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Sample records for total neutron structure

  1. Structure analysis of liquids and disordered materials using pulsed neutron diffraction and total scattering

    International Nuclear Information System (INIS)

    Suzuya, Kentaro

    2011-01-01

    Neutron diffraction·total scattering at pulsed neutron source is a powerful method to analyze the complex structure of disordered materials: liquids, glasses, amorphous materials and disordered crystals. The basic idea of the structure of disordered materials, the fundamental diffraction theory for disordered materials, and structure analysis of disordered materials using pulsed neutron diffraction·total scattering technique (TOF method) are described in detail. In addition, the precise information of the world highest class J-PARC MLF spallation neutron source and typical J-PARC neutron total scattering instrument NOVA are also given. Recent structural modelling methods of disordered materials such like reverse Monte Carlo (RMC) simulation method is briefly described using an example of the analysis of a typical disordered material silica glass. (author)

  2. The Structure of Ethylbenzene, Styrene and Phenylacetylene Determined by Total Neutron Scattering

    OpenAIRE

    Szala‐Bilnik, Joanna; Falkowska, Marta; Bowron, Daniel T.; Hardacre, Christopher; Youngs, Tristan G. A.

    2017-01-01

    Abstract Organic solvents such as phenylacetylene, styrene and ethylbenzene are widely used in industrial processes, especially in the production of rubber or thermoplastics. Despite their important applications detailed knowledge about their structure is limited. In this paper the structures of these three aromatic solvents were investigated using neutron diffraction. The results show that many of their structural characteristics are similar, although the structure of phenylacetylene is more...

  3. Resonance structure of 32S+n from measurements of neutron total and capture cross sections

    International Nuclear Information System (INIS)

    Halperin, J.; Johnson, C.H.; Winters, R.R.; Macklin, R.L.

    1980-01-01

    Neutron total and capture cross sections of 32 S have been measured up to 1100 keV neutron energy [E/sub exc/( 33 S) =9700 keV]. Spin and parity assignments have been made for 28 of the 64 resonances found in this region. Values of total radiation widths, reduced neutron widths, level spacings, and neutron strength functions have been evaluated for s/sub 1/2/, p/sub 1/2/, p/sub 3/2/, and d/sub 5/2/ levels. Single particle contributions using the valency model account for a significant portion of the total radiation width only for the p/sub 1/2/-wave resonances. A significant number of resonances can be identified with reported levels excited in 32 S(d,p) and 29 Si(α,n) reactions. A calculation of the Maxwellian average cross section appropriate to stellar interiors indicates an average capture cross section at 30 keV, sigma-bar approx. = 4.2(2) mb, a result that is relatively insensitive to the assumed stellar temperature. Direct (potential) capture and the s-wave resonance capture contributions to the thermal capture cross section do not fully account for the reported thermal cross section (530 +- 40 mb) and a bound state is invoked to account for the discrepancy

  4. The Structure of Ethylbenzene, Styrene and Phenylacetylene Determined by Total Neutron Scattering.

    Science.gov (United States)

    Szala-Bilnik, Joanna; Falkowska, Marta; Bowron, Daniel T; Hardacre, Christopher; Youngs, Tristan G A

    2017-09-20

    Organic solvents such as phenylacetylene, styrene and ethylbenzene are widely used in industrial processes, especially in the production of rubber or thermoplastics. Despite their important applications detailed knowledge about their structure is limited. In this paper the structures of these three aromatic solvents were investigated using neutron diffraction. The results show that many of their structural characteristics are similar, although the structure of phenylacetylene is more ordered and has a smaller solvation sphere than either ethylbenzene or styrene. Two regions within the first coordination sphere, in which the surrounding molecules show different preferable orientations with respect to the central molecule, were found for each liquid. Additionally, the localisation of the aliphatic chains reveals that they tend to favour closer interactions with each other than to the aromatic rings of the adjacent molecules. © 2017 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

  5. Examination of total cross section resonance structure of niobium and silicon in neutron transmission experiments

    Science.gov (United States)

    Andrianova, Olga; Lomakov, Gleb; Manturov, Gennady

    2017-09-01

    The neutron transmission experiments are one of the main sources of information about the neutron cross section resonance structure and effect in the self-shielding. Such kind of data for niobium and silicon nuclides in energy range 7 keV to 3 MeV can be obtained from low-resolution transmission measurements performed earlier in Russia (with samples of 0.027 to 0.871 atom/barn for niobium and 0.076 to 1.803 atom/barn for silicon). A significant calculation-to-experiment discrepancy in energy range 100 to 600 keV and 300 to 800 keV for niobium and silicon, respectively, obtained using the evaluated nuclear data library ROSFOND, were found. The EVPAR code was used for estimation the average resonance parameters in energy range 7 to 600 keV for niobium. For silicon a stochastic optimization method was used to modify the resolved resonance parameters in energy range 300 to 800 keV. The improved ROSFOND evaluated nuclear data files were tested in calculation of ICSBEP integral benchmark experiments.

  6. NIF total neutron yield diagnostic

    International Nuclear Information System (INIS)

    Cooper, Gary W.; Ruiz, Carlos L.

    2001-01-01

    We have designed a total neutron yield diagnostic for the National Ignition Facility (NIF) which is based on the activation of In and Cu samples. The particular approach that we have chosen is one in which we calibrate the entire counting system and which we call the ''F factor'' method. In this method, In and/or Cu samples are exposed to known sources of DD and DT neutrons. The activated samples are then counted with an appropriate system: a high purity Ge detector for In and a NaI coincidence system for Cu. We can then calculate a calibration factor, which relates measured activity to total neutron yield. The advantage of this approach is that specific knowledge of such quantities as cross sections and detector efficiencies is not needed. Unless the actual scattering environment of the NIF can be mocked up in the calibration experiment, the F factor will have to be modified using the results of a numerical simulation of the NIF scattering environment. In this article, the calibration factor methodology will be discussed and experimental results for the calibration factors will be presented. Total NIF neutron yields of 10 9 --10 19 can be measured with this method assuming a 50 cm stand-off distance can be employed for the lower yields

  7. Total neutron cross section for 181Ta

    Directory of Open Access Journals (Sweden)

    Schilling K.-D.

    2010-10-01

    Full Text Available The neutron time of flight facility nELBE, produces fast neutrons in the energy range from 0.1 MeV to 10 MeV by impinging a pulsed relativistic electron beam on a liquid lead circuit [1]. The short beam pulses (∼10 ps and a small radiator volume give an energy resolution better than 1% at 1 MeV using a short flight path of about 6 m, for neutron TOF measurements. The present neutron source provides 2 ⋅ 104  n/cm2s at the target position using an electron charge of 77 pC and 100 kHz pulse repetition rate. This neutron intensity enables to measure neutron total cross section with a 2%–5% statistical uncertainty within a few days. In February 2008, neutron radiator, plastic detector [2] and data acquisition system were tested by measurements of the neutron total cross section for 181Ta and 27Al. Measurement of 181Ta was chosen because lack of high quality data in an anergy region below 700 keV. The total neutron cross – section for 27Al was measured as a control target, since there exists data for 27Al with high resolution and low statistical error [3].

  8. Neutron structural biology

    International Nuclear Information System (INIS)

    Niimura, Nobuo

    1999-01-01

    Neutron structural biology will be one of the most important fields in the life sciences which will interest human beings in the 21st century because neutrons can provide not only the position of hydrogen atoms in biological macromolecules but also the dynamic molecular motion of hydrogen atoms and water molecules. However, there are only a few examples experimentally determined at present because of the lack of neutron source intensity. Next generation neutron source scheduled in JAERI (Performance of which is 100 times better than that of JRR-3M) opens the life science of the 21st century. (author)

  9. Total neutron cross section of lead

    International Nuclear Information System (INIS)

    Kanda, K.; Aizawa, O.

    1976-01-01

    The total thermal-neutron cross section of natural lead under various physical conditions was measured by the transmission method. It became clear that the total cross section at room temperature previously reported is lower than the present data. The total cross section at 400, 500, and 600 0 C, above the melting point of lead, 327 0 C, was also measured, and the changes in the cross section as a function of temperature were examined, especially near and below the melting point. The data obtained for the randomly oriented polycrystalline state at room temperature were in reasonable agreement with the theoretical values calculated by the THRUSH and UNCLE-TOM codes

  10. Total variation-based neutron computed tomography

    Science.gov (United States)

    Barnard, Richard C.; Bilheux, Hassina; Toops, Todd; Nafziger, Eric; Finney, Charles; Splitter, Derek; Archibald, Rick

    2018-05-01

    We perform the neutron computed tomography reconstruction problem via an inverse problem formulation with a total variation penalty. In the case of highly under-resolved angular measurements, the total variation penalty suppresses high-frequency artifacts which appear in filtered back projections. In order to efficiently compute solutions for this problem, we implement a variation of the split Bregman algorithm; due to the error-forgetting nature of the algorithm, the computational cost of updating can be significantly reduced via very inexact approximate linear solvers. We present the effectiveness of the algorithm in the significantly low-angular sampling case using synthetic test problems as well as data obtained from a high flux neutron source. The algorithm removes artifacts and can even roughly capture small features when an extremely low number of angles are used.

  11. Determination of the separate lipid and protein profile structures derived from the total membrane profile structure or isolated sarcoplasmic reticulum via x-ray and neutron diffraction

    International Nuclear Information System (INIS)

    Herbette, L.; Blasie, J.K.

    1984-01-01

    Sarcoplasmic reticulum (SR) membranes were prepared to contain biosynthetically deuterated SR phospholipids utilizing specific and general phospholipid exchange proteins (PLEP). Functional measurements and freeze fracture on SR dispersions and x-ray diffraction of hydrated oriented membrane multilayers revealed that the exchanged SR membranes were very similar to unexchanged SR membranes. Low resolution (28-A) neutron diffraction studies utilizing SR membranes exchanged with either protonated or perdeuterated SR phospholipids allowed direct determination of the lipid profile within the isolated SR membrane at two different unit cell repeat distances. These lipid profile structures were found to be highly asymmetric regarding the conformation of the fatty acid chain extents and compositional distribution of phospholipid molecules in the inner vs. outer monolayer of the SR membrane bilayer. The relatively high resolution (11-A) electron-density profile from x-ray diffraction was decomposed by utilizing the asymmetry in the number of phospholipid molecules residing in the inner vs. outer monolayer of the SR lipid bilayer as obtained from the neutron diffraction study. To our knowledge, this represents the first direct determination of a lipid bilayer profile structure within an isolated membrane system

  12. Neutron structural biology

    International Nuclear Information System (INIS)

    Schoenborn, B.

    1997-01-01

    This is the final report of a one-year, Laboratory Directed Research and Development (LDRD) project at Los Alamos National Laboratory (LANL). We investigated design concepts of neutron scattering capabilities for structural biology at spallation sources. This included the analysis of design parameters for protein crystallography as well as membrane diffraction instruments. These instruments are designed to be general user facilities and will be used by scientists from industry, universities, and other national laboratories

  13. Porosity effects in the neutron total cross section of graphite

    International Nuclear Information System (INIS)

    Santisteban, J. R; Dawidowski, J; Petriw, S. N

    2009-01-01

    Graphite has been used in nuclear reactors since the birth of the nuclear industry due to its good performance as a neutron moderator material. Graphite is still an option as moderator for generation IV reactors due to its good mechanical and thermal properties at high operation temperatures. So, there has been renewed interest in a revision of the computer libraries used to describe the neutron cross section of graphite. For sub-thermal neutron energies, polycrystalline graphite shows a larger total cross section (between 4 and 8 barns) than predicted by existing theoretical models (0.2 barns). In order to investigate the origin of this discrepancy we measured the total cross section of graphite samples of three different origins, in the energy range from 0.001 eV to 10 eV. Different experimental arrangements and sample treatments were explored, to identify the effect of various experimental parameters on the total cross section measurement. The experiments showed that the increase in total cross section is due to neutrons scattered around the forward direction. We associate these small-angle scattered neutrons (SANS) to the porous structure of graphite, and formulate a very simple model to compute its contribution to the total cross section of the material. This results in an analytic expression that explicitly depends on the density and mean size of the pores, which can be easily incorporated in nuclear library codes. [es

  14. Neutron spectroscopy, nuclear structure, related topics. Abstracts

    International Nuclear Information System (INIS)

    Sukhovoj, A.M.

    1996-01-01

    Neutron spectroscopy, nuclear structure and related topics are considered. P, T-breaking, neutron beta decay, neutron radiative capture and neutron polarizability are discussed. Reaction with fast neutrons, methodical aspect low-energy fission are considered too

  15. Structure of neutron stars

    International Nuclear Information System (INIS)

    Cheong, C.K.

    1974-01-01

    Structure of neutron stars consisting of a cold and catalyzed superdense matter were investigated by integrating the equations for hydrostatic equilibrium based on the General Relativity theory. The equations of state were obtained with the help of semiempirical nuclear mass formulae. A large phase transition was found between the nuclear and subnuclear density regions. The density phase transition points were calculated as 6.2 x 10 11 and 3.8 x 10 13 g/cm 3 . Due to such a large phase transition, the equation of state practically consists of two parts: The nuclear and subnuclear phases wich are in contact under the thermodynamical equilibrium at the corresponding pressure. Some macroscopic properties of neutron stars are discussed. (Author) [pt

  16. Neutron total cross section measurements of gold and tantalum at the nELBE photoneutron source

    CERN Document Server

    Hannaske, Roland; Beyer, Roland; Junghans, Arnd; Bemmerer, Daniel; Birgersson, Evert; Ferrari, Anna; Grosse, Eckart; Kempe, Mathias; Kögler, Toni; Marta, Michele; Massarczyk, Ralph; Matic, Andrija; Schramm, Georg; Schwengner, Ronald; Wagner, Andreas

    2014-01-01

    Neutron total cross sections of 197 Au and nat Ta have been measured at the nELBE photoneutron source in the energy range from 0.1 - 10 MeV with a statistical uncertainty of up to 2 % and a total systematic uncertainty of 1 %. This facility is optimized for the fast neutron energy range and combines an excellent t ime structure of the neutron pulses (electron bunch width 5 ps) with a short flight path of 7 m. Because of the low instantaneous neutron flux transmission measurements of neutron total cross sections are possible, that exhibit very different beam and back ground conditions than found at other neutron sources.

  17. Neutron structural biology

    Energy Technology Data Exchange (ETDEWEB)

    Niimura, Nobuo [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    1998-03-01

    Neutron diffraction provides an experimental method of directly locating hydrogen atoms in protein which play important roles in physiological functions. However, there are relatively few examples of neutron crystallography in biology since it takes a lot of time to collect a sufficient number of Bragg reflections due to the low flux of neutrons illuminating the sample. In order to overcome the flux problem, we have successfully developed the neutron IP, where the neutron converter, {sup 6}Li or Gd, was mixed with a photostimulated luminescence material on flexible plastic support. Neutron Laue diffraction 2A data from tetragonal lysozyme were collected for 10 days with neutron imaging plates, and 960 hydrogen atoms in the molecule and 157 bound water molecules were identified. These results explain the proposed hydrolysis mechanism of the sugar by the lysozyme molecule and that lysozyme is less active at pH7.0. (author)

  18. NEUTRONIC REACTOR STRUCTURE

    Science.gov (United States)

    Weinberg, A.M.; Vernon, H.C.

    1961-05-30

    A neutronic reactor is described. It has a core consisting of natural uranium and heavy water and having a K-factor greater than unity which is surrounded by a reflector consisting of natural uranium and ordinary water having a Kfactor less than unity.

  19. Secondary standard neutron detector for measuring total reaction cross sections

    International Nuclear Information System (INIS)

    Sekharan, K.K.; Laumer, H.; Gabbard, F.

    1975-01-01

    A neutron detector has been constructed and calibrated for the accurate measurement of total neutron-production cross sections. The detector consists of a polyethylene sphere of 24'' diameter in which 8- 10 BF 3 counters have been installed radially. The relative efficiency of this detector has been determined for average neutron energies, from 30 keV to 1.5 MeV by counting neutrons from 7 Li(p,n) 7 Be. By adjusting the radial positions of the BF 3 counters in the polyethylene sphere the efficiency for neutron detection was made nearly constant for this energy range. Measurement of absolute efficiency for the same neutron energy range has been done by counting the neutrons from 51 V(p,n) 51 Cr and 57 Fe(p,n) 57 Co reactions and determining the absolute number of residual nuclei produced during the measurement of neutron yield. Details of absolute efficiency measurements and the use of the detector for measurement of total neutron yields from neutron producing reactions such as 23 Na(p,n) 23 Mg are given

  20. Proton and neutron structure functions

    International Nuclear Information System (INIS)

    Rock, S.

    1991-01-01

    New result on charged lepton scattering from hydrogen and deuterium targets by the BCDMS, NMC and SLAC collaborations have greatly increased our knowledge of the structure functions of protons and neutrons. The disagreement between the high energy muon scattering cross sections obtained by the EMC and BCDMS collaborations have been almost completely resolved by comparison with a global analysis of old and new SLAC data and a reanalysis of EMC data. We now have a consistent set of structure functions which covers an approximate range 1 ≤ Q 2 ≤ 200 (GeV/c) 2 and 0.07 ≤ x ≤ 0.7. The ratio of neutron to proton structure functions decreases with increasing Q 2 for values of x ≥ 0.1. The difference between proton and neutron structure functions approaches zero as x decreases, consistent with the expected √x behavior. (orig.)

  1. Observation of neutron standing waves at total reflection by precision gamma spectroscopy

    International Nuclear Information System (INIS)

    Aksenov, V.L.; Gundorin, N.A.; Nikitenko, Yu.V.; Popov, Yu.P.; Cser, L.

    1998-01-01

    Total reflection of polarized neutrons from the layered structure glass/Fe (1000 A Angstrom)/Gd (50 A Angstrom) is investigated by registering neutrons and gamma-quanta from thermal neutron capture. The polarization ratio of gamma counts of neutron beams polarized in and opposite the direction of the magnetic field is measured. The polarization ratio is larger than unity for the neutron wavelengths λ 2.2 A Angstrom. Such behaviour of the wavelength dependence of the gamma-quanta polarization ratio points to the fact that over the surface of the Fe Layer a neutron standing wave caused by the interference of the incident neutron wave and the wave refracted from the magnetized Fe layer is formed

  2. Neutron multimonochromator-bipolarizer based on magnetic multilayer Fe/Co and new scheme for the total neutron polarization analysis

    International Nuclear Information System (INIS)

    Syromyatnikov, V.G.; Zaw Lin, Kyaw

    2017-01-01

    In this paper, we present a new neutron-optical element, Neutron Multimonochromator-Bipolarizer (NMB). It consists of a multimultilayer structure made of 12 periodic multilayer Fe/Co magnetic nanostructures whose period increases with distance from the substrate. Results are presented of calculations of the reflection coefficients from the NMB. We propose a new scheme of the total neutron polarization analysis for the time-of-flight method in the reflectometry. In this scheme, double NMB is used as a polarizer and there is no spin-flipper before the sample. NMB can be used in polarized neutron reflectometry, in SESANS, and for research of low-angle and inelastic scattering of polarized neutrons. (paper)

  3. Generation of neutron standing waves at total reflection of polarized neutrons

    International Nuclear Information System (INIS)

    Aksenov, V.L.; Nikitenko, Yu.V.; Kozhevnikov, S.V.; Radu, F.; Kruijs, R.; Rekveldt, M.Th.

    1999-01-01

    The regime of neutron standing waves at reflection of polarized thermal neutrons from the structure glass/Cu (1000 A Angstrom)/Ti (2000 A Angstrom)/Co (60 A Angstrom)/Ti (300 A Angstrom) in a magnetic field directed at an angle to the sample plane is realized. The intensity of neutrons with a particular spin projection on the external magnetic field direction appears to be a periodic function of the neutron wavelength and the glancing angle of the reflected beam. It is shown that the neutron standing wave regime can be a very sensitive method for the determination of changes in the spatial position of magnetic noncollinear layers. (author)

  4. Neutron total scattering cross sections of elemental antimony

    Energy Technology Data Exchange (ETDEWEB)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-11-01

    Neutron total cross sections are measured from 0.8 to 4.5 MeV with broad resolutions. Differential-neutron-elastic-scattering cross sections are measured from 1.5 to 4.0 MeV at intervals of 50 to 200 keV and at scattering angles distributed between 20 and 160 degrees. Lumped-level neutron-inelastic-scattering cross sections are measured over the same angular and energy range. The exPerimental results are discussed in terms of an optical-statistical model and are compared with respective values given in ENDF/B-V.

  5. Neutron total scattering cross sections of elemental antimony

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-11-01

    Neutron total cross sections are measured from 0.8 to 4.5 MeV with broad resolutions. Differential-neutron-elastic-scattering cross sections are measured from 1.5 to 4.0 MeV at intervals of 50 to 200 keV and at scattering angles distributed between 20 and 160 degrees. Lumped-level neutron-inelastic-scattering cross sections are measured over the same angular and energy range. The exPerimental results are discussed in terms of an optical-statistical model and are compared with respective values given in ENDF/B-V

  6. Neutron total cross section measurements on 249Cf

    International Nuclear Information System (INIS)

    Carlton, R.F.; Harvey, J.A.; Hill, N.W.; Pandey, M.S.; Benjamin, R.W.

    1979-01-01

    Neutron total cross section measurements were performed on a sample of 249 Cf (5.65 mg total weight) with the ORELA as a source of pulsed neutrons. The sample, the inverse thickness of which was 1542 barns/atom, consisted of 85.3% 249 Cf and 14.4% 249 Bk, and was cooled to liquid nitrogen temperature. Analyses were also made of data from a thin sample (l/n = 17430) of 65% 249 Cf in the region of the large fission resonance at 0.7 eV. Fifty-five resonances in 249 Cf were observed and analyzed over the energy range 0.1 eV to 90 eV by use of an R-matrix multilevel formalism. The resonance parameters obtained were used to determine the level spacing and the s-wave neutron and fission strength functions. Thermal total cross section measurements were also performed. 5 figures, 3 tables

  7. Evaluation of the 238U neutron total cross section

    International Nuclear Information System (INIS)

    Smith, A.; Poenitz, W.P.; Howerton, R.J.

    1982-12-01

    Experimental energy-averaged neutron total cross sections of 238 U were evaluated from 0.044 to 20.0 MeV using regorous numerical methods. The evaluated results are presented together with the associated uncertainties and correlation matrix. They indicate that this energy-averaged neutron total cross section is known to better than 1% over wide energy regions. There are somwewhat larger uncertainties at low energies (e.g., less than or equal to 0.2 MeV), near 8 MeV and above 15 MeV. The present evaluation is compard with values given in ENDF/B-V

  8. Contribution to the study of nuclear structure using neutron total cross-section measurements between 400 and 1200 keV: isolated resonances and intermediate structure; Contribution a l'etude de la structure nucleaire par des mesures de sections efficaces neutroniques entre 400 keV et 1200 keV. Resonances isolees et structure intermediaire

    Energy Technology Data Exchange (ETDEWEB)

    Cabe, J [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1967-06-15

    The neutron total cross sections have been measured over the energy range 400 keV - 1200 keV for fluorine, aluminium, silicon, phosphorus, vanadium, chromium, manganese, iron, nickel, cobalt and lead with an energy spread of 3 keV. The neutrons were produced by the T (p,n) {sup 3}He reaction, the proton beam was supplied by a 2 MeV Van de Graaff. The structure in {sup 56}Fe has been studied in a more detailed way by measuring six angular distributions in the above range and the elastic scattering excitation curves at four angles. The measurements have made it possible to show the existence of the compound nucleus, as well as the presence of an intermediate structure in certain nuclei. (author) [French] Nous avons mesure les sections efficaces totales neutroniques entre 400 keV et 1200 keV du fluor, de l'aluminium, du silicium, du phosphore, du vanadium, du chrome, du manganese, du fer, du nickel, du cobalt et du plomb avec une dispersion en energie de 3 keV. Les neutrons etaient produits a l'aide de la reaction T (p,n) {sup 3}He, les protons etant acceleres par un Van de Graaff 2 MeV. Nous presentons de plus quatre courbes d'excitation de la diffusion elastique des neutrons sur le fer ainsi que six distributions angulaires. Ces mesures ont permis de mettre en evidence un certain nombres de resonances du noyau compose, ainsi que la presence d'une structure intermediaire dans. certains noyaux. (auteur)

  9. Magnetic structures: neutron diffraction studies

    International Nuclear Information System (INIS)

    Bouree-Vigneron, F.

