WorldWideScience

Sample records for tssd results obtained

  1. Kinetics of the isothermal decomposition of zirconium hydride: terminal solid solubility for precipitation and dissolution

    Science.gov (United States)

    Denisov, E. A.; Kompaniets, T. N.; Voyt, A. P.

    2018-05-01

    The hydrogen permeation technique in the surface-limited regime (SLR) was first used to study the isothermal decomposition of zirconium hydride. It is shown that under isothermal conditions, the hydrogen terminal solid solubility in the α-phase for hydride precipitation (TSSp) and dissolution (TSSd) differ only by 6%, in contrast to the 20-30% indicated in the available literature. It is demonstrated that even the minimum heating/cooling rate (1 C/min) used in the traditional methods of studying TSSp and TSSd is too high to exclude the effect of kinetics on the results obtained.

  2. Low speed turbines for nuclear power plants

    International Nuclear Information System (INIS)

    Ugol'nikov, V.V.; Kosyak, Yu.F.; Virchenko, M.A.

    1975-01-01

    Work of the Kharkov turbine plant on planning and manufacture for nuclear power plants of low-speed (1500 rpm) turbines with a power of 500-1000 MW is described. The selection of a construction diagram for the turbine assembly, determined basically by the presence or absence of parts of average pressure, is considered. Special construction features of the condenser and turbine are described. Turbine K-500, with a rate of 1500 rpm, was calculated for operation in a two-loop nuclear power plant with saturated steam with intermediate separation and two-stage steam regeneration. On the base of this turbine, three models of 1000-MW turbines were developed. The first model has a cylinder of average pressure (TsSD) and a lateral condenser. The second has no TsSD but a low location of the condensers. The third has no TsSD and the condensers are located laterally. Calculations of the heat efficiency of the three types of turbines showed that several advantages are offered by the model with a TsSD. Better aerodynamic properties of the exhaust nozzles and condensers with lateral location allows decreasing the specific heat consumption to 0.5-1% or, at the same power, a 10-20% decrease in cooling water consumption

  3. Experimental results obtained at GANIL

    International Nuclear Information System (INIS)

    Borrel, V.

    1993-01-01

    A review of experimental results obtained at GANIL on the study of nuclear structure and nuclear reactions with secondary radioactive beams is presented. Mass measurements by means of the GANIL cyclotrons are described. The possibilities of GANIL/LISE3 for the production and separation of radioactive beams are illustrated through a large variety of experiments. (author). 19 refs., 8 figs

  4. Evaluation of the DSC technique in the determination of the terminal temperature solubility of hydrogen in Zircaloy 4

    International Nuclear Information System (INIS)

    Vizcaino, Pablo; Banchik, Abraham D.

    1999-01-01

    The determination of the terminal temperature solubility of hydrogen in the zirconium alloys is a matter of our interest, since the hydride precipitation in these materials make them susceptible to the delay hydrogen cracking (DHC). Nowadays efforts are directed to the determination of this parameter on irradiated materials. In this frame we have begun a program to determine these curves on irradiated zirconium alloys like Zircaloys, Zr 2.5% Nb, Zr 1% Nb, zirconium sponge and high oxygen zirconium with different microstructures using the differential scanning calorimeter technique. The earlier task that we have imposed to us is the evaluation the reproducibility of this technique and the influence of the heating and cooling rates on the results. With these objectives we have initiated this work measuring the terminal temperature solubility (TTS) in unirradiated recrystallized and cold worked Zircaloy-4. We have found that the reproducibility of the technique is good; the average values (TSSD) and (TSSP) agree within the experimental error and the dispersions are low. Variance analysis indicates that the values of TSSD and TSSP do not depend on the heating and cooling rates. Within the rank analyzed the differences in the measurements are only possible to be attributed to statistical and/or experimental errors. The obtained curves of solubility show to a good agreement with the values obtained by others authors until 200 ppm (weight) of hydrogen. Similar comparisons between precipitation curves have not been made in regard to which these values depend on the maximum temperature reached in the experience. (author)

  5. Test Beam Results Obtained with the Q4 Prototype

    Energy Technology Data Exchange (ETDEWEB)

    Aguilar-Benitez, M.; Alberdi, J.; Cerrada, M.; Colino, N.; Daniel, M.; Fouz, M. c.; Marin, J.; Mocholi, J.; Oller, J. C.; Puerta, J.; Romero, L.; Salicio, J. M.

    2000-07-01

    A prototype of the CMS Barrel Muon Detector incorporating all the features of the final chambers was built at CIEMAT using the mass production assembly procedures and tools. The performance of this prototype was studied in a muon test beam at CERN and the results obtained are presented here. (Author)

  6. Test beam results obtained with the Q4 prototype

    International Nuclear Information System (INIS)

    Aguilar-Benitez, M.; Alberdi, J.; Cerrada, M.; Colino, N.; Daniel, M.; Fouz, M.C.; Marin, J.; Mocholi, J.; Oller, J. C.; Puerta, J.; Romero, L.; Salicio, J. M.; Willmott, C.

    2000-10-01

    A prototype of the CMS Barrel Muon Detector incorporating all the features of the final chambers was built at CIEMAT using the mass production assembly procedures and tools. The performance of this prototype was studied in a muon test beam at CERN and the results obtained are presented here. (Author)

  7. DIFFERENCES IN RESULTS OBTAINED BY STUDENTS OF DIFFERENT FACULTIES

    Directory of Open Access Journals (Sweden)

    OTAVOVÁ, Miroslava

    2016-03-01

    Full Text Available The paper presents and discusses the results of statistical analysis of differences among scores obtained by students of different faculties of the University of Economics in Prague. The analysed dataset contains the scores for 2256 students that took basic mathematics course during the academic year 2013/2014. A two way analysis of variance was performed with semester and faculty as main factors. The interaction between these two factors was also considered. Students have to take two tests. At first, the sum of the scores obtained from both tests is analysed and then, the two tests are analysed separately. It turns out that the significance of factors is the same in the three analyses. The assumptions of linear models are verified. Due to problem of heteroscedasticity, weighted least squares are used and the possibility of using Box-Cox transformation is also discussed, as the errors are not normally distributed. Finally, the differences between the faculties are described.

  8. An overview of results obtained in intercomparison exercises for determination of actinides

    International Nuclear Information System (INIS)

    Benedik, L.

    2013-01-01

    In recent years the Jožef Stefan Institute participated in numerous intercomparison exercises for determination of natural and man-made radionuclides. The reported values were mostly in good agreement with the resulting reference values. This paper describes an analysis of the measurement results obtained in intercomparison exercises for determination of actinides in the period from 2009 to 2011, organised by the National Physical Laboratory and the Bundesamt für Strahlenschutz. The review covers neptunium, plutonium and americium radioisotopes over this period. - Highlights: • The goal of this study is an overview of results obtained in intercomparison exercises for determination of actinides. • The disagreement of results for Np-237 was evaluated. • Improvements in separation procedures were done

  9. Study of variables that affect hydrogen solubility in α + β Zr-alloys

    Energy Technology Data Exchange (ETDEWEB)

    Parodi, Santiago A. [Instituto Sabato, UNSAM–CNEA, Av. Gral. Paz 1499, San Martín B1650KNA, Buenos Aires (Argentina); Ponzoni, Lucio M.E.; De Las Heras, M. Evangelina [División Hidrógeno en Materiales, Gerencia Materiales, GAEN, Centro Atómico Constituyentes, Av. Gral. Paz 1499, San Martín, B1650KNA, Buenos Aires (Argentina); Mieza, J. Ignacio [Instituto Sabato, UNSAM–CNEA, Av. Gral. Paz 1499, San Martín B1650KNA, Buenos Aires (Argentina); División Hidrógeno en Materiales, Gerencia Materiales, GAEN, Centro Atómico Constituyentes, Av. Gral. Paz 1499, San Martín, B1650KNA, Buenos Aires (Argentina); Domizzi, Gladys, E-mail: domizzi@cnea.gov.ar [Instituto Sabato, UNSAM–CNEA, Av. Gral. Paz 1499, San Martín B1650KNA, Buenos Aires (Argentina); División Hidrógeno en Materiales, Gerencia Materiales, GAEN, Centro Atómico Constituyentes, Av. Gral. Paz 1499, San Martín, B1650KNA, Buenos Aires (Argentina)

    2016-08-15

    Zr–2.5Nb and Excel pressure tubes, both containing α and β phases were submitted to different heat treatments. Then, hydrogen Terminal Solid Solubility for Dissolution (TSSD) and Precipitation (TSSP) curves were measured by Differential Scanning Calorimetry (DSC). The solvus of Excel heat treated at 380 °C–24 h or 750 °C–0.5 h exceeds the solvus of Zr–2.5Nb in standard conditions of CANDU pressure tubes. Aging at 500 °C–168 h decreases the limit of solubility. The lowest solubility was obtained in Excel aged at 500°C–168 h. In DSC measurements the effect of maximum temperature and hold time at such temperature on solubility curves were studied. The TSSD decreases when thermal cycle causes decomposition of the β phase, and is recuperated when α → α + β transformation temperature is exceeded. The TSSP is affected not only by βZr phase decomposition but also by the relief of defects produced during hydride precipitation. - Highlights: • We heat treated Zr-2.5Nb and Excel to change α and β-phase fraction and composition. • We measured Hydrogen solvus after each heat treatment with different thermal cycles. • We found that dissolution and precipitation solvus depend on the β phase state. • Precipitation is also affected by the relief of memory effect during the thermal cycle. • Excel treated at 750 °C 0.5 h or 380 °C 24 h showed highest solubility.

  10. Hydride phase dissolution enthalpy in neutron irradiated Zircaloy-4

    International Nuclear Information System (INIS)

    Vizcaino, Pablo; Banchik, Abraham D.

    2003-01-01

    The differential calorimetric technique has been applied to measure the dissolution enthalpy, ΔH irrad δ→α , of zirconium hydrides precipitated in structural components removed from the Argentine Atucha 1 PHWR nuclear power plant after 10.3 EFPY. An average value of ΔH irrad δ→α = 5 kJ/mol H was obtained after the first calorimetric run. That value is seven times lower than the value of ΔH δ→α = 37.7 kJ/mol H recently determined in Zircaloy-4 specimens taken from similar unirradiated structural components using the same calorimetric technique, [1]. Post-irradiation thermal treatments gradually increase that low value towards the unirradiated value with increasing annealing temperature similar to that observed for TSSd irrad . Therefore the same H atom trapping mechanism during reactor operation already proposed to explain the evolution of TSSd irrad is also valid for Q irrad δ→α . As the ratio Q/ΔH is proportional to the number N H of H atoms precipitated as hydrides, the increment of Q irrad δ→α with the thermal treatment indicates that the value of N H also grows with the annealing reaching the value corresponding to the bulk H concentration when ΔH irrad δ→α ≅ 37 kJ/mol H. That is a direct indication that the post-irradiation thermal treatment releases the H atoms from their traps increasing the number of H atoms available to precipitate at the end of each calorimetric run and/or isothermal treatment. (author)

  11. Analysis of the results obtained by optical measurements in plasma focus equipments

    International Nuclear Information System (INIS)

    Bilbao, L.; Bruzzone, H.

    1982-01-01

    The results obtained by shadow and Schlieren photographies and interferometry in a 1MJ plasma focus device of Frascati (CNEN-EURATOM, Italy) are compared with a great number of similar measurement results in several devices of the world. A critical analysis of the above results is presented. (L.C.) [pt

  12. Self-propelled prospection methodology: first results obtained in the northeast basin (Uruguay)

    International Nuclear Information System (INIS)

    Goso, H; Spoturno, J; Peciozzi, F.

    2008-01-01

    This report refers about uranium prospection methodology in Uruguay and its first results obtained in the northeast basin.The preliminary radiometric researching is carried out four works phases: material preparation, radiometric, statistics analysis, anomalies revision

  13. Overview of galactic results obtained by MAGIC

    Energy Technology Data Exchange (ETDEWEB)

    Zanin, Roberta

    2013-06-15

    MAGIC is a system of two atmospheric Cherenkov telescopes which explores the very-high-energy sky, from some tens of GeV up to tens of TeV. Located in the Canary island of La Palma, MAGIC has the lowest energy threshold among the instruments of its kind, well suited to study the still poorly explored energy band below 100 GeV. Although the space-borne gamma-ray telescope Fermi/LAT is sensitive up to 300 GeV, gamma-ray rates drop fast with increasing energy, so γ-ray collection areas larger than 10{sup 4}m{sup 2}, as those provided by grounds-based instruments, are crucial above a few GeV. The combination of MAGIC and Fermi/LAT observations have provided the first astrophysical spectra sampled in the inverse Compton peak region, resulting in a complete coverage from MeV up to TeV energies, as well as the discovery of a pulsed emission in the very-high-energy band. This paper focuses on the latest results on Galactic sources obtained by MAGIC which are highlighted by the detection of the pulsed gamma-ray emission from the Crab pulsar up to 400 GeV. In addition, we will present the morphological study on the W51 complex which allowed to pinpoint the location of the majority of the emission around the interaction point between the supernova remnant W51C and the star forming region W51B, but also to find a possible contribution from the associated pulsar wind nebula. Other important scientific achievements involve the Crab Nebula with an unprecedented spectrum covering three decades in energy starting from 50 GeV and a morphological study of the unidentified source HESS J1857+026 which supports the pulsar wind nebula scenario. Finally we will report on the searches of very-high-energy signals from gamma-ray binaries, mainly LS I 303+ and HESS J0632+057.

  14. CIEMAT interlaboratories comparison of the results obtained in the proficiency test run by IAEA

    International Nuclear Information System (INIS)

    Gasco, C.; Anton, M. P.; Alvarez, A.; Navarro, N.; Meral, J.; Gonzalez, A.; Higueras Lafaja, E.

    2000-01-01

    This report contains the results obtained by two different laboratories from CIEMAT after participating in the Proficiency Test organised by IAEA (International Atomic Energy Agency) in 1999. This test involves the analysis of fly ashes containing natural radionuclides and different amounts of added transuranics. The extraction techniques, counting methods and results obtained are detailed. This type of test are used for the labs to achieve their accreditation and check the reliability of the procedures routinely employed. (Author) 4 refs

  15. LEP and results obtained by DELPHI after four years of operation

    International Nuclear Information System (INIS)

    Blocki, J.

    1993-10-01

    We characterize the most important problems of modern elementary particles physics, for the solution of which the LEP (Large Electron Positron) accelerator was built. We present the characteristics of this accelerator. The structure and properties of the DELPHI detector are described with special emphasis on the contribution of Polish groups. The most important results obtained so far in the LEP accelerator are discussed. (author). 12 refs, 17 figs, 1 tab

  16. Comparison of the results of radiation transport calculation obtained by means of different programs

    International Nuclear Information System (INIS)

    Gorbatkov, D.V.; Kruchkov, V.P.

    1995-01-01

    Verification of calculational results of radiation transport, obtained by the known, programs and constant libraries (MCNP+ENDF/B, ANISN+HILO, FLUKA92) by means of their comparison with the precision results calculations through ROZ-6N+Sadko program constant complex and with experimental data, is carried out. Satisfactory agreement is shown with the MCNP+ENDF/B package data for the energy range of E<14 MeV. Analysis of the results derivations, obtained trough the ANISN-HILO package for E<400 MeV and the FLUKA92 programs of E<200 GeV is carried out. 25 refs., 12 figs., 3 tabs

  17. Obtaining patient test results from clinical laboratories: a survey of state law for pharmacists.

    Science.gov (United States)

    Witry, Matthew J; Doucette, William R

    2009-01-01

    To identify states with laws that restrict to whom clinical laboratories may release copies of laboratory test results and to describe how these laws may affect pharmacists' ability to obtain patient laboratory test results. Researchers examined state statutes and administrative codes for all 50 states and the District of Columbia at the University of Iowa Law Library between June and July 2007. Researchers also consulted with lawyers, state Clinical Laboratory Improvement Amendments officers, and law librarians. Laws relating to the study objective were analyzed. 34 jurisdictions do not restrict the release of laboratory test results, while 17 states have laws that restrict to whom clinical laboratories can send copies of test results. In these states, pharmacists will have to use alternative sources, such as physician offices, to obtain test results. Pharmacists must consider state law before requesting copies of laboratory test results from clinical laboratories. This may be an issue that state pharmacy associations can address to increase pharmacist access to important patient information.

  18. Deep-sequencing protocols influence the results obtained in small-RNA sequencing.

    Directory of Open Access Journals (Sweden)

    Joern Toedling

    Full Text Available Second-generation sequencing is a powerful method for identifying and quantifying small-RNA components of cells. However, little attention has been paid to the effects of the choice of sequencing platform and library preparation protocol on the results obtained. We present a thorough comparison of small-RNA sequencing libraries generated from the same embryonic stem cell lines, using different sequencing platforms, which represent the three major second-generation sequencing technologies, and protocols. We have analysed and compared the expression of microRNAs, as well as populations of small RNAs derived from repetitive elements. Despite the fact that different libraries display a good correlation between sequencing platforms, qualitative and quantitative variations in the results were found, depending on the protocol used. Thus, when comparing libraries from different biological samples, it is strongly recommended to use the same sequencing platform and protocol in order to ensure the biological relevance of the comparisons.

  19. Summary of personal neutron dosemeter results obtained within the EVIDOS project

    International Nuclear Information System (INIS)

    Luszik-Bhadra, M.; Reginatto, M.; Schuhmacher, H.; Bolognese-Milsztajn, T.; Lacoste, V.; Boschung, M.; Fiechtner, A.; Coeck, M.; Vanhavere, F.; Curzio, G.; Errico d', F.; Kylloenen, J.-E.; Lindborg, L.; Bartlett, D.; Tanner, R.

    2005-01-01

    Full text: Within the EC project EVIDOS ('Evaluation of Individual Dosimetry in Mixed Neutron and Photon Radiation Fields'), different types of neutron personal dosemeters were irradiated in workplace fields in nuclear installations in Europe. Mostly electronic personal neutron dosemeters were tested, among them commercial devices (Thermo Electron EPD-N, Aloka PDM-313), devices from first industrial prototype series (Thermo Electron EPD-N2, Saphydose-n) and laboratory prototypes which were already in the stage of lightweight battery-operated instruments (PTB DOS-2002). In addition, dosemeters with (almost) immediate readout (BTI bubble detectors, Rados DIS-N) and passive dosemeters which needed no fielddependent calibration factors (PADC track detectors from PSI and NRPB) were used, as well as those TLD albedo dosemeters which are routinely used in the facilities visited. The results of measurements obtained within the EVIDOS project in workplace fields in nuclear installations in Europe, i.e. at Kruemmel (boiling water reactor, transport cask), at Mol (Venus research reactor, fuel facility Belgonucleaire) and at Ringhals (pressurized water reactor, transport cask) are presented and compared to reference values of personal dose equivalent H p (10) determined by means of Bonner spheres and novel directional spectrometers. In fields with strong back-scatter and moderation of neutrons, several dosemeters showed overreadings by more than a factor of two. In strongly directed fields with neutron dose equivalent peaked at about 1 MeV (MOX fuel), the same dosemeters showed under-readings of about a factor of two. These under- and over-readings in the workplace fields can be explained in terms of the dosemeter response functions for mono-energetic neutrons, which show over-responses in the thermal and intermediate neutron energy region and under-responses at about 1 MeV neutron energy. The dosemeter readings obtained in the workplace fields were checked for consistency by

  20. New dynamics information from experimental results obtained in d-Au collisions at RHIC-BNL energies

    International Nuclear Information System (INIS)

    Jipa, Alexandru

    2004-01-01

    During the last runs d-Au collisions at √s NN = 200 GeV have been investigated at RHIC-BNL using the BRAHMS Experiment. Some interesting experimental results on charged particle multiplicities, rapidity distributions, transverse momentum spectra, antiparticle to particle ratios, participant spectator evolution have been obtained. In this work the most interesting results are presented for different rapidity and collision centrality ranges. Taking into account the importance of the collision geometry and collision symmetry in the collision dynamics, comparisons with the similar experimental results obtained in Au-Au collisions have been done. New interesting results can be reported. The most significant are related to the evolution of the nuclear modification factor with rapidity and collision centrality. The high transverse momentum suppression and the behaviours in different rapidity and centrality ranges suggest strong initial state effects. These effects could be related to the gluonic structure of the colliding nuclei. Some insights on the Color Glass Condensate formation are possible. (author)

  1. Lambing results obtained with imported Ile de France rarn semen

    African Journals Online (AJOL)

    insemination was carried out either 54,5 h (fixed time single ... Table 1 Conception rate obtained using two batches of frozen lle de France ... Pregnant mare serum gonadotrophin (Fostim, 300 ... Effect of initial freezing temperature, addition.

  2. Preliminary results obtained from a dense plasma focus

    International Nuclear Information System (INIS)

    Sinman, S.; Sinman, A.

    1982-01-01

    In this study, for the data processing in our Dense Plasma Focus (DPF) system, a multiparameters numerical hierarchy obtained from the fundamental equations based on the snowplows model and its conclusions have been developed. Evaluating the data along the transients of the total plasma current, the anode current and the focus voltage recorded by an oscilloscope, they have been possible to determine the time domain plasma parameters such as the shock thickness, the sheath temperature, velocity and electron density, the pressure at the focus phase and the plasma temperature. Besides, the dissipated energy through the focus notch or in other words, the plasma temperature has also been calculated by means of the numerical integration. In the text, a performance chart together with some other correlation curves for the optimization of the DPF systems are submitted and discussed. (author)

  3. Near-Infrared Scintillation of Liquid Argon: Recent Results Obtained with the NIR Facility at Fermilab

    Energy Technology Data Exchange (ETDEWEB)

    Escobar, C. O. [Fermilab; Rubinov, P. [Fermilab; Tilly, E. [Sewanee U.

    2018-03-19

    After a short review of previous attempts to observe and measure the near-infrared scintillation in liquid argon, we present new results obtained with NIR, a dedicated cryostat at the Fermilab Proton Assembly Building (PAB). The new results give confidence that the near-infrared light can be used as the much needed light signal in large liquid argon time projection chambers.11 pages,

  4. Results of Investigative Tests of Gas Turbine Engine Compressor Blades Obtained by Electrochemical Machining

    Science.gov (United States)

    Kozhina, T. D.; Kurochkin, A. V.

    2016-04-01

    The paper highlights results of the investigative tests of GTE compressor Ti-alloy blades obtained by the method of electrochemical machining with oscillating tool-electrodes, carried out in order to define the optimal parameters of the ECM process providing attainment of specified blade quality parameters given in the design documentation, while providing maximal performance. The new technological methods suggested based on the results of the tests; in particular application of vibrating tool-electrodes and employment of locating elements made of high-strength materials, significantly extend the capabilities of this method.

  5. Results obtained on dileptons and prospects

    International Nuclear Information System (INIS)

    Roche, G.

    1992-01-01

    Experimental results (mostly from the DLS collaboration at LBL) and model calculations of dielectron production in pp/pd/pBe (1-5 GeV) and CaCa (1-2 GeV/A) are presented. Dileptons appear to be a suitable probe to approach in-medium properties of hadrons in nuclear matter. At the present time, the ρ/ω region looks the most promising. Oncoming programs are briefly presented, in particular the HADES project at GSI. 7 figs

  6. First results obtained from the Cello liquid argon end cap calorimeters

    International Nuclear Information System (INIS)

    Le Diberder, F.

    1981-05-01

    The Cello liquid argon calorimeter is presented in the first part of this thesis. The cryogenic system has to supply three cryostats filled with liquid argon: one cylindrical cryostat of 25 m 3 volume contains 2x8 separate modules; each of the two symmetric end cap cryostats contains two half cylindrical modules. Each module in the end cap part consists of 42 layers of lead strips interleaved with 43 full plates. The strips are alternatively vertical, horizontal and circular. In front of the lead calorimeter are 4 planes of copper foils glued on epoxy for dE/dx measurement. The electronics, signal processing and data acquisition system are described. In the second part, the performance and analysis of data measured by the end cap calorimeters are reported: study of Bhabha scattering e + e - → e + e - ; preliminary results obtained in two photon physics e + e - → e + e - γγ → e + e - X [fr

  7. Preliminary observations and results obtained with the ultraviolet spectrometer and polarimeter

    International Nuclear Information System (INIS)

    Tandberg-Hanssen, E.; Athay, R.G.; Beckers, J.M.; Brandt, J.C.; Bruner, E.C.; Chapman, R.D.; Cheng, C.C.; Burman, J.G.; Henze, W.; Hyder, C.L.; Michalitsianos, A.G.; Shine, R.A.; Schoolman, S.A.; Woodgate, B.E.

    1981-01-01

    We present new observations with the Ultraviolet Spectrometer and Polarimeter (UVSP) of a number of manifestations of solar activity obtained during the first 3 months of Solar Maximum Mission operations

  8. The effect of uncertainty of reactor parameters obtained using k0-NAA on result of analysis

    International Nuclear Information System (INIS)

    Sasajima, Fumio

    2006-01-01

    Neutron Activation Analysis using the k 0 method is a useful method allowing convenient and accurate simultaneous analysis of plural elements, eliminating the need for the use of comparative reference samples. As already well known, it is essential for the correct result of an analysis to obtain the α-factor and f-factor for a neutron spectrum in an irradiation field accurately when an attempt is made to use the k 0 method. For this reason, based on data obtained from the experiment conducted in the JRR-3 PN-3 system, how uncertainty of the measured values for α-factor and f-factor affects the result of an analysis was evaluated. The process of evaluation involved intentionally varying the values for reactor parameters followed by making an analysis of environmental reference samples (NIST SRM-1632c) using the k 0 method to examine the effect of these factors on the concentrations of 19 elements. The result of the evaluation revealed that the degree of the effect of uncertainty on the concentrations of 19 elements was at best approx. 1% under the condition of this experiment assuming that the factor α, a reactor parameter, had uncertainty of approx. 200%. (author)

  9. Results obtained with the passive radiation detectors in the ICCHIBAN-4 experiment

    International Nuclear Information System (INIS)

    Bilski, P.; Horwacik, T.

    2005-05-01

    In frame of the InterComparison of Cosmic rays with Heavy Ions Beams at NIRS (ICCHIBAN) organized at the HIMAC accelerator in Chiba several types of the thermoluminescent detectors (TLD), as well as CR-39 track detectors, were exposed. Four different types of TLDs were used: MTS-7 ( 7 LiF:Mg,Ti), MTS-6 ( 6 LiF:Mg,Ti), MCP-7 ( 7 LiF:Mg,Cu,P) and MTT-7 ( 7 LiF:Mg,Ti with changed activator composition. All TLDs were manufactured at the Institute of Nuclear Physics (INP) in Cracow. The detectors were irradiated with various doses of He, C, Ne and Fe ions. Part of exposures were done in unknown conditions, to test measuring capabilities of the detectors. For analyses of these results, the method of obtaining information on ionisation density of an unknown radiation field, which is based on ratios of responses of different LiF detectors, was successfully used. (author)

  10. Brief review of topmost scientific results obtained in 2016 at the Joint Institute for Nuclear Research

    International Nuclear Information System (INIS)

    Kravchenko, E.I.; Sabaeva, E.V.

    2017-01-01

    This brief review presents the topmost scientific results obtained in 2016 at the Joint Institute for Nuclear Research in such fields as theoretical and experimental physics, radiation and radiobiological research, accelerators, information technology and computer physics. It also provides information about the publications by JINR staff members and activities carried out at the JINR University Centre in 2016. [ru

  11. New high-definition thickness data obtained at tropical glaciers: preliminary results from Antisana volcano (Ecuador) using GPR prospection

    Science.gov (United States)

    Zapata, Camilo; Andrade, Daniel; Córdova, Jorge; Maisincho, Luis; Carvajal, Juan; Calispa, Marlon; Villacís, Marcos

    2014-05-01

    The study of tropical glaciers has been a significant contribution to the understanding of glacier dynamics and climate change. Much of the data and results have been obtained by analyzing plan-view images obtained by air- and space-borne sensors, as well as depth data obtained by diverse methodologies at selected points on the glacier surface. However, the measurement of glacier thicknesses has remained an elusive task in tropical glaciers, often located in rough terrains where the application of geophysical surveys (i.e. seismic surveys) requires logistics sometimes hardly justified by the amount of obtained data. In the case of Ecuador, however, where most glaciers have developed on active volcanoes and represent sources/reservoirs of fresh water, the precise knowledge of such information is fundamental for scientific research but also in order to better assess key aspects for the society. The relatively recent but fast development of the GPR technology has helped to obtain new highdefinition thickness data at Antisana volcano that will be used to: 1) better understand the dynamics and fate of tropical glaciers; 2) better estimate the amount of fresh water stored in the glaciers; 3) better assess the hazards associated with the sudden widespread melting of glaciers during volcanic eruptions. The measurements have been obtained at glaciers 12 and 15 of Antisana volcano, with the help of a commercial GPR equipped with a 25 MHz antenna. A total of 30 transects have been obtained, covering a distance of more than 3 km, from the glacier ablation zone, located at ~ 4600 masl, up to the level of 5200 masl. The preliminary results show a positive correlation between altitude and glacier thickness, with maximum and minimum calculated values reaching up to 80 m, and down to 15 m, respectively. The experience gained at Antisana volcano will be used to prepare a more widespread GPR survey in the glaciers of Cotopaxi volcano, whose implications in terms of volcanic hazards

  12. Brief review of topmost scientific results obtained in 2015 at the Joint Institute for Nuclear Research

    International Nuclear Information System (INIS)

    Sabaeva, E.V.; Krupko, E.I.

    2016-01-01

    This brief review presents the topmost scientific results obtained in 2015 at the Joint Institute for Nuclear Research in such fields as theoretical and experimental physics, radiation and radiobiological research, accelerators, information technology and computer physics. It also provides information about the publications by JINR staff members, awards given to JINR scientists, and activities carried out at the JINR University Centre in 2015. [ru

  13. Brief review of topmost scientific results obtained in 2013 at the Joint Institute for Nuclear Research

    International Nuclear Information System (INIS)

    Sabaeva, E.V.; Kravchenko, E.I.

    2014-01-01

    This brief review presents the topmost scientific results obtained in 2013 at the Joint Institute for Nuclear Research in such areas as theoretical physics, experimental physics, radiation and radiobiological research, accelerators, information technology and computer physics. It also provides information on the number of publications by JINR staff members, awards given to JINR scientists, and activities carried out at the JINR University Centre in 2013.

  14. Brief review of topmost scientific results obtained in 2014 at the Joint Institute for Nuclear Research

    International Nuclear Information System (INIS)

    Bulatova, V.V.; Sabaeva, E.V.

    2015-01-01

    This brief review presents the topmost scientific results obtained in 2014 at the Joint Institute for Nuclear Research in such fields as theoretical and experimental physics, radiation and radiobiological research, accelerators, information technology and computer physics. It also provides information about the publications by JINR staff members, patents for inventions, awards given to JINR scientists, and activities carried out at the JINR University Centre in 2014. [ru

  15. Pipeline inspection - failures selection and results obtained; Inspeccion interna de ductos - seleccion de fallas y resultados obtenidos

    Energy Technology Data Exchange (ETDEWEB)

    Motylicki, Juan Enrique [Oleoductos del Valle S.A. (OLDEVAL S.A.), (Argentina)

    2003-07-01

    The main objective of the pipelines maintenance is to assure the integrity of them in order to have a reliable operation and with an acceptable level of risk that minimizes the impact to people, to the environment and the business. The objective of this work is to expose the experiences obtained before by Oldelval and after the passages of the intelligent pig, carried out in the years 1999/2000. In the same one they will be described: How the flaws were selected to verify / to repair. Results obtained in digs. Laboratory studies to determine like they affect to the integrity of the pipeline, the different types of opposing plane defects. Conclusions. (author)

  16. Method of forecasting pollutant transfer in an aquifer initial results obtained in a sandy medium (Barp site, Gironde)

    International Nuclear Information System (INIS)

    Madoz-Escande, C.; Peyrus, J.-C.

    1979-01-01

    Hydrogeological studies are undertaken in the context of the radiological safety of nuclear plants to forecast consequences of accidental releases of radioactive pollutants into an aquifer (transfer time, concentration at points of emergence). This quantitative forecast is obtained with the aid of a mathematical model with sequential emission. This requires a knowledge of the physical parameters of the aquifer and of the behavior of the pollutant in relation to the water-bearing medium. The physical parameters of a saturated porous medium are presented with the aid of radioactive tracer tests on a model and also in the field. The initial results obtained in a sandy medium are presented. In view of the difficulty of extrapolating to field conditions the conclusions of tests on models, it was necessary to set up a mobile laboratory with which in situ studies could be undertaken. The behavior of the pollutant in relation to the water-bearing medium is the subject of preliminary laboratory research on the laws of adsorption under different pH and temperature conditions. The numerical results obtained call for confirmation in the field. A description is given of a method which should enable the distribution coefficients to be evaluated in situ

  17. Calorimetric determination of the δ hydride dissolution enthalpy in Zircaloy-4

    International Nuclear Information System (INIS)

    Vizcaino, Pablo; Banchik, Abraham D.

    2003-01-01

    In this work, the dissolution enthalpy, ΔH δ→α , of the δ hydride phase in the αZr matrix in Zircaloy-4 has been determined with a differential scanning calorimeter (DSC) in two different ways: by means of a vant Hoff equation, measuring the terminal solubility temperature in dissolution, TSSd, and by direct measurement of the dissolution heat, Q δ→α , as the area between the base line and the calorimetric curve. The application of the DSC technique to the hydride dissolution heat measurements, a transformation which covers an extended temperature range, is completely original and requires a special treatment of the calorimetric curve. These measurements were done on samples, which practically cover the whole solubility range of hydrogen in αZr phase (80-640 ppm). The values obtained, 36.9 kJ/mol H and 39.3 kJ/mol H respectively, are self-consistent and in good agreement with the values of the more recent revisions, but reduces considerably the scatter of the literature data. (author)

  18. The results obtained by INR-Pitesti to an international in-situ intercomparison exercise

    International Nuclear Information System (INIS)

    Dobrin, Relu; Dulama, Cristian; Toma, Alexandru

    2008-01-01

    Full text: The determination of soil contamination, dose rate measurements and in-situ gamma spectrometry are well established and widely used measurement procedures, especially after large scale nuclear incidents. To support decision makers and first responders with a more comprehensive and accurate overview immediately after a large scale nuclear or radiological emergency, as releases from a nuclear power plant or a terrorist attack with a dirty bomb, a fast and clear presentation of measurement data is indispensable. In 2007, the Austrian Research Centers GmbH - ARC (Seibersdorf) in cooperation with IAEA and the Austrian NBC Defense School organized an international measurement campaign, 'In-Situ Intercomparison Scenario' ISIS 2007, with the focus on In-Situ Gamma Spectrometry and Dose Rate Measurements in Emergency Situations. 56 teams from 25 countries, worldwide, took part to this exercise. The only Romanian team was 'CROWN'. The CROWN Laboratory is part of the Radiation Protection Laboratory of the Institute for Nuclear Research - Pitesti, certified for characterization of radioactive wastes and nuclear materials. The paper presents results obtained during different tasks of the exercise: 'Dose rate mapping'; 'Localization - Drive by'; 'Simulation of a contamination'; 'Identification Shielded; 'Identification/Quantification'; 'Buried sources; 'Environmental measurement'. (authors)

  19. Comparison between dosimeter films and electronic dosimeters results obtained in F-18 production practices at IEN/CNEN

    International Nuclear Information System (INIS)

    Paulo, Osvaldir; Carlos, Luiz R.J.; Mendes, Milton

    2008-01-01

    Full text: The aim of the present work is the comparison of the dose rates values obtained from dosimeter films with the values obtained from electronic dosimeters used by radiological protection technician involved in practices with fluorine-18 production in CV-28 cyclotron at IEN/CNEN. The motivation for this work was the increase on the demand of this radiopharmaceutical. Nowadays there is an increase demand on the number of clinics and hospitals which had started to use the technique of radiodiagnostic using positron-emission tomography (PET). Therefore, the produced radionuclide activities (physics quantity) and also the complexity of the practices of radiological protection in the areas of that facility had increased a lot. The conventional statistical methods will be used to evaluate the results obtained in the analysis of the data obtained in the reading of the dosimeters. This comparative method is however a first step to taking decisions regarding radiological protection service. Therefore that the radiometric surveys of routine are taken in consideration, as well as the information from the technician of radiological protection that is working in those areas. All this data will give support to improve and implement methods and practices on the accelerators' facilities. In addition, the use of these electronic dosimeters will makes possible the technician read these dose rates received immediately during the practices and use these information you make decisions. In case of dose rates values to present above the expected the practice will be ploughed. Another point to be considered is that this work will propitiate the future updates of the procedures designated to those practices and to conduct at the radiological protection optimization. (author)

  20. Experimental results obtained with the simulated cold moderator system. System characteristics and technical issues

    CERN Document Server

    Aso, T; Hino, R; Kaminaga, M; Kinoshita, H; Takahashi, T

    2002-01-01

    The Japan Atomic Energy Research Institute and the High Energy Accelerator Research Organization have been developing a Mega-Watt scale spallation target system. In the system, neutrons generated in a target are sorted out their energy to the proper values in liquid-hydrogen moderators. Then, the liquid-hydrogen is forced to circulate in order to suppress hydrogen temperature increase. In the operation of moderators, it is very important to establish a safety protection system against emergency shutdown of the accelerator or accidents of the cold moderator system. In order to obtain a technical data for design and safety review of the liquid-hydrogen system, we have fabricated an experimental apparatus simulated the cold moderator system using liquid nitrogen (max. 1.5 MPa, mini. 77 K) instead of liquid hydrogen. The experiments on a controllability of the system were carried out to investigate dynamic characteristics of the system. This report presents the experimental results and technical issues for the co...

  1. Experimental Results Obtained with Air Liquide Cold Compression System CERN LHC and SNS Projects

    CERN Document Server

    Delcayre, F; Hamber, F; Hilbert, B; Monneret, E; Toia, J L

    2006-01-01

    Large scale collider facilities will make intensive use of superconducting magnets, operating below 2.0 K. This dictates high‐capacity refrigeration systems operating below 2.0 K. These systems, making use of cryogenic centrifugal compressors in a series arrangement with room temperature screw compressors will be coupled to a refrigerator, providing a certain power at 4.5 K. A first Air Liquide Cold Compression System (CCS) unit was built and delivered to CERN in 2001. Installed at the beginning of 2002, it was commissioned and tested successfully during year 2002. A series of four sets of identical CCS were then tested in 2004. Another set of four cryogenic centrifugal compressors (CCC) has been delivered to Thomas Jefferson National Accelerator Facility (JLAB) for the Spallation Neutron Source (SNS) in 2002. These compressors were tested and commissioned from December 2004 to July 2005. The experimental results obtained with these systems will be presented and discussed: the characteristics of the CCC wil...

  2. Measurement results obtained from air quality monitoring system

    Energy Technology Data Exchange (ETDEWEB)

    Turzanski, P.K.; Beres, R. [Provincial Inspection of Environmental Protection, Cracow (Poland)

    1995-12-31

    An automatic system of air pollution monitoring operates in Cracow since 1991. The organization, assembling and start-up of the network is a result of joint efforts of the US Environmental Protection Agency and the Cracow environmental protection service. At present the automatic monitoring network is operated by the Provincial Inspection of Environmental Protection. There are in total seven stationary stations situated in Cracow to measure air pollution. These stations are supported continuously by one semi-mobile (transportable) station. It allows to modify periodically the area under investigation and therefore the 3-dimensional picture of creation and distribution of air pollutants within Cracow area could be more intelligible.

  3. Potential theory for stationary Schrödinger operators: a survey of results obtained with non-probabilistic methods

    Directory of Open Access Journals (Sweden)

    Marco Bramanti

    1992-05-01

    Full Text Available In this paper we deal with a uniformly elliptic operator of the kind: Lu  Au + Vu, where the principal part A is in divergence form, and V is a function assumed in a “Kato class”. This operator has been studied in different contexts, especially using probabilistic techniques. The aim of the present work is to give a unified and simplified presentation of the results obtained with non probabilistic methods for the operator L on a bounded Lipschitz domain. These results regard: continuity of the solutions of Lu=0; Harnack inequality; estimates on the Green's function and L-harmonic measure; boundary behavior of positive solutions of Lu=0, in particular a “Fatou's theorem”.

  4. Experimental Results Obtained with Air Liquide Cold Compression System: CERN LHC and SNS Projects

    Science.gov (United States)

    Delcayre, F.; Courty, J.-C.; Hamber, F.; Hilbert, B.; Monneret, E.; Toia, J.-L.

    2006-04-01

    Large scale collider facilities will make intensive use of superconducting magnets, operating below 2.0 K. This dictates high-capacity refrigeration systems operating below 2.0 K. These systems, making use of cryogenic centrifugal compressors in a series arrangement with room temperature screw compressors will be coupled to a refrigerator, providing a certain power at 4.5 K. A first Air Liquide Cold Compression System (CCS) unit was built and delivered to CERN in 2001. Installed at the beginning of 2002, it was commissioned and tested successfully during year 2002. A series of four sets of identical CCS were then tested in 2004. Another set of four cryogenic centrifugal compressors (CCC) has been delivered to Thomas Jefferson National Accelerator Facility (JLAB) for the Spallation Neutron Source (SNS) in 2002. These compressors were tested and commissioned from December 2004 to July 2005. The experimental results obtained with these systems will be presented and discussed: the characteristics of the CCC will be detailed. The principles of control for the CCC in series will be detailed.

  5. Experimental results obtained with the simulated cold moderator system. System characteristics and technical issues

    Energy Technology Data Exchange (ETDEWEB)

    Aso, Tomokazu; Kaminaga, Masanori; Haga, Katsuhiro; Kinoshita, Hidetaka; Takahashi, Toshio; Hino, Ryutaro [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    2002-12-01

    The Japan Atomic Energy Research Institute and the High Energy Accelerator Research Organization have been developing a Mega-Watt scale spallation target system. In the system, neutrons generated in a target are sorted out their energy to the proper values in liquid-hydrogen moderators. Then, the liquid-hydrogen is forced to circulate in order to suppress hydrogen temperature increase. In the operation of moderators, it is very important to establish a safety protection system against emergency shutdown of the accelerator or accidents of the cold moderator system. In order to obtain a technical data for design and safety review of the liquid-hydrogen system, we have fabricated an experimental apparatus simulated the cold moderator system using liquid nitrogen (max. 1.5 MPa, mini. 77 K) instead of liquid hydrogen. The experiments on a controllability of the system were carried out to investigate dynamic characteristics of the system. This report presents the experimental results and technical issues for the construction of a practical liquid-hydrogen moderator system of the Mega-Watt scale target system. (author)

  6. Pregnancy does not affect HIV incidence test results obtained using the BED capture enzyme immunoassay or an antibody avidity assay.

    Directory of Open Access Journals (Sweden)

    Oliver Laeyendecker

    2010-10-01

    Full Text Available Accurate incidence estimates are needed for surveillance of the HIV epidemic. HIV surveillance occurs at maternal-child health clinics, but it is not known if pregnancy affects HIV incidence testing.We used the BED capture immunoassay (BED and an antibody avidity assay to test longitudinal samples from 51 HIV-infected Ugandan women infected with subtype A, C, D and intersubtype recombinant HIV who were enrolled in the HIVNET 012 trial (37 baseline samples collected near the time of delivery and 135 follow-up samples collected 3, 4 or 5 years later. Nineteen of 51 women were also pregnant at the time of one or more of the follow-up visits. The BED assay was performed according to the manufacturer's instructions. The avidity assay was performed using a Genetic Systems HIV-1/HIV-2 + O EIA using 0.1M diethylamine as the chaotropic agent.During the HIVNET 012 follow-up study, there was no difference in normalized optical density values (OD-n obtained with the BED assay or in the avidity test results (% when women were pregnant (n = 20 results compared to those obtained when women were not pregnant (n = 115; for BED: p = 0.9, generalized estimating equations model; for avidity: p = 0.7, Wilcoxon rank sum. In addition, BED and avidity results were almost exactly the same in longitudinal samples from the 18 women who were pregnant at only one study visit during the follow-up study (p = 0.6, paired t-test.These results from 51 Ugandan women suggest that any changes in the antibody response to HIV infection that occur during pregnancy are not sufficient to alter results obtained with the BED and avidity assays. Confirmation with larger studies and with other HIV subtypes is needed.

  7. Echocardiographic phase imaging to predict reverse remodeling after cardiac resynchronization therapy.

    Science.gov (United States)

    Buss, Sebastian J; Humpert, Per M; Bekeredjian, Raffi; Hardt, Stefan E; Zugck, Christian; Schellberg, Dieter; Bauer, Alexander; Filusch, Arthur; Kuecherer, Helmut; Katus, Hugo A; Korosoglou, Grigorios

    2009-05-01

    The aim of our study was to investigate whether echocardiographic phase imaging (EPI) can predict response in patients who are considered for cardiac resynchronization therapy (CRT). CRT improves quality of life, exercise capacity, and outcome in patients with bundle-branch block and advanced heart failure. Previous studies used QRS duration to select patients for CRT; the accuracy of this parameter to predict functional recovery, however, is controversial. We examined 42 patients with advanced heart failure (New York Heart Association [NYHA] functional class III to IV, QRS duration >130 ms, and ejection fraction or=15% at 6 to 8 months of follow-up were defined as responders. All others were classified as nonresponders. The Ts-SD and the mean EPI-Index were related to Delta ESV (r = 0.43 for Ts-SD and r = 0.67 for mean EPI-Index, p < 0.01 for both), and both parameters yielded similar accuracy for the prediction of LV remodeling (area under the curve of 0.87 for TDI vs. 0.90 for EPI, difference between areas = 0.03, p = NS) and ejection fraction (EF) improvement (area under the curve of 0.87 for TDI vs. 0.93 for EPI, difference between areas = 0.06, p = NS). Furthermore, patients classified as responders by EPI (mean EPI-Index

  8. Paternity tests in Mexico: Results obtained in 3005 cases.

    Science.gov (United States)

    García-Aceves, M E; Romero Rentería, O; Díaz-Navarro, X X; Rangel-Villalobos, H

    2018-04-01

    National and international reports regarding the paternity testing activity scarcely include information from Mexico and other Latin American countries. Therefore, we report different results from the analysis of 3005 paternity cases analyzed during a period of five years in a Mexican paternity testing laboratory. Motherless tests were the most frequent (77.27%), followed by trio cases (20.70%); the remaining 2.04% included different cases of kinship reconstruction. The paternity exclusion rate was 29.58%, higher but into the range reported by the American Association of Blood Banks (average 24.12%). We detected 65 mutations, most of them involving one-step (93.8% and the remaining were two-step mutations (6.2%) thus, we were able to estimate the paternal mutation rate for 17 different STR loci: 0.0018 (95% CI 0.0005-0.0047). Five triallelic patterns and 12 suspected null alleles were detected during this period; however, re-amplification of these samples with a different Human Identification (HID) kit confirmed the homozygous genotypes, which suggests that most of these exclusions actually are one-step mutations. HID kits with ≥20 STRs detected more exclusions, diminishing the rate of inconclusive results with isolated exclusions (Powerplex 21 kit (20 STRs) and Powerplex Fusion kit (22 STRs) offered similar PI (p = 0.379) and average number of exclusions (PE) (p = 0.339) when a daughter was involved in motherless tests. In brief, besides to report forensic parameters from paternity tests in Mexico, results describe improvements to solve motherless paternity tests using HID kits with ≥20 STRs instead of one including 15 STRs. Copyright © 2018 Elsevier Ltd and Faculty of Forensic and Legal Medicine. All rights reserved.

  9. Determination of averaged axisymmetric flow surfaces according to results obtained by numerical simulation of flow in turbomachinery

    Directory of Open Access Journals (Sweden)

    Bogdanović-Jovanović Jasmina B.

    2012-01-01

    Full Text Available In the increasing need for energy saving worldwide, the designing process of turbomachinery, as an essential part of thermal and hydroenergy systems, goes in the direction of enlarging efficiency. Therefore, the optimization of turbomachinery designing strongly affects the energy efficiency of the entire system. In the designing process of turbomachinery blade profiling, the model of axisymmetric fluid flows is commonly used in technical practice, even though this model suits only the profile cascades with infinite number of infinitely thin blades. The actual flow in turbomachinery profile cascades is not axisymmetric, and it can be fictively derived into the axisymmetric flow by averaging flow parameters in the blade passages according to the circular coordinate. Using numerical simulations of flow in turbomachinery runners, its operating parameters can be preliminarily determined. Furthermore, using the numerically obtained flow parameters in the blade passages, averaged axisymmetric flow surfaces in blade profile cascades can also be determined. The method of determination of averaged flow parameters and averaged meridian streamlines is presented in this paper, using the integral continuity equation for averaged flow parameters. With thus obtained results, every designer can be able to compare the obtained averaged flow surfaces with axisymmetric flow surfaces, as well as the specific work of elementary stages, which are used in the procedure of blade designing. Numerical simulations of flow in an exemplary axial flow pump, used as a part of the thermal power plant cooling system, were performed using Ansys CFX. [Projekat Ministarstva nauke Republike Srbije, br. TR33040: Revitalization of existing and designing new micro and mini hydropower plants (from 100 kW to 1000 kW in the territory of South and Southeast Serbia

  10. Interobserver agreement of the injury diagnoses obtained by postmortem computed tomography of traffic fatality victims and a comparison with autopsy results

    DEFF Research Database (Denmark)

    Leth, Peter Mygind; Struckmann, Henrik; Lauritsen, Jens

    2013-01-01

    The present study investigated the interobserver variation between a radiologist and a forensic pathologist in 994 injury diagnoses obtained by postmortem computed tomography (CT) of 67 traffic fatality victims, and the results were compared with diagnoses obtained by autopsy. The injuries were...... system, but the pathologist diagnosed more organ injuries. We recommend the use of a radiologist as a consultant for the evaluation of postmortem CT images. Training in radiology should be included in forensic medicine postgraduate training. CT was superior to autopsy in detecting abnormal air...

  11. Assessment of the French environment radiological status in 2009. Synthesis of the results obtained by the IRSN survey networks

    International Nuclear Information System (INIS)

    2009-01-01

    After a brief recall of the IRSN's missions, this report describes why and how radioactivity is controlled in France. It presents the national network for environment radioactivity measurements, and indicates the objectives of this radiological survey. It comments the status and levels of the natural and artificial radioactivity in France, discusses the results of the territory general survey (atmosphere, inland, coast, regions), the results of fuel cycle related sites (nuclear sites, old mining sites, front end industries, electricity production plants, back end industries, waste storage sites), the results concerning the nuclear medicine radioactive releases, the results obtained during selective expertises, and discusses the assessment of the exposure of the French population to ionizing radiations. It finally indicates how those data are published

  12. Standardization of a fluconazole bioassay and correlation of results with those obtained by high-pressure liquid chromatography.

    Science.gov (United States)

    Rex, J H; Hanson, L H; Amantea, M A; Stevens, D A; Bennett, J E

    1991-01-01

    An improved bioassay for fluconazole was developed. This assay is sensitive in the clinically relevant range (2 to 40 micrograms/ml) and analyzes plasma, serum, and cerebrospinal fluid specimens; bioassay results correlate with results obtained by high-pressure liquid chromatography (HPLC). Bioassay and HPLC analyses of spiked plasma, serum, and cerebrospinal fluid samples (run as unknowns) gave good agreement with expected values. Analysis of specimens from patients gave equivalent results by both HPLC and bioassay. HPLC had a lower within-run coefficient of variation (less than 2.5% for HPLC versus less than 11% for bioassay) and a lower between-run coefficient of variation (less than 5% versus less than 12% for bioassay) and was more sensitive (lower limit of detection, 0.1 micrograms/ml [versus 2 micrograms/ml for bioassay]). The bioassay is, however, sufficiently accurate and sensitive for clinical specimens, and its relative simplicity, low sample volume requirement, and low equipment cost should make it the technique of choice for analysis of routine clinical specimens. PMID:1854166

  13. Edaphic macrofauna as biological indicator of the conservation/disturbance status of soil. Results obtained in Cuba

    International Nuclear Information System (INIS)

    Cabrera, Grisel

    2012-01-01

    In order to predict the degradation status of a soil, a group of variables comprising its physical, chemical and/or biological properties is used. Macrofauna, which includes soil invertebrates higher than 2 mm of diameter, is a biological component that can be used for such purpose. Its taxonomic richness as well as its density, biomass and functional composition change depending on the effect of diverse land uses and managements. This review reaffirms that the macrofauna characteristics and the results obtained, mainly in Cuba, about its variation in ecosystems with different anthropization levels, support the potential use of this fauna as biological indicator of the soil's conservation status. Future studies should consider a lower taxonomic level in the identification of macrofauna, and relate its taxonomic and functional composition to the climate and pedological factors. (author)

  14. Results obtained by Trillo Nuclear Power Plant in 2001

    International Nuclear Information System (INIS)

    Solar, V.

    2002-01-01

    Unification of the Almaraz and Trillo plant managements was given a strong boost with unification of the central offices and management computer platforms (economic and technical) and with signature of an agreement with Madrid's trade unions providing for appropriate management of surpluses and the transfer of knowledge between people leaving the company and those taking their place. The operating results have been maintained at a high level although they were lower than last year, which was exceptional. The plant was on line for 7,979 hours, most of them at full load. (Author)

  15. Report of test and research results on atomic energy obtained in national institutes in fiscal 1985

    International Nuclear Information System (INIS)

    1986-01-01

    As for the test and research on the utilization of atomic energy in national institutes, the budget was appropriated for the first time in fiscal year 1956, and since then, the many valuable results of research have been obtained so far in the diversified fields of nuclear fusion, safety research, the irradiation of foods, medicine and others, thus the test and research accomplished the large role for promoting the utilization of atomic energy in Japan. In this report, the gists of the results of the test and research on the utilization of atomic energy carried out by national institutes in fiscal year 1985 are collected. No.1 of this report was published in 1960, and this is No.26. It is desired to increase the understanding about the recent trend and the results of the test and research on atomic energy utilization with this book. The researches on nuclear fusion, engineering safety and environmental radioactivity safety, the irradiation of foods, the countermeasures against cancer, fertilized soil, the quality improvement of brewing and farm products, the protection of farm products and the improvement of breeding, diagnosis and medical treatment, pharmaceuticals, environmental hygiene, the application to physiology and pathology, radiochemistry, radiation measurement, process analysis, nuclear reactor materials, nuclear powered ships, civil engineering, radioactivation analysis and injury prevention are reported. (Kako, I.)

  16. Results obtained during wall breaching research

    CSIR Research Space (South Africa)

    Hattingh, S

    2008-11-01

    Full Text Available To understand the physics of what is happening inside the wall directly after the detonation and the application of this knowledge in the improvement of the charge Measure the shock/stress waves in the masonry material and then in the wall as a whole... to maximise the effect of the charges on the walls and to broaden the knowledge of the physics of shock and stress waves. The thickness and characteristics of walls are not usually known in an operation. The effect of the charges on real buildings is still...

  17. Aircraft and ground vehicle friction correlation test results obtained under winter runway conditions during joint FAA/NASA Runway Friction Program

    Science.gov (United States)

    Yager, Thomas J.; Vogler, William A.; Baldasare, Paul

    1988-01-01

    Aircraft and ground vehicle friction data collected during the Joint FAA/NASA Runway Friction Program under winter runway conditions are discussed and test results are summarized. The relationship between the different ground vehicle friction measurements obtained on compacted snow- and ice-covered conditions is defined together with the correlation to aircraft tire friction performance under similar runway conditions.

  18. Results Obtained in Training Romanian Sport Horses for Jumping Competitions

    Directory of Open Access Journals (Sweden)

    Flavia Luminiţa Bochiş

    2012-10-01

    Full Text Available A number of 29 equines, Romanian Sport Horse stallions, were taken as green horses, break into the saddle, andteach into basic training while later train as jumpers over three years. The obstacle courses results had been obtainedin our country, in Hungary and in Serbia. There were courses jumped in the national championship, somedemonstrations organized in Romania or in the two foreign countries, or periodically test pattern courses run on theown arena. The best results, respectively more than 50% obstacle courses with no fault points over 3 years, were runby five stallions, and the same percent for 2 seasons, was reached by nine stallions.

  19. Analysis of results obtained from field tracing test under natural rain condition

    International Nuclear Information System (INIS)

    Mukai, M.; Kamiyama, H.; Tanaka, T.; Wang Zhiming; Zhao Yingjie; Li Zhengtang

    1993-01-01

    As one of the tests arranged by the cooperative research between CIRP and JAERI, field tracing tests using 3 H, 60 Co, 85 Sr and 134 Cs were conducted in pits at the CIRP's field test site located on a loess tableland under natural rain condition. Precipitation amount and evaporation rate were measured to study complicated spatial-temporal behavior of soil water movement under that condition. The evaporation rate was obtained through an analysis on the measured data by a combined method of heat balance and eddy correlation. Numerical model, that is based on piston flow assumption of soil water movement, was developed and applied to determine the behavior of the soil water movement in the pits. Using the determined water movement, 3 H migration was evaluated by numerical simulation. Change of 3 H distribution as a function of elapsed time as well explained by careful evaluation of the soil water movement that carried out before the analysis. (5 figs.)

  20. Evaluation of instrumental parameters for obtaining acceptable analytical results of the Dosimetry Laboratory of Chemistry of the Regional Center of Nuclear Sciences, CNEN-NE, Recife, Brazil

    International Nuclear Information System (INIS)

    Souza, V.L.B.; Figueiredo, M.D.C.; Cunha, M.S.

    2008-01-01

    Instrumental parameters need to be evaluated for obtaining acceptable analytical results for a specific instrument. The performance of the UV-VIS spectrophotometer can be verified for wavelengths and absorbances with appropriate materials (solutions of different concentrations of K 2 CrO 4 , for example). The aim of this work was to demonstrate the results of the procedures to control the quality of the measurements carried out in the laboratory in the last four years. The samples were analyzed in the spectrophotometer and control graphics were obtained for K 2 CrO 4 and Fe 3+ absorbance values. The variation in the results obtained for the stability of the spectrophotometer and for the control of its calibration did not exceed 2%. (author)

  1. Aero thermal test results obtained on the n. C 5 EL 4 Cluster in the atmospheric pressure cell

    International Nuclear Information System (INIS)

    Gasc, B.

    1964-01-01

    In the framework of thermal studies on the EL-4 cluster, the full-scale tests at atmospheric pressure are designed to permit measurement of local values of the wall temperature, of the velocity and of the temperature in the fluid. The experimental results, obtained with the help of an original measuring apparatus, make it possible to follow the changes in these values along the cluster and to predict in much detail the in-pile thermal behaviour. In particular it is shown that changes in the wall temperature along the cluster are greatly influenced by disruption of the flow caused by grids and supports. (author) [fr

  2. Evaluation of the CDTN's cementation facility using the results obtained in two different sizes: laboratory and facility

    International Nuclear Information System (INIS)

    Haucz, Maria Judite A.; Calabria, Jaqueline A. Almeida; Tello, Cledola Cassia O.; Candido, Francisco Donizete; Seles, Sandro Rogerio Novaes

    2011-01-01

    At CDTN R and D activities generate low-level radioactive wastes, among them the aqueous liquid ones, which need special attention due to their volumes. The usual treatment for these wastes is the volume reduction process using chemicals in order to change the radionuclides of the waste to an insoluble form. The resultant sludge is incorporated into cement in 200-liter drums using an in-line batch mixing system (CDTN Cementation Facility). The process parameters and solidified product quality are evaluated at the Cementation Laboratory (LABCIM), where tests are carried out to determine the viscosity, set time and density of the paste. In addition of the visual examination, compressive strength test and density are also established in the solidified product. In the cementation facility some pastes are also prepared for the immobilization of non-compactable waste, such as dump, scrap metal, wood, and other ones. This paper aims to present the study comparing the results of tests done in the pastes and products prepared in LABCIM and the ones obtained in CDTN's cementation facility, in order to check the efficiency of the cementation system. (author)

  3. Evaluation of the CDTN cementation facility using the results obtained in two different sizes: laboratory and facility

    International Nuclear Information System (INIS)

    Haucz, Maria Judite A.; Calabria, Jaqueline A. Almeida; Tello, Cledola Cassia O.; Candido, Francisco Donizete; Seles, Sandro Rogerio Novaes

    2011-01-01

    At CDTN R and D activities generate low-level radioactive wastes, among them the aqueous liquid ones, which need special attention due to their volumes. The usual treatment for these wastes is the volume reduction process using chemicals in order to change the radionuclides of the waste to an insoluble form. The resultant sludge is incorporated into cement in 200-liter drums using an in-line batch mixing system (CDTN Cementation Facility). The process parameters and solidified product quality are evaluated at the Cementation Laboratory (LABCIM), where tests are carried out to determine the viscosity, set time and density of the paste. In addition of the visual examination, compressive strength test and density are also established in the solidified product. In the cementation facility some pastes are also prepared for the immobilization of non-compactable waste, such as dump, scrap metal, wood, and other ones. This paper aims to present the study comparing the results of tests done in the pastes and products prepared in LABCIM and the ones obtained in CDTN's cementation facility, in order to check the efficiency of the cementation system. (author)

  4. First in-core measurement results obtained with the innovative mobile calorimeter CALMOS inside the OSIRIS material testing reactor

    International Nuclear Information System (INIS)

    Carcreff, Hubert; Salmon, Laurent; Courtaux, Cedric

    2014-01-01

    Nuclear heating rate inside an MTR has to be known in order to design and to run irradiation experiments which have to fulfill target temperature constraints. This measurement is usually carried out by calorimetry. An innovative calorimetric system, CALMOS, has been studied and built in 2011 for the 70 MWth OSIRIS reactor operated by CEA. Thanks to a new calorimetric probe, associated to a specific displacement system, it provides measurements along the fissile height and above the core. Development of the calorimetric probe required manufacturing and irradiation of mock-ups in the ex-core area, where nuclear heating rate does not exceed 2 W.g -1 . The calorimeter working mode, the different measurement procedures, main modeling and ex-core experimental results have been already presented in previous papers. In this paper, we present in-core results obtained from 2011 to 2013 with the final device. For the first time, this new experimental measurement system was operated in several experimental locations, with nominal in-core thermal hydraulic conditions, nominal neutron flux and nuclear heating rate up to 6 W.g -1 (in graphite). After a brief presentation of the displacement system specificities, first nuclear heating distributions are presented and discussed. The Finite Element model of the calorimeter was upgraded in order to match calculated temperatures with measured ones. This 'validated' model allowed to estimate a Kc factor which tends to correct small nonlinearities when heating rate is calculated from the 'calibration method'. A comparison is made between nuclear heating rates determined from 'calibration' and 'zero methods'. In addition, an evaluation of the global uncertainty associated to the measurements is detailed. Finally, a comparison is made with available measurements obtained from previous calorimeters. (authors)

  5. First In-Core Measurement Results Obtained with the Innovative Mobile Calorimeter CALMOS inside the OSIRIS Material Testing Reactor

    International Nuclear Information System (INIS)

    Carcreff, Hubert; Salmon, Laurent; Courtaux, Cedric

    2013-06-01

    Nuclear heating rate inside an MTR has to be known in order to design and to run irradiation experiments which have to fulfill target temperature constraints. This measurement is usually carried out by calorimetry [1, 2]. An innovative calorimetric system, CALMOS, has been studied and built in 2011 for the 70 MWth OSIRIS reactor operated by CEA. Thanks to a new calorimetric probe, associated to a specific displacement system, it provides measurements along the fissile height and above the core. The development of the calorimetric probe required the manufacturing and the irradiation of mock-ups in the ex-core area, where nuclear heating rate does not exceed 2 W.g -1 . The calorimeter working mode, the different measurement procedures allowed with such a new probe and main modeling and experimental results have been already presented [3, 4]. In this paper, we present the first results obtained during several measurement campaigns carried out in 2012 and 2013 inside the OSIRIS core with the final device. For the first time, this new experimental measurement system was operated in nominal in-core thermo hydraulic conditions with nominal neutron and gamma fluxes (up to 6 W.g -1 ) in several experimental locations. After a brief presentation of the displacement system specificities, first nuclear heating distributions are presented and discussed. Experimental data were also used to upgrade the Finite Element model of the calorimeter in order to match measured temperatures with calculated ones. This model allowed to estimate a Kc correction factor which takes into account small nonlinearities when the heating rate is deduced from the calibration method. A comparison is made between nuclear heating rates determined from the probe calibration and from the zero method. In addition, an evaluation of the global uncertainty associated to the measurements is detailed. Finally, a global comparison is made with available measurements obtained from previous calorimeters. (authors)

  6. Preliminary observations and results obtained with the ultraviolet spectrometer and polarimeter. [for Solar Maximum Mission

    Science.gov (United States)

    Tandberg-Hassen, E.; Cheng, C. C.; Athay, R. G.; Beckers, J. M.; Brandt, J. C.; Chapman, R. D.; Bruner, E. C.; Henze, W.; Hyder, C. L.; Gurman, J. B.

    1981-01-01

    New observation with the Ultraviolet Spectrometer and Polarimeter (UVSP) of a number of manifestations of solar activity obtained during the first three months of Solar Maximum Mission operations are presented. Attention is given to polarimetry in sunspots, oscillations above sunspots, density diagnostics of transition-zone plasmas in active regions, and the eruptive prominence - coronal transient link.

  7. Matching the results of a theoretical model with failure rates obtained from a population of non-nuclear pressure vessels

    International Nuclear Information System (INIS)

    Harrop, L.P.

    1982-02-01

    Failure rates for non-nuclear pressure vessel populations are often regarded as showing a decrease with time. Empirical evidence can be cited which supports this view. On the other hand theoretical predictions of PWR type reactor pressure vessel failure rates have shown an increasing failure rate with time. It is shown that these two situations are not necessarily incompatible. If adjustments are made to the input data of the theoretical model to treat a non-nuclear pressure vessel population, the model can produce a failure rate which decreases with time. These adjustments are explained and the results obtained are shown. (author)

  8. Comparison between two sampling methods by results obtained using petrographic techniques, specially developed for minerals of the Itataia uranium phosphate deposit, Ceara, Brazil

    International Nuclear Information System (INIS)

    Salas, H.T.; Murta, R.L.L.

