying the decoupler system or application of the angular dispersive neutron diffraction technique are important to improve the resolution of the diffraction experiment using the compact neutron source. In contrast, the texture evolution due to plastic deformation was successfully observed by measuring a change in the diffraction peak intensity by RANS. Furthermore, the volume fraction of the austenitic phase in the dual phase mock specimen was also successfully evaluated by fitting the diffraction pattern using a Rietveld code. Consequently, RANS has been proved to be capable for neutron engineering diffraction aiming for the easy access

Single-crystal neutron diffraction study of ammonium nitrate phase III

International Nuclear Information System (INIS)

Choi, C.S.; Prask, H.J.

1982-01-01

The crystal structure of ammonium nitrate phase III has been studied at room temperature by neutron diffraction using a single crystal containing 5% KNO 3 in solid-solution form. The space group is Pnma, with a = 7.6772 (4), b = 5.8208 (4), c = 7.1396 (5) A, Z = 4. The final residual after full-matrix least-squares refinement was R = 0.042 for 348 observed reflections. The ammonium ions are thermally disordered into two orientations, displaced by an angle of approximately 42 0 about an axis parallel to the c axis. (Auth.)

Model experiment of in vivo synchrotron X-ray diffraction of human kidney stones

Energy Technology Data Exchange (ETDEWEB)

Ancharov, A.I. [Institute of Solid State Chemistry and Mechanochemistry SB RAS, Novosibirsk (Russian Federation)]. E-mail: ancharov@mail.ru; Potapov, S.S. [Institute of Mineralogy UB RAS, Miass (Russian Federation); Moiseenko, T.N. [The State Regional Clinical Hospital, Novosibirsk (Russian Federation); Feofilov, I.V. [The State Regional Clinical Hospital, Novosibirsk (Russian Federation); Nizovskii, A.I. [Boreskov Institute of Catalysis SB RAS, Novosibirsk (Russian Federation)

2007-05-21

The diffraction of synchrotron radiation (SR) was used to explore the phase composition of kidney stones placed into a specific object phantom, which imitated the human body. As an imitation of the patient breath, the kidney stone was moved vertically and rotated to an angle of 15{sup o} during the recording of the X-ray pattern. It was shown that rotation and displacement did not distort the X-ray pattern.

Model experiment of in vivo synchrotron X-ray diffraction of human kidney stones

International Nuclear Information System (INIS)

Ancharov, A.I.; Potapov, S.S.; Moiseenko, T.N.; Feofilov, I.V.; Nizovskii, A.I.

2007-01-01

The diffraction of synchrotron radiation (SR) was used to explore the phase composition of kidney stones placed into a specific object phantom, which imitated the human body. As an imitation of the patient breath, the kidney stone was moved vertically and rotated to an angle of 15 o during the recording of the X-ray pattern. It was shown that rotation and displacement did not distort the X-ray pattern

SU-F-T-84: Measurement and Monte-Carlo Simulation of Electron Phase Spaces Using a Wide Angle Magnetic Electron Spectrometer

Energy Technology Data Exchange (ETDEWEB)

Englbrecht, F; Lindner, F; Bin, J; Wislsperger, A; Reiner, M; Kamp, F; Belka, C; Dedes, G; Schreiber, J; Parodi, K [LMU Munich, Munich, Bavaria (Germany)

2016-06-15

Purpose: To measure and simulate well-defined electron spectra using a linear accelerator and a permanent-magnetic wide-angle spectrometer to test the performance of a novel reconstruction algorithm for retrieval of unknown electron-sources, in view of application to diagnostics of laser-driven particle acceleration. Methods: Six electron energies (6, 9, 12, 15, 18 and 21 MeV, 40cm × 40cm field-size) delivered by a Siemens Oncor linear accelerator were recorded using a permanent-magnetic wide-angle electron spectrometer (150mT) with a one dimensional slit (0.2mm × 5cm). Two dimensional maps representing beam-energy and entrance-position along the slit were measured using different scintillating screens, read by an online CMOS detector of high resolution (0.048mm × 0.048mm pixels) and large field of view (5cm × 10cm). Measured energy-slit position maps were compared to forward FLUKA simulations of electron transport through the spectrometer, starting from IAEA phase-spaces of the accelerator. The latter ones were validated against measured depth-dose and lateral profiles in water. Agreement of forward simulation and measurement was quantified in terms of position and shape of the signal distribution on the detector. Results: Measured depth-dose distributions and lateral profiles in the water phantom showed good agreement with forward simulations of IAEA phase-spaces, thus supporting usage of this simulation source in the study. Measured energy-slit position maps and those obtained by forward Monte-Carlo simulations showed satisfactory agreement in shape and position. Conclusion: Well-defined electron beams of known energy and shape will provide an ideal scenario to study the performance of a novel reconstruction algorithm using measured and simulated signal. Future work will increase the stability and convergence of the reconstruction-algorithm for unknown electron sources, towards final application to the electrons which drive the interaction of TW-class laser

Zone-boundary optimization for direct laser writing of continuous-relief diffractive optical elements.

Science.gov (United States)

Korolkov, Victor P; Nasyrov, Ruslan K; Shimansky, Ruslan V

2006-01-01

Enhancing the diffraction efficiency of continuous-relief diffractive optical elements fabricated by direct laser writing is discussed. A new method of zone-boundary optimization is proposed to correct exposure data only in narrow areas along the boundaries of diffractive zones. The optimization decreases the loss of diffraction efficiency related to convolution of a desired phase profile with a writing-beam intensity distribution. A simplified stepped transition function that describes optimized exposure data near zone boundaries can be made universal for a wide range of zone periods. The approach permits a similar increase in the diffraction efficiency as an individual-pixel optimization but with fewer computation efforts. Computer simulations demonstrated that the zone-boundary optimization for a 6 microm period grating increases the efficiency by 7% and 14.5% for 0.6 microm and 1.65 microm writing-spot diameters, respectively. The diffraction efficiency of as much as 65%-90% for 4-10 microm zone periods was obtained experimentally with this method.