    1990-01-01

    Neutron diffraction is often an unequivocal method for determining magnetic structures. Here we present some typical examples, stressing the sequence through experiments, data analysis, interpretation and modelisation. Two series of compounds are chosen: Tb Ni 2 Ge 2 and RBe 13 (R = Gd, Tb, Dy, Ho, Er). Depending on the nature of the elements, the magnetic structures produced can be commensurate, incommensurate or even show a transition between two such phases as a function of temperature. A model, taking magnetic exchange and anisotropy into account, will be presented in the case of commensurate-incommensurate magnetic transitions in RBe 13

  10. A neutron detector for measurement of total neutron production cross sections

    Energy Technology Data Exchange (ETDEWEB)

    Sekharan, K K; Laumer, H; Kern, B D; Gabbard, F [Kentucky Univ., Lexington (USA). Dept. of Physics and Astronomy

    1976-03-01

    A neutron detector has been constructed and calibrated for the accurate measurement of total neutron production cross sections. The detector consists of a polyethylene sphere of 60 cm diameter in which eight /sup 10/BF/sub 3/ counters have been installed radially. The relative efficiency of this detector has been determined for average neutron energies from 30 keV to 1.5 MeV by counting neutrons from /sup 7/Li(p, n)/sup 7/Be. By adjusting the radial positions of the BF/sub 3/ counters in the polyethylene sphere the efficiency for neutron detection was made nearly constant for this energy range. Measurement of absolute efficiency for the same neutron energy range has been done by counting the neutrons from /sup 51/V(p, n)/sup 51/Cr and /sup 57/Fe(p, n)/sup 57/Co reactions and determining the absolute number of residual nuclei produced during the measurement of neutron yield. Details of absolute efficiency measurements and the use of the detector for determination of neutron production cross sections are given.

  11. A neutron detector for measurement of total neutron production cross sections

    International Nuclear Information System (INIS)

    Sekharan, K.K.; Laumer, H.; Kern, B.D.; Gabbard, F.

    1976-01-01

    A neutron detector has been constructed and calibrated for the accurate measurement of total neutron production cross sections. The detector consists of a polyethylene sphere of 60 cm diameter in which eight 10 BF 3 counters have been installed radially. The relative efficiency of this detector has been determined for average neutron energies from 30 keV to 1.5 MeV by counting neutrons from 7 Li(p, n) 7 Be. By adjusting the radial positions of the BF 3 counters in the polyethylene sphere the efficiency for neutron detection was made nearly constant for this energy range. Measurement of absolute efficiency for the same neutron energy range has been done by counting the neutrons from 51 V(p, n) 51 Cr and 57 Fe(p, n) 57 Co reactions and determining the absolute number of residual nuclei produced during the measurement of neutron yield. Details of absolute efficiency measurements and the use of the detector for determination of neutron production cross sections are given. (Auth.)

  12. The evaluation of neutron total cross section for natural iron and aluminium

    International Nuclear Information System (INIS)

    Liu Shirui; Wang Chunhao; Zhao Defang

    1990-05-01

    The experimental data of total cross section were collected and evaluated for natural iron in the energy region from 1 keV to 20 MeV and for natural aluminium from 4.07 keV to 20 MeV. The evaluated data were recommended in the regions for them. The minimum values of Fe total cross section in the keV region were specially recommended. The resonance structures were briefly discussed for both Fe and Al. To make the evaluation better, all experimental measurements of neutron total cross section relative to Fe and Al were studied. Considering the resonance feature of medium weight nuclides, two criteria for selecting total cross section were presented: 1) the correlation between the precission of total cross section and neutron source; 2) the correlation between the accuracy of total cross section and the resolving power of the neutron spectrometer

  13. Modern techniques of structural neutron diffraction

    International Nuclear Information System (INIS)

    Aksenov, V.L.; )

    1997-01-01

    Modern techniques of neutron diffraction for structural investigations are analyzed. The time-of-flight method and the reverse time-of-flight method are considered briefly. Characteristics of two-crystal and time-of-flight neutron diffractometers are compared. It is pointed that in the future, the great importance will be possessed the development of high-resolution Fourier neutron diffractometers [ru

  14. Neutron reflection effect on total absorption detector method used in SWINPC neutron multiplication experiment for beryllium

    International Nuclear Information System (INIS)

    Tian Dongfeng; Ho Yukun; Yang Fujia

    2001-01-01

    The SWINPC integral experiment on neutron multiplication in bulk beryllium showed that there were marked discrepancies between experimental data and calculated values with the ENDF/B-VI data. The calculated values become higher than experimental ones as the sample thickness increases. Several works had been devoted to find problems existing in the experiment. This paper discusses the neutron reflection effect on the total absorption detector method which was used in the experiment to measure the neutron leakage from samples. One systematic correction is suggested to make the experimental values agree with the calculated ones with the ENDF/B-VI data within experimental errors. (author)

  15. Solving crystal structures from neutron diffraction data

    International Nuclear Information System (INIS)

    Wilson, C.C.

    1987-07-01

    In order to pursue crystal structure determination using neutron diffraction data, and given the wide experience available of solving structures using X-ray data, the codes used in X-ray structural analysis should be adapted to the different requirements of a neutron experiment. Modifications have been made to a direct methods program MITHRIL and to a Patterson methods program PATMET to incorporate into these the features of neutron rather than X-ray diffraction. While to date these modifications have been fairly straightforward and many sophistications remain to be exploited, results obtained from the neutron versions of both programs are promising. (author)

  16. Fast-neutron total and scattering cross sections of niobium

    Energy Technology Data Exchange (ETDEWEB)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-07-01

    Neutron total cross sections of niobium were measured from approx. = 0.7 to 4.5 MeV at intervals of less than or equal to 50 keV with broad resolution. Differential-elastic-scattering cross sections were measured from approx. = 1.5 to 4.0 MeV at intervals of 0.1 to 0.2 MeV and at 10 to 20 scattering angles distributed between approx. = 20 and 160 degrees. Inelastically-scattered neutrons, corresponding to the excitation of levels at: 788 +- 23, 982 +- 17, 1088 +- 27, 1335 +- 35, 1504 +- 30, 1697 +- 19, 1971 +- 22, 2176 +- 28, 2456 +- (.), and 2581 +- (.) keV, were observed. An optical-statistical model, giving a good description of the observables, was deduced from the measured differential-elastic-scattering cross sections. The experimental-results were compared with the respective evaluated quantities given in ENDF/B-V.

  17. Fast-neutron total and scattering cross sections of niobium

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-07-01

    Neutron total cross sections of niobium were measured from approx. = 0.7 to 4.5 MeV at intervals of less than or equal to 50 keV with broad resolution. Differential-elastic-scattering cross sections were measured from approx. = 1.5 to 4.0 MeV at intervals of 0.1 to 0.2 MeV and at 10 to 20 scattering angles distributed between approx. = 20 and 160 degrees. Inelastically-scattered neutrons, corresponding to the excitation of levels at: 788 +- 23, 982 +- 17, 1088 +- 27, 1335 +- 35, 1504 +- 30, 1697 +- 19, 1971 +- 22, 2176 +- 28, 2456 +- (.), and 2581 +- (.) keV, were observed. An optical-statistical model, giving a good description of the observables, was deduced from the measured differential-elastic-scattering cross sections. The experimental-results were compared with the respective evaluated quantities given in ENDF/B-V

  18. Measurement of neutron total cross-sections for {sup nat}Dy at Pohang Neutron Facility

    Energy Technology Data Exchange (ETDEWEB)

    Shin, S. G.; Kye, Y. U.; Shvetsov, Valery; Cho, M. H. [POSTECH, Pohang (Korea, Republic of); Namkung, W.; Cho, M. H. [Pohang Accelerator Laboratory, Pohang (Korea, Republic of); Kim, G. N. [Kyungpook National Univ., Daegu (Korea, Republic of); Lee, M. W. [Dongnam Inst. of radiological and Medical Science, Busan (Korea, Republic of)

    2013-05-15

    There are few measurements for Dy below 100 eV. Moreover, there exist discrepancies among the measurements. In the present work, the total neutron cross-sections for {sup nat}Dy were measured by using the time-of-flight (TOF) method at the Pohang Neutron Facility (PNF). The PNF consists of an electron linac, a water-cooled Ta target, and an 11-m-long TOF path. The characteristics of PNF are described elsewhere. We also briefly discuss the future plan to verify our experimental result. We have measured the total neutron cross-sections of {sup nat}Dy in the neutron energy region from 0.1 eV to 100 eV with the TOF method at the Po hang Neutron Facility. The present result is in good agreement with the previous data and the evaluated data in ENDF/B-VI. We would like to get resonance parameters by using SAMMY or REFIT codes.

  19. Determination of the total neutron cross section using average energy shift method for filtered neutron beam

    Directory of Open Access Journals (Sweden)

    О. О. Gritzay

    2016-12-01

    Full Text Available Development of the technique for determination of the total neutron cross sections from the measurements of sample transmission by filtered neutrons, scattered on hydrogen is described. One of the methods of the transmission determination TH52Cr from the measurements of 52Cr sample, using average energy shift method for filtered neutron beam is presented. Using two methods of the experimental data processing, one of which is presented in this paper (another in [1], there is presented a set of transmissions, obtained for different samples and for different measurement angles. Two methods are fundamentally different; therefore, we can consider the obtained processing results, using these methods as independent. In future, obtained set of transmissions is planned to be used for determination of the parameters E0, Гn and R/ of the resonance 52Cr at the energy of 50 keV.

  20. Pasta structures in neutron stars

    International Nuclear Information System (INIS)

    Gupta, Neha; Shabnam, I.S.; Arumugam, P.

    2011-01-01

    A neutron star (NS) is a stellar remnant, a super-compressed object left over when stars with a mass between 1.4 and about 3 times the mass of our Sun exhaust their nuclear fuel and collapse inwards. The result of such an implosion is a condensed sphere of matter about 10 km across. The outer layer of the of NS, with density less than the nuclear saturation density, represent different challenges and observational opportunities like thermal evolution, X-ray burst, glitches and the very important core-crust transition region. At this density, nucleons are correlated at short distances by attractive strong interactions, they are anti-correlated at large distances because of the Coulomb repulsion. Competition among short- and long-range interactions (i.e., frustration) leads to the development of complex and exotic nuclear shapes, such as sphere, bubbles, rods, slabs and tubes. The term 'pasta phases' has been coined to describe these complex structures. In this work the nuclear pasta phases using different mean-field models along with a droplet model has been studied

  1. Amino acids analysis by total neutron cross-sections determinations: part V

    International Nuclear Information System (INIS)

    Voi, Dante L.; Ferreira, Francisco de O.; Rocha, Helio F. da

    2013-01-01

    Total neutron cross-sections of twenty essential and non-essential amino acids to human were determined using crystal spectrometer installed on the Argonauta reactor of IEN (Instituto de Engenharia Nuclear (CNEN-RJ) and compared with data generated by parceling and grouping methodologies developed at this institution. For each amino acid was calculated the respective neutron cross-section by molecular structure, conformation and chemistry analysis. The results obtained for eighteen of twenty amino acids confirm the specifications and product formulations indicated by manufactures. These initial results allow to build a neutron cross-sections database as part of quality control of the amino supplied to hospitals for production of nutriments for parenteral or enteral formulations used in critical patients dependent on artificial feed, and for application in future studies of structure and dynamics for more complex molecules, including proteins, enzymes, fatty acids, membranes, organelles and other cell components. (author)

  2. Neutron star structure from QCD

    CERN Document Server

    Fraga, Eduardo S; Vuorinen, Aleksi

    2016-01-01

    In this review article, we argue that our current understanding of the thermodynamic properties of cold QCD matter, originating from first principles calculations at high and low densities, can be used to efficiently constrain the macroscopic properties of neutron stars. In particular, we demonstrate that combining state-of-the-art results from Chiral Effective Theory and perturbative QCD with the current bounds on neutron star masses, the Equation of State of neutron star matter can be obtained to an accuracy better than 30% at all densities.

  3. Total body neutron activation analysis of calcium: calibration and normalisation

    Energy Technology Data Exchange (ETDEWEB)

    Kennedy, N S.J.; Eastell, R; Ferrington, C M; Simpson, J D; Strong, J A [Western General Hospital, Edinburgh (UK); Smith, M A; Tothill, P [Royal Infirmary, Edinburgh (UK)

    1982-05-01

    An irradiation system has been designed, using a neutron beam from a cyclotron, which optimises the uniformity of activation of calcium. Induced activity is measured in a scanning, shadow-shield whole-body counter. Calibration has been effected and reproducibility assessed with three different types of phantom. Corrections were derived for variations in body height, depth and fat thickness. The coefficient of variation for repeated measurements of an anthropomorphic phantom was 1.8% for an absorbed dose equivalent of 13 mSv (1.3 rem). Measurements of total body calcium in 40 normal adults were used to derive normalisation factors which predict the normal calcium in a subject of given size and age. The coefficient of variation of normalised calcium was 6.2% in men and 6.6% in women, with the demonstration of an annual loss of 1.5% after the menopause. The narrow range should make single measurements useful for diagnostic purposes.

  4. Modified model of neutron resonance widths distribution. Results of total gamma-widths approximation

    International Nuclear Information System (INIS)

    Sukhovoj, A.M.; Khitrov, V.A.

    2011-01-01

    Functional dependences of probability to observe given Γ n 0 value and algorithms for determination of the most probable magnitudes of the modified model of resonance parameter distributions were used for analysis of the experimental data on the total radiative widths of neutron resonances. As in the case of neutron widths, precise description of the Γ γ spectra requires a superposition of three and more probability distributions for squares of the random normally distributed values with different nonzero average and nonunit dispersion. This result confirms the preliminary conclusion obtained earlier at analysis of Γ n 0 that practically in all 56 tested sets of total gamma widths there are several groups noticeably differing from each other by the structure of their wave functions. In addition, it was determined that radiative widths are much more sensitive than the neutron ones to resonance wave functions structure. Analysis of early obtained neutron reduced widths distribution parameters for 157 resonance sets in the mass region of nuclei 35 ≤ A ≤ 249 was also performed. It was shown that the experimental values of widths can correspond with high probability to superposition of several expected independent distributions with their nonzero mean values and nonunit dispersion

  5. Neutron star structure: Theory, observation, and speculation

    International Nuclear Information System (INIS)

    Pandharipande, V.R.; Pines, D.; Smith, R.A.

    1976-01-01

    The broad physical aspects of the neutron-neutron interaction in dense matter are reviewed, and an examination is made of the extent to which the equation of state of neutron star matter is influenced by phase transitions which have been proposed for the high-density regime. The dependence of the maximum neutron star mass and the stellar structure on the neutron-neutron interaction is studied through calculations of the equation of state of neutron matter based on four different models for this interaction: the Reid (R) and Bethe-Johnson (BJ) models, a tensor-interaction (TI) model which assumes that the attraction between nucleons comes from the higher order contribution of the pion-exchange tensor interaction, and a mean field (MF) model which assumes that all the attraction between nucleons is due to the exchange of an effective scalar meson. It is shown that the harder equations of state which result from the BJ, TI, and MF models give rise to significant modifications in the structure of neutron stars; heavy neutron stars (approximately-greater-than1 M/sub sun/) have both larger radii and thicker crusts than were predicted using the R model.These stars are used as a basis for comparing theory with observation for the mass and structure of neutron stars such as the Crab and Vela pulsars, and the compact X-ray sources Her X-1 and Vela X-1. We find that both theory and observation tend to favor an equation of state that is stiff in the region of 10 14 --10 15 g cm -3 and that a neutron star such as Her X-1 (Mapprox.1.3 M/sub sun/) has a radius of the order of 15 km with a crust thickness of order 5 km. Based on starquake theory, it is concluded that the Crab pulsar could have a mass as large as 1.3 M/sub sun/, with a critical strain angle approx.10 -3 , comparable to that suggested for Her X-1. The possibility of solid-core neutron stars and some of their observational consequences is discussed

  6. Structure and texture investigations by neutron diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Vratislav, S [Ceske Vysoke Uceni Technicke, Prague (Czechoslovakia). Fakulta Jaderna a Fysikalne Inzenyrska

    1982-01-01

    Analysis of the KSN-2 neutron diffractometer parameters helped improve the KSN-2 resolution to 7.5x10/sup -3/. Structure analysis of compounds with elementary cell volume down to 5 nm/sup 3/ can now be performed. Resolution analysis of the neutron powder diffractometer and its conclusions are described, results of the structure determination of zeolites and the magnetic structure determination of perovskites are given. The three-dimensional distribution function and its use in calculating the elastic modulus of aluminium sheets are mentioned.

  7. Structure of neutron-rich nuclei

    International Nuclear Information System (INIS)

    Nazarewicz, W.

    2000-01-01

    Complete text of publication follows. The uncharted regions of the (N,Z) plane contain information that can answer many questions of fundamental importance for science: How many protons and neutrons can be clustered together by the strong interaction to form a bound nucleus? What are the proton and neutron magic numbers of the exotic nuclei? What are the properties of very short-lived exotic nuclei with extreme neutron-to-proton ratios? What is the effective nucleon-nucleon interaction in a nucleus that has a very large neutron excess? Nuclear life far from stability is different from that around the stability line; the promised access to completely new combinations of proton and neutron numbers offers prospects for new structural phenomena. The main objective of this talk is to discuss some of the challenges and opportunities of research with exotic nuclei. The covered topics will include: Theoretical challenges; Skins and halos in heavy nuclei; Shape coexistence in exotic nuclei; Beta-decays of neutron-rich nuclei. (author)

  8. Mass number dependence of total neutron cross section; a discussion based on the semi-classical optical model

    International Nuclear Information System (INIS)

    Angeli, Istvan

    1990-01-01

    The dependence of total neutron cross section on mass number can be calculated by the black nucleus formula, according to the optical model. The fine structure of mass number dependence is studied, and a correction factor formula is given on the basis of a semi-classical optical model. Yielding results in good agreement with experimental data. In addition to the mass number dependence, the neutron-energy dependence can also be calculated using this model. (K.A.)

  9. Total Analysis System for Ship Structural Strength

    OpenAIRE

    Takuya, Yoneya; Hiroyuki, Kobayashi; Abdul M., Rahim; Yoshimichi, Sasaki; Masaki, Irisawa; Technical Investigation and Information Department, Research Center; Technical Investigation and Information Department, Research Center; Singapore Office; Technical Investigation and Information Department, Research Center; Technical Investigation and Information Department, Research Center

    2001-01-01

    This paper outlines a total analysis system for ship hull structures, which integrates a wide variety of analysis functions to realise practical applications of rational methods for assessing ship structural strength. It is based on direct calculation of wave-induced loads as well as three-dimensional structural analysis of an entire-ship or hold structure. Three major analysis functions of the total system are ship motion and wave load analysis, ship structural analysis and statistical analy...

  10. A recent investigation of neutron total cross section of zirconium in the wavelength range (0.1-1.25) Ao

    International Nuclear Information System (INIS)

    Abu El-Ela, M.A.

    1996-01-01

    The neutron total cross section of zirconium has been investigated in the neutron wavelength range (0.1 -1.52) A o by using slow neutron time of flight spectrometer, installed in front of the horizontal channel No.6 of the ETRR-1 reactor (2MW). The results have showed that the neutrons with short wavelength (0.1 - 0.76) A o cannot interact with the crystal structure while it can interact with the free bound atom to give the value (6.2 +0.1) barns for the potential scattering cross section or (the scattering length = 6.2 fermi)). The present measured value is in good agreement with the international published values by different technique. The neutrons with longer wavelength (0.76 - 1.52) A o have showed dependence of the total cross section on the neutron wavelength. Such dependence between the total cross section and the neutron wavelength can not be observed in the reported previous measurements, which can be attributed to the limited number of the measured values. 4 figs

  11. Symmetry structure in neutron deficient xenon nuclei

    International Nuclear Information System (INIS)

    Govil, I. M.

    1998-01-01

    The paper describes the measurements of the lifetimes of the excited states in the ground state band of the Neutron deficient Xe nuclei ( 122,124 Xe) by recoil Distance Method (RDM). The lifetimes of the 2 + state in 122 Xe agrees with the RDM measurements but for 124 Xe it does not agree the RDM measurements but agrees with the earlier Coulomb-excitation experiment. The experimental results are compared with the existing theories to understand the changes in the symmetry structure of the Xe-nuclei as the Neutron number decreases from N=76( 130 Xe) to N=64( 118 Xe)

  12. Symmetry structure in neutron deficient xenon nuclei

    Science.gov (United States)

    Govil, I. M.

    1998-12-01

    The paper describes the measurements of the lifetimes of the excited states in the ground state band of the Neutron deficient Xe nuclei (122,124Xe) by recoil Distance Method (RDM). The lifetimes of the 2+ state in 122Xe agrees with the RDM measurements but for 124Xe it does not agree the RDM measurements but agrees with the earlier Coulomb-excitation experiment. The experimental results are compared with the existing theories to understand the changes in the symmetry structure of the Xe-nuclei as the Neutron number decreases from N=76(130Xe) to N=64(118Xe).

  13. Structure of neutron-rich nuclei

    International Nuclear Information System (INIS)

    Nazarewicz, W.; Oak Ridge National Lab., TN; Warsaw Univ.

    1997-11-01

    One of the frontiers of today's nuclear science is the ''journey to the limits'': of atomic charge and nuclear mass, of neutron-to-proton ratio, and of angular momentum. The new data on exotic nuclei are expected to bring qualitatively new information about the fundamental properties of the nucleonic many-body system, the nature of the nuclear interaction, and nucleonic correlations at various energy-distance scales. In this talk, current developments in nuclear structure of neutron-rich nuclei are discussed from a theoretical perspective

  14. Nuclear structure studies via neutron interactions

    International Nuclear Information System (INIS)

    Carlton, R.F.

    1990-03-01

    Research performed consisted of: refinement of previous analysis of high resolution total cross sections for n + 40 Ar in an effort to remove some ambiguities in J π assignments and completion of two papers dealing with this analysis and a comparison theoretical treatment of the associated scattering functions and R-functions; extension of the analysis of neutron total cross section data on 48 Ca to 3.5 MeV in neutron energy and modeling of the results with a dispersive optical model based on parameters from 40 Ca scattering data; attempted improvement of spin and parity assignments for data on 122 Sn and determination of external R-function parameters; development of a graphical interface, coupled with a code for calculation of R-matrix based total cross sections and parameter minimization, for an MS-DOS-based microcomputer. 11 refs., 13 figs

  15. Powder Neutron Diffraction and Magnetic structures

    International Nuclear Information System (INIS)

    Vigneron, F.