    1985-01-01

    The results of comparison of two sampling methods applied to a gallery of the uranium-phosphate ore body of Itataia-Ceara State, Brazil, along 235 metres of mineralized zone, are presented. The results were obtained through petrographic techniques especially developed and applied to both samplings. In the first one it was studied hand samples from a systematically sampling made at intervals of 2 metres. After that, the estimated mineralogical composition studies were carried out. Some petrogenetic observations were for the first time verified. The second sampling was made at intervals of 20 metres and 570 tons of ore extracted and distributed in sections and a sample representing each section was studied after crushing at -65. Their mineralogy were quantified and the degree of liberation of apatite calculated. Based on the mineralogical data obtained it was possible to represent both samplings and to make the comparison of the main mineralogical groups (phosphates, carbonates and silicates). In spite of utilizing different methods and methodology and the kind of mineralization, stockwork, being quite irregular, the results were satisfactory. (Author) [pt

  9. LEP and results obtained by DELPHI after four years of operation; LEP i wyniki uzyskane przez DELPHI po czterech latach dzialania

    Energy Technology Data Exchange (ETDEWEB)

    Blocki, J. [Warsaw Univ. (Poland). Inst. Fizyki Doswiadczalnej; Brueckman de Renstrom, P.; Budziak, A. [Institute of Nuclear Physics, Cracow (Poland)] [and others

    1993-10-01

    We characterize the most important problems of modern elementary particles physics, for the solution of which the LEP (Large Electron Positron) accelerator was built. We present the characteristics of this accelerator. The structure and properties of the DELPHI detector are described with special emphasis on the contribution of Polish groups. The most important results obtained so far in the LEP accelerator are discussed. (author). 12 refs, 17 figs, 1 tab.

  10. Comparison of visual field test results obtained through Humphrey matrix frequency doubling technology perimetry versus standard automated perimetry in healthy children

    Directory of Open Access Journals (Sweden)

    Sibel Kocabeyoglu

    2013-01-01

    Full Text Available Aims : The aim of this study was to compare the visual field test results in healthy children obtained via the Humphrey matrix 24-2 threshold program and standard automated perimetry (SAP using the Swedish interactive threshold algorithm (SITA-Standard 24-2 test. Materials and Methods: This prospective study included 55 healthy children without ocular or systemic disorders who underwent both SAP and frequency doubling technology (FDT perimetry visual field testing. Visual field test reliability indices, test duration, global indices (mean deviation [MD], and pattern standard deviation [PSD] were compared between the 2 tests using the Wilcoxon signed-rank test and paired t-test. The performance of the Humphrey field analyzer (HFA 24-2 SITA-standard and frequency-doubling technology Matrix 24-2 tests between genders were compared with Mann-Whitney U-test. Results: Fifty-five healthy children with a mean age of 12.2 ± 1.9 years (range from 8 years to 16 years were included in this prospective study. The test durations of SAP and FDT were similar (5.2 ± 0.5 and 5.1 ± 0.2 min, respectively, P = 0.651. MD and the PSD values obtained via FDT Matrix were significantly higher than those obtained via SAP (P < 0.001, and fixation losses and false negative errors were significantly less with SAP (P < 0.05. A weak positive correlation between the two tests in terms of MD (r = 0.352, P = 0.008 and PSD (r = 0.329, P = 0.014 was observed. Conclusion: Children were able to complete both the visual test algorithms successfully within 6 min. However, SAP testing appears to be associated with less depression of the visual field indices of healthy children. FDT Matrix and SAP should not be used interchangeably in the follow-up of children.

  11. The similia principle: results obtained in a cellular model system.

    Science.gov (United States)

    Wiegant, Fred; Van Wijk, Roeland

    2010-01-01

    This paper describes the results of a research program focused on the beneficial effect of low dose stress conditions that were applied according to the similia principle to cells previously disturbed by more severe stress conditions. In first instance, we discuss criteria for research on the similia principle at the cellular level. Then, the homologous ('isopathic') approach is reviewed, in which the initial (high dose) stress used to disturb cellular physiology and the subsequent (low dose) stress are identical. Beneficial effects of low dose stress are described in terms of increased cellular survival capacity and at the molecular level as an increase in the synthesis of heat shock proteins (hsps). Both phenomena reflect a stimulation of the endogenous cellular self-recovery capacity. Low dose stress conditions applied in a homologous approach stimulate the synthesis of hsps and enhance survival in comparison with stressed cells that were incubated in the absence of low dose stress conditions. Thirdly, the specificity of the low dose stress condition is described where the initial (high dose) stress is different in nature from the subsequently applied (low dose) stress; the heterologous or 'heteropathic' approach. The results support the similia principle at the cellular level and add to understanding of how low dose stress conditions influence the regulatory processes underlying self-recovery. In addition, the phenomenon of 'symptom aggravation' which is also observed at the cellular level, is discussed in the context of self-recovery. Finally, the difference in efficiency between the homologous and the heterologous approach is discussed; a perspective is indicated for further research; and the relationship between studies on the similia principle and the recently introduced concept of 'postconditioning hormesis' is emphasized. Copyright 2009 The Faculty of Homeopathy. Published by Elsevier Ltd. All rights reserved.

  12. Experiments for obtaining field influence mass particles.

    CERN Document Server

    Yahalomi, E

    2010-01-01

    Analyzing time dilation experiments the existence of a universal field interacting with moving mass particles is obtained. It is found that mass particle changes its properties depend on its velocity relative to this universal scalar field and not on its velocity relative to the laboratory. High energy proton momentum, energy and mass were calculated obtaining new results. Experiments in high energy accelerators are suggested as additional proofs for the existence of this universal field. This universal field may explain some results of other high energy experiments.

  13. Analysis of results obtained with different cutting techniques and associated filtration systems for the dismantling of radioactive metallic components

    International Nuclear Information System (INIS)

    Bach, F.W.; Steiner, H.; Schreck, G.

    1993-01-01

    The present joint study performed by the Commissariat a l'energie atomique and the Universitaet Hannover and coordinated by the Commission of the European Communities was intended to analyse the results generated in a number of research contracts concerned with cutting tests in air and underwater, with consideration of the prevailing working conditions. The analysis has led to a large database, giving broadly-assessed information for the dismantling of radioactive components. The range of study was enlarged, where possible, to include recently obtained results outside the present research programme, consideration also being given to supplementary cutting tools and filtration systems not covered by the present programme. Data was concentrated in structured information packages on practical experience available for a series of cutting tools and filters. These were introduced into a computerized user-friendly databank, to be considered as a first-stage development, which should be continuously updated and possibly oriented in the future to an expert system

  14. Review of the scientific results obtained at the research reactor-booster IBR-30 and the Program of investigations at the neutron source IREN

    CERN Document Server

    Furman, W

    2002-01-01

    Brief review of the main scientific results obtained at research reactor booster IBR-30 and its predecessor IBR and IBR-1 for the period 1960 - 2001 is presented. The thesis of the scientific program for the upgrade of IBR-30 resonance neutron source IREN are adduced

  15. Determination of residual stresses in steel 20 comparison of the results obtained by the Barkhausen noise and X-ray diffraction

    International Nuclear Information System (INIS)

    Fernandez, L. M.; Herrera, V.; Suarez, J.C.; Merino, F.J.

    1997-01-01

    During a heat treatment (quenching, surface hardening, Thermochemical treatment) the metallic alloys undergo temperature variations and phase transformation. The resulting changes give rise to internal stresses in the piece. Phase transformation modifies the thermomechanical behavior of the material through the change of mechanical properties ( hardness, fatigue-behaviour, corrosion resistance, electric resistivity, etc.) The aim of this paper is residual stress measurements in specimens of steel-20 submitted to different heat treatment, by two non destructive methods: Barkhausen and X-ray diffraction. Brakhausen Effects utilizes the magnetic properties of ferromagnetic materials such as ferritic and perlitic steels and provides a practical tool for surface streets evaluation. X-ray streets analysis is based on the measurement of lattice strains in different directions of specimen The results obtained by two techniques are compared, avowing a good agreement

  16. Process for obtaining cobalt and lanthanum nickelate

    International Nuclear Information System (INIS)

    Tapcov, V.; Samusi, N.; Gulea, A.; Horosun, I.; Stasiuc, V.; Petrenco, P.

    1999-01-01

    The invention relates to the process for obtaining polycrystalline ceramics of cobalt and lanthanum nickelate with the perovskite structure from coordinative hetero metallic compounds. The obtained products can be utilized in the industry in the capacity of catalysts. Summary of the invention consists in obtaining polycrystalline ceramics LaCoO 3 and LaNiO 3 with the perovskite structure by pyrolysis of the parent compounds, namely, the coordinative hetero metallic compounds of the lanthanum cobalt or lanthanum nickel. The pyrolysis of the parent compound runs during one hour at 800 C. The technical result of the invention consists in lowering the temperature of the parent compound pyrolysis containing the precise ratio of metals necessary for ceramics obtaining

  17. Comparative analysis of the results obtained by computer code ASTEC V2 and RELAP 5.3.2 for small leak ID 80 for VVER 1000

    International Nuclear Information System (INIS)

    Atanasova, B.; Grudev, P.

    2011-01-01

    The purpose of this report is to present the results obtained by simulation and subsequent analysis of emergency mode for small leak with ID 80 for WWER 1000/B320 - Kozloduy NPP Units 5 and 6. Calculations were performed with the ASTEC v2 computer code used for calculation of severe accident, which was designed by French and German groups - IRSN and GRS. Integral RELAP5 computer code is used as a reference for comparison of results. The analyzes are focused on the processes occurring in reactor internals phase of emergency mode with significant core damage. The main thermohydraulic parameters, start of reactor core degradation and subsequent fuel relocalization till reactor vessel failure are evaluated in the analysis. RELAP5 computer code is used as a reference code to compare the results obtained till early core degradation that occurs after core stripping and excising of fuel temperature above 1200 0 C

  18. Obtaining of ceramics biphasic dense and porous

    International Nuclear Information System (INIS)

    Pallone, E.M.J.A.; Rigo, E.C.S.; Fraga, A.F.

    2010-01-01

    Among the bioceramic hydroxyapatite (HAP) and beta-tricalcium phosphate (beta-TCP) are materials commonly used in biomedical field. Their combined properties result in a material with absorbable and at the same time with bioactive surface. Called biphasic ceramics such materials respond more quickly when exposed to physiological environment. In this work, powders of HAP/beta-TCP were obtained by chemical precipitation. After obtaining the post-phase was added at a ratio of 0, 15% and 30w% aqueous solutions of corn starch in order to obtain porous bodies. After mixing the resulting solutions were dried, resigned in tablet form and sintered at 1300 deg C. The initial powder was characterized by X-ray diffraction with Rietveld refinement to quantify the phases present. Bodies-of-evidence has been characterized by calculating the bulk density, X-ray diffraction (XRD), scanning electron microscopy and diametral compression. (author)

  19. Preliminary Results from Duplex Procedure for Obtain of Fe Based Materials for Automotive Applications

    Science.gov (United States)

    Crăciun, R. C.; Stanciu, S.; Geantă, V.; Voiculescu, I.; Manole, V.; Gârneţ, I. A.; Alexandru, A.; Cimpoesu, N.; Săndulache, F.

    2017-06-01

    Abstract Iron based materials still represent a high percentage from metallic materials used in industry, in general, and in automotive industry, in particular. In this case we used a duplex process in order to obtain the FeMnSiAl experimental alloy for a more efficient use of various units. In the first stage iron, manganese, silicon and aluminum were melted and mixed together using arc melting technology and for the second stage the alloy was re-melt for homogeneity in an induction furnace. Chemical composition, after each melting step, was analyzed using EDS Bruker detector for various areas and microstructural characterization using SEM, VegaTescan LMH II with SE detector, equipment. This alloy is proposed as a metallic approach of mechanical dumpers used in automotive industry for low and medium impact contacts.

  20. Most recent developments in combined radium and high voltage therapy of uterine tumours as shown by the results obtained at the municipal hospital Passau

    International Nuclear Information System (INIS)

    Moos, G.

    1987-01-01

    It was the aim of the study described here to review data on healing successes achieved in malignant changes of the uterus. The results obtained were analysed on the bais of tumour stage and, in particular, the radiation dose actually administered. It could be shown that the treatment results currently achieved at this clinic are in keeping with relevant patient data collected previously or by other centres. (orig./MG) [de

  1. Fermentation Results and Chemical Composition of Agricultural Distillates Obtained from Rye and Barley Grains and the Corresponding Malts as a Source of Amylolytic Enzymes and Starch.

    Science.gov (United States)

    Balcerek, Maria; Pielech-Przybylska, Katarzyna; Dziekońska-Kubczak, Urszula; Patelski, Piotr; Strąk, Ewelina

    2016-10-01

    The objective of this study was to determine the efficiency of rye and barley starch hydrolysis in mashing processes using cereal malts as a source of amylolytic enzymes and starch, and to establish the volatile profile of the obtained agricultural distillates. In addition, the effects of the pretreatment method of unmalted cereal grains on the physicochemical composition of the prepared mashes, fermentation results, and the composition of the obtained distillates were investigated. The raw materials used were unmalted rye and barley grains, as well as the corresponding malts. All experiments were first performed on a semi-technical scale, and then verified under industrial conditions in a Polish distillery. The fermentable sugars present in sweet mashes mostly consisted of maltose, followed by glucose and maltotriose. Pressure-thermal treatment of unmalted cereals, and especially rye grains, resulted in higher ethanol content in mashes in comparison with samples subjected to pressureless liberation of starch. All agricultural distillates originating from mashes containing rye and barley grains and the corresponding malts were characterized by low concentrations of undesirable compounds, such as acetaldehyde and methanol. The distillates obtained under industrial conditions contained lower concentrations of higher alcohols (apart from 1-propanol) than those obtained on a semi-technical scale.

  2. Fermentation Results and Chemical Composition of Agricultural Distillates Obtained from Rye and Barley Grains and the Corresponding Malts as a Source of Amylolytic Enzymes and Starch

    Directory of Open Access Journals (Sweden)

    Maria Balcerek

    2016-10-01

    Full Text Available The objective of this study was to determine the efficiency of rye and barley starch hydrolysis in mashing processes using cereal malts as a source of amylolytic enzymes and starch, and to establish the volatile profile of the obtained agricultural distillates. In addition, the effects of the pretreatment method of unmalted cereal grains on the physicochemical composition of the prepared mashes, fermentation results, and the composition of the obtained distillates were investigated. The raw materials used were unmalted rye and barley grains, as well as the corresponding malts. All experiments were first performed on a semi-technical scale, and then verified under industrial conditions in a Polish distillery. The fermentable sugars present in sweet mashes mostly consisted of maltose, followed by glucose and maltotriose. Pressure-thermal treatment of unmalted cereals, and especially rye grains, resulted in higher ethanol content in mashes in comparison with samples subjected to pressureless liberation of starch. All agricultural distillates originating from mashes containing rye and barley grains and the corresponding malts were characterized by low concentrations of undesirable compounds, such as acetaldehyde and methanol. The distillates obtained under industrial conditions contained lower concentrations of higher alcohols (apart from 1-propanol than those obtained on a semi-technical scale.

  3. Design, operational experiences and beam results obtained with the SNS H- ion source and LEBT at Berkeley Lab

    International Nuclear Information System (INIS)

    Keller, R.; Thomae, R.; Stockli, M.; Welton, R.

    2002-01-01

    The ion source and Low-Energy Transport (LEBT) system that will provide H - ion beams to the Spallation Neutron Source (SNS)** Front End and the accelerator chain have been developed into a mature unit that fully satisfies the operational requirements through the commissioning and early operating phases of SNS. Compared to the early R and D version, many features of the ion source have been improved, and reliable operation at 6% duty factor has been achieved producing beam currents in the 35-mA range and above. LEBT operation proved that the purely electrostatic focusing principle is well suited to inject the ion beam into the RFQ accelerator, including the steering and pre-chopping functions. This paper will discuss the latest design features of the ion source and LEBT, give performance data for the integrated system, and report on commissioning results obtained with the SNS RFQ and Medium-Energy Beam Transport (MEBT) system. Prospects for further improvements will be outlined in concluding remarks

  4. Results obtained using the pellet charge exchange diagnostic on TFTR

    International Nuclear Information System (INIS)

    McChesney, J.M.; Fisher, R.K.; Parks, P.B.; Duong, H.H.; Mansfield, D.K.; Medley, S.S.; Roquemore, A.L.; Petrov, M.P.

    1994-05-01

    Experiments are underway on TFTR to measure the confined alpha particle distribution functions using small low-Z pellets injected into the plasma. Upon entering the plasma, the pellet ablates, forming a plasma ablation cloud, elongated in the magnetic field direction, that travels alongside the pellet. A small fraction of the fusion produced 3.5 MeV alpha particles incident on the cloud are converted to helium neutrals. By measuring the resultant helium neutrals escaping from the plasma by means of a mass and energy resolving charge exchange analyzer, the energy distribution of the alpha particles incident on the cloud can be inferred. Preliminary experiments to observe neutrals from the 100-1000 keV He tail produced during ICRF minority heating experiments were successful. However, no significant alpha particle signals have been observed during D-T operation on TFTR. The authors attribute this lack of signal to stochastic toroidal field ripple loss in the outer regions of the plasma. They are studying ways to improve the pellet penetration so that the pellet penetrates into the central regions of the plasma where ripple induced losses are small and the alpha population is high

  5. Purification of alcohol obtained from molasses

    Energy Technology Data Exchange (ETDEWEB)

    Visnevskaya, G L; Egorov, A S; Sokol' skaya, E V

    1960-01-01

    A study of the composition of alcohol liquids on different plates of a fractionation column of indirect action during purification of alcohol obtained from normal and defective molasses, and from starch raw material, showed that there were two local strength minima in the lower part of the column and on the plates (adjacent and feed). Aldehydes behaved as a typical head impurity; a noticeable increase in their concentration occurred only on the highest plates in the fractionation column. In the zone of the column containing liquids of a strength of 86 to 94% alcohol by weight a sharply pronounced local maximum of ester accumulation were observed, provisionally designated as intermediate, whose presence is apparently one of the causes of the specific sharp taste of alcohol obtained from molasses. These esters hinder the obtaining of high-grade alcohols which are standard in respect to ester content and oxidizability test. Reduction with 0.05N KMnO/sub 4/ occurs most rapidly with alcohol liquids in the zone of ester accumulation; purification of alcohols obtained from grain and potato raw material resulted in no zones of ester accumulation in the column.

  6. Biomonitoring of heavy metal deposition in the south Ural region: some preliminary results obtained by nuclear and related techniques

    International Nuclear Information System (INIS)

    Frontas'eva, M.V.; Steinnes, E.; Lyapunov, S.M.; Cherchintsev, V.D.; Smirnov, L.I.

    1999-01-01

    The first results are reported from the analysis of feather mosses used to study heavy metal atmospheric deposition in the vicinity of Magnitogorsk, the center of the steel industry in Russia. Moss samples collected at sites 30 km to the north-west of the industry were analyzed by instrumental neutron activation analysis using epithermal neutrons (ENAA), Results for a total of 38 elements are reported, including Pb, Cd, and Cu determined by atomic absorption spectroscopy (AAS). The element concentrations in moss samples from this work are compared with relevant literature data for strongly polluted areas in Central and Northern Europe and background values from Norway obtained by the same biomonitoring technique. The concentrations of Sb in the examined area are the highest ever reported for mosses, and also levels of Fe, Cr, and V are found to be particularly high. A scanning electron microscope connected to an XRF analyzer (SEM-XRF) was used to examine the surface of the moss samples. Photographs of identified iron spherules along with other aerosol particles made at magnification of 3500 to 5000 times and corresponding XRF analyses verifying the nature of typical particles are presented

  7. Obtaining zircaloy powder through hydriding

    International Nuclear Information System (INIS)

    Dupim, Ivaldete da Silva; Moreira, Joao M.L.

    2009-01-01

    Zirconium alloys are good options for the metal matrix in dispersion fuels for power reactors due to their low thermal neutron absorption cross-section, good corrosion resistance, good mechanical strength and high thermal conductivity. A necessary step for obtaining such fuels is producing Zr alloy powder for the metal matrix composite material. This article presents results from the Zircaloy-4 hydrogenation tests with the purpose to embrittle the alloy as a first step for comminuting. Several hydrogenation tests were performed and studied through thermogravimetric analysis. They included H 2 pressures of 25 and 50 kPa and temperatures ranging between from 20 to 670 deg C. X-ray diffraction analysis showed in the hydrogenated samples the predominant presence of ZrH 2 and some ZrO 2 . Some kinetics parameters for the Zircaloy-4 hydrogenation reaction were obtained: the time required to reach the equilibrium state at the dwell temperature was about 100 minutes; the hydrogenation rate during the heating process from 20 to 670 deg C was about 21 mg/h, and at constant temperature of 670 deg C, the hydride rate was about 1.15 mg/h. The hydrogenation rate is largest during the heating process and most of it occurs during this period. After hydrogenated, the samples could easily be comminuted indicating that this is a possible technology to obtain Zircaloy powder. The results show that only few minutes of hydrogenation are necessary to reach the hydride levels required for comminuting the Zircaloy. The final hydride stoichiometry was between 2.7 and 2.8 H for each Zr atom in the sample (author)

  8. Organoclays obtaining starting up of clays sodium

    International Nuclear Information System (INIS)

    Silva, M.M. da; Mota, M.F.; Oliveira, G.C. de; Rodrigues, M.G.F.

    2012-01-01

    Clays have several applications in many areas of fields of technology, however, modification of these materials using organic compounds can be performed to obtain further hydrophobic materials, for applications in the adsorption of organic pollutants. This study aimed to analyze the effects of modifying two clays using sodium quaternary ammonium surfactants through ion exchange reaction process, in obtaining organoclays. The samples with sodium and organoclays were characterized by the techniques of X-ray diffraction (XRD), Infrared Spectroscopy in the region (IV), Gravimetric and Differential Thermal Analysis (DTA / TG) and organic adsorption tests. The results show that the process of obtaining organoclay is efficient, and materials have the potential for future applications in removing organic contaminants. (author)

  9. Geopolymer obtained from coal ash

    International Nuclear Information System (INIS)

    Conte, V.; Bissari, E.S.; Uggioni, E.; Bernardin, A.M.

    2011-01-01

    Geopolymers are three-dimensional alumino silicates that can be rapidly formed at low temperature from naturally occurring aluminosilicates with a structure similar to zeolites. In this work coal ash (Tractebel Energy) was used as source of aluminosilicate according a full factorial design in eight formulations with three factors (hydroxide type and concentration and temperature) and two-levels. The ash was dried and hydroxide was added according type and concentration. The geopolymer was poured into cylindrical molds, cured (14 days) and subjected to compression test. The coal ash from power plants belongs to the Si-Al system and thus can easily form geopolymers. The compression tests showed that it is possible to obtain samples with strength comparable to conventional Portland cement. As a result, temperature and molarity are the main factors affecting the compressive strength of the obtained geopolymer. (author)

  10. Radon in Estonian buildings. Establishment of a measurement system and obtained results

    International Nuclear Information System (INIS)

    Pahapill, L.; Rulkov, A.; Swedjemark, G.A.

    1996-12-01

    One purpose of this project was the establishment of a radon monitoring programme inside the state environmental monitoring programme. Another purpose was to investigate regions, expected to have high radon levels indoors. A new method for the long-term measurement of indoor radon was established and the staff for these measurements was trained. The results of the measurement can be used by Estonian decision-makers to work out rules and standards. There is no legislative act in the field of radiation in Estonian at this time. To summarize the results of the measurements we can say that indoor radon concentrations vary by region. The radon investigations must be continued to identify the risk areas and types of housing construction. The results of the state radon monitoring are provided to the municipalities, who advice the owners of planned new houses to select the right construction for the house. A new project will follow with an investigation of radon in randomly selected dwellings, training and equipment for radon measurement in soil, and general advice with regard to radon, as well as assistance in preparing information about radon. 7 refs, 5 figs

  11. Comparison of visual field test results obtained through Humphrey matrix frequency doubling technology perimetry versus standard automated perimetry in healthy children.

    Science.gov (United States)

    Kocabeyoglu, Sibel; Uzun, Salih; Mocan, Mehmet Cem; Bozkurt, Banu; Irkec, Murat; Orhan, Mehmet

    2013-10-01

    The aim of this study was to compare the visual field test results in healthy children obtained via the Humphrey matrix 24-2 threshold program and standard automated perimetry (SAP) using the Swedish interactive threshold algorithm (SITA)-Standard 24-2 test. This prospective study included 55 healthy children without ocular or systemic disorders who underwent both SAP and frequency doubling technology (FDT) perimetry visual field testing. Visual field test reliability indices, test duration, global indices (mean deviation [MD], and pattern standard deviation [PSD]) were compared between the 2 tests using the Wilcoxon signed-rank test and paired t-test. The performance of the Humphrey field analyzer (HFA) 24-2 SITA-standard and frequency-doubling technology Matrix 24-2 tests between genders were compared with Mann-Whitney U-test. Fifty-five healthy children with a mean age of 12.2 ± 1.9 years (range from 8 years to 16 years) were included in this prospective study. The test durations of SAP and FDT were similar (5.2 ± 0.5 and 5.1 ± 0.2 min, respectively, P = 0.651). MD and the PSD values obtained via FDT Matrix were significantly higher than those obtained via SAP (P tests in terms of MD (r = 0.352, P = 0.008) and PSD (r = 0.329, P = 0.014) was observed. Children were able to complete both the visual test algorithms successfully within 6 min. However, SAP testing appears to be associated with less depression of the visual field indices of healthy children. FDT Matrix and SAP should not be used interchangeably in the follow-up of children.

  12. The ion-exchange obtaining of high purity samarium oxide

    International Nuclear Information System (INIS)

    Brzyska, W.; Soltysiak, I.; Cygan, J.

    1987-01-01

    The use of lactic acid - EDTA mixture as an eluent for the obtaining of high purity samarium oxide was studied. The studies were carried out at room temperature on cation exchange resin Wofatit KPS X 8. The best results were obtained for lactic acid (0,26 mol/dm 3 ) - EDTA (0,013 mol/dm 3 ) mixture at pH 3,3. As the result of 57% samarium concentrate elution with column load 1:3 and flow rate 0,4 cm/min, over 99% pure samarium oxide with 73% yield has been obtained. The yield of spectrally pure Sm 2 O 3 exceeded 45%. (author)

  13. Obtaining of polycrystalline silicon for semiconductor industry

    International Nuclear Information System (INIS)

    Mukashev, F.; Nauryzbaev, M.; Kolesnikov, B.; Ivanov, Y.

    1996-01-01

    The purpose of the project is to create pilot equipment and optimize the process of obtaining polycrystalline silicon on semi-industrial level. In the past several decades, the historical experience in the developing countries has shown that one of the most promising ways to improve the economy,of a country is to establish semiconductor industry. First of all, the results can help increase defense, national security and create industrial production. The silane method, which has been traditionally' used for obtaining technical and polycrystalline silicon, is to obtain and then to pyrolyzed mono-and poly silanes. Although the traditional methods of obtaining silicon hydrides have specific advantages, such as utilizing by-products, they also have clear shortcomings, i.e. either low output of the ultimate product ( through hydrolysis of Mg 2 Si) or high contents of by-products in it or high contents of dissolving vapors (through decomposing Mg 2 Si in non-water solutions)

  14. Transvenous versus open chest lead placement for resynchronization therapy in patients with heart failure: comparison of ventricular electromechanical synchronicity.

    Science.gov (United States)

    Zhang, Hai-Bo; Meng, Xu; Han, Jie; Li, Yan; Zhang, Ye; Jiang, Teng-Yong; Zhao, Ying-Xin; Zhou, Yu-Jie

    2017-04-01

    Transvenous lead placement is the standard approach for left ventricular (LV) pacing in cardiac resynchronization therapy (CRT), while the open chest access epicardial lead placement is currently the most frequently used second choice. Our study aimed to compare the ventricular electromechanical synchronicity in patients with heart failure after CRT with these two different LV pacing techniques. We enrolled 33 consecutive patients with refractory heart failure secondly to dilated cardiomyopathy who were eligible for CRT in this study. Nineteen patients received transvenous (TV group) while 14 received open chest (OP group) LV lead pacing. Intra- and inter-ventricular electromechanical synchronicity was assessed by tissue Doppler imaging (TDI) before and one year after CRT procedure. Before CRT procedure, the mean QRS-duration, maximum time difference to systolic peak velocity among 12 left ventricle segments (LV Ts-12), standard deviation of time difference to systolic peak velocity of 12 left ventricle segments (LV Ts-SD), and inter-ventricular mechanical delay (IVMD) in OP and TV group were 166 ± 17 ms and 170 ± 21 ms, 391 ± 42 ms and 397 ± 36 ms, 144 ± 30 ms and 148 ± 22 ms, 58 ± 25 ms and 60 ± 36 ms, respectively (all P > 0.05). At one year after the CRT, the mean QRS-duration, LV Ts-12, LV Ts-SD, and IVMD in TV and OP group were 128 ± 14 ms and 141 ± 22 ms ( P = 0.031), 136 ± 37 ms and 294 ± 119 ms ( P = 0.023), 50 ± 22 ms and 96 ± 34 ms ( P = 0.015), 27 ± 11 ms and 27 ± 26 ms ( P = 0.86), respectively. The LV lead implantation procedure time was 53.4 ± 16.3 min for OP group and 136 ± 35.1 min for TV group ( P = 0.016). The mean LV pacing threshold increased significantly from 1.7 ± 0.6 V/0.5 ms to 2.3 ± 1.6 V/0.5 ms ( P open chest access of LV pacing for CRT leads to better improvement of the intraventricular synchronization.

  15. Obtaining a citric tristeza virus p65 protein antibody and preliminary results of p65 in vivo expression

    Directory of Open Access Journals (Sweden)

    Yanneth Torres

    2003-07-01

    Full Text Available The citric tristeza virus (CTV belongs to the Closteroviridae family which indudes the only vegetal viruses possessing genes homologous to HSP70 thermal cellular shock proteins in their genome. Such is the case of the gene encoding for the CTV p65 protein which presents high homology with the HSP70 protein family. It has been shown recently that HSP70h viral proteins (such as CTV p65 are involved both in viral assembly, as a microtubule binding protein, and in cell-cell movement. Since CTV is the most deleterious citrus pathogen, understanding this protein's role in the pathogenesis process is important. Rabbits were immunised with four synthetic peptides (corresponding to CTV p65 thermal shock protein's carboxyl-terminal region to obtain polyclonal antibodies. All the peptides used were immunogenic, even though two of them showed greater response. Whilst none of the antibodies obtained reacted to non-infected plant extract, the p65 proteins was detected in extracts taken from citric plants infected with CTV Based on the antibody's reaction to two Colombian isolates having different serological characteristics, the p65 antibody's immunological behaviour appeared to be independent of the symptomatic severity of the CTV isolates. It was shown that the ORF encoded for the HSP70 homologue in CTV was expressed in vivo, even though the p65 antibody was only detected in concentrated protein extracts taken from infected plants, supporting reports from other studies that the concentration of this protein in plants infected with CTV is low. This is the first time that a polyclonal CTV antibody has been obtained in Colombia against p65 (a protein intervening in viral assembly and movement. Adapting a technique for obtaining p65 antibodies by using synthetic peptides as immunogens could be useful in the future for detecting or diagnosing p65 proteins present in different Colombian CTV isolates, especially in developing studies contributing towards greater

  16. Do the results of respirable dust samples obtained from direct-on-filter X-ray diffraction, direct-on-filter infrared and indirect infrared (KBr pellet) methods correlate?

    CSIR Research Space (South Africa)

    Pretorius, C

    2010-11-01

    Full Text Available The objective of this study was to determine whether a correlation exists between the quartz results obtained from direct-on-filter X-ray Diffraction analysis, direct-on-filter Fourier-Transform Infrared analysis and indirect analysis (Potassium...

  17. Obtaining of inulin acetate

    OpenAIRE

    Khusenov, Arslonnazar; Rakhmanberdiev, Gappar; Rakhimov, Dilshod; Khalikov, Muzaffar

    2014-01-01

    In the article first obtained inulin ester inulin acetate, by etherification of inulin with acetic anhydride has been exposed. Obtained product has been studied using elementary analysis and IR spectroscopy.

  18. Carbon and nitrogen determination in Zr by photon or proton activation analysis. Comparison between the results obtained by this method and other analytical techniques

    International Nuclear Information System (INIS)

    Petit, J.; Gosset, J.; Engelmann, C.

    1977-01-01

    Carbon and nitrogen are determined by the following nuclear reactions: 12 C(γ,n) 11 C and 14 N(p,α) 11 C. The performances of the method and the main interferences are considered. The process developed for the separation of carbon-11 from zirconium is described and its efficiency evaluated. The results obtained are compared with those given by different laboratories using various analytical techniques [fr

  19. First results obtained by the Cluster STAFF experiment

    Czech Academy of Sciences Publication Activity Database

    Cornilleau-Wehrlin, N.; Chanteur, G.; Perraut, S.; Rezeau, L.; Robert, P.; Roux, A.; Villedary de, C.; Canu, P.; Maksimovic, M.; Conchy de, Y.; Hubert, D.; Lacombe, C.; Lefeuvre, F.; Parrot, M.; Pincon, J. L.; Decrau, P. M. E.; Harvey, C. C.; Louarn, Ph.; Santolík, Ondřej; Alleyne, H. St. C.; Roth, M.; Chust, T.; Contel Le, O.

    2003-01-01

    Roč. 21, - (2003), s. 437-456 ISSN 0992-7689 R&D Projects: GA ČR GA202/03/0832; GA MŠk ME 650 Institutional research plan: CEZ:AV0Z3042911 Keywords : magnetospheric physics * space plasma physics Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 1.031, year: 2003

  20. Calibration results obtained with Liulin-4 type dosimeters

    Czech Academy of Sciences Publication Activity Database

    Dacheva, T.; Tomova, B.; Matviichuka, Y.; Dimitrova, P.; Lemaireb, J.; Gregoirec, G.; Cyamukunguc, M.; Schmitzc, H.; Fujitakad, K.; Uchihorid, Y.; Kitamurad, H.; Reitze, G.; Beaujeanf, R.; Petrovg, V.; Shurshakovg, V.; Benghing, V.; Spurný, František

    2002-01-01

    Roč. 30, č. 4 (2002), s. 917-925 ISSN 0273-1177 Institutional research plan: CEZ:AV0Z1048901 Keywords : CERN high-energy reference field * detector * dosimeter Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 0.448, year: 2002

  1. Occupational radioprotection program at Nuclear Engineering Institute -IEN: results obtained in 1991

    International Nuclear Information System (INIS)

    Fajardo, P.W.; Pastura, V.F.S.; Soares, M.L.; LeRoy, C.L.; Teixeira, M.V.; Santos, I.H.T.; Pujol Filho, S.V.

    1992-01-01

    The results of occupational radioprotection program at Nuclear Engineering Institute-IEN- in 1991 are presented. The personnel monitoring, the routine monitoring of limited areas, the operational monitoring during the operation and the cyclotron CV-28 maintenance, the radioisotope processing and Argonauta Reactor operation, the control of radioprotection equipment and the control of radiation sources are included. (C.G.C.)

  2. A review of experimental results obtained in Au-Au collisions at the RHIC-BNL energies using BRAHMS experimental set-up

    International Nuclear Information System (INIS)

    Jipa, Alexandru

    2003-01-01

    Ultrarelativistic heavy ion collisions are useful tools to investigate highly excited dense nuclear matter. At sufficiently high temperature, nuclear matter is expected to undergo a phase transition to quark-gluon plasma. Therefore, new experiments have been proposed to investigate the behaviour of the highly excited dense nuclear matter. One of the experiments performed at the Relativistic Heavy Ion Collider from Brookhaven National Laboratory is the BRAHMS Experiment. In the three running years many experimental data have been obtained. These data permitted to establish significant experimental results on charged pion, charged kaon, proton and antiproton production in Au-Au collisions at 130 A GeV and 200 A GeV in CMS. The present work summarizes the main experimental results on charged particle multiplicities, rapidity distributions, momentum spectra, antiparticle to particle ratios and connects these results with some interesting physical quantities. Their dependencies on the available energies in the CMS in similar collisions are included. Interesting behaviours with the increase of this energy are reported. The most interesting are related to the behaviour of the antiproton to proton ratio on the collision centrality and on the available energy in the centre of mass system, the strangeness production, Coulomb repulsion and slope parameters of the momentum spectra. A few new steps in the knowledge of the behaviour of the highly excited and dense nuclear matter can be reported. (authors)

  3. Latest results of SEE measurements obtained by the STRURED demonstrator ASIC

    Energy Technology Data Exchange (ETDEWEB)

    Candelori, A. [INFN, Section of Padova, Via Marzolo 8, c.a.p. 35131, Padova (Italy); De Robertis, G. [INFN Section of Bari, Via Orabona 4, c.a.p. 70126, Bari (Italy); Gabrielli, A. [Physics Department, University of Bologna, Viale Berti Pichat 6/2, c.a.p. 40127, Bologna (Italy); Mattiazzo, S.; Pantano, D. [INFN, Section of Padova, Via Marzolo 8, c.a.p. 35131, Padova (Italy); Ranieri, A., E-mail: antonio.ranieri@ba.infn.i [INFN Section of Bari, Via Orabona 4, c.a.p. 70126, Bari (Italy); Tessaro, M. [INFN, Section of Padova, Via Marzolo 8, c.a.p. 35131, Padova (Italy)

    2011-01-21

    With the perspective to develop a radiation-tolerant circuit for High Energy Physics (HEP) applications, a test digital ASIC VLSI chip, called STRURED, has been designed and fabricated using a standard-cell library of commercial 130 nm CMOS technology by implementing three different radiation-tolerant architectures (Hamming, Triple Modular Redundancy and Triple Time Redundancy) in order to correct circuit malfunctions induced by the occurrence of Soft Errors (SEs). SEs are one of the main reasons of failures affecting electronic digital circuits operating in harsh radiation environments, such as in experiments performed at HEP colliders or in apparatus to be operated in space. In this paper we present and discuss the latest results of SE cross-section measurements performed using the STRURED digital device, exposed to high energy heavy ions at the SIRAD irradiation facility of the INFN National Laboratories of Legnaro (Padova, Italy). In particular the different behaviors of the input part and the core of the three radiation-tolerant architectures are analyzed in detail.

  4. Mathematical models for correction of images, obtained at radioisotope scan

    International Nuclear Information System (INIS)

    Glaz, A.; Lubans, A.

    2002-01-01

    The images, which obtained at radioisotope scintigraphy, contain distortions. Distortions appear as a result of absorption of radiation by patient's body's tissues. Two mathematical models for reducing of such distortions are proposed. Image obtained by only one gamma camera is used in the first mathematical model. Unfortunately, this model allows processing of the images only in case, when it can be assumed, that the investigated organ has a symmetric form. The images obtained by two gamma cameras are used in the second model. It gives possibility to assume that the investigated organ has non-symmetric form and to acquire more precise results. (authors)

  5. Vibrational properties of gold nanoparticles obtained by green synthesis

    Science.gov (United States)

    Alvarez, Ramón A. B.; Cortez-Valadez, M.; Bueno, L. Oscar Neira; Britto Hurtado, R.; Rocha-Rocha, O.; Delgado-Beleño, Y.; Martinez-Nuñez, C. E.; Serrano-Corrales, Luis Ivan; Arizpe-Chávez, H.; Flores-Acosta, M.

    2016-10-01

    This study reports the synthesis and characterization of gold nanoparticles through an ecological method to obtain nanostructures from the extract of the plant Opuntia ficus-indica. Colloidal nanoparticles show sizes that vary between 10-20 nm, and present various geometric morphologies. The samples were characterized through optical absorption, Raman Spectroscopy and Transmission Electron Microscopy (TEM). Additionally, low energy metallic clusters of Aun (n=2-20 atoms) were modeled by computational quantum chemistry. The theoretical results were obtained with Density Functional Theory (DFT). The predicted results of Au clusters show a tendency and are correlated with the experimental results concerning the optical absorption bands and Raman spectroscopy in gold nanoparticles.

  6. Acoustic emission results obtained from testing the ZB-1 intermediate scale pressure vessel

    International Nuclear Information System (INIS)

    Hutton, P.H.; Kurtz, R.J.; Pappas, R.A.; Dawson, J.F.; Dake, L.S.; Skorpik, J.R.

    1985-09-01

    Acoustic emission (AE) monitoring of flaw growth in an intermediate scale vessel during cyclic loading at 65 0 C and 288 0 C is described in this report. The report deals with background, methodology, and results. The work discussed is of major significance in a program supported by NRC to develop and demonstrate application of AE monitoring for continuous surveillance of reactor pressure boundaries to detect and evaluate growing flaws. Several areas of technical concern are addressed. Results support the feasibility of effective continuous monitoring

  7. Solar heating by radiant floor: Experimental results and emission reduction obtained with a micro photovoltaic–heat pump system

    International Nuclear Information System (INIS)

    Izquierdo, M.; Agustín-Camacho, P. de

    2015-01-01

    Highlights: • This work presents a PVT multicrystalline solar heating system for buildings. • The PV DC electricity generated was converted to AC to drive an air–water heat pump. • Experimental results obtained from December 1, 2012 to April 30, 2013 are detailed. • An environmental study is also presented. - Abstract: An experimental research with a solar photovoltaic thermal (PVT) micro grid feeding a reversible air–water, 6 kW heating capacity heat pump, has been carried out from December 2012 to April 2013. Its purpose is to heat a laboratory that is used as a house prototype for the study of heating/cooling systems. It was built in accordance with the 2013 Spanish CTE, and has an area of 35 m 2 divided into two internal rooms: one of them housing the storage system, the solar controller, the inverter and the control system; the other one is occupied by three people. Its main thermal characteristics are: UA = 125 W/°C and a maximum thermal load about 6.0 kW at the initial time. The PVT field consists of 12 modules, with a total area of 15.7 m 2 and useful area of 14 m 2 . Each module is composed of 48 polycrystalline silicon cells of 243.4 cm 2 , which with a nominal efficiency 14% can generate a power of 180 W, being the total nominal power installed 2.16 kW. The PV system stores electricity in 250 Ah batteries from where is converted from DC to AC through a 3.0 kW inverter that feeds the heat pump. This works supplying 840 l/h of hot water at 35–45 °C to the radiant floor. The data storing system is recording variables such as solar radiation; temperatures; input power to batteries; heat produced; heat transferred by the radiant floor; heat pump’s COP; isolated ratio; and solar fraction. The objective of this work is to present and discuss the experimental results and the emission reduction of CO 2 obtained during the period from 01/12/2012 to 30/04/2013, including the detailed results of two representative days of Madrid’s climate: 28

  8. Can Malin's gravitational-field equations be modified to obtain a viable theory of gravity to obtain a viable theory of gravity to obtain a viable theory of gravity

    International Nuclear Information System (INIS)

    Smalley, L.L.; Prestage, J.

    1976-01-01

    Malin's gravitational theory, which was recently shown by Lindblom and Nester to be incorrect, is modified by means of a recently proposed method for obtaining viable gravitational theories. The resulting self-consistent theory, which is in effect a Rastall-type modification of the Einstein theory, exhibits nonconservation of momentum, yet agrees with all experimental limits known to date within the PPN framework

  9. Prenatal cytogenetic diagnosis in Spain: analysis and evaluation of the results obtained from amniotic fluid samples during the last decade.

    Science.gov (United States)

    Mademont-Soler, Irene; Morales, Carme; Clusellas, Núria; Soler, Anna; Sánchez, Aurora

    2011-08-01

    Chromosome abnormalities are one of the main causes of congenital defects, and establishing their frequency according to the different clinical indications for invasive procedure during pregnancy is especially important for genetic counselling. We analyzed the results of 29,883 amniotic fluid samples referred to our laboratory for cytogenetic studies from 1998 to 2009, which constitutes the largest series of cytogenetic analysis performed on amniotic fluid samples in Spain. The number of samples received tended to increase from 1998 to 2005, but after 2005 it decreased substantially. Cytogenetic results were obtained in 99.5% of the samples, and the detected incidence of chromosome abnormalities was 2.9%. Of these, 48.1% consisted of classical autosomal aneuploidies, trisomy 21 being the most frequent one. The main clinical indications for amniocentesis were positive prenatal screening and advanced maternal age, but referral reasons with highest positive predictive values were, excluding parental chromosome rearrangement, increased nuchal translucency (9.2%) and ultrasound abnormalities (6.6%). In conclusion, performing the karyotype on amniotic fluid samples is a good method for the detection of chromosome abnormalities during pregnancy. The number of cytogenetic studies on amniotic fluid has now decreased, however, due to the implementation of first trimester prenatal screening for the detection of Down syndrome, which allows karyotyping on chorionic villus samples. Our results also show that both ultrasound abnormalities and increased nuchal translucency are excellent clinical indicators for fetal chromosome abnormality. Copyright © 2011 Elsevier Ireland Ltd. All rights reserved.

  10. Decontamination in preparation for dismantlement - AREVA's chemical decontamination technologies, projects performed and results obtained in the period 2011-2016

    International Nuclear Information System (INIS)

    Topf, C.; Sempere Belda, L.

    2017-01-01

    As a consequence of the nuclear phase-out decreed by the German government, several nuclear power plants in the country have already ceased operation. The remaining ones will cease operation by 2022. This has turned Germany into one of the most active regions worldwide in the field of nuclear decommissioning, with new and emerging technologies being deployed on the field, and already preexisting technologies being put to the test, optimized and developed into full maturity. The chemistry services division of AREVA GmbH has already performed 5 Full System Decontaminations (FSD) in preparation for decommissioning in this period - three in PWRs and two in BWRs - along with other international projects of relevance for decommissioning operations. During a FSD, the complete primary circuit of a nuclear power plant including auxiliary systems is subject to a chemical treatment; designed to remove radioactive matter accumulated onto system surfaces during operation. Through the effective removal of this radioactive accumulations contact dose rates on the different components of the primary circuit can be consistently reduced by factors larger than 50. This results in much lower ambient dose rates and, hence, in very significant dose savings for subsequent decommissioning activities. Additionally, dismantlement operations of large components are considerably simplified and can be performed under conditions that wouldn't have been possible before. The project specific objectives and challenges, the technologies employed, and the results obtained are presented and commented here. (authors)

  11. How many replicate tests do I need?$-$ Variability of cookstove performance and emissions has implications for obtaining useful results

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Yungang [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Environmental Energy Technologies Division; Sohn, Michael D. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Environmental Energy Technologies Division; Gadgil, Ashok J. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Environmental Energy Technologies Division; Wang, Yilun [ISO Innovative Analytics San Francisco, CA (United States); Lask, Kathleen M. [Univ. of California, Berkeley, CA (United States). College of Engineering Applied Science and Technology Program; Kirchstetter, Thomas W. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Environmental Energy Technologies Division

    2013-02-01

    Almost half of the world’s population still cooks on biomass cookstoves of poor efficiency and primitive design, such as three stone fires (TSF). Emissions from biomass cookstoves contribute to adverse health effects and climate change. A number of “improved cookstoves” with higher energy efficiency and lower emissions have been designed and promoted across the world. During the design development, and for selection of a stove for dissemination, the stove performance and emissions are commonly evaluated, communicated and compared using the arithmetic average of replicate tests made using a standardized laboratory-based test, commonly the water boiling test (WBT). However, published literature shows different WBT results reported from different laboratories for the same stove technology. Also, there is no agreement in the literature on how many replicate tests should be performed to ensure “significance” in the reported average performance. This matter has not received attention in the rapidly growing literature on stoves, and yet is crucial for estimating and communicating the performance of a stove, and for comparing the performance between stoves. We present results of statistical analyses using data from a number of replicate tests of performance and emission of the Berkeley-Darfur Stove (BDS) and the TSF under well-controlled laboratory conditions. We observed moderate variability in the test results for the TSF and BDS when measuring several characteristics. Here we focus on two as illustrative: time-to-boil and PM2.5 (particulate matter less than or equal to 2.5 micrometers in diameter) emissions. We demonstrate that interpretation of the results comparing these stoves could be misleading if only a small number of replicates had been conducted. We then describe a practical approach, useful to both stove testers and designers, to assess the number of replicates needed to obtain useful data. Caution should be exercised in attaching high credibility to

  12. Macromolecular crystallographic results obtained using a 2048x2048 CCD detector at CHESS

    International Nuclear Information System (INIS)

    Thiel, D.J.; Ealick, S.E.; Tate, M.W.; Gruner, S.M.; Eikenberry, E.F.

    1996-01-01

    We present results of macromolecular crystallographic experiments performed at the Cornell High Energy Synchrotron Source (CHESS) with a new CCD-based detector. This detector, installed in January 1995, complements a 1024x1024 CCD detector that has been in continuous operation at CHESS since December 1993. The new detector is based on a 4-port, 2048x2048 pixel CCD that is directly coupled to a Gd 2 O 2 S:Tb phosphor by a 3:1 tapered fiber optic. The active area of the phosphor is a square 82 mm on an edge. The readout time is 7 seconds. In the standard mode of operation, the pixel size at the active area is 41 μm on the edge leading to the capability of resolving approximately 200 orders of diffraction across the detector face. The detector also operates in a 1024x1024 mode in which the pixel size is electronically increased by a factor of 4 in area resulting in smaller data files and faster detector readout but at the expense of spatial resolution. Most of the data that has been collected by this detector has been collected in this mode. Dozens of data sets have been collected by many experimenters using this detector at CHESS during the four month period from its installation until the start of the six-month down period of the storage ring. The capabilities of the detector will be illustrated with results from various crystallographic measurements including experiments in which the recorded diffraction patterns extend in resolution as far as 1 A. The results demonstrate that this detector is capable of collecting data of quality at least equal to that of imaging plates but, in many circumstances, with much greater beamline efficiency. copyright 1996 American Institute of Physics

  13. Internal friction study of hydrides in zirconium at low hydrogen contents

    International Nuclear Information System (INIS)

    Peretti, H.A.; Corso, H.L.; Gonzalez, O.A.; Fernandez, L.; Ghilarducci, A.A.; Salva, H.R.

    1999-01-01

    Full text: Internal friction and shear modulus measurements were carried out on crystal bar zirconium in the as received and hydride conditions using an inverted forced pendulum. Hydriding was achieved in two ways: inside and out of the pendulum. The final hydrogen content determined by fusion analysis in the 'in situ' hydride sample was of 36 ppm. Another sample was hydride by the cathodic charge method with 25 ppm. The thermal solid solubility (TSS) phase boundary presents hysteresis between the precipitation (TSSP) and the dissolution (TSSD) temperatures for the zirconium hydrides. During the first thermal cycling the anelastic effects could be attributed to the δ, ε and metastable γ zirconium hydrides. After 'in situ' annealing at 490 K, these peaks completely disappear in the electrolytically charged sample, while in the 'in situ' hydride, the peaks remain with decreasing intensity. This effect can be understood in terms of the different surface conditions of the samples. (author)

  14. Obtainment of tantalum oxide from national ores

    International Nuclear Information System (INIS)

    Pinatti, D.G.; Ribeiro, S.; Martins, A.H.

    1988-01-01

    The experimental results of tantalum oxides (Ta 2 O 5 ) obtainment from Brazilian ores of tantalite and columbite are described. This study is a part of the technologic and scientific research design of refractory metals (Ti, Zr, Hf, V, Nb, Ta, Cr, Mo and W) and correlate ceramics. (C.G.C.) [pt

  15. Process optimization for obtaining nano cellulose from curaua fiber

    International Nuclear Information System (INIS)

    Lunz, Juliana do N.; Cordeiro, Suellem B.; Mota, Jose Carlos F.; Marques, Maria de Fatima V.

    2011-01-01

    This study focuses on the methodology for optimization to obtain nanocellulose from vegetal fibers. An experimental planning was carried out for the treatment of curaua fibers and parameters were estimated, having the concentration of H 2 SO 4 , hydrolysis time, reaction temperature and time of sonication applied as independent variables for further statistical analysis. According to the estimated parameters, the statistically significant effects were determined for the process of obtaining nanocellulose. According to the results obtained from the thermogravimetric analysis (TGA) it was observed that certain conditions led to cellulose with degradation temperatures near or even above that of untreated cellulose fibers. The crystallinity index (IC) obtained after fiber treatment (X-ray diffraction) were higher than that of the pure fiber. Treatments with high acid concentrations led to higher IC. (author)

  16. Warm magnetic measurements of MCBCs: comparison between the results obtained with the Quadrupole Industrial Magnetic Measurement and the Corrector Industrial Magnetic Measurement systems

    CERN Document Server

    Remondino, Vittorio; Catalan-Lasheras, N

    2005-01-01

    MCBCs modules are first magnetically measured at Tesla using a second-generation Corrector Industrial Magnetic Measurement (CIMM). After assembly into the SSS quadrupoles, measurements are repeated at CERN using the Quadrupole Industrial Magnetic Measurement (QIMM) system. In this note, we compare the measurements provided by the two systems. In all the 18 cases examined, the correlation found is excellent. The consistency of the results obtained indicates that both systems are effective, that modules are correctly measured by the firm personnel and that magnetic characteristics of the modules do not change during their assembly in cold masses.

  17. Understanding AlN Obtaining Through Computational Thermodynamics Combined with Experimental Investigation

    Science.gov (United States)

    Florea, R. M.

    2017-06-01

    Basic material concept, technology and some results of studies on aluminum matrix composite with dispersive aluminum nitride reinforcement was shown. Studied composites were manufactured by „in situ” technique. Aluminum nitride (AlN) has attracted large interest recently, because of its high thermal conductivity, good dielectric properties, high flexural strength, thermal expansion coefficient matches that of Si and its non-toxic nature, as a suitable material for hybrid integrated circuit substrates. AlMg alloys are the best matrix for AlN obtaining. Al2O3-AlMg, AlN-Al2O3, and AlN-AlMg binary diagrams were thermodynamically modelled. The obtained Gibbs free energies of components, solution parameters and stoichiometric phases were used to build a thermodynamic database of AlN- Al2O3-AlMg system. Obtaining of AlN with Liquid-phase of AlMg as matrix has been studied and compared with the thermodynamic results. The secondary phase microstructure has a significant effect on the final thermal conductivity of the obtained AlN. Thermodynamic modelling of AlN-Al2O3-AlMg system provided an important basis for understanding the obtaining behavior and interpreting the experimental results.

  18. Cotton nanofibers obtained by different acid conditions

    International Nuclear Information System (INIS)

    Teixeira, Eliangela de M.; Oliveira, Caue Ribeiro de; Mattoso, Luiz H.C.; Correa, Ana Carolina; Palladin, Priscila

    2009-01-01

    The thermal stability of cellulose nanofibers is related to their application and especially to polymer processing which temperatures of processing are around 200 deg C. In this work, nanofibers of commercial cotton were obtained by acid hydrolysis employing different acids: sulfuric, hydrochloric and a mixture (2:1; sulfuric acid: hydrochloric acid).The morphology of the nanofibers were characterized by transmission microscopy (TEM), crystallinity by x-ray diffraction (XRD) and thermal stability in air atmosphere by thermogravimetric analysis (TGA). The results indicated a very similar morphology and crystallinity among them. The main differences were relative to aggregation state e and thermal stability. The aggregation state of the suspensions decreases in the order HCl 2 SO 4 :HCl 2 SO 4- . The hydrolysis with a mix of HCl and H 2 SO 4 resulted in cellulose nanofibers with higher thermal stability than those hydrolyzed with H 2 SO 4 . The hydrolysis employed with a mixture of sulphuric and hydrochloric acids also showed a better dispersion than those suspensions of nanofibers obtained by hydrolysis with only HCl. (author)

  19. Health Outcomes of Obtaining Housing Among Older Homeless Adults

    Science.gov (United States)

    Miao, Yinghui; Mitchell, Susan L.; Bharel, Monica; Patel, Mitkumar; Ard, Kevin L.; Grande, Laura J.; Blazey-Martin, Deborah; Floru, Daniella; Steinman, Michael A.

    2015-01-01

    Objectives. We determined the impact of obtaining housing on geriatric conditions and acute care utilization among older homeless adults. Methods. We conducted a 12-month prospective cohort study of 250 older homeless adults recruited from shelters in Boston, Massachusetts, between January and June 2010. We determined housing status at follow-up, determined number of emergency department visits and hospitalizations over 12 months, and examined 4 measures of geriatric conditions at baseline and 12 months. Using multivariable regression models, we evaluated the association between obtaining housing and our outcomes of interest. Results. At 12-month follow-up, 41% of participants had obtained housing. Compared with participants who remained homeless, those with housing had fewer depressive symptoms. Other measures of health status did not differ by housing status. Participants who obtained housing had a lower rate of acute care use, with an adjusted annualized rate of acute care visits of 2.5 per year among participants who obtained housing and 5.3 per year among participants who remained homeless. Conclusions. Older homeless adults who obtained housing experienced improved depressive symptoms and reduced acute care utilization compared with those who remained homeless. PMID:25973822

  20. Lactation curves and economic results of Saanen goats fed increasing dietary energy levels obtained by the addition of calcium salts of fatty acids

    Directory of Open Access Journals (Sweden)

    Rodrigo de Souza

    2014-02-01

    Full Text Available The objective of this study was to evaluate the use of calcium salts of fatty acids (CSFA to increase the dietary energy levels for Saanen goats and their effects on the lactation curve, dry matter intake, body weight, and economic results of the goats. Twenty multiparous goats, weighing an average of 63.5±10.3 kg, were randomly assigned to one of four treatment groups, each receiving one of the following dietary energy levels: a control diet consisting of 2.6 Mcal of metabolizable energy per kg of dry matter (Mcal ME/kg DM or a test diet supplemented with CSFA (Lactoplus® to obtain 2.7, 2.8, or 2.9 Mcal ME/kg DM. Goats were housed in individual stalls and were fed and milked twice daily. The animals were evaluated until 180 days in milk by measuring dry matter intake and milk yield. These measurements were used to calculate feed efficiencies and the cost-benefit ratio of diet and lactation curves using Wood's nonlinear model. Increasing dietary energy levels showed no effect on body weight. Supplementation with CSFA did not limit dry matter intake; however, it changed the shape of the lactation curve by promoting a late peak lactation with a longer duration. Milk yields at 180 days in milk had a quadratic increase with a maximum energy level at 2.85 Mcal ME/kg DM. Increasing the dietary energy level for Saanen goats using CSFA changes their lactation curves, with the best milk production achieved with a 2.85 Mcal ME/kg DM diet; however, the greatest economic results were obtained with a 2.7 Mcal ME/kg DM diet.

  1. Obtaining land cover changes information from multitemporal analysis of Landsat-TM images: results from a case study in West African dryland

    Science.gov (United States)

    Nutini, F.; Boschetti, M.; Brivio, P. A.; Antoninetti, M.

    2012-04-01

    The Sahelian belt of West Africa is a semiarid region characterized by wide climate variations, which can in turn affect the livelihood of local populations particularly in rangeland areas, as happens during the dramatic food crisis in the 70-80s caused by rainfall scarcity. The monitoring of natural resources and rainfed agricultural activities, with the aim to provide information to support Sahelian food security action, needs the production of detailed thematic maps as emphasized by several scientific papers. In this framework, a study was conducted to develop a method to exploit time series of remote sensed satellite data to 1) provide reliable land cover (LC) map at local scale in a dry region and 2) obtain a LC change (LCC) map that contribute to identify the plausible causes of local environmental instability. Satellite images used for this work consist in a time series of Landsat Thematic Mapper (TM) (path row 195-50) acquired in the 2000 (6 scenes) and 2007 (9 scenes) from February (Dry season) to September (end of wet season). The study investigates the different contribution provided by spectra information of a single Landsat TM image and by time series of derived NDVI. Different tests have been conducted with different combination of data set (spectral and temporal)in order to identify the best approach to obtain a LC map in five classes of interest: Shrubland, Cultivated Land, Water body, Herbaceous vegetation and Bare soil. The best classification approach is exposed and applied on two years in the last decade. The comparison between this two LC results in land cover change map, that displays the changes of vegetation patterns that have been characterized the area. The discussed results show a largely stable dryland region, but locally characterized by hot-spot of decreasing in natural vegetation inside the rangelands and an increasing of cultivations along fossil valleys where human activities are slightly intense. The discussion shows that this hot

  2. On the influence of infiltration of radioactive beds by flushing fluid on γ-ray logging results obtained from uranium deposit No. 387

    International Nuclear Information System (INIS)

    Ren Bingxiang; Zhang Yuechun; Ai Shuyi.

    1985-01-01

    A large number of field logging data obtained during the course of exploration on uranium deposit No. 387 show when the radioactive beds are encountered by drill holes and the drilling continues the γ-ray intensity decreases. It is considered that the escape of emanation does not considerably influence the logging results. Therefore, based upon the experiment of immerseing ores in fluid and geological and hydrogeological data of the deposit, the hypotheses that the γ-ray intensity in drill hole is closely related with the infiltration of flushing fluid is suggested. The ore bodies are strictly controlled by faults. Most of the uranium and thorium are absorbed by pelitic-carbonaceous cements or fill the porous spaces in structural breccia and cataclasite. They are easy to dissolve in water. Moreover, the ore-bearing structures are the unique water aquifers which is under pressure. As the level of flushing fluid is higher than the pressure head so it continuously pours into the ore-bearing beds, resulting in the infiltration of U and Ra. Consequently, the radioactivity detected is low

  3. Characterization of Wastewaters obtained from Hatay Tanneries

    Directory of Open Access Journals (Sweden)

    Şana Sungur

    2017-06-01

    Full Text Available The leather tanning industry is one of the most significant pollutants in terms of both conventional and toxic parameters. On the other hand, leather industry has an important economic role both in Turkey and in the World. In this study, wastewater samples were taken from 15 different tanneries in the Hatay Region. Wastewaters obtained from liming process and chromium tanning process was analyzed. Sulfide, chromium (III, chromium (VI, oil and grease, total suspended solids (TSS, organic matters, biochemical oxygen demand (BOD, chemical oxygen demand (COD, pH and alkalinity were determined according to Turkish Standard Methods. The determined averages values belong to wastewaters obtained from liming process were as following: pH 11.71; COD 16821 mg L-1; BOD 4357 mg L-1; TSS 39023 mg L-1; oil and grease 364 mg L-1; S-2 concentration 802 mg L-1; alkalinity 2115 mg L-1. The determined averages values belong to wastewaters obtained from chromium tanning process were also as following: pH 4.23; COD 6740 mg L-1; BOD 377 mg L-1; Cr+3 concentrations 372 mg L-1; Cr+6 concentrations 127 mg L-1; TSS 14553 mg L-1; oil and grease 343 mg L-1. The results of all analyzes were higher than wastewater discharge standards. As a result, it’s necessary to use more effective treatments in order to reduce the negative impacts of leather tanning industry that affect environment, natural water resources and at last human health and welfare.

  4. Recent Advances in Solid Catalysts Obtained by Metalloporphyrins Immobilization on Layered Anionic Exchangers: A Short Review and Some New Catalytic Results

    Directory of Open Access Journals (Sweden)

    Shirley Nakagaki

    2016-02-01

    Full Text Available Layered materials are a very interesting class of compounds obtained by stacking of two-dimensional layers along the basal axis. A remarkable property of these materials is their capacity to interact with a variety of chemical species, irrespective of their charge (neutral, cationic or anionic. These species can be grafted onto the surface of the layered materials or intercalated between the layers, to expand or contract the interlayer distance. Metalloporphyrins, which are typically soluble oxidation catalysts, are examples of molecules that can interact with layered materials. This work presents a short review of the studies involving metalloporphyrin immobilization on two different anionic exchangers, Layered Double Hydroxides (LDHs and Layered Hydroxide Salts (LHSs, published over the past year. After immobilization of anionic porphyrins, the resulting solids behave as reusable catalysts for heterogeneous oxidation processes. Although a large number of publications involving metalloporphyrin immobilization on LDHs exist, only a few papers have dealt with LHSs as supports, so metalloporphyrins immobilized on LHSs represent a new and promising research field. This work also describes new results on an anionic manganese porphyrin (MnP immobilized on Mg/Al-LDH solids with different nominal Mg/Al molar ratios (2:1, 3:1 and 4:1 and intercalated with different anions (CO32− or NO3−. The influence of the support composition on the MnP immobilization rates and the catalytic performance of the resulting solid in cyclooctene oxidation reactions will be reported.

  5. Recent Advances in Solid Catalysts Obtained by Metalloporphyrins Immobilization on Layered Anionic Exchangers: A Short Review and Some New Catalytic Results.

    Science.gov (United States)

    Nakagaki, Shirley; Mantovani, Karen Mary; Machado, Guilherme Sippel; Castro, Kelly Aparecida Dias de Freitas; Wypych, Fernando

    2016-02-29

    Layered materials are a very interesting class of compounds obtained by stacking of two-dimensional layers along the basal axis. A remarkable property of these materials is their capacity to interact with a variety of chemical species, irrespective of their charge (neutral, cationic or anionic). These species can be grafted onto the surface of the layered materials or intercalated between the layers, to expand or contract the interlayer distance. Metalloporphyrins, which are typically soluble oxidation catalysts, are examples of molecules that can interact with layered materials. This work presents a short review of the studies involving metalloporphyrin immobilization on two different anionic exchangers, Layered Double Hydroxides (LDHs) and Layered Hydroxide Salts (LHSs), published over the past year. After immobilization of anionic porphyrins, the resulting solids behave as reusable catalysts for heterogeneous oxidation processes. Although a large number of publications involving metalloporphyrin immobilization on LDHs exist, only a few papers have dealt with LHSs as supports, so metalloporphyrins immobilized on LHSs represent a new and promising research field. This work also describes new results on an anionic manganese porphyrin (MnP) immobilized on Mg/Al-LDH solids with different nominal Mg/Al molar ratios (2:1, 3:1 and 4:1) and intercalated with different anions (CO₃(2-) or NO₃(-)). The influence of the support composition on the MnP immobilization rates and the catalytic performance of the resulting solid in cyclooctene oxidation reactions will be reported.

  6. Obtainment, machining and wear of metal matrix composites processed by powder metallurgy

    International Nuclear Information System (INIS)

    Jesus, Edilson Rosa Barbosa de.

    1998-01-01

    The aim of this investigation was the obtainment of metal matrix composites (MMC) by the route of powder metallurgy, and the valuation of these materials with relation to their machining and wear characteristics. Firstly, were obtained pure commercial aluminium matrix composites materials, with 5, 10 and 15% volumetric fraction of silicon carbide particles. Was also obtained a material without reinforcement particles in order to verify by comparison, the influence of addition of reinforcement particles. The obtained materials were characterized physics (hydrostatic density), mechanics (hardness and tensile tests) and microstructurally (optical microscopy and scanning electron microscopy). The results showed a homogeneous distribution of reinforcement particles in the composite, and improvement in the mechanical properties, mainly tensile strength (UTS) in comparison to the unreinforced material. After, tests were made to verify the materials behavior during machining and to check the performance of several tool materials (cemented carbide, ceramics and polycrystalline diamond). In these tests, values of the cutting force were measured by instrumented tool-holders. Phenomena such as tool wear, built-up edge formation and mechanism of chip formation were also observed and evaluated. The results from the cemented carbide tool tests, were utilised for the machinability index determination of each material. These results were applied to the Taylor equation and the equation constants for each material and test conditions were determined. The results showed that the inclusion of silicon carbide particles made extremely difficult the machining of the composites, and only with diamond tool, satisfactory results were obtained. At last, wear tests were performed to verify the influence of the reinforcement particles in the characteristics of wear resistance of the materials. The results obtained were utilized in the wear coefficient determination for each material. The

  7. Some Results on Sea Ice Rheology for the Seasonal Ice Zone, Obtained from the Deformation Field of Sea Ice Drift Pattern

    Science.gov (United States)

    Toyota, T.; Kimura, N.