Improvement of diffraction efficiency of three-dimensional magneto-optic spatial light modulator with magnetophotonic crystal

Energy Technology Data Exchange (ETDEWEB)

Nakamura, K.; Takagi, H., E-mail: takagi@ee.tut.ac.jp; Lim, P. B.; Inoue, M., E-mail: inoue@tut.ac.jp [Department of Electrical and Electronic Information Engineering, Toyohashi University of Technology, Toyohashi, Aichi 441 8580 (Japan); Goto, Taichi [Department of Electrical and Electronic Information Engineering, Toyohashi University of Technology, Toyohashi, Aichi 441 8580 (Japan); JST, PRESTO, 4-1-8 Honcho, Kawaguchi, Saitama 332-0012 (Japan); Horimai, H. [HolyMine Corporation, Atsugi, Kanagawa 243 0813 (Japan); Yoshikawa, H. [Department of Computer Engineering, College of Science and Technology, Nihon University, Funabashi, Chiba 274 8501 (Japan); Bove, V. M. [MIT Media Lab, Cambridge, Massachusetts 02139 (United States)

2016-01-11

We have developed three-dimensional magneto-optic spatial light modulators (3D-MOSLMs) that use magnetic domains as submicron scale pixels to represent holograms. Our display system uses a submicron-scale magnetic pixel array on an amorphous TbFe film to create a wide viewing angle hologram. However, in previous work the reconstructed images had a low intensity and a low optical contrast; brightness of the reconstructed image was 4.4 × 10{sup −2 }cd/m{sup 2} with 532 nm illumination light at 10.8 mW/cm{sup 2}, while display standard ISO13406 recommends 100 cd/m{sup 2} or more. In this paper, we describe our development of a 3D-MOSLM composed of an artificial magnetic lattice structure of magnetophotonic crystals (MPCs). The MPCs enhance the diffraction efficiency of reconstructed 3D images and reduce the power consumption for controlling the magnetic pixels by a light localization effect. We demonstrate reconstructed 3D images using the MPC and show significant brightness improvement.

Morphological and structural characterization of PHBV/organoclay nanocomposites by small angle X-ray scattering

Energy Technology Data Exchange (ETDEWEB)

Carli, Larissa N., E-mail: lncarli@ucs.br [Instituto de Quimica, Universidade Federal do Rio Grande do Sul, Av. Bento Goncalves, 9500, Porto Alegre, 91501-970, RS (Brazil); Centro de Ciencias Exatas e Tecnologia, Universidade de Caxias do Sul, Rua Francisco Getulio Vargas, 1130, Caxias do Sul, 95070-560, RS (Brazil); Bianchi, Otavio, E-mail: obianchi@ucs.br [Centro de Ciencias Exatas e Tecnologia, Universidade de Caxias do Sul, Rua Francisco Getulio Vargas, 1130, Caxias do Sul, 95070-560, RS (Brazil); Machado, Giovanna, E-mail: giovannamachado@uol.com.br [Centro de Tecnologias Estrategicas do Nordeste, Av. Prof. Luiz Freire, 01, Cidade Universitaria, Recife, 50740-540, PE (Brazil); Programa de Pos-Graduacao de Materiais, Universidade Federal de Pernambuco, Av. Prof. Moraes Rego, 1235, Recife, 50670-901, PE (Brazil); Crespo, Janaina S., E-mail: jscrespo@ucs.br [Centro de Ciencias Exatas e Tecnologia, Universidade de Caxias do Sul, Rua Francisco Getulio Vargas, 1130, Caxias do Sul, 95070-560, RS (Brazil); Mauler, Raquel S., E-mail: raquel.mauler@ufrgs.br [Instituto de Quimica, Universidade Federal do Rio Grande do Sul, Av. Bento Goncalves, 9500, Porto Alegre, 91501-970, RS (Brazil)

2013-03-01

In this work, the morphological and structural behaviors of poly(hydroxybutyrate-co-hydroxyvalerate) (PHBV) nanocomposites were investigated using small angle X-ray scattering (SAXS), wide angle X-ray diffraction (WAXD) and transmission electron microscopy (TEM). The nanocomposites with 1, 3 and 5 wt.% of organically modified montmorillonite Cloisite Registered-Sign 30B (OMMT) were prepared by melt processing in a twin screw extruder using two different processing conditions (low and high shear intensity). The lamellar long period of the polymer was lower for the nanocomposites, with high polydispersity values. However, the crystalline thickness increased with the clay content and was independent of the processing conditions. This behavior resulted in a high linear crystallinity of the nanocomposites with 3 and 5 wt.% OMMT. The disruption factor ({beta}) was in agreement with the WAXD and TEM findings, indicating a good dispersion of the nanoparticles in the PHBV matrix with 3 wt.% of OMMT during the high shear intensity of melt processing. Highlights: Black-Right-Pointing-Pointer SAXS was used for morphological and crystalline studies of PHBV/OMMT nanocomposites. Black-Right-Pointing-Pointer The crystalline structure was influenced by the presence of clay. Black-Right-Pointing-Pointer The degree of clay dispersion in a polymer matrix was quantified. Black-Right-Pointing-Pointer The morphology comprised exfoliated particles, nanoscale and microscale clusters. Black-Right-Pointing-Pointer The results obtained by SAXS agreed well with TEM and WAXD results.

Anisotropic parameter inversion in VTI media using diffraction data

KAUST Repository

Waheed, Umair bin

2013-09-22

Diffracted waves contain useful information regarding the subsurface geometry and velocity. They are particularly valuable for anisotropic media as they inherently possess a wide range of dips necessary to resolve angular dependence of velocity. Using this property of diffraction data to our vantage, we develop an algorithm to invert for effective η model, assuming no prior knowledge of it. The obtained effective η model is then converted to interval η model using Dix-type inversion formula. The effectiveness of this approach is tested on the VTI Marmousi model, which yields good structural match even for a highly complex media such as the Marmousi model.

Three-dimensional electron diffraction as a complementary technique to powder X-ray diffraction for phase identification and structure solution of powders

Directory of Open Access Journals (Sweden)

Yifeng Yun

2015-03-01

Full Text Available Phase identification and structure determination are important and widely used techniques in chemistry, physics and materials science. Recently, two methods for automated three-dimensional electron diffraction (ED data collection, namely automated diffraction tomography (ADT and rotation electron diffraction (RED, have been developed. Compared with X-ray diffraction (XRD and two-dimensional zonal ED, three-dimensional ED methods have many advantages in identifying phases and determining unknown structures. Almost complete three-dimensional ED data can be collected using the ADT and RED methods. Since each ED pattern is usually measured off the zone axes by three-dimensional ED methods, dynamic effects are much reduced compared with zonal ED patterns. Data collection is easy and fast, and can start at any arbitrary orientation of the crystal, which facilitates automation. Three-dimensional ED is a powerful technique for structure identification and structure solution from individual nano- or micron-sized particles, while powder X-ray diffraction (PXRD provides information from all phases present in a sample. ED suffers from dynamic scattering, while PXRD data are kinematic. Three-dimensional ED methods and PXRD are complementary and their combinations are promising for studying multiphase samples and complicated crystal structures. Here, two three-dimensional ED methods, ADT and RED, are described. Examples are given of combinations of three-dimensional ED methods and PXRD for phase identification and structure determination over a large number of different materials, from Ni–Se–O–Cl crystals, zeolites, germanates, metal–organic frameworks and organic compounds to intermetallics with modulated structures. It is shown that three-dimensional ED is now as feasible as X-ray diffraction for phase identification and structure solution, but still needs further development in order to be as accurate as X-ray diffraction. It is expected that three

Three-dimensional electron diffraction as a complementary technique to powder X-ray diffraction for phase identification and structure solution of powders.