    1986-01-01

    The determination of the magnetic structures of materials (ferromagnetic, antiferromagnetic, helimagnetic, .) can be achieved only by neutron diffraction. A general survey of the powder technique is given: 2-axis spectrometer and analysis of the magnetic data. For the REBe/sb13/ intermetallic compounds (RE = Rare Earth), commensurate and/or incommensurate magnetic structures are observed and discussed as a function of RE (Gd, Tb, Dy, Ho, Er)

  16. Neutron scattering studies of modulated magnetic structures

    Energy Technology Data Exchange (ETDEWEB)

    Aagaard Soerensen, Steen

    1999-08-01

    This report describes investigations of the magnetic systems DyFe{sub 4}Al{sub 8} and MnSi by neutron scattering and in the former case also by X-ray magnetic resonant scattering. The report is divided into three parts: An introduction to the technique of neutron scattering with special emphasis on the relation between the scattering cross section and the correlations between the scattering entities of the sample. The theoretical framework of neutron scattering experiments using polarized beam technique is outlined. The second part describes neutron and X-ray scattering investigation of the magnetic structures of DyFe{sub 4}Al{sub 8}. The Fe sublattice of the compound order at 180 K in a cycloidal structure in the basal plane of the bct crystal structure. At 25 K the ordering of the Dy sublattice shows up. By the element specific technique of X-ray resonant magnetic scattering, the basal plane cycloidal structure was also found for the Dy sublattice. The work also includes neutron scattering studies of DyFe{sub 4}Al{sub 8} in magnetic fields up to 5 T applied along a <110> direction. The modulated structure at the Dy sublattice is quenched by a field lower than 1 T, whereas modulation is present at the Fe sublattice even when the 5 T field is applied. In the third part of the report, results from three small angle neutron experiments on MnSi are presented. At ambient pressure, a MnSi is known to form a helical spin density wave at temperature below 29 K. The application of 4.5 kbar pressure intended as hydrostatic decreased the Neel temperature to 25 K and changed the orientation of the modulation vector. To understand this reorientation within the current theoretical framework, anisotropic deformation of the sample crystal must be present. The development of magnetic critical scattering with an isotropic distribution of intensity has been studied at a level of detail higher than that of work found in the literature. Finally the potential of a novel polarization

  17. Neutron diffractometers for structural biology at spallation neutron sources

    Energy Technology Data Exchange (ETDEWEB)

    Schoenborn, B.P.; Pitcher, E. [Los Alamos National Laboratory, NM (United States)

    1994-12-31

    Spallation neutron sources are ideal for diffraction studies of proteins and oriented molecular complexes. With spoliation neutrons and their time dependent wavelength structure, it is easy to electronically select data with an optimal wavelength bandwidth and cover the whole Laue spectrum as time (wavelength) resolved snapshots. This optimized data quality with best peak-to-background ratios and provides adequate spatial and energy resolution to eliminate peak overlaps. The application of this concept will use choppers to select the desired Laue wavelength spectrum and employ focusing optics and large cylindrical {sup 3}He detectors to optimize data collection rates. Such a diffractometer will cover a Laue wavelength range from 1 to 5{Angstrom} with a flight path length of 10m and an energy resolution of 0.25{Angstrom}. Moderator concepts for maximal flux distribution within this energy range will be discussed using calculated flux profiles. Since the energy resolution required for such timed data collection in this super Laue techniques is not very high, the use of a linac only (LAMPF) spoliation target is an exciting possibility with an order of magnitude increase in flux.

  18. Neutron diffractometers for structural biology at spallation neutron sources

    International Nuclear Information System (INIS)

    Schoenborn, B.P.; Pitcher, E.

    1994-01-01

    Spallation neutron sources are ideal for diffraction studies of proteins and oriented molecular complexes. With spoliation neutrons and their time dependent wavelength structure, it is easy to electronically select data with an optimal wavelength bandwidth and cover the whole Laue spectrum as time (wavelength) resolved snapshots. This optimized data quality with best peak-to-background ratios and provides adequate spatial and energy resolution to eliminate peak overlaps. The application of this concept will use choppers to select the desired Laue wavelength spectrum and employ focusing optics and large cylindrical 3 He detectors to optimize data collection rates. Such a diffractometer will cover a Laue wavelength range from 1 to 5 Angstrom with a flight path length of 10m and an energy resolution of 0.25 Angstrom. Moderator concepts for maximal flux distribution within this energy range will be discussed using calculated flux profiles. Since the energy resolution required for such timed data collection in this super Laue techniques is not very high, the use of a linac only (LAMPF) spoliation target is an exciting possibility with an order of magnitude increase in flux

  19. Measurement of the neutron total cross section of sodium

    International Nuclear Information System (INIS)

    Larson, D.C.; Harvey, J.A.; Hill, M.W.

    1976-01-01

    The transmission of neutrons through a sample of pure sodium was measured in the energy range 40 keV to 20 MeV. The measurement points out several areas for improvement in the sodium evaluation for ENDF/B-V, the most important being the broadening of the minimum at 300 keV

  20. The structure of pumice by neutron diffraction

    International Nuclear Information System (INIS)

    Floriano, M.A.; Venezia, A.M.; Deganello, G.; Svensson, E.C.; Root, J.H.

    1994-01-01

    Small-angle neutron scattering (SANS) and wide-angle neutron scattering (WANS) measurements on pumice, an amorphous natural aluminosilicate used as support for metals in the preparation of catalysts, are reported. The SANS spectrum indicates the presence of a broad size distribution of pores and the absence of volume fractality. Surface fractality, however, cannot be ruled out. The structure of pumice, suggested by the pair-correlation function derived from the WANS spectrum and simulated by a random-network structure model, is very similar to that of vitreous silica, consisting mainly of SiO 4- 4 tetrahedra interconnected by bridging O atoms with additional local disorder generated by the replacement, on average, of one in ten Si atoms by aluminium. (orig.)

  1. Expected total counts for the Self-Interrogation Neutron Resonance Densitometry measurements of spent nuclear fuel

    Energy Technology Data Exchange (ETDEWEB)

    Rossa, Riccardo [Belgian nuclear research centre SCK.CEN (Belgium); Universite Libre de Bruxelles (Belgium); Borella, Alessandro; Van der Meer, Klaas [Belgian nuclear research centre SCK.CEN. Boeretang 200, 2400 Mol (Belgium); Labeau, Pierre-Etienne; Pauly, Nicolas [Universite Libre de Bruxelles. Av. F. D. Roosevelt 50, B1050 Brussels (Belgium)

    2015-07-01

    The Self-Interrogation Neutron Resonance Densitometry (SINRD) is a passive neutron technique that aims at a direct quantification of {sup 239}Pu in spent fuel assemblies by measuring the attenuation of the neutron flux in the energy region close to the 0.3 eV resonance of {sup 239}Pu. The {sup 239}Pu mass is estimated by calculating the SINRD signature, that is the ratio between the neutron counts in the fast energy region and around the 0.3 eV resonance region. The SINRD measurement approach in this study consisted in introducing a small neutron detector in the central guide tube of a PWR 17x17 fuel assembly. In order to measure the neutron flux in the energy regions defined in the SINRD signature, different detector types were used. The response of a bare {sup 238}U fission chamber is considered for the determination of the fast neutron flux, while other thermal-epithermal detectors wrapped in neutron absorbers are envisaged to measure the neutron flux around the resonance region. This paper provides an estimation of the total neutron counts that can be achieved with the detector types proposed for the SINRD measurement. In the first section a set of detectors are evaluated in terms of total neutron counts and sensitivity to the {sup 239}Pu content, in order to identify the optimal measurement configuration for each detector type. Then a study is performed to increase the total neutron counts by increasing the detector size. The study shows that the highest total neutron counts are achieved by using either {sup 3}He or {sup 10}B proportional counters because of the high neutron efficiency of these detectors. However, the calculations indicate that the biggest contribution to the measurement uncertainty is due to the measurement of the fast neutron flux. Finally, similar sensitivity to the {sup 239}Pu content is obtained by using the different detector types for the measurement of the neutron flux close to the resonance region. Therefore, the total neutron counts

  2. Structure and stability of warm cores in neutron stars

    Energy Technology Data Exchange (ETDEWEB)

    Ibanez Cabanell, J M [Departamento de Mecanica y Astronomia, Facultad de Matematicas, Burjasot-Valencia (Spain)

    1981-12-01

    Relativistic equations of structure are solved using Lamb's equations of state for warm neutron degenerate matter. The stability of isothermal cores in neutron stars is discussed and also the possible compatibility of the results obtained with experimental evidence is shown.

  3. Nano-structured Fabry–Pérot resonators in neutron optics and tunneling of neutron wave-particles

    International Nuclear Information System (INIS)

    Maaza, M.; Hamidi, D.

    2012-01-01

    Correlated to the quantum mechanics wave-particle duality, the optical analogy between electromagnetic waves and cold neutrons manifests itself through several interference phenomena particularly the so called Frustrated Total Reflection i.e., the tunneling process in Fabry–Pérot nano-structured cavities. Prominent resonant situations offered by this configuration allow the attainment of numerous fundamental investigations and surface-interface studies as well as to devise new kinds of neutron optics devices. This review contribution reports such possibilities in addition to the recently observed peculiar Goos–Hänchen longitudinal shift of neutron wave-particles which was predicted by Sir Isaac Newton as early as 1730.

  4. Proton-neutron interaction and nuclear structure

    International Nuclear Information System (INIS)

    Casten, R.F.

    1986-01-01

    The pervasive role of the proton-neutron interaction in nuclear structure is discussed. Particular emphasis is given to its influence on the onset of collectivity and deformation, on intruder states, and on the evolution of subshell structure. The N/sub p/N/sub n/ scheme is outlined and some applications of it to collective model calculations and to nuclei far off stability are described. The concept of N/sub p/N/sub n/ multiplets is introduced. 32 refs., 20 figs

  5. Experimental and theoretical total neutron scattering cross-section of water confined in silica microspheres

    Energy Technology Data Exchange (ETDEWEB)

    Muhrer, G., E-mail: muhrer@lanl.gov [Los Alamos National Laboratory, Los Alamos, 87545 NM (United States); Hartl, M.; Mocko, M.; Tovesson, F.; Daemen, L. [Los Alamos National Laboratory, Los Alamos, 87545 NM (United States)

    2012-07-21

    In the search for moderator materials encapsulated materials have been discussed, but very little is known regarding the effect of encapsulation on neutron moderation properties. As a first step toward a better understanding, we present the measured total neutron cross-section of water confined in silica microspheres and compare the measured data to the predicted theoretical cross-section.

  6. The total neutron cross sections for 14N and 24Mg

    International Nuclear Information System (INIS)

    Bommer, J.

    This report contains tables of the total neutron cross sections of 14 N and 24 Mg as determined in a recent measurement for neutron energies between 1 and 5.3 MeV. Graphic representations and details on the evaluation of the cross sections are included. (orig.) [de

  7. The total neutron cross-section of Nb at different temperatures for neutrons with energies below 1 eV

    International Nuclear Information System (INIS)

    Adib, M.; Abdel-Kawy, A.; Maayouf, R.M.A.; Fayek, M.; Mostafa, M.; Hamouda, I.

    1981-09-01

    Total neutron cross-section measurements have been performed for natural Nb at liquid nitrogen, room and 425 0 K temperatures in the energy range from 2 MeV - 1 eV. The measurements were performed using two time-of-flight spectrometers installed in front of two of the ET-RR-1 reactor horizontal channels. The neutron diffraction pattern of Nb, at room temperature, was obtained using a double axis crystal spectrometer installed also at the ET-RR-1 reactor. The obtained total neutron cross-sections were analyzed using the single level Breit-Wigner formula. The coherent scattering amplitude was determined from the Bragg reflections observed in the total neutron cross-section of Nb and the analysis of its neutron diffraction pattern. The incoherent and thermal inelastic scattering cross-sections of Nb were determined from the analysis of the total cross-section of Nb beyond the cut-off wavelength. The following results have been obtained: sigmasub(t) = (6.30+-0.20)b; sigmasub(coh) = (6.0+-0.3)b; sigmasub(incoh) = (2.0+-1.0)b; bsub(coh) = (6.91+-0.08)fm

  8. Neutron scattering applications in structural biology: now and the future

    Energy Technology Data Exchange (ETDEWEB)

    Trewhella, J [Los Alamos National Lab., NM (United States)

    1996-05-01

    Neutrons have an important role to play in structural biology. Neutron crystallography, small-angle neutron scattering and inelastic neutron scattering techniques all contribute unique information on biomolecular structures. In particular, solution scattering techniques give critical information on the conformations and dispositions of the components of complex assemblies under a wide variety of relevant conditions. The power of these methods is demonstrated here by studies of protein/DNA complexes, and Ca{sup 2+}-binding proteins complexed with their regulatory targets. In addition, we demonstrate the utility of a new structural approach using neutron resonance scattering. The impact of biological neutron scattering to date has been constrained principally by the available fluxes at neutron sources and the true potential of these approaches will only be realized with the development of new more powerful neutron sources. (author)

  9. Status report and measurement of total cross-sections at the Pohang Neutron Facility

    International Nuclear Information System (INIS)

    Kim, G.N.; Meaze, A.K.M.M.H.; Ahmed, H.

    2004-01-01

    We report the status of the Pohang Neutron Facility which consists of an electron linear accelerator, a water-cooled Ta target, and an 11-m time-of-flight path. It has been equipped with a four-position sample changer controlled remotely by a CAMAC data acquisition system, which allows simultaneous accumulation of the neutron time of flight spectra from 4 different detectors. It is possible to measure the neutron total cross-sections in the neutron energy range from 0.1 eV to 100 eV by using the neutron time of flight method. A 6 LiZnS(Ag) glass scintillator was used as a neutron detector. The neutron flight path from the water-cooled Ta target to the neutron detector was 10.81±0.02 m. The background level was determined by using notch-filters of Co, In, Ta, and Cd sheets. In order to reduce the gamma rays from Bremsstrahlung and those from neutron capture, we employed a neutron-gamma separation system based on their different pulse shapes. The present measurements are in general agreement with the evaluated data in ENDF/B-VI. The resonance parameters were extracted from the transmission data from the SAMMY fitting and compared with the previous ones. (author)

  10. The total kinetic energy release in the fast neutron-induced fission of {sup 232}Th

    Energy Technology Data Exchange (ETDEWEB)

    King, Jonathan; Yanez, Ricardo; Loveland, Walter; Barrett, J. Spencer; Oscar, Breland [Oregon State University, Dept. of Chemistry, Corvallis, OR (United States); Fotiades, Nikolaos; Tovesson, Fredrik; Young Lee, Hye [Los Alamos National Laboratory, Physics Division, Los Alamos, NM (United States)

    2017-12-15

    The post-emission total kinetic energy release (TKE) in the neutron-induced fission of {sup 232}Th was measured (using white spectrum neutrons from LANSCE) for neutron energies from E{sub n} = 3 to 91 MeV. In this energy range the average post-neutron total kinetic energy release decreases from 162.3 ± 0.3 at E{sub n} = 3 MeV to 154.9 ± 0.3 MeV at E{sub n} = 91 MeV. Analysis of the fission mass distributions indicates that the decrease in TKE with increasing neutron energy is a combination of increasing yields of symmetric fission (which has a lower associated TKE) and a decrease in the TKE release in asymmetric fission. (orig.)

  11. Measurements and analysis of the 127I and 129I neutron capture and total cross sections

    International Nuclear Information System (INIS)

    Noguere, G.

    2005-01-01

    Most of the experimental work on the interaction of neutrons with matter has focused on materials important to reactor physics and reactor structures. By comparison, the corresponding data for minor actinides or long-lived fission products are poor. A significant demand has developed for improved neutron cross-section data of these little-studied nuclides due to the surge of interest in the transmutation of nuclear waste. With 400 kg of 129 I produced yearly in the reactors of the EU countries and a very long β - half-life of 1.57 x 10 7 years, iodine requires disposal strategies that will isolate this isotope from the environment for long periods of time. Therefore, 129 I is potentially a key long-lived fission product for transmutation applications, since 129 I transmutes in 130 I after a single neutron capture and decays to 130 Xe with a 12.36 h half-life. Accurate capture cross sections would help to reduce uncertainties in waste management concepts. For that purpose, Time-Of-Flight measurements covering the [0.5 eV-100 keV] energy range have been carried out at the 150 MeV pulsed neutron source GELINA of the Institute for Reference Materials and Measurements (IRMM). Two types of experiments have been performed at the IRMM, namely capture and transmission experiments. They are respectively related to the neutron capture and total cross sections. Since the PbI 2 samples used in this work contain natural and radioactive iodine, extensive measurements of 129 I have been carried out under the same experimental conditions as for the 129 I. The data reduction process was performed with the AGS system, and the resonance parameters were extracted with the SAMMY and REFIT shape analysis codes. In a last step, the parameters have been converted into ENDF-6 format and processed with the NJOY code to produce point-wise and multigroup cross sections, as well as MCNP and ERANOS libraries. (author)

  12. The spin-spin effect in the total neutron cross section of polarized neutrons on polarized 165Ho

    International Nuclear Information System (INIS)

    Fasoli, U.; Galeazzi, G.; Pavan, P.; Toniolo, D.; Zago, G.; Zannoni, R.

    1978-01-01

    The spin-spin effect in the total neutron cross section of polarized neutrons on polarized 165 Ho has been measured in the energy interval 0.4 to 2.5 MeV, in perpendicular geometry. The results are consistent with zero effect. The spin-spin cross section sigmasub(ss) has been theoretically evaluated by a non-adiabatic coupled-channel calculation. From the comparison between the experimental and theoretical results a value Vsub(ss) = 9+-77 keV for the strength of the spin-spin potential has been obtained. Compound-nucleus effects do not seem to be relevant. (Auth.)

  13. Total body-calcium measurements: comparison of two delayed-gamma neutron activation facilities

    International Nuclear Information System (INIS)

    Ma, R.; Ellis, K.J.; Shypailo, R.J.; Pierson, R.N. Jr.

    1999-01-01

    This study compares two independently calibrated delayed-gamma neutron activation (DGNA) facilities, one at the Brookhaven National Laboratory (BNL), Upton, New York, and the other at the Children's Nutrition Research Center (CNRC), Houston, Texas that measure total body calcium (TBCa). A set of BNL phantoms was sent to CNRC for neutron activation analysis, and a set of CNRC phantoms was measured at BNL. Both facilities showed high precision (<2%), and the results were in good agreement, within 5%. (author)

  14. Measurement of total reaction cross sections of exotic neutron rich nuclei

    International Nuclear Information System (INIS)

    Mittig, W.; Chouvel, J.M.; Wen Long, Z.

    1987-01-01

    Total reaction cross-sections of neutron rich nuclei from C to Mg in a thick Si-target have been measured using the detection of the associated γ-rays in a 4Π-geometry. This cross-section strongly increases with neutron excess, indicating an increase of as much as 15% of the reduced strong absorption radius with respect to stable nuclei

  15. The nTOF Total Absorption Calorimeter for neutron capture measurements at CERN

    International Nuclear Information System (INIS)

    Guerrero, C.; Abbondanno, U.; Aerts, G.; Alvarez, H.; Alvarez-Velarde, F.; Andriamonje, S.; Andrzejewski, J.; Assimakopoulos, P.; Audouin, L.; Badurek, G.; Baumann, P.; Becvar, F.; Berthoumieux, E.; Calvino, F.; Calviani, M.; Cano-Ott, D.; Capote, R.; Carrapico, C.; Cennini, P.; Chepel, V.

    2009-01-01

    The n T OF Collaboration has built and commissioned a high-performance detector for (n,γ) measurements called the Total Absorption Calorimeter (TAC). The TAC was especially designed for measuring neutron capture cross-sections of low-mass and/or radioactive samples with the accuracy required for nuclear technology and stellar nucleosynthesis. We present a detailed description of the TAC and discuss its overall performance in terms of energy and time resolution, background discrimination, detection efficiency and neutron sensitivity.

  16. The effect of surface texture on total reflection of neutrons and X-rays from modified interfaces

    DEFF Research Database (Denmark)

    Goldar, A.; Roser, S.J.; Hughes, A.

    2002-01-01

    X-ray and neutron scattering from macroscopically rough surfaces and interfaces is considered and a new method of analysis based on the variation of the shape of the total reflection edge in the reflectivity profile is proposed. It was shown that in the limit that the correlation length and the h......X-ray and neutron scattering from macroscopically rough surfaces and interfaces is considered and a new method of analysis based on the variation of the shape of the total reflection edge in the reflectivity profile is proposed. It was shown that in the limit that the correlation length...... and the height of the surface roughness are larger than the wavelength (at least 100 times bigger) of the incoming beam, the total reflection edge in the reflection profile becomes rounded. This technique allows direct analysis of the variation of the reflectivity pro le in terms of the structure of the surface...

  17. Quantitation of the degree of osteoporosis by measure of total-body calcium employing neutron activation

    International Nuclear Information System (INIS)

    Cohn, S.H.; Zanzi, I.; Vaswani, A.; Wallach, S.; Aloia, J.; Ellis, K.J.

    1975-01-01

    Two techniques for measuring the amount of Ca in the total skeleton were employed: total-body neutron activation analysis (TBNAA) and the determination of the mineral content of a bone of the appendicular skeleton (absorptiometric measurement of the radius, BMC). (U.S.)

  18. Local magnetic structure determination using polarized neutron holography

    International Nuclear Information System (INIS)

    Szakál, Alex; Markó, Márton; Cser, László

    2015-01-01

    A unique and important property of the neutron is that it possesses magnetic moment. This property is widely used for determination of magnetic structure of crystalline samples observing the magnetic components of the diffraction peaks. Investigations of diffraction patterns give information only about the averaged structure of a crystal but for discovering of local spin arrangement around a specific (e.g., impurity) nucleus remains still a challenging problem. Neutron holography is a useful tool to investigate the local structure around a specific nucleus embedded in a crystal lattice. The method has been successfully applied experimentally in several cases using non-magnetic short range interaction of the neutron and the nucleus. A mathematical model of the hologram using interaction between magnetic moment of the atom and the neutron spin for polarized neutron holography is provided. Validity of a polarized neutron holographic experiment is demonstrated by applying the proposed method on model systems

  19. Structure of Light Neutron-rich Nuclei

    International Nuclear Information System (INIS)

    Dlouhy, Zdenek

    2007-01-01

    In this contribution we searched for irregularities in various separation energies in the frame of mass measurement of neutron-rich nuclei at GANIL. On this basis we can summarize that the new doubly magic nuclei are 8 He, 22 O and 24 O. They are characterized by extra stability and, except 24 O, they cannot accept and bind additional neutrons. However, if we add to these nuclei a proton we obtain 9 Li and 25 F which are the core for two-neutron halo nucleus 11 Li and enables that fluorine can bound even 6 more neutrons, respectively. In that aspect the doubly magic nuclei in the neutron-rich region can form the basis either for neutron halo or very neutron-rich nuclei. (Author)

  20. Etude de la diagraphie neutron du granite de Beauvoir. Effet neutron des altérations et de la matrice du granite. Calibration granite. Porosité totale à l'eau et porosité neutron Analysis of the Beauvoir Granite Neutron Log. Neutron Effect of Alterations and of the Granite Matrix. Granite Calibration. Total Water Porosity and Neutron Porosity

    Directory of Open Access Journals (Sweden)

    Galle C.

