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Sample records for vacuum arc discharge

  1. Influence of discharge gap on the discharge stability in a short vacuum arc ion source

    Energy Technology Data Exchange (ETDEWEB)

    Chen, L. [Institute of Electronic Engineering, China Academy of Engineering Physics, Mianyang, Sichuan 621900 (China); Department of Engineering Physics, Tsinghua University, Beijing 100084 (China); Zhang, G. L.; Jin, D. Z.; Dai, J. Y. [Institute of Electronic Engineering, China Academy of Engineering Physics, Mianyang, Sichuan 621900 (China); Yang, L. [Institute of Nuclear Science and Technology, Louzhou University, Lanzhou, Gansu 730000 (China)

    2012-02-15

    The influence of the discharge gap between cathode and anode on the discharge stability in a short vacuum arc (SVA) ion source is presented in this paper. Planar cathode and cylindrical hollow anode made of titanium are investigated. There is a great need in present accelerator injection research for SVA source to produce the small deviation of the ion current beam. Current research shows that increasing the short discharge gap can reduce the level of ion current deviation and ion charge deviation from 29% and 31% to 15% and 17%, respectively. A microplasma plume generation mechanism in SVA and scanning electron microscopic results can be used to explain this interesting phenomenon.

  2. Technological plasma source equipped with combined system of vacuum-arc discharge initiation

    International Nuclear Information System (INIS)

    Sysoev, Yu.O.

    2013-01-01

    The construction and the operation principle of erosion plasma source with a three-stage system of vacuum-arc discharge excitation is described. As first two step was used the modified contactless start system with plasma injector, which was widely used in standard plasma sources of the ''Bulat'' systems. The operation principle of the third stage was based on the transition of glow discharge to arc discharge. Coordinated operation of three stages during various stages of coating deposition provided significant increasing of service life and reliability of the system of vacuum-arc discharge initiation and extended the functionality of the plasma source

  3. Discharge modes at the anode of a vacuum arc

    International Nuclear Information System (INIS)

    Miller, H.C.

    1982-01-01

    The two most common anode modes in a vacuum arc are the low current mode, where the anode is basically inert; and the high current mode with a fully developed anode spot. This anode spot is very bright, has a temperature near the boiling point of the anode material, and is a copious source of vapor and energetic ions. However, other anode modes can exist. A low current vacuum arc with electrodes of readily sputterable material will emit a flux of sputtered atoms from the anode. An intermediate currents an anode footpoint can form. This footpoint is luminous, but much cooler than a true anode spot. Finally, a high current mode can exist where several small anode spots are present instead of a single large anode spot

  4. INFLUENCE OF VACUUM ARC PLASMA EVAPORATOR CATHODE GEOMETRY OF ON VALUE OF ADMISSIBLE ARC DISCHARGE CURRENT

    Directory of Open Access Journals (Sweden)

    I. A. Ivanou

    2015-01-01

    Full Text Available An analysis of main design parameters that determine a level of droplet formation intensity at the generating stage of plasma flow has been given in the paper. The paper considers the most widely used designs of water cooled consumable cathodes. Ti or Ti–Si and Fe–Cr alloys have been taken as a material for cathodes. The following calculated data: average ionic charge Zi for titanium plasma +1.6; for «titanium–silicon plasma» +1.2, an electronic discharge 1.6022 ⋅ 10–19 C, an ion velocity vi = 2 ⋅ 104 m/s, an effective volt energy equivalent of heat flow diverted in the cathode Uк = 12 V, temperature of erosion cathode surface Тп = 550 К; temperature of the cooled cathode surface То = 350 К have been accepted in order to determine dependence of a maximum admissible arc discharge current on cathode height. The calculations have been carried out for various values of the cathode heights hк (from 0.02 to 0.05 m. Diameter of a target cathode is equal to 0.08 m for a majority of technological plasma devices, therefore, the area of the erosion surface is S = 0.005 m2.A thickness selection for a consumable target cathode part in the vacuum arc plasma source has been justified in the paper. The thickness ensures formation of minimum drop phase in the plasma flow during arc cathode material evaporation. It has been shown that a maximum admissible current of an arc discharge is practically equal to the minimum current of stable arcing when thickness of the consumable cathode part is equal to 0.05 m. The admissible discharge current can be rather significant and ensure high productivity during coating process with formation of relatively low amount of droplet phase in the coating at small values of hк.

  5. Discharge behavior of vacuum arc ion source working in pulse mode

    International Nuclear Information System (INIS)

    Tang Pingying; Dai Jingyi; Tan Xiaohua; Jin Dazhi; Liu Tie; Ding Bonan

    2005-01-01

    Discharge behavior of the vacuum arc ion source working in pulse mode was investigated using high-speed photography and spectrum diagnosis. The evolvement of cathode spot on hydrogen-impregnated electrode was captured by high-speed photography, and the emission spectra of cathode spot at different pulse currents were analyzed. The experimental results show that in most cases, only one cathode spot can be found in the discharge zone of vacuum arc ion source, and the spot moves a little during the same discharge. Temperature of the cathode spot may rise while the discharge current increases, and ultimately the density of hydrogen ion will be increased. At the same time, sputtering of the electrode is enhanced and the quality of ion plasma will be reduced. (authors)

  6. TVA - Thermionic Vacuum Arc - A new type of discharge generating pure metal vapor plasma

    International Nuclear Information System (INIS)

    Musa, G.; Popescu, A.; Mustata, I.; Borcoman, I.; Cretu, M.; Leu, G.F.; Salambas, A.; Ehrich, H.; Schumann, I.

    1996-01-01

    In this paper it is presented a new type of discharge in vacuum conditions generating pure metal vapor plasma with energetic metal ions content. The peculiarities of this heated cathode discharge are described and the dependence of the measured ion energy of the working parameters are established. The ion energy value can be easily and smoothly changed. A nearly linear dependence between energy of ions and arc voltage drop has been observed. The ion energy can be increased by the increase of the interelectrode distance, decrease of cathode temperature, change of the relative position of the electrodes and by the decrease of the arc discharge current. A special configuration with cylindrical geometry has been used to develop a small size and compact metal vapour plasma gun. Due to the mentioned peculiarities, this discharge offers new openings for important applications. (author)

  7. Behaviour of gas conditions during vacuum arc discharges used for deposition of thin films

    International Nuclear Information System (INIS)

    Strzyzewski, J.; Langner, J.; Sadowski, M.; Witkowski, J.; Mirowski, R.; Catani, L.; Cianchi, A.; Russo, R.; Tazzari, S.

    2005-01-01

    The vacuum arc, which is one of the oldest techniques used for the deposition of thin films, is now widely used for the Plasma Immersion Ion Implantation and Deposition (PIII and D) in laboratory and industry. Despite of high progress in this field observed during last three decades, involving e.g. magnetic filters for the elimination of micro-droplets, some problems have not been resolved so far. The paper concerns an important problem which is connected with the inclusion of some impurities in the deposited metal film. It was found that appearance of contaminants in the film is induced mainly by water vapour remnants inside the vacuum chamber. The high adsorption of such contaminants by the deposited thin films is observed particularly in so-called getter materials, as niobium and titanium. Such materials can absorb impurities from the surrounding and dissolve them inside the layer. In order to eliminate this problem, in 2000 a new approach was proposed to perform arc discharges at the ultra-high vacuum (UHV) conditions. It was demonstrated experimentally that the deposited pure Nb-films have similar properties to the bulk-Nb samples. These results are very promising from the point of the application of such coating processes in super-conducting RF cavities of future charged-particle accelerators. The paper describes different methods used for the reduction of the background pressure in the UHV stand below 10 -10 hPa. The most important methods involve the selection of appropriate materials and the backing of whole vacuum system. In order to reduce the contaminants a laser triggering system has been applied instead of a common system, which used high-voltage discharges along the surface of an insulated trigger electrode. Particular attention is paid to a comparison of different gas conditions during arc discharges at high-vacuum conditions (background pressure in the range of 10 -8 -10 -7 hPa) and at UHV experiments (background pressure within the range of 10 -11

  8. The mechanism of liquid metal jet formation in the cathode spot of vacuum arc discharge

    Science.gov (United States)

    Gashkov, M. A.; Zubarev, N. M.; Mesyats, G. A.; Uimanov, I. V.

    2016-08-01

    We have theoretically studied the dynamics of molten metal during crater formation in the cathode spot of vacuum arc discharge. At the initial stage, a liquid-metal ridge is formed around the crater. This process has been numerically simulated in the framework of the two-dimensional axisymmetric heat and mass transfer problem in the approximation of viscous incompressible liquid. At a more developed stage, the motion of liquid metal loses axial symmetry, which corresponds to a tendency toward jet formation. The development of azimuthal instabilities of the ridge is analyzed in terms of dispersion relations for surface waves. It is shown that maximum increments correspond to instability of the Rayleigh-Plateau type. Estimations of the time of formation of liquid metal jets and their probable number are obtained.

  9. Vacuum arc anode phenomena

    International Nuclear Information System (INIS)

    Miller, H.C.

    1976-01-01

    A brief review of anode phenomena in vacuum arcs is presented. Discussed in succession are: the transition of the arc into the anode spot mode; the temperature of the anode before, during and after the anode spot forms; and anode ions. Characteristically the anode spot has a temperature of the order of the atmospheric boiling point of the anode material and is a copious source of vapor and energetic ions. The dominant mechanism controlling the transition of the vacuum arc into the anode spot mode appears to depend upon the electrode geometry, the electrode material, and the current waveform of the particular vacuum arc being considered. Either magnetic constriction in the gap plasma or gross anode melting can trigger the transition; indeed, a combination of the two is a common cause of anode spot formation

  10. Study of the ionization rate of the released deuterium in vacuum arc discharges with metal deuteride cathodes

    Science.gov (United States)

    Liu, Fei-Xiang; Long, Ji-Dong; Zheng, Le; Dong, Pan; Li, Chen; Chen, Wei

    2018-02-01

    The ionization rate of the released deuterium from a metal deuteride cathode in vacuum arc discharges is investigated by both experiments and modeling analysis. Experimental results show that the deuterium ionization rate increases from 2% to 30% with the increasing arc current in the range of 2-100 A. Thus the full ionization assumption, as is widely used in arc plasma simulations, is not satisfied for the released deuterium at low discharge current. According to the modeling results, the neutral-to-ion conversion efficiency for the deuterium traveling across the cathodic spot region can be significantly less than one, due to the fast plasma expansion and rarefaction in the vacuum. In addition, the model also reveals that, unlike the metal atoms which are mainly ionized in the sheath region and flow back to the cathode, the deuterium ionization primarily occurs in the quasi-neutral region and moves towards the anode. Consequently, the cathodic sheath layer acts like a filter that increases the deuterium fraction beyond the sheath region.

  11. Vacuum Arc Ion Sources

    CERN Document Server

    Brown, I.

    2013-12-16

    The vacuum arc ion source has evolved into a more or less standard laboratory tool for the production of high-current beams of metal ions, and is now used in a number of different embodiments at many laboratories around the world. Applications include primarily ion implantation for material surface modification research, and good performance has been obtained for the injection of high-current beams of heavy-metal ions, in particular uranium, into particle accelerators. As the use of the source has grown, so also have the operational characteristics been improved in a variety of different ways. Here we review the principles, design, and performance of vacuum arc ion sources.

  12. Model of liquid-metal splashing in the cathode spot of a vacuum arc discharge

    International Nuclear Information System (INIS)

    Gashkov, M. A.; Zubarev, N. M.; Zubareva, O. V.; Mesyats, G. A.; Uimanov, I. V.

    2016-01-01

    The formation of microjets is studied during the extrusion of a melted metal by the plasma pressure from craters formed on a cathode in a burning vacuum arc. An analytic model of liquid-metal splashing that includes two stages is proposed. At the first stage, the liquid motion has the axial symmetry and a liquid-metal wall surrounding the crater is formed. At the second stage, the axial symmetry is broken due to the development of the Plateau–Rayleigh instability in the upper part of the wall. The wall breakup process is shown to have a threshold. The minimal plasma pressure and the minimal electric current flowing through the crater required for obtaining the liquid-metal splashing regime are found. The basic spatial and temporal characteristics of the jet formation process are found using the analytic model.

  13. Modeling Vacuum Arcs On Spacecraft Solar Panel Arrays, Phase I

    Data.gov (United States)

    National Aeronautics and Space Administration — Spacecraft charging and subsequent vacuum arcing poses a significant threat to satellites in LEO and GEO plasma conditions. Localized arc discharges can cause a...

  14. Magnetically enhanced vacuum arc thruster

    International Nuclear Information System (INIS)

    Keidar, Michael; Schein, Jochen; Wilson, Kristi; Gerhan, Andrew; Au, Michael; Tang, Benjamin; Idzkowski, Luke; Krishnan, Mahadevan; Beilis, Isak I

    2005-01-01

    A hydrodynamic model of the vacuum arc thruster and its plume is described. Primarily an effect of the magnetic field on the plume expansion and plasma generation is considered. Two particular examples are investigated, namely the magnetically enhanced co-axial vacuum arc thruster (MVAT) and the vacuum arc thruster with ring electrodes (RVAT). It is found that the magnetic field significantly decreases the plasma plume radial expansion under typical conditions. Predicted plasma density profiles in the plume of the MVAT are compared with experimental profiles, and generally a good agreement is found. In the case of the RVAT the influence of the magnetic field leads to plasma jet deceleration, which explains the non-monotonic dependence of the ion current density, on an axial magnetic field observed experimentally

  15. Magnetically enhanced vacuum arc thruster

    Energy Technology Data Exchange (ETDEWEB)

    Keidar, Michael [University of Michigan, Ann Arbor 48109 MI (United States); Schein, Jochen [Alameda Applied Science Corporation, San Leandro, CA 94577 (United States); Wilson, Kristi [Alameda Applied Science Corporation, San Leandro, CA 94577 (United States); Gerhan, Andrew [Alameda Applied Science Corporation, San Leandro, CA 94577 (United States); Au, Michael [Alameda Applied Science Corporation, San Leandro, CA 94577 (United States); Tang, Benjamin [Alameda Applied Science Corporation, San Leandro, CA 94577 (United States); Idzkowski, Luke [Alameda Applied Science Corporation, San Leandro, CA 94577 (United States); Krishnan, Mahadevan [Alameda Applied Science Corporation, San Leandro, CA 94577 (United States); Beilis, Isak I [Tel Aviv University, Tel Aviv (Israel)

    2005-11-01

    A hydrodynamic model of the vacuum arc thruster and its plume is described. Primarily an effect of the magnetic field on the plume expansion and plasma generation is considered. Two particular examples are investigated, namely the magnetically enhanced co-axial vacuum arc thruster (MVAT) and the vacuum arc thruster with ring electrodes (RVAT). It is found that the magnetic field significantly decreases the plasma plume radial expansion under typical conditions. Predicted plasma density profiles in the plume of the MVAT are compared with experimental profiles, and generally a good agreement is found. In the case of the RVAT the influence of the magnetic field leads to plasma jet deceleration, which explains the non-monotonic dependence of the ion current density, on an axial magnetic field observed experimentally.

  16. Influence of N2 partial pressure on structural and microhardness properties of TiN/ZrN multilayers deposited by Ar/N2 vacuum arc discharge

    Science.gov (United States)

    Naddaf, M.; Abdallah, B.; Ahmad, M.; A-Kharroub, M.

    2016-08-01

    The influence of N2 partial pressure on structural, mechanical and wetting properties of multilayered TiN/ZrN thin films deposited on silicon substrates by vacuum arc discharge of (N2 + Ar) gas mixtures is investigated. X-ray diffraction (XRD) results show that the average texturing coefficient of (1 1 1) orientation and the grain size of both TiN and ZrN individual layers increase with increasing the N2 partial pressure. The Rutherford back scattering (RBS) measurements and analysis reveal that incorporation of the nitrogen in the film increases with increasing the N2 partial pressure and both TiN and ZrN individual layers have a nitrogen over-stoichiometry for N2 partial pressure ⩾50%. The change in the film micro-hardness is correlated to the changes in crystallographic texture, grain size, stoichiometry and the residual stress in the film as a function of the N2 partial pressure. In particular, stoichiometry of ZrN and TiN individual is found to play the vital role in determining the multilayer hardness. The multilayer film deposited at N2 partial pressure of 25% has the best stoichiometric ratio of both TiN and ZrN layers and the highest micro-hardness of about 32 GPa. In addition, water contact angle (WCA) measurements and analysis show a decrease in the work of adhesion on increasing the N2 partial pressure.

  17. Influence of N_2 partial pressure on structural and microhardness properties of TiN/ZrN multilayers deposited by Ar/N_2 vacuum arc discharge

    International Nuclear Information System (INIS)

    Naddaf, M.; Abdallah, B.; Ahmad, M.; A-Kharroub, M.

    2016-01-01

    The influence of N_2 partial pressure on structural, mechanical and wetting properties of multilayered TiN/ZrN thin films deposited on silicon substrates by vacuum arc discharge of (N_2 + Ar) gas mixtures is investigated. X-ray diffraction (XRD) results show that the average texturing coefficient of (1 1 1) orientation and the grain size of both TiN and ZrN individual layers increase with increasing the N_2 partial pressure. The Rutherford back scattering (RBS) measurements and analysis reveal that incorporation of the nitrogen in the film increases with increasing the N_2 partial pressure and both TiN and ZrN individual layers have a nitrogen over-stoichiometry for N_2 partial pressure ⩾50%. The change in the film micro-hardness is correlated to the changes in crystallographic texture, grain size, stoichiometry and the residual stress in the film as a function of the N_2 partial pressure. In particular, stoichiometry of ZrN and TiN individual is found to play the vital role in determining the multilayer hardness. The multilayer film deposited at N_2 partial pressure of 25% has the best stoichiometric ratio of both TiN and ZrN layers and the highest micro-hardness of about 32 GPa. In addition, water contact angle (WCA) measurements and analysis show a decrease in the work of adhesion on increasing the N_2 partial pressure.

  18. Plasma instability of a vacuum arc centrifuge

    International Nuclear Information System (INIS)

    Hole, M.J.; Dallaqua, R.S.; Simpson, S.W.; Del Bosco, E.

    2002-01-01

    Ever since conception of the vacuum arc centrifuge in 1980, periodic fluctuations in the ion saturation current and floating potential have been observed in Langmuir probe measurements in the rotation region of a vacuum arc centrifuge. In this work we develop a linearized theoretical model to describe a range of instabilities in the vacuum arc centrifuge plasma column, and then test the validity of the description through comparison with experiment. We conclude that the observed instability is a 'universal' instability, driven by the density gradient, in a plasma with finite conductivity

  19. Investigations Of A Pulsed Cathodic Vacuum Arc

    Science.gov (United States)

    Oates, T. W. H.; Pigott, J.; Denniss, P.; Mckenzie, D. R.; Bilek, M. M. M.

    2003-06-01

    Cathodic vacuum arcs are well established as a method for producing thin films for coatings and as a source of metal ions. Research into DC vacuum arcs has been going on for over ten years in the School of Physics at the University of Sydney. Recently a project was undertaken in the school to design and build a pulsed CVA for use in the investigation of plasma sheaths and plasma immersion ion implantation. Pulsed cathodic vacuum arcs generally have a higher current and plasma density and also provide a more stable and reproducible plasma density than their DC counterparts. Additionally it has been shown that if a high repetition frequency can be established the deposition rate of pulsed arcs is equal to or greater than that of DC arcs with a concomitant reduction in the rate of macro-particle formation. We present here results of our investigations into the building of a center-triggered pulsed cathodic vacuum arc. The design of the power supply and trigger mechanism and the geometry of the anode and cathode are examined. Observations of type I and II arc spots using a CCD camera, and cathode spot velocity dependence on arc current will be presented. The role of retrograde motion in a high current pulsed arc is discussed.

  20. Investigations Of A Pulsed Cathodic Vacuum Arc

    International Nuclear Information System (INIS)

    Oates, T.W.H.; Pigott, J.; Denniss, P.; Mckenzie, D.R.; Bilek, M.M.M.

    2003-01-01

    Cathodic vacuum arcs are well established as a method for producing thin films for coatings and as a source of metal ions. Research into DC vacuum arcs has been going on for over ten years in the School of Physics at the University of Sydney. Recently a project was undertaken in the school to design and build a pulsed CVA for use in the investigation of plasma sheaths and plasma immersion ion implantation. Pulsed cathodic vacuum arcs generally have a higher current and plasma density and also provide a more stable and reproducible plasma density than their DC counterparts. Additionally it has been shown that if a high repetition frequency can be established the deposition rate of pulsed arcs is equal to or greater than that of DC arcs with a concomitant reduction in the rate of macro-particle formation. We present here results of our investigations into the building of a center-triggered pulsed cathodic vacuum arc. The design of the power supply and trigger mechanism and the geometry of the anode and cathode are examined. Observations of type I and II arc spots using a CCD camera, and cathode spot velocity dependence on arc current will be presented. The role of retrograde motion in a high current pulsed arc is discussed

  1. Note: Triggering behavior of a vacuum arc plasma source

    Energy Technology Data Exchange (ETDEWEB)

    Lan, C. H., E-mail: lanchaohui@163.com; Long, J. D.; Zheng, L.; Dong, P.; Yang, Z.; Li, J.; Wang, T.; He, J. L. [Institute of Fluid Physics, China Academy of Engineering Physics, Mianyang 621900 (China)

    2016-08-15

    Axial symmetry of discharge is very important for application of vacuum arc plasma. It is discovered that the triggering method is a significant factor that would influence the symmetry of arc discharge at the final stable stage. Using high-speed multiframe photography, the transition processes from cathode-trigger discharge to cathode-anode discharge were observed. It is shown that the performances of the two triggering methods investigated are quite different. Arc discharge triggered by independent electric source can be stabilized at the center of anode grid, but it is difficult to achieve such good symmetry through resistance triggering. It is also found that the triggering process is highly correlated to the behavior of emitted electrons.

  2. Structural, mechanical, electrical and wetting properties of ZrNx films deposited by Ar/N2 vacuum arc discharge: Effect of nitrogen partial pressure

    Science.gov (United States)

    Abdallah, B.; Naddaf, M.; A-Kharroub, M.

    2013-03-01

    Non-stiochiometric zirconium nitride (ZrNx) thin films have been deposited on silicon substrates by vacuum arc discharge of (N2 + Ar) gas mixtures at different N2 partial pressure ratio. The microstructure, mechanical, electrical and wetting properties of these films are studied by means of X-ray diffraction (XRD), micro-Raman spectroscopy, Rutherford back scattering (RBS) technique, conventional micro-hardness testing, electrical resistivity, atomic force microscopy (AFM) and contact angle (CA) measurements. RBS results and analysis show that the (N/Zr) ratio in the film increases with increasing the N2 partial pressure. A ZrNx film with (Zr/N) ratio in the vicinity of stoichiometric ZrN is obtained at N2 partial pressure of 10%. XRD and Raman results indicate that all deposited films have strained cubic crystal phase of ZrN, regardless of the N2 partial pressure. On increasing the N2 partial pressure, the relative intensity of (1 1 1) orientation with respect to (2 0 0) orientation is seen to decrease. The effect of N2 partial pressure on micro-hardness and the resistivity of the deposited film is revealed and correlated to the alteration of grain size, crystallographic texture, stoichiometry and residual stress developed in the film. In particular, it is found that residual stress and nitrogen incorporation in the film play crucial role in the alteration of micro-hardness and resistivity respectively. In addition, CA and AFM results demonstrate that as N2 partial pressure increases, both the surface hydrophobicity and roughness of the deposited film increase, leading to a significant decrease in the film surface free energy (SFE).

  3. High efficient vacuum arc plant for coating deposition

    International Nuclear Information System (INIS)

    Aksenov, I.I.; Belous, V.A.

    2008-01-01

    A number of progressive technical solutions are used in the 'Bulat-9' machine designed for vacuum arc coating deposition. The features of the machine are: a dome shaped working chamber that allows to 'wash' its inner surfaces with hot nitrogen or argon gas; a system of automatic loading/unloading of articles to be treated into the chamber through its bottom; shielding of the inner surfaces of the chamber by heated panels; improved vacuum arc plasma sources including filtered one; four ported power supply for the vacuum arc discharges; LC oscillatory circuits suppressing microarcs on the substrate; the system of automatic control of a working process. The said technical features cause the apparatus originality and novelty preserved up to-day

  4. Metal transfer during vacuum consumable arc remelting

    International Nuclear Information System (INIS)

    Zanner, F.J.

    1977-11-01

    A description of the vacuum consumable arc remelt process as related to solidification and a review of vacuum arc literature is presented. Metal transfer at arc lengths less than or equal to 3 cm was found to occur when liquid metal spikes hanging from the cathode form a low resistance bridge (drop short) by touching the anode and subsequently rupturing. During the bridge lifetime (0.0003 to 0.020 s) the arc is extinguished and all of the electrical power is directed through the molten bridge. The formation and rupture of these molten metal bridges are confirmed with electrical resistance measurements. At long arc lengths (greater than 10 cm) the spikes separate before touching the anode

  5. Experiments with background gas in a vacuum arc centrifuge

    International Nuclear Information System (INIS)

    Dallaqua, R.S.; Simpson, S.W.; Del Bosco, E.

    1996-01-01

    Since promising isotope separation results were first reported by Krishnan et al. in 1981, a range of vacuum arc centrifuge experiments have been conducted in laboratories around the world. The PCEN (Plasma CENtrifuge) vacuum arc centrifuge at the Brazilian National Institute for Space Research has been used for isotope separation studies with cathode materials of carbon and magnesium and also to investigate the performance in terms of the rotational velocity attained for different cathode materials. Here, a vacuum arc centrifuge has been operated with an initial filling gas of either argon or hydrogen for pressures ranging from 10 -3 to 10 -1 Pa. The angular velocity ω of the plasma has been determined by cross-correlating the signals from potential probes, and the electron temperature T has been deduced from Langmuir probe data. At high gas pressures and early times during the 14 ms plasma lifetime, high-frequency nonuniformities frequently observed in the vacuum discharge disappear, suggesting that the associated instability is suppressed. Under the same conditions, nonuniformities rotating with much lower angular velocities are observed in the plasma. Temperatures are reduced in the presence of the background gas, and the theoretical figure of merit for separation proportional to ω 2 /T is increased compared to its value in the vacuum discharge for both argon and hydrogen gas fillings

  6. Metal halide arc discharge lamp having short arc length

    Science.gov (United States)

    Muzeroll, Martin E. (Inventor)

    1994-01-01

    A metal halide arc discharge lamp includes a sealed light-transmissive outer jacket, a light-transmissive shroud located within the outer jacket and an arc tube assembly located within the shroud. The arc tube assembly includes an arc tube, electrodes mounted within the arc tube and a fill material for supporting an arc discharge. The electrodes have a spacing such that an electric field in a range of about 60 to 95 volts per centimeter is established between the electrodes. The diameter of the arc tube and the spacing of the electrodes are selected to provide an arc having an arc diameter to arc length ratio in a range of about 1.6 to 1.8. The fill material includes mercury, sodium iodide, scandium tri-iodide and a rare gas, and may include lithium iodide. The lamp exhibits a high color rendering index, high lumen output and high color temperature.

  7. Study of gliding arc discharge plasma

    International Nuclear Information System (INIS)

    Yang Chi; Lin Lie; Wu Bin

    2006-01-01

    The electric parameters change during discharge is studied and the relationship between non-equilibrium degree and parameters is discussed for gliding arc discharges. Using two-channel model, the rules of arc moving due to effect of the airflow is simulated. The numerical simulation results can help analyzing the generation mechanism of gliding arc non-equilibrium plasma. (authors)

  8. Vacuum arc ion charge state distributions

    International Nuclear Information System (INIS)

    Brown, I.G.; Godechot, X.

    1990-06-01

    We have measured vacuum arc ion charge state spectra for a wide range of metallic cathode materials. The charge state distributions were measured using a time-of-flight diagnostic to monitor the energetic ion beam produced by a metal vapor vacuum arc ion source. We have obtained data for 48 metallic cathode elements: Li, C, Mg, Al, Si, Ca, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ge, Sr, Y, Zr, Nb, Mo, Pd, Ag, Cd, In, Sn, Ba, La, Ce, Pr, Nd, Sm, Gd, Dy, Ho, Er, Yb, Hf, Ta, W, Ir, Pt, Au, Pb, Bi, Th and U. The arc was operated in a pulsed mode with pulse length 0.25 msec; arc current was 100 A throughout. This array of elements extends and completes previous work by us. In this paper the measured distributions are cataloged and compared with our earlier results and with those of other workers. We also make some observations about the performance of the various elements as suitable vacuum arc cathode materials

  9. Vacuum arc ion charge-state distributions

    International Nuclear Information System (INIS)

    Brown, I.G.; Godechot, X.

    1991-01-01

    The authors have measured vacuum arc ion charge-state spectra for a wide range of metallic cathode materials. The charge-state distributions were measured using a time-of-flight diagnostic to monitor the energetic ion beam produced by a metal vapor vacuum arc ion source. They have obtained data for 48 metallic cathode elements: Li, C, Mg, Al, Si, Ca, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ge, Sr, Y, Zr, Nb, Mo, Pd, Ag, Cd, In, Sn, Ba, La, Ce, Pr, Nd, Sm, Gd, Dy, Ho, Er, Yb, Hf, Ta, W, Ir, Pt, Au, Pb, Bi, Th, and U. The arc was operated in a pulsed mode with pulse length 0.25 ms; arc current was 100 A throughout. This array of elements extends and completes previous work by the authors. In this paper the measured distributions are cataloged and compared with their earlier results and those of other workers. They also make some observations about the performance of the various elements as suitable vacuum arc cathode materials

  10. Coefficient of electrical transport vacuum arc for metals and alloys

    International Nuclear Information System (INIS)

    Markov, G.V.; Ehjzner, B.A.

    1998-01-01

    In this article the authors propose formulas for estimation coefficient of electrical transport vacuum arc for metals and alloys. They also represent results of analysis principal physical processes which take place in cathode spot vacuum arc

  11. Recent advances in vacuum arc ion sources

    International Nuclear Information System (INIS)

    Brown, I.G.; Anders, A.; Anders, S.; Dickinson, M.R.; MacGill, R.A.; Oks, E.M.

    1995-07-01

    Intense beams of metal ions can be formed from a vacuum arc ion source. Broadbeam extraction is convenient, and the time-averaged ion beam current delivered downstream can readily be in the tens of milliamperes range. The vacuum arc ion source has for these reasons found good application for metallurgical surface modification--it provides relatively simple and inexpensive access to high dose metal ion implantation. Several important source developments have been demonstrated recently, including very broad beam operation, macroparticle removal, charge state enhancement, and formation of gaseous beams. The authors have made a very broad beam source embodiment with beam formation electrodes 50 cm in diameter, producing a beam of width ∼35 cm for a nominal beam area of ∼1,000 cm 2 , and a pulsed Ti beam current of about 7 A was formed at a mean ion energy of ∼100 keV. Separately, they've developed high efficiency macroparticle-removing magnetic filters and incorporated such a filter into a vacuum arc ion source so as to form macroparticle-free ion beams. Jointly with researchers at the High Current Electronics Institute at Tomsk, Russia, and the Gesellschaft fuer Schwerionenforschung at Darmstadt, Germany, they've developed a compact technique for increasing the charge states of ions produced in the vacuum arc plasma and thus providing a simple means of increasing the ion energy at fixed extractor voltage. Finally, operation with mixed metal and gaseous ion species has been demonstrated. Here, they briefly review the operation of vacuum marc ion sources and the typical beam and implantation parameters that can be obtained, and describe these source advances and their bearing on metal ion implantation applications

  12. Cathodic Vacuum Arc Plasma of Thallium

    International Nuclear Information System (INIS)

    Yushkov, Georgy Yu.; Anders, Andre

    2006-01-01

    Thallium arc plasma was investigated in a vacuum arc ion source. As expected from previous consideration of cathode materials in the Periodic Table of the Elements, thallium plasma shows lead-like behavior. Its mean ion charge state exceeds 2.0 immediately after arc triggering, reaches the predicted 1.60 and 1.45 after about 100 microsec and 150 microsec, respectively. The most likely ion velocity is initially8000 m/s and decays to 6500 m/s and 6200 m/s after 100 microsec and 150microsec, respectively. Both ion charge states and ion velocities decay further towards steady state values, which are not reached within the 300microsec pulses used here. It is argued that the exceptionally high vapor pressure and charge exchange reactions are associated with the establishment of steady state ion values

  13. Proceedings of the workshop on vacuum arc ion sources

    International Nuclear Information System (INIS)

    Brown, I.

    1996-08-01

    Topics included in the papers presented at this conference are: vacuum arc ion source development at GSI (Gesellschaft fuer Schwerionenforschung, Germany), ITEP (Institute for Theoretical and Experimental Physics, Russia), Lawrence Berkeley Laboratory, and ANSTO (Australian Nuclear Science and Technology Organization); triggers for vacuum arc sources; plasma distribution of cathodic arc deposition system; high ion charge states in vacuum arc ion sources; and gas and metal ion sources. Selected papers are indexed separately for inclusion in the Energy Science and Technology Database

  14. A high current metal vapour vacuum arc ion source for ion implantation studies

    International Nuclear Information System (INIS)

    Evans, P.J.; Noorman, J.T.; Watt, G.C.; Cohen, D.D.; Bailey, G.M.

    1989-01-01

    The main features of the metal vapour vacuum arc(MEVA) as an ion source are presented. The technology utilizes the plasma production capabilities of a vacuum arc cathode. Some of the ions produced in this discharge flow through the anode and the 3 extraction grids to form an extracted ion beam. The high beam current and the potential for generating broad beams, make this technology suitable for implantation of large surface areas. The composition of the vacuum arc cathode determines the particular ions obtained from the MEVA source. 3 refs., 1 tab., 2 figs

  15. Properties of DLC coatings deposited by dc and dc with superimposed pulsed vacuum arc

    International Nuclear Information System (INIS)

    Zavaleyev, V.; Walkowicz, J.; Aksyonov, D.S.; Luchaninov, A.A.; Reshetnyak, E.N.; Strel'nitskij, V.E.

    2014-01-01

    Comparative studies of the structure, mechanical and tribological properties of DLC coatings deposited in DC and DC with superimposed high current pulse modes of operation vacuum-arc plasma source with the graphite cathode are presented. Imposition the pulses of high current on DC vacuum-arc discharge allows both increase the deposition rate of DLC coating and reduce the residual compressive stress in the coatings what promotes substantial improvement the adhesion to the substrate. Effect of vacuum arc plasma filtration with Venetian blind filter on the deposition rate and tribological characteristics of the coatings analyzed.

  16. Advances in high voltage insulation and arc interruption in SF6 and vacuum

    CERN Document Server

    Maller, V N

    1982-01-01

    Advances in High Voltage Insulation and Arc Interruption in SF6 and Vacuum deals with high voltage breakdown and arc extinction in sulfur hexafluoride (SF6) and high vacuum, with special emphasis on the application of these insulating media in high voltage power apparatus and devices. The design and developmental aspects of various high voltage power apparatus using SF6 and high vacuum are highlighted. This book is comprised of eight chapters and opens with a discussion on electrical discharges in SF6 and high vacuum, along with the properties and handling of SF6 gas. The following chapters fo

  17. Baking of tandem accelerator tube by low voltage arc discharge

    International Nuclear Information System (INIS)

    Nakajima, Yutaka

    1982-01-01

    In designing the accelerating tube for a static tandem accelerator in Kyushu University, the basic policy was as described below: individual unit composing the accelerating tube should fully withstand the electric field of 2 MV/m, and electric discharge must not be propagated from one unit to the adjacent unit when these are assembled to the accelerating tube. The accelerating tube units are each 25 cm in length, and both high and low energy sides are composed of 20 units, respectively. Although about 10 -9 Torr vacuum was obtained at the both ends of the accelerating tube by baking the tube at 300 to 350 deg C with electric heaters wound outside the tube in the conventional method, vast outgas was generated, which decreased vacuum by two or three figures if breakdown occurred through the intermediary of outgas. As a method of positively outgassing and cleaning the electrodes inside the accelerating tube, it was attempted to directly bake all the electrodes in the accelerating tube by causing strong arc discharge flowing H 2 gas in the tube. As a result of considering the conditions for this method, the low voltage arc discharge was employed using oxide cathodes. Thus, after implementing 10A arc discharge for several hours, the voltage was able to be raised to 10 MV almost immediately after the vacuum recovery, and further, after another conditioning for several hours, it was successful to raise voltage up to 11 MV. (Wakatsuki, Y.)

  18. Vacuum arc ion sources - micro to macro

    International Nuclear Information System (INIS)

    MacGill, R.A.; Dickinson, M.R.; Brown, I.G.

    1995-08-01

    Vacuum arc ion sources provide a convenient tool for the production of intense beams of metal ions. The sources are relatively easy to construct and they can produce beams from all of the solid metals as well as of compounds, alloys and mixtures. We have made a number of different kinds of such sources over the course of our development work at LBL in the past decade, from very small open-quote thumb-size close-quote versions to a very large one with 50-cm diameter extractor. Beam current ranges from a few milliamperes up to almost 10 amperes and extraction voltage from about 1 kV to 100 kV. Multicathode versions have been made so that one can switch between metal ion species simply and quickly. Most of the sources have been operated in a repetitively pulsed mode, and we've tested a dc version also. Here we outline some construction features of the array of vacuum arc ion sources that we've developed and used, and describe their performance and limitations

  19. Vacuum arc anode plasma. I. Spectroscopic investigation

    International Nuclear Information System (INIS)

    Bacon, F.M.

    1975-01-01

    A spectroscopic investigation was made of the anode plasma of a pulsed vacuum arc with an aluminum anode and a molybdenum cathode. The arc was triggered by a third trigger electrode and was driven by a 150-A 10-μs current pulse. The average current density at the anode was sufficiently high that anode spots were formed; these spots are believed to be the source of the aluminum in the plasma investigated in this experiment. By simultaneously measuring spectral emission lines of Al I, Al II, and Al III, the plasma electron temperature was shown to decrease sequentially through the norm temperatures of Al III, Al II, and Al I as the arc was extinguished. The Boltzmann distribution temperature T/subD/ of four Al III excited levels was shown to be kT/subD//e=2.0plus-or-minus0.5 V, and the peak Al III 4D excited state density was shown to be about 5times10 17 m -3 . These data suggest a non-local-thermodynamic-equilibrium (non-LTE) model of the anode plasma when compared with the Al 3+ production in the plasma. The plasma was theoretically shown to be optically thin to the observed Al III spectral lines

  20. Influence of Gap Distance on Vacuum Arc Characteristics of Cup Type AMF Electrode in Vacuum Interrupters

    International Nuclear Information System (INIS)

    Cheng Shaoyong; Xiu Shixin; Wang Jimei; Shen Zhengchao

    2006-01-01

    The greenhouse effect of SF 6 is a great concern today. The development of high voltage vacuum circuit breakers becomes more important. The vacuum circuit breaker has minimum pollution to the environment. The vacuum interrupter is the key part of a vacuum circuit breaker. The interrupting characteristics in vacuum and arc-controlling technique are the main problems to be solved for a longer gap distance in developing high voltage vacuum interrupters. To understand the vacuum arc characteristics and provide effective technique to control vacuum arc in a long gap distance, the arc mode transition of a cup-type axial magnetic field electrode is observed by a high-speed charge coupled device (CCD) video camera under different gap distances while the arc voltage and arc current are recorded. The controlling ability of the axial magnetic field on vacuum arc obviously decreases when the gap distance is longer than 40 mm. The noise components and mean value of the arc voltage significantly increase. The effective method for controlling the vacuum arc characteristics is provided by long gap distances based on the test results. The test results can be used as a reference to develop high voltage and large capacity vacuum interrupters

  1. ARC discharge sliding over a conducting surface

    NARCIS (Netherlands)

    van Goor, F.A.; Mitko, S.; Ochkin, V.N.; Paramonov, A.P.; Witteman, W.J.

    1997-01-01

    Results of experimental and theoretical studies of the arc discharge which slides over the surface of a conductor are reported. Experiments were performed in air and argon ambients at various pressures. It is found that the velocity of the discharge plasma front depends linearly on the strength of

  2. Dye laser spectrometer for the analysis of pulsed vacuum arcs

    International Nuclear Information System (INIS)

    Hargis, P.J. Jr.; Robertson, M.M.

    1975-01-01

    A pulsed dye laser spectrometer which is used to obtain detailed single shot spectroscopic measurements of the plasma in a pulsed vacuum arc was developed. The capabilities of this spectrometer are indicated by the detection of laser induced fluorescence signals from 10 6 neutral Ti atoms in the plasma of a pulsed vacuum arc with a Ti anode. (U.S.)

  3. Current and voltage distribution in the diffuse vacuum arc

    NARCIS (Netherlands)

    Schellekens, H.; Schram, D.C.

    1985-01-01

    On the basis of extensive measurements, a model is developed for the diffuse plasma of the high-current vacuum arc. The model shows that the current constriction and the voltage distribution in the diffuse vacuum arc prior to anode-spot formation are caused by the pressure source to which the

  4. Time dependence of vacuum arc parameters

    International Nuclear Information System (INIS)

    Anders, A.; Anders, S.; Brown, I.G.

    1993-01-01

    Time-resolved investigations of the expanded plasma of vacuum arc cathode spots are described, including the study of the ion charge state distribution, the random cathode spot motion, and the crater formation. It was found that the ion charge state distribution changes over a time scale on the order of hundreds of microseconds. For the random spot motion two time scales were observed: a very short spot residence time of tens of nanoseconds which gives, combined with the step width, the diffusion parameter of the random motion, and a longer time scale on the order of 100 μs during which the diffusion parameter changes. Crater formation studies by scanning electron microscopy indicate the occurrence of larger craters at the end of crater chains. The existence of a time scale, much longer than the elementary times for crater formation and spot residence, can be explained by local heat accumulation

  5. Instability of a Vacuum Arc Centrifuge

    International Nuclear Information System (INIS)

    Hole, M.J.; Dallaqua, R.S.; Bosco, E. del; Simpson, S.W.

    2003-01-01

    Ever since conception of the Vacuum Arc Centrifuge (VAC) in 1980, periodic fluctuations in the ion saturation current and floating potential have been observed in Langmuir probe measurements in the rotation region of a VAC. Our theoretical and experimental research suggests that these fluctuations are in fact a pressure-gradient driven drift mode. In this work, we summarise the properties of a theoretical model describing the range of instabilities in the VAC plasma column, present theoretical predictions and compare with detailed experiments conducted on the PCEN centrifuge at the Brazilian National Space Research Institute (INPE). We conclude that the observed instability is a 'universal' instability, driven by the density-gradient, in a plasma with finite conductivity

  6. Metal vapor vacuum arc ion sources

    International Nuclear Information System (INIS)

    Brown, I.G.; Dickinson, M.R.; Galvin, J.E.; Godechot, X.; MacGill, R.A.

    1990-06-01

    We have developed a family of metal vapor vacuum are (MEVVA) high current metal ion sources. The sources were initially developed for the production of high current beams of metal ions for heavy ion synchrotron injection for basic nuclear physics research; more recently they have also been used for metal ion implantation. A number of different embodiments of the source have been developed for these specific applications. Presently the sources operate in a pulsed mode, with pulse width of order 1 ms and repetition rate up to 100 pps. Beam extraction voltage is up to 100 kV, and since the ions produced in the vacuum arc plasma are in general multiply ionized the ion energy is up to several hundred keV. Beam current is up to several Amperes peak and around 10 mA time averaged delivered onto target. Nearly all of the solid metals of the Periodic Table have been use to produce beam. A number of novel features have been incorporated into the sources, including multiple cathodes and the ability to switch between up to 18 separate cathode materials simply and quickly, and a broad beam source version as well as miniature versions. here we review the source designs and their performance. 45 refs., 7 figs

  7. Is this an arc or a glow discharge?

    International Nuclear Information System (INIS)

    Puchkarev, V.F.; Bochkarev, M.B.

    1994-01-01

    A well known criterion for distinguishing an arc discharge from a glow discharge is a low voltage drop (10--30 V) and a high current density that varies from a few tens to 10 6 A/cm 2 depending on arc type. The high current density is an attribute of arcs with cathode spots. The authors report here a study of the mechanism of emission in cathode spot arc where they realized a spotless discharge with a low voltage drop (30--50 V) and a high mean current density (10 4 --10 6 A/cm 2 ). The discharge was initiated between a broad cathode and point anode. The cathode was a smooth tungsten sphere electrode of about 100 μm in diameter. The point anode was made of various materials (Mo, Cu, Cd) with initial radius 1 μm. Before the experiment the cathode was cleaned by heating at 2,000 K at high vacuum (10 -8 Torr). The discharge was initiated by self-breakdown when electrodes under the voltage 200--500 V were brought to close proximity with each other. The cathode-anode spacing d at the moment of breakdown was estimated to be < 1 μm. The discharge current was varied within 1--3 A by changing the applied voltage and impedance of coaxial cable generator. The discharge burned during 100--1,000 ns. After the single discharge the cathode and anode were examined with a scanning electron microscope. The cathode surface exposed to the discharge was smooth, i.e. no erosion pits similar to arc craters were found on the cathode surface. The anode was shortened after discharge by 5--50 μm depending on current, material and cone angle. A high current density and low voltage drop implies that this is an arc discharge, while the cold cathode and the absence f cathode spot trace are pertinent to a dense glow discharge. The mechanism of emission involving secondary electron emission is to be discussed

  8. Scaling of rotation and isotope separation in a vacuum-arc centrifuge

    International Nuclear Information System (INIS)

    Prasad, R.R.; Krishnan, M.

    1987-01-01

    Scaling is described of rotation, plasma column size and separation in a vacuum-arc centrifuge. The vacuum-arc centrifuge is a magnetized, fulled ionized, quasineutral column of plasma. The source of plasma is a vacuum-arc discharge between a negatively biased cathode and a grounded mesh anode. Rigid-body rotation, induced by the J x B force, causes radial, centrifugal separation of isotopes in the plasma column. Salient features of a fluid model that provides an understanding of rotation and the concomitant isotope separation in the vacuum-arc centrifuge are described. Scaling of rotation and plasma column size is found be consistent with the model. Measurements of isotope separation, also found to agree with the predictions of the model, are presented. Results of a parametric analysis of isotope separation in such a vacuum-arc centrifuge, using the fluid model and the observed scaling laws, are described. An analysis of the energy cost of separation of the vacuum-arc centrifuge shows that it typically requires only 70 keV/separated atom. (orig.)

  9. Upgraded vacuum arc ion source for metal ion implantation

    International Nuclear Information System (INIS)

    Nikolaev, A. G.; Oks, E. M.; Savkin, K. P.; Yushkov, G. Yu.; Brown, I. G.

    2012-01-01

    Vacuum arc ion sources have been made and used by a large number of research groups around the world over the past twenty years. The first generation of vacuum arc ion sources (dubbed ''Mevva,'' for metal vapor vacuum arc) was developed at Lawrence Berkeley National Laboratory in the 1980s. This paper considers the design, performance parameters, and some applications of a new modified version of this kind of source which we have called Mevva-V.Ru. The source produces broad beams of metal ions at an extraction voltage of up to 60 kV and a time-averaged ion beam current in the milliampere range. Here, we describe the Mevva-V.Ru vacuum arc ion source that we have developed at Tomsk and summarize its beam characteristics along with some of the applications to which we have put it. We also describe the source performance using compound cathodes.

  10. Bibliography and author index for electrical discharges in vacuum (1897 to 1980)

    Energy Technology Data Exchange (ETDEWEB)

    Miller, H.C.

    1982-01-29

    This bibliography covers the field of electrical discharges in vacuum, comprising both electrical breakdown in vacuum and vacuum arcs. A brief review section lists some review papers which would be helpful to the novice in this field. The bulk of the paper consists of bibliographic listings, arranged by year of publication and within each year, alphabetically by first author. An author index refers one to all papers authored or coauthored by a particular person. There are 2450 papers listed through December 1980.

  11. Bibliography and author index for electrical discharges in vacuum (1897-1978)

    International Nuclear Information System (INIS)

    Miller, H.C.

    1980-01-01

    This bibliography covers the field of electrical discharges in vacuum, comprising both electrical breakdown in vacuum and vacuum arcs. A breif review section lists some review papers which would be helpful to the novice in this field. The bulk of the paper consists of bibliographic listings, arranged by year of publication and within each year, alphabetically by first author. An author index refers one to all papers authored or coauthored by a particular person. There are 2032 papers listed through December 1978

  12. Cold cathode arc model in mercury discharges

    International Nuclear Information System (INIS)

    Li, Y.M.; Byszewski, W.W.; Budinger, A.B.

    1990-01-01

    Voltage/current characteristics measured during the starting of metal halide lamps indicate a low voltage discharge when condensates (mainly mercury) are localized on the electrodes. In this case, even with a cold cathode which does not emit electrons, the current is very high and voltage across the lamp drops to about 15 to 20 V. This type of discharge is similar to the cold cathode mercury vapor arc found in mercury pool rectifiers. The cathode sheath in the mercury vapor arc is characterized by very small cathode spot size, on the order of 10 -c cm 2 , very high current density of about 10 6 A/cm 2 and very low cathode fall of approximately 10 volts. The discharge is modified and generalized to describe the cathode phenomena in the cold cathode mercury vapor arc. The sensitivity of calculated discharge parameters with respect to such modifications were examined. Results show that the cathode fall voltage remains fairly constant (7-8 volts) with large fractional variations of metastable mercury atoms bombarding the cathode. This result compares very well with experimental waveforms when anode fall and plasma voltage approximations are incorporated

  13. Electrical and optical investigations on the low voltage vacuum arc

    International Nuclear Information System (INIS)

    Braic, M.; Braic, V.; Pavelescu, G.; Balaceanu, M.; Pavelescu, D.; Dumitrescu, G.; Gherendi, F.

    2002-01-01

    Preliminary investigations of a low voltage circuit breaker, adapted from a real industrial device, were carried out by electrical and optical methods. Electrical, parameters were measured in the high current arc period and in zero current moment (C.Z) and corroborated with the arc plasma spectroscopic investigations. For the first time in vacuum arc diagnostics, the paper presents results based on single shot time resolved emission spectroscopy around C.Z. The short-circuit current was produced in a special high power installation in order to reproduce exactly the short-circuit regimes developing in low voltage distribution networks. A stainless steel vacuum chamber with classical Cu-Cr electrodes was used. Tests were performed for different current values in the range 3 - 20 kA rms , the voltages being varied between 200 and 1000 V ac . Interruption processes in the different arc regimes (from the diffuse arc mode to the constricted column mode) were analyzed. The success of the arc interruption was analyzed in terms of electric arc energy achieved in the first current halfperiod. The results obtained were corroborated with arc plasma spectroscopic investigations. The emission spectroscopy setup, using an Acton spectrograph and an intensified CCD camera, allowed the spatial and time-resolved investigation of spectra emitted by the vacuum arc plasma. The first truly time-resolved spectroscopic measurements on a single half-period was proven to be a good method to investigate the vacuum arc. Using single shot time resolved spectroscopy around zero current on partial unsuccessful interruption we concluded that the Cu ions, more that Cr ions were responsible for the arc reignition. The financial support for this work comes from NATO-STI SfP /974083 and CORINT-Romania projects. (authors)

  14. Influence of N{sub 2} partial pressure on structural and microhardness properties of TiN/ZrN multilayers deposited by Ar/N{sub 2} vacuum arc discharge

    Energy Technology Data Exchange (ETDEWEB)

    Naddaf, M., E-mail: ascientific24@aec.org.sy [Department of Molecular Biology and Biotechnology, Atomic Energy Commission of Syria (AECS), P.O. Box 6091, Damascus (Syrian Arab Republic); Abdallah, B. [Department of Physics, Atomic Energy Commission of Syria, P.O. Box 6091, Damascus (Syrian Arab Republic); Ahmad, M. [IBA Laboratory, Department of Chemistry, Atomic Energy Commission of Syria, P.O. Box 6091, Damascus (Syrian Arab Republic); A-Kharroub, M. [Department of Physics, Atomic Energy Commission of Syria, P.O. Box 6091, Damascus (Syrian Arab Republic)

    2016-08-15

    The influence of N{sub 2} partial pressure on structural, mechanical and wetting properties of multilayered TiN/ZrN thin films deposited on silicon substrates by vacuum arc discharge of (N{sub 2} + Ar) gas mixtures is investigated. X-ray diffraction (XRD) results show that the average texturing coefficient of (1 1 1) orientation and the grain size of both TiN and ZrN individual layers increase with increasing the N{sub 2} partial pressure. The Rutherford back scattering (RBS) measurements and analysis reveal that incorporation of the nitrogen in the film increases with increasing the N{sub 2} partial pressure and both TiN and ZrN individual layers have a nitrogen over-stoichiometry for N{sub 2} partial pressure ⩾50%. The change in the film micro-hardness is correlated to the changes in crystallographic texture, grain size, stoichiometry and the residual stress in the film as a function of the N{sub 2} partial pressure. In particular, stoichiometry of ZrN and TiN individual is found to play the vital role in determining the multilayer hardness. The multilayer film deposited at N{sub 2} partial pressure of 25% has the best stoichiometric ratio of both TiN and ZrN layers and the highest micro-hardness of about 32 GPa. In addition, water contact angle (WCA) measurements and analysis show a decrease in the work of adhesion on increasing the N{sub 2} partial pressure.

  15. Production of hyperthermal hydrogen atoms by an arc discharge

    International Nuclear Information System (INIS)

    Samano, E.C.

    1993-01-01

    A magnetically confined thermal electric arc gas heater has been designed and built as a suitable source of heat for dissociating hydrogen molecules with energy in the range of a few eV. Specifically, the average beam kinetic energy is determined to be 1.5 eV, the dissociation rate is 0.5 atoms per molecule and the atom beam intensity in the forward direction is 1018 atoms/sr-sec. The working pressure in the arc discharge region is from 15 to 25 torr. This novel atom source has been successfully ignited and operated with pure hydrogen during several hours of continuous performance, maintaining its characteristics. The hyperthermal hydrogen atom beam, which is obtained from this source is analyzed and characterized in a high vacuum system, the characterization of the atom beam is accomplished by two different methods: calorimetry and surface ionization. Calorimetic sensor were used for detecting the atom beam by measuring the delivered power of the impinging atoms on the sensor surface. In the second approach an H-surface production backscattering experiment from a low work function surface was conducted. The validity of these two methods is discussed, and the results are compared. The different collision mechanisms to dissociate and ionize hydrogen molecules in the arch discharge are reviewed, as well as the physics of electric arcs. Finally, a Monte Carlo simulation program is used to calculate the ionization probability of low energy atoms perpendicularly reflected from a surface converter, as a model for atom surface ionization

  16. Macroparticle generation in DC arc discharge from a WC cathode

    Science.gov (United States)

    Zhirkov, Igor; Polcik, Peter; Kolozsvári, Szilard; Rosen, Johanna

    2017-03-01

    We have studied macroparticle generation from a tungsten carbide cathode used in a dc vacuum arc discharge. Despite a relatively high decomposition/melting point (˜3100 K), there is an intensive generation of visible particles with sizes in the range 20-35 μm. Visual observations during the discharge and scanning electron microscopy of the cathode surface and of collected macroparticles indicate a new mechanism for particle formation and acceleration. Based on the W-C phase diagram, there is an intensive sublimation of carbon from the melt resulting from the cathode spot. The sublimation supports the formation of a sphere, which is accelerated upon an explosion initiated by Joule heating at the critical contact area between the sphere and the cathode body. The explosive nature of the particle acceleration is confirmed by surface features resembling the remains of a splash on the droplet surface.

  17. Ecton mechanism of ion flow generation in vacuum arc

    CERN Document Server

    Mesyats, G A

    2001-01-01

    The basic characteristics of cathode plasma generation in vacuum arc (ion erosion, ion average charge) were studied from the point of an ecton model of a cathode spot in vacuum arc. The estimates of ion parameters obtained for a single cell of a cathode spot show qualitative conformity with the experimental data. One introduces the following mechanism of cathode plasma generation in vacuum arc. In case of explosion-like destruction of a cathode segment under the effect of the Joule heating the cathode matter changes sequentially its state: condensed one, nonideal and ideal plasma ones. During this change one observes formation of plasma charge composition and ion acceleration under the effect of plasma pressure gradient

  18. The interaction of vacuum arcs with magnetic fields and applications

    International Nuclear Information System (INIS)

    Gorman, J.G.; Kimblin, C.W.; Slade, P.G.; Voshall, R.E.; Wien, R.E.

    1983-01-01

    Vacuum arc/magnetic field interactions are reviewed and extended. An axial magnetic field (parallel to current flow) produces a stable and diffuse vacuum arc. These properties have been used to build a reliable dc switch for the Tokamak Fusion Test Reactor at Princeton. The switching duty for this Ohmic Heating Interrupter involves repetitive interruption of 24kA dc against a 27kV recovery voltage. A transverse magnetic field (perpendicular to current flow) produces an unstable arc with an ensuing high arc voltage. This property has been used to complete a metallic return transfer breaker for the Pacific HVDC Intertie, here the switching duty involves interruption of currents up to 2200A dc against an 80kV recovery voltage

  19. High Charge State Ions Extracted from Metal Plasmas in the Transition Regime from Vacuum Spark to High Current Vacuum Arc

    International Nuclear Information System (INIS)

    Yushkov, Georgy Yu.; Anders, A.

    2008-01-01

    Metal ions were extracted from pulsed discharge plasmas operating in the transition region between vacuum spark (transient high voltage of kV) and vacuum arc (arc voltage ∼ 20 V). At a peak current of about 4 kA, and with a pulse duration of 8 (micro)s, we observed mean ion charges states of about 6 for several cathode materials. In the case of platinum, the highest average charge state was 6.74 with ions of charge states as high as 10 present. For gold we found traces of charge state 11, with the highest average charge state of 7.25. At currents higher than 5 kA, non-metallic contaminations started to dominate the ion beam, preventing further enhancement of the metal charge states

  20. Modelling vacuum arcs : from plasma initiation to surface interactions

    International Nuclear Information System (INIS)

    Timko, H.

    2011-01-01

    A better understanding of vacuum arcs is desirable in many of today's 'big science' projects including linear colliders, fusion devices, and satellite systems. For the Compact Linear Collider (CLIC) design, radio-frequency (RF) breakdowns occurring in accelerating cavities influence efficiency optimisation and cost reduction issues. Studying vacuum arcs both theoretically as well as experimentally under well-defined and reproducible direct-current (DC) conditions is the first step towards exploring RF breakdowns. In this thesis, we have studied Cu DC vacuum arcs with a combination of experiments, a particle-in-cell (PIC) model of the arc plasma, and molecular dynamics (MD) simulations of the subsequent surface damaging mechanism. We have also developed the 2D Arc-PIC code and the physics model incorporated in it, especially for the purpose of modelling the plasma initiation in vacuum arcs. Assuming the presence of a field emitter at the cathode initially, we have identified the conditions for plasma formation and have studied the transitions from field emission stage to a fully developed arc. The 'footing' of the plasma is the cathode spot that supplies the arc continuously with particles; the high-density core of the plasma is located above this cathode spot. Our results have shown that once an arc plasma is initiated, and as long as energy is available, the arc is self-maintaining due to the plasma sheath that ensures enhanced field emission and sputtering.The plasma model can already give an estimate on how the time-to-breakdown changes with the neutral evaporation rate, which is yet to be determined by atomistic simulations. Due to the non-linearity of the problem, we have also performed a code-to-code comparison. The reproducibility of plasma behaviour and time-to-breakdown with independent codes increased confidence in the results presented here. Our MD simulations identified high-flux, high-energy ion bombardment as a possible mechanism forming the early

  1. Vacuum ARC ion sources - activities ampersand developments at LBL

    International Nuclear Information System (INIS)

    Brown, I.

    1996-01-01

    The author describes work at LBL on the development and application of vacuum arc ion sources. Work has been done on vacuum spark sources - to produce very high charge states, studies of high charge states in magnetic field, hybrid ion source operation on metal/gas plasma, multipole operation, work on MEVVA V for implantation applications, development of broad beam sources, and removal of particles from the output of the source

  2. Treatment of hazardous wastes by DC thermal plasma arc discharge

    International Nuclear Information System (INIS)

    Toru, Iwao; Yafang, Liu; Furuta, N.; Tsuginori, Inaba

    2001-01-01

    The temperature of the DC thermal plasma arc discharge is discussed, and examples of the waste treatment for the inorganic compounds such as fly ash, asbestos, and for the organic compounds such as the toxic dioxines and TBT by using the DC plasma arc discharge are shown. In addition, the plasma treatment by using a radiant power emitted from the DC plasma arc discharge is also shown as another new kind of ones. (authors)

  3. Discharge Characteristics of DC Arc Water Plasma for Environmental Applications

    Science.gov (United States)

    Li, Tianming; Sooseok, Choi; Takayuki, Watanabe

    2012-12-01

    A water plasma was generated by DC arc discharge with a hafnium embedded rod-type cathode and a nozzle-type anode. The discharge characteristics were examined by changing the operation parameter of the arc current. The dynamic behavior of the arc discharge led to significant fluctuations in the arc voltage and its frequency. Analyses of the high speed image and the arc voltage waveform showed that the arc discharge was in the restrike mode and its frequency varied within several tens of kilohertz according to the operating conditions. The larger thermal plasma volume was generated by the higher flow from the forming steam with a higher restrike frequency in the higher arc current conditions. In addition, the characteristics of the water plasma jet were investigated by means of optical emission spectroscopy to identify the abundant radicals required in an efficient waste treatment process.

  4. Discharge Characteristics of DC Arc Water Plasma for Environmental Applications

    International Nuclear Information System (INIS)

    Choi, Sooseok; Watanabe, Takayuki; Li Tianming

    2012-01-01

    A water plasma was generated by DC arc discharge with a hafnium embedded rod-type cathode and a nozzle-type anode. The discharge characteristics were examined by changing the operation parameter of the arc current. The dynamic behavior of the arc discharge led to significant fluctuations in the arc voltage and its frequency. Analyses of the high speed image and the arc voltage waveform showed that the arc discharge was in the restrike mode and its frequency varied within several tens of kilohertz according to the operating conditions. The larger thermal plasma volume was generated by the higher flow from the forming steam with a higher restrike frequency in the higher arc current conditions. In addition, the characteristics of the water plasma jet were investigated by means of optical emission spectroscopy to identify the abundant radicals required in an efficient waste treatment process. (plasma technology)

  5. Ion spectra of the metal vapor vacuum arc ion source with compound and alloy cathodes

    Science.gov (United States)

    Sasaki, Jun; Brown, Ian G.

    1990-01-01

    In metal vapor vacuum arc (MEVVA) ion sources, vacuum arc plasma with cathodes of single, pure elements has been utilized for the production of metal ions. In this study, we have investigated the charge state distributions of ions produced in vacuum arc plasmas in a MEVVA ion source for the case when the cathode is an alloy or a compound material. The ion charge state spectra were analyzed by means of a time-of-flight apparatus. We have compared the ion spectra for a cathode of an alloy or a compound material with its constituent elements: TiC/TiN/TiO2/Ti/C, SiC/Si/C, WC/W/C U/UN/(UN-ZrC)/Zr/C, and brass/Zn/Cu. We find that the MEVVA produces ions of all constituent elements in the compound and the alloy cathodes. The charge state distribution of each element differs, however, from the charge state distribution obtained in the vacuum arc with a cathode made of the pure, single constituent element. Fractional values of the total ion numbers of each constituent element in the extracted beam depart from the stoichiometry of the elements in the cathode material. In an operation with a TiC cathode, we irradiated a 304 stainless-steel plate with the extracted beam. Results from glow-discharge spectroscopy (GDS) of the surface show that both titanium and carbon are implanted in the substrate after the irradiation.

  6. Effect of arc behaviour on the temperature fluctuation of carbon electrode in DC arc discharge

    International Nuclear Information System (INIS)

    Liang, F; Tanaka, M; Choi, S; Watanabe, T

    2014-01-01

    Diffuse and multiple arc-anode attachment modes were observed in a DC arc discharge with a carbon electrode. During the arc discharge, the surface temperature of the electrode was successfully measured by two-colour pyrometry combined with a high-speed camera which employs appropriate band-pass filters. The relationship between the arc-anode attachment mode and the temperature fluctuation of electrode surface was investigated. The diffuse arc-anode attachment mode leads to relatively large temperature fluctuation on anode surface due to the rotation of the arc spot. In the case of diffuse mode, the purity of synthesized multi-wall carbon nanotube was deteriorated with temperature fluctuation

  7. Bibliography and author index for electrical discharges in vacuum (1897--1976)

    International Nuclear Information System (INIS)

    Miller, H.C.

    1978-01-01

    This bibliography covers the field of electrical discharges in vacuum, comprising both electrical breakdown in vacuum and vacuum arcs. A brief review section lists some review papers that would be helpful to the novice in this field. The bulk of the report consists of bibliographic listings, arranged by year of publication, and within each year, alphabetically by first author. An author index refers one to all papers authored or coauthored by a particular person. A total of 1,813 papers from 1897 through December 1976 are listed

  8. Simulation Research of Magnetic Constriction Effect and Controlling by Axial Magnetic Field of Vacuum Arc

    Institute of Scientific and Technical Information of China (English)

    王立军; 贾申利; 史宗谦; 荣命哲

    2005-01-01

    Based on magnetohydrodynamic (MHD) model of vacuum arc, the computer simulation of vacuum arc was carried out in this paper. In the MHD model, mass conservation equation,momentum conservation equations, energy conservation equations, generalized ohm's law and Maxwell equation were considered. MHD equations were calculated by numerical method, and the distribution of vacuum arc plasma parameters and current density were obtained. Simulation results showed that the magnetic constriction effect of vacuum arc is primarily caused by the Hall effect. In addition, the inhibition of axial magnetic field (AMF) on constriction of vacuum arc was calculated and analyzed.

  9. A Summary of Recent Experimental Research on Ion Energy and Charge States of Pulsed Vacuum Arcs

    International Nuclear Information System (INIS)

    Oks, Efim M.; Yushkov, Georgy Yu.; Anders, Andre

    2008-01-01

    The paper reviews the results of vacuum arc experimental investigations made collaboratively by research groups from Berkeley and Tomsk over the last two years, i.e. since the last ISDEIV in 2006. Vacuum arc plasma of various metals was produced in pulses of a few hundred microseconds duration, and the research focused on three topics: (i) the energy distribution functions for different ion charge states, (ii) the temporal development of the ion charge state distribution, and (iii) the evolution of the mean directed ion velocities during plasma expansion. A combined quadruple mass-to-charge and energy analyzer (EQP by HIDEN Ltd) and a time-of-flight spectrometer were employed. Cross-checking data by those complimentary techniques helped to avoid possible pitfalls in interpretation. It was found that the ion energy distribution functions in the plasma were independent of the ion charge state, which implies that the energy distribution on a substrate are not equal to due to acceleration in the substrate's sheath. In pulsed arc mode, the individual ion charge states fractions showed changes leading to a decrease of the mean charge state toward a steady-state value. This decrease can be reduced by lower arc current, higher pulse repetition rate and reduced length of the discharge gap. It was also found that the directed ion velocity slightly decreased as the plasma expanded into vacuum

  10. Streaming metal plasma generation by vacuum arc plasma guns

    International Nuclear Information System (INIS)

    MacGill, R.A.; Dickinson, M.R.; Anders, A.; Monteiro, O.R.; Brown, I.G.

    1998-01-01

    We have developed several different embodiments of repetitively pulsed vacuum arc metal plasma gun, including miniature versions, multicathode versions that can produce up to 18 different metal plasma species between which one can switch, and a compact high-duty cycle well-cooled version, as well as a larger dc gun. Plasma guns of this kind can be incorporated into a vacuum arc ion source for the production of high-energy metal ion beams, or used as a plasma source for thin film formation and for metal plasma immersion ion implantation and deposition. The source can also be viewed as a low-energy metal ion source with ion drift velocity in the range 20 - 200 eV depending on the metal species used. Here we describe the plasma sources that we have developed, the properties of the plasma generated, and summarize their performance and limitations. copyright 1998 American Institute of Physics

  11. Vacuum arc localization in CLIC prototype radio frequency accelerating structures

    CERN Document Server

    AUTHOR|(CDS)2091976; Koivunen, Visa

    2016-04-04

    A future linear collider capable of reaching TeV collision energies should support accelerating gradients beyond 100 MV/m. At such high fields, the occurrence of vacuum arcs have to be mitigated through conditioning, during which an accelerating structure’s resilience against breakdowns is slowly increased through repeated radio frequency pulsing. Conditioning is very time and resource consuming, which is why developing more efficient procedures is desirable. At CERN, conditioning related research is conducted at the CLIC high-power X-band test stands. Breakdown localization is an important diagnostic tool of accelerating structure tests. Abnormal position distributions highlight issues in structure design, manufacturing or operation and may consequently help improve these processes. Additionally, positioning can provide insight into the physics of vacuum arcs. In this work, two established positioning methods based on the time-difference-ofarrival of radio frequency waves are extended. The first method i...