Science.gov (United States)

Yun, Yifeng; Zou, Xiaodong; Hovmöller, Sven; Wan, Wei

2015-03-01

Phase identification and structure determination are important and widely used techniques in chemistry, physics and materials science. Recently, two methods for automated three-dimensional electron diffraction (ED) data collection, namely automated diffraction tomography (ADT) and rotation electron diffraction (RED), have been developed. Compared with X-ray diffraction (XRD) and two-dimensional zonal ED, three-dimensional ED methods have many advantages in identifying phases and determining unknown structures. Almost complete three-dimensional ED data can be collected using the ADT and RED methods. Since each ED pattern is usually measured off the zone axes by three-dimensional ED methods, dynamic effects are much reduced compared with zonal ED patterns. Data collection is easy and fast, and can start at any arbitrary orientation of the crystal, which facilitates automation. Three-dimensional ED is a powerful technique for structure identification and structure solution from individual nano- or micron-sized particles, while powder X-ray diffraction (PXRD) provides information from all phases present in a sample. ED suffers from dynamic scattering, while PXRD data are kinematic. Three-dimensional ED methods and PXRD are complementary and their combinations are promising for studying multiphase samples and complicated crystal structures. Here, two three-dimensional ED methods, ADT and RED, are described. Examples are given of combinations of three-dimensional ED methods and PXRD for phase identification and structure determination over a large number of different materials, from Ni-Se-O-Cl crystals, zeolites, germanates, metal-organic frameworks and organic compounds to intermetallics with modulated structures. It is shown that three-dimensional ED is now as feasible as X-ray diffraction for phase identification and structure solution, but still needs further development in order to be as accurate as X-ray diffraction. It is expected that three-dimensional ED methods

Diffractive optics and nanophotonics resolution below the diffraction limit

CERN Document Server

Minin, Igor

2016-01-01

In this book the authors present several examples of techniques used to overcome the Abby diffraction limit using flat and 3D diffractive optical elements, photonic crystal lenses, photonic jets, and surface plasmon diffractive optics. The structures discussed can be used in the microwave and THz range and also as scaled models for optical frequencies. Such nano-optical microlenses can be integrated, for example, into existing semiconductor heterostructure platforms for next-generation optoelectronic applications. Chapter 1 considers flat diffractive lenses and innovative 3D radiating structures including a conical millimeter-wave Fresnel zone plate (FZP) lens proposed for subwavelength focusing. In chapter 2 the subwavelength focusing properties of diffractive photonic crystal lenses are considered and it is shown that at least three different types of photonic crystal lens are possible.  With the aim of achieving subwavelength focusing, in chapter 3 an alternative mechanism to produce photonic jets at Tera...

Time-resolved measurements with streaked diffraction patterns from electrons generated in laser plasma wakefield

Science.gov (United States)

He, Zhaohan; Nees, John; Hou, Bixue; Krushelnick, Karl; Thomas, Alec; Beaurepaire, Benoît; Malka, Victor; Faure, Jérôme

2013-10-01

Femtosecond bunches of electrons with relativistic to ultra-relativistic energies can be robustly produced in laser plasma wakefield accelerators (LWFA). Scaling the electron energy down to sub-relativistic and MeV level using a millijoule laser system will make such electron source a promising candidate for ultrafast electron diffraction (UED) applications due to the intrinsic short bunch duration and perfect synchronization with the optical pump. Recent results of electron diffraction from a single crystal gold foil, using LWFA electrons driven by 8-mJ, 35-fs laser pulses at 500 Hz, will be presented. The accelerated electrons were collimated with a solenoid magnetic lens. By applying a small-angle tilt to the magnetic lens, the diffraction pattern can be streaked such that the temporal evolution is separated spatially on the detector screen after propagation. The observable time window and achievable temporal resolution are studied in pump-probe measurements of photo-induced heating on the gold foil.

Opalescence of quartz: a study by high energy x-ray diffraction

Science.gov (United States)

Bastie, P.; Dolino, G.; Hamelin, B.

2003-05-01

The origin of the opalescence observed at the α-β transition of quartz remains an open question. This intense light scattering occurs during the coexistence, at the first order transition, of the α and incommensurate (inc) phases, in the vicinity of the phase interface. New hard x-ray diffraction experiment shows that the large angle light scattering is mainly in the α-phase region of the crystal and reveals the existence of an intermediate structure between the α-phase and the 3q inc phase.

Opalescence of quartz: a study by high energy x-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Bastie, P [Laboratoire de Spectrometrie Physique, Universite Joseph Fourier-Grenoble 1 - CNRS, UMR No 5588, BP 87, 38402 Saint Martin d' Heres Cedex (France); Dolino, G [Laboratoire de Spectrometrie Physique, Universite Joseph Fourier-Grenoble 1 - CNRS, UMR No 5588, BP 87, 38402 Saint Martin d' Heres Cedex (France); Hamelin, B [Institut Laue Langevin, BP 156X, 38042 Grenoble Cedex 9 (France)

2003-05-21

The origin of the opalescence observed at the {alpha}-{beta} transition of quartz remains an open question. This intense light scattering occurs during the coexistence, at the first order transition, of the {alpha} and incommensurate (inc) phases, in the vicinity of the phase interface. New hard x-ray diffraction experiment shows that the large angle light scattering is mainly in the {alpha}-phase region of the crystal and reveals the existence of an intermediate structure between the {alpha}-phase and the 3q inc phase.

Nonparaxial propagation and focusing properties of azimuthal-variant vector fields diffracted by an annular aperture.

Science.gov (United States)

Gu, Bing; Xu, Danfeng; Pan, Yang; Cui, Yiping

2014-07-01

Based on the vectorial Rayleigh-Sommerfeld integrals, the analytical expressions for azimuthal-variant vector fields diffracted by an annular aperture are presented. This helps us to investigate the propagation behaviors and the focusing properties of apertured azimuthal-variant vector fields under nonparaxial and paraxial approximations. The diffraction by a circular aperture, a circular disk, or propagation in free space can be treated as special cases of this general result. Simulation results show that the transverse intensity, longitudinal intensity, and far-field divergence angle of nonparaxially apertured azimuthal-variant vector fields depend strongly on the azimuthal index, the outer truncation parameter and the inner truncation parameter of the annular aperture, as well as the ratio of the waist width to the wavelength. Moreover, the multiple-ring-structured intensity pattern of the focused azimuthal-variant vector field, which originates from the diffraction effect caused by an annular aperture, is experimentally demonstrated.

Instrumentation of x-ray diffraction and materials research on the National Synchrotron Light Source. Final report

International Nuclear Information System (INIS)

Liedl, G.L.