    2006-11-01

    Full Text Available Cet article rend compte des travaux effectués sur la porosité du granite de Beauvoir (Sondage GPF 1 d'Echassières, Massif Central français. L'objectif de notre étude est de pouvoir obtenir des valeurs représentatives de la saturation en eau (porosité totale à l'eau n du granite de Beauvoir à partir des mesures de porosité neutron PorositéN (diagraphie neutron BRGM sans avoir recours aux mesures sur carottes. Notre démarche est expérimentale et nous avons tenté d'approfondir certains problèmes liés à l'utilisation de la diagraphie neutron dans une roche granitique. Deux facteurs principaux conditionnent la réponse neutron : la concentration en hydrogène de la formation (eau libre et eau de constitution de certains minéraux et la présence d'éléments absorbeurs à forte section de capture comme le gadolinium, le cadmium, le bore, . . . et dans le cas du granite de Beauvoir, le lithium. A partir des mesures de porosité totale à l'eau n sur carottes, des essais de pertes au feu sur poudre qui nous permettent de déterminer la porosité neutron liée à l'eau de constitution PorositéN(OH- et des analyses chimiques avec lesquelles nous évaluons la porosité neutron thermique PorositéN(ox (Programme SNUPAR, Schlumberger liée à la capture neutronique, nous reconstituons la porosité neutron totale PorositéNR du granite de Beauvoir. Pour 7 échantillons caractéristiques du granite de Beauvoir, nous réalisons grâce à ces résultats une nouvelle calibration du taux de comptage neutron initial corrigé du gradient thermique et de l'effet de trou. Grâce à cette opération, il est possible de déterminer, pour les échantillons traités, la porosité neutron du granite avec une calibration granite (PorositéNg et non calcaire (PorositéNc. La connaissance de l'effet neutron de la matrice nous permet enfin d'évaluer la teneur en eau du granite (porosité totale à l'eau et de comparer celle-ci avec la porosité mesurée sur

  1. International seminar on structural investigations on pulsed neutron sources. Proceedings

    International Nuclear Information System (INIS)

    Aksenov, V.L.; Balagurov, A.M.; Taran, Yu.V.

    1993-01-01

    The proceedings of the International seminar on structural investigations using pulsed neutron sources are presented. The seminar is dedicated to the memory of Dr. Yu.M. Ostanevich, a world acknowledged physicist. The problems of structural analysis using pulsed neutron source at the IBR-2 reactor are discussed

  2. ISINN-3. Neutron spectroscopy, nuclear structure, related topics

    International Nuclear Information System (INIS)

    1995-01-01

    The proceedings contain the materials presented at the Third International Seminar on Neutron-Nucleus Interactions (ISINN-3) dealing with the problems of neutron spectroscopy, nuclear structure and related topics. The Seminar took place in Dubna on April 26-28, 1995. Over 100 scientists from Belgium, Bulgaria, Czech Republic, Germany, Japan, Latvia, Mexico, Poland, Slovakia, Ukraine, USA and from more than 10 Russian research institutes took part in the Seminar. The Seminar is dedicated to the memory of the founder of the Neutron Physics Laboratory of JINR, the famous soviet scientist Professor Fedor L. Shapiro, whose 80th anniversary is being observed. The main problems discussed are the following: fundamental interactions and symmetries in neutron-induced reactions, fundamental properties of the neutron, properties of excited nuclei after neutron capture and some other ones. Special emphasis is laid upon γ decay and neutron induced nuclear fission as well as upon the methodical aspects of new experiments

  3. Nuclear-structure aspects of theoretical neutron physics

    International Nuclear Information System (INIS)

    Soloviev, V.G.

    1976-01-01

    The structure of neutron resonances is studied on the basis of the semimicroscopic nuclear theory. Few-quasiparticle components of the wave functions of neutron resonances are calculated which determine the neutron and radiational strength functions. It is stated that it is necessary to clarify the role of their many-quasiparticle components. The structure of neutron resonances is studied within the framework of the general approach based on the operator form of the wave functions. The role of three-quasiparticle components in the wave functions of neutron resonances is studied and the cases of validity of the valence neutron model are pointed out. It is shown that the experimental information about the structure of neutron resonances is limited to few-quasiparticle components which are of 10 -3 -10 -6 part of the normalization of their wave functions. To study the structure of neutron resonances it is necessary to find the values of many-quasiparticle components of the wave functions. The ways of experimental finding of these components based on the study of γ-transitions between highly excited states are discussed. The fragmentation of single-particle states in deformed nuclei is studied within the framework of the model based on the quasiparticle--phonon interactions. The S-, p-, and α-wave neutron strength functions are determined

  4. Neutron total, scattering and inelastic gamma-ray cross sections of yttrium at few MeV energies

    International Nuclear Information System (INIS)

    Budtz-Joergensen, C.; Guenther, P.; Smith, A.; Whalen, J.; McMurray, W.R.; Renan, M.J.; Heerden, I.J. van

    1984-01-01

    Neutron total, scattering and (n; n', γ) cross sections of elemental yttrium ( 89 Y) were measured in the few-MeV region. The neutron total-cross-section measurements were made with broad resolutions from approx.=0.5 to 4.2 MeV in steps of < or approx.0.1 MeV. Neutron elastic- and inelastic-scattering cross sections were measured from approx.=1.5 to 4.0 MeV, at incident-neutron energy intervals of approx.=50 keV and at ten or more scattering angles distributed between 20 and 160 degrees using neutron detection. Inelastic-scattering cross sections were also determined using the (n; n', γ) reaction at incident energies from 1.6 to 3.8 MeV at intervals of 0.1 MeV. Gamma-rays and/or inelastically-scattered neutrons were observed corresponding to the excitation of levels at: 909.0+-0.5, 1,507.4+-0.3, 1,744.5+-0.3, 2,222.6+-0.5, 2,530+-0.8, 2,566.4+-1.0, 2,622.5+-1.0, 2,871.9+-1.5, 2,880.6+-2.0, 3,067.0+-2.0, 3,107.0+-2.0, 3,140.0+-2.0, 3,410.0+-2.0, 3,450.0+-2.0, 3,504.0+-1.5, 3,514.0+-2.0, 3,556.0+-2.0, 3,619.0+-3.0, 3,629.0+-3.0 and 3,715.0+-3.0 keV. The experimental results are discussed in terms of the spherical-optical-statistical, coupled-channels, and core-coupling models, and in the context of previously reported excited-level structure. (orig.)

  5. ISINN-2. Neutron spectroscopy, nuclear structure and related topics

    International Nuclear Information System (INIS)

    1994-01-01

    The proceedings contain the materials presented at the Second International Seminar on Neutron-Nucleus Interactions (ISINN-2) dealing with the problems of neutron spectroscopy, nuclear structure and related topics. The Seminar took place in Dubna on April 26-28, 1994. Over 120 scientists from Belgium, Bulgaria, Czech Republic, Germany, Holland, Italy, Japan, Latvia, Mexico, Poland, Slovakia, Slovenia, Ukraine, US and about 10 Russian research institutes took part in the Seminar. The main problems discussed are the following: P-odd and P-even angular correlation and T-reversal invariance in neutron reactions, nuclear structure investigations by neutron capture, the mechanism of neutron reactions, nuclear fission processes, as well as neutron data for nuclear astrophysics

  6. Neutron diffraction studies of thin film multilayer structures

    International Nuclear Information System (INIS)

    Majkrzak, C.F.

    1985-01-01

    The application of neutron diffraction methods to the study of the microscopic chemical and magnetic structures of thin film multilayers is reviewed. Multilayer diffraction phenomena are described in general and in particular for the case in which one of the materials of a bilayer is ferromagnetic and the neutron beam polarized. Recent neutron diffraction measurements performed on some interesting multilayer systems are discussed. 70 refs., 5 figs

  7. AHTR Mechanical, Structural, and Neutronic Preconceptual Design

    Energy Technology Data Exchange (ETDEWEB)

    Varma, V.K.; Holcomb, D.E.; Peretz, F.J.; Bradley, E.C.; Ilas, D.; Qualls, A.L.; Zaharia, N.M.

    2012-09-15

    This report provides an overview of the mechanical, structural, and neutronic aspects of the Advanced High Temperature Reactor (AHTR) design concept. The AHTR is a design concept for a large output Fluoride salt cooled High-temperature Reactor (FHR) that is being developed to enable evaluation of the technology hurdles remaining to be overcome prior to FHRs becoming an option for commercial reactor deployment. This report documents the incremental AHTR design maturation performed over the past year and is focused on advancing the design concept to a level of a functional, self-consistent system. The reactor concept development remains at a preconceptual level of maturity. While the overall appearance of an AHTR design is anticipated to be similar to the current concept, optimized dimensions will differ from those presented here. The AHTR employs plate type coated particle fuel assemblies with rapid, off-line refueling. Neutronic analysis of the core has confirmed the viability of a 6-month two-batch cycle with 9 wt. % enriched uranium fuel. Refueling is intended to be performed automatically under visual guidance using dedicated robotic manipulators. The report includes a preconceptual design of the manipulators, the fuel transfer system, and the used fuel storage system. The present design intent is for used fuel to be stored inside of containment for at least six months and then transferred to local dry wells for intermediate term, on-site storage. The mechanical and structural concept development effort has included an emphasis on transportation and constructability to minimize construction costs and schedule. The design intent is that all components be factory fabricated into rail transportable modules that are assembled into subsystems at an on-site workshop prior to being lifted into position using a heavy-lift crane in an open-top style construction. While detailed accident identification and response sequence analysis has yet to be performed, the design

  8. AHTR Mechanical, Structural, And Neutronic Preconceptual Design

    Energy Technology Data Exchange (ETDEWEB)

    Varma, Venugopal Koikal [ORNL; Holcomb, David Eugene [ORNL; Peretz, Fred J [ORNL; Bradley, Eric Craig [ORNL; Ilas, Dan [ORNL; Qualls, A L [ORNL; Zaharia, Nathaniel M [ORNL

    2012-10-01

    This report provides an overview of the mechanical, structural, and neutronic aspects of the Advanced High Temperature Reactor (AHTR) design concept. The AHTR is a design concept for a large output Fluoride salt cooled High-temperature Reactor (FHR) that is being developed to enable evaluation of the technology hurdles remaining to be overcome prior to FHRs becoming a commercial reactor class. This report documents the incremental AHTR design maturation performed over the past year and is focused on advancing the design concept to a level of a functional, self-consistent system. The AHTR employs plate type coated particle fuel assemblies with rapid, off-line refueling. Neutronic analysis of the core has confirmed the viability of a 6-month 2-batch cycle with 9 weight-percent enriched uranium fuel. Refueling is intended to be performed automatically under visual guidance using dedicated robotic manipulators. The present design intent is for used fuel to be stored inside of containment for at least 6 months and then transferred to local dry wells for intermediate term, on-site storage. The mechanical and structural concept development effort has included an emphasis on transportation and constructability to minimize construction costs and schedule. The design intent is that all components be factory fabricated into rail transportable modules that are assembled into subsystems at an on-site workshop prior to being lifted into position using a heavy-lift crane in an open-top style construction. While detailed accident identification and response sequence analysis has yet to be performed, the design concept incorporates multiple levels of radioactive material containment including fully passive responses to all identified design basis or non-very-low frequency beyond design basis accidents. Key building design elements include: 1) below grade siting to minimize vulnerability to aircraft impact, 2) multiple natural circulation decay heat rejection chimneys, 3) seismic

  9. Structural science using single crystal and pulse neutron scattering

    International Nuclear Information System (INIS)

    Noda, Yukio; Kimura, Hiroyuki; Watanabe, Masashi; Ishikawa, Yoshihisa; Tamura, Itaru; Arai, Masatoshi; Takahashi, Miwako; Ohshima, Ken-ichi; Abe, Hiroshi; Kamiyama, Takashi

    2008-01-01

    The application to single crystal neutron structural analysis is overviewed. Special attention is paid to the pulse neutron method, which will be available soon under J-PARC project in Japan. New proposal and preliminary experiment using Sirius at KENS are described. (author)

  10. The Spin Structure of the Neutron

    Energy Technology Data Exchange (ETDEWEB)

    Churchwell, S

    2003-12-18

    A description of SLAC experiment E154, a precision measurement of the neutron's longitudinal spin structure function g{sub 1}{sup n}, is presented. Deep inelastic electron scattering was used to measure the structure function in the kinematic range 0.014 < x < 0.7, and 1 < Q{sup 2} < 17 GeV{sup 2}. A measurement of the transverse spin structure function g{sub 2}{sup n} was also made, but with significantly lower statistical precision. Electrons with an average polarization of 82 {+-} 2% and an energy of 48.3 GeV were scattered off polarized {sup 3}He nuclei having an average polarization of 38%. Two independent magnetic spectrometers set at scattering angles of 2.75{sup o} and 5.5{sup o} were used to acquire about 100 million events during a two month run in late 1995. The data were analyzed to yield the integral over the measured region: {integral}{sub 0.014}{sup 0.7} g{sub 1}{sup n}(x)dx = -0.036 {+-} 0.004(stat) {+-} 0.005(syst), which is several standard deviations below the Ellis-Jaffe sum rule predictions. When these data were combined with the proton g{sub 1}{sup p} structure function data from the SMC and E143 experiments, the Bjorken sum rule over the measured x range was found to be within 10% of the predicted value. The integral of the g{sub 2}{sup n} data, dominated by the statistical uncertainty, was found to be {integral}{sub 0.014}{sup 0.7} g{sub 2}{sup n}(x)dx = 0.19 {+-} 0.17(stat) {+-} 0.02(syst), in agreement with the Burkhardt-Cottingham sum rule prediction. The g{sub 1}{sup n} structure function data at low x were found to be inconsistent with the traditional asymptotic forms, bringing into question the methods used in the past.

  11. Neutron stars structure in the context of massive gravity

    Energy Technology Data Exchange (ETDEWEB)

    Hendi, S.H.; Bordbar, G.H.; Panah, B. Eslam; Panahiyan, S., E-mail: hendi@shirazu.ac.ir, E-mail: ghbordbar@shirazu.ac.ir, E-mail: behzad.eslampanah@gmail.com, E-mail: sh.panahiyan@gmail.com [Physics Department and Biruni Observatory, College of Sciences, Shiraz University, Shiraz 71454 (Iran, Islamic Republic of)

    2017-07-01

    Motivated by the recent interests in spin−2 massive gravitons, we study the structure of neutron star in the context of massive gravity. The modifications of TOV equation in the presence of massive gravity are explored in 4 and higher dimensions. Next, by considering the modern equation of state for the neutron star matter (which is extracted by the lowest order constrained variational (LOCV) method with the AV18 potential), different physical properties of the neutron star (such as Le Chatelier's principle, stability and energy conditions) are investigated. It is shown that consideration of the massive gravity has specific contributions into the structure of neutron star and introduces new prescriptions for the massive astrophysical objects. The mass-radius relation is examined and the effects of massive gravity on the Schwarzschild radius, average density, compactness, gravitational redshift and dynamical stability are studied. Finally, a relation between mass and radius of neutron star versus the Planck mass is extracted.

  12. Neutron stars structure in the context of massive gravity

    Science.gov (United States)

    Hendi, S. H.; Bordbar, G. H.; Eslam Panah, B.; Panahiyan, S.

    2017-07-01

    Motivated by the recent interests in spin-2 massive gravitons, we study the structure of neutron star in the context of massive gravity. The modifications of TOV equation in the presence of massive gravity are explored in 4 and higher dimensions. Next, by considering the modern equation of state for the neutron star matter (which is extracted by the lowest order constrained variational (LOCV) method with the AV18 potential), different physical properties of the neutron star (such as Le Chatelier's principle, stability and energy conditions) are investigated. It is shown that consideration of the massive gravity has specific contributions into the structure of neutron star and introduces new prescriptions for the massive astrophysical objects. The mass-radius relation is examined and the effects of massive gravity on the Schwarzschild radius, average density, compactness, gravitational redshift and dynamical stability are studied. Finally, a relation between mass and radius of neutron star versus the Planck mass is extracted.

  13. Neutron stars structure in the context of massive gravity

    International Nuclear Information System (INIS)

    Hendi, S.H.; Bordbar, G.H.; Panah, B. Eslam; Panahiyan, S.

    2017-01-01

    Motivated by the recent interests in spin−2 massive gravitons, we study the structure of neutron star in the context of massive gravity. The modifications of TOV equation in the presence of massive gravity are explored in 4 and higher dimensions. Next, by considering the modern equation of state for the neutron star matter (which is extracted by the lowest order constrained variational (LOCV) method with the AV18 potential), different physical properties of the neutron star (such as Le Chatelier's principle, stability and energy conditions) are investigated. It is shown that consideration of the massive gravity has specific contributions into the structure of neutron star and introduces new prescriptions for the massive astrophysical objects. The mass-radius relation is examined and the effects of massive gravity on the Schwarzschild radius, average density, compactness, gravitational redshift and dynamical stability are studied. Finally, a relation between mass and radius of neutron star versus the Planck mass is extracted.

  14. Neutron total and scattering cross sections of 6Li in the few MeV region

    International Nuclear Information System (INIS)

    Smith, A.; Guenther, P.; Whalen, J.

    1980-02-01

    Neutron total cross sections of 6 Li are measured from approx. 0.5 to approx. 4.8 MeV at intervals of approx. 10 scattering angles and at incident-neutron intervals of approx.< 100 keV. Neutron differential inelastic-scattering cross sections are measured in the incident-energy range 3.5 to 4.0 MeV. The experimental results are extended to lower energies using measured neutron total cross sections recently reported elsewhere by the authors. The composite experimental data (total cross sections from 0.1 to 4.8 MeV and scattering cross sections from 0.22 to 4.0 MeV) are interpreted in terms of a simple two-level R-matrix model which describes the observed cross sections and implies the reaction cross section in unobserved channels; notably the (n;α)t reaction (Q = 4.783 MeV). The experimental and calculational results are compared with previously reported results as summarized in the ENDF/B-V evaluated nuclear data file

  15. Fast-neutron total and scattering cross sections of sup 58 Ni and nuclear models

    Energy Technology Data Exchange (ETDEWEB)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F. (Argonne National Lab., IL (United States)); Chiba, S. (Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment)

    1991-07-01

    The neutron total cross sections of {sup 58}Ni were measured from {approx} 1 to > 10 MeV using white-source techniques. Differential neutron elastic-scattering cross sections were measured from {approx} 4.5 to 10 MeV at {approx} 0.5 MeV intervals with {ge} 75 differential values per distribution. Differential neutron inelastic-scattering cross sections were measured, corresponding to fourteen levels with excitations up to 4.8 MeV. The measured results, combined with relevant values available in the literature, were interpreted in terms of optical-statistical and coupled-channels model using both vibrational and rotational coupling schemes. The physical implications of the experimental results nd their interpretation are discussed in the contexts of optical-statistical, dispersive-optical, and coupled-channels models. 61 refs.

  16. In vivo measurement of total body carbon using 238Pu/Be neutron sources

    International Nuclear Information System (INIS)

    Sutcliffe, J.F.; Mitra, S.; Hill, G.L.

    1990-01-01

    Total body carbon has been measured by in vivo neutron activation analysis (IVNAA) in 278 surgical gastroenterological patients and 29 normal volunteers. This is based on the inelastic scattering reaction { 12 C(n,n') 12 C*} for neutrons with energy above 4.8MeV, producing 4.43 MeV gamma rays. Since only part of the body is scanned, total body carbon is estimated as the ratio of the gamma ray emission from carbon to the emission from hydrogen, using hydrogen as the internal standard. The precision of the estimate is ±1.6kg for a whole body dose of 0.3mSv. There is a significant difference between the estimates of total body water from IVNAA measurements of carbon and nitrogen and measurements of body water in these subjects by tritium dilution (t=3.1, p < 0.005). (author)

  17. Proceedings of the 182nd basic science seminar (The workshop on neutron structural biology ) 'New frontiers of structural biology advanced by solution scattering'

    International Nuclear Information System (INIS)

    Fujiwara, Satoru

    2001-03-01

    182nd advanced science seminar (the workshop on neutron structural biology) was held in February 9-10, 2000 at Tokai. Thirty-six participants from universities, research institutes, and private companies took part in the workshop, and total of 24 lectures were given. This proceedings collects abstracts, the figures and tables, which the speakers used in their lectures. The proceedings contains two reviews from the point of view of x-ray and neutron scatterings, and six subjects (21 papers) including neutron and x-ray scattering in the era of structure genomics, structural changes detected with solution scattering, a new way in structural biology opened by neutron crystallography and neutron scattering, x-ray sources and detectors, simulation and solution scattering, and neutron sources and detectors. (Kazumata, Y.)

  18. Proceedings of the 182nd basic science seminar (The workshop on neutron structural biology ) 'New frontiers of structural biology advanced by solution scattering'

    Energy Technology Data Exchange (ETDEWEB)

    Fujiwara, Satoru (ed.) [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    2001-03-01

    182nd advanced science seminar (the workshop on neutron structural biology) was held in February 9-10, 2000 at Tokai. Thirty-six participants from universities, research institutes, and private companies took part in the workshop, and total of 24 lectures were given. This proceedings collects abstracts, the figures and tables, which the speakers used in their lectures. The proceedings contains two reviews from the point of view of x-ray and neutron scatterings, and six subjects (21 papers) including neutron and x-ray scattering in the era of structure genomics, structural changes detected with solution scattering, a new way in structural biology opened by neutron crystallography and neutron scattering, x-ray sources and detectors, simulation and solution scattering, and neutron sources and detectors. (Kazumata, Y.)

  19. Total neutron cross sections of berkelium-249 and californium-249 below 100 eV

    International Nuclear Information System (INIS)

    Benjamin, R.W.; Harvey, J.A.; Hill, N.W.; Pandey, M.S.; Carlton, R.F.

    1979-01-01

    The neutron total cross sections of 249 Bk and 249 Cf have been measured from 0.03 to 100 eV using the Oak Ridge Electron Linear Accelerator (ORELA) as a source of pulsed neutrons. The 1.6 mm dia. cylindrical transmission samples contained initially up to 5.3 mg of 98% 249 Bk and 2% 249 Cf: 4.5 years later, when the final measurements were made, the composition of the samples had become 2.5% 249 Bk, 96.9% 249 Cf, and 0.6% 245 Cm. Samples were cooled with liquid nitrogen to reduce Doppler broadening. Thirty-nine resonances were identified in 249 Bk and analyzed using a single-level Breit-Wigner formalism. Fifty-five resonances were identified in 249 Cf and analyzed using an R-matrix multilevel formalism. Fifty-five resonances were identified in 249 Cf and analyzed using an R-matrix multilevel formalism. The resonance parameters obtained have been used to determine the average level spacings and the s-wave neutron and fission strength functions. Where possible, bound-level parameters were derived to fit the thermal neutron total cross section data

  20. Total cross section measurement of radioactive isotopes with a thin beam neutron spectrometer

    International Nuclear Information System (INIS)

    Razbudej, V.F.; Vertebnyj, V.P.; Padun, G.S.; Muravitskij, A.V.

    1975-01-01

    The method for measuring the neutron total cross sections of radioactive isotopes by a time-of-flight spectrometer with a narrow (0.17 mm in diameter) beam of thermal neutrons is described. The distinguishing feature of this method is the use of capillary samples with a small amount of substance (0.05-1.0 mg). The energy range is 0.01-0.3 eV. The total cross sections of irradiated samples of sub(153)Eu and sub(151)Eu are measured. From them are obtained the cross sections of sub(152)Eu (Tsub(1/2)=12.4 g) and of sub(154)E (Tsub(1/2)=8.6 yr); they equal 11400+-1400 and 1530+-190 barn at E=0.0253 eV. The cross section of the sub(152)Eu absorption for the thermal spectrum (T=333 K) is determined by the activation method; it is 8900+-1200 barn

  1. Crystallographic structures of absorbates and neutron diffraction

    International Nuclear Information System (INIS)

    Marti, C.; Thorel, P.