  12. High current vacuum arc ion source for heavy ion fusion

    International Nuclear Information System (INIS)

    Qi, N.; Schein, J.; Gensler, S.; Prasad, R.R.; Krishnan, M.; Brown, I.

    1999-01-01

    Heavy Ion fusion (HIF) is one of the approaches for the controlled thermonuclear power production. A source of heavy ions with charge states 1+ to 2+, in ∼0.5 A current beams with ∼20 micros pulse widths and ∼10 Hz repetition rates are required. Thermionic sources have been the workhorse for the HIF program to date, but suffer from sloe turn-on, heating problems for large areas, are limited to low (contact) ionization potential elements and offer relatively low ion fluxes with a charge state limited to 1+. Gas injection sources suffer from partial ionization and deleterious neutral gas effects. The above shortcomings of the thermionic ion sources can be overcome by a vacuum arc ion source. The vacuum arc ion source is a good candidate for HIF applications. It is capable of providing ions of various elements and different charge states, in short and long pulse bursts, with low emittance and high beam currents. Under a Phase-I STTR from DOE, the feasibility of the vacuum arc ion source for the HIF applications is investigated. An existing ion source at LBNL was modified to produce ∼0.5 A, ∼60 keV Gd (A∼158) ion beams. The experimental effort concentrated on beam noise reduction, pulse-to-pulse reproducibility and achieving low beam emittance at 0.5 A ion current level. Details of the source development will be reported

  13. Electric arc discharge damage to ion thruster grids

    Science.gov (United States)

    Beebe, D. D.; Nakanishi, S.; Finke, R. C.

    1974-01-01

    Arcs representative of those occurring between the grids of a mercury ion thruster were simulated. Parameters affecting an arc and the resulting damage were studied. The parameters investigated were arc energy, arc duration, and grid geometry. Arc attenuation techniques were also investigated. Potentially serious damage occurred at all energy levels representative of actual thruster operating conditions. Of the grids tested, the lowest open-area configuration sustained the least damage for given conditions. At a fixed energy level a long duration discharge caused greater damage than a short discharge. Attenuation of arc current using various impedances proved to be effective in reducing arc damage. Faults were also deliberately caused using chips of sputtered materials formed during the operation of an actual thruster. These faults were cleared with no serious grid damage resulting using the principles and methods developed in this study.

  14. Preparation and investigation of diamond-like carbon stripper foils by filtered cathodic vacuum arc

    International Nuclear Information System (INIS)

    Fan, Qiwen; Du, Yinghui; Zhang, Rong; Xu, Guoji

    2013-01-01

    Thin diamond-like carbon (DLC) stripper foils ∼5μg/cm 2 in thickness were produced and evaluated as heavy-ion strippers for the Beijing HI-13 Tandem Accelerator. The DLC layers ∼4μg/cm 2 in thickness were produced by the filtered cathodic vacuum arc technology onto glass slides coated with betaine–saccharose as releasing agent, which were previously covered with evaporated carbon layers ∼1μg/cm 2 in thickness by the controlled ac arc-discharge method. Irradiation lifetimes of the DLC stripper foils were tested using the heavy-ion beams at the terminal of the Beijing HI-13 Tandem Accelerator, and compared with those of the standard carbon stripper foils made by the combined dc and ac arc-discharge method. The measurements indicate that the DLC stripper foils outlast the standard combined dc and ac arc-discharge carbon stripper foils by a factor of at least 13 and 4 for the 197 Au − (∼9MeV, ∼1μA) and 63 Cu − (∼9MeV, ∼1μA) ion beams, respectively. The structure and properties of the DLC foils deposited onto silicon substrates by the filtered cathodic vacuum arc technology were also evaluated and analyzed by scanning electron microscopy, Raman spectroscopy and X-ray photoelectron spectroscopy. The scanning electron microscopy images show that the DLC foils contain hardly droplets through the double 90° filters. The X-ray photoelectron spectrum indicates that sp 3 bonds of the DLC foils exceed 70%. The integral intensity ratio of the D peak to the G peak (I D /I G ) measured by the Raman spectroscopy is 0.78

  15. Direct-current cathodic vacuum arc system with magnetic-field mechanism for plasma stabilization.

    Science.gov (United States)

    Zhang, H-S; Komvopoulos, K

    2008-07-01

    Filtered cathodic vacuum arc (FCVA) deposition is characterized by plasma beam directionality, plasma energy adjustment via substrate biasing, macroparticle filtering, and independent substrate temperature control. Between the two modes of FCVA deposition, namely, direct current (dc) and pulsed arc, the dc mode yields higher deposition rates than the pulsed mode. However, maintaining the dc arc discharge is challenging because of its inherent plasma instabilities. A system generating a special configuration of magnetic field that stabilizes the dc arc discharge during film deposition is presented. This magnetic field is also part of the out-of-plane magnetic filter used to focus the plasma beam and prevent macroparticle film contamination. The efficiency of the plasma-stabilizing magnetic-field mechanism is demonstrated by the deposition of amorphous carbon (a-C) films exhibiting significantly high hardness and tetrahedral carbon hybridization (sp3) contents higher than 70%. Such high-quality films cannot be produced by dc arc deposition without the plasma-stabilizing mechanism presented in this study.

  16. Direct-current cathodic vacuum arc system with magnetic-field mechanism for plasma stabilization

    International Nuclear Information System (INIS)

    Zhang, H.-S.; Komvopoulos, K.

    2008-01-01

    Filtered cathodic vacuum arc (FCVA) deposition is characterized by plasma beam directionality, plasma energy adjustment via substrate biasing, macroparticle filtering, and independent substrate temperature control. Between the two modes of FCVA deposition, namely, direct current (dc) and pulsed arc, the dc mode yields higher deposition rates than the pulsed mode. However, maintaining the dc arc discharge is challenging because of its inherent plasma instabilities. A system generating a special configuration of magnetic field that stabilizes the dc arc discharge during film deposition is presented. This magnetic field is also part of the out-of-plane magnetic filter used to focus the plasma beam and prevent macroparticle film contamination. The efficiency of the plasma-stabilizing magnetic-field mechanism is demonstrated by the deposition of amorphous carbon (a-C) films exhibiting significantly high hardness and tetrahedral carbon hybridization (sp 3 ) contents higher than 70%. Such high-quality films cannot be produced by dc arc deposition without the plasma-stabilizing mechanism presented in this study

  17. Ion kinetic energy distribution in a pulsed vacuum arc with a straight magnetic filter

    International Nuclear Information System (INIS)

    Giuliani, L; Grondona, D; Kelly, H; Minotti, F

    2008-01-01

    In vacuum arcs of interest for film deposition the ion kinetic energy is of importance because it influences the coating properties. In this kind of discharge, the ions come out from the cathode spots with a high kinetic energy (20-150 eV). In the present work, we present measurements of vacuum arc ion energy distributions in a pulsed vacuum arc with a straight magnetic filter. A retarding field analyser (RFA) was used to perform the measurements that were carried out with a variable magnetic field strength (of the order of 10 mT). Since the interpretation of the results obtained from the RFA lies in the knowledge of the plasma and floating potential values, we have employed also Langmuir probes for determining those quantities. The obtained results for the ion kinetic energy are similar to those reported by other authors, but they were also found to be independent of the magnetic field strength. The electron temperature was also found to be independent of the magnetic field strength and of the axial position along the filter, indicating the absence of collisions.

  18. Thermionic vacuum arc (TVA) technique for magnesium thin film deposition

    Energy Technology Data Exchange (ETDEWEB)

    Balbag, M.Z., E-mail: zbalbag@ogu.edu.t [Eskisehir Osmangazi University, Education Faculty, Primary Education, Meselik Campus, Eskisehir 26480 (Turkey); Pat, S.; Ozkan, M.; Ekem, N. [Eskisehir Osmangazi University, Art and Science Faculty, Physics Department, Eskisehir 26480 (Turkey); Musa, G. [Ovidius University, Physics Department, Constanta (Romania)

    2010-08-15

    In this study, magnesium thin films were deposited on glass substrate by the Thermionic Vacuum Arc (TVA) technique for the first time. We present a different technique for deposition of high-quality magnesium thin films. By means of this technique, the production of films is achieved by condensing the plasma of anode material generated using Thermionic Vacuum Arc (TVA) under high vacuum conditions onto the surface to be coated. The crystal orientation and morphology of the deposited films were investigated by using XRD, EDX, SEM and AFM. The aim of this study is to search the use of TVA technique to coat magnesium thin films and to determine some of the physical properties of the films generated. Furthermore, this study will contribute to the scientific studies which search the thin films of magnesium or the compounds containing magnesium. In future, this study will be preliminary work to entirely produce magnesium diboride (MgB{sub 2}) superconductor thin film with the TVA technique.

  19. DC switch power supply for vacuum-arc coatings deposition

    International Nuclear Information System (INIS)

    Zalesskij, D.Yu.; Volkov, Yu.Ya.; Vasil'ev, V.V.; Kozhushko, V.V.; Luchaninov, A.A.; Strel'nitskij, V.E.

    2008-01-01

    Special DC Switch Power Supply for vacuum-arc deposition was developed and tested in the mode of depositing Al and AlN films. Maximum output power was 6 kW, maximum output current - 120 A, open-circuit voltage - 150 V. The Power Supply allows to adjust and stabilize output current in a wide range. Testing of the Power Supply revealed an advantages over the standard 'Bulat-6' power supply, especially for deposition of non-conductive AlN films.

  20. Vacuum arc switched inverter tests at 2.5 MVA

    International Nuclear Information System (INIS)

    Miller, R.N.; Gilmour, A.S. Jr.

    1979-01-01

    A mathematical analysis of the unloaded vacuum arc switch (VAS) inverter is undertaken; a key element in this analysis is the assumption of a constant voltage drop of 50 volts across each VAS while it is conducting. From this analysis a constant VAS-voltage model is developed to explain the VAS inverter operation. A comparison of data obtained from laboratory tests of the inverter is made with data obtained from this model, and agreement is found to be within 10% for up to 15 alternations

  1. Studies of hydrogen pellet acceleration by electric arc discharge

    International Nuclear Information System (INIS)

    Andersen, S.

    1986-01-01

    A preliminary design for an arc heated gas gun is described. The experimental development of the final design constitutes the final phase in contract work for JET. The gun consist of a cryogenic arc chamber connected to the inlet of a gun barrel. With a dose of H 2 -gas condensed in the arc chamber and a D 2 -pellet punch loaded into the barrel the gun is fired by the ignition of an electrical discharge in the arc chamber. The pellet is accelerated by the exhaust of hot H 2 -gas from the arc chamber and its velocity and acceleration is measured by time-of-flight along and outside the barrel. The pressure development by the arc is monitored by pressure transducers as well in the arc chamber as in the barrel. The performance of the gun is described in terms of arc current and voltage versus time as functions of power supply configuration and H 2 propellant dose. The time behaviour of the propellant pressure in the arc chamber and in the barrel is shown in relation to the arc current. Pellet acceleration and pressure development in the gun barrel for the arc heated gas gun is discussed and compared to results obtained by conventional fast valve acceleration

  2. Degradation of Verapamil hydrochloride in water by gliding arc discharge

    Czech Academy of Sciences Publication Activity Database

    Krishna, S.; Mašláni, Alan; Izdebski, T.; Horáková, M.; Klementová, Š.; Špatenka, P.

    2016-01-01

    Roč. 152, June (2016), s. 47-54 ISSN 0045-6535 Institutional support: RVO:61389021 Keywords : Gliding arc discharge * Emission spectroscopy * Pharmaceuticals * Half-life * Degradation mechanism Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 4.208, year: 2016 http://www.sciencedirect.com/science/article/pii/S0045653516302442

  3. Decomposition of naphthalene by dc gliding arc gas discharge.

    Science.gov (United States)

    Yu, Liang; Li, Xiaodong; Tu, Xin; Wang, Yu; Lu, Shengyong; Yan, Jianhua

    2010-01-14

    Gliding arc discharge has been proved to be effective in treatment of gas and liquid contaminants. In this study, physical characteristics of dc gliding arc discharge and its application to naphthalene destruction are investigated with different external resistances and carrier gases. The decomposition rate increases with increasing of oxygen concentration and decreases with external resistance. This value can be achieved up to 92.3% at the external resistance of 50 kOmega in the oxygen discharge, while the highest destruction energy efficiency reaches 3.6 g (kW h)(-1) with the external resistance of 93 kOmega. Possible reaction pathways and degradation mechanisms in the plasma with different gases are proposed by qualitative analysis of postdestructed products. In the air and oxygen gliding arc discharges, the naphthalene degradation is mainly governed by reactions with oxygen-derived radicals.

  4. Reinvestigation of the charge density distribution in arc discharge fusion system

    Energy Technology Data Exchange (ETDEWEB)

    Sheng, Lin Horng; Yee, Lee Kim; Nan, Phua Yeong; Thung, Yong Yun; Khok, Yong Thian; Rahman, Faidz Abd [Centre of Photonics and Advance Material, Universiti Tunku Abdul Rahman Kuala Lumpur (Malaysia)

    2015-04-24

    A continual arc discharge system has been setup and the light intensity of arc discharge has been profiled. The mathematical model of local energy density distribution in arc discharge fusion has been simulated which is in good qualitative agreement with light intensity profile of arc discharge in the experiments. Eventually, the local energy density distribution of arc discharge system is able to be precisely manipulated to act as heat source in the fabrication of fused fiber devices.

  5. Reinvestigation of the charge density distribution in arc discharge fusion system

    International Nuclear Information System (INIS)

    Sheng, Lin Horng; Yee, Lee Kim; Nan, Phua Yeong; Thung, Yong Yun; Khok, Yong Thian; Rahman, Faidz Abd

    2015-01-01

    A continual arc discharge system has been setup and the light intensity of arc discharge has been profiled. The mathematical model of local energy density distribution in arc discharge fusion has been simulated which is in good qualitative agreement with light intensity profile of arc discharge in the experiments. Eventually, the local energy density distribution of arc discharge system is able to be precisely manipulated to act as heat source in the fabrication of fused fiber devices

  6. High ion charge states in a high-current, short-pulse, vacuum ARC ion sources

    International Nuclear Information System (INIS)

    Anders, A.; Brown, I.; MacGill, R.; Dickinson, M.

    1996-01-01

    Ions of the cathode material are formed at vacuum arc cathode spots and extracted by a grid system. The ion charge states (typically 1-4) depend on the cathode material and only little on the discharge current as long as the current is low. Here the authors report on experiments with short pulses (several μs) and high currents (several kA); this regime of operation is thus approaching a more vacuum spark-like regime. Mean ion charge states of up to 6.2 for tungsten and 3.7 for titanium have been measured, with the corresponding maximum charge states of up to 8+ and 6+, respectively. The results are discussed in terms of Saha calculations and freezing of the charge state distribution

  7. High ion charge states in a high-current, short-pulse, vacuum arc ion source

    International Nuclear Information System (INIS)

    Anders, A.; Brown, I.; MacGill, R.; Dickinson, M.

    1995-09-01

    Ions of the cathode material are formed at vacuum arc cathode spots and extracted by a grid system. The ion charge states (typically 1--4) depend on the cathode material and only little on the discharge current as long as the current is low. Here the authors report on experiments with short pulses (several micros) and high currents (several kA); this regime of operation is thus approaching a more vacuum spark-like regime. Mean ion charge states of up to 6.2 for tungsten and 3.7 for titanium have been measured, with the corresponding maximum charge states of up to 8+ and 6+, respectively. The results are discussed in terms of Saha calculations and freezing of the charge state distribution

  8. Vacuum arc plasma generation and thin film deposition from a TiB{sub 2} cathode

    Energy Technology Data Exchange (ETDEWEB)

    Zhirkov, Igor, E-mail: igozh@ifm.liu.se; Petruhins, Andrejs; Naslund, Lars-Ake; Rosen, Johanna [Thin Film Physics Division, Department of Physics, Chemistry and Biology (IFM), Linköping University, SE-581 83 Linköping (Sweden); Kolozsvári, Szilard; Polcik, Peter [PLANSEE Composite Materials GmbH, Siebenbürgerstraße 23, 86983 Lechbruck am See (Germany)

    2015-11-02

    We have studied the utilization of TiB{sub 2} cathodes for thin film deposition in a DC vacuum arc system. We present a route for attaining a stable, reproducible, and fully ionized plasma flux of Ti and B by removal of the external magnetic field, which leads to dissipation of the vacuum arc discharge and an increased active surface area of the cathode. Applying a magnetic field resulted in instability and cracking, consistent with the previous reports. Plasma analysis shows average energies of 115 and 26 eV, average ion charge states of 2.1 and 1.1 for Ti and B, respectively, and a plasma ion composition of approximately 50% Ti and 50% B. This is consistent with measured resulting film composition from X-ray photoelectron spectroscopy, suggesting a negligible contribution of neutrals and macroparticles to the film growth. Also, despite the observations of macroparticle generation, the film surface is very smooth. These results are of importance for the utilization of cathodic arc as a method for synthesis of metal borides.

  9. Experimental investigation on the initial expansion stage of vacuum arc on cup-shaped TMF contacts

    Science.gov (United States)

    Wang, Ting; Xiu, Shixin; Liu, Zixi; Zhang, Yanzhe; Feng, Dingyu

    2018-02-01

    Arc behavior and measures to control it directly affect the properties of vacuum circuit breakers. Nowadays, transverse magnetic field (TMF) contacts are widely used for medium voltages. A magnetic field perpendicular to the current direction between the TMF contacts makes the arc move, transmitting its energy to the whole contact and avoiding excessive local ablation. Previous research on TMF arc behavior concentrated mainly on the arc movement and less on the initial stage (from arc ignition to an unstable arc column). A significant amount of experiment results suggest that there is a short period of arc stagnation after ignition. The duration of this arc stagnation and the arc characteristics during this stage affect the subsequent arc motion and even the breaking property of interrupters. The present study is of the arc characteristics in the initial stage. Experiments were carried out in a demountable vacuum chamber with cup-shaped TMF contacts. Using a high-speed camera, both single-point arc ignition mode and multiple-point arc ignition (MPAI) mode were observed. The experimental data show that the probability of MPAI mode occurring is related to the arc current. The influences of arc-ignition mode, arc current, and contact diameter on the initial expansion process were investigated. In addition, simulations were performed to analyze the multiple arc expansion process mechanically. Based on the experimental phenomena and simulation results, the mechanism of the arc expansion motion was analyzed.

  10. Modelling of plasma generation and expansion in a vacuum arc: application to the vacuum arc remelting process

    International Nuclear Information System (INIS)

    Chapelle, P.; Bellot, J.P.; Duval, H.; Jardy, A.; Ablitzer, D.

    2002-01-01

    As part of a complete theoretical description of the behaviour of the electric arc in the vacuum arc remelting process, a model has been developed for the column of plasma generated by a single cluster of cathode spots. The model combines a kinetic approach, taking into account the formation of the plasma in the cathodic region, and a hydrodynamic approach, describing the expansion of the plasma in the vacuum between the electrodes. The kinetic model is based on a system of Boltzmann-Vlasov-Poisson equations and uses a particle-type simulation procedure, combining the PIC (particle in cell) and FPM (finite point set method) methods. In the two-dimensional hydrodynamic model, the plasma is assimilated to a mixture of two continuous fluids (the electrons and the ions), each described by a system of coupled transport equations. Finally, a simplified method has been defined for calculating the electric current density and the energy flux density transmitted by the plasma to the anode. The results of the numerical simulation presented are consistent with a certain number of experimental data available in the literature. In particular, the model predicts a percentage of the electric power of the cluster transmitted to the anode (25%) in good agreement with the value indicated in the literature. (author)

  11. Electrode erosion in arc discharges at atmospheric pressure

    Science.gov (United States)

    Hardy, T. L.

    1985-01-01

    An experimental investigation was performed in an effort to measure and increase lifetime of electrodes in an arcjet thruster. The electrode erosion of various anode and cathode materials was measured after tests in an atmospheric pressure nitrogen arc discharge at powers less than 1 kW. A free-burning arc configuration and a constricted arc configuration were used to test the materials. Lanthanum hexboride and thoriated tungsten had low cathode erosion rates while thoriated tungsten and pure tungsten had the lowest anode erosion rates of the materials tested. Anode cooling, reverse gas flow, an external magnetic fields were all found to reduce electrode mass loss.

  12. Studies of pellet acceleration with arc discharge heated propellants

    International Nuclear Information System (INIS)

    Schuresko, D.D.

    1986-01-01

    An arc discharge has been utilized to heat gaseous propellants in a pneumatic pellet gun. A cylindrical arc chamber is interposed between the propellant inlet valve and the gun breech and fitted with a ceramic insert for generating swirl in the incoming gas stream. The arc is initiated after the propellant valve opens and the breech pressure starts to rise; a typical discharge lasts 300 microseconds with peak currents up to 2 kA at arc voltages ranging from 100-400 V. The system is instrumented with piezoelectric pressure transducers at the propellant valve outlet, gun breech, and gun muzzle. The gun has been operated with 4 mm diameter polyurethane foam pellets (density = 0.14 g/cm 3 ), a 40 cm-long barrel, and various gas propellants at pressures exceeding 70 bar. At I/sub arc/ = 1 kA, V/sub arc/ = 200 V, with helium propellant, the arc produces a 2-3 fold prompt increase in P/sub breech/ and a delayed increase in P/sub muzzle/; the pellets exit the gun from 0.5-1.0 ms earlier than with the gas alone at 40% higher speeds. Comparisons with the so-called ideal gun theory and with full one-dimensional hydrodynamic calculations of the pellet acceleration will be presented

  13. Studies of pellet acceleration with arc discharge heated propellants

    International Nuclear Information System (INIS)

    Schuresko, D.D.

    1985-01-01

    An arc discharge has been utilized to heat gaseous propellants in a pneumatic pellet gun. A cylindrical arc chamber is interposed between the propellant inlet valve and the gun breech and fitted with a ceramic insert for generating swirl in the incoming gas stream. The arc is initiated after the propellant valve opens and the breech pressure starts to rise; a typical discharge lasts 300 microseconds with peak currents u to 2 kA at arc voltages ranging from 100 to 400 V. The system is instrumented with piezoelectric pressure transducers at the propellant valve outlet, gun breech, and gun muzzle. The gun has been operated with 4 mm diameter polyurethane foam pellets (density = 0.14 g/cm 3 ), a 40 cm-long barrel, and various gas propellants at pressures exceeding 70 bar. At I/sub arc/ = 1 kA, V/sub arc/ = 200 V, with helium propellant, the arc produces a 2 to 3 fold prompt increase in P/sub breech/ and a delayed increase in P/sub muzzle/; the pellets exit the gun from 0.5 to 1.0 ms earlier than with the gas alone at 40% higher speeds. Comparisons with the so-called ideal gun theory and with full one-dimensional hydrodynamic calculations of the pellet acceleration will be presented

  14. Investigation of Vacuum Arc Voltage Characteristics Under Different Axial Magnetic Field Profiles

    International Nuclear Information System (INIS)

    Jia Shenli; Song Xiaochuan; Huo Xintao; Shi Zongqian; Wang Lijun

    2010-01-01

    Characteristics of the arc voltage under different profiles of axial magnetic field were investigated experimentally in a detachable vacuum chamber with five pairs of specially designed electrodes generating both bell-shaped and saddle-shaped magnetic field profile. The arc column and cathode spot images were photographed by a high speed digital camera. The dependence of the arc voltage on arcing evolution is analyzed. It is indicated that the axial magnetic field profile could affect the arc behaviors significantly, and the arc voltage is closely related to the arc light intensity.

  15. A high-current pulsed cathodic vacuum arc plasma source

    International Nuclear Information System (INIS)

    Oates, T.W.H.; Pigott, J.; Mckenzie, D.R.; Bilek, M.M.M.

    2003-01-01

    Cathodic vacuum arcs (CVAs) are well established as a method for producing metal plasmas for thin film deposition and as a source of metal ions. Fundamental differences exist between direct current (dc) and pulsed CVAs. We present here results of our investigations into the design and construction of a high-current center-triggered pulsed CVA. Power supply design based on electrolytic capacitors is discussed and optimized based on obtaining the most effective utilization of the cathode material. Anode configuration is also discussed with respect to the optimization of the electron collection capability. Type I and II cathode spots are observed and discussed with respect to cathode surface contamination. An unfiltered deposition rate of 1.7 nm per pulse, at a distance of 100 mm from the source, has been demonstrated. Instantaneous plasma densities in excess of 1x10 19 m -3 are observed after magnetic filtering. Time averaged densities an order of magnitude greater than common dc arc densities have been demonstrated, limited by pulse repetition rate and filter efficiency

  16. Investigation of Combined High-Frequency and Arc Discharges

    International Nuclear Information System (INIS)

    Taran, V.S.; Nezovibatko, Yu.N.; Marinin, V.G.; Shvets, O.M.; Ridozub, V.N.; Gasilin, V.V.

    2001-01-01

    In this paper we analyze experiment with arc and high-frequency (HF) plasma sources carried out in modified devise of the ''Bulat'' type. The HF-sources and combined discharges have attracted considerable attention for surface cleaning and coating. The utilization of such discharges allows decreasing droplet fraction formation and providing better adhesion and microhardness values. The existence of HF-field in plasma allows obtaining either conductive or dielectric coatings and they can be deposited on any substrates. (author)

  17. Laser-assisted vacuum arc extreme ultraviolet source: a comparison of picosecond and nanosecond laser triggering

    Science.gov (United States)

    Beyene, Girum A.; Tobin, Isaac; Juschkin, Larissa; Hayden, Patrick; O'Sullivan, Gerry; Sokell, Emma; Zakharov, Vassily S.; Zakharov, Sergey V.; O'Reilly, Fergal

    2016-06-01

    Extreme ultraviolet (EUV) light generation by hybrid laser-assisted vacuum arc discharge plasmas, utilizing Sn-coated rotating-disc-electrodes, was investigated. The discharge was initiated by localized ablation of the liquid tin coating of the cathode disc by a laser pulse. The laser pulse, at 1064 nm, was generated by Nd:YAG lasers with variable energy from 1 to 100 mJ per pulse. The impact of shortening the laser pulse from 7 ns to 170 ps on the EUV generation has been investigated in detail. The use of ps pulses resulted in an increase in emission of EUV radiation. With a fixed discharge energy of ~4 J, the EUV conversion efficiency tends to plateau at ~2.4  ±  0.25% for the ps laser pulses, while for the ns pulses, it saturates at ~1.7  ±  0.3%. Under similar discharge and laser energy conditions, operating the EUV source with the ps-triggering resulted also in narrower spectral profiles of the emission in comparison to ns-triggering. The results indicate an advantage in using ps-triggering in laser-assisted discharges to produce brighter plasmas required for applications such as metrology.

  18. Arc-discharge and magnetron sputtering combined equipment for nanocomposite coating deposition

    International Nuclear Information System (INIS)

    Koval, N.N.; Borisov, D.P.; Savostikov, V.M.

    2005-01-01

    It is known that characteristics of nanocomposite coatings produced by reactive magnetron sputtering undergo an essential influence on the following parameters such as original component composition of targets being sputtered, as well as abundance ratio of such components in the coatings deposited, relative content of inert and reactionary gases in a gas mixture used and a value of operating pressure in a chamber, substrate temperature, and a value of substrate bias potential, determining energy of ionized atoms, ionized atoms flow density, i.e. ion current density on a substrate. The multifactor character of production process of nanocomposite coatings with certain physical and mechanical properties demands a purposeful and complex control on all above-mentioned parameters. To solve such a problem, an arc-discharge and magnetron sputtering combined equipment including a vacuum chamber of approximately ∼ 0.5 m 3 with a built-in low-pressure plasma generator made on the basis of non-self-sustained discharge with a thermal cathode and a planar magnetron combined with two sputtered targets has been created. Construction of such a complex set-up provides both an autonomous mode of operation and simultaneous operation of an arc plasma generator and magnetron sputtering system. Magnetron sputtering of either one or two targets simultaneously is provided as well. An arc plasma generator enables ions current density control on a substrate in a wide range due to discharge current varying from 1 to 100 A. Energy of ions is also being controlled in a wide range by a negative bias potential from 0 to 1000 V applied to a substrate. The wide control range of gas plasma density of a arc discharge of approximately 10 9 -10 11 cm -3 and high uniformity of its distribution over the total volume of an operating chamber (about 15% error with regard to the mean value) provides a purposeful and simultaneous control either of magnetron discharge characteristics (operating pressure of

  19. Interaction of a vacuum arc plasma beam with an obstacle positioned normal to the plasma flow

    International Nuclear Information System (INIS)

    Zarchin, O; Zhitomirsky, V N; Goldsmith, S; Boxman, R L

    2003-01-01

    The effect of an obstacle positioned normal to a plasma jet produced by a vacuum arc plasma source on the radial distribution of ion flux in the vicinity of the obstacle was studied. This study was motivated by interest in the mutual influence of tightly packed substrates on coatings in industrial vacuum arc deposition systems. The experimental system consisted of a vacuum arc plasma source, a straight plasma duct, and a multi-probe consisting of a removable disc obstacle and a set of ring probes for measuring the radial ion flux. A dc arc discharge was ignited in vacuum between a truncated cone-shaped Cu cathode and an annular anode. The plasma jet produced by cathode spots passed through the anode aperture into the straight plasma duct. An axial magnetic field guided the plasma jet in the duct. The multi-probe consisted of a removable disc obstacle and a set of five ring probes for measuring the radial plasma flux as a function of distance from the disc obstacle. The rings and the disc probes were coaxially arranged on the multi-probe assembly and positioned so that plasma from the source passed through the ring probes and then encountered the disc. The influence of the obstacle was determined by measuring the ring ion currents, both in the presence of the obstacle, and when the disc obstacle was removed. The difference between the measured ion currents with and without the obstacle was interpreted to be the contribution of reflected or sputtered particles from the obstacle to the radial ion flux. The ring probes were biased by -60 V with respect to the grounded anode, to collect the saturated ion current. The multi-probe was connected to a movable stem, and positioned at different distances from the plasma source. A plasma density of ∼6 x 10 17 m -3 was estimated in this study based on the ion current to the obstacle. The radial ion flux collected by the ring probes increased by 20-25% due to the presence of the obstacle. As the calculated mean free path for

  20. Avoiding vacuum arcs in high gradient normal conducting RF structures

    CERN Document Server

    Sjøbæk, Kyrre Ness; Adli, Erik; Grudiev, Alexej; Wuensch, Walter

    In order to build the Compact LInear Collider (CLIC), accelerating structures reaching extremely high accelerating gradients are needed. Such structures have been built and tested using normal-conducting copper, powered by X-band RF power and reaching gradients of 100 MV/m and above. One phenomenon that must be avoided in order to reliably reach such gradients, is vacuum arcs or “breakdowns”. This can be accomplished by carefully designing the structure geometry such that high surface fields and large local power flows are avoided. The research presented in this thesis presents a method for optimizing the geometry of accelerating structures so that these breakdowns are made less likely, allowing the structure to operate reliably at high gradients. This was done primarily based on a phenomenological scaling model, which predicted the maximum gradient as a function of the break down rate, pulse length, and field distribution in the structure. The model is written in such a way that it allows direct comparis...

  1. Vacuum-arc plasma centrifuge applied to stable isotope separation

    International Nuclear Information System (INIS)

    Del Bosco, E.

    1989-09-01

    This work describes the results of a vacuum-arc plasma centrifuge experiment. A plasma centrifuge is an apparatus where a plasma column is produced due to the interaction of an electric current with an externally applied magnetic field, sup(→)J x sup(→)B. Among the applications of a rotating plasma, this work deals particularly with its utilization in an isotope enrichment device. The main characteristics of the plasma produced in this experiment are presented, with special attention to the plasma column rotation and the isotope enrichment. The analysis of the results is performed using a fluid model for a completely ionized rigid body rotating plasma column in steady state equilibrium. The main results are: a) rotation frequency of the plasma column in the range 2 x 10 sup(4) to 3 x 10 sup(5) rad/s; b) enrichment of 10 to 30% for the magnesium isotopes, and of 290 to 490% for the carbon 13 isotope; c) rigid body rotation of the plasma column only for radii smaller than the characteristic radius of the plasma column. re; d) linear dependence of the rotation frequency upon the magnetic field strength only for r < re; e) existence of an optimum value of the magnetic field for maximum enrichment; and f) dependence of the rotation frequency upon the inverse of the atomic mass. (author)

  2. Amorphous boron coatings produced with vacuum arc deposition technology

    CERN Document Server

    Klepper, C C; Yadlowsky, E J; Carlson, E P; Keitz, M D; Williams, J M; Zuhr, R A; Poker, D B

    2002-01-01

    In principle, boron (B) as a material has many excellent surface properties, including corrosion resistance, very high hardness, refractory properties, and a strong tendency to bond with most substrates. The potential technological benefits of the material have not been realized, because it is difficult to deposit it as coatings. B is difficult to evaporate, does not sputter well, and cannot be thermally sprayed. In this article, first successful deposition results from a robust system, based on the vacuum (cathodic) arc technology, are reported. Adherent coatings have been produced on 1100 Al, CP-Ti, Ti-6Al-4V, 316 SS, hard chrome plate, and 52 100 steel. Composition and thickness analyses have been performed by Rutherford backscattering spectroscopy. Hardness (H) and modules (E) have been evaluated by nanoindentation. The coatings are very pure and have properties characteristic of B suboxides. A microhardness of up to 27 GPa has been measured on a 400-nm-thick film deposited on 52 100 steel, with a corresp...

  3. The evolution of ion charge states in cathodic vacuum arc plasmas: a review

    Energy Technology Data Exchange (ETDEWEB)

    Anders, Andre

    2011-12-18

    Cathodic vacuum arc plasmas are known to contain multiply charged ions. 20 years after “Pressure Ionization: its role in metal vapour vacuum arc plasmas and ion sources” appeared in vol. 1 of Plasma Sources Science and Technology, it is a great opportunity to re-visit the issue of pressure ionization, a non-ideal plasma effect, and put it in perspective to the many other factors that influence observable charge state distributions, such as the role of the cathode material, the path in the density-temperature phase diagram, the “noise” in vacuum arc plasma as described by a fractal model approach, the effects of external magnetic fields and charge exchange collisions with neutrals. A much more complex image of the vacuum arc plasma emerges putting decades of experimentation and modeling in perspective.

  4. The multilayered structure of ultrathin amorphous carbon films synthesized by filtered cathodic vacuum arc deposition

    KAUST Repository

    Wang, Na; Komvopoulos, Kyriakos

    2013-01-01

    The structure of ultrathin amorphous carbon (a-C) films synthesized by filtered cathodic vacuum arc (FCVA) deposition was investigated by high-resolution transmission electron microscopy, electron energy loss spectroscopy, and x-ray photoelectron

  5. Preparation of gold nanoparticles by arc discharge in water

    International Nuclear Information System (INIS)

    Lung, Jen-Kuang; Huang, Jen-Chuen; Tien, Der-Chi; Liao, Chih-Yu; Tseng, Kuo-Hsiung; Tsung, Tsing-Tshin; Kao, Wen-Shiow; Tsai, Teh-Hua; Jwo, Ching-Song; Lin, Hong-Ming; Stobinski, Leszek

    2007-01-01

    Gold nanoparticles have been attracting attention due to their extensive application in chemistry, physics, material science, electronics, catalysis and bionanotechnology. Synthesis of gold nanoparticles often involves toxic and expensive physical-chemistry methods. Preparation of gold nanoparticles by arc discharge in water is proposed for the first time. Fabrication of gold nanostructures in deionized water has been successfully established. The evidence of gold particles' light absorbance reveals a unique surface plasmon resonance for Au nanoparticles suspended in deionized water. Gold nanostructures uniformly dispersed in water, their UV-Vis absorption and crystalline size are shown. Our experimental results demonstrate that fabrication of gold nanoparticles by arc discharge in water is an alternative, cheap, effective and environmentally friendly method

  6. Production of ceramic-metal joints for high-vacuum applications and development of simulation program for discharge tube

    Energy Technology Data Exchange (ETDEWEB)

    Kang, S. H.; Chung, K. H. [Seoul National University, Seoul (Korea)

    2000-04-01

    To develop a ceramic-metal jointed tube for high-vacuum applications, metalizing process and active metal brazing were investigated. Active metal brazing was adopted as a joining process to produce a high-vacuum tube which had high joint strength and reliability. A possibility for the development of new composition of Mo-Mn paste was studied. Also, to improve the strength and reliability of active metal brazed joint, TiN coating was introduced as a diffusion barrier. It was revealed that TiN coating could improve the joint strength and reliability. 100mm {phi} tube joint was produced using incusil ABA brazing alloy. The strength and reliability of manufactured tube showed higher value than commercial one. The electric field distribution in ceramic tube under high voltage was analyzed. Two dimensional electric field distribution was investigated under the existence of charged particles. From this result, electric field distribution at the surface of ceramic tube and the location of high electric field was predicted. Finally, Arc discharge was simulated to analyze the effect of arc discharge on the discharge tube wall. The maximum temperature of arc was 12000-13000K. The wall temperature was increased 100-170K by the arc discharge. 45 refs., 57 figs., 4 tabs. (Author)

  7. Large area, surface discharge pumped, vacuum ultraviolet light source

    Science.gov (United States)

    Sze, R.C.; Quigley, G.P.

    1996-12-17

    Large area, surface discharge pumped, vacuum ultraviolet (VUV) light source is disclosed. A contamination-free VUV light source having a 225 cm{sup 2} emission area in the 240-340 nm region of the electromagnetic spectrum with an average output power in this band of about 2 J/cm{sup 2} at a wall-plug efficiency of approximately 5% is described. Only ceramics and metal parts are employed in this surface discharge source. Because of the contamination-free, high photon energy and flux, and short pulse characteristics of the source, it is suitable for semiconductor and flat panel display material processing. 3 figs.

  8. The Studies of a Vacuum Gap Breakdown after High-Current Arc Interruption with Increasing the Voltage

    Science.gov (United States)

    Schneider, A. V.; Popov, S. A.; Batrakov, A. V.; Dubrovskaya, E. L.; Lavrinovich, V. A.

    2017-12-01

    Vacuum-gap breakdown has been studied after high-current arc interruption with a subsequent increase in the transient recovery voltage across a gap. The effects of factors, such as the rate of the rise in the transient voltage, the potential of the shield that surrounds a discharge gap, and the arc burning time, have been determined. It has been revealed that opening the contacts earlier leads to the formation of an anode spot, which is the source of electrode material vapors into the discharge gap after current zero moment. Under the conditions of increasing voltage, this fact results in the breakdown. Too late opening leads to the breakdown of a short gap due to the high electric fields.

  9. Vacuum arcing behavior between transverse magnetic field contacts subjected to variable axial magnetic field

    Energy Technology Data Exchange (ETDEWEB)

    Ma, Hui; Wang, Jianhua; Liu, Zhiyuan, E-mail: liuzy@mail.xjtu.edu.cn; Geng, Yingsan; Wang, Zhenxing; Yan, Jing [State Key Laboratory of Electrical Insulation and Power Equipment, Xi' an Jiaotong University, Xi' an 710049 (China)

    2016-06-15

    The objective of this work is to reveal the effects of an axial magnetic field (AMF) on the vacuum arc characteristics between transverse magnetic field (TMF) contacts. These vacuum arc characteristics include the vacuum arcing behavior and the arc voltage waveform. In the experiments, an external AMF was applied to a pair of TMF contacts. The external AMF flux density B{sub AMF} can be adjusted from 0 to 110 mT. The arc current in the tests varied over a range from 0 to 20 kA rms at 45 Hz. The contact material was CuCr25 (25% Cr). A high-speed charge-coupled device video camera was used to record the vacuum arc evolution. The experimental results show that the application of the AMF effectively reduces the TMF arc voltage noise component and reduces the formation of liquid metal drops between the contacts. The diffuse arc duration increases linearly with increasing AMF flux density, but it also decreases linearly with increasing arc current under application of the external AMF. The results also indicate that the diffuse arc duration before the current zero is usually more than 1 ms under the condition that the value of the AMF per kiloampere is more than 2.0 mT/kA. Finally, under application of the AMF, the arc column of the TMF contacts may constrict and remain in the center region without transverse rotation. Therefore, the combined TMF–AMF contacts should be designed such that they guarantee that the AMF is not so strong as to oppose transverse rotation of the arc column.

  10. Vacuum arcing behavior between transverse magnetic field contacts subjected to variable axial magnetic field

    International Nuclear Information System (INIS)

    Ma, Hui; Wang, Jianhua; Liu, Zhiyuan; Geng, Yingsan; Wang, Zhenxing; Yan, Jing

    2016-01-01

    The objective of this work is to reveal the effects of an axial magnetic field (AMF) on the vacuum arc characteristics between transverse magnetic field (TMF) contacts. These vacuum arc characteristics include the vacuum arcing behavior and the arc voltage waveform. In the experiments, an external AMF was applied to a pair of TMF contacts. The external AMF flux density B AMF can be adjusted from 0 to 110 mT. The arc current in the tests varied over a range from 0 to 20 kA rms at 45 Hz. The contact material was CuCr25 (25% Cr). A high-speed charge-coupled device video camera was used to record the vacuum arc evolution. The experimental results show that the application of the AMF effectively reduces the TMF arc voltage noise component and reduces the formation of liquid metal drops between the contacts. The diffuse arc duration increases linearly with increasing AMF flux density, but it also decreases linearly with increasing arc current under application of the external AMF. The results also indicate that the diffuse arc duration before the current zero is usually more than 1 ms under the condition that the value of the AMF per kiloampere is more than 2.0 mT/kA. Finally, under application of the AMF, the arc column of the TMF contacts may constrict and remain in the center region without transverse rotation. Therefore, the combined TMF–AMF contacts should be designed such that they guarantee that the AMF is not so strong as to oppose transverse rotation of the arc column.

  11. Vacuum arcing behavior between transverse magnetic field contacts subjected to variable axial magnetic field

    Science.gov (United States)

    Ma, Hui; Wang, Jianhua; Liu, Zhiyuan; Geng, Yingsan; Wang, Zhenxing; Yan, Jing

    2016-06-01

    The objective of this work is to reveal the effects of an axial magnetic field (AMF) on the vacuum arc characteristics between transverse magnetic field (TMF) contacts. These vacuum arc characteristics include the vacuum arcing behavior and the arc voltage waveform. In the experiments, an external AMF was applied to a pair of TMF contacts. The external AMF flux density BAMF can be adjusted from 0 to 110 mT. The arc current in the tests varied over a range from 0 to 20 kA rms at 45 Hz. The contact material was CuCr25 (25% Cr). A high-speed charge-coupled device video camera was used to record the vacuum arc evolution. The experimental results show that the application of the AMF effectively reduces the TMF arc voltage noise component and reduces the formation of liquid metal drops between the contacts. The diffuse arc duration increases linearly with increasing AMF flux density, but it also decreases linearly with increasing arc current under application of the external AMF. The results also indicate that the diffuse arc duration before the current zero is usually more than 1 ms under the condition that the value of the AMF per kiloampere is more than 2.0 mT/kA. Finally, under application of the AMF, the arc column of the TMF contacts may constrict and remain in the center region without transverse rotation. Therefore, the combined TMF-AMF contacts should be designed such that they guarantee that the AMF is not so strong as to oppose transverse rotation of the arc column.

  12. Modelling of crater formation on anode surface by high-current vacuum arcs

    Science.gov (United States)

    Tian, Yunbo; Wang, Zhenxing; Jiang, Yanjun; Ma, Hui; Liu, Zhiyuan; Geng, Yingsan; Wang, Jianhua; Nordlund, Kai; Djurabekova, Flyura

    2016-11-01

    Anode melting and crater formation significantly affect interruption of high-current vacuum arcs. The primary objective of this paper is to theoretically investigate the mechanism of anode surface crater formation, caused by the combined effect of surface heating during the vacuum arc and pressure exerted on the molten surface by ions and electrons from the arc plasma. A model of fluid flow and heat transfer in the arc anode is developed and combined with a magnetohydrodynamics model of the vacuum arc plasma. Crater formation is observed in simulation for a peak arcing current higher than 15 kA on 40 mm diam. Cu electrodes spaced 10 mm apart. The flow of liquid metal starts after 4 or 5 ms of arcing, and the maximum velocities are 0.95 m/s and 1.39 m/s for 20 kA and 25 kA arcs, respectively. This flow redistributes thermal energy, and the maximum temperature of the anode surface does not remain in the center. Moreover, the condition for the liquid droplet formation on the anode surfaces is developed. The solidification process after current zero is also analyzed. The solidification time has been found to be more than 3 ms after 25 kA arcing. The long solidification time and sharp features on crater rims induce Taylor cone formation.

  13. Atmospheric pressure arc discharge with ablating graphite anode

    International Nuclear Information System (INIS)

    Nemchinsky, V A; Raitses, Y

    2015-01-01

    The anodic carbon arc discharge is used to produce carbon nanoparticles. Recent experiments with the carbon arc at atmospheric pressure helium demonstrated the enhanced ablation rate for narrow graphite anodes resulting in high deposition rates of carbonaceous products on the copper cathode (Fetterman et al 2008 Carbon 46 1322–6). The proposed model explains these results with interconnected steady-state models of the cathode and the anode processes. When considering cathode functioning, the model predicts circulation of the particles in the near-cathode region: evaporation of the cathode material, ionization of evaporated atoms and molecules in the near-cathode plasma, return of the resulting ions to the cathode, surface recombination of ions and electrons followed again by cathode evaporation etc. In the case of the low anode ablation rate, the ion acceleration in the cathode sheath provides the major cathode heating mechanism. In the case of an intensive anode ablation, an additional cathode heating is due to latent fusion heat of the atomic species evaporated from the anode and depositing at the cathode. Using the experimental arc voltage as the only input discharge parameter, the model allows us to calculate the anode ablation rate. A comparison of the results of calculations with the available experimental data shows reasonable agreement. (paper)

  14. Atmospheric pressure arc discharge with ablating graphite anode

    Science.gov (United States)

    Nemchinsky, V. A.; Raitses, Y.

    2015-06-01

    The anodic carbon arc discharge is used to produce carbon nanoparticles. Recent experiments with the carbon arc at atmospheric pressure helium demonstrated the enhanced ablation rate for narrow graphite anodes resulting in high deposition rates of carbonaceous products on the copper cathode (Fetterman et al 2008 Carbon 46 1322-6). The proposed model explains these results with interconnected steady-state models of the cathode and the anode processes. When considering cathode functioning, the model predicts circulation of the particles in the near-cathode region: evaporation of the cathode material, ionization of evaporated atoms and molecules in the near-cathode plasma, return of the resulting ions to the cathode, surface recombination of ions and electrons followed again by cathode evaporation etc. In the case of the low anode ablation rate, the ion acceleration in the cathode sheath provides the major cathode heating mechanism. In the case of an intensive anode ablation, an additional cathode heating is due to latent fusion heat of the atomic species evaporated from the anode and depositing at the cathode. Using the experimental arc voltage as the only input discharge parameter, the model allows us to calculate the anode ablation rate. A comparison of the results of calculations with the available experimental data shows reasonable agreement.

  15. New developments in metal ion implantation by vacuum arc ion sources and metal plasma immersion

    International Nuclear Information System (INIS)

    Brown, I.G.; Anders, A.; Anders, S.

    1996-01-01

    Ion implantation by intense beams of metal ions can be accomplished using the dense metal plasma formed in a vacuum arc discharge embodied either in a vacuum arc ion source or in a metal plasma immersion configuration. In the former case high energy metal ion beams are formed and implantation is done in a more-or-less conventional way, and in the latter case the substrate is immersed in the plasma and repetitively pulse-biased so as to accelerate the ions at the high voltage plasma sheath formed at the substrate. A number of advances have been made in the last few years, both in plasma technology and in the surface modification procedures, that enhance the effectiveness and versatility of the methods, including for example: controlled increase of the in charge states produced; operation in a dual metal-gaseous ion species mode; very large area beam formation; macroparticle filtering; and the development of processing regimes for optimizing adhesion, morphology and structure. These complementary ion processing techniques provide the plasma tools for doing ion surface modification over a very wide parameter regime, from pure ion implantation at energies approaching the MeV level, through ion mixing at energies in the ∼1 to ∼100 keV range, to IBAD-like processing at energies from a few tens of eV to a few keV. Here the authors review the methods, describe a number of recent developments, and outline some of the surface modification applications to which the methods have been put. 54 refs., 9 figs

  16. The development of shock wave overpressure driven by channel expansion of high current impulse discharge arc

    Science.gov (United States)

    Xiong, Jia-ming; Li, Lee; Dai, Hong-yu; Wu, Hai-bo; Peng, Ming-yang; Lin, Fu-chang

    2018-03-01

    During the formation of a high current impulse discharge arc, objects near the discharge arc will be strongly impacted. In this paper, a high power, high current gas switch is used as the site of the impulse discharge arc. The explosion wave theory and the arc channel energy balance equation are introduced to analyze the development of the shock wave overpressure driven by the high current impulse discharge arc, and the demarcation point of the arc channel is given, from which the energy of the arc channel is no longer converted into shock waves. Through the analysis and calculation, it is found that the magnitude of the shock wave overpressure caused by impulse discharge arc expansion is closely related to the arc current rising rate. The arc shock wave overpressure will undergo a slow decay process and then decay rapidly. The study of this paper will perform the function of deepening the understanding of the physical nature of the impulse arc discharge, which can be used to explain the damage effect of the high current impulse discharge arc.

  17. Magnetic circuit design of magnetically driving gliding arc discharge device

    International Nuclear Information System (INIS)

    Jiang Zhonghe; Liu Minghai; Gu Chenglin; Pan Yuan

    2002-01-01

    A gliding arc discharge driven by magnetic field at atmospheric pressure can generate non-equilibrium plasma with good confinement property, and has extensive application in the areas of microelectronic fabrication, environmental engineering, etc. The magnetic circuit of the generator is designed with the permeance method, and analytic expression is obtained on the magnetic induction, the permeant magnetic material thickness and length of air gap. The results have been compared with those of the finite element method, the difference is 3.1%. But the permeance method is more concise and convenient and more universal and economical. So the permeance method is a more credible and useful engineering arithmetic

  18. Design and analysis of high current DC power supply for vacuum arc melting furnace

    International Nuclear Information System (INIS)

    Adhikary, Santu; Sharma, Vishnu Kumar; Sharma, Archana

    2015-01-01

    Vacuum Arc furnace (VAR), is used for melting of ingot in many industrial units. Till now in many industries the existing power supply for VAR is based on magnetic amplifier, which is a lossy component. Thus an efficient topology is needed to develop as a suitable alternative for the existing power supply. Basically Arc in electrical furnace is an unstable phenomena, it has drooping characteristic in nature so to stabilize the arc we need a power supply across the load (arc), which is more drooping in nature than arc characteristics. So this paper highlights the stability and response analysis of several alternative topologies and Stabilization of arc using the feedback and firing angle control in MATLAB. The work also covers comparison among those topologies to choose the optimized topology as a suitable alternative of the existing magnetic amplifier based power supply and the detail design of the proposed topology with a tested trail circuit in PROTEUS. (author)

  19. Fundamentals studies of a magnetically steered vacuum arc

    Science.gov (United States)

    Walke, Paul

    In recent years demand from production industry for high performance cutting tools, aero and automobile engine parts has prompted research into both existing and novel methods of laying down hard, low friction coatings . A key process for the production of such coatings has been Physical Vapour Deposition (PVD) which has proved to be a consistent and reliable tool for industry. For this technique to continue to be improved and more advanced coatings to be produced, research at the fundamental level is required. This thesis describes research investigating the behaviour of the steered arc cathode spot and methods of improving existing steered arc coating technology.The majority of existing steered arc systems use either permanent magnets or a combination of permanent and electromagnets to steer the arc. Described here is a novel system which employs a pair of electromagnetic coils of cylindrical geometry which enable the arc to be positioned on a circular orbit through a range of continuously variable radii. In addition to this the coils are capable of controlling the transverse and normal magnetic field profiles independently of the steering radius selected. This enables the behaviour of the arc spot to be investigated under a range of magnetic field conditions thus allowing the comparison of measured arc behaviour with a new model of arc motion. Care has described the motion of the arc spot as a biased random walk and has derived an analytical solution to describe the time dependent, probability density function for the arc position in two dimensions. Two distributions are proposed (one in each dimension); the first describes the probability density for the arc position in the direction of driven motion, the second the probability density in the direction of arc confinement. The shape of these distributions is dependent upon the transverse and normal components of the applied magnetic field.A series of experiments are described here that measure the shape of these

  20. Free double layers in mercury-arc discharges

    International Nuclear Information System (INIS)

    Maciel, H.S.; Allen, J.E.

    1989-01-01

    A study has been carried out of free double layers formed within the plasma volume of a low-pressure mercury-arc discharge at high current densities. The free double layer is observed to form as a visible boundary, which drifts slowly from the central section of the discharge. Current-driven instabilities are observed as the discharge current is gradually increased to a critical value, at which current limitation is observed to occur. This process, which is accompanied by high-current spikes, ceases when the free double layer becomes visible as a sharp boundary dividing the discharge column into two regions of different luminosities. The layer is observed to form in the later stages of current limitation, the onset of which occurs for a ratio of drift to thermal speed of electrons of about unity. Electrical energy is converted by the layer into kinetic energy of the changed particles. Accordingly high-energy ions were measured by means of an electrostatic energy analyser. The multiple-sheath character of the free 'double layer'', which is inferred from probe measurements of potential profiles, is discussed and comparisons with other space-charge structures with the same topology are made. (author)

  1. Scintillation screen applications in a vacuum arc ion source with composite hydride cathode

    Science.gov (United States)

    Wang, X. H.; Tuo, X. G.; Yang, Z.; Peng, Y. F.; Li, J.; Lv, H. Y.; Li, J. H.; Long, J. D.

    2018-05-01

    Vacuum arc ion source with composite hydride cathode was developed to produce intense ion beams which can be applied in particle accelerator injections. Beam profile and beam composition are two fundamental parameters of the beam for the vacuum arc ion source in such specific applications. An aluminum-coated scintillation screen with an ICCD camera readout was used to show the space-time distribution of the beam directly. A simple magnetic analysis assembly with the scintillation screen shows the beam composition information of this kind ion source. Some physical and technical issues are discussed and analyzed in the text.

  2. Increasing of charge of uranium ion beam in vacuum-arc-type source (MEVVA)

    CERN Document Server

    Kulevoj, T V; Petrenko, S V; Seleznev, D N; Pershin, V I; Batalin, V A; Kolomiets, A A

    2002-01-01

    Research efforts with MEVVA type source (Metal Vapor Vacuum Arc) and with its modifications are in progress now in the ITEP. In the course of research one revealed possibility to increase charge state of generated beam of uranium ions. Increase of charge results from propagation of high-current vacuum-arc charge from the source cathode to the extra anode located in increasing axial magnetic field. One obtained uranium ion beam with 150 mA output current 10% of which were contributed by U sup 7 sup + uranium ions

  3. Miniature pulsed vacuum arc plasma gun and apparatus for thin-film fabrication

    Science.gov (United States)

    Brown, Ian G.; MacGill, Robert A.; Galvin, James E.; Ogletree, David F.; Salmeron, Miquel

    1998-01-01

    A miniature (dime-size in cross-section) vapor vacuum arc plasma gun is described for use in an apparatus to produce thin films. Any conductive material can be layered as a film on virtually any substrate. Because the entire apparatus can easily be contained in a small vacuum chamber, multiple dissimilar layers can be applied without risk of additional contamination. The invention has special applications in semiconductor manufacturing.

  4. The fractal nature of vacuum arc cathode spots

    International Nuclear Information System (INIS)

    Anders, Andre

    2005-01-01

    Cathode spot phenomena show many features of fractals, for example self-similar patterns in the emitted light and arc erosion traces. Although there have been hints on the fractal nature of cathode spots in the literature, the fractal approach to spot interpretation is underutilized. In this work, a brief review of spot properties is given, touching the differences between spot type 1 (on cathodes surfaces with dielectric layers) and spot type 2 (on metallic, clean surfaces) as well as the known spot fragment or cell structure. The basic properties of self-similarity, power laws, random colored noise, and fractals are introduced. Several points of evidence for the fractal nature of spots are provided. Specifically power laws are identified as signature of fractal properties, such as spectral power of noisy arc parameters (ion current, arc voltage, etc) obtained by fast Fourier transform. It is shown that fractal properties can be observed down to the cutoff by measurement resolution or occurrence of elementary steps in physical processes. Random walk models of cathode spot motion are well established: they go asymptotically to Brownian motion for infinitesimal step width. The power spectrum of the arc voltage noise falls as 1/f 2 , where f is frequency, supporting a fractal spot model associated with Brownian motion

  5. Effects of an anode sheath on energy and momentum transfer in vacuum arcs

    International Nuclear Information System (INIS)

    Wang, Zhenxing; Zhou, Zhipeng; Tian, Yunbo; Wang, Haoran; Wang, Jianhua; Geng, Yingsan; Liu, Zhiyuan

    2017-01-01

    Anode phenomena under high-current vacuum arcs have a significant impact on the interrupting capacity of vacuum interrupters. However, the vacuum arc energy flux and momentum flux on the anode—which are necessary boundary conditions for simulations—are either set to an imaginary distribution or calculated using simple formulas without considering anode sheath regulatory effects. The objective of this paper is to reveal the anode sheath effects on regulating the energy and momentum transfer from the arc column to the anode surface in vacuum arcs. A particle-in-cell model for the anode sheath is developed. The required input parameters are obtained from a magnetohydrodynamic model for the arc column. From the results, there exists a sheath near the anode with a negative voltage drop. Both the electron density and the ion density significantly decline in the anode sheath region. The kinetic energy of the ions absorbed by the anode consists of directed kinetic energy, random kinetic energy, and sheath acceleration energy. The sheath acceleration energy contribution is the largest, and the random kinetic energy also accounts for a large part that cannot be ignored. The arc pressure on the anode surface is mainly caused by ion impact, and the accelerating effect of the anode sheath on the ions cannot be neglected in pressure calculations. In addition, in the case of an arc current at 15 kA, the input energy and momentum upon the anode surface is not obviously affected by the evaporated atoms at surface temperatures of 1600 K and 2000 K. (paper)

  6. Application of high speed photography for high current vacuum arcs

    NARCIS (Netherlands)

    Damstra, G.C.; Merck, W.F.H.; Vossen, J.W.G.L.; Janssen, M.F.P.; Bouwmeester, C.E.

    1998-01-01

    A high speed image detection system for 106 frames per second or 107 streaks per second has been developed for the testing of vacuum circuit breakers, using 10×16 optical fibres for light transfer to 160 fast photo diodes. The output of these diodes is multiplexed, AD converted in a 4 bit

  7. Low pressure arc discharge lamp apparatus with magnetic field generating means

    Science.gov (United States)

    Grossman, Mark W.; George, William A.; Maya, Jakob

    1987-01-01

    A low-pressure arc discharge apparatus having a magnetic field generating means for increasing the output of a discharge lamp is disclosed. The magnetic field generating means, which in one embodiment includes a plurality of permanent magnets, is disposed along the lamp for applying a constant transverse magnetic field over at least a portion of the positive discharge column produced in the arc discharge lamp operating at an ambient temperature greater than about 25.degree. C.

  8. Low pressure arc discharge lamp apparatus with magnetic field generating means

    Science.gov (United States)

    Grossman, M.W.; George, W.A.; Maya, J.

    1987-10-06

    A low-pressure arc discharge apparatus having a magnetic field generating means for increasing the output of a discharge lamp is disclosed. The magnetic field generating means, which in one embodiment includes a plurality of permanent magnets, is disposed along the lamp for applying a constant transverse magnetic field over at least a portion of the positive discharge column produced in the arc discharge lamp operating at an ambient temperature greater than about 25 C. 3 figs.

  9. Influences of arc current on composition and properties of MgO thin films prepared by cathodic vacuum arc deposition

    International Nuclear Information System (INIS)

    Zhu Daoyun; Zheng Changxi; Wang Mingdong; Liu Yi; Chen Dihu; He Zhenhui; Wen Lishi; Cheung, W.Y.

    2010-01-01

    MgO thin films with high optical transmittances (more than 90%) were prepared by cathodic vacuum arc deposition technique. With the increase of arc current from 40 to 80 A, the deposition pressure decreases and the film thickness increases; the atomic ratio of Mg/O in MgO thin films (obtained by RBS) increases from 0.97 to 1.17, giving that deposited at 50 A most close to the stoichiometric composition of the bulk MgO; the grains of MgO thin films grow gradually as shown in SEM images. XRD patterns show that MgO (1 1 0) orientation is predominant for films prepared at the arc currents ranged from 50 to 70 A. The MgO (1 0 0) orientation is much enhanced and comparable to that of MgO (1 1 0) for films prepared at the arc current of 80 A. The secondary electron emission coefficient of MgO thin film increases with arc current ranged from 50 to 70 A.

  10. The Effect of Flow Distribution on the Concentration of NO Produced by Pulsed Arc Discharge

    International Nuclear Information System (INIS)

    Hu Hui; Bao Bin; Wang Heli; Liang Haiyan; He Junjia; He Zhenghao; Li Jin

    2007-01-01

    As a new method to cure acute respiratory distress syndrome (ARDS), high blood pressure and some illnesses related to the lung, NO has recently received more attention. Thermal plasmas produced by arc discharge can create medical NO, but the concentration of NO 2 produced by arc discharge must be controlled simultaneously. This paper investigates the characteristics and regulations of NO production at different flow distribution by pulsed arc discharge in dry air with a special pulsed power. The experimental results show that the flow distribution has a considerable effect on the NO concentration, the stabilization of NO. The production of NO 2 could be controlled and the ratio of NO 2 /NO was decreased to about 10% in the arc discharge. Therefore, the arc discharge could produce stable inhaled NO for medical treatment by changing the flow distribution

  11. Copper-Silver Alloy Depositions Using Thermionic Vacuum ARC (TVA)

    International Nuclear Information System (INIS)

    Akan, T.

    2004-01-01

    TVA is a plasma source generating pure metal vapor plasma and consists of a heated cathode emitting thermo electrons and an anode containing material to be evaporated. We used Cu and Ag pieces as anode materials and produced their alloys by electron bombarding. Cu-Ag alloys in various mass ratios were prepared by using the TVA and the TVA discharges were generated in the vapors of these alloys. The volt-ampere characteristics of the TVA discharges generated in the vapors of these alloys were investigated with respect to the ratio of Ag in the Cu-Ag alloy. Cu-Ag alloy thin films with various mass ratios were deposited onto the glass substrates by using their TVA discharges. The ratios of Cu and Ag in the thin Cu-Ag alloy films were found using scanning electron microscope-energy dispersive xray (SEM-EDX) microanalyses

  12. Arc discharge characteristics of molten salts used in an MHD generator

    International Nuclear Information System (INIS)

    Korenaga, Sadayoshi; Mohri, Motoichi.

    1981-01-01

    The seed arc discharge phenomena in an MHD generator were studied. The behavior of arc was observed, which was generated by using K 2 CO 3 and K 2 SO 4 heated up to 1150 degree C as cathodes and a water-cooled copper as an anode. The generated arcs were classified into 3 types, such as free spot arc (point arc), line emission arc (line arc) and plane arc. The estimated temperature of arc foot was lower than the boiling point of seed material. The relation between arc voltage and arc length and that between arc voltage and arc current were measured. From these data, the potential gradient of arc was obtained. The gradients were same for almost all materials of cathode. The potential drop at cathodes depended remarkably on the kinds of molten salt, and also depended on the shapes of cathodes. The evaporation rate of cathode materials was larger when the cathode potential drop was larger and the arc current was larger. (Kato, T.)

  13. Plasma discharge in ferritic first wall vacuum vessel of the Hitachi Tokamak HT-2

    International Nuclear Information System (INIS)

    Abe, Mitsushi; Nakayama, Takeshi; Asano, Katsuhiko; Otsuka, Michio

    1997-01-01

    A tokamak discharge with ferritic material first wall was tried successfully. The Hitachi Tokamak HT-2 had a stainless steel SUS304 vacuum vessel and modified to have a ferritic plate first wall for experiments to investigate the possibility of ferritic material usage in magnetic fusion devices. The achieved vacuum pressure and times used for discharge cleaning was roughly identical with the stainless steel first wall or the original HT-2. We concluded that ferritic material vacuum vessel is possible for tokamaks. (author)

  14. Finite Element Analysis of a 3D Moving Vacuum Arc for Transverse Magnetic Field Contacts Based on Gundlach's Formula

    International Nuclear Information System (INIS)

    Kwak, Chang-Seob; Kim, Hong-Kyu; Kim, Tae-Hoon; Lee, Se-Hee

    2017-01-01

    A systematic numerical method for analyzing a 3D moving vacuum arc was proposed and tested in this research by using a transverse magnetic field (TMF) contact. The analysis was carried out by employing the finite element method and the experimental energy equation defined by Gundlach's formula. In the literature, the vacuum interrupter has been widely applied to medium-voltage switching circuits. TMF-type contacts use the Lorentz force density to move a high-temperature arc so as to prevent the contacts from being melted and damaged. The material erosion caused by the arc on the electrode's surface is an important process that results in the interruptive capabilities of these vacuum interrupters. In a classical arc model, to move the vacuum arc, it is required that the magneto-hydrodynamics be analyzed in the arc region at each step. However, with this approach convergence is difficult, resulting in a very time-consuming. Therefore, we propose a new technique to predict the behaviors of vacuum arc between two electrodes. This new approach adopts the experimental arc voltage equation between two electrodes defined by Gundlach's formula. We verify our proposed model by comparing its results with the arcing behaviors obtained from earlier experiments.

  15. Effect of vacuum arc cathode spot distribution on breaking capacity of the arc-extinguishing chamber

    Science.gov (United States)

    Ding, Can; Yuan, Zhao; He, Junjia

    2017-10-01

    A DC circuit breaker performs a key function in breaking an intermediate-frequency (IF) current since breaking a pure IF current is equivalent to breaking a very small DC with a reverse IF current. In this study, it is found that cathode spots show a ring-shaped distribution at 2000 Hz. An arc with an uneven distribution of cathode spots has been simulated. The simulation results show that the distribution of cathode spots significantly affect the microparameter distribution of arc plasma. The current distribution on the anode side differs from that on the cathode side under the total radial electric field. Specifically, the anode current distribution is both uneven and concentrated. The applied axial magnetic field, which cannot reduce the concentrated anode current distribution effectively, might increase the concentration of the anode current. Finally, the uneven distribution of cathode spots reduces the breaking capacity of the arc-extinguishing chamber.

  16. Interelectrode plasma evolution in a hot refractory anode vacuum arc: Theory and comparison with experiment

    International Nuclear Information System (INIS)

    Beilis, I.I.; Goldsmith, S.; Boxman, R.L.

    2002-01-01

    In this paper a theoretical study of a hot refractory anode vacuum arc, which was previously investigated experimentally [Phys. Plasmas 7, 3068 (2000)], is presented. The arc was sustained between a thermally isolated refractory anode and a water-cooled copper cathode. The arc started as a multicathode-spot (MCS) vacuum arc and then switched to the hot refractory anode vacuum arc (HRAVA) mode. In the MCS mode, the cathodic plasma jet deposits a film of the cathode material on the anode. Simultaneously, the temperature of the thermally isolated anode begins to rise, reaching eventually a sufficiently high temperature to re-evaporate the deposited material, which is subsequently ionized in the interelectrode gap. The transition to the HRAVA mode is completed when the density of the interelectrode plasma consists mostly of ionized re-evaporated atoms--the anode plasma. The evolution of the HRAVA mode is characterized by the propagation of a luminous plasma plume from the anode to the cathode. The time dependent model of the various physical processes taking place during the transition to the HRAVA mode is represented by a system of equations describing atom re-evaporation, atom ionization through the interaction of the cathode jet and the interelectrode plasma with the anode vapor, plasma plume propagation, plasma radial expansion, plasma energy, and heavy particle density balance. The time dependence of the anode heat flux and the effective anode voltage were obtained by solving these equations. In addition, the time dependent plasma electron temperature, plasma density, anode potential drop, arc voltage, and anode temperature distribution were calculated and compared with previous measurements. It was shown that the observed decrease of the effective anode voltage with time during the mode transition is due to decrease of the heat flux incident on the anode surface from the cathode spot jets

  17. Theory of the arc discharge in air blast breakers

    International Nuclear Information System (INIS)

    Vogel, H.F.