    2017-12-01

    Sea ice rheology which relates sea ice stress to the large-scale deformation of the ice cover has been a big issue to numerical sea ice modelling. At present the treatment of internal stress within sea ice area is based mostly on the rheology formulated by Hibler (1979), where the whole sea ice area behaves like an isotropic and plastic matter under the ordinary stress with the yield curve given by an ellipse with an aspect ratio (e) of 2, irrespective of sea ice area and horizontal resolution of the model. However, this formulation was initially developed to reproduce the seasonal variation of the perennial ice in the Arctic Ocean. As for its applicability to the seasonal ice zones (SIZ), where various types of sea ice are present, it still needs validation from observational data. In this study, the validity of this rheology was examined for the Sea of Okhotsk ice, typical of the SIZ, based on the AMSR-derived ice drift pattern in comparison with the result obtained for the Beaufort Sea. To examine the dependence on a horizontal scale, the coastal radar data operated near the Hokkaido coast, Japan, were also used. Ice drift pattern was obtained by a maximum cross-correlation method with grid spacings of 37.5 km from the 89 GHz brightness temperature of AMSR-E for the entire Sea of Okhotsk and the Beaufort Sea and 1.3 km from the coastal radar for the near-shore Sea of Okhotsk. The validity of this rheology was investigated from a standpoint of work rate done by deformation field, following the theory of Rothrock (1975). In analysis, the relative rates of convergence were compared between theory and observation to check the shape of yield curve, and the strain ellipse at each grid cell was estimated to see the horizontal variation of deformation field. The result shows that the ellipse of e=1.7-2.0 as the yield curve represents the observed relative conversion rates well for all the ice areas. Since this result corresponds with the yield criterion by Tresca and

  8. Comparison of the identification results of Candida species obtained by BD Phoenix™ and Maldi-TOF (Bruker Microflex LT Biotyper 3.1).

    Science.gov (United States)

    Marucco, Andrea P; Minervini, Patricia; Snitman, Gabriela V; Sorge, Adriana; Guelfand, Liliana I; Moral, Laura López

    2018-02-05

    In patients with invasive fungal infections, the accurate and rapid identification of the genus Candida is of utmost importance since antimycotic sensitivity is closely related to the species. The aim of the present study was to compare the identification results of species of the genus Candida obtained by BD Phoenix™ (Becton Dickinson [BD]) and Maldi-TOF MS (Bruker Microflex LT Biotyper 3.1). A total of 192 isolates from the strain collection belonging to the Mycology Network of the Autonomous City of Buenos Aires, Argentina, were analyzed. The observed concordance was 95%. Only 10 strains (5%) were not correctly identified by the BD Phoenix™ system. The average identification time with the Yeast ID panels was 8h 22min. The BD Phoenix™ system proved to be a simple, reliable and effective method for identifying the main species of the genus Candida. Copyright © 2017 Asociación Argentina de Microbiología. Publicado por Elsevier España, S.L.U. All rights reserved.

  9. Obtaining of potassium dicyan-argentate

    International Nuclear Information System (INIS)

    Sattarova, M.A.; Solojenkin, P.M.

    1997-01-01

    This work is devoted to obtaining of potassium dicyan-argentate. By means of exchange reaction between silver nitrate and potassium cyanide the potassium dicyan-argentate was synthesized. The analysis of obtained samples was carried out by means of titration and potentiometry.

  10. Using the Viking biology experimental results to obtain chemical information about Martian regolith

    Science.gov (United States)

    Plumb, Robert C.

    1992-01-01

    Although initially formulated as biology experiments, most of the results produced by the Viking Labeled Release (LR), Gas Exchange (GEX), and Pyrolytic Release (PR) experiments have been reproduced by chemical means. The experiments do not need more study as 'biological' phenomena, but they do deserve much more careful consideration from a chemical viewpoint. They are the only 'wet-chemical' experiments that scientists have performed on another planet, but they have not found very general use as sources of scientific information. There is a large set of potentially useful chemical observations, e.g., the three resolvable and precisely measured kinetic components of the release of C-14-labeled gases, the thermal sensitivity and magnitudes of the oxidation reaction(s) of the LR experiments, the kinetics and magnitude of the O2 and CO2 release of the GEX experiments, the thermal sensitivity of the GEX results, the differences between the thermal sensitivity of the GEX and the thermal sensitivity of the LR responses, and the kinetics and magnitudes of the LR successive injection reabsorption effect. It should be possible to test many chemical aspects of hypothetical martian phenomena in experiments using the biology experimental configurations and derive much valuable information by comparisons with the Viking observations.

  11. GHM method for obtaining rationalsolutions of nonlinear differential equations.

    Science.gov (United States)

    Vazquez-Leal, Hector; Sarmiento-Reyes, Arturo

    2015-01-01

    In this paper, we propose the application of the general homotopy method (GHM) to obtain rational solutions of nonlinear differential equations. It delivers a high precision representation of the nonlinear differential equation using a few linear algebraic terms. In order to assess the benefits of this proposal, three nonlinear problems are solved and compared against other semi-analytic methods or numerical methods. The obtained results show that GHM is a powerful tool, capable to generate highly accurate rational solutions. AMS subject classification 34L30.

  12. Optical properties of Cd Se thin films obtained by pyrolytic dew

    International Nuclear Information System (INIS)

    Perez G, A.M.; Tepantlan, C.S.; Renero C, F.

    2006-01-01

    In this paper the optical properties of Cd Se thin films obtained by spray pyrolysis are presented. The films are prepared by Sodium Seleno sulphate (Na 2 SSeO 3 ) and Cadmium Chloride (CdC 12 ) mixing in aqueous environment. Optical parameters of the films (refractive index, absorption coefficient and optical ban gap) were calculated from transmittance spectra. The obtained values of the optical ban gap are compared with the result obtained by other deposition method. (Author)

  13. Development of the NAA Laboratory for an Accreditation Obtains

    International Nuclear Information System (INIS)

    Sri Wardani; Rina M, Th.; Sunarko, M.; Ratnawati, E.

    2004-01-01

    The evaluation of capability of the neutron activation analysis comparative method and laboratory equipment at P2TRR have been performed by analyzed a reference standard materials prepared by NIST, namely: SRM 1646a and SRM 1648 by a both of comparative and ko- NAA methods. From the analysis results used a comparative method shown that the method and laboratory equipment used at P2TRR obtained in a good precision, accuracy and high sensitivity. In this experiments a few elements could analyzed, namely: V, Ti, Mn, Cl, As, Sm, La, Na, Sc, Cr, Fe, Co, Se, Br, In, Sb, Ba, Cs, Ce, W, U, and Zn. The deviation values results compared with certificate values (NIST) obtained in a range 2 - 12.5% with confidence levels in range 68 - 98%. While, a reference standard material of SRM 1648 analyzed by k 0 -NAA method shown that the method need more research and study continued. From the qualitatively analysis results for short-lived nuclides category analysis by k 0 -NAA could identified a few elements, namely: V, Cu, Na, As and U with standard deviation values in range 1- 11% and limit detection values are 1.6 (U), 6.4 (Cu), 11.2 (V), 73.3 (As) and 199.9 (Na) μg/g for a SRM 1648. For analysis of CRM 8 the results obtained on standard deviation values in range 1 - 13 % and limit detection of 0.71 (Cu), 1.2 (As), 2.4 (V) and 375.9 (Na) μg/g. (author)

  14. Uncertainty and Sensitivity Analysis Results Obtained in the 1996 Performance Assessment for the Waste Isolation Pilot Plant

    International Nuclear Information System (INIS)

    Bean, J.E.; Berglund, J.W.; Davis, F.J.; Economy, K.; Garner, J.W.; Helton, J.C.; Johnson, J.D.; MacKinnon, R.J.; Miller, J.; O'Brien, D.G.; Ramsey, J.L.; Schreiber, J.D.; Shinta, A.; Smith, L.N.; Stockman, C.; Stoelzel, D.M.; Vaughn, P.

    1998-01-01

    The Waste Isolation Pilot Plant (WPP) is located in southeastern New Mexico and is being developed by the U.S. Department of Energy (DOE) for the geologic (deep underground) disposal of transuranic (TRU) waste. A detailed performance assessment (PA) for the WIPP was carried out in 1996 and supports an application by the DOE to the U.S. Environmental Protection Agency (EPA) for the certification of the WIPP for the disposal of TRU waste. The 1996 WIPP PA uses a computational structure that maintains a separation between stochastic (i.e., aleatory) and subjective (i.e., epistemic) uncertainty, with stochastic uncertainty arising from the many possible disruptions that could occur over the 10,000 yr regulatory period that applies to the WIPP and subjective uncertainty arising from the imprecision with which many of the quantities required in the PA are known. Important parts of this structure are (1) the use of Latin hypercube sampling to incorporate the effects of subjective uncertainty, (2) the use of Monte Carlo (i.e., random) sampling to incorporate the effects of stochastic uncertainty, and (3) the efficient use of the necessarily limited number of mechanistic calculations that can be performed to support the analysis. The use of Latin hypercube sampling generates a mapping from imprecisely known analysis inputs to analysis outcomes of interest that provides both a display of the uncertainty in analysis outcomes (i.e., uncertainty analysis) and a basis for investigating the effects of individual inputs on these outcomes (i.e., sensitivity analysis). The sensitivity analysis procedures used in the PA include examination of scatterplots, stepwise regression analysis, and partial correlation analysis. Uncertainty and sensitivity analysis results obtained as part of the 1996 WIPP PA are presented and discussed. Specific topics considered include two phase flow in the vicinity of the repository, radionuclide release from the repository, fluid flow and radionuclide

  15. Uncertainty and Sensitivity Analysis Results Obtained in the 1996 Performance Assessment for the Waste Isolation Pilot Plant

    Energy Technology Data Exchange (ETDEWEB)

    Bean, J.E.; Berglund, J.W.; Davis, F.J.; Economy, K.; Garner, J.W.; Helton, J.C.; Johnson, J.D.; MacKinnon, R.J.; Miller, J.; O' Brien, D.G.; Ramsey, J.L.; Schreiber, J.D.; Shinta, A.; Smith, L.N.; Stockman, C.; Stoelzel, D.M.; Vaughn, P.

    1998-09-01

    The Waste Isolation Pilot Plant (WPP) is located in southeastern New Mexico and is being developed by the U.S. Department of Energy (DOE) for the geologic (deep underground) disposal of transuranic (TRU) waste. A detailed performance assessment (PA) for the WIPP was carried out in 1996 and supports an application by the DOE to the U.S. Environmental Protection Agency (EPA) for the certification of the WIPP for the disposal of TRU waste. The 1996 WIPP PA uses a computational structure that maintains a separation between stochastic (i.e., aleatory) and subjective (i.e., epistemic) uncertainty, with stochastic uncertainty arising from the many possible disruptions that could occur over the 10,000 yr regulatory period that applies to the WIPP and subjective uncertainty arising from the imprecision with which many of the quantities required in the PA are known. Important parts of this structure are (1) the use of Latin hypercube sampling to incorporate the effects of subjective uncertainty, (2) the use of Monte Carlo (i.e., random) sampling to incorporate the effects of stochastic uncertainty, and (3) the efficient use of the necessarily limited number of mechanistic calculations that can be performed to support the analysis. The use of Latin hypercube sampling generates a mapping from imprecisely known analysis inputs to analysis outcomes of interest that provides both a display of the uncertainty in analysis outcomes (i.e., uncertainty analysis) and a basis for investigating the effects of individual inputs on these outcomes (i.e., sensitivity analysis). The sensitivity analysis procedures used in the PA include examination of scatterplots, stepwise regression analysis, and partial correlation analysis. Uncertainty and sensitivity analysis results obtained as part of the 1996 WIPP PA are presented and discussed. Specific topics considered include two phase flow in the vicinity of the repository, radionuclide release from the repository, fluid flow and radionuclide

  16. Containment Evaluation under Severe Accidents (CESA): synthesis of the predictive calculations and analysis of the first experimental results obtained on the Civaux mock-up

    International Nuclear Information System (INIS)

    Granger, L.; Rieg, C.Y.; Touret, J.P.; Fleury, F.; Nahas, G.; Danisch, R.; Brusa, L.; Millard, A.; Laborderie, C.; Ulm, F.; Contri, P.; Schimmelpfennig, K.; Barre, F.; Firnhaber, M.; Gauvain, J; Coulon, N.; Dutton, L.M.C.; Tuson, A.

    2001-01-01

    In 1996, EDF decided to build a containment model at the scale 1:3, the MAEVA mock-up, in order to check and study the behaviour of a pre-stressed concrete containment vessel without a liner in terms of mechanical strength and leaktightness, for loadings corresponding to its design and beyond design conditions. In parallel with the construction and testing of the mock-up, a cost-shared R and D action supported by the European Union, the CESA project, is dealing with quantification of leak rates through concrete cracks and porosity, predictive calculations of the behaviour of the mock-up and analysis of the experimental results. In this paper, we propose a synthesis of the main theoretical and experimental results, obtained after 2.5 years. It should however be noted that, due to some unexpected delays in the experimental programme, quite natural with such a huge and unique experimental set-up, only the design-basis accident sequences, already performed, have been reported in this paper. The first results are nevertheless very interesting, both from a scientific and nuclear utility point of view

  17. Experimental results on advanced inertial fusion schemes obtained within the HiPER project

    International Nuclear Information System (INIS)

    Batani, Dimitri; Santos, Jorge J.; Schurtz, Guy; Hulin, Sebastien; Ribeyre, Xavier; Nicolai, Philippe; Vauzour, Benjamin; Dorchies, Fabien; Gizzi, Leonida A.; Koester, Petra; Labate, Luca; Honrubia, Javier; Antonelli, Luca; Morace, Alessio; Volpe, Luca; Nazarov, Wiger; Pasley, John; Richetta, Maria; Lancaster, Kate; Spindloe, Christopher; Tolley, Martin; Neely, David; Kozlova, Michaela; Nejdl, Jaroslav; Rus, Bedrich; Wolowski, Jerzy; Badziak, Jan

    2012-01-01

    This paper presents the results of experiments conducted within the Work Package 10 (fusion experimental programme) of the HiPER project. The aim of these experiments was to study the physics relevant for advanced ignition schemes for inertial confinement fusion, i.e. the fast ignition and the shock ignition. Such schemes allow to achieve a higher fusion gain compared to the indirect drive approach adopted in the National Ignition Facility in United States, which is important for the future inertial fusion energy reactors and for realising the inertial fusion with smaller facilities. (authors)

  18. Visualization of atomic distances at the 1MV electron microscope: first results obtained on the Grenoble 1MV microscope

    International Nuclear Information System (INIS)

    Bourret, A.

    1975-01-01

    Practical and theoretical conditions for obtaining high resolution lattice images are presented. The use of a high voltage electron microscope is particularly powerful to visualize distances smaller than 3A. A 2A resolution test on (200) gold planes has been carried out on the Grenoble 1MV microscope. It would be possible at this level to study the crystalline defects such as dislocations or grain boundaries [fr

  19. Shaking table testing of a HTGR reactor core, comparison with the results obtained using a nonlinear mathematical model

    International Nuclear Information System (INIS)

    Berriaud, C.; Cebe, E.; Livolant, M.; Buland, P.

    1975-01-01

    Two series of horizontal tests have been performed at Saclay on the shaking table VESUVE: sinusoidal test and time history response. Sinusoidal tests have shown the strongly nonlinear dynamic behavior of the core. The resonant frequency of the core is dependent on the level of the excitation. These phenomena have been explained by a computer code, which is a lumped mass nonlinear model. El Centro time history displacement at the level of PCRV was reproduced on the shaking table. The analytical model was applied to this excitation and good comparison was obtained for forces and velocities [fr

  20. Analysis of ADU structure obtained under different precipitation conditions

    International Nuclear Information System (INIS)

    Ramella, Jose L.; Esteban, Adolfo; Mendez De Leo, Lucia P.; Sassone, Ariel; Novara, Oscar E.; Boero, Norma L.; Leyva, Ana G.

    1999-01-01

    ADU is the nominal name for ammonium poly uranate. It is a very complex compound of polymeric structure, which may have, according to precipitation conditions, different chemical composition and crystallographic structure. ADU is used as uranium oxide precursor in the manufacture of fuel elements. In former papers it was proved that if ultrasound is applied during precipitation and digestion the characteristics of the final product (U 3 O 8 UO 2 ) improve. By studying ADU thermal decomposition obtained by ultrasonic application, it was intended to obtain its composition. Therefore, differential thermal gravimetric and differential thermal analyses were performed. Samples were taken from special points and analyzed by X-ray diffraction, infra-red spectroscopy and scanning. An experiment was also designed to identify the products released during heating. Results and conclusions obtained are presented in this work. (author)

  1. Technical and technological solution for vegetal bio-stimulants obtaining

    Science.gov (United States)

    Anghelache, D. G.; Diaconescu, I.; Pătraşcu, R.

    2017-08-01

    The paper presents a modern technology for bio fertilizers resulted from waste plant mass after harvesting crops Experimental products were obtained rich in nutrients, but unstable in terms of existing microorganisms. Therefore, they conducted further studies to obtaining bio fungicide herb, so in all investigations undertaken so far in the laboratory, were able to conclude that the introduction of medicinal plant extracts with fungicidal effect into the bio fertilizers obtained by degradation of plant material post-harvest can get various bio-stimulants with nourishing effect upon the plants. Following this technology the paper’s objective is to identify a flux scheme for experimental equipment which can produce as final outcome this type of bio-stimulant. Also, in this work, this equipment will be chosen and will be designed following and obeying to the request of every step of the above technology.

  2. New method in obtaining correction factor of power confirming

    International Nuclear Information System (INIS)

    Deng Yongjun; Li Rundong; Liu Yongkang; Zhou Wei

    2010-01-01

    Westcott theory is the most widely used method in reactor power calibration, which particularly suited to research reactor. But this method is very fussy because lots of correction parameters which rely on empirical formula to special reactor type are needed. The incidence coefficient between foil activity and reactor power was obtained by Monte-Carlo calculation, which was carried out with precise description of the reactor core and the foil arrangement position by MCNP input card. So the reactor power was determined by the core neutron fluence profile and the foil activity placed in the position for normalization use. The characteristic of this new method is simpler, more flexible and accurate than Westcott theory. In this paper, the results of SPRR-300 obtained by the new method in theory were compared with the experimental results, which verified the possibility of this new method. (authors)

  3. Perovskite type nanopowders and thin films obtained by chemical methods

    Directory of Open Access Journals (Sweden)

    Viktor Fruth

    2010-09-01

    Full Text Available The review presents the contribution of the authors, to the preparation of two types of perovskites, namely BiFeO3 and LaCoO3, by innovative methods. The studied perovskites were obtained as powders, films and sintered bodies. Their complex structural and morphological characterization is also presented. The obtained results have underlined the important influence of the method of preparation on the properties of the synthesized perovskites.

  4. Obtaining water with a high degree of purity by using reverse osmosis

    Directory of Open Access Journals (Sweden)

    Nicolae Chirilă

    2011-12-01

    Full Text Available In this paper, we used the method of reverse osmosis in order to obtain water with a high degree of purity. For this aim, we used the TKA 20-120ECO device. We completed physic-chemical determinations for the water of supply, as well as for the water obtained after the osmosis process. The results that we obtained are relevant and interesting.

  5. Experimental methodology for obtaining sound absorption coefficients

    Directory of Open Access Journals (Sweden)

    Carlos A. Macía M

    2011-07-01

    Full Text Available Objective: the authors propose a new methodology for estimating sound absorption coefficients using genetic algorithms. Methodology: sound waves are generated and conducted along a rectangular silencer. The waves are then attenuated by the absorbing material covering the silencer’s walls. The attenuated sound pressure level is used in a genetic algorithm-based search to find the parameters of the proposed attenuation expressions that include geometric factors, the wavelength and the absorption coefficient. Results: a variety of adjusted mathematical models were found that make it possible to estimate the absorption coefficients based on the characteristics of a rectangular silencer used for measuring the attenuation of the noise that passes through it. Conclusions: this methodology makes it possible to obtain the absorption coefficients of new materials in a cheap and simple manner. Although these coefficients might be slightly different from those obtained through other methodologies, they provide solutions within the engineering accuracy ranges that are used for designing noise control systems.

  6. Lifetime obtained by ion beam assisted deposition

    Energy Technology Data Exchange (ETDEWEB)

    Chakaroun, M. [XLIM-MINACOM-UMR 6172, Faculte des Sciences et Techniques, 123 av. Albert Thomas, 87060 Limoges cedex (France); Antony, R. [XLIM-MINACOM-UMR 6172, Faculte des Sciences et Techniques, 123 av. Albert Thomas, 87060 Limoges cedex (France)], E-mail: remi.antony@unilim.fr; Taillepierre, P.; Moliton, A. [XLIM-MINACOM-UMR 6172, Faculte des Sciences et Techniques, 123 av. Albert Thomas, 87060 Limoges cedex (France)

    2007-09-15

    We have fabricated green organic light-emitting diodes based on tris-(8-hydroxyquinoline)aluminium (Alq3) thin films. In order to favor the charge carriers transport from the anode, we have deposited a N,N'-diphenyl-N,N'-bis (3-methylphenyl)-1,1'-diphenyl-4,4'-diamine (TPD) layer (hole transport layer) on a ITO anode. Cathode is obtained with a calcium layer covered with a silver layer. This silver layer is used to protect the other layers against oxygen during the OLED use. All the depositions are performed under vacuum and the devices are not exposed to air during their realisation. In order to improve the silver layer characteristics, we have realized this layer with the ion beam assisted deposition process. The aim of this process is to densify the layer and then reduce the permeation of H{sub 2}O and O{sub 2}. We have used argon ions to assist the silver deposition. All the OLEDs optoelectronic characterizations (I = f(V), L = f(V)) are performed in the ambient air. We compare the results obtained with the assisted layer with those obtained with a classical cathode realized by thermal unassisted evaporation. We have realized lifetime measurements in the ambient air and we discuss about the assisted layer influence on the OLEDs performances.

  7. Results of environmental radiation monitoring and meteorology measurements (material prepared for obtaining the licence for RA reactor experimental operation)

    International Nuclear Information System (INIS)

    1980-10-01

    According to the demands for obtaining the licence for restarting the Ra reactor and the experimental operation this document includes the radiation monitoring measured data in the working space and environment of the RA reactor, i.e. Boris Kidric Institute. The meteorology measured data are included as well. All the measurements are performed according to the radiation protection program applied actually from the first reactor start-up at the end of 1959 [sr

  8. Evaluation of marginal and internal gaps of metal ceramic crowns obtained from conventional impressions and casting techniques with those obtained from digital techniques

    Directory of Open Access Journals (Sweden)

    Rathika Rai

    2017-01-01

    Full Text Available Background: Accuracy in fit of cast metal restoration has always remained as one of the primary factors in determining the success of the restoration. A well-fitting restoration needs to be accurate both along its margin and with regard to its internal surface. Aim: The aim of the study is to evaluate the marginal fit of metal ceramic crowns obtained by conventional inlay casting wax pattern using conventional impression with the metal ceramic crowns obtained by computer-aided design and computer-aided manufacturing (CAD/CAM technique using direct and indirect optical scanning. Materials and Methods: This in vitro study on preformed custom-made stainless steel models with former assembly that resembles prepared tooth surfaces of standardized dimensions comprised three groups: the first group included ten samples of metal ceramic crowns fabricated with conventional technique, the second group included CAD/CAM-milled direct metal laser sintering (DMLS crowns using indirect scanning, and the third group included DMLS crowns fabricated by direct scanning of the stainless steel model. The vertical marginal gap and the internal gap were evaluated with the stereomicroscope (Zoomstar 4; post hoc Turkey's test was used for statistical analysis. One-way analysis of variance method was used to compare the mean values. Results and Conclusion: Metal ceramic crowns obtained from direct optical scanning showed the least marginal and internal gap when compared to the castings obtained from inlay casting wax and indirect optical scanning. Indirect and direct optical scanning had yielded results within clinically acceptable range.

  9. High purity zirconium obtainment through the iodine compounds transport method

    International Nuclear Information System (INIS)

    Bolcich, J.C.; Zuzek, E.; Dutrus, S.M.; Corso, H.L.

    1987-01-01

    This paper describes the experimental method and the equipment designed, constructed and actually applied for the high purity zirconium obtainment from a zirconium sponge of the nuclear type. The mechanism of purification is based on the impure metal attack with gaseous iodine (at 200 deg C) to obtain zirconium tetra iodine as main product which is then transformed into a pure zirconium base (at 1000-1300 deg C), precipitating the metallic zirconium and releasing the gaseous iodine. From the first experiences carried out, pure zirconium has been obtained from an initial filament of 0.5 mm of diameter as well as wires up to 2.5 mm of diameter. This work presents the results from the studies and analysis made to characterize the material obtained. Finally, the refining methods to which the zirconium produced may be submitted so as to optimize the final purity are discussed. (Author)

  10. Optimization in obtaining PLA nanofibers/nHAP for pharmaceuticals release

    International Nuclear Information System (INIS)

    Becaro, A.A.; Paris, E.C.; Mattoso, L.H.C.; Sciena, C.R.; Malafatti, J.D.

    2016-01-01

    Hydroxyapatite (HAP) belongs to the family of calcium apatites. In nanometric form (nHAP) can be used as a drug carrier. The objective was to improve PLA nanofibers with nHAP insert for use in drug delivery. nHAP were obtained by coprecipitation method and characterized by XRD and TEM techniques. PLA fibers (10%) and 5% nHAP were obtained at a distance of 6 cm and flow rate of 0.1, 0.3 and 0.5 ml h"-"1, and characterized by SEM. The nHAP were single phase with rod shape, rounded tip and from 10 to 20 nm in diameter. The fibers obtained from pure PLA had to be more porous than in the presence of HAP. The diameters ranged from 0.2 to 2.4 micrometers. Among the fibers obtained that showed the best result was to flow 0.3 ml h"-"1. (author)

  11. Operating results obtained in a nuclear power plant with a sensor surveillance prototype

    International Nuclear Information System (INIS)

    Jacquot, J.P.; Poujol, A.; Beaubatie, J.; Ciaramitaro, W.

    1983-03-01

    Surveillance methods have been validated and specific equipment have been built to measure the response time of sensors from a nuclear power plant protection channel. The reason of the choice of this parameter is twofold: the sensor response time is representative of the sensor physical status and is also part of the overall channel response time. Two surveillance methods are used: noise analysis (by AR or PSD modeling), and loop current step response (for resistance thermometer detectors only). The methods were validated on test facilities and on nuclear power plants. Two test equipments were built and tested on plants. Results are represented and conclusions are drawn on the feasibility of such methods for sensor surveillance [fr

  12. The effects of metal ion PCR inhibitors on results obtained with the Quantifiler(®) Human DNA Quantification Kit.

    Science.gov (United States)

    Combs, Laura Gaydosh; Warren, Joseph E; Huynh, Vivian; Castaneda, Joanna; Golden, Teresa D; Roby, Rhonda K

    2015-11-01

    Forensic DNA samples may include the presence of PCR inhibitors, even after extraction and purification. Studies have demonstrated that metal ions, co-purified at specific concentrations, inhibit DNA amplifications. Metal ions are endogenous to sample types, such as bone, and can be introduced from environmental sources. In order to examine the effect of metal ions as PCR inhibitors during quantitative real-time PCR, 2800 M DNA was treated with 0.0025-18.750 mM concentrations of aluminum, calcium, copper, iron, nickel, and lead. DNA samples, both untreated and metal-treated, were quantified using the Quantifiler(®) Human DNA Quantification Kit. Quantification cycle (Cq) values for the Quantifiler(®) Human DNA and internal PCR control (IPC) assays were measured and the estimated concentrations of human DNA were obtained. Comparisons were conducted between metal-treated and control DNA samples to determine the accuracy of the quantification estimates and to test the efficacy of the IPC inhibition detection. This kit is most resistant to the presence of calcium as compared to all metals tested; the maximum concentration tested does not affect the amplification of the IPC or quantification of the sample. This kit is most sensitive to the presence of aluminum; concentrations greater than 0.0750 mM negatively affected the quantification, although the IPC assay accurately assessed the presence of PCR inhibition. The Quantifiler(®) Human DNA Quantification Kit accurately quantifies human DNA in the presence of 0.5000 mM copper, iron, nickel, and lead; however, the IPC does not indicate the presence of PCR inhibition at this concentration of these metals. Unexpectedly, estimates of DNA quantity in samples treated with 18.750 mM copper yielded values in excess of the actual concentration of DNA in the samples; fluorescence spectroscopy experiments indicated this increase was not a direct interaction between the copper metal and 6-FAM dye used to label the probe that

  13. Nanocrystalline and ultrafine grain copper obtained by mechanical attrition

    Directory of Open Access Journals (Sweden)

    Rodolfo Rodríguez Baracaldo

    2010-01-01

    Full Text Available This article presents a method for the sample preparation and characterisation of bulk copper having grain size lower than 1 μm (ultra-fine grain and lower than 100 nm grain size (nanocrystalline. Copper is initially manufactured by a milling/alloying me- chanical method thereby obtaining a powder having a nanocrystalline structure which is then consolidated through a process of warm compaction at high pressure. Microstructural characterisation of bulk copper samples showed the evolution of grain size during all stages involved in obtaining it. The results led to determining the necessary conditions for achieving a wide range of grain sizes. Mechanical characterisation indicated an increase in microhardness to values of around 3.40 GPa for unconsolida- ted nanocrystalline powder. Compressivee strength was increased by reducing the grain size, thereby obtaining an elastic limit of 650 MPa for consolidated copper having a ~ 62 nm grain size.

  14. Biodegradable Polyelectrolyte Obtained by Radiation Polymerization

    International Nuclear Information System (INIS)

    Craciun, G.; Martin, D.; Manaila, E.; Nemtanu, M.; Brasoveanu, M.; Ighigeanu, D.

    2009-01-01

    Poly electrolytes are water-soluble polymers carrying ionic charge along the polymer chain. Depending upon the charge, these polymers are anionic or cationic. The inherent solid - liquid separating efficiency makes these poly electrolytes a unique class of polymers which find extensive application in potable water, industrial raw and process water, municipal sewage treatment, mineral processing and metallurgy, oil drilling and recovery, etc. Also, due to their ability to produce advanced induced coagulation, a considerable amount of bacteria and viruses are precipitated together with the suspended solids. Especially the acrylamide polymers are very efficacious for water treatment but acrylamide is a toxic monomer and therefore their use are governed by international standards that provide the residual acrylamide monomer content (RAMC) in them be less than 0.05%. Under these circumstances our attention was focused on the following research steps that are presented in this paper: 1) Preparation of a special class of poly electrolytes, named Pn, with very low RAMC values, based on electron beam (EB), microwave (MW) and EB + MW induced co-polymerization of aqueous solutions containing appropriate mixtures of acrylamide (AMD) and acrylic acid (AA) monomers (AMD - AA co-polymers). The Pn were obtained by radiation technology with very small RAMC (under 0.01%) as well as in a wide range of molecular weights and charge densities. Very low AMD monomer content of Pn is due to the major advantages of radiation induced polymerization in aqueous solution containing monomers. Due to water presence in the EB irradiated system, irradiated water radicals facilitate the polymerization process and increase rate and level of monomers conversion in co-polymers. Also, once again, by the presence of water, which absorbs MW energy very strongly, the MW polymerization reaction rate is much enhanced resulting in a reaction time about 50-100 times lowers than by conventional heating. Also

  15. Obtaining porous silicon suitable for sensor technology using MacEtch nonelectrolytic etching

    Directory of Open Access Journals (Sweden)

    Iatsunskyi I. R.

    2013-12-01

    Full Text Available The author suggests to use the etching method MacEtch (metal-assisted chemical etching for production of micro- and nanostructures of porous silicon. The paper presents research results on the morphology structures obtained at different parameters of deposition and etching processes. The research has shown that, depending on the parameters of deposition of silver particles and silicon wafers etching, the obtained surface morphology may be different. There may be both individual crater-like pores and developed porous or macroporous surface. These results indicate that the MacEtch etching is a promising method for obtaining micro-porous silicon nanostructures suitable for effective use in gas sensors and biological object sensors.

  16. Comparison of Hematologic and Biochemical Test Results in Blood Samples Obtained by Jugular Venipuncture Versus Nail Clip in Moluccan Cockatoos (Cacatua moluccensis).

    Science.gov (United States)

    Bennett, Tracy D; Lejnieks, Daniel V; Koepke, Hoyt; Grimson, Fiona; Szucs, Jennifer; Omaits, Kerri; Lane, Rosalie

    2015-12-01

    In birds, blood samples are often collected from the jugular, medial metatarsal, and basilic vein. Samples are sometimes collected by toe nail clip, but concerns to avoid drawing blood from the nail include pain after nail clips for blood collection, potential differences in complete blood count (CBC) results, and potential contamination with uric acid values. To compare differences in biochemical and hematologic values in blood samples obtained by jugular venipuncture versus toenail clip, blood samples were collected from Moluccan cockatoos (Cacatua moluccensis) (N = 23) and sent to a commercial laboratory for routine CBCs and serum biochemical analysis. Results showed good agreement between venipuncture and nail clip blood samples in red blood cell count, packed cell volume, heterophil count and percentage, lymphocyte count and percentage, aspartate aminotransferase, chloride, creatine phosphokinase, glucose, lactate dehydrogenase, total protein, and uric acid values. Constant bias was found in values of bile acids, cholesterol, and hemoglobin. Proportional bias toward higher values in the jugular sample were found in total white blood cell (WBC) count and inorganic phosphorus. Serum calcium plots revealed a proportional bias toward higher values in the toe nail blood when values were increased. Results suggest some differences in WBC count, bile acids, calcium, cholesterol, hemoglobin, and phosphorus values between blood samples collected by jugular venipuncture and samples collected by toe nail clip, but the differences are mostly minor and, with the possible exception of inorganic phosphorus and marginally elevated or very low WBC counts, are unlikely to affect the use or interpretation of the avian blood panel.

  17. Histology of periapical lesions obtained during apical surgery.

    Science.gov (United States)

    Schulz, Malte; von Arx, Thomas; Altermatt, Hans Jörg; Bosshardt, Dieter

    2009-05-01

    The aim of this was to evaluate the histology of periapical lesions in teeth treated with periapical surgery. After root-end resection, the root tip was removed together with the periapical pathological tissue. Histologic sectioning was performed on calcified specimens embedded in methylmethacrylate (MMA) and on demineralized specimens embedded in LR White (Fluka, Buchs, Switzerland). The samples were evaluated with light and transmission electron microscopy (TEM). The histologic findings were classified into periapical abscesses, granulomas, or cystic lesions (true or pocket cysts). The final material comprised 70% granulomas, 23% cysts and 5% abscesses, 1% scar tissues, and 1% keratocysts. Six of 125 samples could not be used. The cystic lesions could not be subdivided into pocket or true cysts. All cysts had an epithelium-lined cavity, two of them with cilia-lined epithelium. These results show the high incidence of periapical granulomas among periapical lesions obtained during apical surgery. Periapical abscesses were a rare occasion. The histologic findings from samples obtained during apical surgery may differ from findings obtained by teeth extractions. A determination between pocket and true apical cysts is hardly possible when collecting samples by apical surgery.

  18. Dependency of Delayed Hydride Crack Velocity on the Direction of an Approach to Test Temperatures in Zirconium Alloys

    International Nuclear Information System (INIS)

    Kim, Young Suk; Kim, Kang Soo; Im, Kyung Soo; Ahn, Sang Bok; Cheong, Yong Moo

    2005-01-01

    crack tip, leading to the transfer of hydrogen from the bulk region to the crack tip. In short, this is the driving force for the DHC of zirconium alloys upon an approach to the test temperature by a heating. It should be noted that Kim's proposition that the terminal solid solubility for dissolution (TSSD) of the γ-hydride is higher than that of the δ-hydride is based on the experimental results reported by Cann and Mishra. The objective of this study is to demonstrate if the water-quenched Zr-2.5Nb will have the DHC crack growth even at the temperatures above 180 .deg. C where the furnace-cooled Zr-2.5Nb will not. This experiment will provide supportive evidence that the TSSD of γ- hydrides is higher than that of δ-hydrides and furthermore, it will confirm the feasibility of Kim's DHC model

  19. Dependency of Delayed Hydride Crack Velocity on the Direction of an Approach to Test Temperatures in Zirconium Alloys

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Young Suk; Kim, Kang Soo; Im, Kyung Soo; Ahn, Sang Bok; Cheong, Yong Moo [Korea Atomic Energy Research Institute, Taejon (Korea, Republic of)

    2005-07-01

    hydrogen concentration or .C between the bulk and the crack tip, leading to the transfer of hydrogen from the bulk region to the crack tip. In short, this is the driving force for the DHC of zirconium alloys upon an approach to the test temperature by a heating. It should be noted that Kim's proposition that the terminal solid solubility for dissolution (TSSD) of the {gamma}-hydride is higher than that of the {delta}-hydride is based on the experimental results reported by Cann and Mishra. The objective of this study is to demonstrate if the water-quenched Zr-2.5Nb will have the DHC crack growth even at the temperatures above 180 .deg. C where the furnace-cooled Zr-2.5Nb will not. This experiment will provide supportive evidence that the TSSD of {gamma}- hydrides is higher than that of {delta}-hydrides and furthermore, it will confirm the feasibility of Kim's DHC model.

  20. Evaluation of agreement between temporal series obtained from electrocardiogram and pulse wave.

    Science.gov (United States)

    Leikan, GM; Rossi, E.; Sanz, MCuadra; Delisle Rodríguez, D.; Mántaras, MC; Nicolet, J.; Zapata, D.; Lapyckyj, I.; Siri, L. Nicola; Perrone, MS

    2016-04-01

    Heart rate variability allows to study the cardiovascular autonomic nervous system modulation. Usually, this signal is obtained from the electrocardiogram (ECG). A simpler method for recording the pulse wave (PW) is by means of finger photoplethysmography (PPG), which also provides information about the duration of the cardiac cycle. In this study, the correlation and agreement between the time series of the intervals between heartbeats obtained from the ECG with those obtained from the PPG, were studied. Signals analyzed were obtained from young, healthy and resting subjects. For statistical analysis, the Pearson correlation coefficient and the Bland and Altman limits of agreement were used. Results show that the time series constructed from the PW would not replace the ones obtained from ECG.

  1. Thermoluminescence properties of zinc oxide obtained by solution combustion synthesis

    Energy Technology Data Exchange (ETDEWEB)

    Orante B, V. R.; Escobar O, F. M.; Cruz V, C. [Universidad de Sonora, Departamento de Investigacion en Polimeros y Materiales, Apdo. Postal 130, 83000 Hermosillo, Sonora (Mexico); Bernal, R., E-mail: victor.orante@polimeros.uson.mx [Universidad de Sonora, Departamento de Investigacion en Fisica, Apdo. Postal 5-088, 83190 Hermosillo, Sonora (Mexico)

    2014-08-15

    High-dose thermoluminescence dosimetry properties of novel zinc oxide obtained by solution combustion synthesis in a glycine-nitrate process, with a non-stoichiometric value of the elemental stoichiometric coefficient (Φ{sub c}) are presented in this work. Zn O powder samples obtained were annealed afterwards at 900 grades C during 2 h in air. Sintered particles of sizes between ∼ 0.5 and ∼ 2 μm were obtained, according to scanning electron microscopy results. X-ray diffraction indicates the presence of the hexagonal phase of Zn O for the powder samples obtained, before and after thermal annealing, without any remaining nitrate peaks observed. Thermoluminescence glow curves of Zn O obtained after being exposed to beta radiation consists of two maxima; one located at ∼ 149 grades C and another at ∼ 308 grades C, being the latter the dosimetric component of the curve. Dosimetric characterization of non-stoichiometric zinc oxide provided experimental evidence like asymptotic behavior of the Tl signal fading for times greater than 16 h between irradiation and the corresponding Tl readout, as well as the linear behaviour of the dose response without saturation in the dose interval studied (from 12.5 up to 400 Gy). Such characteristics place Zn O phosphors obtained in this work as a promising material for high-dose radiation dosimetry applications (e.g., radiotherapy and food industry). (author)

  2. Thermoluminescence properties of zinc oxide obtained by solution combustion synthesis

    International Nuclear Information System (INIS)

    Orante B, V. R.; Escobar O, F. M.; Cruz V, C.; Bernal, R.

    2014-08-01

    High-dose thermoluminescence dosimetry properties of novel zinc oxide obtained by solution combustion synthesis in a glycine-nitrate process, with a non-stoichiometric value of the elemental stoichiometric coefficient (Φ c ) are presented in this work. Zn O powder samples obtained were annealed afterwards at 900 grades C during 2 h in air. Sintered particles of sizes between ∼ 0.5 and ∼ 2 μm were obtained, according to scanning electron microscopy results. X-ray diffraction indicates the presence of the hexagonal phase of Zn O for the powder samples obtained, before and after thermal annealing, without any remaining nitrate peaks observed. Thermoluminescence glow curves of Zn O obtained after being exposed to beta radiation consists of two maxima; one located at ∼ 149 grades C and another at ∼ 308 grades C, being the latter the dosimetric component of the curve. Dosimetric characterization of non-stoichiometric zinc oxide provided experimental evidence like asymptotic behavior of the Tl signal fading for times greater than 16 h between irradiation and the corresponding Tl readout, as well as the linear behaviour of the dose response without saturation in the dose interval studied (from 12.5 up to 400 Gy). Such characteristics place Zn O phosphors obtained in this work as a promising material for high-dose radiation dosimetry applications (e.g., radiotherapy and food industry). (author)

  3. Radiochemical schemes of obtaining 89Sr and 90Y radionuclides

    International Nuclear Information System (INIS)

    Usarov, Z. O.

    2010-03-01

    Key words: strontium-89, yttrium-90, extraction and extraction-chromatographic purification of radionuclides, radiopharmaceuticals. Subjects of research: strontium-89 and yttrium-90 radionuclides and their chloride forms. Purpose of work is developing of radiochemical technologies on obtaining of 89 Sr and 90 Y on the WWR-SM reactor with high radionuclide purity. Methods of research: extraction and extraction-chromatographic methods of radionuclides separation, beta- and gamma-spectrometric methods of activity measuring. The results obtained and their novelty: Were determined the conformity to laws of Y and Sr distribution in two-phase systems TBP-HNO 3 , TBP-NH 4 NO 3 , TBP-HCI, HDEHP-NO 3 , HDEHP-NH 4 NO 3 and HDEHP-HCI. Were determined the conformity to laws of Y and Sr distribution in systems with craun ethers DB-18K-6 and DTBDB-18K-6 from water solutions of HNO 3 . Radiochemical technologies on obtaining of 89 Sr and 90 Y radionuclides including radiochemical process of yttrium target with using the systems TBP-HNO 3 and HDEHP/Teflone were developed. Practical value: the radiochemical technology of obtaining 89 Sr with high radionuclide purity was developed. The method of preparation a chloride compound of 89 SrCl 2 which is used as a drug form for preparation of 89 Sr- 'Metastron' was developed. The relatively simple method of on the way obtaining 90 Y in the reactor with high radionuclidic purity that is useful for follow using in medical practice was offered. Degree of embed and economic effectivity: the developed technologies have approbation in manufacturing conditions in Radiopreparat Enterprise of INP AS RU and were offered for receiving of domestic preparations against of import foreign analogues. The statement about using the invention by obtained patent is attached to dissertation. Field of application: the received results will be introduced in manufacture at Radiopreparat Enterprise of INP AS RU for receiving of domestic preparations

  4. Obtaining shale oil suitable for lighting

    Energy Technology Data Exchange (ETDEWEB)

    Giraudel, M

    1851-11-12

    Treats with sulphuric acid and then with soda, obtaining 57 per cent of products suitable for lighting in place of the usual 35 to 40 per cent as obtained by present processes. The product has a less disagreeable odor.

  5. Carbon nanofibers obtained from electrospinning process

    Science.gov (United States)

    Bovi de Oliveira, Juliana; Müller Guerrini, Lília; Sizuka Oishi, Silvia; Rogerio de Oliveira Hein, Luis; dos Santos Conejo, Luíza; Cerqueira Rezende, Mirabel; Cocchieri Botelho, Edson

    2018-02-01

    In recent years, reinforcements consisting of carbon nanostructures, such as carbon nanotubes, fullerenes, graphenes, and carbon nanofibers have received significant attention due mainly to their chemical inertness and good mechanical, electrical and thermal properties. Since carbon nanofibers comprise a continuous reinforcing with high specific surface area, associated with the fact that they can be obtained at a low cost and in a large amount, they have shown to be advantageous compared to traditional carbon nanotubes. The main objective of this work is the processing of carbon nanofibers, using polyacrylonitrile (PAN) as a precursor, obtained by the electrospinning process via polymer solution, with subsequent use for airspace applications as reinforcement in polymer composites. In this work, firstly PAN nanofibers were produced by electrospinning with diameters in the range of (375 ± 85) nm, using a dimethylformamide solution. Using a furnace, the PAN nanofiber was converted into carbon nanofiber. Morphologies and structures of PAN and carbon nanofibers were investigated by scanning electron microscopy, Raman Spectroscopy, thermogravimetric analyses and differential scanning calorimeter. The resulting residual weight after carbonization was approximately 38% in weight, with a diameters reduction of 50%, and the same showed a carbon yield of 25%. From the analysis of the crystalline structure of the carbonized material, it was found that the material presented a disordered structure.

  6. Nanostructured synthetic carbons obtained by pyrolysis of spherical acrylonitrile/divinylbenzene copolymers.

    Directory of Open Access Journals (Sweden)

    Danish J Malik

    Full Text Available Novel carbon materials have been prepared by the carbonization of acrylonitrile (AN/divinylbenzene (DVB suspension porous copolymers having nominal crosslinking degrees in the range of 30-70% and obtained in the presence of various amounts of porogens. The carbons were obtained by pre-oxidation of AN/DVB copolymers at 250-350°C in air followed by pyrolysis at 850°C in an N(2 atmosphere. Both processes were carried out in one furnace and the resulting material needed no further activation. Resulting materials were characterized by XPS and low temperature nitrogen adsorption/desorption. It was found that maximum pyrolysis yield was ca. 50% depending on the oxidation conditions but almost independent of the crosslinking degree of the polymers. Porous structure of the carbons was characterized for the presence of micropores and macropores, when obtained from highly crosslinked polymers or polymers oxidized at 350°C and meso- and macropores in all other cases. The latter pores are prevailing in the structure of carbons obtained from less porous AN/DVB resins. Specific surface area (BET of polymer derived carbons can vary between 440 m(2/g and 250 m(2/g depending on the amount of porogen used in the synthesis of the AN/DVB polymeric precursors.

  7. Analysis of the fuel influence in obtaining HAp by combustion reaction

    International Nuclear Information System (INIS)

    Santos, T.L.; Leite, A.M.D.; Viana, K.M.S.

    2016-01-01

    The search for new materials for biomedical applications has led to investigation of the calcium phosphate bioceramics, and in particular hydroxyapatite (HAp), being a material similar to bone tissue, with excellent biocompatibility and high osteoconduction, enabling bone regeneration which allows the use at implants and prostheses. The synthesis of the nanometric HAp by combustion reaction enables obtaining the nanometric HAp with a more similar structure biological apatite as possible. This work aims to synthesize HAp by combustion reaction using two different routes of synthesis, first, using urea as fuel and the second using glycine, after this, evaluate the influence of fuels used in the microstructure of the hydroxyapatite obtained. The HAp obtained was characterized by: XRD, FTIR and SEM. Through analysis of the results, there is the synthesis conditions used that glycine has performed more favorable to obtaining HAp. (author)

  8. Method to obtain platelet-rich plasma from rabbits (Oryctolagus cuniculus

    Directory of Open Access Journals (Sweden)

    Josiane M. Pazzini

    2016-01-01

    Full Text Available Abstract: Platelet-rich plasma (PRP is a product easy and inxpesnsive, and stands out to for its growth factors in tissue repair. To obtain PRP, centrifugation of whole blood is made with specific time and gravitational forces. Thus, the present work aimed to study a method of double centrifugation to obtain PRP in order to evaluate the effective increase of platelet concentration in the final product, the preparation of PRP gel, and to optimize preparation time of the final sample. Fifteen female White New Zealand rabbits underwent blood sampling for the preparation of PRP. Samples were separated in two sterile tubes containing sodium citrate. Tubes were submitted to the double centrifugation protocol, with lid closed and 1600 revolutions per minute (rpm for 10 minutes, resulting in the separation of red blood cells, plasma with platelets and leucocytes. After were opened and plasma was pipetted and transferred into another sterile tube. Plasma was centrifuged again at 2000rpm for 10 minutes; as a result it was split into two parts: on the top, consisting of platelet-poor plasma (PPP and at the bottom of the platelet button. Part of the PPP was discarded so that only 1ml remained in the tube along with the platelet button. This material was gently agitated to promote platelets resuspension and activated when added 0.3ml of calcium gluconate, resulting in PRP gel. Double centrifugation protocol was able to make platelet concentration 3 times higher in relation to the initial blood sample. The volume of calcium gluconate used for platelet activation was 0.3ml, and was sufficient to coagulate the sample. Coagulation time ranged from 8 to 20 minutes, with an average of 17.6 minutes. Therefore, time of blood centrifugation until to obtain PRP gel took only 40 minutes. It was concluded that PRP was successfully obtained by double centrifugation protocol, which is able to increase the platelet concentration in the sample compared with whole blood

  9. 38 CFR 21.5725 - Obtaining benefits.

    Science.gov (United States)

    2010-07-01

    ... 38 Pensions, Bonuses, and Veterans' Relief 2 2010-07-01 2010-07-01 false Obtaining benefits. 21... benefits. (a) Actions required of the individual. In order to obtain benefits under the educational assistance and subsistence allowance program, an individual must— (1) File a claim for benefits with VA, and...

  10. [Lymphoscintigrams with anatomical landmarks obtained with vector graphics].

    Science.gov (United States)

    Rubini, Giuseppe; Antonica, Filippo; Renna, Maria Antonia; Ferrari, Cristina; Iuele, Francesca; Stabile Ianora, Antonio Amato; Losco, Matteo; Niccoli Asabella, Artor

    2012-11-01

    Nuclear medicine images are difficult to interpret because they do not include anatomical details. The aim of this study was to obtain lymphoscintigrams with anatomical landmarks that could be easily interpreted by General Physicians. Traditional lymphoscintigrams were processed with Adobe© Photoshop® CS6 and converted into vector images created by Illustrator®. The combination with a silhouette vector improved image interpretation, without resulting in longer radiation exposure or acquisition times.

  11. Biochemical Characterization of Lipases Obtained from Acinetobacter psychrotolerans Strains

    Directory of Open Access Journals (Sweden)

    Şule SEREN

    2017-12-01

    Full Text Available In this study, extracellular lipases obtained from Acinetobacter psychrotolerans strains (Xg1 and Xg2 were characterized. The effects of varying pH values (3.0-10.0 and various temperatures (10-90 °C on lipase activities were examined. Also the effects of different metal ions, organic solvents and detergents on lipases were studied. The extracellular crude lipases were concentrated using ultrafiltration. Zymogram analysis of these lipases was performed. Lipases exhibited maximum activity at pH 8 and 30 °C.  While lipase obtained from the Xg1 strain exhibited the highest stability in the presence of various organic solvents, including hexane, ethyl acetate, chloroform and N,N dietil formamide, lipase obtained from the Xg2 strain was sensitive in the presence of isopropanol, acetonitrile, and butan-1-ol. The lipases of the Xg1 and Xg2 strains were inhibited in the presence of Cu2+ and Zn2+. Also, the lipase of the Xg1 strain was inhibited in the presence of Fe3+. In the presence of EDTA, the lipase activities of the Xg1 and Xg2 strains were partially inhibited. In presence of SDS, they were exactly inhibited. According to the zymogram results, the molecular weights of the lipases obtained from the Acinetobacter psychrotolerans Xg1 and Xg2 strains have been found approximately 37 and 30 kDa, respectively.

  12. Improved dielectric functions in metallic films obtained via template stripping

    Science.gov (United States)

    Hyuk Park, Jong; Nagpal, Prashant; Oh, Sang-Hyun; Norris, David J.

    2012-02-01

    We compare the dielectric functions of silver interfaces obtained via thermal evaporation with those obtained with template stripping. Ellipsometry measurements show that the smoother template-stripped surfaces exhibit effective dielectric functions with a more negative real component and a smaller imaginary component, implying higher conductivity and less energy loss, respectively. These results agree with the relation between dielectric function and surface roughness derived from combining the effective-medium model and the Drude-Lorentz model. The improvement in the effective dielectric properties shows that metallic films prepared via template stripping can be favorable for applications in electronics, nanophotonics, and plasmonics.

  13. Obtaining hydroxyapatite coatings on titanium by the biomimetic method

    International Nuclear Information System (INIS)

    Paz, A.; Martin, Y.; Pazos, L. M.; Parodi, M. B.; Ybarra, G. O.; Gonzalez, J. E.

    2011-01-01

    In this work, a study about the deposition of hydroxyapatite on a titanium substrate employing the biomimetic method is presented. A solution with high content of calcium and phosphorus (SCS) was used. In addition, activation of titanium with hydrogen peroxide and hydrochloric acid and a subsequent heat treatment was performed. The characterization of materials used and the coating obtained was carried out by Infrared Spectroscopy (FT-IR), X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Spectroscopy (EDX). As a result of the activation processes a hydrated titanium oxide was formed. On the active surface, a coating of hydroxyapatite was obtained after a period of 24 h, which has a thickness of about 2-4 μm. (Author) 21 refs.

  14. Associative self-anchoring interacts with obtainability of chosen objects

    Directory of Open Access Journals (Sweden)

    Dean eMobbs

    2016-01-01

    Full Text Available While there is evidence that implicit self-esteem transfers to chosen objects (associative self-anchoring, it is still unknown whether this phenomenon extends to explicit self-esteem. Moreover, whether the knowledge that these objects might belong to the self in the future or not affects the evaluation of these objects has yet to be tested. Here, we demonstrate that evaluations of chosen objects are further enhanced when they are obtainable as compared to when they are not in participants with high explicit self-esteem, whereas participants with low explicit self-esteem exhibit the opposite pattern. These findings extend previous results and shed new light on the role of self-esteem in altering preferences for chosen objects depending on their obtainability.

  15. Treating shale oil to obtain sulfonates

    Energy Technology Data Exchange (ETDEWEB)

    Schaeffer, H

    1921-01-21

    The process shows as its principal characteristics: (1) treating the oil with chlorsulfonic acid at a temperature of about 100/sup 0/C; (2) the transformation of the sulfonic acid obtained into salts; (3) as new industrial products, the sulfonates obtained and their industrial application as disinfectants for hides and wood.

  16. Theoretical galactic cosmic ray electron spectrum obtained for sources of varying geometry

    International Nuclear Information System (INIS)

    Cohen, M.E.

    1969-01-01

    Jokipii and Meyer have recently obtained an electron density energy spectrum of the cosmic rays, originating in the Galaxy, using integral solutions of the steady state transfer equations, by considering a circular cylindric galactic disc as source and approximating the resulting fourth order integral. In this report, we present general results, obtained by using an arbitrary circular cylindric source, without restricting ourselves to the galactic disc. The integrals are treated exactly. The conclusions of Jokipii and Meyer form special cases of these results. We also obtain an exponential energy variation which, at the moment, is not observed experimentally. The second part of this work deals with more complicated, but perhaps more realistic models of elliptic cylindric and ellipsoidal galactic disc sources. One may also note that a very large source concentrated in a very small region gives a spectrum not unlike that for a small source distributed throughout a large volume. Finally, it may be remarked that the model adopted is much less restrictive than the artificial conception of 'leakage time' followed by other workers. (author) [fr

  17. Thermoelectric generator based on composites obtained by sintering of detonation nanodiamonds

    Science.gov (United States)

    Eidelman, E. D.; Meilakhs, A. P.; Semak, B. V.; Shakhov, F. M.

    2017-11-01

    A model of a thermoelectric generator is proposed, in which composite materials obtained by sintering diamond nanoparticles are used as the main component. To increase the useful conversion of heat into electric current, it is proposed to use the effect of electron drag by ballistic phonons. To reduce the ineffective heat spread, it is proposed to use the effect of thermal resistance of the boundaries between the graphite-like and diamond-like phases of the composite. An experimental confirmation of the existence of an optimal volume ratio between graphite-like and diamond-like phases of the composite is predicted and obtained. The highest achieved value of thermoelectric coefficient in the actual structure is 80 µV K-1 (which means 20 times increase compared to that of composites not of the optimal structure), with a thermal conductivity of 50 W m-1 K-1. These results were obtained with constant electrical conductivity. The combined influence of these two effects in case of the ideal composite structure should result in an increase of the thermoelectric efficiency parameter by three orders of magnitude.

  18. Alecto - results obtained with homogeneous critical experiments on plutonium 239, uranium 235 and uranium 233

    International Nuclear Information System (INIS)

    Bruna, J.G.; Brunet, J.P.; Caizegues, R.; Clouet d'Orval, Ch.; Kremser, J.; Tellier, H.; Verriere, Ph.

    1965-01-01

    In this report are given the results of the homogeneous critical experiments ALECTO, made on plutonium 239, uranium 235 and uranium 233. After a brief description of the equipment, the critical masses for cylinders of diameters varying from 25 to 42 cm, are given and compared with other values (foreign results, criticality guide). With respect to the specific conditions of neutron reflection in the ALECTO experiments the minimal values of critical masses are: Pu239 M c = 910 ± 10 g, U235 M c = 1180 ± 12 g and U233 M c = 960 ± 10 g. Experiments relating to cross sections and constants to be used on these materials are presented. Lastly, kinetic experiments allow to compare pulsed neutron methods to fluctuation methods [fr

  19. Nanostructured Thin Films Obtained from Fischer Aminocarbene Complexes

    Directory of Open Access Journals (Sweden)

    Rosa E. Lazo-Jiménez

    2016-03-01

    Full Text Available The synthesis of four amphiphilic organometallic complexes with the general formula RC = M(CO5NH(CH215CH3, where R is a ferrocenyl 2(a-b or a phenyl 4(a-b group as a donor moiety and a Fischer carbene of chromium (0 or tungsten (0 as an acceptor group, are reported. These four push-pull systems formed Langmuir (L monolayers at the air-water interface, which were characterized by isotherms of surface pressure versus molecular area and compression/expansion cycles (hysteresis curves; Brewster angle microscopic images were also obtained. By using the Langmuir–Blodgett (LB method, molecular monolayers were transferred onto glass substrates forming Z-type multilayers. LB films were characterized through ultraviolet-visible spectroscopy, atomic force microscopy and X-ray diffraction techniques. Results indicated that films obtained from 2b complex [(Ferrocenyl(hexadecylaminemethylidene] pentacarbonyl tungsten (0 are the most stable and homogeneous; due to their properties, these materials may be incorporated into organic electronic devices.

  20. Nanostructured Thin Films Obtained from Fischer Aminocarbene Complexes

    Science.gov (United States)

    Lazo-Jiménez, Rosa E.; Ortega-Alfaro, M. Carmen; López-Cortés, José G.; Alvarez-Toledano, Cecilio; Chávez-Carvayar, José Á.; Ignés-Mullol, Jordi; González-Torres, Maykel; Carreón-Castro, Pilar

    2016-01-01

    The synthesis of four amphiphilic organometallic complexes with the general formula RC = M(CO)5NH(CH2)15CH3, where R is a ferrocenyl 2(a-b) or a phenyl 4(a-b) group as a donor moiety and a Fischer carbene of chromium (0) or tungsten (0) as an acceptor group, are reported. These four push-pull systems formed Langmuir (L) monolayers at the air-water interface, which were characterized by isotherms of surface pressure versus molecular area and compression/expansion cycles (hysteresis curves); Brewster angle microscopic images were also obtained. By using the Langmuir–Blodgett (LB) method, molecular monolayers were transferred onto glass substrates forming Z-type multilayers. LB films were characterized through ultraviolet-visible spectroscopy, atomic force microscopy and X-ray diffraction techniques. Results indicated that films obtained from 2b complex [(Ferrocenyl)(hexadecylamine)methylidene] pentacarbonyl tungsten (0) are the most stable and homogeneous; due to their properties, these materials may be incorporated into organic electronic devices. PMID:28773289

  1. Field sludge characterization obtained from inner of pipelines

    Energy Technology Data Exchange (ETDEWEB)

    Nava, N.; Sosa, E.; Alamilla, J.L. [Instituto Mexicano del Petroleo, Programa de Integridad de Ductos, Eje Central Lazaro Cardenas Norte 152, San Bartolo Atepehuacan, C.P. 07730 (Mexico); Knigth, C. [PEMEX Refinacion, Avenida Marina Nacional 329, Edificio B-2, Piso 11, C.P. 11311 (Mexico); Contreras, A. [Instituto Mexicano del Petroleo, Programa de Integridad de Ductos, Eje Central Lazaro Cardenas Norte 152, San Bartolo Atepehuacan, C.P. 07730 (Mexico)], E-mail: acontrer@imp.mx

    2009-11-15

    Physicochemical characterization of sludge obtained from refined hydrocarbons transmission pipeline was carried out through Moessbauer spectroscopy and X-ray diffraction. The Moessbauer and X-ray patterns indicate the presence of corrosion products composed of different iron oxide and sulfide phases. Hematite ({alpha}-Fe{sub 2}O{sub 3}), magnetite (Fe{sub 3}O{sub 4}), maghemite ({gamma}-Fe{sub 2}O{sub 3}), magnetic and superparamagnetic goethite ({alpha}-FeOOH), pyrrhotite (Fe{sub 1-x}S), akaganeite ({beta}-FeOOH), and lepidocrocite ({gamma}-FeOOH) were identified as corrosion products in samples obtained from pipeline transporting Magna and Premium gasoline. For diesel transmission pipeline, hematite, magnetite, and magnetic goethite were identified. Corrosion products follow a simple reaction mechanism of steel dissolution in aerated aqueous media at a near-neutral pH. Chemical composition of the corrosion products depends on H{sub 2}O and sulfur inherent in fluids (traces). These results can be useful for decision-making with regard to pipeline corrosion control.

  2. Acid formic effect in zinc coatings obtained by galvanostatic deposition

    International Nuclear Information System (INIS)

    Lopes, C.; David, M.; Souza, E.C.

    2016-01-01

    Zinc deposits obtained from electrodeposition is widely used for the purpose of protecting steel substrates from corrosion. They are generally added to Zn deposition bath many additives for improving certain characteristics of the deposit. As far as is known there is no information in literature about the effect of formic acid in corrosion resistance of a Zn deposit. Because it is an acid additive, it has the use of cyclohexylamine, in order for the electrolytic bath continue with a pH equal to the one used commercially, around 5. The main goal of this study is analyze the effect of the formic acid addition in the corrosion resistance of an Zn electrodeposition obtained by galvanostatic deposition. The results obtained by performance tests, cyclic voltammetry and X-ray diffraction showed that the formic acid addition may be promising in combating the corrosion of materials. (author)

  3. Gravity Changes and Internal Processes: Some Results Obtained from Observations at Three Volcanoes

    Science.gov (United States)

    Jentzsch, Gerhard; Weise, Adelheid; Rey, Carlos; Gerstenecker, Carl

    Temporal gravity changes provide information about mass and/or density variations within and below the volcano edifice. Three active volcanoes have been under investigation; each of them related to a plate boundary: Mayon/Luzon/Philippines, Merapi/Java/Indonesia, and Galeras/Colombia. The observed gravity changes are smaller than previously expected but significant. For the three volcanoes under investigation, and within the observation period, mainly the increase of gravity is observed, ranging from 1,000 nm-2 to 1,600 nms-2. Unexpectedly, the gravity increase is confined to a rather small area with radii of 5 to 8 km around the summit. At Mayon and Merapi the parallel GPS measurements yield no significant elevation changes. This is crucial for the interpretation, as the internal pressure variations do not lead to significant deformation at the surface. Thus the classical Mogi-model for a shallow extending magma reservoir cannot apply. To confine the possible models, the attraction due to changes of groundwater level or soil moisture is estimated along the slope of Merapi exemplarily by 2-D modelling. Mass redistribution or density changes were evaluated within the vent as well as deeper fluid processes to explain the gravity variations; the results are compared to the model incorporating the additional effect of elastic deformation.

  4. Application of the final flotation waste for obtaining the glass-ceramic materials

    Directory of Open Access Journals (Sweden)

    Cocić Mira

    2017-01-01

    Full Text Available This work describes the investigation of the final flotation waste (FFW, originating from the RTB Bor Company (Serbia, as the main component for the production of glass-ceramic materials. The glass-ceramics was synthesized by the sintering of FFW, mixtures of FFW with basalt (10%, 20%, and 40%, and mixtures of FFW with tuff (20% and 40%. The sintering was conducted at the different temperatures and with the different time duration in order to find the optimal composition and conditions for crystallization. The increase of temperature, from 1100 to 1480°C, and sintering time, from 4 to 6h resulted in a higher content of hematite crystal in the obtained glass-ceramic (up to 44%. The glass-ceramics sintered from pure FFW (1080°C/36h has good mechanical properties, such as high propagation speed (4500 m/s and hardness (10800 MPa, as well as very good thermal stability. The glass-ceramics obtained from mixtures shows weaker mechanical properties compared to that obtained from pure FFW. The mixtures of FFW with tuff have a significantly lower bulk density compared to other obtained glass-ceramics. Our results indicate that FFW can be applied as a basis for obtaining the construction materials. [Project of the Serbian Ministry of Education, Science and Technological Development, Grant no. 176010: Composition, genesis, application, and contribution to the environmental sustainability

  5. Evaluation of cross-linked chitosan microparticles containing acyclovir obtained by spray-drying

    International Nuclear Information System (INIS)

    Stulzer, Hellen Karine; Tagliari, Monika Piazzon; Parize, Alexandre Luis; Silva, Marcos Antonio Segatto; Laranjeira, Mauro Cesar Marghetti

    2009-01-01

    The aim of this study was to obtain microparticles containing acyclovir (ACV) and chitosan cross-linked with tripolyphosphate using the spray-drying technique. The resultant system was evaluated through loading efficiency, differential scanning calorimetry (DSC), thermogravimetric analysis (TG), X-ray powder diffraction (XRPD), scanning electron microscopy (SEM), in vitro release and stability studies. The results obtained indicated that the polymer/ACV ratio influenced the final properties of the microparticles, with higher ratios giving the best encapsulation efficiency, dissolution profiles and stability. The DSC and XRPD analyses indicated that the ACV was transformed into amorphous form during the spray-drying process

  6. Photoemission in nanosecond and picosecond regimes obtained from macro and micro cathodes

    International Nuclear Information System (INIS)

    Boussoukaya, M.; Bergeret, H.; Chehab, R.; Leblond, B.; Franco, M.