    1975-01-01

    The advantage of neutron diffraction is that it is possible to work at any pressure and therefore to study an adsorbant-adsorbate couple within a wide pressure and temperature range and at thermodynamic equilibrium. Nitrogen adsorbed on graphite and CF 4 adsorbed on graphite were measured [fr

  2. Structural elements for fast-neutron reactors

    International Nuclear Information System (INIS)

    Blin, J.C.; Sainfort, Gerard; Silvent, Alain; Silvestres, Georges.

    1974-01-01

    These elements are characterized in that they are obtained from a nickel-alloy and at least a material M, selected from the group comprising iron and silicon, in proportions, by weight, such that irradiation by fast neutrons leads to the generation of Ni 3 -M with no noticeable swelling of said elements. This can be applied to fuel assembly cladding [fr

  3. A Determination of the Neutron Spin Structure Function

    Energy Technology Data Exchange (ETDEWEB)

    Hughes, Emlyn W

    2003-08-18

    The authors report the results of the experiment E142 which measured the spin dependent structure function of the neutron, g{sub 1}{sup n}(x, Q{sup 2}). The experiment was carried out at the Stanford Linear Accelerator Center by measuring an asymmetry in the deep inelastic scattering of polarized electrons from a polarized {sup 3}He target, at electron energies from 19 to 26 GeV. The structure function was determined over the kinematic range 0.03 < BJorken x < 0.6 and 1.0 < Q{sup 2} < 5.5 (GeV/c){sup 2}. An evaluation of the integral {integral}{sub 0}{sup 1} g{sub 1}{sup n}(x,Q{sup 2})dx at fixed Q{sup 2} = 2 (GeV/c){sup 2} yields the final result {Lambda}{sub 1}{sup n} = -0.032 {+-} 0.006 (stat.) {+-} 0.009 (syst.). This result, when combined with the integral of the proton spin structure function measured in other experiments, confirms the fundamental Bjorken sum rule with O({alpha}{sub s}{sup 3}) corrections to within one standard deviation. This is a major success for perturbative Quantum Chromodynamics. Some ancillary results include the findings that the Ellis-Jaffe sum rule for the neutron is violated at the 2 {sigma} level, and that the total contribution of the quarks to the helicity of the nucleon is 0.36 {+-} 0.10. The strange sea polarization is estimated to be small and negative, {Delta}s = -0.07 {+-} 0.04.

  4. Measurement of total body chlorine by prompt gamma in vivo neutron activation analysis

    International Nuclear Information System (INIS)

    Beddoe, A.H.; Streat, S.J.; Hill, G.L.

    1987-01-01

    A method of measuring total body chlorine (TBCl) by prompt gamma in vivo neutron activation analysis is described depending on the same NaI(Tl) spectra used for determinations of total body nitrogen. Ratios of chlorine to hydrogen are derived and TBCl determined using a model of body composition depending on measured body weight, total body water (by tritium dilution) and protein (6.25 x nitrogen) as well as estimated body minerals and glycogen. The precision of the method based on scanning an anthropomorphic phantom is approximately 9% (SD), for a patient dose equivalent of less than 0.30 mSv. Spectra collected from 67 normal volunteers (32 male, 35 female) yielded mean values of TBCl of 72 +- 19 (SD) g in males and 53.6 +- 15 g in females, in broad agreement with values reported by workers using delayed gamma methods. Results are presented for two human cadavers analysed by neutron activation and conventional chemical analysis; the ratios of TBCl (neutron activation) to TBCl (chemical) were 0.980 +- 0.028 (SEM) and 0.91 +- 0.09. It is suggested that an improvement in precision will be achieved by increasing the scanning time (thereby increasing the radiation dose equivalent) and by adding two more detectors. (author)

  5. Pinpointing chiral structures with front-back polarized neutron reflectometry.

    Science.gov (United States)

    O'Donovan, K V; Borchers, J A; Majkrzak, C F; Hellwig, O; Fullerton, E E

    2002-02-11

    A new development in spin-polarized neutron reflectometry enables us to more fully characterize the nucleation and growth of buried domain walls in layered magnetic materials. We applied this technique to a thin-film exchange-spring magnet. After first measuring the reflectivity with the neutrons striking the front, we measure with the neutrons striking the back. Simultaneous fits are sensitive to the presence of spiral spin structures. The technique reveals previously unresolved features of field-dependent domain walls in exchange-spring systems and has sufficient generality to apply to a variety of magnetic systems.

  6. Future prospects of superfine structure of neutron resonance levels

    International Nuclear Information System (INIS)

    Ideno, Kazumi

    1996-01-01

    Neutron resonance spectra appear simply and regularly in the light of superfine structure (SFS). It is found that the relative shifts (i.e. the relative distances) between the SFSs for groups of nuclei have definite values and are closely interrelated to the symmetry properties of the compound systems if we treat neutron zero energy as a common reference point. An origin of the SFSs and its possible application to an evaluation of nuclear data are discussed. (author)

  7. High resolution neutron total and capture cross-sections in separated isotopes of copper (6365Cu)

    International Nuclear Information System (INIS)

    Pandey, M.S.

    1975-01-01

    High resolution neutron total and capture cross section measurements have been performed on separated isotopes of copper ( 63 65 Cu). Measurements for capture cross section were made from about 1 keV to a few hundreds of keV. The total cross section measurements were made in the energy interval of approximately 10 keV to 150 keV. The resulting capture data have been analyzed by a generalized least square peak fitting computer code in the energy interval of 2.5 keV to 50 keV. Photon strengths are determined using the data up to approximately 250 keV. The resulting total cross section data have been analyzed by area-analysis on the transmission values and by R-matrix multilevel code on cross section values. Average s- and p-wave level spacing and s- and p-wave strength function values are determined. From the resonance parameters thus obtained, by the analysis, statistical distribution is studied for s- and p-wave level spacings and reduced neutron widths. A comparison has been made for adjacent level spacings with the theoretical predictions of level repulsion (of same J/sup π/) by Wigner considering levels with various spin states separately for s-wave resonances where confident spin assignment has been possible. Reduced neutron widths are compared with the Porter-Thomas distribution. Optical model formulated by Feshbach, Porter and Weiskopf describes the neutron-nucleus interaction. A comparison has been made between experimentally determined values of the s- and p-wave strength functions and that obtainable from optical model calculations, thereby determining the appropriate optical model parameters. The experimental arrangement, pertinent theoretical discussion, and the processes of data reduction and the analyses along with the comparison of the previously reported results with the present work are presented in detail

  8. Normal levels of total body sodium and chlorine by neutron activation analysis

    International Nuclear Information System (INIS)

    Kennedy, N.S.J.; Eastell, R.; Smith, M.A.; Tothill, P.

    1983-01-01

    In vivo neutron activation analysis was used to measure total body sodium and chlorine in 18 male and 18 female normal adults. Corrections for body size were developed. Normalisation factors were derived which enable the prediction of the normal levels of sodium and chlorine in a subject. The coefficient of variation of normalised sodium was 5.9% in men and 6.9% in women, and of normalised chlorine 9.3% in men and 5.5% in women. In the range examined (40-70 years) no significant age dependence was observed for either element. Total body sodium was correlated with total body chlorine and total body calcium. Sodium excess, defined as the amount of body sodium in excess of that associated with chlorine, also correlated well with total body calcium. In females there was a mean annual loss of sodium excess of 1.2% after the menopause, similar to the loss of calcium. (author)

  9. In vivo Prompt Gamma Neutron Activation Analysis Facility for Total Body Nitrogen and Cd

    International Nuclear Information System (INIS)

    Munive, Marco; Revilla, Angel; Solis, Jose L.

    2007-01-01

    A Prompt Gamma Neutron Activation Analysis (PGNAA) system has been designed and constructed to measure the total body nitrogen and Cd for in vivo studies. An aqueous solution of KNO 3 was used as phantom for system calibration. The facility has been used to monitor total body nitrogen (TBN) of mice and found that is related to their diet. Some mice swallowed diluted water with Cl 2 Cd, and the presence of Cd was detected in the animals. The minimum Cd concentration that the system can detect was 20 ppm

  10. Total energy calculations for structural phase transformations

    International Nuclear Information System (INIS)

    Ye, Y.Y.; Chan, C.T.; Ho, K.M.; Harmon, B.N.

    1990-01-01

    The structural integrity and physical properties of crystalline solids are frequently limited or enhanced by the occurrence of phase transformations. Martensitic transformations involve the collective displacement of atoms from one ordered state to another. Modern methods to determine the microscopic electronic changes as the atoms move are now accurate enough to evaluate the very small energy differences involved. Extensive first principles calculations for the prototypical martensitic transformation from body-centered cubic (bcc) to closepacked 9R structure in sodium metal are described. The minimum energy coordinate or configuration path between the bcc and 9R structures is determined as well as paths to other competing close-packed structures. The energy barriers and important anharmonic interactions are identified and general conclusions drawn. The calculational methods used to solve the Schrodinger equation include pseudopotentials, fast Fourier transforms, efficient matrix diagnonalization, and supercells with many atoms

  11. Slow neutron total cross-section, transmission and reflection calculation for poly- and mono-NaCl and PbF{sub 2} crystals

    Energy Technology Data Exchange (ETDEWEB)

    Mansy, Muhammad S., E-mail: mmansy88@asrt.sci.eg [Reactor Physics Department, Nuclear Research Centre, Atomic Energy Authority, Cairo (Egypt); Radioactive Waste Management Unit, Hot Labs Centre, Atomic Energy Authority, Cairo (Egypt); Adib, M.; Habib, N. [Reactor Physics Department, Nuclear Research Centre, Atomic Energy Authority, Cairo (Egypt); Bashter, I.I. [Physics Department, Faculty of Science, Zagazig University (Egypt); Morcos, H.N.; El-Mesiry, M.S. [Reactor Physics Department, Nuclear Research Centre, Atomic Energy Authority, Cairo (Egypt)

    2016-10-01

    Highlights: • Slow neutron cross-section calculation for poly- and mono-crystalline materials. • Monochromatic features of PbF{sub 2} and NaCl mono-crystals. • Characterization of poly- and mono-crystal filters used in neutron diffraction. • Computer code developed calculates neutron cross-section, transmission & reflection. - Abstract: A detailed study about the calculation of total neutron cross-section, transmission and reflection from crystalline materials was performed. The developed computer code is approved to be sufficient for the required calculations, also an excellent agreement has been shown when comparing the code results with the other calculated and measured values. The optimal monochromator and filter parameters were discussed in terms of crystal orientation, mosaic spread, and thickness. Calculations show that 30 cm thick of PbF{sub 2} poly-crystal is an excellent cold neutron filter producing neutron wavelengths longer than 0.66 nm needed for the investigation of magnetic structure experiments. While mono-crystal filter PbF{sub 2} cut along its (1 1 1), having mosaic spread (η = 0.5°) and thickness 10 cm can only transmit thermal neutrons of the desired wavelengths and suppress epithermal and γ-rays forming unwanted background, when it is cooled to liquid nitrogen temperature. NaCl (2 0 0) and PbF{sub 2} (1 1 1) monochromator crystals having mosaic spread (η = 0.5°) and thickness 10 mm shows high neutron reflectivity for neutron wavelengths (λ = 0.114 nm and λ = 0.43 nm) when they used as a thermal and cold neutron monochromators respectively with very low contamination from higher order reflections.

  12. Fast-neutron total and scattering cross sections of elemental palladium

    Energy Technology Data Exchange (ETDEWEB)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-06-01

    Neutron total cross sections of palladium are measured from approx. = 0.6 to 4.5 MeV with resolutions of approx. = 30 to 70 keV at intervals of less than or equal to 50 keV. Differential neutron elastic- and inelastic-scattering cross sections are measured from 1.4 to 3.85 MeV at intervals of 50 to 100 keV and at 10 to 20 scattering angles distributed between approx. = 20 and 160/sup 0/. The experimental results are compared with respective quantities given in ENDF/B-V and used to deduce an optical potential that provides a good description of the measured values.

  13. Fast-neutron total and scattering cross sections of elemental palladium

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-06-01

    Neutron total cross sections of palladium are measured from approx. = 0.6 to 4.5 MeV with resolutions of approx. = 30 to 70 keV at intervals of less than or equal to 50 keV. Differential neutron elastic- and inelastic-scattering cross sections are measured from 1.4 to 3.85 MeV at intervals of 50 to 100 keV and at 10 to 20 scattering angles distributed between approx. = 20 and 160 0 . The experimental results are compared with respective quantities given in ENDF/B-V and used to deduce an optical potential that provides a good description of the measured values

  14. One-speed neutron transport in spheres with totally absorbing cores

    International Nuclear Information System (INIS)

    Sjoestrand, N.G.

    1988-01-01

    Stationary and time-dependent transport of neutrons of one speed has been studied in spheres with totally absorbing cores. For stationary, critical reactors the number of secondaries per collision has been calculated numerically for various inner and outer radii. In the time-dependent case, the decay constant has been calculated for spherical shells of different inner radii and thicknesses. For a fixed ratio between shell thickness and inner radius, the curve of the decay constant versus shell thickness crosses the Corngold limit in the same way as the curve for a homogeneous sphere. When the ratio goes to zero the curve approaches that for an infinite slab. The behaviour is discussed in view of a new result from collision theory, viz. that the following condition must be fulfilled for a body at the point where the decay constant curve crosses the Corngold limit: the average exit distance of the neutrons is equal to the mean free path for scattering

  15. Fast-neutron total and scattering cross sections of 103Rh

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-07-01

    Fast-neutron total cross sections of 103 Rh are measured with 30 to 50 keV resolutions from 0.7 to 4.5 MeV. Differential elastic- and inelastic-scattering cross sections are measured from 1.45 to 3.85 MeV. Scattered-neutron groups corresponding to excited levels at 334 +- 13, 536 +- 7, 648 +- 25, 796 +- 20, 864 +- 22, 1120 +- 22, 1279 +- 50, 1481 +- 27, 1683 +- 39, 1840 +- 79, 1991 +- 71 and 2050 (tentative) keV are observed. An optical-statistical model is derived from the elastic-scattering results. The experimental values are compared with comparable quantities given in the ENDF/B-V evaluation

  16. Measurement of the polarized neutron---polarized 3He total cross section

    International Nuclear Information System (INIS)

    Keith, C.D.; Gould, C.R.; Haase, D.G.; Seely, M.L.; Huffman, P.R.; Roberson, N.R.; Tornow, W.; Wilburn, W.S.

    1995-01-01

    The first measurements of polarized neutron--polarized 3 He scattering in the few MeV energy region are reported. The total cross section difference Δσ T for transversely polarized target and beam has been measured for neutron energies between 1.9 and 7.5 MeV. Comparison is made to predictions of Δσ T using various descriptions of the 4 He continuum. A brute-force polarized target of solid 3 He has been developed for these measurements. The target is 4.3x10 22 atoms/cm 2 thick and is polarized to 38% at 7 Telsa and 12 mK. copyright 1995 American Institute of Physics

  17. Neutron stars

    International Nuclear Information System (INIS)

    Irvine, J.M.

    1978-01-01

    The subject is covered in chapters entitled: introduction (resume of stellar evolution, gross characteristics of neutron stars); pulsars (pulsar characteristics, pulsars as neutron stars); neutron star temperatures (neutron star cooling, superfluidity and superconductivity in neutron stars); the exterior of neutron stars (the magnetosphere, the neutron star 'atmosphere', pulses); neutron star structure; neutron star equations of state. (U.K.)

  18. Slow neutron total cross-section, transmission and reflection calculation for poly- and mono-NaCl and PbF2 crystals

    Science.gov (United States)

    Mansy, Muhammad S.; Adib, M.; Habib, N.; Bashter, I. I.; Morcos, H. N.; El-Mesiry, M. S.

    2016-10-01

    A detailed study about the calculation of total neutron cross-section, transmission and reflection from crystalline materials was performed. The developed computer code is approved to be sufficient for the required calculations, also an excellent agreement has been shown when comparing the code results with the other calculated and measured values. The optimal monochromator and filter parameters were discussed in terms of crystal orientation, mosaic spread, and thickness. Calculations show that 30 cm thick of PbF2 poly-crystal is an excellent cold neutron filter producing neutron wavelengths longer than 0.66 nm needed for the investigation of magnetic structure experiments. While mono-crystal filter PbF2 cut along its (1 1 1), having mosaic spread (η = 0.5°) and thickness 10 cm can only transmit thermal neutrons of the desired wavelengths and suppress epithermal and γ-rays forming unwanted background, when it is cooled to liquid nitrogen temperature. NaCl (2 0 0) and PbF2 (1 1 1) monochromator crystals having mosaic spread (η = 0.5°) and thickness 10 mm shows high neutron reflectivity for neutron wavelengths (λ = 0.114 nm and λ = 0.43 nm) when they used as a thermal and cold neutron monochromators respectively with very low contamination from higher order reflections.

  19. Measurements of the total neutron cross-sections of poly- and mono-germanium crystals at neutron energies below 1 eV

    International Nuclear Information System (INIS)

    Maayouf, R.M.A.; Abdel-Kawy, A.; Abbas, Y.; Habib, N.; Adib, M.; Hamouda, I.

    1983-12-01

    Total neutron cross-section measurements have been performed for poly and mono-germanium crystals in the energy range from 2 meV-1eV. The measurements were performed using two TOF and a double axis crystal spectrometer installed at the ET-RR-1 reactor. The obtained neutron cross-sections were analyzed using the single level Breit-Wigner formula. The coherent scattering amplitude was determined from the Bragg reflections observed in the total neutron cross-section of Ge and the analysis of its neutron diffraction pattern. The incoherent and thermal diffuse scattering cross-sections of Ge were estimated from the analysis of the total cross-section data obtained for Ge mono-crystal

  20. On the Fifth Force and the Structure of Neutron Star

    Directory of Open Access Journals (Sweden)

    D. J. Song

    1994-06-01

    Full Text Available In the framework of Thomas-Fermi equation, we have examined the properties of neutron star by assuming the existence of a new intermediate force which is composition dependent. We have found that the structure, size and mass of neutron star are affected by the strength and range of this new force. In the ultrarelativistic limit, we have also confirmed that Chandrasekhar mass, Mch-(1-α^(- 3/2 (m_pl^3/m^2 is determined by the constants of classical physical laws, which take part in the selfgravitating processes on neutron star as well as the constant of hypothetical fifth force. In the experimental limits of the fifth force, the changes of size and mass of a neutron star are in the order of strength parameter α.

  1. Structure and thermal evolution of spinning-down neutron stars

    International Nuclear Information System (INIS)

    Negreiros, R.; Schramm, S.; Weber, F.

    2011-01-01

    In this paper we address the effects of spin-down on the cooling of neutron stars. During its evolution, stellar composition and structure might be substantially altered, as a result of spin-down and the consequent density increase. Since the timescale of cooling might be comparable to to that of the spin-evolution, the modifications to the structure/composition might have important effects on the thermal evolution of the object. We show that the direct Urca process might be delayed or supressed, when spin-down is taken into account. This leads to neutron stars with slow cooling, as opposed to enhanced cooling as would be the case if a "froze-in" structure and composition were considered. In conclusion we demonstrate that the inclusion of spin-down effects on the cooling of neutron stars have far-reaching implications for the interpretation of pulsars. (author)

  2. SASSI, Total and Differential Elastic and Inelastic Neutron Cross-Sections by Hauser-Feshbach

    International Nuclear Information System (INIS)

    Benzi, V.; Fabbri, F.; Zuffi, L.

    2001-01-01

    1 - Nature of physical problem solved: Neutron total and differential elastic and inelastic cross-section evaluation by means of the statistical model of Hauser-Feshbach (1) as modified by D. Goldman (2) (3). The Goldman modification includes the effect of spin-orbit coupling on transmission coefficients. 2 - Method of solution: For numerical integration the Fox-Goodwins method is used. 3 - Restrictions on the complexity of the problem: Angular momentum I less than or equal to 50. Number of excited levels less than or equal to 30

  3. Total body calcium by neutron activation analysis. Reference data for children

    International Nuclear Information System (INIS)

    Ellis, K.J.; Shypailo, R.J.

    2001-01-01

    There is a paucity of data on the chemical composition of the human body during growth. Total body calcium (TBCa) has been reported for only one male child, aged 41/2 yr. TBCa values for 25 children and 27 young women using in vivo neutron activation analysis have been obtained. TBCa results were lower than those reported for the one male cadaver, as well as the estimates derived for the 'Reference Man' model. It was concluded that the reference values for TBCa may need to be adjusted to appropriately describe skeletal mineralization of contemporary children. (author)

  4. The use of Total Body In Vivo Neutron Activation Analysis (TBIVNAA) in balance studies in rodents

    International Nuclear Information System (INIS)

    Smith, D.A.; Lindsay, R.L.; Anderson, J.

    1976-01-01

    In the investigation of animals subject to alteration in diet or other metabolic experiments, the measurements of change in body calcium, phosphorus, sodium and nitrogen are of considerable interest. However, conventional balance studies are tedious and subject to both random and cumulative error, necessitating as they do accurate estimates of dietary intake and faecal and urinary output. The object of the present study was to determine the usefulness of total body in vivo neutron activation analysis, used at the beginning and end of the experimental period, as an alternative to conventional balance techniques. (orig.) [de

  5. Fast-neutron total and elastic-scattering cross sections of elemental indium

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-11-01

    Broad-resolution neutron total cross sections of elemental indium were measured from 0.8 to 4.5 MeV. Differential-elastic-scattering cross sections were measured from approx. = 1.5 to 3.8 MeV at intervals of approx. = 50 to 200 keV and at scattering angles in the range 20 to 160 degrees. The experimental results are interpreted in terms of the optical-statistical model and are compared with respective values given in ENDF/B-V

  6. Development Of A Method For Measurement Of Total Neutron Cross Sections Based On The Neutron Transmission Method Using A He-3 Counter On Filtered Neutron Beams At Dalat Research Reactor

    International Nuclear Information System (INIS)

    Tran Tuan Anh; Dang Lanh; Nguyen Canh Hai; Nguyen Xuan Hai; Pham Kien; Nguyen Thuy Nham; Pham Ngoc Son; Ho Huu Thang

    2007-01-01

    Determination of total neutron cross sections and average resonance parameters in the energy range from tens keV to hundreds keV is important for fast reactors calculations and designs because this energy range gives the most output of all neutron induced reactions in the spectrum of fast reactors. Besides, the total neutron cross section measurement is also one of the methods for determination of s, p and d-wave neutron strength functions. The purpose of this project is to develop a method for measurement of total neutron cross sections based on the neutron transmission technique using a He-3 counter. The average total neutron cross sections of 238 U were obtained from neutron transmission measurements on filtered neutron beams of 55 keV and 144 keV at the horizontal channel No.4 of the Dalat research reactor. The present results have been compared with the previous measurements, and the evaluated data from ENDF/B-6.8 library. (author)

  7. Molecular dynamical and structural studies for the bakelite by neutron cross section measurements

    International Nuclear Information System (INIS)

    Voi, D.L.