    1980-08-01

    The complete set of equations obtaining in the arc's length element are given. The arc length is determined when the external circuit equations are closed by an expression for the arc inductance as a function of the radius and length, in addition to our relationships for the radius and voltage gradients

  18. Theory of the arc discharge in air blast breakers

    Energy Technology Data Exchange (ETDEWEB)

    Vogel, H.F.

    1980-08-01

    The complete set of equations obtaining in the arc's length element are given. The arc length is determined when the external circuit equations are closed by an expression for the arc inductance as a function of the radius and length, in addition to our relationships for the radius and voltage gradients.

  19. Approach to modeling of the fast energy discharge in cryogenic systems in the form of an electric arc

    CERN Multimedia

    CERN. Geneva

    2016-01-01

    Superconducting magnets are supplied with a few kA of electric current and can store a large amount of energy. Therefore, cryogenic systems which are comprised of such magnets are subject to the risk of fast energy discharge from the magnets themselves in the form of an electric arc. The arcing can be a result of failure in the insulation of an electric circuit or in the connection between the magnet and its current lead. During the discharge, energy can be partially dissipated into the cryogen and partially into the cryogenic system metallic structure. The part of the energy that is transferred to the metallic structure will strongly heat up the metal surface, which can lead to material burning. In this case, the cryogen will flow through the perforation to the insulation vacuum space, which can trigger a rapid increase in pressure in the vacuum enclosure. However, the discharged energy that has been stored in the cryogen also causes a rapid increase in cryogenic pressure. Hence, the proper estimation of the...

  20. Preparation of gold ethanol colloid by the arc discharge method

    International Nuclear Information System (INIS)

    Tseng, K.-H.; Huang, J.-C.; Liao, C.-Y.; Tien, D.-C.; Tsung, T.-T.

    2009-01-01

    A new method using the arc discharge method (ADM) to synthesize gold nanoparticles in an anhydrous ethanol was studied. Fabricated gold nanoparticles were characterized by different techniques. Unlike conventional methods for metal nanoparticles synthesis, the ADM method does not require application of chemical surfactants and stabilizers. The microstructure of ADM-produced gold nanoparticles was examined by transmission electron microscope (TEM) and scanning electron microscope (SEM). The particle size was found in the range of 2-40 nm. The chemical composition of gold nanoparticles has been confirmed by the energy dispersive X-ray analysis (EDX). The crystal structure of the nanoscale gold particles was studied using the X-ray diffraction (XRD) method. Images of the gold nanoparticles, Zeta potential, size distribution, and ultraviolet-visible (UV-vis) absorbance were investigated. This innovative approach for gold nanoparticles preparation has been successfully established. The experimental results showed that the ADM technique is easy, cheap and clean method which can be used to manufacture gold nanoparticles suspended in ethanol solution without any surfactant

  1. Sustained diffusive alternating current gliding arc discharge in atmospheric pressure air

    Science.gov (United States)

    Zhu, Jiajian; Gao, Jinlong; Li, Zhongshan; Ehn, Andreas; Aldén, Marcus; Larsson, Anders; Kusano, Yukihiro

    2014-12-01

    Rapid transition from glow discharge to thermal arc has been a common problem in generating stable high-power non-thermal plasmas especially at ambient conditions. A sustained diffusive gliding arc discharge was generated in a large volume in atmospheric pressure air, driven by an alternating current (AC) power source. The plasma column extended beyond the water-cooled stainless steel electrodes and was stabilized by matching the flow speed of the turbulent air jet with the rated output power. Comprehensive investigations were performed using high-speed movies measured over the plasma column, synchronized with simultaneously recorded current and voltage waveforms. Dynamic details of the novel non-equilibrium discharge are revealed, which is characterized by a sinusoidal current waveform with amplitude stabilized at around 200 mA intermediate between thermal arc and glow discharge, shedding light to the governing mechanism of the sustained spark-suppressed AC gliding arc discharge.

  2. A new method for decontamination of radioactive waste using low-pressure arc discharge

    International Nuclear Information System (INIS)

    Fujiwara, Kazutoshi; Furukawa, Shizue; Adachi, Kazuo; Amakawa, Tadashi; Kanbe, Hiromi

    2006-01-01

    In this paper, the decontamination features of the low-pressure arc-discharge method for radioactive waste generated in the operation and maintenance of nuclear power plants were examined. The low-pressure arc-discharge method was applied to type 304 stainless-steel, type 316L stainless-steel, alloy 600 and carbon-steel covered with radioactive corrosion products. Approximately, 80% of the radioactivity build up on stainless-steels could be removed by the low-pressure arc discharge

  3. Steady state behavior of rotating plasmas in a vacuum-arc centrifuge

    International Nuclear Information System (INIS)

    Bittencourt, J.A.; Ludwig, G.O.

    1987-01-01

    The steady state behaviour of the fully ionized, multiple species, rotating, magnetized plasma in a vacuum-arc plasma centrifuge is described in detail. The analysis is based on a multiple species fluid model which includes electromagnetic, pressure gradient, centrifugal and collisional forces, for each species, in cylindrical geometry. It is shown that there is a family of theoretically possible dynamical equilibrium configurations, which can be achieved by different combinations of ion rotation velocity, radial ion density distribution and radial dependence of internal electric potential. The parametric dependences of the various plasma parameters under equilibrium conditions, including the ion separation factor, are presented for a nickel-copper plasma. The numerical results are analysed and discussed in light of experimentally measured plasma characteristics in a vacuum-arc plasma centrifuge. (author)

  4. Steady state behavior of rotating plasmas in a vacuum-arc centrifuge

    International Nuclear Information System (INIS)

    Bittencourt, J.A.; Ludwig, G.O.

    1986-06-01

    The steady state behavior of the fully ionized, multiple species, rotating, magnetized plasma in a vacuum-arc plasma centrifuge is described in detail. The analysis is based on a multiple species fluid model which includes electromagnetic, pressure gradient, centrifugal and collisional forces, for each species, in cylindrical geometry. It is showm that there is a family of theoretically possible dynamical equilibrium configurations, which can be achieved by different combinations of ion rotation velocity, radial ion density distribution and radial dependence of internal electric potential. The parametric dependences of the various plasma parameters under equilibrium conditions, including the ion separation factor, are presented for a nickel-copper plasma. The numerical results are analysed and discussed on light of experimentally measured plasma characteristics in a vacuum-arc plasma centrifuge. (Author) [pt

  5. Optical emission spectra of a copper plasma produced by a metal vapour vacuum arc plasma source

    International Nuclear Information System (INIS)

    Yotsombat, B.; Poolcharuansin, P.; Vilaithong, T.; Davydov, S.; Brown, I.G.

    2001-01-01

    Optical emission spectroscopy in the range 200-800 nm was applied for investigation of the copper plasma produced by a metal vapour vacuum arc plasma source. The experiments were conducted for the cases when the plasma was guided by straight and Ω-shaped curved solenoids as well as without solenoids, and also for different vacuum conditions. It was found that, besides singly- and doubly-charged ions, a relatively high concentration of excited neutral copper atoms was present in the plasma. The relative fraction of excited atoms was much higher in the region close to the cathode surface than in the plasma column inside the solenoid. The concentration of excited neutral, singly- and doubly-ionized atoms increased proportionally when the arc current was increased to 400 A. Some weak lines were attributed to more highly ionized copper species and impurities in the cathode material. (author)

  6. Research of influence of mobile cathodic stains of the vacuum arc for reception of the adjustable roughness of metal surfaces

    Science.gov (United States)

    Anikeev, V. N.; Dokukin, M. Yu

    2017-05-01

    In the modern technics there is a requirement in micro- and macrorough surfaces of products for improvement of their operational characteristics (improvement of adhesive properties of various coverings, decrease in deterioration of rubbing details because of the best deduction of greasing, increase of the heat exchanging coefficient from a surface, stimulation of adhesive processes on sites of contact to a bone fabric of medical implants in stomatology and orthopedy etc.). In the given work the modes of reception regulated micro- and macrorough surfaces on samples from a titanic alloy and stainless steel by electrothermal influence of moving cathodic stains in the vacuum arc discharge are investigated. Chaotically moving stains, possessing high specific power allocation (∼ 107 W/cm2), “scan” the difficult design of a product, including “shadow” sites, doing rough its blanket. The sizes of roughnesses are regulated by a current and time of influence of the discharge, pressure in the vacuum chamber and a number of other parameters. The scheme of experimental device, photo and the characteristic of rough surfaces and technological modes of their reception are resulted.

  7. Self-Similar Vacuums Arc Plasma Cloud Expansion

    International Nuclear Information System (INIS)

    Gidalevich, E.; Goldsmith, S.; Boxman, R.L.

    1999-01-01

    A spherical plasma cloud generated by a vacuum are, is considered as expanding in an ambient neutral gas in a self-similar approximation. Under the assumption that the cathode erosion rate as well as density of the ambient neutral gas are constant during the plasma expansion, the self-similarity parameter is A = (1/ρ 3 dM/dt) 1/3 where ρ 3 is the density of undisturbed gas, M is the mass of the expanding metal vapor, and t is time, while the dimensionless independent variable is ξ = r/At 1/3 , where r is the distance from the cloud center. The equations of plasma motion and continuity are: ∂v/∂t + ∂n/∂r +1∂p/ρ∂r = 0 ∂ρ/∂t + ∂ρ/∂r + ρ(∂v/∂r + 2v/r) = 0 where v, ρ, P are plasma velocity, density and pressure, transformed in the self-similar form and solved numerically. Boundary conditions were formulated on the front of the plasma expansion taking into account that 1) the front edge of the shock wave expanding in the ambient neutral gas and 2) the rate of cathode erosion is a constant. For an erosion rate of 104 g/C, a cathode ion current of about 20 A and an ambient gas pressure about 0.1 Torr, the radius of the plasma cloud is r (m) = 0.834 x t 1/3 . At t = 10 -5 s, the plasma cloud radius is about 0.018 m, while the front velocity is v f = 600 m/s

  8. Method of triggering the vacuum arc in source with a resistor

    International Nuclear Information System (INIS)

    Zheng Le; Lan Zhaohui; Long Jidong; Peng Yufei; Li Jie; Yang Zhen; Dong Pan; Shi Jinshui

    2014-01-01

    Background: The metal vapor vacuum arc (MEVVA) ion source is a common source which provides strong metal ion flow. To trigger this ion source, a high-voltage trigger pulse generator and a high-voltage isolation pulse transformer are needed, which makes the power supply system complex. Purpose: To simplify the power supply system, a trigger method with a resistor was introduced, and some characteristics of this method were studied. Methods: The ion flow provided by different main arc current was measured, as well as the trigger current. The main arc current and the ion current were recorded with different trigger resistances. Results: Experimental results showed that, within a certain range of resistances, the larger the resistance value, the more difficult it was to success fully trigger the source. Meanwhile, the main arc rising edge became slower on the increasing in the trigger time. However, the resistance value increment had hardly impact on the intensity of ion flow extracted in the end, The ion flow became stronger with the increasing main arc current. Conclusion: The power supply system of ion source is simplified by using the trigger method with a resistor. Only a suitable resistor was needed to complete the conversion process from trigger to arc initiating. (authors)

  9. Vacuum Arc Melting Processes for Biomedical Ni-Ti Shape Memory Alloy

    OpenAIRE

    Tsai De-Chang; Chiang Chen-Hsueh

    2015-01-01

    This study primarily involved using a vacuum arc remelting (VAR) process to prepare a nitinol shape-memory alloy with distinct ratios of alloy components (nitinol: 54.5 wt% to 57 wt%). An advantage of using the VAR process is the adoption of a water-cooled copper crucible, which effectively prevents crucible pollution and impurity infiltration. Optimising the melting production process enables control of the alloy component and facilitates a uniformly mixed compound during subsequent processi...

  10. Spatiotemporally resolved characteristics of a gliding arc discharge in a turbulent air flow at atmospheric pressure

    DEFF Research Database (Denmark)

    Zhu, Jiajian; Gao, Jinlong; Ehn, Andreas

    2017-01-01

    A gliding arc discharge was generated in a turbulent air flow at atmospheric pressure driven by a 35 kHz alternating current (AC) electric power. The spatiotemporally resolved characteristics of the gliding arc discharge, including glow-type discharges, spark-type discharges, short-cutting events...... and transitions among the different types of discharges, were investigated using simultaneously optical and electrical diagnostics. The glow-type discharge shows sinusoidal-like voltage and current waveforms with a peak current of hundreds of milliamperes. The frequency of the emission intensity variation...... of the glow-type discharge is the same as that of the electronic power dissipated in the plasma column. The glow-type discharge can transfer into a spark discharge characterized by a sharp peak current of several amperes and a sudden increase of the brightness in the plasma column. Transitions can also...

  11. Effect of annealing process on TiN/TiC bilayers grown by pulsed arc discharge

    International Nuclear Information System (INIS)

    Ramos-Rivera, L.; Escobar, D.; Benavides-Palacios, V.; Arango, P.J.; Restrepo-Parra, E.

    2012-01-01

    In this work, a study of annealing process effect on TiN/TiC bilayer is presented. The annealing temperature was varied between room temperature and 500 °C. Materials were produced by the plasma-assisted pulsed vacuum arc discharge technique. In order to grow the films, a target of Ti with 99.9999% purity and stainless-steel 304 substrate were used. For the production of TiN layer, the reaction chamber was filled up with nitrogen gas until reaching 25 Pa and the discharge was performed at 310 V. The TiC layer was grown in a methane atmosphere at 30 Pa and 270 V. X-ray diffraction and X photoelectron spectroscopy were employed for studying the structure and chemical composition evolution during the annealing process. At 400 °C, TiO 2 phase begun to appear and it was well observed at 500 °C. Crystallite size and microstrain was obtained as a function of the annealing temperature. XPS technique was employed for analyzing the bilayers before and after the annealing process. Narrow spectra of Ti2p, N1s and O1s were obtained, presenting TiO phases.

  12. Electric field induced needle-pulsed arc discharge carbon nanotube production apparatus: Circuitry and mechanical design

    Energy Technology Data Exchange (ETDEWEB)

    Kia, Kaveh Kazemi [Department of Electrical and Computer Engineering, Islamic Azad University of Bonab, Bonab (Iran, Islamic Republic of); Bonabi, Fahimeh [Department of Engineering, Islamic Azad University of Bonab, Bonab (Iran, Islamic Republic of)

    2012-12-15

    A simple and low cost apparatus is reported to produce multiwall carbon nanotubes and carbon nano-onions by a low power short pulsed arc discharge reactor. The electric circuitry and the mechanical design details and a micro-filtering assembly are described. The pulsed-plasma is generated and applied between two graphite electrodes. The pulse width is 0.3 {mu}s. A strong dc electric field is established along side the electrodes. The repetitive discharges occur in less than 1 mm distance between a sharp tip graphite rod as anode, and a tubular graphite as cathode. A hydrocarbon vapor, as carbon source, is introduced through the graphite nozzle in the cathode assembly. The pressure of the chamber is controlled by a vacuum pump. A magnetic field, perpendicular to the plasma path, is provided. The results show that the synergetic use of a pulsed-current and a dc power supply enables us to synthesize carbon nanoparticles with short pulsed plasma. The simplicity and inexpensiveness of this plan is noticeable. Pulsed nature of plasma provides some extra degrees of freedom that make the production more controllable. Effects of some design parameters such as electric field, pulse frequency, and cathode shape are discussed. The products are examined using scanning probe microscopy techniques.

  13. Electric field induced needle-pulsed arc discharge carbon nanotube production apparatus: circuitry and mechanical design.

    Science.gov (United States)

    Kia, Kaveh Kazemi; Bonabi, Fahimeh

    2012-12-01

    A simple and low cost apparatus is reported to produce multiwall carbon nanotubes and carbon nano-onions by a low power short pulsed arc discharge reactor. The electric circuitry and the mechanical design details and a micro-filtering assembly are described. The pulsed-plasma is generated and applied between two graphite electrodes. The pulse width is 0.3 μs. A strong dc electric field is established along side the electrodes. The repetitive discharges occur in less than 1 mm distance between a sharp tip graphite rod as anode, and a tubular graphite as cathode. A hydrocarbon vapor, as carbon source, is introduced through the graphite nozzle in the cathode assembly. The pressure of the chamber is controlled by a vacuum pump. A magnetic field, perpendicular to the plasma path, is provided. The results show that the synergetic use of a pulsed-current and a dc power supply enables us to synthesize carbon nanoparticles with short pulsed plasma. The simplicity and inexpensiveness of this plan is noticeable. Pulsed nature of plasma provides some extra degrees of freedom that make the production more controllable. Effects of some design parameters such as electric field, pulse frequency, and cathode shape are discussed. The products are examined using scanning probe microscopy techniques.

  14. Investigation of carbon cathode surface before and after the passage of combined dc vacuum arc with superimposed high-current arc pulses

    International Nuclear Information System (INIS)

    Zavaleyev, V.; Walkowicz, J.; Moszynski, D.

    2016-01-01

    The paper presents the results of studies of carbon cathode surface before and after the passage of the combined DC vacuum-arc with superimposed high-current arc pulses. Investigations of surface morphology of carbon cathode showed, that secondary nuclei of high-density are formed after passing of the combined DC-pulse vacuum-arc, which results in the formation of a globular structures. The phase structure analysis by Raman spectroscopy showed that even at a minimum operation time (5 s) of the combined DC-pulse vacuum-arc broadening of the peaks 1355 and 1583 cm-1 occurs, which means that the carbon cathode surface undergo phase transformation. Results obtained by XPS spectroscopy demonstrate that the globular structures formed on the cathode surface are composed of sp 3 -bonded carbon atoms and carbon-oxygen bonds.

  15. Modification of anti-bacterial surface properties of textile polymers by vacuum arc ion source implantation

    International Nuclear Information System (INIS)

    Nikolaev, A.G.; Yushkov, G.Yu.; Oks, E.M.; Oztarhan, A.; Akpek, A.; Hames-Kocabas, E.; Urkac, E.S.; Brown, I.G.

    2014-01-01

    Highlights: • Ion implantation. • Anti-bacterial properties. • Textile polymer. • Vacuum arc ion source. - Abstract: Ion implantation provides an important technology for the modification of material surface properties. The vacuum arc ion source is a unique instrument for the generation of intense beams of metal ions as well as gaseous ions, including mixed metal–gas beams with controllable metal:gas ion ratio. Here we describe our exploratory work on the application of vacuum arc ion source-generated ion beams for ion implantation into polymer textile materials for modification of their biological cell compatibility surface properties. We have investigated two specific aspects of cell compatibility: (i) enhancement of the antibacterial characteristics (we chose to use Staphylococcus aureus bacteria) of ion implanted polymer textile fabric, and (ii) the “inverse” concern of enhancement of neural cell growth rate (we chose Rat B-35 neuroblastoma cells) on ion implanted polymer textile. The results of both investigations were positive, with implantation-generated antibacterial efficiency factor up to about 90%, fully comparable to alternative conventional (non-implantation) approaches and with some potentially important advantages over the conventional approach; and with enhancement of neural cell growth rate of up to a factor of 3.5 when grown on suitably implanted polymer textile material

  16. Modification of anti-bacterial surface properties of textile polymers by vacuum arc ion source implantation

    Energy Technology Data Exchange (ETDEWEB)

    Nikolaev, A.G., E-mail: nik@opee.hcei.tsc.ru [High Current Electronics Institute, Siberian Branch of the Russian Academy of Sciences, Tomsk 634055 (Russian Federation); Yushkov, G.Yu.; Oks, E.M. [High Current Electronics Institute, Siberian Branch of the Russian Academy of Sciences, Tomsk 634055 (Russian Federation); Oztarhan, A. [Izmir University, Izmir 35140 (Turkey); Akpek, A.; Hames-Kocabas, E.; Urkac, E.S. [Bioengineering Department, Ege University, Bornova 35100, Izmir (Turkey); Brown, I.G. [Lawrence Berkeley National Laboratory, Berkeley, CA 94708 (United States)

    2014-08-15

    Highlights: • Ion implantation. • Anti-bacterial properties. • Textile polymer. • Vacuum arc ion source. - Abstract: Ion implantation provides an important technology for the modification of material surface properties. The vacuum arc ion source is a unique instrument for the generation of intense beams of metal ions as well as gaseous ions, including mixed metal–gas beams with controllable metal:gas ion ratio. Here we describe our exploratory work on the application of vacuum arc ion source-generated ion beams for ion implantation into polymer textile materials for modification of their biological cell compatibility surface properties. We have investigated two specific aspects of cell compatibility: (i) enhancement of the antibacterial characteristics (we chose to use Staphylococcus aureus bacteria) of ion implanted polymer textile fabric, and (ii) the “inverse” concern of enhancement of neural cell growth rate (we chose Rat B-35 neuroblastoma cells) on ion implanted polymer textile. The results of both investigations were positive, with implantation-generated antibacterial efficiency factor up to about 90%, fully comparable to alternative conventional (non-implantation) approaches and with some potentially important advantages over the conventional approach; and with enhancement of neural cell growth rate of up to a factor of 3.5 when grown on suitably implanted polymer textile material.

  17. Recent advances in high current vacuum arc ion sources for heavy ion fusion

    CERN Document Server

    Qi Nian Sheng; Prasad, R R; Krishnan, M S; Anders, A; Kwan, J; Brown, I

    2001-01-01

    For a heavy ion fusion induction linac driver, a source of heavy ions with charge states 1+-3+, approx 0.5 A current beams, approx 20 mu s pulse widths and approx 10 Hz repetition rates is required. Thermionic sources have been the workhorse for the Heavy Ion Fusion (HIF) program to date, but suffer from heating problems for large areas and contamination. They are limited to low (contact) ionization potential elements and offer relatively low ion fluxes with a charge state limited to 1+. Gas injection sources suffer from partial ionization and deleterious neutral gas effects. The above shortcomings of the thermionic ion sources can be overcome by a vacuum arc ion source. The vacuum arc ion source is a good candidate for HIF applications. It is capable of providing ions of various elements and different charge states in short and long pulse bursts and high beam current density. Under a Phase-I STTR from DOE, the feasibility of the vacuum arc ion source for the HIF applications was investigated. We have modifie...

  18. Protective coating of inner surface of steel tubes via vacuum arc deposition

    Energy Technology Data Exchange (ETDEWEB)

    Maile, K.; Roos, E.; Lyutovich, A.; Boese, J.; Itskov, M. [Stuttgart Univ. (DE). Materialpruefungsanstalt (MPA); Ashurov, Kh.; Mirkarimov, A.; Kazantsev, S.; Kadirov, Kh. [Uzbek Academy of Science, Tashkent (Uzbekistan). Arifov Inst. of Electronics

    2010-07-01

    The Vacuum Arc Deposition (VAD) technique based on sputtering a chosen electrode material and its deposition via plasma allows highly-productive technology for creating a wide class of protecting coatings on complex structures. In this work, VAD was applied as a method for the protection of the inner surface of tubes for power-plant boilers against steam oxidation. For this aim, a source cathode of an alloy with high chromium and nickel content was employed in two different VAD treatment systems: a horizontal vacuum chamber (MPA) and a vertical system where the work-piece of the tubes to be protected served as a vacuum changer (Arifov Institute of Electronics). Surface coating with variation of deposition parameters and layer thickness was performed. Characterisation of coated tubes has shown that the method realised in this work allows attainment of material transfer from the cathode to the inner surface with nearly equal chemical composition. It was demonstrated that the initial martensitic structure of the tubes was kept after the vacuum-arc treatment which can provide for both the high mechanical robustness and the corrosion-resistance of the final material. (orig.)

  19. Translational, rotational, vibrational and electron temperatures of a gliding arc discharge

    DEFF Research Database (Denmark)

    Zhu, Jiajian; Ehn, Andreas; Gao, Jinlong

    2017-01-01

    , 0) band was used to simulate the rotational temperature (Tr) of the gliding arc discharge whereas the NO A–X (1, 0) and (0, 1) bands were used to determine its vibrational temperature (Tv). The instantaneous reduced electric field strength E/N was obtained by simultaneously measuring......Translational, rotational, vibrational and electron temperatures of a gliding arc discharge in atmospheric pressure air were experimentally investigated using in situ, non-intrusive optical diagnostic techniques. The gliding arc discharge was driven by a 35 kHz alternating current (AC) power source...... and operated in a glow-type regime. The two-dimensional distribution of the translational temperature (Tt) of the gliding arc discharge was determined using planar laser-induced Rayleigh scattering. The rotational and vibrational temperatures were obtained by simulating the experimental spectra. The OH A–X (0...

  20. Modeling of the anode surface deformation in high-current vacuum arcs with AMF contacts

    International Nuclear Information System (INIS)

    Huang, Xiaolong; Wang, Lijun; Deng, Jie; Jia, Shenli; Qin, Kang; Shi, Zongqian

    2016-01-01

    A high-current vacuum arc subjected to an axial magnetic field is maintained in a diffuse status. With an increase in arc current, the energy carried by the arc column to the anode becomes larger and finally leads to the anode temperature exceeding the melting point of the anode material. When the anode melting pool is formed, and the rotational plasma of the arc column delivers its momentum to the melting pool, the anode melting pool starts to rotate and also flow outwards along the radial direction, which has been photographed by some researchers using high-speed cameras. In this paper, the anode temperature and melting status is calculated using the melting and solidification model. The swirl flow of the anode melting pool and deformation of the anode is calculated using the magneto-hydrodynamic (MHD) model with the volume of fraction (VOF) method. All the models are transient 2D axial-rotational symmetric models. The influence of the impaction force of the arc plasma, electromagnetic force, viscosity force, and surface tension of the liquid metal are all considered in the model. The heat flux density injected into the anode and the arc pressure are obtained from the 3D numerical simulation of the high-current vacuum arc using the MHD model, which gives more realistic parameters for the anode simulation. Simulation results show that the depth of the anode melting pool increases with an increase in the arc current. Some droplets sputter out from the anode surface, which is caused by the inertial centrifugal force of the rotational melting pool and strong plasma pressure. Compared with the previous anode melting model without consideration of anode deformation, when the deformation and swirl flow of the anode melting pool are considered, the anode temperature is relatively lower, and just a little more than the melting point of Cu. This is because of liquid droplets sputtering out of the anode surface taking much of the energy away from the anode surface. The

  1. Adhesion improvement of glass-fibre-reinforced polyester composites by gliding arc discharge treatment

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Sørensen, Bent F.; Løgstrup Andersen, Tom

    2013-01-01

    A gliding arc is a plasma that can be operated at atmospheric pressure and applied for plasma surface treatment for adhesion improvement. In the present work, glass-fibre-reinforced polyester plates were treated using an atmospheric pressure gliding arc discharge with an air flow to improve...

  2. Experimental study of unipolar arcs in a low pressure mercury discharge

    International Nuclear Information System (INIS)

    Johnson, C.T.

    1979-01-01

    An experimental study of unipolar arcs was conducted in a low pressure mercury discharge inductively heated with RF. The results were found to be consistent with the concept of a sheath mechanism for driving the unipolar arcs. Floating double-probe measurements of the unipolar arc plasma parameters yielded electron temperatures of approx. 2 eV and electron number densities of approx. 1 x 10 11 cm -3 assuming quasi-neutral plasma conditions. The variation of the unipolar arc current with: (1) the RF power input; and (2) the metal surface area exposed to the plasma verified the predicted dependence of the arc current on the plasma parameters and the metal surface area. Finally, alternative mechanisms for sustaining the observed arcs by high frequency rectification were ruled out on the basis of the recorded current waveforms of the unipolar arcs

  3. Enhanced ablation of small anodes in a carbon nanotube arc discharge

    Science.gov (United States)

    Raitses, Yevgeny; Fetterman, Abraham; Keidar, Michael

    2008-11-01

    An atmospheric pressure helium arc discharge is used for carbon nanotube synthesis. The arc discharge operates in an anodic mode with the ablating anode made from a graphite material. For such conditions, models predict the electron-repelling (negative) anode sheath. In the present experiments, the anode ablation rate is investigated as a function of the anode diameter. It is found that anomalously high ablation occurs for small anode diameters (Fetterman, Y. Raitses and M. Keidar, Carbon (2008).

  4. Identification by force modulation microscopy of nanoparticles generated in vacuum arcs Identification by force modulation microscopy of nanoparticles generated in vacuum arcs

    Directory of Open Access Journals (Sweden)

    M. Arroyave Franco

    2006-06-01

    Full Text Available An alternative method based on force modulation microscopy (FMM for identification of nanoparticles produced in the plasma generated by the cathode spots of vacuum arcs is presented. FMM technique is enabled for the detection of variations in the mechanical properties of a surface with high sensitiveness. Titanium nitride (TiN coatings deposited on oriented silicon by pulsed vacuum arc process have been analyzed. AFM (Atomic Force Microscopy and FMM images were simultaneously obtained, and in all cases it was possible to identify nanoparticle presence. Further X-ray Diffraction spectra of sample coating were taken. Existence of contaminant particles of 47 nanometers in diameter was reported.En este trabajo se presenta un método alternativo basado en microscopia de modulación de fuerza (FMM, para la identificación de nanogotas producidas en el plasma generado por los spots catódicos de los arcos en vacío. La técnica FMM esta habilitada para la detección de variaciones en las propiedades mecánicas de una superficie, con alta sensibilidad. Se han analizado recubrimientos de nitruro de titanio (TiN depositados sobre Silicio orientado por el proceso de arco en vacío pulsado. Se han obtenido simultáneamente imágenes de microscopia de fuerza atómica (AFM y de microscopia FMM mediante las cuales se ha podido identificar la presencia de nanogotas. Adicionalmente se han tomado espectros de difracción de rayos X (XRD de las muestras recubiertas. Se ha reportado la existencia de partículas contaminantes de 47 nanómetros de diámetro sobre los recubrimientos.

  5. Study on a negative hydrogen ion source with hot cathode arc discharge.

    Science.gov (United States)

    Lin, S H; Fang, X; Zhang, H J; Qian, C; Ma, B H; Wang, H; Li, X X; Zhang, X Z; Sun, L T; Zhang, Z M; Yuan, P; Zhao, H W

    2014-02-01

    A negative hydrogen (H(-)) ion source with hot cathode arc discharge was designed and fabricated as a primary injector for a 10 MeV PET cyclotron at IMP. 1 mA dc H(-) beam with ɛ N, RMS = 0.08 π mm mrad was extracted at 25 kV. Halbach hexapole was adopted to confine the plasma. The state of arc discharge, the parameters including filament current, arc current, gas pressure, plasma electrode bias, and the ratio of I(e(-))/I(H(-)) were experimentally studied. The discussion on the result, and opinions to improve the source were given.

  6. Multiwalled Carbon Nanotube Synthesis Using Arc Discharge with Hydrocarbon as Feedstock

    Directory of Open Access Journals (Sweden)

    K. T. Chaudhary

    2013-01-01

    Full Text Available Synthesis of multiwalled carbon nanotube (MWCNT by arc discharge process is investigated with methane (CH4 as background and feedstock gas. The arc discharge is carried out between two graphite electrodes for ambient pressures 100, 300, and 500 torr and arc currents 50, 70, and 90 A. Plasma kinetics such as the density and temperature for arc discharge carbon plasma is determined to find out the contribution of physical parameters as arc current and ambient pressure on the plasma dynamics and growth of MWCNT. With increase in applied arc current and ambient pressure, an increase in plasma temperature and density is observed. The synthesized samples of MWCNT at different experimental conditions are characterized by transmission electron microscopy, scanning electron microscopy, Raman spectroscopy, Fourier transform infrared spectroscopy, and X-ray diffraction. A decrease in the diameter and improvement in structure quality and growth of MWCNT are observed with increase in CH4 ambient pressure and arc current. For CH4 ambient pressure 500 torr and arc current 90 A, the well-aligned and straight MWCNT along with graphene stakes are detected.

  7. Double-ended metal halide arc discharge lamp with electrically isolated containment shroud

    Science.gov (United States)

    Muzeroll, Martin M. (Inventor)

    1994-01-01

    A double-ended arc discharge lamp includes a sealed, light-transmissive outer jacket, a light-transmissive shroud mounted within the outer jacket and directly supported by the outer jacket, and an arc discharge tube mounted within the shroud. The arc tube is typically a metal halide arc discharge tube. In a preferred embodiment, the shroud includes an outwardly flared portion at each end. The outwardly flared portions space the shroud from the outer jacket and support the shroud within the outer jacket. The outwardly flared portions of the shroud can be affixed to the outer jacket by fusing. The outer jacket can be provided with inwardly extending dimples for locating the shroud with respect to the outer jacket. In another embodiment, the outer jacket includes reduced diameter portions near each end which are attached to the shroud.

  8. Stable synthesis of few-layered boron nitride nanotubes by anodic arc discharge.

    Science.gov (United States)

    Yeh, Yao-Wen; Raitses, Yevgeny; Koel, Bruce E; Yao, Nan

    2017-06-08

    Boron nitride nanotubes (BNNTs) were successfully synthesized by a dc arc discharge using a boron-rich anode as synthesis feedstock in a nitrogen gas environment at near atmospheric pressure. The synthesis was achieved independent of the cathode material suggesting that under such conditions the arc operates in so-called anodic mode with the anode material being consumed by evaporation due to the arc heating. To sustain the arc current by thermionic electron emission, the cathode has to be at sufficiently high temperature, which for a typical arc current density of ~100 A/cm 2 , is above the boron melting point (2350 K). With both electrodes made from the same boron-rich alloy, we found that the arc operation unstable due to frequent sticking between two molten electrodes and formation of molten droplets. Stable and reliable arc operation and arc synthesis were achieved with the boron-rich anode and the cathode made from a refractory metal which has a melting temperature above the melting point of boron. Ex-situ characterization of synthesized BNNTs with electron microscopy and Raman spectroscopy revealed that independent of the cathode material, the tubes are primarily single and double walled. The results also show evidence of root-growth of BNNTs produced in the arc discharge.

  9. On the square arc voltage waveform model in magnetic discharge lamp studies

    OpenAIRE

    Molina, Julio; Sainz Sapera, Luis; Mesas García, Juan José

    2011-01-01

    The current number of magnetic and electronic ballast discharge lamps in power distribution systems is increasing because they perform better than incandescent lamps. This paper studies the magnetic discharge lamp modeling. In particular, the arc voltage waveform is analyzed and the limitations of the square waveform model are revealed from experimental measurements.

  10. Vacuum arc cathode spot motion in oblique magnetic fields: An interpretation of the Robson experiment

    Energy Technology Data Exchange (ETDEWEB)

    Beilis, I. I. [Electrical Discharge and Plasma Laboratory, School of Electrical Engineering, Fleischman Faculty of Engineering, Tel Aviv University, P.O.B. 39040, Tel Aviv 69978 (Israel)

    2016-09-15

    A model was developed of vacuum arc cathode spot motion in a magnetic field that obliquely intercepts the cathode surface. The model takes into account a force under an electric field caused by retrograde spot motion across the normal component of the magnetic field, producing a drift velocity component in the direction of the acute angle between the magnetic field and the cathode surface. The relationship between velocity of the retrograde direction and drift velocity of the cathode spot motion to the acute angle was developed. The dependencies of the drift angle θ on the acute angle φ, magnetic field strength B, and arc current I were calculated. It was found that the calculated θ increased with φ, B, and I in accordance with Robson's measurements.

  11. High charge state metal ion production in vacuum arc ion sources

    International Nuclear Information System (INIS)

    Brown, I.G.; Anders, A.; Anders, S.

    1994-01-01

    The vacuum arc is a rich source of highly ionized metal plasma that can be used to make a high current metal ion source. Vacuum arc ion sources have been developed for a range of applications including ion implantation for materials surface modification, particle accelerator injection for fundamental nuclear physics research, and other fundamental and applied purposes. Typically the source is repetitively pulsed with pulse length of order a millisecond and duty cycle or order 1% and operation of a dc embodiment has been demonstrated also. Beams have been produced from over 50 of the solid metals of the periodic table, with mean ion energy up to several hundred keV and with peak (pulsed) beam current up to several amperes. The ion charge state distribution has been extensively studied. Ion spectra have been measured for a wide range of metallic cathode materials, including Li, C, Mg, Al, Si, Ca, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ge, Sr, Y, Zr, Nb, Mo, Pd, Ag, Cd, In, Sn, Sb, Ba, La, Ce, Pr, Nd, Sm, Gd, Dy, Ho, Er, Tm, Yb, Hf, Ta, W, Ir, Pt, Au, Pb, Bi, Th and U, as well as compound and alloy cathode materials such as TiC, SiC, UC, PbS, brass, and stainless steel. The ions generated are in general multiply-stripped with a mean charge state of from 1 to 3, depending on the particular metal species, and the charge state distribution can have components from Q = 1+ to 6+. Here the authors review the characteristics of vacuum arc ion sources from the perspective of their high charge state metal ion production

  12. The vacuum-arc plasma motion in a toroidal magnetic field

    International Nuclear Information System (INIS)

    Timoshenko, A.I.; Gnybida, M.V.; Taran, V.S.; Tereshin, V.I.; Chechelnitskij, O.G.

    2005-01-01

    The separation of the vacuum-arc plasma from macro-particles in the curvilinear plasma filters allows obtaining coatings with especially high characteristics. However, inside such filters the significant plasma losses also have been occurred. At the same time, increasing in the filter's efficiency is a difficult task without an effective mathematical model that really would describe the vacuum-arc plasma motion in a toroidal magnetic field. The description based on the flax-tube model was in fact only the first approximation in the decision of this problem. According to detailed flax-tube analysis of ions passage through the quarter torus plasma guide, the efficiency of the filter should grow up to 85% as the positive potential U, applied to the body of the plasma guide, is on the increase. However, the experiment showed that maximum of transparency reach up to ∼ 12%, at potential about of +18 Volts, and comes down under the further increase in potential. Such big digression from experiment does not justify the use of flux-tube model for designing of curvilinear plasma filters. We offer the new approach to the description of the vacuum-arc plasma motion in a toroidal magnetic field based on the solutions of steady-state (∂/∂t=0) Vlasov-Maxwell equations for the long plasma column aligned parallel to a constant axial magnetic field. The relations for the self-consistent electric polarization fields, which appear due to displacement of the electron component from ionic one on the curvilinear part of motion, were derived within a framework of the drift approximation. The dynamics of the central part of the plasma flow in the electric polarization fields was considered in detail. The displacement of the plasma flow at the output of the plasma guide was calculated for the carbon and titanium plasmas. The good agreement with the experimental data was obtained. (author)

  13. Arc dynamics of a pulsed DC nitrogen rotating gliding arc discharge

    Science.gov (United States)

    Zhu, Fengsen; Zhang, Hao; Li, Xiaodong; Wu, Angjian; Yan, Jianhua; Ni, Mingjiang; Tu, Xin

    2018-03-01

    In this study, a novel pulsed direct current (DC) rotating gliding arc (RGA) plasma reactor co-driven by an external magnetic field and a tangential gas flow has been developed. The dynamic characteristics of the rotating gliding arc have been investigated by means of numerical simulation and experiment. The simulation results show that a highly turbulent vortex flow can be generated at the bottom of the RGA reactor to accelerate the arc rotation after arc ignition, whereas the magnitude of gas velocity declined significantly along the axial direction of the RGA reactor. The calculated arc rotation frequency (14.4 Hz) is reasonably close to the experimental result (18.5 Hz) at a gas flow rate of 10 l min-1. In the presence of an external magnet, the arc rotation frequency is around five times higher than that of the RGA reactor without using a magnet, which suggests that the external magnetic field plays a dominant role in the maintenance of the arc rotation in the upper zone of the RGA reactor. In addition, when the magnet is placed outside the reactor reversely to form a reverse external magnetic field, the arc can be stabilized at a fixed position in the inner wall of the outer electrode at a critical gas flow rate of 16 l min-1.

  14. Vacuum Arc Melting Processes for Biomedical Ni-Ti Shape Memory Alloy

    Directory of Open Access Journals (Sweden)

    Tsai De-Chang

    2015-01-01

    Full Text Available This study primarily involved using a vacuum arc remelting (VAR process to prepare a nitinol shape-memory alloy with distinct ratios of alloy components (nitinol: 54.5 wt% to 57 wt%. An advantage of using the VAR process is the adoption of a water-cooled copper crucible, which effectively prevents crucible pollution and impurity infiltration. Optimising the melting production process enables control of the alloy component and facilitates a uniformly mixed compound during subsequent processing. This study involved purifying nickel and titanium and examining the characteristics of nitinol alloy after alloy melt, including its microstructure, mechanical properties, phase transition temperature, and chemical components.

  15. Investigation of the crystallization process of titanium alloy ingots produced by vacuum arc melting method

    International Nuclear Information System (INIS)

    Tetyukhin, V.V.; Kurapov, V.N.; Trubin, A.N.; Demchenko, M.V.; Lazarev, V.G.; Ponedilko, S.V.; Dubrovina, N.T.; Kurapova, L.A.

    1978-01-01

    The process of crystallization and hardening of the VT3-1 and VT9 titanium alloys ingots during the vacuum-arc remelting (VAR) has been studied. In order to investigate the kinetics of the hole shape changing and the peculiarities of the ingot formation during the VAR, the radiography method has been used. It is established that the VAR of the titanium alloy ingots is basically a continuous process. An intense heating of the liquid bath mirror and the availability of high temperature gradients in the hole are the typical features of the VAR process

  16. Contamination due to memory effects in filtered vacuum arc plasma deposition systems

    CERN Document Server

    Martins, D R; Verdonck, P; Brown, I G

    2002-01-01

    Thin film synthesis by filtered vacuum arc plasma deposition is a widely used technique with a number of important emerging technological applications. A characteristic feature of the method is that during the deposition process not only is the substrate coated by the plasma, but the plasma gun itself and the magnetic field coil and/or vacuum vessel section constituting the macroparticle filter are also coated to some extent. If then the plasma gun cathode is changed to a new element, there can be a contamination of the subsequent film deposition by sputtering from various parts of the system of the previous coating species. We have experimentally explored this effect and compared our results with theoretical estimates of sputtering from the SRIM (Stopping and Range of Ions in Matter) code. We find film contamination of order 10-4 - 10-3, and the memory of the prior history of the deposition hardware can be relatively long-lasting.

  17. Contamination due to memory effects in filtered vacuum arc plasma deposition systems

    International Nuclear Information System (INIS)

    Martins, D.R.; Salvadori, M.C.; Verdonck, P.; Brown, I.G.

    2002-01-01

    Thin film synthesis by filtered vacuum arc plasma deposition is a widely used technique with a number of important emerging technological applications. A characteristic feature of the method is that during the deposition process not only is the substrate coated by the plasma, but the plasma gun itself and the magnetic field coil and/or vacuum vessel section constituting the macroparticle filter are also coated to some extent. If then the plasma gun cathode is changed to a new element, there can be a contamination of the subsequent film deposition by sputtering from various parts of the system of the previous coating species. We have experimentally explored this effect and compared our results with theoretical estimates of sputtering from the stopping and range of ions in matter code. We find film contamination of the order of 10 -4 -10 -3 , and the memory of the prior history of the deposition hardware can be relatively long lasting

  18. Contamination due to memory effects in filtered vacuum arc plasma deposition systems

    Energy Technology Data Exchange (ETDEWEB)

    Martins, D.R.; Salvadori, M.C.; Verdonck, P.; Brown, I.G.

    2002-08-13

    Thin film synthesis by filtered vacuum arc plasma deposition is a widely used technique with a number of important emerging technological applications. A characteristic feature of the method is that during the deposition process not only is the substrate coated by the plasma, but the plasma gun itself and the magnetic field coil and/or vacuum vessel section constituting the macroparticle filter are also coated to some extent. If then the plasma gun cathode is changed to a new element, there can be a contamination of the subsequent film deposition by sputtering from various parts of the system of the previous coating species. We have experimentally explored this effect and compared our results with theoretical estimates of sputtering from the SRIM (Stopping and Range of Ions in Matter) code. We find film contamination of order 10-4 - 10-3, and the memory of the prior history of the deposition hardware can be relatively long-lasting.

  19. Various Characteristics of Electromagnetic Contactor when Arc Discharge are Generated only Make Arc(Researches and Overseas Activities)--(Reports of Overseas Activities)

    OpenAIRE

    Kiyoshi, Yoshida

    2017-01-01

    Experiments are carried out to clarify the influence on the current and voltage for various characteristics.A small electromagnetic contactor that has two contacts is used.The arc discharge with only a make arc is generated and various characteristics are measured.Source voltage is set to 100V DC, closed contacts currents are changed from 10A 20A and 30A.From the waveforms, the arc duration time and the bounce time are read out.Arc energy is calculated from the arc voltage and arc current.The...

  20. Sheath and arc-column voltages in high-pressure arc discharges

    International Nuclear Information System (INIS)

    Benilov, M S; Benilova, L G; Li Heping; Wu Guiqing

    2012-01-01

    Electrical characteristics of a 1 cm-long free-burning atmospheric-pressure argon arc are calculated by means of a model taking into account the existence of a near-cathode space-charge sheath and the discrepancy between the electron and heavy-particle temperatures in the arc column. The computed arc voltage exhibits a variation with the arc current I similar to the one revealed by the experiment and exceeds experimental values by no more than approximately 2 V in the current range 20-175 A. The sheath contributes about two-thirds or more of the arc voltage. The LTE model predicts a different variation of the arc voltage with I and underestimates the experimental values appreciably for low currents but by no more than approximately 2 V for I ≳ 120 A. However, the latter can hardly be considered as a proof of unimportance of the space-charge sheath at high currents: the LTE model overestimates both the resistance of the bulk of the arc column and the resistance of the part of the column that is adjacent to the cathode, and this overestimation to a certain extent compensates for the neglect of the voltage drop in the sheath. Furthermore, if the latter resistance were evaluated in the framework of the LTE model in an accurate way, then the overestimation would be still much stronger and the obtained voltage would significantly exceed those observed in the experiment.

  1. Glow discharge processing vs bakeout for aluminum storage ring vacuum chambers

    International Nuclear Information System (INIS)

    Dean, N.R.; Hoyt, E.W.; Palrang, M.T.; Walker, B.G.

    1977-11-01

    Experiments were carried out on laboratory and prototype scale systems in order to establish the feasibility of argon discharge processing the PEP storage ring aluminum vacuum chambers. Electron-induced desorption rates showed significant reductions following bakeout and/or argon glow discharge treatment (>10 19 ions cm -1 ). Data are presented and discussed in relation to advantages and problems associated with: water removal, argon trapping and subsequent release, electron energy dependence, discharge distribution, and surface plasma chemical effects

  2. Arc-discharge system for nondestructive detection of flaws in thin ceramic coatings

    International Nuclear Information System (INIS)

    Scott, G.W.; Davis, E.V.

    1978-04-01

    The feasibility of nondestructively detecting small cracks or holes in plasma-sprayed ceramic coatings with an electric arc-discharge system was studied. We inspected ZrO 2 coatings 0.46 mm (0.018 in.) thick on Incoloy alloy 800 substrates. Cracks were artificially induced in controlled areas of the specimens by straining the substrates in tension. We designed and built a system to scan the specimen's surface at approximately 50 μm (0.002 in.) clearance with a sharp-pointed metal-tipped probe at high dc potential. The system measures the arc currents occurring at flaws, or plots a map of the scanned area showing points where the arc current exceeds a preset threshold. A theoretical model of the probe-specimen circuit shows constant dc potential to be the best choice for arc-discharge inspection of insulating coatings. Experimental observations and analysis of the data disclosed some potential for flaw description

  3. The influence of gap distance on the random walk of cathode spot in vacuum arc

    International Nuclear Information System (INIS)

    Shi Zongqian; Xiao Jia; Jia Shenli; Liu Zhigang; Wang Lijun

    2007-01-01

    Experiments were conducted in a detachable vacuum chamber for Cu vacuum arc with arc current in the range 19-24 A. Experimental results indicated that the gap distance had a distinct influence on the characteristics of the random walk of the cathode spot (CS) for the gap distance adopted, i.e. d = 4.8 mm and d = 6.8 mm. It was found that the increase in the gap distance could lead to a larger diffusion parameter. Based on the dynamics of fragments constituting the CS, it was proposed that with a longer gap distance, the magnetic interaction between fragments would be strengthened. It would result in the increase of the mean step length of the CS and the decrease of the mean step time, which would lead to a larger diffusion parameter as observed. The plasma density in the region of the CS was also found to decrease with the increase in the gap distance. It would result in the CS having a higher probability of jumping to the contaminated region but not to the vicinity of the existing crater

  4. Vacuum arc behavior and its voltage characteristics in drawing process controlled by composite magnetic fields along axial and transverse directions

    International Nuclear Information System (INIS)

    Wang, Lijun; Deng, Jie; Wang, Haijing; Jia, Shenli; Qin, Kang; Shi, Zongqian

    2015-01-01

    In this research, drawing vacuum arc (VA) experiments were conducted using composite contacts under currents ranging from 5 kA to 20 kA root mean square (rms). The new type of contact comprised an axial magnetic field (AMF) configuration and a transverse magnetic field (TMF) configuration. The TMF plate was in the center, surrounded by the AMF plate. The contact generated both AMFs and TMFs simultaneously. VA appearances and arc voltages were recorded, and the VA was modeled as a conductor for electromagnetic force analysis in ANSYS software. The results showed that the coaxiality of operating mechanisms significantly influenced arc behavior just as the arc was ignited. When arc brightness did not increase after ignition, there was a voltage drop accompanied with diffusion of the VA. As to VA development, when an arc was ignited on an AMF plate, it spread on the plate and rotated. Over time the arc current increased, the constricting arc forms, and the arc column rotated on the TMF plate under the action of Ampere's force. With regard to the influence of a magnetic field on a VA at different stages, in the initial drawing arc stage the TMF was dominant, and the arc started to rotate under the action of Ampere's force. Afterwards, the AMF was dominant, with a steadily burning arc. As for contact melting, in the initial arcing period, a contracted short arc caused severe melting and erosion of the contact plate. When the ignition spot or root was close to the slot of plate, the electromagnetic force pushed the arc toward slot and contact edge, resulting in local erosion of the slot region

  5. Thermal motion of carbon clusters and production of carbon nanotubes by gravity-free arc discharge

    International Nuclear Information System (INIS)

    Mieno, T.; Takeguchi, M.

    2006-01-01

    Thermal and diffusion properties of hot gas around a dc arc discharge under a gravity-free condition are investigated using a jet plane in order to improve the arc production of carbon clusters. Spherically symmetric temperature distribution of He gas around the arc plasma and monotonic slow expansion of the high-temperature region are observed. By means of the passive-type Mie scattering method, random slow diffusion of carbon clusters around the arc plasma is clearly observed under the gravity-free condition. This indicates that carbon clusters including single-walled carbon nanotubes are synthesized around the arc plasma where the He temperature is higher than 1000 K. It is confirmed that large bundles of fatter single-walled carbon nanotubes are produced under the gravity-free condition

  6. Formation of self-organized anode patterns in arc discharge simulations

    International Nuclear Information System (INIS)

    Trelles, Juan Pablo

    2013-01-01

    Pattern formation and self-organization are phenomena commonly observed experimentally in diverse types of plasma systems, including atmospheric-pressure electric arc discharges. However, numerical simulations reproducing anode pattern formation in arc discharges have proven exceedingly elusive. Time-dependent three-dimensional thermodynamic non-equilibrium simulations reveal the spontaneous formation of self-organized patterns of anode attachment spots in the free-burning arc, a canonical thermal plasma flow established by a constant dc current between an axi-symmetric electrode configuration in the absence of external forcing. The number of spots, their size and distribution within the pattern depend on the applied total current and on the resolution of the spatial discretization, whereas the main properties of the plasma flow, such as maximum temperatures, velocity and voltage drop, depend only on the former. The sensibility of the solution to the spatial discretization stresses the computational requirements for comprehensive arc discharge simulations. The obtained anode patterns qualitatively agree with experimental observations and confirm that the spots originate at the fringes of the arc–anode attachment. The results imply that heavy-species–electron energy equilibration, in addition to thermal instability, has a dominant role in the formation of anode spots in arc discharges. (paper)

  7. Sustained diffusive alternating current gliding arc discharge in atmospheric pressure air

    DEFF Research Database (Denmark)

    Zhu, Jiajian; Gao, Jinlong; Li, Zhongshan

    2014-01-01

    Rapid transition from glow discharge to thermal arc has been a common problem in generating stable high-power non-thermal plasmas especially at ambient conditions. A sustained diffusive gliding arc discharge was generated in a large volume in atmospheric pressure air, driven by an alternating...... current (AC) power source. The plasma column extended beyond the water-cooled stainless steel electrodes and was stabilized by matching the flow speed of the turbulent air jet with the rated output power. Comprehensive investigations were performed using high-speed movies measured over the plasma column...

  8. Cathode-constriction and column-constriction in high current vacuum arcs subjected to an axial magnetic field

    Science.gov (United States)

    Zhang, Zaiqin; Ma, Hui; Liu, Zhiyuan; Geng, Yingsan; Wang, Jianhua

    2018-04-01

    The influence of the applied axial magnetic field on the current density distribution in the arc column and electrodes is intensively studied. However, the previous results only provide a qualitative explanation, which cannot quantitatively explain a recent experimental data on anode current density. The objective of this paper is to quantitatively determine the current constriction subjected to an axial magnetic field in high-current vacuum arcs according to the recent experimental data. A magnetohydrodynamic model is adopted to describe the high current vacuum arcs. The vacuum arc is in a diffuse arc mode with an arc current ranged from 6 kArms to 14 kArms and an axial magnetic field ranged from 20 mT to 110 mT. By a comparison of the recent experimental work of current density distribution on the anode, the modelling results show that there are two types of current constriction. On one hand, the current on the cathode shows a constriction, and this constriction is termed as the cathode-constriction. On the other hand, the current constricts in the arc column region, and this constriction is termed as the column-constriction. The cathode boundary is of vital importance in a quantitative model. An improved cathode constriction boundary is proposed. Under the improved boundary, the simulation results are in good agreement with the recent experimental data on the anode current density distribution. It is demonstrated that the current density distribution at the anode is sensitive to that at the cathode, so that measurements of the anode current density can be used, in combination with the vacuum arc model, to infer the cathode current density distribution.

  9. Formation of chemical compounds under vacuum plasma-arc deposition of nickel and its alloy onto piezoceramics

    International Nuclear Information System (INIS)

    Grinchenko, V.T.; Lyakhovich, T.K.; Prosina, N.I.; Khromov, S.M.

    1988-01-01

    The phase composition of the transition layer appearing during vacuum-arc coating of nickel and nickel alloy with copper on barium titanate and lead zirconate-titanate is identified. During vacuum plasma-arc coating of nickel and its alloy at the boundary with barium titanate and lead zirconate-titanate the Ni 2 Ti 4 O compound appears which has the crystal lattice type identical with substrate with the parity of lattice parameters. The transition layer contains nickel oxides and NiTiO 3 in the case of barium titanate. When titanate content in substrate increases the zone of reaction diffusion increases in value and becomes more complicate in composition

  10. Temperature and Nitric Oxide Generation in a Pulsed Arc Discharge Plasma

    International Nuclear Information System (INIS)

    Namihira, T.; Sakai, S.; Matsuda, M.; Wang, D.; Kiyan, T.; Akiyama, H.; Okamoto, K.; Toda, K.

    2007-01-01

    Nitric oxide (NO) is increasingly being used in medical treatments of high blood pressure, acute respiratory distress syndrome and other illnesses related to the lungs. Currently a NO inhalation system consists of a gas cylinder of N 2 mixed with a high concentration of NO. This arrangement is potentially risky due to the possibility of an accidental leak of NO from the cylinder. The presence of NO in the air leads to the formation of nitric dioxide (NO 2 ), which is toxic to the lungs. Therefore, an on-site generator of NO would be highly desirable for medical doctors to use with patients with lung disease. To develop the NO inhalation system without a gas cylinder, which would include a high concentration of NO, NAMIHIRA et al have recently reported on the production of NO from room air using a pulsed arc discharge. In the present work, the temperature of the pulsed arc discharge plasma used to generate NO was measured to optimize the discharge condition. The results of the temperature measurements showed the temperature of the pulsed arc discharge plasma reached about 10,000 K immediately after discharge initiation and gradually decreased over tens of microseconds. In addition, it was found that NO was formed in a discharge plasma having temperatures higher than 9,000 K and a smaller input energy into the discharge plasma generates NO more efficiently than a larger one

  11. Automatic production of fullerenes by a JxB arc jet discharge

    International Nuclear Information System (INIS)

    Mieno, Tetsu

    1995-01-01

    Effective production of many kinds of fullerenes including higher fullerenes and endohedral metallo-fullerenes are necessary to advance fullerene science and technology. Currently, the DC arc discharge method is the most effective method to produce fullerenes. However, carbon atoms evaporated from the anode tend to deposit on the cathode, which grow towards the anode, and obstruct the control of the arc discharge. Furthermore, deposited carbon should be removed to maintain continuous fullerene production. Here, to reduce the deposition of carbon on the cathode, a new discharge method is introduced and the experiment performed. When steady magnetic field is applied perpendicular to the DC current of the arc, ions and electrons are accelerated by JxB force as a plasma jet in the vertical direction. This plasma flow also accelerates helium convection due to the viscosity effect. Therefore, the carbon atoms and carbon neutrals are both blown up by the arc jet before arriving at the cathode. The arc flame in the experiment is actually observed to extend upwards, which dearly indicates the effect of the JxB force

  12. Pulse discharge cleaning of the vacuum vessel of HL-1 tokamak

    International Nuclear Information System (INIS)

    Li Guodong; Zhu Yukun; Xiao Zhenggui; Sun Shouqi; Ze Mingrui

    1986-01-01

    The HL-1 Tokamak was test-operated on September 21, 1984. During the period of vacuum conditioning, including 60 hours of baking up to 200 deg C and 7 x 10 4 shots of pulse discharge cleaning, the calculated quantities of carbon and oxygen removed are equivalent to 24 and 6 monolayers, respectively. Then, 124 shots of tokamak discharge were performed with low level plasma parameters. The plasma current and pulse length achieved were 60 kA and 85 ms at the toroidal magnetic field of 15 kG. This paper described the techniques used and the effect on discharge characteristics of bakeout and pulse discharge cleaning of the vacuum vessel

  13. Growth of small diameter multi-walled carbon nanotubes by arc discharge process

    International Nuclear Information System (INIS)

    Chaudhary, K. T.; Ali, J.; Yupapin, P. P.

    2014-01-01

    Multi-walled carbon nanotubes (MWCNTs) are grown by arc discharge method in a controlled methane environment. The arc discharge is produced between two graphite electrodes at the ambient pressures of 100 torr, 300 torr, and 500 torr. Arc plasma parameters such as temperature and density are estimated to investigate the influences of the ambient pressure and the contributions of the ambient pressure to the growth and the structure of the nanotubes. The plasma temperature and density are observed to increase with the increase in the methane ambient pressure. The samples of MWCNT synthesized at different ambient pressures are analyzed using transmission electron microscopy, scanning electron microscopy, Raman spectroscopy, Fourier transform infrared spectroscopy, and X-ray diffraction. An increase in the growth of MWCNT and a decrease in the inner tube diameter are observed with the increase in the methane ambient pressure

  14. Simulation of electric arc with hysteresis during discharge of a fusion superconducting magnet system

    International Nuclear Information System (INIS)

    Kraus, H.G.; Jones, J.L.

    1986-01-01

    Simulation of an internal voltage induced arc strike and attendant voltage-current hysteresis characteristics in an FED/INTOR scale superconducting magnet and circuit protection system during discharge was performed. To begin, an analytical solution was used to investigate system response for an internally shorted magnet and simplified circuit protection system during magnet discharge. The short produced a current split within the magnet resulting in a transformer like mutual inductance effect. Thus, the coupling coefficient was introduced in the equations to be physically realistic and to prevent degeneration of the associated eigenvalue problem. The effects of varying short resistance, dump resistance, and number of coil turns shorted are presented. This led to simulation of an arc strike, including hysteresis effects, which is then compared to the usual constant resistance used to simulate magnet shorts. Tracking of arc characteristics was made possible through specially developed multiple tripping capabilities recently incorporated into MSCAP (Magnet Systems Circuitry Analysis Program) for safety and instrumentation control simulation

  15. Combined electron beam and vacuum ARC melting for barrier tube shell material

    International Nuclear Information System (INIS)

    Worcester, S.A.; Woods, C.R.

    1989-01-01

    This patent describes a process of the type wherein zirconium tetrachloride is reduced to produce a metallic zirconium sponge. The sponge is distilled to generally remove residual magnesium and magnesium chloride, and the distilled sponge is melted to produce an ingot, the improvement for making a non-crystal bar material for use in lining the interior of zirconium alloy fuel element cladding which comprises: a. forming the distilled sponge into a consumable electrode; b. melting the consumable electrode in a multiple swept beam electron furnace with a feed rate between 1 and 20 inches per hour to form an intermediate ingot; and c. vacuum arc melting the intermediate ingot to produce a homogeneous final ingot, having 50-500 ppm iron

  16. Device quality ZnO grown using a Filtered Cathodic Vacuum Arc

    International Nuclear Information System (INIS)

    Elzwawi, Salim; Kim, Hyung Suk; Heinhold, Robert; Lynam, Max; Turner, Gary; Partridge, Jim G.; McCulloch, Dougal G.

    2012-01-01

    In this paper we report on the structural, electrical and optical characteristics of unintentionally doped ZnO films grown on a-plane sapphire substrates using the Filtered Cathodic Vacuum Arc (FCVA) technique. The resulting films showed considerable promise for device applications with properties including high transparency, moderate intrinsic carrier concentrations (10 17 -10 19 cm -3 ), electron mobilities up to 30 cm 2 /Vs, low surface roughness (typically <2% of film thickness) and well-structured photoluminescence. Post-annealing in oxygen at temperatures up to 800 °C produced significant improvements in the properties of these films. Silver oxide Schottky diodes fabricated on FCVA ZnO showed ideality factors as low as 1.20 and good sensitivity to ultraviolet light.

  17. Preparation of anatase TiO2 thin films by vacuum arc plasma evaporation

    International Nuclear Information System (INIS)

    Miyata, Toshihiro; Tsukada, Satoshi; Minami, Tadatsugu

    2006-01-01

    Anatase titanium dioxide (TiO 2 ) thin films with high photocatalytic activity have been prepared with deposition rates as high as 16 nm/min by a newly developed vacuum arc plasma evaporation (VAPE) method using sintered TiO 2 pellets as the source material. Highly transparent TiO 2 thin films prepared at substrate temperatures from room temperature to 400 deg. C exhibited photocatalytic activity, regardless whether oxygen (O 2 ) gas was introduced during the VAPE deposition. The highest photocatalytic activity and photo-induced hydrophilicity were obtained in anatase TiO 2 thin films prepared at 300 deg. C, which correlated to the best crystallinity of the films, as evidenced from X-ray diffraction. In addition, a transparent and conductive anatase TiO 2 thin film with a resistivity of 2.6 x 10 -1 Ω cm was prepared at a substrate temperature of 400 deg. C without the introduction of O 2 gas

  18. Carbon nanotubes and nanofibers synthesized by CVD on nickel coatings deposited with a vacuum arc

    Energy Technology Data Exchange (ETDEWEB)

    Escobar, M. [LP and MC, Dep. de Fisica-FCEyN-UBA, Cdad. Universitaria Pab.1, (1428), Buenos Aires (Argentina); DQIAQF-FCEyN-UBA, Cdad. Universitaria Pab.1, (1428), Buenos Aires (Argentina); Giuliani, L. [INFIP, CONICET, Dep. de Fisica, FCEyN-UBA, Cdad. Univ. Pab.1, (1428), Buenos Aires (Argentina); Candal, R.J. [INQUIMAE-FCEyN-UBA, Cdad. Universitaria Pab.2, (1428), Buenos Aires (Argentina); Lamas, D.G. [CINSO, CITEFA, CONICET, J.B. de La Salle 4397, (1603) V.Martelli, Buenos Aires (Argentina); Caso, A. [LP and MC, Dep. de Fisica-FCEyN-UBA, Cdad. Universitaria Pab.1, (1428), Buenos Aires (Argentina); Rubiolo, G. [LP and MC, Dep. de Fisica-FCEyN-UBA, Cdad. Universitaria Pab.1, (1428), Buenos Aires (Argentina); UAM-CNEA, Av. Gral Paz 1499, (1650) San Martin, Buenos Aires (Argentina); Grondona, D. [INFIP, CONICET, Dep. de Fisica, FCEyN-UBA, Cdad. Univ. Pab.1, (1428), Buenos Aires (Argentina); Goyanes, S. [LP and MC, Dep. de Fisica-FCEyN-UBA, Cdad. Universitaria Pab.1, (1428), Buenos Aires (Argentina); Marquez, A., E-mail: amarquez@df.uba.a [INFIP, CONICET, Dep. de Fisica, FCEyN-UBA, Cdad. Univ. Pab.1, (1428), Buenos Aires (Argentina)

    2010-04-16

    Nanotubes and nanofibers were grown on Ni coatings deposited by plasma generated with a pulsed vacuum arc on silicon wafers using three different bias conditions: at floating potential (approximately +30 V respect to the grounded cathode); at ground potential; and at -60 V. An atomic force microscopy study showed that the Ni film morphology was affected by the bias condition of the substrate. The morphology of carbonaceous species depended on Ni-films characteristics. FE-SEM and TEM analyses have shown that nanofibers growth was favoured on Ni coatings deposited at -60 V whereas nanotubes grew mainly on Ni coatings obtained at floating and ground potentials. Hence, this new method to produce the precursor can be optimized to obtain nanotubes or nanofibers varying the substrate bias for the Ni deposition.

  19. Quality of the KhN73MBTYu alloy after electroslag remelting and vacuum arc remelting

    International Nuclear Information System (INIS)

    Shelgaeva, A.V.; Krichevets, M.I.; Shinkina, N.S.; Komissarov, A.I.

    1978-01-01

    The structure and properties of the heat-resisting KhN73MBTYu alloy are investigated after electroslag remelting (ESR) and vacuum arc (VAR) remelting in commercial furnaces. The complex investigations of the casted metal were carried out by modern methods along with the standard acceptance tests, and a number of service properties were determined. It is established that the ESR metal contains magnesium and has the reduced sulphur concentration; the alloy has more fine-grained structure at high isotropy of the properties at room and operating temperatures; higher endurance is achieved under reversal rotational bending; no laminated fractures are observed. According to the basic quality factors the ESR metal satisfies all requirements for the VAR metal. Due to exclusion of strippling of ESR electrodes and ingots the yield of steel forgings increases by 20-25% and the prime cost decreases in comparison with the industrial production of VAR metal

  20. Interaction between computational modelling and experiments for vacuum consumable arc remelting

    Energy Technology Data Exchange (ETDEWEB)

    Bertram, L. A.; Zanner, F. J.

    1980-01-01

    A combined computational-experimental modelling effort is currently underway to characterize the vacuum consumable arc remelt process. This effort involves the coupling of experimental results with a magnetohydrodynamic flow model which is capable of time accurate solutions of the interdependent fluid flow-solidification process in the ingot. Models such as this are driven by boundary conditions. Considerable data have been compiled from direct observation of the electrode tip and molten pool surface by means of high speed photography in order to gain an understanding of the processes at the pool surface and the appropriate corresponding boundary conditions. The crucible wall/molten metal miniscus conditions are less well understood. Pool volumes are computed at different melting currents and show reasonable agreement with experimentally determined values. Current flow through the ingot is evaluated numerically and the results indicate that a significant portion of the melt current does not reach the interior of the ingot. U-6 wt. % Nb alloy was used.

  1. Organic impurities harmful to arc discharge in multi-ampere duo-pigatron ion source

    International Nuclear Information System (INIS)

    Peng Zhudong; Wang Shouhu; Chen Miaosun; Huang Chongan; Ge Yishan; Fu Peng; E Maohuai

    1989-01-01

    Besides mechanism producing plasmain Duo-Pigatron Ion Source, the main purpose of this paper is to introduce the problem on arc discharge exhaustion caused by oil pollution. The problem was discovered during developing a 15 cm Duo-Pigatron Ion Source. The paper also describes its physical process

  2. Characterization of a high-power/current pulsed magnetized arc discharge

    NARCIS (Netherlands)

    Zielinski, J. J.; van der Meiden, H. J.; Morgan, T. W.; D.C. Schram,; De Temmerman, G.