    1987-03-01

    For Lasertron studies at LAL, results obtained from tests on different photocathodes are given below. Using respectively two Nd: YAG lasers (a nanosecond one and a picosecond one) we have determined the level and the intensity of pulsed photoemission and the photoelectric yield in UV, green and infrared lights. We obtained a total current of more than 1 A with nanosecond width from a single W needle, and photoconversion yield of more than 1 was reached in green and UV lights. In classical pulsed photoemission, obtained photoconversion yield from LaB 6 photocathode was of about 10 -3 in higher fields

  7. THE ANALYSIS OF SEVERAL RESULTS OBTAINED BY ROMANIA IN THE FIELD OF SUSTAINABLE TRANSPORT

    Directory of Open Access Journals (Sweden)

    Perțicaș Diana Claudia

    2015-07-01

    Full Text Available We know that between the transport sector and all other branches of economy there is a strong interdependence link but also between it and the surrounding environment, being one of the most polluting sectors of activity. Transport is considered a primary field in any national economy development context, especially if we take into account its interdependence with other branches of national economy. Developing of transports also includes improving road, rail, river and sea services, as well as air transports. The objectives of the EU aim especially to modernize the transport infrastructures, be them by road, ship or by air, which would result in increasing the speed of freight transport, fluidizing traffic, attracting new foreign investors in various areas, accelerating the renewal of the auto park and decommissioning morally and physically worn vehicles which are extremely pollutant, the revival of maritime transports through Romanian ports, progressive completion of imposed performances through standards and regulations on the transport market, etc. All these objectives have as a main purpose the reducing of energy consumption, reducing transport costs as well as increasing competition in the national transport system.The development of transport has the role of stimulating public transport services and to guarantee a minimum general accessibility to public services for all citizens. Children, the elderly, disabled people or other vulnerable categories of people are not and will not be forgotten, for which certain standards set by the European Union must be respected.The present paper wishes to analyze a part of the results, either positive or negative, in the field of transports, made by our country.

  8. Seasonal differences in the subjective assessment of outdoor thermal conditions and the impact of analysis techniques on the obtained results

    Science.gov (United States)

    Kántor, Noémi; Kovács, Attila; Takács, Ágnes

    2016-11-01

    Wide research attention has been paid in the last two decades to the thermal comfort conditions of different outdoor and semi-outdoor urban spaces. Field studies were conducted in a wide range of geographical regions in order to investigate the relationship between the thermal sensation of people and thermal comfort indices. Researchers found that the original threshold values of these indices did not describe precisely the actual thermal sensation patterns of subjects, and they reported neutral temperatures that vary among nations and with time of the year. For that reason, thresholds of some objective indices were rescaled and new thermal comfort categories were defined. This research investigates the outdoor thermal perception patterns of Hungarians regarding the Physiologically Equivalent Temperature ( PET) index, based on more than 5800 questionnaires. The surveys were conducted in the city of Szeged on 78 days in spring, summer, and autumn. Various, frequently applied analysis approaches (simple descriptive technique, regression analysis, and probit models) were adopted to reveal seasonal differences in the thermal assessment of people. Thermal sensitivity and neutral temperatures were found to be significantly different, especially between summer and the two transient seasons. Challenges of international comparison are also emphasized, since the results prove that neutral temperatures obtained through different analysis techniques may be considerably different. The outcomes of this study underline the importance of the development of standard measurement and analysis methodologies in order to make future studies comprehensible, hereby facilitating the broadening of the common scientific knowledge about outdoor thermal comfort.

  9. The Escompte - Marseille 2001 International Field Experiment: Ground Based and Lidar Results Obtained At St. Chamas By The Epfl Mobile Laboratory

    Science.gov (United States)

    Balin, I.; Jimenez, R.; Simeonov, V.; Ristori, P.; Navarette, M.; van den Bergh, H.; Calpini, B.

    The assessment of the air pollution problems in term of understanding of the non- linear chemical mechanisms, the transport or the meteorological processes, and the choice of the abatement strategies could be based on the air pollution models. Nowa- days, very few of these models were validated due to the lack of 3D measurements. The goal of the ESCOMPTE experiment was to provide such of 3D database in order to constrain the air pollution models. The EPFL-LPA mobile laboratory was part of the ESCOMPTE extensive network and was located on the northern side of the Berre Lake at St.Chamas. In this framework, measurements of the air pollutants (O3, SO2, NOx, polycyclic aromatic hydrocarbons, black carbon and particulate matter of less than 10 microns mean diameter) and meteorological parameters (wind, temperature, pressure and relative humidity) were continuously performed from June 10 to July 13, 2001. They were combined with ground based lidar observations for ozone and aerosol estimation from 100m above ground level up to the free troposphere at ca.7 km agl. This paper will present an overview of the results obtained and will highlight one of the intensive observation period (IOP) during which clean air conditions were initially observed followed by highly polluted air masses during the second half of the IOP.

  10. CIEMAT Interlaboratories Comparison of the Results obtained in the Proficiency Test Run by IAEA; Comparacion Interlaboratorios del CIEMAT de los Resultados Obtenidos en la Prueba de Capacitacion de Analisis de Transuranicos en Cenizas propocionadas por el OIEA

    Energy Technology Data Exchange (ETDEWEB)

    Gasco, C.; Anton, M. P.; Alvarez, A.; Navarro, N.; Meral, J.; Gonzalez, A.; Higueras Lafaja, E. [Ciemat. Madrid (Spain)

    2000-07-01

    This report contains the results obtained by two different laboratories from CIEMAT after participating in the Proficiency Test organised by IAEA (International Atomic Energy Agency) in 1999. This test involves the analysis of fly ashes containing natural radionuclides and different amounts of added transuranics. The extraction techniques, counting methods and results obtained are detailed. This type of test are used for the labs to achieve their accreditation and check the reliability of the procedures routinely employed. (Author) 4 refs.

  11. Irradiation with protons in order to obtain new rice varieties

    International Nuclear Information System (INIS)

    Gonzalez, Maria C.; Cristo, Elizabeth; Fuentes, Jorge L.

    2001-01-01

    In the Laboratory of Genetics and Improvement of the National Institute of Agricultural Sciences was developed a Program of Genetic Improvement using Biotechnical and Nuclear Techniques in order to obtain new rice varieties of high yield potential under drought stress condition. For them different explants types were used starting from seeds of the Cuban variety of rice Amistad 82 irradiated with protons in dose of 10, 20, 30, 40, 50, 60, 70, 80, 90 and 100 Gy. The explants were cultivated in vitro in order to obtaining callus and later plant regenerate. The plant selected in vitro was multiplied being carried out several selection cycles under field conditions. A remarkable stimulation was observed from the regeneration of plants when using dose of 20 Gy and it was possible to select 4 promising lines that differ of the donor as for cycle, architecture of the plant and tolerance to drought. Tjis result demonstrates the potentialities of this radiation source for obtaining of new rice varieties

  12. Microstructural characterization of the geopolymer obtained from iron-rich metakaolin

    International Nuclear Information System (INIS)

    Vassalo, Erica Antunes de S.; Aguilar, Maria Teresa P.; Gumieri, Adriana Guerra

    2014-01-01

    Geopolymer is a material derived from precursors rich in SiO_2 and Al_2O_3, activated in an alkaline solution by means of a polymerization process. In this process, units of tetrahedral aluminosilicate structures are organized in repetitions that share oxygen. One of the precursors most commonly used to obtain geopolymer is metakaolin. Recent studies have reported iron enhancement in a partial replacement of the aluminium present in metakaolin. This paper presents the microstructural characterization and analysis of a geopolymer obtained by means of the activation of iron-rich metakaolin with sodium hydroxide at 12, 15 and 18 mol, both at room temperature and in an oven at 85±3°C. The geopolymers obtained were classified and analysed using X-ray fluorescence testing (EDX-720), a scanning electron microscope (SEM) and a Fourier transform infrared spectroscopy (FTIR). The results enabled an assessment of their physical-chemical and microstructural characteristics, as well as their reactive potential. (author)

  13. Main results obtained in France in the development of the gaseous diffusion process for uranium isotope separation

    International Nuclear Information System (INIS)

    Frejacques, C.; Bilous, O.; Dixmier, J.; Massignon, D.; Plurien, P.

    1958-01-01

    The main problems which occur in the study of uranium isotope separation by the gaseous diffusion process, concern the development of the porous barrier, the corrosive nature of uranium hexafluoride and also the chemical engineering problems related to process design and the choice of best plant and stage characteristics. Porous barriers may be obtained by chemical attack of non porous media or by agglomeration of very fine powders. Examples of these two types of barriers are given. A whole set of measurement techniques were developed for barrier structure studies, to provide control and guidance of barrier production methods. Uranium hexafluoride reactivity and corrosive properties are the source of many difficult technological problems. A high degree of plant leak tightness must be achieved. This necessity creates a special problem in compressor bearing design. Barrier lifetime is affected by the corrosive properties of the gas, which may lead to a change of barrier structure with time. Barrier hexafluoride permeability measurements have helped to make a systematic study of this point. Finally an example of a plant flowsheet, showing stage types and arrangements and based on a minimisation of enriched product costs is also given as an illustration of some of the chemical engineering problems present. (author) [fr

  14. Evaluation of marginal and internal gaps of metal ceramic crowns obtained from conventional impressions and casting techniques with those obtained from digital techniques.

    Science.gov (United States)

    Rai, Rathika; Kumar, S Arun; Prabhu, R; Govindan, Ranjani Thillai; Tanveer, Faiz Mohamed

    2017-01-01

    Accuracy in fit of cast metal restoration has always remained as one of the primary factors in determining the success of the restoration. A well-fitting restoration needs to be accurate both along its margin and with regard to its internal surface. The aim of the study is to evaluate the marginal fit of metal ceramic crowns obtained by conventional inlay casting wax pattern using conventional impression with the metal ceramic crowns obtained by computer-aided design and computer-aided manufacturing (CAD/CAM) technique using direct and indirect optical scanning. This in vitro study on preformed custom-made stainless steel models with former assembly that resembles prepared tooth surfaces of standardized dimensions comprised three groups: the first group included ten samples of metal ceramic crowns fabricated with conventional technique, the second group included CAD/CAM-milled direct metal laser sintering (DMLS) crowns using indirect scanning, and the third group included DMLS crowns fabricated by direct scanning of the stainless steel model. The vertical marginal gap and the internal gap were evaluated with the stereomicroscope (Zoomstar 4); post hoc Turkey's test was used for statistical analysis. One-way analysis of variance method was used to compare the mean values. Metal ceramic crowns obtained from direct optical scanning showed the least marginal and internal gap when compared to the castings obtained from inlay casting wax and indirect optical scanning. Indirect and direct optical scanning had yielded results within clinically acceptable range.

  15. Method for obtaining a varnish with a base of mineral oil obtained by distillation of bituminous schists

    Energy Technology Data Exchange (ETDEWEB)

    Marchionni, A

    1945-07-24

    A method for obtaining a varnish is described characterized by the fact that the following ingredients are being used; mineral oil from the distillation of bituminous schists in the proportions already cited in the description, diluted with benzene or turpentine, with admixture of coloring matter. Varnish with a base of mineral oil from the distillation of bituminous schists is obtained.

  16. Unfolding neutron spectra obtained from BS–TLD system using genetic algorithm

    International Nuclear Information System (INIS)

    Santos, J.A.L.; Silva, E.R.; Ferreira, T.A.E; Vilela, E.C.

    2012-01-01

    Due to the variability of neutron spectrum within the same environment, it is essential that the spectral distribution as a function of energy should be characterized. The precise information allows radiological quantities establishment related to that spectrum, but it is necessary that a spectrometric system covers a large interval of energy and an unfolding process is appropriate. This paper proposes use of a technique of Artificial Intelligence (AI) called genetic algorithm (GA), which uses bio-inspired mathematical models with the implementation of a specific matrix to unfolding data obtained from a combination of TLDs embedded in a BS system to characterize the neutron spectrum as a function of energy. The results obtained with this method were in accordance with reference spectra, thus enabling this technique to unfold neutron spectra with the BS–TLD system. - Highlights: ► The unfolding code used the artificial intelligence technique called genetic algorithms. ► A response matrix specific to the unfolding data obtained with the BS–TLD system is used by the AGLN. ► The observed results demonstrate the potential use of genetic algorithms in solving complex nuclear problems.

  17. Assessment of the variations in fat content in normal liver using a fast MR imaging method in comparison with results obtained by spectroscopic imaging

    International Nuclear Information System (INIS)

    Irwan, Roy; Edens, Mireille A.; Sijens, Paul E.

    2008-01-01

    A recently published Dixon-based MRI method for quantifying liver fat content using dual-echo breath-hold gradient echo imaging was validated by phantom experiments and compared with results of biopsy in two patients (Radiology 2005;237:1048-1055). We applied this method in ten healthy volunteers and compared the outcomes with the results of MR spectroscopy (MRS), the gold standard in quantifying liver fat content. Novel was the use of spectroscopic imaging yielding the variations in fat content across the liver rather than a single value obtained by single voxel MRS. Compared with the results of MRS, liver fat content according to MRI was too high in nine subjects (range 3.3-10.7% vs. 0.9-7.7%) and correct in one (21.1 vs. 21.3%). Furthermore, in one of the ten subjects the MRI fat content according to the Dixon-based MRI method was incorrect due to a (100-x) versus x percent lipid content mix-up. The second problem was fixed by a minor adjustment of the MRI algorithm. Despite systematic overestimation of liver fat contents by MRI, Spearman's correlation between the adjusted MRI liver fat contents with MRS was high (r = 0.927, P < 0.001). Even after correction of the algorithm, the problem remaining with the Dixon-based MRI method for the assessment of liver fat content,is that, at the lower end range, liver fat content is systematically overestimated by 4%. (orig.)

  18. A comparison between the Structural Results obtained by X-ray Single Crystal Data and by Neutron Powder Data for BaVs/sb3/

    International Nuclear Information System (INIS)

    Marezio, M.

    1986-01-01

    The structure of BaVs/sb3/, as refined from X-ray single-crystal data to an R factor of 0.011, is compared to the structure of the same compound obtained from neutron powder data (Rsb(ro) = 6.82, Rsb(psilon) = 4.09). As expected, the X-ray standard deviations of the positional and thermal parameters are smaller than the corresponding neutron standard deviations. However, the dynamical disorder deduced from the anomalously large thermal vibrations of the vanadium atoms obtained from the X-ray data is also evidenced by the neutron refinement. On the other hand, the neutron standard deviations of the lattice parameters are smaller than the X-ray counterparts

  19. Characterization of some etalon matrices obtained by cement conditioning of the radioactive sludge

    International Nuclear Information System (INIS)

    Nicu, M.; Mihai, F.

    1998-01-01

    The aim of this work was to establish new ways of investigation of some compounds which are important for studying physico-mechanical mechanisms, nature and structure of the intermediate and final products oc curing in reactions of the technological conditioning processes of the radioactive wastes by cementation after their treatment by precipitation or sorption process. Cement conditioning is, presently, the most used technology for the low and intermediate level waste treatment. Besides many advantages it also presents some disadvantages which limit the utilization area depending, firstly, on the chemical composition of the conditioned radioactive waste. In this work, the influence of different iron precipitates on cement structure is studied and assessed by changes in phase composition and mechanical resistance. Using mechanical resistance data, X-rays diffraction spectra and Moessbauer spectroscopy for iron precipitates and cement-iron precipitate samples, we obtained an image concerning chemical reactions and modifications which appear when iron precipitate is included in cement, between major components of cement and the added one. Moessbauer spectroscopy and X-rays diffraction were proved to be very useful to establish composition and structure of iron compounds used in treatment technology by chemical precipitation. Precipitation mechanism may be elucidated only by a thoroughgoing study of intermediate compounds obtained in successive precipitation phases. Depending on precipitation procedure, initial iron cations and order of adding of reactants, it was observed that the structure of finally obtained precipitates is different. Obtained results at compression tests on cement-iron precipitate samples are similarly with those obtained for reference cement matrix. These results demonstrate that iron precipitate in the sample with precipitate/cement ratio of 1/2 does not influence the mechanical resistance of the obtained matrix The presented results are in

  20. Aircrew Exposure To Cosmic Radiation Evaluated By Means Of Several Methods; Results Obtained In 2006

    International Nuclear Information System (INIS)

    Ploc, Ondrej; Spurny, Frantisek; Jadrnickova, Iva; Turek, Karel

    2008-01-01

    Routine evaluation of aircraft crew exposure to cosmic radiation in the Czech Republic is performed by means of calculation method. Measurements onboard aircraft work as a control tool of the routine method, as well as a possibility of comparison of results measured by means of several methods. The following methods were used in 2006: (1) mobile dosimetry unit (MDU) type Liulin--a spectrometer of energy deposited in Si-detector; (2) two types of LET spectrometers based on the chemically etched track detectors (TED); (3) two types of thermoluminescent detectors; and (4) two calculation methods. MDU represents currently one of the most reliable equipments for evaluation of the aircraft crew exposure to cosmic radiation. It is an active device which measures total energy depositions (E dep ) in the semiconductor unit, and, after appropriate calibration, is able to give a separate estimation for non-neutron and neutron-like components of H*(10). This contribution consists mostly of results acquired by means of this equipment; measurements with passive detectors and calculations are mentioned because of comparison. Reasonably good agreement of all data sets could be stated

  1. Polypropylene obtained through zeolite supported catalysts

    Directory of Open Access Journals (Sweden)

    Queli C. Bastos

    2004-01-01

    Full Text Available Propylene polymerizations were carried out with f2C(Flu(CpZrCl2 and SiMe2(Ind2ZrCl2 catalysts supported on silica, zeolite sodic mordenite (NaM and acid mordenite (HM. The polymerizations were performed at different temperatures and varying aluminium/zirconium molar ratios ([Al]/[Zr]. The effect of these reaction parameters on the catalyst activity was investigated using a proposed statistical experimental planning. In the case of f2C(Flu(CpZrCl2, SiO2 and NaM were used as support and the catalyst performance evaluated using toluene and pentane as polymerization solvent. The molecular weight, molecular weight distribution, melting point and crystallinity of the polymers were examined. The results indicate very high activities for the syndiospecific heterogeneous system. Also, the polymers obtained had superior Mw and stereoregularity.

  2. Polypropylene obtained through zeolite supported catalysts

    International Nuclear Information System (INIS)

    Bastos, Queli C.; Marques, Maria de Fatima V.

    2004-01-01

    Propylene polymerizations were carried out with φ 2 C(Flu)(Cp)ZrCl 2 and SiMe 2 (Ind)2ZrCl 2 catalysts supported on silica, zeolite sodic mordenite (NaM) and acid mordenite (HM). The polymerizations were performed at different temperatures and varying aluminium/zirconium molar ratios ([Al]/[Zr]). The effect of these reaction parameters on the catalyst activity was investigated using a proposed statistical experimental planning. In the case of f 2 C(Flu)(Cp)ZrCl 2 , SiO 2 and NaM were used as support and the catalyst performance evaluated using toluene and pentane as polymerization solvent. The molecular weight, molecular weight distribution, melting point and crystallinity of the polymers were examined. The results indicate very high activities for the syndiospecific heterogeneous system. Also, the polymers obtained had superior Mw and stereo regularity. (author)

  3. PbSe nanocubes obtained by high-energy milling

    Energy Technology Data Exchange (ETDEWEB)

    Rojas-Chavez, H., E-mail: hrojasc@ipn.mx [Centro de Investigacion en Ciencia Aplicada y Tecnologia Avanzada - IPN (Mexico); Reyes-Carmona, F. [Facultad de Quimica - UNAM (Mexico); Achimovicova, M. [Slovak Academy of Sciences, Institute of Geotechnics (Slovakia); Daneu, N. [Jozef Stefan Institute, Department for Nanostructured Materials (Slovenia); Jaramillo-Vigueras, D. [Centro de Investigacion e Innovacion Tecnologica - IPN (Mexico)

    2012-06-15

    In this study, PbSe nanocubes were obtained by high-energy milling, and their optical properties were investigated by measuring the UV-VIS-IR spectra in the range of 200-2,000 nm. The optical absorption of all samples showed a strong UV emission band at 1.45 eV. Previously, to obtain only PbSe nanocubes, an intermediate phase was identified, PbSeO{sub 3}. Although both PbSeO{sub 3} and PbSe were traced through this study, a major effort is devoted to characterize the latter. To trace how chemical transitions evolve from precursors to PbSe, X-ray diffraction and Rietveld refinement were carried out. Therefore, the following parameters were evaluated as a function of milling time: phase percentages, area-to-volume ratio, average crystallite dimensions, specific surface area, and morphology changes. To corroborate previous findings, nitrogen adsorption and transmission electron microscopy techniques were used. All the set experimental results unambiguously confirm that crystallites show a cubic morphology, with its average crystallite size distribution being around 24 nm.

  4. Cytogenetical effects of low doses: results obtained by N.N.Luchik and present-day problems

    International Nuclear Information System (INIS)

    Geras'kin, S.A.; Sevan'kaev, A.V.

    1996-01-01

    The analysis of present status of the problem of quantitative assessment of cytogenetic effects low is presented. The importance of works of N.V. Luchik is demonstrated for the development of this field of radiobiology. The results of the author's own experimental and theoretical research on the regularities of induction of cytogenetical damage by low doses of ionising radiation are presented

  5. Electrolytic Hydrogen obtaining by a photovoltaic source

    International Nuclear Information System (INIS)

    Pasculete, E.; Condrea, F.; Stanoiu, L.

    2005-01-01

    At present, the developed countries allocate large funds for the financing of some global programs for fundamental and applicative research for development of hydrogen non-conventional production technologies. One of these technologies is the photo-assisted electrolysis. This technology is adopted in the research, which results are presented in this paper. The experimental model includes as basic equipment 100 W photovoltaic source, electrolysis battery press filter type, control unit of the electric energy discharged, accumulator, hydrogen storage unit. Five types of material have been tested for the electrolysis cell diaphragm: asbestos; Netrom- unwoven material from fibers of polypropylene; ion changing composite membrane - polysulfone support with an active layer of sulfonated poly-sulfone (PSS/PSJ) and poly-sulfone support with an active layer of sulfonated poly-eter cetone (SPEEK/PSf); ion-exchange membrane made from sulfonated poly-eter cetone (SPEEK). The graphics and results from the test system are presented. The analysis of the experimental results lead to the establishment of the optimal configuration of battery and of the operational conditions of the assembly. The experimental results give the opportunity to obtain electrolytic hydrogen with a photovoltaic source, in an efficient system, and promote the Romanian research at a level of a demonstrative installation

  6. Wood-Polymer composites obtained by gamma irradiation

    International Nuclear Information System (INIS)

    Gago, J.; Lopez, A.; Rodriguez, J.; Santiago, J.; Acevedo, M.

    2007-01-01

    In this work we impregnate three Peruvian woods (Calycophy spruceanum Be, Aniba amazonica Meiz and Hura crepitans L) with styrene-polyester resin and methyl methacrylate. The polymerization of the system was promoted by gamma radiation and the experimental optimal condition was obtained with styrene-polyester 1:1 and 15 kGy. The obtained composites show reduced water absorption and better mechanical properties compared to the original wood. The structure of the wood-polymer composites was studied by light microscopy. Water absorption and hardness were also obtained

  7. Wood-Polymer composites obtained by gamma irradiation

    Science.gov (United States)

    Gago, J.; López, A.; Santiago, J.; Acevedo, M.; Rodríguez, J.

    2007-10-01

    In this work we impregnate three Peruvian woods (Calycophy spruceanum Be, Aniba amazonica Meiz and Hura crepitans L) with styrene-polyester resin and methyl methacrylate. The polymerization of the system was promoted by gamma radiation and the experimental optimal condition was obtained with styrene-polyester 1:1 and 15 kGy. The obtained composites show reduced water absorption and better mechanical properties compared to the original wood. The structure of the wood-polymer composites was studied by light microscopy. Water absorption and hardness were also obtained.

  8. A BATCH REACTOR CONSTRUCTION FOR OBTAINING BIODIESEL FROM OIL Ricinus communis

    Directory of Open Access Journals (Sweden)

    Yolimar Fernández

    2014-06-01

    Full Text Available A batch reactor was constructed to obtain biodiesel from 5 liters of extracted from the seed of Ricinus communis. The reactor is made of stainless steel, 29cm length, 15.24 cm of inner diameter and a conical base of 20cm long, wall thickness of 0.2 cm, 1000 W tubular resistance and 110 volt motor. It is extracted and compared with the respective norms the physical and chemical properties of crude oil. Preliminary tests catalyzed transesterification of the oil with NaOH to verify the feasibility of the reaction and define the performed operational conditions. Obtained biodiesel was characterized and compared with references. The results showed that it is possible to obtain the biofuel in the batch reactor with a conversion 88%, confirming its application in transesterification reactions in a basic medium.

  9. Nutritional potential of green banana flour obtained by drying in spouted bed

    Directory of Open Access Journals (Sweden)

    Carolina Vieira Bezerra

    2013-12-01

    Full Text Available This study evaluated the chemical composition of peeled and unpeeled green banana Cavendish (AAA flour obtained by drying in spouted bed, aiming at adding nutritional value to food products. The bananas were sliced and crushed to obtain a paste and fed to the spouted bed dryer (12 cm height and T = 80 ºC in order to obtain flour. The flours obtained were subjected to analysis of moisture, protein, ash, carbohydrates, total starch, resistant starch, fiber. The green banana flours, mainly unpeeled, are good sources of fiber and resistant starch with an average of 21.91g/100g and 68.02g/100g respectively. The protein content was found in an average of 4.76g/100g, being classified as a low biological value protein with lysine as the first limiting amino acid. The results showed that unpeeled green banana flour obtained by spouted bed drying can be a valuable tool to add nutritional value to products in order to increase their non-digestible fraction.

  10. A novel heuristic method for obtaining S-boxes

    International Nuclear Information System (INIS)

    Chen Guo

    2008-01-01

    An efficient algorithm named chaotic multi-swapping and simulated annealing (CMSSA) for obtaining cryptographically strong 8 x 8 S-boxes is presented. The method is based on chaotic maps and simulated annealing. In addition, cryptographic properties such as bijectivity, strict avalanche criterion, nonlinearity, output bits independence criterion and equiprobable input/output XOR distribution are analyzed in detail for the S-box produced. The results of numerical analysis show that the box has nearly fulfilled the criteria for a cryptographically strong S-box and can effectively resist several attacks

  11. The hardness of synthetic products obtained from cooled and crystallized basaltic melts (in Romanian)

    OpenAIRE

    Daniela Ogrean

    2001-01-01

    The Hardness of Synthetic Products Obtained from Cooled and Crystallized Basaltic Melts. Hardness is one of the main properties of the products obtained from cooled and crystallized basaltic melts under a controlled thermal regime. It influences the abrasion tear resistance of the resulted material. The microhardness measurements on the samples (bricks, boards, gutters, armour plates, tubes) indicated Vickers hardness value between 757–926 for the materials obtained from Şanovita basalts (Tim...

  12. MgAl_2O_4 foams obtained by combustion synthesis

    International Nuclear Information System (INIS)

    Moraes, G.G.; Rosa, M.A.; Kronbauer, D.P.; Pozzobom, I.F.; Fernandes, C.P.; Oliveira, A.P. Novaes de

    2014-01-01

    This work aims to study magnesium aluminate (MgAl_2O_4) ceramic foams obtained by combustion synthesis in solution without the need of surfactants to stabilize bubbles. The precursors, Al(NO_3)_3_.9H_2O and Mg(NO_3)_2_.6H_2_O, dispersed in distilled water (20 wt%) were magnetically stirred under heating (70°C). At the beginning of the reaction, a fuel composed by a mixture of residual glycerins from the production of biodiesel was added. The foams were produced by controlling the stirring speed and temperature. The applied thermal cycle to consolidate the foams consisted of heating at 1°C/min to 600°C/120 min and subsequently raising the temperature at 10°C/min to 1600°C/120 min. The obtained materials were characterized by SEM,TEM and from tomographic images. The results showed that the obtained magnesium aluminate foams have a high porosity (97%), a high connectivity and pore sizes (diameters) between 30 and 1200 μm. (author)

  13. A comparison of two methods for prediction of response and rates of inbreeding in selected populations with the results obtained in two selection experiments

    Directory of Open Access Journals (Sweden)

    Verrier Etienne

    2005-05-01

    Full Text Available Abstract Selection programmes are mainly concerned with increasing genetic gain. However, short-term progress should not be obtained at the expense of the within-population genetic variability. Different prediction models for the evolution within a small population of the genetic mean of a selected trait, its genetic variance and its inbreeding have been developed but have mainly been validated through Monte Carlo simulation studies. The purpose of this study was to compare theoretical predictions to experimental results. Two deterministic methods were considered, both grounded on a polygenic additive model. Differences between theoretical predictions and experimental results arise from differences between the true and the assumed genetic model, and from mathematical simplifications applied in the prediction methods. Two sets of experimental lines of chickens were used in this study: the Dutch lines undergoing true truncation mass selection, the other lines (French undergoing mass selection with a restriction on the representation of the different families. This study confirmed, on an experimental basis, that modelling is an efficient approach to make useful predictions of the evolution of selected populations although the basic assumptions considered in the models (polygenic additive model, normality of the distribution, base population at the equilibrium, etc. are not met in reality. The two deterministic methods compared yielded results that were close to those observed in real data, especially when the selection scheme followed the rules of strict mass selection: for instance, both predictions overestimated the genetic gain in the French experiment, whereas both predictions were close to the observed values in the Dutch experiment.

  14. Pharmacological developments obtained from marine natural products and current pipeline perspective.

    Science.gov (United States)

    Galeano, Elkin; Rojas, Jhon J; Martínez, Alejandro

    2011-02-01

    Marine organisms represent a new extensive source for bioactive molecules. They have the potential to provide new therapeutic alternatives to treat human diseases. In this paper, we describe and discuss a variety of isolated and semisynthetic molecules obtained from marine sources. These compounds are in phase II, phase III and at the commercialization stage of new drug development. A description of the mechanism of action, dosage used and side effects are also reported. The positive results obtained from these studies have triggered the development of new studies to evaluate the prospects for utilization of marine organisms.

  15. Highly ordered amorphous silicon-carbon alloys obtained by RF PECVD

    CERN Document Server

    Pereyra, I; Carreno, M N P; Prado, R J; Fantini, M C A

    2000-01-01

    We have shown that close to stoichiometry RF PECVD amorphous silicon carbon alloys deposited under silane starving plasma conditions exhibit a tendency towards c-Si C chemical order. Motivated by this trend, we further explore the effect of increasing RF power and H sub 2 dilution of the gaseous mixtures, aiming to obtain the amorphous counterpart of c-Si C by the RF-PECVD technique. Doping experiments were also performed on ordered material using phosphorus and nitrogen as donor impurities and boron and aluminum as acceptor ones. For nitrogen a doping efficiency close to device quality a-Si:H was obtained, the lower activation energy being 0,12 eV with room temperature dark conductivity of 2.10 sup - sup 3 (OMEGA.cm). Nitrogen doping efficiency was higher than phosphorous for all studied samples. For p-type doping, results indicate that, even though the attained conductivity values are not device levels, aluminum doping conducted to a promising shift in the Fermi level. Also, aluminum resulted a more efficie...

  16. The Data Evaluation for Obtaining Accuracy and Reliability

    International Nuclear Information System (INIS)

    Kim, Chang Geun; Chae, Kyun Shik; Lee, Sang Tae; Bhang, Gun Woong

    2012-01-01

    Nemours scientific measurement results are flooded from the paper, data book, etc. as fast growing of internet. We meet many different measurement results on the same measurand. In this moment, we are face to choose most reliable one out of them. But it is not easy to choose and use the accurate and reliable data as we do at an ice cream parlor. Even expert users feel difficult to distinguish the accurate and reliable scientific data from huge amount of measurement results. For this reason, the data evaluation is getting more important as the fast growing of internet and globalization. Furthermore the expressions of measurement results are not in standardi-zation. As these need, the international movement has been enhanced. At the first step, the global harmonization of terminology used in metrology and the expression of uncertainty in measurement were published in ISO. These methods are wide spread to many area of science on their measurement to obtain the accuracy and reliability. In this paper, it is introduced that the GUM, SRD and data evaluation on atomic collisions.

  17. Multiple-walled BN nanotubes obtained with a mechanical alloying technique

    International Nuclear Information System (INIS)

    Rosas, G.; Sistos, J.; Ascencio, J.A.; Medina, A.; Perez, R.

    2005-01-01

    An experimental method to obtain multiple-walled nanotubes of BN using low energy is presented. The method is based on the use of mechanical alloying techniques with elemental boron powders and nitrogen gas mixed in an autoclave at room temperature. The chemical and structural characteristics of the multiple-walled nanotubes were obtained using different techniques, such as X-ray diffraction, transmission electron microscopy, EELS microanalysis, high-resolution electron microscopy images and theoretical simulations based on the multisliced approach of the electron diffraction theory. This investigation clearly illustrates the production of multiple-wall BN nanotubes at room temperature. These results open up a new kind of synthesis method with low expense and important perspectives for use in large-quantity production. (orig.)

  18. To report the obtained results in the operation multicycle study of the L V U-1 using design data with the FCSII (1D) and PRESTO (3D) codes of the FMS system

    International Nuclear Information System (INIS)

    Montes T, J.L.; Cortes C, C.C.

    1991-07-01

    This work is to carry out a multicycle study for the Laguna Verde U-1 reactor with the FCS-II (1 - 20 cycles) and PRESTO (1 - 6 cycles) codes and to compare the obtained results against those reported by General Electric. (Author)

  19. Structure of Al-CF composites obtained by infiltration methods

    Directory of Open Access Journals (Sweden)

    A. Dolata-Grosz

    2011-04-01

    Full Text Available The structure of the composites obtained in infiltration processes 2D and 3D carbon preform by liquid Al alloy have been presented in thispaper. An aluminum alloy with silicon and manganese AlSi9Mn (trimal 37-TR37 was applied in the researches. As the reinforcementused carbon perform prepared with various protective barriers such as the nickel coating, the coating of silicon carbide and pyrolyticcarbon coating. Carbon preforms was prepared at the Institute for Lightweight Structures and Polymer Technology (ILK TU Dresden andat the Institute of Technology and Ceramic Systems (Fraunhofer-IKTS. The process of infiltration of carbon perform by liquid aluminiumalloy was carried out using a pressure-vacuum infiltration on the Degussa press and gas-pressure infiltration (GPI in an autoclavedesigned and built at the Department of Materials Technology at the Silesian University of Technology. The obtained composites werecharacterized by a regular shape, with no surface casting defects. The best connection of components was observed in AlSi9Mn/Cf(Nicomposite, obtained by gas-pressure infiltration method (GPI. On metallographic specimens, good interface between fibres and thealuminium matrix were observed. The obtained research results justify the application of nickel coatings on the fibres. During the failurecrack propagated across fiber. There was no presence of aluminum carbide on the fiber-matrix. It can be assumed that the composite willbe characterized by the good mechanical properties. However, this requires further experimental verification planned in the next stage of research, in the project realized within the DFG program: "3D textile reinforced aluminium matrix composites for complex loadingsituations in lightweight automobile and machine parts".

  20. Syngas Production from Pyrolysis of Nine Composts Obtained from Nonhybrid and Hybrid Perennial Grasses

    Directory of Open Access Journals (Sweden)

    Adéla Hlavsová

    2014-01-01

    Full Text Available A pyrolysis of compost for the production of syngas with an explicit H2/CO = 2 or H2/CO = 3 was investigated in this study. The composts were obtained from nonhybrid (perennial grasses (NHG and hybrid (perennial grasses (HG. Discrepancies in H2 evolution profiles were found between NHG and HG composts. In addition, positive correlations for NHG composts were obtained between (i H2 yield and lignin content, (ii H2 yield and potassium content, and (iii CO yield and cellulose content. All composts resulted in H2/CO = 2 and five of the nine composts resulted in H2/CO = 3. Exceptionally large higher heating values (HHVs of pyrolysis gas, very close to HHVs of feedstock, were obtained for composts made from mountain brome (MB, 16.23 MJ/kg, hybrid Becva (FB, 16.45 MJ/kg, and tall fescue (TF, 17.43 MJ/kg. The MB and FB composts resulted in the highest syngas formation with H2/CO = 2, whereas TF compost resulted in the highest syngas formation with H2/CO = 3.

  1. 15 CFR 748.2 - Obtaining forms; mailing addresses.

    Science.gov (United States)

    2010-01-01

    ... 15 Commerce and Foreign Trade 2 2010-01-01 2010-01-01 false Obtaining forms; mailing addresses... APPLICATIONS (CLASSIFICATION, ADVISORY, AND LICENSE) AND DOCUMENTATION § 748.2 Obtaining forms; mailing addresses. (a) You may obtain the forms required by the EAR from any U.S. Department of Commerce District...

  2. Magnetically diluted semi-conductor of SnO_2- Fe obtained by controlled precipitation

    International Nuclear Information System (INIS)

    Cajas, P.C.; Munoz, R.; Rodriguez-Paez, J.E.

    2014-01-01

    Solid solutions were synthesized SnO_2 doped with 5% and 8 mol% Fe by the controlled precipitation method. The particles size was obtained of ∼12 nm with heath treatment 450 °C. The presence of iron in the structure is evidenced by Raman spectroscopy The crystallite size we obtained with the results of XRD, and particle size by MET, it was concluded that the nanoparticles obtained were monocrystalline. The particles were characterized magnetically, for the powders doped to 8% Fe was determined ferromagnetic behavior at 5K, with a tendency superparamagnetic and paramagnetic at a temperature of 300K. (author)

  3. Positional quality assessment of orthophotos obtained from sensors onboard multi-rotor UAV platforms.

    Science.gov (United States)

    Mesas-Carrascosa, Francisco Javier; Rumbao, Inmaculada Clavero; Berrocal, Juan Alberto Barrera; Porras, Alfonso García-Ferrer

    2014-11-26

    In this study we explored the positional quality of orthophotos obtained by an unmanned aerial vehicle (UAV). A multi-rotor UAV was used to obtain images using a vertically mounted digital camera. The flight was processed taking into account the photogrammetry workflow: perform the aerial triangulation, generate a digital surface model, orthorectify individual images and finally obtain a mosaic image or final orthophoto. The UAV orthophotos were assessed with various spatial quality tests used by national mapping agencies (NMAs). Results showed that the orthophotos satisfactorily passed the spatial quality tests and are therefore a useful tool for NMAs in their production flowchart.

  4. The synthesis and properties of the phases obtained by solid-solid reactions

    Directory of Open Access Journals (Sweden)

    Blonska-Tabero A.

    2008-01-01

    Full Text Available The presented work encompasses the subject of the studies and the results obtained over the last years by the research workers of the Department of Inorganic Chemistry. They include mainly the studies on the reactivity of metal oxides, searching for new phases in binary and ternary systems of metal oxides as well as describing phase relations establishing in such systems. They also encompass works on the extensive characteristics of physico-chemical properties of the newly obtained compounds.

  5. Use of grape must as a binder to obtain activated carbon briquettes

    Directory of Open Access Journals (Sweden)

    Deiana A. C.

    2004-01-01

    Full Text Available The results of studies on briquetting activated-carbon-based adsorbent materials, prepared from raw materials from the region of Cuyo, Argentina, are reported in this article. Several steps were carried out to obtain activated-carbon briquettes from Eucalyptus camaldulensis Dehn wood. These steps included carbonization of wood to obtain char; blending of char and a novel binder, i.e., grape must; formation of cylinder-like briquettes by pressure; and activation of the resulting material. The material was activated with steam under different temperatures, activation times, and activating agent flow rates. Impact resistance index, axial compressive strength, tensile strength by diametrical compression, BET area, and pore volume were measured for product characterization. Satisfactory surface areas and mechanical strengths were found in the final products.

  6. Silicon dioxide obtained by Polymeric Precursor Method

    International Nuclear Information System (INIS)

    Oliveira, C.T.; Granado, S.R.; Lopes, S.A.; Cavalheiro, A.A.

    2011-01-01

    The Polymeric Precursor Method is able for obtaining several oxide material types with high surface area even obtained in particle form. Several MO 2 oxide types such as titanium, silicon and zirconium ones can be obtained by this methodology. In this work, the synthesis of silicon oxide was monitored by thermal analysis, XRD and surface area analysis in order to demonstrate the influence of the several synthesis and calcining parameters. Surface area values as higher as 370m2/g and increasing in the micropore volume nm were obtained when the material was synthesized by using ethylene glycol as polymerizing agent. XRD analysis showed that the material is amorphous when calcinated at 600°C in despite of the time of calcining, but the material morphology is strongly influenced by the polymeric resin composition. Using Glycerol as polymerizing agent, the pore size increase and the surface area goes down with the increasing in decomposition time, when compared to ethylene glycol. (author)

  7. Development of the safety evaluation system in the respects of organizational factors and workers' consciousness. Pt. 1. Study of validities of functions for necessary evaluation and results obtained

    International Nuclear Information System (INIS)

    Takano, Kenichi; Tsuge, Tadafumi; Hasegawa, Naoko; Hirose, Ayako; Sasou, Kunihide

    2002-01-01

    CRIEPI decided to develop the safety evaluation system to investigate the safety level of the industrial sites due to questionnaires of organizational climate, safety managements, and workers' safety consciousness to workers. This report describes the questionnaire survey to apply to the domestic nuclear power plant for using obtained results as a fundamental data in order to construct the safety evaluation system. This system will be used for promoting safety culture in organizations of nuclear power plants. The questionnaire survey was conducted to 14 nuclear power stations for understanding the present status relating to safety issues. This questionnaire involves 122 items classified into following three categories: (1) safety awareness and behavior of plant personnel; (2) safety management; (3) organizational climate, based on the model considering contributing factor groups to safety culture. Obtained results were analyzed by statistical method to prepare functions of evaluation. Additionally, by applying a multivariate analysis, it was possible to extract several crucial factors influencing safety performance and to find a comprehensive safety indicator representing total organizational safety level. Significant relations were identified between accident rates (both labor accidents and facility failures) and above comprehensive safety indicator. Next, 122 questionnaire items were classified into 20 major safety factors to grasp the safety profiles of each site. This profile is considered as indicating the features of each site and also indicating the direction of progress for improvement of safety situation in the site. These findings can be reflected in developing the safety evaluation system, by confirming the validity of the evaluation method and giving specific functions. (author)

  8. Report of test and research results on atomic energy obtained in national institutes in fiscal 1986

    International Nuclear Information System (INIS)

    1988-01-01

    The test and research regarding the utilization of atomic energy carried out in national institutions have produced many valuable results in diverse fields so far, such as nuclear fusion, safety research, food irradiation and medicine, since the budget had been appropriated for the first time in 1956. It has accomplished large role in the promotion of atomic energy utilization in Japan. This report is volume 27, in which the results of the test and research on atomic energy utilization carried out by national institutions in fiscal year 1986 are summarized. It is hoped that the understanding about the recent trend and the results of the test and research on atomic energy utilization is further promoted by this report. The contents of this report are nuclear fusion; the research on engineering safety and environmental radioactivity safety; food irradiation; the countermeasures against cancer; fertilized soil, the improvement of quality, the protection of plants and the improvement of breeding in agriculture and fishery fields; diagnosis and medical treatment, pharmaceuticals, environmental hygiene and the application to physiology and pathology in medical field; radiation chemistry and radiation measurement in mining and industry fields; nuclear reactor materials and nuclear-powered ships; civil engineering; radioactivation analysis; and the research on the prevention of injuries. (Kako, I.)

  9. Report of test and research results on atomic energy obtained in national institutes in fiscal 1984

    International Nuclear Information System (INIS)

    1985-01-01

    The test and research regarding the utilization of atomic energy carried out in national institutions have produced many valuable results in diverse fields so far, such as nuclear fusion, safety research, food irradiation and medicine, since the budget had been appropriated for the first time in 1956. It has accomplished large role in the promotion of atomic energy utilization in Japan. This report is Volume 25, in which the results of the test and research on atomic energy utilization carried out by national institutions in fiscal year 1984 are summarized. It is hoped that the understanding about the recent trend and the results of the test and research on atomic energy utilization is further promoted by this report. The contents of this report are nuclear fusion; the research on engineering safety and environmental radioactivity safety; food irradiation; the countermeasures against cancer; fertilized soil, the improvement of quality, the protection of plants and the improvement of breeding in agriculture and fishery fields; diagnosis and medical treatment, pharmaceuticals, environmental hygiene and the application to physiology and pathology in medical field; radiation chemistry and radiation measurement in mining and industry fields; nuclear reactor materials and nuclear-powered ships; civil engineering; radioactivation analysis; and the research on the prevention of injuries. (Kako, I.)

  10. Implantation of peritoneal catheters by laparotomy: nephrologists obtained similar results to general surgeons

    Directory of Open Access Journals (Sweden)

    Restrepo CA

    2014-10-01

    Full Text Available Cesar A Restrepo, Carlos Alberto Buitrago, Cielo Holguin Division of Nephrology, Department of Health Sciences, Caldas University, Caldas, ColombiaPurpose: To analyze the complications and costs of minilaparotomies performed by a nephrologist (group A compared with conventional laparotomies performed by a surgeon (group B for peritoneal catheter implantation.Setting: Two university hospitals (Santa Sofia and Caldas in Manizales, Caldas, Colombia.Methods: The study included stage 5 chronic kidney disease patients, with indication of renal replacement therapy, who were candidates for peritoneal dialysis and gave informed consent for a peritoneal catheter implant. Minilaparotomies were performed by a nephrologist in a minor surgery room under local anesthesia. Conventional laparotomies were performed by a surgeon in an operating room under general anesthesia.Results: Two nephrologists inserted 157 peritoneal catheters, and seven general surgeons inserted 185 peritoneal catheters. The groups had similar characteristics: the mean age was 55 years, 49.5% were men, and the primary diagnoses were diabetic nephropathy, hypertensive nephropathy, and unknown etiology. The implant was successful for 98.09% of group A and 99.46% of group B. There was no procedure-related mortality. The most frequent complications in the first 30 days postsurgery in group A versus group B, respectively, were: peritonitis (6.37% versus 3.78%, exit-site infection (3.82% versus 2.16%, tunnel infection (0% versus 0.54%, catheter entrapment by omentum (1.27% versus 3.24%, peritoneal effluent spillover (1.91% versus 2.16%, draining failure (4.46% versus 6.49%, hematoma (0% versus 1.08%, catheter migration with kinking (3.18% versus 2.70%, hemoperitoneum (1.27% versus 0%, and hollow viscera accidental puncture (1.91% versus 0.54%. There were no statistically significant differences in the number of complications between groups. In 2013, the cost of a surgeon-implanted peritoneal

  11. Infrared Fourier spectres of pectin obtained from pumpkin

    International Nuclear Information System (INIS)

    Usmanova, S.R.; Dzhonmurodov, A.S.; Nazirova, Kh.I.; Mukhidinov, Z.K.

    2015-01-01

    Present article is devoted to infrared Fourier spectres of pectin obtained from pumpkin. The analysis of pectin obtained from pumpkin was conducted by means of infrared spectrophotometer with Fourier transformation. The infrared spectroscopic study of pectin polysaccharide fraction of pectin matter, as well as pectin helium and micro helium obtained by means of fast extraction was conducted.

  12. Report of test and research results on atomic energy obtained in national institutes in fiscal 1987

    International Nuclear Information System (INIS)

    1989-01-01

    The test and research regarding the utilization of atomic energy carried out in national institutions have produced many valuable results in diverse fields so far, such as nuclear fusion, safety research, food irradiation and medicine, since the budget had been appropriated for the first time in 1956. It has accomplished large role in the promotion of atomic energy utilization in Japan. This report is volume 28, in which the results of the test and research on atomic energy utilization carried out by national institutions in fiscal year 1987 are summarized. It is hoped that the understanding about the recent trend and the results of the test and research on atomic energy utilization is further promoted by this report. The contents of this report are nuclear fusion; the research on engineering safety and environmental radioactivity safety; food irradiation; the countermeasures against cancer; fertilized soil, the improvement of quality, the protection of plants and the improvement of breeding in agriculture and fishery fields; diagnosis and medical treatment, pharmaceuticals, environmental hygiene and the application to physiology and pathology in medical field; radiation measurement and process analysis in mining and industry fields; nuclear reactor materials and nuclear-powered ships; civil engineering; radioactivation analysis; the research on the prevention of injuries; and the basic researches on materials and acessment and reduction of irradiation risk. (J.P.N.)

  13. 17 CFR 10.93 - Obtaining default order.

    Science.gov (United States)

    2010-04-01

    ... 17 Commodity and Securities Exchanges 1 2010-04-01 2010-04-01 false Obtaining default order. 10.93... Disposition Without Full Hearing § 10.93 Obtaining default order. When a respondent has failed to (a) file an... enter findings and conclusions and a default order against that respondent based upon the matters set...

  14. Strategies for obtaining unpublished drug trial data

    DEFF Research Database (Denmark)

    Wolfe, Nicole; Gøtzsche, Peter C.; Bero, Lisa Anne

    2013-01-01

    Authors of systematic reviews have difficulty obtaining unpublished data for their reviews. This project aimed to provide an in-depth description of the experiences of authors in searching for and gaining access to unpublished data for their systematic reviews, and to give guidance on best...... practices for identifying, obtaining and using unpublished data....

  15. Trained nurses can obtain satisfactory bone marrow aspirates and trephine biopsies.

    Science.gov (United States)

    Lawson, S; Aston, S; Baker, L; Fegan, C D; Milligan, D W

    1999-01-01

    AIMS: To assess the feasibility of training nurse practitioners to perform bone marrow aspiration and trephine biopsy, and to compare the quality of these samples with those obtained by medical staff. METHODS: A retrospective audit was undertaken of nurse practitioner and medical staff performance in bone marrow procedures in a busy haematology day unit. RESULTS: Nurse practitioners fared favourably in comparison with medical staff in performing bone marrow trephine biopsies, with mean biopsy lengths of 11 mm and 10.7 mm respectively. However, only 78% of the smears obtained by the nurses were judged technically satisfactory, compared with 91% prepared by doctors. This discrepancy was thought to be due largely to the quality of slide spreading. CONCLUSIONS: With motivated staff and a structured educational and training programme it is possible for nurse practitioners to perform the techniques of bone marrow aspiration and biopsy, and obtain specimens of satisfactory quality, thus improving efficiency of the haematology day unit and increasing quality of patient care. Images PMID:10396248

  16. Glucose obtained from rice bran by ultrasound-assisted enzymatic hydrolysis

    Directory of Open Access Journals (Sweden)

    Raquel Cristine Kuhn

    2015-05-01

    Full Text Available In this work ultrasound-assisted solid-state enzymatic hydrolysis of rice bran to obtain fermentable sugars was investigated. For this purpose, process variables such as temperature, enzyme concentration and moisture content were evaluated during the enzymatic hydrolysis with and without ultrasound irradiation. The enzyme used is a blend of amylases derived from genetically modified strains of Trichoderma reesei. Kinetic of the enzymatic hydrolysis of rice bran at the constant-reaction rate period were measured. The best results for the ultrasound-assisted enzymatic hydrolysis was obtained using 3 wt% of enzyme, 60 oC and moisture content of 65 wt%, yielding 0.38 g sugar/g rice bran, whereas for the hydrolysis in the absence of ultrasound the highest yield was 0.20 g sugar/g rice bran using 3 wt% of enzyme, 60 oC and moisture content of 50 wt%. The use of ultrasound-assisted enzymatic hydrolysis of rice bran was intensified, obtaining around 74% more fermentable sugar than in the absence, showing that the use of ultrasound is a promising technology to be used in enzymatic reaction as an alternative of process intensification.

  17. An easy way to obtain strong duality results in linear, linear semidefinite and linear semi-infinite programming

    NARCIS (Netherlands)

    Pop, P.C.; Still, Georg J.

    1999-01-01

    In linear programming it is known that an appropriate non-homogeneous Farkas Lemma leads to a short proof of the strong duality results for a pair of primal and dual programs. By using a corresponding generalized Farkas lemma we give a similar proof of the strong duality results for semidefinite

  18. Influence of the microstructure on the resulting 18R martensitic transformation of polycrystalline Cu−Al−Zn thin films obtained by sputtering and reactive annealing

    International Nuclear Information System (INIS)

    Domenichini, P.; Condó, A.M.; Soldera, F.; Sirena, M.; Haberkorn, N.

    2016-01-01

    We report the influence of the microstructure on the martensitic transformation in polycrystalline Cu−Zn−Al thin films with 18R structure. The films are grown in two steps. First, Cu−Al thin films are obtained by DC sputtering. Second, the Zn is introduced in the Cu−Al thin films by the annealing them together with a bulk Cu−Zn−Al reference. The crystalline structure of the films was analyzed by X-ray diffraction and transmission electron microscopy. The martensitic transformation temperature was measured by electrical transport using conventional four probe geometry. It was observed that temperatures above 973 K are necessary for zincification of the samples to occur. The resulting martensitic transformation and its hysteresis (barrier for the transformation) depend on the grain size, topology and films thickness. - Highlights: • Polycrystalline Cu−Al−Zn thin films with nanometric grain size are sintered. • Influence of thermal annealing process on the microstructure is analyzed. • Martensitic transformation of Cu−Al−Zn thin films is strongly affected by the microstructure.

  19. Influence of the microstructure on the resulting 18R martensitic transformation of polycrystalline Cu−Al−Zn thin films obtained by sputtering and reactive annealing

    Energy Technology Data Exchange (ETDEWEB)

    Domenichini, P. [Instituto Balseiro, Bustillo 9500, S. C. de Bariloche (Argentina); Condó, A.M. [Instituto Balseiro, Bustillo 9500, S. C. de Bariloche (Argentina); Centro Atómico Bariloche, Comisión Nacional de Energía Atómica, Av. Bustillo 9500, 8400 San Carlos de Bariloche (Argentina); Soldera, F. [Department of Materials Science & Engineering, Saarland University, D-66123 Saarbruecken (Germany); Sirena, M. [Instituto Balseiro, Bustillo 9500, S. C. de Bariloche (Argentina); Centro Atómico Bariloche, Comisión Nacional de Energía Atómica, Av. Bustillo 9500, 8400 San Carlos de Bariloche (Argentina); Haberkorn, N., E-mail: nhaberk@cab.cnea.gov.ar [Instituto Balseiro, Bustillo 9500, S. C. de Bariloche (Argentina); Centro Atómico Bariloche, Comisión Nacional de Energía Atómica, Av. Bustillo 9500, 8400 San Carlos de Bariloche (Argentina)

    2016-04-15

    We report the influence of the microstructure on the martensitic transformation in polycrystalline Cu−Zn−Al thin films with 18R structure. The films are grown in two steps. First, Cu−Al thin films are obtained by DC sputtering. Second, the Zn is introduced in the Cu−Al thin films by the annealing them together with a bulk Cu−Zn−Al reference. The crystalline structure of the films was analyzed by X-ray diffraction and transmission electron microscopy. The martensitic transformation temperature was measured by electrical transport using conventional four probe geometry. It was observed that temperatures above 973 K are necessary for zincification of the samples to occur. The resulting martensitic transformation and its hysteresis (barrier for the transformation) depend on the grain size, topology and films thickness. - Highlights: • Polycrystalline Cu−Al−Zn thin films with nanometric grain size are sintered. • Influence of thermal annealing process on the microstructure is analyzed. • Martensitic transformation of Cu−Al−Zn thin films is strongly affected by the microstructure.

  20. Obtaining of Solids With Potential Corrosion Inhibitory Effects by Electrocoagulation Vinasse Methods

    Directory of Open Access Journals (Sweden)

    Dra. Elaine Ojeda-Armaignac

    2015-11-01

    Full Text Available In this paper, electrocoagulation experiments are performed at different vinasse samples with a viewto obtaining solids with potential corrosion inhibitory effects. Experimental tests were performed with samples of complex sugar «Argeo Martínez» Guantánamo province, «Urbano Noris Holguín province, in the antique complex Destillery-Brewery «Hatuey» of the province of Santiago de Cuba and in the rum factory of Appleton» in Kingston Jamaica. Electrocoagulation preliminary tests performed with the vinasse from distilleries of Santiago de Cuba, Guantánamo and Holguín allowed the definition of thevariables and their domain, which were considered in the design of experiments to obtain the most favorable conditions of operation. Preliminary experiments corroborated that increasing the current density and pH, increase linearly solids obtained and current density values exceeding 0,194 5 A/cm2 are not feasible because they increase the energy consumption process and the increase of solids is negligible. Validation of electrocoagulation method was demonstrated with results of the experimentaldesign from Jamaica´s vinasse, that were similar to those obtained with Cuban vinasse; reaching favorable conditions for operation at current density of 0,194 5/cm2, pH equal to 8,97 and time 5,6 min, resulting in 15,42 g of total solids for a minimum consumption of 8,44 kW·h/kg.

  1. A method to obtain new cross-sections transport equivalent

    International Nuclear Information System (INIS)

    Palmiotti, G.

    1988-01-01

    We present a method, that allows the calculation, by the mean of variational principle, of equivalent cross-sections in order to take into account the transport and mesh size effects on reactivity variation calculations. The method validation has been made in two and three dimensions geometries. The reactivity variations calculated in three dimensional hexagonal geometry with seven points by subassembly using two sets of equivalent cross-sections for control rods are in a very good agreement with the ones of a transport, extrapolated to zero mesh size, calculation. The difficulty encountered in obtaining a good flux distribution has lead to the utilisation of a single set of equivalent cross-sections calculated by starting from an appropriated R-Z model that allows to take into account also the axial transport effects for the control rod followers. The global results in reactivity variations are still satisfactory with a good performance for the flux distribution. The main interest of the proposed method is the possibility to simulate a full 3D transport calculation, with fine mesh size, using a 3D diffusion code, with a larger mesh size. The results obtained should be affected by uncertainties, which do not exceed ± 4% for a large LMFBR control rod worth and for very different rod configurations. This uncertainty is by far smaller than the experimental uncertainties. (author). 5 refs, 8 figs, 9 tabs

  2. The comparison of two methods to obtain human oral keratinocytes in primary culture

    International Nuclear Information System (INIS)

    Klingbeil, Maria Fatima Guarizo

    2006-01-01

    The therapeutic procedures frequently used in oral treatments for the pathological diseases are surgical, resulting in failures of the mucosal continuity.The possibility to obtain transplantable oral epithelia from an in vitro cell culture opens new utilization perspectives not only to where it comes from, but also as a reconstructive material for other parts of the human body, such as: urethra, epithelia corneo-limbal, cornea, ocular surface. Many researchers still use controversial methods for obtaining cells. It was therefore evaluated and compared the efficiency in both methods: enzymatic and direct explant to obtain oral keratinocytes from human oral mucosa. Fragments of intra oral epithelial tissues from healthy human subjects, undergoing dental surgeries, were donated to the research project. The keratinocytes were cultivated over a feeder-layer from a previously irradiated 3T3 Swiss albino fibroblasts. In this study it was compared the time needed in the cell obtention, the best cell amount between both methods, the life-span, the cell capacity to form an in vitro epithelia and its morphologic structure. The results in the assessment of both methods have shown the possibility to obtain keratinocytes from a small oral fragment, but at the same time we may verify the advantages and peculiar restrictions for each one of both analyzed methods. (author)

  3. Report on the finally obtained results of the study of the basement technology for environmentally friendly type metal base material regenerative utilization; Kankyo chowagata kinzokukei sozai kaisei riyo kiban gijutsu no kenkyu saishu seika hokokusho

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2000-07-01

    For the purpose of contributing to the resource recycling and global environmental preservation, the R and D of metal base scrap regenerative utilization technology were conducted, and the report on the finally obtained results was summed up. As to the technology to remove impurities by the solid phase treatment, the Cu removal rate of more than 96% was made possible by the low temperature fracturing technology, and that of more than 90% by the hue difference discrimination separation system technology. From the results of the FS on the low temperature fracturing technology applied to car scraps, it was found out that the present price condition is not economically efficient in the present price condition, but a possibility of achieving the removal rate of 54% in the initial plan was obtained if applying the hue difference discrimination separation system to the pretreatment. Concerning the Sn removal, the Sn removal rate of more than 70% was obtained by the gaseous phase sulfuration method, and that of more than 50% was obtained in Sn removal/Cu removal/Zn removal by the oxidation reaction method. The targets were achieved. Relating to the treatment of impurities by melting (liquid phase), the Cu removal/Sn removal technology under reduced pressure was effective in vacuum melting furnace of 2-ton scale, but the needs for the development of large capacity plasma torch were recognized in that of 40-ton scale for practical use. (NEDO)

  4. Vehicle Animation Software (VAS) to Animate Results Obtained from Vehicle Handling and Rollover Simulations and Tests

    Science.gov (United States)

    1991-04-01

    Results from vehicle computer simulations usually take the form of numeric data or graphs. While these graphs provide the investigator with the insight into vehicle behavior, it may be difficult to use these graphs to assess complex vehicle motion. C...

  5. Friction and wear in liquid-metal systems: comparability problems of test results obtained from different test facilities

    International Nuclear Information System (INIS)

    Wild, E.; Mack, K.J.

    1976-01-01

    Operational induced relative movements take place between contacting components in the core region of sodium cooled reactors. To ensure reliable long term functioning of such friction loaded components, materials are needed with good sliding properties and high wear resistance. Therefore, tribological properties of material combinations in liquid metal have been investigated experimentally for many years at various research establishments. However, despite identical boundary conditions, the comparison of results published does not yield a satisfactory agreement. The cause must be seen in the individual design and concept of the test sections used. This discrepancy was investigated. The results show that the elasticity, mass movement, and relative motion characteristic to the system prove to be the most important criteria influencing the test results

  6. Obtaining of interspecific hybrids for pea introgressive breeding

    Directory of Open Access Journals (Sweden)

    Sergey Vasilevich Bobkov

    2015-09-01

    Full Text Available Background. Overcoming of reproductive isolation, identification and transfer of agronomic value genes from wild relatives into cultivated pea genomes is an important task for pea introgressive breeding. Materials and methods. Reciprocal hybridization of cultivated pea with wide set of P. fulvum accessions was conducted. Identification of hybrids was carried out with use of biochemical and morphological markers. Identification of unique protein was conducted with use of electrophoretic spectra of mature seeds. Results. Pea interspecific hybrids were obtained in two reciprocal directions of crosses. Cross efficiency in Р. sativum × P. fulvum and P. fulvum × Р. sativum combinations was 36 % and 7 %, respectively. All tested seeds in crosses Р. sativum × P. fulvum were hybrids. Crosses in direction P. fulvum × Р. sativum led to formation of puny seeds restricted in embryo growth. Protein markers of one seed derived in cross P. fulvum × Р. sativum proved its hybrid nature. Morphological markers demonstrated that plant derived from another cross was also a hybrid. Culture of immature embryos was developed for recovering plants in interspecific crosses. Morphogenic calli and regenerated plants were obtained in culture of immature embryos P. fulvum (И592589 × Р. sativum (Aest. Identification of unique protein 7 of P. fulvum was conducted. Inheritance of that protein was proved as monogenic dominant. Conclusion. Efficiency of hybridization in combination P. fulvum × Р. sativum was significantly less in compare to reciprocal one. All products of that cross combination were tested as hybrids. Unique protein 7 of P. fulvum was revealed as a result of mature seed electrophoretic spectra analysis. Inheritance of that protein was determined as monogenic dominant.

  7. Results from CrIS-ATMS Obtained Using the AIRS Science Team Retrieval Methodology

    Science.gov (United States)

    Susskind, Joel; Kouvaris, Louis C.; Iredell, Lena

    2013-01-01

    which significantly improved results of AIRS Version-6. Version-5.70 CrIS/ATMS temperature profile and surface skin temperature retrievals are of very good quality, and are better than AIRS Version-5 retrievals, but are still significantly poorer than those of AIRS Version-6. CrIS/ATMS retrievals should improve when a Neural-Net start-up system is ready for use. We also examined CrIS/ATMS retrievals generated by NOAA using their NUCAPS retrieval algorithm, which is based on earlier versions of the AIRS Science Team retrieval algorithms. We show that the NUCAPS algorithm as currently configured is not well suited for climate monitoring purposes.

  8. Study liquid length penetration results obtained with a direct acting piezo electric injector

    International Nuclear Information System (INIS)

    Payri, Raul; Gimeno, Jaime; Bardi, Michele; Plazas, Alejandro H.

    2013-01-01

    Highlights: ► A direct acting injector capable of controlling needle lift has been used to determine liquid phase penetration. ► The influence of injection pressure, chamber density and chamber temperature have been measured. ► When needle lift is reduced the stabilized liquid length is shortened. ► The relationship between needle lift and liquid length makes needle lift as a new way to control the injection event. - Abstract: A state of the art prototype common rail injector featuring direct control of the needle by means of a piezo stack (direct acting) has been tested. Liquid phase penetration of the sprays in diesel engine-like conditions has been studied via imaging technique in a novel continuous flow test chamber that allows an accurate control on a wide range of thermodynamic conditions (up to 1000 K and 15 MPa). This state of the art injector fitted with a 7-hole nozzle, allows a fully flexible control on the nozzle needle movement, enabling various fuel injection rate typologies. The temporal evolution of the seven sprays has been studied recording movies of the injection event in evaporative conditions via Mie scattering imaging technique and using a high speed camera. The results showed a strong influence of needle position on the stabilized liquid length while the effect of the injection pressure is negligible: the decrease of the needle lift causes a pressure drop in the needle seat and thus a reduction in the effective pressure upstream of the orifices (in the nozzle sac). According to known literature the stabilized liquid-length depends mainly on effective diameter, spray cone-angle and fuel/air properties and does not depend on fuel velocity at the orifice outlet. Therefore, due to small change in the spray cone-angle, higher injection pressures give slightly lower liquid length. However, partial needle lifts has an opposite effect: when needle is partially lifted a dramatic increase of the spray cone-angle and a consequent reduction of

  9. Comparison of ATLAS tilecal module No. 8 high-precision metrology measurement results obtained by laser (JINR) and photogrammetric (CERN) methods

    International Nuclear Information System (INIS)

    Batusov, V.; Budagov, Yu.; Gayde, J.C.