    1992-05-01

    Neutron reaction cross sections were determined by transmission and scattering measurements, to study the dynamics and molecular structure of calcined bakelites. Total cross sections were determined, with a deviation smaller than 5%, from the literature values, by neutron transmission method and a specially devised approximation. These cross sections were then correlated with data obtained with infra-red spectroscopy, elemental analysis and other techniques to get the probable molecular formulae of bakelite. Double differential scattering cross sections, scattering law values and frequency distributions were determined with 15% error using the neutron inelastic scattering method. The frequency distributions as well as the overall results from all experimental techniques used in this work allowed to suggest a structural model like polycyclic hydrocarbons, for calcined bakelite at 800 0 C. (author)

  8. Characterization of Crystallographic Structures Using Bragg-Edge Neutron Imaging at the Spallation Neutron Source

    Directory of Open Access Journals (Sweden)

    Gian Song

    2017-12-01

    Full Text Available Over the past decade, wavelength-dependent neutron radiography, also known as Bragg-edge imaging, has been employed as a non-destructive bulk characterization method due to its sensitivity to coherent elastic neutron scattering that is associated with crystalline structures. Several analysis approaches have been developed to quantitatively determine crystalline orientation, lattice strain, and phase distribution. In this study, we report a systematic investigation of the crystal structures of metallic materials (such as selected textureless powder samples and additively manufactured (AM Inconel 718 samples, using Bragg-edge imaging at the Oak Ridge National Laboratory (ORNL Spallation Neutron Source (SNS. Firstly, we have implemented a phenomenological Gaussian-based fitting in a Python-based computer called iBeatles. Secondly, we have developed a model-based approach to analyze Bragg-edge transmission spectra, which allows quantitative determination of the crystallographic attributes. Moreover, neutron diffraction measurements were carried out to validate the Bragg-edge analytical methods. These results demonstrate that the microstructural complexity (in this case, texture plays a key role in determining the crystallographic parameters (lattice constant or interplanar spacing, which implies that the Bragg-edge image analysis methods must be carefully selected based on the material structures.

  9. Neutron and X-ray diffraction from modulated structures

    International Nuclear Information System (INIS)

    Harris, P.

    1994-07-01

    This thesis describes X-ray and neutron scattering experiments performed on two examples of modulated structures. After an introduction to the subject of modulated structures, the thesis is divided in three parts. A single crystal elastic neutron scattering experiment between 4.2 and 115 Κ has been performed and four-circle X-ray data have been collected at 8 Κ for the monoclinic low-temperature phase of the layered perovskite PAMC. The results from the neutron scattering experiment indicate that magnetoelastic effects influence the ordering of the crystal. The X-ray experiments have made it possible to determine the crystal structure in the low-temperature phase. The superspace group is P2 1 /b(β-30)Os, with β = 1/3. A small-angle neutron scattering experiment has been performed on the magnetic structure of manganese silicide. When a magnetic field is applied, the modulation vectors turn towards the field direction, showing domain growth and diverging peak widths as they approach the field direction. Phase 'A' is established to have the modulation vectors directed perpendicular to the field direction. Cooling in zero field shows increasing peak widths at low temperatures, indicating a lock-in transition below the lowest reached temperature. To be able to analyse the data of the magnetic order in MnSi, and analytical calculation of the three dimensional resolution function for a small-angle neutron scattering spectrometer has been performed. The calculation is done by application of a combination of phase space analysis and Gaussian approximations for the neutron distribution as well as for the transmission functions of the different apertures. A finite mosaic spread of the crystal and finite correlation widths of the Bragg reflections have been included in the cross section. (au) (3 tabs., 48 ills., 100 refs.)

  10. Evaluation of the total gamma-ray production cross-sections for nonelastic interaction of fast neutrons with iron nuclei

    International Nuclear Information System (INIS)

    Savin, M.V.; Nefedov, Yu.Ya; Livke, A.V.; Zvenigorodskij, A.G.

    2001-01-01

    Experimental data on the total gamma-ray production cross-sections for inelastic interaction of fast neutrons with iron nuclei were analysed. The total gamma-ray production cross-sections, grouped according to E γ , were evaluated in the neutron energy range 0.5-19 MeV. The statistical spline approximation method was used to evaluate the experimental data. Evaluated data stored in the ENDF, JENDL, BROND, and other libraries on gamma-ray production spectra and cross-sections for inelastic interaction of fast neutrons with iron nuclei, were analysed. (author)

  11. Influence of cross-section structure on unfolded neutron spectra

    International Nuclear Information System (INIS)

    Ertek, C.; Vlasov, M.F.; Cross, B.; Smith, P.M.

    1979-01-01

    The influence of cross-section structure on neutron spectra unfolded by multiple foil activation technique, SAND-II case, has been studied. For three reactions with evident structure in neutron cross-section above threshold: 27Al(n,α)24Na, 31P(n,p)31Si and 32S(n,p)32P, two remarkably different sets of evaluated data were selected from the available evaluations; one set of data was ''smooth'', the structure having been averaged over by a smooth curve; the other set was ''sharp'' with structure given in detail. These data were used in unfolding procedure together with other reactions, the same in both cases (as well as input spectra and measured reaction rates). It was found that during unfolding calculations less iteration steps were needed to unfold the neutron flux spectrum with the set of ''sharp'' data. In case of ''smooth'' data it was difficult to obtain an agreement between measured and calculated activity values even by increasing the number of iteration steps. Contrary to expectations, considerable deformation of unfolded neutron flux spectrum has been observed in the case of the ''smooth'' data set. (author)

  12. Failure of Stadard Optical Models to Reproduce Neutron Total Cross Section Difference in the W Isotopes

    Energy Technology Data Exchange (ETDEWEB)

    Anderson, J D; Bauer, R W; Dietrich, F S; Grimes, S M; Finlay, R W; Abfalterer, W P; Bateman, F B; Haight, R C; Morgan, G L; Bauge, E; Delaroche, J P; Romain, P

    2001-11-01

    Recently cross section differences among the isotopes{sup 182,184,186}W have been measured as part of a study of total cross sections in the 5-560 MeV energy range. These measurements show oscillations up to 150 mb between 5 and 100 MeV. Spherical and deformed phenomenological optical potentials with typical radial and isospin dependences show very small oscillations, in disagreement with the data. In a simple Ramsauer model, this discrepancy can be traced to a cancellation between radial and isospin effects. Understanding this problem requires a more detailed model that incorporates a realistic description of the neutron and proton density distributions. This has been done with results of Hartree-Fock-Bogolyubov calculations using the Gogny force, together with a microscopic folding model employing a modification of the JLM potential as an effective interaction. This treatment yields a satisfactory interpretation of the observed total cross section differences.

  13. Structural Investigations using a position sensitive Neutron Detector

    International Nuclear Information System (INIS)

    Fruchart, D.; Anne, M.; Wolfers, P.; Lartigue, C.; Roudaut, E.

    1986-01-01

    In the accurate determination of the location of lights atoms such as hydrogen in a metal matrix, several types of difficulty may be encountered. Experimentally, neutron diffraction is the most convenient method for such a structure determination. The use of Position Sensitive Detectors is discussed, and selected examples illustrate the advantages and drawbacks of this type of instrument. Judging from present results, significant improvements in recording technique, data collection and reduction, and structure refinement may be obtained in the near future

  14. Preliminary results of total kinetic energy modelling for neutron-induced fission

    International Nuclear Information System (INIS)

    Visan, I.; Giubega, G.; Tudora, A.

    2015-01-01

    The total kinetic energy as a function of fission fragments mass TKE(A) is an important quantity entering in prompt emission calculations. The experimentally distributions of TKE(A) are referring to a limited number of fission systems and incident energies. In the present paper, a preliminary model for TKE calculation in neutron induced fission system is presented. The range of fission fragments is chosen as in the Point by Point treatment. The model needs as input only mass excesses and deformation parameters taken from available nuclear databases being based on the following approximations: total excitation energy of fully accelerated fission fragments TXE is calculated from energy balance of neutron-induced fission systems as sum of the total excitation energy at scission E*sciss and deformation energy Edef. The deformation energy at scission is given by minimizing the potential energy at the scission configuration. At the scission point, the fission system is described by two spheroidal fragments nearly touching by a pre-scission distance or neck caused by the nuclear forces between fragments. Therefore, the Columbian repulsion depending on neck and, consequently, on the fragments deformation at scission, is essentially in TKE determination. An approximation is made based on the fission modes. For the very symmetric fission, the dominant super long channel is characterized by long distance between fragments leading to low TKE values. Due to magic and double-magic shells closure, the dominant S1 fission mode for pairs with heavy fragment mass AH around 130-134 is characterized by spherical heavy fragment shape and easily deformed light fragment. The nearly spherical shape of the complementary fragments are characterized by minimum distance, and consequently to maximum TKE values. The results obtained for TKE(A) are in good agreement with existing experimental data for many neutron induced fission systems, e.g. ''2''3''3&apos

  15. Monte Carlo efficiency calibration of a neutron generator-based total-body irradiator

    International Nuclear Information System (INIS)

    Shypailo, R.J.; Ellis, K.J.

    2009-01-01

    Many body composition measurement systems are calibrated against a single-sized reference phantom. Prompt-gamma neutron activation (PGNA) provides the only direct measure of total body nitrogen (TBN), an index of the body's lean tissue mass. In PGNA systems, body size influences neutron flux attenuation, induced gamma signal distribution, and counting efficiency. Thus, calibration based on a single-sized phantom could result in inaccurate TBN values. We used Monte Carlo simulations (MCNP-5; Los Alamos National Laboratory) in order to map a system's response to the range of body weights (65-160 kg) and body fat distributions (25-60%) in obese humans. Calibration curves were constructed to derive body-size correction factors relative to a standard reference phantom, providing customized adjustments to account for differences in body habitus of obese adults. The use of MCNP-generated calibration curves should allow for a better estimate of the true changes in lean tissue mass that many occur during intervention programs focused only on weight loss. (author)

  16. NET European Network on Neutron Techniques Standardization for Structural Integrity

    International Nuclear Information System (INIS)

    Youtsos, A.

    2004-01-01

    Improved performance and safety of European energy production systems is essential for providing safe, clean and inexpensive electricity to the citizens of the enlarged EU. The state of the art in assessing internal stresses, micro-structure and defects in welded nuclear components -as well as their evolution due to complex thermo-mechanical loads and irradiation exposure -needs to be improved before relevant structural integrity assessment code requirements can safely become less conservative. This is valid for both experimental characterization techniques and predictive numerical algorithms. In the course of the last two decades neutron methods have proven to be excellent means for providing valuable information required in structural integrity assessment of advanced engineering applications. However, the European industry is hampered from broadly using neutron research due to lack of harmonised and standardized testing methods. 35 European major industrial and research/academic organizations have joined forces, under JRC coordination, to launch the NET European Network on Neutron Techniques Standardization for Structural Integrity in May 2002. The NET collaborative research initiative aims at further development and harmonisation of neutron scattering methods, in support of structural integrity assessment. This is pursued through a number of testing round robin campaigns on neutron diffraction and small angle neutron scattering - SANS and supported by data provided by other more conventional destructive and non-destructive methods, such as X-ray diffraction and deep and surface hole drilling. NET also strives to develop more reliable and harmonized simulation procedures for the prediction of residual stress and damage in steel welded power plant components. This is pursued through a number of computational round robin campaigns based on advanced FEM techniques, and on reliable data obtained by such novel and harmonized experimental methods. The final goal of

  17. Changes in body chemical composition with age measured by total-body neutron activation

    International Nuclear Information System (INIS)

    Cohn, S.H.; Vaswani, A.; Zanzi, I.; Aloia, J.F.; Roginsky, M.S.; Ellis, K.J.

    1976-01-01

    Total-body levels of calcium and phosphorus (reflecting skeletal mass) and total-body levels of potassium (reflecting muscle mass) were measured by neutron activation analysis in 39 men and 40 women ages 30 to 90 yr. In order to intercompare the total body calcium (TBCa) values in a heterogeneous population, such as this, it was necessary to normalize the data for skeletal size. The normalization consisted of dividing the absolute calcium level by the predicted calcium level for each individual matched to a set of critical parameters. The parameter used in the computation of normal values were age, sex, muscle mass, i.e., total body potassium (TBK) and height. For the calcium data of the women, it was necessary to add an age correction factor after the age of 55 yr. The calcium ratio (mean ratio of the predicted to measured TBCa) in men was 1.000 +- 7.8 percent and in women 0.996 +- 7.1 percent. The TBCa of normal males and females can thus be predicted to +-13 percent (at the 90 percent confidence level). An exception to this was found in males (70 to 90 yr) who exhibited a mean calcium ratio greater than 1.13

  18. Fast-neutron capture in structural materials

    International Nuclear Information System (INIS)

    Froehner, F.H.

    1982-01-01

    The discussions of developments in the field of capture data of structural materials since the 1977 Geel meeting were mainly based on the invited paper presented by G. Rohr and on information from the other participants about their own activities. There was not much input about recent work in japan, where the new version JENDL-2 of the Japanese Evaluated Nuclear Data Library has been issued, or on the resonance analysis work on iron and nickel isotopes going on at ORNL. Moreover, the discussion was restricted to the three principal structural material elements Cr, Fe and Ni. Some of the remaining structural materials such as Zr and Mo were covered by the Working Group on Fission Product Nuclides

  19. Determination of Total Arsenic in Seaweed Products by Neutron Activation Analysis

    International Nuclear Information System (INIS)

    Salim, N.; Santoso, M.; Yanuar, A.; Damayanti; Kartawinata, T.G.

    2013-01-01

    Seaweed products are widely consumed as food nowadays. Seaweeds are known to contain arsenic due to their capability to accumulate arsenic from the environment. Arsenic is a known toxic element which naturally occurs in the environment. Ingestion of high levels of arsenic will cause several adverse health effects. Arsenic in food occurs at trace concentrations which require sensitive and selective analysis methods to perform elemental analysis on. Validated neutron activation analysis was used to determine the arsenic contents in seaweed products namely catoni from domestic product and nori from foreign products. The total arsenic concentration in the samples analyzed ranges from 0.79 mg/kg to 30.14 mg/kg with mean concentration 14.39 mg/kg. The estimated exposure to arsenic contributed by the analyzed products is from 0.07% up to 8.54% of the established provisional tolerable daily intake (PTDI) which is still far below the maximum tolerable level. (author)

  20. Determination of Total Arsenic in Seaweed Products by Neutron Activation Analysis

    Directory of Open Access Journals (Sweden)

    N. Salim

    2013-04-01

    Full Text Available Seaweed products are widely consumed as food nowadays. Seaweeds are known to contain arsenic due to their capability to accumulate arsenic from the environment. Arsenic is a known toxic element which naturally occurs in the environment. Ingestion of high levels of arsenic will cause several adverse health effects. Arsenic in food occurs at trace concentrations which require sensitive and selective analysis methods to perform elemental analysis on. Validated neutron activation analysis was used to determine the arsenic contents in seaweed products namely catoni from domestic product and nori from foreign products. The total arsenic concentration in the samples analyzed ranges from 0.79 mg/kg to 30.14 mg/kg with mean concentration 14.39 mg/kg. The estimated exposure to arsenic contributed by the analyzed products is from 0.07% up to 8.54% of the established provisional tolerable daily intake (PTDI which is still far below the maximum tolerable level

  1. Measurement of fluorine total concentration in dental enamel using fast neutron activation

    International Nuclear Information System (INIS)

    Mouadili, A.; Vernais, J.; Isabelle, D.B.

    1988-01-01

    Fluorine which is present in dental enamel, at the level of a few tens to a few hundred ppm, plays an important role in the behaviour of this tissue. Therefore quantitative determination is of interest for particular studies of the dental system. We present a nuclear nondestructive method to determine the total fluorine content in dental enamel by cyclotron-produced fast-neutron activation. The 19 F(n,2n) reaction leads to 18 F which is a β + emitter with a 109.8 min half-life. The irradiated sample activity is measured by detecting in coincidence the annihilation photons. A fluorine standard is used for calibration. The detection limit is of the order of 1 ppm, while the reproducibility is better than 95% [pt

  2. Study of the molecular structure and dynamics of bakelite with neutron cross section measurements

    International Nuclear Information System (INIS)

    Voi, D.L.

    1990-06-01

    The molecular structure and dynamics of calcined bakelite were studied with neutron transmission and scattering cross section measurements. The total cross sections determined were correlated with data obtained with infra-red spectroscopy, elemental analysis and other techniques to get the probable molecular formulae of bakelite. The total cross section determined showed a deviation smaller than 5% from the literature values. The frequency distribution as well as overall experimental results allowed to suggest a structural model like polycyclic hydrocarbons for bakelite calcined at 800 0 C. (F.E.). 65 refs, 31 figs, 5 tabs

  3. Structure of amorphous selenium studied by neutron diffraction

    DEFF Research Database (Denmark)

    Hansen, Flemming Yssing; Knudsen, Torben Steen; Carneiro, K.

    1975-01-01

    Neutron diffraction measurements on amorphous selenium have been performed at 293 and 80 K. Careful analyses of the instrumental corrections were made to avoid systematic errors in the measured structure factor S (kappa) in the wave vector region 0 ? kappa ? 12 Å−1. As a result of the data...... treatment, the neutron scattering cross sections of selenium are determined to be sigmacoh = 8.4±0.1 b and sigmainc = 0.1±0.1 b. Using the fact that S (kappa) for large kappa's is determined by the short distances in the sample, a new method for extrapolation of the experimental S (kappa) until convergence....... Finally, we give a brief discussion of the different models for the structure of amorphous selenium, taking both diffraction measurements and thermodynamic considerations into account. The Journal of Chemical Physics is copyrighted by The American Institute of Physics....

  4. An arc detector for neutron crystal structure investigations

    Energy Technology Data Exchange (ETDEWEB)

    Habib, N [Reactor and Neutron Physics Dept., Nuclear Research Center. AEA, Cairo (Egypt)

    1997-12-31

    An arc detector for neutron structure investigations of powder crystals using time-of-flight technique is described. In order to enable the measurement of integral intensity from about 1/4 of the Debye-Scherrer ring and for simplicity reasons, the scattering angle 20-90 degree was chosen and a special arc collimator was built. The arc collimator-detector had a divergency of about 20 minutes of arc, and the distance between detector-sample was 64 cm. Four {sup 3} He detectors were fixed on the arc of the collimator. Both efficiency and space sensitivity of the detector were determined using a point neutron source. Results of measurements show that parameters of the arc detector are acceptable for high resolution crystal structure investigations. 6 figs.

  5. Neutron scattering investigations of the lipid bilayer structure pressure dependence

    Directory of Open Access Journals (Sweden)

    D. V. Soloviov

    2012-03-01

    Full Text Available Lipid bilayer structure investigation results obtained with small angle neutron scattering method at the Joint Institute for Nuclear Research IBR-2M nuclear reactor (Dubna, Russia are presented. Experiment has been per-formed with small angle neutron scattering spectrometer YuMO, upgraded with the apparatus for performing P-V-T measurements on the substance under investigation. D2O-1,2-dipalmitoyl-sn-glycero-3-phosphocholine (DPPC liquid system, presenting the model of natural live membrane, has been taken as the sample for investiga-tions. The lipid bilayer spatial period was measured in experiment along with isothermal compressibility simulta-neously at different pressures. It has been shown, that the bilayer structural transition from ripple (wavelike gel-phase phase to liquid-crystal phase is accompanied with anomalous rise of isothermal compressibility, indicat-ing occurrence of the phase transition.

  6. Neutron scattering investigations of the lipid bilayer structure pressure dependence

    International Nuclear Information System (INIS)

    Solovjov, D.V.; Gordelyij, V.Yi.; Gorshkova, Yu.Je.; Yivan'kov, O.Yi.; Koval'ov, Yu.S.; Kuklyin, A.Yi.; Solovjov, D.V.; Bulavyin, L.A.; Yivan'kov, O.Yi.; Nyikolajenko, T.Yu.; Kuklyin, A.Yi.; Gordelyij, V.Yi.; Gordelyij, V.Yi.

    2012-01-01

    Lipid bilayer structure investigation results obtained with small angle neutron scattering method at the Joint Institute for Nuclear Research IBR-2M nuclear reactor (Dubna, Russia) are presented. Experiment has been performed with small angle neutron scattering spectrometer YuMO, upgraded with the apparatus for performing PV-T measurements on the substance under investigation. D 2 O-1,2-dipalmitoyl-sn-glycero-3-phosphocholine (DPPC) liquid system, presenting the model of natural live membrane, has been taken as the sample for investigations. The lipid bilayer spatial period was measured in experiment along with isothermal compressibility simultaneously at different pressures. It has been shown, that the bilayer structural transition from ripple (wavelike gel-phase) phase to liquid-crystal phase is accompanied with anomalous rise of isothermal compressibility, indicating occurrence of the phase transition.

  7. Neutron structure of the hydrophobic plant protein crambin

    International Nuclear Information System (INIS)

    Teeter, M.M.; Kossiakoff, A.A.

    1982-01-01

    Crystals of the small hydrophobic protein crambin have been shown to diffract to a resolution of at least 0.88 A. This means that crambin presents a rare opportunity to study a protein structure at virtually atomic resolution. The high resolution of the diffraction pattern coupled with the assets of neutron diffraction present the distinct possibility that crambin's analysis may surpass that of any other protein system in degree and accuracy of detail. The neutron crambin structure is currently being refined at 1.50 A (44.9% of the data to 1.2 A has also been included). It is expected that a nominal resolution of 1.0 A can be achieved. 15 references, 6 figures, 2 tables

  8. Leading twist moments of the neutron structure function F_2n

    Energy Technology Data Exchange (ETDEWEB)

    M. Osipenko; W. Melnitchouk; S. Simula; S. Kulagin; G. Ricco

    2005-10-20

    We perform a global analysis of neutron $F_2^n$ structure function data, obtained by combining proton and deuteron measurements over a large range of kinematics. From these data the lowest moments ($n \\leq 10$) of the leading twist neutron $F_2^n$ structure function are extracted. Particular attention is paid to nuclear effects in the deuteron, which become increasingly important for the higher moments. Our results for the nonsinglet, isovector $p - n$ combination of the leading twist moments are compared with those of available lattice simulations. We also determine the lowest few moments of the higher twist contributions, obtained by subtracting the leading twist from the total structure function, and analyze their isospin dependence.

  9. The potential for biological structure determination with pulsed neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Wilson, C.C. [CLRC Rutherford Appleton Laboratory, Chilton Didcot Oxon (United Kingdom)

    1994-12-31

    The potential of pulsed neutron diffraction in structural determination of biological materials is discussed. The problems and potential solutions in this area are outlined, with reference to both current and future sources and instrumentation. The importance of developing instrumentation on pulsed sources in emphasized, with reference to the likelihood of future expansion in this area. The possibilities and limitations of single crystal, fiber and powder diffraction in this area are assessed.

  10. The potential for biological structure determination with pulsed neutrons

    International Nuclear Information System (INIS)

    Wilson, C.C.

    1994-01-01

    The potential of pulsed neutron diffraction in structural determination of biological materials is discussed. The problems and potential solutions in this area are outlined, with reference to both current and future sources and instrumentation. The importance of developing instrumentation on pulsed sources in emphasized, with reference to the likelihood of future expansion in this area. The possibilities and limitations of single crystal, fiber and powder diffraction in this area are assessed

  11. A measurement of ΔσL(np), the difference between neutron-proton total cross sections in pure longitudinal spin states

    International Nuclear Information System (INIS)

    Beddo, M.E.