    2012-01-01

    A high-power pulsed magnetized arc discharge has been developed to allow the superimposition of a dc plasma and a high-power plasma impulse with a single plasma source. A capacitor bank (8400 mu F) is parallel-coupled to the current regulated power supply. The current is transiently increased from

  3. Characterization of a high-power/current pulsed magnetized arc discharge

    NARCIS (Netherlands)

    Zielinski, J.J.; Meiden, van der H.J.; Morgan, T.W.; Schram, D.C.; De Temmerman, G.C.

    2012-01-01

    A high-power pulsed magnetized arc discharge has been developed to allow the superimposition of a dc plasma and a high-power plasma impulse with a single plasma source. A capacitor bank (8400 µF) is parallel-coupled to the current regulated power supply. The current is transiently increased from its

  4. Influence of Plasma Jet Temperature Profiles in Arc Discharge Methods of Carbon Nanotubes Synthesis.

    Science.gov (United States)

    Raniszewski, Grzegorz; Wiak, Slawomir; Pietrzak, Lukasz; Szymanski, Lukasz; Kolacinski, Zbigniew

    2017-02-23

    One of the most common methods of carbon nanotubes (CNTs) synthesis is application of an electric-arc plasma. However, the final product in the form of cathode deposit is composed of carbon nanotubes and a variety of carbon impurities. An assay of carbon nanotubes produced in arc discharge systems available on the market shows that commercial cathode deposits contain about 10% CNTs. Given that the quality of the final product depends on carbon-plasma jet parameters, it is possible to increase the yield of the synthesis by plasma jet control. Most of the carbon nanotubes are multiwall carbon nanotubes (MWCNTs). It was observed that the addition of catalysts significantly changes the plasma composition, effective ionization potential, the arc channel conductance, and in effect temperature of the arc and carbon elements flux. This paper focuses on the influence of metal components on plasma-jet forming containing carbon nanotubes cathode deposit. The plasma jet temperature control system is presented.

  5. Influence of Plasma Jet Temperature Profiles in Arc Discharge Methods of Carbon Nanotubes Synthesis

    Directory of Open Access Journals (Sweden)

    Grzegorz Raniszewski

    2017-02-01

    Full Text Available One of the most common methods of carbon nanotubes (CNTs synthesis is application of an electric-arc plasma. However, the final product in the form of cathode deposit is composed of carbon nanotubes and a variety of carbon impurities. An assay of carbon nanotubes produced in arc discharge systems available on the market shows that commercial cathode deposits contain about 10% CNTs. Given that the quality of the final product depends on carbon–plasma jet parameters, it is possible to increase the yield of the synthesis by plasma jet control. Most of the carbon nanotubes are multiwall carbon nanotubes (MWCNTs. It was observed that the addition of catalysts significantly changes the plasma composition, effective ionization potential, the arc channel conductance, and in effect temperature of the arc and carbon elements flux. This paper focuses on the influence of metal components on plasma-jet forming containing carbon nanotubes cathode deposit. The plasma jet temperature control system is presented.

  6. The Properties of Binary and Ternary Ti Based Coatings Produced by Thermionic Vacuum Arc (TVA Technology

    Directory of Open Access Journals (Sweden)

    Aurelia Mandes

    2018-03-01

    Full Text Available A series of the multicomponent thin films (binary: Ti-C; Ti-Ag and ternary: Ti-C-Ag; Ti-C-Al were fabricated by Thermionic Vacuum Arc (TVA technology in order to study the wear resistance and the anticorrosion properties. The effects of Ti amount on the microstructure, tribological and morphological properties were subsequently investigated. TVA is an original deposition method using a combination of anodic arc and electron gun systems for the growth of films. The samples were characterized using scanning electron microscope (SEM and a transmission electron microscope (TEM accompanied by selected area electron diffraction (SAED. Tribological properties were studied by a ball-on-disc tribometer in the dry regime and the wettability was assessed by measuring the contact angle with the See System apparatus. Wear Rate results indicate an improved sliding wear behavior for Ti-C-Ag: 1.31 × 10−7 mm3/N m (F = 2 N compared to Ti-C-Al coating wear rate: 4.24 × 10−7 mm3/N m. On the other hand, by increasing the normal load to 3 N an increase to the wear rate was observed for Ti-C-Ag: 2.58 × 10−5 mm3 compared to 2.33 × 10−6 mm3 for Ti-C-Al coating.

  7. Some novel design features of the LBL metal vapor vacuum arc ion sources

    International Nuclear Information System (INIS)

    MacGill, R.A.; Brown, I.G.; Galvin, J.E.

    1990-01-01

    The family of MEVVA (metal vapor vacuum arc) high current metal ion sources developed at LBL over the past several years has grown to include a number of different source versions with a wide range of some of the design and operational parameters. The MicroMEVVA source is a particularly compact version, about 2 cm diam and 10 cm long, while the MEVVA IV weighs some 30 kG. MEVVAs IV and V incorporate multiple cathode assemblies (16 and 18 separate cathodes, respectively), and the operating cathode can be switched rapidly and without downtime. The new MEVVA V embodiment is quite compact considering its broad beam (10 cm), high voltage (100 kV), and multiple cathode features. The large-area extractor grids used in MEVVA V were fabricated using a particularly simple technique, and they are clamped into position and can thus be changed simply and quickly. The electrical system used to drive the arc is particularly simple and incorporates several attractive features. In this article we review and describe a number of the mechanical and electrical design features that have been developed for these sources

  8. Analysis of conditions for magnetron discharge initiation at vacuum camera testing

    International Nuclear Information System (INIS)

    Tzeneva, Raina; Dineff, Peter; Darjanova, Denitza

    2002-01-01

    Models of electric field distribution for two typical cases of vacuum camera internal pressure control are investigated. New relations between the maximum magnetron discharge current value I max and the maximum electric field strength radial component value E τ max are established. (Author)

  9. Experimental investigation on the motion of cathode spots in removing oxide film on metal surface by vacuum arc

    International Nuclear Information System (INIS)

    Shi Zongqian; Jia Shenli; Wang Lijun; Yuan Qingjun; Song Xiaochuan

    2008-01-01

    The motion of vacuum arc cathode spots has a very important influence on the efficiency of removing the oxide film on the metal surface. In this paper, the characteristics of cathode spot motion are investigated experimentally. Experiments were conducted in a detachable vacuum chamber with ac (50 Hz) arc current of 1 kA (rms). A stainless steel plate covered by an oxide layer was used as the cathode. The motion of cathode spots during the descaling process was photographed by a high-speed digital camera with an exposure time of 2 μs. Experimental results indicate that the motion of cathode spots is influenced by the interaction among individual cathode jets and the position of the anode as well as the surface condition. The waveform of arc voltage is also influenced by the motion of cathode spots

  10. Multilayer Ti-Cr-N Coatings Produced by the Vacuum-Arc Deposition

    International Nuclear Information System (INIS)

    Kunchenko, Yu.V.; Kunchenko, V.V.; Neklyudov, I.M.; Kartmazov, G.N.; Andreev, A.A.

    2007-01-01

    A possibility is demonstrated for nanolayer TiN x /CrN x coating formation by the method of vacuum-arc deposition on the substrate, which being rotated around the 'Bulat'-type chamber axis intercepts sequentially the plasma flows generated by three evaporators. The model for calculating the coating deposition rate (thickness) was used to determine the geometrical parameters that provide the formation of layer structures in the nanometer range. The variations of phase-structure characteristics, compression microstresses (σ) microhardness (H v ) of the coating formed have been investigated as functions of nitrogen pressure (P N =0.001...1.0 Pa), bias voltage (U=-100...-300 V) and condensation temperature (T C =330...750 degree C) at focusing magnetic field strength H F =0; 35 and 100 Oe. The mentioned field strengths were responsible for the ion current densities (j∼5,8...10 and ≥15 mA/cm 2 ). A nonmonotonic behaviour of H v as a function of condensation temperature and of vacuum annealing temperature has been established. The maximum H v values (∼35...37 GPa) were observed in the 450...500 degree C range

  11. Effectiveness of recycling light in ultra-bright short-arc discharge lamps.

    Science.gov (United States)

    Malul, Asher; Nakar, Doron; Feuermann, Daniel; Gordon, Jeffrey M

    2007-10-17

    Recycling light back into a plasma lamp's radiant zone can enhance its radiance. Measurements are reported for the effectiveness, spectral properties and modified plasma radiance maps that result from light recycling with a specular hemispherical mirror in commercial 150 W ultrabright Xenon short-arc discharge lamps, motivated by projection, biomedical and high-temperature furnace applications. For certain spectral windows and plasma arc regions, radiance can be heightened by up to 70%. However, the overall light recycling efficiency is reduced to about half this value due to lamp geometry. The manner in which light-plasma interactions affect light recycling efficacy is also elucidated.

  12. Modeling of inhomogeneous mixing of plasma species in argon–steam arc discharge

    Czech Academy of Sciences Publication Activity Database

    Jeništa, Jiří; Takana, H.; Uehara, S.; Nishiyama, H.; Bartlová, M.; Aubrecht, V.; Murphy, A.B.

    2018-01-01

    Roč. 51, č. 4 (2018), č. článku 045202. ISSN 0022-3727 R&D Projects: GA ČR(CZ) GA15-19444S; GA ČR(CZ) GC17-10246J Institutional support: RVO:61389021 Keywords : arc * combined diffusion coefficients * (in)homogeneous mixing * mass (mole) fraction * hybrid-stabilized electric arc Subject RIV: BL - Plasma and Gas Discharge Physics OBOR OECD: Fluids and plasma physics (including surface physics) Impact factor: 2.588, year: 2016 http://iopscience.iop.org/article/10.1088/1361-6463/aa9f6f/meta

  13. Current-Voltage Characteristics of DC Discharge in Micro Gas Jet Injected into Vacuum Environment

    International Nuclear Information System (INIS)

    Matra, K; Furuta, H; Hatta, A

    2013-01-01

    A current-voltage characteristic of direct current (DC) gas discharge operated in a micro gas jet injected into a secondary electron microscope (SEM) chamber is presented. Ar gas was injected through a 30 μm orifice gas nozzle (OGN) and was evacuated by an additional pump to keep the high vacuum environment. Gas discharges were ignited between the OGN as anode and a counter electrode of Si wafer. The discharge was self-pulsating in most of the cases while it was stable at lower pressure, larger gap length, and larger time averaged current. The self-pulsating discharge was oscillated by the RC circuit consisting of a stray capacitor and a large ballast resistor. The real time plots of voltage and current during the pulsating was investigated using a discharge model.

  14. Low pressure arc discharges with hollow cathodes and their using in plasma generators and charged particle sources

    CERN Document Server

    Vintizenko, L G; Koval, N N; Tolkachev, V S; Lopatin, I V; Shchanin, P M

    2001-01-01

    Paper presents the results of investigation into arc discharges with a hollow cathode generating 10 sup 1 sup 0 -10 sup 1 sup 2 concentration gas-discharge plasma in essential (approx 1 m sup 3) volumes at low (10 sup - sup 2 -1 Pa) pressures and up to 200 A discharge currents. One studied design of discharge systems with heated and cold cathodes their peculiar features, presented the parameters of plasma generators and of charged particle sources based on arc discharges and discussed, as well, the problems of more rational application of those systems in the processes for surface modification of solids

  15. Infrared losses from a Na/Sc metal-halide high intensity discharge arc lamp

    International Nuclear Information System (INIS)

    Smith, D J; Bonvallet, G A; Lawler, J E

    2003-01-01

    A study of the near-infrared (IR) emission from the arc of a metal-halide high intensity discharge (MH-HID) lamp with a sodium/scandium chemistry is reported. Radiometrically calibrated spectra from 0.7 to 2.5 μm were recorded as a function of position on the arc tube of a 250 W lamp. These spectra were analysed to determine the relative densities of Na and Sc atoms and the arc temperature as a function of radius. Information from these spectra, combined with absorption measurements in the companion paper (Bonvallet and Lawler 2003), were used to determine the absolute output power in the near-IR from the MH-HID lamp

  16. Preparation of carbon nanotubes by DC arc discharge process under reduced pressure in an air atmosphere

    International Nuclear Information System (INIS)

    Kim, Hyeon Hwan; Kim, Hyeong Joon

    2006-01-01

    Carbon nanotubes (CNTs) were grown using a DC arc discharge process in an air atmosphere and relevant process parameters were investigated. Without using an inert gas, multi walled carbon nanotubes could be synthesized in the deposit area of the cathode even in an air atmosphere, but single walled carbon nanotubes were not detected in the soot area despite using the same process conditions as in the inert gas. The air pressure for the highest yield of multi walled CNTs was 300 Torr. In addition, the quantity of amorphous carbon and other nanoparticles in the process chamber was remarkably reduced by this technique, showing that an efficient, feasible method of large scale CNT fabrication could be achieved by the arc discharge process

  17. Modeling of inhomogeneous mixing of plasma species in argon-steam arc discharge

    Science.gov (United States)

    Jeništa, J.; Takana, H.; Uehara, S.; Nishiyama, H.; Bartlová, M.; Aubrecht, V.; Murphy, A. B.

    2018-01-01

    This paper presents numerical simulation of mixing of argon- and water-plasma species in an argon-steam arc discharge generated in a thermal plasma generator with the combined stabilization of arc by axial gas flow (argon) and water vortex. The diffusion of plasma species itself is described by the combined diffusion coefficients method in which the coefficients describe the diffusion of argon ‘gas,’ with respect to water vapor ‘gas.’ Diffusion processes due to the gradients of mass density, temperature, pressure, and an electric field have been considered in the model. Calculations for currents 150-400 A with 15-22.5 standard liters per minute (slm) of argon reveal inhomogeneous mixing of argon and oxygen-hydrogen species with the argon species prevailing near the arc axis. All the combined diffusion coefficients exhibit highly nonlinear distribution of their values within the discharge, depending on the temperature, pressure, and argon mass fraction of the plasma. The argon diffusion mass flux is driven mainly by the concentration and temperature space gradients. Diffusions due to pressure gradients and due to the electric field are of about 1 order lower. Comparison with our former calculations based on the homogeneous mixing assumption shows differences in temperature, enthalpy, radiation losses, arc efficiency, and velocity at 400 A. Comparison with available experiments exhibits very good qualitative and quantitative agreement for the radial temperature and velocity profiles 2 mm downstream of the exit nozzle.

  18. Characterization of Ni ferrites powders prepared by plasma arc discharge process

    Energy Technology Data Exchange (ETDEWEB)

    Safari, A. [Department of Materials Science and Engineering, Faculty of Engineering, Shahid Chamran University, Ahvaz (Iran, Islamic Republic of); Gheisari, Kh., E-mail: khgheisari@scu.ac.ir [Department of Materials Science and Engineering, Faculty of Engineering, Shahid Chamran University, Ahvaz (Iran, Islamic Republic of); Farbod, M. [Physics Department, Shahid Chamran University, Ahvaz (Iran, Islamic Republic of)

    2017-01-01

    The aim of this work was to synthesize a single-phase spinel structure from a mixture of zinc, iron and nickel powders by plasma arc discharge method. A mixture of zinc, iron and nickel powders with the appropriate molar ratio was prepared and formed into a cylindrical shape. The synthesis process was performed in air, oxygen and argon atmospheres with the applied arc current of 400 A and pressure of 1 atm. After establishing an arc between the electrodes, the produced powders were collected and their structure and magnetic properties were examined by XRD and VSM, respectively. ZnO as an impurity was appeared in the as-produced powders owing to the high reactivity of zinc atoms, preventing the formation of Ni–Zn ferrite. A pure spinel structure with the highest saturation magnetization (43.8 emu/g) was observed as zinc powders removed completely from the initial mixture. Morphological evaluations using field emission scanning electron microscopy showed that the mean size of fabricated nanoparticles was in the range 100–200 nm and was dependent on the production conditions. - Highlights: • Nanocrystalline Ni ferrite powders are prepared by plasma arc discharge process. • The mean particle size of the as-synthesized ceramic powders is about 100 nm. • The highest saturation magnetization is observed as zinc powders removed completely from the initial mixture.

  19. Edge-carboxylated graphene nanoflakes from nitric acid oxidised arc-discharge material

    OpenAIRE

    NICOLOSI, VALERIA

    2010-01-01

    PUBLISHED Graphene nanoflakes (GNFs) with average diameters of 30 nm have been prepared by a single-step oxidation procedure using single-wall carbon nanotube arc-discharge material and nitric acid. The GNFs are predominately single sheets containing a small number of internal defects. The edges are decorated with primarily carboxylic acid groups which allow facile chemical functionalisation and cross-linking of the fragments using multivalent cations

  20. Two-dimensional simulation research of secondary electron emission avalanche discharge on vacuum insulator surface

    Science.gov (United States)

    Cai, Libing; Wang, Jianguo; Zhu, Xiangqin; Wang, Yue; Zhang, Dianhui

    2015-01-01

    Based on the secondary electron emission avalanche (SEEA) model, the SEEA discharge on the vacuum insulator surface is simulated by using a 2D PIC-MCC code developed by ourselves. The evolutions of the number of discharge electrons, insulator surface charge, current, and 2D particle distribution are obtained. The effects of the strength of the applied electric field, secondary electron yield coefficient, rise time of the pulse, length of the insulator on the discharge are investigated. The results show that the number of the SEEA electrons presents a quadratic dependence upon the applied field strength. The SEEA current, which is on the order of Ampere, is directly proportional to the field strength and secondary electron yield coefficient. Finally, the electron-stimulated outgassing is included in the simulation code, and a three-phase discharge curve is presented by the simulation, which agrees with the experimental data.

  1. Two-dimensional simulation research of secondary electron emission avalanche discharge on vacuum insulator surface

    International Nuclear Information System (INIS)

    Cai, Libing; Wang, Jianguo; Zhu, Xiangqin; Wang, Yue; Zhang, Dianhui

    2015-01-01

    Based on the secondary electron emission avalanche (SEEA) model, the SEEA discharge on the vacuum insulator surface is simulated by using a 2D PIC-MCC code developed by ourselves. The evolutions of the number of discharge electrons, insulator surface charge, current, and 2D particle distribution are obtained. The effects of the strength of the applied electric field, secondary electron yield coefficient, rise time of the pulse, length of the insulator on the discharge are investigated. The results show that the number of the SEEA electrons presents a quadratic dependence upon the applied field strength. The SEEA current, which is on the order of Ampere, is directly proportional to the field strength and secondary electron yield coefficient. Finally, the electron-stimulated outgassing is included in the simulation code, and a three-phase discharge curve is presented by the simulation, which agrees with the experimental data

  2. A paradigm study for assessment of phenylalanine's damage under arc-discharge irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Ke Zhigang [Laboratory of Ion Beam Bio-engineering, Institute of Plasma Physics of Chinese Academy of Sciences, P.O. Box 1126, Shushanhu Road 350, Hefei 230031 (China); Huang Qing, E-mail: huangq@ipp.ac.c [Laboratory of Ion Beam Bio-engineering, Institute of Plasma Physics of Chinese Academy of Sciences, P.O. Box 1126, Shushanhu Road 350, Hefei 230031 (China); Su Xi; Jiang Jiang; Wang Xiangqin; Yu Zengliang [Laboratory of Ion Beam Bio-engineering, Institute of Plasma Physics of Chinese Academy of Sciences, P.O. Box 1126, Shushanhu Road 350, Hefei 230031 (China)

    2010-05-15

    Energetic ions induce important biological effects and the research into radiolysis of amino acids can help to clarify radiolysis of proteins. For this purpose, arc-discharge induced radiolysis of the benzyl-containing aromatic amino acid phenylalanine in aqueous solution was studied and the damage was assessed quantitatively. The energetic ions were produced by arc-discharge in nitrogen and argon atmosphere. The arc-discharge induced chemical reactions of the biomolecule in aqueous solution were detected and analyzed by means of UV-Vis absorption, fluorescence, Fourier transformation infrared (FTIR) spectroscopy and high performance liquid chromatography (HPLC). Based on the multiple spectroscopic approach, the damage can be evaluated in a more reliable and convenient way. The fluorescence analysis in this case appears to be a more direct indicator for the assessment of damage, where it reveals that the damage increases with the irradiation time exponentially. On the contrary, the 'plateau region' or 'saddle-shape' apparently shown both in our rough absorption analysis and ninhydrin reaction test, similar to the previously reported feature of the dose effect for low-energy-ion induced damage, may be just a consequence with varied reactions and processes involved at different stages. This work thus demonstrated that application of appropriate combination of spectroscopic tools can effectively dissect the diversity of the radiolysis reaction system and assess the biomolecular damage properly.

  3. Optical and structural properties of colloidal zirconia nanoparticles prepared by arc discharge in liquid

    Science.gov (United States)

    Peymani forooshani, Reza; Poursalehi, Reza; Yourdkhani, Amin

    2018-01-01

    Zirconia is one of the important ceramic materials with unique properties such as high melting point, high ionic conductivity, high mechanical properties and low thermal conductivity. Therefore, zirconia is one of the useful materials in refractories, thermal barriers, cutting tools, oxygen sensors electrolytes, catalysis, catalyst supports and solid oxide fuel cells. Recently, direct current (DC) arc discharge is extensively employed to synthesis of metal oxide nanostructures in liquid environments. The aim of this work is the synthesis of colloidal zirconia nanoparticles by DC arc discharge method in water as a medium. Arc discharge was ignited between two pure zirconium electrodes in water. Optical and structural properties of prepared colloidal nanoparticles were investigated. Scanning Electron Microscopy (SEM), X-Ray Diffraction (XRD) and UV-visible spectroscopy, were employed for characterization of particle size, morphology, crystal structure and optical properties, respectively. SEM images demonstrate that the nanoparticles are spherical in shape with an average size lower than 38 nm. The XRD patterns of the nanoparticles were consistent with tetragonal and monoclinic zirconia crystal structures. The optical transmission spectra of the colloidal solution show optical characteristic of zirconia nanoparticles as a wide band gap semiconductor with no absorption peak in visible wavelength with the considerable amount of oxygen deficiency. Oxidation of colloidal nanoparticles in water could be explained via reaction with either dissociated oxygen from water in hot plasma region or with dissolved oxygen in water. The results provide a simple and flexible method for preparation of zirconia nanoparticles with a capability of mass production without environmental footprints.

  4. Effect of duct bias on transport of vacuum arc plasmas through curved magnetic filters

    International Nuclear Information System (INIS)

    Anders, A.; Anders, S.; Brown, I.G.

    1994-01-01

    The plasma output of a 90 degree magnetic macroparticle filter of vacuum arc plasma was monitored by a Langmuir probe as a function of bias of the duct wall and guiding magnetic field. Maximum plasma transport through the filter was found at a positive bias of about 20 V. A relatively small magnetic field of 10--30 mT is sufficient for effective guiding of the plasma, and further increase of the guiding field improves the filter efficiency only gradually. The potential of a floating duct changes from negative to positive when the guiding field is increased. This can be explained by the balance of electron and ion flux transverse to the magnetic field. Saturation in the plasma output at high guiding field (>120 mT) is observed for carbon but not for heavy elements. The transport of plasma through bent ducts is made possible by the magnetic pressure of the guiding field, and by sheath and space-charge electric fields

  5. Comparative study of titanium carbide and nitride coatings grown by cathodic vacuum arc technique

    International Nuclear Information System (INIS)

    Devia, D.M.; Restrepo-Parra, E.; Arango, P.J.

    2011-01-01

    Titanium nitride (TiN), titanium carbide (TiC) thin films and TiC/TiN bilayers have been deposited on AISI 304 stainless steel substrates by plasma assisted physical vapor deposition technique - reactive pulsed vacuum arc method. The coatings were characterized in terms of crystalline structure, microstructure and chemical nature by X-ray diffraction and X-ray photoelectron spectroscopy, respectively. Tribological behavior was investigated using ball on disc technique. The average coefficient of friction was measured, showing lower values for the TiN/TiC bilayer. Dynamic wear curves were performed for each coating, observing a better wear resistance for TiN/TiC bilayers, compared to TiN and TiC monolayers. On the other hand, the TiCN formation in the TiN/TiC bilayer was observed, being attributed to the interdiffusion between TiN and TiC at the interface. Moreover, the substrate temperature influence was analysing observing a good behavior at T S = 115 °C.

  6. Simulation of cathode spot crater formation and development on CuCr alloy in vacuum arc

    Science.gov (United States)

    Wang, Lijun; Zhang, Xiao; Wang, Yuan; Yang, Ze; Jia, Shenli

    2018-04-01

    The two-dimensional (2D) rotary axisymmetric model is used to describe the formation and development of a cathode spot on a copper-chromium alloy (CuCr) in a vacuum arc. The model includes hydrodynamic equations and the heat transfer equation. Parameters used in this model come from experiments and other researchers' work. The influence of parameters is analyzed, and the simulation results are compared with pure metal simulation results. In simulation, the depth of the cathode crater is from 0.5 μm to 1.1 μm, the radius of the cathode crater is from 1.6 μm to 2.6 μm, the maximum velocity of the droplet is from 200 m/s to 600 m/s, and the maximum temperature is from 3500 K to 5000 K which is located in the area with a radius of 0.5-1.5 μm. The simulation results show that a smooth cathode surface is advantageous for reducing ablation, the ablation on the CuCr alloy is smaller than that on the pure metal cathode electrode, and the cathode spot appears on the chromium grain only on CuCr. The simulation results are in good agreement with the experiment.

  7. Preparation of anatase TiO{sub 2} thin films by vacuum arc plasma evaporation

    Energy Technology Data Exchange (ETDEWEB)

    Miyata, Toshihiro [Optoelectronic Device System R and D Center, Kanazawa Institute of Technology, 7-1 Ohgigaoka, Nonoichi, Ishikawa 921-8501 (Japan)]. E-mail: tmiyata@neptune.kanazawa-it.ac.jp; Tsukada, Satoshi [Optoelectronic Device System R and D Center, Kanazawa Institute of Technology, 7-1 Ohgigaoka, Nonoichi, Ishikawa 921-8501 (Japan); Minami, Tadatsugu [Optoelectronic Device System R and D Center, Kanazawa Institute of Technology, 7-1 Ohgigaoka, Nonoichi, Ishikawa 921-8501 (Japan)

    2006-02-01

    Anatase titanium dioxide (TiO{sub 2}) thin films with high photocatalytic activity have been prepared with deposition rates as high as 16 nm/min by a newly developed vacuum arc plasma evaporation (VAPE) method using sintered TiO{sub 2} pellets as the source material. Highly transparent TiO{sub 2} thin films prepared at substrate temperatures from room temperature to 400 deg. C exhibited photocatalytic activity, regardless whether oxygen (O{sub 2}) gas was introduced during the VAPE deposition. The highest photocatalytic activity and photo-induced hydrophilicity were obtained in anatase TiO{sub 2} thin films prepared at 300 deg. C, which correlated to the best crystallinity of the films, as evidenced from X-ray diffraction. In addition, a transparent and conductive anatase TiO{sub 2} thin film with a resistivity of 2.6 x 10{sup -1} {omega} cm was prepared at a substrate temperature of 400 deg. C without the introduction of O{sub 2} gas.

  8. High rate deposition of transparent conducting oxide thin films by vacuum arc plasma evaporation

    Energy Technology Data Exchange (ETDEWEB)

    Minami, Tadatsugu; Ida, Satoshi; Miyata, Toshihiro

    2002-09-02

    Transparent conducting oxide (TCO) thin films have been deposited at a high rate above 370 nm/min by vacuum arc plasma evaporation (VAPE) using sintered oxide fragments as the source material. It was found that the deposition rate of TCO films was strongly dependent on the deposition pressure, whereas the obtained electrical properties were relatively independent of the pressure. Resistivities of 5.6x10{sup -4} and 2.3x10{sup -4} {omega}{center_dot}cm and an average transmittance above 80% (with substrate included) in the visible range were obtained in Ga-doped ZnO (GZO) thin films deposited at 100 and 350 deg. C, respectively. In addition, a resistivity as low as 1.4x10{sup -4} {omega}{center_dot}cm and an average transmittance above 80% were also obtained in indium-tin-oxide (ITO) films deposited at 300 deg. C. The deposited TCO films exhibited uniform distributions of resistivity and thickness on large area substrates.

  9. The spatial structure of cathode plasma jets in a vacuum arc

    International Nuclear Information System (INIS)

    Krinberg, I.A.; Zverev, E.A.

    1999-01-01

    It is shown that, in cathode plasma jets of a vacuum arc with an interelectrode gap of up to 1 m and a current of 10 2 -10 3 A, there exist three characteristic regions with different ratios β of the plasma pressure to the magnetic field pressure. The plasma emitted from cathode microspots, in the form of microjets, is heated and accelerated predominantly in the region near the cathode (z -2 ), in which β≅10 2 -10 3 . After the microjets merge into one jet, the plasma in the region z≅0.03-3 cm begins to move toward the jet axis because of the compression of the jet by its own magnetic field (β<1). Just before the compression reaches its maximum, the density, temperature, and potential sharply increase, and the compression comes to an end. In the region z≥3 cm, the cathode plasma jet looks like a paraboloid of revolution, whose surface oscillates about the equilibrium position (β≅1), which causes the density, temperature, and potential to oscillate in a similar fashion

  10. High rate deposition of transparent conducting oxide thin films by vacuum arc plasma evaporation

    International Nuclear Information System (INIS)

    Minami, Tadatsugu; Ida, Satoshi; Miyata, Toshihiro

    2002-01-01

    Transparent conducting oxide (TCO) thin films have been deposited at a high rate above 370 nm/min by vacuum arc plasma evaporation (VAPE) using sintered oxide fragments as the source material. It was found that the deposition rate of TCO films was strongly dependent on the deposition pressure, whereas the obtained electrical properties were relatively independent of the pressure. Resistivities of 5.6x10 -4 and 2.3x10 -4 Ω·cm and an average transmittance above 80% (with substrate included) in the visible range were obtained in Ga-doped ZnO (GZO) thin films deposited at 100 and 350 deg. C, respectively. In addition, a resistivity as low as 1.4x10 -4 Ω·cm and an average transmittance above 80% were also obtained in indium-tin-oxide (ITO) films deposited at 300 deg. C. The deposited TCO films exhibited uniform distributions of resistivity and thickness on large area substrates

  11. The multilayered structure of ultrathin amorphous carbon films synthesized by filtered cathodic vacuum arc deposition

    KAUST Repository

    Wang, Na

    2013-08-01

    The structure of ultrathin amorphous carbon (a-C) films synthesized by filtered cathodic vacuum arc (FCVA) deposition was investigated by high-resolution transmission electron microscopy, electron energy loss spectroscopy, and x-ray photoelectron spectroscopy. Results of the plasmon excitation energy shift and through-thickness elemental concentration show a multilayered a-C film structure comprising an interface layer consisting of C, Si, and, possibly, SiC, a buffer layer with continuously increasing sp 3 fraction, a relatively thicker layer (bulk film) of constant sp 3 content, and an ultrathin surface layer rich in sp 2 hybridization. A detailed study of the C K-edge spectrum indicates that the buffer layer between the interface layer and the bulk film is due to the partial backscattering of C+ ions interacting with the heavy atoms of the silicon substrate. The results of this study provide insight into the minimum thickness of a-C films deposited by FCVA under optimum substrate bias conditions. Copyright © 2013 Materials Research Society.

  12. Characterization of diamond-like carbon coatings prepared by pulsed bias cathodic vacuum arc deposition

    International Nuclear Information System (INIS)

    Wu Jinbao; Chang, J.-J.; Li, M.-Y.; Leu, M.-S.; Li, A.-K.

    2007-01-01

    Hydrogen free diamond-like carbon (DLC) coatings have been deposited on Si(100) and stainless steel substrates by cathodic vacuum arc plasma deposition with pulse voltage. Adherent deposits on silicon can be obtained through applying gradient Ti/TiC/DLC layers. A pulse bias of - 100 V was applied to the substrate in order to obtain a denser structure of DLC coating approximately 1 μm thick. The microstructure and hardness value of DLC films were analyzed by using X-ray photoelectron spectroscopy and nano-indenter. The experimental results show that the duty cycle strongly influenced the hardness and sp 3 content of the DLC coatings. We observed that when the duty cycle was raised from 2.5% to 12.5%, the hardness increased from 26 GPa to 49 GPa, and the sp 3 fraction of the DLC films measured by XPS increased from 39% to 50.8 % as well. But at constant duty cycle, say 12.5%, the hardness is dropped from 49 to 14 GPa in proportion to the increase of residual gas pressure from 3 x 10 -3 Pa to 1 Pa. As the residual gas pressure increased, collisional phenomenon will decrease the energy of the ions. Ions with low energy make more graphitic carbon links and result in a low hardness value

  13. Fabrication and dispersion evaluation of single-wall carbon nanotubes produced by FH-arc discharge method.

    Science.gov (United States)

    Chen, B; Zhao, X; Inoue, S; Ando, Y

    2010-06-01

    In this work, we produced SWNTs by a hydrogen DC arc discharge with evaporation of carbon anode containing 1 at% Fe catalyst in H2-Ar mixture gas. This was named as FH-arc discharge method. The as-grown SWNTs synthesized by FH-arc discharge method have high crystallinity. An oxidation purification process of as-grown SWNTs with H2O2 has been developed to remove the coexisting Fe catalyst nanoparticles. As a result, SWNTs with purity higher than 90 at% have been achieved. To exhibit remarkable characteristics, CNTs should be separated from the bundles and kept in homogeneous and stable suspensions. For this purpose, the SWNTs prepared by FH-arc discharge method also have been treated by Nanomizer process with some surfactants. SPM images showed that the SWNTs bundles had become thinner and shorter.

  14. Incidence Angle Effect of Energetic Carbon Ions on Deposition Rate, Topography, and Structure of Ultrathin Amorphous Carbon Films Deposited by Filtered Cathodic Vacuum Arc

    KAUST Repository

    Wang, N.; Komvopoulos, K.

    2012-01-01

    The effect of the incidence angle of energetic carbon ions on the thickness, topography, and structure of ultrathin amorphous carbon (a-C) films synthesized by filtered cathodic vacuum arc (FCVA) was examined in the context of numerical

  15. Experimental analysis on the effects of DC arc discharges at various flow regimes

    Energy Technology Data Exchange (ETDEWEB)

    Bianchi, G. [University of L’Aquila, L’Aquila 67100 (Italy); Saracoglu, B. H., E-mail: saracog@vki.ac.be; Regert, T. [von Karman Institute for Fluid Dynamics, Rhode Saint Genèse B-1640 (Belgium); Paniagua, G. [Purdue University, West-Lafayette, Indiana 47907 (United States)

    2015-03-15

    This paper addresses the control of the boundary layer on a compression ramp by means of DC electrical arc discharges. The development and realization of the control system are first described and then assessed in the wind tunnel. The objective of the research was to control the supersonic flow using the minimum amount of energy. The array of electrodes was located at the base of a ramp, where a low momentum flow develops. The electrical discharge was generated by a custom designed electronic facility based on high-voltage ignition coils. The slanted tungsten electrodes were insulated by mounting them in a ceramic support. The discharge evolution was studied through high-speed flow visualizations, while electrical measurements at the high-voltage section of the circuitry allowed to estimate the energy release. The development of a high-speed short exposure Schlieren imaging technique, based on a very short duration laser pulse illumination and a double shot CCD camera, allowed to observe the macroscopic effects associated with the arc establishment between the electrodes (glow, sound wave and heat release). Due to the long residence time, the thermal perturbation spread along the streamwise direction. Cross correlation of Schlieren images with short time separation revealed that in supersonic conditions, the discharges led to an overall acceleration of the flow field underneath the oblique shock wave.

  16. Synthesis and characteristics of Ag/Pt bimetallic nanocomposites by arc-discharge solution plasma processing.

    Science.gov (United States)

    Pootawang, Panuphong; Saito, Nagahiro; Takai, Osamu; Lee, Sang-Yul

    2012-10-05

    Arc discharge in solution, generated by applying a high voltage of unipolar pulsed dc to electrodes of Ag and Pt, was used as a method to form Ag/Pt bimetallic nanocomposites via electrode erosion by the effects of the electric arc at the cathode (Ag rod) and the sputtering at the anode (Pt rod). Ag/Pt bimetallic nanocomposites were formed as colloidal particles dispersed in solution via the reduction of hydrogen radicals generated during discharge without the addition of chemical precursor or reducing agent. At a discharge time of 30 s, the fine bimetallic nanoparticles with a mean particle size of approximately 5 nm were observed by transmission electron microscopy (TEM). With increasing discharge time, the bimetallic nanoparticle size tended to increase by forming an agglomeration. The presence of the relatively small amount of Pt dispersed in the Ag matrix could be observed by the analytical mapping mode of energy-dispersive x-ray spectroscopy and high-resolution TEM. This demonstrated that the synthesized particle was in the form of a nanocomposite. No contamination of other chemical substances was detected by x-ray photoelectron spectroscopy. Hence, solution plasma could be a clean and simple process to effectively synthesize Ag/Pt bimetallic nanocomposites and it is expected to be widely applicable in the preparation of several types of nanoparticle.

  17. Model experiments to study the first wall erosion by vacuum arcs

    Energy Technology Data Exchange (ETDEWEB)

    Karpov, D.A.; Saksagansky, G.L. (Leningradskij Nauchno-Issledovatel' skij Inst. (USSR). Electrophysical Apparatus); Paszti, F.; Szilagyi, E.; Manuaba, A. (Hungarian Academy of Sciences, Budapest. Central Research Inst. for Physics)

    Unipolar arcs acting on the first wall of future thermonuclear reactors were modelled by bipolar arcs burning on the side surface of a cylindrical titanium cathode. Erosion rate and spatial distribution of the material sputtered in arcs were investigated by Rutherford Backscattering (RBS) analysis of collector probes. The obtianed results will be discussed as a function of arc current and the intensity of the applied vault-shaped magnetic field. (orig.).

  18. Model experiments to study the first wall erosion by vacuum arcs

    International Nuclear Information System (INIS)

    Karpov, D.A.; Saksagansky, G.L.; Paszti, F.; Szilagyi, E.; Manuaba, A.

    1989-01-01

    Unipolar arcs acting on the first wall of future thermonuclear reactors were modelled by bipolar arcs burning on the side surface of a cylindrical titanium cathode. Erosion rate and spatial distribution of the material sputtered in arcs were investigated by Rutherford Backscattering (RBS) analysis of collector probes. The obtianed results will be discussed as a function of arc current and the intensity of the applied vault-shaped magnetic field. (orig.)

  19. Arc-Discharge Synthesis of Iron Encapsulated in Carbon Nanoparticles for Biomedical Applications

    Directory of Open Access Journals (Sweden)

    S. Chaitoglou

    2014-01-01

    Full Text Available The objective of the present work is to improve the protection against the oxidation that usually appears in core@shell nanoparticles. Spherical iron nanoparticles coated with a carbon shell were obtained by a modified arc-discharge reactor, which permits controlling the diameter of the iron core and the carbon shell of the particles. Oxidized iron nanoparticles involve a loss of the magnetic characteristics and also changes in the chemical properties. Our nanoparticles show superparamagnetic behavior and high magnetic saturation owing to the high purity α-Fe of core and to the high core sealing, provided by the carbon shell. A liquid iron precursor was injected in the plasma spot dragged by an inert gas flow. A fixed arc-discharge current of 40 A was used to secure a stable discharge, and several samples were produced at different conditions. Transmission electron microscopy indicated an iron core diameter between 5 and 9 nm. Selected area electron diffraction provided evidences of a highly crystalline and dense iron core. The magnetic properties were studied up to 5 K temperature using a superconducting quantum interference device. The results reveal a superparamagnetic behaviour, a narrow size distribution (σg=1.22, and an average diameter of 6 nm for nanoparticles having a blocking temperature near 40 K.

  20. The Effect of High-Pressure Arc Discharge Plasma on the Degradation of Chlorpyrifos

    International Nuclear Information System (INIS)

    Yin Meiqiang; Ma Tengcai; Zhang Jialiang; Huang Mingjing; Ma Buzhou

    2006-01-01

    A study is conducted to determine the effect of a kind of high-pressure arc discharge plasma on the degradation rate and kinetic equations of chlorpyrifos in different solvents with the treated times and concentrations as variables. The degradation rate was sorted in different solvents as water, methanol, acetone and then acetoacetate. The tendencies of the degradation rates with treated time in water and methanol were optimally fitted with first-order kinetics equations while those in acetone and acetoacetate were fitted with zeroth-order kinetics equations. The difference was attributed to the stronger polarity of water and methanol. The weak correlation of the degradation rates with time was mainly because the high-temperature of the arc discharge tube and the chemically-active species generated by the discharge. The degradation half-life was extended with increase of chlorpyrifos concentration. A degradation half-life less than 3 min was achieved for chlorpyrifos in water and methanol when the initial concentration was less than 300 μg/ml

  1. Experimental Investigation on the Influence of Axial Magnetic Field Distribution on Resisting the Constriction of a High-Current Vacuum Arc

    International Nuclear Information System (INIS)

    Shi Zongqian; Liu Zhigang; Jia Shenli; Song Xiaochuan; Wang Lijun

    2009-01-01

    Effect of the axial magnetic field (AMF) on resisting the constriction of a high-current vacuum arc is studied in this paper. Two typical AMF distributions were investigated, i.e., the traditional bell-shaped AMF, and the saddle-shaped AMF. Experiments were conducted in a detachable vacuum chamber with a rms arc current in the range of 10 kA to 25 kA. The arc column was photographed by a high-speed digital camera with an exposure time of 2 microseconds. The constriction of the vacuum arc was compared by processing the images of the arc column under the two different field configurations and numerically determining the dimensions of the arc column near the electrodes. It was also confirmed that the AMF distribution had a significant influence on its effectiveness in resisting arc constriction. Furthermore, the AMF strength near the periphery of the arc is more influential than that at the centre of the electrodes in resisting arc constriction.

  2. Measurements of 3D slip velocities and plasma column lengths of a gliding arc discharge

    DEFF Research Database (Denmark)

    Zhu, Jiajian; Gao, Jinlong; Ehn, Andreas

    2015-01-01

    A non-thermal gliding arc discharge was generated at atmospheric pressure in an air flow. The dynamics of the plasma column and tracer particles were recorded using two synchronized high-speed cameras. Whereas the data analysis for such systems has previously been performed in 2D (analyzing......, gives more realistic insight into the convection cooling process. Additionally, with the determination of the 3D slip velocity and the 3D length of the plasma column, we give more accurate estimates for the drag force, the electric field strength, the power per unit length, and the radius...

  3. Synthesis of multiwalled carbon nanotube from different grades of carbon black using arc discharge method

    Energy Technology Data Exchange (ETDEWEB)

    Arora, Neha, E-mail: n4neha31@gmail.com [Department of Mechanical Engineering, Birla Institute of Technology and Science, Pilani (India); Sharma, N. N. [Department of Mechanical Engineering, Birla Institute of Technology and Science, Pilani (India); Director, School of Automobile, Mechanical & Mechatronics, Manipal University,Jaipur,India (India)

    2016-04-13

    This paper describes the synthesis of nanotube from different grades (Tread * A(non-ASTM), N134,N121,N660 and N330)of carbon black using DC arc discharge method at 40A current for 60sec. Carbon black samples of different grades were procured from industry (Aditya Birla Science and Technology Limited, India). Scanning Electron Micrographs (SEM) of the deposited carbon nanostructures suggests that MWCNTs are formed at 40A and for a minimal exposure time of 60sec.The result formed indicates the N330 grade of carbon black gets converted to MWCNTs (Multiwall Carbon nanotube) as compared to other grades.

  4. Carbon nanostructures obtained by underwater arc discharge of graphite electrodes: Synthesis and characterization

    International Nuclear Information System (INIS)

    Darias Gonzalez, J. G.; Hernandez Tabare, L.; Herrera Palma, V.; Sierra Trujillo, J. S.; Desdin Garcia, L. F.; Codorniu Pujals, D.; Bermudez Martinez, A.; Arias de Fuentes, O.; Maury Toledo, A.

    2015-01-01

    In the present work, the application of the method of underwater arc discharge of graphite electrodes for obtaining several carbon nano structures is described. The analysis of the obtained products by Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), Raman spectroscopy, Atomic Force Microscopy (AFM) and X-Ray Diffraction (XRD) showed that the samples collected from the material floating on the water surface were composed mainly by polyhedral onion-like particles, while those taken from the precipitate were a mixture multi walled nano-tubes, onion-like particles and other graphitic structures. The main features of the obtained nano structures are discussed. (Author)

  5. Growth of metal micro and/or nanoparticles utilizing arc-discharge immersed in liquid

    Energy Technology Data Exchange (ETDEWEB)

    Rebollo P, B.; Gallardo G, G.; Ortega M, N.; Daniel P, G. [Instituto Tecnologico Superior de Irapuato, Km 12.5 Carretera Irapuato-Silao, 36821 Irapuato, Guanajuato (Mexico); Sampedro, M. P.; Zenteno M, B. [Benemerita Universidad Autonoma de Puebla, Facultad de Ingenieria, Ciudad Universitaria, 72590 Puebla, Puebla (Mexico); Bravo B, C. F. [Comision Federal de Electricidad, Laboratorio de Pruebas de Equipos y Materiales, Irapuato, Guanajuato (Mexico); Hernandez C, D. [Universidad Autonoma de Chiapas, Facultad de Ingenieria, 29050 Tuxtla Gutierrez, Chiapas (Mexico); Jimenez S, S., E-mail: mpstraviata@hotmail.com [Instituto Politecnico Nacional, Centro de Investigacion y de Estudios Avanzados, Laboratorio de Investigacion en Materiales, 76230 Santiago de Queretaro, Queretaro (Mexico)

    2014-07-01

    In this paper, we present results on the metal microcrystals and nanoparticles of Al, Cu and Al-Cu composite growth by arc-discharge with the system immersed in distilled water, under different conditions and varying the current from 50 to 150 A with constant voltage (27 V). These structures are characterized using X-ray diffraction, scanning electron microscopy, Raman spectroscopy and UV-Vis spectroscopy. Our results demonstrate that metal micro and nano structures can be prepared at low cost with high quality. (Author)

  6. Discharge coefficient correlations for circular-arc venturi flowmeters at critical /sonic/ flow

    Science.gov (United States)

    Arnberg, B. T.; Britton, C. L.; Seidl, W. F.

    1973-01-01

    Experimental data are analyzed to support theoretical predictions for discharge coefficients in circular-arc venturi flow meters operating in the critical sonic flow regime at throat Reynolds numbers above 150 thousand. The data tend to verify the predicted 0.25% decrease in the discharge coefficient during transition from a laminar to turbulent boundary layer. Four different test gases and three flow measurement facilities were used in the experiments with 17 venturis with throat sizes from 0.15 to 1.37 in. and Beta ratios ranging from 0.014 to 0.25. Recommendations are given as to how the effectiveness of future studies in the field could be improved.

  7. A Simulation of Pre-Arcing Plasma Discharge Processes in Water Purification

    International Nuclear Information System (INIS)

    Rodriguez-Mendez, B. G.; Piedad-Beneitez, A. de la; Lopez-Callejas, R.; Godoy-Cabrera, O. G.; Benitez-Read, J. S.; Pacheco-Sotelo, J. O.; Pena-Eguiluz, R.; Mercado-Cabrera, A.; Valencia-A, R.; Barocio, S. R.

    2006-01-01

    The simulation of a water purification system within a coaxial cylinder reactor operated by 1 kHz frequency plasma discharges in pre-arcing regimes is presented. In contrast with precedent works, this computational model considers three mechanisms of the system operation: (a) the relevant physical characteristics of water (b) the ionisation and expansion processes in the spark channel including the near-breakdown electric current generated by the rate of change of the effective capacitance and resistance in the discharge, and (c) the energy associated with this initial spark in the water. The outcome of the model seems to meet all main requirements to allow the design and construction of specific water purification technology devices

  8. Structure, phase composition and microhardness of vacuum-arc multilayered Ti/Al, Ti/Cu, Ti/Fe, Ti/Zr nano-structures with different periods

    International Nuclear Information System (INIS)

    Demchishin, A.V.; Gnilitskyi, I.; Orazi, L.; Ascari, A.

    2015-01-01

    Highlights: • Multilayer coatings of Ti/Fe, Ti/Al, Ti/Cu and Ti/Zr are generated. • Microstructure and morphology of the different systems are investigated. • XR diffraction analysis was performed to investigate phases composition. • Effects of inter metallic phases on microhardess are investigated. • Correlations between parameters and layer thickness are outlined. - Abstract: The microstructure, phase composition and microhardness of multilayered Ti/Al, Ti/Cu, Ti/Fe and Ti/Zr condensates produced on stainless steel substrates via vacuum-arc evaporation of pure metals were studied. The sublayer periods (Λ) were regulated in the range 80–850 nm by varying the vacuum discharge current and the duration of the successive depositions of metallic plasma onto the substrates while maintaining the total deposition time constant. The regularity of the obtained nanostructures was investigated by scanning and transmission electron microscopy while phase compositions were identified with X-ray diffraction (XRD) analysis in order to evidence the presence of interdiffusion and the amount of intermetallics. Condensates cross sections were mechanically characterized by means of microhardness tests. Measurements were correlated to the periods and to the presence of intermetallics

  9. Structure, phase composition and microhardness of vacuum-arc multilayered Ti/Al, Ti/Cu, Ti/Fe, Ti/Zr nano-structures with different periods

    Energy Technology Data Exchange (ETDEWEB)

    Demchishin, A.V., E-mail: ademch@meta.ua [Institute of Problems in Material Science, NASU, Kiev (Ukraine); Gnilitskyi, I., E-mail: iaroslav.gnilitskyi@unimore.it [DISMI – Department of Sciences and Methods for Engineering, University of Modena and Reggio Emilia, Reggio Emilia (Italy); Orazi, L., E-mail: leonardo.orazi@unimore.it [DISMI – Department of Sciences and Methods for Engineering, University of Modena and Reggio Emilia, Reggio Emilia (Italy); Ascari, A., E-mail: a.ascari@unibo.it [DIN – Department of Industrial Engineering, University of Bologna, Bologna (Italy)

    2015-07-01

    Highlights: • Multilayer coatings of Ti/Fe, Ti/Al, Ti/Cu and Ti/Zr are generated. • Microstructure and morphology of the different systems are investigated. • XR diffraction analysis was performed to investigate phases composition. • Effects of inter metallic phases on microhardess are investigated. • Correlations between parameters and layer thickness are outlined. - Abstract: The microstructure, phase composition and microhardness of multilayered Ti/Al, Ti/Cu, Ti/Fe and Ti/Zr condensates produced on stainless steel substrates via vacuum-arc evaporation of pure metals were studied. The sublayer periods (Λ) were regulated in the range 80–850 nm by varying the vacuum discharge current and the duration of the successive depositions of metallic plasma onto the substrates while maintaining the total deposition time constant. The regularity of the obtained nanostructures was investigated by scanning and transmission electron microscopy while phase compositions were identified with X-ray diffraction (XRD) analysis in order to evidence the presence of interdiffusion and the amount of intermetallics. Condensates cross sections were mechanically characterized by means of microhardness tests. Measurements were correlated to the periods and to the presence of intermetallics.

  10. Characterization of Ni ferrites powders prepared by plasma arc discharge process

    Science.gov (United States)

    Safari, A.; Gheisari, Kh.; Farbod, M.

    2017-01-01

    The aim of this work was to synthesize a single-phase spinel structure from a mixture of zinc, iron and nickel powders by plasma arc discharge method. A mixture of zinc, iron and nickel powders with the appropriate molar ratio was prepared and formed into a cylindrical shape. The synthesis process was performed in air, oxygen and argon atmospheres with the applied arc current of 400 A and pressure of 1 atm. After establishing an arc between the electrodes, the produced powders were collected and their structure and magnetic properties were examined by XRD and VSM, respectively. ZnO as an impurity was appeared in the as-produced powders owing to the high reactivity of zinc atoms, preventing the formation of Ni-Zn ferrite. A pure spinel structure with the highest saturation magnetization (43.8 emu/g) was observed as zinc powders removed completely from the initial mixture. Morphological evaluations using field emission scanning electron microscopy showed that the mean size of fabricated nanoparticles was in the range 100-200 nm and was dependent on the production conditions.

  11. Effect of Coil Current on the Properties of Hydrogenated DLC Coatings Fabricated by Filtered Cathodic Vacuum Arc Technique

    Science.gov (United States)

    Liao, Bin; Ouyang, Xiaoping; Zhang, Xu; Wu, Xianying; Bian, Baoan; Ying, Minju; Jianwu, Liu

    2018-01-01

    We successfully prepared hydrogenated DLC (a-C:H) with a thickness higher than 25 μm on stainless steel using a filtered cathode vacuum arc (FCVA) technique. The structural and mechanical properties of DLC were systematically analyzed using different methods such as x-ray photoelectron spectroscopy, Raman spectroscopy, scanning electron microscopy, Vickers hardness, nanohardness, and friction and wear tests. The effect of coil current on the arc voltage, ion current, and mechanical properties of resultant films was systematically investigated. The novelty of this study is the fabrication of DLC with Vickers hardness higher than 1500 HV, in the meanwhile with the thickness higher than 30 μm through varying the coil current with FCVA technique. The results indicated that the ion current, deposition rate, friction coefficient, and Vickers hardness of DLC were significantly affected by the magnetic field inside the filtered duct.

  12. Development of high efficiency Versatile Arc Discharge Ion Source at CERN ISOLDE.

    Science.gov (United States)

    Penescu, L; Catherall, R; Lettry, J; Stora, T

    2010-02-01

    We report here recent developments of Forced Electron Beam Induced Arc Discharge (FEBIAD) ion sources at the ISOLDE radioactive ion beam facility, hosted at the European Organization for Nuclear Research (CERN). As a result of the propositions to improve the ionization efficiency, two FEBIAD prototypes have been produced and successfully tested in 2008. Off-line studies showed that the 1+ ionization efficiencies for noble gases are 5-20 times larger than with the standard ISOLDE FEBIAD ion sources and reach 60% for radon, which allowed the identification at ISOLDE of (229)Rn, an isotope that had never previously been observed in the laboratory. A factor of 3 increase is also expected for the ionization efficiency of the other elements. The experimental and theoretical methodology is presented. The theoretical model, which gives precise insights on the processes affecting the ionization, is used to design optimal sources (grouped under the name of VADIS--Versatile Arc Discharge Ion Source) for the different chemical classes of the produced isotopes, as already demonstrated for the noble gases.

  13. Degradation of gas-liquid gliding arc discharge on Acid Orange II

    International Nuclear Information System (INIS)

    Yan, J.H.; Liu, Y.N.; Bo, Zh.; Li, X.D.; Cen, K.F.

    2008-01-01

    The effects of pH value, initial concentration of dye solution and temperature on the degradation efficiency of Acid Orange II (AO7) using gas-liquid gliding arc discharge were investigated. The influences of pH value and temperature on degradation efficiency were not apparent. Increasing initial solution concentration caused the decrease of degradation rate and the increase of absolute degradation quantity. Considering energy efficiency and absolute degradation quantity, the gas-liquid gliding arc discharge is fit for treating high concentration organic wastewater. A possible mineralization pathway was proposed through the analysis of intermediate products detected by gas chromatograph coupled with mass spectrophotometer (GC-MS) and ion chromatograph (IC). Hydroxyl radicals reacted with the azo linkage-bearing carbon of a hydroxy-substituted ring, leading to the cleavage of -C-N- and degradation of AO7. The solution biodegradability was significantly improved (BOD 5 /COD from 0.02 to 0.43). The toxicity of intermediate products was lower than that of the initial Acid Orange II

  14. Synthesis and structural, magnetic and magnetotransport properties of permalloy powders containing nanoparticles prepared by arc discharge

    International Nuclear Information System (INIS)

    Prakash, Tushara; Williams, Grant V.M.; Kennedy, John; Murmu, Peter P.; Leveneur, Jérôme; Chong, Shen V.; Rubanov, Sergey

    2014-01-01

    Highlights: • New method of arc discharge used to synthesise permalloy containing nanoparticles. • The highest quality powders were made using a 78% Ni permalloy rod in N 2 . • The Saturation moment was slightly less and the coercive field was low (3 mT). • MR contributions from the spin-dependent tunneling between the particles. - Abstract: We report the synthesis of permalloy powders that were made using an arc-discharge method and with 78% or 45% Ni concentrations in N 2 or Ar. Our research was motivated by the fact that magnetic nanoparticles displaying large magnetoresistances are useful for magnetic field sensors applications. The permalloy powders contained some nanoparticles and the particle sizes ranged from 10 nm to ∼20 μm. The highest quality powders were made using a 78% Ni permalloy rod in N 2 where the coercivity was low (0.3 mT) and the saturation moment per formula unit was slightly less than that expected for the bulk compound. Magnetoresistance was observed in a cold pressed pellet where it is likely to be dominated by the ordinary magnetoresistance and spin-dependent tunneling between the particles

  15. Conditioning of SST-1 Tokamak Vacuum Vessel by Baking and Glow Discharge Cleaning

    International Nuclear Information System (INIS)

    Khan, Ziauddin; George, Siju; Semwal, Pratibha; Dhanani, Kalpeshkumar R.; Pathan, Firozkhan S.; Paravastu, Yuvakiran; Raval, Dilip C.; Babu, Gattu Ramesh; Khan, Mohammed Shoaib; Pradhan, Subrata

    2016-01-01

    Highlights: • SST-1 Tokamak was successfully commissioned. • Vacuum vessel was pumped down to 4.5 × 10"–"8 mbar after baking and continuous GDC. • GDC reduced the water vapour by additional 57% while oxygen was reduced by 50%. • Under this condition, an initial plasma breakdown with current of 40 kA for 75 ms was achieved. - Abstract: Steady-state Superconducting Tokamak (SST-1) vacuum vessel (VV) adopts moderate baking at 110 ± 10 °C and the limiters baking at 250 ± 10 °C for ∼ 200 h followed by glow discharge cleaning in hydrogen (GDC-H) with 0.15 A/m"2 current density towards its conditioning prior to plasma discharge experiment. The baking in SST-1 reduces the water (H_2O) vapor by 95% and oxygen (O_2) by 60% whereas the GDC reduces the water vapor by an additional 57% and oxygen by another 50% as measured with residual gas analyzer. The minimum breakdown voltage for H-GDC in SST-1 tokamak was experimentally observed to 300 V at 8 mbar cm. As a result of these adherences, SST-1 VV achieves an ultimate of 4.5 × 10"−"8 mbar with two turbo-molecular pumps with effective pumping speed of 3250 l/s. In the last campaign, SST-1 has achieved successful plasma breakdown, impurity burn through and a plasma current of ∼ 40 kA for 75 ms.

  16. IN-SITU EXPERIMENTS OF VACUUM DISCHARGE USING SCANNING ELECTRON MICROSCOPES

    CERN Document Server

    Muranaka, T; Leifer, K; Ziemann, V

    2011-01-01

    The fundamental understanding of vacuum discharge mechanisms and induced surface damage is indispensable for the CLIC feasibility study. We have been conducting dc sparc experiments inside a Scanning Electron Microscope (SEM) at Uppsala university in order to investigate localized breakdown phenomena. By using a SEM, we achieve the resolution of the electron probe in the few-nm range, which is of great advantage as the surface roughness of the polished accelerating structures is in the same scale. The high accelerating field of 1 GV/m is realized by biasing an electrode with 1 kV set above the sample with a gap of sub μm. Furthermore, a second SEM equipped with a Focused Ion Beam (FIB) is used to modify the topography of sample surfaces thus the geometrical dependence of field emissions and vacuum discharges can be studied. The FIB can be used for the surface damage analysis as well. We have demonstrated subsurface damage observations by using FIB to sputter a rectangular recess into the sample in the breakd...

  17. A comparison of the microstructures and electrochemical capacitive properties of 2 graphenes prepared by arc discharge method and chemical method

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, H.; Yang, Y. [Research Inst. of Chemical Defense, Beijing (China); Univ. of Science and Technology, Beijing (China); Cao, G.; Xu, B. [Research Inst. of Chemical Defense, Beijing (China)

    2010-07-01

    In this study, 2 kinds of graphene materials were prepared using both arc discharge and chemical methods. The pore structures and electrochemical capacitive properties of the materials were investigated. A mesopore structure was obtained for the graphene prepared using the arc discharge method, with a capacitance of 12.9 F/g and a high rate capability when used in electrochemical applications. The graphene prepared with the chemical method demonstrated a more highly developed micropore structure and capacitances greater than 70 F/g. However, rate performance for the graphene was normal. 2 figs.

  18. Vacuum arc plasma deposition of thin titanium dioxide films on silicone elastomer as a functional coating for medical applications

    Energy Technology Data Exchange (ETDEWEB)

    Boudot, Cécile, E-mail: cecile.boudot@tum.de [Technical University of Munich, Department of Mechanical Engineering, Boltzmannstraße 15, D-85748 Garching bei München (Germany); Kühn, Marvin; Kühn-Kauffeldt, Marina; Schein, Jochen [Institute for Plasma Technology and Mathematics, University of Federal Armed Forces Munich, Werner-Heisenberg-Weg 39, D-85577 Neubiberg (Germany)

    2017-05-01

    Silicone elastomer is a promising material for medical applications and is widely used for implants with blood and tissue contact. However, its strong hydrophobicity limits adhesion of tissue cells to silicone surfaces, which can impair the healing process. To improve the biological properties of silicone, a triggerless pulsed vacuum cathodic arc plasma deposition technique was applied to deposit titanium dioxide (TiO{sub 2}) films onto the surface. Scanning electron microscopy, atomic force microscopy, X-ray photoelectron spectroscopy, Raman spectroscopy and contact angle measurements were used for coating characterization. Deposited films were about 150 nm thick and exhibited good adhesion to the underlying silicone substrate. Surface wettability and roughness both increased after deposition of the TiO{sub 2} layer. In addition, cell-biological investigations demonstrated that the in-vitro cytocompatibility of TiO{sub 2}-coated samples was greatly improved without impacting silicone's nontoxicity. For validation of use in medical devices, further investigations were conducted and demonstrated stability of surface properties in an aqueous environment for a period of 68 days and the coating's resistance to several sterilization methods. - Highlights: • Vacuum arc plasma was applied to deposit titanium dioxide films onto silicone. • Thickness, roughness and composition of the films were determined. • Cytocompatibility of coated silicone elastomer is greatly improved. • Films have good adhesion to the substrate and are stable, non-toxic and sterilizable.

  19. Solidification observations and sliding wear behavior of vacuum arc melting processed Ni–Al–TiC composites

    International Nuclear Information System (INIS)

    Karantzalis, A.E.; Lekatou, A.; Tsirka, K.

    2012-01-01

    Monolithic Ni 3 Al and Ni–25 at.%Al intermetallic matrix TiC-reinforced composites were successfully produced by vacuum arc melting. TiC crystals were formed through a dissolution–reprecipitation mechanism and their final morphology is explained by means of a) Jackson's classical nucleation and growth phenomena and b) solidification rate considerations. The TiC presence altered the matrix microconstituents most likely due to specific melt–particle interactions and crystal plane epitaxial matching. TiC particles caused a significant decrease on the specific wear rate of the monolithic Ni 3 Al alloy and the possible wear mechanisms are approached by means of a) surface oxidation, b) crack/flaws formation, c) material detachment and d) debris–counter surfaces interactions. - Highlights: ► Vacuum arc melting (VAM) of Ni-Al based intermetallic matrix composite materials. ► Solidification phenomena examination. ► TiC crystal formation and growth mechanisms. ► Sliding wear examination.

  20. Generation of metallic arc spectrum of pumping discharge of XeCl laser; XeCl ekishima laser reiki hoden ni okeru arc iko to kinzoku supekutoru no hassei

    Energy Technology Data Exchange (ETDEWEB)

    Koike, H.; Yukimura, K. [Doshisha University, Kyoto (Japan)

    1997-12-20

    An arc generation of a long-pulse spiker-sustainer excimer laser with about 250ns of pulse width , is discussed by using time-varying spectroscopic method. First arcing occurs during a main discharge for laser excitation and shows XeII spectrum, while a glow-like discharge represents only XeI spectrum, the metallic spectrum such as Nil caused by vaporization of electrode material begins to appear just after the termination of the main discharge. Second arcing occurs after about 2{mu}s, which brings strong intensity of Nil spectrum. It means that the reignition arc might be produced in a metallic vapor that appears during the main discharge. Accordingly, it is concluded that the reignition arc is inherently metallic, which is different from the main arc with rare gas plasma. 9 refs., 9 figs.

  1. Space and time resolved observations of hot spots dynamics in a vacuum spark discharge

    International Nuclear Information System (INIS)

    Chuaqui, H.; Favre, M.; Saavedra, R.; Wyndham, E.

    1996-01-01

    Experimental observations of the plasma formations in a vacuum spark discharge are presented. A low power Nd:YAG laser pulse incident onto a titanium cathode initiates the discharge. The evolution of the titanium plasma electron density and temperature is followed both in the visible and the soft X-ray part of the spectrum. The former uses a novel micro holographic interferometric technique permitting a spatial resolution better than 20 μm. The probing beam is a 6 ns frequency doubled Nd:YAG laser. The latter emission is resolved using a number of different methods. The spatial information is derived from a 1 ns multi framing camera X-ray camera which projects the plasma image using four different slit wire pinhole images and six pinhole images, each aperture being filtered differently. The temporal evolution of the emission of each discharge is followed using several silicon PIN diodes. The x-ray spectrum is unfolded from the filter and detector response and interpreted using a collisional radiative package. The hot spots are seen to form in a submillimeter pinch stemming from the incident laser focus which has a life time about 20 ns. The hot spots are much shorter events, reaching substantially higher densities, but involve only part of the line density of the pinch column. (author). 4 figs., 8 refs

  2. Space and time resolved observations of hot spots dynamics in a vacuum spark discharge

    Energy Technology Data Exchange (ETDEWEB)

    Chuaqui, H; Favre, M; Saavedra, R; Wyndham, E [Universidad Catolica de Chile, Santiago (Chile). Facultad de Fisica; Choi, P; Dumitrescu-Zoita, C [Ecole Polytechnique, Palaiseau (France). Laboratoire de Physique des Milieux Ionises; Soto, L [Comision Chilena de Energia Nuclear, Santiago (Chile)

    1997-12-31

    Experimental observations of the plasma formations in a vacuum spark discharge are presented. A low power Nd:YAG laser pulse incident onto a titanium cathode initiates the discharge. The evolution of the titanium plasma electron density and temperature is followed both in the visible and the soft X-ray part of the spectrum. The former uses a novel micro holographic interferometric technique permitting a spatial resolution better than 20 {mu}m. The probing beam is a 6 ns frequency doubled Nd:YAG laser. The latter emission is resolved using a number of different methods. The spatial information is derived from a 1 ns multi framing camera X-ray camera which projects the plasma image using four different slit wire pinhole images and six pinhole images, each aperture being filtered differently. The temporal evolution of the emission of each discharge is followed using several silicon PIN diodes. The x-ray spectrum is unfolded from the filter and detector response and interpreted using a collisional radiative package. The hot spots are seen to form in a submillimeter pinch stemming from the incident laser focus which has a life time about 20 ns. The hot spots are much shorter events, reaching substantially higher densities, but involve only part of the line density of the pinch column. (author). 4 figs., 8 refs.

  3. Post-arc current simulation based on measurement in vacuum circuit breaker with a one-dimensional particle-in-cell model

    Science.gov (United States)

    Jia, Shenli; Mo, Yongpeng; Shi, Zongqian; Li, Junliang; Wang, Lijun

    2017-10-01

    The post-arc dielectric recovery process has a decisive effect on the current interruption performance in a vacuum circuit breaker. The dissipation of residual plasma at the moment of current zero under the transient recovery voltage, which is the first stage of the post-arc dielectric recovery process and forms the post-arc current, has attracted many concerns. A one-dimensional particle-in-cell model is developed to simulate the measured post-arc current in the vacuum circuit breaker in this paper. At first, the parameters of the residual plasma are estimated roughly by the waveform of the post-arc current which is taken from measurements. After that, different components of the post-arc current, which are formed by the movement of charged particles in the residual plasma, are discussed. Then, the residual plasma density is adjusted according to the proportion of electrons and ions absorbed by the post-arc anode derived from the particle-in-cell simulation. After this adjustment, the post-arc current waveform obtained from the simulation is closer to that obtained from measurements.