    2002-01-01

    The high-precision assembly of large experimental set-ups is of a principal necessity for the successful execution of the forthcoming LHC research programme in the TeV-beams. The creation of an adequate survey and control metrology method is an essential part of the detector construction scenario. This work contains the dimension measurement data for ATLAS hadron calorimeter MODULE No. 8 (6 m, 22 tons) which were obtained by laser and by photogrammetry methods. The comparative data analysis demonstrates the measurements agreement within ± 70 μm. It means, these two clearly independent methods can be combined and lead to the rise of a new-generation engineering culture: high-precision metrology when precision assembling of large scale massive objects

  10. Comparison of ATLAS Tilecal MODULE No 8 high-precision metrology measurement results obtained by laser (JINR) and photogrammetric (CERN) methods

    CERN Document Server

    Batusov, V; Gayde, J C; Khubua, J I; Lasseur, C; Lyablin, M V; Miralles-Verge, L; Nessi, Marzio; Rusakovitch, N A; Sissakian, A N; Topilin, N D

    2002-01-01

    The high-precision assembly of large experimental set-ups is of a principal necessity for the successful execution of the forthcoming LHC research programme in the TeV-beams. The creation of an adequate survey and control metrology method is an essential part of the detector construction scenario. This work contains the dimension measurement data for ATLAS hadron calorimeter MODULE No. 8 (6 m, 22 tons) which were obtained by laser and by photogrammetry methods. The comparative data analysis demonstrates the measurements agreement within +or-70 mu m. It means, these two clearly independent methods can be combined and lead to the rise of a new-generation engineering culture: high-precision metrology when precision assembling of large scale massive objects. (3 refs).

  11. Study of the nuclear multifragmentation: recent results obtained with the INDRA detector in the intermediate energy domain

    International Nuclear Information System (INIS)

    Saint-Laurent, F.

    1994-01-01

    The new 4π multidetector INDRA, designed for the study of hot nuclear systems decaying by multifragmentation, is available for experiments since the beginning of 1993. First results emphasize its very high detection capabilities. Preliminary results on multiplicity distributions and elemental charge distributions in the most violent collisions for the 36 Ar + 58 Ni and 129 Xe + nat Sn systems are presented. (author) 5 figs., 22 refs

  12. A new look on anomalous thermal gradient values obtained in South Portugal

    Science.gov (United States)

    Duque, M. R.; Malico, I.

    2012-04-01

    A NEW LOOK ON THE ANOMALOUS THERMAL GRADIENT VALUES OBTAINED IN SOUTH PORTUGAL Duque, M. R. and Malico, I. M. Physics Department, University of Évora, Rua Romão Ramalho, 59,7000-671, Évora, Portugal It is well known that soil temperatures can be altered by water circulation. In this paper, we study numerically this effect by simulating some aquifers occurring in South Portugal. At this location, the thermal gradient values obtained in boreholes with depths less than 200 m, range between 22 and 30 °C km-1. However, there, it is easy to find places where temperatures are around 30 °C, at depths of 100 m. The obtained thermal gradient values show an increase one day after raining and a decrease during the dry season. Additionally, the curve of temperature as function of depth showed no hot water inlet in the hole. The region studied shows a smooth topography due to intensive erosion, but it was affected by alpine and hercinian orogenies. As a result, a high topography in depth, with folds and wrinkles is present. The space between adjacent folds is now filled by small sedimentary basins. Aquifers existing in this region can reach considerable depths and return to depths near the surface, but hot springs in the area are scarce. Water temperature rises in depth, and when the speed is high enough high temperatures near the surface, due to water circulation, can be found. The ability of the fluid to flow through the system depends on topography relief, rock permeability and basal heat flow. In this study, the steady-state fluid flow and heat transfer by conduction and advection are modeled. Fractures in the medium are simulated by an equivalent porous medium saturated with liquid. Thermal conductivity values for the water and the rocks can vary in space .Porosities used have high values in the region of the aquifer, low values in the lower region of the model and intermediate values in the upper regions. The results obtained show that temperature anomaly values

  13. Antimicrobial material obtained from pulping white paper waste

    International Nuclear Information System (INIS)

    Angioletto, E.; Fiori, M.A.; Pitch, C.T.; Mendes, E.; Oliveira, C.M.; Melo, C.R.; Riella, H.G.

    2011-01-01

    The paper industry produces white waste, consisting of 45% kaolin, 45% calcium carbonate and 10% cellulose. After calcination at 903K for two hours, the cellulose is burnt and decomposed kaolin in metakaolin. Held treatment of the calcined material with hydrochloric acid to remove calcium carbonate. The metakaolin is treated with sodium hydroxide solution to obtain the type of zeolite 4A. The zeolites were characterized using XRD, XRF and SEM. The zeolite was subjected to ion exchange with zinc sulphate and silver nitrate at room temperature, stirring, for six hours. This material was tested with Staphylococcus aureus and Escherichia coli, to get excellent results with regard to bactericidal properties.(author)

  14. Using Internet Search Engines to Obtain Medical Information: A Comparative Study

    Science.gov (United States)

    Wang, Liupu; Wang, Juexin; Wang, Michael; Li, Yong; Liang, Yanchun

    2012-01-01

    Background The Internet has become one of the most important means to obtain health and medical information. It is often the first step in checking for basic information about a disease and its treatment. The search results are often useful to general users. Various search engines such as Google, Yahoo!, Bing, and Ask.com can play an important role in obtaining medical information for both medical professionals and lay people. However, the usability and effectiveness of various search engines for medical information have not been comprehensively compared and evaluated. Objective To compare major Internet search engines in their usability of obtaining medical and health information. Methods We applied usability testing as a software engineering technique and a standard industry practice to compare the four major search engines (Google, Yahoo!, Bing, and Ask.com) in obtaining health and medical information. For this purpose, we searched the keyword breast cancer in Google, Yahoo!, Bing, and Ask.com and saved the results of the top 200 links from each search engine. We combined nonredundant links from the four search engines and gave them to volunteer users in an alphabetical order. The volunteer users evaluated the websites and scored each website from 0 to 10 (lowest to highest) based on the usefulness of the content relevant to breast cancer. A medical expert identified six well-known websites related to breast cancer in advance as standards. We also used five keywords associated with breast cancer defined in the latest release of Systematized Nomenclature of Medicine-Clinical Terms (SNOMED CT) and analyzed their occurrence in the websites. Results Each search engine provided rich information related to breast cancer in the search results. All six standard websites were among the top 30 in search results of all four search engines. Google had the best search validity (in terms of whether a website could be opened), followed by Bing, Ask.com, and Yahoo!. The search

  15. Lithium storage into carbonaceous materials obtained from sugarcane bagasse

    International Nuclear Information System (INIS)

    Matsubara, Elaine Y.; Lala, Stella M.; Rosolen, Jose Mauricio

    2010-01-01

    Carbonaceous materials with different structures are prepared by carbonization of sugarcane bagasse. Depending on carbonization conditions, it is possible to obtain soot rich in flakes or in honeycomb-shaped micrometric particles, whose concentration has large influence on lithium storage into electrodes. The soot rich in honeycomb-shaped particles provides the best electrochemical performance, with a reversible specific capacity of 310 mAh g -1 . The results suggest that the sugarcane bagasse can be potentially used in the design of anodic materials for lithium ion batteries. (author)

  16. Techniques for combining isotopic images obtained at different energies

    International Nuclear Information System (INIS)

    Soussaline, F.; Di Paola, R.; Bazin, J.P.

    1976-01-01

    The technique described should be considered as a first step towards the classification of scintigraphic data where the energy is included. As in all such studies the interpretation of the resulting images is not necessarily at first evident, and certain experience needs to be established. This applies in particular to the images obtained with the higher factors. It is possible that the use of this technique may resolve, without requiring a priori information, the problem previously encountered using the other 'subtraction' type techniques [fr

  17. Chelate forms of biometalls. Theoretical aspects of obtaining and characteristics

    Directory of Open Access Journals (Sweden)

    A. Kapustyan

    2017-04-01

    Full Text Available The problem of microelements bioavailability is highlighted and the correct ways of its solution are substantiated as a result of generalization of theoretical aspects of obtaining of the biometals chelate forms. The characteristics of the main biogenic elements, their physiological significance, electrochemical properties are presented. The main examples of the participation of biometals in various biological processes are given. The properties and the structure peculiarities of biometals coordination complexes are considered in detail. It is shown that in obtaining of biometals chelate forms, there is the mutual selectivity and the affinity of biometals and ligands. The main factors of obtaining a hard metal complex are given. Potential bioligands for obtaining bioavailable forms of microelements are detailed. Among them there are amino acids, peptides, proteins, nucleic acids, carbohydrates. The possible character of complexation depending on the nature of the bioligand is indicated. Practical examples of preparation of biometals mixed ligand complexes are given. The expediency of using metabolic products and processing of lactic acid bacteria as promising components of mixed ligand chelate complexes is substantiated. These substances contain in their composition a mass of potential donor atoms that are capable to form covalent and coordination bonds with biomethalles, and also possess high biological and immunotropic activities. The use of this system in the biocoordination compounds of the "metals of life" can provide a synergistic effect of the components, significantly to expand the range of their physiological activity and to increase the degree of assimilation by the body.

  18. The obtaining of giant laser pulses by optical pumping

    International Nuclear Information System (INIS)

    Briquet, Georges

    1970-12-01

    From coherent pumping studies a laser of short pulse duration was developed. Further study of laser effects in organic substances was envisaged. The first part of the work yielded awaited results, and led to the development of a single mode emitter (due to the small dimensions of the cavity). The principles of laser action were enumerated and the relative parameters defined. Various methods of obtaining pulses were discussed; the reasons behind the particular choice mode were given. A theoretical study was then made leading to the establishment of the fundamental equations defining the pulse formation process. An important part of the test deals with technical implications and the experimental results, which have arisen. The conclusion reviews possible applications. (author) [fr

  19. Ozonation and sol-gel method to obtain Cu/Cu O nanoparticles from cyanidation wastewater

    Energy Technology Data Exchange (ETDEWEB)

    Soria A, M. J.; Puente S, D. M.; Carrillo P, F. R. [Universidad Autonoma de Coahuila, Facultad de Metalurgia, Carretera 57 Km 4.5, 25710 Monclova, Coahuila (Mexico); Garcia C, L. A. [Centro de Investigacion en Quimica Aplicada, Blvd. Enrique Reyna No. 140, Col. Los Pinos, 25253 Saltillo, Coahuila (Mexico); Velazquez S, J., E-mail: frrcarrillo@yahoo.com.mx [University of Texas at San Antonio, Department of Physics and Astronomy, San Antonio TX 78249 (United States)

    2015-07-01

    The extraction process of gold and silver by cyanidation generates large amounts of effluent which also contain contaminants such as cyanide and significant metal values such as copper. This paper presents the results of the removal and recovery of copper from ozonation treatment of a residual aqueous cyanide. The residual solution was treated by ozonation-precipitation to obtain a precipitate of copper. From this, copper nano composites obtained by Pechini modified sol-gel method were obtained. The compounds obtained were characterized by X-ray diffraction, showing a dependence of the type of compounds formed over time of ozonation and heat treatment of the gel. The particle size was measured by scanning electron microscopy and calculated by the Scherrer equation, being between 50 and 120 nm. (Author)

  20. Rotation technique for irradiation of the bladder and the results obtained

    Energy Technology Data Exchange (ETDEWEB)

    Backhouse, T W [Coventry and Warwickshire Hospital (UK). Dept. of Radiotherapy and Oncology

    1979-05-01

    An argument is advanced for the use of partial rotational techniques for the treatment of carcinoma of the bladder. One hundred and seventy cases are analysed; the majority were T3 solid transitional cell lesions with an overall (corrected) survival rate of 24.7%. Salvage cystectomy produced a four-year survival rate of 40% when performed within six months of the radiotherapy.

  1. Polythiophene films obtained by polymerization under atmospheric pressure plasma conditions

    Energy Technology Data Exchange (ETDEWEB)

    Teslaru, T.; Topala, I., E-mail: ionut.topala@uaic.ro; Dobromir, M.; Pohoata, V.; Curecheriu, L.; Dumitrascu, N.

    2016-02-01

    The present work describes the experimental arrangement used to initiate polymerization reactions of thiophene monomer based on a dielectric barrier discharge with plane – parallel geometry, working at atmospheric pressure in argon, in turn to obtain conductive polymeric films for different applications. The resulting plasma polymerized polythiophene (pPTh) film was characterized by FT-IR, UV–Vis, XPS spectroscopy, AFM and contact angle measurements. Characterization of pPTh films showed a higher hydrophobic character and roughness, as compared with films obtained by chemical methods, and the thickness is depending on polymerization duration. Also it can conclude that our samples represent oxidised state of pPTh. As a possible application, it analysed in situ the iodine absorption phenomenon in the pPTh matrix and its time evolution by UV–Vis spectroscopy. The presence of iodine 3d{sub 5/2} and 3d{sub 3/2} peaks in the pPTh sample after absorption was identified by XPS spectroscopy. The hydrophobic pPTh film is transformed in a super hydrophilic film after absorption of iodine vapors. - Highlights: • We obtained polythiophene films (pPTh) by atmospheric pressure plasma technique. • The pPTh films showed a hydrophobic character and conducting properties. • The pPTh films were used as sensor for iodine vapors in biological environment.

  2. Report of test and research results on atomic energy obtained in national institutes in fiscal 1990

    International Nuclear Information System (INIS)

    1991-01-01

    The tests and researches on the development and utilization of atomic energy in national laboratories were begun in 1956, and have accomplished the great role for the advance of the development and utilization of atomic energy in Japan by having produced many valuable results so far. Atomic energy has been utilized in diverse fields, and also in national laboratories, the research for expanding the development and utilization of atomic energy in food irradiation, medicine, agriculture, forestry, fishery and others in addition to the basic research on nuclear fusion and safety have been advanced. Further expecting the pervasive effect to general science and technology, the development of basic technology and integrated research are promoted from the viewpoint of new techical innovation and creative technology. This is 31st report in which the results of the tests and researches carried out by national laboratories in fiscal year 1990 are summarized. Nuclear fusion, safety research, food irradiation, cancer countermeasures, agriculture, forestry, fishery, medicine, mining and manufacture, power utilization, construction, radioactivation analysis and so on were the main subjects. (K.I.)

  3. Report of test and research results on atomic energy obtained in national institutes in fiscal 1983

    International Nuclear Information System (INIS)

    1984-01-01

    As for the test and research on the utilization of atomic energy by national organizations, the budget was appropriated for the first time in fiscal year 1956. Since then, many valuable results of research have been produced in the diverse fields of nuclear fusion, safety research, food irradiation, medicine and others, in this way, the test and research have played large roles in the promotion of the utilization of atomic energy in Japan. This is the 24th report, in which the results of the test and research on the utilization of atomic energy carried out in fiscal year 1983 by national organizations are summarized. 5 researches on nuclear fusion, 19 researches on engineering safety and environmental radioactivity safety, 3 researches on food irradiation, 6 researches on the countermeasures to cancer, 19 researches on agriculture, forestry and fishery, 30 researches on medicine, pharmaceuticals and environmental hygiene, 6 researches on mining and industry, 6 researches on power reactors and nuclear ships, 1 research on agricultural water, 7 researches on activation analysis and 4 researches on injury prevention are reported. (Kako, I.)

  4. Obtaining of ceramics biphasic dense and porous; Obtencao de ceramicas bifasicas densas e porosas

    Energy Technology Data Exchange (ETDEWEB)

    Pallone, E.M.J.A.; Rigo, E.C.S., E-mail: eliria@usp.b [Universidade de Sao Paulo (FZEA/USP), Pirassununga, SP (Brazil). Dept. de Ciencias Basicas; Silva, K.L. [Universidade Estadual de Campinas (FEM/UNICAMP), SP (Brazil). Faculdade de Engenharia Mecanica; Rezende, M.E. [Universidade Sao Francisco, Itatiba, SP (Brazil); Fraga, A.F. [Universidade Federal de Sao Carlos (DEMa/UFSCar), SP (Brazil). Dept. de Engenharia de Materiais; Marques, R.F.C. [Universidade Federal de Alfenas (UNIFAL), Pocos de Caldas, MG (Brazil)

    2010-07-01

    Among the bioceramic hydroxyapatite (HAP) and beta-tricalcium phosphate (beta-TCP) are materials commonly used in biomedical field. Their combined properties result in a material with absorbable and at the same time with bioactive surface. Called biphasic ceramics such materials respond more quickly when exposed to physiological environment. In this work, powders of HAP/beta-TCP were obtained by chemical precipitation. After obtaining the post-phase was added at a ratio of 0, 15% and 30w% aqueous solutions of corn starch in order to obtain porous bodies. After mixing the resulting solutions were dried, resigned in tablet form and sintered at 1300 deg C. The initial powder was characterized by X-ray diffraction with Rietveld refinement to quantify the phases present. Bodies-of-evidence has been characterized by calculating the bulk density, X-ray diffraction (XRD), scanning electron microscopy and diametral compression. (author)

  5. Mesoporous silicon oxide films and their uses as templates in obtaining nanostructured conductive polymers

    Science.gov (United States)

    Salgado, R.; Arteaga, G. C.; Arias, J. M.

    2018-04-01

    Obtaining conductive polymers (CPs) for the manufacture of OLEDs, solar cells, electrochromic devices, sensors, etc., has been possible through the use of electrochemical techniques that allow obtaining films of controlled thickness with positive results in different applications. Current trends point towards the manufacture of nanomaterials, and therefore it is necessary to develop methods that allow obtaining CPs with nanostructured morphology. This is possible by using a porous template to allow the growth of the polymeric materials. However, prior and subsequent treatments are required to separate the material from the template so that it can be evaluated in the applications mentioned above. This is why mesoporous silicon oxide films (template) are essential for the synthesis of nanostructured polymers since both the template and the polymer are obtained on the electrode surface, and therefore it is not necessary to separate the material from the template. Thus, the material can be evaluated directly in the applications mentioned above. The dimensions of the resulting nanostructures will depend on the power, time and technique used for electropolymerization as well as the monomer and the surfactant of the mesoporous film.

  6. Loss of high-molecular-weight cytokeratin antigenicity in prostate tissue obtained by transurethral resections

    DEFF Research Database (Denmark)

    Multhaupt, H A; Fessler, J N; Warhol, M J

    2000-01-01

    could be restored in these specimens by antigen retrieval in a low pH citrate buffer using a microwave heat technique. Keratin staining in needle biopsies and total prostatectomies was unaffected. CONCLUSION: In summary, our results indicate the technique of transurethral resection results in a specific......OBJECTIVE: Staining of prostatic basal cells for the expression of high-molecular-weight cytokeratin has been suggested as a way of distinguishing benign from malignant prostate glands. We evaluated the utility of high-molecular-weight cytokeratin in the diagnosis of malignancy in prostate...... specimens obtained in various ways. DESIGN: Prostate tissues obtained from needle biopsies, transurethral resections, and total prostatectomies were immunostained with monoclonal antibody 34betaE12, an antibody directed against high-molecular-weight cytokeratins. RESULTS: Antiserum to high...

  7. Process to Obtain Quick Counts from PREP

    Directory of Open Access Journals (Sweden)

    Martínez–Cruz M.Á.

    2011-10-01

    Full Text Available Considering the Preliminary Electoral Results Program (PERP as a database of the federal elections for president of the Mexican Republic, a methodology was developed in order to find representative samples of ballot boxes installed in the election’s day (quick count in different hours, due to its characteristics of gathering of information, the PREP in the first hours forms a non-representative sample of data. In a particular way, in the election of July 2, 2006, after 3 hours of opening the PREP, it was observed that the accuracy of the process of the quick counts was better than the one obtained by the IFE. Among other things, this allows to lower the cost, to increase the confidentiality of the ballot boxes used in the sampling and to distinguish in a precise moment the winning candidate long before PREP finishes.

  8. Obtain of uranium concentrates from fertil liquids

    International Nuclear Information System (INIS)

    Narvaez Castillo, W.A.

    1992-01-01

    This research tried to encounter the form to remove uranium from the rock in the best way, for that it was used different process like leaching, extraction, concentration and precipitation. To leach the mineral was chosen basic leaching, using a mixture of carbonate-sodium bicarbonate, this method is more adequated for the basic nature of the mineral. In extraction was used specific uranium ionic interchanges, so was chosen a tertiary amine like Alamina 336. The concentration phase is intimately binding with the extraction by ionic interchange, for the capability of resine's extraction to obtain concentrated liquids. When the liquids were obtained with high concentration of uranium in the same time were purified and then were precipitated, for that we employed a precipitant agent like: Sodium hydroxide, Amonium hydroxide, Magnesium hydroxide, Hydrogen peroxide and phosphates. With all concentrates we obtain the YELLOW CAKE

  9. Importance of clean-up for comparison of TEQ-values obtained by CALUX and chemo-analysis.

    Science.gov (United States)

    Van Wouwe, N; Windal, I; Vanderperren, H; Eppe, G; Xhrouet, C; De Pauw, E; Goeyens, L; Baeyens, W

    2004-08-08

    This paper presents Chemically Activated LUciferine gene eXpression (CALUX) TEQ-values obtained for nine plasma samples following two different purification procedures, one of them involving fractionation. CALUX results obtained for the dioxin (DX) and dioxin + PCB (DX + PCB) fractions were then compared to the GC-HRMS TEQ-values calculated for the 17 polychlorinated dibenzo-p-dioxins and polychlorinated dibenzofurans (17 PCDD/F) and 17 PCDD/F + 4 cPCB congeners, respectively. The overestimation of the CALUX (DX fraction) TEQ-values in comparison with the chemo-analyses of the 17 PCDD/F is mainly explained by the presence of other AhR agonists, like brominated compounds. Otherwise, the constancy of the CALUX (DX + PCB fraction) TEQ-value which compares to increasing the GC-HRMS (17 PCDD/F + 4 cPCB) TEQ results raises questions concerning (1) the significance of CALUX results obtained without fractionation as well as (2) the toxicological effect of a cocktail of contaminants on the human health.

  10. BN-based nano-composites obtained by pulsed laser deposition

    International Nuclear Information System (INIS)

    Major, B.; Kosydar, R.; Major, L; Mroz, W.; Burdynska, S.; Jelinek, M.; Kot, M.; Kustosz, R.

    2006-01-01

    Boron nitride thin layers were produced by means of the pulsed laser deposition technique from hexagonal boron nitride target. Two types of laser i.e. Nd: YAG with Q-switch as well as KrF coupled with RF generator were used. Influence of deposition parameters on surface morphology, phase composition as well as mechanical properties is discussed. Results obtained using Fourier Transformed Infrared Spectroscopy, Transmission and Scanning Electron Microscopy, Atomic Force Microscopy are presented. Micromechanical properties measured during micro indentation, scratch and wear tests are also shown. (authors)

  11. Multi-Grid detector for neutron spectroscopy: results obtained on time-of-flight spectrometer CNCS

    Science.gov (United States)

    Anastasopoulos, M.; Bebb, R.; Berry, K.; Birch, J.; Bryś, T.; Buffet, J.-C.; Clergeau, J.-F.; Deen, P. P.; Ehlers, G.; van Esch, P.; Everett, S. M.; Guerard, B.; Hall-Wilton, R.; Herwig, K.; Hultman, L.; Höglund, C.; Iruretagoiena, I.; Issa, F.; Jensen, J.; Khaplanov, A.; Kirstein, O.; Lopez Higuera, I.; Piscitelli, F.; Robinson, L.; Schmidt, S.; Stefanescu, I.

    2017-04-01

    The Multi-Grid detector technology has evolved from the proof-of-principle and characterisation stages. Here we report on the performance of the Multi-Grid detector, the MG.CNCS prototype, which has been installed and tested at the Cold Neutron Chopper Spectrometer, CNCS at SNS. This has allowed a side-by-side comparison to the performance of 3He detectors on an operational instrument. The demonstrator has an active area of 0.2 m2. It is specifically tailored to the specifications of CNCS. The detector was installed in June 2016 and has operated since then, collecting neutron scattering data in parallel to the He-3 detectors of CNCS. In this paper, we present a comprehensive analysis of this data, in particular on instrument energy resolution, rate capability, background and relative efficiency. Stability, gamma-ray and fast neutron sensitivity have also been investigated. The effect of scattering in the detector components has been measured and provides input to comparison for Monte Carlo simulations. All data is presented in comparison to that measured by the 3He detectors simultaneously, showing that all features recorded by one detector are also recorded by the other. The energy resolution matches closely. We find that the Multi-Grid is able to match the data collected by 3He, and see an indication of a considerable advantage in the count rate capability. Based on these results, we are confident that the Multi-Grid detector will be capable of producing high quality scientific data on chopper spectrometers utilising the unprecedented neutron flux of the ESS.

  12. Visual Perception Studies in CT images obtained lo low dose

    International Nuclear Information System (INIS)

    Adame Brooks, D.; Miller-Clemente, R. A.

    2015-01-01

    This paper has as aims to describe a strategy to evaluate the diagnostic quality of obtained images of method for dose reduction, with the purpose of determining the dose value or values from which the image quality is significantly degraded making it insufficient for the diagnostic. To complement and have an estimate of the quality of the images we established a group of measures of objective type, and the diagnostic quality of the images was evaluated through a group of observers using the analysis ROC and LROC. For ROC and LROC analyzes the behavior of the area under the curve in relation to the four proposed dose levels was obtained. For high dose levels, detection was good. The values of area under the curve decreased as the dose rate decreased, falling to values indicating low accuracy in diagnosis. This result indicates that the area under the curve decreases by the dose rate. We conclude that the objective quality measures selected are representative of the changes that occur in the resulting image and provided information on changes in the perception of observers. The experiments ROC and LROC allowed determine the range of dose values from which the image degradation causes a low accuracy in the diagnostic. (Author)

  13. In Silico Genomic Fingerprints of the Bacillus anthracis Group Obtained by Virtual Hybridization

    Directory of Open Access Journals (Sweden)

    Hueman Jaimes-Díaz

    2015-02-01

    Full Text Available In this study we evaluate the capacity of Virtual Hybridization to identify between highly related bacterial strains. Eight genomic fingerprints were obtained by virtual hybridization for the Bacillus anthracis genome set, and a set of 15,264 13-nucleotide short probes designed to produce genomic fingerprints unique for each organism. The data obtained from each genomic fingerprint were used to obtain hybridization patterns simulating a DNA microarray. Two virtual hybridization methods were used: the Direct and the Extended method to identify the number of potential hybridization sites and thus determine the minimum sensitivity value to discriminate between genomes with 99.9% similarity. Genomic fingerprints were compared using both methods and phylogenomic trees were constructed to verify that the minimum detection value is 0.000017. Results obtained from the genomic fingerprints suggest that the distribution in the trees is correct, as compared to other taxonomic methods. Specific virtual hybridization sites for each of the genomes studied were also identified.

  14. The structure of Cu-Cd alloys obtained by electrolysis on monocrystalline silver substrates

    International Nuclear Information System (INIS)

    Lagiewka, E.

    1981-01-01

    The structure of Cu-Cd alloys obtained by electrolysis on monocrystalline silver cathodes with a surface parallel to the (111), (110) and (100) planes has been investigated. It has been found that depending on the range of the cathode potentials, one-phase (phase α) or two-phase (phase α + cadmium) alloy are obtained. In the alloys the occurrence of twins has been observed, the orientation of which is the result of twinning along the [111] planes of crystallites with epitaxial orientation with respect to the cathode surface and of a random orientation of crystallites. The volume of the layer containing crystallites with a random arrangement increases with the obtaining potential of the alloy and with the decrease in the surface density of the cathode atoms. (author)

  15. 2D and 3D core-collapse supernovae simulation results obtained with the CHIMERA code

    Energy Technology Data Exchange (ETDEWEB)

    Bruenn, S W; Marronetti, P; Dirk, C J [Physics Department, Florida Atlantic University, 777 W. Glades Road, Boca Raton, FL 33431-0991 (United States); Mezzacappa, A; Hix, W R [Physics Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831-6354 (United States); Blondin, J M [Department of Physics, North Carolina State University, Raleigh, NC 27695-8202 (United States); Messer, O E B [Center for Computational Sciences, Oak Ridge National Laboratory, Oak Ridge, TN 37831-6354 (United States); Yoshida, S, E-mail: bruenn@fau.ed [Max-Planck-Institut fur Gravitationsphysik, Albert Einstein Institut, Golm (Germany)

    2009-07-01

    Much progress in realistic modeling of core-collapse supernovae has occurred recently through the availability of multi-teraflop machines and the increasing sophistication of supernova codes. These improvements are enabling simulations with enough realism that the explosion mechanism, long a mystery, may soon be delineated. We briefly describe the CHIMERA code, a supernova code we have developed to simulate core-collapse supernovae in 1, 2, and 3 spatial dimensions. We then describe the results of an ongoing suite of 2D simulations initiated from a 12, 15, 20, and 25 M{sub o-dot} progenitor. These have all exhibited explosions and are currently in the expanding phase with the shock at between 5,000 and 20,000 km. We also briefly describe an ongoing simulation in 3 spatial dimensions initiated from the 15 M{sub o-dot} progenitor.

  16. Characterization of High-Power Turbomachinery Tilting Pad Journal Bearings: First Results Obtained on a Novel Test Bench

    Directory of Open Access Journals (Sweden)

    Enrico Ciulli

    2018-01-01

    Full Text Available Tilting pad journal bearings are usually employed in turbomachines for their stable behavior at high rotational speeds. Devoted test rigs have been realized to validate the predictions of theoretical models. However, the design of new high-performance and large-size bearings needs to be supported by experimental investigations on high-performance large test rigs. The main characteristics of a recently built facility for testing large tilting pad journal bearings with diameters from 150 to 300 mm are described in this work. The test rig is versatile and can be used to test bearings of different size, configurations and to investigate the influence of many parameters, even the effect of misalignment. Sample results of the static characterization of a four-pad high-performance tilting pad journal bearing are reported evidencing some transient effects. A few sample dynamic results are also reported. The presented experimental results demonstrated the capabilities of the rig for investigating the static and the dynamic characteristics of the bearings accurately measuring slow and fast variables.

  17. Process for obtaining luminescent glass layers

    International Nuclear Information System (INIS)

    Heindi, R.; Robert, A.

    1984-01-01

    Process for obtaining luminescent glass layers, application to the production of devices provided with said layers and to the construction of photoscintillators. The process comprises projecting onto a support, by cathodic sputtering, the material of at least one target, each target including silica and at least one chemical compound able to give luminescent centers, such as a cerium oxide, so as to form at least one luminescent glass layer of the said support. The layer or layers formed preferably undergo a heat treatment such as annealing in order to increase the luminous efficiency thereof. It is in this way possible to form a scintillating glass layer on the previously frosted entrance window of a photomultiplier in order to obtain an integrated photoscintillator

  18. Radio-induced oxidation of n-paraffins for obtaining biodegradable detergents

    International Nuclear Information System (INIS)

    Puig, J.R.; Laizier, J.; Blin, M.F.; Marchand, J.

    1968-01-01

    N-paraffins oxidation is a feasible way to obtain biodegradable detergents. This reaction can be radio-initiated and it proceeds by a branched chain mechanism, with an induction pseudo-period. A suitable analysis of the reaction is allowed by the semi-logarithmic plot of its evolution. Influence of the different parameters of the reaction is studied, results show that the use of radiation for initiating the reaction is of no economical interest. (authors) [fr

  19. Using Internet search engines to obtain medical information: a comparative study.

    Science.gov (United States)

    Wang, Liupu; Wang, Juexin; Wang, Michael; Li, Yong; Liang, Yanchun; Xu, Dong

    2012-05-16

    The Internet has become one of the most important means to obtain health and medical information. It is often the first step in checking for basic information about a disease and its treatment. The search results are often useful to general users. Various search engines such as Google, Yahoo!, Bing, and Ask.com can play an important role in obtaining medical information for both medical professionals and lay people. However, the usability and effectiveness of various search engines for medical information have not been comprehensively compared and evaluated. To compare major Internet search engines in their usability of obtaining medical and health information. We applied usability testing as a software engineering technique and a standard industry practice to compare the four major search engines (Google, Yahoo!, Bing, and Ask.com) in obtaining health and medical information. For this purpose, we searched the keyword breast cancer in Google, Yahoo!, Bing, and Ask.com and saved the results of the top 200 links from each search engine. We combined nonredundant links from the four search engines and gave them to volunteer users in an alphabetical order. The volunteer users evaluated the websites and scored each website from 0 to 10 (lowest to highest) based on the usefulness of the content relevant to breast cancer. A medical expert identified six well-known websites related to breast cancer in advance as standards. We also used five keywords associated with breast cancer defined in the latest release of Systematized Nomenclature of Medicine-Clinical Terms (SNOMED CT) and analyzed their occurrence in the websites. Each search engine provided rich information related to breast cancer in the search results. All six standard websites were among the top 30 in search results of all four search engines. Google had the best search validity (in terms of whether a website could be opened), followed by Bing, Ask.com, and Yahoo!. The search results highly overlapped between the

  20. Left ventricle ejection fraction obtained by radioisotopic angiocardiography. Correlation between the values of the conventional ventriclegraphy

    International Nuclear Information System (INIS)

    Ascer, E.; Pimentel Filho, W.A.; Martins, L.R.F.; Marioni Filho, H.; Queiroga Filho, A.F.; Alonso, G.; Germek, O.A.; Thom, A.F.; Souza, J.E.M.R.

    1983-01-01

    Forty-two patients with clinical signs of coronary insuficiency underwent cineangiographic and radioisotopic examinations with the purpose of analysing the correlation between the values of left ventricle ejection fraction (LVEF) obtained by both methods. The values of EF obtained by the hemodynamic method (HEMO) ranged from 0.14 to 0.85 (x-bar = 0.566) and by radioisotopic method (RM) from 0.22 to 0.89 (x-bar = 0.573). The Student T test did not demonstrate statistically significant differences between the two methods (mean of differences = 0.007; t = 0.38 and p ≥ 0.353). A regression equation was obtained in order to estimate the EF by HEMO deriving from results obtained by RM (y = 0.11 + 0.80x) and to estimate the EF through RN from the results obtained by HEMO (x = 0.08 + 0.86y), where y = hemodynamic method and x = radioisotopic method. The authors conclude that the calculation of the EF by the methods used showed a good correlation and that this fact is evidenced by the elevated Pearson's correlation coefficient (r = 0.833). (author) [pt

  1. Irradiation devices for fusion reactor materials results obtained from irradiated lithium aluminate at the OSIRIS reactor

    International Nuclear Information System (INIS)

    Lefevre, F.; Thevenot, G.; Rasneur, B.; Botter, F.

    1986-06-01

    Studies about controlled fusion reactor of the Tokamak type require the examination of the radiation effects on the behaviour of various potential materials. Thus, in the first part of this paper, are presented the devices adapted to these materials studies and used in the OSIRIS reactor. In a second part, is described an experiment of irradiation ceramics used as candidates for breeding material and are given the first results

  2. Terminal solid solubility of hydrogen in titanium

    International Nuclear Information System (INIS)

    Giroldi, J.P.; Vizcaino, Pablo; Banchik, Abraham David

    2003-01-01

    A Research and Development program to build a data base is currently under progress to support the local titanium fabrication. In the present work the temperature of the Terminal Solid Solubility on dissolution (TSSd) and precipitation (TSSp) of titanium hydrides in the Ti α-phase were both measured in the same thermal cycle with a Differential Scanning Calorimeter (DSC). The local titanium producer (FAESA) provided ASTM grade 1 pure Ti bars of about 2,5 cm in diameter. Samples weighting between 50 to 200 mg were cut with a diamond disc and the parallelepiped faces were all carefully ground with SiC papers, then picked in a HNO 3 plus HF aqueous solution and finally dried out with ethanol and hot air. Pairs of (TSSd, TSSp) values for α + δ → α and α → α + δ transformation temperatures in titanium were determined with the same calorimetric procedure already used to calculate the TSS values in zirconium. Data were taken from the same sample during the heating up and cooling down cycle of the second calorimeter run made with the same rate of 20 C degrees / minute. The Cathodic Charging technique was used to charge the samples at different hydrogen concentrations between the 'as fabricated' value and the concentration corresponding to the eutectoid temperature. A mixture of glycerin and phosphoric acid in a 2:1 ratio and a current density of 0,05 to 0,1 Amp/cm 2 were applied to different samples during 24 to 96 hours to get a wide range of hydrogen concentrations. A homogenization heat treatment at 400 C degrees for 45 minutes -made at open air in an electric furnace- was applied to each sample to dissolve the massive hydrides at the sample surfaces and diffuse them into the bulk of the sample. The hydrogen concentration of each sample was measured after the final calorimetric run using the Extraction Method in Liquid State under an inert atmosphere using a Leco RH-404 model Hydrogen Determinator. The experimental data follows a linear relationship -with a

  3. Report of test and research results on atomic energy obtained in national institutes in fiscal 1982

    International Nuclear Information System (INIS)

    1983-01-01

    As for the test and research on the utilization of atomic energy by national organizations, the budget was appropriated for the first time in fiscal year 1956. Since then, many valuable results of research have been produced in the diverse fields of nuclear fusion, safety research, food irradiation, medicine and others, in this way, the test and research have played large roles in the promotion of the utilization of atomic energy in Japan. This is the 23rd report, in which the results of the test and research on the utilization of atomic energy carried out in fiscal year 1982 by national organizations are summarized. 5 researches on nuclear fusion, 12 researches on engineering safety, 5 researches on environmental radioactivity safety, 3 researches on food irradiation, 5 researches on the countermeasures to cancer, 8 researches on soil fertilization, 4 researches on quality improvement, 7 researches on crop protection, 5 researches on the improvement of breeding, 8 researches on diagnosis and treatment, 8 researches on pharmaceuticals, 10 researches on the application to pathology, 6 researches on mining and industry, 6 researches on power reactors and nuclear ships, 1 research on underground water, 6 researches on activation analysis and 3 researches on injury prevention are reported. (Kako, I.)

  4. Report of test and research results on atomic energy obtained in national institutes in fiscal 1992

    International Nuclear Information System (INIS)

    1994-01-01

    The tests and researches on the development and utilization of atomic energy in national laboratories were begun in 1956, and have accomplished the great role for the advance of the development and utilization of atomic energy in Japan by having produced many valuable results so far. Atomic energy has been utilized not only in the field of nuclear power but also in diverse fields, and in national laboratories, the research for expanding the development and utilization of atomic energy in medicine, agriculture, forestry, fishery, radioactivation analysis and others in addition the basic research on nuclear fusion have been advanced. Further expecting the pervasive effect to general science and technology, the development of integrated research are promoted from the viewpoint of new technical innovation and creative technology. The safety research of nuclear facilities have been carried out to keep them high level on the basis of the yearly program enacted by Nuclear Safety Commission. This is the report No. 33, in which the results of the test and research in the fields of nuclear fusion safety research, food irradiation, cancer countermeasures, agriculture, forestry, fishery, medicine, mining and manufacture, power utilization, construction, radioactivation analysis carried on in fiscal 1992 are summarized. (J.P.N.)

  5. Treatment of biomass to obtain ethanol

    Science.gov (United States)

    Dunson, Jr., James B.; Elander, Richard T [Evergreen, CO; Tucker, III, Melvin P.; Hennessey, Susan Marie [Avondale, PA

    2011-08-16

    Ethanol was produced using biocatalysts that are able to ferment sugars derived from treated biomass. Sugars were obtained by pretreating biomass under conditions of high solids and low ammonia concentration, followed by saccharification.

  6. Simbol-X Hard X-ray Focusing Mirrors: Results Obtained During the Phase A Study

    Science.gov (United States)

    Tagliaferri, G.; Basso, S.; Borghi, G.; Burkert, W.; Citterio, O.; Civitani, M.; Conconi, P.; Cotroneo, V.; Freyberg, M.; Garoli, D.; Gorenstein, P.; Hartner, G.; Mattarello, V.; Orlandi, A.; Pareschi, G.; Romaine, S.; Spiga, D.; Valsecchi, G.; Vernani, D.

    2009-05-01

    Simbol-X will push grazing incidence imaging up to 80 keV, providing a strong improvement both in sensitivity and angular resolution compared to all instruments that have operated so far above 10 keV. The superb hard X-ray imaging capability will be guaranteed by a mirror module of 100 electroformed Nickel shells with a multilayer reflecting coating. Here we will describe the technogical development and solutions adopted for the fabrication of the mirror module, that must guarantee an Half Energy Width (HEW) better than 20 arcsec from 0.5 up to 30 keV and a goal of 40 arcsec at 60 keV. During the phase A, terminated at the end of 2008, we have developed three engineering models with two, two and three shells, respectively. The most critical aspects in the development of the Simbol-X mirrors are i) the production of the 100 mandrels with very good surface quality within the timeline of the mission, ii) the replication of shells that must be very thin (a factor of 2 thinner than those of XMM-Newton) and still have very good image quality up to 80 keV, iii) the development of an integration process that allows us to integrate these very thin mirrors maintaining their intrinsic good image quality. The Phase A study has shown that we can fabricate the mandrels with the needed quality and that we have developed a valid integration process. The shells that we have produced so far have a quite good image quality, e.g. HEW <~30 arcsec at 30 keV, and effective area. However, we still need to make some improvements to reach the requirements. We will briefly present these results and discuss the possible improvements that we will investigate during phase B.

  7. Simbol-X Hard X-ray Focusing Mirrors: Results Obtained During the Phase A Study

    International Nuclear Information System (INIS)

    Tagliaferri, G.; Basso, S.; Civitani, M.; Conconi, P.; Cotroneo, V.; Pareschi, G.; Spiga, D.; Borghi, G.; Garoli, D.; Mattarello, V.; Orlandi, A.; Valsecchi, G.; Vernani, D.; Burkert, W.; Freyberg, M.; Hartner, G.; Citterio, O.; Gorenstein, P.; Romaine, S.

    2009-01-01

    Simbol-X will push grazing incidence imaging up to 80 keV, providing a strong improvement both in sensitivity and angular resolution compared to all instruments that have operated so far above 10 keV. The superb hard X-ray imaging capability will be guaranteed by a mirror module of 100 electroformed Nickel shells with a multilayer reflecting coating. Here we will describe the technogical development and solutions adopted for the fabrication of the mirror module, that must guarantee an Half Energy Width (HEW) better than 20 arcsec from 0.5 up to 30 keV and a goal of 40 arcsec at 60 keV. During the phase A, terminated at the end of 2008, we have developed three engineering models with two, two and three shells, respectively. The most critical aspects in the development of the Simbol-X mirrors are i) the production of the 100 mandrels with very good surface quality within the timeline of the mission, ii) the replication of shells that must be very thin (a factor of 2 thinner than those of XMM-Newton) and still have very good image quality up to 80 keV, iii) the development of an integration process that allows us to integrate these very thin mirrors maintaining their intrinsic good image quality. The Phase A study has shown that we can fabricate the mandrels with the needed quality and that we have developed a valid integration process. The shells that we have produced so far have a quite good image quality, e.g. HEW < or approx. 30 arcsec at 30 keV, and effective area. However, we still need to make some improvements to reach the requirements. We will briefly present these results and discuss the possible improvements that we will investigate during phase B.

  8. Research of plasma-electrolyte discharge in the processes of obtaining metallic powders

    Science.gov (United States)

    Kashapov, R. N.; Kashapov, L. N.; Kashapov, N. F.

    2017-11-01

    The use of the plasma electrolyte process has never been considered as a simple, cheap and fast method of obtaining powders used in selective laser melting processes. Therefore, the adaptation of the plasma-electrolyte process to the production of metal powders used in additive production is an urgent task. The paper presents the results of studies of gas discharge parameters between a metal and liquid electrode in the processes of obtaining metallic iron powders. The discharge combustion conditions necessary for the formation of metal powders of micron size are determined. A possible mechanism for the formation of powder particles in a discharge plasma is proposed.

  9. PULP OBTAINING METHOD FOR PACKAGE PRODUCTION

    Directory of Open Access Journals (Sweden)

    V. V. Kuzmich

    2015-01-01

    Full Text Available The paper presents a new method for obtaining pulp which is used for production of cardboard, paper and package while using carbon dioxide and hydrazine hydrate and neutral-sulfite  shive cooking. Output increase of  the desired product can be explained by reduction in destruction of plant raw material carbohydrates during its cooking process. Quality improvement of the desired product (improvement in bleaching and output is attributed to the fact that usage of carbon dioxide and hydrazine contributes to provision of polysaccharide chain resistance to destruction due to the presence of  end links having structure of metasaccharinic and aldonic acids.The author has developed a new method for pulp obtaining on the basis of the executed investigations  and literature data.  СО2 and hydrazine hydrate have been used for obtaining pulp. Method invention concerns pulp obtaining and it can be used for paper and cardboard package manufacturing in pulp and paper industry.The method is to be carried in the following way: pulp-containing plant raw material is loaded into an autoclave and then aqua solution of sodium monosulfite containing hydrazine hydrate that constitutes 4–5 % of absolute dry pulp-containing raw material mass with liquid module 1:6–1:8 is supplied into the autoclave. The autoclave is closed for operation under pressure and the solution is carbonated under pressure which constitutes 5–8 % of absolute dry plant raw material (shover. Temperature is subsequently raised up to 180 °С in the space of 2 hours and cooking is carried out in the course of 4 hours. Usage of  the proposed method for shover cooking makes it possible to reduce monosulfite cooking process and improve qualitative characteristics and output of the desired product.  In addition to above mentioned fact there is a possibility to improve bleaching and final product output. 

  10. Lunar tidal acceleration obtained from satellite-derived ocean tide parameters

    Science.gov (United States)

    Goad, C. C.; Douglas, B. C.

    1978-01-01

    One hundred sets of mean elements of GEOS-3 computed at 2-day intervals yielded observation equations for the M sub 2 ocean tide from the long periodic variations of the inclination and node of the orbit. The 2nd degree Love number was given the value k sub 2 = 0.30 and the solid tide phase angle was taken to be zero. Combining obtained equations with results for the satellite 1967-92A gives the M sub 2 ocean tide parameter values. Under the same assumption of zero solid tide phase lag, the lunar tidal acceleration was found mostly due to the C sub 22 term in the expansion of the M sub 2 tide with additional small contributions from the 0 sub 1 and N sub 2 tides. Using Lambeck's (1975) estimates for the latter, the obtained acceleration in lunar longitudal in excellent agreement with the most recent determinations from ancient and modern astronomical data.

  11. Obtaining low-congealing oils and paraffins by carbamide deparaffinization method

    Energy Technology Data Exchange (ETDEWEB)

    Kalambet, I A; Dorodnova, V S

    1982-07-01

    Ethane cooling is required to obtain oils with congealing points lower than 15-20/sup 0/C. Thus a process of carbamide deparaffinization that would be relatively simple and would not require special cooling equipment was deemed desirable. Filtrates were selected from an oil separating device after basic solid paraffins had been removed. They were subjected to hydropurification with an alumimum-cobalt-molybdenum catalyst at 4 MPa pressure, 320/sup 0/C, feed of 1.5c/sup -1/ and hydrogen-containing gas compressed to 500 m/sup 3//m/sup 3/. Results showed that the initial mixed hydrocarbon filtrate was deparaffinized under these conditions to produce an oil that congealed on the average at temperatures 2-3/sup 0/ lower than controls. A benzine fraction at 80-120/sup 0/C was used as the solvent and methanol served as the activator. Using distillates from Stavropol crude oil, it was possible to obtain oils.

  12. Pulsed system for obtaining microdosimetric data with high intensity beams

    International Nuclear Information System (INIS)

    Zaider, M.; Dicello, J.F.; Hiebert, R.D.

    1977-01-01

    The use of heavy particle accelerators for radiation therapy requires high intensity beams in order to produce useful dose rates. The 800-MeV proton beam at LAMPF passes through different production targets to generate secondary pion beams. Conventional microdosimetric techniques are not applicable under these conditions because exceedingly high count rates result in detector damage, gas breakdown, and saturation effects in the electronics. We describe a new microdosimetric system developed at the Pion Biomedical Channel of LAMPF. The accelerator provides a variable low intensity pulse once every ten high intensity macropulses. The voltage on the detector is pulsed in coincidence with the low intensity pulse so that we were able to operate the detector under optimum data-taking conditions. A low noise two-stage preamplifier was built in connection with the pulsed mode operation. A comparison is made between data obtained in pulsed (high intensity beam) and unpulsed (low intensity beam) modes. The spectra obtained by the two methods agree within the experimental uncertainties

  13. A comparison of two methods for prediction of response and rates of inbreeding in selected populations with the results obtained in two selection experiments

    NARCIS (Netherlands)

    Loywyck, V.; Bijma, P.; Pinard-van der Laan, M.H.; Arendonk, van J.A.M.; Verrier, E.

    2005-01-01

    Selection programmes are mainly concerned with increasing genetic gain. However, short-term progress should not be obtained at the expense of the within-population genetic variability. Different prediction models for the evolution within a small population of the genetic mean of a selected trait,

  14. Comparison of different methodologies for obtaining nickel nanoferrites

    Energy Technology Data Exchange (ETDEWEB)

    Galindo, R.; Menendez, N. [Departamento de Química Física Aplicada, Facultad de Ciencias, Universidad Autónoma de Madrid, Cantoblanco, E-28049 Madrid (Spain); Crespo, P.; Velasco, V. [Instituto de Magnetismo Aplicado, UCM, ADIF CSIC, E-28230 Madrid (Spain); Bomati-Miguel, O.; Díaz-Fernández, D. [Departamento de Física Aplicada and Instituto Nicolás Cabrera, Facultad de Ciencias Universidad Autónoma de Madrid, Cantoblanco, E-28049 Madrid (Spain); Herrasti, P., E-mail: pilar.herrasti@uam.es [Departamento de Química Física Aplicada, Facultad de Ciencias, Universidad Autónoma de Madrid, Cantoblanco, E-28049 Madrid (Spain)

    2014-06-01

    Nickel nanoferrites were obtained by means of four different synthetic wet-routes: co-precipitation (CP), sonochemistry (SC), sonoelectrochemistry (SE) and electrochemistry (E). The influence of the synthesis method on the structural and magnetic properties of nickel ferrite nanoparticles is studied. Although similar experimental conditions such as temperature, pH and time of synthesis were used, a strong dependence of composition and microstructure on the synthesis procedure is found, as electron microscopy, X-ray diffraction and Mössbauer spectroscopy studies reveal. Whereas by means of the CP and SC methods particles of a small size around 5–10 nm, respectively, and composed by different phases are obtained, the electrochemical routes (E and SE) allow obtaining monodisperse nanoparticles, with sizes ranging from 30 to 40 nm, and very close to stoichiometry. Magnetic characterization evidences a superparamagnetic behavior for samples obtained by CP and SC methods, whereas the electrochemical route leads to ferromagnetic ferrite nanoparticles. - Highlights: • Electrochemical synthesis produces pure NiFe{sub 2}O{sub 4} nanonoparticles with 40 nm particle size. • Coprecipitation and sonochemistry techniques generate NiFe{sub 2}O{sub 4} nanoparticles with impurities. • Nanoparticles obtained by coprecipitation and sonochemistry are superparamagnetic. • Electrochemical and sonoelectrochemical methods produce ferromagnetic nanoparticles.

  15. Experimental Characterization of Aluminum-Based Hybrid Composites Obtained Through Powder Metallurgy

    Science.gov (United States)

    Marcu, D. F.; Buzatu, M.; Ghica, V. G.; Petrescu, M. I.; Popescu, G.; Niculescu, F.; Iacob, G.

    2018-06-01

    The paper presents some experimental results concerning fabrication through powder metallurgy (P/M) of aluminum-based hybrid composites - Al/Al2O3/Gr. In order to understand the mechanisms that occur during the P/M processes of obtaining Al/Al2O3/Gr composite, we correlated the physical characteristics with their micro-structural characteristics. The characterization was performed using analysis techniques specific for P/M process, SEM-EDS and XRD analyses. Micro-structural characterization of the composites has revealed fairly uniform distribution this resulting in good properties of the final composite material.

  16. The possibility of obtaining beta-anhydrite from waste nitrogypsum

    Directory of Open Access Journals (Sweden)

    Marinković S.

    2004-01-01

    Full Text Available The possibility of obtaining β - anhydrite from nitrogypsum, which is waste from a nitrocellulose plant, was investigated. It was shown by means of qualitative IR analysis that the product obtained by heating nitrogypsum for 5 hours at 700 o C was â - anhydrite. When the β- anhydrite was mixed with water at a W/S (water/solid ratio of 0.54 in presence of different accelerators (CaO, mixture CaO - ash, ash, Na2SO4 and K2SO4, pastes were formed which hardened on standing. The compressive strength of the hardened samples was measured after 7 and 28 days and their composition determined by qualitative IR analysis. On the basis of these results, it was observed that a relationship exists between the composition (depending on the used accelerator and the compression strength of the samples. Namely, the formation of large cores of double salts: syngenite (K2SO4 ⋅CaSO4 ⋅H2O and glauberite (Na2SO4 ⋅CaSO4, in the presence of the accelerators K2SO4 and Na2SO4, respectively, was due to the rapid and complete crystallization of the dihydrate (CaSO4 ⋅2H2O. This fast crystal growth of the dihydrate resulted in high compressive strengths of these samples. In the other samples (prepared in presence of the accelerators: CaO, mixture CaO - ash and ash, dihydrate did not form and, consequently, their compressive strength was low.

  17. Pressure suppression system (PSS) for nuclear ships. Experimental results obtained at the GKSS PSS-test-facillity

    International Nuclear Information System (INIS)

    Aust, E.; Niemann, H.R.; Schwan, H.; Vollbrandt, J.

    1978-01-01

    The PSS-test facility is shortly presented which was designed to show experimentally the operation of the pressure suppression containment for the NCS 80 concept. The results of the experimental LOCA-simulation tests in the PSS-test facility are illustrated by diagrams. The observed phenomena as chugging and pessure oscillations immediately after vent clearing are reported as well as the thermohydraulic loadings of the total system. Finally a short view is given on the future test program

  18. Comparison of Vespula germanica venoms obtained from different sources.

    Science.gov (United States)

    Sanchez, F; Blanca, M; Miranda, A; Carmona, M J; Garcia, J; Fernandez, J; Torres, M J; Rondon, M C; Juarez, C

    1994-08-01

    This study was carried out to compare the allergenic potency of Vespula germanica (VG) venoms extracted by different methods and commercially available venoms from Vespula species currently used for in vivo and in vitro studies including immunotherapy. Pure VG venom was used as the reference material. Protein content and enzymatic and allergenic properties of all venoms studied were determined by dye stain reagent, hyaluronidase and phospholipase A1B enzyme activities, and radioallergosorbent test inhibition studies, respectively. Radioallergosorbent test discs sensitized with commercial and pure VG venom were compared using specific IgE antibodies from subjects allergic to VG venom. The data obtained indicate that there were important differences in the allergenic potency between the Vespula species venoms employed for in vivo and/or in vitro assays, VG venom obtained by sac dissection, and pure VG venom. These results indicate that venoms from Vespula species used for in vitro and in vivo tests have a lower concentration of allergens and contain nonvenom proteins. These data should be taken into account when these vespid venoms are used for diagnostic purposes and also when evaluating immunotherapy studies.

  19. Evaluation of gels obtained from acetylation of chitosan in heterogeneous medium

    International Nuclear Information System (INIS)

    Garcia, Rosangela Balaban; Silva, Dayse Luzia Pinheiro da; Costa, Marta

    2008-01-01

    Chitosan was acetylated during 2, 5 and 10 h and physical gels were obtained at different polymer concentrations in N,N-dimethylacetamide containing 5% of LiCl. Acetylation was confirmed by infrared spectroscopy and 13 C NMR, and degrees of acetylation in the range of 0.82-0.91 were determined by NMR. The O-acetylation degree (0.12-0.15) was exclusively determined by a volumetric method. Rheological studies showed that the storage modulus values were smaller for the more acetylated samples and increased with the temperature and the polymer concentration. All the gels presented storage modulus superior to loss modulus, evidencing more elastic than viscous characteristics. The results obtained in this work suggest a gelation process based on a balance between O and N-acetylation and intermolecular bonds. (author)

  20. Microbiological quality of five potato products obtained at retail markets.

    OpenAIRE

    Duran, A P; Swartzentruber, A; Lanier, J M; Wentz, B A; Schwab, A H; Barnard, R J; Read, R B

    1982-01-01

    The microbiological quality of frozen hash brown potatoes, dried hash brown potatoes with onions, frozen french fried potatoes, dried instant mashed potatoes, and potato salad was determined by a national sampling at the retail level. A wide range of results was obtained, with most sampling units of each products having excellent microbiological quality. Geometric mean aerobic plate counts were as follows: dried hash brown potatoes, 270/g; frozen hash brown potatoes with onions, 580/g; frozen...

  1. Machining tools in AISI M2 high-speed steel obtained by spray forming process

    International Nuclear Information System (INIS)

    Jesus, Edilson Rosa Barbosa de.

    2004-01-01

    The aim of the present work was the obtention of AISI M2 high-speed steel by spray forming technique and the material evaluation when used as machining tool. The obtained material was hot rolled at 50% and 72% reduction ratios, and from which it was manufactured inserts for machining tests. The performance of inserts made of the spray formed material was compared to inserts obtained from conventional and powder metallurgy (MP) processed materials. The spray formed material was chemical, physical, mechanical and microstructural characterised. For further characterisation, the materials were submitted to machining tests for performance evaluation under real work condition. The results of material characterisation highlight the potential of the spray forming technique, in the obtention of materials with good characteristics and properties. Under the current processing, hot rolling and heat treatments condition, the analysis of the results of the machining tests revealed a very similar behaviour among the tested materials. Proceeding a criterious analysis of the machining results tests, it was verified that the performance presented by the powder metallurgy material (MP) was slight superior, followed by conventional obtained material (MConv), which presented a insignificant advantage over the spray formed and hot rolled (72% reduction ratio) material. The worst result was encountered for the spray forming and hot rolled (50% reduction ratio) material that presented the highest wear values. (author)

  2. Detection of occlusal caries lesions using fluorescence: correlation between histology and obtained results for Diagnodent and spectroscopy

    International Nuclear Information System (INIS)

    Rocha-Cabral, Renata Maciel

    2006-01-01

    The aims of this study were to develop and test a method to detect caries lesions in vivo and in vitro, using a portable spectrometer (PS); to analyze the performance of PS as well as the commercial device Diagnodent (Dd); correlate them with the gold standard, their transversal section areas and lesions depth and between themselves. 66 occlusal pre-molars sites were examined in vivo with Dd. Sequentially, fluorescence (λexc ∼ 657 nm) was collected by an optical fiber, conducted to PS and then analyzed as spectra, which were normalized and had calculated the Ratios of their Areas Under the Curves (RAUC) of carious and sound tissues. Experiments were conducted in vitro in the same sites. Gold Standard was obtained by polarized light microscopy. Pearson correlation was used to compare the devices with transversal section area, lesions depth and between themselves. The area under ROC curve, sensitivity, specificity as well as accuracy were calculated and verified with McNemar test. Dd and RAUC showed statistically significant correlation with gold standard (p < 0.01 for Dd and p < 0.05 for RAUC) and between themselves (r = 0,83 in vivo and r = 0,87 in vitro). Although it was significant, the devices showed low correlation with depth of lesions in vivo and in vitro (r = ∼ 0.43). The transversal section area of the lesion had no influence on readings in both devices. Dd showed higher sensitivity (0.76) than PS (0.60) in vivo (p < 0.05), though this fact was not able to improve its performance. In turn, PS showed higher sensitivity (0.88) than Dd (0.79) in vitro, but this difference was not significantly. The other parameters did not show statistically significant differences (p < 0.05) between methods. PS showed positive correlation with Dd, equal correlation with lesions depth and higher ability of detecting the disease in vitro, what suggests that if accompanied with a conic and an angulated probe and a dedicated software, the PS method could be useful in clinics

  3. Conditions optimization for obtaining biodiesel from soybean oil using the mixture experimental design

    Directory of Open Access Journals (Sweden)

    Kelly Roberta Spacino

    2010-09-01

    Full Text Available The optimization of the yield of transesterification reaction to obtain the B100 biodiesel has been studied using sodium hydroxide, potassium hydroxide, methoxide and sodium ethoxide as catalysts. We applied a randomized simplex centroid mixture and the results of optimization indicate, when using methanol, a yield of 97.61% when using 30,77% NaOH and 69,23% of sodium methoxide and a yield of 89,32% when using only the sodium ethoxide whit ethanol. Chromatographic analysis indicated that the B100 biodiesel obtained is within the parameters established by Brazilian Legislation.

  4. 32 CFR 806b.8 - Obtaining law enforcement records.

    Science.gov (United States)

    2010-07-01

    ... 32 National Defense 6 2010-07-01 2010-07-01 false Obtaining law enforcement records. 806b.8 Section 806b.8 National Defense Department of Defense (Continued) DEPARTMENT OF THE AIR FORCE ADMINISTRATION PRIVACY ACT PROGRAM Obtaining Law Enforcement Records and Confidentiality Promises § 806b.8 Obtaining law enforcement records. The Commander, Air...

  5. Characterization of microstructure and catalytic of cerium oxide obtained by colloidal solution

    International Nuclear Information System (INIS)

    Senisse, C.A.L.; Bergmann, C.P.; Alves, A.K.

    2012-01-01

    This study investigated to obtain particles of cerium oxide, for use as catalysts for the combustion of methane using the technique of through polymeric colloidal solution. Obtaining the colloidal system is based on hydrolysis of salts such as cerium acetylacetonate, cerium nitrate in the presence of additives such as polyvinylbutyral (PVB), polyvinylpyrrolidone (PVP) and polyvinyl acetate (PVA), at concentrations of 5, 10 and 15% in aqueous or alcoholic medium. These solutions containing ions of interest were subjected to a heat treatment at 650° C for 30 minutes, with heating rate of 2 ° C/ min. After heat treatment, the fibers were characterized according to their morphology, surface area, crystallinity, weight loss and catalytic activity. Samples obtained from cerium acetylacetonate were more reactive than the cerium nitrate to the combustion of methane, as showed greater conversions and higher temperatures reached during the process, which is of utmost importance since the combustion catalytic methane is used for generating thermal energy. After the reaction with methane, the samples underwent significant change in surface area, probably due to the intensity of combustion reactions of the nitrate and the generation of heat involved in this reaction, which gave rise to coarse particles. During the combustion process using the obtained from particles of cerium acetylacetonate, there was the release of large quantities of nitrogen compared to the results of assays with the particles obtained with cerium nitrate. (author)

  6. HgI2 nanostructures obtained hydrothermally for application in ionizing radiation detection

    International Nuclear Information System (INIS)

    Pérez Barthaburu, María; Bentos Pereira, Heinkel; Fornaro, Laura; Galain, Isabel; Aguiar, Ivana

    2016-01-01

    The compound semiconductor HgI 2 has been widely studied and employed as a material for ionizing radiation detection. Monocrystal growth is an intricate method for obtaining materials for this application. With the aim of finding a simpler and more effective way to develop ionizing radiation detectors, we employed HgI 2 nanostructures subjected to a hydrothermal treatment and then pressed for this purpose. In the synthesis procedure, aqueous solutions of Hg(NO 3 ) 2 and NaI were mixed until their reaction completed and the suspension obtained was then placed in a homemade autoclave and heated at 120 °C for 2, 10 or 24 h. We confirmed the HgI 2 tetragonal phase by powder XRD in all cases, independently of the synthesis conditions employed. Nanoparticles were characterized by their size and morphology by TEM. We used the HgI 2 nanostructures to obtain a pellet by applying 0.7 GPa of pressure at room temperature. The pellet was then used to construct the detector, and we studied the electrical properties of the detector and its response to 241 Am sources of different exposure rates. The resistivity and signal-to-noise ratio obtained are of the order of those reported for HgI 2 detectors assembled with monocrystals. The results obtained in this work encourage us to work further on this topic, improving the method, scaling the detector’s size and studying its spectrometric grade. (paper)

  7. Obtaining Application-based and Content-based Internet Traffic Statistics

    DEFF Research Database (Denmark)

    Bujlow, Tomasz; Pedersen, Jens Myrup

    2012-01-01

    the Volunteer-Based System for Research on the Internet, developed at Aalborg University, is capable of providing detailed statistics of Internet usage. Since an increasing amount of HTTP traffic has been observed during the last few years, the system also supports creating statistics of different kinds of HTTP...... traffic, like audio, video, file transfers, etc. All statistics can be obtained for individual users of the system, for groups of users, or for all users altogether. This paper presents results with real data collected from a limited number of real users over six months. We demonstrate that the system can...

  8. Calculation of multigroup constants in WIMS format with programs fedgroup and flange and comparison of the results obtained using different evaluated libraries

    International Nuclear Information System (INIS)

    Trkov, A.; Budnar, M.; Copic, M.; Perdan, A.; Ravnik, M.

    1982-01-01

    Multigroup constants for 1-H-1, 92-U-235, and 92-U-238 have been calculated. Averaged cross-sections and other constants have been prepared in the WIMS 69-group format. Comparison has been made between group constants obtained with several evaluated libraries (KEDAK-3 1975, 1979, ENDF/B-4, ENDF/B-5) and the WIMS-D library. Observed differences are most pronounced in the resonance and fast region. From test runs on fuel cell with the WIMS program it can be deduced that these differences affect the fewgroup constants significantly. (author)

  9. Evaluation of the depth of infiltration of urothelial carcinoma in the vesical wall obtained by transurethral intravesical echotomography

    Directory of Open Access Journals (Sweden)

    Milošević Radovan

    2007-01-01

    Full Text Available Background/Aim. Transitional cell carcinoma (TCC is the most frequent tumor of the bladder and represents 95−98% of blader neoplasams and 2−3% of all carcinomas in the body. In urogenital oncology more frequent is only prostatic cancer. Evaluation of the depth of infiltration of urothelial carcinoma in the vesical wall represents the clinical base in treatment planning and prognosis. Clinical investigation and convential radiological procedures have a low level of accuracy in estimating the local growth of the tumor. The aims of our investigation were to determine the depth of infiltration of urothelial carcinoma in the vesical wall in the investigated group of patients by transurethral intravesical echotomography (TIE and computerised tomography (CT scan and to compare results obtained by both methods with pathohistological (PH results, and, based on the difference of the results determine which method was more accurate in the evaluation of the depth of infiltration of urothelial carcinoma in the vesical wall. Methods. Thirty patients with TCC of the bladder both genders, aged 51−81 years were involved in our investigation. In all of these patients, radical cystectomy (RC was performed. This was neccessary to provide the defintive PH result. Transurethral intravesical echotomography was performed by ultrasound scanner type 1846 Bruel and Kjaer, sond type 1850, and the CT scan was perfomed by Pace plus, General Electric, U.S.A. The specimen for the definitive PH result obtained by RC includes all standards of the TNM classification. Results. Using CT scan, the most frequent was T1 stage (17 patients or 56.68%. Using TIE, the most frequent was T2 stage (22 patients or 73.33%. After RC the most frequent was T2 stage (21 patients or 70%. The Kolmogorov-Smirnov test, showed a high significant difference between the results obtained using CT and definitive PH results after RC. The same test showed no statistically significant difference between

  10. Synthesis and characterization of Zn_2SiO_4 ceramic pigments obtained by chemical method

    International Nuclear Information System (INIS)

    Rangel, J.H.G.; Silva, J.S.; Oliveira, M.M.; Azevedo, E.; Costa, M.G.S.; Longo, E.

