Experimental hot-wire measurements in a centrifugal compressor with vaned diffuser

International Nuclear Information System (INIS)

Pinarbasi, Ali

2008-01-01

The purpose of this study was to improve the understanding of the flow physics in a centrifugal compressor with vaned diffuser. For this reason three component hot wire measurements in the vaneless space and vane region of a low speed centrifugal compressor are presented. A low speed compressor with a 19 bladed backswept impeller and diffuser with 16 wedge vanes were used. The measurements were made at three inter-vane positions and are presented as mean velocity, turbulent kinetic energy and flow angle distributions. The flow entering the diffuser closely resembles the classic jet-wake flow characteristic of centrifugal impeller discharges. A strong upstream influence of the diffuser vanes is observed which results in significant variations in flow quantities between the vane-to-vane locations. The circumferential variations due to the passage and blade wakes rapidly mix out in the vaneless space, although some variations are still discernible in the vaned region. The impeller blade wakes mix out rapidly within the vaneless space and more rapidly than in an equivalent vaneless diffuser. Although the flow is highly non uniform in velocity at the impeller exit, there is no evidence in the results of any separation from the diffuser vanes

Numerical Analysis and Geometry Optimisation of Vertical Vane of Room Air-conditioner

Directory of Open Access Journals (Sweden)

Al-Obaidi Abdulkareem Sh. Mahdi

2018-01-01

Full Text Available Vertical vanes of room air-conditioners are used to control and direct cold air. This paper aims to study vertical vane as one of the parameters that affect the efficiency of dissipating cold air to a given space. The vertical vane geometry is analysed and optimised for lower production cost using CFD. The optimised geometry of the vertical vane should have the same or increased efficiency of dissipating cold air and have lesser mass compared to the existing original design. The existing original design of vertical vane is simplified and analysed by using ANSYS Fluent. Efficiency of wind direction is define as how accurate the direction of airflow coming out from vertical vane. In order to calculate the efficiency of wind direction, 15° and 30° rotation of vertical vane inside room air-conditioner are simulated. The efficiency of wind direction for 15° rotation of vertical vane is 57.81% while efficiency of wind direction for 30° rotation of vertical vane is 47.54%. The results of the efficiency of wind direction are used as base reference for parametric study. The parameters investigated for optimisation of vertical vane are focused at length of long span, tip chord and short span. The design of 15% decreased in vane surface area at tip chord is the best optimised design of vertical vane because the efficiency of wind direction is the highest as 60.32%.

A three dimensional model of a vane rheometer

International Nuclear Information System (INIS)

Nazari, Behzad; Moghaddam, Ramin Heidari; Bousfield, Douglas

2013-01-01

Highlights: • FEM was used to calculate the isothermal flow parameters in a vane geometry. • Velocity, pressure and then stress fields were obtained. • Using total stress, shaft torque was calculated to compare with experimental data. • A modified cell Reynolds number and power number were used to study flow pattern. • A comparison between 2D and 3D modeling was done based on calculated torques. -- Abstract: Vane type geometries are often used in rheometers to avoid slippage between the sample and the fixtures. While yield stress and other rheological properties can be obtained with this geometry, a complete analysis of this complex flow field is lacking in the literature. In this work, a finite element method is used to calculate the isothermal flow parameters in a vane geometry. The method solves the mass and momentum continuity equations to obtain velocity, pressure and then stress fields. Using the total stress numerical data, we calculated the torque applied on solid surfaces. The validity of the computational model was established by comparing the results to experimental results of shaft torque at different angular velocities. The conditions where inertial terms become important and the linear relationship between torque and stress are quantified with dimensionless groups. The accuracy of a two dimensional analysis is compared to the three dimensional results

Solar energy system with wind vane

Science.gov (United States)

Grip, Robert E

2015-11-03

A solar energy system including a pedestal defining a longitudinal axis, a frame that is supported by the pedestal and that is rotateable relative to the pedestal about the longitudinal axis, the frame including at least one solar device, and a wind vane operatively connected to the frame to urge the frame relative to the pedestal about the longitudinal axis in response to wind acting on the wind vane.

Optimization analysis of a new vane MRF damper

Energy Technology Data Exchange (ETDEWEB)

Zhang, J Q; Feng, Z Z; Jing, Q [Department of Technical Support Engineering, Academy of Armored Force Engineering, Beijing, 100072 (China)], E-mail: zhangjq63@yahoo.com.cn

2009-02-01

The primary purpose of this study was to provide the optimization analysis certain characteristics and benefits of a vane MRF damper. Based on the structure of conventional vane hydraulic damper for heavy vehicle, a narrow arc gap between clapboard and rotary vane axle, which one rotates relative to the other, was designed for MRF valve and the mathematical model of damping was deduced. Subsequently, the finite element analysis of electromagnetic circuit was done by ANSYS to perform the optimization process. Some ways were presented to augment the damping adjustable multiple under the condition of keeping initial damping forces and to increase fluid dwell time through the magnetic field. The results show that the method is useful in the design of MR dampers and the damping adjustable range of vane MRF damper can meet the requirement of heavy vehicle semi-active suspension system.

Turbocharger with variable nozzle having vane sealing surfaces

Science.gov (United States)

Arnold, Philippe [Hennecourt, FR; Petitjean, Dominique [Julienrupt, FR; Ruquart, Anthony [Thaon les Vosges, FR; Dupont, Guillaume [Thaon les Vosges, FR; Jeckel, Denis [Thaon les Vosges, FR

2011-11-15

A variable nozzle for a turbocharger includes a plurality of vanes rotatably mounted on a nozzle ring and disposed in a nozzle flow path defined between the nozzle ring and an opposite nozzle wall. Either or both of the faces of the nozzle ring and nozzle wall include(s) at least one step that defines sealing surfaces positioned to be substantially abutted by airfoil surfaces of the vanes in the closed position of the vanes and to be spaced from the airfoil surfaces in positions other than the closed position. This substantial abutment between the airfoil surfaces and the sealing surfaces serves to substantially prevent exhaust gas from leaking past the ends of the airfoil portions. At the same time, clearances between the nozzle ring face and the end faces of the airfoil portions can be sufficiently large to prevent binding of the vanes under all operating conditions.

Demonstration and Field Evaluation of Streambank Stabilization with Submerged Vanes

Science.gov (United States)

Whitman, H.; Hoopes, J.; Poggi, D.; Fitzpatrick, F.; Walz, K.; ,

2001-01-01

The effectiveness of submerged vanes for reducing bank erosion and improving aquatic habitat is being evaluated at a site on North Fish Creek, a Lake Superior tributary. Increased runoff from agricultural areas with clayey soils has increased flood magnitudes and the erosion potential/transport capacity of the stream. Most of the creek's sediment load originates from the erosion of 17 large bluffs. This creek contains important recreational fisheries that are potentially limited by the loss of aquatic habitat from deposition of sediment on spawning beds. Submerged vanes are a cost effective and environmentally less intrusive alternative to traditional structural stabilization measures. Submerged vanes protrude from a channel bed, are oriented at an angle to the local velocity, and are distributed along a portion of channel. They induce a transverse force and torque on the flow along with longitudinal vortexes that alter the cross sectional shape and alignment of the channel. Submerged vanes were installed at a bluff/bend site in summer and fall 2000. The number, size, and layout of the vanes were based upon the channel morphology under estimated bankfull conditions. The effectiveness of the vanes will be evaluated by comparing surveys of the bluff face, streamflow, and channel conditions for several years after installation of the submerged vanes with surveys before and immediately after their installation.

Suppression of tonal noise in a centrifugal fan using guide vanes

Science.gov (United States)

Paramasivam, Kishokanna; Rajoo, Srithar; Romagnoli, Alessandro

2015-11-01

This paper presents the work aiming for tonal noise reduction in a centrifugal fan. In previous studies, it is well documented that tonal noise is the dominant noise source generated in centrifugal fans. Tonal noise is generated due to the aerodynamic interaction between the rotating impeller and stationary diffuser vanes. The generation of tonal noise is related to the pressure fluctuation at the leading edge of the stationary vane. The tonal noise is periodic in time which occurs at the blade passing frequency (BPF) and its harmonics. Much of previous studies, have shown that the stationary vane causes the tonal noise and generation of non-rotational turbulent noise. However, omitting stationary vanes will lead to the increase of non-rotational turbulent noise resulted from the high velocity of the flow leaving the impeller. Hence in order to reduce the tonal noise and the non-rotational noise, guide vanes were designed as part of this study to replace the diffuser vanes, which were originally used in the chosen centrifugal fan. The leading edge of the guide vane is tapered. This modification reduces the strength of pressure fluctuation resulting from the interaction between the impeller outflow and stationary vane. The sound pressure level at blade passing frequency (BPF) is reduced by 6.8 dB, the 2nd BPF is reduced by 4.1 dB and the 3rd BPF reduced by about 17.5 dB. The overall reduction was 0.9 dB. The centrifugal fan with tapered guide vanes radiates lower tonal noise compared to the existing diffuser vanes. These reductions are achieved without compromising the performance of the centrifugal fan. The behavior of the fluid flow was studied using computational fluid dynamics (CFD) tools and the acoustics characteristics were determined through experiments in an anechoic chamber.

Study on Orbital Liquid Transport and Interface Behavior in Vane Tank

Science.gov (United States)

Kang, Qi; Rui, Wei

2016-07-01

Liquid propellant tank is used to supply gas free liquid for spacecraft as an important part of propulsion system. The liquid behavior dominated by surface tension in microgravity is obviously different with that on the ground, which put forward a new challenge to the liquid transport and relocation. The experiments which are investigated at drop tower in National Microgravity Lab have concentrated on liquid relocation following thruster firing. Considered that the liquid located at the bottom in the direction of the acceleration vector, a sphere scale vane tank is used to study the liquid-gas interface behaviors with different acceleration vector and different filling independently and we obtain a series of stable equilibrium interface and relocation time. We find that there is an obvious sedimentation in the direction of acceleration vector when fill rate greater than 2% fill. Suggestions have been put forward that outer vanes transferring liquid to the outlet should be fixed and small holes should be dogged at the vane close to the center post to improve the liquid flow between different vanes when B0 is greater than 2.5. The research about liquid transport alone ribbon vanes is simulated though software Flow3D. The simulation process is verified by comparing the liquid lip and vapor-liquid interface obtained from drop tower experiment and simulation result when fill rate is 15%. Then the influence of fill rate, numbers of vanes and the gap between vane and wall is studied through the same simulate process. Vanes' configurations are also changed to study the effect on the lip and liquid volume below some section. Some suggestions are put forward for the design of vanes.

Bed erosion control at 60 degree river confluence using vanes

Science.gov (United States)

Wuppukondur, Ananth; Chandra, Venu

2017-04-01

Confluences are common occurrences along natural rivers. Hydrodynamics at the confluence is complex due to merging of main and lateral flows with different characteristics. Bed erosion occurs at the confluence due to turbulence and also secondary circulation induced by centrifugal action of the lateral flow. The eroded sediment poses various problems in the river ecosystem including river bank failure. Reservoirs are majorly affected due to sediment deposition which reduces storage capacity. The bed erosion also endangers stability of pipeline crossings and bridge piers. The aim of this experimental study is to check the performance of vanes in controlling bed erosion at the confluence. Experiments are performed in a 600 confluence mobile bed model with a non-uniform sediment of mean particle size d50 = 0.28mm. Discharge ratio (q=ratio of lateral flow discharge to main flow discharge) is maintained as 0.5 and 0.75 with a constant average main flow depth (h) of 5cm. Vanes of width 0.3h (1.5cm) and thickness of 1 mm are placed along the mixing layer at an angle of 150, 300 and 600(with respect to main flow) to perform the experiments. Also, two different spacing of 2h and 3h (10cm and 15cm) between the vanes are used for conducting the experiments. A digital point gauge with an accuracy of ±0.1mm is used to measure bed levels and flow depths at the confluence. An Acoustic Doppler Velocitimeter (ADV) with a frequency of 25Hz and accuracy of ±1mm/s is used to measure flow velocities. Maximum scour depth ratio Rmax, which is ratio between maximum scour depth (Ds) and flow depth (h), is used to present the experimental results.From the experiments without vanes, it is observed that the velocities are increasing along the mixing layer and Rmax=0.82 and 1.06, for q=0.5 and 0.75, respectively. The velocities reduce with vanes since roughness increases along the mixing layer. For q=0.5 and 0.75, Rmax reduces to 0.62 and 0.7 with vanes at 2h spacing, respectively. Similarly

Hot spot detection system for vanes or blades of a combustion turbine

Science.gov (United States)

Twerdochlib, M.

1999-02-02

This invention includes a detection system that can determine if a turbine component, such as a turbine vane or blade, has exceeded a critical temperature, such as a melting point, along any point along the entire surface of the vane or blade. This system can be employed in a conventional combustion turbine having a compressor, a combustor and a turbine section. Included within this system is a chemical coating disposed along the entire interior surface of a vane or blade and a closed loop cooling system that circulates a coolant through the interior of the vane or blade. If the temperature of the vane or blade exceeds a critical temperature, the chemical coating will be expelled from the vane or blade into the coolant. Since while traversing the closed loop cooling system the coolant passes through a detector, the presence of the chemical coating in the coolant will be sensed by the system. If the chemical coating is detected, this indicates that the vane or blade has exceeded a critical temperature. 5 figs.

Powerful Swirl Generation of Flow-driven Rotating Mixing Vane for Enhancing CHF

International Nuclear Information System (INIS)

Seo, Han; Seo, Seok Bin; Heo, Hyo; Bang, In Cheol

2014-01-01

Mixing vanes are utilized to improve CHF and heat transfer performance in the rod bundle during normal operation. Experimental measurement of the swirling flow from a split vane pair was conducted using particle image velocimetry (PIV) and boroscope. The lateral velocity fields show that the swirling flow was initially centered in the subchannel and the computational fluid dynamics (CFD) analysis was performed based on the experiment. To visualize flow patterns in the 5Χ5 subchannel using PIV, matching the refraction between the working fluid and the structure was considered and the experiment aimed to develop the experimental data for providing fundamental information of the CFD analysis. The fixed split vane is the main mixing inducer in the fuel assembly. In a heat exchanger research, propeller type swirl generates at several pitch ratios and different blades angles were used to enhance heat transfer rate. Significant improvements of the heat transfer rate using the propellers were confirmed due to creation of tangential flow. In the present study, the mixing effect of rotation vane which has a shape of propeller was studied using PIV. A split vane was considered in the experiment to show the effect of rotation vane. Vertical and horizontal flow analyses were conducted to show the possible use of rotation vane in a subchannel. In the present work, the study of flow visualization using three types of vanes is conducted to show the mixing effect. The vertical flow and the horizontal flow distributions were analyzed in the two experimental facilities. For the vertical flow facility, flow distributions, flow profiles, and the turbulence kinetic energy are analyzed at the centerline of the channel. The results show that the rotation vane has the highest flow and turbulence kinetic intensity at the centerline of the channel. For the horizontal flow facility, the results indicate that lateral flow of the rotation vane is generated and maintained along with the flow

A new wind vane for the measurement of atmospheric turbulence

Energy Technology Data Exchange (ETDEWEB)

Parker, M.J.; Heverly, M.

1997-02-01

A Cooperative Research and Development Agreement (CRADA) between Met One Instruments, Incorporated (Met One) and Westinghouse Savannah River Company (WSRC) was created to develop a new wind vane that more accurately measures atmospheric turbulence. Through a process that had several phases, Met One created a prototype vane that was designed to attach to the existing Model 1585 Bi-Directional Wind Vane instrument structure. The prototype contained over 20% less mass to enhance responsiveness, which was also increased through the use of a teardrop-shaped fin structure. The prototype vane can be readily manufactured for commercial retail. Tests in wind tunnel of Building 735-7A, the Meteorological Engineering Facility, indicated that the new vane has a superior starting threshold of less than 0.14 meter per second, a delay distance of 0.72 meter, and a damping ratio of 0.4. The relative accuracy of less than one degree is unchanged from the previous design. The vane bias was acceptable at 0.8 degree for the horizontal wind angle, but was slightly high at 1.4 degree for the verticle wind angle. The high value of the verticle wind angle bias can most likely be reduced to the desired less than one degree value with standard manufacturing production techniques. The durability of the prototype vane was not tested in the field but is expected to be slightly less due to the use of hollow rather than foam-filled fins. However, the loss of some durability is more than compensated with increased sensitivity at low wind speeds. Field testing of the prototype is required to test for adequacy of durability.

Numerical modelling of multi-vane expander operating conditions in ORC system

Science.gov (United States)

Rak, Józef; Błasiak, Przemysław; Kolasiński, Piotr

2017-11-01

Multi-vane expanders are positive displacement volumetric machines which are nowadays considered for application in micro-power domestic ORC systems as promising alternative to micro turbines and other volumetric expanders. The multi-vane expander features very simple design, low gas flow capacity, low expansion ratios, an advantageous ratio of the power output to the external dimensions and are insensitive to the negative influence of the gas-liquid mixture expansion. Moreover, the multi-vane expander can be easily hermetically sealed, which is one of the key issues in the ORC system design. A literature review indicates that issues concerning the application of multi-vane expanders in such systems, especially related to operating of multi-vane expander with different low-boiling working fluids, are innovative, not fully scientifically described and have the potential for practical implementation. In this paper the results of numerical investigations on multi-vane expander operating conditions are presented. The analyses were performed on three-dimensional numerical model of the expander in ANSYS CFX software. The numerical model of the expander was validated using the data obtained from the experiment carried out on a lab test-stand. Then a series of computational analysis were performed using expanders' numerical model in order to determine its operating conditions under various flow conditions of different working fluids.

Split coaxial RFQ structure with modulated vanes

International Nuclear Information System (INIS)

Arai, S.

1983-10-01

A new split coaxial RFO structure with modulated vanes is proposed. The structure is designed to accelerate 238 U 4+ from 1.68 keV/u to 45.1 keV/u at frequency of 12.5 MHz. The cavity is 1.6 m in diameter and 8 m in length. The cavity consists of four cavity modules divided by three stems which support horizontal and vertical vanes periodically and alternatively. At the same time, problems on the beam dynamics and design procedures are described and discussed. (orig.)

Numerical analysis and experiment research on fluid orbital performance of vane type propellant management device

International Nuclear Information System (INIS)

Hu, Q; Li, Y; Pan, H L; Liu, J T; Zhuang, B T

2015-01-01

Vane type propellant management device (PMD) is one of the key components of the vane-type surface tension tank (STT), and its fluid orbital performance directly determines the STT's success or failure. In present paper, numerical analysis and microgravity experiment study on fluid orbital performance of a vane type PMD were carried out. By using two-phase flow model of volume of fluid (VOF), fluid flow characteristics in the tank with the vane type PMD were numerically calculated, and the rules of fluid transfer and distribution were gotten. A abbreviate model test system of the vane type PMD is established and microgravity drop tower tests were performed, then fluid management and transmission rules of the vane type PMD were obtained under microgravity environment. The analysis and tests results show that the vane type PMD has good and initiative fluid orbital management ability and meets the demands of fluid orbital extrusion in the vane type STT. The results offer valuable guidance for the design and optimization of the new generation of vane type PMD, and also provide a new approach for fluid management and control in space environment

Fluid-structure coupling in the guide vanes cascade of a pump-turbine scale model

International Nuclear Information System (INIS)

Roth, S; Hasmatuchi, V; Botero, F; Farhat, M; Avellan, F

2010-01-01

The present study concerns fluid-structure coupling phenomena occurring in a guide vane cascade of a pump-turbine scale model placed in the EPFL PF3 test rig. An advanced instrument set is used to monitor both vibrating structures and the surrounding flow. The paper highlights the interaction between vibrating guide vanes and the flow behavior. The pressure fluctuations in the stay vanes region are found to be strongly influenced by the amplitude of the vibrating guide vanes. Moreover, the flow induces different hydrodynamic damping on the vibrating guide vanes depending on the operating point of the pump-turbine.

Fluid-structure coupling in the guide vanes cascade of a pump-turbine scale model

Science.gov (United States)

Roth, S.; Hasmatuchi, V.; Botero, F.; Farhat, M.; Avellan, F.

2010-08-01

The present study concerns fluid-structure coupling phenomena occurring in a guide vane cascade of a pump-turbine scale model placed in the EPFL PF3 test rig. An advanced instrument set is used to monitor both vibrating structures and the surrounding flow. The paper highlights the interaction between vibrating guide vanes and the flow behavior. The pressure fluctuations in the stay vanes region are found to be strongly influenced by the amplitude of the vibrating guide vanes. Moreover, the flow induces different hydrodynamic damping on the vibrating guide vanes depending on the operating point of the pump-turbine.

Numerical modelling of multi-vane expander operating conditions in ORC system

Directory of Open Access Journals (Sweden)

Rak Józef

2017-01-01

Full Text Available Multi-vane expanders are positive displacement volumetric machines which are nowadays considered for application in micro-power domestic ORC systems as promising alternative to micro turbines and other volumetric expanders. The multi-vane expander features very simple design, low gas flow capacity, low expansion ratios, an advantageous ratio of the power output to the external dimensions and are insensitive to the negative influence of the gas-liquid mixture expansion. Moreover, the multi-vane expander can be easily hermetically sealed, which is one of the key issues in the ORC system design. A literature review indicates that issues concerning the application of multi-vane expanders in such systems, especially related to operating of multi-vane expander with different low-boiling working fluids, are innovative, not fully scientifically described and have the potential for practical implementation. In this paper the results of numerical investigations on multi-vane expander operating conditions are presented. The analyses were performed on three-dimensional numerical model of the expander in ANSYS CFX software. The numerical model of the expander was validated using the data obtained from the experiment carried out on a lab test-stand. Then a series of computational analysis were performed using expanders' numerical model in order to determine its operating conditions under various flow conditions of different working fluids.

Vane-Cam - camshaft controls with new functionalities; Vane-Cam - Nockenwellenversteller mit neuen Funktionalitaeten

Energy Technology Data Exchange (ETDEWEB)

Knecht, A.; Pohl, D. [Hydraulik-Ring GmbH, Nuertingen (Germany); Hannibal, W. [Fachhochschule Suedwestfalen, Iserlohn (Germany). Labor fuer Konstruktion und CAE-Anwendungen; enTec Consulting GmbH, Hemer (Germany)

2007-01-15

Infinitely variable camshaft phasing systems will be used in the future in practically all gasoline internal combustion engines high volume production. This paper of Hydraulik-Ring GmbH gives an overview of the current system concepts of the latest generation of camshaft controls utilizing the principle of the vane motor. (orig.)

The Screw-Conveyor Vane Design for Piece-Wise Construction ...

African Journals Online (AJOL)

Such a method of manufacture is beyond the resources of a general-purpose metal workshop that may require the odd spiral vane once in a while and can neither afford the time nor the cost of ordering from abroad. In this article the method of six blanks which the author has developed for the building up of the vane ...

A horizontal vane radiometer: experiment, theory and simulation

OpenAIRE

Wolfe, David; Lazarra, Andres; Garcia, Alejandro

2015-01-01

The existence of two motive forces on a Crookes radiometer has complicated the investigation of either force independently. The thermal creep shear force in particular has been subject to differing interpretations of the direction in which it acts and its order of magnitude. In this article we provide a horizontal vane radiometer design which isolates the thermal creep shear force. The horizontal vane radiometer is explored through experiment, kinetic theory, and the Direct Simulation Monte C...

Vane fabrication for the proof-of-principle radio-frequency quadrupole accelerator

International Nuclear Information System (INIS)

Williams, S.W.; Potter, J.M.

1981-01-01

The electrodes for the Proof-of-Principle (POP) Radio-Frequency Quadrupole (RFQ) accelerator were machined on a numerically controlled, three-axis, vertical mill. These pole tips, or vanes, were prepared for, and used, in the successful demonstration of RFQ practicality at Los Alamos National Laboratory in February 1980. The data set that described the vanes contained about 10 million bits of tool position data. The vanes were cut from OFHC copper blanks. The tolerances achieved were approximately +- 0.005 cm. The design and manufacturing procedures are described

Solar updraft power generator with radial and curved vanes

Science.gov (United States)

Hafizh, Hadyan; Hamsan, Raziff; Zamri, Aidil Azlan Ahmad; Keprawi, Mohamad Fairuz Mohamad; Shirato, Hiromichi

2018-02-01

Solar radiation is the largest source of energy available on earth and the solar updraft power generator (SUPG) is a renewable energy facility capable of harnessing its abundant power. Unlike the conventional wind turbines that harness natural wind in the atmosphere and often encounter with the intermittent issue or even complete cut-off from airflow, the SUPG creates artificial wind as a result of solar-induced convective flows. However, the SUPG has an inherent low total efficiency due to the conversion of thermal energy into pressure energy. Acknowledging the low efficiency and considering its potential as a renewable energy facility, the current work aims to increase the total efficiency by installing a series of guide walls inside the collector. Two types of guide walls were used i.e. radial and curved vanes. The result with curved vanes showed that the updraft velocity is higher compare to those without vanes. About 18% and 64% improvement of updraft velocity and mechanical power were attained respectively. Furthermore, it was observed that the role of radial vanes configuration was more to produce a smooth updraft velocity profile rather than increasing the total efficiency.

Water table tests of proposed heat transfer tunnels for small turbine vanes

Science.gov (United States)

Meitner, P. L.

1974-01-01

Water-table flow tests were conducted for proposed heat-transfer tunnels which were designed to provide uniform flow into their respective test sections of a single core engine turbine vane and a full annular ring of helicopter turbine vanes. Water-table tests were also performed for the single-vane test section of the core engine tunnel. The flow in the heat-transfer tunnels was shown to be acceptable.

Testing of Composite Fan Vanes With Erosion-Resistant Coating Accelerated

Science.gov (United States)

Bowman, Cheryl L.; Sutter, James K.; Otten, Kim D.; Samorezov, Sergey; Perusek, Gail P.

2004-01-01

The high-cycle fatigue of composite stator vanes provided an accelerated life-state prior to insertion in a test stand engine. The accelerated testing was performed in the Structural Dynamics Laboratory at the NASA Glenn Research Center under the guidance of Structural Mechanics and Dynamics Branch personnel. Previous research on fixturing and test procedures developed at Glenn determined that engine vibratory conditions could be simulated for polymer matrix composite vanes by using the excitation of a combined slip table and electrodynamic shaker in Glenn's Structural Dynamics Laboratory. Bench-top testing gave researchers the confidence to test the coated vanes in a full-scale engine test.

Theoretical morphology and development of flight feather vane asymmetry with experimental tests in parrots.

Science.gov (United States)

Feo, Teresa J; Prum, Richard O

2014-06-01

Asymmetry in flight feather vane width is a major functional innovation associated with the evolution of flight in the ancestors of birds. However, the developmental and morphological basis of feather shape is not simple, and the developmental processes involved in vane width asymmetry are poorly understood. We present a theoretical model of feather morphology and development that describes the possible ways to modify feather development and produce vane asymmetry. Our model finds that the theoretical morphospace of feather shape is redundant, and that many different combinations of parameters could be responsible for vane asymmetry in a given feather. Next, we empirically measured morphological and developmental model parameters in asymmetric and symmetric feathers from two species of parrots to identify which combinations of parameters create vane asymmetry in real feathers. We found that both longer barbs, and larger barb angles in the relatively wider trailing vane drove asymmetry in tail feathers. Developmentally, longer barbs were the result of an offset of the radial position of the new barb locus, whereas larger barb angles were produced by differential expansion of barbs as the feather unfurls from the tubular feather germ. In contrast, the helical angle of barb ridge development did not contribute to vane asymmetry and could be indicative of a constraint. This research provides the first comprehensive description of both the morphological and developmental modifications responsible for vane asymmetry within real feathers, and identifies key steps that must have occurred during the evolution of vane asymmetry. © 2014 Wiley Periodicals, Inc.

Interaction of impeller and guide vane in a series-designed axial-flow pump

International Nuclear Information System (INIS)

Kim, S; Choi, Y S; Lee, K Y; Kim, J H

2012-01-01

In this paper, the interaction of the impeller and guide vane in a series-designed axial-flow pump was examined through the implementation of a commercial CFD code. The impeller series design refers to the general design procedure of the base impeller shape which must satisfy the various flow rate and head requirements by changing the impeller setting angle and number of blades of the base impeller. An arc type meridional shape was used to keep the meridional shape of the hub and shroud with various impeller setting angles. The blade angle and the thickness distribution of the impeller were designed as an NACA airfoil type. In the design of the guide vane, it was necessary to consider the outlet flow condition of the impeller with the given setting angle. The meridional shape of the guide vane were designed taking into consideration the setting angle of the impeller, and the blade angle distribution of the guide vane was determined with a traditional design method using vane plane development. In order to achieve the optimum impeller design and guide vane, three-dimensional computational fluid dynamics and the DOE method were applied. The interaction between the impeller and guide vane with different combination set of impeller setting angles and number of impeller blades was addressed by analyzing the flow field of the computational results.

Study on effects of mixing vane grids on coolant temperature distribution by subchannel analysis

Energy Technology Data Exchange (ETDEWEB)

Mao, H.; Yang, B.W.; Han, B. [Xi' an Jiaotong Univ., Shaanxi (China). Science and Technology Center for Advanced Nuclear Fuel Research

2016-07-15

Mixing vane grids (MVG) have great influence on coolant temperature field in the rod bundle. The MVG could enhance convective heat transfer between the fuel rod wall and the coolant, and promote inter-subchannel mixing at the same time. For the influence of the MVG on convective heat transfer enhancement, many experiments have been done and several correlations have been developed based on the experimental data. However, inter-subchannel mixing promotion caused by the MVG is not well estimated in subchannel analysis because the information of mixing vanes is totally missing in most subchannel codes. This paper analyzes the influence of mixing vanes on coolant temperature distribution using the improved MVG model in subchannel analysis. The coolant temperature distributions with the MVG are analyzed, and the results show that mixing vanes lead to a more uniform temperature distribution. The performances of split vane grids under different power conditions are evaluated. The results are compared with those of spacer grids without mixing vanes and some conclusions are obtained.

Study on effects of mixing vane grids on coolant temperature distribution by subchannel analysis

International Nuclear Information System (INIS)

Mao, H.; Yang, B.W.; Han, B.

2016-01-01

Mixing vane grids (MVG) have great influence on coolant temperature field in the rod bundle. The MVG could enhance convective heat transfer between the fuel rod wall and the coolant, and promote inter-subchannel mixing at the same time. For the influence of the MVG on convective heat transfer enhancement, many experiments have been done and several correlations have been developed based on the experimental data. However, inter-subchannel mixing promotion caused by the MVG is not well estimated in subchannel analysis because the information of mixing vanes is totally missing in most subchannel codes. This paper analyzes the influence of mixing vanes on coolant temperature distribution using the improved MVG model in subchannel analysis. The coolant temperature distributions with the MVG are analyzed, and the results show that mixing vanes lead to a more uniform temperature distribution. The performances of split vane grids under different power conditions are evaluated. The results are compared with those of spacer grids without mixing vanes and some conclusions are obtained.

Performance improvement of a centrifugal compressor stage by using different vaned diffusers

International Nuclear Information System (INIS)

Zhang, Y C; Kong, X Z; Li, F; Sun, W; Chen, Q G

2013-01-01

The vaneless diffuser (VLD) is usually adopted in the traditional design of the multi-stage centrifugal compressor because of the stage's match problem. The drawback of the stage with vaneless diffusers is low efficiency. In order to increase the efficiency and at the same time, induce no significant decline in the operating range of the stage, three different types of vaned diffusers are designed and numerically investigated: the traditional vaned diffuser (TVD), the low-solidity cascade diffuser (LSD) and the partial-height vane diffuser (PVD). These three types of vaned diffusers have different influences on the performance of the centrifugal compressor. In the present investigation, the first part investigates the performance of a centrifugal compressor stage with three different vaned diffusers. The second part studies the influences of the height and the position of partial height vanes on the stage performance, and discusses the matching problem between the PVD and the downstream return channel. The stage investigated in this paper includes the impeller, the diffuser, the bend and the return channel. In the process of numerical investigation, the flow is assumed to be steady, and this process includes calculation and simulation. The calculation of 3-D turbulent flow in the stage uses the commercial CFD code NUMECA together with the Spalart-Allmaras turbulence model. The simulation of the computational region includes the impeller passages, the diffuser passages and return channel passages. The structure and surrounding region are assumed to have a perfect cyclic symmetry, so the single channel model and periodic boundary condition are applied at the middle of the passage, that is to reduce the calculation region to only one region. The investigation showed that the low-solidity cascade diffuser would be a better choice as a middle course for the first stage of the multistage centrifugal compressor. Besides, the influences of the height and the position

Experimental Study on Series Operation of Sliding Vane Pump and Centrifugal Pump

OpenAIRE

Li, Tao; Zhang, Weiming; Jiang, Ming; Li, Zhengyang

2013-01-01

A platform for sliding vane pump and centrifugal pump tests is installed to study the series operation of them under different characteristics of pipeline. Firstly, the sliding vane pump and the centrifugal pump work independently, and the performance is recorded. Then, the two types of pumps are combined together, with the sliding vane pump acting as the feeding pump. Comparison is made between the performance of the independently working pump and the performance of series operation pump. Re...

Numerical Analysis of a Centrifugal Fan for Improved Performance using Splitter Vanes

OpenAIRE

N. Yagnesh Sharma; K. Vasudeva Karanth

2009-01-01

The flow field in a centrifugal fan is highly complex with flow reversal taking place on the suction side of impeller and diffuser vanes. Generally performance of the centrifugal fan could be enhanced by judiciously introducing splitter vanes so as to improve the diffusion process. An extensive numerical whole field analysis on the effect of splitter vanes placed in discrete regions of suspected separation points is possible using CFD. This paper examines the effect of sp...

Twisted Vanes Would Enhance Fuel/Air Mixing In Turbines

Science.gov (United States)

Nguyen, H. Lee; Micklow, Gerald J.; Dogra, Anju S.

1994-01-01

Computations of flow show performance of high-shear airblast fuel injector in gas-turbine engine enhanced by use of appropriately proportioned twisted (instead of flat) dome swirl vanes. Resultant more nearly uniform fuel/air mixture burns more efficiently, emitting smaller amounts of nitrogen oxides. Twisted-vane high-shear airblast injectors also incorporated into paint sprayers, providing advantages of low pressure drop characteristic of airblast injectors in general and finer atomization of advanced twisted-blade design.

Pressure Drop Test of Hybrid Mixing Vane Spacer Grid

Energy Technology Data Exchange (ETDEWEB)

Oh, D. S.; Chang, S. K.; Kim, B. D.; Chun, S. Y.; Chun, T. H

2007-08-15

The pressure loss test has been accomplished in the test section containing 5x5 rod bundle with a length of 2 m including 3 spacer grids. The test has been performed for the 5 kinds of spacer grids to compare the pressure loss characteristics: 1. Plain spacer grid which has the same body of the Hybrid but without vane (Plain), 2. Hybrid Vane spacer grid (Hybrid), 3. Hybrid-SC spacer grid which is constructed with coined, chamfered strip and is fabricated by spot welding, 4. Hybrid-LC spacer grid which is constructed with coined, chamfered strip and is fabricated by line welding along intersection line, 5. Westinghouse spacer grid with split vane (Plus-7). The pressure loss coefficient of the Plain, Hybrid, Hybrid-SC, Hybrid-LC, and Plus-7 spacer grid is 0.93, 1.15, 1.02, 1.04, and 1.08, respectively.

On the study of wavy leading-edge vanes to achieve low fan interaction noise

Science.gov (United States)

Tong, Fan; Qiao, Weiyang; Xu, Kunbo; Wang, Liangfeng; Chen, Weijie; Wang, Xunnian

2018-04-01

The application of wavy leading-edge vanes to reduce a single-stage axial fan noise is numerically studied. The aerodynamic and acoustic performance of the fan is numerically investigated using a hybrid unsteady Reynolds averaged Navier-Stokes (URANS)/acoustic analogy method (Goldstein equations). First, the hybrid URANS/Goldstein method is developed and successfully validated against experiment results. Next, numerical simulations are performed to investigate the noise reduction effects of the wavy leading-edge vanes. The aerodynamic and acoustic performance is assessed for a fan with vanes equipped with two different wavy leading-edge profiles and compared with the performance of conventional straight leading-edge vanes. Results indicate that a fan with wavy leading-edge vanes produces lower interaction noise than the baseline fan without a significant loss in aerodynamic performance. In fact, it is demonstrated that wavy leading-edge vanes have the potential to lead to both aerodynamic and acoustic improvements. The two different wavy leading-edge profiles are shown to successfully reduce the fan tone sound power level by 1.2 dB and 4.3 dB, respectively. Fan efficiency is also improved by about 1% with one of the tested wavy leading-edge profiles. Large eddy simulation (LES) is also performed for a simplified fan stage model to assess the effects of wavy leading-edge vanes on the broadband fan noise. Results indicate that the overall sound power level of a fan can be reduced by about 4 dB with the larger wavy leading-edge profile. Finally, the noise reduction mechanisms are investigated and analysed. It is found that the wavy leading-edge profiles can induce significant streamwise vorticity around the leading-edge protuberances and reduce pressure fluctuations (especially at locations of wavy leading-edge hills) and unsteady forces on the stator vanes. The underlying mechanism of the reduced pressure fluctuations is also discussed by examining the magnitude

Design and experimental validation of the inlet guide vane system of a mini hydraulic bulb-turbine

Energy Technology Data Exchange (ETDEWEB)

Ferro, L.M.C. [Department of Mechanical Engineering, Escola Superior de Tecnologia de Setubal, Polytechnic Institute of Setubal, Campus do IPS, Estefanilha, 2910-761 Setubal (Portugal); IDMEC, Instituto Superior Tecnico, Technical University of Lisbon, Av. Rovisco Pais,1049-001 Lisboa (Portugal); Gato, L.M.C.; Falcao, A.F.O. [IDMEC, Instituto Superior Tecnico, Technical University of Lisbon, Av. Rovisco Pais,1049-001 Lisboa (Portugal)

2010-09-15

The paper presents a fast design method for the inlet guide vanes of low-cost mini hydraulic bulb turbines. The guide vanes are positioned between two conical surfaces with a common vertex and have constant thickness distribution, except close to the leading and the trailing edges. The conical-walled inlet guide vane row is designed using a quasi-three-dimensional calculation method, by prescribing the angular-momentum distribution along the span at the outlet section of the guide vanes. The meridional through-flow is computed by a streamline curvature method and the blade-to-blade flow by a singularity surface method. The stagger angle and the vane camber are computed to fulfil the required design circulation and zero-incidence flow at the leading edge. The final vane shape is a single-curvature surface with straight leading and trailing edges. To validate the design method, a conical-walled inlet guide vane row nozzle-model with six fixed vanes was designed, manufactured and tested in an airflow rig. Traversing measurements along the circumferential and radial directions were made with a five-hole probe. The experimental results are compared with the prescribed design conditions and with numerical results from the three-dimensional inviscid and viscous flow computed with the FLUENT code. (author)

Research and development on the hydraulic design system of the guide vanes of multistage centrifugal pumps

International Nuclear Information System (INIS)

Zhang, Q H; Xu, Y; Shi, W D; Lu, W G

2012-01-01

To improve the hydraulic design accuracy and efficiency of the guide vanes of the multistage centrifugal pumps, four different-structured guide vanes are investigated, and the design processes of those systems are established. The secondary development platforms of the ObjectArx2000 and the UG/NX OPEN are utilized to develop the hydraulic design systems of the guide vanes. The error triangle method is adopted to calculate the coordinates of the vanes, the profiles of the vanes are constructed by Bezier curves, and then the curves of the flow areas along the flow-path are calculated. Two-dimensional and three-dimensional hydraulic models can be developed by this system.

ESRC guide vanes of hydraulic turbine for Three Gorges project

Directory of Open Access Journals (Sweden)

Rui CHEN

2005-05-01

Full Text Available The mechanical properties and internal quality of low carbon martensite Electroslag Remelting Casting (ESRCstainless steel castings are superior to that of sand casting ones. The key technologies for the equipments and ESRC processes have been resolved during the experimental research period of guide vanes of hydraulic turbines for Three Gorges project. And ESRC guide vanes of hydraulic turbines for Three Gorges project have been produced successfully.

Study of turbine and guide vanes integration to enhance the performance of cross flow vertical axis wind turbine

Science.gov (United States)

Wibowo, Andreas; Tjahjana, Dominicus Danardono Dwi Prija; Santoso, Budi; Situmorang, Marcelinus Risky Clinton

2018-02-01

The main purpose of this study is to investigate the best configuration between guide vanes and cross flow vertical axis wind turbine with variation of several parameters including guide vanes tilt angle and the number of turbine and guide vane blades. The experimental test were conducted under various wind speed and directions for testing cross flow wind turbine, consisted of 8, 12 and 16 blades. Two types of guide vane were developed in this study, employing 20° and 60° tilt angle. Both of the two types of guide vane had three variations of blade numbers which had same blade numbers variations as the turbines. The result showed that the configurations between 60° guide vane with 16 blade numbers and turbine with 16 blade numbers had the best configurations. The result also showed that for certain configuration, guide vane was able to increase the power generated by the turbine significantly by 271.39% compared to the baseline configuration without using of guide vane.

Design and Analysis of a Split Deswirl Vane in a Two-Stage Refrigeration Centrifugal Compressor

Directory of Open Access Journals (Sweden)

Jeng-Min Huang

2014-09-01

Full Text Available This study numerically investigated the influence of using the second row of a double-row deswirl vane as the inlet guide vane of the second stage on the performance of the first stage in a two-stage refrigeration centrifugal compressor. The working fluid was R134a, and the turbulence model was the Spalart-Allmaras model. The parameters discussed included the cutting position of the deswirl vane, the staggered angle of two rows of vane, and the rotation angle of the second row. The results showed that the performance of staggered angle 7.5° was better than that of 15° or 22.5°. When the staggered angle was 7.5°, the performance of cutting at 1/3 and 1/2 of the original deswirl vane length was slightly different from that of the original vane but obviously better than that of cutting at 2/3. When the staggered angle was 15°, the cutting position influenced the performance slightly. At a low flow rate prone to surge, when the second row at a staggered angle 7.5° cutting at the half of vane rotated 10°, the efficiency was reduced by only about 0.6%, and 10% of the swirl remained as the preswirl of the second stage, which is generally better than other designs.

CMC vane assembly apparatus and method

Science.gov (United States)

Schiavo, Anthony L; Gonzalez, Malberto F; Huang, Kuangwei; Radonovich, David C

2012-10-23

A metal vane core or strut (64) is formed integrally with an outer backing plate (40). An inner backing plate (38) is formed separately. A spring (74) with holes (75) is installed in a peripheral spring chamber (76) on the strut. Inner and outer CMC shroud covers (46, 48) are formed, cured, then attached to facing surfaces of the inner and outer backing plates (38, 40). A CMC vane airfoil (22) is formed, cured, and slid over the strut (64). The spring (74) urges continuous contact between the strut (64) and airfoil (66), eliminating vibrations while allowing differential expansion. The inner end (88) of the strut is fastened to the inner backing plate (38). A cooling channel (68) in the strut is connected by holes (69) along the leading edge of the strut to peripheral cooling paths (70, 71) around the strut. Coolant flows through and around the strut, including through the spring holes.

Performance improvement of centrifugal compressor stage with pinched geometry or vaned diffuser

Energy Technology Data Exchange (ETDEWEB)

Jaatinen, A.

2009-07-01

Centrifugal compressors are widely used for example in refrigeration processes, the oil and gas industry, superchargers, and waste water treatment. In this work, five different vaneless diffusers and six different vaned diffusers are investigated numerically. The vaneless diffusers vary only by their diffuser width, so that four of the geometries have pinch implemented to them. Pinch means a decrease in the diffuser width. Four of the vaned diffusers have the same vane turning angle and a different number of vanes, and two have different vane turning angles. The flow solver used to solve the flow fields is Finfo, which is a Navier-Stokes solver. All the cases are modeled Chien's k-epsilon turbulence model. All five vaneless diffusers and three vaned diffusers are investigated also experimentally. For each construction, the compressor operating map is measured according to relevant standards. In addition to this, the flow fields before and after the diffuser are measured with static and total pressure, flow angle and total temperature measurements k-omega SST turbulence model. The simulation results indicate that it is possible to improve the efficiency with the pinch, and according to the numerical results, the two best geometries are the ones with most pinch at the shroud. These geometries have approximately 4 percentage points higher effciency than the unpinched vaneless diffusers. The hub pinch does not seem to have any major benefits. In general, the pinches make the flow fields before and after the diffuser more uniform. The pinch also seems to improve the impeller effciency. This is down to two reasons. The major reason is that the pinch decreases the size of slow flow and possible backflow region located near the shroud after the impeller. Secondly, the pinches decrease the flow velocity in the tip clearance, leading to a smaller tip leakage flow and therefore slightly better impeller efficiency. Also some of the vaned diffusers improve the efficiency

Discussion on the re-irradiated fuel assembly with damaged guide vanes

International Nuclear Information System (INIS)

Li Ligang

2013-01-01

In January 2011, during the second plant of CNNC Nuclear Power Operations Management Co., Ltd.(hereinafter referred to as the second plant) refueling outage, the visual inspection found the guide vanes of fuel assembly A had felling off. After the National Nuclear Safety Administration (NNSA) estimated and approved, the fuel assembly A was reloaded in the specified location of reactor core. During the refueling outage in March 2012, the fuel assembly A was removed again from the reactor core. Visual inspection confirmed that the fuel assembly A was complete and without abnormal changes. The practice provides reference for re-irradiated of fuel assembly with the same type of damaged guide vanes, and provides case support for standard development for the same type of re-irradiated fuel assembly with damaged guide vanes. (author)

Effect of spacer grid mixing vanes on coolant outlet temperature distribution

Energy Technology Data Exchange (ETDEWEB)

Raemae, Tommi; Lahtinen, Tuukka; Brandt, Tellervo; Toppila, Timo [Fortum Power and Heat, Fortum (Finland). Nuclear Competence Center

2012-08-15

In Loviisa VVER-440-type NPP the coolant outlet temperature of the hot subchannel is constantly monitored during the operation. According to the authority requirement the maximum subchannel outlet temperature must not exceed the saturation temperature. Coolant temperature distribution inside the fuel assembly is affected by the efficiency of the coolant mixing. In order to enhance the coolant mixing the fuel manufacturer is introducing the additional mixing vanes on the fuel bundle spacer grids. In the paper the effect of the different mixing vane modifications is studied with computational fluid dynamics (CFD) simulation. Goal of the modelling is to find vane modifications with which sufficient mixing is reached with acceptable increase in the spacer grid pressure loss. The results of the studies are discussed in the paper. (orig.)

Numerical prediction for effects of guide vane blade numbers on hydraulic turbine performance

International Nuclear Information System (INIS)

Shi, F X; Yang, J H; Wang, X H; Li, C E

2013-01-01

Using unstructured hybrid grid technique and SIMPLEC algorithm,a general three-dimensional simulation based on Reynolds Navier- stocks in multiple reference frames and the RNG k-ε turbulence model, is presented for the reversal centrifugal pump (PAT) with a guide vane. Four different schemes are designed by a change of the number of guide vane blade of PAT. The inner flow field in every scheme is simulated, accordingly, the external characteristic and static pressure distribution in flow field in PAT is obtained. The results obtained show that the efficiency can be improved by adding a guide vane for the PAT, besides, the high efficiency area is wider than before. Guide blade numbers changed, external characteristics of turbine changed, and the external characteristic changed. The optimal value is existent for the guide vane blade number, which has a great impact on the distribution of pressure in runner inlet

Turbofan gas turbine engine with variable fan outlet guide vanes

Science.gov (United States)

Wood, Peter John (Inventor); LaChapelle, Donald George (Inventor); Grant, Carl (Inventor); Zenon, Ruby Lasandra (Inventor); Mielke, Mark Joseph (Inventor)

2010-01-01

A turbofan gas turbine engine includes a forward fan section with a row of fan rotor blades, a core engine, and a fan bypass duct downstream of the forward fan section and radially outwardly of the core engine. The forward fan section has only a single stage of variable fan guide vanes which are variable fan outlet guide vanes downstream of the forward fan rotor blades. An exemplary embodiment of the engine includes an afterburner downstream of the fan bypass duct between the core engine and an exhaust nozzle. The variable fan outlet guide vanes are operable to pivot from a nominal OGV position at take-off to an open OGV position at a high flight Mach Number which may be in a range of between about 2.5-4+. Struts extend radially across a radially inwardly curved portion of a flowpath of the engine between the forward fan section and the core engine.

Design and numerical investigation of swirl recovery vanes for the Fokker 29 propeller

Directory of Open Access Journals (Sweden)

Wang Yangang

2014-10-01

Full Text Available Swirl recovery vanes (SRVs are a set of stationary vanes located downstream from a propeller, which may recover some of the residual swirl from the propeller, hoping for an improvement in both thrust and efficiency. The SRV concept design for a scaled version representing the Fokker 29 propeller is performed in this paper, which may give rise to a promotion in propulsive performance of this traditional propeller. Firstly the numerical strategy is validated from two aspects of global quantities and the local flow field of the propeller compared with experimental data, and then the exit flow together with the development of propeller wake is analyzed in detail. Three kinds of SRV are designed with multiple circular airfoils. The numerical results show that the swirl behind the propeller is recovered significantly with Model V3, which is characterized by the highest solidity along spanwise, for various working conditions, and the combination of rotor and vane produced 5.76% extra thrust at the design point. However, a lower efficiency is observed asking for a better vane design and the choice of a working point. The vane position is studied which shows that there is an optimum range for higher thrust and efficiency.

Static thrust-vectoring performance of nonaxisymmetric convergent-divergent nozzles with post-exit yaw vanes. M.S. Thesis - George Washington Univ., Aug. 1988

Science.gov (United States)

Foley, Robert J.; Pendergraft, Odis C., Jr.

1991-01-01

A static (wind-off) test was conducted in the Static Test Facility of the 16-ft transonic tunnel to determine the performance and turning effectiveness of post-exit yaw vanes installed on two-dimensional convergent-divergent nozzles. One nozzle design that was previously tested was used as a baseline, simulating dry power and afterburning power nozzles at both 0 and 20 degree pitch vectoring conditions. Vanes were installed on these four nozzle configurations to study the effects of vane deflection angle, longitudinal and lateral location, size, and camber. All vanes were hinged at the nozzle sidewall exit, and in addition, some were also hinged at the vane quarter chord (double-hinged). The vane concepts tested generally produced yaw thrust vectoring angles much less than the geometric vane angles, for (up to 8 percent) resultant thrust losses. When the nozzles were pitch vectored, yawing effectiveness decreased as the vanes were moved downstream. Thrust penalties and yawing effectiveness both decreased rapidly as the vanes were moved outboard (laterally). Vane length and height changes increased yawing effectiveness and thrust ratio losses, while using vane camber, and double-hinged vanes increased resultant yaw angles by 50 to 100 percent.

Numerical and experimental study of the leakage flow in guide vanes with different hydrofoils

Directory of Open Access Journals (Sweden)

Sailesh Chitrakar

2017-07-01

Full Text Available Clearance gaps between guide vanes and cover plates of Francis turbines tend to increase in size due to simultaneous effect of secondary flow and erosion in sediment affected hydropower plants. The pressure difference between the two sides of the guide vane induces leakage flow through the gap. This flow enters into the suction side with high acceleration, disturbing the primary flow and causing more erosion and losses in downstream turbine components. A cascade rig containing a single guide vane passage has been built to study the effect of the clearance gap using pressure sensors and PIV (Particle Image Velocimetry technique. This study focuses on developing a numerical model of the test rig, validating the results with experiments and investigating the behavior of leakage flow numerically. It was observed from both CFD and experiment that the leakage flow forms a passage vortex, which shifts away from the wall while travelling downstream. The streamlines contributing to the formation of this vortex have been discussed. Furthermore, the reference guide vane with symmetrical hydrofoil has been compared with four cambered profiles, in terms of the guide vane loading and the consequent effect on the leakage flow. A dimensionless term called Leakage Flow Factor (Lff has been introduced to compare the performances of hydrofoils. It is shown that the leakage flow and its effect on increasing losses and erosion can be minimized by changing the pressure distribution over the guide vane.

Influence of blockage effect on measurement by vane anemometers

Directory of Open Access Journals (Sweden)

Sluse Jan

2017-01-01

Full Text Available The article deals with influence of blockage effect caused by vane anemometer in the wind tunnel by measurement via this anemometer. The influences will be represented by correction coefficient. The first part of this article is focused on the design of the impeller of vane anemometers. The impellers are printed on 3D printer with variable parameters. The anemometer is fixed in an open section of the wind tunnel with closed loop and the velocity profile is measured by Laser Doppler velocimetry (LDV in front and behind it for all impellers. The experimental data are compared with the numerical simulation in OpenFOAM. The results are correction coefficients.

Analysis on influence of guide vanes closure laws of pump-turbine on load rejection transient process

Science.gov (United States)

Yao, Z.; Bi, H. L.; Huang, Q. S.; Li, Z. J.; Wang, Z. W.

2013-12-01

In load rejection transient process, the sudden shut down of guide vanes may cause units speed rise and a sharp increase in water hammer pressure of diversion system, which endangers the safety operation of the power plant. Adopting reasonable guide vane closure law is a kind of economic and effective measurement to reduce the water hammer pressure and limit rotational speed increases. In this paper, combined with Guangzhou Pumped Storage Power Station plant A, the load rejection condition under different guide vanes closure laws is calculated and the key factor of guide vanes closure laws on the impact of the load rejection transition process is analyzed. The different inflection points, which are the closure modes, on the impact of unit speed change, water level fluctuation of surge tank, and the pressure fluctuation of volute inlet and draft tube inlet are further discussed. By compared with the calculation results, a reasonable guide vanes inflection point position can be determined according to security requirements and a reasonable guide vanes closure law can be attained to effectively coordinate the unit speed rise and the rapid pressure change in the load rejection transient process.

Effects of the friction coefficient on the torque characteristics of a hydraulic cam-rotor vane motor

Energy Technology Data Exchange (ETDEWEB)

Ma, Qiankun; Wang, Xuyong; Yuan, Fan; Chen, Liang Shen; Tao, Jian Feng [School of Mechanical Engineering, Shanghai Jiao Tong University, Shanghai (China); Miao, Zhong Hua [School of Mechatronic Engineering and Automation, Shanghai University, Shanghai (China)

2016-08-15

The friction coefficient between the vane and the slot is one of the most critical factors that affects the performance of a continuous rotary hydraulic cam-rotor vane motor. To study the effects of this coefficient on the torque characteristics of the motor, the mathematical model for the normal force and the disturbing torque between the cam rotors and the vanes of the motor was established by analyzing the forces exerted on the vanes. The mathematical model was simulated with MATLAB, and simulation results show that an increase in the friction coefficient would simultaneously decrease the normal force and increase the disturbing torque, which would negatively affect the performance of the motor. Further experimental research indicated that the low-speed performance of the hydraulic cam-rotor motor was significantly improved when the friction coefficient was reduced by controlling the parallelism tolerance, flatness and roughness between the vanes and the slots.

Evaluation of effect of low opening operation on increasing wear of bearing bushings of guide vanes used in hydropower plants

International Nuclear Information System (INIS)

Kim, Jong Sung; Kim, Se Na

2012-01-01

A guide vane plays a key role in controlling the flow rate of water supplied to the turbine of a hydropower plant. It has been reported that guide vane bearing bushings are subjected to considerable wear, which requires them to be maintained. An ancillary service such as frequency control and black start causes cyclic low opening operation of the guide vanes. It is empirically well known that such operation increases the wear rate of the guide vane bearing bushing. In this study, the effect of low opening operation on the increasing wear of the guide vane bearing bushing is quantitatively assessed via finite element flow analysis, finite element stress analysis, and relative wear evaluation. As a result of the assessment, it is identified that the pressure applied on the guide vane surface increases and the contact length between the outer surface of the guide vane stem and the inner surface of the bearing bushing decreases with a decrease in the opening of the guide vane. In addition, low opening of the guide vanes results in an increase in the relative wear owing to the generation of high contact pressure on the bearing bushing surfaces

The image evaluation of iterative motion correction reconstruction algorithm PROPELLER T2-weighted imaging compared with MultiVane T2-weighted imaging

Science.gov (United States)

Lee, Suk-Jun; Yu, Seung-Man

2017-08-01

The purpose of this study was to evaluate the usefulness and clinical applications of MultiVaneXD which was applying iterative motion correction reconstruction algorithm T2-weighted images compared with MultiVane images taken with a 3T MRI. A total of 20 patients with suspected pathologies of the liver and pancreatic-biliary system based on clinical and laboratory findings underwent upper abdominal MRI, acquired using the MultiVane and MultiVaneXD techniques. Two reviewers analyzed the MultiVane and MultiVaneXD T2-weighted images qualitatively and quantitatively. Each reviewer evaluated vessel conspicuity by observing motion artifacts and the sharpness of the portal vein, hepatic vein, and upper organs. The signal-to-noise ratio (SNR) and contrast-to-noise ratio (CNR) were calculated by one reviewer for quantitative analysis. The interclass correlation coefficient was evaluated to measure inter-observer reliability. There were significant differences between MultiVane and MultiVaneXD in motion artifact evaluation. Furthermore, MultiVane was given a better score than MultiVaneXD in abdominal organ sharpness and vessel conspicuity, but the difference was insignificant. The reliability coefficient values were over 0.8 in every evaluation. MultiVaneXD (2.12) showed a higher value than did MultiVane (1.98), but the difference was insignificant ( p = 0.135). MultiVaneXD is a motion correction method that is more advanced than MultiVane, and it produced an increased SNR, resulting in a greater ability to detect focal abdominal lesions.

Effect of Guide Vane Clearance Gap on Francis Turbine Performance

Directory of Open Access Journals (Sweden)

Ravi Koirala

2016-04-01

Full Text Available Francis turbine guide vanes have pivoted support with external control mechanism, for conversion of pressure to kinetic energy and to direct them to runner vanes. This movement along the support is dependent on variation of load and flow (operating conditions. Small clearance gaps between facing plates and the upper and lower guide vane tips are available to aid this movement, through which leakage flow occurs. This secondary flow disturbs the main flow stream, resulting performance loss. Additionally, these increased horseshoe vortex, in presence of sand, when crosses through the gaps, both the surfaces are eroded. This causes further serious effect on performance and structural property by increasing gaps. This paper discusses the observation of the severity in hydropower plants and effect of clearance gaps on general performance of the Francis turbine through computational methods. It also relates the primary result with the empirical relation for leakage flow prediction. Additionally, a possible method to computationally estimate thickness depletion has also been presented. With increasing clearance gap, leakage increases, which lowers energy conversion and turbine efficiency along with larger secondary vortex.

Performance of an alpha-vane and pitot tube in simulated heavy rain environment

Science.gov (United States)

Luers, J. K.; Fiscus, I. B.