  4. Electroless nickel plating of arc discharge synthesized carbon nanotubes for metal matrix composites

    Science.gov (United States)

    Jagannatham, M.; Sankaran, S.; Prathap, Haridoss

    2015-01-01

    Electroless nickel (EN) plating was performed on arc discharge synthesized multiwalled carbon nanotubes for various deposition times. X-ray diffraction (XRD), Transmission electron microscopy (TEM), and Raman spectroscopy characterization techniques are used to identify the presence of nickel deposition on the carbon nanotubes (CNTs) and the degree of graphitization. The results indicate that impurities are less in the purified CNTs as compared to raw carbon soot. Increasing deposition time up to 60 min increases uniform deposition of nickel throughout the length of the CNTs. However, for deposition time longer than 60 min, nickel particles are seen separated from the surface of the CNTs. Uniformly coated nickel CNTs throughout their length are potential candidates for reinforcements in composite materials. Magnetic properties of the nickel coated CNTs, with deposition time of 30 and 60 min were also evaluated. The magnetic saturation of nickel coated CNTs with deposition time of 30 min is less compared to nickel coated CNTs with deposition time of 60 min.

  5. Growth of linear Ni-filled carbon nanotubes by local arc discharge in liquid ethanol

    Energy Technology Data Exchange (ETDEWEB)

    Sagara, Takuya [Department of Electric Engineering, Graduated School of Science and Technology, Nihon University, 1-8-14 Surugadai Kanda, Chiyoda, Tokyo 101-8308 (Japan); Kurumi, Satoshi [Department of Electric Engineering, College of Science and Technology, Nihon University, 1-8-14 Surugadai Kanda, Chiyoda, Tokyo 101-8308 (Japan); Suzuki, Kaoru, E-mail: kaoru@ele.cst.nihon-u.ac.jp [Department of Electric Engineering, College of Science and Technology, Nihon University, 1-8-14 Surugadai Kanda, Chiyoda, Tokyo 101-8308 (Japan)

    2014-02-15

    The cylindrical geometry of carbon nanotubes (CNTs) allows them to be filled with metal catalysts; the resulting metal-filled CNTs possess different properties depending on the filler metal. Here we report the synthesis of Ni-filled CNTs in which Ni is situated linearly and homogeneously by local arc discharge in liquid ethanol. The structural characteristics of synthesized Ni-filled CNTs were determined by transmission electron microscopy (TEM), and the relationship between pyrolysis conditions and the length and diameter of Ni-filled CNTs was examined. The encapsulated Ni was identified by a TEM-equipped energy-dispersive X-ray spectroscope and found to have a single-crystal fcc structure by nano-beam diffraction. The features of linear Ni-filled CNT are expected to be applicable to probes for magnetic force microscopy.

  6. Study of Ag and Au Nanoparticles Synthesized by Arc Discharge in Deionized Water

    Directory of Open Access Journals (Sweden)

    Der-Chi Tien

    2010-01-01

    Full Text Available The paper presents a study of Ag and Au nanofluids synthesized by the arc discharge method (ADM in deionized water. The metallic Ag nanoparticle (Ag0 and ionic Ag (Ag+ have played an important role in the battle against germs which are becoming more drug-resistant every year. Our study indicates that Ag nanoparticle suspension (SNPS fabricated by using ADM without added surfactants exclusively contains the metallic Ag nanoparticle and ionic Ag. Besides that, the ADM in deionized water has also been employed for the fabrication process of Au nanoparticles. The experimental results indicate that the prepared Ag nanoparticles can react with the dissolved H2CO3 in deionized water, leading to the formation of Ag2CO3. Significantly different to Ag, the prepared Au nanoparticles with their surfaces bonded by oxygen are suspended in deionized water by the formation of hydrogen bonded with the neighboring water molecules.

  7. Carbon Nano-particle Synthesized by Pulsed Arc Discharge Method as a Light Emitting Device

    Science.gov (United States)

    Ahmadi, Ramin; Ahmadi, Mohamad Taghi; Ismail, Razali

    2018-04-01

    Owing to the specific properties such as high mobility, ballistic carrier transport and light emission, carbon nano-particles (CNPs) have been employed in nanotechnology applications. In the presented work, the CNPs are synthesized by using the pulsed arc discharge method between two copper electrodes. The rectifying behaviour of produced CNPs is explored by assuming an Ohmic contact between the CNPs and the electrodes. The synthesized sample is characterized by electrical investigation and modelling. The current-voltage (I-V) relationship is investigated and bright visible light emission from the produced CNPs was measured. The electroluminescence (EL) intensity was explored by changing the distance between two electrodes. An incremental behaviour on EL by a resistance gradient and distance reduction is identified.

  8. Synthesis and electrochemical properties of silicon nanosheets by DC arc discharge for lithium-ion batteries.

    Science.gov (United States)

    Yu, Xiuhong; Xue, Fanghong; Huang, Hao; Liu, Chunjing; Yu, Jieyi; Sun, Yuejun; Dong, Xinglong; Cao, Guozhong; Jung, Youngguan

    2014-06-21

    Two-dimensional (2D) ultrathin silicon nanosheets (Si NSs) were synthesized by DC arc discharge method and investigated as anode material for Li-ion batteries. The 2D ultrathin characteristics of Si NSs is confirmed by means of transmission electron microscopy (TEM) and atomic force microscopy (AFM). The average size of Si NSs is about 20 nm, with thickness less than 2.5 nm. The characteristic Raman peak of Si NSs is found to have an appreciable (20 nm) shift to low frequency, presumably due to the size effect. The synergistic effects of Ar(+) and H(+) lead to 2D growth of Si NSs under high temperature and energy. Electrochemical analyses reveal that Si NSs anode possesses stable cycling performance and fast diffusion of Li-ions with insertion/extraction processes. Such Si NSs might be a promising candidate for anode of Li-ion batteries.

  9. Instantaneous imaging of ozone in a gliding arc discharge using photofragmentation laser-induced fluorescence

    Science.gov (United States)

    Larsson, Kajsa; Hot, Dina; Gao, Jinlong; Kong, Chengdong; Li, Zhongshan; Aldén, Marcus; Bood, Joakim; Ehn, Andreas

    2018-04-01

    Ozone vapor, O3, is here visualized in a gliding arc discharge using photofragmentation laser-induced fluorescence. Ozone is imaged by first photodissociating the O3 molecule into an O radical and a vibrationally hot O2 fragment by a pump photon. Thereafter, the vibrationally excited O2 molecule absorbs a second (probe) photon that further transits the O2-molecule to an excited electronic state, and hence, fluorescence from the deexcitation process in the molecule can be detected. Both the photodissociation and excitation processes are achieved within one 248 nm KrF excimer laser pulse that is formed into a laser sheet and the fluorescence is imaged using an intensified CCD camera. The laser-induced signal in the vicinity of the plasma column formed by the gliding arc is confirmed to stem from O3 rather than plasma produced vibrationally hot O2. While both these products can be produced in plasmas a second laser pulse at 266 nm was utilized to separate the pump- from the probe-processes. Such arrangement allowed lifetime studies of vibrationally hot O2, which under these conditions were several orders of magnitude shorter than the lifetime of plasma-produced ozone.

  10. Highly zone-dependent synthesis of different carbon nanostructures using plasma-enhanced arc discharge technique

    Energy Technology Data Exchange (ETDEWEB)

    Kumar, Rajesh, E-mail: rajeshbhu1@gmail.com [Yonsei University, Department of Materials Science & Engineering (Korea, Republic of); Singh, Rajesh Kumar, E-mail: rksbhu@gmail.com [Banaras Hindu University, Department of Applied Physics, Indian Institute of Technology (India); Dubey, Pawan Kumar [University of Allahabad, Nanotechnology Application Centre (India); Yadav, Ram Manohar [Rice University, Department of Materials Science and Nano Engineering (United States); Singh, Dinesh Pratap [Universidad de Santiago de Chile, Departamento de Física (Chile); Tiwari, R. S.; Srivastava, O. N. [Banaras Hindu University, Department of Physics (India)

    2015-01-15

    Three kinds of carbon nanostructures, i.e., graphene nanoflakes (GNFs), multi walled carbon nanotubes (MWCNTs), and spherical carbon nanoparticles (SCNPs) were comparatively investigated in one run experiment. These carbon nanostructures are located at specific location inside the direct current plasma-assisted arc discharge chamber. These carbon nanomaterials have been successfully synthesized using graphite as arcing electrodes at 400 torr in helium (He) atmosphere. The SCNPs were found in the deposits formed on the cathode holder, in which highly curled graphitic structure are found in majority. The diameter varies from 20 to 60 nm and it also appears that these particles are self-assembled to each other. The MWCNTs with the diameter of 10–30 nm were obtained which were present inside the swelling portion of cathode deposited. These MWCNTs have 14–18 graphitic layers with 3.59 Å interlayer spacing. The GNFs have average lateral sizes of 1–5 μm and few of them are stacked layers and shows crumpled like structure. The GNFs are more stable at low temperature (low mass loss) but SCNPs have low mass loss at high temperature.

  11. UV and humidity sensing properties of ZnO nanorods prepared by the arc discharge method

    International Nuclear Information System (INIS)

    Fang, F; Futter, J; Markwitz, A; Kennedy, J

    2009-01-01

    The UV and humidity sensing properties of ZnO nanorods prepared by arc discharge have been studied. Scanning electron microscopy and photoluminescence spectroscopy were carried out to analyze the morphology and optical properties of the as-synthesized ZnO nanorods. Proton induced x-ray emission was used to probe the impurities in the ZnO nanorods. A large quantity of high purity ZnO nanorod structures were obtained with lengths of 0.5-1 μm. The diameters of the as-synthesized ZnO nanorods were found to be between 40 and 400 nm. The nanorods interlace with each other, forming 3D networks which make them suitable for sensing application. The addition of a polymeric film-forming agent (BASF LUVISKOL VA 64) improved the conductivity, as it facilitates the construction of conducting networks. Ultrasonication helped to separate the ZnO nanorods and disperse them evenly through the polymeric agent. Improved photoconductivity was measured for a ZnO nanorod sensor annealed in air at 200 deg. C for 30 min. The ZnO nanorod sensors showed a UV-sensitive photoconduction, where the photocurrent increased by nearly four orders of magnitude from 2.7 x 10 -10 to 1.0 x 10 -6 A at 18 V under 340 nm UV illumination. High humidity sensitivity and good stability were also measured. The resistance of the ZnO nanorod sensor decreased almost linearly with increasing relative humidity (RH). The resistance of the ZnO nanorods changed by approximately five orders of magnitude from 4.35 x 10 11 Ω in dry air (7% RH) to about 4.95 x 10 6 Ω in 95% RH air. It is experimentally demonstrated that ZnO nanorods obtained by the arc discharge method show excellent performance and promise for applications in both UV and humidity sensors.

  12. Absolute calibration of a hydrogen discharge lamp in the vacuum ultraviolet

    Science.gov (United States)

    Nealy, J. E.

    1975-01-01

    A low-pressure hydrogen discharge lamp was calibrated for radiant intensity in the vacuum ultraviolet spectral region on an absolute basis and was employed as a laboratory standard source in spectrograph calibrations. This calibration was accomplished through the use of a standard photodiode detector obtained from the National Bureau of Standards together with onsite measurements of spectral properties of optical components used. The stability of the light source for use in the calibration of vacuum ultraviolet spectrographs and optical systems was investigated and found to be amenable to laboratory applications. The lamp was studied for a range of operating parameters; the results indicate that with appropriate peripheral instrumentation, the light source can be used as a secondary laboratory standard source when operated under preset controlled conditions. Absolute intensity measurements were recorded for the wavelengths 127.7, 158.0, 177.5, and 195.0 nm for a time period of over 1 month, and the measurements were found to be repeatable to within 11 percent.

  13. An intense lithium ion beam source using vacuum baking and discharge cleaning techniques

    International Nuclear Information System (INIS)

    Moschella, J.J.; Kusse, B.R.; Longfellow, J.P.; Olson, J.C.

    1991-01-01

    We have developed a high-purity, intense, lithium ion beam source which operates at 500 kV and 120 A/cm 2 with pulse widths of 125 ns full width half maximum. The beams were generated using a lithium chloride anode in planar magnetically insulated geometry. We have found that the combination of vacuum baking of the anode at 250 degree C followed by the application of 100 W of pure argon, steady-state, glow discharge cleaning reduced the impurity concentration in the beam to approximately 10% (components other than chlorine or lithium were considered impurities). Although the impurities were low, the concentration of chlorine in the 1+ and 2+ charge states was significant (∼25%). The remaining 65% of the beam consisted of Li + ions. Without the special cleaning process, over half the beam particles were impurities. It was determined that these impurities entered the beam at the anode surface but came originally from material in the vacuum chamber. After the cleaning process, recontamination was observed to occur in approximately 6 min. This long recontamination time, which was much greater than the expected monolayer formation time, was attributed to the elevated temperature of the anode. We also compared the electrical characteristics of the beams produced by LiCl anodes to those generated by a standard polyethylene proton source. In contrast to the polyethylene anode, the LiCl source exhibited a higher impedance, produced beams of lower ion current efficiency and had longer turn on times

  14. Conditioning of SST-1 Tokamak Vacuum Vessel by Baking and Glow Discharge Cleaning

    Energy Technology Data Exchange (ETDEWEB)

    Khan, Ziauddin, E-mail: ziauddin@ipr.res.in; George, Siju; Semwal, Pratibha; Dhanani, Kalpeshkumar R.; Pathan, Firozkhan S.; Paravastu, Yuvakiran; Raval, Dilip C.; Babu, Gattu Ramesh; Khan, Mohammed Shoaib; Pradhan, Subrata

    2016-02-15

    Highlights: • SST-1 Tokamak was successfully commissioned. • Vacuum vessel was pumped down to 4.5 × 10{sup –8} mbar after baking and continuous GDC. • GDC reduced the water vapour by additional 57% while oxygen was reduced by 50%. • Under this condition, an initial plasma breakdown with current of 40 kA for 75 ms was achieved. - Abstract: Steady-state Superconducting Tokamak (SST-1) vacuum vessel (VV) adopts moderate baking at 110 ± 10 °C and the limiters baking at 250 ± 10 °C for ∼ 200 h followed by glow discharge cleaning in hydrogen (GDC-H) with 0.15 A/m{sup 2} current density towards its conditioning prior to plasma discharge experiment. The baking in SST-1 reduces the water (H{sub 2}O) vapor by 95% and oxygen (O{sub 2}) by 60% whereas the GDC reduces the water vapor by an additional 57% and oxygen by another 50% as measured with residual gas analyzer. The minimum breakdown voltage for H-GDC in SST-1 tokamak was experimentally observed to 300 V at 8 mbar cm. As a result of these adherences, SST-1 VV achieves an ultimate of 4.5 × 10{sup −8} mbar with two turbo-molecular pumps with effective pumping speed of 3250 l/s. In the last campaign, SST-1 has achieved successful plasma breakdown, impurity burn through and a plasma current of ∼ 40 kA for 75 ms.

  15. Direct evidence of departure from local thermodynamic equilibrium in a free-burning arc-discharge plasma

    International Nuclear Information System (INIS)

    Snyder, S.C.; Lassahn, G.D.; Reynolds, L.D.

    1993-01-01

    Radial profiles of gas temperature, electron temperature, and electron density were measured in a free-burning atmospheric-pressure argon arc-discharge plasma using line-shape analysis of scattered laser light. This method yields gas temperature, electron temperature, and electron density directly, with no reliance on the assumption of local thermodynamic equilibrium (LTE). Our results show a significant departure from LTE in the center of the discharge, contrary to expectations

  16. Microplasma discharge vacuum ultraviolet photoionization source for atmospheric pressure ionization mass spectrometry.

    Science.gov (United States)

    Symonds, Joshua M; Gann, Reuben N; Fernández, Facundo M; Orlando, Thomas M

    2014-09-01

    In this paper, we demonstrate the first use of an atmospheric pressure microplasma-based vacuum ultraviolet (VUV) photoionization source in atmospheric pressure mass spectrometry applications. The device is a robust, easy-to-operate microhollow cathode discharge (MHCD) that enables generation of VUV photons from Ne and Ne/H(2) gas mixtures. Photons were detected by excitation of a microchannel plate detector and by analysis of diagnostic sample ions using a mass spectrometer. Reactive ions, charged particles, and metastables produced in the discharge were blocked from entering the ionization region by means of a lithium fluoride window, and photoionization was performed in a nitrogen-purged environment. By reducing the output pressure of the MHCD, we observed heightened production of higher-energy photons, making the photoionization source more effective. The initial performance of the MHCD VUV source has been evaluated by ionizing model analytes such as acetone, azulene, benzene, dimethylaniline, and glycine, which were introduced in solid or liquid phase. These molecules represent species with both high and low proton affinities, and ionization energies ranging from 7.12 to 9.7 eV.

  17. Filling the vacuum chamber of a technological system with homogeneous plasma using a stationary glow discharge

    International Nuclear Information System (INIS)

    Metel, A. S.; Grigoriev, S. N.; Melnik, Yu. A.; Panin, V. V.

    2009-01-01

    Experimental study of a glow discharge with electrostatic confinement of electrons is carried out in the vacuum chamber volume V ∼ 0.12 m 3 of a technological system 'Bulat-6' in argon pressure range 0.005-5 Pa. The chamber is used as a hollow cathode of the discharge with the inner surface area S ∼ 1.5 m 2 . It is equipped with two feedthroughs, which make it possible to immerse in the discharge plasma interchangeable anodes with surface area S a ranging from ∼0.001 to ∼0.1 m 2 , as well as floating electrodes isolated from both the chamber and the anode. Dependences of the cathode fall U c = 0.4-3 kV on the pressure p at a constant discharge current in the range I = 0.2-2 A proved that aperture of the electron escape out of the electrostatic trap is equal to the sum S o = S a + S f of the anode surface S a and the floating electrode surface S f . The sum S o defines the lower limit p o of the pressure range, in which U c is independent of p. At p o the cathode fall U c grows up dramatically, when the pressure decreases, and the pressure p tends to the limit p ex , which is in fact the discharge extinction pressure. At p ∼ p ex electrons emitted by the cathode and the first generation of fast electrons produced in the cathode sheath spend almost all their energy up to 3 keV on heating the anode and the floating electrode up to 600-800 o C and higher. In this case the gas in the chamber is being ionized by the next generations of electrons produced in the cathode sheath, their energy being one order of magnitude lower. When S a 1/2 S, where m is the electron mass and M is the ion mass, the anode may be additionally heated by plasma electrons accelerated by the anode fall of potential U a up to 0.5 kV.

  18. Nanodiamond embedded ta-C composite film by pulsed filtered vacuum arc deposition from a single target

    Science.gov (United States)

    Iyer, Ajai; Etula, Jarkko; Ge, Yanling; Liu, Xuwen; Koskinen, Jari

    2016-11-01

    Detonation Nanodiamonds (DNDs) are known to have sp3 core, sp2 shell, small size (few nm) and are gaining importance as multi-functional nanoparticles. Diverse methods have been used to form composites, containing detonation nanodiamonds (DNDs) embedded in conductive and dielectric matrices for various applications. Here we show a method, wherein DND-ta-C composite film, consisting of DNDs embedded in ta-C matrix have been co-deposited from the same cathode by pulsed filtered cathodic vacuum arc method. Transmission Electron Microscope analysis of these films revel the presence of DNDs embedded in the matrix of amorphous carbon. Raman spectroscopy indicates that the presence of DNDs does not adversely affect the sp3 content of DND-ta-C composite film compared to ta-C film of same thickness. Nanoindentation and nanowear tests indicate that DND-ta-C composite films possess improved mechanical properties in comparison to ta-C films of similar thickness.

  19. Mo-containing tetrahedral amorphous carbon deposited by dual filtered cathodic vacuum arc with selective pulsed bias voltage

    International Nuclear Information System (INIS)

    Pasaja, Nitisak; Sansongsiri, Sakon; Intarasiri, Saweat; Vilaithong, Thiraphat; Anders, Andre

    2007-01-01

    Metal-containing tetrahedral amorphous carbon films were produced by dual filtered cathodic vacuum arc plasma sources operated in sequentially pulsed mode. Negatively pulsed bias was applied to the substrate when carbon plasma was generated, whereas it was absent when the molybdenum plasma was presented. Film thickness was measured after deposition by profilometry. Glass slides with silver pads were used as substrates for the measurement of the sheet resistance. The microstructure and composition of the films were characterized by Raman spectroscopy and Rutherford backscattering, respectively. It was found that the electrical resistivity decreases with an increase of the Mo content, which can be ascribed to an increase of the sp 2 content and an increase of the sp 2 cluster size

  20. Improving the conductance of ZnO thin film doping with Ti by using a cathodic vacuum arc deposition process

    International Nuclear Information System (INIS)

    Wu, Chun-Sen; Lin, Bor-Tsuen; Jean, Ming-Der

    2011-01-01

    The Ti-doped ZnO films compared to un-doped ZnO films were deposited onto Corning XG glass substrates by using a cathodic vacuum arc deposition process in a mixture of oxygen and argon gases. The structural, electrical and optical properties of un-doped and Ti-doped ZnO films have been investigated. When the Ti target power is about 750 W, the incorporation of titanium atoms into zinc oxide films is obviously effective. Additionally, the resistivity of un-doped ZnO films is high and reduces to a value of 3.48 x 10 -3 Ω-cm when Ti is incorporated. The Ti doped in the ZnO films gave rise to the improvement of the conductivity of the films obviously. The Ti-doped ZnO films have > 85% transmittance in a range of 400-700 nm.

  1. Physical-mechanical properties of Ti-Al-N films, deposited from mixed two-component vacuum arc plasma stream

    International Nuclear Information System (INIS)

    Aksenov, D.S.; Aksenov, I.I.; Luchaninov, A.A.; Reshetnyak, E.N.; Strel'nitskij, V.E.; Tolmacheva, G.N.; Yurkov, S.A.

    2011-01-01

    Ti-Al-N films were obtained by vacuum arc system equipped with two-channel T-shaped magnetic filter. The films were deposited by mixing of filtered plasma streams from two sources with cathodes made of aluminium and titanium in nitrogen environment. An influence of aluminium concentration and substrate bias on structure, hardness and elastic modulus of deposited films was studied by X-ray diffraction analysis and nanoindentation techniques. It was found that coatings with aluminium content in range from 13 to 47 at. % are characterized by cubic nitride based on TiN with NaCl structure. An increase of Al content to 71 at. % leads to the formation of hexagonal AlN-based nitride with wurtzite-like structure. Maximum hardness of 35 GPa is observed in films with 47 at. % aluminium concentration and -100 V substrate bias. Elastic modulus falls off along with increase of Al content and negative substrate bias.

  2. Refusion of zircaloy scraps by VAR (vacuum arc remelting): preliminary results; Fusao de cavacos de zircaloy por VAR: resultados preliminares

    Energy Technology Data Exchange (ETDEWEB)

    Pereira, L.A.T.; Mucsi, C.S.; Sato, I.M.; Rossi, J.L.; Martinez, L.G., E-mail: lgallego@ipen.b [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil); Correa, H.P.S. [Universidade Federal do Mato Grosso do Sul (UFMS), Campo Grande, MS (Brazil); Orlando, M.T.D. [Universidade Federal do Espirito Santo (UFES), Vitoria, ES (Brazil)

    2010-07-01

    Fuel elements and structural components of the core of PWR nuclear reactors are made in zirconium alloys known as Zircaloy. Machining chips and shavings resulting from the manufacturing of these components can not be discarded as scrap, once these alloys are strategic materials for the nuclear area, have high costs and are not produced in Brazil on an industrial bases and, consequently, are imported for the manufacture of nuclear fuel. The reuse of Zircaloy chips has economic, strategic and environmental aspects. In this work is proposed a process for recycling Zircaloy scraps using a VAR (vacuum arc remelting) furnace in order to obtain ingots suitable for the manufacture of components of the reactors. The ingots obtained are being studied in order to verify the influence of processing on composition and microstructure of the remelted material. In this work are presented preliminary results of the composition of obtained ingots compared to start material and the resulting microstructure. (author)

  3. Effect of vacuum arc melting/casting parameters on shrinkage cavity/piping of austenitic stainless steel ingot

    International Nuclear Information System (INIS)

    Kamran, J.; Feroz, M.; Sarwar, M.

    2009-01-01

    Shrinkage cavity/piping at the end of the solidified ingot of steels is one of the most common casting problem in 316L austenitic stainless steel ingot, when consumable electrode is melted and cast in a water-cooled copper mould by vacuum arc re-melting furnace. In present study an effort has been made to reduce the size of shrinkage cavity/ piping by establishing the optimum value of hot topping process parameters at the end of the melting process. It is concluded that the shrinkage cavity/piping at the top of the solidified ingot can be reduced to minimum by adjusting the process parameters particularly the melting current density. (author)

  4. The effect of substrate bias on titanium carbide/amorphous carbon nanocomposite films deposited by filtered cathodic vacuum arc

    International Nuclear Information System (INIS)

    Zhang, Xu; Liang, Hong; Wu, Zhenglong; Wu, Xiangying; Zhang, Huixing

    2013-01-01

    The titanium carbide/amorphous carbon nanocomposite films have been deposited on silicon substrate by filtered cathodic vacuum arc (FCVA) technology, the effects of substrate bias on composition, structures and mechanical properties of the films are studied by scanning electron spectroscopy, X-ray diffraction and X-ray photoelectron spectroscopy and nano-indentation. The results show that the Ti content, deposition rate and hardness at first increase and then decrease with increasing the substrate bias. Maximum hardness of the titanium carbide/amorphous carbon nanocomposite film is 51 Gpa prepared at −400 V. The hardness enhancement may be attributed to the compressive stress and the fraction of crystalline TiC phase due to ion bombardment

  5. Simulation of convection-stabilized low-current glow and arc discharges in atmospheric-pressure air

    International Nuclear Information System (INIS)

    Naidis, G V

    2007-01-01

    A two-dimensional model of stationary convection-stabilized low-current glow and arc discharge columns in atmospheric-pressure air is developed which accounts for deviation of the plasma state from the local thermodynamic equilibrium (LTE). In addition to equations of energy, continuity and momentum (analogous to those used in LTE arc models), the non-LTE model includes balance equations for plasma species and for the vibrational energy of nitrogen molecules. The kinetic scheme is used which was developed recently for the simulation of low-current wall-stabilized discharges in air. Results of calculation of discharge parameters over a wide current range are presented. It is shown that the non-equilibrium effects are substantial at currents lower than ∼ 100 mA. The calculated plasma parameters agree with available experimental data

  6. Synthesis and characterization of Ti-Si-C-N nanocomposite coatings prepared by a filtered vacuum arc method

    Energy Technology Data Exchange (ETDEWEB)

    Thangavel, Elangovan, E-mail: t.elangophy@gmail.com [Advanced Thin Film Research Group, Materials Processing Division, Korea Institute of Materials Science, Changwon 641-831 (Korea, Republic of); Center for Nano-Wear, Yonsei University, Seoul 120-749 (Korea, Republic of); Lee, Seunghun; Nam, Kee-Seok; Kim, Jong-Kuk [Advanced Thin Film Research Group, Materials Processing Division, Korea Institute of Materials Science, Changwon 641-831 (Korea, Republic of); Kim, Do-Geun, E-mail: dogeunkim@kims.re.kr [Advanced Thin Film Research Group, Materials Processing Division, Korea Institute of Materials Science, Changwon 641-831 (Korea, Republic of)

    2013-01-15

    Highlights: Black-Right-Pointing-Pointer Preparation method was used as filtered vacuum arc (FVA) deposition. Black-Right-Pointing-Pointer Ternary coating obtained by using single carbon source with TMS gas. Black-Right-Pointing-Pointer Detailed discussion of chemical nature for these coating by using XPS. - Abstract: Ti-Si-C-N nanocomposite coatings were synthesized by a filtered vacuum arc (FVA) technique. A metal organic precursor, tetramethylsilane (TMS), was used as a source for silicon and carbon to deposit the Ti-Si-C-N nanocomposite coating with a Ti cathode source. The chemical and microstructural properties of the as-deposited coatings were systematically investigated using X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Nanoindentation and scratch tests were carried out to evaluate the mechanical and adhesion properties of the coatings. From the XPS analysis, it was found that the Si content in the coating increased from 2 to 16 at.% as the TMS flow rate was increased from 5 to 20 sccm. The TEM analysis clearly demonstrated that the coatings were composed of crystalline TiCN along with amorphous Si{sub 3}N{sub 4} as a secondary phase. From the XRD results, it was found that the crystallite size of TiCN increased with increasing Si content. The microstructure and mechanical properties of the TiSiCN coatings prepared by this method exhibited strong dependencies on the silicon content. A maximum hardness of 49 GPa and a coefficient of friction of 0.17 were obtained for the film with a silicon content of 3 at.%.

  7. Laser-induced incandescence (LII) diagnostic for in situ monitoring of nanoparticle synthesis in a high-pressure arc discharge

    Science.gov (United States)

    Yatom, Shurik; Vekselman, Vladislav; Mitrani, James; Stratton, Brentley; Raitses, Yevgeny; LaboratoryPlasma Nanosynthesis Team

    2016-10-01

    A DC arc discharge is commonly used for synthesis of carbon nanoparticles, including buckyballs, carbon nanotubes, and graphene flakes. In this work we show the first results of nanoparticles monitored during the arc discharge. The graphite electrode is vaporized by high current (60 A) in a buffer Helium gas leading to nanoparticle synthesis in a low temperature plasma. The arc was shown to oscillate, which can possibly influence the nano-synthesis. To visualize the nanoparticles in-situ we employ the LII technique. The nanoparticles with radii >50 nm, emerging from the arc area are heated with a short laser pulse and incandesce. The resulting radiation is captured with an ICCD camera, showing the location of the generated nanoparticles. The images of incandescence are studied together with temporally synchronized fast-framing imaging of C2 emission, to connect the dynamics of arc instabilities, C2 molecules concentration and nanoparticles. The time-resolved incandescence signal is analyzed with combination of ex-situ measurements of the synthesized nanoparticles and LII modeling, to provide the size distribution of produced nanoparticles. This work was supported by US Department of Energy, Office of Science, Basic Energy Sciences, Materials Sciences and Engineering Division.

  8. The Formation of Composite Ti-Al-N Coatings Using Filtered Vacuum Arc Deposition with Separate Cathodes

    Directory of Open Access Journals (Sweden)

    Ivan A. Shulepov

    2017-11-01

    Full Text Available Ti-Al-N coatings were deposited on high-speed steel substrates by filtered vacuum arc deposition (FVAD during evaporation of aluminum and titanium cathodes. Distribution of elements, phase composition, and mechanical properties of Ti-Al-N coatings were investigated using Auger electron spectroscopy (AES, X-ray diffraction (XRD, transmission electron microscopy (TEM and nanoindentation, respectively. Additionally, tribological tests and scratch tests of the coatings were performed. The stoichiometry of the coating changes from Ti0.6Al0.4N to Ti0.48Al0.52N with increasing aluminum arc current from 70 A to 90 A, respectively. XRD and TEM showed only face-centered cubic Ti-Al-N phase with preferred orientation of the crystallites in (220 direction with respect to the sample normal and without precipitates of AlN or intermetallics inside the coatings. Incorporation of Al into the TiN lattice caused shifting of the (220 reflex to a higher 2θ angle with increasing Al content. Low content and size of microdroplets were obtained using coaxial plasma filters, which provides good mechanical and tribological properties of the coatings. The highest value of microhardness (36 GPa and the best wear-resistance were achieved for the coating with higher Al content, thus for Ti0.48Al0.52N. These coatings exhibit good adhesive properties up to 30 N load in the scratch tests.

  9. A One-Dimensional Particle-in-Cell Model of Plasma Build-Up in Vacuum Arcs

    CERN Document Server

    Timko, H; Kovermann, J; Taborelli, M; Nordlund, K; Descoeudres, A; Schneider, R; Calatroni, S; Matyash, K; Wuensch, W; Hansen, A; Grudiev, A

    2011-01-01

    Understanding the mechanism of plasma build-up in vacuum arcs is essential in many fields of physics. A one-dimensional particle-in-cell computer simulation model is presented, which models the plasma developing from a field emitter tip under electrical breakdown conditions, taking into account the relevant physical phenomena. As a starting point, only an external electric field and an initial enhancement factor of the tip are assumed. General requirements for plasma formation have been identified and formulated in terms of the initial local field and a critical neutral density. The dependence of plasma build-up on tip melting current, the evaporation rate of neutrals and external circuit time constant has been investigated for copper and simulations imply that arcing involves melting currents around 0.5-1 A/mu m(2),evaporation of neutrals to electron field emission ratios in the regime 0.01 - 0.05, plasma build-up timescales in the order of similar to 1 - 10 ns and two different regimes depending on initial ...

  10. Al-Co Alloys Prepared by Vacuum Arc Melting: Correlating Microstructure Evolution and Aqueous Corrosion Behavior with Co Content

    Directory of Open Access Journals (Sweden)

    Angeliki Lekatou

    2016-02-01

    Full Text Available Hypereutectic Al-Co alloys of various Co contents (7–20 weight % (wt.% Co were prepared by vacuum arc melting, aiming at investigating the influence of the cobalt content on the microstructure and corrosion behavior. Quite uniform and directional microstructures were attained. The obtained microstructures depended on the Co content, ranging from fully eutectic growth (7 wt.% and 10 wt.% Co to coarse primary Al9Co2 predominance (20 wt.% Co. Co dissolution in Al far exceeded the negligible equilibrium solubility of Co in Al; however, it was hardly uniform. By increasing the cobalt content, the fraction and coarseness of Al9Co2, the content of Co dissolved in the Al matrix, and the hardness and porosity of the alloy increased. All alloys exhibited similar corrosion behavior in 3.5 wt.% NaCl with high resistance to localized corrosion. Al-7 wt.% Co showed slightly superior corrosion resistance than the other compositions in terms of relatively low corrosion rate, relatively low passivation current density and scarcity of stress corrosion cracking indications. All Al-Co compositions demonstrated substantially higher resistance to localized corrosion than commercially pure Al produced by casting, cold rolling and arc melting. A corrosion mechanism was formulated. Surface films were identified.

  11. Test of the beam effect on vacuum arc occurrence in a high-gradient accelerating structure for the CLIC project

    CERN Document Server

    AUTHOR|(CDS)2130409; Gagliardi, Martino

    A new generation of lepton colliders capable of reaching TeV energies is pres- ently under development, and to succeed in this task it is necessary to show that the technology for such a machine is available. The Compact Linear Collider (CLIC) is a possible design option among the future lepton collider projects. It consists of two normal-conducting linacs. Accelerating structures with a gradient of the order of 100 MV/m are necessary to reach the required high energies within a reasonable machine length. One of the strictest require- ments for such accelerating structures is a relatively low occurrence of vacuum arcs. CLIC prototype structures have been tested in the past, but only in absence of beam. In order to proof the feasibility of the high gradient technology for building a functional collider, it is necessary to understand the effect of the beam presence on the vacuum breakdowns. Tests of this type have never been performed previously. The main goal of this work is to provide a first measurement of t...

  12. METALLIC CATHODE SURFACE MODIFICATION BY USING LOW-PRESSURE PULSED VACUUM ARC DISCHARGE

    Directory of Open Access Journals (Sweden)

    LUIS ALPIDIO GARCIA

    2012-01-01

    Full Text Available Se produjeron descargas eléctricas en un sistema de arco pulsado a baja presión, con una corriente máxima de 100 A con pulsos de 30 ms. Las descargas se llevaron a cabo aplicando un voltaje de 104 V entre los electrodos. Los materiales utilizados como cátodo fueron Ti, Zr, Ni, Cu, Mo y W. La morfología de cátodos después de la descarga fue estudiada mediante la técnica de microscopía electrónica de barrido (SEM. Los cátodos de Ti y Zr presentaron la mayor erosión. Por otra parte, se observaron cráteres circulares sobre cátodos de Ni y Mo y se analizó una región del cátodo Zr, con alta erosión y gran cantidad de cráteres. Se midió el voltaje de descarga para cada material, obteniendo valores de voltaje del arco. Finalmente, se observaron las relaciones entre los voltajes de arco y algunas características del material como punto de fusión y de ebullición, presentando una tendencia exponencial.

  13. XPS STRUCTURE ANALYSIS OF TiN/TiC BILAYERS PRODUCED BY PULSED VACUUM ARC DISCHARGE

    Directory of Open Access Journals (Sweden)

    ELISABETH RESTREPO PARRA

    2010-01-01

    Full Text Available se crecieron bicapas de TiN/TiC sobre sustratos de acero inoxidable 304 usando un sistema de deposición física de vapor asistida por plasma en forma de arco pulsado a dos diferentes temperaturas del sustrato (50º C y150º C. Para el análisis de la composición química se empleó la técnica de la espectroscopía de fotoelectrones de rayos X (XPS. Se observó el comportamiento de las líneas Ti2p, N1s y C1s. Los análisis de energía de enlace confirmaron la conformación de TiN y TiC. Los picos C1s y Ti2p sufrieron un corrimiento a medida que se incrementó el tiempo de esputtering, revelando contaminación debido a la presencia de hidrocarburos. Además, los perfiles de profundidad de las bicapas de TiN/TiC mostraron que las películas crecidas a una temperatura de 150 ° C tienen una capa de TiN más gruesa que las muestras crecidas a 50º C. El nitrógeno se difundió en la capa de TiC y el carbón en la capa de TiN para ambas temperaturas.

  14. Cold-rolled sheets production of stainless martensite-ageing steel smelted by vacuum arc and electroslag techniques

    Energy Technology Data Exchange (ETDEWEB)

    Rivkin, A A; Grishkov, A I; Suslin, A P; Nesterenko, A A; Lola, V N [Tsentral' nyj Nauchno-Issledovatel' skij Inst. Chernoj Metallurgii, Moscow (USSR)

    1975-05-01

    In cooperation with a number of metallurgical works the production of a high strength sheet stainless maraging steel EHP678 (000KH11N10M2T) has been tested by rolling cylindrical ingots of vacuum arc smelting at the blooming (the mass of rough ingots was 5.1 to 6.0 t, that of cleaned ingots - 3.8 to 5.1 t) or rectangular ingots of electroslag smelting (13 t) at the slabbing. The recommended regimes of heating and deformation are much similar to those used for the steel-KH18N10T. The output of valid cold-rolled sheets proved to be rather low (0.24 t/t for the vacuum arc smelting and 0.30 t/t for the electroslag smelting) mainly due to the losses on cleaning and a considerable portion of wrong-size slabs. The data are presented on the steel-EHP678 properties after various heat treatments. For the production of wide cold-rolled sheets of the steel EHP678 it is recommended to use steelmaking procedure with electroslag smelting including open-hearth melting in arc furnaces, rolling of ingots at the slabbing with heating up to 1260-1280 deg C (hold-up of 4.5 to 5 hrs); electroslag smelting for rectangular section slabs, rolling of ingots of electroslag smelting at the slabbing with their heating up to 1250 deg C (hold-up of 5.5 to 6 hrs), rolling at the 1680-type mill with heating up to 1250-1260 deg C (hold-up of 4 to 4.5 hrs ensuring the rolling temperature after a rough group not below 1100 deg C), quenching of hot-rolled sheets heating up to 920-940 deg C (hold-up of 3 to 3.5 min/mm), shot peening of sheets for descaling (provided the respective equipment is available) with a subsequent short-time pickling in an acid solution and cold rolling with a summary deformation of 35 to 45 %. The steelmaking with the electroslag smelting is much more profitable as regards to the fine technology of number of the main procedures, convenient cooperation of the works and a considerably greater output of the final products out of one ton of the steel produced.

  15. Analysing bifurcations encountered in numerical modelling of current transfer to cathodes of dc glow and arc discharges

    International Nuclear Information System (INIS)

    Almeida, P G C; Benilov, M S; Cunha, M D; Faria, M J

    2009-01-01

    Bifurcations and/or their consequences are frequently encountered in numerical modelling of current transfer to cathodes of gas discharges, also in apparently simple situations, and a failure to recognize and properly analyse a bifurcation may create difficulties in the modelling and hinder the understanding of numerical results and the underlying physics. This work is concerned with analysis of bifurcations that have been encountered in the modelling of steady-state current transfer to cathodes of glow and arc discharges. All basic types of steady-state bifurcations (fold, transcritical, pitchfork) have been identified and analysed. The analysis provides explanations to many results obtained in numerical modelling. In particular, it is shown that dramatic changes in patterns of current transfer to cathodes of both glow and arc discharges, described by numerical modelling, occur through perturbed transcritical bifurcations of first- and second-order contact. The analysis elucidates the reason why the mode of glow discharge associated with the falling section of the current-voltage characteristic in the solution of von Engel and Steenbeck seems not to appear in 2D numerical modelling and the subnormal and normal modes appear instead. A similar effect has been identified in numerical modelling of arc cathodes and explained.

  16. Pulsed laser ablation of borax target in vacuum and hydrogen DC glow discharges

    Science.gov (United States)

    Kale, A. N.; Miotello, A.; Mosaner, P.

    2006-09-01

    The aim of our experiment was to produce a material with B sbnd H bonds for applications in hydrogen storage and generation. By using KrF excimer laser ( λ = 248 nm) ablation of borax (Na 2B 4O 7) target, thin films were deposited on KBr and silicon substrates. Ablation was performed both in vacuum and in hydrogen atmosphere. DC glow discharge technique was utilized to enhance hydrogen gas ionization. Experiments were performed using laser fluence from 5 to 20 J/cm 2. Films were deposited under gas pressure of 1 × 10 -5 to 5 × 10 -2 mbar and substrate temperatures of 130-450 °C. Scanning electron microscopy analysis of films showed presence of circular particulates. Film thickness, roughness and particulates number increased with increase in laser fluence. Energy dispersive X-ray spectroscopy analysis shows that sodium content in the particulates is higher than in the target. This effect is discussed in terms of atomic arrangements (both at surface and bulk) in systems where ionic and covalent bonds are present and by looking at the increased surface/bulk ratio of the particulates with respect to the deposited films. The Fourier transform infrared spectroscopy measurements showed presence of B sbnd O stretching and B sbnd O sbnd B bending bonds. Possible reasons for absence of B sbnd H bonds are attributed to binding enthalpy of the competing molecules.

  17. The diagnostic neutral beam injector with arc-discharge plasma source on the TCV Tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Karpushov, Alexander N. [Ecole Polytechnique Federale de Lausanne (EPFL), Centre de Recherches en Physique des Plasmas, Association Euratom-Confederation Suisse, CH-1015 Lausanne (Switzerland)], E-mail: alexander.karpushov@epfl.ch; Andrebe, Yanis; Duval, Basil P.; Bortolon, Alessandro [Ecole Polytechnique Federale de Lausanne (EPFL), Centre de Recherches en Physique des Plasmas, Association Euratom-Confederation Suisse, CH-1015 Lausanne (Switzerland)

    2009-06-15

    The diagnostic neutral beam injector (DNBI) together with a charge exchange recombination spectroscopy (CXRS) system has been used on the TCV Tokamak as a diagnostic tool for local measurements of plasma ion temperature, velocity and carbon impurity density based on analysis of the beam induced impurity radiation emission since 2000. To improve the performance of the CXRS diagnostic, several upgrades of both the optical system and the neutral beam were performed. An increase of the plasma source size together with beam optimization in 2003 resulted in a twofold increase the beam current. The RF plasma generator was replaced by an arc-discharge plasma source together with a new ion optical system (IOS) in 2006 and subsequent beam optimization is presented herein. This was designed to increase the line brightness of the beam in the CXRS observation region without increasing of the injected power (to avoid plasma perturbation by the beam). The beam characteristics are measured by a multi-chord scanning of Doppler-shifted H{sub {alpha}} emission, thermal measurements on a movable calorimeter and visible optical measurements inside the Tokamak vessel.

  18. Electroless nickel plating of arc discharge synthesized carbon nanotubes for metal matrix composites

    International Nuclear Information System (INIS)

    Jagannatham, M.; Sankaran, S.; Prathap, Haridoss

    2015-01-01

    Highlights: • Electroless Ni coatings have been performed on CNTs for various deposition times. • The deposition of nickel increased with increase in deposition time. • A deposition time of 60 min has been optimum for uniform coating of Ni on CNTs. • The CNTs with uniform coating of Ni are potential for reinforcements in composites. • Electroless nickel coatings are determined to be super paramagnetic behavior. - Abstract: Electroless nickel (EN) plating was performed on arc discharge synthesized multiwalled carbon nanotubes for various deposition times. X-ray diffraction (XRD), Transmission electron microscopy (TEM), and Raman spectroscopy characterization techniques are used to identify the presence of nickel deposition on the carbon nanotubes (CNTs) and the degree of graphitization. The results indicate that impurities are less in the purified CNTs as compared to raw carbon soot. Increasing deposition time up to 60 min increases uniform deposition of nickel throughout the length of the CNTs. However, for deposition time longer than 60 min, nickel particles are seen separated from the surface of the CNTs. Uniformly coated nickel CNTs throughout their length are potential candidates for reinforcements in composite materials. Magnetic properties of the nickel coated CNTs, with deposition time of 30 and 60 min were also evaluated. The magnetic saturation of nickel coated CNTs with deposition time of 30 min is less compared to nickel coated CNTs with deposition time of 60 min

  19. Electroless nickel plating of arc discharge synthesized carbon nanotubes for metal matrix composites

    Energy Technology Data Exchange (ETDEWEB)

    Jagannatham, M.; Sankaran, S.; Prathap, Haridoss, E-mail: prathap@iitm.ac.in

    2015-01-01

    Highlights: • Electroless Ni coatings have been performed on CNTs for various deposition times. • The deposition of nickel increased with increase in deposition time. • A deposition time of 60 min has been optimum for uniform coating of Ni on CNTs. • The CNTs with uniform coating of Ni are potential for reinforcements in composites. • Electroless nickel coatings are determined to be super paramagnetic behavior. - Abstract: Electroless nickel (EN) plating was performed on arc discharge synthesized multiwalled carbon nanotubes for various deposition times. X-ray diffraction (XRD), Transmission electron microscopy (TEM), and Raman spectroscopy characterization techniques are used to identify the presence of nickel deposition on the carbon nanotubes (CNTs) and the degree of graphitization. The results indicate that impurities are less in the purified CNTs as compared to raw carbon soot. Increasing deposition time up to 60 min increases uniform deposition of nickel throughout the length of the CNTs. However, for deposition time longer than 60 min, nickel particles are seen separated from the surface of the CNTs. Uniformly coated nickel CNTs throughout their length are potential candidates for reinforcements in composite materials. Magnetic properties of the nickel coated CNTs, with deposition time of 30 and 60 min were also evaluated. The magnetic saturation of nickel coated CNTs with deposition time of 30 min is less compared to nickel coated CNTs with deposition time of 60 min.

  20. Structural and magnetic properties of Mn nanoparticles prepared by arc-discharge

    International Nuclear Information System (INIS)

    Si, P.Z.; Brueck, E.; Zhang, Z.D.; Tegus, O.; Zhang, W.S.; Buschow, K.H.J.; KlAsse, J.C.P.

    2005-01-01

    Mn nanoparticles are prepared by arc discharge technique. MnO, α-Mn, β-Mn, and γ-Mn are detected by X-ray diffraction, while the presence of Mn 3 O 4 and MnO 2 is revealed by X-ray photoelectron spectroscopy. Transmission electron microscopy observations show that most of the Mn nanoparticles have irregular shapes, rough surfaces and a shell/core structure, with sizes ranging from several nanometers to 80 nm. The magnetic properties of the Mn nanoparticles are investigated between 2 and 350 K at magnetic fields up to 5 T. A magnetic transition occurring near 43 K is attributed to the formation of the ferrimagnetic Mn 3 O 4 . The coercivity of the Mn nanoparticles, arising mainly from Mn 3 O 4 , decreases linearly with increasing temperature below 40 K. Below the blocking temperature T B ∼ 34 K, the hysteresis loops exhibit large coercivity (up to 500 kA/m), owing to finite size effects, and irreversibility in the loops is found up to 4 T, and magnetization is not saturated up to 5 T. The relationship between structure and the magnetic properties are discussed

  1. The effect of calcination on multi-walled carbon nanotubes produced by dc-arc discharge.

    Science.gov (United States)

    Pillai, Sreejarani K; Augustyn, Willem G; Rossouw, Margaretha H; McCrindle, Robert I

    2008-07-01

    Multi-walled carbon nanotubes were synthesized by dc-arc discharge in helium atmosphere and the effect of calcination at different temperatures ranging from 300-600 degrees C was studied in detail. The degree of degradation to the structural integrity of the multi-walled carbon nanotubes during the thermal process was studied by Raman spectroscopy, Scanning electron microscopy and High resolution transmission electron microscopy. The thermal behaviour of the as prepared and calcined samples was investigated by thermogravimetric analysis. Calcination in air at 400 degrees C for 2 hours was found to be an efficient and simple method to eliminate carbonaceous impurities from the nanotube bundles with minimal damage to the tube walls and length. The impurities were oxidized at a faster rate when compared to the nanotubes and gave good yield of about 50%. The nanotubes were observed to be damaged at temperature higher than 450 degrees C. The results show that this method is less destructive when compared liquid phase oxidation with 5 M HNO3.

  2. On the Modeling of Thermal Radiation at the Top Surface of a Vacuum Arc Remelting Ingot

    Science.gov (United States)

    Delzant, P.-O.; Baqué, B.; Chapelle, P.; Jardy, A.

    2018-06-01

    Two models have been implemented for calculating the thermal radiation emitted at the ingot top in the VAR process, namely, a crude model that considers only radiative heat transfer between the free surface and electrode tip and a more detailed model that describes all radiative exchanges between the ingot, electrode, and crucible wall using a radiosity method. From the results of the second model, it is found that the radiative heat flux at the ingot top may depend heavily on the arc gap length and the electrode radius, but remains almost unaffected by variations of the electrode height. Both radiation models have been integrated into a CFD numerical code that simulates the growth and solidification of a VAR ingot. The simulation of a Ti-6-4 alloy melt shows that use of the detailed radiation model leads to some significant modification of the simulation results compared with the simple model. This is especially true during the hot-topping phase, where the top radiation plays an increasingly important role compared with the arc energy input. Thus, while the crude model has the advantage of its simplicity, use of the detailed model should be preferred.

  3. Ultrathin diamond-like carbon films deposited by filtered carbon vacuum arcs

    International Nuclear Information System (INIS)

    Anders, Andre; Fong, Walton; Kulkarni, Ashok; Ryan, Francis W.; Bhatia, C. Singh

    2001-01-01

    Ultrathin ( and lt; 5 nm) hard carbon films are of great interest to the magnetic storage industry as the areal density approaches 100 Gbit/in(sup 2). These films are used as overcoats to protect the magnetic layers on disk media and the active elements of the read-write slider. Tetrahedral amorphous carbon films can be produced by filtered cathodic arc deposition, but the films will only be accepted by the storage industry only if the ''macroparticle'' issue has been solved. Better plasma filters have been developed over recent years. Emphasis is put on the promising twist filter system - a compact, open structure that operates with pulsed arcs and high magnetic field. Based on corrosion tests it is shown that the macroparticle reduction by the twist filter is satisfactory for this demanding application, while plasma throughput is very high. Ultrathin hard carbon films have been synthesized using S-filter and twist filter systems. Film properties such as hardness, elastic modulus, wear, and corrosion resistance have been tested

  4. Gyrocenter Shift of Low-Temperature Plasmas and the Retrograde Motion of Cathode Spots in Arc Discharges

    International Nuclear Information System (INIS)

    Lee, K. C.

    2007-01-01

    The gyrocenter shift phenomenon explained the mechanism of radial electric field formation at the high confinement mode transition in fusion devices. This Letter reports that the theory of gyrocenter shift is also applicable to low temperature high collisional plasmas such as arc discharges by the generalization of the theory resulting from a short mean free path compared with the gyroradius. The retrograde motion of cathode spots in the arc discharge is investigated through a model with the expanded formula of gyrocenter shift. It is found that a reversed electric field is formed in front of the cathode spots when they are under a magnetic field, and this reversed electric field generates a rotation of cathode spots opposite to the Amperian direction. The ion drift velocity profiles calculated from the model are in agreement with the experimental results as functions of magnetic flux density and gas pressure

  5. Quasi-Laminar Flow Characteristics in Hybrid-Stabilized Argon–Water Arc Discharge for Subsonic-Supersonic Regimes

    Czech Academy of Sciences Publication Activity Database

    Jeništa, Jiří; Takana, H.; Nishiyama, H.; Křenek, Petr; Bartlová, M.; Aubrecht, V.

    2014-01-01

    Roč. 42, č. 10 (2014), s. 2632-2633 ISSN 0093-3813 R&D Projects: GA ČR GAP205/11/2070 Institutional support: RVO:61389021 Keywords : Hybrid-stabilized electric arc * large-eddy simulation * partial characteristics * the Smagorinsky subgrid scale model Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 1.101, year: 2014 http://ieeexplore.ieee.org/xpl/articleDetails.jsp?arnumber=6876210

  6. The source of X-rays and high-charged ions based on moderate power vacuum discharge with laser triggering

    Directory of Open Access Journals (Sweden)

    Alkhimova Mariya A.

    2015-06-01

    Full Text Available The source of X-ray radiation with the energy of quanta that may vary in the range hν = 1÷12 keV was developed for studies in X-ray interaction with matter and modification of solid surfaces. It was based on a vacuum spark discharge with the laser triggering. It was shown in our experiments that there is a possibility to adjust X-ray radiation spectrum by changing the configuration of the electrode system when the energy stored in the capacitor is varied within the range of 1÷17 J. A comprehensive study of X-ray imaging and quanta energy was carried out. These experiments were carried out for the case of both direct and reverse polarity of the voltage on the electrodes. Additionally, ion composition of plasma created in a laser-triggered vacuum discharge was analyzed. Highly charged ions Zn(+21, Cu(+20 and Fe(+18 were observed.

  7. On nuclear DD synthesis at the initial stage of nanosecond vacuum discharge with deuterium-loaded Pd anode

    Science.gov (United States)

    Kurilenkov, Yu K.; Gus'kov, S. Yu; Karpukhin, V. T.; Oginov, A. V.; Samoylov, I. S.

    2018-01-01

    Earlier, there was demonstrated generation of DD neutrons in an interelectrode medium of a low-energy (˜ 1 J) nanosecond vacuum discharge with a hollow cathode and a deuterium-loaded Pd anode. There was revealed essential role of formation of a virtual cathode and a potential well corresponding thereto in the processes of collisional DD synthesis in the interelectrode space. In this work, we have obtained as a result of an experiment and discussed the neutron yield at the very initial stage of the discharge, when the beam of auto-electrons just starts to irradiate the non-ideal surface of the deuterium-loaded Pd anode.

  8. Effect of high substrate bias and hydrogen and nitrogen incorporation on filtered cathodic vacuum arc deposited tetrahedral amorphous carbon films

    International Nuclear Information System (INIS)

    Panwar, O.S.; Khan, Mohd. Alim; Kumar, Mahesh; Shivaprasad, S.M.; Satyanarayana, B.S.; Dixit, P.N.; Bhattacharyya, R.; Khan, M.Y.

    2008-01-01

    The application of a sufficiently high negative substrate bias, during the growth of tetrahedral amorphous carbon (ta-C), is usually associated with low sp 3 bonding configuration and stressed films. However, in an effort to understand and utilize the higher pseudo thermo dynamical conditions during the film growth, at high negative substrate bias (- 300 V), reported here is a study on ta-C films grown under different hydrogen and nitrogen concentration. As grown ta-C films were studied under different negative substrate bias conditions. The variation of the sp 3 content and sp 3 /sp 2 ratio in the ta-C films exhibits a trend similar to those reported in literature, with a subtle variation in this report being the substrate bias voltage, which was observed to be around - 200 V, for obtaining the highest sp 3 (80%) bonding and sp 3 /sp 2 (3.95) ratio. The hydrogen and nitrogen incorporated ta-C films studied, at a bias of - 300 V, show an increase in sp 3 (87-91%) bonding and sp 3 /sp 2 (7-10) ratio in the range of studies reported. The inference is drawn on the basis of the set of data obtained from measurements carried out using X-ray photoelectron spectroscopy, X-ray induced Auger electron spectroscopy and Raman spectroscopy of as grown and hydrogen and nitrogen incorporated ta-C films deposited using an S bend filtered cathodic vacuum arc system. The study indicates the possibility of further tailoring ta-C film properties and also extending capabilities of the cathodic arc system for developing carbon based films for electronics and tribological applications

  9. Effect of high substrate bias and hydrogen and nitrogen incorporation on filtered cathodic vacuum arc deposited tetrahedral amorphous carbon films

    Energy Technology Data Exchange (ETDEWEB)

    Panwar, O.S. [Plasma Processed Materials Group, National Physical Laboratory, Dr. K.S. Krishnan Road, New Delhi-110 012 (India)], E-mail: ospanwar@mail.nplindia.ernet.in; Khan, Mohd. Alim [Plasma Processed Materials Group, National Physical Laboratory, Dr. K.S. Krishnan Road, New Delhi-110 012 (India); Kumar, Mahesh; Shivaprasad, S.M. [Surface Physics and Nanostructures Group, National Physical Laboratory, Dr. K.S. Krishnan Road, New Delhi-110 012 (India); Satyanarayana, B.S. [MIT Innovation Centre and Electronics and Communication Department, Manipal Institute of Technology, Manipal-579104 (India); Dixit, P.N. [Plasma Processed Materials Group, National Physical Laboratory, Dr. K.S. Krishnan Road, New Delhi-110 012 (India); Bhattacharyya, R. [Emeritus Scientist, National Physical Laboratory, New Delhi-110012 (India); Khan, M.Y. [Department of Physics, Jamia Millia Islamia, Central University, New Delhi-110025 (India)

    2008-02-29

    The application of a sufficiently high negative substrate bias, during the growth of tetrahedral amorphous carbon (ta-C), is usually associated with low sp{sup 3} bonding configuration and stressed films. However, in an effort to understand and utilize the higher pseudo thermo dynamical conditions during the film growth, at high negative substrate bias (- 300 V), reported here is a study on ta-C films grown under different hydrogen and nitrogen concentration. As grown ta-C films were studied under different negative substrate bias conditions. The variation of the sp{sup 3} content and sp{sup 3}/sp{sup 2} ratio in the ta-C films exhibits a trend similar to those reported in literature, with a subtle variation in this report being the substrate bias voltage, which was observed to be around - 200 V, for obtaining the highest sp{sup 3} (80%) bonding and sp{sup 3}/sp{sup 2} (3.95) ratio. The hydrogen and nitrogen incorporated ta-C films studied, at a bias of - 300 V, show an increase in sp{sup 3} (87-91%) bonding and sp{sup 3}/sp{sup 2} (7-10) ratio in the range of studies reported. The inference is drawn on the basis of the set of data obtained from measurements carried out using X-ray photoelectron spectroscopy, X-ray induced Auger electron spectroscopy and Raman spectroscopy of as grown and hydrogen and nitrogen incorporated ta-C films deposited using an S bend filtered cathodic vacuum arc system. The study indicates the possibility of further tailoring ta-C film properties and also extending capabilities of the cathodic arc system for developing carbon based films for electronics and tribological applications.

  10. A glucose concentration and temperature sensor based on long period fiber gratings induced by electric-arc discharge

    Science.gov (United States)

    Du, Chao; Wang, Qi

    2017-10-01

    As one of the key parameters in biological and chemical reactions, glucose concentration objectively reflects the characteristics of reactions, so the real-time monitoring of glucose concentration is important in the field of biochemical. Meanwhile, the influence from temperature should be considered. The fiber sensors have been studied extensively for decades due to the advantages of small size, immunity to electromagnetic interference and high sensitivity, which are suitable for the application of biochemical sensing. A long period fiber grating (LPFG) sensor induced by electric-arc discharge has been fabricated and demonstrated for simultaneous measurement of glucose concentration and temperature. The proposed sensor was fabricated by inscribing a sing mode fiber (SMF) with periodic electric-arc discharge technology. During the fabrication process, the electric-arc discharge technology was produced by a commercial fusion splicer, and the period of inscribed LPFG was determined by the movement of translation stages. A serials of periodic geometrical deformations would be formed in SMF after the fabrication, and the discharge intensity and discharge time can be adjusted though the fusion splicer settings screen. The core mode can be coupled into the cladding modes at certain wavelength when they satisfy the phase-matching conditions, and there will be several resonance dips in the transmission spectrum in LPFG. The resonance dips formed by the coupling between cladding modes and core mode have different sensitivity responses, so the simultaneous measurement for multi-parameter can be realized by monitoring the wavelength shifts of the resonance dips. Compared with the LPFG based on conventional SMF, the glucose concentration sensitivity has been obviously enhanced by etching the cladding with hydrofluoric acid solution. Based on the independent measured results, a dual-parameter measurement matrix has been built for signal demodulation. Because of the easy

  11. Vacuum-arc chromium coatings for Zr-1%Nb alloy protection against high-temperature oxidation in air

    International Nuclear Information System (INIS)

    Kuprin, A.S.; Belous, V.A.; Bryk, V.V.; Vasilenko, R.L.; Voevodin, V.N.; Ovcharenko, V.D.; Tolmacheva, G.N.; Kolodij, I.V.; Lunev, V.M.; Klimenko, I.O.

    2015-01-01

    The effect of vacuum-arc Cr coatings on the alloy E110 resistance to the oxidation in air at temperatures 1020 and 1100 deg C for 3600 s has been investigated. The methods of scanning electron microscope, X-ray analysis and nanoindentation were used to determine the thickness, phase, mechanical properties of coatings and oxide layers. The results show that the chromium coating can effectively protect fuel tubes against high-temperature oxidation in air for one hour. In the coating during oxidation at T = 1100 deg C a Cr 2 O 3 oxide layer of 5 μm thickness is formed preventing further oxygen penetration into the coating, and thus the tube shape is conserved. Under similar test conditions the oxidation of uncoated tubes with formation of a porous monocline oxide of ZrO 2 of a thickness more than ≥ 250 μm is observed, then the deformation and cracking of samples occur and the oxide layer breaks away

  12. Time and space resolved spectroscopic investigation during anode plume formation in a high-current vacuum arc

    Science.gov (United States)

    Khakpour, A.; Methling, R.; Uhrlandt, D.; Franke, St.; Gortschakow, S.; Popov, S.; Batrakov, A.; Weltmann, K. D.

    2017-05-01

    This paper presents time and space resolved results of spectroscopic measurements during the formation of an anode plume in the late current pulse phase of a high-current vacuum arc. The formation of the anode plume is investigated systematically based on the occurrence of high-current anode spots, depending on gap distance and current for AC 100 Hz and CuCr7525 butt contacts with a diameter of 10 mm. The anode plume is observed after the extinction of anode spot type 2 in which both the anode and cathode are active. It is concluded from the spatial profiles of the atomic and ionic radiation, parallel and perpendicular to anode surface, that the inner part of the plume is dominated by Cu I radiation, whereas a halo of light emitted by Cu II covers the plume. The radiation intensity of Cu III lines is quite low across the whole anode plume. Upper level excited state densities corresponding to Cu I lines at 510.55, 515.32, 521.82, 578.21 nm are determined. The temporal evolution of the resulting excitation temperature in the centre of the plume varies from 8500 K to 6000 K at 500 µs to 100 µs before current zero, respectively. The density calculated for Cu I at position in the plume is in the range of 1-5  ×  1019 m-3.

  13. The electrocatalytic oxidation of carbohydrates at a nickel/carbon paper electrode fabricated by the filtered cathodic vacuum arc technique

    International Nuclear Information System (INIS)

    Fu, Yingyi; Wang, Tong; Su, Wen; Yu, Yanan; Hu, Jingbo

    2015-01-01

    The direct electrochemical behaviour of carbohydrates at a nickel/carbon paper electrode with a novel fabrication method is investigated. The investigation is used for verification the feasibility of using monosaccharides and disaccharides in the application of fuel cell. The selected monosaccharides are glucose, fructose and galactose; the disaccharides are sucrose, maltose and lactose. The modified nickel/carbon paper electrode was prepared using a filtered cathodic vacuum arc technique. The morphology image of the nickel thin film on the carbon paper surface was characterized by scanning electron microscopy (SEM). The existence of nickel was verified by X-ray photoelectron spectroscopy (XPS). The contact angle measurement was also used to characterize the modified electrode. Cyclic voltammetry (CV) was employed to evaluate the electrochemical behaviour of monosaccharides and disaccharides in an alkaline aqueous solution. The modified electrode exhibits good electrocatalytic activities towards carbohydrates. In addition, the stability of the nickel/carbon paper electrode with six sugars was also investigated. The good catalytic effects of the nickel/carbon paper electrode allow for the use of carbohydrates as fuels in fuel cell applications

  14. Structural and Mechanical Properties of Nanostructured C-Ag Thin Films Synthesized by Thermionic Vacuum Arc Method

    Directory of Open Access Journals (Sweden)

    Rodica Vladoiu

    2018-01-01

    Full Text Available Nanostructured C-Ag thin films of 200 nm thickness were successfully synthesized by the Thermionic Vacuum Arc (TVA method. The influence of different substrates (glass, silicon wafers, and stainless steel on the microstructure, morphology, and mechanical properties of nanostructured C-Ag thin films was characterized by High-Resolution Transmission Electron Microscopy (HRTEM, Scanning Electron Microscopy (SEM, Atomic Force Microscopy (AFM, and TI 950 (Hysitron nanoindenter equipped with Berkovich indenter, respectively. The film’s hardness deposited on glass (HC-Ag/Gl = 1.8 GPa was slightly lower than in the case of the C-Ag film deposited on a silicon substrate (HC-Ag/Si = 2.2 GPa. Also the apparent elastic modulus Eeff was lower for C-Ag/Gl sample (Eeff = 100 GPa than for C-Ag/Si (Eeff = 170 GPa, while the values for average roughness are Ra=2.9 nm (C-Ag/Si and Ra=10.6 (C-Ag/Gl. Using the modulus mapping mode, spontaneous and indentation-induced aggregation of the silver nanoparticles was observed for both C-Ag/Gl and C-Ag/Si samples. The nanocomposite C-Ag film exhibited not only higher hardness and effective elastic modulus, but also a higher fracture resistance toughness to the silicon substrate compared to the glass substrate.

  15. Effects of filtered cathodic vacuum arc deposition (FCVAD) conditions on photovoltaic TiO{sub 2} films

    Energy Technology Data Exchange (ETDEWEB)

    Aramwit, C. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Intarasiri, S. [Science and Technology Research Institute, Chiang Mai University, Chiang Mai 50200 (Thailand); Thailand Center of Excellence in Physics, Commission on Higher Education, 328 Si Ayutthaya Road, Bangkok 10400 (Thailand); Bootkul, D. [Thailand Center of Excellence in Physics, Commission on Higher Education, 328 Si Ayutthaya Road, Bangkok 10400 (Thailand); Department of General Science, Faculty of Science, Srinakharinwirot University, Bangkok 10110 (Thailand); Tippawan, U. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Thailand Center of Excellence in Physics, Commission on Higher Education, 328 Si Ayutthaya Road, Bangkok 10400 (Thailand); Supsermpol, B.; Seanphinit, N. [Department of General Science, Faculty of Science, Srinakharinwirot University, Bangkok 10110 (Thailand); Western Digital Thailand Co. Ltd., Ayutthaya 13160 (Thailand); Ruangkul, W. [Thailand Center of Excellence in Physics, Commission on Higher Education, 328 Si Ayutthaya Road, Bangkok 10400 (Thailand); Yu, L.D., E-mail: yuld@thep-center.org [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Thailand Center of Excellence in Physics, Commission on Higher Education, 328 Si Ayutthaya Road, Bangkok 10400 (Thailand)

    2014-08-15

    Highlights: • Titanium dioxide films were synthesized using the FCVAD technique. • Various FCVAD conditions were tested. • The TiO{sub 2} films were characterized. • The FCVAD condition effects on the film characteristics were studied. • The O{sub 2} pressure had the most important effect on the film quality. - Abstract: Titanium dioxide (TiO{sub 2}) films for photovoltaic applications were synthesized using filtered cathodic vacuum arc deposition (FCVAD) technique. Various deposition conditions were tested for an optimal film formation. The conditions included the oxygen (O{sub 2}) pressure which was varied from a base pressure 10{sup −5} to 10{sup −4}, 10{sup −3}, 10{sup −2} and 10{sup −1} Torr, sample holder bias varied using 0 or −250 V, deposition time varied from 10, 20 to 30 min, and deposition distance varied from 1 to 3 cm. The deposited films were also annealed and compared with unannealed ones. The films under various conditions were characterized using optical microscopy, scanning electron microscopy (SEM), atomic force microscopy (AFM), energy-dispersive X-ray spectroscopy (EDS) and Raman spectroscopy techniques. The film transparency increased and thickness decreased to a nanoscale with increasing of the O{sub 2} pressure. The transparent deposited films contained stoichiometric titanium and oxygen under the medium O{sub 2} pressure. The as-deposited films were TiO{sub 2} containing some rutile but no anatase which needed annealing to form.