    2014-01-01

    The silicates provide a wide field of application, ranging from molecular sieves to catalyst supports, and therefore their morphology resulting from the obtaining method of production has been widely studied. The isomorphous replacement of cation Zn in the structure of willemite by a chromophore metal has been widely studied in the use of silicate as ceramic pigments. In this study the polymeric precursor was used to synthesize zinc silicates of nickel-doped to obtain ceramic pigments. The polymeric precursor was treated at 350 deg C/2h and the material was calcined at temperatures from 700 to 1000 deg C/4h on plates of sintered alumina at a heating rate of 10 deg C/min under ambient atmosphere in a muffle furnace type. The results of the XRD indicated the presence of the rhombohedral phase of the willemite and the presence of ZnO as an secondary phase. The micrographs, obtained by SEM, showed that the increasing in the temperature of calcination of the material from 700 to 1000 deg C caused an increasing in particle size due to the formation of aggregates. The reissue spectra of Kubelka-Munk measured by diffuse reflectance showed signs that suggest the presence of different cations in coordination. Based on the results obtained by means of colorimetric coordinates, it was observed that the material had bluish gray color. (author)

  11. A Systematic Approach for Obtaining Performance on Matrix-Like Operations

    Science.gov (United States)

    Veras, Richard Michael

    Scientific Computation provides a critical role in the scientific process because it allows us ask complex queries and test predictions that would otherwise be unfeasible to perform experimentally. Because of its power, Scientific Computing has helped drive advances in many fields ranging from Engineering and Physics to Biology and Sociology to Economics and Drug Development and even to Machine Learning and Artificial Intelligence. Common among these domains is the desire for timely computational results, thus a considerable amount of human expert effort is spent towards obtaining performance for these scientific codes. However, this is no easy task because each of these domains present their own unique set of challenges to software developers, such as domain specific operations, structurally complex data and ever-growing datasets. Compounding these problems are the myriads of constantly changing, complex and unique hardware platforms that an expert must target. Unfortunately, an expert is typically forced to reproduce their effort across multiple problem domains and hardware platforms. In this thesis, we demonstrate the automatic generation of expert level high-performance scientific codes for Dense Linear Algebra (DLA), Structured Mesh (Stencil), Sparse Linear Algebra and Graph Analytic. In particular, this thesis seeks to address the issue of obtaining performance on many complex platforms for a certain class of matrix-like operations that span across many scientific, engineering and social fields. We do this by automating a method used for obtaining high performance in DLA and extending it to structured, sparse and scale-free domains. We argue that it is through the use of the underlying structure found in the data from these domains that enables this process. Thus, obtaining performance for most operations does not occur in isolation of the data being operated on, but instead depends significantly on the structure of the data.

  12. Combustion behaviour of ultra clean coal obtained by chemical demineralisation

    Energy Technology Data Exchange (ETDEWEB)

    F. Rubiera; A. Arenillas; B. Arias; J.J. Pis; I. Suarez-Ruiz; K.M. Steel; J.W. Patrick [Instituto Nacional del Carbon, CSIC, Oviedo (Spain)

    2003-10-01

    The increasing environmental concern caused by the use of fossil fuels and the concomitant need for improved combustion efficiency is leading to the development of new coal cleaning and utilisation processes. However, the benefits achieved by the removal of most mineral matter from coal either by physical or chemical methods can be annulled if poor coal combustibility characteristics are attained. In this work a high volatile bituminous coal with 6% ash content was subjected to chemical demineralisation via hydrofluoric and nitric acid leaching, the ash content of the clean coal was reduced to 0.3%. The original and treated coals were devolatilised in a drop tube furnace and the structure and morphology of the resultant chars was analysed by optical and scanning electron microscopies. The reactivity characteristics of the chars were studied by isothermal combustion tests in air at different temperatures in a thermogravimetric system. Comparison of the combustion behaviour and pollutant emissions of both coals was conducted in a drop tube furnace operating at 1000{sup o}C. The results of this work indicate that the char obtained from the chemically treated coal presents very different structure, morphology and reactivity behaviour than the char from the original coal. The changes induced by the chemical treatment increased the combustion efficiency determined in the drop tube furnace, in fact higher burnout levels were obtained for the demineralised coal.

  13. Preliminary physico-chemical results obtained on water using new data acquisition systems for deep wells

    International Nuclear Information System (INIS)

    Vinson, J.M.; Peyrus, J.C.

    1984-02-01

    Data acquisition systems recently developed in the context of research on deep storage facilities have provided with an initial set of interesting observations for the physico-chemical study of boreholes. It is possible to make correlations between the chemical compositions of water, pH and the nature of the substrate. The sampling done at Auriat with a Gerhardt-Owen probe shows the variability in the composition of water as a function of depth. The variation in calcium content, following that of pH, is particularly notable. Examination of pH measurements is of particular interest. A general gradient correlates exactly with the nature of the substrate. Whereas steel piping has a very alkaline pH, distinct pH values correspond to the two types of granite substrate. In this general gradient, series of disturbances can be seen which correspond perfectly to fracturation zones or large fractures. These most promising preliminary results lead to believe that in situ physico-chemical measurements should be continued and developed with a view to improved evaluation of the safety of deep storage facilities

  14. Iterative schemes for obtaining dominant alpha-modes of the neutron diffusion equation

    International Nuclear Information System (INIS)

    Singh, K.P.; Modak, R.S.; Degweker, S.B.; Singh, Kanchhi

    2009-01-01

    Two new methods of obtaining dominant prompt alpha-modes (sometimes referred to as time-eigenfunctions) of the multigroup neutron diffusion equation are discussed. In the first of these, we initially compute the dominant K-eigenfunctions and K-eigenvalues (denoted by λ 1 , λ 2 , λ 3 ...λ 1 being equal to the K eff ) for the given nuclear reactor model, by existing method based on sub-space iteration (SSI) which is an improved version of power iteration method. Subsequently, a uniformly distributed (positive or negative) 1/v absorber of sufficient concentration is added so as to make a particular eigenvalue λ i equal to unity. This gives ith alpha-mode. This procedure is repeated to find all the required alpha-modes. In the second method, we solve the alpha-eigenvalue problem directly by SSI method. This is clearly possible for a sub-critical reactor for which the inverse of the dominant alpha-eigenvalues are also the largest in magnitude as required by the SSI method. Here, the procedure is made applicable even to a super-critical reactor by making the reactor model sub-critical by the addition of a 1/v absorber. Results of these calculations for a 3-D two group PHWR test-case are given. These results are validated against the results as obtained by a completely different approach based on Orthomin(1) algorithm published earlier. The direct method based on the sub-space iteration strategy is found to be a simple and reliable method for obtaining any number of alpha-modes. Also comments have been made on the relationship between fundamental α and k values.

  15. Optimizing Methods of Obtaining Stellar Parameters for the H3 Survey

    Science.gov (United States)

    Ivory, KeShawn; Conroy, Charlie; Cargile, Phillip

    2018-01-01

    The Stellar Halo at High Resolution with Hectochelle Survey (H3) is in the process of observing and collecting stellar parameters for stars in the Milky Way's halo. With a goal of measuring radial velocities for fainter stars, it is crucial that we have optimal methods of obtaining this and other parameters from the data from these stars.The method currently developed is The Payne, named after Cecilia Payne-Gaposchkin, a code that uses neural networks and Markov Chain Monte Carlo methods to utilize both spectra and photometry to obtain values for stellar parameters. This project was to investigate the benefit of fitting both spectra and spectral energy distributions (SED). Mock spectra using the parameters of the Sun were created and noise was inserted at various signal to noise values. The Payne then fit each mock spectrum with and without a mock SED also generated from solar parameters. The result was that at high signal to noise, the spectrum dominated and the effect of fitting the SED was minimal. But at low signal to noise, the addition of the SED greatly decreased the standard deviation of the data and resulted in more accurate values for temperature and metallicity.

  16. Recent results from Pb - Au collisions at 158 GeV/c per nucleon obtained with the CERES spectrometer

    CERN Document Server

    Agakichiev, G; Baur, R; Braun-Munzinger, P; Ceretto, F; Cherlin, A; Drees, A; Esumi, S C; Faschingbauer, U; Fraenkel, Zeev; Glässel, P; Hering, G; Holl, P; Jung, C; Lenkeit, B C; Marin, A; Messer, M; Miskowiec, D; Panebratsev, Yu A; Pfeiffer, A; Rak, J; Ravinovich, I; Razin, S V; Rehak, P; Richter, M; Saveljic, N; Schmitz, W; Schükraft, Jürgen; Seipp, W; Shimansky, S S; Slivova, J; Socol, E; Specht, H J; Stachel, J J; Tserruya, Itzhak; Ullrich, T S; Voigt, C A; Voloshin, S A; Weber, C; Wessels, J P; Wienold, T; Wurm, J P; Yurevich, V I

    1999-01-01

    During the 1996 lead run time, CERES has accumulated 42 million events, corresponding to a factor of 5 more statistics than in 1995 and 2.5 million events of a special photon-run. We report on the results of the low-mass e/sup +/e/sup -/-pair analysis. Since the most critical item is the poor signal-to-background ratio we also discuss the understanding of this background, in absolute terms, with the help of a detailed Monte Carlo simulation. We show preliminary results of the photon analysis and summarize the results of the hadron analysis preliminarily reported on already at QM'97. (19 refs) .

  17. ELECTROCHEMICAL TECHNOLOGIES FOR OBTAINING MOULDS FOR SOLES OF SHOES

    Directory of Open Access Journals (Sweden)

    Cornelia LUCA

    2013-05-01

    Full Text Available The paper presents contributions in the designing of some electrochemical technologiesfor the manufacturing of the moulds used in the footwear soles obtaining. There are presented a fewmethods for the moulds obtaining, using electro-deposit processes. There are presented thetechnological phases of the obtaining process of the electrolytes and electrodes preparing and thetechnological stages of the moulds manufacturing.

  18. Blind pre-analysis of the main building complex WWER-1000 Kozloduy. Comparison of analytical and experimental results obtained by explosive testing (task 8a of workplan 96/97)

    International Nuclear Information System (INIS)

    Krutzik, N.J.

    1999-01-01

    In accordance with the 96/97 workplan of the Research Programme on 'Benchmark Studies for Seismic Analysis and Testing of WWER-Type Nuclear Power Plants', blind pre analyses were prepared for the main building complex of the WWER-1000 based on given excitations derived from explosive tests. The investigations were performed by several institutions based on various mathematical models and procedures for consideration of soil-structure interaction effects, but on the same explosive test input data recently obtained. The methods of calculation and software tools used will also be different. The aim of this investigation is to validate different idealization concepts (mathematical models for the idealization of the structures and the soil) as well as investigation procedures (time domain and frequency domain analysis) and finally the software tools by comparing structural response results (time histories and response spectra). This report contains the results of the blind pre analysis performed by Siemens using an equivalent beam model of the main building of the WWER 1000. The calculations were performed by means of a frequency domain calculation

  19. Synthesis of 4A zeolites from kaolin for obtaining 5A zeolites through ionic exchange for adsorption of arsenic

    International Nuclear Information System (INIS)

    Resmini Melo, Carolina; Gracher Riella, Humberto; Cabral Kuhnen, Nivaldo; Angioletto, Elidio; Melo, Aline Resmini; Bernardin, Adriano Michael; Rocha, Marcio Roberto da; Silva, Luciano da

    2012-01-01

    Highlights: ► We synthesize 4A zeolite from kaolin by hydrothermal reaction with sodium hydroxide. ► The 4A zeolite synthesized underwent ion exchange with calcium ions, with different parameters, to obtain 5A zeolites. ► The best 4A zeolite obtained was used as adsorbent material for arsenic ions. ► The results showed that the 5A zeolite material obtained is a good adsorber of heavy ions. - Abstract: The synthesis of adsorbing zeolite materials requires fine control of the processing variables. There are distinct process variable settings for obtaining specific desired types of zeolites. The intent of this study was to obtain 4A zeolites from kaolin in order to obtain 5A zeolites through ionic exchange with the previously synthesized zeolite. This zeolite 5A was used as an adsorbent for arsenic ions. The results obtained were satisfactory.

  20. Correlation of the Condylar Guidance Obtained by Protrusive Interocclusal Record and Panoramic Radiographs in Completely Edentulous Patients: An in Vivo Study

    Directory of Open Access Journals (Sweden)

    Khyati Shah

    2014-01-01

    Results: The results showed statistically significant difference between the condylar guidance values obtained from Orthopantomograph (Radiograph and the condylar guidance values obtained at the stage of jaw relation. Conclusion: Within the limitations of the study, it can be concluded that the condylar guidance values obtained from the Radiographs were higher than those obtained at the stage of jaw relation recording stage.

  1. A comparative analysis of the EEDF obtained by Regularization and by Least square fit methods

    International Nuclear Information System (INIS)

    Gutierrez T, C.; Flores Ll, H.

    2004-01-01

    The second derived of the characteristic curve current-voltage (I - V) of a Langmuir probe (I - V) is numerically calculated using the Tikhonov method for to determine the distribution function of the electrons energy (EEDF). One comparison of the obtained EEDF and a fit by least square are discussed (LS). The I - V experimental curve is obtained in a plasma source in the electron cyclotron resonance (ECR) using a cylindrical probe. The parameters of plasma are determined of the EEDF by means of the Laframboise theory. For the case of the LS fit, the obtained results are similar to those obtained by the Tikhonov method, but in the first case the procedure is slow to achieve the best fit. (Author)

  2. From global to local statistical shape priors novel methods to obtain accurate reconstruction results with a limited amount of training shapes

    CERN Document Server

    Last, Carsten

    2017-01-01

    This book proposes a new approach to handle the problem of limited training data. Common approaches to cope with this problem are to model the shape variability independently across predefined segments or to allow artificial shape variations that cannot be explained through the training data, both of which have their drawbacks. The approach presented uses a local shape prior in each element of the underlying data domain and couples all local shape priors via smoothness constraints. The book provides a sound mathematical foundation in order to embed this new shape prior formulation into the well-known variational image segmentation framework. The new segmentation approach so obtained allows accurate reconstruction of even complex object classes with only a few training shapes at hand.

  3. Truncated States Obtained by Iteration

    International Nuclear Information System (INIS)

    Cardoso, W. B.; Almeida, N. G. de

    2008-01-01

    We introduce the concept of truncated states obtained via iterative processes (TSI) and study its statistical features, making an analogy with dynamical systems theory (DST). As a specific example, we have studied TSI for the doubling and the logistic functions, which are standard functions in studying chaos. TSI for both the doubling and logistic functions exhibit certain similar patterns when their statistical features are compared from the point of view of DST

  4. 32 CFR Appendix B to Part 275 - Obtaining Customer Authorization

    Science.gov (United States)

    2010-07-01

    ... 32 National Defense 2 2010-07-01 2010-07-01 false Obtaining Customer Authorization B Appendix B to... OF 1978 Pt. 275, App. B Appendix B to Part 275—Obtaining Customer Authorization A. A DoD law... feasible, obtain the customer's consent. B. Any authorization obtained under paragraph A. of this appendix...

  5. NON-EQUILIBRIUM MOLECULAR DYNAMICS USED TO OBTAIN SORET COEFFICIENTS OF BINARY HYDROCARBON MIXTURES

    Directory of Open Access Journals (Sweden)

    F. A. Furtado

    2015-09-01

    Full Text Available AbstractThe Boundary Driven Non-Equilibrium Molecular Dynamics (BD-NEMD method is employed to evaluate Soret coefficients of binary mixtures. Using a n-decane/n-pentane mixture at 298 K, we study several parameters and conditions of the simulation procedure such as system size, time step size, frequency of perturbation, and the undesired warming up of the system during the simulation. The Soret coefficients obtained here deviated around 20% when comparing with experimental data and with simulated results from the literature. We showed that fluctuations in composition gradients and the consequent deviations of the Soret coefficient may be due to characteristic fluctuations of the composition gradient. Best results were obtained with the smallest time steps and without using a thermostat, which shows that there is room for improvement and/or development of new BD-NEMD algorithms.

  6. Study of TiO{sub 2} nanomembranes obtained by an induction heated MOCVD reactor

    Energy Technology Data Exchange (ETDEWEB)

    Crisbasan, A., E-mail: andreea.crisbasan@yahoo.com [NANOFORM Group, ICB, Université de Bourgogne, BP 47 870, 21078 Dijon (France); Chaumont, D. [NANOFORM Group, ICB, Université de Bourgogne, BP 47 870, 21078 Dijon (France); Sacilotti, M. [NANOFORM Group, ICB, Université de Bourgogne, BP 47 870, 21078 Dijon (France); Departamento de Fisica – Universidade Federal de Pernambuco, Recife (Brazil); Crisan, A.; Lazar, A.M.; Ciobanu, I. [Science and Materials Engineering Faculty, University of Transilvania, Brasov (Romania); Lacroute, Y.; Chassagnon, R. [Université de Bourgogne, BP 47 870, 21078 Dijon (France)

    2015-12-15

    Highlights: • The TiO{sub 2} structures have been obtained by the MOCVD technique using ferrocene, cobalt layer (annealed at 350 °C) and Ti(OC{sub 3}H{sub 7}){sub 4}. • The TiO{sub 2} growth at 550 °C, during 20 min on the cobalt layer (obtained by electron beam evaporation method) on soda-lime glass has as result TiO{sub 2} nanomembranes. • The TiO{sub 2} nanomembranes grow on the cobalt nuclei. • The TiO{sub 2} nanomembranes are polycrystalline, built from TiO{sub 2} anatase and rutile crystals. - Abstract: Nanostructures of TiO{sub 2} were grown using the metal oxide chemical vapor deposition (MOCVD) technique. The procedure used induction heating on a graphite susceptor. This specific feature and the use of cobalt and ferrocene catalysts resulted in nanomembranes never obtained by common MOCVD reactors. The present study discusses the preparation of TiO{sub 2} nanomembranes and the dependence of nanomembrane structure and morphology on growth parameters.

  7. Cellulose acetate nanocomposite with nanocellulose obtained from bagasse of sugarcane

    International Nuclear Information System (INIS)

    Santos, Frirllei Cardozo dos

    2016-01-01

    This study presents a methodology for the extraction of nanocellulose of sugarcane bagasse for use in nanocomposites with cellulose acetate (CA). The bagasse sugarcane was treated with sodium hydroxide (NaOH) and sodium hypochlorite (NaClO) to remove lignin, hemicellulose, pectin and impurities. For removal of the amorphous region of cellulose microfibrils obtained from alkali treatments were submitted to acid hydrolysis with sulfuric acid under different temperature conditions. The nanocellulose obtained through acid hydrolysis heated at 45 ° C was used for the formulation of nanocomposites by smaller dimensions presented. The films were formulated at different concentrations (1, 2, 4 and 6 wt%) by the casting technique at room temperature. Each alkaline treatment was accompanied by spectrophotometry by infrared and fluorescence analysis to confirm the removal of the amorphous fraction, micrographs carried out by Scanning Electron Microscope (SEM) to display the fiber defibration. The efficiency of acid hydrolysis was confirmed by micrographs obtained by transmission electron microscope (TEM). The crystallinity index (CI) of the nanocrystals was determined by X-ray Diffraction (XRD). The surface of the obtained films were characterized by SEM and AFM microscopy of. The results showed that the sugarcane bagasse is an excellent source for nanocellulose extraction, the amorphous fraction of the fiber can be removed with the suggested alkaline treatments, and hydrolysis with H_2SO_4 was efficient both in the removal of amorphous cellulose as in reducing cellulose nanoscale with a length around 250 nm and a diameter of about 10 nm. The use of heated nanocellulose obtained through hydrolysis was selected after analysis of XRD, it was confirmed that this material had higher when compared to IC hydrolysis at room temperature. The nanocomposites showed high rigidity and brittleness with high crystallinity when compared to the pure polymer film was observed by AFM and SEM

  8. Securing recruitment and obtaining informed consent in minority ethnic groups in the UK

    Directory of Open Access Journals (Sweden)

    Roy Tapash

    2008-03-01

    Full Text Available Abstract Background Previous health research has often explicitly excluded individuals from minority ethnic backgrounds due to perceived cultural and communication difficulties, including studies where there might be language/literacy problems in obtaining informed consent. This study addressed these difficulties by developing audio-recorded methods of obtaining informed consent and recording data. This report outlines 1 our experiences with securing recruitment to a qualitative study investigating alternative methods of data collection, and 2 the development of a standardised process for obtaining informed consent from individuals from minority ethnic backgrounds whose main language does not have an agreed written form. Methods Two researchers from South Asian backgrounds recruited adults with Type 2 diabetes whose main language was spoken and not written, to attend a series of focus groups. A screening tool was used at recruitment in order to assess literacy skills in potential participants. Informed consent was obtained using audio-recordings of the patient information and recording patients' verbal consent. Participants' perceptions of this method of obtaining consent were recorded. Results Recruitment rates were improved by using telephone compared to face-to-face methods. The screening tool was found to be acceptable by all potential participants. Audio-recorded methods of obtaining informed consent were easy to implement and accepted by all participants. Attrition rates differed according to ethnic group. Snowballing techniques only partly improved participation rates. Conclusion Audio-recorded methods of obtaining informed consent are an acceptable alternative to written consent in study populations where literacy skills are variable. Further exploration of issues relating to attrition is required, and a range of methods may be necessary in order to maximise response and participation rates.

  9. Analysis of multiplex gene expression maps obtained by voxelation

    Directory of Open Access Journals (Sweden)

    Smith Desmond J

    2009-04-01

    Full Text Available Abstract Background Gene expression signatures in the mammalian brain hold the key to understanding neural development and neurological disease. Researchers have previously used voxelation in combination with microarrays for acquisition of genome-wide atlases of expression patterns in the mouse brain. On the other hand, some work has been performed on studying gene functions, without taking into account the location information of a gene's expression in a mouse brain. In this paper, we present an approach for identifying the relation between gene expression maps obtained by voxelation and gene functions. Results To analyze the dataset, we chose typical genes as queries and aimed at discovering similar gene groups. Gene similarity was determined by using the wavelet features extracted from the left and right hemispheres averaged gene expression maps, and by the Euclidean distance between each pair of feature vectors. We also performed a multiple clustering approach on the gene expression maps, combined with hierarchical clustering. Among each group of similar genes and clusters, the gene function similarity was measured by calculating the average gene function distances in the gene ontology structure. By applying our methodology to find similar genes to certain target genes we were able to improve our understanding of gene expression patterns and gene functions. By applying the clustering analysis method, we obtained significant clusters, which have both very similar gene expression maps and very similar gene functions respectively to their corresponding gene ontologies. The cellular component ontology resulted in prominent clusters expressed in cortex and corpus callosum. The molecular function ontology gave prominent clusters in cortex, corpus callosum and hypothalamus. The biological process ontology resulted in clusters in cortex, hypothalamus and choroid plexus. Clusters from all three ontologies combined were most prominently expressed in

  10. Obtaining of Peracetic Cellulose from Oat Straw for Paper Manufacturing

    Directory of Open Access Journals (Sweden)

    Tetyana V. Zelenchuk

    2017-10-01

    Full Text Available Background. Development of technology for obtaining peracetic pulp from oat straw and its use in the production of one of the paper mass types. Objective. Determination of peracetic cooking technological parameters’ optimal values for oat straw peracetic cellulose quality indicators. Methods. The oat straw cooking was carried out with peracetic acid at 95 ± 1 °C from 90 to 180 min for hydromodulus 8:1 and 7:1, using a sodium tungstate catalyst. To determine the oat straw peracetic cellulose mechanical indexes, laboratory samples of paper weighing 70 g/m2 were made. Results. Technological parameters’ optimum values (temperature, cooking duration, hydromodulus, hydrogen peroxide and acetic acid concentration for the oat straw delignification process were established. It is shown that the sodium tungstate catalyst addition to the cooking solution at a rate of up to 1 % of the plant raw material weight helps to reduce the lignin content in cellulose to 15 %. A diagram of the cellulose yield dependence on its residual lignin content for various methods of non-wood plant material species delignification is constructed. The high efficiency of the peracetic method for obtaining cellulose from non-wood plant raw materials, in particular from oat straw, has been confirmed. It is determined that the obtained peracetic cellulose from oat straw has high mechanical indexes. Conclusions. Oat straw peracetic cellulose can be used for the production of paper and cardboard mass types, in particular wrapping paper.

  11. Experimental device for obtaining calibration factor for the total count technique

    International Nuclear Information System (INIS)

    Gonçalves, Eduardo R.; Braz, Delson; Brandão, Luís Eduardo B.

    2017-01-01

    Nuclear technologies have widely used on industry plants in order to help to solve troubles processes/design or just obtain information of them. The Total Count technique for flow measurement has as main advantages: being an absolute technique, because it is independent of additional devices readings unless the directly used for recording the radioactive cloud, requiring only a single detector to provide the final result; the independence of the internal volume of the transport duct, can be applied in the presence or absence of obstructions; no restriction as to the nature of the product or material to be conveyed; it is a noninvasive technique which allows real-time diagnostics. To use Total Count Technique, knowledge of a geometric calibration factor is required. Called Factor F, it is obtained in the laboratory using an experimental apparatus to faithfully reproduce the geometry of the detection system and the pipeline that being analyzed and using the same radiotracer, therefore, its value is constant for each specific measuring system under survey. This experimental apparatus for obtaining the factor F consisting by a pipe of 2 ″PVC, which simulates a transmission line, where they were deposited 500 ml oil and the use of a specific pipette for use viscous fluids were added sequentially aliquots (50.00 ± 0.01) μl radiotracer (radionuclide photopeak energy of 198 Au 411.8 keV) and analyzing data obtained by three distinct detection systems composed of detectors NaI scintillators 1″ x 1 ″ and a data acquisition system. (author)

  12. Experimental device for obtaining calibration factor for the total count technique

    Energy Technology Data Exchange (ETDEWEB)

    Gonçalves, Eduardo R.; Braz, Delson [Coordenacao de Pos-Graduacao e Pesquisa de Engenharia (PEN/COPPE/UFRJ), Rio de Janeiro, RJ (Brazil). Programa de Engenharia Nuclear; Brandão, Luís Eduardo B. [Instituto de Engenharia Nuclear (IEN/CNEN-RJ), Rio de Janeiro, RJ (Brazil). Divisao de Reatores

    2017-07-01

    Nuclear technologies have widely used on industry plants in order to help to solve troubles processes/design or just obtain information of them. The Total Count technique for flow measurement has as main advantages: being an absolute technique, because it is independent of additional devices readings unless the directly used for recording the radioactive cloud, requiring only a single detector to provide the final result; the independence of the internal volume of the transport duct, can be applied in the presence or absence of obstructions; no restriction as to the nature of the product or material to be conveyed; it is a noninvasive technique which allows real-time diagnostics. To use Total Count Technique, knowledge of a geometric calibration factor is required. Called Factor F, it is obtained in the laboratory using an experimental apparatus to faithfully reproduce the geometry of the detection system and the pipeline that being analyzed and using the same radiotracer, therefore, its value is constant for each specific measuring system under survey. This experimental apparatus for obtaining the factor F consisting by a pipe of 2 ″PVC, which simulates a transmission line, where they were deposited 500 ml oil and the use of a specific pipette for use viscous fluids were added sequentially aliquots (50.00 ± 0.01) μl radiotracer (radionuclide photopeak energy of 198 Au 411.8 keV) and analyzing data obtained by three distinct detection systems composed of detectors NaI scintillators 1″ x 1 ″ and a data acquisition system. (author)

  13. Obtaining the Andersen's chart, triangulation algorithm

    DEFF Research Database (Denmark)

    Sabaliauskas, Tomas; Ibsen, Lars Bo

    Andersen’s chart (Andersen & Berre, 1999) is a graphical method of observing cyclic soil response. It allows observing soil response to various stress amplitudes that can lead to liquefaction, excess plastic deformation or stabilizing soil response. The process of obtaining the original chart has...

  14. Assessment of differences between products obtained in conventional and vacuum spray dryer

    Directory of Open Access Journals (Sweden)

    Fernanda de Melo RAMOS

    Full Text Available Abstract In this work, an experimental unit of a vacuum spray dryer was built. This prototype attempted to combine the advantages of freeze-drying (drying at low temperatures due to vacuum and spray drying (increase of surface area aiming the improvement of heat transfer efficiency. Maltodextrin solutions were dried in the vacuum operated equipment and in conventional spray dryer. The vacuum spray dryer system allowed obtaining powder at low temperatures due to the lowering of pressure conditions (2-5 kPa inside the drying chamber. The products obtained in the two systems were characterized and compared for particle size distribution, moisture content, water activity, bulk density and solubility in water. The processes yields were also evaluated and compared. The vacuum spray dryer system allowed the production of larger, more soluble and less dense particles than those obtained in the conventional configuration of the equipment, resulting in drier and, therefore, with lower water activity particles. Thus, the use of the vacuum spray dryer as a drying technique may be an alternative for the production of powder rich in thermosensitive compounds.

  15. How to obtain traceability on optical radiation measurements?

    Science.gov (United States)

    Matamoros García, Carlos H.

    2006-02-01

    Traceability to national standards provides confidence in measurements results, granting a guaranty when carrying out governmental rules and when demonstrating conformity with quality requirements such as ISO 9000 or ISO/IEC 17025 (and the Mexican equivalent standards). The appropriate traceability contributes with confidence of the quality of products or services. This paper presents different ways to obtain traceability in Mexico for the optical radiation measurements, mentioning some applications, and highlighting the necessity of having traceability to the appropriate units of the SI. Additionally it present the national standards maintained by Centro Nacional de Metrologia (CENAM), the national metrology institute in Mexico, that give the technical support to Mexican measurements in this field and the international recognition that the personal of the Optics and Radiometry Division had gained in 10 years of development.

  16. Results of regular study on radionuclidic purity of sup(99m)Tc obtained from 99Mo-sup(99m)Tc generators

    International Nuclear Information System (INIS)

    Vlcek, J.; Rohacek, J.; Husak, V.

    1979-01-01

    A total of 39 sup(99m)Tc eluates obtained from 9 99 Mo-sup(99m)Tc generators delivered by The Radiochemical Centre Amersham during one year was studied with regard to their radionuclide purity. Using a Ge(Li) spectrometer the contaminants 60 Co, 103 Ru, 131 I, 134 Cs, 140 La and 188 Re were found in sup(99m)Tc-eluates with average levels ranging from 2.9 x 10 -3 to 2.8 x 10 -1 per cent of sup(99m)Tc activity. The additional total body absorbed dose caused by these contaminants, as calculated from their average content in sup(99m)Tc eluates, was less than 1% of the dose due to sup(99m)Tc pertechnetate. (orig.) 891 MG/orig. 892 CS [de

  17. Characterisation of Aronia powders obtained by different drying processes.

    Science.gov (United States)

    Horszwald, Anna; Julien, Heritier; Andlauer, Wilfried

    2013-12-01

    Nowadays, food industry is facing challenges connected with the preservation of the highest possible quality of fruit products obtained after processing. Attention has been drawn to Aronia fruits due to numerous health promoting properties of their products. However, processing of Aronia, like other berries, leads to difficulties that stem from the preparation process, as well as changes in the composition of bioactive compounds. Consequently, in this study, Aronia commercial juice was subjected to different drying techniques: spray drying, freeze drying and vacuum drying with the temperature range of 40-80 °C. All powders obtained had a high content of total polyphenols. Powders gained by spray drying had the highest values which corresponded to a high content of total flavonoids, total monomeric anthocyanins, cyaniding-3-glucoside and total proanthocyanidins. Analysis of the results exhibited a correlation between selected bioactive compounds and their antioxidant capacity. In conclusion, drying techniques have an impact on selected quality parameters, and different drying techniques cause changes in the content of bioactives analysed. Spray drying can be recommended for preservation of bioactives in Aronia products. Powder quality depends mainly on the process applied and parameters chosen. Therefore, Aronia powders production should be adapted to the requirements and design of the final product. Copyright © 2013 Elsevier Ltd. All rights reserved.

  18. Water based suspensions of iron oxide obtained by laser target evaporation for biomedical applications

    Energy Technology Data Exchange (ETDEWEB)

    Novoselova, I.P. [Ural Federal University, Department of Magnetism and Magnetic Nanomaterials, Lenin Ave. 51, 620083 Yekaterinburg (Russian Federation); Immanuel Kant Baltic Federal University, Science and Technology Park “Fabrica”, Gaidara St. 6, 236022 Kaliningrad (Russian Federation); Safronov, A.P. [Ural Federal University, Department of Magnetism and Magnetic Nanomaterials, Lenin Ave. 51, 620083 Yekaterinburg (Russian Federation); Institute of Electrophysics UD RAS, Amundsena St. 106, 620016 Yekaterinburg (Russian Federation); Samatov, O.M. [Institute of Electrophysics UD RAS, Amundsena St. 106, 620016 Yekaterinburg (Russian Federation); Beketov, I.V.; Medvedev, A.I. [Ural Federal University, Department of Magnetism and Magnetic Nanomaterials, Lenin Ave. 51, 620083 Yekaterinburg (Russian Federation); Institute of Electrophysics UD RAS, Amundsena St. 106, 620016 Yekaterinburg (Russian Federation); Kurlyandskaya, G.V. [Ural Federal University, Department of Magnetism and Magnetic Nanomaterials, Lenin Ave. 51, 620083 Yekaterinburg (Russian Federation); Universidad del País Vasco, UPV/EHU, Dpto. de Electricidad y Electrónica, P.O. Box 644, Bilbao 48080 (Spain)

    2016-10-01

    In this work spherical magnetic nanoparticles (MNPs) of iron oxide were obtained by laser target evaporation technique (LTE). Water based suspensions were prepared on the basis of obtained MNPs and their properties were also studied including inductive heat capacity. Their structure and properties were studied by a number of techniques including magnetometry and heat capacity measurements. Magnetic induction heating experiment show the specific loss power (SLP) value in the narrow range from 1.30 to 1.45 W/g for all samples under consideration when using alternating magnetic field of 1.7 kA/m and frequency of 210 kHz. These parameters insure that LTE MNPs are interesting materials promising for magnetic fluid hyperthermia. - Highlights: • Spheric oxide nanoparticles obtained by productive laser target evaporation method. • Experiment shows the specific loss power value in the narrow range for all samples. • Obtained results insure these objects as interesting material for hyperthermia.

  19. Water based suspensions of iron oxide obtained by laser target evaporation for biomedical applications

    International Nuclear Information System (INIS)

    Novoselova, I.P.; Safronov, A.P.; Samatov, O.M.; Beketov, I.V.; Medvedev, A.I.; Kurlyandskaya, G.V.

    2016-01-01

    In this work spherical magnetic nanoparticles (MNPs) of iron oxide were obtained by laser target evaporation technique (LTE). Water based suspensions were prepared on the basis of obtained MNPs and their properties were also studied including inductive heat capacity. Their structure and properties were studied by a number of techniques including magnetometry and heat capacity measurements. Magnetic induction heating experiment show the specific loss power (SLP) value in the narrow range from 1.30 to 1.45 W/g for all samples under consideration when using alternating magnetic field of 1.7 kA/m and frequency of 210 kHz. These parameters insure that LTE MNPs are interesting materials promising for magnetic fluid hyperthermia. - Highlights: • Spheric oxide nanoparticles obtained by productive laser target evaporation method. • Experiment shows the specific loss power value in the narrow range for all samples. • Obtained results insure these objects as interesting material for hyperthermia.

  20. Development, calibration and experimental results obtained with an innovative calorimeter (CALMOS) for nuclear heating measurements

    International Nuclear Information System (INIS)

    Carcreff, H.; Cloute-Cazalaa, V.; Salmon, L.

    2011-01-01

    Nuclear heating inside an MTR reactor has to be known in order to be able to control samples temperature during irradiation experiments. An R and D program has been carried out at CEA to design a new type of in-core calorimetric system. This new development, started in 2002, has for main objective to manufacture a calorimeter suitable to monitoring nuclear heating inside the 70 MWth OSIRIS material testing reactor operated by CEA's Nuclear Energy Div. at the Saclay research center. An innovative calorimetric probe, associated to a specific handling system, has been designed to provide access to measurements both along the fissile height and on the upper part of the core, where nuclear heating still remains high. Two mock-ups of the probe were manufactured and tested in 2005 and 2009 in ex-core area of OSIRIS reactor for process validation, while a displacement system has been especially studied to move the probe along a given axial measurement range. This paper deals with the development, tests on preliminary mock-ups and the finalization of the probe. Main modeling and experimental results are presented. Moreover, alternative methods to calibration for nuclear heating rate measurements which are now possible with this new calorimeter are presented and discussed. (authors)

  1. Development, calibration, and experimental results obtained with an innovative calorimeter (CALMOS) for nuclear heating measurements

    International Nuclear Information System (INIS)

    Carcreff, Hubert; Cloute-Cazalaa, Veronique; Salmon, Laurent

    2012-01-01

    Nuclear heating inside an MTR reactor has to be known in order to be able to control samples temperature during irradiation experiments. An R and D program has been carried out at CEA to design a new type of in-core calorimetric system. This new development, started in 2002, has for main objective to manufacture a calorimeter suitable to monitoring nuclear heating inside the 70 MWth OSIRIS material testing reactor operated by CEA's Nuclear Energy Division at the Saclay research center. An innovative calorimetric probe, associated to a specific handling system, has been designed to provide access to measurements both along the fissile height and on the upper part of the core, where nuclear heating still remains high. Two mock-ups of the probe were manufactured and tested in 2005 and 2009 in ex-core area of OSIRIS reactor for process validation, while a displacement system has been especially studied to move the probe along a given axial measurement range. This paper deals with the development, tests on preliminary mock-ups and the finalization of the probe. Main modeling and experimental results are presented. Moreover, alternative methods to calibration for nuclear heating rate measurements which are now possible with this new calorimeter are presented and discussed. (authors)

  2. Structural investigations of zirconia powders obtained by hf-plasmochemical denitration

    International Nuclear Information System (INIS)

    Dedov, N.V.; Ivanov, Yu.F.; Dorda, F.A.; Paul', A.V.; Zav'yalov, A.V.; Koneva, N.A.; Korobtsev, V.P.; Kutyavin, E.M.; Mazin, V.I.; Matyukha, V.A.

    1992-01-01

    Results are presented of structural and physicochemical investigations of unstabilized and stabilized (using yttria, magnesia, calcium oxide and alumina) zirconia, obtained from nitrate solutions on pilot HF-plasmochemical equipment with an electric rating of 63 kW. The phase composition of the ultradispersed powder is shown. Morphological and grain-size analyses were carried out on the EM-125K electron diffraction microscope. specimens were prepared by applying powder to a carbon film obtained in a VUP-4 vacuum cell. The phase composition was studied by x-ray analysis on the DRON-3 diffractometer. These studies established that the main morphological constituents of the ZrO 2 powder are polycrystalline hollow spheres and fragments of films. The average sizes (diameter) of the spheres in 0.77 μ (mean square deviation σ n = 0.57μ) and for the grains in them 31 nm (σ n = 9.5 nm). There exists a certain correlation between the dimensions of the polycrystalline spheres and their grain structure - the coarser the powders, the larger the grains observed

  3. Automatic processing of isotopic dilution curves obtained by precordial detection

    International Nuclear Information System (INIS)

    Verite, J.C.

    1973-01-01

    Dilution curves pose two distinct problems: that of their acquisition and that of their processing. A study devoted to the latter aspect only was presented. It was necessary to satisfy two important conditions: the treatment procedure, although applied to a single category of curves (isotopic dilution curves obtained by precordial detection), had to be as general as possible; to allow dissemination of the method the equipment used had to be relatively modest and inexpensive. A simple method, considering the curve processing as a process identification, was developed and should enable the mean heart cavity volume and certain pulmonary circulation parameters to be determined. Considerable difficulties were encountered, limiting the value of the results obtained though not condemning the method itself. The curve processing question raised the problem of their acquisition, i.e. the number of these curves and their meaning. A list of the difficulties encountered is followed by a set of possible solutions, a solution being understood to mean a curve processing combination where the overlapping between the two aspects of the problem is accounted for [fr

  4. Design and construction of a prototype to obtain TeO2

    International Nuclear Information System (INIS)

    Roque H, I.

    1997-01-01

    At the National Institute of Nuclear Research is developed the process to produce the radioisotope Iodine 131 which is employed in medicine with therapeutical purposes. The raw material to produce iodine 131 is tellurium dioxide (TeO 2 ). TeO 2 is intended to be produced from a prototype being this aim of this thesis named D esign and construction of a prototype to obtain TeO 2 . The TeO 2 obtained must have specific physicochemical characteristics, being necessary an special design of a prototype which will guarantee the quality of tellurium dioxide obtention. Design and building the final prototype project, was developed in to three stages. At the first stage, the TeO 2 was obtained at the laboratory, this allows to know the basic reaction characteristics. The second stage purpose, was to work with an former prototype which allowed to produce 100 g of tellurium dioxide. In the last stage a depurated chemical process parameters was made and the prototype was refined in regard to its mechanical design, giving us as result the final prototype. With this final prototype, the production reaches 2 Kg/week of tellurium dioxide with the best physicochemical properties which is to be employed as raw material in order to produce iodine 131. (Author)

  5. Global market trade policy analysis for petroleum oils and oils obtained from bituminous minerals, crude

    Directory of Open Access Journals (Sweden)

    Bagheri, F.

    2012-01-01

    Full Text Available This article is based on surveying the custom tariffs imposed on the world export market of Petroleum Oils and Oils Obtained from Bituminous Minerals, Crude. We obtained the data according to the most updated available data provided online by UNCTAD and World Bank. The results indicate that none of the 142 countries in the world market of this product have imposed non-tariff trade barriers on the import of Petroleum Oils and Oils Obtained from Bituminous Minerals, Crude. The developed countries and the countries with transition economies are the main world import partners. European Union, United States, China, Japan, South Korea, Canada, Singapore, Taiwan, Thailand, South Africa, Australia, Turkey, Brazil, Sweden and Belarus are the examples and have imposed low custom tariffs on Petroleum Oils and Oils Obtained from Bituminous Minerals, Crude.

  6. The hardness of synthetic products obtained from cooled and crystallized basaltic melts (in Romanian

    Directory of Open Access Journals (Sweden)

    Daniela Ogrean

    2001-04-01

    Full Text Available The Hardness of Synthetic Products Obtained from Cooled and Crystallized Basaltic Melts. Hardness is one of the main properties of the products obtained from cooled and crystallized basaltic melts under a controlled thermal regime. It influences the abrasion tear resistance of the resulted material. The microhardness measurements on the samples (bricks, boards, gutters, armour plates, tubes indicated Vickers hardness value between 757–926 for the materials obtained from Şanovita basalts (Timiş district and between 539–958 respectively, in case of the Racoş basalts (Braşov district. There is a certain variation of the hardness within the same sample, in various measurement points, within the theoretical limits of the hardnesses of the pyroxenes and that of the spinels.

  7. Acoustic barriers obtained from industrial wastes.

    Science.gov (United States)

    Garcia-Valles, M; Avila, G; Martinez, S; Terradas, R; Nogués, J M

    2008-07-01

    Acoustic pollution is an environmental problem that is becoming increasingly more important in our society. Likewise, the accumulation of generated waste and the need for waste management are also becoming more and more pressing. In this study we describe a new material--called PROUSO--obtained from industrial wastes. PROUSO has a variety of commercial and engineering, as well as building, applications. The main raw materials used for this environmentally friendly material come from slag from the aluminium recycling process, dust from the marble industry, foundry sands, and recycled expanded polystyrene from recycled packaging. Some natural materials, such as plastic clays, are also used. To obtain PROUSO we used a conventional ceramic process, forming new mineral phases and incorporating polluted elements into the structure. Its physical properties make PROUSO an excellent acoustic and thermal insulation material. It absorbs 95% of the sound in the frequency band of the 500 Hz. Its compressive strength makes it ideal for use in ceramic wall building.

  8. Minimally processed beetroot waste as an alternative source to obtain functional ingredients.

    Science.gov (United States)

    Costa, Anne Porto Dalla; Hermes, Vanessa Stahl; Rios, Alessandro de Oliveira; Flôres, Simone Hickmann

    2017-06-01

    Large amounts of waste are generated by the minimally processed vegetables industry, such as those from beetroot processing. The aim of this study was to determine the best method to obtain flour from minimally processed beetroot waste dried at different temperatures, besides producing a colorant from such waste and assessing its stability along 45 days. Beetroot waste dried at 70 °C originates flour with significant antioxidant activity and higher betalain content than flour produced from waste dried at 60 and 80 °C, while chlorination had no impact on the process since microbiological results were consistent for its application. The colorant obtained from beetroot waste showed color stability for 20 days and potential antioxidant activity over the analysis period, thus it can be used as a functional additive to improve nutritional characteristics and appearance of food products. These results are promising since minimally processed beetroot waste can be used as an alternative source of natural and functional ingredients with high antioxidant activity and betalain content.

  9. Synthesis and characterization of hematite pigment obtained from a steel waste industry.

    Science.gov (United States)

    Prim, S R; Folgueras, M V; de Lima, M A; Hotza, D

    2011-09-15

    Pigments that meet environmental and technology requirements are the focus of the research in the ceramic sector. This study focuses on the synthesis of ceramic pigment by encapsulation of hematite in crystalline and amorphous silica matrix. Iron oxide from a metal sheet rolling process was used as chromophore. A different content of hematite and silica was homogenized by conventional and high energy milling. The powders obtained after calcinations between 1050 and 1200 °C for 2h were characterized by X-ray diffraction and SEM analysis. The pigments were applied to ceramic enamel and porcelain body. The effect of pigment was measured by comparing L*a*b* values of the heated samples. Results showed that the color developed is influenced by variables such as oxide content employed, conditions of milling and processing temperature. The results showed that the use of pigment developed does not interfere in microstructural characteristics of pigmented material. The best hue was obtained from samples with 15 wt% of chromophore, heated at 1200 °C in amorphous silica matrix. Copyright © 2011 Elsevier B.V. All rights reserved.

  10. Evaluation of magnetic properties of NI-ZN ferrites obtained by different synthesis methods

    International Nuclear Information System (INIS)

    Simoes, A.N.; Neiva, L.S.; Simoes, V.N.; Gama, L.; Gomes Filho, A.C.; Oliveira, J.B.L.

    2012-01-01

    Ceramic oxides that exhibit ferromagnetic behavior represent important commercial products for the electronics industry and are commonly known as ferrites. The Ni-Zn ferrites are considered to be one of the most versatile and soft due to its high electrical resistivity and low eddy current losses. Thus, this study aims to evaluate the magnetic properties of Ni-Zn ferrite obtained by the Pechini and combustion reaction. After synthesis the powders were characterized by XRD, SEM, BET and magnetic measurements. The results showed that for both methods of synthesis used was the formation of the spinel phase of Ni-Zn ferrite. The micrographs show that the powders obtained by both methods have regular shapes and spherical. Were determined by BET surface area is 26 m 2 /g by the Pechini and 13 m 2 /g by combustion. And the samples synthesized by Pechini method obtained the best magnetic characteristics (author)

  11. Characterization and obtainment of phosphate rock concentrates of Turmequé, Boyacá

    Science.gov (United States)

    Zanguña, S. Quijano; Lozano Gómez, L. F.; Pineda Triana, Y.

    2017-12-01

    The work focuses on the use and exploitation of the mineral concentrates from phosphate rock (PR) coming from mines with a low percentage of phosphorus. The procedure was based on the collection of a source of phosphate rock from the department of Boyacá (municipality of Turmequé), using a randomized design with three replications. The samples were initially milled and sifted using meshes between 140 and 200 US standard, homogenizing them and improving the process of solubility of the phosphorus in the soil. We conduced Z-potential tests, which show that by performing a prior wash on the mineral and maintaining certain concentrations and pH defined, better results are achieved in terms of the buoyancy of the particles in the flotation process. The results obtained from the microflotation tests; both direct and inverse, and the results of chemical composition, with X-Ray Fluorescence (XRF) and X-Ray Diffraction (XRD), before and after the microflotation process, were carried out to obtain of commercial laws grade phosphate rock concentrate, confirm that the protocol used increases by 9% the value of total phosphorus in the collected sample. These concentrates from phosphate rock, could be used in the future for the attainment of simple superphosphate (SSP), with the help of sulphuric acid and ammonium thiosulphate mixtures.

  12. Agreement between direct and indirect blood pressure measurements obtained from anesthetized Hispaniolan Amazon parrots.

    Science.gov (United States)

    Acierno, Mark J; da Cunha, Anderson; Smith, Julie; Tully, Thomas N; Guzman, David Sanchez-Migallon; Serra, Verna; Mitchell, Mark A

    2008-11-15

    To determine the level of agreement between direct and indirect blood pressure measurements obtained from healthy Hispaniolan Amazon parrots (Amazona ventralis) anesthetized with isoflurane. Validation study. 16 healthy adult Hispaniolan Amazon parrots. Parrots were anesthetized, and a 26-gauge, 19-mm catheter was placed percutaneously in the superficial ulnar artery for direct measurement of systolic, mean, and diastolic arterial pressures. Indirect blood pressure measurements were obtained with a Doppler ultrasonic flow detector and an oscillometric unit. The Bland-Altman method was used to compare direct and indirect blood pressure values. There was substantial disagreement between direct systolic arterial blood pressure and indirect blood pressure measurements obtained with the Doppler detector from the wing (bias, 24 mm Hg; limits of agreement, -37 to 85 mm Hg) and from the leg (bias, 14 mm Hg; limits of agreement, -14 to 42 mm Hg). Attempts to obtain indirect blood pressure measurements with the oscillometric unit were unsuccessful. Results suggested that there was substantial disagreement between indirect blood pressure measurements obtained with a Doppler ultrasonic flow detector in anesthetized Hispaniolan Amazon parrots and directly measured systolic arterial blood pressure.

  13. Image enhancement by spatial frequency post-processing of images obtained with pupil filters

    Science.gov (United States)

    Estévez, Irene; Escalera, Juan C.; Stefano, Quimey Pears; Iemmi, Claudio; Ledesma, Silvia; Yzuel, María J.; Campos, Juan

    2016-12-01

    The use of apodizing or superresolving filters improves the performance of an optical system in different frequency bands. This improvement can be seen as an increase in the OTF value compared to the OTF for the clear aperture. In this paper we propose a method to enhance the contrast of an image in both its low and its high frequencies. The method is based on the generation of a synthetic Optical Transfer Function, by multiplexing the OTFs given by the use of different non-uniform transmission filters on the pupil. We propose to capture three images, one obtained with a clear pupil, one obtained with an apodizing filter that enhances the low frequencies and another one taken with a superresolving filter that improves the high frequencies. In the Fourier domain the three spectra are combined by using smoothed passband filters, and then the inverse transform is performed. We show that we can create an enhanced image better than the image obtained with the clear aperture. To evaluate the performance of the method, bar tests (sinusoidal tests) with different frequency content are used. The results show that a contrast improvement in the high and low frequencies is obtained.

  14. Obtaining of mullite by fast burning from bentonite clays from Paraiba state, BR

    International Nuclear Information System (INIS)

    Gomes, J.; Rocha, A.I.O.; Oliveira, S.S.; Neves, G.A.; Lira, H.L.; Santana, L.N.L.; Menezes, R.R.

    2012-01-01

    Bentonite clays are aluminium-silicates that when heated turn into mullite. The sintering of mullite obtained from these mineral clays by quick microwaves heating comes up as an alternative process for mullite powders synthesis. The use of quick heating on ceramics nanopowders synthesis is a recent technology that is being successfully used on synthesis with microwaves and synthesis process by combustion. The quick microwaves heating enables adding heat quickly and equally, accelerating the nucleation kinetics and the development of the mullite stage. Thus, the purpose of this work is to analyze the effect of the microwaves heating process variables, analyzing the influence of the applied power and of the heating rate on the mullite powders obtaining from bentonite clays. The clays have been favored and submitted to the following characterizations: chemical granulometric and mineralogically. Subsequently, the clays have been delaminated aiming deagglomeration and separation of the thinner fractions and submitted to granulometric and mineralogical characterization. The synthesis has been realized on a domestic microwaves oven. The obtained powders have been characterized by X-ray diffraction. The results showed that the applied power variation and the sintering time are fundamental on the obtaining of mullite powders. (author)

  15. Chemical characterization of xyloglucan obtained from Tamarindus indica seeds from the semi arid northeastern (Brazil)

    International Nuclear Information System (INIS)

    Rodrigues, Delane da C.; Cunha, Arcelina P.; Silva, Sarah M.F.; Gallao, Maria Izabel; Azeredo, Henriette M.C. de

    2015-01-01

    Playing an important role in food, seeds are sources of carbohydrates, proteins and lipids, so they have been explored for a long time by the food industry. For this reason, the objective of present work is to obtain and characterize xyloglucan obtained from tamarind seeds (Tamarindus indica). In order to assess possible industrial applications of the polysaccharide, it was characterized by Infrared Fourier Transform spectroscopy (FTIR), Nuclear Magnetic Resonance (NMR) and Thermogravimetric Analysis (TGA). Search results showed that it was possible to perform xyloglucan extraction but the process still requires improvements in order to increase the extraction yield. FTIR, NMR and TGA results were similar to those found in literature. (author)

  16. On obtaining Knuth, Morris, and Pratt's string matcher by partial evaluation

    DEFF Research Database (Denmark)

    Ager, Mads Sig; Danvy, Olivier; Rohde, Henning Korsholm

    2002-01-01

    We present the first formal proof that partial evaluation of a quadratic string matcher can yield the precise behaviour of the KMP string matcher. Obtaining the KMP is a canonical example of partial evaluation: one starts from the naive, quadratic program checking whether a pattern occurs in a text......; one observes that backtracking can be performed at partial-evaluation time (a binding-time shift); and one obtains a specialized program that does not back up on the text, a la KMP. We are not aware, however, of any formal proof that partial evaluation of a staged string matcher precisely yields...... the KMP string matcher. To compare the performance of the KMP and the result of specializing a staged string matcher, we have compared the traces of the successive indices at which the text is addressed. We have found that staged string matchers keeping no negative information do not perform as well...

  17. On Obtaining Knuth, Morris, and Pratt's String Matcher by Partial Evaluation

    DEFF Research Database (Denmark)

    Ager, Mads Sig; Danvy, Olivier; Rohde, Henning Korsholm

    2002-01-01

    We present the first formal proof that partial evaluation of a quadratic string matcher can yield the precise behaviour of the KMP string matcher. Obtaining the KMP is a canonical example of partial evaluation: one starts from the naive, quadratic program checking whether a pattern occurs in a text......; one observes that backtracking can be performed at partial-evaluation time (a binding-time shift); and one obtains a specialized program that does not back up on the text, a la KMP. We are not aware, however, of any formal proof that partial evaluation of a staged string matcher precisely yields...... the KMP string matcher. To compare the performance of the KMP and the result of specializing a staged string matcher, we have compared the traces of the successive indices at which the text is addressed. We have found that staged string matchers keeping no negative information do not perform as well...

  18. Coating multilayer material with improved tribological properties obtained by magnetron sputtering

    Science.gov (United States)

    Mateescu, A. O.; Mateescu, G.; Balasoiu, M.; Pompilian, G. O.; Lungu, M.

    2017-02-01

    This work is based on the Patent no. RO 128094 B1, granted by the Romanian State Office for Inventions and Trademarks. The goal of the work is to obtain for investigations tribological coatings with multilayer structure with improved tribological properties, deposited by magnetron sputtering process from three materials (sputtering targets). Starting from compound chemical materials (TiC, TiB2 and WC), as sputtering targets, by deposition in argon atmosphere on polished stainless steel, we have obtained, based on the claims of the above patent, thin films of multilayer design with promising results regarding their hardness, elastic modulus, adherence, coefficient of friction and wear resistance. The sputtering process took place in a special sequence in order to ensure better tribological properties to the coating, comparing to those of the individual component materials. The tribological properties, such as the coefficient of friction, are evaluated using the tribometer test.

  19. Analysis shear wave velocity structure obtained from surface wave methods in Bornova, Izmir

    Energy Technology Data Exchange (ETDEWEB)

    Pamuk, Eren, E-mail: eren.pamuk@deu.edu.tr; Akgün, Mustafa, E-mail: mustafa.akgun@deu.edu.tr [Department of Geophysical Engineering, Dokuz Eylul University, Izmir (Turkey); Özdağ, Özkan Cevdet, E-mail: cevdet.ozdag@deu.edu.tr [Dokuz Eylul University Rectorate, Izmir (Turkey)

    2016-04-18

    Properties of the soil from the bedrock is necessary to describe accurately and reliably for the reduction of earthquake damage. Because seismic waves change their amplitude and frequency content owing to acoustic impedance difference between soil and bedrock. Firstly, shear wave velocity and depth information of layers on bedrock is needed to detect this changing. Shear wave velocity can be obtained using inversion of Rayleigh wave dispersion curves obtained from surface wave methods (MASW- the Multichannel Analysis of Surface Waves, ReMi-Refraction Microtremor, SPAC-Spatial Autocorrelation). While research depth is limeted in active source study, a passive source methods are utilized for deep depth which is not reached using active source methods. ReMi method is used to determine layer thickness and velocity up to 100 m using seismic refraction measurement systems.The research carried out up to desired depth depending on radius using SPAC which is utilized easily in conditions that district using of seismic studies in the city. Vs profiles which are required to calculate deformations in under static and dynamic loads can be obtained with high resolution using combining rayleigh wave dispersion curve obtained from active and passive source methods. In the this study, Surface waves data were collected using the measurements of MASW, ReMi and SPAC at the İzmir Bornova region. Dispersion curves obtained from surface wave methods were combined in wide frequency band and Vs-depth profiles were obtained using inversion. Reliability of the resulting soil profiles were provided by comparison with theoretical transfer function obtained from soil paremeters and observed soil transfer function from Nakamura technique and by examination of fitting between these functions. Vs values are changed between 200-830 m/s and engineering bedrock (Vs>760 m/s) depth is approximately 150 m.

  20. Using some results about the Lie evolution of differential operators to obtain the Fokker-Planck equation for non-Hamiltonian dynamical systems of interest

    Science.gov (United States)

    Bianucci, Marco

    2018-05-01

    Finding the generalized Fokker-Planck Equation (FPE) for the reduced probability density function of a subpart of a given complex system is a classical issue of statistical mechanics. Zwanzig projection perturbation approach to this issue leads to the trouble of resumming a series of commutators of differential operators that we show to correspond to solving the Lie evolution of first order differential operators along the unperturbed Liouvillian of the dynamical system of interest. In this paper, we develop in a systematic way the procedure to formally solve this problem. In particular, here we show which the basic assumptions are, concerning the dynamical system of interest, necessary for the Lie evolution to be a group on the space of first order differential operators, and we obtain the coefficients of the so-evolved operators. It is thus demonstrated that if the Liouvillian of the system of interest is not a first order differential operator, in general, the FPE structure breaks down and the master equation contains all the power of the partial derivatives, up to infinity. Therefore, this work shed some light on the trouble of the ubiquitous emergence of both thermodynamics from microscopic systems and regular regression laws at macroscopic scales. However these results are very general and can be applied also in other contexts that are non-Hamiltonian as, for example, geophysical fluid dynamics, where important events, like El Niño, can be considered as large time scale phenomena emerging from the observation of few ocean degrees of freedom of a more complex system, including the interaction with the atmosphere.

  1. Semi-conducting material obtained from natural fiber modified with PAni

    International Nuclear Information System (INIS)

    Rocha, Eli V. da; Silva Junior, Fernando Gomes; Oliveira, Geiza E.; Pinto, Jose Carlos

    2009-01-01

    The surface of natural Brazilian Amazonic fibers (curaua, Ananas erectifolius) was modified with polyaniline nanoparticles, through in-situ preparation of polyaniline nanoparticles in presence of the curaua fibers. As it was shown here, this modification allowed a very significant increase of the electrical conductivity of the fibers (about 2.500 times). The modified materials were also characterized by FTIR (Fourier Transform Infrared Spectroscopy), AFM (Atomic Force Microscopy) and SAXS (Small Angle X-ray Scattering) and the obtained results were used to explain some of the chemical and morphological aspects of the materials. (author)

  2. 2-D images of the metal-halide lamp obtained by experiment and model

    NARCIS (Netherlands)

    Flikweert, A.J.; Beks, M.L.; Nimalasuriya, T.; Kroesen, G.M.W.; Mullen, van der J.J.A.M.; Stoffels, W.W.

    2008-01-01

    The metal-halide lamp shows color segregation caused by diffusion and convection. Two-dimensional imaging of the arc discharge under varying gravity conditions aids in the understanding of the flow phenomena. In this paper, we show results obtained by experiments and by numerical simulations in

  3. 47 CFR 54.615 - Obtaining services.

    Science.gov (United States)

    2010-10-01

    ... provided under § 54.621, that the requester cannot obtain toll-free access to an Internet service provider... thing of value; (6) If the service or services are being purchased as part of an aggregated purchase... submitted and select the most cost-effective alternative. (b) Receiving supported rate. Except with regard...

  4. First donation of human skin obtained from corpse

    International Nuclear Information System (INIS)

    Reyes F, M.L.; Luna Z, D.

    2007-01-01

    The first donation of human skin coming from a cadaverous donor was obtained in the State of Mexico. The skin was obtained of a 34 year-old multi organic donor, the extraction of the same was carried out in an operating theatre by medical personnel, supported by personal of the Radio sterilized Tissue Bank (BTR) of the ININ. The skin was transported to the BTR for it processing. (Author)

  5. 48 CFR 1815.403 - Obtaining cost or pricing data.

    Science.gov (United States)

    2010-10-01

    ... 48 Federal Acquisition Regulations System 6 2010-10-01 2010-10-01 true Obtaining cost or pricing... ADMINISTRATION CONTRACTING METHODS AND CONTRACT TYPES CONTRACTING BY NEGOTIATION Contract Pricing 1815.403 Obtaining cost or pricing data. ...

  6. Benchmark on traveling wave fast reactor with negative reactivity feedback obtained with MCNPX code

    International Nuclear Information System (INIS)

    Gann, V.V.; Gann, A.V.

    2012-01-01

    This paper presents results of computer simulations of traveling wave fast reactor with negative reactivity feedback. The results were obtained using MCNPX code combined with CINDER90 subroutine for depletion calculations. We considered 1-D model of TWR containing 4 m long core made of mixture of 66 at. % 238 U and 34 at. % 10 B. Ignitor made of 235 U was located in the center of the core. Boron was included as imitator of structural in-core materials and coolant. Negative reactivity feedback was adjusted to reactor power of 500 MW. In this case two burning waves originated from the igniter and travel to the ends of the core during the following 40 years; coefficient of utilization of 238 U reached 80 %. Distribution of specific power in traveling wave, isotope concentration of fission products and actinides, neutron flux, fast neutron spectrum, specific activity were calculated. Data of the computer simulation is in qualitative agreement with theoretical results obtained in slow burning wave approximation

  7. Space resolution obtained with a highly segmented SCIFI e.m. calorimeter

    International Nuclear Information System (INIS)

    De Zorzi, G.; Bertino, M.; Bini, C.; De Pedis, D.; Diambrini Palazzi, G.; Di Cosimo, G.; Di Domenico, A.; Gauzzi, P.; Zanello, D.

    1992-01-01

    During the setting up of the LEP-5 experiment, we tested a longitudinal SCIFI e.m. calorimeter, having a module cross area 25x25 mm 2 and 12.5x12.5 mm 2 for large and small modules respectively. The results were obtained with 10 and 50 GeV electrons, and concern the impact point resolution and the transverse distribution of the e.m. shower energy inside the calorimeter. (orig.)

  8. Procedure for the obtainment of ammonium uranyl-tricarbonate suitable for the preparation of sinterable UO2

    International Nuclear Information System (INIS)

    Anasco, Roberto; Amendolara, M.M.; De La Fuente, M.; Gonzalez, A.G.; La Gamma de Batistoni, A.M.; Garcia, E.

    1980-01-01

    Experiments carried out to obtain Ammonium Uranyl-Tricarbonate (AUC) of nuclear purity and with the appropriate physical characteristics to serve as an intermediate stage for the obtainment of sinterable Uranium Dioxide are described. AUC was obtained by precipitation with gaseous ammonium and carbon dioxide from aqueous solutions re-circulation, controlling, in both cases, the flow of the reactive gases, the pH and the temperature. The analyzed working conditions are described, giving also the results from the distribution of the particle size and morphology of the crystals. (M.E.L.) [es

  9. Answers to the questions about food irradiation. Concerning results of animal experiments in the specified integrated research. Data carrying a problem in human health were obtained?

    International Nuclear Information System (INIS)

    Ito, Hitoshi

    2007-01-01

    Experts of Food and Agriculture Organization (FAO)/ International Atomic Energy Agency (IAEA)/ World Health Organization (WHO) committee obtained their conclusion in 1980 that food irradiated with <10 kGy of radiation is safe for human health, which is now globally approved. However, in Japan, there have been still opposite opinions based on the doubt in the title on the safety of irradiated food. In this paper, the author answers those questions as he was a member to arrange the Research in the title for food irradiation. Described are data presentation and explanation about results of toxicity studies of diets added with irradiated materials of: weight reductions in rat ovary by irradiated potato (ip) in chronic studies, and in mouse testicle and ovary of F3 generation from the ancestor mice kept on diet with irradiated onion (io); bone malformation in mice by io; and reduction of body weight gain in female rats by ip and increase of mortality of male rats by ip. These are analyzed on the aspects of radiation dose-response, sustained tendency of results throughout the living period or generation, and apparent abnormality by other factors; and normal variation due to individual difference is pointed out to contribute to these findings. The safety test of irradiated food has been conducted valid not only in animal experiments but also other tests like genotoxicity and analysis of radiation-degraded products. (R.T.)