1985-01-01

Experimental tests were conducted in the UDRI Environmental Wind/Rain Tunnel to establish the performance of an alpha-vane, that measures angle of attack, in a simulated heavy rain environment. The tests consisted of emersing the alpha-vane in an airstream with a concurrent water spray penetrating vertically through the airstream. The direction of the spray was varied to make an angle of 5.8 to 18 deg with the airstream direction in order to simulate the conditions that occur when an aircraft lands in a heavy rain environment. Rainrates simulated varied from 1000 to 1200 mm/hr which are the most severe ever expected to be encountered by an aircraft over even a 30 second period. Tunnel airspeeds ranged from 85 to 125 miles per hour. The results showed that even the most severe rainrates produced a misalignment in the alpha-vane of only 1 deg away from the airstream direction. Thus for normal rain conditions experienced by landing aircraft no significant deterioration in alpha-vane performance is expected.

Precision Model for Microwave Rotary Vane Attenuator

DEFF Research Database (Denmark)

Guldbrandsen, Tom

1979-01-01

A model for a rotary vane attenuator is developed to describe the attenuator reflection and transmission coefficients in detail. All the parameters of the model can be measured in situ, i.e., without diassembling any part. The tranmission errors caused by internal reflections are calculated from ...

Design optimization of a T mixing vane in nuclear fuel assembly

International Nuclear Information System (INIS)

Jung, Sang-Ho; Moon, Mi-Ae; Kim, Kwang-Yong

2009-01-01

The purposes of present work are to analyze the convective heat transfer with three-dimensional Reynolds-averaged Navier-Stokes analysis, and to optimize shape of the mixing vane using the analysis results. PLUS7 that is designed by KNF and Westinghouse is used as reference geometry. Shear stress transport turbulence model is used as a turbulence closure. Two bend angles of mixing vane are selected as design variable. The objective function is defined as a combination of inverse of heat transfer rate and friction loss. Response surface method is employed as an optimization technique. The calculation domains of 1x2 geometry are analyzed with translational and rotational periodic boundary conditions which take flow directions into account. The fluid flow and heat transfer characteristics have been explained through velocity vectors, streamlines and Nusselt numbers. The results show that the optimized geometry improves the heat transfer performance of the mixing vane with a relatively small pressure drop increment and has higher Critical Heat Flux. (author)

Flow control in axial fan inlet guide vanes by synthetic jets

Directory of Open Access Journals (Sweden)

Wurst P.

2013-04-01

Full Text Available Tested high pressure axial flow fan with hub/tip ratio of 0.70 and external diameter of 600 mm consisted of inlet guide vanes (IGV, rotor and stator blade rows. Fan peripheral velocity was 47 m/s. Air volume flow rate was changed by turning of rear part of the inlet guide vanes. At turning of 20 deg the flow was separated on the IGV profiles. The synthetic jets were introduced through radial holes in machine casing in the location before flow separation origin. Synthetic jet actuator was designed with the use of a speaker by UT AVCR. Its membrane had diameter of 63 mm. Excitation frequency was chosen in the range of 500 Hz – 700 Hz. Synthetic jets favourably influenced separated flow on the vane profiles in the distance of (5 – 12 mm from the casing surface. The reduction of flow separation area caused in the region near the casing the decrease of the profile loss coefficient approximately by 20%.

Flow control in axial fan inlet guide vanes by synthetic jets

Science.gov (United States)

Cyrus, V.; Trávníček, Z.; Wurst, P.; Kordík, J.

2013-04-01

Tested high pressure axial flow fan with hub/tip ratio of 0.70 and external diameter of 600 mm consisted of inlet guide vanes (IGV), rotor and stator blade rows. Fan peripheral velocity was 47 m/s. Air volume flow rate was changed by turning of rear part of the inlet guide vanes. At turning of 20 deg the flow was separated on the IGV profiles. The synthetic jets were introduced through radial holes in machine casing in the location before flow separation origin. Synthetic jet actuator was designed with the use of a speaker by UT AVCR. Its membrane had diameter of 63 mm. Excitation frequency was chosen in the range of 500 Hz - 700 Hz. Synthetic jets favourably influenced separated flow on the vane profiles in the distance of (5 - 12) mm from the casing surface. The reduction of flow separation area caused in the region near the casing the decrease of the profile loss coefficient approximately by 20%.

Reduction of background noise induced by wind tunnel jet exit vanes

Science.gov (United States)

Martin, R. M.; Brooks, T. F.; Hoad, D. R.

1985-01-01

The NASA-Langley 4 x 7 m wind tunnel develops low frequency flow pulsations at certain velocity ranges during open throat mode operation, affecting the aerodynamics of the flow and degrading the resulting model test data. Triangular vanes attached to the trailing edge of flat steel rails, mounted 10 cm from the inside of the jet exit walls, have been used to reduce this effect; attention is presently given to methods used to reduce the inherent noise generation of the vanes while retaining their pulsation reduction features.

Further development and performance evaluation of the autonomous sailing boat Maribot Vane

OpenAIRE

Dhomé, Ulysse

2018-01-01

This paper describes the ongoing development of Maribot Vane, an autonomous sailing vessel at the Maritime Robotics Laboratory of KTH, the Royal Institute of Technology, Stockholm. There is an ac-celerating need for ocean sensing where autonomous vehicles can play a key role in assisting scientists with environmental monitoring and collecting oceanographic data. The purpose of Maribot Vane is to offer a sus-tainable alternative for these autonomous missions by using wind and an energy efficie...

Erosion estimation of guide vane end clearance in hydraulic turbines with sediment water flow

Science.gov (United States)

Han, Wei; Kang, Jingbo; Wang, Jie; Peng, Guoyi; Li, Lianyuan; Su, Min

2018-04-01

The end surface of guide vane or head cover is one of the most serious parts of sediment erosion for high-head hydraulic turbines. In order to investigate the relationship between erosion depth of wall surface and the characteristic parameter of erosion, an estimative method including a simplified flow model and a modificatory erosion calculative function is proposed in this paper. The flow between the end surfaces of guide vane and head cover is simplified as a clearance flow around a circular cylinder with a backward facing step. Erosion characteristic parameter of csws3 is calculated with the mixture model for multiphase flow and the renormalization group (RNG) k-𝜀 turbulence model under the actual working conditions, based on which, erosion depths of guide vane and head cover end surfaces are estimated with a modification of erosion coefficient K. The estimation results agree well with the actual situation. It is shown that the estimative method is reasonable for erosion prediction of guide vane and can provide a significant reference to determine the optimal maintenance cycle for hydraulic turbine in the future.

CFD analysis for spacer grid mixing vane design

International Nuclear Information System (INIS)

Park, Sung-Kew; Kim, Kang-Hoon; Park, Eung-Jun; Jung, Yil-Sup; Suh, Jung-Min; Jeong, Ji-Hun

2008-01-01

A computational fluid dynamics (CFD) analysis for a rod bundle with the larger scale model (6x6 array model) has been performed to develop the base shape of mixing vane in accordance with the hydraulic and thermal performance. Explanatory parameters are span pressure drop and span average heat transfer coefficient. The concern related to hot spot is also considered as a subsidiary criterion. Of the several candidates, the final candidate was determined by using the CFD analysis code, STAR-CD. And then, the optimization for it was performed using the response surface method (RSM) that the proper tolerance was considered under the two acceptance criteria such as lower span pressure drop while maintaining the span average heat transfer coefficient with respect to the current shape. The optimized mixing vane shape was verified by the CFD analysis including the effects of allowable tolerance. (author)

Background noise measurements from jet exit vanes designed to reduced flow pulsations in an open-jet wind tunnel

Science.gov (United States)

Hoad, D. R.; Martin, R. M.

1985-01-01

Many open jet wind tunnels experience pulsations of the flow which are typically characterized by periodic low frequency velocity and pressure variations. One method of reducing these fluctuations is to install vanes around the perimeter of the jet exit to protrude into the flow. Although these vanes were shown to be effective in reducing the fluctuation content, they can also increase the test section background noise level. The results of an experimental acoustic program in the Langley 4- by 7-Meter Tunnel is presented which evaluates the effect on tunnel background noise of such modifications to the jet exit nozzle. Noise levels for the baseline tunnel configuration are compared with those for three jet exit nozzle modifications, including an enhanced noise reduction configuration that minimizes the effect of the vanes on the background noise. Although the noise levels for this modified vane configuration were comparable to baseline tunnel background noise levels in this facility, installation of these modified vanes in an acoustic tunnel may be of concern because the noise levels for the vanes could be well above background noise levels in a quiet facility.

''VaneCAM'' - the third generation of camshaft adjustment systems; ''VaneCAM'' - Nockenwellenversteller der dritten Generation

Energy Technology Data Exchange (ETDEWEB)

Knecht, A. [Hydraulik-Ring GmbH, Nuertingen (Germany). Entwicklung Motorentechnik; Stephan, W. [Hydraulik-Ring GmbH, Nuertingen (Germany); Hannibal, W. [Fachhochschule Suedwestfalen, Iserlohn (Germany). Labor fuer Konstruktion und CAE-Anwendungen

2002-04-01

Continuously variable camphasers are now well established for modern spark-ignition engines in high-volume production. With the latest generation of camshaft adjustment systems using the vane-type actuator principle, it is possible to move rapidly and reliably through a large adjustment angle. The layout of these adjusting systems is very simple. The production costs are low in comparison to the first generation of camphasers using spur/helical gears to vary the valve timing. The new-generation systems are mechatronic, with the function depending on the coordination and tuning of hydraulic actuation and engine electronics. The term 'VaneCAM' is used for the continuously variable systems of this new generation supplied by Hydraulik-Ring in Nuertingen, Germany. (orig.) [German] Stufenlos wirkende Nockenwellenversteller haben sich an modernen Ottomotoren in den letzten Jahren in der Grossserie etabliert. Mit der neuesten Generation von Nockenwellenverstellern, die nach dem Schwenkmotor-Prinzip aufgebaut sind, lassen sich grosse Verdrehwinkel sehr schnell und betriebssicher verstellen. Der Aufbau dieser Versteller ist einfach, und die Herstellkosten sind gering im Vergleich zur ersten Generation von Verstellern. Bei den Systemen der neuen Generation handelt es sich um mechatronische Systeme, deren Funktion von dem Zusammenspiel und der Abstimmung von hydraulischer Ansteuerung und Motorelektronik abhaengt. Mit dem Begriff 'VaneCAM' werden die stufenlos wirkenden Systeme dieser neuen Generation von Hydraulik-Ring aus Nuertingen bezeichnet. (orig.)

Static pressure recovery analysis in the vane island diffuser of a centrifugal pump

Energy Technology Data Exchange (ETDEWEB)

Si, Qiaorui [National Research Center of Pumps, Jiangsu University, Zhenjiang (China); Dupont, Patrick; Bayeul-Laine, Annie-Claude; Dazin, Antoine; Roussette, Olivier; Bois, Gerard [LML, UMR CNRS 8107 Ecole Centrale de Lille, Lille (France)

2016-02-15

The overall performance of a vane-island type diffuser of a centrifugal pump model was obtained by means of directional probe traverses. These measurements were performed in an air model of a real hydraulic pump for five volume flow rates. Directional probe traverses are performed with a classical three-hole probe to cover most of the complete inlet section of the diffuser from hub to shroud and from pressure to suction side. Existing Particle image velocimetry (PIV) measurement results are also used to compare probe measurement results between the inlet and outlet throats of vane island diffuser at mid-span. Some assistance from already existing unsteady calculation, including leakage effects, is used to evaluate the numerical approach capability and to correctly define the mean initial conditions at impeller's outlet section. Pressure recovery and the measured total pressure loss levels inside this particular vane diffuser geometry are then calculated. Detailed analysis of the flow structure at the inlet section of the vane island diffuser is presented to focus on pressure evolution inside the entire diffuser section for different flow rates. The combined effects of incidence angle and blockage distributions along hub to shroud direction are found to play an important role on loss distribution in such a diffuser.

A novel thermally driven rotor-vane/pressure-exchange ejector refrigeration system with environmental benefits and energy efficiency

International Nuclear Information System (INIS)

Hong, W.J.; Alhussan, Khaled; Zhang Hongfang; Garris, Charles A.

2004-01-01

The latest results of an ongoing coordinated experimental and computational program on the design and performance of a novel supersonic rotor-vane/pressure-exchange ejector for thermally driven ejector refrigeration systems are presented. For the supersonic rotor-vane/pressure-exchange ejector, careful management of the entropy rise through the oblique shocks and boundary layers is required for obtaining an advance in ejector performance. Since the invention of this new ejector is quite recent, understanding its aerodynamics, with the consequent optimization of performance, is in the formative stage. This paper shows how the supersonic aerodynamics is managed to provide the desirable flow induction characteristics through computational study and, in parallel, experimental results including flow visualization showing actual behavior with different-shaped rotor vanes. The importance of the existence of the tail part with a long expansion ramp, the sharp leading edge such as knife-edge, the proper height of leading edges, for the overall shape of rotor vane, were observed. Also the larger spin-angle rotor vane produces better flow induction and mixing between primary flow and secondary flow

Assessment of guide vane self-excitation stability at small openings in pump flow

International Nuclear Information System (INIS)

Nennemann, B; Sallaberger, M; Henggeler, U; Gentner, C; Parkinson, E

2012-01-01

A parameter study of self-excited pump turbine guide vane instability at small openings using a combined CFD-1DOF approach shows that clear tendencies are difficult to obtain. Two types of boundary conditions can be used in the simulations: prescribed mass flow and prescribed pressure. Simulations with both show results that - for one specific operating condition - are consistent with a self-excited guide vane incident at a prototype pump turbine. However, over a larger range of reduced velocities, the tendencies obtained with the two boundary condition types are not always consistent. Pressure boundary conditions may be the more realistic option. Results then show that with increasing reduced velocity, guide vanes will eventually reach static instability or divergence. This may not be problematic. In contrast, passing through a zone of dynamic instability during operation should and can be avoided.

Test procedure for use of the shear vane in tanks 103-SY, 103-AN, and 103-AW

International Nuclear Information System (INIS)

LeClair, M.D.; Waters, E.

1995-01-01

This is a record copy of a test procedure for application of the full-scale shear vane to underground waste tanks at Hanford. The introduction of the report provides background information on the development and proof-testing of the shear vane, as well as information about its current location. The document was originally prepared in 1988, and the work as shelved temporarily for lack of funds. Activities to utilize the shear vane will be expedited by use of this information

Velocity and pressure measurements in guide vane clearance gap of a low specific speed Francis turbine

Science.gov (United States)

Thapa, B. S.; Dahlhaug, O. G.; Thapa, B.

2016-11-01

In Francis turbine, a small clearance gap between the guide vanes and the cover plates is usually required to pivot guide vanes as a part of governing system. Deflection of cover plates and erosion of mating surfaces causes this gap to increase from its design value. The clearance gap induces the secondary flow in the distributor system. This effects the main flow at the runner inlet, which causes losses in efficiency and instability. A guide vane cascade of a low specific speed Francis turbine has been developed for experimental investigations. The test setup is able to produce similar velocity distributions at the runner inlet as that of a reference prototype turbine. The setup is designed for particle image velocimetry (PIV) measurements from the position of stay vane outlet to the position of runner inlet. In this study, velocity and pressure measurements are conducted with 2 mm clearance gap on one side of guide vane. Leakage flow is observed and measured together with pressure measurements. It is concluded that the leakage flow behaves as a jet and mixes with the main flow in cross-wise direction and forms a vortex filament. This causes non-uniform inlet flow conditions at runner blades.

Enlarging the operation range of a centrifugal compressor by cutting vanes based on CFD

International Nuclear Information System (INIS)

Mo, J T; Pan, X H; Gu, C H; Zheng, S Y

2013-01-01

Many centrifugal compressors are liable to insufficient operation range. The purpose of this paper is to enlarge the operation range of a centrifugal compressor used in turbocharger by cutting vanes. Some numerical works have been done based on CFD. The comparison of the calculated and measured results shows good agreement. The overall performance characteristics of the centrifugal compressor with different cutted vanes are observed and analyzed. The performance characteristic curves show that cutting vanes can increase the operation range by more than 50% with the loss of the highest efficiency limited in 1%. The flow fields are also shown in this paper and related explanations about the change of the performance characteristics curves are given. Shock wave is also detected in the simulation, and some related characteristics are summed up

Preliminary Investigation on Turbulent Flow in Tight-lattice Rod Bundle with Twist-mixing Vane Spacer Grid

International Nuclear Information System (INIS)

Lee, Chiyoung; Kwack, Youngkyun; Park, Juyong; Shin, Changhwan; In, Wangkee

2013-01-01

Our research group has investigated the effect of P/D difference on the behavior of turbulent rod bundle flow without the mixing vane spacer grid, using PIV (Particle Image Velocimetry) and MIR (Matching Index of Refraction) techniques for tight lattice fuel rod bundle application. In this work, using the tight-lattice rod bundle with a twist-mixing vane spacer grid, the turbulent rod bundle flow is preliminarily examined to validate the PIV measurement and CFD (Computational Fluid Dynamics) simulation. The turbulent flow in the tight-lattice rod bundle with a twist-mixing vane spacer grid was preliminarily examined to validate the PIV measurement and CFD simulation. Both were in agreement with each other within a reasonable degree of accuracy. Using PIV measurement and CFD simulation tested in this work, the detailed investigations on the behavior of turbulent rod bundle flow with the twist-mixing vane spacer grid will be performed at various conditions, and reported in the near future

Prospects for the domestic production of large-sized cast blades and vanes for industrial gas turbines

Science.gov (United States)

Kazanskiy, D. A.; Grin, E. A.; Klimov, A. N.; Berestevich, A. I.

2017-10-01

Russian experience in the production of large-sized cast blades and vanes for industrial gas turbines is analyzed for the past decades. It is noted that the production of small- and medium-sized blades and vanes made of Russian alloys using technologies for aviation, marine, and gas-pumping turbines cannot be scaled for industrial gas turbines. It is shown that, in order to provide manufacturability under large-scale casting from domestic nickel alloys, it is necessary to solve complex problems in changing their chemical composition, to develop new casting technologies and to optimize the heat treatment modes. An experience of PAO NPO Saturn in manufacturing the blades and vanes made of ChS88U-VI and IN738-LC foundry nickel alloys for the turbines of the GTE-110 gas turbine unit is considered in detail. Potentialities for achieving adopted target parameters for the mechanical properties of working blades cast from ChS88UM-VI modified alloy are established. For the blades made of IN738-LC alloy manufactured using the existing foundry technology, a complete compliance with the requirements of normative and technical documentation has been established. Currently, in Russia, the basis of the fleet of gas turbine plants is composed by foreign turbines, and, for the implementation of the import substitution program, one can use the positive experience of PAO NPO Saturn in casting blades from IN738-LC alloy based on a reverse engineering technique. A preliminary complex of studies of the original manufacturer's blades should be carried out, involving, first of all, the determination of geometric size using modern measurement methods as well as the studies on the chemical compositions of the used materials (base metal and protective coatings). Further, verifying the constructed calculation models based on the obtained data, one could choose available domestic materials that would meet the operating conditions of the blades according to their heat resistance and corrosion

Improvement of wells turbine performance by means of 3D guide vanes; Sanjigen annai hane ni yoru wells turbine seino no kaizen

Energy Technology Data Exchange (ETDEWEB)

Takao, M.; Kim, T.H. [Saga University, Saga (Japan); Setoguchi, T. [Saga University, Saga (Japan). Faculty of Science and Engineering; Inoue, M. [Kyushu University, Fukuoka (Japan). Faculty of Engineering

2000-02-25

Performance of a Wells turbine was improved by equipping 3D guide vanes before and behind a rotor. For further improvement, 3D guide vanes have been proposed in this paper. The performance of the Wells turbine with 2D and 3D guide vanes have been investigated experimentally by model testing under steady flow conditions. Then, the running and starting characteristics in irregular ocean waves have been obtained by a computer simulation. As a result, it is found that both of the running and starting characteristics of the Wells turbine with 3D guide vanes are superior to those of the turbine with 2D guide vanes. (author)

The effect of grid assembly mixing vanes on critical heat flux values and azimuthal location in fuel assemblies

International Nuclear Information System (INIS)

De Crecy, F.

1994-01-01

Critical heat flux (CHF) is one of the limiting phenomena for a PWR. It has been widely studied for years, but many facts are still not satisfactorily understood. This paper deals with the effect of the grid assembly mixing vanes on both the value of the CHF and the azimuthal location of the departure from nucleate boiling (DNB). A series of experimental studies was performed on electrically heated, 5x5 square pitched, vertical rod bundles. Two specific grid assembly designs were used: with and without mixing vanes. DNB was detected by eight thermocouples welded internally in each rod at the same level in order to determine the azimuthal location. The coolant was Freon-12 flowing upwards to simulate high pressure water (as defined by Stevens). Single-phase flow experiments were also conducted to measure the exit temperature field in order to obtain the mixing coefficients for subchannel analysis.The results show very clearly that the mixing vanes have a significant effect on both the DNB azimuthal location and the CHF value. - Without mixing vanes, DNB occurs mainly on the most central rod and preferentially at the azimuthal location facing the adjacent rod. - With mixing vanes, DNB can occur on any of the nine central rods and is distributed in an apparently random way around the rod. -The effect of the mixing vanes on CHF is dramatic and depends a great deal on the parameter range (pressure, local mass velocity and local quality). Generally speaking, CHF with mixing vanes is significantly higher than without mixing vanes, but this effect can be inverted in some cases.In order to understand this fact more clearly, it is necessary to perform detailed analysis of subchannel behavior. Indeed, the analyses show that the magnitude of this effect is closely related to the mixing coefficients used. These mixing coefficients, estimated from the single-phase flow experiments, are subject to large uncertainties in two-phase flow. ((orig.))

Experimental investigation of in-cylinder air flow to optimize number of helical guide vanes to enhance DI diesel engine performance using mamey sapote biodiesel

Science.gov (United States)

Kumar, A. Raj; Janardhana Raju, G.; Hemachandra Reddy, K.

2018-03-01

The current research work investigates the influence of helical guide vanes in to the intake runner of a D.I diesel engine operating by the high viscous Mamey Sapote biodiesel to enhance in-cylinder suction air flow features. Helical guide vanes of different number of vanes are produced from 3D printing and placed in the intake manifold to examine the air flow characteristics. Four different helical guide vane devices namely 3, 4, 5 and 6 vanes of the same dimensions are tested in a D.I diesel engine operating with Mamey Sapote biodiesel blend. As per the experimental results of engine performance and emission characteristics, it is found that 5 vanes helical guide vane swirl device exhibited in addition number of increased improvements such as the brake power and bake thermal efficiency by 2.4% and 8.63% respectively and the HC, NOx, Carbon monoxide and, Smoke densities are reduced by 15.62%, 4.23%, 14.27% and 9.6% at peak load operating conditions as collate with normal engine at the same load. Hence this investigation concluded that Helical Guide Vane Devices successfully enhanced the in-cylinder air flow to improve better addition of Mamey Sapote biodiesel with air leading in better performance of the engine than without vanes.

Extension of the Vane Pump-Grinder Technology to Manufacture Finely Dispersed Meat Batters.

Science.gov (United States)

Irmscher, Stefan B; Gibis, Monika; Herrmann, Kurt; Oechsle, Anja Maria; Kohlus, Reinhard; Weiss, Jochen

2016-03-01

A vane pump-grinder system was extended to enable the manufacture of finely dispersed emulsion-type sausages by constructing and attaching a high-shear homogenizer at the outlet. We hypothesized that the dispersing capabilities of the extended system may be improved to the point of facilitating meat-fat emulsification due to an overall increased volumetric energy input EV . Coarsely ground raw material mixtures were processed to yield meat batters at varying volume flow rates (10 to 60 L/min) and rotational rotor speeds of the homogenizer nrotor (1000 to 3400 rpm). The normalized torques acting on pump, grinder, and homogenizer motors were recorded and unit power consumptions were calculated. The structure of the manufactured meat batters and sausages were analyzed via image analysis. Key physicochemical properties of unheated and heated batters, that is, texture, water-binding, color, and solubilized protein were determined. The mean diameter d10 of the visible lean meat particles varied between 352 and 406 μm whereas the mean volume-surface diameter d32 varied between 603 and 796 μm. The lightness L* ranged from 66.2 to 70.7 and correlated with the volumetric energy input and product structure. By contrast, varying process parameters did not impact color values a* (approximately 11) and b* (approximately 8). Interestingly, water-binding and protein solubilization were not affected. An exponential process-structure relationship was identified allowing manufacturers to predict product properties as a function of applied process parameters. Raw material mixtures can be continuously comminuted, emulsified, and subsequently filled into casings using an extended vane pump-grinder. © 2016 Institute of Food Technologists®

The effect of mixing-vane arrangements in a subchannel turbulent flow

International Nuclear Information System (INIS)

Ikeno, Tsutomu; Murata, Tamotsu; Kajishima, Takeo

2006-01-01

Large eddy simulation (LES) of developed turbulent flows in a rod bundle was carried out for four spacer designs. The mixing-vanes attached at the spacer were inclined at 30degC or 20deg; they were arranged to promote the swirling or convective flow. These arrangements are possible elements to compose an actual rod bundle. Our LES technique with a consistent higher-order immersed boundary method and a one-equation dynamic sub-grid scale model contributed to an efficient treatment of the complex wall configurations of rods and spacers. The computational results reasonably reproduced experimental results for the drag coefficient and the decay rate of swirling flow. The profiles of the axial velocities and the turbulence intensities indicated reasonable trend for the turbulent flow in the rod bundle. The effect of mixing-vane arrangement on the lateral flows was successfully clarified: the cross flow took the longer way on the rod surface than the swirling flow and then was more significantly influenced by momentum diffusion at the no-slip wall. Therefore, the largely inclined mixing-vanes promoted the cross flow only in the neighborhood of the spacer, the swirling flow inside a subchannel could reach farther downstream than the cross flow. (author)

Performance and internal flow characteristics of a cross-flow turbine by guide vane angle

International Nuclear Information System (INIS)

Chen, Z M; Choi, Y D

2013-01-01

This study attempts to investigate the performance and internal flow characteristics of a cross-flow turbine by guide vane angle. In order to improve the performance of a cross flow turbine, the paper presents a numerical investigation of the turbine with air supply and discusses the influence of variable guide vane angle on the internal flow. A newly developed air supply from air suction Hole is adopted. To investigate the performance and internal flow of the cross-flow turbine, the CFD software based on the two-phase flow model is utilized. The numerical grids are made in two-dimensional geometry in order to shorten the time of two-phase calculations. Then a series of CFD analysis has been conducted in the range of different guide vane angle. Moreover, local output power is divided at different stages and the effect of air layer in each stage is examined

Introduction on KPS's maintenance experience of the swirl vane assemblies of primary separators for SG model F in Korea

International Nuclear Information System (INIS)

Kim, Yong tae

2003-01-01

Recently, we had experienced to replace the Swirl Vane Assemblies of primary moisture separator for SG model F in Korea because of serious degradation (Thinning) in carbon steel swirl vane blades and carbon steel separator barrel wall adjacent to swirl vane blades. When the symptom was observed by us at the first time on the swirl vane assemblies, there were small or a bit clear erosion / or corrosion marks on the edge regions of the blades but within 3 cycles of operation, we found that those marks became holes which penetrated the most of swirl vane assemblies and even more seriously, some parts of the assemblies were worn-out. Therefore, we concluded that the speed of degradation would be very rapid and serious from the beginning stage. It had been assumed that these kinds of thinning problems would be due to FAC(Flow Accelerated Corrosion) because the plants having these problems are using a highly concentrated hydrazine for the water treatment of secondary side which lead to reduce the oxygen and pH in the water. What are more serious reasons will be that the swirl vane assemblies are very weak to FAC because they were made by a low concentrated chromium carbon steel and the assemblies would have to be under the operation conditions of the highly turbulent steam-water mixed fluid with the operating temperature of higher than 280 .deg. C. Potentially, the damaged swirl vane assemblies of the primary moisture separator may create bad influences for the plant operation because it may cause the rupture of SG Tubes and over-exceed fluid influx onto the turbine and etc. KPS had successfully performed the replacement of the degraded swirl vane assemblies through our own planning and preparation. This was the unique case in all over the world and I would like to introduce you about our unique repair experience to prepare an expected future situation as we see the similar problems in other model F SGs operating in Korea

An analytical model for droplet separation in vane separators and measurements of grade efficiency and pressure drop

International Nuclear Information System (INIS)

Koopman, Hans K.; Köksoy, Çağatay; Ertunç, Özgür; Lienhart, Hermann; Hedwig, Heinz; Delgado, Antonio

2014-01-01

Highlights: • An analytical model for efficiency is extended with additional geometrical features. • A simplified and a novel vane separator design are investigated experimentally. • Experimental results are significantly affected by re-entrainment effects. • Outlet droplet size spectra are accurately predicted by the model. • The improved grade efficiency doubles the pressure drop. - Abstract: This study investigates the predictive power of analytical models for the droplet separation efficiency of vane separators and compares experimental results of two different vane separator geometries. The ability to predict the separation efficiency of vane separators simplifies their design process, especially when analytical research allows the identification of the most important physical and geometrical parameters and can quantify their contribution. In this paper, an extension of a classical analytical model for separation efficiency is proposed that accounts for the contributions provided by straight wall sections. The extension of the analytical model is benchmarked against experiments performed by Leber (2003) on a single stage straight vane separator. The model is in very reasonable agreement with the experimental values. Results from the analytical model are also compared with experiments performed on a vane separator of simplified geometry (VS-1). The experimental separation efficiencies, computed from the measured liquid mass balances, are significantly below the model predictions, which lie arbitrarily close to unity. This difference is attributed to re-entrainment through film detachment from the last stage of the vane separators. After adjustment for re-entrainment effects, by applying a cut-off filter to the outlet droplet size spectra, the experimental and theoretical outlet Sauter mean diameters show very good agreement. A novel vane separator geometry of patented design (VS-2) is also investigated, comparing experimental results with VS-1

Performance Analysis of a Centrifugal Compressor for HFC-134a with aviation of Diffuser Vane Angle

International Nuclear Information System (INIS)

Park, Han Young; Chung, Jin Taek; Shin, You Hwan; Lee, Yoon Pyo; Kim, Kwang Ho; Cho, Yong Hun; Kim, Jong Seong

2007-01-01

Numerical simulation on the two-stage centrifugal compressor with Low Solidity Vaned Diffuser (LSVD) for HFC-134a turbo-chiller was performed using a commercial code. The comparative study with experimental results from other compressor was also investigated to testify the simulation schemes. The numerical analysis was separately simulated for each stage of the compressor and the effect of impeller-diffuser flow interaction was considered. Setting angle of the diffuser vane changed in the range of 15 .deg. and the effects on its variation were discussed in detail including the flow analysis in the passage of the compressor. The vane setting angle obtained from the preliminary design was slightly adjusted to the optimal value by the performance enhancement in terms of pressure recovery and flow characteristics

LOX/LH2 vane pump for auxiliary propulsion systems

Science.gov (United States)

Hemminger, J. A.; Ulbricht, T. E.

1985-01-01

Positive displacement pumps offer potential efficiency advantages over centrifugal pumps for future low thrust space missions. Low flow rate applications, such as space station auxiliary propulsion or dedicated low thrust orbiter transfer vehicles, are typical of missions where low flow and high head rise challenge centrifugal pumps. The positive displacement vane pump for pumping of LOX and LH2 is investigated. This effort has included: (1) a testing program in which pump performance was investigated for differing pump clearances and for differing pump materials while pumping LN2, LOX, and LH2; and (2) an analysis effort, in which a comprehensive pump performance analysis computer code was developed and exercised. An overview of the theoretical framework of the performance analysis computer code is presented, along with a summary of analysis results. Experimental results are presented for pump operating in liquid nitrogen. Included are data on the effects on pump performance of pump clearance, speed, and pressure rise. Pump suction performance is also presented.

Numerical Study of Bubble Coalescence and Breakup in the Reactor Fuel Channel with a Vaned Grid

Directory of Open Access Journals (Sweden)

Tenglong Cong

2018-01-01

Full Text Available The characteristics of bubbles of different sizes in fuel assembly are vital to two-phase flow resistance and heat transfer capacity. However, due to the swirl flow caused by the mixing vane, bubbles can crowd at the heated surface, which may anticipate the occurrence of departure from nucleation boiling. In the current work, the adiabatic two-phase flow in a simplified fuel assembly was analyzed by using the Eulerian two-fluid model and the MUSIG (MUltiple SIze Group model. This computational domain consists of two coolant channels and two sets of vaned spacers, with three sets of periodic boundary conditions at the side faces of the domain. The distributions of vapor phase and bubble diameters were obtained, based on which the effects of mixing vanes on the bubble characteristics were analyzed. Vapor phase crowded at the rod surface in the higher inlet vapor fraction case, but crowded in the channel center in the lower inlet vapor fraction cases. This work can be used as a reference for the design of mixing vanes to avoid the anticipation of departure of nucleation boiling that may be caused by unreasonable design.

Computational model for turbulent flow around a grid spacer with mixing vane

International Nuclear Information System (INIS)

Tsutomu Ikeno; Takeo Kajishima

2005-01-01

Turbulent mixing coefficient and pressure drop are important factors in subchannel analysis to predict onset of DNB. However, universal correlations are difficult since these factors are significantly affected by the geometry of subchannel and a grid spacer with mixing vane. Therefore, we propose a computational model to estimate these factors. Computational model: To represent the effect of geometry of grid spacer in computational model, we applied a large eddy simulation (LES) technique in couple with an improved immersed-boundary method. In our previous work (Ikeno, et al., NURETH-10), detailed properties of turbulence in subchannel were successfully investigated by developing the immersed boundary method in LES. In this study, additional improvements are given: new one-equation dynamic sub-grid scale (SGS) model is introduced to account for the complex geometry without any artificial modification; the higher order accuracy is maintained by consistent treatment for boundary conditions for velocity and pressure. NUMERICAL TEST AND DISCUSSION: Turbulent mixing coefficient and pressure drop are affected strongly by the arrangement and inclination of mixing vane. Therefore, computations are carried out for each of convolute and periodic arrangements, and for each of 30 degree and 20 degree inclinations. The difference in turbulent mixing coefficient due to these factors is reasonably predicted by our method. (An example of this numerical test is shown in Fig. 1.) Turbulent flow of the problem includes unsteady separation behind the mixing vane and vortex shedding in downstream. Anisotropic distribution of turbulent stress is also appeared in rod gap. Therefore, our computational model has advantage for assessing the influence of arrangement and inclination of mixing vane. By coarser computational mesh, one can screen several candidates for spacer design. Then, by finer mesh, more quantitative analysis is possible. By such a scheme, we believe this method is useful

A Three-Dimensional Coupled Internal/External Simulation of a Film-Cooled Turbine Vane

Science.gov (United States)

Heidmann, James D.; Rigby, David L.; Ameri, Ali A.

1999-01-01

A three-dimensional Navier-Stokes simulation has been performed for a realistic film-cooled turbine vane using the LeRC-HT code. The simulation includes the flow regions inside the coolant plena and film cooling holes in addition to the external flow. The vane is the subject of an upcoming NASA Glenn Research Center experiment and has both circular cross-section and shaped film cooling holes. This complex geometry is modeled using a multi-block grid which accurately discretizes the actual vane geometry including shaped holes. The simulation matches operating conditions for the planned experiment and assumes periodicity in the spanwise direction on the scale of one pitch of the film cooling hole pattern. Two computations were performed for different isothermal wall temperatures, allowing independent determination of heat transfer coefficients and film effectiveness values. The results indicate separate localized regions of high heat transfer coefficient values, while the shaped holes provide a reduction in heat flux through both parameters. Hole exit data indicate rather simple skewed profiles for the round holes, but complex profiles for the shaped holes with mass fluxes skewed strongly toward their leading edges.

Measuring Undrained Shear Strength using CPT and Field Vane

DEFF Research Database (Denmark)

Luke, Kirsten

1992-01-01

This paper presents the results of CPT's and Field Vane tests from two small test areas with different soils, Glacial Till and Yoldia Clay. An average of Nk = qt/cv for the Yoldia Clay is 7.7 with a standard deviation of 0.7. The average of Nk for the Glacial Till is 9.7 with a standard deviation...

T2-weighted liver MRI using the multiVane technique at 3T: Comparison with conventional T2-weighted MRI

Energy Technology Data Exchange (ETDEWEB)

Kang, Kyung A [Dept. of Radiology, Myongji Hospital, Seonam University College of Medicine, Goyang (Korea, Republic of); Kim, Young Kon; Jeong, Woo Kyoung; Choi, Dong Il; Lee, Won Jae [Dept. of Radiology and Center for Imaging Science, Samsung Medical Center, Sungkyunkwan University School of Medicine, Seoul (Korea, Republic of); Kim, Eun Ju [Philips Healthcare Korea, Philips, Seoul (Korea, Republic of); Jung, Sin Ho; Baek, Sun Young [Biostatistics and Clinical Epidemiology Center, Samsung Medical Center, Seoul (Korea, Republic of)

2015-10-15

To assess the value of applying MultiVane to liver T2-weighted imaging (T2WI) compared with conventional T2WIs with emphasis on detection of focal liver lesions. Seventy-eight patients (43 men and 35 women) with 86 hepatic lesions and 20 pancreatico-biliary diseases underwent MRI including T2WIs acquired using breath-hold (BH), respiratory-triggered (RT), and MultiVane technique at 3T. Two reviewers evaluated each T2WI with respect to artefacts, organ sharpness, and conspicuity of intrahepatic vessels, hilar duct, and main lesion using five-point scales, and made pairwise comparisons between T2WI sequences for these categories. Diagnostic accuracy (Az) and sensitivity for hepatic lesion detection were evaluated using alternative free-response receiver operating characteristic analysis. MultiVane T2WI was significantly better than BH-T2WI or RT-T2WI for organ sharpness and conspicuity of intrahepatic vessels and main lesion in both separate reviews and pairwise comparisons (p < 0.001). With regard to motion artefacts, MultiVane T2WI or BH-T2WI was better than RT-T2WI (p < 0.001). Conspicuity of hilar duct was better with BH-T2WI than with MultiVane T2WI (p = 0.030) or RT-T2WI (p < 0.001). For detection of 86 hepatic lesions, sensitivity (mean, 97.7%) of MultiVane T2WI was significantly higher than that of BH-T2WI (mean, 89.5%) (p = 0.008) or RT-T2WI (mean, 84.9%) (p = 0.001). Applying the MultiVane technique to T2WI of the liver is a promising approach to improving image quality that results in increased detection of focal liver lesions compared with conventional T2WI.

Investigating the thermal hydraulic performance of spacer grid with mixing vanes using STAR-CCM+ and MATRA

International Nuclear Information System (INIS)

Agbodemegbe, V. Y.

2014-07-01

Enhancement of heat transfer for flow through rod bundles is linked to the extent and sustainability of mixing in the flow geometry. Spacer grids used as support for rod bundles in nuclear reactors, when attached with ditferent designs of mixing vanes promote turbulent mixing by inducing swirl or forced lateral convection that improves mixing within or between sub-channels. The improved turbulent mixing raises the margin of the onset of critical heat flux in light water reactors (LWR) and also ensures a higher fuel cycle economy. To optimize design of mixing vanes and performance of spacer grids with mixing vanes, computational fluid dynamic simulations arc carried out on new designs and validated experimentally prior to industrial application. In the present study, computational fluid dynamic simulation using STAR-CCM+ and sub-channel analysis with MATRA were performed for flow of water through a 5 X 5 rod bundle geometry for which the rod to rod pitch to diameter ratio was 1.33 and the wall to rod pitch to diameter ratio was 0.74. The two layer k-epsilon turbulence model with an all- y + automatic wall treatment function in STAR-CCM+ were adopted for an isothermal single phase flow through the geometry with imposed cyclic periodic and non-cyclic periodic interface boundary conditions. The objective was to primarily investigate the detail flow behavior in rod bundle in the presence of spacer grids with and without attached mixing vanes. Furthermore, the present study also investigated the extent of turbulent mixing and lateral mass flux induced by the mixing vanes through comparative analysis of parametric trends for spacer grid with and without mixing vanes. New models and empirical correlations for describing the mixing vanes effects were also developed. These semi-empirical correlations improved the prediction for lateral mass flux due to turbulence, fraction of flow diverted through gaps and cross-flow resistance coefficients. Validation of simulation results

Heat transfer coefficient testing in nuclear fuel rod bundles with mixing vane grids

International Nuclear Information System (INIS)

Conner, Michael E.; Smith, L. David III; Holloway, Mary V.; Beasley, Donald E.

2005-01-01

An air heat transfer test facility was developed to test the heat transfer downstream of support grids in simulated PWR nuclear fuel rod bundles. The goal of this testing is to study the single-phase heat transfer coefficients downstream of grids with mixing vanes in a square-pitch rod bundle. The technique developed utilizes fully-heated grid spans and a specially designed thermocouple holder that can be moved axially down the rod bundle and aximuthally within a test rod. From this testing, the axial and aximuthally varying heat transfer coefficient can be determined. Different grid designs are tested and compared to determine the heat transfer enhancement associated with key grid features such as mixing vanes. (author)

CFD analysis of supercritical water flow and heat transfer in single channel with mixing vane

International Nuclear Information System (INIS)

Zuo Guoping; Xie Hongyan; Yu Tao

2012-01-01

Three-dimensional rectangular channel with the mixing wane in supercritical water reactor is investigated with CFX. The mixing vane elevation influenced on temperature distribution and flow field are simulated in the model. The results showed the mixing vane cause fluid circumferential flow, making flow hot and cold fluids mixed and fluid temperature uniform distribution, effectively improve the fuel rod surface temperature distribution and reduced hot temperature. Among the mixing wing elevation of 15, 30, 45, 50, 60 and 70 angle, the 30 angle is the best case in improving temperature distribution. (authors)

RF field measurement of a four-vane type RFQ with PISLs

International Nuclear Information System (INIS)

Ueno, A.; Yamajaki, Y.

1992-01-01

Field instability due to a dipole mode mixing is the most significant disadvantage of an original four-vane type radio-frequency quadrupole (RFQ) linac. In order to avoid any dipole mode mixing, several pairs of vane coupling rings (VCRs) have mainly been used so far. However the VCR has complicated shape and is difficult to fabricate, particularly in the RFQ linac operated with a high-duty factor. Thus, a new field-stabilization concept was proposed and was referred to as a π-mode stabilizing loop (PISL) in a previous paper. The results of rf characteristics measurements on a low-power model cavity with or without PISLs are presented in this paper. The measurements showed that the PISLs were capable of stabilizing the accelerating mode, reducing the ratio of a dipole mode mixing from 7% to less than 1.5% (Author) 4 figs., tab., 10 refs

Performance Enhancement of the In-Line Fan Equipped with the Guiding Vane and the Tail Body

Directory of Open Access Journals (Sweden)

Hung-Cheng Yen

2014-02-01

Full Text Available This integrated numerical and experimental study intends to enhance the performance of an in-line fan with the implement of the guiding vane and the tail body. At first the flow flied associated with the original in-line fan is simulated and analyzed within the framework of CFD code Fluent, in which the finite volume method is applied. Next, the guiding vane is constructed based on the calculated flow characteristics, and attached in the downstream of rotor to smoothen the flow pattern. An appropriate guiding vane with high-performance and low-noise features can be achieved after several design iterations. In addition, the tail body connected to the motor is introduced for further enhancing the fan performance by reducing the sizes of wake and reversed flow behind the hub. Thereafter, to manufacture the mockup for experimental verification, the modified fan with guiding vane is plotted in the CAD/CAM format for mockup fabrication via the rapid-prototype technique. Moreover, a set of relations correlating the performance and noise of this fan prototype are executed inside AMCA test chamber and semianechoic chamber, respectively. Consequently, the feasibility of design scheme and numerical system can be verified according to these experimental results. In summary, this work provides a systematic scheme for designing and analyzing the in-line fan.

Study and Control of a Radial Vaned Diffuser Stall

Directory of Open Access Journals (Sweden)

Aurélien Marsan

2012-01-01

Full Text Available The aim of the present study is to evaluate the efficiency of a boundary layer suction technique in case of a centrifugal compressor stage in order to extend its stable operating range. First, an analysis of the flow pattern within the radial vaned diffuser is presented. It highlights the stall of the diffuser vanes when reaching a low massflow. A boundary layer separation in the hub-suction side corner grows when decreasing the massflow from the nominal operating point to the surge and finally leads to a massive stall. An aspiration strategy is investigated in order to control the stall. The suction slot is put in the vicinity of the saddle that originates the main separating skin-friction line, identified thanks to the analysis of the skin-friction pattern. Several aspiration massflow rates are tested, and two different modelings of the aspiration are evaluated. Finally, an efficient control is reached with a removal of only 0,1% of the global massflow and leads—from a steady-state calculations point of view—to an increase by 40% of the compressor operating range extent.

The VanE operon in Enterococcus faecalis N00-410 is found on a putative integrative and conjugative element, Tn6202.

Science.gov (United States)

Boyd, D A; Mulvey, M R

2013-02-01

To date no complete genetic structure of acquired DNA harbouring a d-Ala-d-Ser operon in an Enterococcus is known. We wished to characterize the acquired DNA harbouring the vanE operon located in the Enterococcus faecalis N00-410 chromosome. Whole genome sequencing of E. faecalis N00-410 was conducted by massively parallel sequencing. Two sequence contigs harbouring the vanE region were linked by PCR and the acquired DNA harbouring the vanE operon was completely characterized. Excision/integration of the region was determined by PCR and transfer attempted by conjugation. The regions flanking the vanE operon were analysed and a total of 42 open reading frames were identified in a region flanked by inverted terminal and direct repeats (Tn6202). Tn6202 could be excised from the chromosome, circularized and the target site rejoined, but transfer could not be demonstrated. The vanE operon was found on the putative integrative and conjugative element Tn6202 in the E. faecalis N00-410 chromosome. This represents the first characterization of acquired DNA harbouring a D-Ala-D-Ser operon.

Numerical investigation of variable inlet guide vanes with trailing-edge dual slots to decrease the aerodynamic load on centrifugal compressor impeller

Directory of Open Access Journals (Sweden)

Jianchi Xin

2016-03-01

Full Text Available In engineering practice, most centrifugal compressors use variable inlet guide vanes which can provide pre-whirl and control volume flow rates. As the impeller of a centrifugal compressor passes through the wakes created from the guide vanes, the aerodynamic parameters change significantly. The concept of adding dual slots at the trailing-edge of the guide vanes is proposed for reducing the aerodynamic load on the compressor impeller blades. In this article, the steady and unsteady performances of the new guide vanes are analysed under two compressor operating conditions (winter and design conditions. The results show that the average amplitude of the impeller passing frequency at the leading edge has a 13% decrease under the winter condition, especially at the middle and root parts. Moreover, the dual slots structure has no effect on the overall compressor performance.

Numerical study of pressure fluctuations in different guide vanes' opening angle in pump mode of a pump turbine

International Nuclear Information System (INIS)

Sun, Y K; Zuo, Z G; Liu, S H; Wu, Y L; Liu, J T

2012-01-01

A numerical model based on a pumped storage power station was built to develop the numerical simulation, to analyze the pressure fluctuations in a pump turbine in different guide vanes' opening angle. The different guide vanes' opening angles were simulated using the SST k-ω turbulence model and SIMPLEC Pressure-Velocity coupling scheme. The pressure sensor were placed in mainly three positions, they are: bottom ring between runner and the wicket gates, downstream and left side in the draft tube cone below the runner. All the peak to peak values of pressure fluctuation meet signal probability of 97%. The frequency is gained by Fast Fourier Transform. The pressure fluctuations in different positions of the model in pump condition were showed when the guide vanes' opening angels were different. The simulation results confirmed the results gained in model tests. The results show that pressure fluctuations in design opening angle were much lower than those in off design opening angle. The main source of pressure fluctuations between runner and guide vanes is rotor stator interaction. While a lower frequency is the main frequency of the pressure fluctuation in draft tube.

Suction Side Roughness Effects on Film Cooling Heat Transfer on a Turbine Vane

National Research Council Canada - National Science Library

Rutledge, James

2004-01-01

An experimental study was conducted in a simulated three vane linear cascade to determine the effects of surface roughness and film cooling on the heat transfer coefficient distribution in the region...

Analytical solution for the electrical properties of a radio-frequency quadrupole (RFQ) with simple vanes

International Nuclear Information System (INIS)

Lancaster, H.

1982-01-01

Although the SUPERFISH program is used for calculating the design parameters of an RFQ structure with complex vanes, an analytical solution for electrical properties of an RFQ with simple vanes provides insight into the parametric behavior of these more complicated resonators. The fields in an inclined plane wave guide with proper boundary conditions match those in one quadrant of an RFQ. The principle of duality is used to exploit the solutions to a radial transmission line in solving the field equations. Calculated are the frequency equation, frequency sensitivity factors, electric field, magnetic field, stored energy (U), power dissipation, and quality factor

Numerical research on the effects of impeller pump-out vanes on axial force in a solid-liquid screw centrifugal pump

International Nuclear Information System (INIS)

Cheng, X R; Li, R N; Gao, Y; Guo, W L

2013-01-01

A commercial CFD code has been used to predict the performance of a screw centrifugal pump with pump-out vanes, especially when changing regularity of impeller axial force based on the solid-liquid two-phase flow. The Unsteady Reynolds Averaged Navier-Stokes (URANS) approach has been applied to solve the unsteady, incompressible, three-dimensional turbulent. The SIMPLEC algorithm, standard wall functions and mix two-phase flow model were applied. The RNG k ε-model was used to account the turbulence effects. By changing the number of impeller pump-out vanes and width, six different screw centrifugal pump numerical simulation projects were given, and each scheme in the different solid volume fraction were calculated respectively. The change rules of axial force, velocity and pressure distribution of flow field were obtained on the different condition and different volume fraction. The results showed that the axial forces values based solid-fluid two-phase greater than based single-phase clear water, but both changing regularity of the axial force were consistent; as same condition, the same solid-phase volume concentration, with the increase of pump-out vanes number or width, the impeller axial force increased as well. Meanwhile the number of the pump-out vanes and the width of pump-out vanes in balancing the impeller axial force, there are the most optimal value

Investigation of Blade-row Flow Distributions in Axial-flow-compressor Stage Consisting of Guide Vanes and Rotor-blade Row

Science.gov (United States)

Mahoney, John J; Dugan, Paul D; Budinger, Raymond E; Goelzer, H Fred

1950-01-01

A 30-inch tip-diameter axial-flow compressor stage was investigated with and without rotor to determine individual blade-row performance, interblade-row effects, and outer-wall boundary-layer conditions. Velocity gradients at guide-vane outlet without rotor approximated design assumptions, when the measured variation of leaving angle was considered. With rotor in operation, Mach number and rotor-blade effects changed flow distribution leaving guide vanes and invalidated design assumption of radial equilibrium. Rotor-blade performance correlated interpolated two-dimensional results within 2 degrees, although tip stall was indicated in experimental and not two-dimensional results. Boundary-displacement thickness was less than 1.0 and 1.5 percent of passage height after guide vanes and after rotor, respectively, but increased rapidly after rotor when tip stall occurred.

Effect of long time service exposure on microstructure and mechanical properties of gas turbine vanes made of IN939 alloy

International Nuclear Information System (INIS)

Jahangiri, M.R.; Abedini, M.

2014-01-01

Highlights: • Microstructure of service-exposed turbine vanes made of IN939 was investigated. • Mechanical properties of service-exposed alloy were also investigated. • Formation of M 23 C 6 films on GBs and degeneration of MCs are microstructural changes. • Despite its thermodynamic favorability, σ phase is not observed in microstructure. • Microstructural changes lead to a loss in tensile ductility and creep life. - Abstract: In the present study, the effects of long-term service exposure have been investigated on microstructure and mechanical properties of gas turbine vanes made of IN939 superalloy. The major microstructural changes for the investigated service-exposed vanes include the formation of continuous grain boundary carbides and the transformation (degeneration) of MC carbides located at the grain boundaries. The brittle σ phase, which is predicted to be stable on the basis of thermodynamic calculations, is not observed in the microstructure of service-exposed vanes. The microstructural changes during service lead to a loss in room temperature ductility as well as in creep properties of the alloy

Analysis of waves in the plasma guided by a periodical vane-type slow wave structure

International Nuclear Information System (INIS)

Wu, T.J.; Kou, C.S.

2005-01-01

In this study, the dispersion relation has been derived to characterize the propagation of the waves in the plasma guided by a periodical vane-type slow wave structure. The plasma is confined by a quartz plate. Results indicate that there are two different waves in this structure. One is the plasma mode that originates from the plasma surface wave propagating along the interface between the plasma and the quartz plate, and the other is the guide mode that originally travels along the vane-type slow wave structure. In contrast to its original slow wave characteristics, the guide mode becomes a fast wave in the low-frequency portion of the passband, and there exists a cut-off frequency for the guide mode. The vane-type guiding structure has been shown to limit the upper frequency of the passband of the plasma mode, compared with that of the plasma surface wave. In addition, the passband of the plasma mode increases with the plasma density while it becomes narrower for the guide mode. The influences of the parameters of the guiding structure and plasma density on the propagation of waves are also presented

Material sampling for rotor evaluation

International Nuclear Information System (INIS)

Mercaldi, D.; Parker, J.

1990-01-01

Decisions regarding continued operation of aging rotating machinery must often be made without adequate knowledge of rotor material conditions. Physical specimens of the material are not generally available due to lack of an appropriate sampling technique or the high cost and inconvenience of obtaining such samples. This is despite the fact that examination of such samples may be critical to effectively assess the degradation of mechanical properties of the components in service or to permit detailed examination of microstructure and surface flaws. Such information permits a reduction in the uncertainty of remaining life estimates for turbine rotors to avoid unnecessarily premature and costly rotor retirement decisions. This paper describes the operation and use of a recently developed material sampling device which machines and recovers an undeformed specimen from the surface of rotor bores or other components for metallurgical analysis. The removal of the thin, wafer-like sample has a negligible effect on the structural integrity of these components, due to the geometry and smooth surface finish of the resulting shallow depression. Samples measuring approximately 0.03 to 0.1 inches (0.76 to 2.5 mm) thick by 0.5 to 1.0 inch (1.3 to 2.5 cm) in diameter can be removed without mechanical deformation or thermal degradation of the sample or the remaining component material. The device is operated remotely from a control console and can be used externally or internally on any surface for which there is at least a three inch (7.6 cm) working clearance. Application of the device in two case studies of turbine-generator evaluations are presented

Materials and structural aspects of advanced gas-turbine helicopter engines

Science.gov (United States)

Freche, J. C.; Acurio, J.

1979-01-01

Advances in materials, coatings, turbine cooling technology, structural and design concepts, and component-life prediction of helicopter gas-turbine-engine components are presented. Stationary parts including the inlet particle separator, the front frame, rotor tip seals, vanes and combustors and rotating components - compressor blades, disks, and turbine blades - are discussed. Advanced composite materials are considered for the front frame and compressor blades, prealloyed powder superalloys will increase strength and reduce costs of disks, the oxide dispersion strengthened alloys will have 100C higher use temperature in combustors and vanes than conventional superalloys, ceramics will provide the highest use temperature of 1400C for stator vanes and 1370C for turbine blades, and directionally solidified eutectics will afford up to 50C temperature advantage at turbine blade operating conditions. Coatings for surface protection at higher surface temperatures and design trends in turbine cooling technology are discussed. New analytical methods of life prediction such as strain gage partitioning for high temperature prediction, fatigue life, computerized prediction of oxidation resistance, and advanced techniques for estimating coating life are described.

An Empirical Model for Vane-Type Vortex Generators in a Navier-Stokes Code

Science.gov (United States)

Dudek, Julianne C.

2005-01-01

An empirical model which simulates the effects of vane-type vortex generators in ducts was incorporated into the Wind-US Navier-Stokes computational fluid dynamics code. The model enables the effects of the vortex generators to be simulated without defining the details of the geometry within the grid, and makes it practical for researchers to evaluate multiple combinations of vortex generator arrangements. The model determines the strength of each vortex based on the generator geometry and the local flow conditions. Validation results are presented for flow in a straight pipe with a counter-rotating vortex generator arrangement, and the results are compared with experimental data and computational simulations using a gridded vane generator. Results are also presented for vortex generator arrays in two S-duct diffusers, along with accompanying experimental data. The effects of grid resolution and turbulence model are also examined.

Investigating temporal patterns of a native bee community in a remnant North American bunchgrass prairie using blue vane traps.

Science.gov (United States)

Kimoto, Chiho; Debano, Sandra J; Thorp, Robbin W; Rao, Sujaya; Stephen, William P

2012-01-01

Native bees are important ecologically and economically because their role as pollinators fulfills a vital ecosystem service. Pollinators are declining due to various factors, including habitat degradation and destruction. Grasslands, an important habitat for native bees, are particularly vulnerable. One highly imperiled and understudied grassland type in the United States is the Pacific Northwest Bunchgrass Prairie. No studies have examined native bee communities in this prairie type. To fill this gap, the bee fauna of the Zumwalt Prairie, a large, relatively intact remnant of the Pacific Northwest Bunchgrass Prairie, was examined. Native bees were sampled during the summers of 2007 and 2008 in sixteen 40-ha study pastures on a plateau in northeastern Oregon, using a sampling method not previously used in grassland studies-blue vane traps. This grassland habitat contained an abundant and diverse community of native bees that experienced marked seasonal and inter-annual variation, which appears to be related to weather and plant phenology. Temporal variability evident over the entire study area was also reflected at the individual trap level, indicating a consistent response across the spatial scale of the study. These results demonstrate that temporal variability in bee communities can have important implications for long-term monitoring protocols. In addition, the blue vane trap method appears to be well-suited for studies of native bees in large expanses of grasslands or other open habitats, and may be a useful tool for monitoring native bee communities in these systems.