1984-11-01

MATRIX was organized in 1980 to formulate a research team to design and construct a beam line at NSLS for x-ray diffraction studies of materials. A versatile system was designed to allow a full range of experimental capabilities for wide angle x-ray scattering experiments including surface diffraction studies. The design and construction of the system has been completed. Testing of parts of the system was completed at CHESS and with x-ray sources or other equipment at member institutions. Installation of the beam line at NSLS is in progress and will proceed in parallel with the commissioning of the x-ray ring at NSLS. Full operation of the beam line is expected to be ready by December 1, 1984 being limited only by the source power of NSLS at that time. Useful experiments could be started if the power is at least 2 GeV and 100ma. The MATRIX beam line was one of the first x-ray beam lines to see light in the beam line in early spring of 1984. In July of 1984, the MATRIX beam line as the first port at NSLS to have a monochromatic beam and to scan part of the spectrum from the source. As part of this contract, six publications have resulted from the various projects. Three publications are concerned directly with the beam line and/or its operation while the other three publications are the result of research associated with the project

The structure of pumice by neutron diffraction

International Nuclear Information System (INIS)

Floriano, M.A.; Venezia, A.M.; Deganello, G.; Svensson, E.C.; Root, J.H.

1994-01-01

Small-angle neutron scattering (SANS) and wide-angle neutron scattering (WANS) measurements on pumice, an amorphous natural aluminosilicate used as support for metals in the preparation of catalysts, are reported. The SANS spectrum indicates the presence of a broad size distribution of pores and the absence of volume fractality. Surface fractality, however, cannot be ruled out. The structure of pumice, suggested by the pair-correlation function derived from the WANS spectrum and simulated by a random-network structure model, is very similar to that of vitreous silica, consisting mainly of SiO 4- 4 tetrahedra interconnected by bridging O atoms with additional local disorder generated by the replacement, on average, of one in ten Si atoms by aluminium. (orig.)

New tubes and techniques for flash X-ray diffraction and high contrast radiography

International Nuclear Information System (INIS)

Charbonnier, F.M.; Barbour, J.P.; Brewster, J.L.

High energy electrons are particularly efficient in producing characteristic X-rays and soft polychromatic. A line of wide spectrum beryllium window flash X-ray tubes, ranging from 150 to 600kV, has been developed to exploit this property. Laue and Debye Scherrer flash X-ray diffraction patterns have been obtained using a single 30 ns pulse exposure. X-ray diffraction tests obtained are shown. Extremely high contrast flash radiography of small, low density objects has been obtained using industrial film without screen. Alternatively, particularly at high voltages and for subjects which include a broad range of materials and thicknesses, special film techniques can be used to produce extremely wide latitudes. Equipment, techniques and results are discussed

Selecting a summation base in diffraction transformation of seismic recordings (in an example of Northern Sakhalin)

Energy Technology Data Exchange (ETDEWEB)

Bulatov, M.G.; Telegin, A.N.

1984-01-01

The effect of the dimensions of a processing base on the results of diffraction transformation of seismic recordings is examined. A formula is cited for rating the optimal summation base on the basis of a proposed range of slant angles of the reflecting boundaries. The recommendations for selecting a processing base are confirmed by factual material.

ATTENUATION OF DIFFRACTED MULTIPLES WITH AN APEX-SHIFTED TANGENT-SQUARED RADON TRANSFORM IN IMAGE SPACE

Directory of Open Access Journals (Sweden)

Alvarez Gabriel

2006-12-01

Full Text Available In this paper, we propose a method to attenuate diffracted multiples with an apex-shifted tangent-squared Radon transform in angle domain common image gathers (ADCIG . Usually, where diffracted multiples are a problem, the wave field propagation is complex and the moveout of primaries and multiples in data space is irregular. The method handles the complexity of the wave field propagation by wave-equation migration provided that migration velocities are reasonably accurate. As a result, the moveout of the multiples is well behaved in the ADCIGs. For 2D data, the apex-shifted tangent-squared Radon transform maps the 2D space image into a 3D space-cube model whose dimensions are depth, curvature and apex-shift distance.
Well-corrected primaries map to or near the zero curvature plane and specularly-reflected multiples map to or near the zero apex-shift plane. Diffracted multiples map elsewhere in the cube according to their curvature and apex-shift distance. Thus, specularly reflected as well as diffracted multiples can be attenuated simultaneously. This approach is illustrated with a segment of a 2D seismic line over a large salt body in the Gulf of Mexico. It is shown that ignoring the apex shift compromises the attenuation of the diffracted multiples, whereas the approach proposed attenuates both the specularly-reflected and the diffracted multiples without compromising the primaries.

Contact angle determination procedure and detection of an invisible surface film

Science.gov (United States)

Meyer, G.; Grat, R.

1990-01-01

The contact angle value, i.e., the tangent angle of liquid resting on a planar solid surface, is a basic parameter which can be applied to a wide range of applications. The goal is to provide a basic understanding of the contact angle measurement technique and to present a simple illustration that can be applied as a quality control method; namely, detection of a surface contaminant which exists on a surface that appears clean to the unaided eye. The equipment and experimental procedures are detailed.

Diffraction of 4He atoms from the (001) face of LiF at 10 deg K

International Nuclear Information System (INIS)

Boato, G.; Cantini, P.; Cardillo, M.J.; Tatarek, R.

1974-01-01

A new atom-surface scattering apparatus, which takes advantage of the use of low temperatures, is described. The apparatus allows differential cross section measurements to be carried out with good angular resolution and sensitivity, holding the surface around liquid helium temperatures. The diffractive scattering of a supersonic helium beam from a (001) cleaved LiF surface at 10 deg K was studied. The normalized integrated intensities of all diffracted peaks for normal incidence are given and compared with a quantum surface rainbow theory developed by LEVI et al. The observation of bound state resonances in the peak intensity plotted as a function of incident angle is discussed

High Efficiency Large-Angle Pancharatnam Phase Deflector Based on Dual Twist Design

Science.gov (United States)

2016-12-16

construction and characterization of a ±40° beam steering device with 90% diffraction efficiency based on our dual-twist design at 633nm wavelength...N. & Escuti, M. J. Achromatic Wollaston prism beam splitter using polarization gratings. Opt. Lett. 41, 4461–4463 (2016). 13. Slussarenko, S., et...High-efficiency large-angle Pancharatnam phase deflector based on dual-twist design Kun Gao1, Colin McGinty1, Harold Payson2, Shaun Berry2, Joseph

Large angle tracking and high discriminating tracking in nuclear emulsion

International Nuclear Information System (INIS)

Matsuo, Tomokazu; Shibuya, Hiroshi; Ogawa, Satoru; Fukuda, Tsutomu; Mikado, Shoji

2015-01-01

Nuclear emulsion is a high resolution and re-analyzable detector. Conventional “Track Selector” which have angle acceptance |tan θ|<0.6 are widely used to find tracks in emulsion. We made a new track selector “Fine Track Selector” (FTS) which has large angle acceptance and high discriminating ability. The FTS reduces fake tracks using new algorithms, navigation etc. FTS also keeps finding efficiency of tracks around 90% in an angle range of |tan θ| < 3.5. FTS was applied to the τ candidate in OPERA and no additional tracks found. FTS will be useful to our new J-PARC emulsion experiment.