  10. Simulation of simultaneously obtaining ocean temperature and salinity using dual-wavelength Brillouin lidar

    International Nuclear Information System (INIS)

    Yu, Yin; Ma, Yong; Li, Hao; Huang, Jun; Fang, Yu; Liang, Kun; Zhou, Bo

    2014-01-01

    A method for simultaneously obtaining the ocean temperature and salinity based on dual-wavelength Brillouin lidar is proposed in this letter. On the basis of the relationships between the temperature and salinity and the Brillouin shifts, a retrieval model for retrieving the temperature and salinity is established. By using the retrieval model, the ocean temperature and salinity can be simultaneously obtained through the Brillouin shifts. Simulation based on dual-wavelength Brillouin lidar is also carried out for verification of the accuracy of the retrieval model. Results show that the errors of the retrieval model for temperature and salinity are ±0.27 °C and ±0.33‰. (letter)

  11. Does obtaining an initial magnetic resonance imaging decrease the reamputation rates in the diabetic foot?

    Directory of Open Access Journals (Sweden)

    Marlena Jbara

    2016-06-01

    Full Text Available Objective: Diabetes mellitus (DM through its over glycosylation of neurovascular structures and resultant peripheral neuropathy continues to be the major risk factor for pedal amputation. Repetitive trauma to the insensate foot results in diabetic foot ulcers, which are at high risk to develop osteomyelitis. Many patients who present with diabetic foot complications will undergo one or more pedal amputations during the course of their disease. The purpose of this study was to determine if obtaining an initial magnetic resonance imaging (MRI, prior to the first amputation, is associated with a decreased rate of reamputation in the diabetic foot. Our hypothesis was that the rate of reamputation may be associated with underutilization of obtaining an initial MRI, useful in presurgical planning. This study was designed to determine whether there was an association between the reamputation rate in diabetic patients and utilization of MRI in the presurgical planning and prior to initial forefoot amputations. Methods: Following approval by our institutional review board, our study design consisted of a retrospective cohort analysis of 413 patients at Staten Island University Hospital, a 700-bed tertiary referral center between 2008 and 2013 who underwent an initial great toe (hallux amputation. Of the 413 patients with a hallux amputation, there were 368 eligible patients who had a history of DM with documented hemoglobin A1c (HbA1c within 3 months of the initial first ray (hallux and first metatarsal amputation and available radiographic data. Statistical analysis compared the incidence rates of reamputation between patients who underwent initial MRI and those who did not obtain an initial MRI prior to their first amputation. The reamputation rate was compared after adjustment for age, gender, ethnicity, HbA1c, cardiovascular disease, hypoalbuminemia, smoking, body mass index, and prior antibiotic treatment. Results: The results of our statistical

  12. [Biotechnological cultivation of edible macrofungi: an alternative for obtaining nutraceutics].

    Science.gov (United States)

    Suárez Arango, Carolina; Nieto, Ivonne Jeannette

    2013-01-03

    Macromycetes have been part of the human culture for thousand years, and have been reported as food in the most important civilizations in history. Many nutraceutical properties of macromycetes have been described, such as anti-cancer, anti-tumour, cholesterol lowering, antiviral, antibacterial, or immunomodulatory, among others. Given that production of mushrooms by traditional cultivation and extraction of bioactive metabolites is very difficult in some cases, biotechnology is essential for the development of profitable and productive techniques for obtaining these metabolites. It is the development of this technology, and the ease in which it enables the use of its variables that has allowed mycelium to be cultivated in liquid medium of macrofungi, with a significant reduction in time and an increased production of metabolites. This increased production has led to the study of compounds that have medicinal, nutriceutical and quasi-farmaceutical potential, in the exhausted media and the mycelium. The aim of this review is to provide an overview of the use of liquid-state fermentation as a technological tool for obtaining edible fungi, and the study of these and their metabolites, by describing the different cultivation conditions used in recent years, as well as the results obtained. The relevance of Agaricus, Flammulina, Grifola, Pleurotus and Lentinula genera, will also be discussed, with emphasis on the last one, since Shiitake has been always considered as the ultimate medicinal mushroom. Copyright © 2011 Revista Iberoamericana de Micología. Published by Elsevier España, S.L. All rights reserved.

  13. Characterization of an ecological binder for mortars obtained from recycling of ladle furnace slag

    International Nuclear Information System (INIS)

    Marinho, A.B.; Santos, C.M.; Fontes, W.C.; Matias, A.C.P.; Brigolini, G.J.; Peixoto, R.A.F.; Carvalho, J.F.

    2016-01-01

    A sustainable binder obtained from recycling of a ladle furnace slag from Piracicaba, Sao Paulo, was produced in Laboratory of Construction Materials of Federal University of Ouro Preto (UFOP). A characterization work was performed and the results are presented. The physical, chemical and mineralogical properties was obtained using, among others, the following techniques: X-ray fluorescence (XRF), X-ray diffraction (XRD) with Rietveld refining method, optical microscopy and Scanning electronic microscopy (SEM) with energy dispersive spectroscopy (EDS). The chemical analysis showed predominance of CaO and SiO_3; the mineralogical analysis pointed the predominant presence of calcium-olivine, merwinite and pyroxene and; the images showed predominance of angulous and elongated grains. According to results, the material was classified as a hydraulic binder, with characteristics comparable to hydraulic limes. (author)

  14. Gold nanoparticle assemblies of controllable size obtained by hydroxylamine reduction at room temperature

    Science.gov (United States)

    Tódor, István Sz.; Szabó, László; Marişca, Oana T.; Chiş, Vasile; Leopold, Nicolae

    2014-12-01

    Colloidal nanoparticle assemblies (NPAs) were obtained in a one-step procedure, by reduction of HAuCl4 by hydroxylamine hydrochloride, at room temperature, without the use of any additional nucleating agent. By changing the order of the reactants, NPAs with mean size of 20 and 120 nm were obtained. Because of their size and irregular popcorn like shape, the larger size NPAs show absorption in the NIR spectral region. The building blocks of the resulted nanoassemblies are spherical nanoparticles with diameters of 4-8 and 10-30 nm, respectively. Moreover, by stabilizing the colloid with bovine serum albumin at different time moments after synthesis, NPAs of controlled size between 20 and 120 nm, could be obtained. The NPAs were characterized using UV-Vis spectroscopy, TEM and SEM electron microscopies. In addition, the possibility of using the here proposed NPAs as surface-enhanced Raman scattering (SERS) substrate was assessed and found to provide a higher enhancement compared to conventional citrate-reduced nanoparticles.

  15. Basil (Ocimum basilicum L. essential oil and extracts obtained by supercritical fluid extraction

    Directory of Open Access Journals (Sweden)

    Zeković Zoran P.

    2015-01-01

    Full Text Available The extracts obtained from sweet basil (Ocimum basilicum L. by hydrodistillation and supercritical fluid extraction (SFE were qualitative and quantitative analyzed by GC-MS and GC-FID. Essential oil (EO content of basil sample, determined by an official method, was 0.565% (V/w. The yields of basil obtained by SFE were from 0.719 to 1.483% (w/w, depending on the supercritical fluid (carbon dioxide density (from 0.378 to 0.929 g mL-1. The dominant compounds detected in all investigated samples (EO obtained by hydrodistillation and different SFE extracts were: linalool, as the major compound of basil EO (content from 10.14 to 49.79%, w/w, eugenol (from 3.74 to 9.78% and ä-cardinene (from 3.94 to 8.07%. The quantitative results of GC-MS from peak areas and by GC-FID using external standard method involving main standards, were compared and discussed. [Projekat Ministarstva nauke Republike Srbije, br. TR 31013

  16. Analytical and numerical comparisons of the α parameter obtained from several expressions versus reactivity

    International Nuclear Information System (INIS)

    Minguez, E.

    1983-01-01

    A review of the analytical expressions between α-parameter and reactivity (rho) has been done in this article. Finally, several lineal approximations have been obtained for two important points of values. The analytical expansion has been made using only one family of precursors from delayed neutrons; diffusion equation in one energy groups; neutron flux separability with known spatial function. Numerical results have been obtained using typical data from fast and thermal reactors; considering and homogeneous media of Pu 239 in the first case, and U-235 in the second one. (author)

  17. Ten years of sodium cooled steam generator tests on the C.G.V.S. Synthesis of the results obtained on these equipments and operation experiments of an industrial size test facility

    International Nuclear Information System (INIS)

    Fontaine, J.P.; Llory, M.; Quinet, J.L.

    1984-04-01

    From 1970 to 1980, Electricite de France carried out tests on four steam generators of the fast neutron reactor series on an industrial size testing equipment, the C.G.V.S. (large power testing Circuit for Steam Generators heated by Sodium). After a presentation of the testing installation, types of tests carried out and tested apparatus, a balance of lessons drawn from the circuit exploitation, and from the main results obtained on the tested equipments and on the means of calculation COPI and SICLE codes developed or adopted to simulate steam generator operation. 33 figs., 50 refs [fr

  18. THE IMPORTANCE OF OBSERVING THE DIFFERENCE IN WEBSITE EVALUATIONS OBTAINED FROM DIFFERENT PERSPECTIVES

    Directory of Open Access Journals (Sweden)

    Biljana Rondović

    2017-06-01

    Full Text Available The purpose of this paper is to show how website evaulations differ if performed by different evaluators despite the same methodological framework being used for the assessment. A quantitative analysis of websites was performed according to the modified evaluation framework based on the 2QCV3Q-model. The AHP method was used for the verification of the weight criteria, while a single-factor ANOVA was used to check the difference in the average scores of the evaluations performed by three groups of evaluators The results obtained by the single-factor ANOVA showed a statistically significant difference in the average scores of internal evaluation when compared to the evaluation done by clients and independent evaluators. The results obtained can be used in the banking industry as guidelines and recommendations for the future design or redesign of websites, as well as a literary base for comparative analyses of this kind in developing countries.

  19. Aircraft and ground vehicle friction measurements obtained under winter runway conditions

    Science.gov (United States)

    Yager, Thomas J.

    1989-01-01

    Tests with specially instrumented NASA B-737 and B-727 aircraft together with several different ground friction measuring devices have been conducted for a variety of runway surface types and wetness conditions. This effort is part of the Joint FAA/NASA Aircraft/Ground Vehicle Runway Friction Program aimed at obtaining a better understanding of aircraft ground handling performance under adverse weather conditions, and defining relationships between aircraft and ground vehicle tire friction measurements. Aircraft braking performance on dry, wet, snow-, and ice-covered runway conditions is discussed together with ground vehicle friction data obtained under similar runway conditions. For the wet, compacted snow- and ice-covered runway conditions, the relationship between ground vehicles and aircraft friction data is identified. The influence of major test parameters on friction measurements such as speed, test tire characteristics, and surface contaminant-type are discussed. The test results indicate that use of properly maintained and calibrated ground vehicles for monitoring runway friction conditions should be encouraged particularly under adverse weather conditions.

  20. Manipulating potential wells in Logical Stochastic Resonance to obtain XOR logic

    International Nuclear Information System (INIS)

    Storni, Remo; Ando, Hiroyasu; Aihara, Kazuyuki; Murali, K.; Sinha, Sudeshna

    2012-01-01

    Logical Stochastic Resonance (LSR) is the application of Stochastic Resonance to logic computation, namely the phenomenon where a nonlinear system driven by weak signals representing logic inputs, under optimal noise, can yield logic outputs. We extend the existing results, obtained in the context of bistable systems, to multi-stable dynamical systems, allowing us to obtain XOR logic, in addition to the AND (NAND) and OR (NOR) logic observed in earlier studies. This strategy widens the scope of LSR from the application point of view, as XOR forms the basis of ubiquitous bit-by-bit addition, and conceptually, showing the ability to yield non-monotonic input–output logic associations. -- Highlights: ► We generalize Logical Stochastic Resonance from bistable to multi-stable systems. ► We propose a tristable dynamical system formed of piecewise linear functions. ► The system can correctly reproduce XOR logic behavior using the LSR principle. ► The system yields different logic behavior without the need to change the dynamics.

  1. Obtaining tetracalcium phosphate and hydroxyapatite in powder form by wet method

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, Sara Verusca de; Fook, Marcus Vinicius Lia; Araujo, Elaine Patricia; Medeiros, Keila Machado; Rabello, Guilherme Portela; Barbosa Renata; Araujo, Edcleide Maria, E-mail: saraveruscadeoliveira@yahoo.com.br, E-mail: marcusvinicius@dema.ufcg.edu.br, E-mail: elainepatriciaaraujo@yahoo.com.br, E-mail: keilamm@ig.com.br, E-mail: guilhermeportel@hotmail.com, E-mail: rrenatabarbosa@yahoo.com, E-mail: edcleide@dema.ufcg.edu.br [Universidade Federal de Campina Grande (UAEMa/CCT/UFCG), Campina Grande, PB (Brazil)

    2009-07-01

    The development of research in the area of advanced materials and tissue engineering has increased greatly in recent years found that bioceramics are outstanding in the replacement and regeneration of bone tissue, mainly formed by the calcium phosphate ceramics. The objective of this research is to obtain the calcium phosphate where Ca/P = 1.67 and 2.0, to observe the formation of phases after having subjected these materials to heat treatment. The calcium phosphate was produced by the wet method using a direct reaction of neutralization and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and X-ray microanalysis (EDS). The XRD results confirm the presence of hydroxyapatite phase in the sample with Ca/P = 1.67, whereas the phosphates prepared with Ca/P = 2.0 ratio show a combination of hydroxyapatite and phase β- tricalcium phosphate. The micrographs obtained are characteristic of ceramic material called calcium phosphate. EDS confirmed the presence of Ca, P and O in the material. (author)

  2. SIMULATION OF THE DISTILLATION BY PRESSURE REDUCTION TO OBTAIN ANHYDROUS ETHANOL

    Directory of Open Access Journals (Sweden)

    Yeney Lauzurique Guerra

    2016-10-01

    Full Text Available In this work the distillation by pressure reduction was evaluated through the HYSYS v3.2 process simulator. Due to the lack of data in the consulted bibliography to perform the simulation, the STATGRAPHICS Centurion XVI software was used to obtain a response surface that would define optimal operating conditions. The property package selected to work was based on the Margules model. An anhydrous ethanol molar composition of 0.9917 was obtained. Temperature profiles were analyzed as well as liquid and vapor molar flows and dehydration column composition profiles. The influence of operating parameters on the efficiency of simulated technology was determined by analyzing one case study. According to economic evaluation, the implementation of this technology is not economically profitable; taking into account current prices and costs mostly due to high energy consumption and construction costs of the tower. This result contributes to the pursuit of other profitable technologies from the economic point of view.

  3. Obtaining tetracalcium phosphate and hydroxyapatite in powder form by wet method

    International Nuclear Information System (INIS)

    Oliveira, Sara Verusca de; Fook, Marcus Vinicius Lia; Araujo, Elaine Patricia; Medeiros, Keila Machado; Rabello, Guilherme Portela; Barbosa Renata; Araujo, Edcleide Maria

    2009-01-01

    The development of research in the area of advanced materials and tissue engineering has increased greatly in recent years found that bioceramics are outstanding in the replacement and regeneration of bone tissue, mainly formed by the calcium phosphate ceramics. The objective of this research is to obtain the calcium phosphate where Ca/P = 1.67 and 2.0, to observe the formation of phases after having subjected these materials to heat treatment. The calcium phosphate was produced by the wet method using a direct reaction of neutralization and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and X-ray microanalysis (EDS). The XRD results confirm the presence of hydroxyapatite phase in the sample with Ca/P = 1.67, whereas the phosphates prepared with Ca/P = 2.0 ratio show a combination of hydroxyapatite and phase β- tricalcium phosphate. The micrographs obtained are characteristic of ceramic material called calcium phosphate. EDS confirmed the presence of Ca, P and O in the material. (author)

  4. Correlations between radiological technology graduates academic achievement and their obtainment of a license

    International Nuclear Information System (INIS)

    Park, Myeong Hwan; Kwon, Deok Moon; Seo, Soo Kyo

    2006-01-01

    The study analyzed the correlations between variables like characteristics related to admission, academic achievement, obtainment of a radiological technology license. A majority of participants were from Daegu and academic high schools. Many participants were accepted by general admission selection, and their reason to apply to Daegu Health College was high graduate employment. Their selection for the academic program was made by their parents and themselves. Those who took the same course twice held 35.1%, and those who got an academic warning took 8.5%. The degree of participants' academic achievement showed somewhat low, and they had difficulty in taking their major courses. The average grade for admission was lower in a following selection order: college graduates, general, special, and rural areas. The admission selections and taking science courses in high school showed little significant correlations with obtainment of a radiological technology license. However, the obtainment of the license had significant correlations with retaking the same course, getting an academic warning, and the degree of academic achievement. The results also revealed that the obtainment of the license had little significant correlations with a part-time job experience, having a boy/girlfriend, and student club participation, but it had significant correlations with accommodations and study club participation. In conclusion, it is important to point out that radiological technology graduates' obtainment of a license is closely related with the degree of their academic achievement and their college life

  5. Comparison of NDT techniques to evaluate CFRP. Results obtained in a MAIzfp round robin test

    Energy Technology Data Exchange (ETDEWEB)

    Grosse, Christian U. [Technische Univ. Muenchen (Germany). Chair of Non-destructive Testing; Goldammer, Matthias; Grager, Jan-Carl [Siemens AG Corporate Technology, Muenchen (Germany); and others

    2016-10-01

    Fiber reinforced polymeric materials are used for lightweight constructions and are an integral part of cars, airplanes or rotor blades of wind turbines. Nondestructive testing (NDT) methods play an increasing role concerning the manufacturing process and the inspection during lifetime. The selection of the best NDT technique for a certain application depends - of course - on many factors including the type, position and size of the defect to be detected but also on secondary issues like accessibility, automation, testing costs, reliability and resolution to mention only some. For the more technical-scientific part of these issues, the determination of the probability of detection (PoD) plays a significant role. Early in the design process questions should be raised concerning the probability with which certain attribute of interest (a defect that has an effect on the structural behavior) can be detected (and localized) in a certain construction. Several defect types have been identified to be critical like impact damages, undulations and porosity. Test samples out of differently processed Carbon Fiber-Reinforced Polymers (CFRP) as used in the automotive or aeronautical industry have been produced including defects of different type and size. In order to determine the PoD and to check whether a technique is applicable the different partners applied a broad variety of selected NDT techniques including Micro CT, Ultrasound (including phased-array and air-coupled UT), Active Thermography, Eddy Current, Vibration and Visual Analysis and Local Acoustic Resonance Spectroscopy (LARS). The presentation will summarize some of the results of the experiments and ongoing data analysis.

  6. Comparison of NDT techniques to evaluate CFRP. Results obtained in a MAIzfp round robin test

    International Nuclear Information System (INIS)

    Grosse, Christian U.

    2016-01-01

    Fiber reinforced polymeric materials are used for lightweight constructions and are an integral part of cars, airplanes or rotor blades of wind turbines. Nondestructive testing (NDT) methods play an increasing role concerning the manufacturing process and the inspection during lifetime. The selection of the best NDT technique for a certain application depends - of course - on many factors including the type, position and size of the defect to be detected but also on secondary issues like accessibility, automation, testing costs, reliability and resolution to mention only some. For the more technical-scientific part of these issues, the determination of the probability of detection (PoD) plays a significant role. Early in the design process questions should be raised concerning the probability with which certain attribute of interest (a defect that has an effect on the structural behavior) can be detected (and localized) in a certain construction. Several defect types have been identified to be critical like impact damages, undulations and porosity. Test samples out of differently processed Carbon Fiber-Reinforced Polymers (CFRP) as used in the automotive or aeronautical industry have been produced including defects of different type and size. In order to determine the PoD and to check whether a technique is applicable the different partners applied a broad variety of selected NDT techniques including Micro CT, Ultrasound (including phased-array and air-coupled UT), Active Thermography, Eddy Current, Vibration and Visual Analysis and Local Acoustic Resonance Spectroscopy (LARS). The presentation will summarize some of the results of the experiments and ongoing data analysis.

  7. Validity of proxy data obtained by different psychological autopsy information reconstruction techniques.

    Science.gov (United States)

    Fang, L; Zhang, J

    2010-01-01

    Two informants were interviewed for each of 416 living controls (individuals sampled from the normal population) interviewed in a Chinese case-control psychological autopsy study. The validity of proxy data, obtained using seven psychological autopsy information reconstruction techniques (types 1, 2 and A - E), was evaluated, with living controls' self reports used as the gold-standard. Proxy data for reconstruction technique types 1, 2 and D on the Impulsivity Inventory Scale (total impulsivity score) were no different from the living controls' self report gold standard, whereas data for types A and E were smaller than data from living controls. On the 'acceptance or resignation' sub-scale of the avoidance coping dimension of the Moos Coping Response Inventory, information obtained by reconstruction technique types 1 and D was not significantly different from the living controls' self reports, whereas proxy data from types 2, A and E were smaller than those from the living controls. No statistically significant differences were identified for other proxy data obtained by reconstruction technique types 1, 2, A, D and E. These results indicate that using a second informant does not significantly enhance information reconstruction for the target.

  8. [The meaning of autonomy in Chinese culture: obtaining informed consent for operation].

    Science.gov (United States)

    Lin, Mei-Ling; Wu, Jo Yung-Wei; Huang, Mei-Chih

    2008-10-01

    The purpose of gaining the patient's informed consent is ethical, lying in respect for his or her autonomy, and such consent forms the foundation for the performance of clinical medical treatment. In order to respect the patient's autonomy, for example, during decisions about operations, doctors have the obligation to clearly explain that patient's medical condition to him/her. A thorough briefing should be given prior to the obtaining of the patients' consent. In fulfillment of their duties as medical professionals, both doctors and nurses should be involved in clinically informing patients as well as in obtaining their signature for operation and anesthesia. Although informing patients about their physical state is not the responsibility of nurses, it remains absolutely necessary for nurses to understand how people in Asian cultures understand autonomy. This paper begins with a discussion of autonomy in ethics, and then outlines the differences between the Eastern and Western concepts of autonomy, before discussing the obtaining of the signature of consent, a process performed by the nursing staff during clinical treatment, and resulting in the provision of such signatures by patients with the legal capacity to provide them.

  9. Improvement of Low-Frequency Sound Field Obtained by an Optimized Boundary

    Institute of Scientific and Technical Information of China (English)

    JING Lu; ZHU Xiao-tian

    2006-01-01

    An approach based on the finite element analysis was introduced to improve low-frequency sound field. The optimized scatters on the wall redistribute the modes of the room and provide effective diffusion of sound field. The frequency response, eigenfrequency, spatial distribution and transient response were calculated. Experimental data were obtained through a 1:5 scaled set up. The results show that the optimized treatment has a positive effect on sound field and the improvement is obvious.

  10. A rapid alternative technique for obtaining silver-positive patterns in chromosomes

    OpenAIRE

    Kavalco,Karine Frehner; Pazza,Rubens

    2004-01-01

    Silver nitrate chromosome staining to evidence nucleolar organizer regions (NORs) is a widely adopted methodology. The aim of the present work was to improve this technique, reducing the preparation time without decreasing the quality of the results. Microwave irradiation proved to be quite efficient and reliable for this purpose, as it allowed to identify Ag-NORs equivalent to those obtained by the conventional procedure and also to reduce the concentration of the employed reagents, as well ...

  11. Obtaining shale distillate free from sulphur

    Energy Technology Data Exchange (ETDEWEB)

    Heyl, G E

    1917-09-14

    A process whereby, from sulfur-containing shale, products free from sulfur may be obtained, consisting of mixing with the finely ground shale a portion of iron salts containing sufficient metal to unite with all the sulfur in the shale and form sulfide therewith, grinding the mixture to a fine state of subdivision and subsequently subjecting it to destructive distillation.

  12. Acclimatization of Phalaenopsis and Cattleya obtained by micropropagation

    OpenAIRE

    Lucía Primitiva Díaz; Jorge Julio Namur; Sebastián Agustín Bollati; Osvaldo Ernesto Antonio Arce

    2010-01-01

    Título en español: Aclimatización de Phalaenopsis y Cattleya obtenidas por micropropagación ABSTRACT The quality of micropropagated plants relies on the acclimatization stage. This research intends to develop an efficient protocol to obtain the acclimatization of Phalaenopsis and Cattleya. Plants of Phalaenopsis obtained from protocorms were selected. They came from flowering stalks grown at modified Murashige and Skoog (MS) (1962) medium and classified by growth ranks and put into mo...

  13. Recent results from TASSO

    International Nuclear Information System (INIS)

    Foster, B.

    1982-03-01

    Results are presented on the inclusive production of π 0 , K 0 and antiK 0 and lambda and antilambda in e + e - annihilation. These results, together with those on inclusive charged hadron production are used to obtain information on fragmentation mechanisms and the production of heavy quark flavours in e + e - annihilation. (author)

  14. Patterned growth of carbon nanotubes obtained by high density plasma chemical vapor deposition

    Science.gov (United States)

    Mousinho, A. P.; Mansano, R. D.

    2015-03-01

    Patterned growth of carbon nanotubes by chemical vapor deposition represents an assembly approach to place and orient nanotubes at a stage as early as when they are synthesized. In this work, the carbon nanotubes were obtained at room temperature by High Density Plasmas Chemical Vapor Deposition (HDPCVD) system. This CVD system uses a new concept of plasma generation, where a planar coil coupled to an RF system for plasma generation was used with an electrostatic shield for plasma densification. In this mode, high density plasmas are obtained. We also report the patterned growth of carbon nanotubes on full 4-in Si wafers, using pure methane plasmas and iron as precursor material (seed). Photolithography processes were used to pattern the regions on the silicon wafers. The carbon nanotubes were characterized by micro-Raman spectroscopy, the spectra showed very single-walled carbon nanotubes axial vibration modes around 1590 cm-1 and radial breathing modes (RBM) around 120-400 cm-1, confirming that high quality of the carbon nanotubes obtained in this work. The carbon nanotubes were analyzed by atomic force microscopy and scanning electron microscopy too. The results showed that is possible obtain high-aligned carbon nanotubes with patterned growth on a silicon wafer with high reproducibility and control.

  15. Comparison of model results obtained with several European regional air quality models

    NARCIS (Netherlands)

    Hass, H.; Builtjes, P.J.H.; Simpson, D.; Stern, R.

    1997-01-01

    An intercomparison study has been performed with four photo-oxidant dispersion models (EMEP, EURAD, LOTOS and REM3) which are currently capable of performing photo-oxidant formation calculations over larger path of Europe. The models, in principle, were run in the mode in which they are normally

  16. Are safe results obtained when SAFT equations are applied to ordinary chemicals?

    DEFF Research Database (Denmark)

    Privat, Romain; Conte, Elisa; Jaubert, Jean-Noël

    2012-01-01

    to five molar volumes, thus leading to the simultaneous existence of pseudo liquid–liquid and liquid–vapour phase equilibria at a same temperature. In this work, low-temperature calculations are performed using the PC-SAFT EoS which is combined with a fugacity model for the solid phase in order to predict...

  17. Interventional MR imaging: Clinical results obtained with a 1.5 Tesla system

    International Nuclear Information System (INIS)

    Adam, G.; Guenther, R.W.

    1997-01-01

    The clinical feasibility of using interventional examination techniques was tested with an equipment combining fluoroscopy and MR imaging. This hybrid system showed to be of advantage in a great number of interventional examinations. The 1.5 Tesla magnet proved to be superior to open MR scanning systems in terms of image quality and scanning times. (orig.) [de

  18. Individual flight styles in ski jumping: results obtained during Olympic Games competitions.

    Science.gov (United States)

    Schmölzer, B; Müller, W

    2005-05-01

    From the physics point of view, the jump length in ski jumping depends on: the in-run velocity v(0), the velocity perpendicular to the ramp v(p0) due to the athlete's jumping force, the lift and drag forces acting during take-off and during the flight, and the weight of the athlete and his equipment. The aerodynamic forces are a function of the flight position and of the equipment features. They are a predominant performance factor and can largely be influenced by the athlete. The field study conducted during the Olympic Games competitions 2002 at Park City (elevation: 2000 m) showed an impressive ability of the Olympic medallists to reproduce their flight style and remarkable differences between different athletes have been found. The aerodynamic forces are proportional to the air density. Elite athletes are able to adapt their flight style to thin air conditions in order to maximise jump length and to keep the flight stable. The effects of flight position variations on the performance have been analysed by means of a computer model which is based on the equations of motion and on wind tunnel data corresponding to the flight positions found in the field. Athletes have to solve extremely difficult optimisation problems within fractions of a second. The computer simulation can be used as a reliable starting point for the improvement of training methods and gives an insight into the "implicit" knowledge of physics that the ski jumping athlete must have available for a good performance.

  19. Obtaining of uranium tetrafluoride UF4 by electrodialysis reactive from uranium concentrates

    International Nuclear Information System (INIS)

    Munoz Lay, Danny Mauricio

    2014-01-01

    The generation of uranium fuels has always been a topic worldwide. The uranium fuel manufacturing base is made under very strict parameters of radiological and industrial safety, being a stage called 'nuclear fuel cycle'. In Chile, it is done constant research for fuels. This report focuses primarily on participating in such research; mainly in the production of uranium tetrafluoride (UF 4 ) .The tetrafluoride production is very crucial for the nuclear fuel industry. Its production varies from precipitation in stirred conditions to electrolysis in mercury. However, both processes has shortcomings either in performance and environmental pollution, which is why it is proposed a new method of production based on a friendly process to the environment and easier to operate, the reactive electrodialysis (RED). Electrodialysis is a hybrid reactive process of separation by membranes, cationic and / or anionic, namely, ionic species. In the process, ions are induced to move by an electric potential applied and separated by these membranes, a highly selective physical barrier which allows passage of ions with certain charge, and prevents the passage of oppositely charged ions. And in turn, it is reactive because it forces a chemical reaction, redox, to obtain uranium tetrafluoride (UF 4 ). The results of these experiments show that by reactive electrodialysis, NH 4 UF 5 deposits were obtained. However, calcinating the NH 4 UF 5 to 450 o C, it decomposes to obtain uranium tetrafluoride, UF 4 . The best working conditions were obtained with an electric current of 0.5 (A), 41 o C and a flow of 16 (ml / s) of the electrolyte. It was possible to obtain 5,995 (g) to 3 (h), giving a current efficiency of 71.42%. In turn, working at high temperatures and flow recirculation is possible to operate with a potential difference of 1.7 (V)

  20. Production and characterization of pectinases obtained from ...

    African Journals Online (AJOL)

    Production and characterization of pectinases obtained from Aspergillus fumigatus in submerged fermentation system using pectin extracted from mango peels as carbon source. AL Ezugwu, SOO Eze, FC Chilaka, CU Anyanwu ...

  1. Analysis of multiplex gene expression maps obtained by voxelation.

    Science.gov (United States)

    An, Li; Xie, Hongbo; Chin, Mark H; Obradovic, Zoran; Smith, Desmond J; Megalooikonomou, Vasileios

    2009-04-29

    Gene expression signatures in the mammalian brain hold the key to understanding neural development and neurological disease. Researchers have previously used voxelation in combination with microarrays for acquisition of genome-wide atlases of expression patterns in the mouse brain. On the other hand, some work has been performed on studying gene functions, without taking into account the location information of a gene's expression in a mouse brain. In this paper, we present an approach for identifying the relation between gene expression maps obtained by voxelation and gene functions. To analyze the dataset, we chose typical genes as queries and aimed at discovering similar gene groups. Gene similarity was determined by using the wavelet features extracted from the left and right hemispheres averaged gene expression maps, and by the Euclidean distance between each pair of feature vectors. We also performed a multiple clustering approach on the gene expression maps, combined with hierarchical clustering. Among each group of similar genes and clusters, the gene function similarity was measured by calculating the average gene function distances in the gene ontology structure. By applying our methodology to find similar genes to certain target genes we were able to improve our understanding of gene expression patterns and gene functions. By applying the clustering analysis method, we obtained significant clusters, which have both very similar gene expression maps and very similar gene functions respectively to their corresponding gene ontologies. The cellular component ontology resulted in prominent clusters expressed in cortex and corpus callosum. The molecular function ontology gave prominent clusters in cortex, corpus callosum and hypothalamus. The biological process ontology resulted in clusters in cortex, hypothalamus and choroid plexus. Clusters from all three ontologies combined were most prominently expressed in cortex and corpus callosum. The experimental

  2. Concretes of low environmental impact obtained by geopolymerization of Metakaolin

    Science.gov (United States)

    Sandoval, D. C.; Montaño, A. M.; González, C. P.; Gutiérrez, J.

    2018-04-01

    This work shows results of partial replacement of Portland Type I cement®, by geopolymers obtained through alkaline activation of Metakaolin, in concrete mixtures. Replacement was made with 10%, 20% and 30% of geopolymers at 7, 14, 28 and 90 days of setting. Cement samples was mechanical and electrically tested. Mechanical resistance to compression assay shows that the best percentage of replacement is 10% for every setting time; highest value is 26.75MPa at 90 days. Nyquist diagrams at different times of immersion exhibit same trend: decreasing of electrical resistance as time of assay goes by.

  3. Quantification of platelets obtained by different centrifugation protocols in SHR rats

    Directory of Open Access Journals (Sweden)

    João Alberto Yazigi Junior

    2015-12-01

    Full Text Available ABSTRACT OBJECTIVE: To quantify the platelet concentration in the blood of SHR rats, by means of different centrifugation protocols, and to evaluate what the most effective method for obtaining platelets is. METHODS: We used 40 male rats of the isogenic SHR lineage. The animals were divided into three groups: control, using whole blood without centrifugation; single centrifugation, using whole blood subjected to a single centrifugation at 200 × gand 400 × g; and double centrifugation, using whole blood subjected one centrifugation at different rotations, followed by collection of whole plasma subjected to another centrifugation at different rotations: 200 × g+ 200 ×g; 200 × g+ 400 × g; 200 × g+ 800 × g; 400 ×g+ 400 × g; 400 × g+ 800 × g. Samples of 3 ml of blood were drawn from each animal by means of cardiac puncture. The blood was stored in Vacutainer collection tubes containing 3.2% sodium citrate. The blood from the control group animals was analyzed without being subjected to centrifugation. After the blood from the other groups of animals had been subjected to centrifugation, the whole plasma was collected and subjected to platelet counting in the lower third of the sample. RESULTS: We obtained greatest platelet enrichment in the subgroup with two centrifugations comprising 400 × gfor 10 min + 400 ×gfor 10 min, in which the mean platelet concentration was 11.30 times higher than that of the control group. CONCLUSION: It was possible to obtain a high platelet concentration using viable simple techniques, by means of centrifugation of whole blood and use of commonly used materials. The most effective method for obtaining platelet concentrate was found in samples subjected to two centrifugations.

  4. Application of Oversampling to obtain the MTF of Digital Radiology Equipment.

    Science.gov (United States)

    Narváez, M.; Graffigna, J. P.; Gómez, M. E.; Romo, R.

    2016-04-01

    Within the objectives of theproject Medical Image Processing for QualityAssessment ofX Ray Imaging, the present research work is aimed at developinga phantomX ray image and itsassociated processing algorithms in order to evaluatethe image quality rendered by digital X ray equipment. These tools are used to measure various image parameters, among which spatial resolution shows afundamental property that can be characterized by the Modulation Transfer Function (MTF)of an imaging system [1]. After performing a thorough literature surveyon imaging quality control in digital X film in Argentine and international publications, it was decided to adopt for this work the Norm IEC 62220 1:2003 that recommends using an image edge as a testingmethod. In order to obtain the characterizing MTF, a protocol was designedfor unifying the conditions under which the images are acquired for later evaluation. The protocol implied acquiring a radiography image by means of a specific referential technique, i.e. referred either to voltage, current, time, distance focus plate (/film?) distance, or other referential parameter, and to interpret the image through a system of computed radiology or direct digital radiology. The contribution of the work stems from the fact that, even though the traditional way of evaluating an X film image quality has relied mostly on subjective methods, this work presents an objective evaluative toolfor the images obtained with a givenequipment, followed by a contrastive analysis with the renderings from other X filmimaging sets.Once the images were obtained, specific calculations were carried out. Though there exist some methods based on the subjective evaluation of the quality of image, this work offers an objective evaluation of the equipment under study. Finally, we present the results obtained on different equipment.

  5. Application of Oversampling to obtain the MTF of Digital Radiology Equipment

    International Nuclear Information System (INIS)

    Narváez, M.; Graffigna, J. P.; Gómez, M. E.; Romo, R.

    2016-01-01

    Within the objectives of theproject Medical Image Processing for QualityAssessment ofX Ray Imaging, the present research work is aimed at developinga phantomX ray image and itsassociated processing algorithms in order to evaluatethe image quality rendered by digital X ray equipment. These tools are used to measure various image parameters, among which spatial resolution shows afundamental property that can be characterized by the Modulation Transfer Function (MTF)of an imaging system [1]. After performing a thorough literature surveyon imaging quality control in digital X film in Argentine and international publications, it was decided to adopt for this work the Norm IEC 62220 1:2003 that recommends using an image edge as a testingmethod. In order to obtain the characterizing MTF, a protocol was designedfor unifying the conditions under which the images are acquired for later evaluation. The protocol implied acquiring a radiography image by means of a specific referential technique, i.e. referred either to voltage, current, time, distance focus plate (/film?) distance, or other referential parameter, and to interpret the image through a system of computed radiology or direct digital radiology. The contribution of the work stems from the fact that, even though the traditional way of evaluating an X film image quality has relied mostly on subjective methods, this work presents an objective evaluative toolfor the images obtained with a givenequipment, followed by a contrastive analysis with the renderings from other X filmimaging sets.Once the images were obtained, specific calculations were carried out. Though there exist some methods based on the subjective evaluation of the quality of image, this work offers an objective evaluation of the equipment under study. Finally, we present the results obtained on different equipment. (paper)

  6. Crystal structure of TiNi nanoparticles obtained by Ar ion beam deposition

    International Nuclear Information System (INIS)

    Castro, A. Torres; Cuellar, E. Lopez; Mendez, U. Ortiz; Yacaman, M. Jose

    2008-01-01

    Nanoparticles are a state of matter that have properties different from either molecules or bulk solids, turning them into a very interesting class of materials to study. In the present work, the crystal structure of TiNi nanoparticles obtained by ion beam deposition is characterized. TiNi nanoparticles were obtained from TiNi wire samples by sputtering with Ar ions using a Gatan precision ion polishing system. The TiNi nanoparticles were deposited on a Lacey carbon film that was used for characterization by transmission electron microscopy. The nanoparticles were characterized by high-resolution transmission electron microscopy, high-angle annular dark-field imaging, electron diffraction, scanning transmission electron microscopy and energy-dispersive X-ray spectroscopy. Results of nanodiffraction seem to indicate that the nanoparticles keep the same B2 crystal structure as the bulk material but with a decreased lattice parameter

  7. Nanofiber production of poly (vinylidene fluoride) / hexaferrite, obtained by Blow Spinning Technique

    International Nuclear Information System (INIS)

    Dias, G.C.; Zadorosny, L.; Malmonge, J.A.; Malmonge, L.F.

    2014-01-01

    In this study, fibrous films of poly (vinylidene fluoride) - PVDF with barium hexaferrite particles were obtained by Solution Blow Spinning technique. In such technique, the polymer solution is injected through an inner nozzle which experiences the action of an accelerated flux of gas that drags and stretches the jet solution forming the nanofibers. The films were obtained from solutions of PVDF/DMF (30% w/v), which was incorporated into barium hexaferrite particles in proportions of 1, 3 and 5% (w / w). The results of the micrographs revealed the formation of a fibrous film with good dispersion of the particles. Xray analyzes showed the predominance of the β crystalline phase of PVDF. The increase of the amount of particles induces the appearance of a characteristic peak of PVDF. EDX measurements confirmed the presence of particles in the films. (author)

  8. Doped ZnS:Mn nanoparticles obtained by sonochemical synthesis.

    Science.gov (United States)

    Korotchenkov, O A; Cantarero, A; Shpak, A P; Kunitskii, Yu A; Senkevich, A I; Borovoy, M O; Nadtochii, A B

    2005-10-01

    A study of sonochemically synthesized ZnS:Mn nanoparticles is presented. The particles prepared at low rf power (about 20 W) and room temperature coalesce to form morphologically amorphous large species (30-100 nm in diameter). As the power is increased in the range from 20 to 70 W, and the solution temperature is raised to 60 to 80 degrees C, finer particles are produced with the size ranging from 2 to 20 nm and improved crystallinity. The results indicate the dispersion of the Mn(2+) ions at near-surface sites in the particles. It is shown that the sonochemically fabricated particles approach the quality of the ones obtained by a standard chemical route and show a reasonable luminescence performance.

  9. Variables of synthesis in obtaining nanosilicas with sol-gel

    International Nuclear Information System (INIS)

    Elia, A; Martin-Aispuro, P; Musante, L; Martin-Martinez, J.M; Vazquez, P

    2008-01-01

    (c), as a catalyst, had a smaller particle size than those obtained with other acids (such as acetic acid, for example). These samples also revealed an almost spherical morphology with a nanometric particle size. Meanwhile, using the EDX analysis technique, the compositions of the synthesized samples were determined and the results show that the atomic percentage relationship between O and Si is about 66% to 33% (SiO 2 ), for specific study conditions. Therefore, this work offers a new proposal for the synthesis of materials with technological applications which involves easy processes and low costs for the region's small enterprises. The substitution of very expensive pyrogenic silica with silica obtained with sol-gel in its different uses is one of the aims of this research

  10. Synthesis and characterization of superparamagnetic nanoparticles obtained by precipitation in inverse microemulsion for biomedical applications

    International Nuclear Information System (INIS)

    Puca Pacheco, Mercedes; Guerrero Aquino, Marco; Tacuri Calanchi, Enrique; Lopez Campos, Raul G.

    2013-01-01

    In this work the preparation of nanoparticles of magnetite by methods of precipitation in inverse microemulsions and the conventional method 'Chemical Co-precipitation' is reported. Magnetite nanoparticles were characterized by X-ray diffraction, Moessbauer spectroscopy and vibrating sample magnetometer (VSM). The results showed that the nanoparticles obtained by the method of precipitation in inverse microemulsion showed a superparamagnetic behavior and had a particle average diameter of 9 nm, while by the conventional method 'Chemical Co-precipitation' were 17 nm. In addition, other benefits observed in the application of the method of precipitation in inverse microemulsion with regard to the conventional method is that it allowed obtaining spheroidal magnetite nanoparticles, monodisperse and with magnetic and chemical properties which might have better results in medical applications. (author)

  11. Alcoholic Beverages Obtained from Black Mulberry

    Directory of Open Access Journals (Sweden)

    Jacinto Darias-Martín

    2003-01-01

    Full Text Available Black mulberry (Morus nigra is a fruit not known only for its nutritional qualities and its flavour, but also for its traditional use in natural medicine as it has a high content of active therapeutic compounds. However, this fruit is not widely produced in Spain but some trees are still found growing in the Canary Islands, particularly on the edges of the ravine. The inhabitants of these islands (Tenerife, La Gomera, La Palma, El Hierro and Lanzarote collect the fruit and prepare homemade beverages for medicinal purposes. Numerous authors have reported that type II diabetes mellitus can be controlled by taking a mixture containing black mulberry and water. Apart from that, this fruit has been used for the treatment of mouth, tongue and throat inflammations. In this study we present some characteristics of black mulberry juice (TSS, pH, titratable acidity, citric acid, lactic acid, polyphenols, anthocyanins, the potassium etc. and alcoholic beverages (alcoholic grade, pH, total acidity, volatile acidity, tannins, phenols etc. obtained from black mulberry. Moreover, we have studied the quality of liquors obtained from black mulberry in Canary Islands.

  12. Comparison of different scenarios for the deployment of fast reactors in France. Results obtained with COSI

    International Nuclear Information System (INIS)

    Coquelet-Pascal, Christine; Meyer, Maryan; Girieud, Richard

    2011-01-01

    In the frame of the French Act for waste management, scenarios studies are carried out with the simulation software COSI to compare different options of evolution of the French reactor fleet, possibilities of plutonium recycling, and options of separation and transmutation of minor actinides. The goal of these studies is to evaluate the sustainability of Sodium cooled Fast Reactors (SFR) deployment from plutonium availability viewpoint, as well as the interest of minor actinides transmutation options in SFR and associated impacts (decay heat and toxicity) on cycle facilities and geological storage. Each option has been evaluated separately in dynamic scenarios taking into account the transition between the current nuclear reactor fleet and a generation IV fleet, with the deployment of SFR in replacement of PWR. In this paper, the results of three types of scenarios, in the continuity of the paper of GLOBAL 2009, are discussed: 1 - plutonium recycling in SFR; 2 - plutonium recycling and minor actinides transmutation in SFR; 3 - plutonium recycling and americium transmutation in SFR. MA transmutation in heterogeneous mode (named 'het.') and in homogeneous mode (named 'hom.') are distinguished. By comparison with the previous paper, new scenarios and extended results are added and a global comparison between transmutation performances is done. Scenarios have been optimized to minimize the impacts on fuel cycle: stabilization of plants capacities over 40 years, limitation of minor actinides storage in the case of heterogeneous transmutation, limitation of MA content in the case of homogeneous transmutation. The impact of MA transmutation on decay heat of fresh and spent fuel are also assessed. The selected scenarios bring also elements on the impact of a SFR deployment delayed from 2040 to 2080, with or without MA transmutation, and the impact of an increase in the total power capacity installed by maximizing the SFR share in a symbiotic fleet PWR-SFR. Whatever the

  13. LC-MS-MS identification of drug metabolites obtained by metalloporphyrin mediated oxidation

    Directory of Open Access Journals (Sweden)

    Maurin Andrea J. M.

    2003-01-01

    Full Text Available In this paper we report the application of liquid chromatography-mass spectrometry (LC-MS-MS to the identification of the products formed by oxidation of albendazole and disopyramide with metalloporphyrins in dichloroethane, using iodosylbenzene as an oxygen donor. Our results show that LC-MS-MS is a powerful tool to study the in vitro metabolism of drugs, allowing the identification of known and unknown metabolites. In addition, it was observed that the catalyst system used resulted in the formation of the same metabolites as obtained in vivo, although for disopyramide other products were also observed.

  14. New experimental limits on heavy neutrino mixing in 8B decay obtained with the BOREXINO counting test facility

    International Nuclear Information System (INIS)

    Back, H.O.; Hagner, C.; Vogelaar, R.B.

    2003-01-01

    If heavy neutrinos with mass m νH ≥2m e are emitted in the decays of 8 B in the Sun, then decays ν H →ν L +e + +e - should be observed. The results of background measurements with the BOREXINO Counting Test Facility have been used to obtain bounds on the number of these decays. As a result, new limits on the coupling |U eH | 2 of a massive neutrino in the range of 1.1 to 12 MeV have been derived (|U eH | 2 ≤10 -3 -10 -5 ). The obtained limits on the mixing parameter are stronger than those obtained in the previous experiments using nuclear reactors and accelerators

  15. Results obtained in a spectrometry using junction detectors (1962); Resultats en spectrometrie {alpha} a l'aide de ''detecteurs jonction'' (1962)

    Energy Technology Data Exchange (ETDEWEB)

    Beaumevieille, H; Fontenille, J; Lottgequeue, J P; Longequeue, N; Rabour, C [Commissariat a l' Energie Atomique, Grenoble (France). Centre d' Etudes Nucleaires

    1962-07-01

    Junction detectors have been used for studying {alpha} spectra obtained by nuclear reactions (p, {alpha}), the protons being produced by an electrostatic accelerator (E{sub p} varying from 100 to 600 keV). Difficulties have been encountered arising from parasitic noise from the accelerator and from the distance (60 metres) between detectors and electronic equipment. Resolution of the counter has been found to be 0.6 per cent with {alpha} from {sup 210}Po and 1.2 pour cent with {alpha} (5.8 MeV) from the reaction {sup 11}B (p, {alpha}{sub 0}). (authors) [French] Des detecteurs a jonction ont ete utilises pour l'etude de spectres {alpha} obtenus par reactions nucleaires (p, {alpha}), les protons etant acceleres par un accelerateur electrostatique (E{sub p} variant de 100 a 600 keV). Des difficultes ont ete recontrees dues aux parasites provenant de l'accelerateur et a la distance des cables (60 metres) entre detecteurs et appareils de mesure. Le pouvoir de resolution de l'ensemble a ete de 0, 6 pour cent avec les {alpha} du {sup 210}Po et de 1,2 pour cent avec les {alpha} (5,8 MeV) de la reaction {sup 11}B (p, {alpha}{sub 0}). (auteurs)

  16. Preliminary results from the hierarchical glitch pipeline

    International Nuclear Information System (INIS)

    Mukherjee, Soma

    2007-01-01

    This paper reports on the preliminary results obtained from the hierarchical glitch classification pipeline on LIGO data. The pipeline that has been under construction for the past year is now complete and end-to-end tested. It is ready to generate analysis results on a daily basis. The details of the pipeline, the classification algorithms employed and the results obtained with one days analysis on the gravitational wave and several auxiliary and environmental channels from all three LIGO detectors are discussed

  17. Obtaining the Electron Angular Momentum Coupling Spectroscopic Terms, jj

    Science.gov (United States)

    Orofino, Hugo; Faria, Roberto B.

    2010-01-01

    A systematic procedure is developed to obtain the electron angular momentum coupling (jj) spectroscopic terms, which is based on building microstates in which each individual electron is placed in a different m[subscript j] "orbital". This approach is similar to that used to obtain the spectroscopic terms under the Russell-Saunders (LS) coupling…

  18. Gold nanoparticle assemblies of controllable size obtained by hydroxylamine reduction at room temperature

    Energy Technology Data Exchange (ETDEWEB)

    Tódor, István Sz.; Szabó, László; Marişca, Oana T.; Chiş, Vasile; Leopold, Nicolae, E-mail: nicolae.leopold@phys.ubbcluj.ro [Babeş-Bolyai University, Faculty of Physics (Romania)

    2014-12-15

    Colloidal nanoparticle assemblies (NPAs) were obtained in a one-step procedure, by reduction of HAuCl{sub 4} by hydroxylamine hydrochloride, at room temperature, without the use of any additional nucleating agent. By changing the order of the reactants, NPAs with mean size of ∼20 and ∼120 nm were obtained. Because of their size and irregular popcorn like shape, the larger size NPAs show absorption in the NIR spectral region. The building blocks of the resulted nanoassemblies are spherical nanoparticles with diameters of 4–8 and 10–30 nm, respectively. Moreover, by stabilizing the colloid with bovine serum albumin at different time moments after synthesis, NPAs of controlled size between 20 and 120 nm, could be obtained. The NPAs were characterized using UV–Vis spectroscopy, TEM and SEM electron microscopies. In addition, the possibility of using the here proposed NPAs as surface-enhanced Raman scattering (SERS) substrate was assessed and found to provide a higher enhancement compared to conventional citrate-reduced nanoparticles.

  19. Phase fields of nickel silicides obtained by mechanical alloying in the nanocrystalline state

    Science.gov (United States)

    Datta, M. K.; Pabi, S. K.; Murty, B. S.

    2000-06-01

    Solid state reactions induced by mechanical alloying (MA) of elemental blends of Ni and Si have been studied over the entire composition range of the Ni-Si system. A monotonous increase of the lattice parameter of the Ni rich solid solution, Ni(Si), is observed with refinement of crystallite size. Nanocrystalline phase/phase mixtures of Ni(Si), Ni(Si)+Ni31Si12, Ni31Si12+Ni2Si, Ni2Si+NiSi and NiSi+Si, have been obtained during MA, over the composition ranges of 0-10, 10-28, 28-33, 33-50, and >50 at. % Si, respectively. The results clearly suggest that only congruent melting phases, Ni31Si12, Ni2Si, and NiSi form, while the formation of noncongruent melting phases, Ni3Si, Ni3Si2, and NiSi2, is bypassed in the nanocrystalline state. The phase formation during MA has been discussed based on thermodynamic arguments. The predicted phase fields obtained from effective free energy calculations are quite consistent with those obtained during MA.

  20. Chromosome segregation analysis in human embryos obtained from couples involving male carriers of reciprocal or Robertsonian translocation.

    Directory of Open Access Journals (Sweden)

    Ahmet Yilmaz

    Full Text Available The objective of this study was to investigate the frequency and type of chromosome segregation patterns in cleavage stage embryos obtained from male carriers of Robertsonian (ROB and reciprocal (REC translocations undergoing preimplantation genetic diagnosis (PGD at our reproductive center. We used FISH to analyze chromosome segregation in 308 day 3 cleavage stage embryos obtained from 26 patients. The percentage of embryos consistent with normal or balanced segregation (55.1% vs. 27.1% and clinical pregnancy (62.5% vs. 19.2% rates were higher in ROB than the REC translocation carriers. Involvement of non-acrocentric chromosome(s or terminal breakpoint(s in reciprocal translocations was associated with an increase in the percent of embryos consistent with adjacent 1 but with a decrease in 3∶1 segregation. Similar results were obtained in the analysis of nontransferred embryos donated for research. 3∶1 segregation was the most frequent segregation type in both day 3 (31% and spare (35% embryos obtained from carriers of t(11;22(q23;q11, the only non-random REC with the same breakpoint reported in a large number of unrelated families mainly identified by the birth of a child with derivative chromosome 22. These results suggest that chromosome segregation patterns in day 3 and nontransferred embryos obtained from male translocation carriers vary with the type of translocation and involvement of acrocentric chromosome(s or terminal breakpoint(s. These results should be helpful in estimating reproductive success in translocation carriers undergoing PGD.

  1. Image-derived input function obtained in a 3TMR-brainPET

    Energy Technology Data Exchange (ETDEWEB)

    Silva, N.A. da [Institute of Biophysics and Biomedical Engineering, University of Lisbon (Portugal); Institute of Neurosciences and Medicine - 4, Juelich (Germany); Herzog, H., E-mail: h.herzog@fz-juelich.de [Institute of Neurosciences and Medicine - 4, Juelich (Germany); Weirich, C.; Tellmann, L.; Rota Kops, E. [Institute of Neurosciences and Medicine - 4, Juelich (Germany); Hautzel, H. [Department of Nuclear Medicine (KME), University of Duesseldorf, Medical Faculty at Research Center Juelich, Juelich (Germany); Almeida, P. [Institute of Biophysics and Biomedical Engineering, University of Lisbon (Portugal)

    2013-02-21

    Aim: The combination of a high-resolution MR-compatible BrainPET insert operated within a 3 T MAGNETOM Trio MR scanner is an excellent tool for obtaining an image derived input function (IDIF), due to simultaneous imaging. In this work, we explore the possibility of obtaining an IDIF from volumes of interest (VOI) defined over the carotid arteries (CAs) using the MR data. Material and methods: FDG data from three patients without brain disorders were included. VOIs were drawn bilaterally over the CAs on a MPRAGE image using a 50% isocontour (MR50VOI). CA PET/MR co-registration was examined based on an individual and combined CA co-registration. After that, to estimate the IDIF, the MR50VOI average (IDIF-A), four hottest pixels per plane (IDIF-4H) and four hottest pixels in VOI (IDIF-4V) were considered. A model-based correction for residual partial volume effects involving venous blood samples was applied, from which partial volume (PV) and spillover (SP) coefficients were estimated. Additionally, a theoretical PV coefficient (PVt) was calculated based on MR50VOI. Results: The results show an excellent co-registration between the MR and PET, with an area under the curve ratio between both co-registration methods of 1.00±0.04. A good agreement between PV and PVt was found for IDIF-A, with PV of 0.39±0.06 and PVt 0.40±0.03, and for IDIF-4H, with PV of 0.47±0.05 and PVt 0.47±0.03. The SPs were 0.20±0.03 and 0.21±0.03 for IDIF-A and IDIF-4H, respectively. Conclusion: The integration of a high resolution BrainPET in an MR scanner allows to obtain an IDIF from an MR-based VOI. This must be corrected for a residual partial volume effect.

  2. Obtaining the general forms of the effective coefficients of laminate magneto-electro - elastic

    International Nuclear Information System (INIS)

    Cabañas, J. H.; Otero, A.; Castillero, B.; Rodríguez, R.

    2008-01-01

    In this work using the asymptotic homogenization method obtained general expressions for the calculation of the effective characteristics of magnetoelectro-elastic laminates with layers of any symmetry. You will reach an array of auxiliary functions for determining the effective coefficients for a serial connection and displays a result similar to the case of parallel connection.

  3. School Nurses' Perceptions and Practices of Assisting Students in Obtaining Public Health Insurance

    Science.gov (United States)

    Rickard, Megan L.; Hendershot, Candace; Khubchandani, Jagdish; Price, James H.; Thompson, Amy

    2010-01-01

    Background: From January through June 2009, 6.1 million children were uninsured in the United States. On average, students with health insurance are healthier and as a result are more likely to be academically successful. Some schools help students obtain health insurance with the help of school nurses. Methods: This study assessed public school…

  4. Formation and characterization of nanotubes of La(OH)3 obtained using porous alumina membranes

    International Nuclear Information System (INIS)

    Gonzalez-Rovira, L; Sanchez-Amaya, J M; Botana, F J; Lopez-Haro, M; Hungria, A B; Boukha, Z; Bernal, S

    2008-01-01

    An electrodeposition process is used to synthesize nanotubes of a lanthanum-containing phase, employing porous alumina membranes as templates. This method should lead to the formation of La(OH) 3 nanowires, according to the previous results presented by Bocchetta et al (2007 Electrochem. Commun. 9 683-8), which can be decomposed to La 2 O 3 , as the latter shows more interest for different applications. The results obtained by means of different electron microscopy techniques indicate that this method leads to the formation of nanotubes of about 200 nm in diameter and 30-40 μm in length, instead of the nanowires proposed in the literature. Additionally, the chemical characterization demonstrates that the material synthesized is composed of lanthanum hydroxycarbonate. The presence of carbonates is found to be crucial in determining the conditions for the preparation of La 2 O 3 from the nanotubes here obtained.

  5. Formation and characterization of nanotubes of La(OH)3 obtained using porous alumina membranes

    Science.gov (United States)

    González-Rovira, L.; Sánchez-Amaya, J. M.; López-Haro, M.; Hungria, A. B.; Boukha, Z.; Bernal, S.; Botana, F. J.

    2008-12-01

    An electrodeposition process is used to synthesize nanotubes of a lanthanum-containing phase, employing porous alumina membranes as templates. This method should lead to the formation of La(OH)3 nanowires, according to the previous results presented by Bocchetta et al (2007 Electrochem. Commun. 9 683-8), which can be decomposed to La2O3, as the latter shows more interest for different applications. The results obtained by means of different electron microscopy techniques indicate that this method leads to the formation of nanotubes of about 200 nm in diameter and 30-40 µm in length, instead of the nanowires proposed in the literature. Additionally, the chemical characterization demonstrates that the material synthesized is composed of lanthanum hydroxycarbonate. The presence of carbonates is found to be crucial in determining the conditions for the preparation of La2O3 from the nanotubes here obtained.

  6. The legal status of evidence obtained through human rights ...

    African Journals Online (AJOL)

    The Constitution of the Republic of Uganda, 1995 is silent on the issue of dealing with evidence obtained through human rights violations. This silence dates to the earlier Constitutions of 1962, 1966 and 1967. It is only the Prohibition and Prevention of Torture Act of 2012 that renders evidence obtained through torture and ...

  7. Magnetic susceptibility measurements of boring cores obtained from regional hydrological study project

    International Nuclear Information System (INIS)

    Hasegawa, Ken

    2010-02-01

    We measured the magnetic susceptibility of boring cores obtained from the Regional Hydrological Study Project to interpret the aeromagnetic survey data which was carried out in Tono area with about 40km square surrounding Tono Geoscience Center. The result of measurements indicates that the magnetic susceptibility of the Toki Granite is not distributed uniformly and the maximum value becomes two orders in magnitude larger than its minimum value. (author)

  8. Spectral inversion of frequency-domain IP data obtained in Haenam, South Korea

    Science.gov (United States)

    Kim, B.; Nam, M. J.; Son, J. S.

    2017-12-01

    Spectral induced polarization (SIP) method using a range of source frequencies have been performed for not only exploring minerals resources, but also engineering or environmental application. SIP interpretation first makes inversion of individual frequency data to obtain complex resistivity structures, which will further analyzed employing Cole-Cole model to explain the frequency-dependent characteristics. However, due to the difficulty in fitting Cole-Cole model, there is a movement to interpret complex resistivity structure inverted only from a single frequency data: that is so-called "complex resistivity survey". Further, simultaneous inversion of multi-frequency SIP data, rather than making a single frequency SIP data, has been studied to improve ambiguity and artefacts of independent single frequency inversion in obtaining a complex resistivity structure, even though the dispersion characteristics of complex resistivity with respect to source frequency. Employing the simultaneous inversion method, this study makes inversion of field SIP data obtained over epithermal mineralized area, Haenam, in the southernmost tip of South Korea. The area has a polarizable structure because of extensive hydrothermal alteration, gold-silver deposits. After the inversion, we compare between inversion results considering multi-frequency data and single frequency data set to evaluate the performance of simultaneous inversion of multi-frequency SIP data.

  9. Dielectric Properties and Characterisation of Titanium Dioxide Obtained by Different Chemistry Methods

    Directory of Open Access Journals (Sweden)

    Aleksandra Wypych

    2014-01-01

    Full Text Available We made comparison of titanium dioxide powders obtained from three syntheses including sol-gel and precipitation methods as well as using layered (tetramethylammonium titanate as a source of TiO2. The obtained precursors were subjected to step annealing at elevated temperatures to transform into rutile form. The transformation was determined by Raman measurements in each case. The resulting products were characterised using Raman spectroscopy and dynamic light scattering. The main goal of the studies performed was to compare the temperature of the transformation in three titania precursors obtained by different methods of soft chemistry routes and to evaluate dielectric properties of rutile products by means of broadband dielectric spectroscopy. Different factors affecting the electrical properties of calcinated products were discussed. It was found that sol-gel synthesis provided rutile form after annealing at 850°C with the smallest particles size about 20 nm, the highest value of dielectric permittivity equal to 63.7, and loss tangent equal to 0.051 at MHz frequencies. The other powders transformed to rutile at higher temperature, that is, 900°C, exhibit lower value of dielectric permittivity and had a higher value of particles size. The correlation between the anatase-rutile transformation temperature and the size of annealed particles was proposed.

  10. Characterization of mesoporous VOx/MCM-41 composite materials obtained via post-synthesis impregnation

    International Nuclear Information System (INIS)

    Bukallah, Saeed B.; Bumajdad, Ali; Khalil, Kamal M.S.; Zaki, Mohamed I.

    2010-01-01

    Spherical-particle MCM-41 was synthesized at room temperature, and, then, impregnated with aqueous solutions of NH 4 VO 3 to produce variously loaded VO x /MCM-41 composite materials. Bulk and surface properties of the materials thus produced were characterized by means of X-ray powder diffractometry (XRD), infrared spectroscopy (FTIR), N 2 sorptiometry and X-ray photoelectron spectroscopy (XPS). Results obtained indicated that subsequent calcination at 550 deg. C (for 2 h) of the blank and impregnated MCM-41 particles, results in materials assuming the same bulk structure of MCM-41, and exposing uniformly mesporous, high area surfaces (P w = 2.0-2.3 nm; 974-829 m 2 /g), except for the material obtained at 20 wt%-V 2 O 5 that was shown to suffer a considerable loss on surface area (down to 503 m 2 /g). XPS results implied that the immobilization of the VO x species occurs via interaction with surface OH/H 2 O groups of MCM-41, leading to the formation of vanadate (VO 3 - ) surface species, as well as minor V-O-Si and V 2 O 5 -like species. However, in all cases, the vanadium sites remained pentavalent and exposed on the surface.

  11. The main tasks and obtained results within soil protection working group of the Danube countries

    International Nuclear Information System (INIS)

    Dzatko, M.

    1997-01-01

    In the frame of the Danube Countries Working Community activities was in 1993 constituted independent Soil Protection Working Group (SPWG). Its primary task is to elaborate principles and common soil protection concept in given countries accepted on the level of governments and related authorities, and also to the solution of the solution of the problems on regional levels. Final objective is to implement such concept of soil protection policy, which is able to maintain its quality and productivity potential for next generations also. Based on four years activities coordination could be significance and the SPWG relevance expressed in following topics: (1) Soil pollution and soil degradation, particularly in most pos-communistic countries has been attaining high degree, and in many locations also the threshold of ecological be arability. As reclamation and revitalization of the degraded and polluted soils require long time and considerable financial means, it is not only moral;, even also economically more effective to protect preventively than subsequent reclamation. (2) Main objective of the correct soil protection policy should be its high quality conservation also for the next generations. To this is joined also the protection not only productional, but also non-productional functions, particularly filtrational, transformational and buffering capacibility, including its role and significance, as land and environment. From, in this way considered relationships reality is resulting that the soil protection objectives are not only laws and prohibition approvement, but also active relationships harmonization between the man requirements and soil productivity potential, in order of the sustainable land resources use for the next generations. (3) Based on mentioned realities and relationships we consider the SPWG as an active gremium for elaboration of the the uniform soil protection concepts for governments and responsible organisations that in financial consequence

  12. Nanostructured films of metal particles obtained by laser ablation

    Energy Technology Data Exchange (ETDEWEB)

    Muniz-Miranda, M., E-mail: muniz@unifi.it [Dipartimento di Chimica “U. Schiff”, Università di Firenze, Via della Lastruccia 3, 50019 Sesto Fiorentino (Italy); Gellini, C. [Dipartimento di Chimica “U. Schiff”, Università di Firenze, Via della Lastruccia 3, 50019 Sesto Fiorentino (Italy); Giorgetti, E.; Margheri, G.; Marsili, P. [Istituto Sistemi Complessi (CNR), Via Madonna del Piano 10, 50019 Sesto Fiorentino (Italy); Lascialfari, L.; Becucci, L. [Dipartimento di Chimica “U. Schiff”, Università di Firenze, Via della Lastruccia 3, 50019 Sesto Fiorentino (Italy); Trigari, S. [Istituto Sistemi Complessi (CNR), Via Madonna del Piano 10, 50019 Sesto Fiorentino (Italy); Giammanco, F. [Dipartimento di Fisica “E. Fermi”, Università di Pisa, Largo Pontecorvo 3, 56127 Pisa (Italy)

    2013-09-30

    Colloidal dispersions of silver and gold nanoparticles were obtained in pure water by ablation with nanosecond pulsed laser. Then, by filtration of the metal particles on alumina, we fabricated nanostructured films, whose surface morphology was examined by atomic force microscopy (AFM) and related to surface-enhanced Raman scattering (SERS) after adsorption of adenine. - Highlights: • Ag and Au colloidal nanoparticles were obtained by laser ablation. • Nanostructured Ag and Au films were fabricated by filtration of metal nanoparticles. • Surface morphology of metal films was investigated by atomic force microscopy. • Surface-enhanced Raman spectra (SERS) of adenine on metal films were obtained. • SERS enhancements were related to the surface roughness of the metal films.