Cooling Strategies for Vane Leading Edges in a Syngas Environment Including Effects of Deposition and Turbulence

Energy Technology Data Exchange (ETDEWEB)

Ames, Forrest [Univ. of North Dakota, Grand Forks, ND (United States); Bons, Jeffrey [Univ. of North Dakota, Grand Forks, ND (United States)

2014-09-30

The Department of Energy has goals to move land based gas turbine systems to alternate fuels including coal derived synthetic gas and hydrogen. Coal is the most abundant energy resource in the US and in the world and it is economically advantageous to develop power systems which can use coal. Integrated gasification combined cycles are (IGCC) expected to allow the clean use of coal derived fuels while improving the ability to capture and sequester carbon dioxide. These cycles will need to maintain or increase turbine entry temperatures to develop competitive efficiencies. The use of coal derived syngas introduces a range of potential contaminants into the hot section of the gas turbine including sulfur, iron, calcium, and various alkali metals. Depending on the effectiveness of the gas clean up processes, there exists significant likelihood that the remaining materials will become molten in the combustion process and potentially deposit on downstream turbine surfaces. Past evidence suggests that deposition will be a strong function of increasing temperature. Currently, even with the best gas cleanup processes a small level of particulate matter in the syngas is expected. Consequently, particulate deposition is expected to be an important consideration in the design of turbine components. The leading edge region of first stage vanes most often have higher deposition rates than other areas due to strong fluid acceleration and streamline curvature in the vicinity of the surface. This region remains one of the most difficult areas in a turbine nozzle to cool due to high inlet temperatures and only a small pressure ratio for cooling. The leading edge of a vane often has relatively high heat transfer coefficients and is often cooled using showerhead film cooling arrays. The throat of the first stage nozzle is another area where deposition potentially has a strongly adverse effect on turbine performance as this region meters the turbine inlet flow. Based on roughness

Advanced Instrumentation for Measuring Fluid-Structure Coupling Phenomena in the Guide Vanes Cascade of a Pump-Turbine Scale Model

OpenAIRE

Roth, Steven; Hasmatuchi, Vlad; Botero, Francisco; Farhat, Mohamed; Avellan, François

2010-01-01

In the present study, the fluid-structure coupling is investigated in the guide vanes of a pump-turbine scale model placed in one of the test rigs of the Laboratory for Hydraulic Machines (EPFL) in Lausanne. The paper focuses on the advanced instrumentation used to get reliable and complete fluid-structure coupling results. Semi-conductor strain gages are installed on three guide vanes which are especially weakened to account for stronger fluid-structure coupling phenomena. These are statical...

Characterization of Rotating Detonation Engine Exhaust Through Nozzle Guide Vanes

Science.gov (United States)

2013-03-21

ENY/13-M09 Abstract A Rotating Detonation Engine ( RDE ) has higher thermal efficiencies in comparison to its traditional gas turbine counterparts. Thus...as budgets decrease and fuel costs increase, RDEs have become a research focus for the United States Air Force. An integration assembly for attaching...the first Nozzle Guide Vane (NGV) section from a T63 gas turbine engine to a 6 inch diameter RDE was designed and built for this study. Pressure

Aerodynamic forces estimation on jet vanes exposed to supersonic exhaust of a CD Nozzle

International Nuclear Information System (INIS)

Bukhari, S.B.H.; Jehan, I.; Zahir, S.; Khan, M.A.

2003-01-01

A comprehensive study has been made for the estimation of aerodynamic forces on the jet Vane placed in the supersonic exhaust of a Convergent Divergent, CD-Nozzle. Such a system is used to provide the control forces that consist of four orthogonal vanes mounted in the supersonic exhaust of the CD-Nozzles. The flow field parameters for a CD Nozzle were analyzed and validated earlier. In this paper the published experimental and CFD results from RAMPANT Code from Fluent Inc. were used to estimate the axial and normal forces by using PAK-3D, a Computational Fluid Dynamics (CFD) software based on Navier-Stokes Equations solver. Results got verified quantitatively with a maximum error of 8% between PAK-3D and experiment, while 4% between PAK-3D and a CFD code, RAMPANT for the axial force. (author)

Analysis of swirl recovery vanes for increased propulsive efficiency in tractor propeller aircraft

NARCIS (Netherlands)

Veldhuis, L.L.M.; Stokkermans, T.C.A.; Sinnige, T.; Eitelberg, G.

2016-01-01

In this paper we address a preliminary assessment of the performance effects of swirl recovery vanes (SRVs) in a installed and uninstalled tractor propeller arrangement. A numerical analysis was performed on a propeller and a propeller-wing configuration after the SRVs were optimized first in a

Automatic efficiency optimization of an axial compressor with adjustable inlet guide vanes

Science.gov (United States)

Li, Jichao; Lin, Feng; Nie, Chaoqun; Chen, Jingyi

2012-04-01

The inlet attack angle of rotor blade reasonably can be adjusted with the change of the stagger angle of inlet guide vane (IGV); so the efficiency of each condition will be affected. For the purpose to improve the efficiency, the DSP (Digital Signal Processor) controller is designed to adjust the stagger angle of IGV automatically in order to optimize the efficiency at any operating condition. The A/D signal collection includes inlet static pressure, outlet static pressure, outlet total pressure, rotor speed and torque signal, the efficiency can be calculated in the DSP, and the angle signal for the stepping motor which control the IGV will be sent out from the D/A. Experimental investigations are performed in a three-stage, low-speed axial compressor with variable inlet guide vanes. It is demonstrated that the DSP designed can well adjust the stagger angle of IGV online, the efficiency under different conditions can be optimized. This establishment of DSP online adjustment scheme may provide a practical solution for improving performance of multi-stage axial flow compressor when its operating condition is varied.

Electrofracturing test system and method of determining material characteristics of electrofractured material samples

Science.gov (United States)

Bauer, Stephen J.; Glover, Steven F.; Pfeifle, Tom; Su, Jiann-Cherng; Williamson, Kenneth Martin; Broome, Scott Thomas; Gardner, William Payton

2017-08-01

A device for electrofracturing a material sample and analyzing the material sample is disclosed. The device simulates an in situ electrofracturing environment so as to obtain electrofractured material characteristics representative of field applications while allowing permeability testing of the fractured sample under in situ conditions.

Methodology of Computer-Aided Design of Variable Guide Vanes of Aircraft Engines

Science.gov (United States)

Falaleev, Sergei V.; Melentjev, Vladimir S.; Gvozdev, Alexander S.

2016-01-01

The paper presents a methodology which helps to avoid a great amount of costly experimental research. This methodology includes thermo-gas dynamic design of an engine and its mounts, the profiling of compressor flow path and cascade design of guide vanes. Employing a method elaborated by Howell, we provide a theoretical solution to the task of…

Sequential cooling insert for turbine stator vane

Science.gov (United States)

Jones, Russel B

2017-04-04

A sequential flow cooling insert for a turbine stator vane of a small gas turbine engine, where the impingement cooling insert is formed as a single piece from a metal additive manufacturing process such as 3D metal printing, and where the insert includes a plurality of rows of radial extending impingement cooling air holes alternating with rows of radial extending return air holes on a pressure side wall, and where the insert includes a plurality of rows of chordwise extending second impingement cooling air holes on a suction side wall. The insert includes alternating rows of radial extending cooling air supply channels and return air channels that form a series of impingement cooling on the pressure side followed by the suction side of the insert.

Gas turbine structural mounting arrangement between combustion gas duct annular chamber and turbine vane carrier

Science.gov (United States)

Wiebe, David J.; Charron, Richard C.; Morrison, Jay A.

2016-10-18

A gas turbine engine ducting arrangement (10), including: an annular chamber (14) configured to receive a plurality of discrete flows of combustion gases originating in respective can combustors and to deliver the discrete flows to a turbine inlet annulus, wherein the annular chamber includes an inner diameter (52) and an outer diameter (60); an outer diameter mounting arrangement (34) configured to permit relative radial movement and to prevent relative axial and circumferential movement between the outer diameter and a turbine vane carrier (20); and an inner diameter mounting arrangement (36) including a bracket (64) secured to the turbine vane carrier, wherein the bracket is configured to permit the inner diameter to move radially with the outer diameter and prevent axial deflection of the inner diameter with respect to the outer diameter.

Novel investigation of the different Omni-direction-guide-vane angles effects on the urban vertical axis wind turbine output power via three-dimensional numerical simulation

International Nuclear Information System (INIS)

Shahizare, B.; Nik-Ghazali, N.; Chong, W.T.; Tabatabaeikia, S.; Izadyar, Nima; Esmaeilzadeh, Alireza

2016-01-01

Highlights: • Investigation of the Omni-direction-guide-vane impacts on the VAWT performance. • Obtain the best position of the guide vane angles in order to achieve the maximum performance. • Validation of the 3D computational fluid dynamics with experimental data. • Acquire the optimal Omni-direction-guide-vane based on numerical simulation results. - Abstract: The aim of this study is to present the effects of different Omni-direction-guide-vane (ODGV) angles on the performance of the vertical axis wind turbine (VAWT). For this purpose, five different straight-bladed VAWTs have been simulated via three-dimensional (3D) computational fluid dynamics (CFD). Hence, the VAWT without ODGV covering, were simulated and validated via CFD and experimental fluid dynamics (EFD) data, respectively in the first step. Indeed, grid and time step independency test as well as the effect of domain size, have been conducted and a suitable agreement was found based on comparison of the CFD and EFD results. In the next step, the VAWT was shrouded by ODGV cover and the whole system was simulated for 52 angles of the ODGV in four different tip speed ratios (TSR), to investigate the impact of guide vanes angles on the VAWT performance. Results of this study indicated that output power of the VAWT with α = 20° and β = 55° ODGV guide vanes, was improved 40.9%, 36.5%, 35.3% and 33.2%, respectively in four different TSR including 0.745, 1.091, 1.901 and 2.53.

3D shape optimization of fan vanes for multiple operating regimes subject to efficiency and noise-related excellence criteria and constraints

Directory of Open Access Journals (Sweden)

Ivo Marinić-Kragić

2016-01-01

Full Text Available Fully generic 3D shapes of centrifugal roof fan vanes are explored based on a custom-developed numerical workflow with the ability to vary the vane 3D shape by manipulating the control points of parametric surfaces and change the number of vanes and rotation speed. An excellence formulation is based on design flow efficiency, multi-regime operational conditions and noise criteria for various cases, including multi-objective optimization. Multiple cases of optimization demonstrate the suitability of customized and individualized fan designs for specific working environments according to the selected excellence criteria. Noise analysis is considered as an additional decision-making tool for cases where multiple solutions of equal efficiency are generated and as an additional criteria for multi-objective optimization. The 3D vane shape enables further gains in efficiency compared to 2D shape optimization, while multi-objective optimization with noise as an additional criterion shows potential to greatly reduce the roof fan noise with only small losses in efficiency. The developed workflow which comprises (i a 3D parametric shape modeler, (ii an evolutionary optimizer and (iii a computational fluid dynamics (CFD simulator can be viewed as an integral tool for optimizing the designs of roof fans under custom conditions.

RF structure design of the China Material Irradiation Facility RFQ

Science.gov (United States)

Li, Chenxing; He, Yuan; Xu, Xianbo; Zhang, Zhouli; Wang, Fengfeng; Dou, Weiping; Wang, Zhijun; Wang, Tieshan

2017-10-01

The radio frequency structure design of the radio frequency quadrupole (RFQ) for the front end of China Material Irradiation Facility (CMIF), which is an accelerator based neutron irradiation facility for fusion reactor material qualification, has been completed. The RFQ is specified to accelerate 10 mA continuous deuteron beams from the energies of 20 keV/u to 1.5 MeV/u within the vane length of 5250 mm. The working frequency of the RFQ is selected to 162.5 MHz and the inter-vane voltage is set to 65 kV. Four-vane cavity type is selected and the cavity structure is designed drawing on the experience of China Initiative Accelerator Driven System (CIADS) Injector II RFQ. In order to reduce the azimuthal asymmetry of the field caused from errors in fabrication and assembly, a frequency separation between the working mode and its nearest dipole mode is reached to 17.66 MHz by utilizing 20 pairs of π-mode stabilizing loops (PISLs) distributed along the longitudinal direction with equal intervals. For the purpose of tuning, 100 slug tuners were introduced to compensate the errors caused by machining and assembly. In order to obtain a homogeneous electrical field distribution along cavity, vane cutbacks are introduced and output endplate is modified. Multi-physics study of the cavity with radio frequency power and water cooling is performed to obtain the water temperature tuning coefficients. Through comparing to the worldwide CW RFQs, it is indicated that the power density of the designed structure is moderate for operation under continuous wave (CW) mode.

Influence of the Applied Working Fluid and the Arrangement of the Steering Edges on Multi-Vane Expander Performance in Micro ORC System

Directory of Open Access Journals (Sweden)

Józef Rak

2018-04-01

Full Text Available Micro-power domestic organic Rankine cycle (ORC systems are nowadays of great interest. These systems are considered for combined heat and power (CHP generation in domestic and distributed applications. The main issues of ORC systems design is selection of the expander and the working fluid. Thanks to their positive features, multi-vane expanders are especially promising for application in micro-power ORC systems. These expanders are very simple in design, small in dimensions, inexpensive and feature low gas flow capacity and expansion ratio. The application of multi-vane expanders in ORC systems is innovative and currently limited to prototype applications. However, a literature review indicates the growing interest in these machines and the potential for practical implementation. For this reason, it is necessary to conduct detailed studies on the multi-vane expanders operation in ORC systems. In this paper the results of experimental and numerical investigations on the influence of the applied working fluid and the arrangement of the steering edges on multi-vane expander performance in micro ORC system are reported. The experiments were performed using the specially designed lab test-stand, i.e. the domestic ORC system. Numerical simulations were proceeded in ANSYS CFX software (ANSYS, Inc., Canonsburg, PA, USA and were focused on determining the expander performance under various flow conditions of different working fluids. Detailed numerical analysis of the arrangement of the machine steering edges showed existence of optimal mutual position of the inlet and outlet port for which the multi-vane expander achieves maximum internal work and internal efficiency.

The impact of inlet angle and outlet angle of guide vane on pump in reversal based hydraulic turbine performance

International Nuclear Information System (INIS)

Shi, F X; Yang, J H; Wang, X H; Zhang, R H; Li, C E

2012-01-01

In this paper, in order to research the impact of inlet angle and outlet angle of guide vane on hydraulic turbine performance, a centrifugal pump in reversal is adopted as turbine. A numerical simulation method is adopted for researching outer performance and flow field of turbine. The results show: inlet angle has a crucial role to turbine, to the same flow, there is a noticeable decline for the efficiency and head of turbine with the inlet angle increases. At the best efficiency point(EFP),to a same inlet angle, when the inlet angle greater than inlet angle, velocity circulation in guide vane outlet decreases, which lead the efficiency of turbine to reduce, Contrarily, the efficiency rises. With the increase of inlet angle and outlet angle, the EFP moves to the big flow area and the uniformity of pressure distribution becomes worse. The paper indicates that the inlet angle and outlet angle have great impact on the turbine performance, and the best combination exists for the inlet angle and outlet angle of the guide vane.

Hydraulic analysis of river training cross-vanes as part of post-restoration monitoring

Directory of Open Access Journals (Sweden)

T. A. Endreny

2011-07-01

Full Text Available River restoration design methods are incrementally improved by studying and learning from monitoring data in previous projects. In this paper we report post-restoration monitoring data and simulation analysis for a Natural Channel Design (NCD restoration project along 1600 m of the Batavia Kill (14 km² watershed in the Catskill Mountains, NY. The restoration project was completed in 2002 with goals to reduce bank erosion and determine the efficacy of NCD approaches for restoring headwater streams in the Catskill Mountains, NY. The NCD approach used a reference-reach to determine channel form, empirical relations between the project site and reference site bankfull dimensions to size channel geometry, and hydraulic and sediment computations based on a bankfull (1.3 yr return interval discharge to test channel capacity and sediment stability. The NCD project included 12 cross-vanes and 48 j-hook vanes as river training structures along 19 meander bends to protect against bank erosion and maintain scour pools for fish habitat. Monitoring data collected from 2002 to 2004 were used to identify aggradation of pools in meander bends and below some structures. Aggradation in pools was attributed to the meandering riffle-pool channel trending toward step-pool morphology and cross-vane arms not concentrating flow in the center of the channel. The aggradation subsequently caused flow splitting and 4 partial point bar avulsions during a spring 2005 flood with a 25-yr return interval. Processing the pre-flood monitoring data with hydraulic analysis software provided clues the reach was unstable and preventative maintenance was needed. River restoration and monitoring teams should be trained in robust hydraulic analytical methods that help them extend project restoration goals and structure stability.

Thermal modelling of a dry revolving vane compressor

Science.gov (United States)

Ooi, K. T.; Aw, K. T.

2017-08-01

The lubricant used in compressors serves to lubricate, to seal the gaps to reduce internal leakage and to a certain extent, to cool. However, a lubricant free compressor is attractive if lubricants become a source of contaminant, or in areas where the compressor needs be placed under any orientation, such as those in military or portable computing. In this paper, a thermal model for a dry revolving vane compressor is presented. This thermal model sets out to predict the steady-state operating temperatures of the compressor components. The lumped thermal conductance method was employed. The results of the components temperature will be presented and discussed. A high potential for overheating is observed at the shaft bearings.

Effect of turbulence intensity on cross-injection film cooling at a stepped or smooth endwall of a gas turbine vane passage.

Science.gov (United States)

Wu, Pey-Shey; Tsai, Shen-Ta; Jhuo, Yue-Hua

2014-01-01

This study is concerned with a film cooling technique applicable to the protection of the endwalls of a gas turbine vane. In the experiments, cross-injection coolant flow from two-row, paired, inclined holes with nonintersecting centerlines was utilized. The test model is a scaled two-half vane. The levels of turbulence intensity used in the experiments are T.I. = 1.8%, 7%, and 12%. Other parameters considered in the film cooling experiments include three inlet Reynolds numbers (9.20 × 10(4), 1.24 × 10(5), and 1.50 × 10(5)), three blowing ratios (0.5, 1.0, and 2.0), and three endwall conditions (smooth endwall and stepped endwall with forward-facing or backward-facing step). Thermochromic liquid crystal (TLC) technique with steady-state heat transfer experiments was used to obtain the whole-field film cooling effectiveness. Results show that, at low turbulence intensity, increasing Reynolds number decreases the effectiveness in most of the vane passage. There is no monotonic trend of influence by Reynolds number at high turbulence intensity. The effect of blowing ratio on the effectiveness has opposite trends at low and high turbulence levels. Increasing turbulent intensity decreases the effectiveness, especially near the inlet of the vane passage. With a stepped endwall, turbulence intensity has only mild effect on the film cooling effectiveness.

Effect of Turbulence Intensity on Cross-Injection Film Cooling at a Stepped or Smooth Endwall of a Gas Turbine Vane Passage

Directory of Open Access Journals (Sweden)

Pey-Shey Wu

2014-01-01

Full Text Available This study is concerned with a film cooling technique applicable to the protection of the endwalls of a gas turbine vane. In the experiments, cross-injection coolant flow from two-row, paired, inclined holes with nonintersecting centerlines was utilized. The test model is a scaled two-half vane. The levels of turbulence intensity used in the experiments are T.I.=1.8%, 7%, and 12%. Other parameters considered in the film cooling experiments include three inlet Reynolds numbers (9.20×104 , 1.24×105, and  1.50×105, three blowing ratios (0.5, 1.0, and 2.0, and three endwall conditions (smooth endwall and stepped endwall with forward-facing or backward-facing step. Thermochromic liquid crystal (TLC technique with steady-state heat transfer experiments was used to obtain the whole-field film cooling effectiveness. Results show that, at low turbulence intensity, increasing Reynolds number decreases the effectiveness in most of the vane passage. There is no monotonic trend of influence by Reynolds number at high turbulence intensity. The effect of blowing ratio on the effectiveness has opposite trends at low and high turbulence levels. Increasing turbulent intensity decreases the effectiveness, especially near the inlet of the vane passage. With a stepped endwall, turbulence intensity has only mild effect on the film cooling effectiveness.

Enhancing sediment distribution at the vicinity of power plant intakes using double rows of vanes and groins (Case study: New tebbin power plant

Directory of Open Access Journals (Sweden)

Sayed Mahgoub

2013-12-01

The study results showed that, in case of vanes absence, sediments with rates 1–2 m3/week were stuck within the sediment trap under the winter conditions. Also, the results indicated that the submerged vanes play an important role in preventing the sediment intrusion. Also, it was clear that using groins might lead to enhancing the sediment distribution at the intake vicinity.

Considerations for sampling nuclear materials for SNM accounting measurements. Special nuclear material accountability report

International Nuclear Information System (INIS)

Brouns, R.J.; Roberts, F.P.; Upson, U.L.

1978-05-01

This report presents principles and guidelines for sampling nuclear materials to measure chemical and isotopic content of the material. Development of sampling plans and procedures that maintain the random and systematic errors of sampling within acceptable limits for SNM(Special Nuclear Materials) accounting purposes are emphasized

Loss model for off-design performance analysis of radial turbines with pivoting-vane, variable-area stators

Science.gov (United States)

Meitner, P. L.; Glassman, A. J.

1980-01-01

An off-design performance loss model for a radial turbine with pivoting, variable-area stators is developed through a combination of analytical modeling and experimental data analysis. A viscous loss model is used for the variation in stator loss with setting angle, and stator vane end-clearance leakage effects are predicted by a clearance flow model. The variation of rotor loss coefficient with stator setting angle is obtained by means of an analytical matching of experimental data for a rotor that was tested with six stators, having throat areas from 20 to 144% of the design area. An incidence loss model is selected to obtain best agreement with experimental data. The stator vane end-clearance leakage model predicts increasing mass flow and decreasing efficiency as a result of end-clearances, with changes becoming significantly larger with decreasing stator area.

Flow characteristics of guide vane of diffuser pump by PIV measurement

International Nuclear Information System (INIS)

Kim, J. H.; Lee, Young Ho; Choi, J. W.; Kim, M. Y.; Lee, H.

2000-01-01

The present experimental study is focused on the application of multi-point simultaneous measurement by PIV(Particle Image Velocimetry) to guide vane region within a diffuser pump. Various different kinds of clearance were selected as experimental conditions. Optimized cross correlation identification to obtain velocity vectors was implemented with direct calculation of correlation coefficients. Fine optical setup important in PIV performance is arranged for the accurate PIV measurement of high-speed complex flow. Various flow patterns are represented quantitatively at the stator passages

Numerical Investigations of Unsteady Flow in a Centrifugal Pump with a Vaned Diffuser

Directory of Open Access Journals (Sweden)

Olivier Petit

2013-01-01

Full Text Available Computational fluid dynamics (CFD analyses were made to study the unsteady three-dimensional turbulence in the ERCOFTAC centrifugal pump test case. The simulations were carried out using the OpenFOAM Open Source CFD software. The test case consists of an unshrouded centrifugal impeller with seven blades and a radial vaned diffuser with 12 vanes. A large number of measurements are available in the radial gap between the impeller and the diffuse, making this case ideal for validating numerical methods. Results of steady and unsteady calculations of the flow in the pump are compared with the experimental ones, and four different turbulent models are analyzed. The steady simulation uses the frozen rotor concept, while the unsteady simulation uses a fully resolved sliding grid approach. The comparisons show that the unsteady numerical results accurately predict the unsteadiness of the flow, demonstrating the validity and applicability of that methodology for unsteady incompressible turbomachinery flow computations. The steady approach is less accurate, with an unphysical advection of the impeller wakes, but accurate enough for a crude approximation. The different turbulence models predict the flow at the same level of accuracy, with slightly different results.

MATHEMATICAL MODEL FOR THE STUDY AND DESIGN OF A ROTARY-VANE GAS REFRIGERATION MACHINE

Directory of Open Access Journals (Sweden)

V. V. Trandafilov

2016-08-01

Full Text Available This paper presents a mathematical model of calculating the main parameters the operating cycle, rotary-vane gas refrigerating machine that affect installation, machine control and working processes occurring in it at the specified criteria. A procedure and a graphical method for the rotary-vane gas refrigerating machine (RVGRM are proposed. A parametric study of the main geometric variables and temperature variables on the thermal behavior of the system is analyzed. The model considers polytrope index for the compression and expansion in the chamber. Graphs of the pressure and temperature in the chamber of the angle of rotation of the output shaft are received. The possibility of inclusion in the cycle regenerative heat exchanger is appreciated. The change of the coefficient of performance machine after turning the cycle regenerative heat exchanger is analyzed. It is shown that the installation of a regenerator RVGRM cycle results in increased COP more than 30%. The simulation results show that the proposed model can be used to design and optimize gas refrigerator Stirling.

Scaling laws for gas–liquid flow in swirl vane separators

International Nuclear Information System (INIS)

Liu, Li; Bai, Bofeng

2016-01-01

Highlights: • Model for swirl vane separator performance is established with similarity criteria. • Scaling laws are developed to correlate downscale test with prototype separator. • Effects of key similarity criteria on separation performance are studied. • The vital role of droplet size distribution on separation performance is discussed. - Abstract: Laboratory tests on gas–liquid flow in swirl vane separators are usually carried out to help establish an experimental database for separator design and performance improvement. Such model tests are generally performed in the reduced scale and not on the actual working conditions. Though great efficiency is often obtainable in the reduced model, the performance of the full-sized prototype usually cannot be well predicted. To design downscale model tests and apply the experimental results to predict the prototype, a general relationship to correlate them is required. In this paper, the relation of the similitude-criterion concerning the pressure loss is presented by using the dimensionless analysis, and mathematical models for critical droplet diameter, grade efficiency and overall separation efficiency are established by analyzing the features of the droplet trajectory in gas swirling flow field. The essential similarity criteria accounting for pressure loss and separation efficiency are obtained, respectively. On this basis, the scaling laws which enable a comparison between the reduced model and the full-sized prototype under similar conditions are also developed. It is found that the overall separation efficiency is significantly affected by the size distribution of the small droplets, especially when the mean diameter is smaller than the critical droplet diameter.

Sampling and sample preparation methods for the analysis of trace elements in biological material

International Nuclear Information System (INIS)

Sansoni, B.; Iyengar, V.

1978-05-01

The authors attempt to give a most systamtic possible treatment of the sample taking and sample preparation of biological material (particularly in human medicine) for trace analysis (e.g. neutron activation analysis, atomic absorption spectrometry). Contamination and loss problems are discussed as well as the manifold problems of the different consistency of solid and liquid biological materials, as well as the stabilization of the sample material. The process of dry and wet ashing is particularly dealt with, where new methods are also described. (RB) [de

Neutron-Irradiated Samples as Test Materials for MPEX

International Nuclear Information System (INIS)

Ellis, Ronald James; Rapp, Juergen

2015-01-01

Plasma Material Interaction (PMI) is a major concern in fusion reactor design and analysis. The Material-Plasma Exposure eXperiment (MPEX) will explore PMI under fusion reactor plasma conditions. Samples with accumulated displacements per atom (DPA) damage produced by fast neutron irradiations in the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory (ORNL) will be studied in the MPEX facility. This paper presents assessments of the calculated induced radioactivity and resulting radiation dose rates of a variety of potential fusion reactor plasma-facing materials (such as tungsten). The scientific code packages MCNP and SCALE were used to simulate irradiation of the samples in HFIR including the generation and depletion of nuclides in the material and the subsequent composition, activity levels, gamma radiation fields, and resultant dose rates as a function of cooling time. A challenge of the MPEX project is to minimize the radioactive inventory in the preparation of the samples and the sample dose rates for inclusion in the MPEX facility

Considerations for sampling nuclear materials for SNM accounting measurements

International Nuclear Information System (INIS)

Brouns, R.J.; Roberts, F.P.; Upson, U.L.

1978-01-01

This report presents principles and guidelines for sampling nuclear materials to measure chemical and isotopic content of the material. Development of sampling plans and procedures that maintain the random and systematic errors of sampling within acceptable limits for SNM accounting purposes are emphasized

Combining effect of optimized axial compressor variable guide vanes and bleed air on the thermodynamic performance of aircraft engine system

International Nuclear Information System (INIS)

Kim, Sangjo; Son, Changmin; Kim, Kuisoon

2017-01-01

Aim of this work is to provide evidence of the effectiveness of combined use of the variable guide vanes (VGVs) and bleed air on the thermodynamic performance of aircraft engine system. This paper performed the comparative study to evaluate the overall thermal performance of an aircraft engine with optimized VGVs and bleed air, separately or simultaneously. The low-bypass ratio turbofan engine has been modeled with a 0D/1D modeling approach. The genetic algorithm is employed to find the optimum schedule of VGVs and bleed air. There are four types of design variables: (1) the inlet guide vane (IGV) angle, (2) the IGV and 1st stator vane (SV) angles, (3) bleed air mass flow rate at the exit of the axial compressor, and (4) both type 2 and type 3. The optimization is conducted with surge margin constraints of more than 10% and 15% in the axial compressor. The results show that the additional use of the bleed air increases the efficiency of the compressors. Overall, the percentage reductions of the total fuel consumption for the engine with the IGV, 1st SV and bleed air schedule is 1.63% for 15% surge margin constraints when compared with the engine with the IGV schedule. - Highlights: • The effect of combined use of variable guide vanes and bleed air is evaluated. • The genetic algorithm is employed to find the optimum setting angle and bleed air. • A low bypass ratio mixed turbofan engine is analyzed for optimization. • Additional use of the bleed air shows improved overall performance of the engine.

Special nuclear material inventory sampling plans

International Nuclear Information System (INIS)

Vaccaro, H.; Goldman, A.

1987-01-01

Since their introduction in 1942, sampling inspection procedures have been common quality assurance practice. The U.S. Department of Energy (DOE) supports such sampling of special nuclear materials inventories. The DOE Order 5630.7 states, Operations Offices may develop and use statistically valid sampling plans appropriate for their site-specific needs. The benefits for nuclear facilities operations include reduced worker exposure and reduced work load. Improved procedures have been developed for obtaining statistically valid sampling plans that maximize these benefits. The double sampling concept is described and the resulting sample sizes for double sample plans are compared with other plans. An algorithm is given for finding optimal double sampling plans that assist in choosing the appropriate detection and false alarm probabilities for various sampling plans

A new low threshold bi-directional wind vane and its potential impact on unplanned atmospheric release prediction

International Nuclear Information System (INIS)

Parker, M.J.

1996-01-01

At the Savannah River Site, the Environmental Transport Group (ETG) maintains and develops a comprehensive meteorological monitoring program which employs bi-directional wind vanes (bivanes) for the measurement of horizontal and vertical wind direction and turbulence. Wind data collected near and below instrument starting thresholds under stable nighttime conditions with these bivanes can result in artificially large standard deviations of horizontal wind direction (σA). In one hypothetical case, downwind concentrations could be underestimated by a factor of 40 by using artificially high σA data in a Gaussian dispersion model. In an effort to improve low wind speed measurements of wind direction, a Cooperative Research and Development Agreement (CRADA) between Met One Instruments and the Westinghouse Savannah River Company (WSRC) has been created to improve the dynamic performance of the Met One Model 1585 Bi-Directional Wind Vane

Device for sampling liquid radioactive materials

International Nuclear Information System (INIS)

Vlasak, L.

1987-01-01

Remote sampling of radioactive materials in the process of radioactive waste treatment is claimed by the Czechoslovak Patent Document 238599. The existing difficulties are eliminated consisting in a complex remote control of sampling featuring the control of sliding and rotary movements of the sampling device. The new device consists of a vertical pipe with an opening provided with a cover. A bend is provided above the opening level housing flow distributors. A sampling tray is pivoted in the cover. In sampling, the tray is tilted in the vertical pipe space while it tilts back when filled. The sample flows into a vessel below the tray. Only rotary movement is thus sufficient for controlling the tray. (Z.M.)

Change of performance of a horizontal wind turbine with V type tip vane%风力机加V型小翼后的性能变化

Institute of Scientific and Technical Information of China (English)

贾瑞博; 汪建文

2011-01-01

试验和数值模拟证明,在风力机叶片的叶尖添加小翼,可以提高风能转化效率.为了清楚地了解小翼对风力机动力放大的影响,文章基于叶轮周围流场的数值模拟结果,分析了加V型小翼和不加小翼的风力机流场-速度场和压力场特性.可以看出,小翼对风力机叶片叶端的影响较大,风力机叶尖的漩涡强度降低,能量转换效率提高.%It was proved that a tip vane could improve thewind turbine's efficiency by the test and the numerical simulation. In order to distinctly understand the power augmentation effect of the wind turbine by the tip vane, this paper analyzed the flow field of the wind turbine with the V type tip vane and without a tip vane, as well as the characteristics of the velocity field and the pressure field, which based on the numerical simulation result of the flow field of the wind turbine. The tip vane has more influence to the blade tip of the wind turbine. The vortex intensity around the blade tip was reduced and the energy transformation efficiency was improved.

New materials for sample preparation techniques in bioanalysis.

Science.gov (United States)

Nazario, Carlos Eduardo Domingues; Fumes, Bruno Henrique; da Silva, Meire Ribeiro; Lanças, Fernando Mauro

2017-02-01

The analysis of biological samples is a complex and difficult task owing to two basic and complementary issues: the high complexity of most biological matrices and the need to determine minute quantities of active substances and contaminants in such complex sample. To succeed in this endeavor samples are usually subject to three steps of a comprehensive analytical methodological approach: sample preparation, analytes isolation (usually utilizing a chromatographic technique) and qualitative/quantitative analysis (usually with the aid of mass spectrometric tools). Owing to the complex nature of bio-samples, and the very low concentration of the target analytes to be determined, selective sample preparation techniques is mandatory in order to overcome the difficulties imposed by these two constraints. During the last decade new chemical synthesis approaches has been developed and optimized, such as sol-gel and molecularly imprinting technologies, allowing the preparation of novel materials for sample preparation including graphene and derivatives, magnetic materials, ionic liquids, molecularly imprinted polymers, and much more. In this contribution we will review these novel techniques and materials, as well as their application to the bioanalysis niche. Copyright © 2016 Elsevier B.V. All rights reserved.

Predicting sample lifetimes in creep fracture of heterogeneous materials

Science.gov (United States)

Koivisto, Juha; Ovaska, Markus; Miksic, Amandine; Laurson, Lasse; Alava, Mikko J.

2016-08-01

Materials flow—under creep or constant loads—and, finally, fail. The prediction of sample lifetimes is an important and highly challenging problem because of the inherently heterogeneous nature of most materials that results in large sample-to-sample lifetime fluctuations, even under the same conditions. We study creep deformation of paper sheets as one heterogeneous material and thus show how to predict lifetimes of individual samples by exploiting the "universal" features in the sample-inherent creep curves, particularly the passage to an accelerating creep rate. Using simulations of a viscoelastic fiber bundle model, we illustrate how deformation localization controls the shape of the creep curve and thus the degree of lifetime predictability.

Mapping of the lateral flow field in typical subchannels of a support grid with vanes

International Nuclear Information System (INIS)

McClusky, Heather L.; Holloway, Mary V.; Conover, Timothy A.; Beasley, Donald E.; Conner, Michael E.; Smith III, L. David

2003-01-01

Lateral flow fields in four subchannels of a model rod bundle fuel assembly are measured using particle image velocimetry. Vanes (split-vane pairs) are located on the downstream edge of the support grids in the rod bundle fuel assembly and generate swirling flow. Measurements are acquired at a nominal Reynolds number of 28,000 and for seven streamwise locations ranging from 1.4 to 17.0 hydraulic diameters downstream of the grid. The streamwise development of the lateral flow field is divided into two regions based on the lateral flow structure. In Region I, multiple vortices are present in the flow field and vortex interactions occur. Either a single circular vortex or a hairpin shaped flow structure is formed in Region II. Lateral kinetic energy, maximum lateral velocity, centroid of vorticity, radial profiles of azimuthal velocity, and angular momentum are employed as measures of the streamwise development of the lateral flow field. The particle image velocimetry measurements of the present study are compared with laser doppler velocimetry measurements taken for the identical support grids and flow condition. (author)

On development of RFQ vanes from beam dynamics data

International Nuclear Information System (INIS)

Chatterjee, Avik; Padhi, Rakesh; Banerjee, M.K.; Naik, Vaishali; Sanyal, Dirtha; Choudhury, Siddhartha De; Chakrabarti, Alok

2005-01-01

Simulation at critical steps of product development greatly helps to detect the design flaws at the earlier stage and gives a digital platform to iterate the design and process at the initial stage. This helps to reduce the risk of failure considerably and gives an alternative to reduce the number of physical prototypes for design validation. Modern concepts of virtual prototyping for predicting functional behaviour of a product and process are gaining momentum globally as it is the fully integrated approach to converge the concepts of functional design, Design for Manufacturing (DFM), Design for Assembly (DFA) and manufacturing process simulation. This concept has been partially implemented in development of RFQ (Radio Frequency Quadruple) vanes and the basic guidelines have been discussed. (author)

Sampling by electro-erosion on irradiated materials

International Nuclear Information System (INIS)

Riviere, M.; Pizzanelli, J.P.

1986-05-01

Sampling on irradiated materials, in particular for mechanical property study of steels in the FAST NEUTRON program needed the set in a hot cell of a machining device by electroerosion. This device allows sampling of tenacity, traction, resilience test pieces [fr

Investigation of the Optimal Omni-Direction-Guide-Vane Design for Vertical Axis Wind Turbines Based on Unsteady Flow CFD Simulation

Directory of Open Access Journals (Sweden)

Behzad Shahizare

2016-03-01

Full Text Available With soaring energy demands, the desire to explore alternate and renewable energy resources has become the focal point of various active research fronts. Therefore, the scientific community is revisiting the notion to tap wind resources in more rigorous and novel ways. In this study, a two-dimensional computational investigation of the vertical axis wind turbine (VAWT with omni-direction-guide-vane (ODGV is proposed to determine the effects of this guide vane. In addition, the mesh and time step (dt size dependency test, as well as the effect of the different turbulence models on results accuracy are investigated. Eight different shape ratios (R of the omni-direction-guide-vane were also examined in this study. Further, the CFD model is validated by comparing the numerical results with the experimental data. Validation results show a good agreement in terms of shape and trend in CFD simulation. Based on these results, all the shape ratios, except two ratios including 0.3 and 0.4 at TSR of 1.3 to 3, have a positive effect on the power and torque coefficient improvement. Moreover, results show that the best case has a shape ratio of 0.55, which improves the power coefficient by 48% and the torque coefficient up to 58%.

Preliminary results for validation of Computational Fluid Dynamics for prediction of flow through a split vane spacer grid

International Nuclear Information System (INIS)

Rashkovan, A.; Novog, D.R.

2012-01-01

This paper presents the results of the CFD simulations of turbulent flow past spacer grid with mixing vanes. This study summarizes the first stage of the ongoing numerical blind exercise organized by OECD-NEA. McMaster University along with other participants plan to submit a numerical prediction of the detailed flow field and turbulence characteristics of the flow past 5x5 rod bundle with a spacer grid equipped with two types of mixing vanes. The results will be compared with blind experimental measurements performed in Korea. Due to the fact that a number of the modeling strategies are suggested in literature for such types of flows, we have performed a series of tests to assess the mesh requirements, flow steadiness, turbulence modeling and wall treatment effects. Results of these studies are reported in the present paper. (author)

2.5 MeV CW 4-vane RFQ accelerator design for BNCT applications

Science.gov (United States)

Zhu, Xiaowen; Wang, Hu; Lu, Yuanrong; Wang, Zhi; Zhu, Kun; Zou, Yubin; Guo, Zhiyu

2018-03-01

Boron Neutron Capture Therapy (BNCT) promises a bright future in cancer therapy for its highly selective destruction of cancer cells, using the 10B +n→7Li +4 He reaction. It offers a more satisfactory therapeutic effect than traditional methods for the treatment of malignant brain tumors, head and neck cancer, melanoma, liver cancer and so on. A CW 4-vane RFQ, operating at 162.5 MHz, provides acceleration of a 20 mA proton beam to 2.5 MeV, bombarding a liquid lithium target for neutron production with a soft neutron energy spectrum. The fast neutron yield is about 1.73×1013 n/s. We preliminarily develop and optimize a beam shaping assembly design for the 7Li(p, n)7Be reaction with a 2.5 MeV proton beam. The epithermal neutron flux simulated at the beam port will reach up to 1 . 575 ×109 n/s/cm2. The beam dynamics design, simulation and benchmark for 2.5 MeV BNCT RFQ have been performed with both ParmteqM (V3.05) and Toutatis, with a transmission efficiency higher than 99.6% at 20 mA. To ease the thermal management in the CW RFQ operation, we adopt a modest inter-vane voltage design (U = 65 kV), though this does increase the accelerator length (reaching 5.2 m). Using the well-developed 3D electromagnetic codes, CST MWS and ANSYS HFSS, we are able to deal with the complexity of the BNCT RFQ, taking the contribution of each component in the RF volume into consideration. This allows us to optimize the longitudinal field distribution in a full-length model. Also, the parametric modeling technique is of great benefit to extensive modifications and simulations. In addition, the resonant frequency tuning of this RFQ is studied, giving the tuning sensitivities of vane channel and wall channel as -16.3 kHz/°C and 12.4 kHz/°C, respectively. Finally, both the multipacting level of this RFQ and multipacting suppressing in the coaxial coupler are investigated.

Effects of Mie tip-vane on pressure distribution of rotor blade and power augmentation of horizontal axis wind turbine; Yokutan shoyoku Mie ben ni yoru suiheijiku fusha yokumenjo no atsuryoku bunpu no kaizen to seino kojo tono kankei

Energy Technology Data Exchange (ETDEWEB)

Shimizu, Y.; Maeda, T.; Kamada, Y. [Mie Univ., Mie (Japan); Seto, H. [Mitsubishi Motors Corp., Tokyo (Japan)

2000-04-01

By recent developments of exclusive rotor blade, the efficiency of wind turbine is improved substantially. By measuring pressure on rotor blades of horizontal axis wind turbines rotating in wind tunnels, this report clarified relation between improvement of pressure distribution on main rotor blades by Mie vane and upgrade of wind turbine performance. The results under mentioned have been got by measuring pressure distribution on rotor blades, visualization by tuft, and measuring resistance of Mie vane. (1) The difference of pressure between suction surface and pressure surface on the end of rotor blade increase, and output power of wind turbine improves. (2) Vortex of blade end is inhibited by Mie vane. (3) The reason of reduction on wind turbine performance with Mie vane in aria of high rotating speed ratio is the increase of Mie vane flow resistance.(NEDO)

Influence of omni-directional guide vane on the performance of cross-flow rotor for urban wind energy

Science.gov (United States)

Wicaksono, Yoga Arob; Tjahjana, Dominicus Danardono Dwi Prija; Hadi, Syamsul

2018-02-01

Vertical axis wind turbine like cross-flow rotor have some advantage there are, high self-starting torque, low noise, and high stability; so, it can be installed in the urban area to produce electricity. But, the urban area has poor wind condition, so the cross-flow rotor needs a guide vane to increase its performance. The aim of this study is to determine experimentally the effect of Omni-Directional Guide Vane (ODGV) on the performance of a cross-flow wind turbine. Wind tunnel experiment has been carried out for various configurations. The ODGV was placed around the cross-flow rotor in order to increase ambient wind environment of the wind turbine. The maximum power coefficient is obtained as Cpmax = 0.125 at 60° wind direction. It was 21.46% higher compared to cross-flow wind turbine without ODGV. This result showed that the ODGV able to increase the performance of the cross-flow wind turbine.

3D computations of flow field in a guide vane blading designed by means of 2D model for a low head hydraulic turbine

International Nuclear Information System (INIS)

Krzemianowski, Z; Puzyrewski, R

2014-01-01

The paper presents the main parameters of the flow field behind the guide vane cascade designed by means of 2D inverse problem and following check by means of 3D commercial program ANSYS/Fluent applied for a direct problem. This approach of using different models reflects the contemporary design procedure for non-standardized turbomachinery stage. Depending on the model, the set of conservation equation to be solved differs, although the physical background remains the same. The example of computations for guide vane cascade for a low head hydraulic turbine is presented.

Sampling, storage and sample preparation procedures for X ray fluorescence analysis of environmental materials

International Nuclear Information System (INIS)

1997-06-01

X ray fluorescence (XRF) method is one of the most commonly used nuclear analytical technique because of its multielement and non-destructive character, speed, economy and ease of operation. From the point of view of quality assurance practices, sampling and sample preparation procedures are the most crucial steps in all analytical techniques, (including X ray fluorescence) applied for the analysis of heterogeneous materials. This technical document covers recent modes of the X ray fluorescence method and recent developments in sample preparation techniques for the analysis of environmental materials. Refs, figs, tabs

Proposal of a novel compact P-band magnetically insulated transmission line oscillator with inclined vanes

Science.gov (United States)

Zhang, Xiaoping; Dang, Fangchao; Li, Yangmei; Jin, Zhenxing

2015-06-01

In this paper, we present a novel compact P-band magnetically insulated transmission line oscillator (MILO) with specially inclined slow-wave-structure (SWS) vanes to decrease its total dimension and weight. The dispersion characteristics of the inclined SWS are investigated in detail and made comparisons with that of the traditional straight SWS. The results show that the inclined SWS is more advantageous in operating on a steady frequency in a wide voltage range and has a better asymmetric mode segregation and a relatively large band-gap between the TM00 and TM01 modes which are in favor of avoiding the asymmetric and transverse mode competition. Besides, the transverse dimension of the proposed novel inclined SWS with the same operation frequency is decreased by about 50%, and correspondingly the device volume shrinks remarkably to its 0.35 times. In particle-in-cell simulation, the electron bunching spokes are obviously formed in the inclined SWS, and a P-band high-power microwave with a power of 5.8 GW, frequency of 645 MHz, and efficiency of 17.2% is generated by the proposed device, which indicates the feasibility of the compact design with the inclined vanes at the P-band.

Membrane materials for storing biological samples intended for comparative nanotoxicological testing

Science.gov (United States)

Metelkin, A.; Kuznetsov, D.; Kolesnikov, E.; Chuprunov, K.; Kondakov, S.; Osipov, A.; Samsonova, J.

2015-11-01

The study is aimed at identifying the samples of most promising membrane materials for storing dry specimens of biological fluids (Dried Blood Spots, DBS technology). Existing sampling systems using cellulose fiber filter paper have a number of drawbacks such as uneven distribution of the sample spot, dependence of the spot spreading area on the individual biosample properties, incomplete washing-off of the sample due to partially inconvertible sorption of blood components on cellulose fibers, etc. Samples of membrane materials based on cellulose, polymers and glass fiber with applied biosamples were studied using methods of scanning electron microscopy, FT-IR spectroscopy and surface-wetting measurement. It was discovered that cellulose-based membrane materials sorb components of biological fluids inside their structure, while membranes based on glass fiber display almost no interaction with the samples and biological fluid components dry to films in the membrane pores between the structural fibers. This characteristic, together with the fact that membrane materials based on glass fiber possess sufficient strength, high wetting properties and good storage capacity, attests them as promising material for dry samples of biological fluids storage systems.

Membrane materials for storing biological samples intended for comparative nanotoxicological testing

International Nuclear Information System (INIS)

Metelkin, A; Kuznetsov, D; Kolesnikov, E; Chuprunov, K; Kondakov, S; Osipov, A; Samsonova, J

2015-01-01

The study is aimed at identifying the samples of most promising membrane materials for storing dry specimens of biological fluids (Dried Blood Spots, DBS technology). Existing sampling systems using cellulose fiber filter paper have a number of drawbacks such as uneven distribution of the sample spot, dependence of the spot spreading area on the individual biosample properties, incomplete washing-off of the sample due to partially inconvertible sorption of blood components on cellulose fibers, etc. Samples of membrane materials based on cellulose, polymers and glass fiber with applied biosamples were studied using methods of scanning electron microscopy, FT-IR spectroscopy and surface-wetting measurement. It was discovered that cellulose-based membrane materials sorb components of biological fluids inside their structure, while membranes based on glass fiber display almost no interaction with the samples and biological fluid components dry to films in the membrane pores between the structural fibers. This characteristic, together with the fact that membrane materials based on glass fiber possess sufficient strength, high wetting properties and good storage capacity, attests them as promising material for dry samples of biological fluids storage systems. (paper)

Turbine blade and vane heat flux sensor development, phase 2

Science.gov (United States)

Atkinson, W. H.; Cyr, M. A.; Strange, R. R.

1985-01-01

The development of heat flux sensors for gas turbine blades and vanes and the demonstration of heat transfer measurement methods are reported. The performance of the heat flux sensors was evaluated in a cylinder in cross flow experiment and compared with two other heat flux measurement methods, the slug calorimeter and a dynamic method based on fluctuating gas and surface temperature. Two cylinders, each instrumented with an embedded thermocouple sensor, a Gardon gauge, and a slug calorimeter, were fabricated. Each sensor type was calibrated using a quartz lamp bank facility. The instrumented cylinders were then tested in an atmospheric pressure combustor rig at conditions up to gas stream temperatures of 1700K and velocities to Mach 0.74. The test data are compared to other measurements and analytical prediction.

Computational Fluid Dynamics (CFD) Analyses in Support of Space Shuttle Main Engine (SSME) Heat Exchanger (HX) Vane Cracking Investigation

Science.gov (United States)

Garcia, Roberto; Benjamin, Theodore G.; Cornelison, J.; Fredmonski, A. J.

1993-01-01

Integration issues involved with installing the alternate turbopump (ATP) High Pressure Oxygen Turbopump (HPOTP) into the SSME have raised questions regarding the flow in the HPOTP turnaround duct (TAD). Steady-state Navier-Stokes CFD analyses have been performed by NASA and Pratt & Whitney (P&W) to address these questions. The analyses have consisted of two-dimensional axisymmetric calculations done at Marshall Space Flight Center and three-dimensional calculations performed at P&W. These analyses have identified flowfield differences between the baseline ATP and the Rocketdyne configurations. The results show that the baseline ATP configuration represents a more severe environment to the inner HX guide vane. This vane has limited life when tested in conjunction with the ATP but infinite life when tested with the current SSME HPOTP. The CFD results have helped interpret test results and have been used to assess proposed redesigns. This paper includes details of the axisymmetric model, its results, and its contribution towards resolving the problem.

Sampling and Characterization of 618-2 Anomalous Material

International Nuclear Information System (INIS)

Zacharias, A.E.

2006-01-01

This as low as reasonably achievable (ALARA) Level II review documents radiological engineering and administrative controls necessary for the sampling and characterization of anomalous materials discovered during the remediation of the 618-2 solid waste burial ground. The goals of these engineering and administrative controls are to keep personnel exposure ALARA, control contamination levels, and minimize potential for airborne contamination. Excavation of the 618-2 Burial Ground has produced many items of anomalous waste. Prior to temporary packaging and/or storage, these items have been characterized in the field to identify radiological and industrial safety conditions. Further sampling and characterization of these items, as well as those remaining from an excavated combination safe, is the subject of this ALARA Level II review. An ALARA in-progress review will also be performed prior to sampling and characterization of 618-2 anomalous materials offering risks of differing natures. General categories of anomalies requiring further characterization include the following: (1) Containers of unknown liquids and/or solids and powders (excluding transuranics); (2) Drums containing unknown liquids and/or solids; (3) Metal containers with unknown contents; and (4) Known or suspected transuranic material.

Electrostatic Evaluation of the ARES I FTS Antenna Materials

Science.gov (United States)

Hogue, Michael D.; Calle, Carlos I.

2010-01-01

Surface resistivity and volume resistivity data show all the tested non-metallic materials of the Ares I FTS antenna assembly to be insulative. The external materials (White foam, phenolic) should be able to develop a large surface charge density upon tribocharging with ice crystal impingement. Dielectric breakdown tests on the FTS antenna housing materials show that each of the insulative materials are very resistive to electrical breakdown. The thicknesses of these materials in a nominal housing should protect the antenna from direct breakdown from external triboelectric charging potentials. Per data from the Air Force study, a maximum external electric potential in the range of 100kV can be developed on surfaces tribocharged by ice crystal impingement. Testing showed that under operational pressure ranges, this level of exterior voltage can result in a potential of about 6 kV induced on the electrically floating interior antenna vanes. Testing the vanes up to this voltage level showed that electrostatic discharges can occur between the electrically floating vanes and the center, grounded screw heads. Repeated tests with multiple invisible and visible discharges caused only superficial physical damage to the vanes. Fourier analysis of the discharge signals showed that the frequency range of credible discharges would not interfere with the nominal operation of the FTS antenna. However, due to the limited scope, short timetable, and limited funding of this study, a direct measurement of the triboelectric charge that could be generated on the Ares I antenna housing when the rocket traverses an ice cloud at supersonic speeds was not performed. Instead, data for the limited Air Force study [3] was used as input for our experiments. The Air Force data used was not collected with a sensor located to provide us with the best approximation at the geometry of the Ares I rocket, namely that of the windshield electrometer, because brush discharges to the metal frame of the

Sampling and analysis of alien materials in soil

Energy Technology Data Exchange (ETDEWEB)

Liphard, K G

1987-02-01

For the determination of alien materials in soil, sampling is the decisive step. After minute planning, samples can be obtained by probing, boring or abrasion. Some types of substances can be verified by advance sampling, partly already in the field. Inorganic substances present as anions or cations are eluted and determined with water, heavy metals are determined after preparing a number of solutions by spectroscopic methods. Organic alien substances are extracted with solvents and, as a rule, analysed by chromatography.

Rheology and TIC/TOC results of ORNL tank samples

International Nuclear Information System (INIS)

Pareizs, J. M.; Hansen, E. K.

2013-01-01

The Savannah River National Laboratory (SRNL)) was requested by Oak Ridge National Laboratory (ORNL) to perform total inorganic carbon (TIC), total organic carbon (TOC), and rheological measurements for several Oak Ridge tank samples. As received slurry samples were diluted and submitted to SRNL-Analytical for TIC and TOC analyses. Settled solids yield stress (also known as settled shear strength) of the as received settled sludge samples were determined using the vane method and these measurements were obtained 24 hours after the samples were allowed to settled undisturbed. Rheological or flow properties (Bingham Plastic viscosity and Bingham Plastic yield stress) were determined from flow curves of the homogenized or well mixed samples. Other targeted total suspended solids (TSS) concentrations samples were also analyzed for flow properties and these samples were obtained by diluting the as-received sample with de-ionized (DI) water

Spiked natural matrix materials as quality assessment samples

International Nuclear Information System (INIS)

Feiner, M.S.; Sanderson, C.G.

1988-01-01

The Environmental Measurements Laboratory has conducted the Quality Assessment Program since 1976 to evaluate the quality of the environmental radioactivity data, which is reported to the Department of Energy by as many as 42 commercial contractors involved in nuclear work. In this program, matrix materials of known radionuclide concentrations are distributed routinely to the contractors and the reported results are compared. The five matrices used are: soil, vegetation, animal tissue, water and filter paper. Environmental soil, vegetation and animal tissue are used, but the water and filter paper samples are prepared by spiking with known amounts of standard solutions traceable to the National Bureau of Standards. A summary of results is given to illustrate the successful operation of the program. Because of the difficulty and high cost of collecting large samples of natural matrix material and to increase the versatility of the program, an attempt was recently made to prepare the soil, vegetation and animal tissue samples with spiked solutions. A description of the preparation of these reference samples and the results of analyses are presented along with a discussion of the pitfalls and advantages of this approach. 19 refs.; 6 tabs

Amoebae and other protozoa in material samples from moisture-damaged buildings

International Nuclear Information System (INIS)

Yli-Pirilae, T.; Kusnetsov, Jaana; Haatainen, Susanna; Haenninen, Marja; Jalava, Pasi; Reiman, Marjut; Seuri, Markku; Hirvonen, Maija-Riitta; Nevalainen, Aino

2004-01-01

Mold growth in buildings has been shown to be associated with adverse health effects. The fungal and bacterial growth on moistened building materials has been studied, but little attention has been paid to the other organisms spawning in the damaged materials. We examined moist building materials for protozoa, concentrating on amoebae. Material samples (n=124) from moisture-damaged buildings were analyzed for amoebae, fungi, and bacteria. Amoebae were detected in 22% of the samples, and they were found to favor cooccurrence with bacteria and the fungi Acremonium spp., Aspergillus versicolor, Chaetomium spp., and Trichoderma spp. In addition, 11 seriously damaged samples were screened for other protozoa. Ciliates and flagellates were found in almost every sample analyzed. Amoebae are known to host pathogenic bacteria, such as chlamydiae, legionellae, and mycobacteria and they may have a role in the complex of exposure that contributes to the health effects associated with moisture damage in buildings

Laser Materials Processing Final Report CRADA No. TC-1526-98

Energy Technology Data Exchange (ETDEWEB)

Crane, J. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Lehane, C. J. [United Technologies Corp., East Hartford, CT (United States)

2017-09-08

This CRADA project was a joint effort between Lawrence Livermore National Laboratory (LLNL) and United Technologies Corporation (UTC)/Pratt & Whitney (P&W) to demonstrate process capability for drilling holes in turbine airfoils using LLNL-developed femtosecond laser machining technology. The basis for this development was the ability of femtosecond lasers to drill precision holes in variety of materials with little or no collateral damage. The ultimate objective was to develop a laser machine tool consisting of an extremely advanced femtosecond laser subsystem to be developed by LLNL on a best-effort basis and a drilling station for turbine blades and vanes to be developed by P&W. In addition, P&W was responsible for commercializing the system. The goal of the so called Advanced Laser Drilling (ALD) system was to drill specified complex hole-shapes in turbine blades and vanes with a high degree precision and repeatability and simultaneously capable of very high speed processing.

Sample size optimization in nuclear material control. 1

International Nuclear Information System (INIS)

Gladitz, J.

1982-01-01

Equations have been derived and exemplified which allow the determination of the minimum variables sample size for given false alarm and detection probabilities of nuclear material losses and diversions, respectively. (author)

Experimental comparison of the optical measurements of a cross-flow in a rod bundle with mixing vanes

International Nuclear Information System (INIS)

Chang, Seok Kyu; Choo, Yeon Jun; Kim, Bok Deuk; Song, Chul Hwa

2008-01-01

The lateral crossflow on subchannels in a rod bundle array was investigated to understand the flow characteristics related to the mixing vane types on a spacer grid by using the PIV technique. For more measurement resolutions, a 5x5 rod bundle was fabricated a 2.6 times larger than the real rod bundle size in a pressurized water reactor. A rod-embedded optic array was specially designed and used for the illumination of the inner subchannels. The crossflow field in a subchannel was characterized by the type and the arrangement of the mixing vanes. At a near downstream location from the spacer grid (z/D h =1) in the case of the split type, a couple of small vortices were generated diagonally in a subchannel. On the other hand, in the case of the swirl type, there was a large elliptic vortex generated in the center of a subchannel. The measurement results were compared with the experimental results which had been performed with the LDV technique at the same test facility. The magnitudes of the flow velocity and the vorticity in PIV results were less than those in LDV measurement results. It was shown that the instantaneous flow fields in a subchannel frequently have quite different shapes from the averaged one

Sampling for the verification of materials balances

International Nuclear Information System (INIS)

Avenhaus, R.; Goeres, H.J.; Beedgen, R.

1983-08-01

The results of a theory for verification of nuclear materials balance data are presented. The sampling theory is based on two diversion models where also a combination of models is taken into account. The theoretical considerations are illustrated with numerical examples using the data of a highly enriched uranium fabrication plant. (orig.) [de

Improved explosive collection and detection with rationally assembled surface sampling materials

Energy Technology Data Exchange (ETDEWEB)

Chouyyok, Wilaiwan; Bays, J. Timothy; Gerasimenko, Aleksandr A.; Cinson, Anthony D.; Ewing, Robert G.; Atkinson, David A.; Addleman, R. Shane

2016-01-01

Sampling and detection of trace explosives is a key analytical process in modern transportation safety. In this work we have explored some of the fundamental analytical processes for collection and detection of trace level explosive on surfaces with the most widely utilized system, thermal desorption IMS. The performance of the standard muslin swipe material was compared with chemically modified fiberglass cloth. The fiberglass surface was modified to include phenyl functional groups. When compared to standard muslin, the phenyl functionalized fiberglass sampling material showed better analyte release from the sampling material as well as improved response and repeatability from multiple uses of the same swipe. The improved sample release of the functionalized fiberglass swipes resulted in a significant increase in sensitivity. Various physical and chemical properties were systematically explored to determine optimal performance. The results herein have relevance to improving the detection of other explosive compounds and potentially to a wide range of other chemical sampling and field detection challenges.