Design of angle-resolved illumination optics using nonimaging bi-telecentricity for 193 nm scatterfield microscopy.

Science.gov (United States)

Sohn, Martin Y; Barnes, Bryan M; Silver, Richard M

2018-03-01

Accurate optics-based dimensional measurements of features sized well-below the diffraction limit require a thorough understanding of the illumination within the optical column and of the three-dimensional scattered fields that contain the information required for quantitative metrology. Scatterfield microscopy can pair simulations with angle-resolved tool characterization to improve agreement between the experiment and calculated libraries, yielding sub-nanometer parametric uncertainties. Optimized angle-resolved illumination requires bi-telecentric optics in which a telecentric sample plane defined by a Köhler illumination configuration and a telecentric conjugate back focal plane (CBFP) of the objective lens; scanning an aperture or an aperture source at the CBFP allows control of the illumination beam angle at the sample plane with minimal distortion. A bi-telecentric illumination optics have been designed enabling angle-resolved illumination for both aperture and source scanning modes while yielding low distortion and chief ray parallelism. The optimized design features a maximum chief ray angle at the CBFP of 0.002° and maximum wavefront deviations of less than 0.06 λ for angle-resolved illumination beams at the sample plane, holding promise for high quality angle-resolved illumination for improved measurements of deep-subwavelength structures using deep-ultraviolet light.

Powder X-ray diffraction laboratory, Reston, Virginia

Science.gov (United States)

Piatak, Nadine M.; Dulong, Frank T.; Jackson, John C.; Folger, Helen W.

2014-01-01

The powder x-ray diffraction (XRD) laboratory is managed jointly by the Eastern Mineral and Environmental Resources and Eastern Energy Resources Science Centers. Laboratory scientists collaborate on a wide variety of research problems involving other U.S. Geological Survey (USGS) science centers and government agencies, universities, and industry. Capabilities include identification and quantification of crystalline and amorphous phases, and crystallographic and atomic structure analysis for a wide variety of sample media. Customized laboratory procedures and analyses commonly are used to characterize non-routine samples including, but not limited to, organic and inorganic components in petroleum source rocks, ore and mine waste, clay minerals, and glassy phases. Procedures can be adapted to meet a variety of research objectives.

Evaluation of In-Vacuum Imaging Plate Detector for X-Ray Diffraction Microscopy

International Nuclear Information System (INIS)

Nishino, Yoshinori; Takahashi, Yukio; Yamamoto, Masaki; Ishikawa, Tetsuya

2007-01-01

We performed evaluation tests of a newly developed in-vacuum imaging plate (IP) detector for x-ray diffraction microscopy. IP detectors have advantages over direct x-ray detection charge-coupled device (CCD) detectors, which have been commonly used in x-ray diffraction microscopy experiments, in the capabilities for a high photon count and for a wide area. The detector system contains two IPs to make measurement efficient by recording data with the one while reading or erasing the other. We compared speckled diffraction patterns of single particles taken with the IP and a direct x-ray detection CCD. The IP was inferior to the CCD in spatial resolution and in signal-to-noise ratio at a low photon count

Natural and synthetic prion structure from X-ray fiber diffraction

Energy Technology Data Exchange (ETDEWEB)

Wille, Holger; Bian, Wen; McDonald, Michele; Kendall, Amy; Colby, David W.; Bloch, Lillian; Ollesch, Julian; Borovinskiy, Alexander L.; Cohen, Fred E.; Prusiner, Stanley B.; Stubbs, Gerald; (Vanderbilt); (UCSF)

2009-10-21

A conformational isoform of the mammalian prion protein (PrP{sup Sc}) is the sole component of the infectious pathogen that causes the prion diseases. We have obtained X-ray fiber diffraction patterns from infectious prions that show cross-{beta} diffraction: meridional intensity at 4.8 {angstrom} resolution, indicating the presence of {beta} strands running approximately at right angles to the filament axis and characteristic of amyloid structure. Some of the patterns also indicated the presence of a repeating unit along the fiber axis, corresponding to four {beta}-strands. We found that recombinant (rec) PrP amyloid differs substantially from highly infectious brain-derived prions, both in structure as demonstrated by the diffraction data, and in heterogeneity as shown by electron microscopy. In addition to the strong 4.8 {angstrom} meridional reflection, the recPrP amyloid diffraction is characterized by strong equatorial intensity at approximately 10.5 {angstrom}, absent from brain-derived prions, and indicating the presence of stacked {beta}-sheets. Synthetic prions recovered from transgenic mice inoculated with recPrP amyloid displayed structural characteristics and homogeneity similar to those of naturally occurring prions. The relationship between the structural differences and prion infectivity is uncertain, but might be explained by any of several hypotheses: only a minority of recPrP amyloid possesses a replication-competent conformation, the majority of recPrP amyloid has to undergo a conformational maturation to acquire replication competency, or inhibitory forms of recPrP amyloid interfere with replication during the initial transmission.

Dual-mode switching of a liquid crystal panel for viewing angle control

Science.gov (United States)

Baek, Jong-In; Kwon, Yong-Hoan; Kim, Jae Chang; Yoon, Tae-Hoon

2007-03-01

The authors propose a method to control the viewing angle of a liquid crystal (LC) panel using dual-mode switching. To realize both wide viewing angle (WVA) characteristics and narrow viewing angle (NVA) characteristics with a single LC panel, the authors use two different dark states. The LC layer can be aligned homogeneously parallel to the transmission axis of the bottom polarizer for WVA dark state operation, while it can be aligned vertically for NVA dark state operation. The authors demonstrated that viewing angle control can be achieved with a single panel without any loss of contrast at the front.

The basics of crystallography and diffraction

CERN Document Server

Hammond, C

2015-01-01

This title provides a clear and very broadly based introduction to crystallography, light, X-ray, and electron diffraction; a knowledge of which is essential to students in a wide range of scientific disciplines but which is otherwise generally covered in subject-specific and more mathematically detailed texts. The book is also designed to appeal to the more general reader since it shows, by historical and biographical references, how the subject has developed from the work and insights of successive generations of crystallographers and scientists.

Contact angle and local wetting at contact line.