  13. Synthesis and characterization of nanoparticles of nickel obtained by laser ablation

    International Nuclear Information System (INIS)

    Aviles, R.; Escobar A, L.; Camps, E.; Santiago, P.; Ascencio, J.A.; Von, H.

    2002-01-01

    The result of the formation of nickel nanoparticles by the laser ablation technique with a size less or equal to 1.3 nm is reported, also the formation of agglomerates of tens of nanometers is shown. Under the experimental conditions used a high particle density (around 10 5 particles/μm 2 ) is obtained. The stability of the particles in function of its atom quantity, for less or equal sizes to 2 nm is studied, finding that the most stable structure is the icosahedron. (Author)

  14. A rapid alternative technique for obtaining silver-positive patterns in chromosomes

    Directory of Open Access Journals (Sweden)

    Karine Frehner Kavalco

    2004-01-01

    Full Text Available Silver nitrate chromosome staining to evidence nucleolar organizer regions (NORs is a widely adopted methodology. The aim of the present work was to improve this technique, reducing the preparation time without decreasing the quality of the results. Microwave irradiation proved to be quite efficient and reliable for this purpose, as it allowed to identify Ag-NORs equivalent to those obtained by the conventional procedure and also to reduce the concentration of the employed reagents, as well as the precipitation of debris on the preparation.

  15. 7 CFR 29.91 - How to obtain an appeal.

    Science.gov (United States)

    2010-01-01

    ... 7 Agriculture 2 2010-01-01 2010-01-01 false How to obtain an appeal. 29.91 Section 29.91... REGULATIONS TOBACCO INSPECTION Regulations Appeal § 29.91 How to obtain an appeal. An appeal shall be made in writing and filed with the Division or the office of inspection for the type of tobacco involved. Such...

  16. Novel Antimicrobial Titanium Dioxide Nanotubes Obtained through a Combination of Atomic Layer Deposition and Electrospinning Technologies

    Science.gov (United States)

    Patiño, Cristian; Galotto, María Jose; Palma, Juan Luis; Alburquenque, Daniela

    2018-01-01

    The search for new antimicrobial substances has increased in recent years. Antimicrobial nanostructures are one of the most promising alternatives. In this work, titanium dioxide nanotubes were obtained by an atomic layer deposition (ALD) process over electrospun polyvinyl alcohol nanofibers (PVN) at different temperatures with the purpose of obtaining antimicrobial nanostructures with a high specific area. Electrospinning and ALD parameters were studied in order to obtain PVN with smallest diameter and highest deposition rate, respectively. Chamber temperature was a key factor during ALD process and an appropriate titanium dioxide deposition performance was achieved at 200 °C. Subsequently, thermal and morphological analysis by SEM and TEM microscopies revealed hollow nanotubes were obtained after calcination process at 600 °C. This temperature allowed complete polymer removal and influenced the resulting anatase crystallographic structure of titanium dioxide that positively affected their antimicrobial activities. X-ray analysis confirmed the change of titanium dioxide crystallographic structure from amorphous phase of deposited PVN to anatase crystalline structure of nanotubes. These new nanostructures with very large surface areas resulted in interesting antimicrobial properties against Gram-positive and Gram-negative bacteria. Titanium dioxide nanotubes presented the highest activity against Escherichia coli with 5 log cycles reduction at 200 μg/mL concentration. PMID:29495318

  17. Microwave sintering of cordierite ceramic precursors obtained by starch direct consolidation

    International Nuclear Information System (INIS)

    Sandoval, M.L.; Talou, M.H.; Camerucci, M.A.; Universidad Nacional de Mar Del Plata; Souto, P.M. de; Kiminami, R.H.G.A.

    2009-01-01

    Microwave sintering of cordierite disk precursors (mixture of kaolin, talc and alumina) with potato starch was studied. Green disks were obtained by thermal consolidation of stable aqueous suspensions of the ceramic powders (29.6 % vol.) with potato starch (11.5 % vol.) at 75 and 85 deg C, 4h; drying (50 deg C,12h) and calcination (650 deg C, 2h). The reaction-sintering by microwave heating (power: 2.45 GHz; heating rate: 50 deg C/min) at different temperatures (1250-1330 deg C) and dwell times (10-20 min) was carried out. For comparative purposes, the reaction-sintering by conventional heating was analyzed (1330 deg C, 4h a 3 deg C/min). The evolution of the phases as a function of temperature and time was studied by XRD analysis. The developed microstructures (dense or porous) were characterized by density and porosity measurements, and SEM. The obtained results were analyzed in relation to the characteristics of starch behavior in aqueous suspension at temperature and the employed consolidation and sintering conditions. (author)

  18. Alternatives for clarifying glucose syrup obtained by enzymatic hydrolysis of starch

    Directory of Open Access Journals (Sweden)

    Gloria Teresa Cruz Guerrero

    2004-05-01

    Full Text Available The present paper studies some routes for separating and purifying glucose syrup obtained by enzymatic hydrolysis of potato starch. The clarifying process is done in three stages. The first one (solids remotion is done by applying conventional solid-liquid separation techniiques such as sedimentation, centrifugation and filtration, as well as studying the effect of using flocculant and coagulant agents, prior to the already mentioned operations. Purification is done by adding decolouring agents, followed by ultrafiltration of the syrup. The last step (concentration is done by vacuum evaporation. The results showed that separation, centrifuging and sedimation reached 50% yield whilst filtration and ultrafiltration achieved 78% and 98% respectively. It was found that adsorbent agents such as activated carbon and diatomaceous earth were effective in removing colour during the purification stage. The most suitable alternative for separation can be suggested from the foregoing, allowing a syrup to be obtained having similar characteristics and propierties to the commercial product. The most appropriate technological module for carrying out the operation is also represented.

  19. Results and discussion

    International Nuclear Information System (INIS)

    1998-01-01

    The author deals with the experimental study of sorption, desorption and vertical migration of radionuclides in Sr-85 and Cs-137 in selected soil samples from around of NPP Bohunice and NPP Mochovce and other localities of the Slovakia. The influence of different materials [concurrent ions (K + , Ca 2+ , NH 4 + , pH), organic matter (peat) and zeolite, humidity] on kinetic of sorption and desorption of strontium and cesium as well as distribution coefficient (K D ) and transfer coefficients in followed samples of soils were followed. Obtained adsorption isotherm are presented and discussed. Using the Tessiere's sequential extraction analysis a gross variability in binding of radionuclides on soils was found. The obtained results were processed with the correlation analysis and the compartment model

  20. An overview of JET results

    International Nuclear Information System (INIS)

    Adams, J.M.; Alladio, F.; Altmann, H.

    1989-01-01

    An overview is given of experimental results obtained on JET during 1988, and in particular of results at high total power input into plasmas with various configurations. An account is given of the various interpretations of these results and some of the difficulties encountered are related. The progress is summarised in terms of the projected D-T performance. (author)

  1. OBTAINING AND PROPERTIES OF AgInS2 FILMS

    Directory of Open Access Journals (Sweden)

    M. A. Abdullaev

    2016-01-01

    Full Text Available Aim. The aim is to obtain AgInS2 films and study their electrical and optical properties.Methods. The samples of thin AgInS2 films for measurement were obtained by the method of magnetron sputtering with direct current. The structure, phase and elemental composition were studied using DRON-2 X-ray diffractometer (СuKа - radiation and the microscope LEO-1450 with EDS attachment for X-ray microanalysis. The optical transmittance and absorption were examined using MDR-2 monochromator in the wavelength range of 400-800 nm with the Keitley electrometer and FD-10G; we applied the spectral resolution of ± 1 meV. The electrical conductivity, Hall effect was measured by the four-point probe method with indium ohmic contacts. Measurements were carried out in the temperature range of 77-400 K.Findings. We obtained indium disulfide and silver films with the thickness of up to 1 μm on quartz substrates by magnetron sputtering. It is shown that increasing the substrate temperature to about 450 0С allows to obtain single phase film with a chalcopyrite structure with a band gap of 1.88 eV and high absorption coefficient (>104см-1.Conclusions. The possibility of obtaining films in a wide range of the electrical resistance and variation of the electrical parameters at constant stoichiometry is of interest for efficient technologies of phototransduction.

  2. Characterization of Niobium Platings Obtained from NaCl-KCl Melts

    DEFF Research Database (Denmark)

    Gillesberg, Bo; Barner, Jens H. Von; Bjerrum, Niels

    1998-01-01

    -uniform in thickness. At temperatures below 550°C no niobium metal could be identified in the product.When metallic nickel was used as substrate intermetallic compounds (e.g. NbNi3) were formed in the interface between the substrate and the deposit. This resulted in poor adherence of the deposit. In the case of AISI......316 stainless steel substrates no intermetallic phases were observed. Further an excellent adhesion of the deposited niobium layer was obtained.Deposits (on nickel substrates) from NaCl-KCl melts at 750°C with oxide added (molar ratio O/Nb greater than 0.5) were thin and consisted of niobium...

  3. Obtaining a minimal set of rewrite rules

    CSIR Research Space (South Africa)

    Davel, M

    2005-11-01

    Full Text Available In this paper the authors describe a new approach to rewrite rule extraction and analysis, using Minimal Representation Graphs. This approach provides a mechanism for obtaining the smallest possible rule set – within a context-dependent rewrite rule...

  4. Optimizing the Operation of Maceration to Obtain Quality White Wines

    Directory of Open Access Journals (Sweden)

    Stegărus Diana

    2014-06-01

    Full Text Available This study monitors the physico-chemical properties of wines from Dragasani under the influence of pectolytic enzymes in various temperature conditions. during maceration contact is made between the grape skins and selected the optimal time leads to wines with more pronounced floral character. The physico-chemical extraction maceration leads to a more pronounced specific compounds, the time of maceration is very important in this case. The curing time is of great importance in producing varieties Muscat Ottonel and Tămâioasă Românească primarily for successful extraction of aromatic components from grape. As noted in the literature flavored grapes contain large amounts of terpene compounds are in free form or bound. To optimize the technological process is able to extract these compounds and to achieve a harmonious and balanced wine. The variants considered in the study presents the results of physico-chemical and aromatic wines obtained from the Muscat Ottonel and Tămâioasă Românească, which took into consideration both during maceration and the use of selected yeasts and enzymes, which form the basis for the selection of the optimal procedure for obtaining aromatic white wines in Dragasani Vineyard.

  5. Suppression of Noise to Obtain a High-Performance Low-Cost Optical Encoder

    Directory of Open Access Journals (Sweden)

    Sergio Alvarez-Rodríguez

    2018-01-01

    Full Text Available Currently, commercial encoders endowed with high precision are expensive sensors, and optical low-cost designs to measure the positioning angle have undesirable levels of system noise which reduce the good performance of devices. This research is devoted to the designing of mathematical filters to suppress noise in polarized transducers, in order to obtain high accuracy, precision, and resolution, along with an adaptive maximum response speed for low-cost optical encoders. This design was proved through a prototype inside a research platform, and experimental results show an accuracy of 3.9, a precision of 26, and a resolution of 17 [arc seconds], at least for the specified working conditions, for the sensing of the angular position of a rotary polarizer. From this work has been obtained a high-performance low-cost polyphase optical encoder, which uses filtering mathematical principles potentially generalizable to other inventions.

  6. Obtaining Competitiveness Through Reverse Logistics: A Case Study in a Wood Industry

    Directory of Open Access Journals (Sweden)

    Patricia Guarnieri

    2006-10-01

    Full Text Available The reverse logistics make possible the return of residues to productive and/or business cycle. The present study has as objective to analyse the practices of a wood industry regarding to the residues and the ecological, lawful, and economic returns, obtained with the application of the reverse logistics concepts in the business environment. The technical procedure adopted was the case study. The data collection was made through the direct observation and interviews with the people in charge of the production and logistics sectors. The main results found were: the residues generated returns to the productive cycle obeying the environmental legislation, transforming itself in raw material again. The lawful revaluing of wood residues obtain competitiveness to company, because solve the residues destination problem providing the return for productive and business cycle, thus aggregating economic, lawful and ecological value to the wood residues.

  7. Biomaterials recycling: bioglasses obtained from reuse of hydroxyapatite (HA) bovine bone with term exceeded validity

    International Nuclear Information System (INIS)

    Silva, A.C.; Santos, S.C.; Braga, F.J.C.; Aparecida, A.H.

    2012-01-01

    The hydroxyapatite (HA) is a reference bioceramic for bone replacement and regeneration medical practice, becoming one of the most produced and researched bone graft material. Since it is a material for biomedical application, the manufacture and storage of this bioceramic must comply with severe conservation criteria, and its validity date is the lawful major factor for disposal. Materials with the exceeded expiration date are usually discarded and incinerated, resulting in ash, environmental contamination and energy expenditure. This study evaluates the possibility of reuse of bovine HA collected after its validity date as raw material to obtain bioglass, aiming to natural resources saving and environmental emissions mitigation. 45S5 similar compositions were obtained by melting the materials at 1500 ° C, followed by rapid cooling and annealing thermal treatment (500 ° C for 2h), analytical grade chemical reagents were used to set the final composition. The obtained materials were characterized by X-ray diffraction, infrared spectroscopy (FT-IR), and hydrolysis resistance techniques. The results of comparative chemical resistance (Hydrolytic) tests indicate the potential use of the materials developed for bone replacement applications. (author)

  8. Results and interpretation of groundwater data obtained from multiport-instrumented coreholes (GW-131 through GS-135), fiscal years 1990 and 1991

    International Nuclear Information System (INIS)

    Dreier, R.B.; Early, T.O.; King, H.L.

    1993-01-01

    With the increased emphasis by Department of Energy personnel on assessing the environmental impact of past waste disposal practices at all of its facilities, there has been an associated increase in characterization activities that focus on delineating site-specific groundwater flow regimes and contaminant migration pathways. At the Oak Ridge Y-12 Plant, the complex geologic and hydrologic relationships require a more detailed understanding of the three-dimensional properties of groundwater flow regimes than can be obtained by conventional monitoring activities. Thus, as part of groundwater characterization activities conducted by the Environmental Surveillance Section staff of the Y-12 Plant Environmental Management Department, five existing deep core holes were instrumented with multiport monitoring systems to provide greatly enhanced resolution of the hydraulic and hydrochemical properties of the groundwater system within Bear Creek Valley. With a multiport system, it is possible to measure hydraulic head and hydraulic conductivity and collect water samples from multiple levels within a single borehole. In this report, multiport data collected during fiscal years (FYs) 1990 and 1991 are summarized

  9. Synthesis and characterization of hematite pigment obtained from a steel waste industry

    Energy Technology Data Exchange (ETDEWEB)

    Prim, S.R. [Department of Mechanical Engineering, University of the State of Santa Catarina, Santa Catarina (Brazil); Folgueras, M.V., E-mail: dem2mvf@joinville.udesc.br [Department of Mechanical Engineering, University of the State of Santa Catarina, Santa Catarina (Brazil); Lima, M.A. de [Department of Mechanical Engineering, University of the State of Santa Catarina, Santa Catarina (Brazil); Hotza, D. [Departamento de Engenharia Quimica, Federal University of Santa Catarina, Santa Catarina (Brazil)

    2011-09-15

    Highlights: {yields} The study of using of a industrial waste for the synthesis of hematite pigments. {yields} The nanometer dimension this waste and your behavior as chromophore. {yields} The effect of process variables on the mechanisms of encapsulation sintered pigments. - Abstract: Pigments that meet environmental and technology requirements are the focus of the research in the ceramic sector. This study focuses on the synthesis of ceramic pigment by encapsulation of hematite in crystalline and amorphous silica matrix. Iron oxide from a metal sheet rolling process was used as chromophore. A different content of hematite and silica was homogenized by conventional and high energy milling. The powders obtained after calcinations between 1050 and 1200 {sup o}C for 2 h were characterized by X-ray diffraction and SEM analysis. The pigments were applied to ceramic enamel and porcelain body. The effect of pigment was measured by comparing L*a*b* values of the heated samples. Results showed that the color developed is influenced by variables such as oxide content employed, conditions of milling and processing temperature. The results showed that the use of pigment developed does not interfere in microstructural characteristics of pigmented material. The best hue was obtained from samples with 15 wt% of chromophore, heated at 1200 {sup o}C in amorphous silica matrix.

  10. Comparison between freeze and spray drying to obtain powder Rubrivivax gelatinosus biomass

    Directory of Open Access Journals (Sweden)

    Edson Francisco do Espírito Santo

    2013-03-01

    Full Text Available The use of colorants in products of animal origin is justified by the improvement in the color of foods since this attribute is considered a quality criterion. These additives can be produced using industrial effluents as substrates and appropriate organisms, such as Rubrivivax gelatinosus. Oxycarotenoids represent a class of carotenes responsible for the pigmentation of animals and vegetables. R. gelatinosus grows in fish industry effluent with the resulting production of a bacterial biomass containing oxycarotenoids. The purpose of this study was to compare the use of two drying processes - spray and freeze drying - to obtain powder biomass in terms of the process parameters (yield, productivity, and product recovery and the product characteristics (color, proximate composition, and oxycarotenoids. No difference was detected in the yield between these techniques, while productivity was higher using spray drying. Higher product recovery and moisture were achieved with freeze drying, while ash was higher with spray drying. The freeze dried biomass was redder, darker and less saturated than the spray dried biomass. No difference in oxycarotenoids was detected between the biomasses. Although it results in lower recovery rate, spray drying was faster and more productive, and it provided the same yield as freeze drying, which makes it the method of choice for obtaining R. gelatinosus biomass.

  11. Obtaining of potato microtubers cv. ‘Andinita’ in Temporary Immersion Systems

    Directory of Open Access Journals (Sweden)

    Janet Igarza Castro

    2011-01-01

    Full Text Available The Instituto Nacional de Investigaciones Agrícolas (INIA, Venezuela, is producing potato seed by biotechnology in its National Seed Plan. The seeds needed are greater than the installed capacity. The acquisition of temporary immersion system (ITS enables developing research in the production of seed potatoes to ensure quality, efficiency and reduced production costs. The purchase of seeds will decrease and contribute to food security and sovereignty of the country. This work was aimed to obtain potato microtubers cv. ‘Andinita’ in SIT. In vitro plants propagated by organogenesis and SIT in 10 liters capacity were used. Explants (100 were inoculated per pot. After five weeks in multiplication a change of culture medium was carried out to induce tuberization. Three immersion frequencies were tested. Plant height was measured and the number of microtubers and fresh dough was quantified. Potato microtubers cv. ‘Andinita’ in SIT were obtained. The best results were achieved with immersions every four hours, averaging five to seven microtubers per plant (approximately 600 microtubers per culture vessel, with sizes between 4 and 16 mm, with an average of 3 g fresh weight, which ensured budding efficiency and allow direct field planting. This result constitutes the first report of the use of SIT for propagation of potatoes in Venezuela. This is a new possibility to use SIT in other varieties. Key words: shoot tip, immersion frequency, seed

  12. Oceanic Geoid and Tides Obtained from GEOS-3 Satellite Data in the Northwestern Atlantic Ocean

    Science.gov (United States)

    Won, I. J.; Miller, L. S.

    1978-01-01

    Two sets of GEO-3 altimeter data which fall within about a 2.5 degree width are analyzed for ocean geoid and tides. One set covers a linear path from Newfoundland to Cuba and the other from Puerto Rico to the North Carolina coast. Forty different analyses using various parameters are performed in order to investigate convergence. Profiles of the geoid and four tides, M sub 2 O sub 1, S sub 2, and K sub 1, are obtained along the two strips. The results demonstrate convergent solutions for all forty cases and show, within expectation, fair agreement with those obtained from the MODE deep-sea tide gauge. It is also shown that the oceanic geoid obtained through this analysis can potentially improve the short wavelength structure over existing geoid models.

  13. The treatment of irradiated uranium fuel. Results obtained while operating the pilot plant at Fontenay-aux-Roses; Le traitement de l'uranium irradie. Resultats d'exploitation de l'usine-pilote de Fontenay-aux-Roses

    Energy Technology Data Exchange (ETDEWEB)

    Regnaut, P; Faugeras, P; Brut, A; Helou, R; Redon, A [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1958-07-01

    In this paper the results obtained from four years operation of the pilot plant when using bars of increasing activity, are summarised and compared with the results of parallel studies carried out in the laboratory. As a conclusion to the article, the optimum conditions for the different phases of a process based on solvent extraction are given. (author)Fren. [French] Cette conference resume les resultats obtenus durant quatre annees de fonctionnement de l'Usine-Pilote, avec des barreaux d'activite croissante et les compare aux resultats d'etudes conduites parallelement en laboratoire. En conclusion sont donnees les conditions optima pour les differentes phases d'un procede base sur l'extraction par solvant. (auteur)

  14. New particles: experimental results

    International Nuclear Information System (INIS)

    Augustin, J.E.

    The results of studies on production and properties of psi(3100) and psi(3700) resonances are presented, particular attention being given to spin, parity, g-parity and isospin determination. Evidence obtained in the SPEAR and DORIS storage rings in psi'→γ chi and psi→γX intermediate states are presented, together with SPEAR results on e-μ events and high energy jet production. (39 references) [fr

  15. Statistical data and results obtained on irradiated transistors 2N.2221 Sesco and 2N.2907 SGS; Donnees de fiabilite et resultats statistiques obtenus sur des transistors 2n.2221 Sesco et 2n.2907 SGS irradies

    Energy Technology Data Exchange (ETDEWEB)

    Blin, A; Le Ber, J

    1966-07-01

    This document provides results obtained on many samples of transistors irradiated in the laboratories of the Institut of Nuclear Physic of Lyon. The physical aspects of the irradiation,the statistical aspects of the study and the reliability under irradiation have been studied, but the accent is done on the statistical analysis. (A.L.B.)

  16. Microstructural characteristics of low-temperature (1400°C sintered MgO obtained from seawater

    Directory of Open Access Journals (Sweden)

    Jakić Jelena

    2017-01-01

    Full Text Available The purpose of this study was to investigate the influence of a rinsing of Mg(OH2 precipitated from seawater by substoichiometric precipitation (80% precipitation and the addition of TiO2 on microstructural characteristics of the MgO obtained by sintering at low temperature (1400°C. The results of examination indicate that the method of rinsing of the magnesium hydroxide precipitate in the technological process of obtaining MgO from seawater significantly affects the chemical composition of samples, primarily with regard to the CaO and B2O3 content. The samples were doped with TiO2 to improve the evaporation of B2O3 and sintering of MgO samples that were characterized by XRD and SEM/EDS. These techniques confirmed the high purity of MgO samples obtained and the formation of secondary compounds in very small quantities that have a positive effect on the densification.

  17. Biodegradable, pH-sensitive chitosan beads obtained under microwave radiation for advanced cell culture.

    Science.gov (United States)

    Piątkowski, Marek; Janus, Łukasz; Radwan-Pragłowska, Julia; Bogdał, Dariusz; Matysek, Dalibor

    2018-04-01

    A new type of promising chitosan beads with advanced properties were obtained under microwave radiation according to Green Chemistry principles. Biomaterials were prepared using chitosan as raw material and glutamic acid/1,5-pentanodiol mixture as crosslinking agents. Additionally beads were modified with Tilia platyphyllos extract to enhance their antioxidant properties. Beads were investigated over their chemical structure by FT-IR analysis. Also their morphology has been investigated by SEM method. Additionally swelling capacity of the obtained hydrogels was determined. Lack of cytotoxicity has been confirmed by MTT assay. Proliferation studies were carried out on L929 mouse fibroblasts. Advanced properties of the obtained beads were investigated by studying pH sensitivity and antioxidant properties by DPPH method. Also susceptibility to degradation and biodegradation by Sturm Test method was evaluated. Results shows that proposed chitosan beads and their eco-friendly synthesis method can be applied in cell therapy and tissue engineering. Copyright © 2018 Elsevier B.V. All rights reserved.

  18. Superconductive ceramics obtained with sol gel method

    International Nuclear Information System (INIS)

    Arcangeli, A.; Mosci, A.; Nardi, A.; Vatteroni, R.; Zondini, C.

    1988-01-01

    Several sol gel routes have been considered, studied and developed to produce large quantities of granulates which can be processed to obtain ceramics having good superconducting characteristics. In the considered process a mixture of commercial nitrates is atomized, at room temperature, in a solution 1:1 of Primene JMT and Benzene and a pale blue gel of the starting elements is suddently formed. The granulates obtained are free flowing, very reactive and well suited for pressing. For their intrinsic characteristics they could be very good precursors for the production of large quantities of superconductive ceramics in different forms. The precipitated gel is dried, calcinated, pressed in the form of cylindrical pellets which are sintered up to 960 degrees C. No griding or different thermal treatments are needed. The sintered material has low electric resistence, shows a clear Meissner effect and has a transition temperature of between 91 and 95 K

  19. Obtaining and Characterization of Flux-Based Products

    Directory of Open Access Journals (Sweden)

    Cosmina Maria Bogăţean

    2015-11-01

    Full Text Available The purpose of creating this assortment was to remind the public of a long forgotten sugar based product, with a high energy value and which can be easily associated both with plain or mineral water consumption. Also we have taken into consideration the well-known '' home-made'' and ''vintage'' concepts. The purpose of this scientific research is to obtain a laboratory created product, as well as obtaining both the cocoa and the lemon sorbet. In the technological process this type of products can be redefined under a new form. The great advantage comes with the fact that it dosen't currently exit on the market and so it can be considered as being a brand new product. The anbalyses both on the raw materials and on the final deliverable product were done in the Faculty's laboratories and it was proven to meet the standars.

  20. Characteristics of Biochar Obtained by Hydrothermal Carbonization of Cellulose for Renewable Energy

    OpenAIRE

    Daegi Kim; Kunio Yoshikawa; Ki Young Park

    2015-01-01

    The effect of hydrothermal carbonization on the properties of cellulose present in lignocellulosic biomass was investigated for converting it into a renewable energy resource with high energy recovery efficiency. The biochar obtained from cellulose subjected to hydrothermal carbonization showed a significant increase in its carbon content and a calorific value. 13C NMR spectroscopy showed that when raw cellulose was subjected to hydrothermal carbonization above 220 °C, the resulting biochar h...

  1. Technical evaluation of the direct denitration process to obtain ceramic-grade UO2 powders using microwaves

    International Nuclear Information System (INIS)

    Lorenzo, Viviana J.; Marchi, Daniel E.; Menghini, Jorge E.

    1999-01-01

    The direct denitration process to obtain ceramic-grade UO 2 powders using microwaves has been studied and developed at laboratory scale. Conditions were given to obtain powders apt for fuel pellets fabrication within the required specifications, where mechanical treatments before pressing are not necessary. This work describes the equipment used in the process, evaluates the necessary supply and waste generation and describes the characteristics of the product obtained, as well as the conditions for its fabrication. Results show that this method allows to reduce the volume of liquid wastes generated due to their partial re-utilization, simplifying their final disposal treatment, which, in addition to their operational advantages, make this method attractive from the economical point of view. (author)

  2. 48 CFR 9.105-1 - Obtaining information.

    Science.gov (United States)

    2010-10-01

    ... information required concerning the adequacy of prospective contractors' accounting systems and these systems... 48 Federal Acquisition Regulations System 1 2010-10-01 2010-10-01 false Obtaining information. 9... accounting systems, and these systems' suitability for use in administering the proposed type of contract. (3...

  3. Fracture behaviour of Cu-Al-Ni shape memory alloys obtained by powder metallurgy

    International Nuclear Information System (INIS)

    Rodriguez, P. P.; Perez-Saez, R. B.; Recarte, V.; San Juan, J.M.; Ruano, O. A.; No, M. L.

    2001-01-01

    Polycrystalline Cu-Al-Ni shape memory alloys have been scarcely employed for technological applications due to their high brittleness. The development of a new elaboration technique based on powder metallurgy has recently overcome this problem, through the improvement of the ductility of the produced alloys without affecting its shape memory properties. The fracture behaviour of an alloy obtained using the elaboration technique has been studied by means of Scanning Electron Microscopy and mechanical testing. The results show a ductile fracture with a maximum strain close to 13%, which is the best fracture behaviour obtained for Cu-Al-Ni polycrystals. The microstructure of such alloys ha been studied by means of Transmission Electron Microscopy, showing a poligonyzed structure in which martensite plated passing through the subboundaries easily. (Author) 19 refs

  4. Using Photogrammetric UAV Measurements as Support for Classical Topographical Measurements in Order to Obtain the Topographic Plan for Urban Areas

    Directory of Open Access Journals (Sweden)

    Elemer Emanuel SUBA

    2017-11-01

    Full Text Available This article aims to highlight the benefits of UAV photogrammetric measurements in addition to classical ones. It will also deal with the processing and integration of the point cloud, respectively the digital elevation model in topo-cadastral works. The main purpose of this paper is to compare the results obtained using the UAV photogrammetric measurements with the results obtained by classical methods. It will briefly present the classical measurements made with the total station. In the present project, the closed-circuit traverse and the supported on the endings traverse were made using known coordinate points. Determining the coordinates of the points used for the traverses was done by GNSS methods. The area on which the measurements were made is 67942m2 and is covered by 31 determined station points. From these points, 13 were used as ground control points, respectively components of the aero-triangulation network and 17 points were used to control the obtained results by comparing their coordinates obtained by classical methods with those obtained by the UAV photogrammetric method. It was intended that the constraint points of the aero triangulation to be uniformly distributed on the studied surface.

  5. Directive Emission Obtained by Mu and Epsilon-Near-Zero Metamaterials

    Directory of Open Access Journals (Sweden)

    J. Yang

    2009-06-01

    Full Text Available In this work, we use Mu and Epsilon-Near-Zero (MENZ metamaterials to realize the substrates that can modify the emission of an embedded line source. Simulation results show that the cylindrical waves emitted from the line source can be perfectly converted to plane wave through the MENZ metamaterial slab with planar exit face. Hence the line source together with the metamaterial slab constructs a high directive slab antenna. The directive radiation pattern of the MENZ metamaterial-assisted slab antenna is independent on the thickness of the slab, the position of the line source, and the shape of the entrance face of the slab, but the slab with grooved entrance side will result in stronger far-field intensity. We also show that the MENZ metamaterials can be applied to the design of antenna array. Moreover, compared with the high directive slab antenna obtained by coordinate transformation approach, the MENZ metamaterial-assisted antenna is more preferable.

  6. First AFP results

    CERN Document Server

    Staszewski, Rafal; The ATLAS collaboration

    2017-01-01

    ATLAS Forward Proton (AFP) are detectors dedicated to measurements of protons scattered diffractively or electromagnetically at small angles in inelastic processes. The first arm of AFP was installed in 2016. The installation of the full system was finished in 2017. Since 2016 AFP has collected data is special and standard runs. The presentation shows the first results obtained with data collected by AFP.

  7. 48 CFR 509.105-1 - Obtaining information.

    Science.gov (United States)

    2010-10-01

    ... Obtaining information. (a) From a prospective contractor. FAR 9.105-1 lists a number of sources of..., Contractor's Qualifications and Financial Information, but only after exhausting other available sources of... finance, and auditors before determining that an offeror is responsible. [74 FR 12732, Mar. 25, 2009] ...

  8. Isolation and characterization of microcrystalline cellulose obtained ...

    African Journals Online (AJOL)

    In this study, microcrystalline cellulose, coded MCC-PNF, was obtained from palm nut (Elaeis guineensis) fibres. MCC-PNF was examined for its physicochemical and powder properties. The powder properties of MCC-PNF were compared to those of the best commercial microcrystalline cellulose grade, Avicel PH 101.

  9. Polymeric polyelectrolytes obtained from renewable sources for biodiesel wastewater treatment by dual-flocculation

    Directory of Open Access Journals (Sweden)

    E. A. M. Ribeiro

    2017-06-01

    Full Text Available Biodiesel wastewater generally contains high levels of oils, soaps and glycerol residues. This needs wastewater treatment. In this study, the biodiesel wastewater treatment was tested (industrial wastewater (EFID and laboratory wastewater (EFLB from biodiesel by performing flocculation and dual-flocculation with renewable polymers. Tannin and cationic hemicellulose (CH were used as cationic flocculant, and cellulose acetate sulfate (CAS was used as an anionic flocculant. Polyacrylamide (PAM was used as a reference anionic flocculant for result efficiencies analysis obtained with CAS (renewable source flocculant. The treatment efficacy in wastewater was evaluated by: turbidity removal, sludge volume formed, chemical oxygen demand (COD and total suspended solids (TSS. The obtained sludge was studied using thermogravimetric analysis (TG. The dual-flocculation application condition of the 25% proportion of tannin (T and 75% proportion of cationic hemicelluloses (i.e., T25/CH75 showed EFLB turbidity removal of 89.1% and 89.5% for CAS and PAM additions respectively, and for EFID of 67% and 41% for CAS and PAM additions respectively. The dual-flocculation performance suggested that the polyelectrolytes obtained from renewable sources can be used for treating biodiesel wastewater.

  10. Obtaining ZnO nanocrystalline through methods of combustion and precipitation

    International Nuclear Information System (INIS)

    Garcia, A.P.; Guaglianoni, W.C.; Cunha, M.A.; Basegio, T.M.; Bergmann, C.P.

    2012-01-01

    Zinc oxide is important technological applications in rubber and industrial paints. The chemical properties and microstructure of ZnO powder depends on the synthesis method employed. In this work, it was obtained nanosized ZnO using different synthesis processes, such as solution combustion and precipitation, varying the concentrations of reactants and the working temperature. The obtained powders were characterized by SEM, BET, XRD, crystallite size determination and thermal analysis (TGA and DTA). It was possible to obtain nanosized ZnO with the methods used. (author)

  11. Secondary nerve lengthening to obtain full knee extension in popliteal pterygium syndrome.

    Science.gov (United States)

    Boeckx, Willy; Misani, Marta; Vandermeeren, Liesbeth; Franck, Diane; Zirak, Christophe; Demey, Albert

    2014-05-01

    Microsurgical nerve lengthening was performed in two siblings presenting a popliteal pterigium syndrome with a knee flexion contracture of 80 degrees. After the first attempt for nerve lengthening and knee extension elsewhere, a repeated lengthening was required due to continuing tip-toe walking and recurrent knee contracture at the age of 3 years. An extensive external and internal interfascicular microsurgical neurolysis resulted in a lengthening of the nerves. A full length of leg procedure had to be performed, inclusive of Achilles tendon lengthening to obtain a complete extension of the knee and a 90-degree ankle flexion. Maintaining the leg in a fully extended position was obtained with a dynamic splinting in the first month after the operation. When timing the operation we have to consider the importance of adequate precision of the microsurgical neurolysis, down to the identification of the Fontana bands, and the adequate postoperative splinting. Thieme Medical Publishers 333 Seventh Avenue, New York, NY 10001, USA.

  12. Processing of hydroxyapatite obtained by combustion synthesis

    International Nuclear Information System (INIS)

    Canillas, M.; Rivero, R.; García-Carrodeguas, R.; Barba, F.; Rodríguez, M.A.

    2017-01-01

    One of the reasons of implants failure are the stress forces appearing in the material–tissue interface due to the differences between their mechanical properties. For this reason, similar mechanical properties to the surrounding tissue are desirable. The synthesis of hydroxyapatite by solution combustion method and its processing have been studied in order to obtain fully dense ceramic bodies with improved mechanical strength. Combustion synthesis provides nanostructured powders characterized by a high surface area to facilitate the following sintering. Moreover, synthesis was conducted in aqueous and oxidizing media. Oxidizing media improve homogenization and increase the energy released during combustion. It gives rise to particles whose morphology and size suggest lower surface energies compared with aqueous media. The obtained powders were sintered by using a controlled sintering rate schedule. Lower surfaces energies minimize the shrinkage during sintering and relative densities measurements and diametral compression test confirm improved densification and consequently mechanical properties. [es

  13. Processing of hydroxyapatite obtained by combustion synthesis

    Directory of Open Access Journals (Sweden)

    M. Canillas

    2017-09-01

    Full Text Available One of the reasons of implants failure are the stress forces appearing in the material–tissue interface due to the differences between their mechanical properties. For this reason, similar mechanical properties to the surrounding tissue are desirable. The synthesis of hydroxyapatite by solution combustion method and its processing have been studied in order to obtain fully dense ceramic bodies with improved mechanical strength. Combustion synthesis provides nanostructured powders characterized by a high surface area to facilitate the following sintering. Moreover, synthesis was conducted in aqueous and oxidizing media. Oxidizing media improve homogenization and increase the energy released during combustion. It gives rise to particles whose morphology and size suggest lower surface energies compared with aqueous media. The obtained powders were sintered by using a controlled sintering rate schedule. Lower surfaces energies minimize the shrinkage during sintering and relative densities measurements and diametral compression test confirm improved densification and consequently mechanical properties.

  14. COMPARISON OF GINGER (Zingiber officiale Roscoe OLEORESIN OBTAINED WITH ETHANOL AND ISOPROPANOL WITH THAT OBTAINED WITH PRESSURIZED CO2

    Directory of Open Access Journals (Sweden)

    Lia P. NOBREGA

    1997-12-01

    Full Text Available Ginger (Zingiber officinale Roscoe belongs to the Zingiberacea family. It is a spice of great commercial importance. In this work ginger oleoresin was obtained with ethanol, isopropanol and liquid carbon dioxide. The chemical compositions of the extract were compared with each other. All oleoresin samples had monoterpenes and sesquiterpenes. Carboxylic acids were found in organic solvent extracts for an extraction time of 2 hours. The component responsible the for pungent characteristic of the oleoresin, gingerois, were detected in samples obtained with organic solvent for extraction times of 6 hours and in samples obtained with CO2 liquid for extraction times of 2 hours.O gengibre (Zingiber officinale Roscoe pertence à família Zingiberacea. É uma especiaria de grande importância comercial. Neste trabalho realizou-se extrações da oleoresina de gengibre com etanol, isopropanol e dióxido de carbono líquido e comparou-se a composição química de cada um dos extratos. A oleoresina obtida tem componentes das classes dos monoterpenos e sesquiterpenos em todas as amostras. Ácidos carboxílicos foram encontrados nos extratos obtidos com solvente orgânico, quando o tempo de extração foi de 2 horas. Os componentes que dão a característica pungente à oleoresina, os gingerois, foram detectados nas amostras obtidas com solvente orgânico, quando o tempo de extração foi de 6 horas e, nas amostras obtidas com CO2 líquido, com 2 horas de extração.

  15. Metagenomics as a tool to obtain full genomes of process-critical bacteria in engineered systems

    DEFF Research Database (Denmark)

    Albertsen, Mads; Hugenholtz, Philip; Tyson, Gene W.

    of the community. The assembled genomes include many of the process-critical bacteria involved in wastewater treatment, such as Competibacter, Tetrasphaera and TM7. The approach is not limited to different extraction methods, but can be applied to any treatment that results in different relative abundance......Bacteria play a pivotal role in engineered systems such as wastewater treatment plants. Obtaining genomes of the bacteria provides the genetic potential of the system and also allows studies of in situ functions through transcriptomics and proteomics. Hence, it enables correlations of operational......, the sequencing of bulk genomic DNA from environmental samples, has the potential to provide genomes of this uncultured majority. However, so far only few bacterial genomes have been obtained from metagenomic data. In this study we present a new approach to obtain individual genomes from metagenomes. We deeply...

  16. Secondary electron images obtained with a standard photoelectron emission microscope set-up

    International Nuclear Information System (INIS)

    Benka, Oswald; Zeppenfeld, Peter

    2005-01-01

    The first results of secondary electron images excited by 3-4.3 keV electrons are presented. The images are obtained with a standard FOCUS-PEEM set-up equipped with an imaging energy filter (IEF). The electron gun was mounted on a standard PEEM entrance flange at an angle of 25 deg. with respect to the sample surface. A low extraction voltage of 500 V was used to minimize the deflection of the electron beam by the PEEM extraction electrode. The secondary electron images are compared to photoelectron images excited by a standard 4.9 eV UV lamp. In the case of a Cu pattern on a Si substrate it is found that the lateral resolution without the IEF is about the same for electron and photon excitation but that the relative electron emission intensities are very different. The use of the IEF reduces the lateral resolution. Images for secondary electron energies between eV 1 and eV 2 were obtained by setting the IEF to -V 1 and -V 2 ∼-(V 1 +5V) potentials and taking the difference of both images. Images up to 100 eV electron energies were recorded. The material contrast obtained in these difference images is discussed in terms of a secondary electron and photoelectron emission model and secondary electron energy spectra measured with a LEED-Auger spectrometer

  17. Structure investigations of ferromagnetic Co-Ni-Al alloys obtained by powder metallurgy.

    Science.gov (United States)

    Maziarz, W; Dutkiewicz, J; Lityńska-Dobrzyńska, L; Santamarta, R; Cesari, E

    2010-03-01

    Elemental powders of Co, Ni and Al in the proper amounts to obtain Co(35)Ni(40)Al(25) and Co(40)Ni(35)Al(25) nominal compositions were ball milled in a high-energy mill for 80 h. After 40 h of milling, the formation of a Co (Ni, Al) solid solution with f.c.c. structure was verified by a change of the original lattice parameter and crystallite size. Analytical transmission electron microscopy observations and X-ray diffraction measurements of the final Co (Ni, Al) solid solution showed that the crystallite size scattered from 4 to 8 nm and lattice parameter a = 0.36086 nm. The chemical EDS point analysis of the milled powder particles allowed the calculation of the e/a ratio and revealed a high degree of chemical homogeneity of the powders. Hot pressing in vacuum of the milled powders resulted in obtaining compacts with a density of about 70% of the theoretical one. An additional heat treatment increased the density and induced the martensitic transformation in a parent phase. Selected area diffraction patterns and dark field images obtained from the heat-treated sample revealed small grains around 300 nm in diameter consisting mainly of the ordered gamma phase (gamma'), often appearing as twins, and a small amount of the L1(0) ordered martensite.

  18. Innovative Formulation Combining Al, Zr and Si Precursors to Obtain Anticorrosion Hybrid Sol-Gel Coating

    Directory of Open Access Journals (Sweden)

    Clément Genet

    2018-05-01

    Full Text Available The aim of our study is to improve the aluminium alloy corrosion resistance with Organic-Inorganic Hybrid (OIH sol-gel coating. Coatings are obtained from unusual formulation with precursors mixing: glycidoxypropyltrimethoxysilane (GPTMS, zirconium (IV propoxide (TPOZ and aluminium tri-sec-butoxide (ASB. This formulation was characterized and compared with sol formulations GPTMS/TPOZ and GPTMS/ASB. In each formulation, a corrosion inhibitor, cerium (III nitrate hexahydrate, is employed to improve the corrosion performance. Coatings obtained from sol based on GPTMS/TPOZ/ASB have good anti-corrosion performances with Natural Salt Spray (NSS resistance of 500 h for a thickness lower than 4 µm. Contact angle measurement showed a coating hydrophobic behaviour. To understand these performances, nuclear magnetic resonance (NMR analyses were performed, results make sol-gel coating condensation evident and are in very good agreement with previous results.

  19. Innovative Formulation Combining Al, Zr and Si Precursors to Obtain Anticorrosion Hybrid Sol-Gel Coating.

    Science.gov (United States)

    Genet, Clément; Menu, Marie-Joëlle; Gavard, Olivier; Ansart, Florence; Gressier, Marie; Montpellaz, Robin

    2018-05-10

    The aim of our study is to improve the aluminium alloy corrosion resistance with Organic-Inorganic Hybrid (OIH) sol-gel coating. Coatings are obtained from unusual formulation with precursors mixing: glycidoxypropyltrimethoxysilane (GPTMS), zirconium (IV) propoxide (TPOZ) and aluminium tri-sec-butoxide (ASB). This formulation was characterized and compared with sol formulations GPTMS/TPOZ and GPTMS/ASB. In each formulation, a corrosion inhibitor, cerium (III) nitrate hexahydrate, is employed to improve the corrosion performance. Coatings obtained from sol based on GPTMS/TPOZ/ASB have good anti-corrosion performances with Natural Salt Spray (NSS) resistance of 500 h for a thickness lower than 4 µm. Contact angle measurement showed a coating hydrophobic behaviour. To understand these performances, nuclear magnetic resonance (NMR) analyses were performed, results make sol-gel coating condensation evident and are in very good agreement with previous results.

  20. Porous titanium obtained by a new powder metallurgy technique: Preliminary results of human osteoblast adhesion on surface polished substrates.

    Science.gov (United States)

    Biasotto, M; Ricceri, R; Scuor, N; Schmid, C; Sandrucci, M A; Di Lenarda, R; Matteazzi, P

    2003-01-01

    This study concerns a novel powder metallurgy method for producing porous titanium (pTi) exhibiting high mechanical properties. The preparation procedure consisted of the following stages: first, the preparation of Ti and titanium hydride (TiH2) powder mixtures and their consolidation with a cold isostatic press, followed by a sintering of the green bodies performed with hot isostatic press (HIP) equipment. Thermal decomposition in controlled environment of the TiH2 phase results in the foam structure. The resulting porosity percolates with a volume fraction of approximately 20%. The final material exhibits interesting mechanical properties, comparable to those of full density titanium (between grade 2 and grade 3), with the advantage of a minor density. The samples produced were tested to verify their biological response by studying the effectiveness of osteoblast adhesion and growth. In this preliminary study, osteoblastic cell morphology was investigated and compared to that observed on fully dense commercially pure titanium (Ti-cp) (ASTM, grade 3). The preliminary results were promising regarding cellular adhesion and spreading. (Journal of Applied Biomaterials & Biomechanics 2003; 1: 172-7).

  1. 30 CFR 204.201 - Who may obtain accounting and auditing relief?

    Science.gov (United States)

    2010-07-01

    ... 30 Mineral Resources 2 2010-07-01 2010-07-01 false Who may obtain accounting and auditing relief... MINERALS REVENUE MANAGEMENT ALTERNATIVES FOR MARGINAL PROPERTIES Accounting and Auditing Relief § 204.201 Who may obtain accounting and auditing relief? (a) You may obtain accounting and auditing relief under...

  2. Microbiological quality of five potato products obtained at retail markets.

    Science.gov (United States)

    Duran, A P; Swartzentruber, A; Lanier, J M; Wentz, B A; Schwab, A H; Barnard, R J; Read, R B

    1982-01-01

    The microbiological quality of frozen hash brown potatoes, dried hash brown potatoes with onions, frozen french fried potatoes, dried instant mashed potatoes, and potato salad was determined by a national sampling at the retail level. A wide range of results was obtained, with most sampling units of each products having excellent microbiological quality. Geometric mean aerobic plate counts were as follows: dried hash brown potatoes, 270/g; frozen hash brown potatoes with onions, 580/g; frozen french fried potatoes 78/g; dried instant mashed potatoes, 1.1 x 10(3)/g; and potato salad, 3.6 x 10(3)/g. Mean values of coliforms, Escherichia coli, and Staphylococcus aureus were less than 10/g. PMID:6758695

  3. Shielding design to obtain compact marine reactor

    International Nuclear Information System (INIS)

    Yamaji, Akio; Sako, Kiyoshi

    1994-01-01

    The marine reactors equipped in previously constructed nuclear ships are in need of the secondary shield which is installed outside the containment vessel. Most of the weight and volume of the reactor plants are occupied by this secondary shield. An advanced marine reactor called MRX (Marine Reactor X) has been designed to obtain a more compact and lightweight marine reactor with enhanced safety. The MRX is a new type of marine reactor which is an integral PWR (The steam generator is installed in the pressure vessel.) with adopting a water-filled containment vessel and a new shielding design method of no installation of the secondary shield. As a result, MRX is considerably lighter in weight and more compact in size as compared with the reactors equipped in previously constructed nuclear ships. For instance, the plant weight and volume of the containment vessel of MRX are about 50% and 70% of those of the Nuclear Ship MUTSU, in spite of the power of MRX is 2.8 times as large as the MUTSU's reactor. The shielding design calculation was made using the ANISN, DOT3.5, QAD-CGGP2 and ORIGEN codes. The computational accuracy was confirmed by experimental analyses. (author)

  4. An audit of the contribution to post-mortem examination diagnosis of individual analyte results obtained from biochemical analysis of the vitreous.

    Science.gov (United States)

    Mitchell, Rebecca; Charlwood, Cheryl; Thomas, Sunethra Devika; Bellis, Maria; Langlois, Neil E I

    2013-12-01

    Biochemical analysis of the vitreous humor from the eye is an accepted accessory test for post-mortem investigation of cause of death. Modern biochemical analyzers allow testing of a range of analytes from a sample. However, it is not clear which analytes should be requested in order to prevent unnecessary testing (and expense). The means and standard deviation of the values obtained from analysis of the vitreous humor for sodium, potassium, chloride, osmolality, glucose, ketones (β-hydroxybutyrate), creatinine, urea, calcium, lactate, and ammonia were calculated from which the contribution of each analyte was reviewed in the context of post-mortem findings and final cause of death. For sodium 32 cases were regarded as high (more than one standard deviation above the mean), from which 9 contributed to post-mortem diagnosis [drowning (4), heat related death (2), diabetic hyperglycemia (2), and dehydration (1)], but 25 low values (greater than one standard deviation below the mean) made no contribution. For chloride 29 high values contributed to 4 cases--3 drowning and 1 heat-related, but these were all previously identified by a high sodium level. There were 29 high and 35 low potassium values, none of which contributed to determining the final cause of death. Of 22 high values of creatinine, 12 contributed to a diagnosis of renal failure. From 32 high values of urea, 18 contributed to 16 cases of renal failure (2 associated with diabetic hyperglycemia), 1 heat-related death, and one case with dehydration. Osmolarity contributed to 12 cases (5 heat-related, 4 diabetes, 2 renal failure, and 1 dehydration) from 36 high values. There was no contribution from 32 high values and 19 low values of calcium and there was no contribution from 4 high and 2 low values of ammonia. There were 11 high values of glucose, which contributed to the diagnosis of 6 cases of diabetic hyperglycemia and 21 high ketone levels contributed to 8 cases: 4 diabetic ketosis, 3 hypothermia, 3

  5. Diversification of the Industrial Use of the Land River Layer: Obtaining Aluminum Sulfate for Water Treatment

    Directory of Open Access Journals (Sweden)

    Leonardo Rodríguez-Suárez

    2017-04-01

    Full Text Available With the objective of obtaining aluminum sulphate to be used as a coagulant in the water treatment, experimental test works were conducted with a sample of the kaolin ore body Río del Callejón located in the special municipality of the Isle of Youth. The sample was characterized from the chemical and granulometric point of view and was subjected to a technological process with calcination and sulphuric acid leaching being the main operations. The Plackett–Burman screening design was used in the technological tests taking calcination temperature, calcination time, leaching temperature, leaching time, agitation velocity, acid concentration and liquid-solid ratio as independent variables. An aluminum sulphate with suitable characteristics to be used as a coagulant substance in water treatment (human consumption and residual was obtained. The experimental results revealed that the aluminum sulphate obtained shows better quality than that of the one currently obtained in the industry using aluminum hydroxide.

  6. Obtaining antibiotics online from within the UK: a cross-sectional study

    Science.gov (United States)

    Boyd, Sara Elizabeth; Moore, Luke Stephen Prockter; Gilchrist, Mark; Costelloe, Ceire; Castro-Sánchez, Enrique; Franklin, Bryony Dean; Holmes, Alison Helen

    2017-01-01

    Background: Improved antibiotic stewardship (AS) and reduced prescribing in primary care, with a parallel increase in personal internet use, could lead citizens to obtain antibiotics from alternative sources online. Objectives: A cross-sectional analysis was performed to: (i) determine the quality and legality of online pharmacies selling antibiotics to the UK public; (ii) describe processes for obtaining antibiotics online from within the UK; and (iii) identify resulting AS and patient safety issues. Methods: Searches were conducted for ‘buy antibiotics online’ using Google and Yahoo. For each search engine, data from the first 10 web sites with unique URL addresses were reviewed. Analysis was conducted on evidence of appropriate pharmacy registration, prescription requirement, whether antibiotic choice was ‘prescriber-driven’ or ‘consumer-driven’, and whether specific information was required (allergies, comorbidities, pregnancy) or given (adverse effects) prior to purchase. Results: Twenty unique URL addresses were analysed in detail. Online pharmacies evidencing their location in the UK (n = 5; 25%) required a prescription before antibiotic purchase, and were appropriately registered. Online pharmacies unclear about the location they were operating from (n = 10; 50%) had variable prescription requirements, and no evidence of appropriate registration. Nine (45%) online pharmacies did not require a prescription prior to purchase. For 16 (80%) online pharmacies, decisions were initially consumer-driven for antibiotic choice, dose and quantity. Conclusions: Wide variation exists among online pharmacies in relation to antibiotic practices, highlighting considerable patient safety and AS issues. Improved education, legislation, regulation and new best practice stewardship guidelines are urgently needed for online antibiotic suppliers. PMID:28333179

  7. 22 CFR 42.1 - Aliens not required to obtain immigrant visas.

    Science.gov (United States)

    2010-04-01

    ... 22 Foreign Relations 1 2010-04-01 2010-04-01 false Aliens not required to obtain immigrant visas... Immigrants § 42.1 Aliens not required to obtain immigrant visas. An immigrant within any of the following categories is not required to obtain an immigrant visa: (a) Aliens lawfully admitted for permanent residence...

  8. Genotoxicity of corrosion eluates obtained from orthodontic brackets in vitro.

    Science.gov (United States)

    Angelieri, Fernanda; Marcondes, Joao Paulo C; de Almeida, Danielle Cristina; Salvadori, Daisy M F; Ribeiro, Daniel A

    2011-04-01

    The purpose of this study was to evaluate whether corrosion eluates obtained from commercially available orthodontic brackets are able to induce genetic damage in vitro. Genotoxicity was assessed by the single cell gel (comet) assay using Chinese hamster ovary (CHO) cells. The following orthodontic metallic brackets were used: Morelli (Sorocaba, Brazil); Abzil (São José do Rio Preto, Brazil); Dentaurum (Pforzheim, Germany); and 3M Unitek (Puchheim, Germany). Each dental bracket was submitted to a corrosion process in a solution containing equal amounts of acetic acid and sodium chloride at 0.1 M concentration for 1, 3, 7, 14, 21, 35, and 70 days. CHO cells were exposed to eluates for 30 minutes at 37°C. The negative control was treated with the same solution used for corrosion process for 30 minutes at 37°C. Independent positive control was performed with methyl methanesulfonate (MMS) (Sigma Aldrich, St. Louis, Mo) at 1 ug/mL for 1 hour. None of the eluates was found to exhibit genotoxicity, regardless of the different commercial brands of orthodontic appliance used. In summary, our results indicate corrosion eluates obtained from orthodontic brackets do not induce genetic damage as assessed by single cell gel (comet) assay. Copyright © 2011 American Association of Orthodontists. Published by Mosby, Inc. All rights reserved.

  9. Peeled Guidewire Coating with Debulked Plaque Obtained by Directional Coronary Atherectomy

    Directory of Open Access Journals (Sweden)

    Rikuta Hamaya

    2017-01-01

    Full Text Available Percutaneous directional coronary atherectomy (DCA is a plaque debulking method performed in Japan, and recently a renewed DCA device has been launched. We present a case with a tight left anterior descending lesion undergoing percutaneous coronary intervention with application of DCA. After several sessions of DCA, white plaques accompanied by green, stringed materials were obtained from the device; some materials were considerably long (approximately 15 mm in length. A drug-eluting stent was subsequently implanted, and the procedure was completed successfully without any complications. The extracted plaques and artificial materials were pathologically examined, and no inflammatory changes were detected on plaques adjacent to the material. Assessing pathological findings and structure of the DCA catheter, the obtained artificial materials were considered as peeled guidewire, possibly resulting from the friction between the guidewire and metallic bearing in the housing of DCA catheter. Of note, this phenomenon has been recognized even in other DCA cases in which guidewires of the other kind are used. We report this phenomenon for the first time, warning of theoretically possible distal embolization of artificial materials caused by any debulking devices.

  10. Cell response to nanocrystallized metallic substrates obtained through severe plastic deformation.

    Science.gov (United States)

    Bagherifard, Sara; Ghelichi, Ramin; Khademhosseini, Ali; Guagliano, Mario

    2014-06-11

    Cell-substrate interface is known to control the cell response and subsequent cell functions. Among the various biophysical signals, grain structure, which indicates the repeating arrangement of atoms in the material, has also proved to play a role of significant importance in mediating the cell activities. Moreover, refining the grain size through severe plastic deformation is known to provide the processed material with novel mechanical properties. The potential application of such advanced materials as biomedical implants has recently been evaluated by investigating the effect of different substrate grain sizes on a wide variety of cell activities. In this review, recent advances in biomedical applications of severe plastic deformation techniques are highlighted with special attention to the effect of the obtained nano/ultra-fine-grain size on cell-substrate interactions. Various severe plastic deformation techniques used for this purpose are discussed presenting a brief description of the mechanism for each process. The results obtained for each treatment on cell morphology, adhesion, proliferation, and differentiation, as well as the in vivo studies, are discussed. Finally, the advantages and challenges regarding the application of these techniques to produce multifunctional bio-implant materials are addressed.

  11. U-Mo Alloy Powder Obtained Through Selective Hydriding. Particle Size Control

    International Nuclear Information System (INIS)

    Balart, S.N.; Bruzzoni, P.; Granovsky, M.S.

    2002-01-01

    Hydride-dehydride methods to obtain U-Mo alloy powder for high-density fuel elements have been successfully tested by different authors. One of these methods is the selective hydriding of the α phase (HSα). In the HSα method, a key step is the partial decomposition of the γ phase (retained by quenching) to α phase and an enriched γ phase or U 2 Mo. This transformation starts mainly at grain boundaries. Subsequent hydrogenation of this material leads to selective hydriding of the α phase, embrittlement and intergranular fracture. According to this picture, the particle size of the final product should be related to the γ grain size of the starting alloy. The feasibility of controlling the particle size of the product by changing the γ grain size of the starting alloy is currently investigated. In this work an U-7 wt% Mo alloy was subjected to various heat treatments in order to obtain different grain sizes. The results on the powder particle size distribution after applying the HSα method to these samples show that there is a strong correlation between the original γ grain size and the particle size distribution of the powder. (author)

  12. The use of nuclear energy for obtaining petroleum

    International Nuclear Information System (INIS)

    Waldmann, H.; Koch, C.; Thelen, H.J.; Kappe, P.

    1982-01-01

    After some basic considerations of petroleum demand, petroleum supply and petroleum reserves, the article gives a survey of the various methods of obtaining petroleum. The use of energy in the form of steam and electricity in the previously used processes and in conventional deposits requires up to 50% of the energy contained in the oil obtained. Now unconventional sources of petroleum (tertiary petroleum, heavy fractions and shale oil) could become of interest to West Germany in the near future. The economy of production can be determined by the energy source used, to a large extent. A series of possibilities are discussed for using nuclear steam raising systems for this purpose. (UA) [de

  13. Carbon/Clay nanostructured composite obtained by hydrothermal method

    International Nuclear Information System (INIS)

    Barin, G.B.; Bispo, T.S.; Gimenez, I.F.; Barreto, L.S.; Souza Filho, A.G.

    2010-01-01

    The development of strategies for converting biomass into useful materials, more efficient energy carrier and / or hydrogen storage is shown a key issue for the present and future. Carbon nanostructure can be obtained by severe processing techniques such as arc discharge, chemical deposition and catalyzed pyrolysis of organic compounds. In this study we used hydrothermal methods for obtaining nanostructured composites of carbon / clay. To this end, we used coir dust and special clays. The samples were characterized by infrared spectroscopy, X-ray diffraction and Raman. The presence of the D band at 1350 cm -1 in the Raman spectrum shows the formation of amorphous carbon with particle size of about 8.85 nm. (author)

  14. SIGNIFICATIVE ANO PROBLEM BASED LEARNING IN IMMUNOLOGY: OBTAINING A KIT TO TYPE NEISSERIA GONORRHOEAE

    Directory of Open Access Journals (Sweden)

    Marina Miguez

    2003-06-01

    Full Text Available Neisseria gonorrhoeae (Ng have been classified serologically on the basis of the antigenicity of the major porin (Por. Por! occurs in two immunochemically distinct serogroups: PorlA and Porffi. Because the diagnostic, therapeutic, social, and legal corisequences of misidentification of a nongonococcal Neisseria isolate as Ng can be substantial, the accurate and rapid identification of this organism is important. Typifying of Ng is done by techniques baséd on phenotypic characteristics and plasmidic content that individually don't reach an adequate discrimination, and so combination of techniques ·must be used. The aim of this work is to obtain polyclonal specificAb that discriminate Ng types Por!Aand Porffi. For this purpose, weimmunized two rabbits with sonicated PorlA and Porm strains ofNg (isolated from clínica! samples and serologically classified. The Ab response was analyzed along the protocol by ELISAand by direct agglutination with latex coated with sonicated Ng. With these data, we selected the bleeding providing the serum with maximum specific Ab ti ter to prepare the typing reagents. Unwanted Ab directed against shared epitopes were removed by adsorption with Ng latex. The typing reagents were obtained by coating latex with each depleted sera. Our results suggest that high titers of specific Ab be obtained for both strains ofNg and the depleted sera be discriminated between both strains. These results suggest that these diagnostic reagents could be useful to confirrn presumptive identification by a simple and rapid method.

  15. High-energy radiation processing, a smart approach to obtain PVP-graft-AA nanogels

    International Nuclear Information System (INIS)

    Grimaldi, N.; Sabatino, M.A.; Przybytniak, G.; Kaluska, I.; Bondì, M.L.; Bulone, D.; Alessi, S.; Spadaro, G.; Dispenza, C.

    2014-01-01

    Poly(N-vinylpyrrolidone)-grafted-acrylic acid biocompatible nanogels (NGs) were prepared using an exiting industrial-type electron accelerator and setups, starting from semi-dilute aqueous solutions of a commercial PVP and the acrylic acid monomer. As a result, NGs with tunable size and structure can be obtained quantitatively. Sterility was also imparted at the integrated dose absorbed. The chemical structure of the NGs produced was confirmed through Fourier Transformer Infrared Spectroscopy (FT-IR). The molecular and physico-chemical properties of NGs, such as the hydrodynamic dimensions and surface charge densities, for various polymer and monomer concentrations in the irradiated solutions, are discussed here. - Highlights: • Aqueous solutions of PVP and AA were irradiated by industrial electron accelerator. • NGs with different physico-chemical and molecular properties can be obtained. • Carboxyl-functionalized NGs produced are promising building blocks for bio-devices

  16. Use of Repeated Fluoropolymer Suspensions to Obtain Composite Electrochemical Coating Based on Zinc

    Science.gov (United States)

    Musikhina, T. A.; Zemtsova, E. A.; Fuks, C. L.

    2017-11-01

    This article deals with the issues of utilization of the waste products of fluoropolymers, namely, the suspensions of fluoroplasts that have lost their consumer properties. Such waste is recommended to be used as a filler of zinc coatings to provide increased corrosion resistance. Using the method of mathematical planning of the experiment, the authors establish the optimal compositions of galvanizing chloride-ammonium electrolytes to obtain the corrosion-resistant composite electrochemical coatings (CEC) of zinc-fluoropolymer. As a result, coatings with a finely crystalline structure were obtained differing in the distribution pattern on the surface of the samples and depending on the variation in the zinc concentration in the electrolytes. The samples of steel reinforcement with the zinc-fluoropolymer coating were tested on corrosion resistance. The increase of anticorrosive properties in CEC zinc-fluoropolymer and a slight decrease in microhardness were indicated.

  17. Modelling of classical ghost images obtained using scattered light

    International Nuclear Information System (INIS)

    Crosby, S; Castelletto, S; Aruldoss, C; Scholten, R E; Roberts, A

    2007-01-01

    The images obtained in ghost imaging with pseudo-thermal light sources are highly dependent on the spatial coherence properties of the incident light. Pseudo-thermal light is often created by reducing the coherence length of a coherent source by passing it through a turbid mixture of scattering spheres. We describe a model for simulating ghost images obtained with such partially coherent light, using a wave-transport model to calculate the influence of the scattering on initially coherent light. The model is able to predict important properties of the pseudo-thermal source, such as the coherence length and the amplitude of the residual unscattered component of the light which influence the resolution and visibility of the final ghost image. We show that the residual ballistic component introduces an additional background in the reconstructed image, and the spatial resolution obtainable depends on the size of the scattering spheres

  18. Modelling of classical ghost images obtained using scattered light

    Energy Technology Data Exchange (ETDEWEB)

    Crosby, S; Castelletto, S; Aruldoss, C; Scholten, R E; Roberts, A [School of Physics, University of Melbourne, Victoria, 3010 (Australia)

    2007-08-15

    The images obtained in ghost imaging with pseudo-thermal light sources are highly dependent on the spatial coherence properties of the incident light. Pseudo-thermal light is often created by reducing the coherence length of a coherent source by passing it through a turbid mixture of scattering spheres. We describe a model for simulating ghost images obtained with such partially coherent light, using a wave-transport model to calculate the influence of the scattering on initially coherent light. The model is able to predict important properties of the pseudo-thermal source, such as the coherence length and the amplitude of the residual unscattered component of the light which influence the resolution and visibility of the final ghost image. We show that the residual ballistic component introduces an additional background in the reconstructed image, and the spatial resolution obtainable depends on the size of the scattering spheres.

  19. Photometric data from some photographs of Mars obtained with the Automatic Interplanetary Station 'Mars 3'

    International Nuclear Information System (INIS)

    Botvinova, V.V.; Bugaenko, O.I.; Koval, I.K.; Narajeva, M.K.; Selivanov, A.S.

    1974-01-01

    The results of detailed photometric treatment of Mars photographs obtained with the Automatic Interplanetary Station 'Mars 3' in three wavelengths are given. Photometric maps of the Martian surface have been constructed; a thin layer observed near the limb has been investigated. (Auth.)

  20. Process for obtaining oxygen doped zinc telluride monocrystals and scintillator crystals obtained by this process

    International Nuclear Information System (INIS)

    Schneider, Maurice; Moreau, Roland; D'Haenen, J.-P.; Merenda, Pierre.

    1976-01-01

    A process is described for obtaining oxygen doped zinc telluride monocrystals, for use as scintillator crystals for ionising radiation detectors. The following operations are carried out in succession: one or several zinc telluride crystals are introduced into a silica ampoule together with a ternary mixture of zinc tellurium and oxygen, as an oxide or hydroxide of these elements; the ampoule is pumped down to a high vacuum and sealed; the sealed ampoule containing the mixture and monocrystals is placed in a kiln and brought to a uniform temperature sufficient to make the mixture three-phased, depending on its composition; the zinc telluride crystalline compound remains solid; the ampoule is then tempered to bring it quickly back to ambient temperature [fr