  16. Single layer and multilayer vacuum-arc coatings based on the nitride TiAlSiYN: composition, structure, properties

    International Nuclear Information System (INIS)

    Beresnev, V.M.; Litovchenko, S.V.; Nemchenko, U.S.; Srebnyuk, P.A.; Mazilin, B.A.; Sobol, O.V.; Mejlekhov, A.A.; Barmin, A.E.; Serenko, TA.; Pogrebnyak, A.D.; Ivanov, O.N.; Kritsyna, E.V.; Stolbovoj, V.A.; Novikov, V.Yu.; Malikov, L.V.

    2017-01-01

    Using high-technological vacuum-arc evaporation in the atmosphere of nitrogen with ion bombardment, single- and multilayer coatings based on TiAlSiYN with high mechanical characteristics were obtained: hardness of the coatings reached 49.5 GPa, resistance to wear, with the value of the critical point L_C_5 reaching 184.92 N. The peculiarities of radiation-induced effect at applying bias potential U_b were found: formation of nitride coatings based on fcc metallic lattice with the preferred orientation of crystallites with the texture axis [111], as well as simultaneous growth of hardness. Hardness of both single- and multilayer coatings increases by 40...50% at the increase of U_b from 50 to 200 V. Formation of silicon-containing layers of TiAlSiYN during the deposition contributes to reaching increased hardness, which, in the case of single-layer coating obtained at U_b = -200 V is 49.5 GPa, which corresponds to superhard state. The mechanisms of structure formation, defining the resulting mechanical characteristics of single- and multi-layer coatings based on TiAlSiYN nitride have been discussed.

  17. Vacuum arc plasma deposition of thin titanium dioxide films on silicone elastomer as a functional coating for medical applications.

    Science.gov (United States)

    Boudot, Cécile; Kühn, Marvin; Kühn-Kauffeldt, Marina; Schein, Jochen

    2017-05-01

    Silicone elastomer is a promising material for medical applications and is widely used for implants with blood and tissue contact. However, its strong hydrophobicity limits adhesion of tissue cells to silicone surfaces, which can impair the healing process. To improve the biological properties of silicone, a triggerless pulsed vacuum cathodic arc plasma deposition technique was applied to deposit titanium dioxide (TiO 2 ) films onto the surface. Scanning electron microscopy, atomic force microscopy, X-ray photoelectron spectroscopy, Raman spectroscopy and contact angle measurements were used for coating characterization. Deposited films were about 150nm thick and exhibited good adhesion to the underlying silicone substrate. Surface wettability and roughness both increased after deposition of the TiO 2 layer. In addition, cell-biological investigations demonstrated that the in-vitro cytocompatibility of TiO 2 -coated samples was greatly improved without impacting silicone's nontoxicity. For validation of use in medical devices, further investigations were conducted and demonstrated stability of surface properties in an aqueous environment for a period of 68days and the coating's resistance to several sterilization methods. Copyright © 2016 Elsevier B.V. All rights reserved.

  18. Superhard nanocomposite nc-TiC/a-C:H film fabricated by filtered cathodic vacuum arc technique

    International Nuclear Information System (INIS)

    Wang Yaohui; Zhang Xu; Wu Xianying; Zhang Huixing; Zhang Xiaoji

    2008-01-01

    Superhard nanocomposite nc-TiC/a-C:H films, with an excellent combination of high elastic recovery, low friction coefficient and good H/E ratio, were prepared by filtered cathodic vacuum arc technique using the C 2 H 2 gas as the precursor. The effect of C 2 H 2 flow rate on the microstructure, phase composition, mechanical and tribological properties of nanocomposite nc-TiC/a-C:H films have been investigated by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), energy disperse spectroscopy (EDS), microindentation and tribotester measurements. It was observed that the C 2 H 2 flow rate significantly affected the Ti content and hardness of films. Furthermore, by selecting the proper value for C 2 H 2 flow rate, 20 sccm, one can deposit the nanocomposite film nc-TiC/a-C:H with excellent properties such as superhardness (66.4 GPa), high elastic recovery (83.3%) and high H/E ratio (0.13)

  19. On generalization of electric field strength in longitudinally blown arcs

    OpenAIRE

    Yas'ko, O.I.; Esipchuk, A.M.; Qing, Z.; Schram, D.C.; Fauchais, P.

    1997-01-01

    Generalization of av. elec. field strength for different discharge conditions in longitudinally blown arcs is considered. Exptl. data for distinctive devices and different gases were used for phys. modeling. Anal. showed that heat transfer processes are responsible for I-E characteristic formation. Turbulent heat transfer is the most effective for atm. pressure discharges while convection plays the main role in vacuum arcs. A generalized I-E characteristic was obtained. [on SciFinder (R)

  20. New Raman-peak at 1850 cm(-1) observed in multiwalled carbon nanotubes produced by hydrogen arc discharge.

    Science.gov (United States)

    Chen, B; Kadowaki, Y; Inoue, S; Ohkohchi, M; Zhao, X; Ando, Y

    2010-06-01

    The new peak (near 1850 cm(-1)) assigned to carbon linear chain included in the centre of very thin innermost multiwalled carbon nanotubes (MWNTs) has been verified by Raman spectroscopy. These MWNTs were produced by dc arc discharge of pure graphite rods in pure hydrogen gas and existed in the cathode deposit. In this paper, we clarified that the new Raman-peaks could also be observed in the cathode deposit including MWNTs produced by hydrogen dc arc discharge using graphite electrode with added Y or La. By changing the quantity of addition (Y or La), dc arc current and pressure of ambient hydrogen gas, the optimum condition to get maximum intensity of the new Raman-peaks was obtained. For the case of 1 wt% La, dc 50 A, H2 pressure of 50 Torr was found to be optimum, and the intensity of new Raman-peak was even higher than the G-band peak. For the case of 1 wt% Y, dc 50 A, H2 pressure of 50 Torr was optimum, but the intensity of new Raman-peak was weaker than the G-band peak. Transmission electron microscopy observation revealed that the crystallinity of MWNTs produced with pure graphite rod was better than those produced with added Y or La.

  1. Interactive Relationship between Silver Ions and Silver Nanoparticles with PVA Prepared by the Submerged Arc Discharge Method

    Directory of Open Access Journals (Sweden)

    Kuo-Hsiung Tseng

    2018-01-01

    Full Text Available This study uses the submerged arc discharge method (SADM and the concentrated energy of arc to melt silver metal in deionized water (DW so as to prepare metal fluid with nanoparticles and submicron particles. The process is free from any chemical agent; it is rapid and simple, and rapid and mass production is available (0.5 L/min. Aside from the silver nanoparticle (Ag0, silver ions (Ag+ exist in the colloidal Ag prepared by the system. In the preparation of colloidal Ag, polyvinyl alcohol (PVA is used as an additive so that the Ag0/Ag+ concentration, arcing rate, peak, and scanning electron microscopic (SEM images in the cases with and without PVA can be analyzed. The findings show that the Ag0/Ag+ concentration increases with the addition level of PVA, while the nano-Ag and Ag+ electrode arcing rate rises. The UV-Vis absorption peak increases Ag0 absorbance and shifts as the dispersity increases with PVA addition. Lastly, with PVA addition, the proposed method can prepare smaller and more amounts of Ag0 nanoparticles, distributed uniformly. PVA possesses many distinct features such as cladding, dispersion, and stability.

  2. Non-platinum nanocatalyst on porous nitrogen-doped carbon fabricated by cathodic vacuum arc plasma technique

    Energy Technology Data Exchange (ETDEWEB)

    Sirirak, Reungruthai [Material Science Research Center, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Department of Chemistry and Center of Excellence for Innovation in Chemistry (PERCH-CIC), Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Sarakonsri, Thapanee, E-mail: tsarakonsri@gmail.com [Material Science Research Center, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Department of Chemistry and Center of Excellence for Innovation in Chemistry (PERCH-CIC), Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Medhesuwakul, Min [Plasma & Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand)

    2015-11-30

    Highlights: • High surface area porous coral-like nitrogen-doped carbon (NC) and non-platinum nanocatalysts were fabricated on proton exchange membrane using the cathodic vacuum arc plasma (CVAP) technique. • It is a one-step catalysts preparation directly on nafion proton exchange membrane. This CVAP technique is the first new method that was applied in a polymer electrolyte membrane fuel cells (PEMFCs) catalysts preparation. • Due to these excellent characteristics of nitrogen-doped carbon, it is expected to exhibit a good catalyst supporter for PEMFC. • In addition, the Fe–NC catalysts fabricated via this CVAP technique are sphere-like nanoparticle and well disperse on coral-like NC film, which particularity exhibits that these prepared catalysts ought to be a good oxygen reduction reaction (ORR) catalyst for PEMFC. • This approach can be extended to the synthesis of other non-platinum ORR catalyst for broad range applications in energy conversion. - Abstract: Polymer electrolyte membrane fuel cells (PEMFCs) convert chemical energy directly into electrical energy where catalysts composing of non-noble transition metals, nitrogen, and carbon compounds are the most promising materials to replace the expensive platinum catalysts for oxygen reduction reaction (ORR). In this research, cathodic vacuum arc plasma (CVAP) technique was used to fabricate porous nitrogen doped carbon (NC) and non-platinum catalyst on porous NC (Fe–NC) directly on ion exchange membrane for being used as an ORR catalyst at the cathode. The porous NC layer was fabricated on silicon wafer at 0.05 mTorr, 0.1 mTorr, 0.5 mTorr, 1 mTorr, and 5 mTorr of nitrogen gas inlet. The AFM, and SEM images are observed to be regularly big with quite high hillocks and thin NC layers; these results indicate that the optimum process pressure of nitrogen gas inlet is 5 mTorr for porous NC fabrication. The SEM–EDS detects Fe, N, and C elements in the prepared catalysts, and the XRD pattern reviews

  3. Non-platinum nanocatalyst on porous nitrogen-doped carbon fabricated by cathodic vacuum arc plasma technique

    International Nuclear Information System (INIS)

    Sirirak, Reungruthai; Sarakonsri, Thapanee; Medhesuwakul, Min

    2015-01-01

    Highlights: • High surface area porous coral-like nitrogen-doped carbon (NC) and non-platinum nanocatalysts were fabricated on proton exchange membrane using the cathodic vacuum arc plasma (CVAP) technique. • It is a one-step catalysts preparation directly on nafion proton exchange membrane. This CVAP technique is the first new method that was applied in a polymer electrolyte membrane fuel cells (PEMFCs) catalysts preparation. • Due to these excellent characteristics of nitrogen-doped carbon, it is expected to exhibit a good catalyst supporter for PEMFC. • In addition, the Fe–NC catalysts fabricated via this CVAP technique are sphere-like nanoparticle and well disperse on coral-like NC film, which particularity exhibits that these prepared catalysts ought to be a good oxygen reduction reaction (ORR) catalyst for PEMFC. • This approach can be extended to the synthesis of other non-platinum ORR catalyst for broad range applications in energy conversion. - Abstract: Polymer electrolyte membrane fuel cells (PEMFCs) convert chemical energy directly into electrical energy where catalysts composing of non-noble transition metals, nitrogen, and carbon compounds are the most promising materials to replace the expensive platinum catalysts for oxygen reduction reaction (ORR). In this research, cathodic vacuum arc plasma (CVAP) technique was used to fabricate porous nitrogen doped carbon (NC) and non-platinum catalyst on porous NC (Fe–NC) directly on ion exchange membrane for being used as an ORR catalyst at the cathode. The porous NC layer was fabricated on silicon wafer at 0.05 mTorr, 0.1 mTorr, 0.5 mTorr, 1 mTorr, and 5 mTorr of nitrogen gas inlet. The AFM, and SEM images are observed to be regularly big with quite high hillocks and thin NC layers; these results indicate that the optimum process pressure of nitrogen gas inlet is 5 mTorr for porous NC fabrication. The SEM–EDS detects Fe, N, and C elements in the prepared catalysts, and the XRD pattern reviews

  4. Annealing effect of thermal spike in MgO thin film prepared by cathodic vacuum arc deposition

    Energy Technology Data Exchange (ETDEWEB)

    Zhu, Daoyun, E-mail: zhudy@gdut.edu.cn [Experiment Teaching Department, Guangdong University of Technology, Guangzhou 510006 (China); State Key Laboratory of Optoelectronic Materials and Technologies, School of Physics and Engineering, Sun Yat-sen University, Guangzhou 510275 (China); Zhao, Shoubai [School of Physics and Electronic Engineering, Guangzhou University, Guangzhou 510400 (China); Zheng, Changxi; Chen, Dihu [State Key Laboratory of Optoelectronic Materials and Technologies, School of Physics and Engineering, Sun Yat-sen University, Guangzhou 510275 (China); He, Zhenhui, E-mail: stshzh@mail.sysu.edu.cn [State Key Laboratory of Optoelectronic Materials and Technologies, School of Physics and Engineering, Sun Yat-sen University, Guangzhou 510275 (China)

    2013-12-16

    MgO films were prepared by using pulsed cathodic vacuum arc deposition technique. The substrate bias voltage was in the range of −150 to −750 V. Film structure was investigated by X-ray diffraction (XRD). The annealing effect of thermal spike produced by the impacting of energetic ions was analyzed. The calculated results showed that the lifetime of a thermal spike generated by an energetic ion with the energy of 150 eV was less than one picosecond and it was sufficient to allow Mg{sup 2+} or O{sup 2-} to move one bond length to satisfy the intrinsic stress relief in the affected volume. The MgO(200) lattice spacings of the films deposited at different bias voltages were all larger than the ideal value of 2.1056 Å. As the bias amplitude increased the lattice spacing decreased, which indicated that the compressive stress in the film was partially relieved with increasing impacting ion energy. The stress relief also could be reflected from the film orientation with bias voltage. The biaxial elastic modulus for MgO(100), MgO(110) and MgO(111) planes were calculated and they were M{sub (100)} = 199 GPa, M{sub (110)} = 335 GPa and M{sub (111)} = 340 GPa, respectively. The M values indicated that the preferred orientation will be MgO(200) due to the minimum energy configuration when the lattice strain was large. It was confirmed by the XRD results in our experiments. - Highlights: • MgO thin films with preferred orientation were obtained by CVAD technique. • Annealing effect of a thermal spike in MgO film was discussed. • Lattice spacing of MgO film decreased with the increase of bias voltage. • Film preferred orientation changed from (200) to (220) as the bias voltage increased.

  5. On the properties of nanocomposite amorphous carbon films prepared by off-plane double bend filtered cathodic vacuum arc

    International Nuclear Information System (INIS)

    Tay, B.K.; Zhang, P.

    2002-01-01

    It is known to deposit hard thin films, such as tetrahedral amorphous carbon (ta-C), using a filtered cathode vacuum arc (FCVA). These ta-C films have interesting and useful properties because of the high sp 3 fraction of carbon atoms (up to 87%) in the film. However, the high internal stress in the films can limit their applications as the film may flake away from the substrate. In order to reduce the internal stress of the ta-C films and in an attempt to improve adhesion of thick films of this type, growth modifications such as incorporating metal into the ta-C films have been carried out. Nanocomposite amorphous carbon films were deposited by FCVA technique using metal-carbon composite target. Atomic force microscopy, Raman, and X-ray photoelectron spectroscopy were used to characterize the morphology and structure of the films. Nanoindenter and surface profilometer were used to determine the hardness, Young's modulus, and internal stress. The same metal composition targets for different elements results in different metal composition in the corresponding nanocomposite amorphous carbon films. We attribute this observation to the dynamic balance deposition effect of the FCVA deposition process. The influence of the type of metallic elements and its composition in the films on the structural, mechanical properties, surface energy and field emission (FE) performance was studied. The incorporation of metal into the films results in the decrease of sp 3 fraction, internal stress in the films, but the hardness and Young's modulus remains at high level. The surface energy of the films increases with incorporating Ni atoms, but decreases after incorporating Fe and Al atoms into the films. After heat-treatment, the incorporation of metal into ta-C films can greatly improve the FE performance

  6. Preparation of carbon-encapsulated iron nanoparticles in high yield by DC arc discharge and their characterization

    International Nuclear Information System (INIS)

    Zhang, Fan; Cui, Lan; Lin, Kui; Jin, Feng-min; Wang, Bin; Shi, Shu-xiu; Yang, De-an; Wang, Hui; He, Fei; Chen, Xiao-ping; Cui, Shen

    2013-01-01

    Highlights: ► CEINPs with core–shell structure and high Fe content were prepared in high yield by DC arc discharge. ► The anode II with a mass ratio of total iron to carbon 8:1 was used in DC arc discharge. ► The possible process of formation of CEINPs is briefly discussed. ► The uniformity of composition of anode is very important for the formation of CEINPs. ► The MEF and MMF of iron element may also play an important role in the formation of CEINPs. -- Abstract: Carbon-encapsulated iron nanoparticles (CEINPs) were prepared by DC arc discharge under nitrogen atmosphere of high temperature. The products were characterized by transmission electron microscope (TEM), high-resolution transmission electron microscope (HRTEM), X-ray diffractometer (XRD), energy dispersive X-ray (EDX) spectroscope, and X-ray photoelectron spectroscope (XPS), and their magnetic properties were measured by physical property measurement system (PPMS). The product B I , obtained from the anode I, contains the nanoparticles of iron and iron carbide, and carbon coating with imperfect and disordered layer structure. The product B II , obtained from the anode II, mainly consists of CEINPs, whose cores mainly consist of iron and iron carbide and shells contain about 3–7 graphitic layers. The iron contents in the products B I and B II are 44.8 and 82.6 wt.%, respectively. The products B I and B II have similar phase composition which includes carbon, iron, iron carbide, ferrous and ferric oxide, iron nitride, and carbon nitride. The saturation magnetization (Ms) of the products B I and B II are 29.35 and 88.66 emu/g and their coercivity (Hc) are 220 and 240 Oe, respectively. The total yields of all the products formed in the arc discharge chamber from anodes I and II, except for the cylinder-shaped deposits formed on the top of the cathode, are 25.8 and 22.3 wt.%, respectively. The possible process of formation of CEINPs is briefly discussed on the foundation of our results and other

  7. Erosion properties of unipolar arcs

    International Nuclear Information System (INIS)

    Chekalin, Eh.K.

    1982-01-01

    Processes modelling the formation of unipolar arcs on the elements of the first wall in limiters of the vacuum chamber and on active elements of tokamak divertor, are experimentally investigated. Erosion, processes that take place at two types of non-stationary cathode spots are considered. Experimental data prove the possibility of reducing erosion intensity by coating the surface of electrodes by oxide films, reduction of the temperature of electrode and discharge current

  8. Gliding arc discharge — Application for adhesion improvement of fibre reinforced polyester composites

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Teodoru, Steluta; Leipold, Frank

    2008-01-01

    production, and surface treatment. However, the application for adhesion improvement of structural materials has been rarely reported. In the present work, glass fibre reinforced polyester plates were treated using atmospheric pressure gliding arcs with high speed air flow for adhesion improvement...

  9. Comparison of carbon stripper foils produced by ARC discharge and laser ablation

    Energy Technology Data Exchange (ETDEWEB)

    Ophel, T.R.; Rhode, A.; Lobanov, N.; Weisser, D.C.; Turkentine, R.; Wolf, B.; Wlliman, R.G. [Australian National Univ. Canberra, ACT (Australia). Research School of Physical Sciences and Engineering

    1998-06-01

    The present work describes a series of investigations which compared the arc-deposited foils, prepared at ANU with a batch of foils from Munich, prepared by laser-ablation. The two foil types were bombarded with a beam of 6.8 MeV of {sup 197}Au recording their behaviour and monitoring the total stripped current. Optical and electron spectroscopy was carried out and indicate that the arc-deposited foils were relatively amorphous and smooth, while the laser-ablated foils appears to be much more crystalline. It was found that the average useful lifetimes of the Munich foils were at least ten times longer than arc-deposited foils. Furthermore, they maintained a constant beam output during the time in marked contrast to the arc-deposited foils, for which the output decreased quite rapidly. The longevity, and no less importantly, the constant beam output of the laser-ablated foils have emerged as critical to the continuance of the ERDA program. More significantly though, such qualities have provoked re-examination of likely energies for heavy beams that could be obtained with the Linac booster if foil stripping were used in the 14UD terminal, rather than gas that had previously been considered the only viable option. A program is in progress to explore the means to produce laser-ablated foils, or their equivalent, locally. Extended abstract. 1 ref., 2 figs.

  10. Comparison of carbon stripper foils produced by ARC discharge and laser ablation

    International Nuclear Information System (INIS)

    Ophel, T.R.; Rhode, A.; Lobanov, N.; Weisser, D.C.; Turkentine, R.; Wolf, B.; Wlliman, R.G.

    1998-01-01

    The present work describes a series of investigations which compared the arc-deposited foils, prepared at ANU with a batch of foils from Munich, prepared by laser-ablation. The two foil types were bombarded with a beam of 6.8 MeV of 197 Au recording their behaviour and monitoring the total stripped current. Optical and electron spectroscopy was carried out and indicate that the arc-deposited foils were relatively amorphous and smooth, while the laser-ablated foils appears to be much more crystalline. It was found that the average useful lifetimes of the Munich foils were at least ten times longer than arc-deposited foils. Furthermore, they maintained a constant beam output during the time in marked contrast to the arc-deposited foils, for which the output decreased quite rapidly. The longevity, and no less importantly, the constant beam output of the laser-ablated foils have emerged as critical to the continuance of the ERDA program. More significantly though, such qualities have provoked re-examination of likely energies for heavy beams that could be obtained with the Linac booster if foil stripping were used in the 14UD terminal, rather than gas that had previously been considered the only viable option. A program is in progress to explore the means to produce laser-ablated foils, or their equivalent, locally

  11. Translational, rotational and vibrational temperatures of a gliding arc discharge at atmospheric pressure air

    DEFF Research Database (Denmark)

    Zhu, Jiajian; Gao, Jinlong; Ehn, Andreas

    2014-01-01

    and vibrational temperatures of a gliding arc generated at atmospheric pressure air are investigated. Translational temperatures (about 1100 K) were measured by laser-induced Rayleigh scattering, and two-dimensional temperature imaging was performed. Rotational and vibrational temperatures (about 3600 K and 6700...

  12. Study on out-gassing by baking and glow discharge during wall conditioning of vacuum chamber

    International Nuclear Information System (INIS)

    Wang Zhiwen; Wei Weixing; Zhao Yuanqing; He Yanhe; Liao Yikui

    2007-01-01

    The model of out-gassing by baking and glow discharge cleaning (GDC) is set up. The properties of them are studied. Out-gassing by baking is from bulk and it obeys the diffusion equation. Out-gassing of glow discharge cleaning is mainly on surface, it is inducement out-gassing by sputtering. Thus the properties of out-gassing for baking and GDC on the HL-1M tokamak are analyzed. Some empirical formulas are given. (authors)

  13. Nitrogen doping for adhesion improvement of DLC film deposited on Si substrate by Filtered Cathodic Vacuum Arc (FCVA) technique

    Energy Technology Data Exchange (ETDEWEB)

    Bootkul, D., E-mail: mo_duangkhae@hotmail.com [Department of General Science, Faculty of Science, Srinakharinwirot University, Bangkok 10110 (Thailand); Supsermpol, B.; Saenphinit, N. [Western Digital Company, Ayutthaya 13160 (Thailand); Aramwit, C. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50202 (Thailand); Intarasiri, S., E-mail: saweat@gmail.com [Science and Technology Research Institute, Chiang Mai University, Chiang Mai 50202 (Thailand)

    2014-08-15

    Diamond-like carbon (DLC) films have been used in many applications due to their attractive combination of properties including chemical inertness, corrosion protection, biocompatibility, high hardness, and low wear rates. However, they still have some limitations such as high internal stresses and low toughness which lead to poor adhesion of films. Synthesis of nitrogen-doped DLC (N-DLC) offers the possibility of overcoming these limitations. In this study, DLC films, namely tetrahedral amorphous carbon (ta-C) and nitrogen doped tetrahedral amorphous carbon (ta-C:N) were deposited on single crystalline Si wafer substrates using the Filtered Cathodic Vacuum Arc (FCVA) technique. Film characterizations were carried out by Raman spectroscopy, atomic force microscopy (AFM), scanning electron microscopy (SEM), triboindenter tester and nano-scratch tester. Measurement results showed that intentionally doping with nitrogen reduced the carbon sp{sup 3} content and increased the surface roughness in comparison with that of pure ta-C films. The hardness measurement confirmed the Raman and AFM analyses that adding nitrogen in ta-C films decreased the hardness, especially with high nitrogen content. However, the nano-scratch test revealed the increasing of the critical load with nitrogen. This work, then, extended its scope to investigate the properties of double-layer ta-C films which were composed of ta-C:N interlayer of various thickness around 10–30 nm and ta-C top-layer with thickness of around 80 nm. Microstructure characterization demonstrated that a ta-C:N interlayer gradually decreased the sp{sup 3} fraction in the films and increased film roughness whenever the ta-C:N interlayer thickness increased. In this structure, the tribological property in terms of adhesion to the Si substrate was significantly improved by about 20–90%, but the mechanical property in terms of hardness was gradually degraded by about 2–10%, compared to pure ta-C film, when the ta

  14. Double plasma arc in a graphite tube - application of discharge atmospheres

    International Nuclear Information System (INIS)

    Arens, C.; Nickel, H.; Mazurkiewicz, M.; Vukanovic, D.

    1981-01-01

    With a view to safety and economic efficiency element-specific limits are required for permissible impurities in reactor graphite. This leads to the necessity of developing suitable methods of analysis. Emission spectroscopy has proved to be a method of analysis featuring a high detection capability and offering the possibility of determining several elements simultaneously. A prolongation of the particle residence time in the plasma (and, thus, an increase in radiation intensity) was the objective when developing a novel spectrochemical source of excitation. The method uses two d.c. arcs burning in a horizontally arranged graphite tube. The double plasma arc in a graphite tube has proved to be an excellent source of excitation for the analysis of powder and solutions. (orig./IHOE)

  15. Seed Mediated Growth of Gold Nanoparticles Based on Liquid Arc Discharge

    International Nuclear Information System (INIS)

    Ashkarran, Ali Akbar

    2013-01-01

    We report studies on the growth of gold nanoparticles by a seed-mediated approach in solution. The synthetic method is adapted from one we published earlier (Ashkarran et al. Appl. Phys. A 2009, 96, 423). The synthesized gold nanoparticles were characterized by X-ray diffraction (XRD), dynamic light scattering (DLS), UV-Vis spectroscopy, optical imaging and atomic force microscopy (AFM). Optical absorption spectroscopy of the prepared samples at 15 A arc current in HAuCl 4 solution shows a surface plasmon resonance around 520 nm. It is found that sodium citrate acts as a stabilizer and surface capping agent of the colloidal nanoparticles. The intensity of the plasmonic peak of the prepared gold nanoparticles for 1 minute arc duration gradually increases due to seed mediation for up to 6 hours. The formation time of gold nanoparticles at higher seed concentrations is less than that at lower seed concentrations. (plasma technology)

  16. Feasibility of arc-discharge and plasma-sputtering methods in cleaning plasma-facing and diagnostics components of fusion reactors

    Energy Technology Data Exchange (ETDEWEB)

    Hakola, Antti, E-mail: antti.hakola@vtt.fi [VTT Technical Research Centre of Finland, VTT (Finland); Likonen, Jari [VTT Technical Research Centre of Finland, VTT (Finland); Karhunen, Juuso; Korhonen, Juuso T. [Department of Applied Physics, Aalto University (Finland); Aints, Märt; Laan, Matti; Paris, Peeter [Department of Physics, University of Tartu (Estonia); Kolehmainen, Jukka; Koskinen, Mika; Tervakangas, Sanna [DIARC-Technology Oy, Espoo (Finland)

    2015-10-15

    Highlights: • Feasibility of the arc-discharge and plasma-sputtering techniques in removing deposited layers from ITER-relevant samples demonstrated. • Samples with the size of an A4 paper can be cleaned from 1-μm thick deposited layers in 10–20 minutes by the arc-discharge method. • The plasma-sputtering method is 5–10 times slower but the resulting surfaces are very smooth. • Arc-discharge method could be used for rapid cleaning of plasma-facing components during maintenance shutdowns of ITER, plasma sputtering is preferred for diagnostics mirrors. - Abstract: We have studied the feasibility of arc-discharge and plasma-sputtering methods in removing deposited layers from ITER-relevant test samples. Prototype devices have been designed and constructed for the experiments and the cleaning process is monitored by a spectral detection system. The present version of the arc-discharge device is capable of removing 1-μm thick layers from 350-mm{sup 2} areas in 4–8 s, but due to the increased roughness of the cleaned surfaces and signs of local melting, mirror-like surfaces cannot be treated by this technique. The plasma-sputtering approach, for its part, is some 5–10 times slower in removing the deposited layers but no changes in surface roughness or morphology of the samples could be observed after the cleaning phase. The arc-discharge technique could therefore be used for rapid cleaning of plasma-facing components during maintenance shutdowns of ITER while in the case of diagnostics mirrors plasma sputtering is preferred.

  17. Experimental Test Of Whether Electrostatically Charged Micro-organisms And Their Spores Contribute To The Onset Of Arcs Across Vacuum Gaps

    Energy Technology Data Exchange (ETDEWEB)

    none,; Grisham, Larry R.

    2014-02-24

    Recently it was proposed [L.R. Grisham, A. vonHalle, A.F. Carpe, Guy Rossi, K.R. Gilton, E.D. McBride, E.P. Gilson, A. Stepanov, T.N. Stevenson, Physics of Plasma 19 023107 (2012)] that one of the initiators of vacuum voltage breakdown between condu cting electrodes might be micro-organisms and their spores, previously deposited during exposure to air, which tnen become electrostatically charged when an electric potential is applied across the vacuum gap. The note describes a simple experiment to compare the number of voltage-conditioning pulses required to reach the nominal maxium operating voltage across a gap between two metallic conductors in a vacuum, comparing cases in which biological cleaning was done just prior to pump-down with cases where this was not done, with each preceded by exposure to ambient air for three days. Based upon these results, it does not appear that air-deposited microbes and their spores constitute a major pathway for arc initiation, at least for exposure periods of a few days, and for vacuum gaps of a few millimeters, in the regime where voltage holding is usually observed to vary linearly with gap distance

  18. Phase-Shifted Eccentric Core Fiber Bragg Grating Fabricated by Electric Arc Discharge for Directional Bending Measurement.

    Science.gov (United States)

    Ouyang, Yang; Liu, Jianxia; Xu, Xiaofeng; Zhao, Yujia; Zhou, Ai

    2018-04-11

    A phase-shifted eccentric core fiber Bragg grating (PS-ECFBG) fabricated by electric arc discharge (EAD) is presented and demonstrated. It is composed of a fraction of eccentric core fiber fusion spliced in between two pieces of commercial single mode fibers, where a PS-FBG was written. The EAD in this work could flexibly change the amount of phase-shift by changing the discharge number or discharge duration. Because of the offset location of the eccentric core and the ultra-narrow resonant peak of the PS-ECFBG, it has a higher accuracy for measuring the directional bend. The elongation and compression of the eccentric core keep the magnitude of phase shift still unchanged during the bending process. The bending sensitivities of the PS-ECFBG at two opposite most sensitive directions are 57.4 pm/m -1 and -51.5 pm/m -1 , respectively. Besides, the PS-ECFBG has the potential to be a tunable narrow bandpass filter, which has a wider bi-directional adjustable range because of the bending responses. The strain and temperature sensitivities of the PS-ECFBG are experimentally measured as well, which are 0.70 pm/με and 8.85 pm/°C, respectively.

  19. Phase-Shifted Eccentric Core Fiber Bragg Grating Fabricated by Electric Arc Discharge for Directional Bending Measurement

    Directory of Open Access Journals (Sweden)

    Yang Ouyang

    2018-04-01

    Full Text Available A phase-shifted eccentric core fiber Bragg grating (PS-ECFBG fabricated by electric arc discharge (EAD is presented and demonstrated. It is composed of a fraction of eccentric core fiber fusion spliced in between two pieces of commercial single mode fibers, where a PS-FBG was written. The EAD in this work could flexibly change the amount of phase-shift by changing the discharge number or discharge duration. Because of the offset location of the eccentric core and the ultra-narrow resonant peak of the PS-ECFBG, it has a higher accuracy for measuring the directional bend. The elongation and compression of the eccentric core keep the magnitude of phase shift still unchanged during the bending process. The bending sensitivities of the PS-ECFBG at two opposite most sensitive directions are 57.4 pm/m−1 and −51.5 pm/m−1, respectively. Besides, the PS-ECFBG has the potential to be a tunable narrow bandpass filter, which has a wider bi-directional adjustable range because of the bending responses. The strain and temperature sensitivities of the PS-ECFBG are experimentally measured as well, which are 0.70 pm/με and 8.85 pm/°C, respectively.

  20. Production of metal and dielectric films in a combined RF and Arc discharge

    International Nuclear Information System (INIS)

    Gasilin, V.V.; Kunchenko, V.V.; Taran, A.V.; Taran, V.S.

    2003-01-01

    The method of HF-cleaning used before the coatings deposition has been developed. Such method of surface cleaning has proved completely reliable in service and rather simple as compared to 'Bulat' one. HF cleaning allows to operate with metallic and dielectric surfaces without their being heated to the high temperatures. Various working gases (N 2 , O 2 , Ar) can be used during condensation. The combination of arc and HF-plasma sources provided low temperature coatings application (below 200 degree C) with the optimal adhesion properties

  1. Comparative study of two- and three-dimensional modeling on arc discharge phenomena inside a thermal plasma torch with hollow electrodes

    International Nuclear Information System (INIS)

    Kim, Keun Su; Park, Jin Myung; Choi, Sooseok; Kim, Jongin; Hong, Sang Hee

    2008-01-01

    A comparative study between two- and three-dimensional (2D and 3D) modeling is carried out on arc discharge phenomena inside a thermal plasma torch with hollow electrodes, in order to evaluate the effects of arc root configuration characterized by either 2D annular or 3D highly localized attachment on the electrode surface. For this purpose, a more precise 3D transient model has been developed by taking account of 3D arc current distribution and arc root rotation. The 3D simulation results apparently reveal that the 3D arc root attachment brings about the inherent 3D and turbulence nature of plasma fields inside the torch. It is also found that the constricted arc column near the vortex chamber plays an important role in heating and acceleration of injected arc gases by concentrating arc currents on the axis of the hollow electrodes. The inherent 3D nature of arc discharge is well preserved inside the cathode region, while these 3D features slowly diminish behind the vortex chamber where the turbulent flow begins to be developed in the anode region. Based on the present simulation results, it is noted that the mixing effects of the strong turbulent flow on the heat and mass transfer are mainly responsible for the gradual relaxation of the 3D structures of plasma fields into the 2D axisymmetric ones that eventually appear in the anode region near the torch exit. From a detailed comparison of the 3D results with the 2D ones, the arc root configuration seems to have a significant effect on the heat transfer to the electrode surfaces interacting with the turbulent plasma flow. That is, in the 2D simulation based on an axisymmetric stationary model, the turbulence phenomena are fairly underestimated and the amount of heat transferred to the cold anode wall is calculated to be smaller than that obtained in the 3D simulation. For the validation of the numerical simulations, calculated plasma temperatures and axial velocities are compared with experimentally measured ones

  2. Surface hardening of optic materials by deposition of diamond like carbon coatings from separated plasma of arc discharge

    Science.gov (United States)

    Osipkov, A. S.; Bashkov, V. M.; Belyaeva, A. O.; Stepanov, R.; Mironov, Y. M.; Galinovsky, A. L.

    2015-02-01

    This article considers the issue of strengthening of optic materials used in the IR spectrum by deposition of diamond like carbon coatings from separated plasma arc discharge. The report shows results of tests of bare and strengthened optical materials such as BaF2, MgF2, Si, Ge, including the testing of their strength and spectral characteristics. Results for the determination of optical constants for the DLC coatings deposited on substrates of Ge and Si, by using separated plasma, are also presented. Investigations showed that surface hardening of optical materials operable in the IR range, by the deposition of diamond like carbon coating onto their surface, according to this technology, considerably improves operational properties and preserves or improves their optic properties.

  3. In situ synthesis of carbon nanotubes decorated with palladium nanoparticles using arc-discharge in solution method

    International Nuclear Information System (INIS)

    Bera, Debasis; Kuiry, Suresh C.; McCutchen, Matthew; Seal, Sudipta; Heinrich, Helge; Slane, Grady C.

    2004-01-01

    A unique, simple, inexpensive, and one-step synthesis route to produce carbon nanotubes (CNTs) decorated with palladium nanoparticles using a simplified dc arc-discharge in solution is reported. Zero-loss energy filtered transmission electron microscopy and scanning transmission electron microscopy confirm the presence of 3 nm palladium nanoparticles. Such palladium nanoparticles form during the reduction of palladium tetra-chloro-square-planar complex. The deconvoluted x-ray photoelectron spectroscopy envelope shows the presence of palladium on the decorated CNTs. The energy dispersive spectroscopy suggests no functionalization of atomic chlorine to the sidewall of the CNTs. The presence of dislodged graphene sheets with wavy morphology supports the formation of CNTs through the 'scroll mechanism'

  4. Change of the arc attachment mode and its effect on the lifetime in automotive high intensity discharge lamps

    Science.gov (United States)

    Alexejev, Alexander; Flesch, Peter; Mentel, Jürgen; Awakowicz, Peter

    2016-10-01

    In modern cars, the new generation Hg-free high intensity discharge (HID) lamps, the so called xenon lamps, take an important role. The long lifetime of these lamps is achieved by doping the tungsten electrodes with thorium. Thorium forms a dipole layer on the electrode surface, thus reducing the work function of tungsten. However, thoriating the electrodes is also an issue of trade and transport regulation, so a substitute is looked into. This work shows the influence of the arc attachment mode on the lifetime of the lamps. The mode of the arc attachment changes during the run-up phase of automotive HID lamps after a characteristic time period depending, i.e., on the filling of the lamps, which is dominated by scandium. It will be shown that this characteristic time period for the change of the attachment mode determines the long term performance of Hg-free xenon lamps. Measurements attributing the mode change to the scandium density in the filling are presented. The emitter effect of scandium will be suggested to be the reason of the mode change.

  5. Computing anode heating voltage in high-pressure arc discharges and modelling rod electrodes in dc and ac regimes

    International Nuclear Information System (INIS)

    Almeida, N A; Cunha, M D; Benilov, M S

    2017-01-01

    Numerical modelling of near-anode layers in arc discharges in several gases (Ar, Xe and Hg) is performed in a wide range of current densities, anode surface temperatures, and plasma pressures. It is shown that the density of energy flux to the anode is only weakly affected by the anode surface temperature and varies linearly with the current density. This allows one to interpret the results in terms of anode heating voltage (volt equivalent of the heat flux to the anode). The computed data may be useful in different ways. An example considered in this work concerns the evaluation of thermal regime of anodes in the shape of a thin rod operating in the diffuse mode. Invoking the model of nonlinear surface heating for cathodes, one obtains a simple and free of empirical parameters model of thin rod electrodes applicable to dc and ac high-pressure arcs provided that no anode spots are present. The model is applied to a variety of experiments reported in the literature and a good agreement with the experimental data found. (paper)

  6. Fabrication of TiO2/Carbon Photocatalyst using Submerged DC Arc Discharged in Ethanol/Acetic Acid Medium

    Science.gov (United States)

    Saraswati, T. E.; Nandika, A. O.; Andhika, I. F.; Patiha; Purnawan, C.; Wahyuningsih, S.; Rahardjo, S. B.

    2017-05-01

    This study aimed to fabricate a modified photocatalyst of TiO2/C to enhance its performance. The fabrication was achieved using the submerged direct current (DC) arc-discharge method employing two graphite electrodes, one of which was filled with a mixture of carbon powder, TiO2, and binder, in ethanol with acetic acid added in various concentrations. The arc-discharge method was conducted by flowing a current of 10-20 A (~20 V). X-ray diffraction (XRD) patterns showed significant placements of the main peak characteristics of TiO2, C graphite, and titanium carbide. The surface analysis using Fourier transform infrared spectroscopy (FTIR) revealed that fabricated TiO2/C nanoparticles had stretching vibrations of Ti-O, C-H, C═O, C-O, O-H and C═C in the regions of 450-550 cm-1, 2900-2880 cm-1, 1690-1760 cm-1, 1050-1300 cm-1, 3400-3700 cm-1 and ~1600 cm-1, respectively. In addition, the study investigated the photocatalysts of unmodified and modified TiO2/C for photodegradation of methylene blue (MB) dye solution under mercury lamp irradiation. The effectiveness of the degradation was defined by the decrease in 60-minute absorbance under a UV-Vis spectrophotometer. Modified TiO2/C proved to be significantly more efficient in reducing dye concentrations, reaching ~70%. It indicated that the oxygen-containing functional groups have been successfully attached to the surface of the nanoparticles and played a role in enhancing photocatalytic activity.

  7. Characterization of n and p-type ZnO thin films grown by pulsed filtered cathodic vacuum arc system

    International Nuclear Information System (INIS)

    Kavak, H.; Erdogan, E.N.; Ozsahin, I.; Esen, R.

    2010-01-01

    Full text : Semiconductor ZnO thin films with wide band gap attract much interest due to their properties such as chemical stability in hydrogen plasma, high optical transparency in the visible and nearinfrared region. Due to these properties ZnO oxide is a promising materials for electronic or optoelectronic applications such as solar cell (as an antireflecting coating and a transparent conducting material), gas sensors, surface acoustic wave devices. The purpose of this research is to improve the properties of n and p-type ZnO thin films for device applications. Polycrystalline ZnO is naturally n-type and very difficult to dope to make p-type. Therefore nowadays hardly produced p-type ZnO attracts a lot of attention. Nitrogen considered as the best dopant for p-type ZnO thin films.The transparent, conductive and very precise thickness controlled n and p-type semiconducting nanocrystalline ZnO thin films were prepared by pulsed filtered cathodic vacuum arc deposition (PFCVAD) method. Structural, optical and electrical properties of these films were investigated. And also photoluminescence properties of these films were investigated. Transparent p-type ZnO thin films were produced by oxidation of PFCVAD deposited zinc nitride. Zinc nitride thin films were deposited with various thicknesses and under different oxygen pressures on glass substrates. Zinc nitride thin films, which were deposited at room temperatures, were amorphous and the optical transmission was below 70%. For oxidation zinc nitride, the sample was annealed in air starting from 350 degrees Celsium up to 550 degrees Celsium for one hour duration. These XRD patterns imply that zinc nitride thin films converted to zinc oxide thin films with the same hexagonal crystalline structures of ZnO. The optical measurements were made for each annealing temperature and the optical transmissions of ZnO thin films were found better than 90 percent in visible range after annealing over 350 degrees Celsium. By

  8. Single-walled nanohorns and other nanocarbons generated by submerged arc discharge between carbon electrodes in liquid argon and other media

    International Nuclear Information System (INIS)

    Vasu, K; Pramoda, K; Govindaraj, A; Rao, C N R; Moses, K

    2014-01-01

    Arc discharge between two graphite electrodes submerged in different liquid media yields various dimensional nanocarbon structures such as 1D carbon nanotubes and 2D graphene. Single-walled carbon nanohorns (SWNHs) prepared by submerged arc discharge in liquid nitrogen medium are found to have nitrogen impurities. Here, we report the structure and properties of pure and nitrogen-doped SWNHs obtained by submerged arc discharge in a liquid argon medium. The absence of an XPS N 1s signal, which is present in nanohorns obtained in liquid nitrogen, indicate that the nanohorns are free from nitrogen impurities. Raman spectra show a strong defect-induced D band and current–voltage characteristics show a slight nonlinear behavior. N 2 adsorption of pure SWNHs shows type-IV isotherms with a surface area of 300 m 2 g −1 . Adsorption of CO 2 and H 2 in pure SWNHs has also been measured. Arc discharge in other liquid media such as water, ethanol, dimethylformamide (DMF), n-methyl pyrrolidone (NMP), formamide, benzene, heptane and acetone yields different nanocarbon structures including multi-walled carbon nanotubes (MWNTs), few-layer graphene, carbon onions and carbon nanoparticles. (papers)

  9. Does Ultrasound-Guided Directional Vacuum-Assisted Removal Help Eliminate Abnormal Nipple Discharge in Patients with Benign Intraductal Single Mass?

    Energy Technology Data Exchange (ETDEWEB)

    Chang, Jung Min; Cho, Na Ri Ya; Moon, Woo Kyung [Seoul National University Hospital, Seoul (Korea, Republic of); Park, Jeong Seon [Hanyang University Hospital, Seoul (Korea, Republic of); Chung, Se Yeong [Seoul National University Boramae Hospital, Seoul (Korea, Republic of); Jang, Mi Jung [Seoul National University Bundang Hospital, Seongnam (Korea, Republic of)

    2009-12-15

    To evaluate whether the removal of an intraductal mass using an ultrasound (US)-guided directional vacuum-assisted device can eliminate symptoms in patients presenting with abnormal nipple discharge. Between March 2004 and October 2006, 36 patients who presented with abnormal nipple discharge, underwent US-guided, 11-gauge vacuum-assisted biopsy for a benign intraductal single mass on US. The ability of the procedure to eliminate nipple discharge was evaluated by physical examination during follow-up US. Lesion characteristics, biopsy variables, and histologic features were analyzed to identify factors affecting symptom resolution. Of the 36 lesions, 25 (69%) were intraductal papillomas, 10 (28%) were fibrocystic changes, and one (3%) was a fibroadenoma. The nipple discharge disappeared in 69% (25 of 36) of the women at a mean follow-up time of 25 months (range 12-42 month). There was no difference in the lesion characteristics, biopsy variables, and the histologic features between groups that eliminated the symptom compared those with persistent nipple discharge. US-guided directional vacuum-assisted removal of an intraductal mass appears to eliminate nipple discharge in only 69% of patients and thus, it should not be considered as an alternative to surgical excision.

  10. Synthesis of aluminium nanoparticles by arc evaporation of an ...

    Indian Academy of Sciences (India)

    Administrator

    Abstract. Aluminium nanoparticles (Al Nps) are synthesized using arc discharge method by applying direct current between aluminium electrodes in liquid environment without any use of vacuum equipment, heat exchangers, high temperatures furnaces and inert gases. After synthesis of Al Nps, in situ coating process on.

  11. The effect of the operation modes of a gas discharge low-pressure amalgam lamp on the intensity of generation of 185 nm UV vacuum radiation

    Energy Technology Data Exchange (ETDEWEB)

    Vasilyak, L. M., E-mail: vasilyak@ihed.ras.ru [Russian Academy of Sciences, Joint Institute of High Temperatures (Russian Federation); Drozdov, L. A., E-mail: lit@npo.lit.ru; Kostyuchenko, S. V.; Sokolov, D. V. [ZAO LIT (Russian Federation); Kudryavtsev, N. N.; Sobur, D. A., E-mail: soburda@gmail.com [Moscow Institute for Physics and Technology (Russian Federation)

    2011-12-15

    The effect of the discharge current, mercury vapor pressure, and the inert gas pressure on the intensity and efficiency of the 185 nm line generation are considered. The spectra of the UV radiation (vacuum ultraviolet) transmission by protective coatings from the oxides of rare earth metals and aluminum are investigated.

  12. On the theory of non-self-maintained low voltage arc discharge

    International Nuclear Information System (INIS)

    Shcherbinin, P.P.; Cherednichenko, Yu.G.

    1980-01-01

    In the approximation of constant temperature of plasma electrons for two emitter temperatures 1440 and 1830 K calculated are the volt-ampere characteristics and components of the voltage internal drop in a thermionic converter in the cases of self-maintained discharge in cesium and with an external source of atom ionization and electron heating. It is obtained, that using an external ionization source the decrease of voltage drop in the interelectrode gap with account of ionization energy constitutes about 0.1 V. Electron heating is not effective. For further reduction of voltage losses it is necessary to search for ways for decreasing electron Coulomb scattering on ions

  13. Theory of hollow cathode arc discharges. II. Metastable state balance inside the cathode. Application to argon

    International Nuclear Information System (INIS)

    Ferreira, C.M.; Delcroix, J.L.

    1975-01-01

    In the hollow cathode the metastable species are created by fast electrons, which are emitted by the cathode wall and injected in the plasma across a space-charge sheath, and destroyed by Maxwellian electrons. A detailed analysis of the different electronic destruction mechanisms in argon shows that the re-excitation up to 3p 5 4p states plays a very important role. Solutions of the metastable balance equation were obtained in a wide range of variation of the discharge parameters displaying the best conditions of operation to obtain high concentrations [fr

  14. Energy Efficiency and Scalability of Metallic Nanoparticle Production Using Arc/Spark Discharge

    Directory of Open Access Journals (Sweden)

    Martin Slotte

    2017-10-01

    Full Text Available The increased global demand for metallic nanoparticles for an ever growing number of applications has given rise to a need for larger scale and more efficient nanoparticle (NP production processes. In this paper one such process is evaluated from the viewpoints of scalability and energy efficiency. Multiple setups of different scale of an arc/spark process were evaluated for energy efficiency and scalability using exergy analysis, heat loss evaluation and life cycle impact assessment, based on data collected from EU FP7 project partners. The energy efficiency of the process is quite low, with e.g., a specific electricity consumption (SEC of producing ~80 nm copper NP of 180 kWh/kg while the thermodynamic minimum energy need is 0.03 kWh/kg. This is due to thermal energy use characteristics of the system. During scale-up of the process the SEC remained similar to that of smaller setups. Loss of NP mass in the tubing of larger setups gives a lower material yield. The variation in material yield has a significant impact on the life cycle impact for the produced NP in both the Human Health and Ecosystem Quality categories while the impact is smaller in the Global Warming and Resource Depletion categories.

  15. Joule heat generation in thermionic cathodes of high-pressure arc discharges

    Energy Technology Data Exchange (ETDEWEB)

    Benilov, M. S.; Cunha, M. D. [Departamento de Fisica, CCCEE, Universidade da Madeira, Largo do Municipio, 9000 Funchal (Portugal)

    2013-02-14

    The nonlinear surface heating model of plasma-cathode interaction in high-pressure arcs is extended to take into account the Joule effect inside the cathode body. Calculation results are given for different modes of current transfer to tungsten cathodes of different configurations in argon plasmas of atmospheric or higher pressures. Special attention is paid to analysis of energy balances of the cathode and the near-cathode plasma layer. In all the cases, the variation of potential inside the cathode is much smaller than the near-cathode voltage drop. However, this variation can be comparable to the volt equivalent of the energy flux from the plasma to the cathode and then the Joule effect is essential. Such is the case of the diffuse and mixed modes on rod cathodes at high currents, where the Joule heating causes a dramatic change of thermal and electrical regimes of the cathode. The Joule heating has virtually no effect over characteristics of spots on rod and infinite planar cathodes.

  16. Stability of very-high pressure arc discharges against perturbations of the electron temperature

    Energy Technology Data Exchange (ETDEWEB)

    Benilov, M. S. [Departamento de Fisica, Ciencias Exactas e Engenharia, Universidade da Madeira, Largo do Municipio, Funchal 9000 (Portugal); Hechtfischer, U. [Philips Lighting, BU Automotive Lamps, Technology, Philipsstrasse 8, Aachen 52068 (Germany)

    2012-04-01

    We study the stability of the energy balance of the electron gas in very high-pressure plasmas against longitudinal perturbations, using a local dispersion analysis. After deriving a dispersion equation, we apply the model to a very high-pressure (100 bar) xenon plasma and find instability for electron temperatures, T{sub e}, in a window between 2400 K and 5500-7000 K x 10{sup 3} K, depending on the current density (10{sup 6}-10{sup 8} A/m{sup 2}). The instability can be traced back to the Joule heating of the electron gas being a growing function of T{sub e}, which is due to a rising dependence of the electron-atom collision frequency on T{sub e}. We then analyze the T{sub e} range occurring in very high-pressure xenon lamps and conclude that only the near-anode region exhibits T{sub e} sufficiently low for this instability to occur. Indeed, previous experiments have revealed that such lamps develop, under certain conditions, voltage oscillations accompanied by electromagnetic interference, and this instability has been pinned down to the plasma-anode interaction. A relation between the mechanisms of the considered instability and multiple anodic attachments of high-pressure arcs is discussed.

  17. Production of ultrafine particles of high-temperature tetragonal WO3 by dc arc discharge in Ar-O2 gases

    International Nuclear Information System (INIS)

    Guo Yumei; Murata, Norihiko; Ono, Kazuya; Okazaki, Tsugio

    2005-01-01

    Ultrafine particles of WO 3 are successfully produced by dc arc discharge in Ar-O 2 gases. Particle sizes are distributed from 10 nm to 1 μm depending on production conditions: gas pressure, collection position and discharge current. Observations of the cooled particles by electron microscopy indicate that the WO 3 particles are tetragonal, a phase that is usually only stable above 725 deg. C. The octahedral crystals are bounded by eight {1 0 1} faces and occasionally truncated by {1 0 0} and/or {0 0 1} faces. This method of producing WO 3 by dc arc discharge therefore affords a high-temperature phase that is preserved upon cooling to room temperature

  18. Explosion symmetry improvement of polyimide-coated tungsten wire in vacuum on negative discharge facility

    Science.gov (United States)

    Li, Mo; Wu, Jian; Lu, Yihan; Li, Xingwen; Li, Yang; Qiu, Mengtong

    2018-01-01

    Tungsten wire explosion is very asymmetric when fast current rate and insulated coatings are both applied on negative discharge facility using a 24-mm-diameter cathode geometry, which is commonly used on mega-ampere facilities. It is inferred, based on an analytical treatment of the guiding center drift and COMSOL simulations, that the large negative radial electric field causes early voltage breakdown and terminates energy deposition into the wire core on the anode side of the wire. After the anode side is short circuited, the radial electric field along the wire surface on the cathode side will change its polarity and thus leading to additional energy deposition into the wire core. This change causes ˜10 times larger energy deposition and ˜14 times faster explosion velocity in the cathode side than the anode side. In order to reduce this asymmetry, a hollow cylindrical cathode geometry was used to reverse the polarity of radial electric field and was optimized to use on multi-MA facilities. In this case, fully vaporized polyimide-coated tungsten wire with great symmetry improvement was achieved with energy deposition of ˜8.8 eV/atom. The atomic and electronic density distributions for the two different load geometries were obtained by the double-wavelength measurement.

  19. Perspectives of Single-Wall Carbon Nano-tube Production in the Arc Discharge Process

    International Nuclear Information System (INIS)

    Krestinin, A.V.; Kiselev, N.A.; Raevskii, A.V; Ryabenko, A.G.; Zakharov, D.N.; Zvereva, G.I.

    2003-01-01

    Single-wall carbon nano tubes (SWNTs) promise wide applications in many technical fields. As a result purified SWNT material is sold now on the West market at more than 1000 dollars per 1 gram. Thus developing an effective technology for SWNTs production rises to a very important sintofene problem. The perspectives of three existing methods providing raw material in the technology of SWNT production have been analyzed. They are i) pulsed laser evaporation of graphite/metal composites, ii) evaporation of graphite electrodes with metal content in the are discharge process, and iii) catalytic decomposition of the mixture of CO and metal carbonyl catalyst precursor. The observed dynamites of SWNT market points to replacing the laser method of SWNTs production by the are process. The conclusion has been made that the technology based on the are process will be the major one for the fabrication of purified SWNTs at least for the next five years. A reliable estimation of a low price limit of SWNTs was derived from a comparison of two technologies based on the are discharge process: the first one is the production of SWNTs and the second one is the production of a fullerene mixture C 6 0 + C 7 0. The main conclusion was made that the price of purified SWNTs should always be more by 2-3 times the price of fullerene mixture. The parameters of a lab-scale technology for the production of purified SWNTs are listed. A large-scale application of the developed technology is expected to reduce the price of purified SWNTs by approximately ten times. The methods now employed for the characterization of products containing SWNTs are briefly observed. It is concluded that electron microscopy, thermogravimetric analysis, absorption and Raman spectroscopy, measurement of the specific surface aria, optical microscopy - each in separation is not enough for extensive characterization of a sample containing SWNTs, and all these methods should be used together. (author)

  20. Optical and structural properties of carbon dots/TiO2 nanostructures prepared via DC arc discharge in liquid

    Science.gov (United States)

    Biazar, Nooshin; Poursalehi, Reza; Delavari, Hamid

    2018-01-01

    Synthesis and development of visible active catalysts is an important issue in photocatalytic applications of nanomaterials. TiO2 nanostructures coupled with carbon dots demonstrate a considerable photocatalytic activity in visible wavelengths. Extending optical absorption of a wide band gap semiconductor such as TiO2 with carbon dots is the origin of the visible activity of carbon dots modified semiconductor nanostructures. In addition, carbon dots exhibit high photostability, appropriate electron transport and chemical stability without considerable toxicity or environmental footprints. In this study, optical and structural properties of carbon dots/TiO2 nanostructures prepared via (direct current) DC arc discharge in liquid were investigated. Crystal structure, morphology and optical properties of the samples were studied by X-ray diffraction (XRD), scanning electron microscopy (SEM), and UV-visible spectroscopy respectively. SEM images show formation of spherical nanoparticles with an average size of 27 nm. In comparison with pristine TiO2, optical transmission spectrum of carbon dots/TiO2 nanostructures demonstrates an absorption edge at longer wavelengths as well a high optical absorption in visible wavelengths which is significant for visible activity of nanostructures as a photocatalyst. Finally, these results can provide a flexible and versatile pathway for synthesis of carbon dots/oxide semiconductor nanostructures with an appropriate activity under visible light.

  1. Determination of plasma spot current and arc discharge plasma current on the system of plasma cathode electron sources using Rogowski coil technique

    International Nuclear Information System (INIS)

    Wirjoadi; Bambang Siswanto; Lely Susita RM; Agus Purwadi; Sudjatmoko

    2015-01-01

    It has been done the function test experiments of ignitor electrode system and the plasma generator electrode system to determine the current spot plasma and arc discharge plasma current with Rogowski coil technique. Ignitor electrode system that gets power supply from IDPS system can generate the plasma spot current of 11.68 ampere to the pulse width of about 33 μs, this value is greater than the design probably because of electronic components used in the IDPS system was not as planned. For the plasma generator electrode system that gets power from ADPS system capable of producing an arc discharge plasma current around 103.15 amperes with a pulse width of about 96 μs, and this value as planned. Based on the value of the arc discharge plasma current can be determined plasma electron density, which is about 10.12 10"1"9 electrons/m"3, and with this electron density value, an ignitor electrode system and a plasma generator system is quite good if used as a plasma cathode electron source system. (author)

  2. Synthesis method for ultrananocrystalline diamond in powder employing a coaxial arc plasma gun

    Science.gov (United States)

    Naragino, Hiroshi; Tominaga, Aki; Hanada, Kenji; Yoshitake, Tsuyoshi

    2015-07-01

    A new method that enables us to synthesize ultrananocrystalline diamond (UNCD) in powder is proposed. Highly energetic carbon species ejected from a graphite cathode of a coaxial arc plasma gun were provided on a quartz plate at a high density by repeated arc discharge in a compact vacuum chamber, and resultant films automatically peeled from the plate were aggregated and powdered. The grain size was easily controlled from 2.4 to 15.0 nm by changing the arc discharge energy. It was experimentally demonstrated that the proposed method is a new and promising method that enables us to synthesize UNCD in powder easily and controllably.

  3. Synthesis method for ultrananocrystalline diamond in powder employing a coaxial arc plasma gun

    International Nuclear Information System (INIS)

    Naragino, Hiroshi; Tominaga, Aki; Yoshitake, Tsuyoshi; Hanada, Kenji

    2015-01-01

    A new method that enables us to synthesize ultrananocrystalline diamond (UNCD) in powder is proposed. Highly energetic carbon species ejected from a graphite cathode of a coaxial arc plasma gun were provided on a quartz plate at a high density by repeated arc discharge in a compact vacuum chamber, and resultant films automatically peeled from the plate were aggregated and powdered. The grain size was easily controlled from 2.4 to 15.0 nm by changing the arc discharge energy. It was experimentally demonstrated that the proposed method is a new and promising method that enables us to synthesize UNCD in powder easily and controllably. (author)

  4. Selective arc-discharge synthesis of Dy2S-clusterfullerenes and their isomer-dependent single molecule magnetism.

    Science.gov (United States)

    Chen, Chia-Hsiang; Krylov, Denis S; Avdoshenko, Stanislav M; Liu, Fupin; Spree, Lukas; Yadav, Ravi; Alvertis, Antonis; Hozoi, Liviu; Nenkov, Konstantin; Kostanyan, Aram; Greber, Thomas; Wolter, Anja U B; Popov, Alexey A

    2017-09-01

    A method for the selective synthesis of sulfide clusterfullerenes Dy 2 S@C 2 n is developed. Addition of methane to the reactive atmosphere reduces the formation of empty fullerenes in the arc-discharge synthesis, whereas the use of Dy 2 S 3 as a source of metal and sulfur affords sulfide clusterfullerenes as the main fullerene products along with smaller amounts of carbide clusterfullerenes. Two isomers of Dy 2 S@C 82 with C s (6) and C 3v (8) cage symmetry, Dy 2 S@C 72 - C s (10528), and a carbide clusterfullerene Dy 2 C 2 @C 82 - C s (6) were isolated. The molecular structure of both Dy 2 S@C 82 isomers was elucidated by single-crystal X-ray diffraction. SQUID magnetometry demonstrates that all of these clusterfullerenes exhibit hysteresis of magnetization, with Dy 2 S@C 82 - C 3v (8) being the strongest single molecule magnet in the series. DC- and AC-susceptibility measurements were used to determine magnetization relaxation times in the temperature range from 1.6 K to 70 K. Unprecedented magnetization relaxation dynamics with three consequent Orbach processes and energy barriers of 10.5, 48, and 1232 K are determined for Dy 2 S@C 82 - C 3v (8). Dy 2 S@C 82 - C s (6) exhibits faster relaxation of magnetization with two barriers of 15.2 and 523 K. Ab initio calculations were used to interpret experimental data and compare the Dy-sulfide clusterfullerenes to other Dy-clusterfullerenes. The smallest and largest barriers are ascribed to the exchange/dipolar barrier and relaxation via crystal-field states, respectively, whereas an intermediate energy barrier of 48 K in Dy 2 S@C 82 - C 3v (8) is assigned to the local phonon mode, corresponding to the librational motion of the Dy 2 S cluster inside the carbon cage.

  5. Magnetic hysterysis evolution of Ni-Al alloy with Fe and Mn substitution by vacuum arc melting to produce the room temperature magnetocaloric effect material

    Energy Technology Data Exchange (ETDEWEB)

    Notonegoro, Hamdan Akbar [PPS Materials Science, FMIPA-Universitas Indonesia, Depok 16424 (Indonesia); Mechanical Engineering Dept., FT-Universitas Sultan Ageng Tirtayasa, Cilegon 42435 (Indonesia); Kurniawan, Budhy; Manaf, Azwar, E-mail: azwar@sci.ui.ac.id [PPS Materials Science, FMIPA-Universitas Indonesia, Depok 16424 (Indonesia); Setiawan, Jan [Center for Nuclear Fuel Tecnology-Badan Tenaga Atom Nasional, Tangerang Selatan 15310 (Indonesia)

    2016-06-17

    The development of magnetocaloric effect (MCE) material is done in order to reduce the damage of the ozone layer caused by the chlorofluorocarbons (CFCs) emitted into the air. The research dealing with synthesis of magnetocaloric materials based of Ni-Al Heusler Alloy structure and by varying substitution some atoms of Ni with Fe and Al with Mn on Ni-Al Heusler Alloy structure to become Ni{sub 44}Fe{sub 6}Mn{sub 32}Al{sub 18}. Vacuum Arc Melting (VAM) equipment is used to form the alloys on vacuum condition and by flowing argon gas atmosphere and then followed by annealing process for 72 hours. X-Ray Diffraction (XRD) reveals that crystallite structure of material is observed. We define that Ni{sub 44}Fe{sub 6} as X{sub 2}, Mn{sub 25} as Y, and Al{sub 18}Mn{sub 7} as Z. Based on the XRD result, we observed that the general formula X{sub 2}YZ is not changed. The PERMAGRAF measurement revealed that there exists of magnetic hysterysis. The hysterysis show that the magnetic structures of the system undego evolution from diamagnetic to soft ferromagnetic material which all of the compound have the same crystallite structure. This evolution indicated that the change in the composition has led to changes the magnetic composition. Mn is the major element that gives strong magnetic properties to the sample. When Mn partially replaced position of Al, the sample became dominant to be influenced to improve their magnetic properties. In addition, substitution a part of Ni by Fe in the composition reveals a pinning of the domain walls in the sample.

  6. Formation of Sn-M (M=Fe, Al, Ni) alloy nanoparticles by DC arc-discharge and their electrochemical properties as anodes for Li-ion batteries

    Science.gov (United States)

    Gao, Song; Huang, Hao; Wu, Aimin; Yu, Jieyi; Gao, Jian; Dong, Xinglong; Liu, Chunjing; Cao, Guozhong

    2016-10-01

    A direct current arc-discharge method was applied to prepare the Sn-M (M=Fe, Al, Ni) bi-alloy nanoparticles. Thermodynamic is introduced to analyze the energy circumstances for the formation of the nanoparticles during the physical condensation process. The electrochemical properties of as-prepared Sn-M alloy nanoparticles are systematically investigated as anodes of Li-ion batteries. Among them, Sn-Fe nanoparticles electrode exhibits high Coulomb efficiency (about 71.2%) in the initial charge/discharge (257.9 mA h g-1/366.6 mA h g-1) and optimal cycle stability (a specific reversible capacity of 240 mA h g-1 maintained after 20 cycles) compared with others. Large differences in the electrochemical behaviors indicate that the chemical composition and microstructure of the nanoparticles determine the lithium-ion storage properties and the long-term cyclic stability during the charge/discharge process.

  7. Synthesis of graphene-like transparent conductive films on dielectric substrates using a modified filtered vacuum arc system

    Energy Technology Data Exchange (ETDEWEB)

    Lux, Helge, E-mail: lux@th-wildau.de; Schrader, Sigurd [Technical University of Applied Sciences Wildau, Hochschulring 1, Wildau 15745 (Germany); Siemroth, Peter [Arc Precision GmbH, Schwartzkopffstraße 2, Wildau 15745 (Germany); Sgarlata, Anna [Department of Physics, University of Roma - Tor Vergata, Via della Ricerca Scientifica 1, Roma 00133 (Italy); Prosposito, Paolo; Casalboni, Mauro [Department of Industrial Engineering, University of Roma - Tor Vergata, and Italian Interuniversity Consortium on Materials Science and Technology (INSTM), Research Unit Roma Tor Vergata Via del Politecnico 1, Roma 00133 (Italy); Schubert, Markus Andreas [IHP Innovations for High Performance Microelectronics, Im Technologiepark 25, Frankfurt (Oder) 15236 (Germany)

    2015-05-21

    Here, we present a reliable process to deposit transparent conductive films on silicon oxide, quartz, and sapphire using a solid carbon source. This layer consists of partially ordered graphene flakes with a lateral dimension of about 5 nm. The process does not require any catalytic metal and exploits a high current arc evaporation (Φ-HCA) to homogeneously deposit a layer of carbon on heated substrates. A gas atmosphere consisting of Argon or Argon/Hydrogen blend acting as a buffer influences the morphology of the growing film. scanning tunneling microscopy, transmission electron microscopy, and Raman spectra were used for a thorough characterization of the samples in order to optimize the growth parameters. The best carbon layers have a surface resistance of 5.7 × 10{sup 3} Ω{sub ◻} whereas the optical transparency of the coatings is 88% with an excellent homogeneity over areas of several cm{sup 2}. Such results are compatible with most semiconductor fabrication processes and make this method very promising for various industrial applications.