Science.gov (United States)

Li, Ri; Shan, Yanguang

2012-11-06

This theoretical study was motivated by recent experiments and theoretical work that had suggested the dependence of the static contact angle on the local wetting at the triple-phase contact line. We revisit this topic because the static contact angle as a local wetting parameter is still not widely understood and clearly known. To further clarify the relationship of the static contact angle with wetting, two approaches are applied to derive a general equation for the static contact angle of a droplet on a composite surface composed of heterogeneous components. A global approach based on the free surface energy of a thermodynamic system containing the droplet and solid surface shows the static contact angle as a function of local surface chemistry and local wetting state at the contact line. A local approach, in which only local forces acting on the contact line are considered, results in the same equation. The fact that the local approach agrees with the global approach further demonstrates the static contact angle as a local wetting parameter. Additionally, the study also suggests that the wetting described by the Wenzel and Cassie equations is also the local wetting of the contact line rather than the global wetting of the droplet.

Improvement of viewing-zone angle and image quality of digital holograms

Energy Technology Data Exchange (ETDEWEB)

Nomura, Takanori, E-mail: nom@sys.wakayama-u.ac.j [Faculty of Systems Enigneering, Wakayama Univesity, 930 Sakaedani, Wakayama, 640-8510 (Japan)

2010-02-01

The method to improve of a viewing-zone angle and an image quality of a digital hologram is presented. A number of digital holograms of a central object are recorded from the position on the circumference. The holograms are used for a hologram synthesis to improve the image quality from whole viewing-zone angle. The synthesis is achieved by a correlation between a hologram and numerically propagated holograms. The large-sized synthesized digital hologram has a wide viewing-zone angle and less speckles. Some experimental results are shown to confirm the proposed method.

X-ray diffraction of modified and graft polymerised cellulose fibres

International Nuclear Information System (INIS)

Ouajai, S.; Hodzic, A.; Shanks, R.A.

2003-01-01

Full text: The aim of this research is to modify natural cellulosic fibres in order to improve and increase consistency of their performance in biodegradable materials. Fibre modification consisted of solvent extraction and NaOH treatment in order to remove wax and lignin before grafting with acrylonitrile monomer. The mechanical properties, moisture regain and pore structures were investigated. Finally an analysis of crystalline structure was performed using quantitative FTIR, WAXD and SAXS to assess the relationship between structure and properties after modification. Materials: Hemp (Cannabis sativa), Australian Hemp Resource and Manufacture (AHRM) and Flax (Durafibre Grade 1, 95 % purity), Cargill, Canada. Pretreatments: Dewaxing by acetone extraction, alkalisation with NaOH solutions, grafting reaction with acrylonitrile and AIBN thermal initiator after absorption of the monomer. Surface and pore structure analysis using Micromeritics ASAP 2000 BET adsorption instrument, FTIR Perkin-Elmer 2000 spectrometer, wide angle X-ray diffraction, Bruker AXS D8, Ni-filtered CuKα radiation (λ 0.1542 nm) at 40 kV and 35 mA. The diffractograms were recorded from 5 to 60 deg of 2 θ (Bragg angle) by a goniometer with a scintillation counter, scanning speed 0.02 deg/s and sampling rate of 2 data/s. The 2-D small-angle X-ray data was collected by Bruker AXS, Nanostar from 0.5 to 14 deg of 2θ (Bragg angle). Typical exposure time was 5 hours at 40 kV and 35 mA. Single fibre mechanical properties were carried out on a Rheometric DMTA IV at 0.03 mm/min. Moisture regain measurements were performed gravimetrically. The crystalline structure of the fibres were changed from cellulose I to cellulose II after NaOH treatment. The intensity of the 1431 cm -1 band was reduced while the 898 cm -1 band was increased and shifted to 893 cm -1 with an increase of NaOH concentration. X-ray diffractograms of flax and hemp were obtained for each treatment. Untreated fibre shows the

Stress-free reference for neutron diffraction measurement of residual stress in butt-welded joints of austenitic stainless steel pipes

International Nuclear Information System (INIS)

Maekawa, Akira; Takahashi, Tsuneo; Tsuji, Takashi; Suzuki, Hiroshi; Moriai, Atsushi

2012-01-01

Stress-free lattice spacing d_0 has the most influence on reliability of neutron stress measurements made using an angle dispersive method. However, it is hard to evaluate the lattice spacing of welded structures and ductile materials such as stainless steel accurately. In this study, suitable measurement conditions for d_0 of welded pipe joints of austenitic stainless steel were discussed. The d_0 values derived from {311} and {111} reflections, which are often used in austenitic stainless steel for residual stress measurement, were examined. Comparison of the residual strains and stresses evaluated using the obtained d_0 and the finite element analysis showed that the way the d_0 values were chosen affected the measurement accuracy significantly. The stress measurement accuracy was remarkably improved when the {311} reflection was used and the proper d_0 value was chosen in the respective neutron diffraction measurements. For instance, for the axial diffraction measurements using the {311} reflection, it was recommended that only the axial d_0 value of the {311} reflection be used; the measurements using the {111} reflection were less accurate due to the large Young's modulus. Additionally, a lower diffraction angle was judged to be one of the factors leading to a decrease of the strain measurement accuracy. (author)

Diffractive interactions

International Nuclear Information System (INIS)

Del Duca, V.; Marage, P.

1996-08-01

The general framework of diffractive deep inelastic scattering is introduced and reports given in the session on diffractive interactions at the international workshop on deep-inelastic scattering and related phenomena, Rome, April 1996, are presented. (orig.)

An optical super-microscope for far-field, real-time imaging beyond the diffraction limit.

Science.gov (United States)

Wong, Alex M H; Eleftheriades, George V

2013-01-01

Optical microscopy suffers from a fundamental resolution limitation arising from the diffractive nature of light. While current solutions to sub-diffraction optical microscopy involve combinations of near-field, non-linear and fine scanning operations, we hereby propose and demonstrate the optical super-microscope (OSM) - a superoscillation-based linear imaging system with far-field working and observation distances - which can image an object in real-time and with sub-diffraction resolution. With our proof-of-principle prototype we report a point spread function with a spot size clearly reduced from the diffraction limit, and demonstrate corresponding improvements in two-point resolution experiments. Harnessing a new understanding of superoscillations, based on antenna array theory, our OSM achieves far-field, sub-diffraction optical imaging of an object without the need for fine scanning, data post-processing or object pre-treatment. Hence the OSM can be used in a wide variety of imaging applications beyond the diffraction limit, including real-time imaging of moving objects.