Influence of steam leakage through vane, gland, and shaft seals on rotordynamics of high-pressure rotor of a 1,000 MW ultra-supercritical steam turbine

Energy Technology Data Exchange (ETDEWEB)

Jiang, P.N. [Shanghai Jiao Tong University, Key Laboratory of Power Machinery and Engineering, Ministry of Education, School of Mechanical Engineering, Shanghai (China); Shanghai Turbine Company, Department of R and D, Shanghai (China); Wang, W.Z.; Liu, Y.Z. [Shanghai Jiao Tong University, Key Laboratory of Power Machinery and Engineering, Ministry of Education, School of Mechanical Engineering, Shanghai (China); Meng, G. [Shanghai Jiao Tong University, State Key Laboratory of Mechanical System and Vibration, School of Mechanical Engineering, Shanghai (China)

2012-02-15

A comparative analysis of the influence of steam leakage through vane, gland, and shaft seals on the rotordynamics of the high-pressure rotor of a 1,000 MW ultra-supercritical steam turbine was performed using numerical calculations. The rotordynamic coefficients associated with steam leakage through the three labyrinth seals were calculated using the control-volume method and perturbation analysis. A stability analysis of the rotor system subject to the steam forcing induced by the leakage flow was performed using the finite element method. An analysis of the influence of the labyrinth seal forcing on the rotordynamics was carried out by varying the geometrical parameters pertaining to the tooth number, seal clearance, and inner diameter of the labyrinth seals, along with the thermal parameters with respect to pressures and temperatures. The results demonstrated that the steam forcing with an increase in the length of the blade for the vane seal significantly influences the rotordynamic coefficients. Furthermore, the contribution of steam forcing to the instability of the rotor is decreased and increased with increases in the seal clearance and tooth number, respectively. The comparison of the rotordynamic coefficients associated with steam leakage through the vane seal, gland seal, and shaft seal convincingly disclosed that, although the steam forcing attenuates the stability of the rotor system, the steam turbine is still operating under safe conditions. (orig.)

Does Passive Sampling Accurately Reflect the Bee (Apoidea: Anthophila) Communities Pollinating Apple and Sour Cherry Orchards?

Science.gov (United States)

Gibbs, Jason; Joshi, Neelendra K; Wilson, Julianna K; Rothwell, Nikki L; Powers, Karen; Haas, Mike; Gut, Larry; Biddinger, David J; Isaacs, Rufus

2017-06-01

During bloom of spring orchard crops, bees are the primary providers of pollination service. Monitoring these insects for research projects is often done by timed observations or by direct aerial netting, but there has been increasing interest in blue vane traps as an efficient passive approach to collecting bees. Over multiple spring seasons in Michigan and Pennsylvania, orchards were monitored for wild bees using timed netting from crop flowers and blue vane traps. This revealed a distinctly different community of wild bees captured using the two methods, suggesting that blue vane traps can complement but cannot replace direct aerial netting. The bee community in blue vane traps was generally composed of nonpollinating species, which can be of interest for broader biodiversity studies. In particular, blue vane traps caught Eucera atriventris (Smith), Eucera hamata (Bradley), Bombus fervidus (F.), and Agapostemon virescens (F.) that were never collected from the orchard crop flowers during the study period. Captures of bee species in nets was generally stable across the 3 yr, whereas we observed significant declines in the abundance of Lasioglossum pilosum (Smith) and Eucera spp. trapped using blue vane traps during the project, suggesting local overtrapping of reproductive individuals. We conclude that blue vane traps are a useful tool for expanding insights into bee communities within orchard crop systems, but they should be used with great caution to avoid local extirpation of these important insects. © The Authors 2017. Published by Oxford University Press on behalf of Entomological Society of America. All rights reserved. For Permissions, please email: journals.permissions@oup.com.

Technicians work with Apollo 14 lunar sample material in Lunar Receiving Lab.

Science.gov (United States)

1971-01-01

Glove handlers work with freshly opened Apollo 14 lunar sample material in modularized cabinets in the Lunar Receiving Laboratory at the Manned Spacecraft Center. The glove operator on the right starts to pour fine lunar material which he has just taken from a tote bag. This powdery sample was among the last to be revealed of the 90-odd pounds of material brought back to Earth by the Apollo 14 crewmen.

导叶对涡轮型垂直轴风力机气动性能的影响%Effects of guiding vanes on aerodynamic performance of vortex vertical axis wind turbine

Institute of Scientific and Technical Information of China (English)

原红红; 赵振宙; 郑源; 黄娟

2013-01-01

To overcome the problem of low efficiency of the traditional vertical axis wind turbine, the structural advantages of the wind turbine with guiding vanes are introduced and the effects of guiding vanes on the vortex vertical axis wind turbine are analyzed in detail. Based on computational fluid dynamics theory, the slippage mesh technique and the k-ε model were used to compare the aerodynamic performance of the vortex vertical axis wind turbine with and without guiding vanes at a design velocity of 12 m/s. Studies have shown that the guiding vanes can effectively prevent the direct impact of the coming flow from acting on the suction section of the blade in the upwind area so as to decrease the drag torque, while the guiding vanes also negatively affect the performance of blades in the downwind area, but the positive effect of the former is more significant, so the performance of a wind turbine with guiding vanes greatly improves. The vortex vertical axis wind turbine with arc-type guiding vanes has a wider operating range, higher optimum tip speed ratio, and higher aerodynamic efficiency. The maximum wind power coefficient can reach 0.24 .%针对传统垂直轴风力机效率低的缺陷,阐述带导叶垂直轴风力机的结构优势,并分析导叶对涡轮型垂直轴风力机的作用。应用计算流体力学理论,在设计风速12 m/s下,采用滑移网格技术及k-着模型对有、无导叶两种涡轮型垂直轴风力机的气动性能进行比较。研究表明,导叶可以有效降低由于来流对逆风区叶片吸力面的直接冲击而造成的阻力扭矩,也会负面影响顺风区叶片的性能,但其负作用效果远不及在逆风区挡流降阻的正作用效果,故加导叶后风轮的性能会有很大提高。带弧线形导叶涡轮型垂直轴风力机最大风能利用系数可达0.24,具有工作范围广、最佳尖速比大的特点。

Tubular-Type Hydroturbine Performance for Variable Guide Vane Opening by CFD

Science.gov (United States)

Kim, Y. T.; Nam, S. H.; Cho, Y. J.; Hwang, Y. C.; Choi, Y. D.; Nam, C. D.; Lee, Y. H.

Micro hydraulic power generation which has output of less or equal to 100kW is attracting considerable attention. This is because of its small, simple, renewable, and large amount of energy resources. By using a small hydro power generator of which main concept is based on using differential water pressures in pipe lines, energy which was initially wasted by use of a reducing valve at an end of the pipeline, is collected by a turbine in the hydro power generator. A propeller shaped hydroturbine has been used in order to make use of this renewable pressure energy. In this study, in order to acquire basic design data of tubular type hydroturbine, output power, head, and efficiency characteristics due to the guide vane opening angle are examined in detail. Moreover, influences of pressure, tangential and axial velocity distributions on turbine performance are investigated by using a commercial CFD code.

Simulation of Material Flow Through a Sample Divider

Directory of Open Access Journals (Sweden)

Jiří Rozbroj

2018-03-01

Full Text Available The prerequisite for a modern approach to innovative procedures of the development of current or even newly created equipment for the transport of particulate materials is the utilization of simulation methods, such as the Discrete Element Method (DEM. This article focuses on the basic, or initial, validation of movement of material through the sample divider. The mechanical-physical properties of brown coal were measured. Based on these parameters the preliminary input values for EDEM Academic were selected, and a simulation of the dividing process was run. The key monitored parameters included density and friction coefficient. Experiments on a realistic model of the equipment were performed and assessed. The total weights of brown coal at the exit from the divider were determined for a specific speed of the divider. The aim of this task was to simulate the realistically determined weight division of the brown coal sample. The result from the DEM was compared with the results of measurement on a realistic model.

Exergy Analysis of the Revolving Vane Compressed Air Engine

Directory of Open Access Journals (Sweden)

Alison Subiantoro

2016-01-01

Full Text Available Exergy analysis was applied to a revolving vane compressed air engine. The engine had a swept volume of 30 cm3. At the benchmark conditions, the suction pressure was 8 bar, the discharge pressure was 1 bar, and the operating speed was 3,000 rev·min−1. It was found that the engine had a second-law efficiency of 29.6% at the benchmark conditions. The contributors of exergy loss were friction (49%, throttling (38%, heat transfer (12%, and fluid mixing (1%. A parametric study was also conducted. The parameters to be examined were suction reservoir pressure (4 to 12 bar, operating speed (2,400 to 3,600 rev·min−1, and rotational cylinder inertia (0.94 to 2.81 g·mm2. The study found that a higher suction reservoir pressure initially increased the second-law efficiency but then plateaued at about 30%. With a higher operating speed and a higher cylinder inertia, second-law efficiency decreased. As compared to suction pressure and operating speed, cylinder inertia is the most practical and significant to be modified.

Determination of sampling constants in NBS geochemical standard reference materials

International Nuclear Information System (INIS)

Filby, R.H.; Bragg, A.E.; Grimm, C.A.

1986-01-01

Recently Filby et al. showed that, for several elements, National Bureau of Standards (NBS) Fly Ash standard reference material (SRM) 1633a was a suitable reference material for microanalysis (sample weights 2 , and the mean sample weight, W vector, K/sub s/ = (S/sub s/%) 2 W vector, could not be determined from these data because it was not possible to quantitate other sources of error in the experimental variances. K/sub s/ values for certified elements in geochemical SRMs provide important homogeneity information for microanalysis. For mineralogically homogeneous SRMs (i.e., small K/sub s/ values for associated elements) such as the proposed clays, it is necessary to determine K/sub s/ by analysis of very small sample aliquots to maximize the subsampling variance relative to other sources of error. This source of error and the blank correction for the sample container can be eliminated by determining K/sub s/ from radionuclide activities of weighed subsamples of a preirradiated SRM

Standard practice for sampling special nuclear materials in multi-container lots

CERN Document Server

American Society for Testing and Materials. Philadelphia

1987-01-01

1.1 This practice provides an aid in designing a sampling and analysis plan for the purpose of minimizing random error in the measurement of the amount of nuclear material in a lot consisting of several containers. The problem addressed is the selection of the number of containers to be sampled, the number of samples to be taken from each sampled container, and the number of aliquot analyses to be performed on each sample. 1.2 This practice provides examples for application as well as the necessary development for understanding the statistics involved. The uniqueness of most situations does not allow presentation of step-by-step procedures for designing sampling plans. It is recommended that a statistician experienced in materials sampling be consulted when developing such plans. 1.3 The values stated in SI units are to be regarded as the standard. 1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standar...

[Sampling in quality control of medicinal materials-A case of Epimedium].

Science.gov (United States)

Wang, Chuanyi; Cao, Jinyi; Liang, Yun; Huang, Wenhua; Guo, Baolin

2009-04-01

To investigate the effect of the different individual number of sampling on the assay results of the medicinal materials. Epimedium pubescens and E. brevicornu were used as samples. The 6 sampling levels were formulated as 1 individual, 5, 10, 20, 30, 50 individuals mix, each level with 3 parallels and 1 individual level5 parallels. The contents of epimedin C and icariin, and the peak areas of epimedin A, epimedin B, rhamnosyl icarisid II and icarisid II in all samples were analyzed by HPLC. The variation degree varied with species and chemical constituents, but the RSD and the deviation from the true value decreased with the increase of individual number on the same chemical constituent. The sampling number should be more than 10 individuals in quality control of Epimedium, and 50 or more individuals would be better for representing the quality of medicinal materials.

Achieving more efficient operation of the nozzle vane and rotor blade rows of gas turbines through using nonaxisymmetric end wall surfaces of interblade channels

Science.gov (United States)

Inozemtsev, A. A.; Samokhvalov, N. Yu.; Tikhonov, A. S.

2012-09-01

Results from a numerical study of three versions of the end-wall generatrix of the interblade channel used in the second-stage nozzle vanes of a prospective engine's turbine are presented. Recommendations for designing nonaxisymmetric end-wall surfaces are suggested based on the obtained data.

Planning for the Collection and Analysis of Samples of Martian Granular Materials Potentially to be Returned by Mars Sample Return

Science.gov (United States)

Carrier, B. L.; Beaty, D. W.

2017-12-01

NASA's Mars 2020 rover is scheduled to land on Mars in 2021 and will be equipped with a sampling system capable of collecting rock cores, as well as a specialized drill bit for collecting unconsolidated granular material. A key mission objective is to collect a set of samples that have enough scientific merit to justify returning to Earth. In the case of granular materials, we would like to catalyze community discussion on what we would do with these samples if they arrived in our laboratories, as input to decision-making related to sampling the regolith. Numerous scientific objectives have been identified which could be achieved or significantly advanced via the analysis of martian rocks, "regolith," and gas samples. The term "regolith" has more than one definition, including one that is general and one that is much more specific. For the purpose of this analysis we use the term "granular materials" to encompass the most general meaning and restrict "regolith" to a subset of that. Our working taxonomy includes the following: 1) globally sourced airfall dust (dust); 2) saltation-sized particles (sand); 3) locally sourced decomposed rock (regolith); 4) crater ejecta (ejecta); and, 5) other. Analysis of martian granular materials could serve to advance our understanding areas including habitability and astrobiology, surface-atmosphere interactions, chemistry, mineralogy, geology and environmental processes. Results of these analyses would also provide input into planning for future human exploration of Mars, elucidating possible health and mechanical hazards caused by the martian surface material, as well as providing valuable information regarding available resources for ISRU and civil engineering purposes. Results would also be relevant to matters of planetary protection and ground-truthing orbital observations. We will present a preliminary analysis of the following, in order to generate community discussion and feedback on all issues relating to: What are the

Characterization of Decommissioned PWR Vessel Internals Materials Samples: Material Certification, Fluence, and Temperature (Nonproprietary Version)

International Nuclear Information System (INIS)

Krug, M.; Shogan, R.; Fero, A.; Snyder, M.

2004-01-01

Pressurized water reactor (PWR) cores, operate under extreme environmental conditions due to coolant chemistry, operating temperature, and neutron exposure. Extending the life of PWRs require detailed knowledge of the changes in mechanical and corrosion properties of the structural austenitic stainless steel components adjacent to the fuel. This report contains basic material characterization information of the as-installed samples of reactor internals material which were harvested from a decommissioned PWR

Screening of IAEA environmental samples for fissile material content

International Nuclear Information System (INIS)

Hembree, Doyle M. Jr.; Carter, Joel A.; Devault, Gerald L.; Whitaker, J. Michael; Glasgow, David

2001-01-01

Full text: Analysis of environmental samples for the International Atomic Energy Agency (IAEA) Strengthened Safeguards Systems program requires that stringent measures be taken to control contamination. To facilitate contamination control, it is extremely useful to have some estimate of the fissile content of a given sample prior to beginning sample preparation and analysis. This is particularly true for laboratories that employ clean rooms during sample preparation. A review of the analytical results for samples submitted between January 1, 1999 and September 1, 2000 revealed that the total uranium content values ranged from 0.2 to greater than 500,000 ng/sample. Poor estimates of the uranium or plutonium content in the samples have caused some of the laboratories in the IAEA Network of Analytical Laboratories (NWAL) to experience clean laboratory contamination, sample cross contamination, and non-ideal uranium spike additions. This has led to significant increases in analysis costs (e.g., recertification of clean rooms after removing contamination, and rerunning samples) and degradation in data quality. A number of methods have been proposed for screening environmental samples for fissile material content, including gamma spectrometry, x-ray fluorescence, kinetic phosphorimetry (KPA), and inductively coupled plasma-mass spectrometry (ICP-MS). Gamma spectrometry and x-ray fluorescence are suitable for screening samples with microgram or greater quantities of uranium. ICP-MS and KPA are used successfully in some DOE NWAL laboratories to screen environmental samples. A neutron activation analysis (NAA) method that offers numerous advantages over other screening techniques for environmental samples has recently been proposed. Fissile materials such as 239 Pu and 235 U can be made to undergo fission in the intense neutron field to which they are exposed during neutron activation analysis (NAA). Some of the fission products emit neutrons referred to as 'delayed

The experimental study on the wind turbine’s guide-vanes and diffuser of an exhaust air energy recovery system integrated with the cooling tower

International Nuclear Information System (INIS)

Chong, W.T.; Hew, W.P.; Yip, S.Y.; Fazlizan, A.; Poh, S.C.; Tan, C.J.; Ong, H.C.

2014-01-01

Highlights: • On-site exhaust air energy recovery turbine generator mounted above cooling tower. • Energy from wasted wind resources is re-used for electricity generation. • Optimum angle arrangement of guide-vanes and diffusers help to improve wind-flow. • Enclosure solves conventional wind turbine problems. • 13.3% reduction in CO 2 emission is expected to be achieved from this system. - Abstract: An assembly of two vertical axis wind turbines (VAWTs) and an enclosure is installed above a cooling tower to harness the discharged wind for electricity generation. The enclosure consists of guide-vanes and diffuser-plates, is used to enhance the rotational speed of the turbines for power augmentation. The angle of the guide-vanes is optimized to ensure the oncoming wind stream impinges the rotor blades of the turbine at an optimum angle. The diffuser-plates are tilted at an optimum angle to increase the discharged airflow rate. The performance of the system is tested in the laboratory followed by a field test on an actual size cooling tower. The VAWT performance is increased in the range of 7–8% with the integration of enclosure. There is no significant difference in the current consumption of the fan motor between the bare cooling tower and the one with installed VAWTs. With the presence of this system, approximately 17.5 GW h/year is expected to be recovered from 3000 units of cooling towers at commercial areas, assuming the cooling tower is driven by a 7.5 kW fan motor and operates 16 h/day. This amount of recovered energy can also be translated into 13% reduction in CO 2 emission

Materials and Methods for Streamlined Laboratory Analysis of Environmental Samples, FY 2016 Report

Energy Technology Data Exchange (ETDEWEB)

Addleman, Raymond S. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Naes, Benjamin E. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); McNamara, Bruce K. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Olsen, Khris B. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Chouyyok, Wilaiwan [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Willingham, David G. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Spigner, Angel C. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

2016-11-30

The International Atomic Energy Agency (IAEA) relies upon laboratory analysis of environmental samples (typically referred to as “swipes”) collected during on-site inspections of safeguarded facilities to support the detection and deterrence of undeclared activities. Unfortunately, chemical processing and assay of the samples is slow and expensive. A rapid, effective, and simple extraction process and analysis method is needed to provide certified results with improved timeliness at reduced costs (principally in the form of reduced labor), while maintaining or improving sensitivity and efficacy. To address these safeguard needs the Pacific Northwest National Laboratory (PNNL) explored and demonstrated improved methods for environmental sample (ES) analysis. Improvements for both bulk and particle analysis were explored. To facilitate continuity and adoption, the new sampling materials and processing methods will be compatible with existing IAEA protocols for ES analysis. PNNL collaborated with Oak Ridge National Laboratory (ORNL), which performed independent validation of the new bulk analysis methods and compared performance to traditional IAEA’s Network of Analytical Laboratories (NWAL) protocol. ORNL efforts are reported separately. This report describes PNNL’s FY 2016 progress, which was focused on analytical application supporting environmental monitoring of uranium enrichment plants and nuclear fuel processing. In the future the technology could be applied to other safeguard applications and analytes related to fuel manufacturing, reprocessing, etc. PNNL’s FY 2016 efforts were broken into two tasks and a summary of progress, accomplishments and highlights are provided below. Principal progress and accomplishments on Task 1, Optimize Materials and Methods for ICP-MS Environmental Sample Analysis, are listed below. • Completed initial procedure for rapid uranium extraction from ES swipes based upon carbonate-peroxide chemistry (delivered to ORNL for

The NTF Inlet Guide Vanes Thermal Gradient Problem and Its Mitigation

Science.gov (United States)

Venkat, Venki S.; Paryz, Roman W.; Bissett, Owen W.; Kilgore, W.

2013-01-01

The National Transonic Facility (NTF) utilizes Inlet Guide Vanes (IGV) to provide precise, quick response Mach number control for the tunnel. During cryogenic operations, the massive IGV structure can experience large thermal gradients, measured as "Delta T or (Delta)T", between the IGV ring and its support structure called the transfer case. If these temperature gradients are too large, the IGV structure can be stressed beyond its safety limit and cease operation. In recent years, (Delta)T readings exceeding the prescribed safety limits were observed frequently during cryogenic operations, particularly during model access. The tactical operation methods of the tunnel to minimize (Delta)T did not always succeed. One obvious option to remedy this condition is to warm up the IGV structure by disabling the main drive operation, but this "natural" warm up method can takes days in some cases, resulting in productivity loss. This paper documents the thermal gradient problem associated with the IGV structure during cryogenic operation and how the facility has recently achieved an acceptable mitigation which has resulted in improved efficiency of operations.

Application of dynamic slip wall modeling to a turbine nozzle guide vane

Science.gov (United States)

Bose, Sanjeeb; Talnikar, Chaitanya; Blonigan, Patrick; Wang, Qiqi

2015-11-01

Resolution of near-wall turbulent structures is computational prohibitive necessitating the need for wall-modeled large-eddy simulation approaches. Standard wall models are often based on assumptions of equilibrium boundary layers, which do not necessarily account for the dissimilarity of the momentum and thermal boundary layers. We investigate the use of the dynamic slip wall boundary condition (Bose and Moin, 2014) for the prediction of surface heat transfer on a turbine nozzle guide vane (Arts and de Rouvroit, 1992). The heat transfer coefficient is well predicted by the slip wall model, including capturing the transition to turbulence. The sensitivity of the heat transfer coefficient to the incident turbulence intensity will additionally be discussed. Lastly, the behavior of the thermal and momentum slip lengths will be contrasted between regions where the strong Reynolds analogy is invalid (near transition on the suction side) and an isothermal, zero pressure gradient flat plate boundary layer (Wu and Moin, 2010).

Characterization of full set material constants of piezoelectric materials based on ultrasonic method and inverse impedance spectroscopy using only one sample.

Science.gov (United States)

Li, Shiyang; Zheng, Limei; Jiang, Wenhua; Sahul, Raffi; Gopalan, Venkatraman; Cao, Wenwu

2013-09-14

The most difficult task in the characterization of complete set material properties for piezoelectric materials is self-consistency. Because there are many independent elastic, dielectric, and piezoelectric constants, several samples are needed to obtain the full set constants. Property variation from sample to sample often makes the obtained data set lack of self-consistency. Here, we present a method, based on pulse-echo ultrasound and inverse impedance spectroscopy, to precisely determine the full set physical properties of piezoelectric materials using only one small sample, which eliminated the sample to sample variation problem to guarantee self-consistency. The method has been applied to characterize the [001] C poled Mn modified 0.27Pb(In 1/2 Nb 1/2 )O 3 -0.46Pb(Mg 1/3 Nb 2/3 )O 3 -0.27PbTiO 3 single crystal and the validity of the measured data is confirmed by a previously established method. For the inverse calculations using impedance spectrum, the stability of reconstructed results is analyzed by fluctuation analysis of input data. In contrast to conventional regression methods, our method here takes the full advantage of both ultrasonic and inverse impedance spectroscopy methods to extract all constants from only one small sample. The method provides a powerful tool for assisting novel piezoelectric materials of small size and for generating needed input data sets for device designs using finite element simulations.

Simulated Irradiation of Samples in HFIR for use as Possible Test Materials in the MPEX (Material Plasma Exposure Experiment) Facility

Energy Technology Data Exchange (ETDEWEB)

Ellis, Ronald James [ORNL; Rapp, Juergen [ORNL

2014-01-01

The importance of Plasma Material Interaction (PMI) is a major concern in fusion reactor design and analysis. The Material-Plasma Exposure eXperiment (MPEX) facility will explore PMI under fusion reactor plasma conditions. Samples with accumulated displacements per atom (DPA) damage produced by irradiations in the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory (ORNL) will be studied in the MPEX facility. The project presented in this paper involved performing assessments of the induced radioactivity and resulting radiation fields of a variety of potential fusion reactor materials. The scientific code packages MCNP and SCALE were used to simulate irradiation of the samples in HFIR; generation and depletion of nuclides in the material and the subsequent composition, activity levels, gamma radiation fields, and resultant dose rates as a function of cooling time. These state-of-the-art simulation methods were used in addressing the challenge of the MPEX project to minimize the radioactive inventory in the preparation of the samples for inclusion in the MPEX facility.

Positioning and tail rotor of a small horizontal axis wind turbine of due to the influence of drag coefficient and lift affecting vane cola

International Nuclear Information System (INIS)

Farinnas Wong, E. Y.; Jauregui Rigo, S.; Betancourt Mena, J.

2009-01-01

In the present investigation was carried out an assessment on the state of technology on guidance systems and tail protection when used in small horizontal axis wind turbines, work was improved methodological approach for the development of guidance systems queue by time of these machines, to incorporate the use of coefficients of lift and drag behavior varies according to the aspect ratio, using the principles of continuum mechanics and CFD methods. Two versions are analyzed , original and updated, the wind turbine CEET-01, on which the author would have been granted a Certificate of Patent of Invention and one of Industrial Model, the updated version was derived from the procedure proposed by the author, this presents a holder for the longest vane and a larger area in the vane. In addition to analyzing the amount and cost of power generated and the capacity factor at three locations in the province of Villa Clara it was concluded that the updated variant of the turbine CEET-01 is superior to the original

An interactive physics-based unmanned ground vehicle simulator leveraging open source gaming technology: progress in the development and application of the virtual autonomous navigation environment (VANE) desktop

Science.gov (United States)

Rohde, Mitchell M.; Crawford, Justin; Toschlog, Matthew; Iagnemma, Karl D.; Kewlani, Guarav; Cummins, Christopher L.; Jones, Randolph A.; Horner, David A.

2009-05-01

It is widely recognized that simulation is pivotal to vehicle development, whether manned or unmanned. There are few dedicated choices, however, for those wishing to perform realistic, end-to-end simulations of unmanned ground vehicles (UGVs). The Virtual Autonomous Navigation Environment (VANE), under development by US Army Engineer Research and Development Center (ERDC), provides such capabilities but utilizes a High Performance Computing (HPC) Computational Testbed (CTB) and is not intended for on-line, real-time performance. A product of the VANE HPC research is a real-time desktop simulation application under development by the authors that provides a portal into the HPC environment as well as interaction with wider-scope semi-automated force simulations (e.g. OneSAF). This VANE desktop application, dubbed the Autonomous Navigation Virtual Environment Laboratory (ANVEL), enables analysis and testing of autonomous vehicle dynamics and terrain/obstacle interaction in real-time with the capability to interact within the HPC constructive geo-environmental CTB for high fidelity sensor evaluations. ANVEL leverages rigorous physics-based vehicle and vehicle-terrain interaction models in conjunction with high-quality, multimedia visualization techniques to form an intuitive, accurate engineering tool. The system provides an adaptable and customizable simulation platform that allows developers a controlled, repeatable testbed for advanced simulations. ANVEL leverages several key technologies not common to traditional engineering simulators, including techniques from the commercial video-game industry. These enable ANVEL to run on inexpensive commercial, off-the-shelf (COTS) hardware. In this paper, the authors describe key aspects of ANVEL and its development, as well as several initial applications of the system.

Wind-tunnel calibration of a combined pitot-static tube and vane-type flow-angularity indicator at Mach numbers of 1.61 and 2.01

Science.gov (United States)

Sinclair, Archibald R; Mace, William D

1956-01-01

A limited calibration of a combined pitot-static tube and vane-type flow-angularity indicator has been made in the Langley 4- by 4-foot supersonic pressure tunnel at Mach numbers of 1.61 and 2.01. The results indicated that the angle-of-yaw indications were affected by unsymmetric shock effects at low angles of attack.

Studi Eksperimen Aliran Melalui Square Duct dan Square Elbow 90º dengan Double Guide Vane pada Variasi Sudut Bukaan Damper

Directory of Open Access Journals (Sweden)

Andrew Jaya Nazar

2017-01-01

Full Text Available Instalasi saluran udara tidak hanya berupa pipa lurus, tetapi juga terdapat fitting/aksesoris perpipaan misalnya elbow 90o dan damper. Aksesoris perpipaan ini berfungsi agar saluran udara dapat terpasang sesuai dengan kebutuhan. Namun, penggunaan aksesoris perpipaan ini menyebabkan bertambahnya pressure drop akibat adanya friction loss dan separation loss. Pemasangan guide vane pada elbow 90o diharapkan dapat mengurangi pressure drop karena dapat mengurangi terjadinya secondary flow, namun hal ini dapat menambah kerugian akibat gaya gesek. Saat ini penghematan energi menjadi sorotan terutama dalam dunia industri. Penurunan pressure drop pada belokan perpipaan sangat diharapkan, agar dapat menghemat energi lebih. Untuk itu perlu dilakukan usaha agar dapat menurunkan pressure drop yang terjadi. Penelitian ini dilakukan secara eksperimen dengan benda uji saluran udara yang terdiri dari: upstream duct (straight duct, square elbow 90o dengan r/Dh=1,5 dan dilengkapi double guide vane, damper, downstream duct (straight duct, dan induced fan. Pengukuran parameter yang dibutuhkan dilakukan dengan menggunakan: pitot tube, inclined manometer, pressure tranducer. Dari eksperimen ini diperoleh bahwa profil kecepatan pada masing-masing variasi sudut bukaan damper sudah mendekati keadaan recovery aliran pada akhir section baik dari bidang vertikal maupun horizontal. Pressure drop yang terjadi semakin naik seiring dengan bertambahnya nilai bilangan Reynolds dan sudut bukaan damper. Nilai konstanta damper semakin naik dari bukaan sudut 0o hingga 30o.

Numerical Study of the Effects of Thermal Barrier Coating and Turbulence Intensity on Cooling Performances of a Nozzle Guide Vane

Directory of Open Access Journals (Sweden)

Prasert Prapamonthon

2017-03-01

Full Text Available This work presents a numerical investigation of the combined effects of thermal barrier coating (TBC with mainstream turbulence intensity (Tu on a modified vane of the real film-cooled nozzle guide vane (NGV reported by Timko (NASA CR-168289. Using a 3D conjugate heat transfer (CHT analysis, the NGVs with and without TBC are simulated at three Tus (Tu = 3.3%, 10% and 20%. The overall cooling effectiveness, TBC effectiveness and heat transfer coefficient are analyzed and discussed. The results indicate the following three interesting phenomena: (1 TBC on the pressure side (PS is more effective than that on the suction side (SS due to a fewer number of film holes on the SS; (2 for all three Tus, the variation trends of the overall cooling effectiveness are similar, and TBC plays the positive and negative roles in heat flux at the same time, and significantly increases the overall cooling effectiveness in regions cooled ineffectively by cooling air; (3 when Tu increases, the TBC effect is more significant, for example, at the highest Tu (Tu = 20% the overall cooling effectiveness can increase as much as 24% in the film cooling ineffective regions, but near the trailing edge (TE and the exits and downstream of film holes on the SS, this phenomenon is slight.

A comparison of results for samples collected with bailers constructed of different materials

International Nuclear Information System (INIS)

Thomey, N.; Ogle, R.; Jackson, J.

1992-01-01

A bailer is one of the most common sampling devices used to collect ground water samples. Bailers constructed from various materials are available; teflon, polyvinyl chloride (PVC), polyethylene, and stainless steel are all commonly used. It is widely recognized that sample results can be affected by the material from which the bailer is constructed. Teflon and stainless steel are usually recommended based upon their inert properties. The cost of these bailers is significantly higher than other types. For the purposes of petroleum storage tank investigations, sampling devices that would not compromise sample quality but be more economical than teflon or stainless steel would be especially desirable. Water samples were collected using the different types of bailers; teflon, stainless steel, PVC, and polyethylene. Split samples were analyzed for benzene, toluene, ethylbenzene, total xylenes, and Total Petroleum Hydrocarbons. The analytical results were compared to determine if differences were due to normal analytical variances or due to interaction of the sample with the sampling device. No difference was noted in the results which were obtained

Measurement of radon exhalation rate in various building materials and soil samples

Science.gov (United States)

Bala, Pankaj; Kumar, Vinod; Mehra, Rohit

2017-03-01

Indoor radon is considered as one of the potential dangerous radioactive elements. Common building materials and soil are the major source of this radon gas in the indoor environment. In the present study, the measurement of radon exhalation rate in the soil and building material samples of Una and Hamirpur districts of Himachal Pradesh has been done with solid state alpha track detectors, LR-115 type-II plastic track detectors. The radon exhalation rate for the soil samples varies from 39.1 to 91.2 mBq kg-1 h-1 with a mean value 59.7 mBq kg-1 h-1. Also the radium concentration of the studied area is found and it varies from 30.6 to 51.9 Bq kg-1 with a mean value 41.6 Bq kg-1. The exhalation rate for the building material samples varies from 40.72 (sandstone) to 81.40 mBq kg-1 h-1 (granite) with a mean value of 59.94 mBq kg-1 h-1.

Experimental measurements and analytical analysis related to gas turbine heat transfer. Part 1: Time-averaged heat-flux and surface-pressure measurements on the vanes and blades of the SSME fuel-side turbine and comparison with prediction. Part 2: Phase-resolved surface-pressure and heat-flux measurements on the first blade of the SSME fuel-side turbine

Science.gov (United States)

1994-01-01

Time averaged Stanton number and surface-pressure distributions are reported for the first-stage vane row, the first stage blade row, and the second stage vane row of the Rocketdyne Space Shuttle Main Engine two-stage fuel-side turbine. Unsteady pressure envelope measurements for the first blade are also reported. These measurements were made at 10 percent, 50 percent, and 90 percent span on both the pressure and suction surfaces of the first stage components. Additional Stanton number measurements were made on the first stage blade platform blade tip, and shroud, and at 50 percent span on the second vane. A shock tube was used as a short duration source of heated and pressurized air to which the turbine was subjected. Platinum thin-film heat flux gages were used to obtain the heat flux measurements, while miniature silicon-diaphragm flush-mounted pressure transducers were used to obtain the pressure measurements. The first stage vane Stanton number distributions are compared with predictions obtained using a version of STAN5 and a quasi-3D Navier-Stokes solution. This same quasi-3D N-S code was also used to obtain predictions for the first blade and the second vane.

Hydrogen determination using secondary processes of recoil proton interaction with sample material

International Nuclear Information System (INIS)

Muminov, V.A.; Khajdarov, R.A.; Navalikhin, L.V.; Pardaev, Eh.

1980-01-01

Possibilities of hydrogen content determination in different materials according to secondary processes of interaction of recoil protons(irradiation in the field of fast neutrons) with sample material resulting in the appearance of characteristic X-ray irradiation are studied. Excitated irradiation is recorded with a detector placed in the protective screen and located at a certain distance from the object analyzed and neutron source. The method is tested taking as an example analysis of bromine-containing samples (30% Br, 0.5% H) and tungsten dioxide. The determination limit of hydrogen content constitutes 0.05% at confidence coefficient of 0.9. Neutron flux constituted 10 3 neutrons/cm 2 xs, the time of measurement being 15-20 minutes, the distance from the sample to the detector being 12-15 cm [ru

Rheological characteristics of waste rock materials in abandoned mine deposit and debris flow hazards

Science.gov (United States)

Jeong, Sueng-Won; Lee, Choonoh; Cho, Yong-Chan; Wu, Ying-Hsin

2015-04-01

In Korea, approximately 5,000 metal mines are spread, but 50% of them are still abandoned without any proper remediation and cleanup. Summer heavy rainfall can result in the physicochemical modification of waste rock materials in the mountainous. From the geotechnical monitoring and field investigation, there are visible traces of mass movements every year. Soil erosion is one of severe phenomena in the study area. In particular, study area is located in the upper part of the Busan Metropolitan City and near the city's water supply. With respect to the supply of drinking water and maintenance of ecological balance, proper disposal of waste rock materials is required. For this reason, we examine the rheological properties of waste rock materials as a function of solid content using a ball- and vane-penetrated rheometer. In the flow curves, which are the relationship between the shear stress and shear rate of waste rock materials, we found that the soil samples exhibited a shear thinning beahivor regardless of solid content. The Bingham, Herschel-Bulkley, Power-law, and Papanastasiou models are used to determine the rheological properties. Assuming that the soil samples behaved as the viscoplastic behavior, the yield stress and viscosity are determined for different water contents. As a result, there are clear relationships between the solid content and rheological values (i.e., Bingham yield stress and plastic viscosity). From these relationships, the maximum and minimum of Bingham yield stresses are ranged from 100 to 2000 Pa. The debris flow mobilization is analysed using a 1D BING and 2D Debris flow models. In addition, the effect of wall slip and test apparatus are discussed.

ICP-MS applications for the analysis of geological materials and environmental samples

International Nuclear Information System (INIS)

Bendl, J.

1997-01-01

This work deals with applications of inductively coupled plasma - mass spectrometry applications for the analysis of geological materials and environmental samples. There are instrumentation, calibration, alternatives of sample introduction, interferences, trace elements analysis, rare earth elements and uranium and thorium, precious metals, isotopic analysis and environmental analysis discussed

Combustion-driven oscillation in a furnace with multispud-type gas burners. 4th Report. Effects of position of secondary air guide sleeve and openness of secondary air guide vane on combustion oscillation condition; Multispud gata gas turner ni okeru nensho shindo. 4. Nijigen kuki sleeve ichi oyobi nijigen kuki vane kaido no shindo reiki ni oyobosu eikyo

Energy Technology Data Exchange (ETDEWEB)

Akiyama, I.; Okiura, K.; Baba, A.; Orimoto, M. [Babcock-Hitachi K.K., Tokyo (Japan)

1994-07-25

Effects of the position of a secondary air guide sleeve and the openness of a secondary air guide vane on combustion oscillation conditions were studied experimentally for multispud-type gas burners. Pressure fluctuation in furnaces was analyzed with the previously reported resonance factor which was proposed as an index to represent the degree of combustion oscillation. As a result, the combustion oscillation region was largely affected by both position of a guide sleeve and openness of a guide vane. As the openness having large effect on the ratio of primary and secondary air/tertiary air and the position hardly having effect on the ratio were adjusted skillfully, the burner with no combustion oscillation region was achieved in its normal operation range. In addition, as the effect of preheating combustion air was arranged with a standard flow rate or mass flow flux of air, it was suggested the combustion oscillation region due to preheating can be described with the same manner as that due to no preheating. 5 refs., 8 figs.

Nuclear reactor fuel element assemblies

International Nuclear Information System (INIS)

Krawiec, D.M.; Bevilacqua, F.

1974-01-01

The fuel elements of each fuel element group are separated from each other by means of a multitude of thin, intersecting plates in the from of grid strips. Flow deflectors near the surface of the fuel elements are used in order to make the coolant flow more turbulent. They are designed as vanes and arranged at a distance on the grid strips. Each deflector vane has two arms stretching in opposite directions, each one into a neighbouring channel. In outward direction, the deflector vanes are converging. The strips with the vanes can be put on the supporting grid of the fuel elements. The vane structure can be reinforced by providing distortions in the strip material near the vanes. (DG) [de

DESIGN AND CALIBRATION OF A VIBRANT SAMPLE MAGNETOMETER: CHARACTERIZATION OF MAGNETIC MATERIALS

Directory of Open Access Journals (Sweden)

Freddy P. Guachun

2018-01-01

Full Text Available This paper presents the process followed in the implementation of a vibrating sample magnetometer (VSM, constructed with materials commonly found in an electromagnetism laboratory. It describes the design, construction, calibration and use in the characterization of some magnetic materials. A VSM measures the magnetic moment of a sample when it is vibrated perpendicular to a uniform magnetic field; Magnetization and magnetic susceptibility can be determined from these readings. This instrument stands out for its simplicity, versatility and low cost, but it is very sensitive and capable of eliminating or minimizing many sources of error that are found in other methods of measurement, allowing to obtain very accurate and reliable results. Its operation is based on the law of magnetic induction of Lenz-Faraday that consists in measuring the induced voltage in coils of detection produced by the variation of the magnetic flux that crosses them. The calibration of the VSM was performed by means of a standard sample (Magnetite and verified by means of a test sample (Nickel.

Tank 12H Acidic Chemical Cleaning Sample Analysis And Material Balance

International Nuclear Information System (INIS)

Martino, C. J.; Reboul, S. H.; Wiersma, B. J.; Coleman, C. J.

2013-01-01

A process of Bulk Oxalic Acid (BOA) chemical cleaning was performed for Tank 12H during June and July of 2013 to remove all or a portion of the approximately 4400 gallon sludge heel. Three strikes of oxalic acid (nominally 4 wt % or 2 wt %) were used at 55 deg C and tank volumes of 96- to 140-thousand gallons. This report details the sample analysis of a scrape sample taken prior to BOA cleaning and dip samples taken during BOA cleaning. It also documents a rudimentary material balance for the Tank 12H cleaning results

Lateral Flow Field Behavior Downstream of Mixing Vanes In a Simulated Nuclear Fuel Rod Bundle

International Nuclear Information System (INIS)

Conner, Michael E.; Smith, L. David III; Holloway, Mary V.; Beasley, Donald E.

2004-01-01

To assess the fuel assembly performance of PWR nuclear fuel assemblies, average subchannel flow values are used in design analyses. However, for this highly complex flow, it is known that local conditions around fuel rods vary dependent upon the location of the fuel rod in the fuel assembly and upon the support grid design that maintains the fuel rod pitch. To investigate the local flow in a simulated nuclear fuel rod bundle, a testing technique has been employed to measure the lateral flow field in a 5 x 5 rod bundle. Particle Image Velocimetry was used to measure the lateral flow field downstream of a support grid with mixing vanes for four unique subchannels in the 5 x 5 bundle. The dominant lateral flow structures for each subchannel are compared in this paper including the decay of these flow structures. (authors)

Evaluation of Botanical Reference Materials for the Determination of Vanadium in Biological Samples

DEFF Research Database (Denmark)

Heydorn, Kaj; Damsgaard, Else

1982-01-01

Three botanical reference materials prepared by the National Bureau of Standards have been studied by neutron activation analysis to evaluate their suitability with respect to the determination of vanadium in biological samples. Various decomposition methods were applied in connection with chemic....... A reference value of 1.15 mg/kg of this material is recommended, based on results from 3 different methods. All three materials are preferable to SRM 1571 Orchard Leaves, while Bowen's Kale remains the material of choice because of its lower concentration....

Active Flow Control in a Radial Vaned Diffuser for Surge Margin Improvement: A Multislot Suction Strategy

Directory of Open Access Journals (Sweden)

Aurélien Marsan

2017-01-01

Full Text Available This work is the final step of a research project that aims at evaluating the possibility of delaying the surge of a centrifugal compressor stage using a boundary-layer suction technique. It is based on Reynolds-Averaged Navier-Stokes numerical simulations. Boundary-layer suction is applied within the radial vaned diffuser. Previous work has shown the necessity to take into account the unsteady behavior of the flow when designing the active flow control technique. In this paper, a multislot strategy is designed according to the characteristics of the unsteady pressure field. Its implementation results in a significant increase of the stable operating range predicted by the unsteady RANS numerical model. A hub-corner separation still exists further downstream in the diffuser passage but does not compromise the stability of the compressor stage.

Numerical Study of Compact Plate-Fin Heat Exchanger for Rotary-Vane Gas Refrigeration Machine

Directory of Open Access Journals (Sweden)

V. V. Trandafilov

2017-10-01

Full Text Available Plate-fin heat exchangers are widely used in refrigeration technique. They are popular because of their compactness and excellent heat transfer performance. Here we present a numerical model for the development, research and optimization of a plate-fin heat exchanger for a rotary-vane gas refrigeration machine. The method of analysis by graphic method of plate - fin heat exchanger is proposed. The model describes the effects of secondary parameters such as axial thermal conductivity through a metal matrix of the heat exchanger. The influence of geometric parameters and heat transfer coefficient is studied. Graphs of dependences of length, efficiency of a fin and pressure drop in a heat exchanger on the thickness of the fin and the number of fins per meter are obtained. To analyze the results of numerical simulation, the heat exchanger was designed in the Aspen HYSYS program. The simulation results show that the total deviation from the proposed numerical model is not more than 15%. 

Sample preparation techniques of biological material for isotope analysis

International Nuclear Information System (INIS)

Axmann, H.; Sebastianelli, A.; Arrillaga, J.L.

1990-01-01

Sample preparation is an essential step in all isotope-aided experiments but often it is not given enough attention. The methods of sample preparation are very important to obtain reliable and precise analytical data and for further interpretation of results. The size of a sample required for chemical analysis is usually very small (10mg-1500mg). On the other hand the amount of harvested plant material from plots in a field experiment is often bulky (several kilograms) and the entire sample is too large for processing. In addition, while approaching maturity many crops show not only differences in physical consistency but also a non-uniformity in 15 N content among plant parts, requiring a plant fractionation or separation into parts (vegetative and reproductive) e.g. shoots and spikes, in case of small grain cereals, shoots and pods in case of grain legumes and tops and roots or beets (including crown) in case of sugar beet, etc. In any case the ultimate goal of these procedures is to obtain representative subsample harvested from greenhouse or field experiments for chemical analysis. Before harvesting an isotopic-aided experiment the method of sampling has to be selected. It should be based on the type of information required in relation to the objectives of the research and the availability of resources (staff, sample preparation equipment, analytical facilities, chemicals and supplies, etc.). 10 refs, 3 figs, 3 tabs

Experimental technique to measure thoron generation rate of building material samples using RAD7 detector

International Nuclear Information System (INIS)

Csige, I.; Szabó, Zs.; Szabó, Cs.

2013-01-01

Thoron ( 220 Rn) is the second most abundant radon isotope in our living environment. In some dwellings it is present in significant amount which calls for its identification and remediation. Indoor thoron originates mainly from building materials. In this work we have developed and tested an experimental technique to measure thoron generation rate in building material samples using RAD7 radon-thoron detector. The mathematical model of the measurement technique provides the thoron concentration response of RAD7 as a function of the sample thickness. For experimental validation of the technique an adobe building material sample was selected for measuring the thoron concentration at nineteen different sample thicknesses. Fitting the parameters of the model to the measurement results, both the generation rate and the diffusion length of thoron was estimated. We have also determined the optimal sample thickness for estimating the thoron generation rate from a single measurement. -- Highlights: • RAD7 is used for the determination of thoron generation rate (emanation). • The described model takes into account the thoron decay and attenuation. • The model describes well the experimental results. • A single point measurement method is offered at a determined sample thickness

Extended residence time centrifugal contactor design modification and centrifugal contactor vane plate valving apparatus for extending mixing zone residence time

Science.gov (United States)

Wardle, Kent E.

2017-06-06

The present invention provides an annular centrifugal contactor, having a housing adapted to receive a plurality of flowing liquids; a rotor on the interior of the housing; an annular mixing zone, wherein the annular mixing zone has a plurality of fluid retention reservoirs with ingress apertures near the bottom of the annular mixing zone and egress apertures located above the ingress apertures of the annular mixing zone; and an adjustable vane plate stem, wherein the stem can be raised to restrict the flow of a liquid into the rotor or lowered to increase the flow of the liquid into the rotor.

Hydrogen, carbon and oxygen determination in proxy material samples using a LaBr3:Ce detector

International Nuclear Information System (INIS)

Naqvi, A.A.; Al-Matouq, Faris A.; Khiari, F.Z.; Isab, A.A.; Raashid, M.; Khateeb-ur-Rehman

2013-01-01

Hydrogen, carbon and oxygen concentrations were measured in caffeine, urea, ammonium acetate and melamine bulk samples via 14 MeV neutron inelastic scattering using a LaBr 3 :Ce detector. The samples tested herein represent drugs, explosives and benign materials, respectively. Despite its intrinsic activity, the LaBr 3 :Ce detector performed well in detecting the hydrogen, carbon and oxygen elements. Because 5.1 MeV nitrogen gamma rays interfere with silicon and calcium prompt gamma rays from the room background, the nitrogen peak was not detected in the samples. An excellent agreement was observed between the experimental and theoretical yields of 2.22, 4.43 and 6.13 MeV gamma rays from the analyzed samples as a function of H, C and O concentrations, respectively. Within statistical errors, the minimum detectable concentration (MDC) of hydrogen, carbon and oxygen elements in the tested materials were consistent with previously reported MDC values for these elements measured in hydrocarbon samples. - Highlights: • Hydrogen, carbon and oxygen concentration measurement in bulk samples using 14 MeV neutrons induced prompt gamma rays. • Prompt gamma analysis of narcotics and explosive proxy materials e.g. ammonium acetate, caffeine, urea and melamine Bulk samples. • Prompt gamma detection using large cylindrical 76×76 mm 2 (diameter x height ) LaBr 3 :Ce detector. • Carbon/oxygen elemental ratio measurement from explosive and narcotics proxy material samples

The effect of epoxidized soybean oil on mechanical and rheological properties of poly(butylene succinate)/lignin via vane extruder

Science.gov (United States)

Liu, Huanyu; Huang, Zhaoxia; Qu, Jinping; Meng, Cong

2016-03-01

Epoxidized Soybean Oil (ESO) have been used as the compatilizer in the Poly (butylene succinate)/lignin (PBS/lignin) composites. Compatibilized composites were fabricated by a novel vane extruder (VE) which can generate global and dynamic elongational flow. The effects of ESO on the mechanical, rheological properties and morphology of PBS/lignin were studied. The results indicated that the use of ESO had plasticizing effect on the matrix PBS while the addition reduced tensile strength. From SEM micrographs it could be clearly observed that there was a better interfacial adhesion between lignin and matrix. Meanwhile, rheological tests showed the incorporation of ESO improved its Newtonian behavior and can enhance PBS's flexibility.

New sorbent materials for selective extraction of cocaine and benzoylecgonine from human urine samples.

Science.gov (United States)

Bujak, Renata; Gadzała-Kopciuch, Renata; Nowaczyk, Alicja; Raczak-Gutknecht, Joanna; Kordalewska, Marta; Struck-Lewicka, Wiktoria; Waszczuk-Jankowska, Małgorzata; Tomczak, Ewa; Kaliszan, Michał; Buszewski, Bogusław; Markuszewski, Michał J

2016-02-20

An increase in cocaine consumption has been observed in Europe during the last decade. Benzoylecgonine, as a main urinary metabolite of cocaine in human, is so far the most reliable marker of cocaine consumption. Determination of cocaine and its metabolite in complex biological samples as urine or blood, requires efficient and selective sample pretreatment. In this preliminary study, the newly synthesized sorbent materials were proposed for selective extraction of cocaine and benzoylecgonine from urine samples. Application of these sorbent media allowed to determine cocaine and benzoylecgonine in urine samples at the concentration level of 100ng/ml with good recovery values as 81.7%±6.6 and 73.8%±4.2, respectively. The newly synthesized materials provided efficient, inexpensive and selective extraction of both cocaine and benzoylecgonine from urine samples, which can consequently lead to an increase of the sensitivity of the current available screening diagnostic tests. Copyright © 2015 Elsevier B.V. All rights reserved.

Analysis of plant gums and saccharide materials in paint samples: comparison of GC-MS analytical procedures and databases.

Science.gov (United States)

Lluveras-Tenorio, Anna; Mazurek, Joy; Restivo, Annalaura; Colombini, Maria Perla; Bonaduce, Ilaria

2012-10-10

Saccharide materials have been used for centuries as binding media, to paint, write and illuminate manuscripts and to apply metallic leaf decorations. Although the technical literature often reports on the use of plant gums as binders, actually several other saccharide materials can be encountered in paint samples, not only as major binders, but also as additives. In the literature, there are a variety of analytical procedures that utilize GC-MS to characterize saccharide materials in paint samples, however the chromatographic profiles are often extremely different and it is impossible to compare them and reliably identify the paint binder. This paper presents a comparison between two different analytical procedures based on GC-MS for the analysis of saccharide materials in works-of-art. The research presented here evaluates the influence of the analytical procedure used, and how it impacts the sugar profiles obtained from the analysis of paint samples that contain saccharide materials. The procedures have been developed, optimised and systematically used to characterise plant gums at the Getty Conservation Institute in Los Angeles, USA (GCI) and the Department of Chemistry and Industrial Chemistry of the University of Pisa, Italy (DCCI). The main steps of the analytical procedures and their optimisation are discussed. The results presented highlight that the two methods give comparable sugar profiles, whether the samples analysed are simple raw materials, pigmented and unpigmented paint replicas, or paint samples collected from hundreds of centuries old polychrome art objects. A common database of sugar profiles of reference materials commonly found in paint samples was thus compiled. The database presents data also from those materials that only contain a minor saccharide fraction. This database highlights how many sources of saccharides can be found in a paint sample, representing an important step forward in the problem of identifying polysaccharide binders in

Optimization of Sample Preparation processes of Bone Material for Raman Spectroscopy.

Science.gov (United States)

Chikhani, Madelen; Wuhrer, Richard; Green, Hayley

2018-03-30

Raman spectroscopy has recently been investigated for use in the calculation of postmortem interval from skeletal material. The fluorescence generated by samples, which affects the interpretation of Raman data, is a major limitation. This study compares the effectiveness of two sample preparation techniques, chemical bleaching and scraping, in the reduction of fluorescence from bone samples during testing with Raman spectroscopy. Visual assessment of Raman spectra obtained at 1064 nm excitation following the preparation protocols indicates an overall reduction in fluorescence. Results demonstrate that scraping is more effective at resolving fluorescence than chemical bleaching. The scraping of skeletonized remains prior to Raman analysis is a less destructive method and allows for the preservation of a bone sample in a state closest to its original form, which is beneficial in forensic investigations. It is recommended that bone scraping supersedes chemical bleaching as the preferred method for sample preparation prior to Raman spectroscopy. © 2018 American Academy of Forensic Sciences.

Fiscal 1993 achievement report. International Clean Energy Network Using Hydrogen Conversion (WE-NET) technology (Subtask 8 - Research and development of hydrogen combustion turbine - Development of ultrahigh-temperature materials); 1993 nendo seika hokokusho. Suiso riyo kokusai clean energy system gijutsu (WE-NET). (Subtask 8. Suiso nensho tabin no kaihatsu - Cho koon zairyo no kaihatsu no kaihatsu)

Energy Technology Data Exchange (ETDEWEB)

NONE

1994-03-01

Current technologies are surveyed and tasks to discharge are extracted relating to heat resistant alloys, intermetallic compounds, ceramic based composite materials, and carbon based composite materials, which are expected to be used for hydrogen combustion turbines. Concerning oxide dispersion strengthened alloys for cooled vanes, tasks to discharge are extracted, which relate to the designing, development, and selection of vane materials, bonding layer materials, and coating materials, and to thermal barrier coating techniques and machining techniques. Concerning porous fiber reinforced ceramic materials for ceramic shells, tasks involve the elucidation of corrosion behavior and manufacturing techniques. MoSi{sub 2}, which is a promising high-melting intermetallic compound, also presents some tasks to discharge for an increase in its high strength and high ductility in an ultrahigh-temperature steam/reducing atmosphere, and for improvement in manufacturing techniques. For the carbon/carbon composite material which is the sole material usable in the ultrahigh-temperature domain of 2,000 degrees C, an analysis and evaluation method taking its anisotropy into consideration needs to be developed, and an oxidation resistant coating has to be also developed. In addition to the designing and development of these materials, development is necessary of materials testing and evaluating techniques. (NEDO)

Numerical investigation on pressure fluctuations in centrifugal compressor with different inlet guide vanes pre-whirl angles

Science.gov (United States)

Wang, Y. C.; Shi, M.; Cao, S. L.; Li, Z. H.

2013-12-01

The pressure fluctuations in a centrifugal compressor with different inlet guide vanes (IGV) pre-whirl angles were investigated numerically, as well as the pre-stress model and static structural of blade. The natural frequency was evaluated by pre-stress model analysis. The results show that, the aero-dynamic pressure acting on blade surface is smaller than rotation pre-stress, which wouldn't result in large deformation of blade. The natural frequencies with rotation pre-stress are slightly higher than without rotation pre-stress. The leading mechanism of pressure fluctuations for normal conditions is the rotor-stator (IGVs) interaction, while is serious flow separations for conditions that are close to surge line. A few frequency components in spectra are close to natural frequency, which possibly result in resonant vibration if amplitude is large enough, which is dangerous for compressor working, and should be avoided.

Sample preparation of energy materials for X-ray nanotomography with micromanipulation.

Science.gov (United States)

Chen-Wiegart, Yu-chen Karen; Camino, Fernando E; Wang, Jun

2014-06-06

X-ray nanotomography presents an unprecedented opportunity to study energy storage/conversion materials at nanometer scales in three dimensions, with both elemental and chemical sensitivity. A critical step in obtaining high-quality X-ray nanotomography data is reliable sample preparation to ensure that the entire sample fits within the field of view of the X-ray microscope. Although focused-ion-beam lift-out has previously been used for large sample (few to tens of microns) preparation, a difficult undercut and lift-out procedure results in a time-consuming sample preparation process. Herein, we propose a much simpler and direct sample preparation method to resolve the issues that block the view of the sample base after milling and during the lift-out process. This method is applied on a solid-oxide fuel cell and a lithium-ion battery electrode, before numerous critical 3D morphological parameters are extracted, which are highly relevant to their electrochemical performance. A broad application of this method for microstructure study with X-ray nanotomography is discussed and presented. © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Tank waste remediation system (TWRS) privatization contractor samples waste envelope D material 241-C-106

Energy Technology Data Exchange (ETDEWEB)

Esch, R.A.

1997-04-14

This report represents the Final Analytical Report on Tank Waste Remediation System (TWRS) Privatization Contractor Samples for Waste Envelope D. All work was conducted in accordance with ''Addendum 1 of the Letter of Instruction (LOI) for TWRS Privatization Contractor Samples Addressing Waste Envelope D Materials - Revision 0, Revision 1, and Revision 2.'' (Jones 1996, Wiemers 1996a, Wiemers 1996b) Tank 241-C-1 06 (C-106) was selected by TWRS Privatization for the Part 1A Envelope D high-level waste demonstration. Twenty bottles of Tank C-106 material were collected by Westinghouse Hanford Company using a grab sampling technique and transferred to the 325 building for processing by the Pacific Northwest National Laboratory (PNNL). At the 325 building, the contents of the twenty bottles were combined into a single Initial Composite Material. This composite was subsampled for the laboratory-scale screening test and characterization testing, and the remainder was transferred to the 324 building for bench-scale preparation of the Privatization Contractor samples.