  8. Nonequilibrium phenomena and determination of plasma parameters in the hot core of the cathode region in free-burning arc discharges

    International Nuclear Information System (INIS)

    Kuehn, Gerrit; Kock, Manfred

    2007-01-01

    We present spectroscopic measurements of plasma parameters (electron density n e , electron temperature T e , gas temperature T g , underpopulation factor b) in the hot-core region in front of the cathode of a low-current, free-burning arc discharge in argon under atmospheric pressure. The discharge is operated in the hot-core mode, creating a hot cathode region with plasma parameters similar to high-current arcs in spite of the fact that we use comparatively low currents (less than 20 A). We use continuum emission and (optically thin) line emission to determine n e and T e . We apply relaxation measurements based on a power-interruption technique to investigate deviations from local thermodynamic equilibrium (LTE). These measurements let us determine the gas temperature T g . All measurements are performed side-on with charge-coupled-device cameras as detectors, so that all measured plasma parameters are spatially resolved after an Abel inversion. This yields the first ever spatially resolved observation of the non-LTE phenomena of the hot core in the near-cathode region of free-burning arcs. The results only partly coincide with previously published predictions and measurements in the literature

  9. CO-AXIAL DISCHARGES

    Science.gov (United States)

    Luce, J.S.; Smith, L.P.

    1960-11-22

    A method and apparatus are given for producing coaxial arc discharges in an evacuated enclosure and within a strong, confining magnetic field. The arcs are maintained at a high potential difference. Electrons will diffuse to the more positive arc from the negative arc, and positive ions will diffuse from the more positive arc to the negative arc. Coaxial arc discharges have the advantage that ions which return to strike the positive arc discharge will lose no energy since they do not strike a solid wall or electrode. Those discharges are useful in confining an ionized plasma between the discharges, and have the advantage of preventing impurities from the walls of the enclosure from entering ihe plasma area because of the arc barrier set up bv the cylindrical outer arc.

  10. Phase transitions of doped carbon in CrCN coatings with modified mechanical and tribological properties via filtered cathodic vacuum arc deposition

    Energy Technology Data Exchange (ETDEWEB)

    Guan, J.J. [Faculty of Materials and Energy, Southwest University, Chongqing 400715 (China); Wang, H.Q. [College of Nuclear Science and Technology, Beijing Normal University, Beijing 100875 (China); Qin, L.Z., E-mail: qin8394@163.com [Faculty of Materials and Energy, Southwest University, Chongqing 400715 (China); Liao, B.; Liang, H. [College of Nuclear Science and Technology, Beijing Normal University, Beijing 100875 (China); Li, B. [Faculty of Materials and Energy, Southwest University, Chongqing 400715 (China)

    2017-04-15

    The CrCN coatings were fabricated onto Si (1 1 1) wafers and SUS304 stainless steel plates using filtered cathodic vacuum arc deposition (FCVAD) technique under different flow ratios of N{sub 2}/C{sub 2}H{sub 2} gas mixture. The morphology, crystalline structure and chemical composition of the coatings were characterized. It was found that the grain size reduce with increasing carbon content, which makes the CrCN coatings refined and smooth. The quasi-one-dimensional carbolite phase was also found in CrN host lattice with C{sub 2}H{sub 2} content ranging from 5% to 20%, and it will be evolved into amorphous carbon and amorphous CN{sub x} phases as C{sub 2}H{sub 2} content exceeds 20%. Moreover, we examined the mechanical and tribological properties of the CrCN coatings, and the experimental results confirmed that the friction coefficient of the coatings descend to the lowest value as 0.39 with 30% C{sub 2}H{sub 2} content, due to the graphite (sp{sup 2} C−C) phase embed in CrN host lattice; while the chromium carbon (Cr{sub 3}C{sub 2}) and diamond (sp{sup 3} C−C) phases may give rise to the increase of the coating hardness with the highest value at 23.97 GPa under 20% C{sub 2}H{sub 2} content.

  11. Incidence Angle Effect of Energetic Carbon Ions on Deposition Rate, Topography, and Structure of Ultrathin Amorphous Carbon Films Deposited by Filtered Cathodic Vacuum Arc

    KAUST Repository

    Wang, N.

    2012-07-01

    The effect of the incidence angle of energetic carbon ions on the thickness, topography, and structure of ultrathin amorphous carbon (a-C) films synthesized by filtered cathodic vacuum arc (FCVA) was examined in the context of numerical and experimental results. The thickness of a-C films deposited at different incidence angles was investigated in the light of Monte Carlo simulations, and the calculated depth profiles were compared with those obtained from high-resolution transmission electron microscopy (TEM). The topography and structure of the a-C films were studied by atomic force microscopy (AFM) and X-ray photoelectron spectroscopy (XPS), respectively. The film thickness decreased with the increase of the incidence angle, while the surface roughness increased and the content of tetrahedral carbon hybridization (sp 3) decreased significantly with the increase of the incidence angle above 45° , measured from the surface normal. TEM, AFM, and XPS results indicate that the smoothest and thinnest a-C films with the highest content of sp 3 carbon bonding were produced for an incidence angle of 45°. The findings of this study have direct implications in ultrahigh-density magnetic recording, where ultrathin and smooth a-C films with high sp 3 contents are of critical importance. © 2012 IEEE.

  12. Effect of modulation periods on the microstructure and mechanical properties of DLC/TiC multilayer films deposited by filtered cathodic vacuum arc method

    International Nuclear Information System (INIS)

    Xu, Zhaoying; Sun, H.; Leng, Y.X.; Li, Xueyuan; Yang, Wenmao; Huang, N.

    2015-01-01

    Highlights: • DLC/TiC multilayer films with different modulation periods at same modulation ratio 1:1 were deposited by FCVA. • The residual stress of DLC/TiC multilayer films decreases with the modulation periods decrease. • The hardness of the multilayer DLC films decreases with modulation periods increasing. - Abstract: The high stress of diamond-like carbon (DLC) film limits its thickness and adhesion on substrate. Multilayer structure is one approach to overcome this disadvantage. In this paper, the DLC/TiC multilayer films with different modulation periods (80 nm, 106 nm or 160 nm) at same modulation ratio of 1:1 were deposited on Si(1 0 0) wafer and Ti-6Al-4V substrate by filtered cathodic vacuum arc (FCVA) technology. X-ray diffraction (XRD), transmission electron microscopy (TEM), nanoindention and wear test were employed to investigate the effect of modulation periods on the microstructure and mechanical properties of the multilayer films. The results showed that the residual stress of the DLC/TiC multilayer films could be effectively reduced and the residual stress decreased with the modulation periods decreasing. The hardness of the DLC/TiC multilayer films increased with modulation periods decreasing. The DLC/TiC multilayer film with modulation period of 106 nm had the best wear resistance due to the good combination of hardness, ductility and low compressive stress

  13. Influence of substrate bias on the structure and properties of (Ti, Al)N films deposited by filtered cathodic vacuum arc

    International Nuclear Information System (INIS)

    Cheng, Y.H.; Tay, B.K.; Lau, S.P.; Shi, X.

    2001-01-01

    (Ti, Al)N films were deposited by an off-plane, double-bend, filtered cathodic vacuum arc technique in N 2 atmosphere at room temperature. The (Ti, Al)N films deposited are atomically smooth. The influence of substrate negative bias at the wide range (0-1000 V) on the deposition rate, surface morphology, crystal structure, internal stress, and mechanical properties of (Ti, Al)N films were systematically studied. Increasing substrate bias results in the decrease of deposition rate and the increase of surface roughness monotonically. At the bias of 0 V, (Ti, Al)N films are amorphous, and the internal stress, hardness, and Young's modulus for the deposited films are fairly low. With increasing substrate bias to 200 V, single-phase face-centered cubic-type nanocrystalline (Ti, Al)N films can be obtained, and the internal stress, hardness, and Young's modulus increase to the maximum of 7 GPa, 28 GPa, and 240 GPa, respectively. Further increase of substrate bias results in the decrease of intensity and the broadening of x-ray diffraction lines, and the gradual decrease of internal stress, hardness, and Young's modulus in (Ti, Al)N films

  14. Phase transitions of doped carbon in CrCN coatings with modified mechanical and tribological properties via filtered cathodic vacuum arc deposition

    International Nuclear Information System (INIS)

    Guan, J.J.; Wang, H.Q.; Qin, L.Z.; Liao, B.; Liang, H.; Li, B.

    2017-01-01

    The CrCN coatings were fabricated onto Si (1 1 1) wafers and SUS304 stainless steel plates using filtered cathodic vacuum arc deposition (FCVAD) technique under different flow ratios of N_2/C_2H_2 gas mixture. The morphology, crystalline structure and chemical composition of the coatings were characterized. It was found that the grain size reduce with increasing carbon content, which makes the CrCN coatings refined and smooth. The quasi-one-dimensional carbolite phase was also found in CrN host lattice with C_2H_2 content ranging from 5% to 20%, and it will be evolved into amorphous carbon and amorphous CN_x phases as C_2H_2 content exceeds 20%. Moreover, we examined the mechanical and tribological properties of the CrCN coatings, and the experimental results confirmed that the friction coefficient of the coatings descend to the lowest value as 0.39 with 30% C_2H_2 content, due to the graphite (sp"2 C−C) phase embed in CrN host lattice; while the chromium carbon (Cr_3C_2) and diamond (sp"3 C−C) phases may give rise to the increase of the coating hardness with the highest value at 23.97 GPa under 20% C_2H_2 content.

  15. Phase transitions of doped carbon in CrCN coatings with modified mechanical and tribological properties via filtered cathodic vacuum arc deposition

    Science.gov (United States)

    Guan, J. J.; Wang, H. Q.; Qin, L. Z.; Liao, B.; Liang, H.; Li, B.

    2017-04-01

    The CrCN coatings were fabricated onto Si (1 1 1) wafers and SUS304 stainless steel plates using filtered cathodic vacuum arc deposition (FCVAD) technique under different flow ratios of N2/C2H2 gas mixture. The morphology, crystalline structure and chemical composition of the coatings were characterized. It was found that the grain size reduce with increasing carbon content, which makes the CrCN coatings refined and smooth. The quasi-one-dimensional carbolite phase was also found in CrN host lattice with C2H2 content ranging from 5% to 20%, and it will be evolved into amorphous carbon and amorphous CNx phases as C2H2 content exceeds 20%. Moreover, we examined the mechanical and tribological properties of the CrCN coatings, and the experimental results confirmed that the friction coefficient of the coatings descend to the lowest value as 0.39 with 30% C2H2 content, due to the graphite (sp2 Csbnd C) phase embed in CrN host lattice; while the chromium carbon (Cr3C2) and diamond (sp3 Csbnd C) phases may give rise to the increase of the coating hardness with the highest value at 23.97 GPa under 20% C2H2 content.

  16. Influence of pulsed substrate bias on the structure and properties of Ti-Al-N films deposited by cathodic vacuum arc

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, G.P., E-mail: princeterry@163.com [Institute of Physics, Chinese Academy of Science, Beijing 100080 (China); Gao, G.J. [Changchun University of Science and Technology, College of Science, Changchun 130000 (China); Wang, X.Q.; Lv, G.H.; Zhou, L.; Chen, H.; Pang, H.; Yang, S.Z. [Institute of Physics, Chinese Academy of Science, Beijing 100080 (China)

    2012-07-15

    Ti-Al-N films were deposited by cathodic vacuum arc (CVA) technique in N{sub 2} atmosphere with different pulsed substrate bias. The influence of pulsed substrate bias (0 to -800 V) on the deposition rate, surface morphology, crystal structure, and mechanical properties of the Ti-Al-N films were systematically investigated. Increasing pulsed bias voltage resulted in the decrease of deposition rate but the increase of surface roughness. It was found that there was a strong correlation between the pulsed bias and film structure. All the films studied in this paper were composed of TiN, AlN, and Ti-Al-N ternary phases. The grains changed from equiaxial to columnar and exhibited preferred orientation when the pulsed bias increased. With the increase of pulsed bias voltage, the atomic ratio of Ti to Al element increased gradually, while the N to (Ti + Al) ratio decreased. The composite films present an enhanced nanohardness compared with binary TiN and ZrN films. The film deposited with pulsed bias of -200 V possessed the maximum scratch critical load and nanohardness. The minimum friction coefficient with pulsed bias of -300 V was obtained.

  17. Investigation of the structural, surface, optical and electrical properties of the Indium doped CuxO thin films deposited by a thermionic vacuum arc

    Science.gov (United States)

    Musaoğlu, Caner; Pat, Suat; Özen, Soner; Korkmaz, Şadan; Mohammadigharehbagh, Reza

    2018-03-01

    In this study, investigation of some physical properties of In-doped CuxO thin films onto amorphous glass substrates were done. The thin films were depsoied by thermionic vacuum arc technique (TVA). TVA technique gives a thin film with lower precursor impurity according to the other chemical and physical depsoition methods. The microstructural properties of the produced thin films was determined by x-ray diffraction device (XRD). The thickness values were measured as to be 30 nm and 60 nm, respectively. The miller indices of the thin films’ crystalline planes were determined as to be Cu (111), CuO (\\bar{1} 12), CuInO2 (107) and Cu2O (200), Cu (111), CuO (\\bar{1} 12), CuO (\\bar{2} 02), CuInO2 (015) for sample C1 and C2, respectively. The produced In-doped CuO thin films are in polycrystalline structure. The surface properties of produced In doped CuO thin films were determined by using an atomic force microscope (AFM) and field emission scanning electron microscope (FESEM) tools. The optical properties of the In doped CuO thin films were determined by UV–vis spectrophotometer, interferometer, and photoluminescence devices. p-type semiconductor thin film was obtained by TVA depsoition.

  18. Pressure-dependent synthesis of high-quality few-layer graphene by plasma-enhanced arc discharge and their thermal stability

    International Nuclear Information System (INIS)

    Kumar, Rajesh; Singh, Rajesh Kumar; Dubey, Pawan Kumar; Kumar, Pradip; Tiwari, Radhey Shyam; Oh, Il-Kwon

    2013-01-01

    In this article, a simple and cost-effective method to produce high-quality few-layer graphene (FLG) sheets (∼4 layers) have been achieved by the direct current arc discharge under argon atmosphere, using pure graphite rods as the electrodes. Ar was used as a buffer gas with pure graphite rods as anode and cathode electrodes. We explored the suitable conditions for producing FLG by changing the Ar gas pressure inside the arcing chamber. This method has several advantages over the previous methods to produce graphene for research applications. No toxic and hazardous intercalant was used for producing FLG in this process. The optimum Ar pressure was 500 Torr, for producing minimum number of FLG and this also shows the good thermal stability. The FLG product so obtained has been characterized by X-ray diffraction, scanning and electron microscopy, Raman and Fourier transform infrared spectroscopy. Thermal stabilities of FLG were determined by thermal gravimetric analysis

  19. The electrical, elemental, optical, and surface properties of Si-doped ZnO thin films prepared by thermionic vacuum arc

    Science.gov (United States)

    Mohammadigharehbagh, Reza; Özen, Soner; Yudar, Hafizittin Hakan; Pat, Suat; Korkmaz, Şadan

    2017-09-01

    The purpose of this work is to study the properties of Si-doped ZnO (SZO) thin films, which were prepared using the non-reactive thermionic vacuum arc technique. The analysis of the elemental, optical, and surface properties of ZnO:Si thin films was carried out using energy dispersive x-ray spectroscopy, UV-VIS spectrophotometry, atomic force microscopy, and scanning electron microscopy, respectively. The current-voltage measurement was employed in order to study the electrical properties of the films. The effect of Si doping on the physical properties of ZnO films was investigated. The film thicknesses were measured as 55 and 35 nm for glass and PET substrates, respectively. It was clearly observed from the x-ray diffraction results that the Si and ZnO peaks were present in the coated SZO films for all samples. The morphological studies showed that the deposited surfaces are homogenous, dense, and have a uniform surface, with the existence of some cracks only on the glass substrate. The elemental composition has confirmed the existence of Zn, Si, and O elements within the prepared films. Using a UV-VIS spectrophotometer, the optical parameters such as transmittance, absorbance, refractive index, and reflectance were calculated. It should be noted that the transparency and refractive indices obtained from the measurements decrease with increasing Si concentration. The obtained optical bandgap values using transmittance spectra were determined to be 3.74 and 3.84 eV for the glass and PET substrates, respectively. An increase in the bandgap results demonstrates that the Si doping concentration is comparable to the pure ZnO thin films. The current versus voltage curves revealed the ohmic nature of the films. Subsequently, the development and fabrication of excellent transparent conducting electrodes enabled the appropriate use of Si-doped ZnO thin films.

  20. Inertial electrostatic confinement and nuclear fusion in the interelectrode plasma of a nanosecond vacuum discharge. II: Particle-in-cell simulations

    International Nuclear Information System (INIS)

    Kurilenkov, Yu. K.; Tarakanov, V. P.; Gus'kov, S. Yu.

    2010-01-01

    Results of particle-in-sell simulations of ion acceleration by using the KARAT code in a cylindrical geometry in the problem formulation corresponding to an actual experiment with a low-energy vacuum discharge with a hollow cathode are presented. The fundamental role of the formed virtual cathode is analyzed. The space-time dynamics of potential wells related to the formation of the virtual cathode is discussed. Quasi-steady potential wells (with a depth of ∼80% of the applied voltage) cause acceleration of deuterium ions to energies about the electron beam energy (∼50 keV). In the well, a quasi-isotropic velocity distribution function of fast ions forms. The results obtained are compared with available data on inertial electrostatic confinement fusion (IECF). In particular, similar correlations between the structure of potential wells and the neutron yield, as well as the scaling of the fusion power density, which increases with decreasing virtual cathode radius and increasing potential well depth, are considered. The chosen electrode configuration and potential well parameters provide power densities of nuclear DD fusion in a nanosecond vacuum discharge noticeably higher than those achieved in other similar IECF systems.

  1. Recent advances in incoherent light sources in the vacuum-ultraviolet (88-200nm) based on electric discharge plasmas

    International Nuclear Information System (INIS)

    Ward, B.K.; Carman, R.J.; Mildren, R.P.; Kane, D.M.

    2004-01-01

    Full text: Rare-gas and rare gas-halide excimer lamps are powerful, frequency agile, mercury-free sources of high power, narrow band (10nm-30nm), UV and VUV radiation covering the wavelength range 88nm-320nm. A very efficient and practically convenient method of excitation is achieved using the dielectric barrier discharge (DBD). In the DBD, charge build-up on an insulating (dielectric) barrier at one or both of the electrodes provides an intrinsic mechanism for quenching the discharge before the transition to a high current discharge. The UV/VUV output from rare-gas DBD lamps is highly monochromatic, derived predominantly from 2nd excimer continuum, with negligible output at visible and infrared wavelengths. For DBD lamps powered by sinusoidal voltage waveforms (50Hz-100kHz), the electrical to optical conversion efficiency typically reaches 10-20%. The discharge structure consists of multiple transient plasma aments that occur stochastically in time during the discharge cycle leading to VUV output pulses with irregular spacing and amplitude. We have shown, however, that using discrete high-voltage pulses of relatively short duration, produces a short-lived homogeneous discharge that generates much higher peak power from short (sub-microsecond) VUV output pulses, with an additional increase (two- fold) in overall efficiency. Conversion efficiencies between 40-60% have also been reported for short-pulse excitation techniques. Efficient generation of pulsed, high peak-power VUV output is of interest for a broad range of applications in time-resolved spectroscopy, photo-lithography, materials processing and surface modification/cleaning, killing of micro- organisms and bacteria, sterilization, and in ozone production for water purification

  2. Formation of Sn–M (M=Fe, Al, Ni) alloy nanoparticles by DC arc-discharge and their electrochemical properties as anodes for Li-ion batteries

    International Nuclear Information System (INIS)

    Gao, Song; Huang, Hao; Wu, Aimin; Yu, Jieyi; Gao, Jian; Dong, Xinglong; Liu, Chunjing; Cao, Guozhong

    2016-01-01

    A direct current arc-discharge method was applied to prepare the Sn–M (M=Fe, Al, Ni) bi-alloy nanoparticles. Thermodynamic is introduced to analyze the energy circumstances for the formation of the nanoparticles during the physical condensation process. The electrochemical properties of as-prepared Sn–M alloy nanoparticles are systematically investigated as anodes of Li-ion batteries. Among them, Sn–Fe nanoparticles electrode exhibits high Coulomb efficiency (about 71.2%) in the initial charge/discharge (257.9 mA h g −1 /366.6 mA h g −1 ) and optimal cycle stability (a specific reversible capacity of 240 mA h g −1 maintained after 20 cycles) compared with others. Large differences in the electrochemical behaviors indicate that the chemical composition and microstructure of the nanoparticles determine the lithium-ion storage properties and the long-term cyclic stability during the charge/discharge process. - Graphical abstract: The growth mechanism and electrochemical performance of Sn-based alloy nanoparticles. - Highlights: • Thermodynamic analyses of oxides on Sn-M nanoparticles surface. • The relationship between chemical components and electrochemical responses. • Sn-Fe nanoparticles show excellent electrode performance.

  3. Formation of Sn–M (M=Fe, Al, Ni) alloy nanoparticles by DC arc-discharge and their electrochemical properties as anodes for Li-ion batteries

    Energy Technology Data Exchange (ETDEWEB)

    Gao, Song [Key Laboratory of Materials Modification by Laser, Ion and Electron Beams (Ministry of Education), School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China); Huang, Hao, E-mail: huanghao@dlut.edu.cn [Key Laboratory of Materials Modification by Laser, Ion and Electron Beams (Ministry of Education), School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China); Wu, Aimin; Yu, Jieyi; Gao, Jian; Dong, Xinglong; Liu, Chunjing [Key Laboratory of Materials Modification by Laser, Ion and Electron Beams (Ministry of Education), School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China); Cao, Guozhong, E-mail: gzcao@u.washington.edu [Key Laboratory of Materials Modification by Laser, Ion and Electron Beams (Ministry of Education), School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China); Department of Materials Science and Engineering, University of Washington, Seattle, WA 98195 (United States)

    2016-10-15

    A direct current arc-discharge method was applied to prepare the Sn–M (M=Fe, Al, Ni) bi-alloy nanoparticles. Thermodynamic is introduced to analyze the energy circumstances for the formation of the nanoparticles during the physical condensation process. The electrochemical properties of as-prepared Sn–M alloy nanoparticles are systematically investigated as anodes of Li-ion batteries. Among them, Sn–Fe nanoparticles electrode exhibits high Coulomb efficiency (about 71.2%) in the initial charge/discharge (257.9 mA h g{sup −1}/366.6 mA h g{sup −1}) and optimal cycle stability (a specific reversible capacity of 240 mA h g{sup −1} maintained after 20 cycles) compared with others. Large differences in the electrochemical behaviors indicate that the chemical composition and microstructure of the nanoparticles determine the lithium-ion storage properties and the long-term cyclic stability during the charge/discharge process. - Graphical abstract: The growth mechanism and electrochemical performance of Sn-based alloy nanoparticles. - Highlights: • Thermodynamic analyses of oxides on Sn-M nanoparticles surface. • The relationship between chemical components and electrochemical responses. • Sn-Fe nanoparticles show excellent electrode performance.

  4. X-ray photoelectron spectroscopy of nano-multilayered Zr-O/Al-O coatings deposited by cathodic vacuum arc plasma

    International Nuclear Information System (INIS)

    Zhitomirsky, V.N.; Kim, S.K.; Burstein, L.; Boxman, R.L.

    2010-01-01

    Nano-multilayered Zr-O/Al-O coatings with alternating Zr-O and Al-O layers having a bi-layer period of 6-7 nm and total coating thickness of 1.0-1.2 μm were deposited using a cathodic vacuum arc plasma process on rotating Si substrates. Plasmas generated from two cathodes, Zr and Al, were deposited simultaneously in a mixture of Ar and O 2 background gases. The Zr-O/Al-O coatings, as well as bulk ZrO 2 and Al 2 O 3 reference samples, were studied using X-ray photoelectron spectroscopy (XPS). The XPS spectra were analyzed on the surface and after sputtering with a 4 kV Ar + ion gun. High resolution angle resolved spectra were obtained at three take-off angles: 15 o , 45 o and 75 o relative to the sample surface. It was shown that preferential sputtering of oxygen took place during XPS of bulk reference ZrO 2 samples, producing ZrO and free Zr along with ZrO 2 in the XPS spectra. In contrast, no preferential sputtering was observed with Al 2 O 3 reference samples. The Zr-O/Al-O coatings contained a large amount of free metals along with their oxides. Free Zr and Al were observed in the coating spectra both before and after sputtering, and thus cannot be due solely to preferential sputtering. Transmission electron microscopy revealed that the Zr-O/Al-O coatings had a nano-multilayered structure with well distinguished alternating layers. However, both of the alternating layers of the coating contained of a mixture of aluminum and zirconium oxides and free Al and Zr metals. The concentration of Zr and Al changed periodically with distance normal to the coating surface: the Zr maximum coincided with the Al minimum and vice versa. However the concentration of Zr in both alternating layers was significantly larger than that of Al. Despite the large free metal concentration, the Knoop hardness, 21.5 GPa, was relatively high, which might be attributed to super-lattice formation or formation of a metal-oxide nanocomposite within the layers.

  5. Synthesis of Ti-doped DLC film on SS304 steels by Filtered Cathodic Vacuum Arc (FCVA) technique for tribological improvement

    Science.gov (United States)

    Bootkul, D.; Saenphinit, N.; Supsermpol, B.; Aramwit, C.; Intarasiri, S.

    2014-08-01

    Currently, stainless steels are widely used in various industrial applications due to their excellence in toughness and corrosion resistance. But their resistance to wear needs to be improved for appropriate use in tribological applications. The Filtered Cathodic Vacuum Arc (FCVA) is a superior technique for forming a high-density film structure of amorphous carbon, especially for a tetrahedral amorphous carbon (ta-C) type, because it can produce a plasma of highly energetic ions that can penetrate into a growing coating, resulting in densification of the film. However, this technique tends to generate high internal stress, due to serious accumulation of energy in the film structure that then leads to film delamination. In general, there are numerous solutions that have been used to reduce the internal stress. DLC with various additive elements such as Ti, Cr or W as strong-carbide-forming (SCF) metals is one of the popular methods to provide attractive combinations of properties of wear resistance and film adhesion as well as reducing the internal stress. The present study was focused on investigation of titanium-doped DLC coating on SS304 steel, mainly for adhesion improvement in optimizing for tribological applications. The synthesized films were formed by the FCVA technique at normal substrate temperature. In the experimental set-up, the films were produced by mixing the titanium and carbon ions generated by dual cathode plasma source operating in synchronous pulsed mode. Their compositions were adjusted by varying the relative duration of the pulse length from each cathode. Titanium doping concentration was varied from pure DLC deposition as the control group to titanium and graphite trigger pulses ratios of 1:16, 1:12, 1:10, 1:8 and 1:4, as the Ti-doped DLC group. The results showed that by increasing titanium trigger pulses ratio from 1:16, 1:12, 1:10 and 1:8, respectively, the film adhesion was increased while the wear rate did not change significantly as

  6. Study on nanocomposite Ti-Al-Si-Cu-N films with various Si contents deposited by cathodic vacuum arc ion plating

    Energy Technology Data Exchange (ETDEWEB)

    Shi, J. [State Key Laboratory of Corrosion and Protection, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, Shenyang 110016 (China); Institute of Materials Engineering, University of Siegen, Paul-Bonatz-Strasse 9-11, Siegen 57076 (Germany); Muders, C.M.; Kumar, A. [Institute of Materials Engineering, University of Siegen, Paul-Bonatz-Strasse 9-11, Siegen 57076 (Germany); Jiang, X., E-mail: xin.jiang@uni-siegen.de [Institute of Materials Engineering, University of Siegen, Paul-Bonatz-Strasse 9-11, Siegen 57076 (Germany); Pei, Z.L.; Gong, J. [State Key Laboratory of Corrosion and Protection, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, Shenyang 110016 (China); Sun, C., E-mail: csun@imr.ac.cn [State Key Laboratory of Corrosion and Protection, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, Shenyang 110016 (China)

    2012-10-01

    Highlights: Black-Right-Pointing-Pointer XRD peaks show a tendency of decreasing intensity with increasing Si content. Black-Right-Pointing-Pointer Ti-Al-Si-Cu-N films present different microstructure with increasing Si content. Black-Right-Pointing-Pointer Films with 6 at.% Si content obtain the highest hardness, elastic modulus and H{sup 3}/E{sup 2}. Black-Right-Pointing-Pointer The wear rate decreases with an increase in hardness. - Abstract: In this study, nanocomposite Ti-Al-Si-Cu-N films were deposited on high speed steel substrates by the vacuum cathode arc ion plating (AIP) technique. By virtue of X-ray diffraction (XRD) analysis, X-ray photoelectron spectroscopy (XPS), and field emission scanning electron microscopy (FESEM), the influence of silicon content on the film microstructure and characteristics was investigated systematically, including the chemical composition, crystalline structure as well as cross-section morphologies. With increasing the silicon content, a deterioration of the preferred orientation and a dense globular structure were detected. In the meanwhile, atomic force microscopy (AFM), nano-indentation, Rockwell indenter and reciprocating test were also utilized to analyze the hardness, elastic modulus, H{sup 3}/E{sup 2}, friction coefficient, adhesive strength and wear rate of the Ti-Al-Si-Cu-N films. The results showed that an optimal silicon content correlated with the best mechanical and tribological properties of the presented Ti-Al-Si-Cu-N films existed. With increasing the silicon content, the hardness, elastic modulus and the ratio H{sup 3}/E{sup 2} first were improved gradually, and then were impaired sharply again. When the silicon content reached to 6 at.%, the film possessed the highest hardness, elastic modulus and ratio H{sup 3}/E{sup 2} of approximately 24 GPa, 218 GPa and 0.31, respectively. Besides, films containing both 6 at.% and 10 at.% Si contents obtained a relatively low friction coefficient and a good adhesive

  7. Industry-relevant magnetron sputtering and cathodic arc ultra-high vacuum deposition system for in situ x-ray diffraction studies of thin film growth using high energy synchrotron radiation

    OpenAIRE

    Schroeder, Jeremy; Thomson, W.; Howard, B.; Schell, N.; Näslund, Lars-Åke; Rogström, Lina; Johansson-Jöesaar, Mats P.; Ghafoor, Naureen; Odén, Magnus; Nothnagel, E.; Shepard, A.; Greer, J.; Birch, Jens

    2015-01-01

    We present an industry-relevant, large-scale, ultra-high vacuum (UHV) magnetron sputtering and cathodic arc deposition system purposefully designed for time-resolved in situ thin film deposition/annealing studies using high-energy (greater than50 keV), high photon flux (greater than10(12) ph/s) synchrotron radiation. The high photon flux, combined with a fast-acquisition-time (less than1 s) two-dimensional (2D) detector, permits time-resolved in situ structural analysis of thin film formation...

  8. Industry-relevant magnetron sputtering and cathodic arc ultra-high vacuum deposition system for in situ x-ray diffraction studies of thin film growth using high energy synchrotron radiation.

    Science.gov (United States)

    Schroeder, J L; Thomson, W; Howard, B; Schell, N; Näslund, L-Å; Rogström, L; Johansson-Jõesaar, M P; Ghafoor, N; Odén, M; Nothnagel, E; Shepard, A; Greer, J; Birch, J

    2015-09-01

    We present an industry-relevant, large-scale, ultra-high vacuum (UHV) magnetron sputtering and cathodic arc deposition system purposefully designed for time-resolved in situ thin film deposition/annealing studies using high-energy (>50 keV), high photon flux (>10(12) ph/s) synchrotron radiation. The high photon flux, combined with a fast-acquisition-time (film formation processes. The high-energy synchrotron-radiation based x-rays result in small scattering angles (industry-relevant processes. We openly encourage the materials research community to contact us for collaborative opportunities using this unique and versatile scientific instrument.

  9. Modernization of serial facility 'BULAT-6' for synthesis of vacuum-arc coatings by the method of plasma-based ion implantation and deposition as well as ion hydrogen-free nitriding

    International Nuclear Information System (INIS)

    Shulaev, V.M.; Andreev, A.A.; Rudenko, V.P.

    2008-01-01

    The model of laboratory vacuum-arc facility for realization of the method of plasma-based ion implantation and deposition is worked out by means modernization of serial industrial facility 'BULAT-6'. The facility is suitable for surface modification of instrumental steel items, including the low-alloyed steels with low temperatures of tempering. The low-temperature deposition of coatings on the preliminary nitrided surface of instrument permits obtaining dense coating with minimum maintenance of macroparticles, as well as with coatings superhigh adhesion to the substrate and with superhardness. The coatings possess high property stableness in time.

  10. Three dimensional numerical study of different parameters effect on the external magnetic field applied to center the arc of the horizontal mercury discharge lamp

    Directory of Open Access Journals (Sweden)

    Mohamed Bechir Ben Hamida

    2015-10-01

    Full Text Available The aim of this paper is to evaluate the magnitude of the external magnetic field to be applied to a horizontal mercury discharge lamp such that the Lorentz forces counterbalance buoyancy forces and the hot region of the arc remains centered inside the lamp with the variation of six parameters of the lamp such as the external temperature of the lamp, envelope thickness, convective loss, Interelectrodeslength, pressure and current supply pointing to the influence of the parameters to the compensating magnetic field value. To achieve this objective, a commercial numerical software “Comsol Multiphysics” is used to implement the model that solves the equations of mass, energy and momentum for laminar compressible flow combined with the Laplace equation for the plasma in a three dimensional.

  11. Comparative study of the interface composition of TiN and TiCN hard coatings on high speed steel substrates obtained by arc discharge

    Energy Technology Data Exchange (ETDEWEB)

    Roman, E. (Lab. de Fisica de Superficies, Inst. de Ciencia de Materiales, CSIC, Madrid (Spain)); Segovia, J.L. de (Lab. de Fisica de Superficies, Inst. de Ciencia de Materiales, CSIC, Madrid (Spain)); Alberdi, A. (TEKNIKER, Asociacion de Investigacion Tecnologica, Eibar (Spain)); Calvo, J. (TEKNIKER, Asociacion de Investigacion Tecnologica, Eibar (Spain)); Laucirica, J. (TEKNIKER, Asociacion de Investigacion Tecnologica, Eibar (Spain))

    1993-05-15

    In this paper the composition of the interface of TiN and TiCN hard coatings deposited onto high speed steel substrates obtained by the arc discharge technique is studied using Auger electron spectroscopy at two different substrate temperatures, 520 K and 720 K. The low temperature (520 K) TiN coating developed an oxygen phase at the interface, producing a weak adherence of 40 N, while the high temperature coatings (720 K) had a less intense oxygen phase, giving a greater adherence to the substrate of 60 N. TiCN coatings at 520 K are characterized by a low oxygen intensity at the interface. However, their adherence of 50 N is lower than the value of 60 N for the high temperature TiN coatings and is independent of the substrate temperature. (orig.)

  12. A straightforward method for Vacuum-Ultraviolet flux measurements: The case of the hydrogen discharge lamp and implications for solid-phase actinometry

    International Nuclear Information System (INIS)

    Fulvio, D.; Brieva, A. C.; Jäger, C.; Cuylle, S. H.; Linnartz, H.; Henning, T.

    2014-01-01

    Vacuum-Ultraviolet (VUV) radiation is responsible for the photo-processing of simple and complex molecules in several terrestrial and extraterrestrial environments. In the laboratory such radiation is commonly simulated by inexpensive and easy-to-use microwave-powered hydrogen discharge lamps. However, VUV flux measurements are not trivial and the methods/devices typically used for this purpose, mainly actinometry and calibrated VUV silicon photodiodes, are not very accurate or expensive and lack of general suitability to experimental setups. Here, we present a straightforward method for measuring the VUV photon flux based on the photoelectric effect and using a gold photodetector. This method is easily applicable to most experimental setups, bypasses the major problems of the other methods, and provides reliable flux measurements. As a case study, the method is applied to a microwave-powered hydrogen discharge lamp. In addition, the comparison of these flux measurements to those obtained by O 2 actinometry experiments allow us to estimate the quantum yield (QY) values QY 122  = 0.44 ± 0.16 and QY 160  = 0.87 ± 0.30 for solid-phase O 2 actinometry.

  13. A straightforward method for Vacuum-Ultraviolet flux measurements: The case of the hydrogen discharge lamp and implications for solid-phase actinometry

    Energy Technology Data Exchange (ETDEWEB)

    Fulvio, D., E-mail: daniele.fulvio@uni-jena.de, E-mail: dfu@oact.inaf.it; Brieva, A. C.; Jäger, C. [Laboratory Astrophysics Group of the Max Planck Institute for Astronomy at the Friedrich Schiller University Jena, Institute of Solid State Physics, Helmholtzweg 3, D-07743 Jena (Germany); Cuylle, S. H.; Linnartz, H. [Raymond and Beverly Sackler Laboratory for Astrophysics, Leiden Observatory, Leiden University, P.O. box 9513, 2300 RA Leiden (Netherlands); Henning, T. [Max Planck Institute for Astronomy, Königstuhl 17, D-69117 Heidelberg (Germany)

    2014-07-07

    Vacuum-Ultraviolet (VUV) radiation is responsible for the photo-processing of simple and complex molecules in several terrestrial and extraterrestrial environments. In the laboratory such radiation is commonly simulated by inexpensive and easy-to-use microwave-powered hydrogen discharge lamps. However, VUV flux measurements are not trivial and the methods/devices typically used for this purpose, mainly actinometry and calibrated VUV silicon photodiodes, are not very accurate or expensive and lack of general suitability to experimental setups. Here, we present a straightforward method for measuring the VUV photon flux based on the photoelectric effect and using a gold photodetector. This method is easily applicable to most experimental setups, bypasses the major problems of the other methods, and provides reliable flux measurements. As a case study, the method is applied to a microwave-powered hydrogen discharge lamp. In addition, the comparison of these flux measurements to those obtained by O{sub 2} actinometry experiments allow us to estimate the quantum yield (QY) values QY{sub 122} = 0.44 ± 0.16 and QY{sub 160} = 0.87 ± 0.30 for solid-phase O{sub 2} actinometry.

  14. Spectroscopic investigations of the vacuum ultra-violet emission in a normal-incidence region from JFT-2 tokamak discharge

    International Nuclear Information System (INIS)

    Kasai, Satoshi; Funahashi, Akimasa; Tazima, Teruhiko; Nakamura, Yukiharu

    1976-10-01

    Spectroscopic investigations have been performed in the wavelength range of 600 to 2300 A on a JFT-2 plasma with peak plasma current 76 kAmp, toroidal magnetic field 9 kGauss, and electron and ion temperature 300--350 eV and 200 eV respectively. Time-histories were measured of spectral lines radiating from oxygen and carbon impurities. The radial profiles of CV(2270.9 A) and OVII(1623.3 A) lines were measured, which showed the spatial distributions with cylindrical shells. The experimental results are compared with the theoretical ones calculated numerically by using a plasma model based on the coronal equilibrium and particle loss due to the diffusion process. Time-variation of the electron temperature during the initial phase of discharge are estimated from the measured time-histories of impurity lines, and the peak electron temperature agrees with that determined from measurements of the ruby laser scattering. The spatial distributions of CV and OVII lines are reasonably explained by the inward-diffusion flux and the diffusion flux, which is several ten times of Pfirsch-Schlueter's one. (auth.)

  15. Vacuum ultraviolet emission spectrum measurement of a microwave-discharge hydrogen-flow lamp in several configurations: Application to photodesorption of CO ice

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Y.-J.; Wu, C.-Y. R. [Space Sciences Center and Department of Physics and Astronomy, University of Southern California, Los Angeles, CA 90089-1341 (United States); Chuang, K.-J.; Chu, C.-C.; Yih, T.-S. [Department of Physics, National Central University, Jhongli City, Taoyuan County 32054, Taiwan (China); Muñoz Caro, G. M. [Centro de Astrobiología, INTA-CSIC, Torrejón de Ardoz, E-28850 Madrid (Spain); Nuevo, M. [NASA Ames Research Center, Moffett Field, CA 94035 (United States); Ip, W.-H., E-mail: yujung@usc.edu [Graduate Institute of Astronomy, National Central University, Jhongli City, Taoyuan County 32049, Taiwan (China)

    2014-01-20

    We report measurements of the vacuum ultraviolet (VUV) emission spectra of a microwave-discharge hydrogen-flow lamp (MDHL), a common tool in astrochemistry laboratories working on ice VUV photoprocessing. The MDHL provides hydrogen Ly-α (121.6 nm) and H{sub 2} molecular emission in the 110-180 nm range. We show that the spectral characteristics of the VUV light emitted in this range, in particular the relative proportion of Ly-α to molecular emission bands, strongly depend on the pressure of H{sub 2} inside the lamp, the lamp geometry (F type versus T type), the gas used (pure H{sub 2} versus H{sub 2} seeded in He), and the optical properties of the window used (MgF{sub 2} versus CaF{sub 2}). These different configurations are used to study the VUV irradiation of CO ice at 14 K. In contrast to the majority of studies dedicated to the VUV irradiation of astrophysical ice analogs, which have not taken into consideration the emission spectrum of the MDHL, our results show that the processes induced by photons in CO ice from a broad energy range are different and more complex than the sum of individual processes induced by monochromatic sources spanning the same energy range, as a result of the existence of multistate electronic transitions and discrepancy in absorption cross sections between parent molecules and products in the Ly-α and H{sub 2} molecular emission ranges.

  16. Vacuum ultraviolet emission spectrum measurement of a microwave-discharge hydrogen-flow lamp in several configurations: Application to photodesorption of CO ice

    International Nuclear Information System (INIS)

    Chen, Y.-J.; Wu, C.-Y. R.; Chuang, K.-J.; Chu, C.-C.; Yih, T.-S.; Muñoz Caro, G. M.; Nuevo, M.; Ip, W.-H.

    2014-01-01

    We report measurements of the vacuum ultraviolet (VUV) emission spectra of a microwave-discharge hydrogen-flow lamp (MDHL), a common tool in astrochemistry laboratories working on ice VUV photoprocessing. The MDHL provides hydrogen Ly-α (121.6 nm) and H 2 molecular emission in the 110-180 nm range. We show that the spectral characteristics of the VUV light emitted in this range, in particular the relative proportion of Ly-α to molecular emission bands, strongly depend on the pressure of H 2 inside the lamp, the lamp geometry (F type versus T type), the gas used (pure H 2 versus H 2 seeded in He), and the optical properties of the window used (MgF 2 versus CaF 2 ). These different configurations are used to study the VUV irradiation of CO ice at 14 K. In contrast to the majority of studies dedicated to the VUV irradiation of astrophysical ice analogs, which have not taken into consideration the emission spectrum of the MDHL, our results show that the processes induced by photons in CO ice from a broad energy range are different and more complex than the sum of individual processes induced by monochromatic sources spanning the same energy range, as a result of the existence of multistate electronic transitions and discrepancy in absorption cross sections between parent molecules and products in the Ly-α and H 2 molecular emission ranges.

  17. ZnO nanoparticles decorated on graphene sheets through liquid arc discharge approach with enhanced photocatalytic performance under visible-light

    International Nuclear Information System (INIS)

    Ashkarran, Ali Akbar; Mohammadi, Bahareh

    2015-01-01

    Graphical abstract: TEM image of ZnO–graphene composite. - Highlights: • Innovative approach for synthesis of zinc oxide–graphene (ZnO–G) hybrid nanostructures. • Combination of bottom-up and top-down methods. • Decoration of ZnO nanoparticles on the surface of graphene. • Visible-light photocatalytic performance. - Abstract: We present an innovative approach for synthesis of zinc oxide–graphene (ZnO–G) hybrid nanostructures through combination of improved hummer and arc discharge methods in liquid. A detailed study of the considerable visible-light photocatalytic activities of these nanostructures for the degradation of Phenol red (PR) and Methyl orange (MO) as standard organic compounds under the irradiation of 90 W halogen light for 2 h has been performed. The ZnO–G nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Brunauer Emmett Teller (BET) and ultra violet–visible absorption spectroscopy (UV–vis). The results revealed that the ZnO–G nanostructures extended the light absorption spectrum toward the visible region and remarkably enhanced the photodegradation of standard dyes under visible-light irradiation. It has been confirmed that the ZnO–G nanostructures could be excited by visible-light (E ∼ 2.6 eV). The major enhancement in the photocatalytic activity of ZnO–G nanostructures under visible-light irradiation can be attributed to the effect of electron transport among ZnO nanoparticles (NPs) and graphene sheets. A mechanism for photocatalytic degradation of organic pollutants over ZnO–G photocatalyst was proposed based on our observations

  18. ZnO nanoparticles decorated on graphene sheets through liquid arc discharge approach with enhanced photocatalytic performance under visible-light

    Energy Technology Data Exchange (ETDEWEB)

    Ashkarran, Ali Akbar, E-mail: ashkarran@umz.ac.ir; Mohammadi, Bahareh

    2015-07-01

    Graphical abstract: TEM image of ZnO–graphene composite. - Highlights: • Innovative approach for synthesis of zinc oxide–graphene (ZnO–G) hybrid nanostructures. • Combination of bottom-up and top-down methods. • Decoration of ZnO nanoparticles on the surface of graphene. • Visible-light photocatalytic performance. - Abstract: We present an innovative approach for synthesis of zinc oxide–graphene (ZnO–G) hybrid nanostructures through combination of improved hummer and arc discharge methods in liquid. A detailed study of the considerable visible-light photocatalytic activities of these nanostructures for the degradation of Phenol red (PR) and Methyl orange (MO) as standard organic compounds under the irradiation of 90 W halogen light for 2 h has been performed. The ZnO–G nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Brunauer Emmett Teller (BET) and ultra violet–visible absorption spectroscopy (UV–vis). The results revealed that the ZnO–G nanostructures extended the light absorption spectrum toward the visible region and remarkably enhanced the photodegradation of standard dyes under visible-light irradiation. It has been confirmed that the ZnO–G nanostructures could be excited by visible-light (E ∼ 2.6 eV). The major enhancement in the photocatalytic activity of ZnO–G nanostructures under visible-light irradiation can be attributed to the effect of electron transport among ZnO nanoparticles (NPs) and graphene sheets. A mechanism for photocatalytic degradation of organic pollutants over ZnO–G photocatalyst was proposed based on our observations.

  19. Arcing phenomena in fusion devices workshop

    International Nuclear Information System (INIS)

    Clausing, R.E.

    1979-01-01

    The workshop on arcing phenomena in fusion devices was organized (1) to review the pesent status of our understanding of arcing as it relates to confinement devices, (2) to determine what informaion is needed to suppress arcing and (3) to define both laboratory and in-situ experiments which can ultimately lead to reduction of impurities in the plasma caused by arcing. The workshop was attended by experts in the area of vacuum arc electrode phenomena and ion source technology, materials scientists, and both theoreticians and experimentalists engaged in assessing the importance of unipolar arcing in today's tokamaks. Abstracts for papers presented at the workshop are included

  20. Regression Analysis of the Effect of Bias Voltage on Nano- and Macrotribological Properties of Diamond-Like Carbon Films Deposited by a Filtered Cathodic Vacuum Arc Ion-Plating Method

    Directory of Open Access Journals (Sweden)

    Shojiro Miyake

    2014-01-01

    Full Text Available Diamond-like carbon (DLC films are deposited by bend filtered cathodic vacuum arc (FCVA technique with DC and pulsed bias voltage. The effects of varying bias voltage on nanoindentation and nanowear properties were evaluated by atomic force microscopy. DLC films deposited with DC bias voltage of −50 V exhibited the greatest hardness at approximately 50 GPa, a low modulus of dissipation, low elastic modulus to nanoindentation hardness ratio, and high nanowear resistance. Nanoindentation hardness was positively correlated with the Raman peak ratio Id/Ig, whereas wear depth was negatively correlated with this ratio. These nanotribological properties highly depend on the films’ nanostructures. The tribological properties of the FCVA-DLC films were also investigated using a ball-on-disk test. The average friction coefficient of DLC films deposited with DC bias voltage was lower than that of DLC films deposited with pulse bias voltage. The friction coefficient calculated from the ball-on-disk test was correlated with the nanoindentation hardness in dry conditions. However, under boundary lubrication conditions, the friction coefficient and specific wear rate had little correlation with nanoindentation hardness, and wear behavior seemed to be influenced by other factors such as adhesion strength between the film and substrate.

  1. Gas and plasma dynamics of RF discharge jet of low pressure in a vacuum chamber with flat electrodes and inside tube, influence of RF discharge on the steel surface parameters

    Science.gov (United States)

    Khristoliubova, V. I.; Kashapov, N. F.; Shaekhov, M. F.

    2016-06-01

    Researches results of the characteristics of the RF discharge jet of low pressure and the discharge influence on the surface modification of high speed and structural steels are introduced in the article. Gas dynamics, power and energy parameters of the RF low pressure discharge flow in the discharge chamber and the electrode gap are studied in the presence of the materials. Plasma flow rate, discharge power, the concentration of electrons, the density of RF power, the ion current density, and the energy of the ions bombarding the surface materials are considered for the definition of basic properties crucial for the process of surface modification of materials as they were put in the plasma jet. The influence of the workpiece and effect of products complex configuration on the RF discharge jet of low pressure is defined. The correlation of the input parameters of the plasma unit on the characteristics of the discharge is established.

  2. Filtered cathodic arc source

    International Nuclear Information System (INIS)

    Falabella, S.; Sanders, D.M.

    1994-01-01

    A continuous, cathodic arc ion source coupled to a macro-particle filter capable of separation or elimination of macro-particles from the ion flux produced by cathodic arc discharge is described. The ion source employs an axial magnetic field on a cathode (target) having tapered sides to confine the arc, thereby providing high target material utilization. A bent magnetic field is used to guide the metal ions from the target to the part to be coated. The macro-particle filter consists of two straight solenoids, end to end, but placed at 45 degree to one another, which prevents line-of-sight from the arc spot on the target to the parts to be coated, yet provides a path for ions and electrons to flow, and includes a series of baffles for trapping the macro-particles. 3 figures

  3. Effects of oxygen gas flow rates and Ga contents on structural properties of Ga-doped ZnO films prepared by ion-plating with a DC arc discharge

    International Nuclear Information System (INIS)

    Terasako, Tomoaki; Nomoto, Junichi; Makino, Hisao; Yamamoto, Naoki; Shirakata, Sho; Yamamoto, Tetsuya

    2015-01-01

    Structural properties of highly c-axis oriented polycrystalline Ga-doped ZnO (GZO) films prepared by ion-plating with a DC arc discharge were studied in terms of the oxygen gas flow rate (F O2 ) introduced into the chamber during the deposition process and the Ga 2 O 3 content in the GZO sintered pellet. The X-ray diffraction (XRD) measurements revealed that the GZO films have the residual compressive stress along the a-axis direction (in-plane) and the tensile stress along the c-axis direction (out-of-plane). The increase in F O2 or the increase in Ga 2 O 3 content was effective for relaxing the in-plane compressive stress induced by the so-called atomic peening effect. The positive correlation between the carrier concentration (n) and the primitive cell volume (V) would be due to the incorporation of Ga atoms substituting Zn sites (Ga Zn s) together with the generation of n-type intrinsic defects or complex defects. - Highlights: • Films of Ga-doped ZnO (GZO) films were deposited by ion-plating with a DC arc discharge. • Structural properties of GZO films were examined by X-ray diffraction measurements. • GZO films had the residual compressive stress along the a-axis direction. • There was the correlation between the carrier concentration and the cell volume.

  4. Effects of oxygen gas flow rates and Ga contents on structural properties of Ga-doped ZnO films prepared by ion-plating with a DC arc discharge

    Energy Technology Data Exchange (ETDEWEB)

    Terasako, Tomoaki, E-mail: terasako.tomoaki.mz@ehime-u.ac.jp [Graduate School of Science and Engineering, Ehime University, 3 Bunkyo-cho, Matsuyama-shi, Ehime 790-8577 (Japan); Nomoto, Junichi; Makino, Hisao; Yamamoto, Naoki [Research Institute, Kochi University of Technology, 185 Miyanokuchi, Tosayamada-cho, Kami-shi, Kochi 782-8502 (Japan); Shirakata, Sho [Graduate School of Science and Engineering, Ehime University, 3 Bunkyo-cho, Matsuyama-shi, Ehime 790-8577 (Japan); Yamamoto, Tetsuya [Research Institute, Kochi University of Technology, 185 Miyanokuchi, Tosayamada-cho, Kami-shi, Kochi 782-8502 (Japan)

    2015-12-01

    Structural properties of highly c-axis oriented polycrystalline Ga-doped ZnO (GZO) films prepared by ion-plating with a DC arc discharge were studied in terms of the oxygen gas flow rate (F{sub O2}) introduced into the chamber during the deposition process and the Ga{sub 2}O{sub 3} content in the GZO sintered pellet. The X-ray diffraction (XRD) measurements revealed that the GZO films have the residual compressive stress along the a-axis direction (in-plane) and the tensile stress along the c-axis direction (out-of-plane). The increase in F{sub O2} or the increase in Ga{sub 2}O{sub 3} content was effective for relaxing the in-plane compressive stress induced by the so-called atomic peening effect. The positive correlation between the carrier concentration (n) and the primitive cell volume (V) would be due to the incorporation of Ga atoms substituting Zn sites (Ga{sub Zn}s) together with the generation of n-type intrinsic defects or complex defects. - Highlights: • Films of Ga-doped ZnO (GZO) films were deposited by ion-plating with a DC arc discharge. • Structural properties of GZO films were examined by X-ray diffraction measurements. • GZO films had the residual compressive stress along the a-axis direction. • There was the correlation between the carrier concentration and the cell volume.

  5. 2D arc-PIC code description: methods and documentation

    CERN Document Server

    Timko, Helga

    2011-01-01

    Vacuum discharges are one of the main limiting factors for future linear collider designs such as that of the Compact LInear Collider. To optimize machine efficiency, maintaining the highest feasible accelerating gradient below a certain breakdown rate is desirable; understanding breakdowns can therefore help us to achieve this goal. As a part of ongoing theoretical research on vacuum discharges at the Helsinki Institute of Physics, the build-up of plasma can be investigated through the particle-in-cell method. For this purpose, we have developed the 2D Arc-PIC code introduced here. We present an exhaustive description of the 2D Arc-PIC code in two parts. In the first part, we introduce the particle-in-cell method in general and detail the techniques used in the code. In the second part, we provide a documentation and derivation of the key equations occurring in the code. The code is original work of the author, written in 2010, and is therefore under the copyright of the author. The development of the code h...

  6. Researches on Position Detection for Vacuum Switch Electrode

    Science.gov (United States)

    Dong, Huajun; Guo, Yingjie; Li, Jie; Kong, Yihan

    2018-03-01

    Form and transformation character of vacuum arc is important influencing factor on the vacuum switch performance, and the dynamic separations of electrode is the chief effecting factor on the transformation of vacuum arcs forms. Consequently, how to detect the position of electrode to calculate the separations in the arcs image is of great significance. However, gray level distribution of vacuum arcs image isn’t even, the gray level of burning arcs is high, but the gray level of electrode is low, meanwhile, the forms of vacuum arcs changes sharply, the problems above restrict electrode position detection precisely. In this paper, algorithm of detecting electrode position base on vacuum arcs image was proposed. The digital image processing technology was used in vacuum switch arcs image analysis, the upper edge and lower edge were detected respectively, then linear fitting was done using the result of edge detection, the fitting result was the position of electrode, thus, accurate position detection of electrode was realized. From the experimental results, we can see that: algorithm described in this paper detected upper and lower edge of arcs successfully and the position of electrode was obtained through calculation.

  7. Angina - discharge

    Science.gov (United States)

    Chest pain - discharge; Stable angina - discharge; Chronic angina - discharge; Variant angina - discharge; Angina pectoris - discharge; Accelerating angina - discharge; New-onset angina - discharge; Angina-unstable - discharge; ...

  8. Fabrication of a segmented composite stainless steel-alumina discharge tube for a theta-pinch coil

    International Nuclear Information System (INIS)

    Dickinson, J.M.; Stoddard, S.D.; Muller, J.F.

    1975-11-01

    An 80-mm-diam segmented discharge tube that simulated in a simplified way the blanket and first wall of the Reference Theta-Pinch Reactor (RTPR) has been constructed. The segments were fabricated by plasma-arc spraying an alumina coating on tubular stainless steel trapezoids. These were laid up to form a cylinder that was contained in a fully dense alumina vacuum tube. The fabrication processes are discussed in detail

  9. Electric arc behaviour in dynamic magnetic fields

    International Nuclear Information System (INIS)

    Put'ko, V.F.

    2000-01-01

    The behaviour of an electric arc in different time-dependent (dynamic) magnetic fields was investigated. New possibilities were found for spatial and energy stabilisation of a discharge, for intensifying heat exchange, extending the electric arc and distributed control of electric arc plasma. Rotating, alternating and travelling magnetic fields were studied. It was found that under the effect of a relatively low frequency of variations of dynamic magnetic fields (f 1000 Hz) the arc stabilised at the axis of the discharge chamber, the pulsation level decreased and discharge stability increased. The borders between these two arc existence modes were formed by a certain critical field variation frequency the period of which was determined by the heat relaxation time of the discharge. (author)

  10. ARC Operations

    Science.gov (United States)

    coordination on a regular basis. The overall ARC organizational structure is shown below. Organizational Structure Dynamics and Control of Vehicles Human Centered Modeling and Simulation High Performance

  11. Model of discharge lamps with magnetic ballast

    OpenAIRE

    Molina, Julio; Sainz Sapera, Luis; Mesas García, Juan José; Bergas Jané, Joan Gabriel

    2013-01-01

    Magnetic ballast discharge lamp modeling has been extensively studied because these lamps can be an important source of harmonics. Discharge lamp models usually represent the arc voltage by a square waveform. However, this waveform can be far from actual arc voltages, which affects the accuracy of the lamp models. This paper investigates the actual arc voltage behavior of discharge lamps from laboratory measurements and proposes a novel characterization of these voltages to reformulate the co...

  12. Vacuum Technology

    Energy Technology Data Exchange (ETDEWEB)

    Biltoft, P J

    2004-10-15

    The environmental condition called vacuum is created any time the pressure of a gas is reduced compared to atmospheric pressure. On earth we typically create a vacuum by connecting a pump capable of moving gas to a relatively leak free vessel. Through operation of the gas pump the number of gas molecules per unit volume is decreased within the vessel. As soon as one creates a vacuum natural forces (in this case entropy) work to restore equilibrium pressure; the practical effect of this is that gas molecules attempt to enter the evacuated space by any means possible. It is useful to think of vacuum in terms of a gas at a pressure below atmospheric pressure. In even the best vacuum vessels ever created there are approximately 3,500,000 molecules of gas per cubic meter of volume remaining inside the vessel. The lowest pressure environment known is in interstellar space where there are approximately four molecules of gas per cubic meter. Researchers are currently developing vacuum technology components (pumps, gauges, valves, etc.) using micro electro mechanical systems (MEMS) technology. Miniature vacuum components and systems will open the possibility for significant savings in energy cost and will open the doors to advances in electronics, manufacturing and semiconductor fabrication. In conclusion, an understanding of the basic principles of vacuum technology as presented in this summary is essential for the successful execution of all projects that involve vacuum technology. Using the principles described above, a practitioner of vacuum technology can design a vacuum system that will achieve the project requirements.

  13. Investigations into electrical discharges in gases

    CERN Document Server

    Klyarfel'D, B N

    2013-01-01

    Investigations into Electrical Discharges in Gases is a compilation of scientific articles that covers the advances in the investigation of the fundamental processes occurring in electrical discharges in gases and vapors. The book details the different aspects of the whole life cycle of an arc, which include the initiation of a discharge, its transition into an arc, the lateral spread of the arc column, and the recovery of electric strength after extinction of an arc. The text also discusses the methods for the dynamic measurement of vapor density in the vicinity of electrical discharges, alon

  14. Vacuum extraction

    DEFF Research Database (Denmark)

    Maagaard, Mathilde; Oestergaard, Jeanett; Johansen, Marianne

    2012-01-01

    Objectives. To develop and validate an Objective Structured Assessment of Technical Skills (OSATS) scale for vacuum extraction. Design. Two-part study design: Primarily, development of a procedure-specific checklist for vacuum extraction. Hereafter, validation of the developed OSATS scale for vac...

  15. Vacuum mechatronics

    Science.gov (United States)

    Hackwood, Susan; Belinski, Steven E.; Beni, Gerardo

    1989-01-01

    The discipline of vacuum mechatronics is defined as the design and development of vacuum-compatible computer-controlled mechanisms for manipulating, sensing and testing in a vacuum environment. The importance of vacuum mechatronics is growing with an increased application of vacuum in space studies and in manufacturing for material processing, medicine, microelectronics, emission studies, lyophylisation, freeze drying and packaging. The quickly developing field of vacuum mechatronics will also be the driving force for the realization of an advanced era of totally enclosed clean manufacturing cells. High technology manufacturing has increasingly demanding requirements for precision manipulation, in situ process monitoring and contamination-free environments. To remove the contamination problems associated with human workers, the tendency in many manufacturing processes is to move towards total automation. This will become a requirement in the near future for e.g., microelectronics manufacturing. Automation in ultra-clean manufacturing environments is evolving into the concept of self-contained and fully enclosed manufacturing. A Self Contained Automated Robotic Factory (SCARF) is being developed as a flexible research facility for totally enclosed manufacturing. The construction and successful operation of a SCARF will provide a novel, flexible, self-contained, clean, vacuum manufacturing environment. SCARF also requires very high reliability and intelligent control. The trends in vacuum mechatronics and some of the key research issues are reviewed.

  16. The ARCS radial collimator

    International Nuclear Information System (INIS)

    Stone, M.B.; Abernathy, D.L.; Niedziela, J.L.; Overbay, M.A.

    2015-01-01

    We have designed, installed, and commissioned a scattered beam radial collimator for use at the ARCS Wide Angular Range Chopper Spectrometer at the Spallation Neutron Source. The collimator has been designed to work effectively for thermal and epithermal neutrons and with a range of sample environments. Other design considerations include the accommodation of working within a high vacuum environment and having the ability to quickly install and remove the collimator from the scattered beam. The collimator is composed of collimating blades (or septa). The septa are 12 micron thick Kapton foils coated on each side with 39 microns of enriched boron carbide ( 10 B 4 C with 10 B > 96%) in an ultra-high vacuum compatible binder. The collimator blades represent an additional 22 m 2 of surface area. In the article we present collimator's design and performance and methodologies for its effective use

  17. High thrust-to-power ratio micro-cathode arc thruster

    Directory of Open Access Journals (Sweden)

    Joseph Lukas

    2016-02-01

    Full Text Available The Micro-Cathode Arc Thruster (μCAT is an electric propulsion device that ablates solid cathode material, through an electrical vacuum arc discharge, to create plasma and ultimately produce thrust in the μN to mN range. About 90% of the arc discharge current is conducted by electrons, which go toward heating the anode and contribute very little to thrust, with only the remaining 10% going toward thrust in the form of ion current. A preliminary set of experiments were conducted to show that, at the same power level, thrust may increase by utilizing an ablative anode. It was shown that ablative anode particles were found on a collection plate, compared to no particles from a non-ablative anode, while another experiment showed an increase in ion-to-arc current by approximately 40% at low frequencies compared to the non-ablative anode. Utilizing anode ablation leads to an increase in thrust-to-power ratio in the case of the μCAT.

  18. Growth feature of ionic nitrogen doped CN_x bilayer films with Ti and TiN interlayer by pulse cathode arc discharge

    International Nuclear Information System (INIS)

    Zhou, Bing; Liu, Zhubo; Piliptsou, D.G.; Rogachev, A.V.; Yu, Shengwang; Wu, Yanxia; Tang, Bin; Rudenkov, A.S.

    2016-01-01

    Graphical abstract: - Highlights: • Ti/ and TiN/CN_x (N"+) bilayers are prepared at various frequencies by pulse cathode arc. • Ti interlayer facilitates the introduction of N atoms into the CN_x (N"+) films. • The most N-sp"2C bonds (mainly graphite-like N) present in the TiN/CN_x (N"+, 3 Hz) film. • Ti/CN_x (N"+, 3 Hz) bilayer possesses small size and disordering of Csp"2 clusters. • The higher hardness and the lower stress presents in the TiN/CN_x (N"+, 10 Hz) bilayer. - Abstract: Using nano-scaled Ti and TiN as interlayer, ionic nitrogen doped carbon (CN_x (N"+)) bilayer films were prepared at various pulse frequencies by cathode arc technique. Elemental distribution at the interface, bonding compositions, microstructure, and mechanical properties of CN_x (N"+) bilayer films were investigated in dependence of interlayer and pulse frequency by Auger electron spectroscopy, X-ray photoelectron spectroscopy, Raman spectroscopy, nanoindentation, and surface profilometer. The results showed that the diffusion extent of C atoms at the interface of CN_x (N"+) bilayers is higher than for the α-C and CN_x (N_2) bilayers with the same interlayer. Nitrogen atoms could diffuse throughout the pre-deposited Ti and TiN layers into the Si substrate for all CN_x (N"+) bilayers. Ti interlayer facilitates the introduction of N atoms into the CN_x (N"+) films and exhibits a certain catalytic effect on the coordination of N atoms with sp"2- and sp"3-C binding. More nitrogenated and intense CN bonding configurations (mainly graphite-like N) form in the TiN/CN_x (N"+) bilayer. Ti/CN_x (N"+) bilayer prepared at low frequency possesses small size and disordering of Csp"2 clusters but TiN interlayer weakens the formation of Csp"2 bonding and increases the disordering of Csp"2 clusters in the films. The residual stress in the bilayer is lower than for CN_x (N"+) monolayer. The higher hardness and the lower residual stress are present in the TiN/CN_x (N"+, 10 Hz) bilayer.

  19. Etching Effect of an Atmospheric DC Arc Plasmatron

    International Nuclear Information System (INIS)

    Chun, Se Min; Kim, Ji Hun; Kang, In Je; Lee, Heon Ju

    2010-01-01

    Thermal plasmas (especially arc plasma) were extensively industrialized, principally by aeronautic sector. Cold plasma technologies have been developed in the microelectronics but their vacuum equipment limits their implantation. Plasmas used in dry etching, thin film deposition and surface treatment for display or semiconductor industries are operating at low pressures in very costly due to the use of vacuum equipment and vacuum components. Use of DC arc plasmatrons in welding, soldering, and cutting of metals is well known. A DC-arc plasmatron with high durability was reported to be a suitable device for etching silicon and photo-resist surfaces

  20. Cosmic vacuum

    International Nuclear Information System (INIS)

    Chernin, Artur D

    2001-01-01

    Recent observational studies of distant supernovae have suggested the existence of cosmic vacuum whose energy density exceeds the total density of all the other energy components in the Universe. The vacuum produces the field of antigravity that causes the cosmological expansion to accelerate. It is this accelerated expansion that has been discovered in the observations. The discovery of cosmic vacuum radically changes our current understanding of the present state of the Universe. It also poses new challenges to both cosmology and fundamental physics. Why is the density of vacuum what it is? Why do the densities of the cosmic energy components differ in exact value but agree in order of magnitude? On the other hand, the discovery made at large cosmological distances of hundreds and thousands Mpc provides new insights into the dynamics of the nearby Universe, the motions of galaxies in the local volume of 10 - 20 Mpc where the cosmological expansion was originally discovered. (reviews of topical problems)

  1. Cosmic vacuum

    Energy Technology Data Exchange (ETDEWEB)

    Chernin, Artur D [P.K. Shternberg State Astronomical Institute at the M.V. Lomonosov Moscow State University, Moscow (Russian Federation)

    2001-11-30

    Recent observational studies of distant supernovae have suggested the existence of cosmic vacuum whose energy density exceeds the total density of all the other energy components in the Universe. The vacuum produces the field of antigravity that causes the cosmological expansion to accelerate. It is this accelerated expansion that has been discovered in the observations. The discovery of cosmic vacuum radically changes our current understanding of the present state of the Universe. It also poses new challenges to both cosmology and fundamental physics. Why is the density of vacuum what it is? Why do the densities of the cosmic energy components differ in exact value but agree in order of magnitude? On the other hand, the discovery made at large cosmological distances of hundreds and thousands Mpc provides new insights into the dynamics of the nearby Universe, the motions of galaxies in the local volume of 10 - 20 Mpc where the cosmological expansion was originally discovered. (reviews of topical problems)

  2. Progress in vacuum metal extraction, refining and consolidation

    International Nuclear Information System (INIS)

    Sundaram, C.V.; Mukherjee, T.K.; Sharma, B.P.