Angle-independent structural colors of silicon

DEFF Research Database (Denmark)

Højlund-Nielsen, Emil; Weirich, Johannes; Nørregaard, Jesper

2014-01-01

Structural colors are optical phenomena of physical origin, where microscale and nanoscale structures determine the reflected spectrum of light. Artificial structural colors have been realized within recent years. However, multilayer structures require substantial fabrication. Instead we considered...... one-layer surface textures of silicon.We explored four patterns of square structures in a square lattice with periods of 500, 400, 300, and 200 nm. The reflectivity and daylight-colors were measured and compared with simulations based on rigorously coupledwave analysis with excellent agreement. Based...... on the 200-nm periodic pattern, it was found that angle-independent specular colors up to 60 deg of incidence may be provided. The underlying mechanisms include (1) the suppression of diffraction and (2) a strong coupling of light to localized surface states. The strong coupling yields absorption anomalies...

Compositional images from the Diffraction Enhanced Imaging technique

International Nuclear Information System (INIS)

Hasnah, M.O.; Zhong, Z.; Parham, C.; Zhang, H.; Chapman, D.

2007-01-01

Diffraction Enhanced Imaging (DEI) derives X-ray contrast from absorption, refraction, and extinction. While the refraction angle image of DEI represents the gradient of the projected mass density of the object, the absorption image measures the projected attenuation (μt)-bar of an object. Using a simple integral method it has been shown that a mass density image (ρt)-bar can be obtained from the refraction angle image. It then is a simple matter to develop a combinational image by dividing these two images to create a μ/ρ image. The μ/ρ is a fundamental property of a material and is therefore useful for identifying the composition of an object. In projection X-ray imaging the μ/ρ image identifies the integrated composition of the elements along the beam path. When applied to DEI computed tomography (CT), the image identifies the composition in each voxel. This method presents a new type of spectroscopy based in radiography. We present the method of obtaining the compositional image, the results of experiments in which we verify the method with known standards and an application of the method to breast cancer imaging

Diffraction coherence in optics

CERN Document Server

Françon, M; Green, L L

2013-01-01

Diffraction: Coherence in Optics presents a detailed account of the course on Fraunhofer diffraction phenomena, studied at the Faculty of Science in Paris. The publication first elaborates on Huygens' principle and diffraction phenomena for a monochromatic point source and diffraction by an aperture of simple form. Discussions focus on diffraction at infinity and at a finite distance, simplified expressions for the field, calculation of the path difference, diffraction by a rectangular aperture, narrow slit, and circular aperture, and distribution of luminous flux in the airy spot. The book th

Improved Resolution Optical Time Stretch Imaging Based on High Efficiency In-Fiber Diffraction.

Science.gov (United States)

Wang, Guoqing; Yan, Zhijun; Yang, Lei; Zhang, Lin; Wang, Chao

2018-01-12

Most overlooked challenges in ultrafast optical time stretch imaging (OTSI) are sacrificed spatial resolution and higher optical loss. These challenges are originated from optical diffraction devices used in OTSI, which encode image into spectra of ultrashort optical pulses. Conventional free-space diffraction gratings, as widely used in existing OTSI systems, suffer from several inherent drawbacks: limited diffraction efficiency in a non-Littrow configuration due to inherent zeroth-order reflection, high coupling loss between free-space gratings and optical fibers, bulky footprint, and more importantly, sacrificed imaging resolution due to non-full-aperture illumination for individual wavelengths. Here we report resolution-improved and diffraction-efficient OTSI using in-fiber diffraction for the first time to our knowledge. The key to overcome the existing challenges is a 45° tilted fiber grating (TFG), which serves as a compact in-fiber diffraction device offering improved diffraction efficiency (up to 97%), inherent compatibility with optical fibers, and improved imaging resolution owning to almost full-aperture illumination for all illumination wavelengths. 50 million frames per second imaging of fast moving object at 46 m/s with improved imaging resolution has been demonstrated. This conceptually new in-fiber diffraction design opens the way towards cost-effective, compact and high-resolution OTSI systems for image-based high-throughput detection and measurement.

Periodic order and defects in Ni-based inverse opal-like crystals on the mesoscopic and atomic scale

NARCIS (Netherlands)

Chumakova, A. V.; Valkovskiy, G. A.; Mistonov, A. A.; Dyadkin, V. A.; Grigoryeva, N. A.; Sapoletova, N. A.; Napolskii, K. S.; Eliseev, A. A.; Petukhov, Andrei V.; Grigoriev, S. V.

2014-01-01

The structure of inverse opal crystals based on nickel was probed on the mesoscopic and atomic levels by a set of complementary techniques such as scanning electron microscopy and synchrotron microradian and wide-angle diffraction. The microradian diffraction revealed the mesoscopic-scale

Near-surface density profiling of Fe ion irradiated Si (100) using extremely asymmetric x-ray diffraction by variation of the wavelength

Energy Technology Data Exchange (ETDEWEB)

Khanbabaee, B., E-mail: khanbabaee@physik.uni-siegen.de; Pietsch, U. [Solid State Physics, University of Siegen, D-57068 Siegen (Germany); Facsko, S. [Helmholtz-Zentrum Dresden-Rossendorf, 01314 Dresden (Germany); Doyle, S. [Synchrotron Light Source ANKA, Hermann-von-Helmholtz-Platz 1, D-76344 Eggenstein-Leopoldshafen (Germany)

2014-10-20

In this work, we report on correlations between surface density variations and ion parameters during ion beam-induced surface patterning process. The near-surface density variations of irradiated Si(100) surfaces were investigated after off-normal irradiation with 5 keV Fe ions at different fluences. In order to reduce the x-ray probing depth to a thickness below 5 nm, the extremely asymmetrical x-ray diffraction by variation of wavelength was applied, exploiting x-ray refraction at the air-sample interface. Depth profiling was achieved by measuring x-ray rocking curves as function of varying wavelengths providing incidence angles down to 0°. The density variation was extracted from the deviations from kinematical Bragg angle at grazing incidence angles due to refraction of the x-ray beam at the air-sample interface. The simulations based on the dynamical theory of x-ray diffraction revealed that while a net near-surface density decreases with increasing ion fluence which is accompanied by surface patterning, there is a certain threshold of ion fluence to surface density modulation. Our finding suggests that the surface density variation can be relevant with the mechanism of pattern formation.

Theory of near-critical-angle scattering from a curved interface

International Nuclear Information System (INIS)

Fiedler-Ferrari, N.; Nussenzveig, H.M.; Wiscombe, W.J.