The Analysis for the Effect of Mixing Vane Shape on TDC

International Nuclear Information System (INIS)

Moon, Kang Hoon; Park, Ho Young; Kim, Kang Hoon; Park, Eung Jun; Suh, Jung Min

2011-01-01

The Thermal Diffusion Coefficient (TDC) is an input parameter to subchannel code, and it is required to predict local flow conditions in a PWR fuel bundle. TDC influences on the prediction of thermal interchange or mixing of thermal energy between the hot subchannel and interconnected adjacent subchannels. The thermal mixing term in the energy equation is generally represented in terms of a non-dimensional inverse Peclet number or TDC. The parameters associated with thermal mixing can be defined as Eq.(1): TDC =Pe x De/a (1) where: Pe : Inverse Peclet Number (dimensionless) = ε/ Va De : Equivalent hydraulic diameter, in. a : Lateral flow area between channels per unit length, in 2 /in ε : Mixing coefficient, in 2 /sec V : Velocity, in/sec TDC is an important factor to evaluate thermal performance. So, flow temperature maps were obtained from the 5x5 rod bundle test section to assess the thermal performance of corresponding fuels. The flow temperatures were measured by thermocouple at the end of heated length and the centroid of subchannel. There are two typical methods to arrange the hot and cold fuel rods as shown in Fig. 1. Configuration Fig. 1(b) is adopted in this work. This paper presents how to determine the TDC and verifies whether all TDC with the effect of mixing vane shape is valid with respect to current design value

Testing smooth and notched samples for identification of brittle material fracture mechanism

International Nuclear Information System (INIS)

Barinov, S.M.; Ivanov, V.S.

1987-01-01

Mechanical tests of cermet made of LaCrO 3 and Cr powder mixture in 3:2 mass ratio were conducted in LaCrO 3 -Cr system. Powder mixtures were exposed to static pressing and sintering (sintered cermets) or to high-speed pressing with following thermal treatment (high-speed pressing cermets). It is shown, that nonlinear deformation strength at deformation of brittle material smooth and notched samples allows to evaluate properly correlation of microplasticity and microcracking at brittle powder materials fracture

Fluorimetric determination of uranium in certain refractory minerals, environmental samples and industrial waste materials

International Nuclear Information System (INIS)

Premadas, A.; Saravanakumar, G.

2005-01-01

A simple sample decomposition and laser fluorimetric determination of uranium at trace level is reported in certain refractory minerals, like ilmenite, rutile, zircon and monazite; environmental samples viz. soil and sediments; industrial waste materials, such as, coal fly ash and red mud. Ilmenite sample is decomposed by heating with ammonium fluoride. Rutile, zircon and monazite minerals are decomposed by fusion using a mixture of potassium bifluoride and sodium fluoride. Environmental and industrial waste materials are brought into solution by treating with a mixture of hydrofluoric and nitric acids. The laser induced fluorimetric determination of uranium is carried out directly in rutile, zircon and in monazite minerals and after separation in other samples. The determination limit was 1 μg x g -1 for ilmenite, soil, sediment, coal fly ash and red mud samples, and it is 5 μg x g -1 for rutile, zircon and monazite. The method is also developed for the optical fluorimetric determination of uranium (determination limit 10 μg x g -1 ) in ilmenite, rutile, zircon and monazite minerals. The methods are simple, accurate, and precise and they require small quantity of sample and can be applied for the routine analysis. (author)

Conformity Assessment in Nuclear Material and Environmental Sample Analysis

International Nuclear Information System (INIS)

Aregbe, Y.; Jakopic, R.; Richter, S.; Venchiarutti, C.

2015-01-01

Safeguards conclusions are based to a large extent on comparison of measurement results between operator and safeguards laboratories. Measurement results must state traceability and uncertainties to be comparable. Recent workshops held at the IAEA and in the frame of the European Safeguards Research and Development Association (ESARDA), reviewed different approaches for Nuclear Material Balance Evaluation (MBE). Among those, the ''bottom-up'' approach requires assessment of operators and safeguards laboratories measurement systems and capabilities. Therefore, inter-laboratory comparisons (ILCs) with independent reference values provided for decades by JRC-IRMM, CEA/CETAMA and US DOE are instrumental to shed light on the current state of practice in measurements of nuclear material and environmental swipe samples. Participating laboratories are requested to report the measurement results with associated uncertainties, and have the possibility to benchmark those results against independent and traceable reference values. The measurement capability of both the IAEA Network of Analytical Laboratories (NWAL) and the nuclear operator's analytical services participating in ILCs can be assessed against the independent reference values as well as against internationally agreed quality goals, in compliance with ISO 13528:2005. The quality goals for nuclear material analysis are the relative combined standard uncertainties listed in the ITV2010. Concerning environmental swipe sample analysis, the IAEA defined measurement quality goals applied in conformity assessment. The paper reports examples from relevant inter-laboratory comparisons, looking at laboratory performance according to the purpose of the measurement and the possible use of the result in line with the IUPAC International Harmonized Protocol. Tendencies of laboratories to either overestimate and/or underestimate uncertainties are discussed using straightforward graphical tools to evaluate

Artificial radioactivity in the environmental samples as IAEA reference materials

International Nuclear Information System (INIS)

Salagean, M.; Pantelica, A.

1998-01-01

. Uncontaminated by nuclear activities: IAEA-327, Podsolic soil collected in 1990 from the Moscow region and considered uncontaminated by radionuclides of the Chernobyl accident or by other nuclear activities. The results obtained by our laboratory are in good agreement with the certified IAEA data. Generally, the concentration of the artificial radionuclides in the investigated samples is higher than that expected from the influence of global fallout in the intercomparison materials distributed before Chernobyl accident. Concerning the nature of these investigated IAEA reference materials, very high values for the concentration levels of cesium radionuclides especially in IAEA-373 (grass) and IAEA-375 (soil) samples collected in the vicinity of Chernobyl Power Station after the nuclear accident in 1986 were found. High levels of radioactivities for the artificial radionuclides were also determined in the samples collected in the neighbourhood of the nuclear installations, especially in marine sediment (IAEA-135). It is of interest to point out the high concentration of cesium radionuclides in IAEA-300 sediment collected in 1992 in the Baltic Sea in comparison with the IAEA-306 sediment collected also in the Baltic Sea in 1986. It seems to be an increase of the Baltic Sea artificial radioactivity by accumulation in time. Marine sediment constitutes an important component of marine ecosystem since it represents the final sink for any releases of wastes into the sea. These certified radioactive materials are very useful to all laboratories engaged in the radioactive pollution investigations on environmental samples. (authors)

Numerical investigation on pressure fluctuations in centrifugal compressor with different inlet guide vanes pre-whirl angles

International Nuclear Information System (INIS)

Wang, Y C; Shi, M; Cao, S L; Li, Z H

2013-01-01

The pressure fluctuations in a centrifugal compressor with different inlet guide vanes (IGV) pre-whirl angles were investigated numerically, as well as the pre-stress model and static structural of blade. The natural frequency was evaluated by pre-stress model analysis. The results show that, the aero-dynamic pressure acting on blade surface is smaller than rotation pre-stress, which wouldn't result in large deformation of blade. The natural frequencies with rotation pre-stress are slightly higher than without rotation pre-stress. The leading mechanism of pressure fluctuations for normal conditions is the rotor-stator (IGVs) interaction, while is serious flow separations for conditions that are close to surge line. A few frequency components in spectra are close to natural frequency, which possibly result in resonant vibration if amplitude is large enough, which is dangerous for compressor working, and should be avoided

Quality assurance and reference material requirements and considerations for environmental sample analysis in nuclear forensics

International Nuclear Information System (INIS)

Swindle, D.W. Jr.; Perrin, R.E.; Goldberg, S.A.; Cappis, J.

2002-01-01

Full text: High-sensitivity nuclear environmental sampling and analysis techniques have been proven in their ability to verify declared nuclear activities, as well as to assist in the detection of undeclared nuclear activities and facilities. Following the Gulf War, the capability and revealing power of environmental sampling and analysis techniques to support international safeguards was demonstrated and subsequently adopted by the International Atomic Energy Agency (IAEA) as routine safeguards measures in safeguards inspections and verifications. In addition to having been proved useful in international safeguards, environmental sampling and analysis techniques have demonstrated their utility in identifying the origins of 'orphaned' nuclear material, as well as the origin of intercepted smuggled nuclear material. Today, environmental sampling and analysis techniques are now being applied in six broad areas to support nonproliferation, disarmament treaty verification, national and international nuclear security, and environmental stewardship of weapons production activities. Consequently, more and more laboratories around the world are establishing capabilities or expanding capabilities to meet these growing applications, and as such requirements for quality assurance and control are increasing. The six areas are: 1) Nuclear safeguards; 2) Nuclear forensics/illicit trafficking; 3) Ongoing monitoring and verification (OMV); 4) Comprehensive Test Ban Treaty (CTBT); 5) Weapons dismantlement/materials disposition; and 6) Research and development (R and D)/environmental stewardship/safety. Application of environmental sampling and analysis techniques and resources to illicit nuclear material trafficking, while embodying the same basic techniques and resources, does have unique requirements for sample management, handling, protocols, chain of custody, archiving, and data interpretation. These requirements are derived from needs of how data from nuclear forensics

Determination of levels of polychlorinated biphenyls (PCBs) present in caulk and window glazing material samples from older buildings

Science.gov (United States)

Levels of polychlorinated biphenyls (PCBs) in caulk and window glazing material samples from older buildings were determined, using a method developed for this purpose. This method was evaluated by analyzing a combination of 47 samples of caulk, glazing materials, including quali...

Radon concentration and exhalation rates in building material samples from crushing zone in Shivalik Foot Hills

International Nuclear Information System (INIS)

Pundir, Anil; Kamboj, Sunil; Bansal, Vakul; Chauhan, R.P.; Rana, Rajinder Singh

2012-01-01

Radon ( 222 Rn) is an inert radioactive gas in the decay chain of uranium ( 238 U). It continuously emanates from soil to the atmosphere. Radon and its progeny are the major natural radioactive sources for the ambient radioactivity on Earth. A number of studies on radon were performed in recent decades focusing on its transport and movement in the atmosphere under different meteorological conditions. Building materials are the main source of radon inside buildings. Some construction materials are naturally more radioactive and removal of such material from the earth's crust and their subsequent use in construction of buildings further enhances the radioactivity level. The knowledge of radioactivity level in the building materials makes us aware about the management, guidelines and standards in construction of buildings. The main objective of the present investigations is to measure radon Concentration and exhalation rates in the samples collected from the Crushing zone of Shivalik foot hills. Different types of materials are being used in Northern part of India for construction of dwellings. For the measurement of radon concentration and its exhalation rates in building materials, LR-115 detectors were exposed in closed plastic canisters for three months. At the end of the exposure time, the detectors were subjected to a chemical etching process in 2.5N NaOH solution. The tracks produced by the alpha particles were observed and counted under an optical Olympus microscope at 600X. The measured track density was converted into radon concentration using a calibration factor. The surface and mass exhalation rates of radon have also been calculated using present data. The results indicate that the radon concentration varies appreciably from sample to sample and they were found to satisfy the safety criteria. There are samples in which radon concentration is higher and may enhance the indoor radiation levels when used as building construction materials. (author)

CFD simulation and validation of turbulent mixing in a rod bundle with vaned spacer grids based on LDV test

International Nuclear Information System (INIS)

Chen Xi; Li Songwei; Li Zhongchun; Du Sijia; Zhang Yu; Peng Huanhuan

2017-01-01

Spacer grids with mixing vanes are generally used in fuel assemblies of Pressurized Water Reactor (PWR), because that mixing vanes could enhance the lateral turbulent mixing in subchannels. Thus, heat exchangements are more efficient, and the value of departure from nucleate boiling (DNB) is greatly increased. Actually turbulent mixing is composed of two kinds of flows: swirling flow inside the subchannel and cross flow between subchannels. Swirling flow could induce mixing between hot water near the rod and cold water in the center of the subchannel, and may accelerate deviation of the bubbles from the rod surface. Besides, crossing flow help to mixing water between hot subchannels and cold subchannels, which impact relatively large flow area. As a result, how to accurately capture and how to predict the complicated mixing phenomenon are of great concernments. Recently many experimental studies has been conducted to provide detailed turbulent mixing in rod bundle, among which Laser Doppler Velocimetry method is widely used. With great development of Computational Fluid Dynamics, CFD has been validated as an analysis method for nuclear engineering, especially for single phase calculation. This paper presents the CFD simulation and validation of the turbulent mixing induced by spacer grid with mixing vanes in rod bundles. Experiment data used for validation came from 5 x 5 rod bundle test with LDV technology, which is organized by Science and Technology on Reactor System Design Technology Laboratory. A 5 x 5 rod bundle with two spacer grids were used. Each rod has dimension of 9.5 mm in outer diameter and distance between rods is 12.6 mm. Two axial bulk velocities were conducted at 3.0 m/s for high Reynolds number and 1.0 m/s for low Reynolds number. Working pressure was 1.0 bar, and temperature was about 25degC. Two different distances from the downstream of the mixing spacer grid and one from upstream were acquired. Mean axial velocities and turbulent intensities

Surface Temperature Measurements from a Stator Vane Doublet in a Turbine Engine Afterburner Flame Using a YAG:Tm Thermographic Phosphor

Science.gov (United States)

Eldridge, J. I.; Walker, D. G.; Gollub, S. L.; Jenkins, T. P.; Allison, S. W.

2015-01-01

Luminescence-based surface temperature measurements were obtained from a YAG:Tm-coated stator vane doublet exposed to the afterburner flame of a J85 test engine at University of Tennessee Space Institute (UTSI). The objective of the testing was to demonstrate that reliable surface temperatures based on luminescence decay of a thermographic phosphor producing short-wavelength emission could be obtained from the surface of an actual engine component in a high gas velocity, highly radiative afterburner flame environment. YAG:Tm was selected as the thermographic phosphor for its blue emission at 456 nm (1D23F4 transition) and UV emission at 365 nm (1D23H6 transition) because background thermal radiation is lower at these wavelengths, which are shorter than those of many previously used thermographic phosphors. Luminescence decay measurements were acquired using a probe designed to operate in the afterburner flame environment. The probe was mounted on the sidewall of a high-pressure turbine vane doublet from a Honeywell TECH7000 turbine engine coated with a standard electron-beam physical vapor deposited (EB-PVD) 200-m-thick TBC composed of yttria-stabilized zirconia (YSZ) onto which a 25-m-thick YAG:Tm thermographic phosphor layer was deposited by solution precursor plasma spray (SPPS). Spot temperature measurements were obtained by measuring luminescence decay times at different afterburner power settings and then converting decay time to temperature via calibration curves. Temperature measurements using the decays of the 456 and 365 nm emissions are compared. While successful afterburner environment measurements were obtained to about 1300C with the 456 nm emission, successful temperature measurements using the 365 nm emission were limited to about 1100C due to interference by autofluorescence of probe optics at short decay times.

Automated SEM and TEM sample preparation applied to copper/low k materials

Science.gov (United States)

Reyes, R.; Shaapur, F.; Griffiths, D.; Diebold, A. C.; Foran, B.; Raz, E.

2001-01-01

We describe the use of automated microcleaving for preparation of both SEM and TEM samples as done by SELA's new MC500 and TEMstation tools. The MC500 is an automated microcleaving tool that is capable of producing cleaves with 0.25 μm accuracy resulting in SEM-ready samples. The TEMstation is capable of taking a sample output from the MC500 (or from SELA's earlier MC200 tool) and producing a FIB ready slice of 25±5 μm, mounted on a TEM-washer and ready for FIB thinning to electron transparency for TEM analysis. The materials selected for the tool set evaluation mainly included the Cu/TaN/HOSP low-k system. The paper is divided into three sections, experimental approach, SEM preparation and analysis of HOSP low-k, and TEM preparation and analysis of Cu/TaN/HOSP low-k samples. For the samples discussed, data is presented to show the quality of preparation provided by these new automated tools.

Experimental Investigation of Turbine Vane Heat Transfer for Alternative Fuels

Energy Technology Data Exchange (ETDEWEB)

Nix, Andrew Carl [West Virginia Univ., Morgantown, WV (United States)

2015-03-23

The focus of this program was to experimentally investigate advanced gas turbine cooling schemes and the effects of and factors that contribute to surface deposition from particulate matter found in coal syngas exhaust flows on turbine airfoil heat transfer and film cooling, as well as to characterize surface roughness and determine the effects of surface deposition on turbine components. The program was a comprehensive, multi-disciplinary collaborative effort between aero-thermal and materials faculty researchers and the Department of Energy, National Energy Technology Laboratory (NETL). The primary technical objectives of the program were to evaluate the effects of combustion of syngas fuels on heat transfer to turbine vanes and blades in land-based power generation gas turbine engines. The primary questions to be answered by this investigation were; What are the factors that contribute to particulate deposition on film cooled gas turbine components? An experimental program was performed in a high-temperature and pressure combustion rig at the DOE NETL; What is the effect of coal syngas combustion and surface deposition on turbine airfoil film cooling? Deposition of particulate matter from the combustion gases can block film cooling holes, decreasing the flow of the film coolant and the film cooling effectiveness; How does surface deposition from coal syngas combustion affect turbine surface roughness? Increased surface roughness can increase aerodynamic losses and result in decreased turbine hot section efficiency, increasing engine fuel consumption to maintain desired power output. Convective heat transfer is also greatly affected by the surface roughness of the airfoil surface; Is there any significant effect of surface deposition or erosion on integrity of turbine airfoil thermal barrier coatings (TBC) and do surface deposits react with the TBC in any way to decrease its thermal insulating capability? Spallation and erosion of TBC is a persistent problem in

Cytotoxicity of Light-Cured Dental Materials according to Different Sample Preparation Methods

Directory of Open Access Journals (Sweden)

Myung-Jin Lee

2017-03-01

Full Text Available Dental light-cured resins can undergo different degrees of polymerization when applied in vivo. When polymerization is incomplete, toxic monomers may be released into the oral cavity. The present study assessed the cytotoxicity of different materials, using sample preparation methods that mirror clinical conditions. Composite and bonding resins were used and divided into four groups according to sample preparation method: uncured; directly cured samples, which were cured after being placed on solidified agar; post-cured samples were polymerized before being placed on agar; and “removed unreacted layer” samples had their oxygen-inhibition layer removed after polymerization. Cytotoxicity was evaluated using an agar diffusion test, MTT assay, and confocal microscopy. Uncured samples were the most cytotoxic, while removed unreacted layer samples were the least cytotoxic (p < 0.05. In the MTT assay, cell viability increased significantly in every group as the concentration of the extracts decreased (p < 0.05. Extracts from post-cured and removed unreacted layer samples of bonding resin were less toxic than post-cured and removed unreacted layer samples of composite resin. Removal of the oxygen-inhibition layer resulted in the lowest cytotoxicity. Clinicians should remove unreacted monomers on the resin surface immediately after restoring teeth with light-curing resin to improve the restoration biocompatibility.

Guide to sampling airborne radioactive materials in nuclear facilities

International Nuclear Information System (INIS)

Glissmeyer, J.A.

1995-01-01

The ANSI N13.1-1969 Guide to Sampling Airborne Radioactive Materials in Nuclear Facilities is currently being revised. The revision is being drafted by a working group under the auspices of the Health Physics Society Standards Committee. The main differences between the original standard and the proposed revision are a narrowed scope, a greater emphasis on the design process, and the verification of meeting performance criteria. Compliance with the revised standard will present new challenges, especially in the area of performance validation. The progress made in the revision and key portions of the standard are discussed. The DOE has recently petitioned EPA for alternate approaches to complying with air-sampling regulations. Dealing with compliance issues until the revised standard is adopted will be a challenge for both designers and regulators. The objective of this paper is to briefly describe the content of the proposed revision in order to point out significant differences from the old standard and to describe the new challenges that the proposed revision will present

Guide to sampling airborne radioactive materials in nuclear facilities

Energy Technology Data Exchange (ETDEWEB)

Glissmeyer, J.A. [Pacific Northwest Laboratory, Richland, WA (United States)

1995-02-01

The ANSI N13.1-1969 Guide to Sampling Airborne Radioactive Materials in Nuclear Facilities is currently being revised. The revision is being drafted by a working group under the auspices of the Health Physics Society Standards Committee. The main differences between the original standard and the proposed revision are a narrowed scope, a greater emphasis on the design process, and the verification of meeting performance criteria. Compliance with the revised standard will present new challenges, especially in the area of performance validation. The progress made in the revision and key portions of the standard are discussed. The DOE has recently petitioned EPA for alternate approaches to complying with air-sampling regulations. Dealing with compliance issues until the revised standard is adopted will be a challenge for both designers and regulators. The objective of this paper is to briefly describe the content of the proposed revision in order to point out significant differences from the old standard and to describe the new challenges that the proposed revision will present.

Evaluation of botanical reference materials for the determination of vanadium in biological samples

International Nuclear Information System (INIS)

Heydorn, K.; Damsgaard, E.

1982-01-01

Three botanical reference materials prepared by the National Bureau of Standards have been studied by neutron activation analysis to evaluate their suitability with respect to the determination of vanadium in biological samples. Various decomposition methods were applied in connection with chemical or radiochemical separations, and results for vanadium were compared with those found by purely instrumental neutron activation analysis. Significantly lower results indicate losses or incomplete dissolution, which makes SRM 1575 Pine Needles and SRM 1573 Tomato Leaves less satisfactory than SRM 1570 Spinach. A reference value of 1.15 mg/kg of this material is recommended, based on results from 3 different methods. All three materials are preferable to SRM 1571 Orchard Leaves, while Bowen's Kale remains the material of choice because of its lower concentration. (author)

Relating the structural strength of concrete sewer pipes and material properties retrieved from core samples

NARCIS (Netherlands)

Stanic, N.; Langeveld, J.G.; Salet, Theo; Clemens, F.H.L.R.

2016-01-01

Drill core samples are taken in practice for an analysis of the material characteristics of concrete pipes in order to improve the quality of the decision-making on rehabilitation actions. Earlier research has demonstrated that core sampling is associated with a significant uncertainty. In this

Determination of temperature dependence of full matrix material constants of PZT-8 piezoceramics using only one sample.

Science.gov (United States)

Zhang, Yang; Tang, Liguo; Tian, Hua; Wang, Jiyang; Cao, Wenwu; Zhang, Zhongwu

2017-08-15

Resonant ultrasound spectroscopy (RUS) was used to determine the temperature dependence of full matrix material constants of PZT-8 piezoceramics from room temperature to 100 °C. Property variations from sample to samples can be eliminated by using only one sample, so that data self-consistency can be guaranteed. The RUS measurement system error was estimated to be lower than 2.35%. The obtained full matrix material constants at different temperatures all have excellent self-consistency, which can help accurately predict device performance at high temperatures using finite element simulations.

Granular motor in the non-Brownian limit

NARCIS (Netherlands)

Oyarte Galvez, Loreto Alejandra; van der Meer, Roger M.

2016-01-01

In this work we experimentally study a granular rotor which is similar to the famous Smoluchowski–Feynman device and which consists of a rotor with four vanes immersed in a granular gas. Each side of the vanes can be composed of two different materials, creating a rotational asymmetry and turning

Zero-gravity Mean Free Surface Curvature of a Confined Liquid in a Radially-Vaned Container

Science.gov (United States)

Chen, Yongkang; Callahan, Michael; Weislogel, Mark

2013-01-01

A variety of increasingly intricate container geometries are under consideration for the passive manipulation of liquids aboard spacecraft where the impact of gravity may be neglected. In this study we examine the mean curvature of a liquid volume confined within a radial array of disconnected vanes of infinite extent. This particular geometry possesses a number of desirable characteristics relevant to waste water treatment aboard spacecraft for life support. It is observed that under certain conditions the slender shape of the free surface approaches an asymptote, which can be predicted analytically using new hybrid boundary conditions proposed herein. This contribution represents possibly the final extension of what has been referred to as the method of de Lazzer et al. (1996). The method enables the integration of the Young-Laplace equation over a domain with its boundaries, including the wetted portion of the solid boundaries, symmetry planes, and circular arcs representing free surfaces at the center plane of the liquid body. Asymptotic solutions at several limits are obtained and the analysis is confirmed with numerical computations.

Methods of and apparatus for extracting oil from shale and like materials

Energy Technology Data Exchange (ETDEWEB)

Edwards, C; Edwards, C L

1933-02-20

The design comprises a casing, a vertical chamber therein divided into a series of superposed zones, a tray fixed in each zone deflecting vanes rotatably mounted above each tray, a conical chute receives material from the circumference of the tray and conducts it to the tray beneath a flue through which heating gases are delivered to a space between the chamber and casing at each zone. An exhaust pipe is in communication with said space, and a fan draws gases therethrough. A pipe from the interior of the chamber at each zone conveys vapour obtained by distillation to an offtake pipe, and a fan is up on top of the offtake pipe.

Testing the homogeneity of candidate reference materials by solid sampling - AAS and INAA

International Nuclear Information System (INIS)

Rossbach, M.; Grobecker, K.-H.

2002-01-01

The necessity to quantify a natural material's homogeneity with respect to its elemental distribution prior to chemical analysis of a given aliquot is emphasised. Available instruments and methods to obtain the relevant information are described. Additionally the calculation of element specific, relative homogeneity factors, H E , and of a minimum sample mass M 5% to achieve 5% precision on a 95% confidence level is given. Especially, in the production and certification of Certified Reference Materials (CRMs) this characteristic information should be determined in order to provide the user with additional inherent properties of the CRM to enable more economical use of the expensive material and to evaluate further systematic bias of the applied analytical technique. (author)

RANdom SAmple Consensus (RANSAC) algorithm for material-informatics: application to photovoltaic solar cells.

Science.gov (United States)

Kaspi, Omer; Yosipof, Abraham; Senderowitz, Hanoch

2017-06-06

An important aspect of chemoinformatics and material-informatics is the usage of machine learning algorithms to build Quantitative Structure Activity Relationship (QSAR) models. The RANdom SAmple Consensus (RANSAC) algorithm is a predictive modeling tool widely used in the image processing field for cleaning datasets from noise. RANSAC could be used as a "one stop shop" algorithm for developing and validating QSAR models, performing outlier removal, descriptors selection, model development and predictions for test set samples using applicability domain. For "future" predictions (i.e., for samples not included in the original test set) RANSAC provides a statistical estimate for the probability of obtaining reliable predictions, i.e., predictions within a pre-defined number of standard deviations from the true values. In this work we describe the first application of RNASAC in material informatics, focusing on the analysis of solar cells. We demonstrate that for three datasets representing different metal oxide (MO) based solar cell libraries RANSAC-derived models select descriptors previously shown to correlate with key photovoltaic properties and lead to good predictive statistics for these properties. These models were subsequently used to predict the properties of virtual solar cells libraries highlighting interesting dependencies of PV properties on MO compositions.

Advanced materials for aircraft engine applications. Koku engine yo zairyo no doko

Energy Technology Data Exchange (ETDEWEB)

1994-05-01

The thrust/weight ratio which is thrust per unit weight of engine is a parameter of aircraft engine performance. With a mean material density of 6.6g/cm[sup 3], some of the supersonic plane engines are 7.9 in thrust/weight ratio. Its attaining 20 is predicted by some reports. The turbine inlet temperature is a parameter of engine temperature heightening exceeds 1400[degree]C. Its attaining 2000[degree]C in the 21st century is also predicted by some reports. By dividing the aircraft engine materials into both improvement and innovation material systems, the present paper explained the characteristics and present status of materials, and how to put them in practical use. As an improvement material, titanium alloy, nickel base alloy and resinous composite materials were exhibited with examples of having improved the established material system in performance and cost. Used as a turbine vane member, the nickel base alloy contributes, as a unidirectional coagulation alloy, single crystal alloy and oxide dispersion exciting alloy, to the creep resistance strengthening at high temperatures against the fatigue due to thermal strain. It is also explained how to put TiAl and FRM to practical use. 8 refs., 13 figs., 2 tabs.

Design and Demonstration of a Material-Plasma Exposure Target Station for Neutron Irradiated Samples

International Nuclear Information System (INIS)

Rapp, Juergen; Aaron, A. M.; Bell, Gary L.; Burgess, Thomas W.; Ellis, Ronald James; Giuliano, D.; Howard, R.; Kiggans, James O.; Lessard, Timothy L.; Ohriner, Evan Keith; Perkins, Dale E.; Varma, Venugopal Koikal

2015-01-01

5-20 MW/m"2 and ion fluxes up to 10"2"4 m"-"2s"-"1. Since PFCs will have to withstand neutron irradiation displacement damage up to 50 dpa, the target station design must accommodate radioactive specimens (materials to be irradiated in HFIR or at SNS) to enable investigations of the impact of neutron damage on materials. Therefore, the system will have to be able to install and extract irradiated specimens using equipment and methods to avoid sample modification, control contamination, and minimize worker dose. Included in the design considerations will be an assessment of all the steps between neutron irradiation and post-exposure materials examination/characterization, as well as an evaluation of the facility hazard categorization. In particular, the factors associated with the acquisition of radioactive specimens and their preparation, transportation, experimental configuration at the plasma-specimen interface, post-plasma-exposure sample handling, and specimen preparation will be evaluated. Neutronics calculations to determine the dose rates of the samples were carried out for a large number of potential plasma-facing materials.

Hydrogen, carbon and oxygen determination in proxy material samples using a LaBr3:Ce detector.

Science.gov (United States)

Naqvi, A A; Al-Matouq, Faris A; Khiari, F Z; Isab, A A; Raashid, M; Khateeb-ur-Rehman

2013-08-01

Hydrogen, carbon and oxygen concentrations were measured in caffeine, urea, ammonium acetate and melamine bulk samples via 14 MeV neutron inelastic scattering using a LaBr3:Ce detector. The samples tested herein represent drugs, explosives and benign materials, respectively. Despite its intrinsic activity, the LaBr3:Ce detector performed well in detecting the hydrogen, carbon and oxygen elements. Because 5.1 MeV nitrogen gamma rays interfere with silicon and calcium prompt gamma rays from the room background, the nitrogen peak was not detected in the samples. An excellent agreement was observed between the experimental and theoretical yields of 2.22, 4.43 and 6.13 MeV gamma rays from the analyzed samples as a function of H, C and O concentrations, respectively. Within statistical errors, the minimum detectable concentration (MDC) of hydrogen, carbon and oxygen elements in the tested materials were consistent with previously reported MDC values for these elements measured in hydrocarbon samples. Copyright © 2013 Elsevier Ltd. All rights reserved.

Special nuclear material inventory sampling plans

International Nuclear Information System (INIS)

Vaccaro, H.S.; Goldman, A.S.

1987-01-01

This paper presents improved procedures for obtaining statistically valid sampling plans for nuclear facilities. The double sampling concept and methods for developing optimal double sampling plans are described. An algorithm is described that is satisfactory for finding optimal double sampling plans and choosing appropriate detection and false alarm probabilities

Rotor boundary layer development with inlet guide vane (IGV) wake impingement

Science.gov (United States)

Jia, Lichao; Zou, Tengda; Zhu, Yiding; Lee, Cunbiao

2018-04-01

This paper examines the transition process in a boundary layer on a rotor blade under the impingement of an inlet guide vane wake. The effects of wake strengths and the reduced frequency on the unsteady boundary layer development on a low-speed axial compressor were investigated using particle image velocimetry. The measurements were carried out at two reduced frequencies (fr = fIGVS0/U2i, fr = 1.35, and fr = 0.675) with the Reynolds number, based on the blade chord and the isentropic inlet velocity, being 97 500. At fr = 1.35, the flow separated at the trailing edge when the wake strength was weak. However, the separation was almost totally suppressed as the wake strength increased. For the stronger wake, both the wake's high turbulence and the negative jet behavior of the wake dominated the interaction between the unsteady wake and the separated boundary layer on the suction surface of the airfoil. The boundary layer displacement thickened first due to the negative jet effect. Then, as the disturbances developed underneath the wake, the boundary layer thickness reduced gradually. The high disturbance region convected downstream at a fraction of the free-stream velocity and spread in the streamwise direction. The separation on the suction surface was suppressed until the next wake's arrival. Because of the long recovery time at fr = 0.675, the boundary layer thickened gradually as the wake convected further downstream and finally separated due to the adverse pressure gradient. The different boundary layer states in turn affected the development of disturbances.

Aspects of cleaning environmental materials for multi-element analysis, e.g. plant samples

International Nuclear Information System (INIS)

Markert, B.

1992-01-01

Cleaning of samples is often the first step in the entire procedure of sample preparation in environmental trace element research. The question must generally be raised of whether cleaning is meaningful before chemical investigations with plant material (e.g. for the determination of transfer factors in the soil/plant system) or not (e.g. for food chain analysis in the plant/animal system). The most varied cleaning procedures for plant samples are currently available ranging from dry and wet wiping of the leaf or needle surface up to the complete removal of the cuticule with the aid of chlorofom. There is at present no standardized cleaning procedure for plant samples so that it is frequently not possible to compare analytical data from different working groups studying the same plant species. (orig.)

Standard operating procedure for combustion of 14C - samples with OX-500 biological material oxidizer

International Nuclear Information System (INIS)

Nashriyah Mat.

1995-01-01

This procedure is for the purpose of safe operation of OX-500 biological material oxidizer. For ease of operation, the operation flow chart (including testing the system and sample combustion) and end of day maintenance flow chart were simplified. The front view, diagrams and switches are duly copied from operating manual. Steps on sample preparation are also included for biotic and a biotic samples. This operating procedure is subjected to future reviews

Natural radioactivity measurement in pumice samples used raw materials in Turkey

International Nuclear Information System (INIS)

Turhan, S.; Yuecel, H.; Guenduez, L.; Sahin, S.; Vural, M.; Parmaksiz, A.; Demircioglu, B.

2007-01-01

The activity concentrations of 232 Th, 226 Ra, and 4 K in different pumice samples have been determined by high-resolution γ-ray spectrometry using a 110% HpGe detector. The radium equivalent activities (Ra eq ), external hazard index (H ex ), and internal hazard index (H in ) associated with the natural radionuclides and representative level index (I γ r ) are calculated to assess the radiation hazard of the natural radioactivity in the pumice samples. The mean values of the measured radioactivity concentrations of 232 Th, 226 Ra, and 4 K for pumice samples from the region of lakes (ROL) are 232.4±8.0, 196.9±7.8, and 1325.8±20.4 Bq kg -1 and for pumice samples from Cukurova region (CR) 16.3±4.0, 16.1±4.9, and 479.7±170.4 Bq kg -1 , respectively. The calculated Ra eq values vary from 435.9±12.5 to 883.6±41.5 Bq kg -1 with a mean of 630.9±20.2 Bq kg -1 for the ROL samples and from 49.7±3.3 to 101.9±7.2 Bq kg -1 with a mean of 76.3±23.7 Bq kg -1 for the CR samples. For the ROL samples, Ra eq are above the limit of 370 Bq kg -1 , equivalent to external γ dose of 1.5 mSv yr -1 , recommended for the safe use of construction materials by NEA-OECD, while for the CR samples, Ra eq values are lower than the limit

Developments of solid materials for UF₆ sampling

Energy Technology Data Exchange (ETDEWEB)

Smith, Nicholas [Argonne National Lab. (ANL), Argonne, IL (United States). Nuclear Engineering Division; Hebden, Andrew [Argonne National Lab. (ANL), Argonne, IL (United States). Nuclear Engineering Division; Savina, Joseph [Argonne National Lab. (ANL), Argonne, IL (United States). Nuclear Engineering Division

2017-11-15

This project demonstrated that a device using majority Commercial Off the Shelf (COTS) components could be used to collect uranium hexafluoride samples safely from gaseous or solid sources. The device was based on the successful Cristallini method developed by ABACC over the past 10 years. The system was designed to capture and store the UF₆ as an inert fluoride salt to ease transportation regulations. In addition, the method was considerably faster than traditional cryogenic methods, collected enough material to perform analyses without undue waste, and could be used either inside a facility or in the storage yard.

Sample Acquisition for Materials in Planetary Exploration (SAMPLE), Phase I

Data.gov (United States)

National Aeronautics and Space Administration — ORBITEC proposes to analyze, design, and develop a device for autonomous lunar surface/subsurface sampling and processing applications. The Sample Acquisition for...

New hybrid materials as Zn(II) sorbents in water samples

International Nuclear Information System (INIS)

Perez-Quintanilla, Damian; Sanchez, Alfredo; Hierro, Isabel del; Fajardo, Mariano; Sierra, Isabel

2010-01-01

Mesoporous silicas have been chemically modified with 5-mercapto-1-methyltetrazole (MTTZ) obtaining hybrid materials denominated MTTZ-MSU-2 and MTTZ-HMS. These materials were employed as Zn(II) sorbents from aqueous media at room temperature. The effect of several variables (stirring time, pH, presence of other metals) has been studied using batch and column techniques. Flame atomic absorption spectrometry (FAAS) was used to determinate Zn(II) concentration in the filtrate or in the eluted solution after the adsorption process. The results indicate that under pH 8, the maximum adsorption value was 0.94 ± 0.01 and 0.72 ± 0.01 mmol Zn(II)/g for MTTZ-MSU-2 and MTTZ-HMS, respectively. In tap water samples, a preconcentration factor of 200 was obtained. On the basis of these results, it can be concluded that it is possible to modify chemically MSU-2 and HMS with 5-mercapto-1-methyltetrazole and to use the resulting modified mesoporous silica as an effective adsorbent for Zn(II) in aqueous media.

Establishment of a clean laboratory for ultra trace analysis of nuclear materials in safeguards environmental samples

International Nuclear Information System (INIS)

Hanzawa, Yukiko; Magara, Masaaki; Watanabe, Kazuo

2003-01-01

The Japan Atomic Energy Research Institute has established a cleanroom facility with cleanliness of ISO Class 5: the Clean Laboratory for Environmental Analysis and Research (CLEAR). It was designed to be used for the analysis of nuclear materials in environmental samples mainly for the safeguards, in addition to the Comprehensive Nuclear-Test-Ban Treaty verification and research on environmental sciences. The CLEAR facility was designed to meet conflicting requirements of a cleanroom and for handling of nuclear materials according to Japanese regulations, i.e., to avoid contamination from outside and to contain nuclear materials inside the facility. This facility has been intended to be used for wet chemical treatment, instrumental analysis and particle handling. A fume-hood to provide a clean work surface for handling of nuclear materials was specially designed. Much attention was paid to the selection of construction materials for use to corrosive acids. The performance of the cleanroom and analytical background in the laboratory are discussed. This facility has satisfactory specification required for joining the International Atomic Energy Agency Network of Analytical Laboratories. It can be concluded that the CLEAR facility enables analysis of ultra trace amounts of nuclear materials at sub-pictogram level in environmental samples. (author)

Are extracted materials truly representative of original samples? Impact of C18 extraction on CDOM optical and chemical properties

Directory of Open Access Journals (Sweden)

Andrea A Andrew

2016-02-01

Full Text Available Some properties of dissolved organic matter (DOM and chromophoric dissolved organic matter (CDOM can be easily measured directly on whole waters, while others require sample concentration and removal of natural salts. To increase CDOM content and eliminate salts, solid phase extraction is often employed. Biases following extraction and elution are inevitable, thus raising the question of how truly representative the extracted material is of the original. In this context, we investigated the wavelength dependence of extraction efficiency for C18 cartridges with respect to CDOM optical properties using samples obtained from the Middle Atlantic Bight (MAB and the Equatorial Atlantic Ocean (EAO. Further, we compared the optical changes of C18 extracts and the corresponding whole water following chemical reduction with sodium borohydride (NaBH4.C18 cartridges preferentially extracted long-wavelength absorbing/emitting material for samples impacted by riverine input. Extraction efficiency overall decreased with offshore distance away from riverine input. Spectral slopes of C18-OM samples were also almost always lower than those of their corresponding CDOM samples supporting the preferential extraction of higher molecular weight absorbing material. The wavelength dependence of the optical properties (absorption, fluorescence emission and quantum yield of the original water samples and their corresponding extracted material were very similar. C18 extracts and corresponding water samples further exhibited comparable optical changes following NaBH4 reduction, thus suggesting a similarity in nature (structure of the optically active extracted material, independent of geographical locale. Altogether, these data suggested a strong similarity between C18 extracts and corresponding whole waters, thus indicating that extracts are representative of the CDOM content of original waters.

Are Extracted Materials Truly Representative of Original Samples? Impact of C18 Extraction on CDOM Optical and Chemical Properties.

Science.gov (United States)

Andrew, Andrea A; Del Vecchio, Rossana; Zhang, Yi; Subramaniam, Ajit; Blough, Neil V

2016-01-01

Some properties of dissolved organic matter (DOM) and chromophoric dissolved organic matter (CDOM) can be easily measured directly on whole waters, while others require sample concentration and removal of natural salts. To increase CDOM content and eliminate salts, solid phase extraction (SPE) is often employed. Biases following extraction and elution are inevitable, thus raising the question of how truly representative the extracted material is of the original. In this context, we investigated the wavelength dependence of extraction efficiency for C18 cartridges with respect to CDOM optical properties using samples obtained from the Middle Atlantic Bight (MAB) and the Equatorial Atlantic Ocean (EAO). Further, we compared the optical changes of C18 extracts and the corresponding whole water following chemical reduction with sodium borohydride (NaBH4). C18 cartridges preferentially extracted long-wavelength absorbing/emitting material for samples impacted by riverine input. Extraction efficiency overall decreased with offshore distance away from riverine input. Spectral slopes of C18-OM samples were also almost always lower than those of their corresponding CDOM samples supporting the preferential extraction of higher molecular weight absorbing material. The wavelength dependence of the optical properties (absorption, fluorescence emission, and quantum yield) of the original water samples and their corresponding extracted material were very similar. C18 extracts and corresponding water samples further exhibited comparable optical changes following NaBH4 reduction, thus suggesting a similarity in nature (structure) of the optically active extracted material, independent of geographical locale. Altogether, these data suggested a strong similarity between C18 extracts and corresponding whole waters, thus indicating that extracts are representative of the CDOM content of original waters.

Are extracted materials truly representative of original samples? Impact of C18 extraction on CDOM optical and chemical properties

Science.gov (United States)

Andrew, Andrea; Del Vecchio, Rossana; Zhang, Yi; Subramaniam, Ajit; Blough, Neil

2016-02-01

Some properties of dissolved organic matter (DOM) and chromophoric dissolved organic matter (CDOM) can be easily measured directly on whole waters, while others require sample concentration and removal of natural salts. To increase CDOM content and eliminate salts, solid phase extraction is often employed. Biases following extraction and elution are inevitable, thus raising the question of how truly representative the extracted material is of the original. In this context, we investigated the wavelength dependence of extraction efficiency for C18 cartridges with respect to CDOM optical properties using samples obtained from the Middle Atlantic Bight (MAB) and the Equatorial Atlantic Ocean (EAO). Further, we compared the optical changes of C18 extracts and the corresponding whole water following chemical reduction with sodium borohydride (NaBH4). C18 cartridges preferentially extracted long-wavelength absorbing/emitting material for samples impacted by riverine input. Extraction efficiency overall decreased with offshore distance away from riverine input. Spectral slopes of C18-OM samples were also almost always lower than those of their corresponding CDOM samples supporting the preferential extraction of higher molecular weight absorbing material. The wavelength dependence of the optical properties (absorption, fluorescence emission and quantum yield) of the original water samples and their corresponding extracted material were very similar. C18 extracts and corresponding water samples further exhibited comparable optical changes following NaBH4 reduction, thus suggesting a similarity in nature (structure) of the optically active extracted material, independent of geographical locale. Altogether, these data suggested a strong similarity between C18 extracts and corresponding whole waters, thus indicating that extracts are representative of the CDOM content of original waters.

Design and Demonstration of a Material-Plasma Exposure Target Station for Neutron Irradiated Samples

Energy Technology Data Exchange (ETDEWEB)

Rapp, Juergen [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Aaron, A. M. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Bell, Gary L. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Burgess, Thomas W. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Ellis, Ronald James [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Giuliano, D. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Howard, R. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Kiggans, James O. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Lessard, Timothy L. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Ohriner, Evan Keith [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Perkins, Dale E. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Varma, Venugopal Koikal [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

2015-10-20

-state heat fluxes of 5–20 MW/m² and ion fluxes up to 10²⁴ m^-2s^-1. Since PFCs will have to withstand neutron irradiation displacement damage up to 50 dpa, the target station design must accommodate radioactive specimens (materials to be irradiated in HFIR or at SNS) to enable investigations of the impact of neutron damage on materials. Therefore, the system will have to be able to install and extract irradiated specimens using equipment and methods to avoid sample modification, control contamination, and minimize worker dose. Included in the design considerations will be an assessment of all the steps between neutron irradiation and post-exposure materials examination/characterization, as well as an evaluation of the facility hazard categorization. In particular, the factors associated with the acquisition of radioactive specimens and their preparation, transportation, experimental configuration at the plasma-specimen interface, post-plasma-exposure sample handling, and specimen preparation will be evaluated. Neutronics calculations to determine the dose rates of the samples were carried out for a large number of potential plasma-facing materials.

A Study of Performance Output of a Multivane Air Engine Applying Optimal Injection and Vane Angles

Directory of Open Access Journals (Sweden)

Bharat Raj Singh

2012-01-01

Full Text Available This paper presents a new concept of the air engine using compressed air as the potential power source for motorbikes, in place of an internal combustion engine. The motorbike is proposed to be equipped with an air engine, which transforms the energy of the compressed air into mechanical motion energy. A mathematical model is presented here, and performance evaluation is carried out on an air-powered novel air turbine engine. The maximum power output is obtained as 3.977 kW (5.50 HP at the different rotor to casing diameter ratios, optimal injection angle 60°, vane angle 45° for linear expansion (i.e., at minimum air consumption when the casing diameter is kept 100 mm, at injection pressure 6 bar (90 psi and speed of rotation 2500 rpm. A prototype air engine is built and tested in the laboratory. The experimental results are also seen much closer to the analytical values, and the performance efficiencies are recorded around 70% to 95% at the speed of rotation 2500–3000 rpm.

Active unsteady aerodynamic suppression of rotating stall in an incompressible flow centrifugal compressor with vaned diffuser

Science.gov (United States)

Lawless, Patrick B.; Fleeter, Sanford

1991-01-01

A mathematical model is developed to analyze the suppression of rotating stall in an incompressible flow centrifugal compressor with a vaned diffuser, thereby addressing the important need for centrifugal compressor rotating stall and surge control. In this model, the precursor to to instability is a weak rotating potential velocity perturbation in the inlet flow field that eventually develops into a finite disturbance. To suppress the growth of this potential disturbance, a rotating control vortical velocity disturbance is introduced into the impeller inlet flow. The effectiveness of this control is analyzed by matching the perturbation pressure in the compressor inlet and exit flow fields with a model for the unsteady behavior of the compressor. To demonstrate instability control, this model is then used to predict the control effectiveness for centrifugal compressor geometries based on a low speed research centrifugal compressor. These results indicate that reductions of 10 to 15 percent in the mean inlet flow coefficient at instability are possible with control waveforms of half the magnitude of the total disturbance at the inlet.

Effects of grid spacer with mixing vane on entrainments and depositions in two-phase annular flows

Directory of Open Access Journals (Sweden)

Akimaro Kawahara

2015-06-01

Full Text Available The effects of mixing vanes (MVs attached to a grid spacer on the characteristics of air–water annular flows were experimentally investigated. To know the effects, a grid spacer with or without MV was inserted in a vertical circular pipe of 16-mm internal diameter. For three cases (i.e., no spacer, spacer without MV, and spacer with MV, the liquid film thickness, liquid entrainment fraction, and deposition rate were measured by the constant current method, single liquid film extraction method, and double liquid film extraction method, respectively. The MVs significantly promote the re-deposition of liquid droplets in the gas core flow into the liquid film on the channel walls. The deposition mass transfer coefficient is three times higher for the spacer with MV than for the spacer without MV, even for cases 0.3-m downstream from the spacer. The liquid film thickness becomes thicker upstream and downstream for the spacer with MV, compared with the thickness for the spacer without MV and for the case with no spacer.

Avian Feathers: An Examination of Lightweight Resilience and Bioinspired Designs

Science.gov (United States)

Sullivan, Tarah Naoe

In bird flight, the majority of the wing surface consists of highly refined and hierarchically organized beta-keratinous feathers. Thus, flight feathers contain ingenious combinations of components that optimize lift, stiffness, aerodynamics, and damage resistance. Their design involves two main parts: a central shaft which prescribes stiffness and lateral vanes that allow for the capture of air. Within the feather vane, barbs branch from the shaft and barbules branch from barbs, forming a flat surface and ensuring lift. Microhooks at the end of barbules hold barbs tightly together, providing a close-knit, unified structure and enabling repair of the vane through the reattachment of un-hooked junctions. In this dissertation, unique aspects of feather architecture are explored to uncover principles translatable to the design of modern aerospace materials and structures. Specifically, understudied aspects of the feather's lightweight yet resilient properties are investigated. This research has revealed several novel characteristics of the feather. Allometric scaling relationships are developed linking the geometry of a bird's wing components to its flight characteristics and total mass. Barbule spacing within the feather vane is found to be 8-16 microm for birds ranging from 0.02-11 kg. Additionally, it is discovered that strength is recovered with the shape recovery property of feathers, and a mechanism for this phenomenon is proposed. Barbule adhesion within the vane is found to prevent barbs from twisting in flexure, maintaining the vane's stiffness, and the extent to which unzipping these connections affects the feather's ability to capture air is related to barb shape. Directional permeability of the feather vane is experimentally confirmed and related to the intricate microstructure of barbules. Lastly, the exceptional architecture of the feather motivated the design of novel bioinspired structures with tailored and unique properties. The avian feather serves

INCIDENCE OF FILAMENTOUS FUNGI WITH TOXIGENIC POTENTIAL ON SAMPLES OF FEED AND RAW MATERIALS FOR THEIR MANUFACTURE

Directory of Open Access Journals (Sweden)

Rodrigo Vera

2016-06-01

Full Text Available The presence and/or accumulation of mycotoxins in foods intended for human and animal nutrition is a constant concern for the harmful health effects resulting from ingestion. The aims of this communication were to analyze samples of feed and raw materials for manufacturing and to determine the presence of strains of filamentous fungi with toxigenic capacity. The values of frequency in the total samples (N = 422, indicated 63% of contamination, where A. flavus represented the most common (29.8%, while in feed and raw materials separately, indicated A. flavus has the highest value in both categories. In the analysis of different type of raw materials, A. flavus contaminated all types of samples, with the bran and soybean meal substrates having higher values for this Aspergillus, and corn substrate more fungal contamination. These results would demonstrate that the presence of mycobiota with toxigenic potential in food for animal feed is a disturbing reality.

Estimated neutron-activation data for TFTR. Part II. Biological dose rate from sample-materials activation

International Nuclear Information System (INIS)

Ku, L.; Kolibal, J.G.

1982-06-01

The neutron induced material activation dose rate data are summarized for the TFTR operation. This report marks the completion of the second phase of the systematic study of the activation problem on the TFTR. The estimations of the neutron induced activation dose rates were made for spherical and slab objects, based on a point kernel method, for a wide range of materials. The dose rates as a function of cooling time for standard samples are presented for a number of typical neutron spectrum expected during TFTR DD and DT operations. The factors which account for the variations of the pulsing history, the characteristic size of the object and the distance of observation relative to the standard samples are also presented

Measurement of residual stresses in welded sample of dissimilar materials

International Nuclear Information System (INIS)

Mansur, Tanius Rodrigues; Gomes, Paulo de Tarso Vida; Scaldaferri, Denis Henrique Bianchi; Martins, Geraldo Antonio Scoralick; Atanazio Filho, Nelson do Nascimento

2008-01-01

reactors, what can generate significant residual stresses due so much to the welding procedure as for the difference of the coefficients of thermal expansion of the involved materials. In this work, are shown the results of the measurement of residual tensions in welded sample of steel carbon SA 508 Cl 3 and stainless steel 316L. The Inconel 182 was used as weld metal. (author)

Boat sampling

International Nuclear Information System (INIS)

Citanovic, M.; Bezlaj, H.

1994-01-01

This presentation describes essential boat sampling activities: on site boat sampling process optimization and qualification; boat sampling of base material (beltline region); boat sampling of weld material (weld No. 4); problems accompanied with weld crown varieties, RPV shell inner radius tolerance, local corrosion pitting and water clarity. The equipment used for boat sampling is described too. 7 pictures

Brittle Materials Design, High Temperature Gas Turbine

Science.gov (United States)

1975-10-01

10oF/sec. The 3 to 5 minute hold at 2500oF will permit data acquisition, vane viewing and/or photography through the horoscope . Cool down...assessed. Several radii appear as flats rather than true radii. The first airfoil with the profiled, torroidal shaped tenon ends was received

Molding of strength testing samples using modern PDCPD material for purpose of automotive industry

Science.gov (United States)

Grabowski, L.; Baier, A.; Sobek, M.

2017-08-01

The casting of metal materials is widely known but the molding of composite polymer materials is not well-known method still. The initial choice of method for producing composite bodies was the method of casting of PDCPD material. For purpose of performing casting of polymer composite material, a special mold was made. Firstly, the 3D printed, using PLA material, mold was used. After several attempts of casting PDCPD many problems were encountered. The second step was to use mold milled from a firm and dense isocyanate foam. After several attempts research shown that this solution is more resistant to high-temperature peak, but this material is too fragile to use it several times. This solution also prevents mold from using external heating, which can be necessary for performing correct molding process. The last process was to use the aluminum mold, which is dedicated to PDCPD polymer composite, because of low adhesiveness. This solution leads to perform correct PDCPD polymer composite material injection. After performing casting operation every PDCPD testing samples were tested. These results were compared together. The result of performed work was to archive correct properties of injection of composite material. Research and results were described in detail in this paper.

A model to predict radon exhalation from walls to indoor air based on the exhalation from building material samples

International Nuclear Information System (INIS)

Sahoo, B.K.; Sapra, B.K.; Gaware, J.J.; Kanse, S.D.; Mayya, Y.S.

2011-01-01

In recognition of the fact that building materials are an important source of indoor radon, second only to soil, surface radon exhalation fluxes have been extensively measured from the samples of these materials. Based on this flux data, several researchers have attempted to predict the inhalation dose attributable to radon emitted from walls and ceilings made up of these materials. However, an important aspect not considered in this methodology is the enhancement of the radon flux from the wall or the ceiling constructed using the same building material. This enhancement occurs mainly because of the change in the radon diffusion process from the former to the latter configuration. To predict the true radon flux from the wall based on the flux data of building material samples, we now propose a semi-empirical model involving radon diffusion length and the physical dimensions of the samples as well as wall thickness as other input parameters. This model has been established by statistically fitting the ratio of the solution to radon diffusion equations for the cases of three-dimensional cuboidal shaped building materials (such as brick, concrete block) and one dimensional wall system to a simple mathematical function. The model predictions have been validated against the measurements made at a new construction site. This model provides an alternative tool (substitute to conventional 1-D model) to estimate radon flux from a wall without relying on 226 Ra content, radon emanation factor and bulk density of the samples. Moreover, it may be very useful in the context of developing building codes for radon regulation in new buildings. - Research highlights: → A model is proposed to predict radon flux from wall using flux of building material. → It is established based on the diffusion mechanism in building material and wall. → Study showed a large difference in radon flux from building material and wall. → Model has been validated against the measurements made at

Radionuclide release from simulated waste material after biogeochemical leaching of uraniferous mineral samples

International Nuclear Information System (INIS)

Williamson, Aimee Lynn; Caron, François; Spiers, Graeme

2014-01-01

Biogeochemical mineral dissolution is a promising method for the released of metals in low-grade host mineralization that contain sulphidic minerals. The application of biogeochemical mineral dissolution to engineered leach heap piles in the Elliot Lake region may be considered as a promising passive technology for the economic recovery of low grade Uranium-bearing ores. In the current investigation, the decrease of radiological activity of uraniferous mineral material after biogeochemical mineral dissolution is quantified by gamma spectroscopy and compared to the results from digestion/ICP-MS analysis of the ore materials to determine if gamma spectroscopy is a simple, viable alternative quantification method for heavy nuclides. The potential release of Uranium (U) and Radium-226 ( 226 Ra) to the aqueous environment from samples that have been treated to represent various stages of leaching and passive closure processes are assessed. Dissolution of U from the solid phase has occurred during biogeochemical mineral dissolution in the presence of Acidithiobacillus ferrooxidans, with gamma spectroscopy indicating an 84% decrease in Uranium-235 ( 235 U) content, a value in accordance with the data obtained by dissolution chemistry. Gamma spectroscopy data indicate that only 30% of the 226 Ra was removed during the biogeochemical mineral dissolution. Chemical inhibition and passivation treatments of waste materials following the biogeochemical mineral dissolution offer greater protection against residual U and 226 Ra leaching. Pacified samples resist the release of 226 Ra contained in the mineral phase and may offer more protection to the aqueous environment for the long term, compared to untreated or inhibited residues, and should be taken into account for future decommissioning. - Highlights: • Gamma counting showed an 84% decrease in 235 U after biogeochemical mineral leaching. • Chemical digestion/ICP-MS analysis also showed an 84% decrease in total U. • Over

21 CFR 211.110 - Sampling and testing of in-process materials and drug products.

Science.gov (United States)

2010-04-01

... PHARMACEUTICALS Production and Process Controls § 211.110 Sampling and testing of in-process materials and drug... capsule weight variation; (2) Disintegration time; (3) Adequacy of mixing to assure uniformity and... production process, e.g., at commencement or completion of significant phases or after storage for long...

Evaluation Of Gas Diffusion Through Plastic Materials Used In Experimental And Sampling Equipment

DEFF Research Database (Denmark)

Kjeldsen, Peter

1993-01-01

. Calculations show that diffusion of oxygen through plastic tubing and reactors into anoxic water can be a serious problem for a series of plastic materials. Comparison of the method for turbulent and laminar flow in tubings shows that the difference is insignificant for most cases. Calculations show also......Plastic materials are often used in experimental and sampling equipment. Plastics are not gas tight, since gases are able to diffuse through the walls of tubing and containers made of plastic. Methods for calculating the significance of gas diffusion through the walls of containers and the walls...... of tubings for both turbulent and laminar flow conditions is presented. A more complex model for diffusion under laminar flow conditions is developed. A comprehensive review on gas diffusion coefficients for the main gases (O2, N2, CO2, CH4 etc.) and for a long range of plastic materials is also presented...

The problem of large samples. An activation analysis study of electronic waste material

International Nuclear Information System (INIS)

Segebade, C.; Goerner, W.; Bode, P.