    1973-01-01

    The unique achievements in the process metallurgy of rare metals in the past quarter century should largely be attributed to advances in vacuum technology. New standards for high purity, increasing demand for pure metals and alloys for established applications, and steady improvement in sophistication and capacity of vacuum furnaces have provided the stimulus for developing and expanding vacuum metal extraction processes, and also exploring totally new processes. The paper discusses the thermochemistry of vacuum metallurgy, carbothermic and metallothermic reduction reactions, consolidation and refining by vacuum arc melting, electron beam melting and high temperature high vacuum sintering, and ultrapurification, with special reference to the reactive and refractory metals of Group IV to VI. (author)

  3. Diffuse and spot mode of cathode arc attachments in an atmospheric magnetically rotating argon arc

    International Nuclear Information System (INIS)

    Chen, Tang; Wang, Cheng; Liao, Meng-Ran; Xia, Wei-Dong

    2016-01-01

    A model including the cathode, near-cathode region, and arc column was constructed. Specifically, a thermal perturbation layer at the arc fringe was calculated in order to couple sheath/presheath modelling with typical arc column modelling. Comparative investigation of two modes of attachment of a dc (100, 150, 200 A) atmospheric-pressure arc in argon to a thermionic cathode made of pure tungsten was conducted. Computational data revealed that there exists two modes of arc discharge: the spot mode, which has an obvious cathode surface temperature peak in the arc attachment centre; and the diffuse mode, which has a flat cathode surface temperature distribution and a larger arc attachment area. The modelling results of the arc attachment agree with previous experimental observations for the diffuse mode. A further 3D simulation is obviously needed to investigate the non-axisymmetrical features, especially for the spot mode. (paper)

  4. Glow discharging device

    International Nuclear Information System (INIS)

    Maeno, Katsuki; Kawasaki, Kozo; Hiratsuka, Hajime; Kawashima, Shuichi.

    1989-01-01

    In a thermonuclear device, etc. impurities adsorbed to inner walls of a vacuum vessel by glow discharge are released to clean the vacuum vessel for preventing intrusion of the impurities into plasmas. The object of the present invention is to minimize the capacity of a power source equipment for the glow discharge device to the least extent. That is, a stabilization resistance is connected in series between each of a plurality of anodes which are inserted and arranged at the inside of a vacuum vessel as a cathode and a power source respectively. The resistance value R is selected so as to satisfy the relation: R < (Vi - Vm)/Ii, in which Vi: glow discharge starting voltage, Vm: glow discharge keeping voltage, Ii: glow discharge starting current. Accordingly, if a voltage is applied from a power source to a plurality of anodes, scattering of electric discharge between the anodes can be suppressed and the effect of voltage drop during discharge by the stabilization resistance can be eliminated. As a result, it is possible to provide an economically advantageous glow discharge device with the capacity for the power source facility being to the least extent. (K.M.)

  5. Electric arc radius and characteristics

    International Nuclear Information System (INIS)

    Fang, T.M.

    1980-01-01

    The heat transfer equation of an arc discharge has been solved. The arc is assumed to be a cylinder with negligible axial variation and the dominant heat transfer process is conduction radially inside the column and radiation/convection at the outside edge. The symmetric consideration allows a simple one-dimensional formulation. By taking into account proper variation of the electrical conductivity as function of temperature, the heat balance equation has been solved analytically. The radius of the arc and its current-field characteristics have also been obtained. The conventional results that E approx. I 0 5385 and R approx. I 0 7693 with E being the applied field, I the current, and R the radius of the cylindrical arc, have been proved to be simply limiting cases of our more general characteristics. The results can be applied quite widely including, among others, the neutral beam injection project in nuclear fusion and MHD energy conversion

  6. Arcing and surface damage in DITE

    International Nuclear Information System (INIS)

    Goodall, D.H.J.; McCracken, G.M.

    1977-11-01

    An investigation into the arcing damage on surfaces exposed to plasmas in the DITE tokamak is described. It has been found that arcing occurs on the fixed limiters, on probes inserted into the plasma and on parts of the torus structure. For surfaces parallel to the toroidal field most of the arcs run across the surface orthogonal to the field direction. Observations in the scanning electron microscope show that the arc tracks are formed by a series of melted craters characteristic of cathode arc spots. The amount of metal removed from the surface is consistent with the concentration of metal observed in the plasma. In plasmas with hydrogen gas puffing during the discharge or with injection of low Z impurities, the arc tracks are observed to be much shallower than in normal low density discharges. Several types of surface damage other than arc tracks have also been observed on probes. These phenomena occur less frequently than arcing and appear to be associated with abnormal discharge conditions. (author)

  7. Stability of alternating current gliding arcs

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Salewski, Mirko; Leipold, Frank

    2014-01-01

    on Ohm’s law indicates that the critical length of alternating current (AC) gliding arc discharge columns can be larger than that of a corresponding direct current (DC) gliding arc. This finding is supported by previously published images of AC and DC gliding arcs. Furthermore, the analysis shows......A gliding arc is a quenched plasma that can be operated as a non-thermal plasma at atmospheric pressure and that is thus suitable for large-scale plasma surface treatment. For its practical industrial use the discharge should be extended stably in ambient air. A simple analytical calculation based...... that the critical length can be increased by increasing the AC frequency, decreasing the serial resistance and lowering the gas flow rate. The predicted dependence of gas flow rate on the arc length is experimentally demonstrated. The gap width is varied to study an optimal electrode design, since the extended non...

  8. Vacuum gauges

    International Nuclear Information System (INIS)

    Power, B.D.; Priestland, C.R.D.

    1978-01-01

    This invention relates to vacuum gauges, particularly of the type known as Penning gauges, which are cold cathode ionisation gauges, in which a magnetic field is used to lengthen the electron path and thereby increase the number of ions produced. (author)

  9. Dynamic voltage-current characteristics for a water jet plasma arc

    International Nuclear Information System (INIS)

    Yang Jiaxiang; Lan Sheng; Xu Zuoming

    2008-01-01

    A virtual instrument technology is used to measure arc current, arc voltage, dynamic V-I characteristics, and nonlinear conductance for a cone-shaped water jet plasma arc under ac voltage. Experimental results show that ac arc discharge mainly happens in water vapor evaporated from water when heated. However, due to water's cooling effect and its conductance, arc conductance, reignition voltage, extinguish voltage, and current zero time are very different from those for ac arc discharge in gas work fluid. These can be valuable to further studies on mechanism and characteristics of plasma ac discharge in water, and even in gas work fluid

  10. Arc modeling for welding analysis

    International Nuclear Information System (INIS)

    Glickstein, S.S.

    1978-04-01

    A one-dimensional model of the welding arc that considers heat generation by the Joule effect and heat losses by radiation and conduction has been used to study the effects of various gases and gas mixtures currently employed for welding applications. Minor additions of low ionization potential impurities to these gases are shown to significantly perturb the electrical properties of the parent gas causing gross changes in the radial temperature distribution of the arc discharge. Such changes are reflected in the current density distribution and ultimately in the input energy distribution to the weldment. The result is observed as a variation in weld penetration. Recently published experiments and analyses of welding arcs are also evaluated and shown to contain erroneous data and results. Contrary to previous beliefs, the inclusion of a radiation loss term in the basic energy balance equation is important and cannot be considered as negligible in an argon arc at temperatures as low as 10,000 0 K. The one-dimensional analysis of the welding arc as well as the evaluation of these earlier published reports helps to explain the effects of various gases used for welding, improves our understanding of the physics of the welding arc, and provides a stepping stone for a more elaborate model which can be applied to help optimize welding parameters

  11. Physical characteristics of welding arc ignition process

    Science.gov (United States)

    Shi, Linan; Song, Yonglun; Xiao, Tianjiao; Ran, Guowei

    2012-07-01

    The existing research of welding arc mainly focuses on the stable combustion state and the research on the mechanism of welding arc ignition process is quite lack. The tungsten inert gas(TIG) touch arc ignition process is observed via a high speed camera and the high time resolution spectral diagnosis system. The changing phenomenon of main ionized element provided the electrons in the arc ignition is found. The metallic element is the main contributor to provide the electrons at the beginning of the discharging, and then the excitated shielding gas element replaces the function of the metallic element. The electron density during the period of the arc ignition is calculated by the Stark-broadened lines of Hα. Through the discussion with the repeatability in relaxation phenomenon, the statistical regularity in the arc ignition process is analyzed. The similar rules as above are observed through the comparison with the laser-assisted arc ignition experiments and the metal inert gas(MIG) arc ignition experiments. This research is helpful to further understanding on the generation mechanism of welding arc ignition and also has a certain academic and practical significance on enriching the welding physical theoretical foundation and improving the precise monitoring on automatic arc welding process.

  12. Experimental laser fusion devices and related vacuum problems

    International Nuclear Information System (INIS)

    O'Neal, W.C.; Campbell, D.E.; Glaros, S.S.; Hurley, C.A.; Kobierecki, M.W.; McFann, C.B. Jr.; Monjes, J.A.; Patton, H.G.; Rienecker, F. Jr.

    1977-01-01

    Laser fusion experiments require hard vacuum in the laser-beam spatial filters, target chambers and for target diagnostics instruments. Laser focusing lenses and windows, and target alignment windows must hold vacuum without optical distortion, and must be protected from target debris. The vacuum must be sufficient to prevent residual gas breakdown in focused laser light, avoid arcing at high voltage terminals, minimize contamination and melting of cryogenic targets, and prevent adsorption of the target's microfusion radiation before it reaches the diagnostics instruments

  13. Initial conditioning of the TFTR vacuum vessel

    International Nuclear Information System (INIS)

    Dylla, H.F.; Blanchard, W.R.; Krawchuk, R.B.; Hawryluk, R.J.; Owens, D.K.

    1984-01-01

    We report on the initial conditioning of the Tokamak Fusion Test Reactor (TFTR) vacuum vessel prior to the initiation of first plasma discharges, and during subsequent operation with high power ohmically-heated plasmas. Following evacuation of the 86 m 3 vessel with the 10 4 1/s high vacuum pumping system, the vessel was conditioned by a 15 A dc glow discharge in H 2 at a pressure of 5 mTorr. Rapid-pulse discharge cleaning was used subsequently to preferentially condition the graphite plasma limiters. The effectiveness of the discharge cleaning was monitored by measuring the exhaust rates of the primary discharge products (CO/C 2 H 4 , CH 4 , and H 2 O). After 175 hours of glow discharge treatment, the equivalent of 50 monolayers of C and O was removed from the vessel, and the partial pressures of impurity gases were reduced to the range of 10 -9 -10 -10 Torr

  14. Quasi-equilibrium channel model of an constant current arc

    Directory of Open Access Journals (Sweden)

    Gerasimov Alexander V.

    2003-01-01

    Full Text Available The rather simple method of calculation of electronic and gas temperature in the channel of arc of plasma generator is offered. This method is based on self-consistent two-temperature channel model of an electric arc. The method proposed enables to obtain radial allocation of gas and electronic temperatures in a non-conducting zone of an constant current arc, for prescribed parameters of discharge (current intensity and power of the discharge, with enough good precision. The results obtained can be used in model and engineering calculations to estimate gas and electronic temperatures in the channel of an arc plasma generator.

  15. Re-circulating linac vacuum system

    International Nuclear Information System (INIS)

    Wells, Russell P.; Corlett, John N.; Zholents, Alexander A.

    2003-01-01

    The vacuum system for a proposed 2.5 GeV, 10ΜA recirculating linac synchrotron light source [1] is readily achievable with conventional vacuum hardware and established fabrication processes. Some of the difficult technical challenges associated with synchrotron light source storage rings are sidestepped by the relatively low beam current and short beam lifetime requirements of a re-circulating linac. This minimal lifetime requirement leads directly to relatively high limits on the background gas pressure through much of the facility. The 10ΜA average beam current produces very little synchrotron radiation induced gas desorption and thus the need for an ante-chamber in the vacuum chamber is eliminated. In the arc bend magnets, and the insertion devices, the vacuum chamber dimensions can be selected to balance the coherent synchrotron radiation and resistive wall wakefield effects, while maintaining the modest limits on the gas pressure and minimal outgassing

  16. Arc saw development report

    International Nuclear Information System (INIS)

    Deichelbohrer, P.R.; Beitel, G.A.

    1981-01-01

    The arc saw is one of the key components of the Contaminated Equipment Volume Reduction (CEVR) Program. This report describes the progress of the arc saw from its inception to its current developmental status. History of the arc saw and early contributors are discussed. Particular features of the arc saw and their advantages for CEVR are detailed. Development of the arc saw including theory of operation, pertinent experimental results, plans for the large arc saw and advanced control systems are covered. Associated topics such as potential applications for the arc saw and other arc saw installations in the world is also touched upon

  17. High-current magnetron discharge with magnetic insulation of anode

    International Nuclear Information System (INIS)

    Bizyukov, A.A.; Sereda, K.N.; Sleptsov, V.V.

    2008-01-01

    In magnetron discharge at currents higher then critical which magnitude is in the range of 15...30 A the transition from glow discharge in transverse magnetic field to arc discharge occurs. In the present time the problem of arc blowout is solved at the expense of pulse and HF power supply applying. In this paper the alternative method of limiting current of magnetron discharge increasing at the expense of increasing of discharge gap resistance by means of additional anode layer transverse magnetic field and arc current interruption by sectioning of current collector of anode surface is carrying out

  18. Pancreatitis - discharge

    Science.gov (United States)

    Chronic pancreatitis - discharge; Pancreatitis - chronic - discharge; Pancreatic insufficiency - discharge; Acute pancreatitis - discharge ... You were in the hospital because you have pancreatitis. This is a swelling of the pancreas. You ...

  19. A centre-triggered magnesium fuelled cathodic arc thruster uses sublimation to deliver a record high specific impulse

    Science.gov (United States)

    Neumann, Patrick R. C.; Bilek, Marcela; McKenzie, David R.

    2016-08-01

    The cathodic arc is a high current, low voltage discharge that operates in vacuum and provides a stream of highly ionised plasma from a solid conducting cathode. The high ion velocities, together with the high ionisation fraction and the quasineutrality of the exhaust stream, make the cathodic arc an attractive plasma source for spacecraft propulsion applications. The specific impulse of the cathodic arc thruster is substantially increased when the emission of neutral species is reduced. Here, we demonstrate a reduction of neutral emission by exploiting sublimation in cathode spots and enhanced ionisation of the plasma in short, high-current pulses. This, combined with the enhanced directionality due to the efficient erosion profiles created by centre-triggering, substantially increases the specific impulse. We present experimentally measured specific impulses and jet power efficiencies for titanium and magnesium fuels. Our Mg fuelled source provides the highest reported specific impulse for a gridless ion thruster and is competitive with all flight rated ion thrusters. We present a model based on cathode sublimation and melting at the cathodic arc spot explaining the outstanding performance of the Mg fuelled source. A further significant advantage of an Mg-fuelled thruster is the abundance of Mg in asteroidal material and in space junk, providing an opportunity for utilising these resources in space.

  20. High-vacuum plasma pump

    International Nuclear Information System (INIS)

    Dorodnov, A.M.; Minajchev, V.E.; Miroshkin, S.I.

    1980-01-01

    The action of an electric-arc high-vacuum pump intended for evacuating the volumes in which the operation processes are followed by a high gas evolution is considered. The operation of the pump is based on the principle of controlling the getter feed according to the gas load and effect of plasma sorbtion pumping. The pump performances are given. The starting pressure is about 5 Pa, the limiting residual pressure is about 5x10 -6 Pa, the pumping out rate of nitrogen in the pressure range 5x10 -5 -5x10 -3 Pa accounts for about 4000 l/s, the power consumption comes to 6 kW. Analyzing the results of the test operation of the pump, it has been concluded that its principal advantages are the high starting pressure, controlled getter feed rate and possibility of pumping out the gases which are usually pumped out with difficulty. The operation reliability of the pump is defined mainly by reliable operation of the ignition system of the vacuum arc [ru

  1. Optical arc sensor using energy harvesting power source

    Science.gov (United States)

    Choi, Kyoo Nam; Rho, Hee Hyuk

    2016-06-01

    Wireless sensors without external power supply gained considerable attention due to convenience both in installation and operation. Optical arc detecting sensor equipping with self sustaining power supply using energy harvesting method was investigated. Continuous energy harvesting method was attempted using thermoelectric generator to supply standby power in micro ampere scale and operating power in mA scale. Peltier module with heat-sink was used for high efficiency electricity generator. Optical arc detecting sensor with hybrid filter showed insensitivity to fluorescent and incandescent lamps under simulated distribution panel condition. Signal processing using integrating function showed selective arc discharge detection capability to different arc energy levels, with a resolution below 17J energy difference, unaffected by bursting arc waveform. The sensor showed possibility for application to arc discharge detecting sensor in power distribution panel. Also experiment with proposed continuous energy harvesting method using thermoelectric power showed possibility as a self sustainable power source of remote sensor.

  2. Optical arc sensor using energy harvesting power source

    Energy Technology Data Exchange (ETDEWEB)

    Choi, Kyoo Nam, E-mail: knchoi@inu.ac.kr; Rho, Hee Hyuk, E-mail: rdoubleh0902@inu.ac.kr [Dept. of Information and Telecommunication Engineering Incheon National University Incheon 22012 (Korea, Republic of)

    2016-06-03

    Wireless sensors without external power supply gained considerable attention due to convenience both in installation and operation. Optical arc detecting sensor equipping with self sustaining power supply using energy harvesting method was investigated. Continuous energy harvesting method was attempted using thermoelectric generator to supply standby power in micro ampere scale and operating power in mA scale. Peltier module with heat-sink was used for high efficiency electricity generator. Optical arc detecting sensor with hybrid filter showed insensitivity to fluorescent and incandescent lamps under simulated distribution panel condition. Signal processing using integrating function showed selective arc discharge detection capability to different arc energy levels, with a resolution below 17 J energy difference, unaffected by bursting arc waveform. The sensor showed possibility for application to arc discharge detecting sensor in power distribution panel. Also experiment with proposed continuous energy harvesting method using thermoelectric power showed possibility as a self sustainable power source of remote sensor.

  3. Electric discharges in an electrostatic machine. Analysis of work by J.A. Staniforth and C.M. Cooke

    International Nuclear Information System (INIS)

    Frick, G.

    1988-04-01

    Electric discharges, stored energy, and transient phenomena in electrostatic accelerators are reviewed in the framework of the Vivitron project. Before discharge, predischarge phenomena governed by the value of the electric field and the geometry appear. Transient phenomena appear after discharge. The alternance lasts from 20 to 100 nsec. Waves propagating along the electrodes can cause other discharges, after a time lapse. Overvoltages of a factor of 1.5 to 2 can appear. If they provoke fresh discharges, formation times may be such that in many cases the overvoltages remain present throughout times of this order of magnitude. The behavior of a solid insulator under such conditions is unknown, and the behavior inside the tube is poorly understood. If the initial arc is produced outside the tube, a large part of the available energy will be dissipated before the arrival of the overvoltage at the sensitive part of the tube. If the discharge begins in the tube, it will propagate outside because of the short circuit created in the tube by the discharges. For rapid phenomena, it is possible that the spark gaps may not always operate efficiently, especially for vacuum discharges [fr

  4. Leybold vacuum handbook

    CERN Document Server

    Diels, K; Diels, Kurt

    1966-01-01

    Leybold Vacuum Handbook presents a collection of data sets that are essential for numerical calculation of vacuum plants and vacuum processes. The title first covers vacuum physics, which includes gas kinetics, flow phenomena, vacuum gauges, and vapor removal. Next, the selection presents data on vacuum, high vacuum process technology, and gas desorption and gettering. The text also deals with materials, vapor pressure, boiling and melting points, and gas permeability. The book will be of great interest to engineers and technicians that deals with vacuum related technologies.

  5. Heart pacemaker - discharge

    Science.gov (United States)

    Cardiac pacemaker implantation - discharge; Artificial pacemaker - discharge; Permanent pacemaker - discharge; Internal pacemaker - discharge; Cardiac resynchronization therapy - discharge; CRT - discharge; ...

  6. Physical electronics handbook of vacuum physics

    CERN Document Server

    Beck, A H

    2013-01-01

    Handbook of Vacuum Physics, Volume 2, Physical Electronics, discusses the fundamentals of electric discharges in gases. Electrical discharges in gases is used generically to denote the passage of electricity through a gas and implicitly embraces the wide variety of physical phenomena which accompany such a discharge of electricity. The discharge currents may be as small as 10-16A in certain ionization growth studies, or be as large as megamperes in thermonuclear and plasma physics studies. Key topics discussed include collision phenomena in gases; surface phenomena and transport of charged par

  7. Baking results of KSTAR vacuum vessel

    Energy Technology Data Exchange (ETDEWEB)

    Kim, S. T.; Kim, Y. J.; Kim, K. M.; Im, D. S.; Joung, N. Y.; Yang, H. L.; Kim, Y. S.; Kwon, M. [National Fusion Research Institute, Daejeon (Korea, Republic of)

    2009-05-15

    The Korea Superconducting Tokamak Advanced Research (KSTAR) is an advanced superconducting tokamak designed to establish a scientific and technological basis for an attractive fusion reactor. The fusion energy in the tokamak device is released through fusion reactions of light atoms such as deuterium or helium in hot plasma state, of which temperature reaches several hundreds of millions Celsius. The high temperature plasma is created in the vacuum vessel that provides ultra high vacuum status. Accordingly, it is most important for the vacuum condition to keep clean not only inner space but also surface of the vacuum vessel to make high quality plasma. There are two methods planned to clean the wall surface of the KSTAR vacuum vessel. One is surface baking and the other is glow discharge cleaning (GDC). To bake the vacuum vessel, De-Ionized (DI) water is heated to 130 .deg. C and circulated in the passage between double walls of the vacuum vessel (VV) in order to bake the surface. The GDC operation uses hydrogen and inert gas discharges. In this paper, general configuration and brief introduction of the baking result will be reported.

  8. Baking results of KSTAR vacuum vessel

    International Nuclear Information System (INIS)

    Kim, S. T.; Kim, Y. J.; Kim, K. M.; Im, D. S.; Joung, N. Y.; Yang, H. L.; Kim, Y. S.; Kwon, M.

    2009-01-01

    The Korea Superconducting Tokamak Advanced Research (KSTAR) is an advanced superconducting tokamak designed to establish a scientific and technological basis for an attractive fusion reactor. The fusion energy in the tokamak device is released through fusion reactions of light atoms such as deuterium or helium in hot plasma state, of which temperature reaches several hundreds of millions Celsius. The high temperature plasma is created in the vacuum vessel that provides ultra high vacuum status. Accordingly, it is most important for the vacuum condition to keep clean not only inner space but also surface of the vacuum vessel to make high quality plasma. There are two methods planned to clean the wall surface of the KSTAR vacuum vessel. One is surface baking and the other is glow discharge cleaning (GDC). To bake the vacuum vessel, De-Ionized (DI) water is heated to 130 .deg. C and circulated in the passage between double walls of the vacuum vessel (VV) in order to bake the surface. The GDC operation uses hydrogen and inert gas discharges. In this paper, general configuration and brief introduction of the baking result will be reported

  9. Argon discharge characteristics in cold cathode penning ion source. Vol. 2

    Energy Technology Data Exchange (ETDEWEB)

    Abd El-Baki, M M; Abd El-Rahman, M M; Basal, N I [Ion Sources and Accelerators Department, Nuclear Research Center, Atomic energy Authority, Cairo, (Egypt)

    1996-03-01

    This study includes the production of argon discharge inside cold cathode penning ion source with axial d.c. extraction. The arc characteristics are investigated under the influence of the discharge parameters such as the pressure, axial magnetic field. At zero magnetic field and pressure 4.2 x 10{sup -4} torr, the arc voltage which is needed for arc initiation is relatively large V{sub arc} = 430 V, and I{sub arc} = 0.3 A. The application of the magnetic field helps the appearance of argon arc at lower voltage, e.g. at I{sub B} = 0.8 A, the arc voltage V{sub arc} = 320 V, and I{sub arc} = 0.3 A. It is found that the arc current increase with the increase of pressure, i.e. the increase of gas flow inside the source, while the arc voltage decreases. 7 fig.

  10. MEA vacuum system

    International Nuclear Information System (INIS)

    Stroo, R.; Schwebke, H.; Heine, E.

    1984-01-01

    This report describes construction and operation of the MEA vacuum system of NIKHEF (Netherlands). First, the klystron vacuum system, beam transport system, diode pump and a triode pump are described. Next, the isolation valve and the fast valves of the vacuum system are considered. Measuring instruments, vacuum system commands and messages of failures are treated in the last chapter. (G.J.P.)

  11. Vacuum system for ISABELLE

    International Nuclear Information System (INIS)

    Hobson, J.P.

    1975-01-01

    An analysis is presented of the proposed vacuum system for the planned ISABELLE storage rings with respect to acceptability and practicality from the vacuum viewport. A comparison is made between the proposed vacuum system and the vacuum system at the CERN ISR, and some comments on various design and operational parameters are made

  12. Helium pressures in RHIC vacuum cryostats and relief valve requirements from magnet cooling line failure

    Energy Technology Data Exchange (ETDEWEB)

    Liaw, C.J.; Than, Y.; Tuozzolo, J.

    2011-03-28

    A catastrophic failure of the RHIC magnet cooling lines, similar to the LHC superconducting bus failure incident, would pressurize the insulating vacuum in the magnet and transfer line cryostats. Insufficient relief valves on the cryostats could cause a structural failure. A SINDA/FLUINT{reg_sign} model, which simulated the 4.5K/4 atm helium flowing through the magnet cooling system distribution lines, then through a line break into the vacuum cryostat and discharging via the reliefs into the RHIC tunnel, had been developed to calculate the helium pressure inside the cryostat. Arc flash energy deposition and heat load from the ambient temperature cryostat surfaces were included in the simulations. Three typical areas: the sextant arc, the Triplet/DX/D0 magnets, and the injection area, had been analyzed. Existing relief valve sizes were reviewed to make sure that the maximum stresses, caused by the calculated maximum pressures inside the cryostats, did not exceed the allowable stresses, based on the ASME Code B31.3 and ANSYS results. The conclusions are as follows: (1) The S/F simulation results show that the highest internal pressure in the cryostats, due to the magnet line failure, is {approx}37 psig (255115 Pa); (2) Based on the simulation, the temperature on the cryostat chamber, INJ Q8-Q9, could drop to 228 K, which is lower than the material minimum design temperature allowed by the Code; (3) Based on the ASME Code and ANSYS results, the reliefs on all the cryostats inside the RHIC tunnel are adequate to protect the vacuum chambers when the magnet cooling lines fail; and (4) In addition to the pressure loading, the thermal deformations, due to the temperature decrease on the cryostat chambers, could also cause a high stress on the chamber, if not properly supported.

  13. Helium pressures in RHIC vacuum cryostats and relief valve requirements from magnet cooling line failure

    International Nuclear Information System (INIS)

    Liaw, C.J.; Than, Y.; Tuozzolo, J.

    2011-01-01

    A catastrophic failure of the RHIC magnet cooling lines, similar to the LHC superconducting bus failure incident, would pressurize the insulating vacuum in the magnet and transfer line cryostats. Insufficient relief valves on the cryostats could cause a structural failure. A SINDA/FLUINT(reg s ign) model, which simulated the 4.5K/4 atm helium flowing through the magnet cooling system distribution lines, then through a line break into the vacuum cryostat and discharging via the reliefs into the RHIC tunnel, had been developed to calculate the helium pressure inside the cryostat. Arc flash energy deposition and heat load from the ambient temperature cryostat surfaces were included in the simulations. Three typical areas: the sextant arc, the Triplet/DX/D0 magnets, and the injection area, had been analyzed. Existing relief valve sizes were reviewed to make sure that the maximum stresses, caused by the calculated maximum pressures inside the cryostats, did not exceed the allowable stresses, based on the ASME Code B31.3 and ANSYS results. The conclusions are as follows: (1) The S/F simulation results show that the highest internal pressure in the cryostats, due to the magnet line failure, is ∼37 psig (255115 Pa); (2) Based on the simulation, the temperature on the cryostat chamber, INJ Q8-Q9, could drop to 228 K, which is lower than the material minimum design temperature allowed by the Code; (3) Based on the ASME Code and ANSYS results, the reliefs on all the cryostats inside the RHIC tunnel are adequate to protect the vacuum chambers when the magnet cooling lines fail; and (4) In addition to the pressure loading, the thermal deformations, due to the temperature decrease on the cryostat chambers, could also cause a high stress on the chamber, if not properly supported.

  14. High Current, High Density Arc Plasma as a New Source for WiPAL

    Science.gov (United States)

    Waleffe, Roger; Endrizzi, Doug; Myers, Rachel; Wallace, John; Clark, Mike; Forest, Cary; WiPAL Team

    2016-10-01

    The Wisconsin Plasma Astrophysics Lab (WiPAL) has installed a new array of nineteen plasma sources (plasma guns) on its 3 m diameter, spherical vacuum vessel. Each gun is a cylindrical, molybdenum, washer-stabilized, arc plasma source. During discharge, the guns are maintained at 1.2 kA across 100 V for 10 ms by the gun power supply establishing a high density plasma. Each plasma source is fired independently allowing for adjustable plasma parameters, with densities varying between 1018 -1019 m-3 and electron temperatures of 5-15 eV. Measurements were characterized using a 16 tip Langmuir probe. The plasma source will be used as a background plasma for the magnetized coaxial plasma gun (MCPG), the Terrestrial Reconnection Experiment (TREX), and as the plasma source for a magnetic mirror experiment. Temperature, density, and confinement results will be presented. This work is supported by the DoE and the NSF.

  15. Thermal Plasma Generators with Water Stabilized Arc

    Czech Academy of Sciences Publication Activity Database

    Hrabovský, Milan

    2009-01-01

    Roč. 2, č. 1 (2009), s. 99-104 ISSN 1876-5343 R&D Projects: GA ČR GA202/08/1084 Institutional research plan: CEZ:AV0Z20430508 Keywords : Thermal plasma * plasma torch * Gerdien arc Subject RIV: BL - Plasma and Gas Discharge Physics http://www.bentham.org/open/toppj/openaccess2.htm

  16. Arc tracks on nanostructured surfaces after microbreakdowns

    International Nuclear Information System (INIS)

    Sinelnikov, D; Bulgadaryan, D; Kolodko, D; Kurnaev, V; Hwangbo, D; Ohno, N; Kajita, S

    2016-01-01

    Studying of initial steps of unipolar arc ignition process is important for reduction of probability of arcing between the plasma and the wall in thermonuclear devices. Tungsten nano-fuzz surface formed by helium plasma irradiation at high fluences and temperatures is a perfect material for arc ignition. Snowflake-like craters were detected on the fuzzy surfaces after short micro-breakdowns. Such sort of craters have not been observed before on any other metallic surfaces. These specific traces are formed due to unique properties of the fuzz structure. The nano-fuzz could be easily melted and vaporized by micro-breakdown current, due to its porosity and bad thermal conductivity, and formation of low conducting metallic vapour under the cathode spot causes discharge movement to the nearest place. Thus, even low current arc can easily move and leave traces, which could be easily observed by a secondary electron microscope. (paper)

  17. Influence of DC arc current on the formation of cobalt-based ...

    Indian Academy of Sciences (India)

    The synthesis of cobalt-based magnetic nanostructures using DC arc discharge technique with varying arc current is reported here. The structural, morphological, compositional and magnetic properties of thesenanostructures were studied as a function of applied arc current. Various techniques like X-ray diffraction, ...

  18. Nipple Discharge

    Science.gov (United States)

    ... any unexpected nipple discharge evaluated by a doctor. Nipple discharge in men under any circumstances could be a problem and needs further evaluation. One or both breasts may produce a nipple discharge, either spontaneously or when you squeeze your ...

  19. Basic Studies of Distributed Discharge Limiters

    Science.gov (United States)

    2014-02-10

    electron avalanche ionization discharges induced by a focused 110 GHz millimeter-wave beam in atmospheric air. Discharges take place in a free volume of...plasma. 3.1.7 Vacuum Ultraviolet emission from pulsed discharges at atmospheric pressure. Fig. 6. Energy level diagram for molecular and...the utilized spectral simulation software, SPECTRAPLOT. 3.1.8 Non-intrusive diagnostic method for dissociation degree in pulsed discharges

  20. Technique eliminates high voltage arcing at electrode-insulator contact area

    Science.gov (United States)

    Mealy, G.

    1967-01-01

    Coating the electrode-insulator contact area with silver epoxy conductive paint and forcing the electrode and insulator tightly together into a permanent connection, eliminates electrical arcing in high-voltage electrodes supplying electrical power to vacuum facilities.

  1. Particle injection into the Castor tokamak by electric arcs

    International Nuclear Information System (INIS)

    Hildebrandt, D.; Juettner, B.; Pursch, H.; Jakubka, K.; Stoeckel, J.; Zacek, F.

    1989-01-01

    The influence of arcing on the tokamak discharge was investigated in the Castor tokamak. A special calibrated gun which emitted tantalum by artificially ignited electric arcs, was used to study the transport of the injected tantalum ions, neutrals and droplets. The injection of tantalum led to an increase in electron density and to a change of plasma position only if the transported charge was higher than 0.01 C. As the naturally occurring arcs are well below this limit, the arcing in tokamaks is rather the consequence than the reason of instabilities. (J.U.)

  2. Discharge current characteristics as an 'electrical method' for glow discharge plasma diagnosis

    International Nuclear Information System (INIS)

    Toma, M.; Paraschivescu, Alina; Morminches, Anisoara

    2001-01-01

    In its simplest form, the glow discharge can be established by passing an electric current through gas between two electrodes. The gas and the electrodes are contained in an insulating envelope. In many technological applications, and not only, the plasma devices are often treated like a black box. There is a series of external parameters or control variables which can be adjusted to obtain a desired effect, namely, the operating voltage, gas pressure, gas nature, gas flow rate, magnetic field strength and magnetic field configuration, electric field geometry, interelectrode distance, and cathode characteristics. The discharge current can be controlled by each of the above control variables. The core idea of this work is the following: a lot of information about the phenomena from the discharge volume, at electrodes or at the discharge bounding wall surface, can be obtained knowing how the change of one of the control parameters influences the discharge current. The following regimes were analyzed: dark discharges (background ionization, saturation regime, Townsend regime, corona regime), glow discharge (the normal and abnormal discharge) and arc discharge (glow to arc transition, non-thermal arcs, thermal arcs). It was concluded that the nonlinearity in the shape of the discharge current characteristics as a function of an external control parameter, can be correlated with the elementary processes and the dynamics of different space charge structures generated in plasma devices. (authors)

  3. Glow-discharge-created electron beams and beam-excited lasers

    International Nuclear Information System (INIS)

    Meyer, J.D.

    1989-01-01

    Efficiently created glow discharge electron beams have been developed and studied in detail. The beam mode of operation occurs in the abnormal glow adjacent to the glow-to-arc transition regime. In contrast to electron beams generated in high vacuum from thermionic electron emitting sources, this type of discharge creates electrons directly in soft vacuum by secondary electron emission from cold cathode surfaces following the bombardment of the cathode surface by fast ions and neutral atoms. Factors influencing the efficient electron emission from cold cathodes are presented with emphasis on cathode materials. Sintered ceramic-metal cathodes and oxide-coated cathodes are presented, both of which can produce high power, efficiently generated, d.c. electron beams with discharge currents up to 1 amp (∼130 mA/cm 2 ) at volt ages of up to 6 kV. Novel cathode designs and discharge geometries are presented with specific emphasis on both self-focussed beams emitted from circular cathodes and line-source electron beams emitted from rectangular cathodes forming a thin sheet of electrons. Electrostatically focussed line-source electron beams are spatially characterized by experimentally measuring the effect of discharge parameters and cathode design upon the focussed beam width, focal point, and uniformity. This is achieved by scanning a current collecting detector in three dimensions in order to profile the distribution of electron beam current. Discharge electron beams are further characterized by their electron energy distribution. Measured electron flux energy distributions of transmitted beam electrons in the negative glow are compared to theoretical models. The relative effects of elastic and inelastic collisions mechanisms upon both the overall form and detailed structure of the energy distribution are discussed

  4. High-voltage high-current triggering vacuum switch

    International Nuclear Information System (INIS)

    Alferov, D.F.; Bunin, R.A.; Evsin, D.V.; Sidorov, V.A.

    2012-01-01

    Experimental investigations of switching and breaking capacities of the new high current triggered vacuum switch (TVS) are carried out at various parameters of discharge current. It has been shown that the high current triggered vacuum switch TVS can switch repeatedly a current from units up to ten kiloampers with duration up to ten millisecond [ru

  5. Method of radiation degradation of PTFE under vacuum conditions

    Energy Technology Data Exchange (ETDEWEB)

    Korenev, Sergey E-mail: sergey_korenev@steris.com

    2004-10-01

    A new method of radiation degradation of Polytetrafluoroethylene (PTFE) under vacuum conditions is considered in this report. The combination of glow gas discharge and electrical surface discharge (on surface and inside PTFE) increases the efficiency of thermal-radiation degradation. The main mechanism of this degradation method consists of the breaking of C-C and C-F bonds. The vacuum conditions allow decreasing of the concentration of toxic compounds, such as a HF. Experimental results for degradation of PTFE are presented.

  6. Method of radiation degradation of PTFE under vacuum conditions

    Science.gov (United States)

    Korenev, Sergey

    2004-09-01

    A new method of radiation degradation of Polytetrafluoroethylene (PTFE) under vacuum conditions is considered in this report. The combination of glow gas discharge and electrical surface discharge (on surface and inside PTFE) increases the efficiency of thermal-radiation degradation. The main mechanism of this degradation method consists of the breaking of C-C and C-F bonds. The vacuum conditions allow decreasing of the concentration of toxic compounds, such as a HF. Experimental results for degradation of PTFE are presented.

  7. Microwave response of ITER vacuum windows

    NARCIS (Netherlands)

    Oosterbeek, J.W.; Maquet, P.; Sirinelli, A.; Udintsev, V.S.; Vayakis, G.; Walsh, M.J.

    2017-01-01

    Diagnostic systems are essential for the development of ITER discharges and to reach the ITER goals. Many of these diagnostics require a line of sight to relay signals from the plasma to the diagnostic, typically located outside the torus hall. Such diagnostics then require vacuum windows that

  8. Fabrication of the vacuum vessel for JT-60 machine upgrade

    International Nuclear Information System (INIS)

    Uchikawa, T.; Takanabe, K.; Tsujimura, S.; Ue, K.; Oka, K.; Kuri, S.; Ioki, K.; Namiki, K.; Suzuki, Y.; Horliike, H.; Ninomiya, H.; Yamamoto, M.; Neyatani, Y.; Ando, T.; Matsukawa, M.

    1992-01-01

    The JT-60 tokamak was upgraded to double the plasma current to 6 MA. In the JT-60 machine upgrade (JT-60U), the vacuum vessel and poloidal field (PF) coils were renewed. The new vacuum vessel features a three-dimensionally curved, thin double-skin torus with multi-arc D-shaped cross section. The double-skin structure is strengthened with square pipes placed in between the outer and inner skins. Fabrication and site installation of the vessel was smoothly completed in February, 1991. This paper describes an overview of the JT-60U vacuum vessel construction

  9. Vacuum-assisted delivery

    Science.gov (United States)

    ... medlineplus.gov/ency/patientinstructions/000514.htm Vacuum-assisted delivery To use the sharing features on this page, ... through the birth canal. When is Vacuum-assisted Delivery Needed? Even after your cervix is fully dilated ( ...

  10. Vacuum system design for the PEP-II B Factory High-Energy Ring

    International Nuclear Information System (INIS)

    Perkins, C.; Bostic, D.; Daly, E.

    1994-06-01

    The design of the vacuum system for the PEP-II B Factory High-Energy Ring is reviewed. The thermal design and vacuum requirements are particularly challenging in PEP-II due to high stored beam currents up to 3.0 amps in 1658 bunches. The vacuum chambers for the HER arcs are fabricated by electron beam welding extruded copper sections up to 6 m long. Design of these chambers and the vacuum PumPing configuration is described with results from vacuum and thermal analyses

  11. Characteristics of Atmospheric Pressure Rotating Gliding Arc Plasmas

    Science.gov (United States)

    Zhang, Hao; Zhu, Fengsen; Tu, Xin; Bo, Zheng; Cen, Kefa; Li, Xiaodong

    2016-05-01

    In this work, a novel direct current (DC) atmospheric pressure rotating gliding arc (RGA) plasma reactor has been developed for plasma-assisted chemical reactions. The influence of the gas composition and the gas flow rate on the arc dynamic behaviour and the formation of reactive species in the N2 and air gliding arc plasmas has been investigated by means of electrical signals, high speed photography, and optical emission spectroscopic diagnostics. Compared to conventional gliding arc reactors with knife-shaped electrodes which generally require a high flow rate (e.g., 10-20 L/min) to maintain a long arc length and reasonable plasma discharge zone, in this RGA system, a lower gas flow rate (e.g., 2 L/min) can also generate a larger effective plasma reaction zone with a longer arc length for chemical reactions. Two different motion patterns can be clearly observed in the N2 and air RGA plasmas. The time-resolved arc voltage signals show that three different arc dynamic modes, the arc restrike mode, takeover mode, and combined modes, can be clearly identified in the RGA plasmas. The occurrence of different motion and arc dynamic modes is strongly dependent on the composition of the working gas and gas flow rate. supported by National Natural Science Foundation of China (No. 51576174), the Specialized Research Fund for the Doctoral Program of Higher Education of China (No. 20120101110099) and the Fundamental Research Funds for the Central Universities (No. 2015FZA4011)

  12. Ignition Features of Plasma-Beam Discharge in Gas-Discharge Electron Gun Operation

    Directory of Open Access Journals (Sweden)

    Valery A. Tutyk

    2013-01-01

    Full Text Available The current paper presents the results of experimental researches to determine the mode features of plasma-beam discharge (PBD generation by an electron beam injected by a low-vacuum gasdischarge electron gun (LGEG with the cold cathode and hollow anode on the basis of the high-voltage glow discharge and in the range of helium pressure of P ? 10 ÷ 130 Pa. The PBD boundaries and their dependences on parameters of an electron beam are found. The influence of PBD on parameters of low-vacuum gas-discharge electron gun is revealed. It causes an avalanche increase of electron beam current and burning of plasma-beam discharge in the whole space of the vacuum chamber volume and generation of electromagnetic radiation is revealed. Achieved results will be used for implementation of various vacuum technologies in the medium of reaction gas and generated electromagnetic radiation.

  13. Shoulder replacement - discharge

    Science.gov (United States)

    Total shoulder arthroplasty - discharge; Endoprosthetic shoulder replacement - discharge; Partial shoulder replacement - discharge; Partial shoulder arthroplasty - discharge; Replacement - shoulder - discharge; Arthroplasty - shoulder - discharge

  14. Multi-cathode metal vapor arc ion source

    International Nuclear Information System (INIS)

    Brown, I.G.; MacGill, R.A.

    1988-01-01

    This patent describes an apparatus for generating an ion beam. It comprises: a vacuum enclosure; a support member; cathodes; an anode; means for transporting; a source of electrical power; means for producing an electric arc; means for guiding; and means for extracting ions

  15. Installation of beam screens in LHC arc cryomagnets

    CERN Document Server

    Cruikshank, P; Schneider, G; Veness, R J M

    1999-01-01

    Beam screens will be installed in the cold bores of the LHC arc cryodipoles and Short Straight Sections (SSS). This note describes the constraints on the beam screen installation imposed by the beam vacuum interconnects and Beam Position Monitors (BPM), and explains the installation scenario which has been adopted.

  16. Monitoring ARC services with GangliARC

    International Nuclear Information System (INIS)

    Cameron, D; Karpenko, D

    2012-01-01

    Monitoring of Grid services is essential to provide a smooth experience for users and provide fast and easy to understand diagnostics for administrators running the services. GangliARC makes use of the widely-used Ganglia monitoring tool to present web-based graphical metrics of the ARC computing element. These include statistics of running and finished jobs, data transfer metrics, as well as showing the availability of the computing element and hardware information such as free disk space left in the ARC cache. Ganglia presents metrics as graphs of the value of the metric over time and shows an easily-digestable summary of how the system is performing, and enables quick and easy diagnosis of common problems. This paper describes how GangliARC works and shows numerous examples of how the generated data can quickly be used by an administrator to investigate problems. It also presents possibilities of combining GangliARC with other commonly-used monitoring tools such as Nagios to easily integrate ARC monitoring into the regular monitoring infrastructure of any site or computing centre.

  17. Indian Vacuum Society: The Indian Vacuum Society

    Science.gov (United States)

    Saha, T. K.

    2008-03-01

    The Indian Vacuum Society (IVS) was established in 1970. It has over 800 members including many from Industry and R & D Institutions spread throughout India. The society has an active chapter at Kolkata. The society was formed with the main aim to promote, encourage and develop the growth of Vacuum Science, Techniques and Applications in India. In order to achieve this aim it has conducted a number of short term courses at graduate and technician levels on vacuum science and technology on topics ranging from low vacuum to ultrahigh vacuum So far it has conducted 39 such courses at different parts of the country and imparted training to more than 1200 persons in the field. Some of these courses were in-plant training courses conducted on the premises of the establishment and designed to take care of the special needs of the establishment. IVS also regularly conducts national and international seminars and symposia on vacuum science and technology with special emphasis on some theme related to applications of vacuum. A large number of delegates from all over India take part in the deliberations of such seminars and symposia and present their work. IVS also arranges technical visits to different industries and research institutes. The society also helped in the UNESCO sponsored post-graduate level courses in vacuum science, technology and applications conducted by Mumbai University. The society has also designed a certificate and diploma course for graduate level students studying vacuum science and technology and has submitted a syllabus to the academic council of the University of Mumbai for their approval, we hope that some colleges affiliated to the university will start this course from the coming academic year. IVS extended its support in standardizing many of the vacuum instruments and played a vital role in helping to set up a Regional Testing Centre along with BARC. As part of the development of vacuum education, the society arranges the participation of

  18. Plasma's sweeping arc

    International Nuclear Information System (INIS)

    Pichon, Max

    2010-01-01

    Full text: It is purely elemental, returning materials to their basic atoms through extreme heat and then recondensing them in useful ways. Plasma arc gasification is the latest advanced waste treatment (AWT)concept to hit our shores, courtesy of Zenergy Australia. According to its fans, plasma technology can eliminate all domestic waste to landfill and turn it into beneficial by-products. Japan has toyed with it for a decade, but the idea is now creating a bit of buzz, in the US in particular. Consultancy URS last year undertook a review of 16 advanced technologies for the City of Los Angeles and determined plasma arc gasification was one of the most promising. The Waste Management Association of Australia (VVMAA), however, is cautious - too many AWT projects here have failed to live up to their promises. Plasma arc gasification works on the same principle as a welding machine. An inert gas is passed through an electrical arc between two electrodes and becomes ionised (called plasma), reaching temperatures as high as 13,900°C. It is then injected into the plasma converter holding the waste. Zenergy is working with US technology company Plasma Waste Recycling (PWR), which says it can convert 80 per cent of waste to syngas, a mixture of carbon monoxide and hydrogen that can be used to generate renewable electricity. The inorganic compounds in the waste come out as a solid, either molten metal to be cast as scrap steel or a slag that can be used as a building material aggregate or spun into mineral wool. “The plasma arc process is the next generation for AWT plants as there is no incineration involved, no fly ash, no bottom ash and nothing left to landfill,” said Zenergy Australia's Paul Prasad. He estimates a plant could convert up to 175,000 tonnes of household waste a year into energy or reusable by-products. Technically, it also gets around Australia's fears over incineration, though whether that is really the case in practice remains to be seen. Prasad says

  19. Vacuum arc plasma thrusters with inductive energy storage driver

    Science.gov (United States)

    Krishnan, Mahadevan (Inventor)

    2009-01-01

    A plasma thruster with a cylindrical inner and cylindrical outer electrode generates plasma particles from the application of energy stored in an inductor to a surface suitable for the formation of a plasma and expansion of plasma particles. The plasma production results in the generation of charged particles suitable for generating a reaction force, and the charged particles are guided by a magnetic field produced by the same inductor used to store the energy used to form the plasma.

  20. dc glow-discharge cleaning for accelerator

    International Nuclear Information System (INIS)

    Chou, T.S.; Hseuh, H.C.

    1982-01-01

    Average pressure of 1 x 10 -11 torr and vacuum stability are necessary for the successful operation of the proton storage rings such as ISABELLE. Vacuum degassing at high temperature and in situ bake-out will reduce the thermoout-gassing rate of the beam tubes to approx. 10 -13 Tl/cm 2 sec, therefore achieving the required static pressure. The vacuum instability caused by beam-induced ion desorption can be solved by dc glow discharge cleaning. With evidence from this study, the present understanding of glow discharge in a cylindrically symmetric geometry is reviewed. Argon and argon/oxygen mixture serve as plasmas in the glow. The role of oxygen in cleaning the beam tubes during the glow discharge is demonstrated experimentally. Glow discharge cleaning with and without bake-out is also studied

  1. Electric arc hydrogen heaters

    International Nuclear Information System (INIS)

    Zasypin, I.M.

    2000-01-01

    The experimental data on the electric arc burning in hydrogen are presented. Empirical and semiempirical dependences for calculating the arc characteristics are derived. An engineering method of calculating plasma torches for hydrogen heating is proposed. A model of interaction of a hydrogen arc with a gas flow is outlined. The characteristics of plasma torches for heating hydrogen and hydrogen-bearing gases are described. (author)

  2. Vacuum leak test technique of JT-60

    International Nuclear Information System (INIS)

    Kaminaga, Atsushi; Arai, Takashi; Kodama, Kozo; Sasaki, Noboru; Saidoh, Masahiro

    1998-01-01

    Since a vacuum vessel of JT-60 is very large (167 m 3 ) and is combined with many components, such as magnetic coils, neutral beam injection systems and RF heating systems, etc., the position of leak testing exceeds 700. The two kind of techniques for vacuum leak test used in JT-60 has been described. Firstly the probe helium gas can be fed remotely in the three-dimensionally sectioned 54 regions of the JT-60 torus. The leak test was very rapidly performed by using this method. Secondly the helium detector system has been modified by the additional installation of the cryopump, which reduced the background level of the deuterium gas. The sensitivity of vacuum leak test with the cryopump was two orders of magnitude larger than that of without it. The examples of the performed vacuum leak test are stated. The vacuum leaks during experiments were 9 times. They were caused by thermal strain and plasma discharge. The vacuum leaks just after maintenance are 36 times which mainly caused by mis-installation. (author)

  3. Magnetically induced vacuum decay

    International Nuclear Information System (INIS)

    Xue Shesheng

    2003-01-01

    We study the fermionic vacuum energy of vacua with and without application of an external magnetic field. The energetic difference of two vacua leads to the vacuum decaying and the vacuum energy being released. In the context of quantum field theories, we discuss why and how the vacuum energy can be released by spontaneous photon emission and/or paramagnetically screening the external magnetic field. In addition, we quantitatively compute the vacuum energy released, the paramagnetic screening effect, and the rate and spectrum of spontaneous photon emission. The possibilities of experimentally detecting such an effect of vacuum-energy release and that this effect accounts for the anomalous x-ray pulsar are discussed

  4. Modification of Ultra-High Vacuum Surfaces Using Free Radicals

    CERN Document Server

    Vorlaufer, G

    2002-01-01

    In ultra-high vacuum systems outgassing from vacuum chamber walls and desorption of surface adsorbates are usually the factors which determine pressure and residual gas composition. In particular in beam vacuum systems of accelerators like the LHC, where surfaces are exposed to intense synchrotron radiation and bombardment by energetic ions and electrons, surface properties like the molecular desorption yield or secondary electron yield can strongly influence the performance of the accelerator. Well-established treatment methods like vacuum bake-out or glow-discharge cleaning have been successfully applied in the past to condition ultra-high vacuum surfaces, but these methods are sometimes difficult to carry out, for example if the vacuum chambers are not accessible. In this work, an alternative treatment method is investigated. This method is based on the strong chemical reactivity of free radicals, electrically neutral fragments of molecules. Free radicals (in the case of this work, nitrogen and oxygen radi...

  5. Gravitation and vacuum field

    International Nuclear Information System (INIS)

    Tevikyan, R.V.

    1986-01-01

    This paper presents equations that describe particles with spins s = 0, 1/2, 1 completely and which also describe 2s + 2 limiting fields as E → ∞. It is shown that the ordinary Hilbert-Einstein action for the gravitation field must be augmented by the action for the Bose vacuum field. This means that one must introduce in the gravitational equations a cosmological term proportional to the square of the strength of the Bose vacuum field. It is shown that the theory of gravitation describes three realities: matter, field, and vacuum field. A new form of matter--the vacuum field--is introduced into field theory

  6. Vacuum Large Current Parallel Transfer Numerical Analysis

    Directory of Open Access Journals (Sweden)

    Enyuan Dong

    2014-01-01

    Full Text Available The stable operation and reliable breaking of large generator current are a difficult problem in power system. It can be solved successfully by the parallel interrupters and proper timing sequence with phase-control technology, in which the strategy of breaker’s control is decided by the time of both the first-opening phase and second-opening phase. The precise transfer current’s model can provide the proper timing sequence to break the generator circuit breaker. By analysis of the transfer current’s experiments and data, the real vacuum arc resistance and precise correctional model in the large transfer current’s process are obtained in this paper. The transfer time calculated by the correctional model of transfer current is very close to the actual transfer time. It can provide guidance for planning proper timing sequence and breaking the vacuum generator circuit breaker with the parallel interrupters.

  7. Surface breakdown igniter for mercury arc devices

    Science.gov (United States)

    Bayless, John R.

    1977-01-01

    Surface breakdown igniter comprises a semiconductor of medium resistivity which has the arc device cathode as one electrode and has an igniter anode electrode so that when voltage is applied between the electrodes a spark is generated when electrical breakdown occurs over the surface of the semiconductor. The geometry of the igniter anode and cathode electrodes causes the igniter discharge to be forced away from the semiconductor surface.

  8. Discharge cleaning for a tokamak

    International Nuclear Information System (INIS)

    Ishii, Shigeyuki

    1983-01-01

    Various methods of discharge cleaning for tokamaks are described. The material of the first walls of tokamaks is usually stainless steel, inconel, titanium and so on. Hydrogen is exclusively used as the discharge gas. Glow discharge cleaning (GDC), Taylor discharge cleaning (TDC), and electron cyclotron resonance discharge cleaning (ECR-DC) are discussed in this paper. The cleaning by GDC is made by moving a movable anode to the center of a tokamak vassel. Taylor found the good cleaning effect of induced discharge by high pressure and low power discharge. This is called TDC. When the frequency of high frequency discharge in a magnetic field is equal to that of the electron cyclotron resonance, the break down potential is lowered if the pressure is sufficiently low. The ECR-CD is made by using this effect. In TDC and ECR-DC, the electron temperature, which has a close relation to the production rate of H 0 , can be controlled by the pressure. In GDC, the operating pressure was improved by the radio frequency glow (RG) method. However, there is still the danger of arcing. In case of GDC and ECR-DC, the position of plasma can be controlled, but not in case of TDC. The TDC is accepted by most of takamak devices in the world. (Kato, T.)

  9. Development of circuit model for arcing on solar panels

    International Nuclear Information System (INIS)

    Mehta, Bhoomi K; Deshpande, S P; Mukherjee, S; Gupta, S B; Ranjan, M; Rane, R; Vaghela, N; Acharya, V; Sudhakar, M; Sankaran, M; Suresh, E P

    2010-01-01

    The increased requirements of payload capacity of the satellites have resulted in much higher power requirements of the satellites. In order to minimize the energy loss during power transmission due to cable loss, use of high voltage solar panels becomes necessary. When a satellite encounters space plasma it floats negatively with respect to the surrounding space plasma environment. At high voltage, charging and discharging on solar panels causes the power system breakdown. Once a solar panel surface is charged and potential difference between surface insulator and conductor exceeds certain value, electrostatic discharge (ESD) may occur. This ESD may trigger a secondary arc that can destroy the solar panel circuit. ESD is also called as primary or minor arc and secondary is called major arc. The energy of minor arc is supplied by the charge stored in the coverglass of solar array and is a pulse of typically several 100 ns to several 100 μs duration. The damage caused by minor arc is less compared to major arcs, but it is observed that the minor arc is cause of major arc. Therefore it is important to develop an understanding of minor arc and mitigation techniques. In this paper we present a linear circuit analysis for minor arcs on solar panels. To study arcing event, a ground experimental facility to simulate space plasma environment has been developed at Facilitation Centre for Industrial Plasma Technologies (Institute for Plasma Research) in collaboration with Indian Space Research Organization's ISRO Satellite Technology Centre (ISAC). A linear circuit model has been developed to explain the experimental results by representing the coverglass, solar cell interconnect and wiring by an LCR circuit and the primary arc by an equivalent LR circuit. The aim of the circuit analysis is to predict the arc current which flows through the arc plasma. It is established from the model that the current depends on various parameters like potential difference between insulator

  10. Gas-discharge sources with charged particle emission from the plasma of glow discharge with a hollow cathode

    CERN Document Server

    Semenov, A P

    2001-01-01

    One studied properties of a magnetron discharge with a cold hollow and uncooled rod cathodes. One demonstrated the dominant effect of thermoelectron emission of a rod cathode heated in a discharge on characteristics of discharge and on emission properties of a gas-discharge plasma and the possibility pf a smooth transition of glow discharge to diffusion mode of arc discharge combustion. Paper describes sources of ions and electrons with improved physical and generalized design and engineering parameters. One shows the promise of the electrode structure of a hollow cathode magnetron discharge to be used as a source, in particular, of the atomic hydrogen and of atom flow of a working rod cathode

  11. Synthesis of aluminum nitride films by plasma immersion ion implantation-deposition using hybrid gas-metal cathodic arc gun

    International Nuclear Information System (INIS)

    Shen Liru; Fu, Ricky K.Y.; Chu, Paul K.

    2004-01-01

    Aluminum nitride (AlN) is of interest in the industry because of its excellent electronic, optical, acoustic, thermal, and mechanical properties. In this work, aluminum nitride films are deposited on silicon wafers (100) by metal plasma immersion ion implantation and deposition (PIIID) using a modified hybrid gas-metal cathodic arc plasma source and with no intentional heating to the substrate. The mixed metal and gaseous plasma is generated by feeding the gas into the arc discharge region. The deposition rate is found to mainly depend on the Al ion flux from the cathodic arc source and is only slightly affected by the N 2 flow rate. The AlN films fabricated by this method exhibit a cubic crystalline microstructure with stable and low internal stress. The surface of the AlN films is quite smooth with the surface roughness on the order of 1/2 nm as determined by atomic force microscopy, homogeneous, and continuous, and the dense granular microstructures give rise to good adhesion with the substrate. The N to Al ratio increases with the bias voltage applied to the substrates. A fairly large amount of O originating from the residual vacuum is found in the samples with low N:Al ratios, but a high bias reduces the oxygen concentration. The compositions, microstructures and crystal states of the deposited films are quite stable and remain unchanged after annealing at 800 deg. C for 1 h. Our hybrid gas-metal source cathodic arc source delivers better AlN thin films than conventional PIIID employing dual plasmas

  12. INFLUENCE OF CHEMICAL COMPOUNDS ON THE FORMING OF ELECTRIC ARC

    Directory of Open Access Journals (Sweden)

    I. O. Vakulenko

    2014-07-01

    Full Text Available Purpose. The purpose of work is a comparative analysis of chemical compounds influence on the process of electric arc forming and condition of its burning. Methodology. Material for an electrode was a wire 3 mm in diameter of low carbon steel with contain of carbon 0.15%. As chemical compounds, which determine the terms of forming of arc welding were used kaolin; CaCO3 with the admixtures of gypsum to 60%; SiO2 and Fe – Si with the iron concentration to 50%. Researches were conducted at the use of direct electric current and the arc of reverse polarity. As a source of electric current the welding transformer of type PSO-500 was used. On the special stand an initial gap between the electrode and metal-plate was equal to 1–1.5 mm. The interelectrode interval was filled with the probed chemical compounds and it was formed an electric arc. In the moment of electric arc arise the values of electric current and the arc voltage were determined. After the natural break of electric arc, the final size of the gap between electrodes was accepted as the maximal value of the arc lengths. Findings. In the conditions of experiment the metal transfer in interelectrode interval corresponded to the drop mechanism. According to external characteristics the ratio between the maximal arc length and the power of electric discharge has the appearance of exponential dependence. Specific power of electric arc characterizes environment of interelectrode interval in the moment of arc forming per unit of its length. Originality. 1. On the basis of influence analysis of the studied chemical compounds on the formation processes of electric arc inversely proportional relationship between the power of the electric current and the maximum arc length to the moment of its natural break is defined. 2. The ratio between the maximal arc length and the power of electric current with sufficiently high correlation coefficient is subjected to the exponential dependence. Influence of

  13. Baking of SST-1 vacuum vessel modules and sectors

    International Nuclear Information System (INIS)

    Pathan, Firozkhan S; Khan, Ziauddin; Yuvakiran, Paravastu; George, Siju; Ramesh, Gattu; Manthena, Himabindu; Shah, Virendrakumar; Raval, Dilip C; Thankey, Prashant L; Dhanani, Kalpesh R; Pradhan, Subrata

    2012-01-01

    SST-1 Tokamak is a steady state super-conducting tokamak for plasma discharge of 1000 sec duration. The plasma discharge of such long time duration can be obtained by reducing the impurities level, which will be possible only when SST-1 vacuum chamber is pumped to ultra high vacuum. In order to achieve UHV inside the chamber, the baking of complete vacuum chamber has to be carried out during pumping. For this purpose the C-channels are welded inside the vacuum vessel. During baking of vacuum vessel, these welded channels should be helium leak tight. Further, these U-channels will be in accessible under operational condition of SST-1. So, it will not possible to repair if any leak is developed during experiment. To avoid such circumstances, a dedicated high vacuum chamber is used for baking of the individual vacuum modules and sectors before assembly so that any fault during welding of the channels will be obtained and repaired. This paper represents the baking of vacuum vessel modules and sectors and their temperature distribution along the entire surface before assembly.

  14. Insulation vacuum and beam vacuum overpressure release

    CERN Document Server

    Parma, V

    2009-01-01

    There is evidence that the incident of 19th September caused a high pressure build-up inside the cryostat insulation vacuum which the existing overpressure devices could not contain. As a result, high longitudinal forces acting on the insulation vacuum barriers developed and broke the floor and the floor fixations of the SSS with vacuum barriers. The consequent large longitudinal displacements of the SSS damaged chains of adjacent dipole cryo-magnets. Estimates of the helium mass flow and the pressure build- up experienced in the incident are presented together with the pressure build-up for an even more hazardous event, the Maximum Credible Incident (MCI). The strategy of limiting the maximum pressure by the installation of addition pressure relieve devices is presented and discussed. Both beam vacuum lines were ruptured during the incident in sector 3-4 giving rise to both mechanical damage and pollution of the system. The sequence, causes and effects of this damage will be briefly reviewed. We will then an...

  15. NIPPLE DISCHARGE

    Directory of Open Access Journals (Sweden)

    T. N. Bukharova

    2008-01-01

    Full Text Available According to the data available in the literature, as high as 50% of women have benign breast tumors frequently accompanied by nip- ple discharge. Nipple discharge may be serous, bloody, purulent, and colostric. The most common causes are breast abscess, injury, drugs, prolactinoma, intraductal pappiloma, ductal ectasia, intraductal cancer (not more than 10%.

  16. Experimental study of anode processes in plasma arc cutting

    Czech Academy of Sciences Publication Activity Database

    Kavka, Tetyana; Chumak, Oleksiy; Šonský, Jiří; Heinrich, M.; Stehrer, T.; Pauser, H.

    2013-01-01

    Roč. 46, č. 6 (2013), 065202-065202 ISSN 0022-3727 R&D Projects: GA ČR GAP205/11/2070 Institutional support: RVO:61389021 ; RVO:61388998 Keywords : Arc cutting * anode attachment * pilot arc * steam plasma cutting * torch * fluctuations * JET Subject RIV: BL - Plasma and Gas Discharge Physics; BL - Plasma and Gas Discharge Physics (UT-L) Impact factor: 2.521, year: 2013 http://iopscience.iop.org/0022-3727/46/6/065202/pdf/0022-3727_46_6_065202.pdf

  17. High speed photography for investigating kiloampere discharges in supersonic air flows

    International Nuclear Information System (INIS)

    Jones, G.R.; Strachan, D.

    1975-01-01

    Examples of the use of conventional high speed photographic techniques are given for obtaining information about the behaviour of high current arc discharges in different gas flow fields. The photographic records yield information about the extent of both the luminous arc core and the surrounding heated volume of gas. A knowledge of these parameters leads to a better understanding of arc discharges which occur in gas blast circuit breakers. (author)

  18. Determining the mode of high voltage breakdowns in vacuum devices

    International Nuclear Information System (INIS)

    Miller, H.C.; Furno, E.J.; Sturtz, J.P.

    1980-01-01

    Devices were constructed which were essentially vacuum diodes equipped with windows allowing observation of high voltage breakdowns. The waveform of the applied voltage was photographed, and the x-ray output was monitored to investigate electrical breakdown in these vacuum diodes. Results indicate that breakdowns may be divided into two types: (1) vacuum (interelectrode) breakdown - characterized by a diffuse moderately bright discharge, a relative slow and smooth voltage collapse, and a large burst of x-rays, and (2) surface (insulator) flashover - characterized by a bright discharge with a very bright filamentary core, a relatively fast and noisy voltage collapse and no x-ray burst. Useful information concerning the type of breakdown in a vacuum device can be obtained by monitoring the voltage (current) waveform and the x-ray output

  19. The physics of ''vacuum'' breakdown

    International Nuclear Information System (INIS)

    Schwirzke, F.

    1993-01-01

    Many discharges form small cathode spots which provide such a high energy density that the cathode material explodes into a dense plasma cloud within a very short time. Despite the fundamental importance of cathode spots for the breakdown process and the formation of a discharge, the structure of the cathode spot plasma and the source of the high energy density were not yet well defined. One model, the whisker explosive emission model, assumes that joule heating by field emitted electrons provides the energy. Current densities of j FE = 10 12 - 10 13 A/m 2 would be required. However, the pre-breakdown j FE is self-limiting. The negative space charge caused by j FE in the cathode-anode gap reduces the effective electric field E on the cathode surface. The maximum current density j CL is space charge limited by Child-Langmuir's law. The field emitting spot cannot deliver j CL without turning itself off, since the negative space charge caused by j CL reduces E congruent 0 at the cathode surface. Hence, it must be that the vacuum j FE CL . The development of a current with j > j FE (vacuum) requires that ions exist in front of the electron emitting spot. Ions cannot be emitted from the surface of the field emitting spot, the enhanced electric field would hold them back. The initial ionization must occur in the cathode-anode gap near the electron emitting spot. Ionization of desorbed neutrals provides the mechanism. This ionization process requires considerably less current than the ionization of solid material by joule heating. Field emission and the impact of ions stimulate desorption of weakly bound adsorbates from the surface of the electron emitting spot. The cross section for ionization of the neutrals has a maximum for ∼ 100 eV electrons

  20. Busbar arcs at large fusion magnets: Conductor to feeder tube arcing model experiments with the LONGARC device

    Energy Technology Data Exchange (ETDEWEB)

    Klimenko, Dmitry, E-mail: dmitry.klimenko@kit.edu; Pasler, Volker

    2014-10-15

    Highlights: •The LONGARC device was successfully implemented for busbar to feeder tubes arcing model experiments. •Arcing at an ITER busbar inside its feeder tube was simulated in scaled model experiments. •The narrower half tubes imply a slight increase of the arc propagation speed in compare to full tube experiments. •All simulated half tubes experiments show severe damage indicating that the ITER inner feeder tube will not withstand a busbar arc. -- Abstract: Electric arcs moving along the power cables (the so-called busbars) of the toroidal field (TF) coils of ITER may reach and penetrate the cryostat wall. Model experiments with the new LONGARC device continue the VACARC (VACuum ARC) experiments that were initiated to investigate the propagation and destruction mechanisms of busbar arcs in small scale [1]. The experiments are intended to support the development and validation of a numerical model. LONGARC overcomes the space limitations inside VACARC and allows also for advanced 1:3 (vs. ITER full scale) model setups. The LONGARC device and first results are presented below.