1990-01-01

A new type of diffraction effect, different from the standard semiclassical ones (rainbow, glory, forward peak, orbiting), takes place near the critical angle for total reflection at a curved interface between two homogeneous media. A theoretical treatment of this new effects is given for Mie scattering, e.g., light scattering by an air bubble in water; it can readily be extended to more general curved interface problems in a variety of different fields (quantum mechanics, acoustics, seismic waves). The relatively slowly-varying Mie diffraction pattern associated with near-critical scattering is obscured by rapid fine-structure oscillations due to interference with unrelated farside contributions. These contributions are evaluated and subtracted from the Mie amplitudes to yield the relevant nearside effects. A zero-order transitional CAM (complex angular momentum) approximation to the nearside amplitude is developed. The most important contributions arise from partial and total reflection, represented by two new diffraction integrals, designated Fresnel-Fock and Pearcey-Fock respectively. Also discussed are the WKB approximation, a known physical optics approximation and a new modified version of this approximation: they are compared with the exact nearside Mie amplitude obtained by numerical partial-wave summation, at scatterer size parameters (circumference/wavelength) ranging from 1,000 to 10,000. (author)

ADVANTAGES OF DIFFRACTIVE OPTICAL ELEMENTS APPLICATION IN SIMPLE OPTICAL IMAGING SYSTEMS

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N. D. Zoric

2015-01-01

Full Text Available The paper deals with the influence of diffractive optical elements on the optical aberrations. The correction of optical aberrations was investigated in the simple optical systems with one and two lenses (singlet and doublet. The advantages of diffractive optical elements are their ability to generate arbitrary complex wave fronts from a piece of optical material that is essentially flat. The optical systems consisting of the standard surfaces were designed and optimized by using the same starting points. Further, the diffractive and aspheric surfaces were introduced into the developed systems. The resulting hybrid systems were optimized. To compare the complicity of the development of narrow field systems and wide field optical systems, the optimization has been done separately for these two types of the instruments. The optical systems were designed by using special Optical Design Software. Тhe characteristics of designed diffractive surfaces were controlled in Software DIFSYS 2.30. Due to the application of diffractive optical elements the longitudinal chromatic aberration was 5 times reduced for the narrow field systems. The absolute value of Seidel coefficient related to the spherical aberration was reduced in the range of 0.03. Considering that diffractive optical elements have the known disadvantages, like possible parasitic diffraction orders and probable decrease of the transmission, we also developed and analyzed the optical systems with combined aspheric and diffractive surfaces. A combination of the aspheric and diffractive surfaces in the optical disk system of the disk reading lens, gave cutting down of the longitudinal color aberrations almost 15 times on-axis, comparing to the lens consisting of the aspherical and standard surfaces. All of the designed diffractive optical elements possess the parameters within the fabrication limits.

X-ray diffraction characteristics of curved monochromators for sychrotron radiation

International Nuclear Information System (INIS)

Boeuf, A.; Rustichelli, F.; Mazkedian, S.; Puliti, P.; Melone, S.

1978-01-01

A theoretical study is presented concerning the diffraction characteristics of curved monochromators for X-ray synchrotron radiation used at the laboratories of Hamburg, Orsay and Stanford. The investigation was performed by extending to the X-ray case a simple model recently developed and fruitfully employed to describe the neutron diffraction properties of curved monochromators. Several diffraction patterns were obtained corresponding to different monochromator materials (Ge, Si) used by the different laboratories, for different reflecting planes (111), (220), asymmetry angles, X-ray wave-lengths (Mo Kα, Cu Kα, Cr Kα) and curvature radii. The results are discussed in physical terms and their implications on the design of curved monochromators for synchrotron radiation are presented. In particular, the study shows that all the monochromators used in the different laboratories should behave practically as perfect crystals and therefore should have a very low integrated reflectivity corresponding to an optimized wavelength passband Δlambda/lambda approximately 10 -4 . The gain that can be obtained by increasing the curvature, by introducing a gradient in the lattice spacing or by any other kind of imperfection is quite limited and much lower than the desirable value. The adopted model can help in obtaining a possible moderate gain in intensity by also taking into consideration other parameters, such as crystal material, reflecting plane, asymmetry of the reflection and X-ray wavelength. (Auth.)

Small-angle neutron scattering study of high-pressure sintered detonation nanodiamonds

Energy Technology Data Exchange (ETDEWEB)

Kidalov, S. V.; Shakhov, F. M., E-mail: fedor.shakhov@mail.ioffe.ru [Ioffe Physical-Technical Institute of the Russian Academy of Sciences (Russian Federation); Lebedev, V. T.; Orlova, D. N.; Grushko, Yu. S. [Russian Academy of Sciences, Konstantinov St. Petersburg Nuclear Physics Institute (Russian Federation)

2011-12-15

The structure of detonation diamonds sintered at a high pressure (7 GPa) and temperatures of 1200-1700 Degree-Sign C has been investigated by small-angle neutron scattering. It is shown that sintering leads to an increase in the particle size from 6 to 30 nm and established that this increase is due to the chainlike oriented attachment of particles. This study supplements the oriented-attachment model, which was suggested based on the X-ray diffraction spectra of detonation nanodiamonds (DNDs) sintered under the same conditions.

Capillary Rise: Validity of the Dynamic Contact Angle Models.

Science.gov (United States)

Wu, Pingkeng; Nikolov, Alex D; Wasan, Darsh T

2017-08-15

The classical Lucas-Washburn-Rideal (LWR) equation, using the equilibrium contact angle, predicts a faster capillary rise process than experiments in many cases. The major contributor to the faster prediction is believed to be the velocity dependent dynamic contact angle. In this work, we investigated the dynamic contact angle models for their ability to correct the dynamic contact angle effect in the capillary rise process. We conducted capillary rise experiments of various wetting liquids in borosilicate glass capillaries and compared the model predictions with our experimental data. The results show that the LWR equations modified by the molecular kinetic theory and hydrodynamic model provide good predictions on the capillary rise of all the testing liquids with fitting parameters, while the one modified by Joos' empirical equation works for specific liquids, such as silicone oils. The LWR equation modified by molecular self-layering model predicts well the capillary rise of carbon tetrachloride, octamethylcyclotetrasiloxane, and n-alkanes with the molecular diameter or measured solvation force data. The molecular self-layering model modified LWR equation also has good predictions on the capillary rise of silicone oils covering a wide range of bulk viscosities with the same key parameter W(0), which results from the molecular self-layering. The advantage of the molecular self-layering model over the other models reveals the importance of the layered molecularly thin wetting film ahead of the main meniscus in the energy dissipation associated with dynamic contact angle. The analysis of the capillary rise of silicone oils with a wide range of bulk viscosities provides new insights into the capillary dynamics of polymer melts.

Structural transformation of compressed solid Ar: An x-ray diffraction study to 114 GPa

International Nuclear Information System (INIS)

Errandonea, D.; Boehler, R.; Japel, S.; Mezouar, M.; Benedetti, L. R.

2006-01-01

Room temperature angle-dispersive x-ray diffraction measurements on solid Ar up to 114 GPa reveal evidence of a structural phase transformation after stress relaxation by laser heating. Beyond 49.6 GPa, Ar exhibits the coexistence of fcc and hcp phases with an increasing hcp/fcc ratio, similar to the observation made recently on krypton and xenon. From the present results, we estimate the fcc-to-hcp transition to be completed at 300 GPa

Contact angle adjustment in equation-of-state-based pseudopotential model.

Science.gov (United States)