2007-01-01

Large-volume instrumental photon activation analysis (IPAA) was used for the investigation of shredded electronic waste material. Sample masses from 1 to 150 grams were analyzed to obtain an estimate of the minimum sample size to be taken to achieve a representativeness of the results which is satisfactory for a defined investigation task. Furthermore, the influence of irradiation and measurement parameters upon the quality of the analytical results were studied. Finally, the analytical data obtained from IPAA and instrumental neutron activation analysis (INAA), both carried out in a large-volume mode, were compared. Only parts of the values were found in satisfactory agreement. (author)

Life prediction of advanced materials for gas turbine application

Energy Technology Data Exchange (ETDEWEB)

Zamrik, S.Y.; Ray, A.; Koss, D.A. [Pennsylvania State Univ., University Park, PA (United States)

1995-10-01

Most of the studies on the low cycle fatigue life prediction have been reported under isothermal conditions where the deformation of the material is strain dependent. In the development of gas turbines, components such as blades and vanes are exposed to temperature variations in addition to strain cycling. As a result, the deformation process becomes temperature and strain dependent. Therefore, the life of the component becomes sensitive to temperature-strain cycling which produces a process known as {open_quotes}thermomechanical fatigue, or TMF{close_quotes}. The TMF fatigue failure phenomenon has been modeled using conventional fatigue life prediction methods, which are not sufficiently accurate to quantitatively establish an allowable design procedure. To add to the complexity of TMF life prediction, blade and vane substrates are normally coated with aluminide, overlay or thermal barrier type coatings (TBC) where the durability of the component is dominated by the coating/substrate constitutive response and by the fatigue behavior of the coating. A number of issues arise from TMF depending on the type of temperature/strain phase cycle: (1) time-dependent inelastic behavior can significantly affect the stress response. For example, creep relaxation during a tensile or compressive loading at elevated temperatures leads to a progressive increase in the mean stress level under cyclic loading. (2) the mismatch in elastic and thermal expansion properties between the coating and the substrate can lead to significant deviations in the coating stress levels due to changes in the elastic modulii. (3) the {open_quotes}dry{close_quotes} corrosion resistance coatings applied to the substrate may act as primary crack initiation sites. Crack initiation in the coating is a function of the coating composition, its mechanical properties, creep relaxation behavior, thermal strain range and the strain/temperature phase relationship.

Method of extruding and packaging a thin sample of reactive material including forming the extrusion die

International Nuclear Information System (INIS)

Lewandowski, E.F.; Peterson, L.L.

1985-01-01

This invention teaches a method of cutting a narrow slot in an extrusion die with an electrical discharge machine by first drilling spaced holes at the ends of where the slot will be, whereby the oil can flow through the holes and slot to flush the material eroded away as the slot is being cut. The invention further teaches a method of extruding a very thin ribbon of solid highly reactive material such as lithium or sodium through the die in an inert atmosphere of nitrogen, argon or the like as in a glovebox. The invention further teaches a method of stamping out sample discs from the ribbon and of packaging each disc by sandwiching it between two aluminum sheets and cold welding the sheets together along an annular seam beyond the outer periphery of the disc. This provides a sample of high purity reactive material that can have a long shelf life

Application of Streaming Effect and Joule Heating Effect of Pulse Current in Crack Healing of Metal Materials

Directory of Open Access Journals (Sweden)

Jian Chu

2017-06-01

Full Text Available Remanufacture engineering is an emerging industry that saves resources as well as protects the environment. However, cracks on remanufactured components can result in serious trouble. Therefore, in order to avoid unnecessary waste of resources and energy, these cracks should be repaired radically in order to ensure the smooth progressing of the remanufacturing process. Consequently, the crack healing technique of metal materials is very important in the field of remanufacturing. In this study, the U-shape vane stainless steel of a centrifugal compressor which had cracks was processed by pulse current using a high pulse current discharge device, and the influence of the streaming effect and Joule heating effect of pulse current on the crack healing of metal materials was studied, aiming to provide references for the better application of this technology in the remanufacturing field in the future.

Determination of element concentrations in biological reference materials by solid sampling and other analytical methods

International Nuclear Information System (INIS)

Schauenburg, H.; Weigert, P.

1992-01-01

Using solid sampling with graphite furnace atomic absorption spectrometry (GFAAS), values for cadmium, copper, lead and zinc in six biological reference materials were obtained from up to four laboratories participating in three collaborative studies. These results are compared with those obtained with other methods used in routine analysis from laboratories of official food control. Under certain conditions solid sampling with GFAAS seems to be suitable for routine analysis as well as conventional methods. (orig.)

Investigating the formation mechanism of soot-like materials present in blast furnace coke samples

Energy Technology Data Exchange (ETDEWEB)

S. Dong; P. A' lvarez; N. Paterson; D.R. Dugwell; R. Kandiyoti [Imperial College London, London (United Kingdom). Department of Chemical Engineering

2008-09-15

An attempt to gain an understanding of the formation mechanism of these 'soot-like' materials has been made by means of tracing the changes in the molecular-mass distribution and molecular structure of the NMP-extractable materials from an injectant coal as well as its partially gasified chars and its pyrolytic tars. Variations in the SEC chromatograms provide clues about changes in the apparent molecular-mass distributions of these NMP extracts. Results suggest that the build-up of 'soot-like' materials follows from the secondary reactions of tars evolved from the injectant coal. The likely secondary-reaction pathways have been probed by collating structural information on these NMP extracts. The time-resolved 13-16 and 22-25 min elution fractions from the SEC column have been characterized using UV fluorescence (UV F) spectroscopy. Greater concentrations of larger aromatic ring systems are found present in samples formed under conditions appearing more prone for soot formation. The 11-16 min (large apparent molecular mass) effluent from SEC has been examined by Fourier transform infrared (FTIR) spectroscopy and transmission electron microscopy (TEM). Results from FTIR spectroscopy are consistent with the UV F data, showing more significant extents of dehydrogenation under conditions more prone to form soot. Similarly, TEM results show that larger amount of graphene layers exist in samples exposed to more soot-prone conditions. The emerging picture for the formation of 'soot-like' materials involves a well-defined sequence. Tars evolved from the injectant coal undergo secondary dehydrogenation, condensation, and repolymerization reactions, which eventually lead to the formation of the NMP-extractable 'soot-like' materials of large apparent molecular mass. 44 refs., 7 figs., 3 tabs.

Meat batter production in an extended vane pump-grinder injecting curing salt solutions to reduce energy requirements: variation of curing salt amount injected with the solution.

Science.gov (United States)

Irmscher, Stefan B; Terjung, Eva-Maria; Gibis, Monika; Herrmann, Kurt; Kohlus, Reinhard; Weiss, Jochen

2017-01-01

The integration of a nozzle in an extended vane pump-grinder system may enable the continuous injection of curing salt solutions during meat batter production. The purpose of this work was to examine the influence of the curing salt amount injected with the solution (0-100%) on protein solubilisation, water-binding, structure, colour and texture of emulsion-type sausages. The amount of myofibrillar protein solubilised during homogenisation varied slightly from 33 to 36 g kg -1 . Reddening was not noticeably impacted by the later addition of nitrite. L * ranged from 66.9 ± 0.3 to 67.8 ± 0.3, a * from 10.9 ± 0.1 to 11.2 ± 0.1 and b * from 7.7 ± 0.1 to 8.0 ± 0.1. Although softer sausages were produced when only water was injected, firmness increased with increasing curing salt amount injected and was similar to the control when the full amount of salt was used. The substitution of two-thirds of ice with a liquid brine may enable energy savings due to reduced power consumptions of the extended vane pump-grinder system by up to 23%. The injection of curing salt solutions is feasible without affecting structure and colour negatively. This constitutes a first step towards of an 'ice-free' meat batter production allowing for substantial energy savings due to lower comminution work. © 2016 Society of Chemical Industry. © 2016 Society of Chemical Industry.

Sample positioning in neutron diffraction experiments using a multi-material fiducial marker

Energy Technology Data Exchange (ETDEWEB)

Marais, D., E-mail: Deon.Marais@necsa.co.za [Research and Development Division, South African Nuclear Energy Corporation (Necsa) SOC Limited, PO Box 582, Pretoria 0001 (South Africa); School of Mechanical and Nuclear Engineering, North-West University, Potchefstroom 2520 (South Africa); Venter, A.M., E-mail: Andrew.Venter@necsa.co.za [Research and Development Division, South African Nuclear Energy Corporation (Necsa) SOC Limited, PO Box 582, Pretoria 0001 (South Africa); Faculty of Agriculture Science and Technology, North-West University, Mahikeng 2790 (South Africa); Markgraaff, J., E-mail: Johan.Markgraaff@nwu.ac.za [School of Mechanical and Nuclear Engineering, North-West University, Potchefstroom 2520 (South Africa); James, J., E-mail: Jon.James@open.ac.uk [Faculty of Mathematics, Computing and Technology, The Open University, Milton Keynes, MK76AA England (United Kingdom)

2017-01-01

An alternative sample positioning method is reported for use in conjunction with sample positioning and experiment planning software systems deployed on some neutron diffraction strain scanners. In this approach, the spherical fiducial markers and location trackers used with optical metrology hardware are replaced with a specifically designed multi-material fiducial marker that requires one diffraction measurement. In a blind setting, the marker position can be determined within an accuracy of ±164 µm with respect to the instrument gauge volume. The scheme is based on a pre-determined relationship that links the diffracted peak intensity to the absolute positioning of the fiducial marker with respect to the instrument gauge volume. Two methods for establishing the linking relationship are presented, respectively based on fitting multi-dimensional quadratic functions and a cross-correlation artificial neural network.

Sample sizing of biological materials analyzed by energy dispersion X-ray fluorescence

International Nuclear Information System (INIS)

Paiva, Jose D.S.; Franca, Elvis J.; Magalhaes, Marcelo R.L.; Almeida, Marcio E.S.; Hazin, Clovis A.

2013-01-01

Analytical portions used in chemical analyses are usually less than 1g. Errors resulting from the sampling are barely evaluated, since this type of study is a time-consuming procedure, with high costs for the chemical analysis of large number of samples. The energy dispersion X-ray fluorescence - EDXRF is a non-destructive and fast analytical technique with the possibility of determining several chemical elements. Therefore, the aim of this study was to provide information on the minimum analytical portion for quantification of chemical elements in biological matrices using EDXRF. Three species were sampled in mangroves from the Pernambuco, Brazil. Tree leaves were washed with distilled water, oven-dried at 60 deg C and milled until 0.5 mm particle size. Ten test-portions of approximately 500 mg for each species were transferred to vials sealed with polypropylene film. The quality of the analytical procedure was evaluated from the reference materials IAEA V10 Hay Powder, SRM 2976 Apple Leaves. After energy calibration, all samples were analyzed under vacuum for 100 seconds for each group of chemical elements. The voltage used was 15 kV and 50 kV for chemical elements of atomic number lower than 22 and the others, respectively. For the best analytical conditions, EDXRF was capable of estimating the sample size uncertainty for further determination of chemical elements in leaves. (author)

Sample sizing of biological materials analyzed by energy dispersion X-ray fluorescence

Energy Technology Data Exchange (ETDEWEB)

Paiva, Jose D.S.; Franca, Elvis J.; Magalhaes, Marcelo R.L.; Almeida, Marcio E.S.; Hazin, Clovis A., E-mail: dan-paiva@hotmail.com, E-mail: ejfranca@cnen.gov.br, E-mail: marcelo_rlm@hotmail.com, E-mail: maensoal@yahoo.com.br, E-mail: chazin@cnen.gov.b [Centro Regional de Ciencias Nucleares do Nordeste (CRCN-NE/CNEN-PE), Recife, PE (Brazil)

2013-07-01

Analytical portions used in chemical analyses are usually less than 1g. Errors resulting from the sampling are barely evaluated, since this type of study is a time-consuming procedure, with high costs for the chemical analysis of large number of samples. The energy dispersion X-ray fluorescence - EDXRF is a non-destructive and fast analytical technique with the possibility of determining several chemical elements. Therefore, the aim of this study was to provide information on the minimum analytical portion for quantification of chemical elements in biological matrices using EDXRF. Three species were sampled in mangroves from the Pernambuco, Brazil. Tree leaves were washed with distilled water, oven-dried at 60 deg C and milled until 0.5 mm particle size. Ten test-portions of approximately 500 mg for each species were transferred to vials sealed with polypropylene film. The quality of the analytical procedure was evaluated from the reference materials IAEA V10 Hay Powder, SRM 2976 Apple Leaves. After energy calibration, all samples were analyzed under vacuum for 100 seconds for each group of chemical elements. The voltage used was 15 kV and 50 kV for chemical elements of atomic number lower than 22 and the others, respectively. For the best analytical conditions, EDXRF was capable of estimating the sample size uncertainty for further determination of chemical elements in leaves. (author)

Design for a low temperature ion implantation and luminescence cryostat

International Nuclear Information System (INIS)

Noonan, J.R.; Kirkpatrick, C.G.; Myers, D.R.; Streetman, B.G.

1976-01-01

Several simple design changes of a conventional liquid helium optical Dewar can significantly improve the cryostat's versatility for use in low temperature particle irradiation. A bellows assembly provides precise sample positioning and allows convenient access for electrical connections. A heat exchanger consisting of thin walled tubing with a 'goose neck' bend provides a simple, effective means of cooling the sample as well as excellent thermal isolation of the sample holder from the coolant reservoir during controlled anneals. The addition of a vane-type vacuum valve, optical windows, and a rotatable tailpiece facilitates the study of optical properties of materials following low temperature ion implantation. (author)

Effects of Radial Gap Ratio between Impeller and Vaned Diffuser on Performance of Centrifugal Compressors

Directory of Open Access Journals (Sweden)

Mohammadjavad Hosseini

2017-07-01

Full Text Available A high-performance centrifugal compressor is needed for numerous industry applications nowadays. The radial gap ratio between the impeller and the diffuser vanes plays an important role in the improvement of the compressor performance. In this paper, the effects of the radial gap ratio on a high-pressure ratio centrifugal compressor are investigated using numerical simulations. The performance and the flow field are compared for six different radial gap ratios and five rotational speeds. The minimal radial gap ratio was 1.04 and the maximal was 1.14. Results showed that reducing the radial gap ratio decreases the choke mass flow rate. For the tip-speed Mach number (impeller inlet with Mu < 1, the pressure recovery and the loss coefficients are not sensitive to the radial gap ratio. However, for Mu ≥ 1, the best radial gap ratio is 1.08 for the pressure recovery and the loss coefficients. Furthermore, the impeller pressure ratio and efficiency are reduced by increasing the radial gap ratio. Finally, the compressor efficiency was compared for different radial gap ratios. For Mu < 1, the radial gap ratio does not have noticeable effects. In comparison, the radial gap ratio of 1.08 has the best performance for Mu ≥ 1.

Experimental evidence of the thermal effect of lubricating oil sprayed in sliding-vane air compressors

Directory of Open Access Journals (Sweden)

Gianluca Valenti

2014-11-01

Full Text Available A way to increase the efficiency of positive-displacement air compressor is spraying the lube oil to exploit it not only as lubricating and sealing agent but also as thermal ballast. This work seeks the experimental evidence in sliding-vane compressors by measuring the air standard volume flow rate and the electrical power input of three diverse configurations. The first configuration, taken as the reference, employs a conventional injection system comprising calibrated straight orifices. The other two, referred to as advanced, adopt smaller orifices and pressure-swirl full-cone nozzles designed for the purpose; the third configuration utilizes a pump to boost the oil pressure. The laser imagining technique shows that the nozzles generate sprays that break-up within a short distance into spherical droplets, ligaments, ramifications and undefined structures. Tests on the packaged compressors reveal that the advanced configurations provide almost the same air flow rate while utilizing half of the oil because the sprays generate a good sealing. Moreover, the sprayed oil is acting as a thermal ballast because the electrical input is reduced by 3.5% and 3.0%, respectively, if the pump is present or not , while the specific energy requirement, accounting for the slightly reduced air flow, by 2.4% and 2.9%, respectively.

Instrumental neutron activation analysis of rib bone samples and of bone reference materials

International Nuclear Information System (INIS)

Saiki, M.; Takata, M.K.; Kramarski, S.; Borelli, A.

2000-01-01

The instrumental neutron activation analysis method was used for the determination of trace elements in rib bone samples taken from autopsies of accident victims. The elements Br, Ca, Cl, Cr, Fe, Mg, Mn, Na, P, Sr, Rb and Zn were determined in cortical tissues by using short and long irradiations with thermal neutron flux of the IEA-R1m nuclear reactor. The reference materials NIST SRM 1400 Bone Ash and NIST SRM 1486 Bone Meal were also analyzed in order to evaluate the precision and the accuracy of the results. It was verified that lyophilization is the most convenient process for drying bone samples since it does not cause any element losses. Comparisons were made between the results obtained for rib samples and the literature values as well as between the results obtained for different ribs from a single individual and for bones from different individuals. (author)

Radon exhalation and its dependence on moisture content from samples of soil and building materials

International Nuclear Information System (INIS)

Faheem, Munazza; Matiullah

2008-01-01

Indoor radon has long been recognized as a potential health hazard for mankind. Building materials are considered as one of the major sources of radon in the indoor environment. To study radon exhalation rate and its dependence on moisture content, samples of soil and some common types of building materials (sand, cement, bricks and marble) were collected from Gujranwala, Gujrat, Hafizabad, Sialkot, Mandibahauddin and Narowal districts of the Punjab province (Pakistan). After processing, samples of 200 g each were placed in plastic vessels. CR-39 based NRPB detector were placed at the top of these vessels and were then hermetically sealed. After exposing to radon for 30 days within the closed vessels, the CR-39 detectors were processed. Radon exhalation rate was found to vary from 122±19 to 681±10mBqm -2 h -1 with an average of 376±147mBqm -2 h -1 in the soil samples whereas an average of 212±34, 195±25, 231±30 and 292±35mBqm -2 h -1 was observed in bricks, sand, cement and marble samples, respectively. Dependence of exhalation on moisture content has also been studied. Radon exhalation rate was found to increase with an increase in moisture, reached its maximum value and then decreased with further increase in the water content

TACT1- TRANSIENT THERMAL ANALYSIS OF A COOLED TURBINE BLADE OR VANE EQUIPPED WITH A COOLANT INSERT

Science.gov (United States)

Gaugler, R. E.

1994-01-01

As turbine-engine core operating conditions become more severe, designers must develop more effective means of cooling blades and vanes. In order to design reliable, cooled turbine blades, advanced transient thermal calculation techniques are required. The TACT1 computer program was developed to perform transient and steady-state heat-transfer and coolant-flow analyses for cooled blades, given the outside hot-gas boundary condition, the coolant inlet conditions, the geometry of the blade shell, and the cooling configuration. TACT1 can analyze turbine blades, or vanes, equipped with a central coolant-plenum insert from which coolant-air impinges on the inner surface of the blade shell. Coolant-side heat-transfer coefficients are calculated with the heat transfer mode at each station being user specified as either impingement with crossflow, forced convection channel flow, or forced convection over pin fins. A limited capability to handle film cooling is also available in the program. The TACT1 program solves for the blade temperature distribution using a transient energy equation for each node. The nodal energy balances are linearized, one-dimensional, heat-conduction equations which are applied at the wall-outer-surface node, at the junction of the cladding and the metal node, and at the wall-inner-surface node. At the mid-metal node a linear, three-dimensional, heat-conduction equation is used. Similarly, the coolant pressure distribution is determined by solving the set of transfer momentum equations for the one-dimensional flow between adjacent fluid nodes. In the coolant channel, energy and momentum equations for one-dimensional compressible flow, including friction and heat transfer, are used for the elemental channel length between two coolant nodes. The TACT1 program first obtains a steady-state solution using iterative calculations to obtain convergence of stable temperatures, pressures, coolant-flow split, and overall coolant mass balance. Transient

Mechanical considerations in cw linacs

International Nuclear Information System (INIS)

King, J.D.

1985-01-01

An 80-MHz radio-frequency quadrupole (RFQ) linac has been designed, fabricated and operated at 100% duty factor (cw) for the Fusion Materials Irradiation Test (FMIT) project at Los Alamos. This paper describes the design features, fabrication techniques, and operational problems of the device. The RFQ is an assembly of heavy steel, copper-plated weldments. It measures about 15 ft (4.5 m) long by 5 ft (1.5 m) in diameter and weighs over 12 t. Major components are two pair of diametrically orthogonal vanes mounted in a core cylinder. The core is assembled into a manifold cylinder that couples rf power into the vane quadrants. The design features discussed include assembly of hollow wall, flood-cooled components; high-conductivity rf seals; removable and adjustable vanes; and tuning devices. Fabrication challenges such as close-tolerance weldments, vane-tip-contour machining and large-component plating requirements are covered

Post-cast EDM method for reducing the thickness of a turbine nozzle wall

Science.gov (United States)

Jones, Raymond Joseph; Bojappa, Parvangada Ganapathy; Kirkpatrick, Francis Lawrence; Schotsch, Margaret Jones; Rajan, Rajiv; Wei, Bin

2002-01-01

A post-cast EDM process is used to remove material from the interior surface of a nozzle vane cavity of a turbine. A thin electrode is passed through the cavity between opposite ends of the nozzle vane and displaced along the interior nozzle wall to remove the material along a predetermined path, thus reducing the thickness of the wall between the cavity and the external surface of the nozzle. In another form, an EDM process employing a profile as an electrode is disposed in the cavity and advanced against the wall to remove material from the wall until the final wall thickness is achieved, with the interior wall surface being complementary to the profile surface.

Computational study: The influence of omni-directional guide vane on the flow pattern characteristic around Savonius wind turbine

Science.gov (United States)

Wicaksono, Yoga Arob; Tjahjana, D. D. D. P.

2017-01-01

Standart Savonius wind turbine have a low performance such as low coefficient of power and low coefficient of torque compared with another type of wind turbine. This phenomenon occurs because the wind stream can cause the negative pressure at the returning rotor. To solve this problem, standard Savonius combined with Omni Directional Guide Vane (ODGV) proposed. The aim of this research is to study the influence of ODGV on the flow pattern characteristic around of Savonius wind turbine. The numerical model is based on the Navier-Stokes equations with the standard k-ɛ turbulent model. This equation solved by a finite volume discretization method. This case was analyzed by commercial computational fluid dynamics solver such as SolidWorks Flow Simulations. Simulations were performed at the different wind directions; there are 0°, 30°,60° at 4 m/s wind speed. The numerical method validated with the past experimental data. The result indicated that the ODGV able to augment air flow to advancing rotor and decrease the negative pressure in the upstream of returning rotor compared to the bare Savonius wind turbine.

Preparation, melting behavior and thermal stability of poly(lactic acid)/poly(propylene carbonate) blends processed by vane extruder

Energy Technology Data Exchange (ETDEWEB)

Zou, Wei, E-mail: zw55624@163.com; Chen, Rongyuan; Zhang, Haichen; Qu, Jinping, E-mail: jpqu@scut.edu.cn [National Engineering Research Center of Novel Equipment for Polymer Processing, South China University of Technology, Guangzhou 510640 (China)

2016-03-09

Poly (lactic acid) (PLA)/Poly (propylene carbonate) (PPC) blends were prepared by vane extruder which is a type of novel polymer processing extruder based on elongation force field. Scanning electron microscope (SEM), differential scanning calorimetry (DSC) and thermogravimetric (TG) were used respectively to analyze the compatibility, the melting behavior and thermal stability properties of PLA/PPC blends affected by the different content of PPC. The results showed that with the increase of the PPC content, the glass transition temperature of PLA was reduced, and the glass transition temperature of PPC was increased, which indicated that PLA and PPC had partial compatibility. The cold crystallization temperature of PLA increased with the increase of the PPC content, which showed that PPC hindered the cold crystallization process of PLA. The addition of PPC had little impact on the melting process of PLA, and the melting temperature of PLA was almost kept the same value. Thermogravimetric analysis showed that the thermal stability of PPC was worse than that of PLA, the addition of PPC reduced the thermal stability of PLA.

Ion beam production with sub-milligram samples of material from an ECR source for AMS

Energy Technology Data Exchange (ETDEWEB)

Scott, R., E-mail: scott@phy.anl.gov; Palchan-Hazan, T.; Pardo, R.; Vondrasek, R. [Argonne Tandem Linac Accelerator System (ATLAS), Argonne National Laboratory, Lemont, Illinois 60439 (United States); Bauder, W. [Argonne Tandem Linac Accelerator System (ATLAS), Argonne National Laboratory, Lemont, Illinois 60439 (United States); Nuclear Structure Laboratory, University of Notre Dame, Notre Dame, Indiana 46556 (United States)

2016-02-15

Current accelerator mass spectrometry experiments at the Argonne Tandem Linac Accelerator System facility at Argonne National Laboratory push us to improve the ion source performance with a large number of samples and a need to minimize cross contamination. These experiments can require the creation of ion beams from as little as a few micrograms of material. These low concentration samples push the limit of our current efficiency and stability capabilities of the electron cyclotron resonance ion source. A combination of laser ablation and sputtering techniques coupled with a newly modified multi-sample changer has been used to meet this demand. We will discuss performance, stability, and consumption rates as well as planned improvements.

COMPATIBILITY OF NAPLS AND OTHER ORGANIC COMPOUNDS WITH MATERIALS UED IN WELL CONSTRUCTION, SAMPLING, AND REMEDIATION

Science.gov (United States)

Structural integrity of well construction, sampling, and remediation materials may be compromised at many hazardous sites by nonaqueous phase liquids (NAPLs) and their dissolved constituents. A literature review of compatibility theory and qualitative field experiences are provid...

Bonding of composites in different industries; Collage des composites dans diverses industries

Energy Technology Data Exchange (ETDEWEB)

Cognard, Ph. [societe Bostik Findley, La Defense 2, 92 (France)

2005-03-01

The walls of vanes of wind-mills are generally carried out in bonded sandwich materials. The interior tighteners can be bonded too to the exterior panels. For these bonding, epoxides or polyurethanes with two components hardening at ambient temperature, at high mechanical resistance and great durability are used. For the bonds of vanes on the turbine, the vanes are bonded on metallic rings with special epoxide adhesives, with two components, able to support high stresses, having a shear resistance of 30 MPa, a very good fatigue resistance for supporting a lot of turns under alternated bending stresses. These wind-mills have to support service temperature of -40 C to +80 C. (O.M.)

Effects of Sample and Indenter Configurations of Nanoindentation Experiment on the Mechanical Behavior and Properties of Ductile Materials

Directory of Open Access Journals (Sweden)

Seyed Saeid Rahimian Koloor

2018-06-01

Full Text Available The nanoindentation test is frequently used as an alternate method to obtain the mechanical properties of ductile materials. However, due to the lack of information about the effects of the sample and indenter physical configurations, the accuracy of the extracted material properties in nanoindentation tests requires further evaluation that has been considered in this study. In this respect, a demonstrator ductile material, aluminum 1100, was tested using the Triboscope nanoindenter system with the Berkovich indenter. A 3D finite element simulation of the nanoindentation test was developed and validated through exact prediction of the structural response with measured data. The validated model was then employed to examine the effects of various test configurations on the load–displacement response of the sample material. These parameters were the different indenter edge-tip radii, different indentation depths, different sample tilts, and different friction conditions between the indenter and the material surface. Within the range of the indenter edge-tip radii examined, the average elastic modulus and hardness were 78.34 ± 14.58 and 1.6 ± 0.24 GPa, respectively. The different indentation depths resulted in average values for the elastic modulus and hardness of 77.03 ± 6.54 and 1.58 ± 0.17 GPa, respectively. The uneven surface morphology, as described by the inclination of the local indentation plane, indicated an exponential increase in the extracted values of elastic modulus and hardness, ranging from 71.83 and 1.47 GPa (for the reference case, θ = 0° to 243.39 and 5.05 GPa at θ = 12°. The mechanical properties that were obtained through nanoindentation on the surface with 6° tilt or higher were outside the range for aluminum properties. The effect of friction on the resulting mechanical response and the properties of the material was negligible.

Transition Process from Diffuser Stall to Stage Stall in a Centrifugal Compressor with a Vaned Diffuser

Directory of Open Access Journals (Sweden)

Nobumichi Fujisawa

2017-01-01

Full Text Available The transition process from a diffuser rotating stall to a stage stall in a centrifugal compressor with a vaned diffuser was investigated by experimental and numerical analyses. From the velocity measurements, it was found that the rotating stall existed on the shroud side of the diffuser passage in the off-design flow condition. The numerical results revealed the typical vortical structure of the diffuser stall. The diffuser stall cell was caused by the systematic vortical structure which consisted of the tornado-type vortex, the longitudinal vortex at the shroud/suction surface corner (i.e., leading edge vortex (LEV, and the vortex in the throat area of the diffuser passages. Furthermore, the stage stall, which rotated within both the impeller and diffuser passages, occurred instead of the diffuser stall as the mass flow rate was decreased. According to the velocity measurements at the diffuser inlet, the diffuser stall which rotated on the shroud side was shifted to the hub side. Then, the diffuser stall moved into the impeller passages and formed the stage stall. Therefore, the stage stall was caused by the development of the diffuser stall, which transferred from the shroud side to the hub side in the vaneless space and expanded to the impeller passages.

Effect of physical, chemical and electro-kinetic properties of pumice samples on radiation shielding properties of pumice material

International Nuclear Information System (INIS)

Tapan, Mücip; Yalçın, Zeynel; İçelli, Orhan; Kara, Hüsnü; Orak, Salim; Özvan, Ali; Depci, Tolga

2014-01-01

Highlights: • Radiation shielding properties of pumice materials are studied. • The relationship between physical, chemical and electro-kinetic properties pumice samples is identified. • The photon atomic parameters are important for the absorber peculiarity of the pumices. - Abstract: Pumice has been used in cement, concrete, brick, and ceramic industries as an additive and aggregate material. In this study, some gamma-ray photon absorption parameters such as the total mass attenuation coefficients, effective atomic number and electronic density have been investigated for six different pumice samples. Numerous values of energy related parameters from low energy (1 keV) to high energy (100 MeV) were calculated using WinXCom programme. The relationship between radiation shielding properties of the pumice samples and their physical, chemical and electro-kinetic properties was evaluated using simple regression analysis. Simple regression analysis indicated a strong correlation between photon energy absorption parameters and density and SiO 2 , Fe 2 O 3 , CaO, MgO, TiO 2 content of pumice samples in this study. It is found that photon energy absorption parameters are not related to electro-kinetic properties of pumice samples

The design, simulation and testing of an urban vertical axis wind turbine with the omni-direction-guide-vane

International Nuclear Information System (INIS)

Chong, W.T.; Fazlizan, A.; Poh, S.C.; Pan, K.C.; Hew, W.P.; Hsiao, F.B.

2013-01-01

Graphical abstract: Solar energy, renewable energy, urban wind energy, environment, augmented wind turbine. Highlights: ► A system for on-site wind–solar hybrid power generation and rain water collection. ► The omni-direction-guide-vane (ODGV) overcomes the weak wind and turbulence conditions in urban areas. ► The ODGV improves the wind turbine performance by speeding-up and guiding the wind. ► The ODGV is designed to blend into the building architecture with safety enhancement. ► The wind tunnel test and CFD simulation results are presented. - Abstract: A novel omni-direction-guide-vane (ODGV) that surrounds a vertical axis wind turbine (VAWT) is designed to improve the wind turbine performance. Wind tunnel testing was performed to evaluate the performance of a 5-bladed (Wortmann FX63-137 airfoil) H-rotor wind turbine, with and without the integration of the ODGV. The test was conducted using a scaled model turbine which was constructed to simulate the VAWT enclosed by the ODGV placed on a building. The VAWT shows an improvement on its self-starting behavior where the cut-in speed was reduced with the integration of the ODGV. Since the VAWT is able to self-start at a lower wind speed, the working hour of the wind turbine would increase. At a wind speed of 6 m/s and under free-running condition (only rotor inertia and bearing friction were applied), the ODGV helps to increase the rotor rotational speed by 182%. With extra load application at the same wind speed (6 m/s), the wind turbine power output was increased by 3.48 times at its peak torque with the aid of the ODGV. The working concept of the ODGV is to minimize the negative torque zone of a lift-type VAWT and to reduce turbulence and rotational speed fluctuation. It was verified by re-simulating the torque coefficient data of a single bladed (NACA 0015 airfoil) VAWT published by the Sandia National Laboratories. From the simulation results, with the presence of the ODGV, it was shown that the

Lower-Conductivity Ceramic Materials for Thermal-Barrier Coatings

Science.gov (United States)

Bansal, Narottam P.; Zhu, Dongming

2006-01-01

Doped pyrochlore oxides of a type described below are under consideration as alternative materials for high-temperature thermal-barrier coatings (TBCs). In comparison with partially-yttria-stabilized zirconia (YSZ), which is the state-of-the-art TBC material now in commercial use, these doped pyrochlore oxides exhibit lower thermal conductivities, which could be exploited to obtain the following advantages: For a given difference in temperature between an outer coating surface and the coating/substrate interface, the coating could be thinner. Reductions in coating thicknesses could translate to reductions in weight of hot-section components of turbine engines (e.g., combustor liners, blades, and vanes) to which TBCs are typically applied. For a given coating thickness, the difference in temperature between the outer coating surface and the coating/substrate interface could be greater. For turbine engines, this could translate to higher operating temperatures, with consequent increases in efficiency and reductions in polluting emissions. TBCs are needed because the temperatures in some turbine-engine hot sections exceed the maximum temperatures that the substrate materials (superalloys, Si-based ceramics, and others) can withstand. YSZ TBCs are applied to engine components as thin layers by plasma spraying or electron-beam physical vapor deposition. During operation at higher temperatures, YSZ layers undergo sintering, which increases their thermal conductivities and thereby renders them less effective as TBCs. Moreover, the sintered YSZ TBCs are less tolerant of stress and strain and, hence, are less durable.

LHS (latin hypercubes) sampling of the material properties of steels for the analysis of the global sensitivity in welding numerical simulation

International Nuclear Information System (INIS)

Petelet, Matthieu; Asserin, Olivier; Iooss, Bertrand; Petelet, Matthieu; Loredo, Alexandre

2006-01-01

In this work, the method of sensitivity analysis allowing to identify the inlet data the most influential on the variability of the responses (residual stresses and distortions). Classically, the sensitivity analysis is carried out locally what limits its validity domain to a given material. A global sensitivity analysis method is proposed; it allows to cover a material domain as wide as those of the steels series. A probabilistic modeling giving the variability of the material parameters in the steels series is proposed. The original aspect of this work consists in the use of the sampling method by latin hypercubes (LHS) of the material parameters which forms the inlet data (dependent of temperature) of the numerical simulations. Thus, a statistical approach has been applied to the welding numerical simulation: LHS sampling of the material properties, global sensitivity analysis what has allowed the reduction of the material parameterization. (O.M.)

GROUND WATER ISSUE: NONAQUEOUS PHASE LIQUIDS COMPATIBILITY WITH MATERIALS USED IN WELL CONSTRUCTION, SAMPLING, AND REMEDIATION.

Science.gov (United States)

This issue paper provides a comprehensive literature review regarding the compatibility of NAPLs with a wide variety of materials used at hazardous waste sites. A condensed reference table of compatibility data for 207 chemicals and 28 commonly used well construction and sampling...

Laser Scribed Graphene Biosensor for Detection of Biogenic Amines in Food Samples Using Locally Sourced Materials

Directory of Open Access Journals (Sweden)

Diana C. Vanegas

2018-04-01

Full Text Available In foods, high levels of biogenic amines (BA are the result of microbial metabolism that could be affected by temperatures and storage conditions. Thus, the level of BA is commonly used as an indicator of food safety and quality. This manuscript outlines the development of laser scribed graphene electrodes, with locally sourced materials, for reagent-free food safety biosensing. To fabricate the biosensors, the graphene surface was functionalized with copper microparticles and diamine oxidase, purchased from a local supermarket; and then compared to biosensors fabricated with analytical grade materials. The amperometric biosensor exhibits good electrochemical performance, with an average histamine sensitivity of 23.3 µA/mM, a lower detection limit of 11.6 µM, and a response time of 7.3 s, showing similar performance to biosensors constructed from analytical grade materials. We demonstrated the application of the biosensor by testing total BA concentration in fish paste samples subjected to fermentation with lactic acid bacteria. Biogenic amines concentrations prior to lactic acid fermentation were below the detection limit of the biosensor, while concentration after fermentation was 19.24 ± 8.21 mg histamine/kg, confirming that the sensor was selective in a complex food matrix. The low-cost, rapid, and accurate device is a promising tool for biogenic amine estimation in food samples, particularly in situations where standard laboratory techniques are unavailable, or are cost prohibitive. This biosensor can be used for screening food samples, potentially limiting food waste, while reducing chances of foodborne outbreaks.

IAEA Sampling Plan

Energy Technology Data Exchange (ETDEWEB)

Geist, William H. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2017-09-15

The objectives for this presentation are to describe the method that the IAEA uses to determine a sampling plan for nuclear material measurements; describe the terms detection probability and significant quantity; list the three nuclear materials measurement types; describe the sampling method applied to an item facility; and describe multiple method sampling.

Dose computation of Ti activated products for its qualification as a material for the sample holder in FBTR

International Nuclear Information System (INIS)

Ashok Kumar, G.V.S.; Kumar, R.; Venkatasubramani, C.R.; Acharya, R.; Reddy, A.V.R.

2014-01-01

Development of a Fast flux experimental facility with a sample holder facility in FBTR has been envisaged to carry out the studies on i) fast neutron activation analysis and ii) fission studies. This paper describes the facility in detail and dose computations that are to be generated due to long irradiation of the material of the sample holder i.e. titanium. (author)

ALLUVIAL DEPOSITS AS A SUBSOIL AND MATERIAL FOR BASIC HYDRO-TECHNICAL CONSTRUCTIONS

Directory of Open Access Journals (Sweden)

Jędrzej Wierzbicki

2015-11-01

Full Text Available The article presents an analysis of geotechnical parameters of the alluvial deposit (the areas of the Vistula and Warta river valleys with a view to using the soil as an earth construction material and as a foundation for buildings constructed on the grounds tested. Strength and deformation parameters of the subsoil tested were identified by the CPTU (cone penetration test and DMT (flat dilatometer test methods, as well as by the vane test (VT. The article includes the analysis of overconsolidation process of the soil tested and a formula for the identification of the overconsolidation ratio OCR. Equation 4 reflects the relation between the undrained shear strength and plasticity of the silts analyzed and the OCR value. The analysis resulted in the determination of the Nkt coefficient, which might be used to identify the undrained shear strength of both sediments tested. On the basis of a detailed analysis of changes in terms of the constrained oedometric modulus M0, the relations between the said modulus, the liquidity index and the OCR value were identified. Mayne’s formula (1995 was used to determine the M0 modulus from the CPTU test. The usefulness of the alluvial deposit as an earth construction material was analysed after their structure had been destroyed and compacted with a Proctor apparatus. In cases of samples characterized by different water content and soil particle density, the analysis of changes in terms of cohesion and the internal friction angle proved that these parameters are influenced by the soil phase composition. On the basis of the tests, it was concluded that the most desirable shear strength parameters are achieved when the silt is compacted below the optimum water content.

Solid phase speciation of arsenic by sequential extraction in standard reference materials and industrially contaminated soil samples

International Nuclear Information System (INIS)

Herreweghe, Samuel van; Swennen, Rudy; Vandecasteele, Carlo; Cappuyns, Valerie

2003-01-01

Leaching experiments, a mineralogical survey and larger samples are preferred when arsenic is present as discrete mineral phases. - Availability, mobility, (phyto)toxicity and potential risk of contaminants is strongly affected by the manner of appearance of elements, the so-called speciation. Operational fractionation methods like sequential extractions have been applied for a long time to determine the solid phase speciation of heavy metals since direct determination of specific chemical compounds can not always be easily achieved. The three-step sequential extraction scheme recommended by the BCR and two extraction schemes based on the phosphorus-like protocol proposed by Manful (1992, Occurrence and Ecochemical Behaviours of Arsenic in a Goldsmelter Impacted Area in Ghana, PhD dissertation, at the RUG) were applied to four standard reference materials (SRM) and to a batch of samples from industrially contaminated sites, heavily contaminated with arsenic and heavy metals. The SRM 2710 (Montana soil) was found to be the most useful reference material for metal (Mn, Cu, Zn, As, Cd and Pb) fractionation using the BCR sequential extraction procedure. Two sequential extraction schemes were developed and compared for arsenic with the aim to establish a better fractionation and recovery rate than the BCR-scheme for this element in the SRM samples. The major part of arsenic was released from the heavily contaminated samples after NaOH-extraction. Inferior extraction variability and recovery in the heavily contaminated samples compared to SRMs could be mainly contributed to subsample heterogeneity

Cavitation on a scaled-down model of a Francis turbine guide vane: high-speed imaging and PIV measurements

Science.gov (United States)

Pervunin, K. S.; Timoshevskiy, M. V.; Churkin, S. A.; Kravtsova, A. Yu; Markovich, D. M.; Hanjalić, K.

2015-12-01

Cavitation on two symmetric foils, a NACA0015 hydrofoil and a scaled-down model of a Francis turbine guide vane (GV), was investigated by high-speed visualization and PIV. At small attack angles the differences between the profiles of the mean and fluctuating velocities for both hydrofoils were shown to be insignificant. However, at the higher angle of incidence, flow separation from the GV surface was discovered for quasi-steady regimes including cavitation-free and cavitation inception cases. The flow separation leads to the appearance of a second maximum in velocity fluctuations distributions downstream far from the GV surface. When the transition to unsteady regimes occurred, the velocity distributions became quite similar for both foils. Additionally, for the GV an unsteady regime characterized by asymmetric spanwise variations of the sheet cavity length along with alternating periodic detachments of clouds between the sidewalls of the test channel was for the first time visualized. This asymmetric behaviour is very likely to be governed by the cross instability that was recently described by Decaix and Goncalvès [8]. Moreover, it was concluded that the existence of the cross instability is independent on the test body shape and its aspect ratio.

Theoretical study of a novel refrigeration compressor - Part II: Performance of a rotating discharge valve in the revolving vane (RV) compressor

Energy Technology Data Exchange (ETDEWEB)

Teh, Y.L.; Ooi, K.T. [Thermal and Fluids Engineering Division, School of Mechanical and Aerospace Engineering, Nanyang Technological University, 50 Nanyang Avenue, S639798 (Singapore); Djamari, D. Wibowo [Engineering Mechanics Division, School of Mechanical and Aerospace Engineering, Nanyang Technological University, 50 Nanyang Avenue, S639798 (Singapore)

2009-08-15

A new refrigeration compressor, named 'Revolving Vane (RV) compressor', has been introduced in Part I of this paper series. For a first time in refrigeration compressors, a rotating discharge valve is employed in the RV compressor mainly due to the rotation of the entire cylinder. This paper presents a theoretical investigation on the dynamic behavior of a reed-type discharge valve undergoing rotatory motion, with the primary objective of elucidating the applicability of such valves in refrigeration compressors. Under the application of the Euler-Bernoulli beam theory, a mathematical model of the rotating valve is formulated and the transient response of the valve under centrifugal loads in addition to pressure forces is analyzed. Results have shown that under careful design considerations, the performance as well as the reliability of the rotating discharge valve can be enhanced as compared to a non-rotating valve that has been used in all refrigeration compressors currently. (author)

Radiator Enhanced Geothermal System - A Revolutionary Method for Extracting Geothermal Energy

Science.gov (United States)

Karimi, S.; Marsh, B. D.; Hilpert, M.

2017-12-01

A new method of extracting geothermal energy, the Radiator Enhanced Geothermal System (RAD-EGS) has been developed. RAD-EGS attempts to mimic natural hydrothermal systems by 1) generating a vertical vane of artificially produced high porosity/permeability material deep in a hot sedimentary aquifer, 2) injecting water at surface temperatures to the bottom of the vane, where the rock is the hottest, 3) extracting super-heated water at the top of the vane. The novel RAD-EGS differs greatly from the currently available Enhanced Geothermal Systems in vane orientation, determined in the governing local crustal stress field by Shmax and Sl (meaning it is vertical), and in the vane location in a hot sedimentary aquifer, which naturally increases the longevity of the system. In this study, we explore several parameters regimes affecting the water temperature in the extraction well, keeping in mind that the minimum temperature of the extracted water has to be 150 °C in order for a geothermal system to be commercially viable. We used the COMSOL finite element package to simulate coupled heat and fluid transfer within the RAD-EGS model. The following geologic layers from top to bottom are accounted for in the model: i) confining upper layer, ii) hot sedimentary aquifer, and iii) underlying basement rock. The vane is placed vertically within the sedimentary aquifer. An injection well and an extraction well are also included in the simulation. We tested the model for a wide range of various parameters including background heat flux, thickness of geologic layers, geometric properties of the vane, diameter and location of the wells, fluid flow within the wells, regional hydraulic gradient, and permeability and porosity of the layers. The results show that among the aforementioned parameters, background heat flux and the depth of vane emplacement are highly significant in determining the level of commercial viability of the geothermal system. These results indicate that for the

Rotationally Adaptive Flight Test Surface

Science.gov (United States)

Barrett, Ron

1999-01-01

Research on a new design of flutter exciter vane using adaptive materials was conducted. This novel design is based on all-moving aerodynamic surface technology and consists of a structurally stiff main spar, a series of piezoelectric actuator elements and an aerodynamic shell which is pivoted around the main spar. The work was built upon the current missile-type all-moving surface designs and change them so they are better suited for flutter excitation through the transonic flight regime. The first portion of research will be centered on aerodynamic and structural modeling of the system. USAF DatCom and vortex lattice codes was used to capture the fundamental aerodynamics of the vane. Finite element codes and laminated plate theory and virtual work analyses will be used to structurally model the aerodynamic vane and wing tip. Following the basic modeling, a flutter test vane was designed. Each component within the structure was designed to meet the design loads. After the design loads are met, then the deflections will be maximized and the internal structure will be laid out. In addition to the structure, a basic electrical control network will be designed which will be capable of driving a scaled exciter vane. The third and final stage of main investigation involved the fabrication of a 1/4 scale vane. This scaled vane was used to verify kinematics and structural mechanics theories on all-moving actuation. Following assembly, a series of bench tests was conducted to determine frequency response, electrical characteristics, mechanical and kinematic properties. Test results indicate peak-to-peak deflections of 1.1 deg with a corner frequency of just over 130 Hz.

W-Band Transmission MeasurementS and X-Band Dielectric Properties Measurements for a Radome Material Sample

Science.gov (United States)

Cravey, Robin L.; Tiemsin, Pacita I.

1997-01-01

This paper describes measurements which were performed on a sample of radome material in the Electromagnetic Properties Measurements Laboratory (EPML). The purpose of the measurements described in this paper was to determine the one-way transmission loss through the flat panel of radome material for a frequency range of 84 to 94 GHz, for varying incidence angles. The panel, which was manufactured by Norton Performance Plastics Corporation, was provided to the EPML by TRW. The size of the panel is 40 in x 36 in x 0.422 in and consists of a foam material with one side coated with a smooth white coating (this side will be referred to as the front side). The dielectric properties of the foam material from the inside of the panel were also determined at X-band (8.2-12.4 GHz). The W-band free space measurements are presented first, followed by the X-band dielectric properties measurements.

Urine sample collection protocols for bioassay samples

Energy Technology Data Exchange (ETDEWEB)

MacLellan, J.A.; McFadden, K.M.

1992-11-01

In vitro radiobioassay analyses are used to measure the amount of radioactive material excreted by personnel exposed to the potential intake of radioactive material. The analytical results are then used with various metabolic models to estimate the amount of radioactive material in the subject`s body and the original intake of radioactive material. Proper application of these metabolic models requires knowledge of the excretion period. It is normal practice to design the bioassay program based on a 24-hour excretion sample. The Hanford bioassay program simulates a total 24-hour urine excretion sample with urine collection periods lasting from one-half hour before retiring to one-half hour after rising on two consecutive days. Urine passed during the specified periods is collected in three 1-L bottles. Because the daily excretion volume given in Publication 23 of the International Commission on Radiological Protection (ICRP 1975, p. 354) for Reference Man is 1.4 L, it was proposed to use only two 1-L bottles as a cost-saving measure. This raised the broader question of what should be the design capacity of a 24-hour urine sample kit.

Urine sample collection protocols for bioassay samples

Energy Technology Data Exchange (ETDEWEB)

MacLellan, J.A.; McFadden, K.M.

1992-11-01

In vitro radiobioassay analyses are used to measure the amount of radioactive material excreted by personnel exposed to the potential intake of radioactive material. The analytical results are then used with various metabolic models to estimate the amount of radioactive material in the subject's body and the original intake of radioactive material. Proper application of these metabolic models requires knowledge of the excretion period. It is normal practice to design the bioassay program based on a 24-hour excretion sample. The Hanford bioassay program simulates a total 24-hour urine excretion sample with urine collection periods lasting from one-half hour before retiring to one-half hour after rising on two consecutive days. Urine passed during the specified periods is collected in three 1-L bottles. Because the daily excretion volume given in Publication 23 of the International Commission on Radiological Protection (ICRP 1975, p. 354) for Reference Man is 1.4 L, it was proposed to use only two 1-L bottles as a cost-saving measure. This raised the broader question of what should be the design capacity of a 24-hour urine sample kit.

Acoustic Performance of Novel Fan Noise Reduction Technologies for a High Bypass Model Turbofan at Simulated Flights Conditions

Science.gov (United States)

Elliott, David M.; Woodward, Richard P.; Podboy, Gary G.

2010-01-01

Two novel fan noise reduction technologies, over the rotor acoustic treatment and soft stator vane technologies, were tested in an ultra-high bypass ratio turbofan model in the NASA Glenn Research Center s 9- by 15-Foot Low-Speed Wind Tunnel. The performance of these technologies was compared to that of the baseline fan configuration, which did not have these technologies. Sideline acoustic data and hot film flow data were acquired and are used to determine the effectiveness of the various treatments. The material used for the over the rotor treatment was foam metal and two different types were used. The soft stator vanes had several internal cavities tuned to target certain frequencies. In order to accommodate the cavities it was necessary to use a cut-on stator to demonstrate the soft vane concept.

Inalienably Yours? The new case for an inalienable property right in human biological material: Empowerment of sample donors or a recipe for a tragic Anti-Commons?

Directory of Open Access Journals (Sweden)

Jasper A. Bovenberg

2004-12-01

Full Text Available Modern biomedical research into the genetic component of common diseases calls for broad access to existing and novel collections of samples of human biological material, aka Biobanks. Groups of donors of these samples, however, increasingly claim a property right in their samples. They perceive the recognition of a personal property right in their biological material as the best means to serve two goals: to secure ongoing control over their samples after donation and to underpin their claim for a share in the proceeds that the research on their samples may yield. Given the objective of ensuring ongoing control, this property right is claimed to be inalienable. Recognition of a personal property right in one’s biological material is problematic, especially where the requirement of inalienability seems at odds with the claim for a share of the profits. Yet, property rights in human biological material may be justified in a certain context, e.g. to enable subsets of patients to negotiate the terms and conditions of the research into their specific disorders. Biobanks, however, contain so many samples, which can be used for so many research purposes, that the unrestricted exercise of personal property rights by the sample donors will lead to a proliferation of rights. This proliferation is likely to deter or slow down both the creation of de novo Biobanks and the use of existing sample collections. Thus, recognising inalienable property rights in human biological material may lead to suboptimal use of these resources and create a classic ‘anticommons property’ scenario. It would also undermine the current trend to simplify existing informed consent requirements which aims to facilitate broad and previously unanticipated research on de novo and existing Biobanks. In addition, the tradition of altruistic participation in research and the notion that large-scale collections of human biological material are global public goods are arguments against

Materials Discovery | Materials Science | NREL

Science.gov (United States)

Discovery Materials Discovery Images of red and yellow particles NREL's research in materials characterization of sample by incoming beam and measuring outgoing particles, with data being stored and analyzed Staff Scientist Dr. Zakutayev specializes in design of novel semiconductor materials for energy

Thermal analysis of the APT materials irradiation samples

International Nuclear Information System (INIS)

Maloy, S.A.; Willcutt, G.J.; James, M.R.; Teague, J.; Diebe, D.A.; Sommer, W.F.; Ferguson, P.D.

1998-01-01

The accelerator production of tritium (APT) project proposes to use a 1.7 GeV, 100 mA proton beam to produce neutrons from an Inconel 718 clad tungsten target. The neutrons are multiplied and moderated in a lead/water blanket before being captured in He 3 to form tritium. In this process, the materials in the target and blanket region are exposed to a wide range of different fluxes comprised of protons and neutrons with energies into the GeV range. To investigate the effect of irradiation on the mechanical properties of candidate APT materials (Inconel 718, 316L stainless steel, Al 6061-T6, Mod 9Cr-1Mo, 304L stainless steel and Al5052-0), the APT Engineering Design and Development group fielded an extensive materials irradiation using the LANSCE (Los Alamos Neutron Science Center) accelerator, which operates at an energy of 800 MeV and a current of 1 mA. The test set-up was designed to place mechanical test specimens in locations in and near the proton beam where the environment of proton and neutron fluxes and temperatures are prototypic to those expected in the APT target/blanket (50--170 C). After irradiating for about 3,600 hours, the maximum achieved proton fluence was 4--5 x 10 21 p/cm 2 for the materials in the center of the beam. To obtain relevant data on the change in the mechanical properties with fluence, it is essential to know the temperature at which the materials were irradiated. This paper explains the method of determining the specimen temperature and reports some specific examples

Sample Curation in Support of the OSIRIS-REx Asteroid Sample Return Mission

Science.gov (United States)

Righter, Kevin; Nakamura-Messenger, Keiko

2017-01-01

The OSIRIS-REx asteroid sample return mission launched to asteroid Bennu Sept. 8, 2016. The spacecraft will arrive at Bennu in late 2019, orbit and map the asteroid, and perform a touch and go (TAG) sampling maneuver in July 2020. After sample is stowed and confirmed the spacecraft will return to Earth, and the sample return capsule (SRC) will land in Utah in September 2023. Samples will be recovered from Utah [2] and then transported and stored in a new sample cleanroom at NASA Johnson Space Center in Houston [3]. The materials curated for the mission are described here. a) Materials Archive and Witness Plate Collection: The SRC and TAGSAM were built between March 2014 and Summer of 2015, and instruments (OTES,OVIRS, OLA, OCAMS, REXIS) were integrated from Summer 2015 until May 2016. A total of 395 items were received for the materials archive at NASA-JSC, with archiving finishing 30 days after launch (with the final archived items being related to launch operations)[4]. The materials fall into several general categories including metals (stainless steel, aluminum, titanium alloys, brass and BeCu alloy), epoxies, paints, polymers, lubricants, non-volatile-residue samples (NVR), sapphire, and various miscellaneous materials. All through the ATLO process (from March 2015 until late August 2016) contamination knowledge witness plates (Si wafer and Al foil) were deployed in the various cleanrooms in Denver and KSC to provide an additional record of particle counts and volatiles that is archived for current and future scientific studies. These plates were deployed in roughly monthly increments with each unit containing 4 Si wafers and 4 Al foils. We archived 128 individual witness plates (64 Si wafers and 64 Al foils); one of each witness plate (Si and Al) was analyzed immediately by the science team after archiving, while the remaining 3 of each are archived indefinitely. Information about each material archived is stored in an extensive database at NASA-JSC, and key

Improvement of the efficiency of the Agnew micro hydro turbine at part loads due to installing guide vanes mechanism

Energy Technology Data Exchange (ETDEWEB)

Yassi, Yousef; hashemloo, Safar [Iranian Research Organization for Science and Technology (IROST), No. 29 Forssat St., Enghelaab Ave., Tehran (Iran)

2010-10-15

Agnew turbine is an axial micro hydro of Kaplan type, with its main shaft subtending 45 to the line of horizon. Due to governmental power generating programs for limited hydro potentials in Iran and on the basis of a joint project between the University of Glasgow and the Iranian Research Organization for Science and Technology (IROST), the turbine was developed to operate under low heads and limited flow potentials in Iran. However the turbine was originally designed to operate without any guide vanes and test results showed that the turbine achieved an efficiency of 62% at its best point of performance. Later a modified Agnew turbine, consisting of a guide blades mechanism was designed and manufactured, at (IROST). The mechanism was so designed that it was also used as a second support for the turbine's main shaft. The standard turbine tests proved that; the modified version of the Agnew turbine had 23% higher efficiency at its best performance point; compared to the original design. Then the effects of the improvements on the turbine were studied on the performance of the turbine at part loads. However, efficiency improvements were observed under all part load conditions. (author)

Improvement of the efficiency of the Agnew micro hydro turbine at part loads due to installing guide vanes mechanism

International Nuclear Information System (INIS)

Yassi, Yousef; Hashemloo, Safar

2010-01-01

Agnew turbine is an axial micro hydro of Kaplan type, with its main shaft subtending 45 deg. to the line of horizon. Due to governmental power generating programs for limited hydro potentials in Iran and on the basis of a joint project between the University of Glasgow and the Iranian Research Organization for Science and Technology (IROST), the turbine was developed to operate under low heads and limited flow potentials in Iran. However the turbine was originally designed to operate without any guide vanes and test results showed that the turbine achieved an efficiency of 62% at its best point of performance. Later a modified Agnew turbine, consisting of a guide blades mechanism was designed and manufactured, at (IROST). The mechanism was so designed that it was also used as a second support for the turbine's main shaft. The standard turbine tests proved that; the modified version of the Agnew turbine had 23% higher efficiency at its best performance point; compared to the original design. Then the effects of the improvements on the turbine were studied on the performance of the turbine at part loads. However, efficiency improvements were observed under all part load conditions.

Certified reference material for radionuclides in fish flesh sample IAEA-414 (mixed fish from the Irish Sea and North Sea)

DEFF Research Database (Denmark)

Pham, M.K.; Sanchez-Cabeza, J.A.; Povinec, P.P.

2006-01-01

A certified reference material (CRM) for radionuclides in fish sample IAEA-414 (mixed fish from the Irish Sea and North Seas) is described and the results of the certification process are presented. Nine radionuclides (K-40, Cs-137, Th-232, U-234, U-235, U-238, Pu-238, Pu239+240 and Am-241) were...... ratios are also included. The CRM can be used for quality assurance/quality control of the analysis of radionuclides in fish sample, for the development and validation of analytical methods and for training purposes. The material is available from IAEA, Vienna, in 100 g units. (c) 2006 Elsevier Ltd. All...

Advanced Joining of Aerospace Metallic Materials.

Science.gov (United States)

1986-07-01

REPAIRED F100 TURBINE VANES tUNDER SIMULATED) SERVICE. CONDI rIONS by A.,I.A.Mom. N.M.Madhava. G.A.KooI and M.IDean 21 REPAIR TECHNIQU ES FOR GAS lII... vapeurs d~gag~es par la decomposition des corps exog~nes. POe) Les cavi t~s (cavit)(fgr4, sont le propre du soudage des fortes paisseurs. Ellas...the most practical information with respect to mechanical properties for gas turbine applications. Generally, sound laser welds (i.e. free from

Sample preparation

International Nuclear Information System (INIS)

Anon.