    1990-10-01

    A measurement off Δσ L (np), the difference between neutron-proton total cross sections in pure longitudinal spin states, is described. The results will help determine the isospin-zero (I = 0) scattering amplitudes, which are not well known above laboratory energies of 500 MeV, whereas the isospin-one (I = 1) amplitudes are fairly well-determined to 1 GeV. Data points were taken at the Los Alamos Meson Physics Facility (LAMPF) at Los Alamos, New Mexico, for five neutron beam energies: 484, 568, 634,720 and 788 MeV; they are the first in this energy range. Polarized neutrons were produced by charge-exchange of polarized protons on a liquid deuterium target (LD 2 ). Large-volume neutron counters detected the neutrons that passed through a polarized proton target. The counters subtended a range of solid angles large enough to allow extrapolation of the scattered neutrons to 0 degree. Two modifications to the LAMPF accelerator system which were made for this work are described. They included a ''beam buncher,'' which modified the normal rf-time structure of the proton beam and allowed for the selection of peak-energy neutrons by time-of-flight means, and a computerized beam steering program, which reduced systematic effects due to beam motion at the LD 2 target. The experimental values of Δσ L (np) are found to be consistent with other np data, including preliminary data from SIN and Saclay, but not with some results from Argonne which used a polarized proton beam and a polarized deuteron target. The I = 0 component was extracted from Δσ L (np) using existing pp data (I = 1), with the unexpected result that Δσ L (I = 0) was found to be essentially identical in shape to Δσ L (I = 1). The significance of this is not yet understood

  12. [Neutron scatter studies of chromatin structure related to function

    International Nuclear Information System (INIS)

    Bradbury, E.M.

    1990-01-01

    This study is concerned with the application of neutron scatter techniques to the different structural states of nucleosomes and chromatin with the long term objective of understanding how the enormous lengths of DNA are folded into chromosomes. Micrococcal nuclease digestion kinetics have defined two subnucleosome particles; the chromatosome with 168 bp DNA, the histone octamer and one H1 and the nucleosome core particle with 146 bp DNA and the histone octamer. As will be discussed, the structure of the 146 bp DNA core particle is known in solution at low resolution from neutron scatter studies and in crystals. Based on this structure, the authors have a working model for the chromatosome and the mode of binding of H1. In order to define the structure of the nucleosome and also the different orders of chromatin structures they need to know the paths of DNA that link nucleosomes and the factors associated with chromosome functions that act on those DNA paths. The major region for this situation is the inherent variabilities in nucleosome DNA sequences, in the histone subtypes and their states of chemical modification and in the precise locations of nucleosomes. Such variabilities obscure the underlying principles that govern the packaging of DNA into the different structural states of nucleosomes and chromatin. The only way to elucidate these principles is to study the structures of nucleosomes and oligonucleosomes that are fully defined. They have largely achieved these objectives

  13. Portable neutron moisture gage for the moisture determination of structure parts

    International Nuclear Information System (INIS)

    Harnisch, M.

    1985-01-01

    For determining the moisture of structure parts during building or before repairing a portable neutron moisture gage consisting of a neutron probe and pulse analyzer has been developed. The measuring process, calibration, and prerequisites of application are briefly discussed

  14. Neutron scattering for the analysis of biological structures. Brookhaven symposia in biology. Number 27

    Energy Technology Data Exchange (ETDEWEB)

    Schoenborn, B P [ed.

    1976-01-01

    Sessions were included on neutron scattering and biological structure analysis, protein crystallography, neutron scattering from oriented systems, solution scattering, preparation of deuterated specimens, inelastic scattering, data analysis, experimental techniques, and instrumentation. Separate entries were made for the individual papers.

  15. Importance of isovector effects in reproducing neutron total cross section differences in the W isotopes

    International Nuclear Information System (INIS)

    Dietrich, F.S.; Anderson, J.D.; Bauer, R.W.; Grimes, S.M.; Finlay, R.W.; Abfalterer, W.P.; Bateman, F.B.; Haight, R.C.; Morgan, G.L.; Bauge, E.; Delaroche, J.-P.; Romain, P.

    2003-01-01

    Cross section differences among the isotopes 182,184,186 W have been measured as a part of a study of total cross sections in the 5-560 MeV energy range. These difference measurements show oscillations up to 150 mb between 5 and 100 MeV. Calculations with spherical and deformed phenomenological optical potentials employing standard radial and isospin dependences show much smaller oscillations than the experimental data. In a simple Ramsauer model, this discrepancy can be traced to a cancellation between radial and isospin effects. Understanding this problem requires a more detailed model that incorporates a realistic description of the neutron and proton density distributions. This has been done with the results of Hartree-Fock-Bogoliubov calculations using the Gogny force, together with a microscopic folding model employing a modification of the Jeukenne, Lejeune, and Mahaux potential as an effective interaction. This treatment yields a satisfactory interpretation of the observed total cross section differences up to 200 MeV. The calculations have been extended above that energy with a folding model based on an empirical effective interaction

  16. Fast-neutron total and scattering cross sections of 58Ni

    International Nuclear Information System (INIS)

    Jorgensen, C.B.; Guenther, P.T.; Smith, A.B.; Whalen, J.F.

    1981-09-01

    Neutron total cross sections of 58 Ni were measured at 25 keV intervals from 0.9 to 4.5 MeV with 50 to 100 keV resolutions. Attention was given to self-shielding corrections to the observed total cross sections. Differential elastic- and inelastic-scattering cross sections were measured at 50 keV intervals from 1.35 to 4.0 MeV with 50 to 100 keV resolutions. Inelastic excitation of levels at 1.458 +- 0.009, 2.462 +- 0.010, 2.791 +- 0.015, 2.927 +- 0.012 and 3.059 +- 0.025 MeV was observed. The experimental results were interpreted in terms of optical-statistical and coupled-channels models. A spherical optical-statistical model was found generally descriptive of an energy-average of the experimental results. However, detailed considerations suggested significant contributions from direct-vibrational interactions, particularly associated with the excitation of the first 2+ level

  17. Deformation effect in the fast neutron total cross section of aligned /sup 59/Co

    Energy Technology Data Exchange (ETDEWEB)

    Fasoli, U.; Pavan, P.; Toniolo, D.; Zago, G.; Zannoni, R.; Galeazzi, G.

    1982-07-19

    The variation of the total neutron cross section, ..delta.. sigma/sub align/, on /sup 59/Co due to nuclear alignment of the target in the beam direction, has been measured over the energy range from 0.8 to 20 MeV, employing a cobalt single-crystal with a 34% nuclear alignment degree. The results show that ..delta.. sigma/sub align/ oscillates from a minimum of -5% at about 2.5 MeV to a maximum of +1% at about 10 MeV. The data were successfully fitted by optical model coupled-channel calculations. The coupling terms were deduced from a model representing the /sup 59/Co nucleus as a virbrational /sup 60/Ni core coupled to a proton-hole in a (lf 7/2) shell, without free parameters. The optical model parameters were determined by fitting the total cross-section independently measured. The theoretical calculations show that, at lower energies, ..delta.. sigma/sub align/ depends appreciably on the coupling with the low-lying levels.

  18. Deformation effect in the fast neutron total cross section of alligned 59Co

    International Nuclear Information System (INIS)

    Fasoli, U.; Pavan, P.; Toniolo, D.; Zago, G.; Zannoni, R.; Galeazzi, G.

    1982-01-01

    The variation of the total neutron cross section, DELTAsigmasub(align), on 59 Co due to nuclear alignement of the target in the beam direction, has been measured over the energy range from 0.8 to 20 MeV, emploing a cobalt single-crystal with a 34% nuclear alignment degree. The results show that DELTAsigmasub(align) oscillates from a minimum of -5% at about 2.5 MeV to a maximum of +1% at about 10 MeV. The data were succesfully fitted by optical model coupled-channel calculations. The coupling terms were deduced from a model representing the 59 Co nucleus as a vibrational 60 Ni core coupled to a proton hole in a (lf7/2) shell, without free parameters. The optical model parameters were determined by fitting the total cross section independently measured. The theoretical calculations show that, at lower energies, DELTAsigmasub(align) depends appreciably on the coupling with the low-liyng levels

  19. Deformation effect in the fast neutron total cross section of aligned 59Co

    International Nuclear Information System (INIS)

    Fasoli, U.; Pavan, P.; Toniolo, D.; Zago, G.; Zannoni, R.; Galeazzi, G.

    1983-01-01

    The variation of the total neutron cross section, Δsigma/sub align/, on 59 Co due to nuclear alignment of the target has been measured over the energy range from 0.8 to 20 MeV employing a cobalt single crystal with a 34% nuclear alignment. The results show that Δsigma/sub align/ oscillates from a minimum of -5% at about 2.5 MeV to a maximum of +1% at about 10 MeV. The data were successfully fitted by optical model coupled-channel calculations. The coupling terms were deduced from a model representing the 59 Co nucleus as a vibrational 60 Ni core coupled to a proton hole in a (1f/sub 7/2/) shell, without free parameters. The optical model parameters were determined by fitting the total cross section, which was independently measured. The theoretical calculations show that, at lower energies, Δsigma/sub align/ depends appreciably on the coupling with the low-lying levels

  20. Total reaction cross sections and neutron-removal cross sections of neutron-rich light nuclei measured by the COMBAS fragment-separator

    Science.gov (United States)

    Hue, B. M.; Isataev, T.; Erdemchimeg, B.; Artukh, A. G.; Aznabaev, D.; Davaa, S.; Klygin, S. A.; Kononenko, G. A.; Khuukhenkhuu, G.; Kuterbekov, K.; Lukyanov, S. M.; Mikhailova, T. I.; Maslov, V. A.; Mendibaev, K.; Sereda, Yu M.; Penionzhkevich, Yu E.; Vorontsov, A. N.

    2017-12-01

    Preliminary results of measurements of the total reaction cross sections σR and neutron removal cross section σ-xn for weakly bound 6He, 8Li, 9Be and 10Be nuclei at energy range (20-35) A MeV with 28Si target is presented. The secondary beams of light nuclei were produced by bombardment of the 22Ne (35 A MeV) primary beam on Be target and separated by COMBAS fragment-separator. In dispersive focal plane a horizontal slit defined the momentum acceptance as 1% and a wedge degrader of 200 μm Al was installed. The Bρ of the second section of the fragment-separator was adjusted for measurements in energy range (20-35) A MeV. Two-neutron removal cross sections for 6He and 10Be and one -neutron removal cross sections 8Li and 9Be were measured.

  1. Structural Characterization of Iron Meteorites through Neutron Tomography

    Directory of Open Access Journals (Sweden)

    Stefano Caporali

    2016-02-01

    Full Text Available In this communication, we demonstrate the use of neutron tomography for the structural characterization of iron meteorites. These materials prevalently consist of metallic iron with variable nickel content. Their study and classification is traditionally based on chemical and structural analysis. The latter requires cutting, polishing and chemical etching of large slabs of the sample in order to determine the average width of the largest kamacite lamellae. Although this approach is useful to infer the genetical history of these meteorites, it is not applicable to small or precious samples. On the base of different attenuation coefficient of cold neutrons for nickel and iron, neutron tomography allows the reconstruction of the Ni-rich (taenite and Ni-poor (kamacite metallic phases. Therefore, the measure of the average width of the largest kamacite lamellae could be determined in a non-destructive way. Furthermore, the size, shape, and spatial correlation between kamacite and taenite crystals were obtained more efficiently and accurately than via metallographic investigation.

  2. Neutron scattering studies of pretransitional phenomena in structural phase transformations

    International Nuclear Information System (INIS)

    Shapiro, S.M.

    1979-03-01

    Materials exhibiting structural phase transformations are well known to possess pretransitional phenomena. Below the transition temperature, T/sub c/, an order parameter appears and the pretransitional effects are associated with the fluctuations of the order parameter. Neutron scattering techniques have proved invaluable in studying the temporal and spatial dependence of these fluctuations. SrTiO 3 is the prototypical example of a structural phase transformation exhibiting features observable in other transformations such as martensitic and order-disorder. The experimental evolution of the understanding of the phase transformation in SrTiO 3 will be reviewed and the features observed will be shown to typify other systems

  3. Structural Analysis and Seismic Design for Cold Neutron Laboratory Building

    International Nuclear Information System (INIS)

    Wu, Sangik; Kim, Y. K.; Kim, H. R.

    2007-05-01

    This report describes all the major results of the dynamic structural analysis and seismic design for the Cold Neutron Laboratory Building which is classified in seismic class II. The results are summarized of the ground response spectrum as seismic input loads, mechanical properties of subsoil, the buoyancy stability due to ground water, the maximum displacement of the main frame under the seismic load and the member design. This report will be used as a basic design report to maintenance its structural integrity in future

  4. Neutron scatter studies of chromatin structures related to functions

    International Nuclear Information System (INIS)

    Bradbury, E.M.

    1992-01-01

    Despite of setbacks in the lack of neutrons for the proposed We have made considerable progress in chromatin reconstitution with the VLR histone H1/H5 and in understanding the dynamics of nucleosomes. A ferromagnetic fluid was developed to align biological molecules for structural studies using small-angle-neutron-scattering. We have also identified and characterized an intrinsically bent DNA region flanking the RNA polymerase I binding site of the ribosomal RNA gene in Physarum Polycephalum. Finally projects in progress are in the areas of studying the interatctions of histone H4 amino-terminus peptide 1-23 and acetylated 1-23 peptide with DNA using thermal denaturation; study of GGAAT repeats found in human centromeres using high resolution Nuclear magnetic Resonance and nuclease sentivity assay; and the role of histones and other sperm specific proteins with sperm chromatin

  5. Neutrons probing the structure and dynamics of liquids

    International Nuclear Information System (INIS)

    Leclercq-Hugeux, F.; Coulet, M.V.; Gaspard, J.P.; Pouget, St.; Zanotti, J.M.

    2007-01-01

    This article illustrates the benefits of neutron techniques to the understanding of the liquid state. As opposed to the nearly complete order of crystals or the nearly complete disorder of gas, the disorder of a liquid is partial and results from dynamical events acting on a broad range of space and time scales. Consequently, no single, simple parameter can encompass the concept of order or disorder in the liquid state. The wide variety of neutron techniques (diffraction, quasi-elastic and inelastic scattering) is a key asset to solve the issue. Selected studies ranging over typical interactions and conditions relevant to liquids (metallic, covalent, molecular, liquids near a phase transition and confined fluids) are presented. In each case, both structural and dynamical aspects, along with the connections to complementary techniques (computer simulation, X-ray absorption and/or scattering) are highlighted. (authors)

  6. The structure of liquid water by polarized neutron diffraction and reverse Monte Carlo modelling.

    Science.gov (United States)

    Temleitner, László; Pusztai, László; Schweika, Werner

    2007-08-22

    The coherent static structure factor of water has been investigated by polarized neutron diffraction. Polarization analysis allows us to separate the huge incoherent scattering background from hydrogen and to obtain high quality data of the coherent scattering from four different mixtures of liquid H(2)O and D(2)O. The information obtained by the variation of the scattering contrast confines the configurational space of water and is used by the reverse Monte Carlo technique to model the total structure factors. Structural characteristics have been calculated directly from the resulting sets of particle coordinates. Consistency with existing partial pair correlation functions, derived without the application of polarized neutrons, was checked by incorporating them into our reverse Monte Carlo calculations. We also performed Monte Carlo simulations of a hard sphere system, which provides an accurate estimate of the information content of the measured data. It is shown that the present combination of polarized neutron scattering and reverse Monte Carlo structural modelling is a promising approach towards a detailed understanding of the microscopic structure of water.

  7. Systematic structure of the neutron drip-line {sup 22}C nucleus

    Energy Technology Data Exchange (ETDEWEB)

    Ismail, Atef [Fundamental and Applied Sciences Department, Universiti Teknologi Petronas, Bandar Seri Iskandar, 31750 Tronoh, Perak, Malaysia and Department of Physics, Al-Azhar University, 71524 Assiut (Egypt); Cheong, Lee Yen; Yahya, Noorhana [Fundamental and Applied Sciences Department, Universiti Teknologi PETRONAS, Bandar Seri Iskandar, 31750 Tronoh, Perak (Malaysia); Tammam, M. [Department of Physics, Al-Azhar University, 71524 Assiut (Egypt)

    2014-10-24

    In the present work we systematically discuss the nuclear structure of the the heaviest particle-bound carbon isotope, {sup 22}C. The ground state wave function of the carbon isotope is calculated using the {sup 20}C core plus two-valence neutron based on a phenomenological mean-field MF potential. We apply the deduced wave function to provide the nuclear matter density which is necessary in the calculations of the total reaction cross section. Calculations show that there is a reasonable good description of the experimental binding energy BE and root-mean square RMS radius. The exotic structure and configuration of the ground state carbon isotope is explained and a consistent explanation on the two-neutron halo (Borromean) nucleus is given.

  8. Hematologic status of mice submitted to sublethal total body irradiation with mixed neutron-gamma radiation

    International Nuclear Information System (INIS)

    Herodin, F.; Court, L.

    1989-01-01

    The hematologic status of mice exposed to sublethal whole body irradiation with mixed neutron-gamma radiation (mainly neutrons) is studied. A slight decrease of the blood cell count is still observed below 1 Gy. The recovery of bone marrow granulocyte-macrophage progenitors seems to require more time than after pure gamma irradiation [fr

  9. Effects of fast neutrons on chromatin: dependence on chromatin structure

    Energy Technology Data Exchange (ETDEWEB)

    Radu, L. [Dept. of Molecular Genetics, V. Babes National Inst., Bd. Timisoara, Bucharest (Romania); Constantinescu, B. [Dept. of Cyclotron, H. Hulubei National Inst., Bucharest (Romania); Gazdaru, D. [Dept. of Biophysics, Physics Faculty, Univ. of Bucharest (Romania)

    2002-07-01

    The effects of fast neutrons (10-100 Gy) on chromatin extracted from normal (liver of Wistar rats) and tumor (Walker carcinosarcoma maintained on Wistar rats) tissues were compared. The spectroscopic assays used were (i) chromatin intrinsic fluorescence, (ii) time-resolved fluorescence of chromatin-proflavine complexes, and (iii) fluorescence resonance energy transfer (FRET) between dansyl chloride and acridine orange coupled to chromatin. For both normal and tumor chromatin, the intensity of intrinsic fluorescence specific for acidic and basic proteins decreased with increasing dose. The relative contributions of the excited-state lifetime of proflavine bound to chromatin were reduced upon fast-neutron irradiation, indicating a decrease in the proportion of chromatin DNA available for ligand binding. The Forster energy transfer efficiencies were also modified by irradiation. These effects were larger for chromatin from tumor tissue. In the range 0-100 Gy, fast neutrons induced alterations in DNA and acidic and basic proteins, as well as in global chromatin structure. The radiosensitivity of chromatin extracted from tumor tissue seems to be higher than that of chromatin extracted from normal tissue, probably because of its higher euchromatin (loose)-heterochromatin (compact) ratio. (author)

  10. Effects of fast neutrons on chromatin: dependence on chromatin structure

    International Nuclear Information System (INIS)

    Radu, L.; Constantinescu, B.; Gazdaru, D.

    2002-01-01

    The effects of fast neutrons (10-100 Gy) on chromatin extracted from normal (liver of Wistar rats) and tumor (Walker carcinosarcoma maintained on Wistar rats) tissues were compared. The spectroscopic assays used were (i) chromatin intrinsic fluorescence, (ii) time-resolved fluorescence of chromatin-proflavine complexes, and (iii) fluorescence resonance energy transfer (FRET) between dansyl chloride and acridine orange coupled to chromatin. For both normal and tumor chromatin, the intensity of intrinsic fluorescence specific for acidic and basic proteins decreased with increasing dose. The relative contributions of the excited-state lifetime of proflavine bound to chromatin were reduced upon fast-neutron irradiation, indicating a decrease in the proportion of chromatin DNA available for ligand binding. The Forster energy transfer efficiencies were also modified by irradiation. These effects were larger for chromatin from tumor tissue. In the range 0-100 Gy, fast neutrons induced alterations in DNA and acidic and basic proteins, as well as in global chromatin structure. The radiosensitivity of chromatin extracted from tumor tissue seems to be higher than that of chromatin extracted from normal tissue, probably because of its higher euchromatin (loose)-heterochromatin (compact) ratio. (author)

  11. Magnetic field effects on the crust structure of neutron stars

    Science.gov (United States)

    Franzon, B.; Negreiros, R.; Schramm, S.

    2017-12-01

    We study the effects of high magnetic fields on the structure and on the geometry of the crust in neutron stars. We find that the crust geometry is substantially modified by the magnetic field inside the star. We build stationary and axis-symmetric magnetized stellar models by using well-known equations of state to describe the neutron star crust, namely, the Skyrme model for the inner crust and the Baym-Pethick-Sutherland equation of state for the outer crust. We show that the magnetic field has a dual role, contributing to the crust deformation via the electromagnetic interaction (manifested in this case as the Lorentz force) and by contributing to curvature due to the energy stored in it. We also study a direct consequence of the crust deformation due to the magnetic field: the thermal relaxation time. This quantity, which is of great importance to the thermal evolution of neutron stars, is sensitive to the crust properties, and, as such, we show that it may be strongly affected by the magnetic field.

  12. Structural properties and neutron irradiation effects of ceramics

    International Nuclear Information System (INIS)

    Yano, Toyohiko

    1994-01-01

    In high temperature gas-cooled reactors and nuclear fusion reactors being developed at present, various ceramics are to be used in the environment of neutron irradiation for undertaking important functions. The change of the characteristics of those materials by neutron irradiation must be exactly forecast, but it has been known that the response of the materials is different respectively. The production method of ceramics and the resulted structures of ceramics which control their characteristics are explained. The features of covalent bond and ionic bond, the synthesis of powder and the phase change by heating, sintering and sintering agent, and grain boundary phase are described. The smelling of ceramics by neutron irradiation is caused by the formation of the clusters of Frenkel defects and minute spot defects. Its restoration by annealing is explained. The defects remaining in materials after irradiation are the physical defects by flipping atoms cut due to the collision with high energy particles and the chemical defects by nuclear transformation. Some physical defects can be restored, but chemical defects are never restored. The mechanical properties of ceramics and the effect of irradiation on them, and the thermal properties of ceramics and the effect of irradiation on them are reported. (K.I.)

  13. Swelling of structural materials in fast neutron reactors

    International Nuclear Information System (INIS)

    Seran, J.L.

    1983-06-01

    The physical origin of swelling in irradiated materials and the main parameters acting on swelling of SS 316 are examined: temperature, neutron dose, dose rate, chemical composition, strain hardening. Results obtained, in Rapsodie and Phenix reactors, with fuel cans and with the hexagonal tube containing the fuel pins are analyzed and compared with results found in litterature. In conclusion hot swelling of SS 316 is too important at high doses and is will be replaced by austenitic steels stabilized by Ti and ferritic steels or high nickel steels with structural hardening [fr

  14. Neutron scattering techniques for structural studies of amorphous solids

    International Nuclear Information System (INIS)

    Wright, A.C.; Yarker, C.A.; Johnson, P.A.V.; Wedgwood, F.A.

    1976-01-01

    Preliminary data are presented for a series of glasses using some of the special features of neutron diffraction. In vitreous K 2 O x TiO 2 x 2SiO 2 each Ti atom is on average surrounded by 5.2 oxygen atoms at a distance of 1.95 A, whereas the structure of V 2 O 5 x TeO 2 is dominated by distorted TeO 6 octahedra. Features in the magnetic correlation function for vitreous O x 79Fe 2 O 3 x P 2 O 5 occur at the Fe,Fe distance found in crystalline FePO 4 . (orig.) [de

  15. Level structures of neutron-rich Xe isotopes

    Energy Technology Data Exchange (ETDEWEB)

    Ahmad, I.; Lister, C.J.; Morss, L.R. [and others

    1995-08-01

    The level structures of neutron-rich Xe isotopes were determined by observing prompt gamma-ray coincidences in {sup 248}Cm fission fragments. A 5-mg {sup 248}Cm, in the form of {sup 248}Cm-KCl pellet, was placed inside Eurogam array which consisted of 45 Compton-suppressed Ge detectors and 5 Low-Energy Photon Spectrometers. Transitions in Xe isotopes were identified by the appearance of new peaks in the {gamma}-ray spectra obtained by gating on the gamma peaks of the complementary Mo fragments.