1992-01-01

Sample preparation prior to HPLC analysis is certainly one of the most important steps to consider in trace or ultratrace analysis. For many years scientists have tried to simplify the sample preparation process. It is rarely possible to inject a neat liquid sample or a sample where preparation may not be any more complex than dissolution of the sample in a given solvent. The last process alone can remove insoluble materials, which is especially helpful with the samples in complex matrices if other interactions do not affect extraction. Here, it is very likely a large number of components will not dissolve and are, therefore, eliminated by a simple filtration process. In most cases, the process of sample preparation is not as simple as dissolution of the component interest. At times, enrichment is necessary, that is, the component of interest is present in very large volume or mass of material. It needs to be concentrated in some manner so a small volume of the concentrated or enriched sample can be injected into HPLC. 88 refs

Neutron multicounter detector for investigation of content and spatial distribution of fission materials in large volume samples

International Nuclear Information System (INIS)

Swiderska-Kowalczyk, M.; Starosta, W.; Zoltowski, T.

1998-01-01

The experimental device is a neutron coincidence well counter. It can be applied for passive assay of fissile - especially for plutonium bearing - materials. It consist of a set of 3 He tubes placed inside a polyethylene moderator; outputs from the tubes, first processed by preamplifier/amplifier/discriminator circuits, are then analysed using neutron correlator connected with a PC, and correlation techniques implemented in software. Such a neutron counter allows for determination of plutonium mass ( 240 Pu effective mass) in nonmultiplying samples having fairly big volume (up to 0.14 m 3 ). For determination of neutron sources distribution inside the sample, the heuristic methods based on hierarchical cluster analysis are applied. As an input parameters, amplitudes and phases of two-dimensional Fourier transformation of the count profiles matrices for known point sources distributions and for the examined samples, are taken. Such matrices are collected by means of sample scanning by detection head. During clustering process, counts profiles for unknown samples fitted into dendrograms using the 'proximity' criterion of the examined sample profile to standard samples profiles. Distribution of neutron sources in an examined sample is then evaluated on the basis of comparison with standard sources distributions. (author)

Multicounter neutron detector for examination of content and spatial distribution of fissile materials in bulk samples

International Nuclear Information System (INIS)

Swiderska-Kowalczyk, M.; Starosta, W.; Zoltowski, T.

1999-01-01

A new neutron coincidence well-counter is presented. This experimental device can be applied for passive assay of fissile and, in particular, for plutonium bearing materials. It contains of a set of the 3 He tubes placed inside a polyethylene moderator. Outputs from the tubes, first processed by preamplifier/amplifier/discriminator circuits, are then analysed using a correlator connected with PC, and correlation techniques implemented in software. Such a neutron counter enables determination of the 240 Pu effective mass in samples of a small Pu content (i.e., where the multiplication effects can be neglected) having a fairly big volume (up to 0.17 m 3 ), if only the isotopic composition is known. For determination of neutron sources distribution inside a sample, a heuristic method based on hierarchical cluster analysis was applied. As input parameters, amplitudes and phases of two-dimensional Fourier transformation of the count profiles matrices for known point sources distributions and for the examined samples were taken. Such matrices of profiles counts are collected using the sample scanning with detection head. In the clustering processes, process, counts profiles of unknown samples are fitted into dendrograms employing the 'proximity' criterion of the examined sample profile to standard samples profiles. Distribution of neutron sources in the examined sample is then evaluated on the basis of a comparison with standard sources distributions. (author)

Air sampling in the workplace

International Nuclear Information System (INIS)

Hickey, E.E.; Stoetzel, G.A.; Strom, D.J.; Cicotte, G.R.; Wiblin, C.M.; McGuire, S.A.

1993-09-01

This report provides technical information on air sampling that will be useful for facilities following the recommendations in the NRC's Regulatory Guide 8.25, Revision 1, ''Air sampling in the Workplace.'' That guide addresses air sampling to meet the requirements in NRC's regulations on radiation protection, 10 CFR Part 20. This report describes how to determine the need for air sampling based on the amount of material in process modified by the type of material, release potential, and confinement of the material. The purposes of air sampling and how the purposes affect the types of air sampling provided are discussed. The report discusses how to locate air samplers to accurately determine the concentrations of airborne radioactive materials that workers will be exposed to. The need for and the methods of performing airflow pattern studies to improve the accuracy of air sampling results are included. The report presents and gives examples of several techniques that can be used to evaluate whether the airborne concentrations of material are representative of the air inhaled by workers. Methods to adjust derived air concentrations for particle size are described. Methods to calibrate for volume of air sampled and estimate the uncertainty in the volume of air sampled are described. Statistical tests for determining minimum detectable concentrations are presented. How to perform an annual evaluation of the adequacy of the air sampling is also discussed

Simulation of performance of centrifugal circulators with vane-less diffuser for GCR applications - HTR2008-58166

International Nuclear Information System (INIS)

Tauveron, N.

2008-01-01

In the frame of the international forum Gen lV, CEA has selected various innovative concepts of Gas cooled Nuclear Reactor. Among them, an indirect-cycle gas reactor is under consideration. Thermal hydraulic performances are a key issue for the design. For transient conditions and decay heat removal situations, the thermal hydraulic performance must remain as high as possible. In this context, all the transient situations, the incidental and accidental scenarios must be evaluated by a validated sys-tem code able to correctly describe, in particular, the thermal-hydraulics of the whole plant. As concepts use a helium compressor to maintain the flow in the core, a special emphasis must be laid on compressor modelling. Centrifugal circulators with a vane-less diffuser have significant properties in term of simplicity, cost, ability to operate over a wide range of conditions. The objective of this paper is to present a dedicated description of centrifugal compressor, based on a one dimensional approach. This type of model requires various correlations as input data. The present contribution consists in establishing and validating the numerical simulations (including different sets of correlations) by comparison with representative experimental data. The results obtained show a qualitatively correct behaviour of the model compared to open literature cases of the gas turbine aircraft community and helium circulators of High Temperature Gas Reactors. Further work on modelling and validation are nevertheless needed to have a better confidence in the simulation predictions. (authors)

Fiscal 1999 achievement report on research and development of industrial technology of new industry creation type. Research and development of intelligent material and structural system (Development of energy use rationalization technology); 1999 nendo chiteki zairyo kozo system no kenkyu kaihatsu seika hokokusho. Energy shiyo gorika gijutsu kaihatsu

Energy Technology Data Exchange (ETDEWEB)

NONE

2000-03-01

Fiber or foil shaped sensor materials and actuator devices were integrated with composite materials and composite material structures for processing and controlling information, and then studies were conducted about materials and structural systems for enabling real-time detection of damage in materials and structures, examination of soundness, control of noise and vibration, and the like. Concerning optical fiber sensors in the development of smart manufacturing technologies, the impact imposed on composite materials by sensors embedded therein was investigated, and the scope of their applicability was determined. In the development of actuator materials and devices, ceramic actuators were fabricated by microwave sintering, and it was found that they were higher in performance by 30% than actuators of the conventional design. In the testing of demonstrators, molded body monitor basic tests using optical fiber sensors were conducted for jet engine static vane models, and temperature dependence of optical intensity was understood. (NEDO)

Application of direct solid sample analysis for the determination of chlorine in biological materials using electrothermal vaporization inductively coupled plasma mass spectrometry

Energy Technology Data Exchange (ETDEWEB)

Santos de Gois, Jefferson; Pereira, Éderson R. [Departamento de Química, Universidade Federal de Santa Catarina, 88040-970 Florianópolis, SC (Brazil); Welz, Bernhard [Departamento de Química, Universidade Federal de Santa Catarina, 88040-970 Florianópolis, SC (Brazil); INCT de Energia e Ambiente do CNPq (Brazil); Borges, Daniel L.G., E-mail: daniel.borges@ufsc.br [Departamento de Química, Universidade Federal de Santa Catarina, 88040-970 Florianópolis, SC (Brazil); INCT de Energia e Ambiente do CNPq (Brazil)

2015-03-01

This work describes a methodology developed to carry out Cl determination in biological materials using electrothermal vaporization inductively coupled plasma mass spectrometry and direct solid sample analysis. The solid samples were directly weighed into graphite ‘cups’ and inserted into the graphite furnace. The RF power and the carrier gas flow rate were optimized at 1300 W and 0.7 L min{sup −1}, respectively. Calibration could be carried out using aqueous standard solutions with pre-dried modifiers (Pd + Nd or Pd + Ca) or using solid certified reference materials with the same pre-dried modifiers or without the use of modifiers. The limit of quantification was determined as 5 μg g{sup −1} under optimized conditions and the Cl concentration was determined in five certified reference materials with certified concentrations for Cl, in addition to three certified reference materials, for which certified values for Cl were unavailable; in the latter case, the results were compared with those obtained using high-resolution continuum source molecular absorption spectrometry. Good agreement at a 95% statistical confidence level was achieved between determined and certified or reference values. - Highlights: • Direct determination of chlorine in solid biological materials is described for the first time using ICP-MS. • Calibration against aqueous standards is feasible. • The method is accurate and sensitive, regardless of the composition of the solid sample.

Resonant Control for Fermilab's PXIE RFQ

Energy Technology Data Exchange (ETDEWEB)

Bowring, Daniel [Fermilab; Biedron, Sandra [Colorado State U., Fort Collins; Chase, Brian [Fermilab; Czajkowski, Jerzy [Fermilab; Edelen, Auralee [Colorado State U., Fort Collins; Edelen, Jonathan [Fermilab; Milton, Stephen [Colorado State U., Fort Collins; Nicklaus, Dennis [Fermilab; Steimel, Jim [Fermilab; Zuchnik, Thomas [Fermilab

2016-06-01

The RFQ for Fermilab's PXIE test program is designed to accelerate a < 10 mA H⁻ CW beam to 2.1 MeV. The RFQ has a four-vane design, with four modules brazed together for a total of 4.45 m in length. The RF power required is < 130 kW at 162.5 MHz. A 3 kHz limit on the maximum allowable frequency error is imposed by the RF amplifiers. This frequency constraint must be managed entirely through differential cooling of the RFQ's vanes and outer body and associated material expansion. Simulations indicate that the body and vane coolant temperature should be controlled to within 0.1 degrees C. We present the design of the cooling network and the resonant control algorithm for this structure, as well as results from initial operation.

Certified reference material for radionuclides in fish flesh sample IAEA-414 (mixed fish from the Irish Sea and North Sea)

International Nuclear Information System (INIS)

Pham, M.K.; Sanchez-Cabeza, J.A.; Povinec, P.P.; Arnold, D.; Benmansour, M.; Bojanowski, R.; Carvalho, F.P.; Kim, C.K.; Esposito, M.; Gastaud, J.; Gasco, C.L.; Ham, G.J.; Hegde, A.G.; Holm, E.; Jaskierowicz, D.; Kanisch, G.; Llaurado, M.; La Rosa, J.; Lee, S.-H.; Liong Wee Kwong, L.; Le Petit, G.; Maruo, Y.; Nielsen, S.P.; Oh, J.-S.; Oregioni, B.; Palomares, J.; Pettersson, H.B.L.; Rulik, P.; Ryan, T.P.; Sato, K.; Schikowski, J.; Skwarzec, B.; Smedley, P.A.; Tarjan, S.; Vajda, N.; Wyse, E.

2006-01-01

A certified reference material (CRM) for radionuclides in fish sample IAEA-414 (mixed fish from the Irish Sea and North Seas) is described and the results of the certification process are presented. Nine radionuclides ( 4 K, 137 Cs, 232 Th, 234 U, 235 U, 238 U, 238 Pu, 239+24 Pu and 241 Am) were certified for this material. Information on massic activities with 95% confidence intervals is given for six other radionuclides ( 9 Sr, 21 Pb( 21 Po), 226 Ra, 239 Pu, 24 Pu 241 Pu). Less frequently reported radionuclides ( 99 Tc, 129 I, 228 Th, 23 Th and 237 Np) and information on some activity and mass ratios are also included. The CRM can be used for quality assurance/quality control of the analysis of radionuclides in fish sample, for the development and validation of analytical methods and for training purposes. The material is available from IAEA, Vienna, in 100 g units

Biological Sampling Variability Study

Energy Technology Data Exchange (ETDEWEB)

Amidan, Brett G. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Hutchison, Janine R. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

2016-11-08

There are many sources of variability that exist in the sample collection and analysis process. This paper addresses many, but not all, sources of variability. The main focus of this paper was to better understand and estimate variability due to differences between samplers. Variability between days was also studied, as well as random variability within each sampler. Experiments were performed using multiple surface materials (ceramic and stainless steel), multiple contaminant concentrations (10 spores and 100 spores), and with and without the presence of interfering material. All testing was done with sponge sticks using 10-inch by 10-inch coupons. Bacillus atrophaeus was used as the BA surrogate. Spores were deposited using wet deposition. Grime was coated on the coupons which were planned to include the interfering material (Section 3.3). Samples were prepared and analyzed at PNNL using CDC protocol (Section 3.4) and then cultured and counted. Five samplers were trained so that samples were taken using the same protocol. Each sampler randomly sampled eight coupons each day, four coupons with 10 spores deposited and four coupons with 100 spores deposited. Each day consisted of one material being tested. The clean samples (no interfering materials) were run first, followed by the dirty samples (coated with interfering material). There was a significant difference in recovery efficiency between the coupons with 10 spores deposited (mean of 48.9%) and those with 100 spores deposited (mean of 59.8%). There was no general significant difference between the clean and dirty (containing interfering material) coupons or between the two surface materials; however, there was a significant interaction between concentration amount and presence of interfering material. The recovery efficiency was close to the same for coupons with 10 spores deposited, but for the coupons with 100 spores deposited, the recovery efficiency for the dirty samples was significantly larger (65

Automated extraction of DNA from reference samples from various types of biological materials on the Qiagen BioRobot EZ1 Workstation

DEFF Research Database (Denmark)

Stangegaard, Michael; Jørgensen, Mads; Hansen, Anders Johannes

2009-01-01

, and muscle biopsies. The DNA extraction was validated according to EN/ISO 17025 for the STR kits AmpFlSTR« Identifiler« and AmpFlSTR« Yfiler« (Applied Biosystems). Of 298 samples extracted, 11 (4%) did not yield acceptable results. In conclusion, we have demonstrated that extraction of DNA from various types......We have validated and implemented a protocol for DNA extraction from various types of biological materials using a Qiagen BioRobot EZ1 Workstation. The sample materials included whole blood, blood from deceased, buccal cells on Omni swabs and FTA Cards, blood on FTA Cards and cotton swabs...... of biological material can be performed quickly and without the use of hazardous chemicals, and that the DNA may be successfully STR typed according to the requirements of forensic genetic investigations accredited according to EN/ISO 17025...

Milk and serum standard reference materials for monitoring organic contaminants in human samples.

Science.gov (United States)

Schantz, Michele M; Eppe, Gauthier; Focant, Jean-François; Hamilton, Coreen; Heckert, N Alan; Heltsley, Rebecca M; Hoover, Dale; Keller, Jennifer M; Leigh, Stefan D; Patterson, Donald G; Pintar, Adam L; Sharpless, Katherine E; Sjödin, Andreas; Turner, Wayman E; Vander Pol, Stacy S; Wise, Stephen A

2013-02-01

Four new Standard Reference Materials (SRMs) have been developed to assist in the quality assurance of chemical contaminant measurements required for human biomonitoring studies, SRM 1953 Organic Contaminants in Non-Fortified Human Milk, SRM 1954 Organic Contaminants in Fortified Human Milk, SRM 1957 Organic Contaminants in Non-Fortified Human Serum, and SRM 1958 Organic Contaminants in Fortified Human Serum. These materials were developed as part of a collaboration between the National Institute of Standards and Technology (NIST) and the Centers for Disease Control and Prevention (CDC) with both agencies contributing data used in the certification of mass fraction values for a wide range of organic contaminants including polychlorinated biphenyl (PCB) congeners, chlorinated pesticides, polybrominated diphenyl ether (PBDE) congeners, and polychlorinated dibenzo-p-dioxin (PCDD) and dibenzofuran (PCDF) congeners. The certified mass fractions of the organic contaminants in unfortified samples, SRM 1953 and SRM 1957, ranged from 12 ng/kg to 2200 ng/kg with the exception of 4,4'-DDE in SRM 1953 at 7400 ng/kg with expanded uncertainties generally <14 %. This agreement suggests that there were no significant biases existing among the multiple methods used for analysis.

The Viking X ray fluorescence experiment - Sampling strategies and laboratory simulations. [Mars soil sampling

Science.gov (United States)

Baird, A. K.; Castro, A. J.; Clark, B. C.; Toulmin, P., III; Rose, H., Jr.; Keil, K.; Gooding, J. L.

1977-01-01

Ten samples of Mars regolith material (six on Viking Lander 1 and four on Viking Lander 2) have been delivered to the X ray fluorescence spectrometers as of March 31, 1977. An additional six samples at least are planned for acquisition in the remaining Extended Mission (to January 1979) for each lander. All samples acquired are Martian fines from the near surface (less than 6-cm depth) of the landing sites except the latest on Viking Lander 1, which is fine material from the bottom of a trench dug to a depth of 25 cm. Several attempts on each lander to acquire fresh rock material (in pebble sizes) for analysis have yielded only cemented surface crustal material (duricrust). Laboratory simulation and experimentation are required both for mission planning of sampling and for interpretation of data returned from Mars. This paper is concerned with the rationale for sample site selections, surface sampler operations, and the supportive laboratory studies needed to interpret X ray results from Mars.

Interactive Sample Book (ISB)

DEFF Research Database (Denmark)

Heimdal, Elisabeth Jacobsen; Lenau, Torben Anker; Guglielmi, Michel

2009-01-01

supervisor Torben A. Lenau. Inspiration to use smart materials Interactive textiles are still quite an unknown phenomenon to many. It is thus often difficult to communicate what kind of potentials lie within these materials. This is why the ISB project was started, as a practice based research project...... and senses in relation to integrated decoration and function primarily to indoor applications. The result of the project will be a number of interactive textiles, to be gathered in an interactive sample book (ISB), in a similar way as the sample books of wallpapers one can take home from the shop and choose...... from. In other words, it is a kind of display material, which in a simple manner can illustrate how different techniques and smart materials work. The sample book should display a number of possibilities where sensor technology, smart materials and textiles are mixed to such an extent that the textile...

Analysis of cement solidified product and ash samples and preparation of a reference material

International Nuclear Information System (INIS)

Ishimori, Ken-ichiro; Haraga, Tomoko; Shimada, Asako; Kameo, Yutaka; Takahashi, Kuniaki

2010-08-01

Simple and rapid analytical methods for radionuclides in low-level radioactive waste have been developed by the present authors. The methods were applied to simulated solidified products and actual metal wastes to confirm their usefulness. The results were summarized as analytical guide lines. In the present work, cement solidified product and ash waste were analyzed followed by the analytical guide lines and subjects were picked up and solved for the application of the analytical guide lines to these wastes. Pulverization and homogenization method for ash waste was improved to prevent a contamination since the radioactivity concentrations of the ash samples were relatively high. Pre-treatment method was altered for the cement solidified product and ash samples taking account for their high concentration of Ca. Newly, an analytical method was also developed to measure 129 I with a dynamic reaction cell inductively coupled plasma mass spectrometer. In the analytical test based on the improved guide lines, gamma-ray emitting nuclides, 60 Co and 137 Cs, were measured to estimate the radioactivity of the other alpha and beta-ray emitting nuclides. The radionuclides assumed detectable, 3 H, 14 C, 36 Cl, 63 Ni, 90 Sr, and alpha-ray emitting nuclides, were analyzed with the improved analytical guide lines and their applicability for cement solidified product and ash samples were confirmed. Additionally a cement solidified product sample was evaluated in terms of the homogeneity and the radioactivity concentrations in order to prepare a reference material for radiochemical analysis. (author)

The method of the gas-dynamic centrifugal compressor stage characteristics recalculation for variable rotor rotational speeds and the rotation angle of inlet guide vanes blades if the kinematic and dynamic similitude conditions are not met

Science.gov (United States)

Vanyashov, A. D.; Karabanova, V. V.

2017-08-01

A mathematical description of the method for obtaining gas-dynamic characteristics of a centrifugal compressor stage is proposed, taking into account the control action by varying the rotor speed and the angle of rotation of the guide vanes relative to the "basic" characteristic, if the kinematic and dynamic similitude conditions are not met. The formulas of the correction terms for the non-dimensional coefficients of specific work, consumption and efficiency are obtained. A comparative analysis of the calculated gas-dynamic characteristics of a high-pressure centrifugal stage with experimental data is performed.

Correlation between radon exhalation and radium content in granite samples used as construction material in Saudi Arabia

Energy Technology Data Exchange (ETDEWEB)

Al-Jarallah, M.I. [Department of Physics, King Fahd University of Petroleum and Minerals, Dhahran 31261 (Saudi Arabia)]. E-mail: mibrahim@kfupm.edu.sa; Fazal-ur-Rehman [Department of Physics, King Fahd University of Petroleum and Minerals, Dhahran 31261 (Saudi Arabia); Musazay, M.S. [Department of Physics, King Fahd University of Petroleum and Minerals, Dhahran 31261 (Saudi Arabia); Aksoy, A. [Department of Physics, King Fahd University of Petroleum and Minerals, Dhahran 31261 (Saudi Arabia)

2005-11-15

Measurements of radon exhalation for a total of 205 selected samples of construction materials used in Saudi Arabia were carried out using an active radon gas analyzer with an emanation container. It was found that granite samples were the main source of radon exhalation. The radon exhalation rates per unit area from these granite samples varied from below the minimum detection limit up to 13.1Bqm{sup -2}h{sup -1} with an average of 1.5 +/-1.9(1{sigma})Bqm{sup -2}h{sup -1}. The radium contents of 27 granite samples were measured using an HPGe-based {gamma} spectroscopy setup. The {sup 226}Ra content of the granites varied from below the minimum detection limit up to 297Bqkg{sup -1}, with an average of 83+/-73(1{sigma})Bqkg{sup -1}. The linear correlation coefficient between exhaled radon and radium content was found to be 0.90.

Cathodoluminescence | Materials Science | NREL

Science.gov (United States)

shown on a computer screen; the image of a sample semiconductor material appears as a striated oval material sample shown above; the image is a high-contrast light and dark oval on a dark background and was top left of copper indium gallium selenide semiconductor material sample; the image is shown on a

Numerical study on dissimilar guide vane design with SCC piston for air and emulsified biofuel mixing improvement

Directory of Open Access Journals (Sweden)

Hamid Mohd Fadzli

2017-01-01

Full Text Available Crude palm oil (CPO is one of the most potential biofuels that can be applied in the conventional diesel engines, where the chemical properties of CPO are comparable to diesel fuel. However, its higher viscosity and heavier molecules can contributes to several engine problems such as low atomization during injection, carbon deposit formation, injector clogging, low mixing with air and lower combustion efficiency. An emulsification of biofuel and modifications of few engine critical components have been identified to mitigate the issues. This paper presents the effects of dissimilar guide vane design (GVD in terms of height variation of 0.25R, 0.3R and 0.35R at the intake manifold with shallow depth re-entrance combustion chamber (SCC piston application to the incylinder air flow characteristics improvement. The simulation results show that the intake manifold with GVD improved the performance of the air flow characteristic particularly swirl, tumble and cross tumble ratios from the intake manifold to the engine. The GVD with the height of 0.3R was found to be the optimum design with respect to the overall improvement of the air flow characteristic. The improvement of the air flow characteristic with the application of GVD and SCC piston in the engine was expected to contribute to a better air fuel mixing, fuel atomization and combustion efficiency of the engine using emulsified biofuel as a source of fuel.

Alternating sample changer and an automatic sample changer for liquid scintillation counting of alpha-emitting materials

International Nuclear Information System (INIS)

Thorngate, J.H.

1977-08-01

Two sample changers are described that were designed for liquid scintillation counting of alpha-emitting samples prepared using solvent-extraction chemistry. One operates manually but changes samples without exposing the photomultiplier tube to light, allowing the high voltage to remain on for improved stability. The other is capable of automatically counting up to 39 samples. An electronic control for the automatic sample changer is also described

Research Paper ISSN 0189-6016©2007

African Journals Online (AJOL)

Prof. Adewunmi

traditionally used for the treatment of fracture and dislocation (Bijoy, 2002). ... The plant material was identified and authenticated at Botanical Survey of India ..... of mild analgesic non-steroidal anti-inflammatory compounds (Ferreira and Vane,.

Sample collection and sample analysis plan in support of the 105-C/190-C concrete and soil sampling activities

International Nuclear Information System (INIS)

Marske, S.G.

1996-07-01

This sampling and analysis plan describes the sample collection and sample analysis in support of the 105-C water tunnels and 190-C main pumphouse concrete and soil sampling activities. These analytical data will be used to identify the radiological contamination and presence of hazardous materials to support the decontamination and disposal activities

Off-design performance loss model for radial turbines with pivoting, variable-area stators

Science.gov (United States)

Meitner, P. L.; Glassman, A. J.

1980-01-01

An off-design performance loss model was developed for variable stator (pivoted vane), radial turbines through analytical modeling and experimental data analysis. Stator loss is determined by a viscous loss model; stator vane end-clearance leakage effects are determined by a clearance flow model. Rotor loss coefficient were obtained by analyzing the experimental data from a turbine rotor previously tested with six stators having throat areas from 20 to 144 percent of design area and were correlated with stator-to-rotor throat area ratio. An incidence loss model was selected to obtain best agreement with experimental results. Predicted turbine performance is compared with experimental results for the design rotor as well as with results for extended and cutback versions of the rotor. Sample calculations were made to show the effects of stator vane end-clearance leakage.

Impact of collection container material and holding times on sample integrity for mercury and methylmercury in water

Energy Technology Data Exchange (ETDEWEB)

Riscassi, Ami L [ORNL; Miller, Carrie L [ORNL; Brooks, Scott C [ORNL

2014-01-01

Mercury (Hg) and methylmercury (MeHg) concentrations in streamwater can vary on short timescales (hourly or less) during storm flow and on a diel cycle; the frequency and timing of sampling required to accurately characterize these dynamics may be difficult to accomplish manually. Automated sampling can assist in sample collection; however use has been limited for Hg and MeHg analysis due to stability concerns of trace concentrations during extended storage times. We examined the viability of using automated samplers with disposable low-density polyethylene (LDPE) sample bags to collect industrially contaminated streamwater for unfiltered and filtered Hg and MeHg analysis. Specifically we investigated the effect of holding times ranging from hours to days on streamwater collected during baseflow and storm flow. Unfiltered and filtered Hg and MeHg concentrations decreased with increases in time prior to sample processing; holding times of 24 hours or less resulted in concentration changes (mean 11 7% different) similar to variability in duplicates collected manually during analogous field conditions (mean 7 10% different). Comparisons of samples collected with manual and automated techniques throughout a year for a wide range of stream conditions were also found to be similar to differences observed between duplicate grab samples. These results demonstrate automated sampling into LDPE bags with holding times of 24 hours or less can be effectively used to collect streamwater for Hg and MeHg analysis, and encourage the testing of these materials and methods for implementation in other aqueous systems where high-frequency sampling is warranted.

Materials Characterization and Microelectronic Implementation of Metal-insulator Transition Materials and Phase Change Materials

Science.gov (United States)

2015-03-26

materials like crystalline semiconductors, graphene , and composites, the materials discussed here could have a significant impact. This thesis investigates...diagnosis [124], crystallinity of pharmaceutical materials [125], materials diagnosis for restoration of paintings [126], and materials research [127...temperature dots and paint were placed on samples on the substrate. Temperature dots are typically used in the transportation of goods such as food in order

Temperature measurement of the reactor materials samples irradiated in the fuel channels of the RA reactor - Annex 16

International Nuclear Information System (INIS)

Nikolic, M.; Djalovic, M.

1964-01-01

Reactor materials as graphite, stainless steel, magnox, zirconium alloys, etc. were exposed to fast neutron flux inside the fuel elements specially adapted for this purpose. Samples in the form ampoules were placed in capsules inside the fuel channels and cooled by heavy water which cools the fuel elements. In order to monitor the samples temperature 42 thermocouples were placed in the samples. That was necessary for reactor safety reasons and for further interpretation of measured results. Temperature monitoring was done continuously by multichannel milivoltmeters. This paper describes the technique of introducing the thermocouples, compensation instruments, control of the cold ends and adaptation of the instruments for precision (0.5%) temperature measurement in the range 30 deg - 130 deg C; 30 deg - 280 deg C and 30 deg - 80 deg C [sr

40 CFR 763.86 - Sampling.

Science.gov (United States)

2010-07-01

... 40 Protection of Environment 30 2010-07-01 2010-07-01 false Sampling. 763.86 Section 763.86 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) TOXIC SUBSTANCES CONTROL ACT ASBESTOS Asbestos-Containing Materials in Schools § 763.86 Sampling. (a) Surfacing material. An accredited inspector...

Three Proposed Compendia for Genesis Solar Wind Samples: Science Results, Collector Materials Characterization and Cleaning Techniques

Science.gov (United States)

Allton, J. H.; Calaway, M. J.; Nyquist, L. E.; Jurewicz, A. J. G.; Burnett, D. S.

2018-01-01

Final Paper and not the abstract is attached. Introduction: Planetary material and cosmochemistry research using Genesis solar wind samples (including the development and implementation of cleaning and analytical techniques) has matured sufficiently that compilations on several topics, if made publically accessible, would be beneficial for researchers and reviewers. We propose here three compendia based on content, organization and source of documents (e.g. published peer-reviewed, published, internal memos, archives). For planning purposes, suggestions are solicited from potential users of Genesis solar wind samples for the type of science content and/or organizational style that would be most useful to them. These compendia are proposed as living documents, periodically updated. Similar to the existing compendia described below, the curation compendia are like library or archival finding aids, they are guides to published or archival documents and should not be cited as primary sources.

Non-destructive alpha-particle activation analysis of P, Cl, K and Ca in marine macro-alga samples using synthetic multielement reference material as comparative standard

International Nuclear Information System (INIS)

Iwata, Y.; Naitoh, H.; Suzuki, N.

1992-01-01

A Synthetic Reference Material (SyRM) composed with accurately known amounts of 12 elements has been prepared. The elemental composition of the SyRM is closely similar to that of marine macro-algae sample. The elemental composition of the SyRM was regulated by the starting materials used for the synthesis. The SyRM was used as a comparative standard for non-destructive alpha-particle activation analysis of marine macro-alga samples. P, Cl, K and Ca were determined simultaneously without correction for alpha range due to difference in the elemental composition between the analytical samples and the comparative standard. (author) 19 refs.; 4 tabs

A soil sampling reference site: The challenge in defining reference material for sampling

International Nuclear Information System (INIS)

De Zorzi, Paolo; Barbizzi, Sabrina; Belli, Maria; Fajgelj, Ales; Jacimovic, Radojko; Jeran, Zvonka; Sansone, Umberto; Perk, Marcel van der

2008-01-01

In the frame of the international SOILSAMP project, funded and coordinated by the Italian Environmental Protection Agency, an agricultural area was established as a reference site suitable for performing soil sampling inter-comparison exercises. The reference site was characterized for trace element content in soil, in terms of the spatial and temporal variability of their mass fraction. Considering that the behaviour of long-lived radionuclides in soil can be expected to be similar to that of some stable trace elements and that the distribution of these trace elements in soil can simulate the distribution of radionuclides, the reference site characterised in term of trace elements, can be also used to compare the soil sampling strategies developed for radionuclide investigations

A soil sampling reference site: The challenge in defining reference material for sampling

Energy Technology Data Exchange (ETDEWEB)

De Zorzi, Paolo [Agenzia per la Protezione dell' Ambiente e per i Servizi Tecnici (APAT), Servizio Metrologia Ambientale, Via di Castel Romano, Rome 100-00128 (Italy)], E-mail: paolo.dezorzi@apat.it; Barbizzi, Sabrina; Belli, Maria [Agenzia per la Protezione dell' Ambiente e per i Servizi Tecnici (APAT), Servizio Metrologia Ambientale, Via di Castel Romano, Rome 100-00128 (Italy); Fajgelj, Ales [International Atomic Energy Agency (IAEA), Agency' s Laboratories Seibersdorf, Vienna A-1400 (Austria); Jacimovic, Radojko; Jeran, Zvonka; Sansone, Umberto [Jozef Stefan Institute, Jamova 39, Ljubljana 1000 (Slovenia); Perk, Marcel van der [Department of Physical Geography, Utrecht University, P.O. Box 80115, TC Utrecht 3508 (Netherlands)

2008-11-15

In the frame of the international SOILSAMP project, funded and coordinated by the Italian Environmental Protection Agency, an agricultural area was established as a reference site suitable for performing soil sampling inter-comparison exercises. The reference site was characterized for trace element content in soil, in terms of the spatial and temporal variability of their mass fraction. Considering that the behaviour of long-lived radionuclides in soil can be expected to be similar to that of some stable trace elements and that the distribution of these trace elements in soil can simulate the distribution of radionuclides, the reference site characterised in term of trace elements, can be also used to compare the soil sampling strategies developed for radionuclide investigations.

A soil sampling reference site: the challenge in defining reference material for sampling.

Science.gov (United States)

de Zorzi, Paolo; Barbizzi, Sabrina; Belli, Maria; Fajgelj, Ales; Jacimovic, Radojko; Jeran, Zvonka; Sansone, Umberto; van der Perk, Marcel

2008-11-01

In the frame of the international SOILSAMP project, funded and coordinated by the Italian Environmental Protection Agency, an agricultural area was established as a reference site suitable for performing soil sampling inter-comparison exercises. The reference site was characterized for trace element content in soil, in terms of the spatial and temporal variability of their mass fraction. Considering that the behaviour of long-lived radionuclides in soil can be expected to be similar to that of some stable trace elements and that the distribution of these trace elements in soil can simulate the distribution of radionuclides, the reference site characterised in term of trace elements, can be also used to compare the soil sampling strategies developed for radionuclide investigations.

Wedge cells during regeneration of juvenile and adult feathers and their role in carving out the branching pattern of barbs.

Science.gov (United States)

Alibardi, Lorenzo

2007-01-01

The present ultrastructural study on regenerating feathers emphasizes the role of supportive cells in determining the branching pattern of barbs. Supportive cells are localized among developing barb and barbule cells, in marginal plates, and underneath the feather sheath, and their differentiative fate, in general, is a form of lipid degeneration. The Latter process determines the carving out of barb branching in both downfeathers and pennaceous feathers. In the latter feathers, some supportive cells (barb vane cells and cylindrical cells of marginal plates) degenerate within each barb ridge leaving separate barbules. Other supportive cells, here termed wedge cells, form columns of cornified material that merge into elongated corneous scaffolds localized among barbs and the rachis. This previously undescribed form of cornification of supportive cells derives from the aggregation of periderm and dense granules present in wedge cells. The latter cells give origin to a corneous material different from feather keratin that may initially sustain the early and soft barbules. After barbules are cornified the supportive cells scaffolds are eventually sloughed as the sheath breaks allowing the new feather to open up and form a planar vane. The corneous material of wedge cells may also contribute to molding of the overlapped nodes of barbule cells that form lateral spines or hooklets in mature barbules. Eventually, the disappearance of wedge cell scaffolding determines the regular spacing of barbs attached to the rachis in order to form a close vane.

Using the sampling method to propagate uncertainties of physical parameters in systems with fissile material

International Nuclear Information System (INIS)

Campolina, Daniel de Almeida Magalhães

2015-01-01

There is an uncertainty for all the components that comprise the model of a nuclear system. Assessing the impact of uncertainties in the simulation of fissionable material systems is essential for a realistic calculation that has been replacing conservative model calculations as the computational power increases. The propagation of uncertainty in a simulation using a Monte Carlo code by sampling the input parameters is recent because of the huge computational effort required. By analyzing the propagated uncertainty to the effective neutron multiplication factor (k eff ), the effects of the sample size, computational uncertainty and efficiency of a random number generator to represent the distributions that characterize physical uncertainty in a light water reactor was investigated. A program entitled GB s ample was implemented to enable the application of the random sampling method, which requires an automated process and robust statistical tools. The program was based on the black box model and the MCNPX code was used in and parallel processing for the calculation of particle transport. The uncertainties considered were taken from a benchmark experiment in which the effects in k eff due to physical uncertainties is done through a conservative method. In this work a script called GB s ample was implemented to automate the sampling based method, use multiprocessing and assure the necessary robustness. It has been found the possibility of improving the efficiency of the random sampling method by selecting distributions obtained from a random number generator in order to obtain a better representation of uncertainty figures. After the convergence of the method is achieved, in order to reduce the variance of the uncertainty propagated without increase in computational time, it was found the best number o components to be sampled. It was also observed that if the sampling method is used to calculate the effect on k eff due to physical uncertainties reported by

Recoil Reactions in Neutron-Activation Analysis. The Szilard-Chalmers Effect Applied in the Analysis of Biological Samples; II. Transfer of Activities from Container Material to Sample

Energy Technology Data Exchange (ETDEWEB)

Brune, D

1965-01-15

The present investigation consists of two parts. The one part concerns the application of the Szilard-Chalmers effect in the separation of activities from neutron-irradiated biological material. The nuclides As-76, Au-198, Br-82, Ca-47, Cd-115, Cl-38, Co-60, Cr-51, Cs-134, Cu-64, Fe-59, Mg-27, Mo-99, Na-24, P-32, Rb-86, Se-75 and Zn-65 were extracted from either liver tissue, whole blood or muscle tissue. The extractions were made in water, 0.1 N HCl, 1 N HCl or conc. HCl respectively. The nuclides belonging to the alkali metals together with Br and Cl, were found present in the water and hydrochloric extracts to 96 per cent or more. In the conc. HCl extracts, the greater part of the nuclides were recovered to 90 per cent or more. The enrichment of the different nuclides obtained in the Szilard-Chalmers process was investigated as follows. After extraction of the nuclides from the irradiated material the solution obtained was divided into two parts, one of which was reactivated. The specific activities of the nuclides in the two solutions were then compared, thus giving the enrichment factor In one case, the residue of organic material after extraction was reactivated and the activity compared to the initial one. The effect of dilution together with the application of short irradiation periods favouring higher yield was investigated in the separation of Fe-59 from whole blood samples irradiated in frozen conditions. The other part of the investigation concerns an estimation of the amounts of the activities originating from polyethylene and quartz containers transferred to container surface due to the recoil effect in the thermal neutron-capture process, thus causing contamination of the sample. The universal range-energy relationship given by Lindhard and Scharff has been applied in these calculations. As regards containers with impurities in the ppm region, the amounts of activities transferred owing to this effect were found to be quite negligible. However, when

Search for Extralunar Materials in Apollo Soil Samples

Science.gov (United States)

Lucey, P. G.; Honniball, C.; Crites, S.; Taylor, G. J.; Martel, L.

2017-12-01

It has long been proposed that the lunar surface is a pristine collector of material from across the solar system. The Moon is exposed to the same meteorite flux as the Earth, but because its surface is unaltered by processes such as plate tectonics, aqueous alteration, or recent volcanism, the Moon may have recorded a much longer meteoritic history than the chemically and physically active Earth. By studying lunar soils at the individual grain level, we have the potential to identify and study material from across the inner solar system. We have developed three hyperspectral imaging microscopes to search a large quantity of lunar soil grains for rare lunar, and extra-lunar minerals. We are using lunar-exotic mineralogy as a tracer to detect extralunar candidates. One hyperspectral microscope covers the 1-2.5 micron region for detection of water and hydroxyl overtones in alteration minerals such as phyllosilicates. The second instrument covers the 2.5 to 5 micron region to characterize the 3 micron water region, and for detection of organics and carbonates. The third covers the thermal infrared for detection of phosphates and zeolites as well as the major lunar silicates. We are examining 1 million grains of varying sizes from Apollo 11 ,12, 14 and 16 landing sites. Using the USGS spectral library and the Tetracorder mineral mapping algorithm, we are matching library mineral spectra with the grain spectra we acquire. To validate our ability to detect and match mineral spectra, we are conducting scans of relevent mineral seperates and mixtures at the individual grain level. Results of this mineral inventory will provide contraints on various models and estimates for material transfer between the terrestrial planets.

Airfoil nozzle and shroud assembly

Science.gov (United States)

Shaffer, J.E.; Norton, P.F.

1997-06-03

An airfoil and nozzle assembly are disclosed including an outer shroud having a plurality of vane members attached to an inner surface and having a cantilevered end. The assembly further includes a inner shroud being formed by a plurality of segments. Each of the segments having a first end and a second end and having a recess positioned in each of the ends. The cantilevered end of the vane member being positioned in the recess. The airfoil and nozzle assembly being made from a material having a lower rate of thermal expansion than that of the components to which the airfoil and nozzle assembly is attached. 5 figs.

Commutability of food microbiology proficiency testing samples.

Science.gov (United States)

Abdelmassih, M; Polet, M; Goffaux, M-J; Planchon, V; Dierick, K; Mahillon, J

2014-03-01

Food microbiology proficiency testing (PT) is a useful tool to assess the analytical performances among laboratories. PT items should be close to routine samples to accurately evaluate the acceptability of the methods. However, most PT providers distribute exclusively artificial samples such as reference materials or irradiated foods. This raises the issue of the suitability of these samples because the equivalence-or 'commutability'-between results obtained on artificial vs. authentic food samples has not been demonstrated. In the clinical field, the use of noncommutable PT samples has led to erroneous evaluation of the performances when different analytical methods were used. This study aimed to provide a first assessment of the commutability of samples distributed in food microbiology PT. REQUASUD and IPH organized 13 food microbiology PTs including 10-28 participants. Three types of PT items were used: genuine food samples, sterile food samples and reference materials. The commutability of the artificial samples (reference material or sterile samples) was assessed by plotting the distribution of the results on natural and artificial PT samples. This comparison highlighted matrix-correlated issues when nonfood matrices, such as reference materials, were used. Artificially inoculated food samples, on the other hand, raised only isolated commutability issues. In the organization of a PT-scheme, authentic or artificially inoculated food samples are necessary to accurately evaluate the analytical performances. Reference materials, used as PT items because of their convenience, may present commutability issues leading to inaccurate penalizing conclusions for methods that would have provided accurate results on food samples. For the first time, the commutability of food microbiology PT samples was investigated. The nature of the samples provided by the organizer turned out to be an important factor because matrix effects can impact on the analytical results. © 2013

k0-NAA applied to certified reference materials and hair samples. Evaluation of exposure level in a galvanising industry

International Nuclear Information System (INIS)

Menezes, M.A. de B.C.; Pereira Maia, E.C.

2000-01-01

The k 0 parametric neutron activation analysis has been applied since 1995 in the Radiochemical Sector/CDTN, Belo Horizonte, Brazil. Several certified reference materials were studied with the aim of analysing biological samples. This work is related to an IAEA co-ordinated research project whose goal is to make a survey of the exposures to metals related to occupational diseases. It has been conducted by CDTN and government departments of health. The hair samples as bioindicators were donated by galvanising factory workers in Belo Horizonte. This city and surrounding area are important industrial centres and that industry is responsible for the majority of patients who look for medical assistance because of metal contamination. The Al, Co, Cu, Cr, La, Mn, Sb and V concentrations determined in the workers' samples suggest endogenous contamination. (author)

Thermal simulation for 35 kW powered prototype radio frequency quadrapole

International Nuclear Information System (INIS)

Kothari, Ashok; Ahuja, Rajeev; Safvan, C.P.; Kumar, Sugam

2011-01-01

As part of the accelerator augmentation program at IUAC, a high current injector (HCI) is being developed to inject highly charged ions into the superconducting LINAC. The HCI consists of a superconducting (High T c ) ECR source operated on a high voltage deck, producing the high currents of highly charged ions. The ion beams produced by the ECR (PKDELIS) source will be injected into a Radio Frequency Quadrupole accelerator (RFQ) and be accelerated to 180 keV/u. RF power of about 100 kW at 48.5 MHz will be fed to the RFQ during it's actual working. Most of the power fed is dissipated in the system as heat. So a continuous removal of this heat is necessary to maintain tuning parameters and normal running of the RFQ. The IUAC RFQ is a four rod cavity structure consisting of individual, demountable vanes on vane posts. All the components are made of copper except the high vacuum chamber. High vacuum chamber is made of stainless steel and electroplated with 100 microns copper on the inner surface. To take out the heat from the system cooling holes for water circulation are provided in the design of the vanes and vane posts, which together form cooling circuits. There are fourteen vanes in three different lengths and these are mounted on five vane posts. Water enters and exits from the vane posts base. From each post it enters into two or three circuits in parallel and exits into the next vane post and the flow combines again. In effect five cooling circuits are further divided into fourteen circuits. Thermal design of the system is analyzed and optimized using a computational fluid dynamics (CFD) software. The CFD software simultaneously solves the equations of mass, momentum and energy with the given structure, material, fluid and applied boundary conditions. An actual 3-dimensional model of the assembly was made using Solidworks modelling software. To save on simulation time, small holes and minor components were suppressed during analysis. The software used for

Images of soft materials: a 3D visualization of interior of the sample in terms of attenuation coefficient

International Nuclear Information System (INIS)

Golosio, B.; Brunetti, A.; Cesareo, R.; Amendolia, S.R.; Rao, D.V.; Seltzer, S.M.

2001-01-01

Images of soft materials are obtained using image intensifier based X-ray system (Rao et al., Nucl. Instr. and Meth. A 437 (1999) 141). The interior of the soft material is visualized using the novel software in order to know the distribution of attenuation coefficient in terms of density. The novel software is based mainly on graphical library and applicable to several operating systems without any change. It can be applied to several applications starting from biomedical to industries, for example, quality control. The results for walnut and brew tooth are presented as a set of images from the internal parts of the sample. A description of the principal parameters required for tomographic visualization is given and some results based on this technique are reported and discussed

Rapid screening of natually occurring radioactive nuclides({sup 2}'3{sup 8}U, {sup 232}Th) in raw materials and by-products samples using XRF

Energy Technology Data Exchange (ETDEWEB)

Park, Ji Young; Lim, Chung Sup [Radiation Biotechnology and Applied Radioiostope Science, University of Science and Technology, Daejeon (Korea, Republic of); Lim, Jong Myoung; Ji, Young Yong; Chung, Kun Ho; Lee, Wan No; Kang, Mun Ja [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of); Jang, Byung Uck [Korea Institute of Nuclear Safety, Daejeon (Korea, Republic of)

2016-12-15

As new legislation has come into force implementing radiation safety management for the use of naturally occurring radioactive materials (NORM), it is necessary to establish a rapid and accurate measurement technique. Measurement of {sup 238}U and {sup 232}Th using conventional methods encounter the most significant difficulties for pretreatment (e.g., purification, speciation, and dilution/enrichment) or require time-consuming processes. Therefore, in this study, the applicability of ED-XRF as a non-destructive and rapid screening method was validated for raw materials and by-product samples. A series of experiments was conducted to test the applicability for rapid screening of XRF measurement to determine activity of {sup 238}U and {sup 23{sup 2}}Th based on certified reference materials (e.g., soil, rock, phosphorus rock, bauxite, zircon, and coal ash) and NORM samples commercially used in Korea. Statistical methods were used to compare the analytical results of ED-XRF to those of certified values of certified reference materials (CRM) and inductively coupled plasma mass spectrometry (ICP-MS). Results of the XRF measurement for {sup 238}U and {sup 232}Th showed under 20% relative error and standard deviation. The results of the U-test were statistically significant except for the case of U in coal fly ash samples. In addition, analytical results of {sup 238}U and {sup 232}Th in the raw material and by-product samples using XRF and the analytical results of those using ICP-MS (R{sup 2}≥0.95) were consistent with each other. Thus, the analytical results rapidly derived using ED-XRF were fairly reliable. Based on the validation results, it can be concluded that the ED-XRF analysis may be applied to rapid screening of radioactivities ({sup 238}U and {sup 232}Th) in NORM samples.

Major- and minor-metal composition of three distinct solid material fractions associated with Juan de Fuca hydrothermal fluids (northeast Pacific), and calculation of dilution fluid samples

Science.gov (United States)

Hinkley, T.K.; Seeley, J.L.; Tatsumoto, M.

1988-01-01

Three distinct types of solid material are associated with each sample of the hydrothermal fluid that was collected from the vents of the Southern Juan de Fuca Ridge. The solid materials appear to be representative of deposits on ocean floors near mid-ocean ridges, and interpretation of the chemistry of the hydrothermal solutions requires understanding of them. Sr isotopic evidence indicates that at least two and probably all three of these solid materials were removed from the solution with which they are associated, by precipitation or adsorption. This occurred after the "pure" hydrothermal fluid was diluted and thoroughly mixed with ambient seawater. The three types of solid materials, are, respectively, a coarse Zn- and Fe-rich material with small amounts of Na and Ca; a finer material also rich in Zn and Fe, but with alkali and alkaline-earth metals; and a scum composed of Ba or Zn, with either considerable Fe or Si, and Sr. Mineral identification is uncertain because of uncertain anion composition. Only in the cases of Ba and Zn were metal masses greater in solid materials than in the associated fluids. For all other metals measured, masses in fluids dwarf those in solids. The fluids themselves contain greater concentrations of all metals measured, except Mg, than seawater. We discuss in detail the relative merits of two methods of determining the mixing proportions of "pure" hydrothermal solution and seawater in the fluids, one based on Sr isotopes, and another previously used method based on Mg concentrations. Comparison of solute concentrations in the several samples shows that degree of dilution of "pure" hydrothermal solutions by seawater, and amounts of original solutes that were removed from it as solid materials, are not related. There is no clear evidence that appreciable amounts of solid materials were not conserved (lost) either during or prior to sample collection. ?? 1988.

HiRadMat at CERN/SPS - A dedicated facility providing high intensity beam pulses to material samples

CERN Multimedia

Charitonidis, N; Efthymiopoulos, I

2014-01-01

HiRadMat (High Radiation to Materials), constructed in 2011, is a facility at CERN designed to provide high‐intensity pulsed beams to an irradiation area where material samples as well as accelerator component assemblies (e.g. vacuum windows, high power beam targets, collimators…) can be tested. The facility uses a 440 GeV proton beam extracted from the CERN SPS with a pulse length of up to 7.2 us, and with a maximum pulse energy of 3.4 MJ (3xE13 proton/pulse). In addition to protons, ion beams with energy of 440 GeV/charge and total pulse energy of 21 kJ can be provided. The beam parameters can be tuned to match the needs of each experiment. HiRadMat is not an irradiation facility where large doses on equipment can be accumulated. It is rather a test area designed to perform single pulse experiments to evaluate the effect of high‐intensity pulsed beams on materials or accelerator component assemblies in a controlled environment. The fa‐ cility is designed for a maximum of 1E16 protons per year, dist...

k0-INAA for APM samples collected in period of June 2004 - March 2005 and some marine certified reference materials

International Nuclear Information System (INIS)

Dung, Ho Manh; Vu, Cao Dong; Y, Truong; Sy, Nguyen Thi

2006-01-01

The airborne particulate matter (APM) samples have been collected in 2004 using two types of polycarbonate membrane filter PM 2.5 and PM 2.5-10 at two sites of industrial (Ho Chi Mihn City) and rural (Dateh) regions in south of Vietnam. Three marine certified reference materials have been selected to establish a k0-NAA procedure for marine samples. The concentration of trace multi-element in the samples has been determined by the k 0 -INAA procedure using K o -DALAT software developed in Dalat NRI. About 28 elements in 224 APM samples collected at two areas of Dateh and HCMC of Vietnam in period from June, 2004 to March, 2005 were presented in report. The statistical analysis was applied to the data set to investigate the pollution source at sampling sites. The results proved that the k 0 -NAA on the Dalat research reactor is a reliable and effective analytical technique for characterization of trace multi-element in APM and marine samples for air and marine environmental pollution study in Vietnam. (author)

Improved orientation sampling for indexing diffraction patterns of polycrystalline materials

DEFF Research Database (Denmark)

Larsen, Peter Mahler; Schmidt, Søren

2017-01-01

to that of optimally distributing points on a four‐dimensional sphere. In doing so, the number of orientation samples needed to achieve a desired indexing accuracy is significantly reduced. Orientation sets at a range of sizes are generated in this way for all Laue groups and are made available online for easy use.......Orientation mapping is a widely used technique for revealing the microstructure of a polycrystalline sample. The crystalline orientation at each point in the sample is determined by analysis of the diffraction pattern, a process known as pattern indexing. A recent development in pattern indexing...... in the presence of noise, it has very high computational requirements. In this article, the computational burden is reduced by developing a method for nearly optimal sampling of orientations. By using the quaternion representation of orientations, it is shown that the optimal sampling problem is equivalent...

Novel Sample-handling Approach for XRD Analysis with Minimal Sample Preparation

Science.gov (United States)

Sarrazin, P.; Chipera, S.; Bish, D.; Blake, D.; Feldman, S.; Vaniman, D.; Bryson, C.

2004-01-01

Sample preparation and sample handling are among the most critical operations associated with X-ray diffraction (XRD) analysis. These operations require attention in a laboratory environment, but they become a major constraint in the deployment of XRD instruments for robotic planetary exploration. We are developing a novel sample handling system that dramatically relaxes the constraints on sample preparation by allowing characterization of coarse-grained material that would normally be impossible to analyze with conventional powder-XRD techniques.

Integration of an Inter Turbine Burner to a Jet Turbine Engine

Science.gov (United States)

2013-03-01

Technology AFRL = Air Force Research Laboratory EGV = Exit Guide Vane HPT = High-Pressure Turbine ID = Inner Diameter IGV = Inlet Guide Vane...been able to show computationally that the compressor exit guide vane (EGV) and the turbine inlet guide vane ( IGV ) could be combined into a single...turbine engine hot section. The red slashed out sections are, from left to right, the compressor exit vane, HPT IGV , and the stator between the HPT and

Correlating activity incorporation with properties of oxide films formed on material samples exposed to BWR and PWR coolants in Finnish nuclear power plants

Energy Technology Data Exchange (ETDEWEB)

Bojinov, M.; Kinnunen, P.; Laitinen, T.; Maekelae, K.; Saario, T.; Sirkiae, P. [VTT Industrial Systems, Espoo (Finland); Buddas, T.; Halin, M.; Kvarnstroem, R.; Tompuri, K. [Fortum Power and Heat Oy, Loviisa Power Plant, Loviisa (Finland); Helin, M.; Muttilainen, E.; Reinvall, A. [Teollisuuden Voima Oy, Olkiluoto (Finland)

2002-07-01

The extent of activity incorporation on primary circuit surfaces in nuclear power plants is connected to the chemical composition of the coolant, to the corrosion behaviour of the material surfaces and to the structure and properties of oxide films formed on circuit surfaces due to corrosion. Possible changes in operational conditions may induce changes in the structure of the oxide films and thus in the rate of activity incorporation. To predict these changes, experimental correlations between water chemistry, oxide films and activity incorporation, as well as mechanistic understanding of the related phenomena need to be established. In order to do this, flow-through cells with material samples and facilities for high-temperature water chemistry monitoring have been installed at Olkiluoto unit 1 (BWR) and Loviisa unit 1 (PWR) in spring 2000. The cells are being used for two major purposes: To observe the changes in the structure and activity levels of oxide films formed on material samples exposed to the primary coolant. Correlating these observations with the abundant chemical and radiochemical data on coolant composition, dose rates etc. collected routinely by the plant, as well as with high-temperature water chemistry monitoring data such as the corrosion potentials of relevant material samples, the redox potential and the high-temperature conductivity of the primary coolant. We describe in this paper the scope of the work, give examples of the observations made and summarize the results on oxide films that have been obtained during one full fuel cycle at both plants. (authors)

Standard methods for sampling and sample preparation for gamma spectroscopy

International Nuclear Information System (INIS)

Taskaeva, M.; Taskaev, E.; Nikolov, P.

1993-01-01

The strategy for sampling and sample preparation is outlined: necessary number of samples; analysis and treatment of the results received; quantity of the analysed material according to the radionuclide concentrations and analytical methods; the minimal quantity and kind of the data needed for making final conclusions and decisions on the base of the results received. This strategy was tested in gamma spectroscopic analysis of radionuclide contamination of the region of Eleshnitsa Uranium Mines. The water samples was taken and stored according to the ASTM D 3370-82. The general sampling procedures were in conformity with the recommendations of ISO 5667. The radionuclides was concentrated by coprecipitation with iron hydroxide and ion exchange. The sampling of soil samples complied with the rules of ASTM C 998, and their sample preparation - with ASTM C 999. After preparation the samples were sealed hermetically and measured. (author)

Cruise report on geotechnical core processing; Cruise: ATLAS-84, ISHTE Component Test, R/V Melville Sept.-Oct., 1984

International Nuclear Information System (INIS)

Silva, A.J.; Lipkin, J.; Brandes, H.

1986-01-01

The primary objectives of the geotechnical core processing program on the component test cruise were to: a) obtain additional base line physical property data of the ISHTE site sediments in MPG-I; b) compare strengths determined in the cored sediments to those obtained in situ with the In Situ Vane (ISV) system; and c) obtain samples for detailed laboratory analysis. Original plans called for processing of at least four cores obtained with the 10.2 cm APL hydrostatic corer (HLC) and at least one core obtained with the 20.3 cm WHOI corer (GC). If possible it was also planned to process one of the HLC cores at dockside in an attempt to assess the effects of ship motions on shear strength measurements. Shipboard laboratory facilities were set up for geotechnical processing with the URI sampling gear. Sandia Laboratory supplied a laboratory miniature vane device and apparatus for conducting thermal conductivity tests. Shipboard measurements included shear strength (miniature vane and Torvane) and thermal conductivity. Sampling included disturbed samples for water content, bulk density and classification tests and undisturbed samples for consolidation, permeability, strength, creep and fabric analyses. Unfortunately no GC cores were obtained. Three HLC cores, obtained on two lowerings of the large platform, were processed in considerable detail. In addition it was decided to process three of the box cores recovered by the SIO biology group. Therefore, a total of six cores were processed for geotechnical purposes. The dockside processing plan was deleted because of uncertainties caused by recovery procedures and the fact that only three HLC cores were available. Results are summarized

A Fully Non-Metallic Gas Turbine Engine Enabled by Additive Manufacturing

Science.gov (United States)

Grady, Joseph E.; Halbig, Michael C.; Singh, Mrityunjay

2015-01-01

In a NASA Aeronautics Research Institute (NARI) sponsored program entitled "A Fully Non-Metallic Gas Turbine Engine Enabled by Additive Manufacturing", evaluation of emerging materials and additive manufacturing technologies was carried out. These technologies may enable fully non-metallic gas turbine engines in the future. This paper highlights the results of engine system trade studies which were carried out to estimate reduction in engine emissions and fuel burn enabled due to advanced materials and manufacturing processes. A number of key engine components were identified in which advanced materials and additive manufacturing processes would provide the most significant benefits to engine operation. In addition, feasibility of using additive manufacturing technologies to fabricate gas turbine engine components from polymer and ceramic matrix composite were demonstrated. A wide variety of prototype components (inlet guide vanes (IGV), acoustic liners, engine access door) were additively manufactured using high temperature polymer materials. Ceramic matrix composite components included first stage nozzle segments and high pressure turbine nozzle segments for a cooled doublet vane. In addition, IGVs and acoustic liners were tested in simulated engine conditions in test rigs. The test results are reported and discussed in detail.

Processes to Open the Container and the Sample Catcher of the Hayabusa Returned Capsule in the Planetary Material Sample Curation Facility of JAXA

Science.gov (United States)

Fujimura, A.; Abe, M.; Yada, T.; Nakamura, T.; Noguchi, T.; Okazaki, R.; Ishibashi, Y.; Shirai, K.; Okada, T.; Yano, H.;

Data analysis of the 1984 and 1986 soil sampling programs at Materials Disposal Area T in the Los Alamos National Laboratory

International Nuclear Information System (INIS)

Nyhan, J.W.; Drennon, B.J.

1993-09-01

An environmental surveillance program for Materials Disposal Area T (MDA-T) at Los Alamos, New Mexico is described. The waste-use history of this disposal site is described, followed by a description of the materials and methods used to analyze data from two surface soil radionuclide sampling programs performed at this disposal site. The disposal site's physical features are related to the spatial distribution of radionuclide concentration contours in an attempt to evaluate radionuclide migration mechanisms in and around the site. The usefulness of the data analysis efforts is evaluated and recommendations are made for future studies

Innovative methods for inorganic sample preparation

Energy Technology Data Exchange (ETDEWEB)

Essling, A.M.; Huff, E.A.; Graczyk, D.G.

1992-04-01

Procedures and guidelines are given for the dissolution of a variety of selected materials using fusion, microwave, and Parr bomb techniques. These materials include germanium glass, corium-concrete mixtures, and zeolites. Emphasis is placed on sample-preparation approaches that produce a single master solution suitable for complete multielement characterization of the sample. In addition, data are presented on the soil microwave digestion method approved by the Environmental Protection Agency (EPA). Advantages and disadvantages of each sample-preparation technique are summarized.

Innovative methods for inorganic sample preparation

International Nuclear Information System (INIS)

Essling, A.M.; Huff, E.A.; Graczyk, D.G.

1992-04-01

Procedures and guidelines are given for the dissolution of a variety of selected materials using fusion, microwave, and Parr bomb techniques. These materials include germanium glass, corium-concrete mixtures, and zeolites. Emphasis is placed on sample-preparation approaches that produce a single master solution suitable for complete multielement characterization of the sample. In addition, data are presented on the soil microwave digestion method approved by the Environmental Protection Agency (EPA). Advantages and disadvantages of each sample-preparation technique are summarized

Derivation of residual radioactive material guidelines for uranium in soil at the Middlesex Sampling Plant Site, Middlesex, New Jersey

International Nuclear Information System (INIS)

Dunning, D.E.

1995-02-01

Residual radioactive material guidelines for uranium in soil were derived for the Middlesex Sampling Plant (MSP) site in Middlesex, New Jersey. This site has been designated for remedial action under the Formerly Utilized Sites Remedial Action Program (FUSRAP) of the US Department of Energy. The site became contaminated from operations conducted in support of the Manhattan Engineer District (MED) and the Atomic Energy Commission (AEC) between 1943 and 1967. Activities conducted at the site included sampling, storage, and shipment of uranium, thorium, and beryllium ores and residues. Uranium guidelines for single radioisotopes and total uranium were derived on the basis of the requirement that the 50-year committed effective dose equivalent to a hypothetical individual living or working in the immediate vicinity of the MSP site should not exceed a dose of 30 mrem/yr following remedial action for the current-use and likely future-use scenarios or a dose of 100 mrem/yr for less likely future-use scenarios. The RESRAD computer code, which implements the methodology described in the DOE manual for establishing residual radioactive material guidelines, was used in this evaluation. Four scenarios were considered for the site. These scenarios vary regarding future land use at the site, sources of water used, and sources of food consumed

The materials irradiation experiment for testing plasma facing materials at fusion relevant conditions

Energy Technology Data Exchange (ETDEWEB)

Garrison, L. M., E-mail: garrisonlm@ornl.gov; Egle, B. J. [Oak Ridge National Laboratory, 1 Bethel Valley Road, Oak Ridge, Tennessee 37831 (United States); Fusion Technology Institute, University of Wisconsin-Madison, 1500 Engineering Drive, Madison, Wisconsin 53706 (United States); Zenobia, S. J.; Kulcinski, G. L.; Santarius, J. F. [Fusion Technology Institute, University of Wisconsin-Madison, 1500 Engineering Drive, Madison, Wisconsin 53706 (United States)

2016-08-15

The Materials Irradiation Experiment (MITE-E) was constructed at the University of Wisconsin-Madison Inertial Electrostatic Confinement Laboratory to test materials for potential use as plasma-facing materials (PFMs) in fusion reactors. PFMs in fusion reactors will be bombarded with x-rays, neutrons, and ions of hydrogen and helium. More needs to be understood about the interactions between the plasma and the materials to validate their use for fusion reactors. The MITE-E simulates some of the fusion reactor conditions by holding samples at temperatures up to 1000 °C while irradiating them with helium or deuterium ions with energies from 10 to 150 keV. The ion gun can irradiate the samples with ion currents of 20 μA–500 μA; the typical current used is 72 μA, which is an average flux of 9 × 10{sup 14} ions/(cm{sup 2} s). The ion gun uses electrostatic lenses to extract and shape the ion beam. A variable power (1-20 W), steady-state, Nd:YAG laser provides additional heating to maintain a constant sample temperature during irradiations. The ion beam current reaching the sample is directly measured and monitored in real-time during irradiations. The ion beam profile has been investigated using a copper sample sputtering experiment. The MITE-E has successfully been used to irradiate polycrystalline and single crystal tungsten samples with helium ions and will continue to be a source of important data for plasma interactions with materials.

Critical assessment of the performance of electronic moisture analyzers for small amounts of environmental samples and biological reference materials.

Science.gov (United States)

Krachler, M

2001-12-01

Two electronic moisture analyzers were critically evaluated with regard to their suitability for determining moisture in small amounts (environmental matrices such as leaves, needles, soil, peat, sediments, and sewage sludge, as well as various biological reference materials. To this end, several homogeneous bulk materials were prepared which were subsequently employed for the development and optimization of all analytical procedures. The key features of the moisture analyzers included a halogen or ceramic heater and an integrated balance with a resolution of 0.1 mg, which is an essential prerequisite for obtaining precise results. Oven drying of the bulk materials in a conventional oven at 105 degrees C until constant mass served as reference method. A heating temperature of 65degrees C was found to provide accurate and precise results for almost all matrices investigated. To further improve the accuracy and precision, other critical parameters such as handling of sample pans, standby temperature, and measurement delay were optimized. Because of its ponderous heating behavior, the performance of the ceramic radiator was inferior to that of the halogen heater, which produced moisture results comparable to those obtained by oven drying. The developed drying procedures were successfully applied to the fast moisture analysis (1.4-6.3 min) of certified biological reference materials of similar provenance to the investigated the bulk materials. Moisture results for 200 mg aliquots ranged from 1.4 to 7.8% and good agreement was obtained between the recommended drying procedure for the reference materials and the electronic moisture analyzers with absolute uncertainties amounting to 0.1% and 0.2-0.3%, respectively.

40 CFR Appendix I to Part 261 - Representative Sampling Methods

Science.gov (United States)

2010-07-01

... 40 Protection of Environment 25 2010-07-01 2010-07-01 false Representative Sampling Methods I...—Representative Sampling Methods The methods and equipment used for sampling waste materials will vary with the form and consistency of the waste materials to be sampled. Samples collected using the sampling...

BWRVIP-123, Revision 1NP: BWR Vessel and Internals Project Removal and Analysis of Material Samples from Core Shroud and Top Guide at Susquehanna Unit 2

International Nuclear Information System (INIS)

Howell, D.; Haertel, T.; Lindberg, J.; Oliver, B.; Greenwood, L.

2005-01-01

Fast and thermal fluence were determined by a laboratory analysis of the samples. Fluence in the upper regions of the shroud (between the H1 and H2 welds) was substantially lower than that in the belt line region (near the H4 weld). Fluence in the top guide was significantly higher than fluence on the core shroud. As expected, helium concentrations were highest in regions where fluence was highest. Estimates of the initial boron concentration were similar to measurements made on materials removed from other reactors. A technical justification evaluated the acceptability of the sampling process with respect to structural consequences of material removal and to increased cracking susceptibility due to the as-left condition. It was determined that the sampling process was acceptable on both counts

Sampling in practice

DEFF Research Database (Denmark)

Esbensen, Kim Harry; Petersen, Lars

2005-01-01

A basic knowledge of the Theory of Sampling (TOS) and a set of only eight sampling unit operations is all the practical sampler needs to ensure representativeness of samples extracted from all kinds of lots: production batches, - truckloads, - barrels, sub-division in the laboratory, sampling...... in nature and in the field (environmental sampling, forestry, geology, biology), from raw materials or manufactory processes etc. We here can only give a brief introduction to the Fundamental Sampling Principle (FSP) and these eight Sampling Unit Operations (SUO’s). Always respecting FSP and invoking only...... the necessary SUO’s (dependent on the practical situation) is the only prerequisite needed for eliminating all sampling bias and simultaneously minimizing sampling variance, and this is in addition a sure guarantee for making the final analytical results trustworthy. No reliable conclusions can be made unless...

Theory of sampling: four critical success factors before analysis.

Science.gov (United States)

Wagner, Claas; Esbensen, Kim H

2015-01-01

Food and feed materials characterization, risk assessment, and safety evaluations can only be ensured if QC measures are based on valid analytical data, stemming from representative samples. The Theory of Sampling (TOS) is the only comprehensive theoretical framework that fully defines all requirements to ensure sampling correctness and representativity, and to provide the guiding principles for sampling in practice. TOS also defines the concept of material heterogeneity and its impact on the sampling process, including the effects from all potential sampling errors. TOS's primary task is to eliminate bias-generating errors and to minimize sampling variability. Quantitative measures are provided to characterize material heterogeneity, on which an optimal sampling strategy should be based. Four critical success factors preceding analysis to ensure a representative sampling process are presented here.

Supporting online materials for mineralogy and petrology of Comet81P/Wild 2 nucleus samples

Energy Technology Data Exchange (ETDEWEB)

Zolensky, Michael E.; Zega, Thomas J.; Yano, Hajime; Wirick, Sue; Westphal, Andrew J.; Weisberg, Mike K.; Weber, Iris; Warren, Jack L.; Velbel, Michael A.; Tsuchiyama, Akira; Tsou, Peter; Toppani, Alice; Tomioka, Naotaka; Tomeoka, Kazushige; Teslich, Nick; Taheri, Mitra; Susini, Jean; Stroud, Rhonda; Stephan, Thomas; Stadermann, Frank J.; Snead, Christopher J.; Simon, Steven B.; Simionovici, Alexandre; See,Thomas H.; Robert Francois; Rietmeijer, Frans J.M.; Rao, William; Perronnet, Murielle C.; Papanastassiou, Dimitri A.; Okudaira, Kyoko; Ohsumi, Kazumasa; Ohnishi, Ichiro; Nakamura-Messenger, Keilo; Nakamura,Tomoki; Mostefaoui, Smail; Mikouchi, Takashi; Meibom, Anders; Matrajt,Graciela; Marcus, Matthew A.; Leroux, Hugues; Lemelle, Laurence; Antonio,Loan Le; Lanzirotti, Antonio; Langenhorst, Falko; Krot, Alexander N.; Keller, Lindsay P.; Kearsley, Anton T.; Joswiak, Davis; Jacob, Damien; Ishii, Hope; Harvey, Ralph; Hagiya, Kenji; Grossman, Lawrence; Grossman,Jeffrey N.; Graham, Giles A.; Gounelle, Matthieu; Gillet, Philippe; Genge, Matthew J.; Flynn, George; Ferroir, Tristan; Fallow, Stewart; Ebel, Denton S.; Dai, Zu Rong; Cordier, Patrick; Clark, Benton; Chi,Miaofang; Butterworth, Anna L.; Brownlee, Donald E.; Bridges, John C.; Brennan, Sean; Brearley, Adrian; Bradley, John P.; Bleuet, Pierre; Bland,Phil A.; Bastien, Ron

2006-01-01

The bulk of the comet 81P/Wild 2 (hereafter Wild 2) samples returned to Earth by the Stardust spacecraft appear to be weakly constructed mixtures of nanometer-scale grains, with occasional much larger (over 1 micrometer) ferromagnesian silicates, Fe-Ni sulfides, Fe-Ni metal, and accessory phases. The very wide range of olivine and low-Ca pyroxene compositions in comet Wild 2 requires a wide range of formation conditions, probably reflecting very different formation locations in the protoplanetary disk. The restricted compositional ranges of Fe-Ni sulfides, the wide range for silicates, and the absence of hydrous phases indicate that comet Wild 2 experienced little or no aqueous alteration. Less abundant Wild 2 materials include a refractory particle, whose presence appears to require radial transport in the early protoplanetary disk.

Ultra low injection angle fuel holes in a combustor fuel nozzle

Science.gov (United States)

York, William David

2012-10-23

A fuel nozzle for a combustor includes a mixing passage through which fluid is directed toward a combustion area and a plurality of swirler vanes disposed in the mixing passage. Each swirler vane of the plurality of swirler vanes includes at least one fuel hole through which fuel enters the mixing passage in an injection direction substantially parallel to an outer surface of the plurality of swirler vanes thereby decreasing a flameholding tendency of the fuel nozzle. A method of operating a fuel nozzle for a combustor includes flowing a fluid through a mixing passage past a plurality of swirler vanes and injecting a fuel into the mixing passage in an injection direction substantially parallel to an outer surface of the plurality of swirler vanes.

Waste classification sampling plan

International Nuclear Information System (INIS)

Landsman, S.D.

1998-01-01

The purpose of this sampling is to explain the method used to collect and analyze data necessary to verify and/or determine the radionuclide content of the B-Cell decontamination and decommissioning waste stream so that the correct waste classification for the waste stream can be made, and to collect samples for studies of decontamination methods that could be used to remove fixed contamination present on the waste. The scope of this plan is to establish the technical basis for collecting samples and compiling quantitative data on the radioactive constituents present in waste generated during deactivation activities in B-Cell. Sampling and radioisotopic analysis will be performed on the fixed layers of contamination present on structural material and internal surfaces of process piping and tanks. In addition, dose rate measurements on existing waste material will be performed to determine the fraction of dose rate attributable to both removable and fixed contamination. Samples will also be collected to support studies of decontamination methods that are effective in removing the fixed contamination present on the waste. Sampling performed under this plan will meet criteria established in BNF-2596, Data Quality Objectives for the B-Cell Waste Stream Classification Sampling, J. M. Barnett, May 1998

Proteomic Challenges: Sample Preparation Techniques for Microgram-Quantity Protein Analysis from Biological Samples

Directory of Open Access Journals (Sweden)

Peter Feist

2015-02-01

Full Text Available Proteins regulate many cellular functions and analyzing the presence and abundance of proteins in biological samples are central focuses in proteomics. The discovery and validation of biomarkers, pathways, and drug targets for various diseases can be accomplished using mass spectrometry-based proteomics. However, with mass-limited samples like tumor biopsies, it can be challenging to obtain sufficient amounts of proteins to generate high-quality mass spectrometric data. Techniques developed for macroscale quantities recover sufficient amounts of protein from milligram quantities of starting material, but sample losses become crippling with these techniques when only microgram amounts of material are available. To combat this challenge, proteomicists have developed micro-scale techniques that are compatible with decreased sample size (100 μg or lower and still enable excellent proteome coverage. Extraction, contaminant removal, protein quantitation, and sample handling techniques for the microgram protein range are reviewed here, with an emphasis on liquid chromatography and bottom-up mass spectrometry-compatible techniques. Also, a range of biological specimens, including mammalian tissues and model cell culture systems, are discussed.

Proteomic Challenges: Sample Preparation Techniques for Microgram-Quantity Protein Analysis from Biological Samples

Science.gov (United States)

Feist, Peter; Hummon, Amanda B.

2015-01-01

Proteins regulate many cellular functions and analyzing the presence and abundance of proteins in biological samples are central focuses in proteomics. The discovery and validation of biomarkers, pathways, and drug targets for various diseases can be accomplished using mass spectrometry-based proteomics. However, with mass-limited samples like tumor biopsies, it can be challenging to obtain sufficient amounts of proteins to generate high-quality mass spectrometric data. Techniques developed for macroscale quantities recover sufficient amounts of protein from milligram quantities of starting material, but sample losses become crippling with these techniques when only microgram amounts of material are available. To combat this challenge, proteomicists have developed micro-scale techniques that are compatible with decreased sample size (100 μg or lower) and still enable excellent proteome coverage. Extraction, contaminant removal, protein quantitation, and sample handling techniques for the microgram protein range are reviewed here, with an emphasis on liquid chromatography and bottom-up mass spectrometry-compatible techniques. Also, a range of biological specimens, including mammalian tissues and model cell culture systems, are discussed. PMID:25664860

Proteomic challenges: sample preparation techniques for microgram-quantity protein analysis from biological samples.

Science.gov (United States)

Feist, Peter; Hummon, Amanda B

2015-02-05

Proteins regulate many cellular functions and analyzing the presence and abundance of proteins in biological samples are central focuses in proteomics. The discovery and validation of biomarkers, pathways, and drug targets for various diseases can be accomplished using mass spectrometry-based proteomics. However, with mass-limited samples like tumor biopsies, it can be challenging to obtain sufficient amounts of proteins to generate high-quality mass spectrometric data. Techniques developed for macroscale quantities recover sufficient amounts of protein from milligram quantities of starting material, but sample losses become crippling with these techniques when only microgram amounts of material are available. To combat this challenge, proteomicists have developed micro-scale techniques that are compatible with decreased sample size (100 μg or lower) and still enable excellent proteome coverage. Extraction, contaminant removal, protein quantitation, and sample handling techniques for the microgram protein range are reviewed here, with an emphasis on liquid chromatography and bottom-up mass spectrometry-compatible techniques. Also, a range of biological specimens, including mammalian tissues and model cell culture systems, are discussed.

Sample environment for neutron scattering measurements of internal stresses in engineering materials in the temperature range of 6 K to 300 K.

Science.gov (United States)

Kirichek, O; Timms, J D; Kelleher, J F; Down, R B E; Offer, C D; Kabra, S; Zhang, S Y

2017-02-01

Internal stresses in materials have a considerable effect on material properties including strength, fracture toughness, and fatigue resistance. The ENGIN-X beamline is an engineering science facility at ISIS optimized for the measurement of strain and stress using the atomic lattice planes as a strain gauge. Nowadays, the rapidly rising interest in the mechanical properties of engineering materials at low temperatures has been stimulated by the dynamic development of the cryogenic industry and the advanced applications of the superconductor technology. Here we present the design and discuss the test results of a new cryogenic sample environment system for neutron scattering measurements of internal stresses in engineering materials under a load of up to 100 kN and in the temperature range of 6 K to 300 K. Complete cooling of the system starting from the room temperature down to the base temperature takes around 90 min. Understanding of internal stresses in engineering materials at cryogenic temperatures is vital for the modelling and designing of cutting-edge superconducting magnets and other superconductor based applications.

Boat sampling technique for assessment of ageing of components

International Nuclear Information System (INIS)

Kumar, Kundan; Shyam, T.V.; Kayal, J.N.; Rupani, B.B.

2006-01-01

Boat sampling technique (BST) is a surface sampling technique, which has been developed for obtaining, in-situ, metal samples from the surface of an operating component without affecting its operating service life. The BST is non-destructive in nature and the sample is obtained without plastic deformation or without thermal degradation of the parent material. The shape and size of the sample depends upon the shape of the cutter and the surface geometry of the parent material. Miniature test specimens are generated from the sample and the specimens are subjected to various tests, viz. Metallurgical Evaluation, Metallographic Evaluation, Micro-hardness Evaluation, sensitisation test, small punch test etc. to confirm the integrity and assessment of safe operating life of the component. This paper highlights design objective of boat sampling technique, description of sampling module, sampling cutter and its performance evaluation, cutting process, boat samples, operational sequence of sampling module, qualification of sampling module, qualification of sampling technique, qualification of scooped region of the parent material, sample retrieval system, inspection, testing and examination to be carried out on the boat samples and scooped region. (author)

40 CFR 761.323 - Sample preparation.

Science.gov (United States)

2010-07-01

... 40 Protection of Environment 30 2010-07-01 2010-07-01 false Sample preparation. 761.323 Section... Remediation Waste Samples § 761.323 Sample preparation. (a) The comparison study requires analysis of a... concentrations by dilution. Any excess material resulting from the preparation of these samples, which is not...

Microstructure Based Material-Sand Particulate Interactions and Assessment of Coatings for High Temperature Turbine Blades

Science.gov (United States)

Murugan, Muthuvel; Ghoshal, Anindya; Walock, Michael; Nieto, Andy; Bravo, Luis; Barnett, Blake; Pepi, Marc; Swab, Jeffrey; Pegg, Robert Tyler; Rowe, Chris;

Minutes of the 28th Annual Plutonium Sample Exchange Meeting. Part II: metal sample exchange

International Nuclear Information System (INIS)

1984-01-01

Contents of this publication include the following list of participating laboratories; agenda; attendees; minutes of October 25 and 26 meeting; and handout materials supplied by speakers. The handout materials cover the following: statistics and reporting; plutonium - chemical assay 100% minus impurities; americium neptunium, uranium, carbon and iron data; emission spectroscopy data; plutonium metal sample exchange; the calorimetry sample exchange; chlorine determination in plutonium metal using phyrohydrolysis; spectrophotometric determination of 238-plutonium in oxide; plutonium measurement capabilities at the Savannah River Plant; and robotics in radiochemical laboratory

Materials and Life Science Experimental Facility at the Japan Proton Accelerator Research Complex III: Neutron Devices and Computational and Sample Environments

Directory of Open Access Journals (Sweden)

Kaoru Sakasai

2017-08-01

Full Text Available Neutron devices such as neutron detectors, optical devices including supermirror devices and 3He neutron spin filters, and choppers are successfully developed and installed at the Materials Life Science Facility (MLF of the Japan Proton Accelerator Research Complex (J-PARC, Tokai, Japan. Four software components of MLF computational environment, instrument control, data acquisition, data analysis, and a database, have been developed and equipped at MLF. MLF also provides a wide variety of sample environment options including high and low temperatures, high magnetic fields, and high pressures. This paper describes the current status of neutron devices, computational and sample environments at MLF.

Vortex Generators in a Streamline-Traced, External-Compression Supersonic Inlet

Science.gov (United States)

Baydar, Ezgihan; Lu, Frank K.; Slater, John W.; Trefny, Charles J.

2017-01-01

Vortex generators within a streamline-traced, external-compression supersonic inlet for Mach 1.66 were investigated to determine their ability to increase total pressure recovery and reduce total pressure distortion. The vortex generators studied were rectangular vanes arranged in counter-rotating and co-rotating arrays. The vane geometric factors of interest included height, length, spacing, angle-of-incidence, and positions upstream and downstream of the inlet terminal shock. The flow through the inlet was simulated numerically through the solution of the steady-state, Reynolds-averaged Navier-Stokes equations on multi-block, structured grids using the Wind-US flow solver. The vanes were simulated using a vortex generator model. The inlet performance was characterized by the inlet total pressure recovery and the radial and circumferential total pressure distortion indices at the engine face. Design of experiments and statistical analysis methods were applied to quantify the effect of the geometric factors of the vanes and search for optimal vane arrays. Co-rotating vane arrays with negative angles-of-incidence positioned on the supersonic diffuser were effective in sweeping low-momentum flow from the top toward the sides of the subsonic diffuser. This distributed the low-momentum flow more evenly about the circumference of the subsonic diffuser and reduced distortion. Co-rotating vane arrays with negative angles-of-incidence or counter-rotating vane arrays positioned downstream of the terminal shock were effective in mixing higher-momentum flow with lower-momentum flow to increase recovery and decrease distortion. A strategy of combining a co-rotating vane array on the supersonic diffuser with a counter-rotating vane array on the subsonic diffuser was effective in increasing recovery and reducing distortion.

Research of performance prediction to energy on hydraulic turbine

International Nuclear Information System (INIS)

Quan, H; Li, R N; Li, Q F; Han, W; Su, Q M

2012-01-01

Refer to the low specific speed Francis turbine blade design principle and double-suction pump structure. Then, design a horizontal double-channel hydraulic turbine Francis. Through adding different guide vane airfoil and and no guide vane airfoil on the hydraulic conductivity components to predict hydraulic turbine energy and using Fluent software to numerical simulation that the operating conditions and point. The results show that the blade pressure surface and suction surface pressure is low when the hydraulic turbine installation is added standard positive curvature of the guide vane and modified positive curvature of guide vane. Therefore, the efficiency of energy recovery is low. However, the pressure of negative curvature guide vane and symmetric guide vane added on hydraulic turbine installations is larger than that of the former ones, and it is conducive to working of runner. With the decreasing of guide vane opening, increasing of inlet angle, flow state gets significantly worse. Then, others obvious phenomena are that the reflux and horizontal flow appeared in blade pressure surface. At the same time, the vortex was formed in Leaf Road, leading to the loss of energy. Through analyzing the distribution of pressure, velocity, flow lines of over-current flow in the the back hydraulic conductivity components in above programs we can known that the hydraulic turbine installation added guide vane is more reasonable than without guide vanes, it is conducive to improve efficiency of energy conversion.

Study of High Efficiency Flow Regulation of VIGV in Centrifugal Compressor

Directory of Open Access Journals (Sweden)

Chunjun Ji

2016-01-01

Full Text Available Variable inlet guide vane (VIGV is used to control the mass flow and generate prewhirl in centrifugal compressors. Due to the tip clearance of the guide vanes and the defect of the traditional guide vane profiles, the mass flow regulation of VIGV is limited, resulting in a large waste of compressed gas. Two kinds of inlet flow channels were proposed to eliminate the influence of tip clearance. These structures were numerically investigated at different setting angles. The results show that the improved channels not only expand the range of mass flow regulation, but also reduce the power and increase the efficiency of the compressor. Ten kinds of guide vane profiles, including different thickness distribution, camber line profile, were selected to compare with the original one and with each other. In the premise of ensuring the performance of compressor, the best guide vane profile was selected. The results show that reducing the guide vane thickness, increasing the guide vane camber angle, and increasing the distance between the maximum camber position and the leading edge of guide vane can help expand the range of mass flow regulation. The achievement of this research can effectively improve the flow regulation ability of VIGV and the performance of compressor.

NEW TECHNOLOGIES FOR RESTORATION AND PROTECTION OF POWER EQUIPMENT WITH THE AID OF COMPOSITE MATERIALS

Directory of Open Access Journals (Sweden)

A. O. Ischenko

2017-01-01

Full Text Available The analysis of possible variants of reconstruction of the power equipment is fulfilled and the conclusion concerning the prospects of such work with the use of composite materials is reached. The data on the technical characteristics of composite repair materials for various purposes are presented, the results of repairs of power equipment, in particular the technology for the recovery of the boarding surfaces of the diffuser rings and protection of the pumps D1250 casings are provided. The technology of the recovery pneumatic cylinder, hydraulic cylinder rod, as well as the unique technology of restoration of working surfaces of the impeller vanes of transfer pump, that had been destroyed by corrosion in conjunction with the cavitation processes and were considered as not restorable is described. The restored impeller was in operation during a year and only thereafter it was removed for restoration. Another composite material discussed in the article – diagum – makes it possible to perform a series of repairs associated with restoration of the rubber-covered surfaces of pump casings as well as with restoration of various surfaces of the conveyor belts. Taking the excellent adhesive properties of this composite into account, restoration of worn stainless steel sieve screens to remove abrasive material was fulfilled with the aid of it. The restoration was accomplished via the use of the conveyor belt which application time had expired, that was glued to a metal sieve with diagum. The use of the composites is economically justified, because the application of them in repairs reduces, firstly, terms of restoration work and, secondly, the price of repairs. Third, equipment that was damaged beyond repair is being commissioned by the use of the mentioned composites. 

Material classification by fast neutron scattering

Energy Technology Data Exchange (ETDEWEB)

Buffler, A. E-mail: abuffler@physci.uct.ac.za; Brooks, F.D. E-mail: brooks@physci.uct.ac.za; Allie, M.S.; Bharuth-Ram, K.; Nchodu, M.R

2001-02-01

The scattering of a beam of fast monoenergetic neutrons is used to determine elemental compositions of bulk samples (0.2-0.8 kg) of materials composed from one or more of the elements H, C, N, O, Al, S, Fe and Pb. Scattered neutrons are detected by liquid scintillators placed at forward and at backward angles. Different elements are identified by their characteristic scattering signatures derived either from a combination of time-of-flight and pulse height measurements, or from pulse height measurements alone. Scattering signatures measured for multi-element samples are analysed to determine atom fractions for H, C, N, O and other elements in the sample. Atom fractions determined from scattering signatures are insensitive to neutron interactions in material surrounding the scattering sample, provided the amount of material is not excessive. The atom fraction data are used to classify scattering material into categories including 'explosives', 'illicit drugs' and 'other materials' for the purpose of contraband detection.

An Inset CT Specimen for Evaluating Fracture in Small Samples of Material

Science.gov (United States)

Yahyazadehfar, M.; Nazari, A.; Kruzic, J.J.; Quinn, G.D.; Arola, D.

2013-01-01

In evaluations on the fracture behavior of hard tissues and many biomaterials, the volume of material available to study is not always sufficient to apply a standard method of practice. In the present study an inset Compact Tension (inset CT) specimen is described, which uses a small cube of material (approximately 2×2×2 mm3) that is molded within a secondary material to form the compact tension geometry. A generalized equation describing the Mode I stress intensity was developed for the specimen using the solutions from a finite element model that was defined over permissible crack lengths, variations in specimen geometry, and a range in elastic properties of the inset and mold materials. A validation of the generalized equation was performed using estimates for the fracture toughness of a commercial dental composite via the “inset CT” specimen and the standard geometry defined by ASTM E399. Results showed that the average fracture toughness obtained from the new specimen (1.23 ± 0.02 MPa•m0.5) was within 2% of that from the standard. Applications of the inset CT specimen are presented for experimental evaluations on the crack growth resistance of dental enamel and root dentin, including their fracture resistance curves. Potential errors in adopting this specimen are then discussed, including the effects of debonding between the inset and molding material on the estimated stress intensity distribution. Results of the investigation show that the inset CT specimen offers a viable approach for studying the fracture behavior of small volumes of structural materials. PMID:24268892

Hot sample archiving. Revision 3

International Nuclear Information System (INIS)

McVey, C.B.

1995-01-01

This Engineering Study revision evaluated the alternatives to provide tank waste characterization analytical samples for a time period as recommended by the Tank Waste Remediation Systems Program. The recommendation of storing 40 ml segment samples for a period of approximately 18 months (6 months past the approval date of the Tank Characterization Report) and then composite the core segment material in 125 ml containers for a period of five years. The study considers storage at 222-S facility. It was determined that the critical storage problem was in the hot cell area. The 40 ml sample container has enough material for approximately 3 times the required amount for a complete laboratory re-analysis. The final result is that 222-S can meet the sample archive storage requirements. During the 100% capture rate the capacity is exceeded in the hot cell area, but quick, inexpensive options are available to meet the requirements

Study of Material Compatibility for a Thermal Energy Storage System with Phase Change Material

Directory of Open Access Journals (Sweden)

Songgang Qiu

2018-03-01

Full Text Available The suitability of stainless steel 316L and Inconel 625 for use in a latent heat thermal energy storage (TES system was investigated. A NaCl–NaF eutectic mixture with a melting temperature of 680 °C was used as the phase change material (PCM. Containers were filled with the PCM prior to heating to 750 °C, then examined after 100 and 2500 h of high-temperature exposure by analyzing the material surface and cross-section areas. A small amount of corrosion was present in both samples after 100 h. Neither sample suffered significant damage after 2500 h. The undesirable inter-granular grain boundary attack found in SS316L samples was in the order of 1–2 µm in depth. On Inconel 625 sample surface, an oxide complex formed, resisting material dissolution into the PCM. The surface morphology of tested samples remained largely unchanged after 2500 h, but the corrosion pattern changed from an initially localized corrosion penetration to a more uniform type. After 2500 h, the corrosion depth of Inconel 625 remained at roughly 1–2 µm, indicating that the corrosion rate decelerated. Both materials demonstrated good compatibility with the chosen NaF–NaCl eutectic salt, but the low corrosion activity in Inconel 625 samples shows a performance advantage for long term operation.

Evaluation of Sampling Methods for Bacillus Spore ...

Science.gov (United States)

Journal Article Following a wide area release of biological materials, mapping the extent of contamination is essential for orderly response and decontamination operations. HVAC filters process large volumes of air and therefore collect highly representative particulate samples in buildings. HVAC filter extraction may have great utility in rapidly estimating the extent of building contamination following a large-scale incident. However, until now, no studies have been conducted comparing the two most appropriate sampling approaches for HVAC filter materials: direct extraction and vacuum-based sampling.

Rheology Modifiers Applied to Kaolin-Bentonite Slurries for SRNL WTP Pulse Jets Tank Pilot Work in Support of RPP at Hanford

International Nuclear Information System (INIS)

WILLIAM, DANIEL

2005-01-01

would be too low. The addition of Laponite (R) (synthetic lithium aluminum silicate) increased the vane yield stress of the clay slurry to values as high as 1500 Pa. However, the flow curve behavior for the laponite samples was not predictable and the secondary objective was dropped based on customer needs and time constraints. Ultimately a 3-wt percent addition of Laponite (R) was chosen to produce a 600 Pa vane yield stress mixture

Isotope dilution analysis of environmental samples

International Nuclear Information System (INIS)

Tolgyessy, J.; Lesny, J.; Korenova, Z.; Klas, J.; Klehr, E.H.

1986-01-01

Isotope dilution analysis has been used for the determination of several trace elements - especially metals - in a variety of environmental samples, including aerosols, water, soils, biological materials and geological materials. Variations of the basic concept include classical IDA, substoichiometric IDA, and more recently, sub-superequivalence IDA. Each variation has its advantages and limitations. A periodic chart has been used to identify those elements which have been measured in environmental samples using one or more of these methods. (author)

Biopolymers for sample collection, protection, and preservation.

Science.gov (United States)

Sorokulova, Iryna; Olsen, Eric; Vodyanoy, Vitaly

2015-07-01

One of the principal challenges in the collection of biological samples from air, water, and soil matrices is that the target agents are not stable enough to be transferred from the collection point to the laboratory of choice without experiencing significant degradation and loss of viability. At present, there is no method to transport biological samples over considerable distances safely, efficiently, and cost-effectively without the use of ice or refrigeration. Current techniques of protection and preservation of biological materials have serious drawbacks. Many known techniques of preservation cause structural damages, so that biological materials lose their structural integrity and viability. We review applications of a novel bacterial preservation process, which is nontoxic and water soluble and allows for the storage of samples without refrigeration. The method is capable of protecting the biological sample from the effects of environment for extended periods of time and then allows for the easy release of these collected biological materials from the protective medium without structural or DNA damage. Strategies for sample collection, preservation, and shipment of bacterial, viral samples are described. The water-soluble polymer is used to immobilize the biological material by replacing the water molecules within the sample with molecules of the biopolymer. The cured polymer results in a solid protective film that is stable to many organic solvents, but quickly removed by the application of the water-based solution. The process of immobilization does not require the use of any additives, accelerators, or plastifiers and does not involve high temperature or radiation to promote polymerization.

Sampling and analysis plan for the consolidated sludge samples from the canisters and floor of the 105-K East basin

International Nuclear Information System (INIS)

BAKER, R.B.

1999-01-01

This Sampling and Analysis Plan (SAP) provides direction for sampling of fuel canister and floor Sludge from the K East Basin to complete the inventory of samples needed for Sludge treatment process testing. Sample volumes and sources consider recent reviews made by the Sludge treatment subproject. The representative samples will be characterized to the extent needed for the material to be used effectively for testing. Sampling equipment used allows drawing of large volume sludge samples and consolidation of sample material from a number of basin locations into one container. Once filled, the containers will be placed in a cask and transported to Hanford laboratories for recovery and evaluation. Included in the present SAP are the logic for sample location selection, laboratory analysis procedures required, and reporting needed to meet the Data Quality Objectives (DQOs) for this initiative

Geotechnical properties of ash deposits near Hilo, Hawaii

Science.gov (United States)

Wieczorek, G.F.; Jibson, R.W.; Wilson, R.C.; Buchanan-Banks, J. M.

1982-01-01

Two holes were hand augered and sampled in ash deposits near Hilo, Hawaii. Color, water content and sensitivity of the ash were measured in the field. The ash alternated between reddish brown and dark reddish brown in color and had water contents as high as 392%. A downhole vane shear device measured sensitivities as high as 6.9. A series of laboratory tests including grain size distribution, Atterberg limits, X-ray diffraction analysis, total carbon determination, vane shear, direct shear and triaxial tests were performed to determine the composition and geotechnical properties of the ash. The ash is very fine grained, highly plastic and composed mostly of gibbsite and amorphous material presumably allophane. The ash has a high angle of internal friction ranging from 40-43? and is classified as medium to very sensitive. A series of different ash layers was distinguished on the basis of plasticity and other geotechnical properties. Sensitivity may be due to a metastable fabric, cementation, leaching, high organic content, and thixotropy. The sensitivity of the volcanic ash deposits near Hilo is consistent with documented slope instability during earthquakes in Hawaii. The high angles of internal friction and cementation permit very steep slopes under static conditions. However, because of high sensitivity of the ash, these slopes are particularly susceptible to seismically-induced landsliding.

Sea Ice as a Sink for CO2 and Biogeochemical Material: a Novel Sampling Method and Astrobiological Applications

Science.gov (United States)

Wilner, J.; Hofmann, A.; Hand, K. P.

2017-12-01

Accurately modelling the intensification of greenhouse gas effects in the polar regions ("polar amplification") necessitates a thorough understanding of the geochemical balance between atmospheric, sea ice, and oceanic layers. Sea ice is highly permeable to CO2 and therefore represents a major sink of oceanic CO2 in winter and of atmospheric CO2 in summer, sinks that are typically either poorly constrained in or fully absent from global climate models. We present a novel method for sampling both trapped and dissolved gases (CO2, CH4 and δ13CH4) in sea ice with a Picarro 2132-i Methane Analyzer, taking the following sampling considerations into account: minimization of water and air contamination, full headspace sampling, prevention of inadvertent sample bag double-puncturing, and ease of use. This method involves melting of vacuum-sealed ice cores to evacuate trapped gases to the headspace and sampling the headspace gas with a blunt needle sheathed by a beveled puncturing needle. A gravity catchment tube prevents input of dangerous levels of liquid water to the Picarro cavity. Subsequent ultrasonic degassing allows for dissolved gas measurement. We are in the process of using this method to sample gases trapped and dissolved in Arctic autumn sea ice cores and atmospheric samples collected during the 2016 Polarstern Expedition and during a May 2017 field campaign north of Barrow, Alaska. We additionally employ this method, together with inductively coupled plasma mass spectrometry (ICP-MS), to analyze the transfer of potential biogeochemical signatures of underlying hydrothermal plumes to sea ice. This has particular relevance to Europa and Enceladus, where hypothetical hydrothermal plumes may deliver seafloor chemicals to the overlying ice shell. Hence, we are presently investigating the entrainment of methane and other hydrothermal material in sea ice cores collected along the Gakkel Ridge that may serve as biosignatures of methanogenic organisms in seafloor

Quantitative NMR measurements on core samples

International Nuclear Information System (INIS)

Olsen, Dan

1997-01-01

Within the frame of an EFP-95 project NMR methods for porosity determination in 2D, and for fluid saturation determination in 1D and 2D have been developed. The three methods have been developed and tested on cleaned core samples of chalk from the Danish North Sea. The main restriction for the use of the methods is the inherently short T2 relaxation constants of rock samples. Referring to measurements conducted at 200 MHz, the 2D porosity determination method is applicable to sample material with T2 relaxation constants down to 5 ms. The 1D fluid saturation determination method is applicable to sample material with T2 relaxation constants down to 3 ms, while the 2D fluid saturation determination method is applicable to material with T2 relaxation constants down to 8 ms. In the case of the 2D methods these constraints as a minimum enables work on the majority of chalk samples of Maastrichtian age. The 1D fluid saturation determination method in addition is applicable to at least some chalk samples of Danian and pre-Maastrichtian age. The spatial resolution of the 2D porosity determination method, the 1D fluid saturation methods, and the 2D fluid saturation method is respectively 0.8 mm, 0.8 mm and 2 mm. Reproducibility of pixel values is for all three methods 2%- points. (au)

Collection and identification of human remains volatiles by non-contact, dynamic airflow sampling and SPME-GC/MS using various sorbent materials.

Science.gov (United States)

DeGreeff, Lauryn E; Furton, Kenneth G

2011-09-01

Human remains detection canines are used in locating deceased humans in diverse scenarios and environments based on odor produced during the decay process of the human body. It has been established that human remains detection canines are capable of locating human remains specifically, as opposed to living humans or animal remains, thus suggesting a difference in odor between the different sources. This work explores the collection and determination of such odors using a dynamic headspace concentration device. The airflow rate and three sorbent materials-Dukal cotton gauze, Johnson & Johnson cotton-blend gauze, and polyester material-used for odor collection were evaluated using standard compounds. It was determined that higher airflow rates and openly woven material, e.g., Dukal cotton gauze, yielded significantly less total volatile compounds due to compound breakthrough through the sorbent material. Collection from polymer- and cellulose-based materials demonstrated that the molecular backbone of the material is a factor in compound collection as well. Volatiles, including cyclic and straight-chain hydrocarbons, organic acids, sulfides, aldehydes, ketones, and alcohols, were collected from a population of 27 deceased bodies from two collection locations. The common compounds between the subjects were compared and the odor profiles were determined. These odor profiles were compared with those of animal remains and living human subjects collected in the same manner. Principal component analysis showed that the odor profiles of the three sample types were distinct.

Experimental investigation of hinged and spring loaded rolling piston compressors pertaining to a turbo rotary engine

International Nuclear Information System (INIS)

Okur, Melih; Akmandor, Ibrahim Sinan

2011-01-01

Hinged rolling piston compressor of a new thermodynamic cycle Pars engine promises high performance figures such as single stage high compression levels and higher volume flow discharge with competitively low input power and torque. The pumping characteristic of the present engine compressor unit has been increased by the implementation of a spring less vane configuration. The reciprocating vane which is usually operated by spring compression in air conditioning and refrigeration unit has been replaced by a hinge vane mechanism. At high speeds, the conventional spring loaded vane which is forced against the eccentrically moving rotor periphery does disconnect and starts rocking. With the new configuration, this mishap has been eliminated and subsequently resulting compressor pressure leaks have been avoided. Compressor experiments have been carried out at predetermined rotor speeds and compressed volume flow amounts and required shaft powers have been measured and derived accordingly. Experimentally determined pressure-volume relations have been compared with isentropic, isothermal, isochoric compressions as well as isobaric process. It is seen that at lower speeds, hinged vane compression is half way between isentropic and isochoric compressions whereas at high speed the compression process approaches further isochoric compression behavior. The isentropic compression efficiency of the hinged vane compressor is around 85% for pressures reaching 9 atm. - Research highlights: → Volume flow rate of rotary vane compressor unit has been increased by a hinged vane mechanism. → Hinged compressor pressure output is almost twice the performance of a spring loaded compressor. → The slipping and rocking of the spring loaded vane against the rolling piston have been eliminated.

Influence of the positive prewhirl on the performance of centrifugal pumps with different airfoils

International Nuclear Information System (INIS)

Zhou, C M; Wang, H M; Huang, X; Lin, H

2012-01-01

According to the basic theory of turbomachinery design and inlet guide vanes prewhirl regulation, two different airfoils inlet guide vanes of prewhirl regulation device were designed, the influence of the positive prewhirl to the performance of centrifugal pump were studied based on different airfoils. The results show that, for a single-suction centrifugal pump: Gottingen bowed blade-type inlet guide vane adjustment effect is better than straight blade-type inlet guide; appropriate design of positive prewhirl can elevate the efficiency of centrifugal pumps. Compared with no vane conditions, the efficiency of centrifugal pump with prewhirl vanes has been greatly improved and the power consumption has been reduced significantly, while has little influence on the head.

Influence of dental filling material type on the concentration of interleukin 9 in the samples of gingival crevicular fluid

Directory of Open Access Journals (Sweden)

Stefanović Vladimir

2016-01-01

Full Text Available Background/Aim. Several cytokines and lymphokines (IL1β, ENA78, IL6, TNFα, IL8 and S100A8 are expressed during dental pulp inflammation. Analysis of gingival crevicu-lar fluid (GCF offers a non-invasive means of studying gen-eral host response in oral cavity. Although GCF levels of various mediators could reflect the state of inflammation both in dental pulp and gingiva adjacent to a tooth, GCF samples of those without significant gingivitis could be inter-preted as reflection of pulpal process. The aim of this study was to investigate IL9 GCF values in patients with dental car-ies and to assess possible influence of various dental fillings materials on local IL9 production. Methods. The study group included 90 patients, aged 18–70, with inclusion and exclusion criteria in the prospective clinical study. Of the 6 types of material used for the restoration of prepared cavities, 3 were intended for temporary and 3 for definitive restora-tion. According to dental fillings weight, all the participants were divided into 3 groups: those with fillings lighter than 0.50 g, those with 0.50–1.00 g, and those with fillings heavier than 1.00 g. Samples were taken from gingival sulcus using the filter paper technique. Clinical parameters were deter-mined by bleeding index, plaque index (Silness-Lou, 0–3, gingival index (0–3, and gingival sulcus depth. Cytokine con-centrations were assessed using commercially available cy-tomix. Results. According to the weight of dental fillings, there was a clear decreament trend of IL9 values meaning that dental defects greater than 1.00 g of dental filling were associated with lower GCF IL9 concentration. The IL9 val-ues correlated with the degree of gingival index and depth of gingival sulcus, being higher with more advanced gingivitis and more pronounced anatomical changes in the tooth edge. Different filling materials exerted various local IL9 responses. Zink polycarbonate cement and amalgam fillings induced

Numerical Calculation and Experiment of Coupled Dynamics of the Differential Velocity Vane Pump Driven by the Hybrid Higher-order Fourier Non-circular Gears

Science.gov (United States)

Xu, Gaohuan; Chen, Jianneng; Zhao, Huacheng

2018-06-01

The transmission systems of the differential velocity vane pumps (DVVP) have periodic vibrations under loads. And it is not easy to find the reason. In order to optimize the performance of the pump, the authors proposed DVVP driven by the hybrid Higher-order Fourier non-circular gears and tested it. There were also similar periodic vibrations and noises under loads. Taking into account this phenomenon, the paper proposes fluid mechanics and solid mechanics simulation methodology to analyze the coupling dynamics between fluid and transmission system and reveals the reason. The results show that the pump has the reverse drive phenomenon, which is that the blades drive the non-circular gears when the suction and discharge is alternating. The reverse drive phenomenon leads the sign of the shaft torque to be changed in positive and negative way. So the transmission system produces torsional vibrations. In order to confirm the simulation results, micro strains of the input shaft of the pump impeller are measured by the Wheatstone bridge and wireless sensor technology. The relationships between strain and torque are obtained by experimental calibration, and then the true torque of input shaft is calculated indirectly. The experimental results are consistent to the simulation results. It is proven that the periodic vibrations are mainly caused by fluid solid coupling, which leads to periodic torsional vibration of the transmission system.

Laser-Induced Fluorescence and Synthetic Jet Fuel Analysis in the Ultra Compact Combustor

Science.gov (United States)

2009-12-01

Performance Turbine Engine Technology ICCD Intensifying Charge Couple Device IGV Inlet guide vanes ISSI Innovative Scientific Solutions Inc. ITB...centerbody in Fig. 5 simulate inlet guide vanes ( IGV ) or stator blades. In each airfoil, there is a radial vane cavity (RVC) establishing an intermediate

Standard practice for bulk sampling of liquid uranium hexafluoride

CERN Document Server

American Society for Testing and Materials. Philadelphia

2001-01-01

1.1 This practice covers methods for withdrawing representative samples of liquid uranium hexafluoride (UF6) from bulk quantities of the material. Such samples are used for determining compliance with the applicable commercial specification, for example Specification C787 and Specification C996. 1.2 It is assumed that the bulk liquid UF6 being sampled comprises a single quality and quantity of material. This practice does not address any special additional arrangements that might be required for taking proportional or composite samples, or when the sampled bulk material is being added to UF6 residues already in a container (“heels recycle”). 1.3 The number of samples to be taken, their nominal sample weight, and their disposition shall be agreed upon between the parties. 1.4 The scope of this practice does not include provisions for preventing criticality incidents. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of th...

77 FR 4646 - Airworthiness Directives; Bombardier, Inc. Airplanes

Science.gov (United States)

2012-01-31

... angle of attack vanes, pitot probes, engine inlets, and windshields, and consequent loss of or... of attack vanes, pitot probes, engine inlets or windshields. In icing conditions, the loss of the ice... of attack vanes, pitot probes, engine inlets, and windshields, and consequent loss of or misleading...

A static investigation of the thrust vectoring system of the F/A-18 high-alpha research vehicle

Science.gov (United States)

Mason, Mary L.; Capone, Francis J.; Asbury, Scott C.

1992-01-01

A static (wind-off) test was conducted in the static test facility of the Langley 16-foot Transonic Tunnel to evaluate the vectoring capability and isolated nozzle performance of the proposed thrust vectoring system of the F/A-18 high alpha research vehicle (HARV). The thrust vectoring system consisted of three asymmetrically spaced vanes installed externally on a single test nozzle. Two nozzle configurations were tested: A maximum afterburner-power nozzle and a military-power nozzle. Vane size and vane actuation geometry were investigated, and an extensive matrix of vane deflection angles was tested. The nozzle pressure ratios ranged from two to six. The results indicate that the three vane system can successfully generate multiaxis (pitch and yaw) thrust vectoring. However, large resultant vector angles incurred large thrust losses. Resultant vector angles were always lower than the vane deflection angles. The maximum thrust vectoring angles achieved for the military-power nozzle were larger than the angles achieved for the maximum afterburner-power nozzle.

Statistical sampling plans

International Nuclear Information System (INIS)

Jaech, J.L.

1984-01-01

In auditing and in inspection, one selects a number of items by some set of procedures and performs measurements which are compared with the operator's values. This session considers the problem of how to select the samples to be measured, and what kinds of measurements to make. In the inspection situation, the ultimate aim is to independently verify the operator's material balance. The effectiveness of the sample plan in achieving this objective is briefly considered. The discussion focuses on the model plant

Current technology in sampling for airborne radionuclides

International Nuclear Information System (INIS)

Schulte, H.F.

1976-01-01

Sampling for airborne radionuclides is an important part of assessing the occupational environment and that of the public or out-plant environment. Both of these are important to the operation of any nuclear facility. Most such facilities do not emit radionuclides continuously to any extent and hence both the occupational and environmental sampling system is designed to detect deviations from normal conditions or untoward events. Work with materials of a low degree of radioactivity or with nonradioactive materials may involve operations which are not enclosed and significant contaminating material may always exist in the air. In this case, the sampling is directed toward measuring this ambient level and assessing its continued impact on the worker and on the environment. Publication No. 12 of the International Commission on Radiological Protection specifies the types of operations where sampling is necessary for worker protection and the American National Standards Institute publication N 13.1-1969 is a guide to the methods used. Increasingly, this field is covered by various regulations which specify when sampling must be done and, in some cases, how it shall be done. These include requirements of the Occupational Safety and Health Administration, the Nuclear Regulatory Commission, and the Environmental Protection Agency. Needless to say, where these have specified methods they must be followed although in most cases exact procedures are not detailed as requirements. Within the plant, needs for sampling are often suggested by surface monitoring results and by bioassay, and outside by analysis of plants, soils, and material from fallout trays. 15 references

Procedures for sampling and sample reduction within quality assurance systems for solid biofuels

Energy Technology Data Exchange (ETDEWEB)

NONE

2005-07-01

The objective of this experimental study on sampling was to determine the size and number of samples of biofuels required (taken at two sampling points in each case) and to compare two methods of sampling. The first objective of the sample-reduction exercise was to compare the reliability of various sampling methods, and the second objective was to measure the variations introduced as a result of reducing the sample size to form suitable test portions. The materials studied were sawdust, wood chips, wood pellets and bales of straw, and these were analysed for moisture, ash, particle size and chloride. The sampling procedures are described. The study was conducted in Scandinavia. The results of the study were presented in Leipzig in October 2004. The work was carried out as part of the UK's DTI Technology Programme: New and Renewable Energy.

An improved integrally formed radio frequency quadrupole

Science.gov (United States)

Abbott, S.R.

1987-10-05

An improved radio frequency quadrupole is provided having an elongate housing with an elongate central axis and top, bottom and two side walls symmetrically disposed about the axis, and vanes formed integrally with the walls, the vanes each having a cross-section at right angles to the central axis which tapers inwardly toward the axis to form electrode tips spaced from each other by predetermined distances. Each of the four walls, and the vanes integral therewith, is a separate structural element having a central lengthwise plane passing through the tip of the vane, the walls having flat mounting surfaces at right angles to and parallel to the control plane, respectively, which are butted together to position the walls and vane tips relative to each other. 4 figs.

Admixing dredged marine clay with cement-bentonite for reduction of compressibility

Science.gov (United States)

Rahilman, Nur Nazihah Nur; Chan, Chee-Ming

2017-11-01

Cement-based solidification/stabilization is a method that is widely used for the treatment of dredged marine clay. The key objective for solidification/stabilization is to improve the engineering properties of the originally soft, weak material. Dredged materials are normally low in shear strength and bearing capacity while high incompressibility. In order to improve the material's properties for possible reuse, a study on the one-dimensional compressibility of lightly solidified dredged marine clay admixed with bentonite was conducted. On the other hand, due to the viscous nature, particularly the swelling property, bentonite is a popular volumising agent for backfills. In the present study, standard oedometer test was carried out to examine the compressibility of the treated sample. Complementary strength measurements were also conducted with laboratory vane shear setup on both the untreated and treated dredged marine clay. The results showed that at the same binder content, the addition of bentonite contributed significantly to the reduction of compressibility and rise in undrained shear strength. These improved properties made the otherwise discarded dredged marine soils potentially reusable for reclamation works, for instance.

How iSamples (Internet of Samples in the Earth Sciences) Improves Sample and Data Stewardship in the Next Generation of Geoscientists

Science.gov (United States)

Hallett, B. W.; Dere, A. L. D.; Lehnert, K.; Carter, M.

2016-12-01

Vast numbers of physical samples are routinely collected by geoscientists to probe key scientific questions related to global climate change, biogeochemical cycles, magmatic processes, mantle dynamics, etc. Despite their value as irreplaceable records of nature the majority of these samples remain undiscoverable by the broader scientific community because they lack a digital presence or are not well-documented enough to facilitate their discovery and reuse for future scientific and educational use. The NSF EarthCube iSamples Research Coordination Network seeks to develop a unified approach across all Earth Science disciplines for the registration, description, identification, and citation of physical specimens in order to take advantage of the new opportunities that cyberinfrastructure offers. Even as consensus around best practices begins to emerge, such as the use of the International Geo Sample Number (IGSN), more work is needed to communicate these practices to investigators to encourage widespread adoption. Recognizing the importance of students and early career scientists in particular to transforming data and sample management practices, the iSamples Education and Training Working Group is developing training modules for sample collection, documentation, and management workflows. These training materials are made available to educators/research supervisors online at http://earthcube.org/group/isamples and can be modularized for supervisors to create a customized research workflow. This study details the design and development of several sample management tutorials, created by early career scientists and documented in collaboration with undergraduate research students in field and lab settings. Modules under development focus on rock outcrops, rock cores, soil cores, and coral samples, with an emphasis on sample management throughout the collection, analysis and archiving process. We invite others to share their sample management/registration workflows and to

Recent advances in applications of nanomaterials for sample preparation.

Science.gov (United States)

Xu, Linnan; Qi, Xiaoyue; Li, Xianjiang; Bai, Yu; Liu, Huwei

2016-01-01

Sample preparation is a key step for qualitative and quantitative analysis of trace analytes in complicated matrix. Along with the rapid development of nanotechnology in material science, numerous nanomaterials have been developed with particularly useful applications in analytical chemistry. Benefitting from their high specific areas, increased surface activities, and unprecedented physical/chemical properties, the potentials of nanomaterials for rapid and efficient sample preparation have been exploited extensively. In this review, recent progress of novel nanomaterials applied in sample preparation has been summarized and discussed. Both nanoparticles and nanoporous materials are evaluated for their unusual performance in sample preparation. Various compositions and functionalizations extended the applications of nanomaterials in sample preparations, and distinct size and shape selectivity was generated from the diversified pore structures of nanoporous materials. Such great variety make nanomaterials a kind of versatile tools in sample preparation for almost all categories of analytes. Copyright © 2015 Elsevier B.V. All rights reserved.

Testing of Small Graphite Samples for Nuclear Qualification

Energy Technology Data Exchange (ETDEWEB)

Julie Chapman

2010-11-01

Accurately determining the mechanical properties of small irradiated samples is crucial to predicting the behavior of the overal irradiated graphite components within a Very High Temperature Reactor. The sample size allowed in a material test reactor, however, is limited, and this poses some difficulties with respect to mechanical testing. In the case of graphite with a larger grain size, a small sample may exhibit characteristics not representative of the bulk material, leading to inaccuracies in the data. A study to determine a potential size effect on the tensile strength was pursued under the Next Generation Nuclear Plant program. It focuses first on optimizing the tensile testing procedure identified in the American Society for Testing and Materials (ASTM) Standard C 781-08. Once the testing procedure was verified, a size effect was assessed by gradually reducing the diameter of the specimens. By monitoring the material response, a size effect was successfully identified.

Contemporary dielectric materials

CERN Document Server

Saravanan, R

2016-01-01

This book deals with experimental results of the physical characterization of several important, dielectric materials of great current interest. The experimental tools used for the analysis of these materials include X-ray diffraction, dielectric measurements, magnetic measurements using a vibrating sample magnetometer, optical measurements using a UV-Visible spectrometer etc.

Enhanced spot preparation for liquid extractive sampling and analysis

Science.gov (United States)

Van Berkel, Gary J.; King, Richard C.

2015-09-22

A method for performing surface sampling of an analyte, includes the step of placing the analyte on a stage with a material in molar excess to the analyte, such that analyte-analyte interactions are prevented and the analyte can be solubilized for further analysis. The material can be a matrix material that is mixed with the analyte. The material can be provided on a sample support. The analyte can then be contacted with a solvent to extract the analyte for further processing, such as by electrospray mass spectrometry.

A laboratory assessment of the Waveband Integrated Bioaerosol Sensor (WIBS-4) using individual samples of pollen and fungal spore material

Science.gov (United States)

Healy, David A.; O'Connor, David J.; Burke, Aoife M.; Sodeau, John R.

2012-12-01