  16. Studies of the neutron spin structure at Jefferson Lab

    International Nuclear Information System (INIS)

    Korsch, W.

    2003-01-01

    The polarized 3 He program of Hall A at Jefferson Lab will be described. Results on the generalized Gerasimov-Drell-Hearn integral for the neutron in a Q 2 range between 0.02 GeV 2 /c 2 2 2 /c 2 will be presented. Preliminary results of the virtual photon asymmetry A 1 n (x,Q 2 ) and the spin structure function g 2 n (x,Q 2 ) at large values of Bjorken x and low Q 2 , respectively, will be discussed. (orig.)

  17. Development of beryllium-based neutron target system with three-layer structure for accelerator-based neutron source for boron neutron capture therapy.

    Science.gov (United States)

    Kumada, Hiroaki; Kurihara, Toshikazu; Yoshioka, Masakazu; Kobayashi, Hitoshi; Matsumoto, Hiroshi; Sugano, Tomei; Sakurai, Hideyuki; Sakae, Takeji; Matsumura, Akira

    2015-12-01

    The iBNCT project team with University of Tsukuba is developing an accelerator-based neutron source. Regarding neutron target material, our project has applied beryllium. To deal with large heat load and blistering of the target system, we developed a three-layer structure for the target system that includes a blistering mitigation material between the beryllium used as the neutron generator and the copper heat sink. The three materials were bonded through diffusion bonding using a hot isostatic pressing method. Based on several verifications, our project chose palladium as the intermediate layer. A prototype of the neutron target system was produced. We will verify that sufficient neutrons for BNCT treatment are generated by the device in the near future. Copyright © 2015 Elsevier Ltd. All rights reserved.

  18. ISINN-5. 5. International seminar on interaction of neutrons with nuclei. Neutron spectroscopy, nuclear structure, related topics

    International Nuclear Information System (INIS)

    1997-01-01

    The materials submitted at the fifth in a series of annual international seminar on interaction of neutrons with nuclei Neutron Spectroscopy, Nuclear Structure, Related Topics (ISINN-5) are given. The Seminar is organized by the Frank Laboratory of Neutron Physics of the Joint Institute for Nuclear Research and took place in Dubna on May 14-17, 1997. About 130 specialists from Belgium, China, Germany, France, Japan, Korea, Latvia, Netherlands, Ukraine, 7 Russian research institutes and a number of JINR laboratories took part in the Seminar. The scope of the problems discussed is traditionally wide. It includes the problems of violation of fundamental symmetries in the interaction of neutrons with nuclei, the properties of the neutron as the fundamental particle, nonstatistical aspects of the radiation capture of neutrons by nuclei, topical problems of the theory of nucleus, and the fission mechanism of heavy nuclei. The latest results obtained with ultracold neutrons (UCN), in particular, different approaches to understanding of the cause of UCN anomalous leakage through the walls of the trap are considered as well. The wide spectrum of methodological aspects of neutron-aided experiments is also discussed in details

  19. Neutron scattering studies on chromatin higher-order structure

    Energy Technology Data Exchange (ETDEWEB)

    Graziano, V.; Gerchman, S.E.; Schneider, D.K.; Ramakrishnan, V. [Brookhaven National Laboratory, Upton, NY (United States)

    1994-12-31

    We have been engaged in studies of the structure and condensation of chromatin into the 30nm filament using small-angle neutron scattering. We have also used deuterated histone H1 to determine its location in the chromatin 30nm filament. Our studies indicate that chromatin condenses with increasing ionic strength to a limiting structure that has a mass per unit length of 6-7 nucleosomes/11 nm. They also show that the linker histone H1/H5 is located in the interior of the chromatin filament, in a position compatible with its binding to the inner face of the nucleosome. Analysis of the mass per unit length as a function of H5 stoichiometry suggests that 5-7 contiguous nucleosomes need to have H5 bound before a stable higher order structure can exist.

  20. Neutron scattering studies on chromatin higher-order structure

    International Nuclear Information System (INIS)

    Graziano, V.; Gerchman, S.E.; Schneider, D.K.; Ramakrishnan, V.

    1994-01-01

    We have been engaged in studies of the structure and condensation of chromatin into the 30nm filament using small-angle neutron scattering. We have also used deuterated histone H1 to determine its location in the chromatin 30nm filament. Our studies indicate that chromatin condenses with increasing ionic strength to a limiting structure that has a mass per unit length of 6-7 nucleosomes/11 nm. They also show that the linker histone H1/H5 is located in the interior of the chromatin filament, in a position compatible with its binding to the inner face of the nucleosome. Analysis of the mass per unit length as a function of H5 stoichiometry suggests that 5-7 contiguous nucleosomes need to have H5 bound before a stable higher order structure can exist

  1. New neutron capture and total cross section measurements on 88Sr and their impact on s-process nucleosynthesis

    International Nuclear Information System (INIS)

    Koehler, P.E.; Spencer, R.R.; Guber, K.H.

    1998-01-01

    The authors have made new and improved measurements of the neutron capture and total cross sections of 88 Sr at the Oak Ridge Electron Linear Accelerator (ORELA). Improvements over previous measurements include a wider incident neutron energy range, the use of metallic rather than carbonate samples, better background subtraction, reduced sensitivity to sample-dependent backgrounds, and better pulse-height weighting functions. Because of its small cross section, the 88 Sr(n,γ) reaction is an important bottleneck during the s-process nucleosynthesis. Hence, an accurate determination of this rate is needed to better constrain the neutron exposure in s-process models and to more fully exploit the recently discovered isotopic anomalies in certain meteorites. They describe the experimental procedures, compare the results to previous data, and discuss their astrophysical impact

  2. Total synthesis of the proposed structure of trichodermatide A.

    Science.gov (United States)

    Myers, Eddie; Herrero-Gómez, Elena; Albrecht, Irina; Lachs, Jennifer; Mayer, Peter; Hanni, Matti; Ochsenfeld, Christian; Trauner, Dirk

    2014-10-17

    A short total synthesis of the published structure of racemic trichodermatide A is reported. Our synthesis involves a Knoevenagel condensation/Michael addition sequence, followed by the formation of tricyclic hexahydroxanthene-dione and a diastereoselective bis-hydroxylation. The final product, the structure of which was confirmed by X-ray crystallography, has NMR spectra that are very similar, but not identical, to those of the isolated natural product. Quantum chemically computed (13)C shifts agree well with the present NMR measurements.

  3. Structure of HIV-1 protease determined by neutron crystallography

    International Nuclear Information System (INIS)

    Adachi, Motoyasu; Kuroki, Ryota

    2009-01-01

    HIV-1 protease is an aspartic protease, and plays an essential role in replication of HIV. To develop HIV-1 protease inhibitors through structure-based drug design, it is necessary to understand the catalytic mechanism and inhibitor recognition of HIV-1 protease. We have determined the crystal structure of HIV-1 protease in complex with KNI-272 to 1.9 A resolution by neutron crystallography in combination with 1.4 A resolution X-ray diffraction data. The results show that the carbonyl group of hydroxymethylcarbonyl (HMC) in KNI-272 forms a hydrogen bonding interaction with protonated Asp 25 and the hydrogen atom from the hydroxyl group of HMC forms a hydrogen bonding interaction with the deprotonated Asp125. This is the first neutron report for HIV-1/inhibitor complex and shows directly the locations of key hydrogen atoms in catalysis and in the binding of a transition-state analog. The results confirm key aspect of the presumed catalytic mechanism of HIV-1 protease and will aid in the further development of protease inhibitors. (author)

  4. Precise structural analysis of methane hydrate by neutron diffraction

    International Nuclear Information System (INIS)

    Igawa, Naoki; Hoshikawa, Akinori; Ishii, Yoshinobu

    2006-01-01

    Methane hydrate has attracted great interest as an energy resource to replace natural gas since this material is deposited in the seafloor and the deposits are estimated to exceed those of natural gas. Understanding the physical proprieties, such as the temperature dependence of the crystal structure, helps to specify the optimum environmental temperature and pressure during drilling, transport, and storage of methane hydrate. Clathrate hydrates consisted of encaging atomic and/or molecular species as a guest and host water formed by a hydrogen bonding. Although many studies on the clathrate hydrate including methane hydrate were reported, no detailed crystallographic property has yet been cleared. We focused on the motion of methane in the clathrate hydrate by the neutron diffraction. The crystal structure of the methane hydrate was analyzed by the applying the combination of the Rietveld refinement and the maximum entropy method (MEM) to neutron powder diffraction. Temperature dependence of the scattering-length density distribution maps revealed that the motion of methane molecules differs between the shapes of dodecahedron and tetrakaidecahedron. (author)

  5. Fast neutron irradiation effects on liver chromatin structure

    International Nuclear Information System (INIS)

    Constantinescu, B.; Radu, L.

    1996-01-01

    The growing interest in neutron therapy requires complex studies on the mechanisms of neutron action on biological systems, especially on chromatin. The chromatin was extracted from a normal tissue-livers of Wistar rats - and from a tumoral tissue - Walker tumour maintained on Wistar rats. Irradiation doses from 5 Gy to 100 Gy by fast neutron intense beams produced via d(13.5 MeV) +Be (thick target) reaction at Bucharest U-120 Classical Cyclotron were used. To study the post-irradiation effects, various methods were employed. So, the variation in the 260 nm absorbency in chromatin thermal transition was pursuit. The chromatin-ethidium bromide complexes fluorescence with λ ex =480 nm and λ em =600 nm was analyzed. To determine chromatin DNA strand breaks a fluorimetric method, with cells' suspensions as starting material was used. This method requires a partial treatment with alkali producing three components: T-estimating the total fluorescence of DNA double helix, P-assigning the untwisting rate and B-the blank, where DNA is completely unfolded The percentsge of DNA double strand,-D-, remaining after this treatment, is: %D=100x(P-B)/(T-B). The intrinsic chromatin fluorescence was determined for tyrosine (λ ex =280 nm, λ em =305 nm), specific for badic chromatin prooteins, and for tryptophane (λ ex =290 nm, λ em =345 nm) specific for acid chromatin proteins. Polyacrylamide gel electrophoresis was performed: The double fluorescent labelling of chromatin was realized with acridine orange for DNA and with dansyl chloride for chromatin proteins. Fluorescence intensity determinations were done with λ ex =505 nm, λ em =530 nm for acridine orange and with λ ex =323 nm, λ em =505 nm for dansyl chloride. A Pye Unicam SP 1800 spectrophotometer and a Aminco SPF 500 spectrofluorimeter were employed. (author)

  6. Total Absorption Spectroscopy Study of the Beta Decay of 60Mn to Constrain the Neutron Capture Rate of 60Fe

    Science.gov (United States)

    Richman, Debra; Spyrou, Artemis; Dombos, Alex; Couture, Aaron; e15034 Collaboration

    2017-09-01

    Interest in 60Fe, a long lived radioisotope synthesized in massive stars, has recently peaked. The signature of its decay allows us to probe astrophysical processes, events such as the early formation of the solar system and nucleosynthesis. To understand these observations a complete understanding of the creation, destruction and nuclear properties of 60Fe in the astrophysical environment are required. Using the beta decay of 60Mn in conjunction with total absorption spectroscopy (TAS), made possible by the high efficiency gamma ray calorimeter SuN (Summing NaI detector) at the National Superconducting Cyclotron Laboratory (NSCL), to study the distribution of beta-decay intensity over the daughter-nucleus 60Fe, provides information about the structure of the daughter and improves the predictive power of astrophysical models. In addition to the ongoing TAS analysis, The Beta-Oslo method will be used to extract the nuclear level density and gamma-strength function of 60Fe providing much needed constraints on the neutron capture reaction rate responsible for the creation of this nucleus.

  7. Analysis of total hydrogen content in palm oil and palm kernel oil using thermal neutron moderation method

    International Nuclear Information System (INIS)

    Akaho, E.H.K.; Dagadu, C.P.K.; Maaku, B.T.; Anim-Sampong, S.; Kyere, A.W.K.; Jonah, S.A.

    2001-01-01

    A fast and non-destructive technique based on thermal neutron moderation has been used for determining the total hydrogen content in two types of red palm oil (dzomi and amidze) and palm kernel oil produced by traditional methods in Ghana. An equipment consisting of an 241 Am-Be neutron source and 3 He neutron detector was used in the investigation. The equipment was originally designed for detection of liquid levels in petrochemical and other process industries. Standards in the form of liquid hydrocarbons were used to obtain calibration lines for thermal neutron reflection parameter as a function of hydrogen content. Measured reflection parameters with respective hydrogen content with or without heat treatment of the three edible palm oils available on the market were compared with a brand cooking oil (frytol). The average total hydrogen content in the local oil samples prior to heating was measured to be 11.62 w% which compared well with acceptable value of 12 w% for palm oils in the sub-region. After heat treatment, the frytol oil (produced through bleaching process) had the least loss of hydrogen content of 0.26% in comparison with palm kernel oil of 0.44% followed by dzomi of 1.96% and by amidze of 3.22%. (author)

  8. Structural studies of liquid alcohols by neutron diffraction

    International Nuclear Information System (INIS)

    Montague, D.G.; Cummings, S.

    1984-01-01

    Neutron diffraction measurements have been made on methyl alcohol at room temperature for an incident wavelength of 0.94 A. Cross sections have been obtained for CD 3 OD, CD 3 OH, and mixtures of these compounds. These data are subtracted to obtain the separated structure factors for intermolecular H 0 H 0 , the hydroxyl components, and the non-hydroxyl components. The Fourier transformations of the structure factors show components of both intra- and intermolecular distribution functions. Width parameters obtained from model fits are too large for thermal vibrations and are interpreted as geometrical broadening due to the stretching of bonds, variations in bond angles, and rotation of the methyl group. Differences in the real space distribution function between hydrogen and deuterium are noted. (author)

  9. Precision measurement of the neutron spin dependent structure functions

    International Nuclear Information System (INIS)

    Kolomensky, Y.G.

    1997-02-01

    In experiment E154 at the Stanford Linear Accelerator Center the spin dependent structure function g 1 n (x, Q 2 ) of the neutron was measured by scattering longitudinally polarized 48.3 GeV electrons off a longitudinally polarized 3 He target. The high beam energy allowed the author to extend the kinematic coverage compared to the previous SLAC experiments to 0.014 ≤ x ≤ 0.7 with an average Q 2 of 5 GeV 2 . The author reports the integral of the spin dependent structure function in the measured range to be ∫ 0.014 0.7 dx g 1 n (x, 5 GeV 2 ) = -0.036 ± 0.004(stat.) ± 0.005(syst.). The author observes relatively large values of g 1 n at low x that call into question the reliability of data extrapolation to x → 0. Such divergent behavior disagrees with predictions of the conventional Regge theory, but is qualitatively explained by perturbative QCD. The author performs a Next-to-Leading Order perturbative QCD analysis of the world data on the nucleon spin dependent structure functions g 1 p and g 1 n paying careful attention to the experimental and theoretical uncertainties. Using the parameterizations of the helicity-dependent parton distributions obtained in the analysis, the author evolves the data to Q 2 = 5 GeV 2 , determines the first moments of the polarized structure functions of the proton and neutron, and finds agreement with the Bjorken sum rule

  10. Energy-averaged neutron cross sections of fast-reactor structural materials

    International Nuclear Information System (INIS)

    Smith, A.; McKnight, R.; Smith, D.

    1978-02-01

    The status of energy-averaged cross sections of fast-reactor structural materials is outlined with emphasis on U.S. data programs in the neutron-energy range 1-10 MeV. Areas of outstanding accomplishment and significant uncertainty are noted with recommendations for future efforts. Attention is primarily given to the main constituents of stainless steel (e.g., Fe, Ni, and Cr) and, secondarily, to alternate structural materials (e.g., V, Ti, Nb, Mo, Zr). Generally, the mass regions of interest are A approximately 50 to 60 and A approximately 90 to 100. Neutron total and elastic-scattering cross sections are discussed with the implication on the non-elastic-cross sections. Cross sections governing discrete-inelastic-neutron-energy transfers are examined in detail. Cross sections for the reactions (n;p), (n;n',p), (n;α), (n;n',α) and (n;2n') are reviewed in the context of fast-reactor performance and/or diagnostics. The primary orientation of the discussion is experimental with some additional attention to the applications of theory, the problems of evaluation and the data sensitivity of representative fast-reactor systems

  11. The total neutron cross-sections of 151Eu, 153Eu and Eu below 1 eV

    International Nuclear Information System (INIS)

    Adib, M.; Maayouf, R.M.A.; Abdel-Kawy, A.; Ashry, A.; Hamouda, I.

    1981-01-01

    Total neutron cross-section measurements have been carried out for natural Eu and its stable isotopes in the energy range from 3 meV to 1 eV. The measurements were performed using two time-of-flight spectrometers installed in front of two of the horizontal channels of the ET-RR-1 reactor. The following results have been obtained: sigmasub(a) ( 151 Eu) = (9180 +- 150) b at 0.0253 eV, sigmasub(s) ( 153 Eu) = (375 +- 20) b at 0.0253 eV, sigmasub(d) (Eu) = (4600 +- 120) b at 0.0253 eV. The contribution of the resonance to the total neutron cross-sections, in the thermal region, was calculated using the single-level Breit-Wigner formula. (orig.)

  12. Total neutron cross-sections of /sup 151/Eu, /sup 153/Eu and Eu below 1 eV

    Energy Technology Data Exchange (ETDEWEB)

    Adib, M.; Maayouf, R.M.A.; Abdel-Kawy, A.; Ashry, A.; Hamouda, I.

    1981-01-01

    Total neutron cross-section measurements have been carried out for natural Eu and its stable isotopes in the energy range from 3 meV to 1 eV. The measurements were performed using two time-of-flight spectrometers installed in front of two of the horizontal channels of the ET-RR-1 reactor. The following results have been obtained: sigmasub(a) (/sup 151/Eu) = (9180 +- 150) b at 0.0253 eV, sigmasub(s) (/sup 153/Eu) = (375 +- 20) b at 0.0253 eV, sigmasub(d) (Eu) = (4600 +- 120) b at 0.0253 eV. The contribution of the resonance to the total neutron cross-sections, in the thermal region, was calculated using the single-level Breit-Wigner formula.

  13. Neutron total cross section measurements in the energy region from 47 keV to 20 MeV

    International Nuclear Information System (INIS)

    Poenitz, W.P.; Whalen, J.F.

    1983-05-01

    Neutron total cross sections were measured for 26 elements. Data were obtained in the energy range from 47 keV to 20 MeV for 11 elements in the range of light-mass fission products. Previously reported measurements for eight heavy and actinide isotopes were extended to 20 MeV. Data were also obtained for Cu (47 keV to 1.4 MeV) and for Sc, Zn, Nd, Hf, and Pt (1.8 to 20 MeV). The present work is part of a continuing effort to provide accurate neutron total cross sections for evaluations and for optical-model parameteriztions. The latter are required for the derivation of other nuclear-data information of importance to applied programs. 37 references

  14. Algorithm for the real-structure design of neutron supermirrors

    International Nuclear Information System (INIS)

    Pleshanov, N.K.

    2004-01-01

    The effect of structure imperfections of neutron supermirrors on their performance is well known. Nevertheless, supermirrors are designed with the algorithms based on the theories of reflection from perfect layered structures. In the present paper an approach is suggested, in which the design of a supermirror is made on the basis of its real-structure model (the RSD algorithm) with the use of exact numerical methods. It allows taking the growth laws and the reflectance of real structures into account. The new algorithm was compared with the Gukasov-Ruban-Bedrizova (GRB) algorithm and with the most frequently used algorithm of Hayter and Mook (HM). Calculations showed that, when the parameters of the algorithms are chosen so that the supermirrors designed for a given angular acceptance m have the same number of bilayers, (a) for perfect layers the GRB, HM and RSD algorithms generate sequences of practically the same reflectance; (b) for real structures with rough interfaces and interdiffusion the GRB and HM algorithms generate sequences with insufficient number of thinner layers and the RSD algorithm turns out to be more responsive and efficient. The efficiency of the RSD algorithm increases for larger m. In addition, calculations have been carried out to demonstrate the effect of fabrication errors and absorption on the reflectance of Ni/Ti supermirrors

  15. The total neutron cross section of 58Fe in the energy range 7 to 325 keV

    International Nuclear Information System (INIS)

    Hong, L.D.; Beer, H.; Kaeppeler, F.

    1976-08-01

    The total neutron cross section of 58 Fe has been determined in the energy range 7-325 keV by a transmission measurement using enriched 58 Fe samples. The data have been shape fitted by means of an R-matrix multi-level formalism to extract resonance parameters for s- and l > 0 wave resonances. The s-wave strength function was determined to S 0 = (4.3 +- 1.9) c 10 -4 . (orig.) [de

  16. Estimation of 242Cm neutron cross sections for total file creation

    International Nuclear Information System (INIS)

    Bakhanovich, L.A.; Klepatskij, A.B.; Maslov, V.M.; Porodzinskij, Yu.V.; Sukhovitskij, E.Sh.

    1989-01-01

    Description of evaluation of 242 Cm neutron cross sections in 10 -5 eV-20 MeV energy range is given. Due to the lack of experimental data the evaluation is largely based on the application of theoretical models and systematics. The data obtained are compared to evaluations by other authors. 10 refs.; 2 figs.; 2 tabs

  17. Discrimination of the wall effect in a thin counter with micro-gap structure for neutron position sensing

    Energy Technology Data Exchange (ETDEWEB)

    Sakae, Takeji; Manabe, Tohru; Kitamura, Yasunori; Nohtomi, Akihiro [Kyushu Univ., Fukuoka (Japan); Sakamoto, Sigeyasu

    1996-07-01

    Simulation by the Monte Carlo method is applied to estimate the wall effect in a thermal neutron counter having a new function for discriminating the effect. The counter is designed to have paralleled electrodes with micro-gap structure. A resistive anode is used for position sensing on the center of a set of the three electrode. The structure can be made by simple arrangement of anode and cathode wires on an insulator plane. The calculation shows discrimination of the wall effect can be achieved by coincident counting of two or three elements included in the counter. By using the coincident counting, the thickness of the neutron counter can be made into 1 mm with the information of the total energy created in the neutron detection. (author)

  18. Study of the fluctuations of the partial and total radiative widths by neutron capture resonance method; Etude des fluctuations des largeurs radiatives partielles et totales par la capture des neutrons de resonance

    Energy Technology Data Exchange (ETDEWEB)

    Huynh, V D [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1965-06-01

    Radiative capture experiments by neutron time-of-flight methods have been made for following studies: distribution of partial radiative widths, effects of correlation between different radiative transitions, fluctuations of total radiative widths {gamma}{sub {gamma}} from resonance to resonance, variation of {gamma}{sub {gamma}} with number of mass and the search for the existence of potential capture. Also, some other experiments with the use of neutron capture gamma-rays spectra have been investigated. (author) [French] Par la capture des neutrons de resonance dont les energies sont selectionnees a l'aide de la technique du temps de vol, differents types d'experiences ont ete realisees concernant les etudes des distributions des largeurs radiatives partielles, des effets de correlation entre differentes voies de desexcitation, de la fluctuation des largeurs radiatives totales {gamma}{sub {gamma}} de resonance a resonance, de la variation de la quantite {gamma}{sub {gamma}} en fonction du nombre de masse et de la mise en evidence de l'existence du processus de capture potentielle. Quelques autres applications de l'emploi du spectre de rayons gamma ont egalement ete presentees. (auteur)

  19. Study of the fluctuations of the partial and total radiative widths by neutron capture resonance method; Etude des fluctuations des largeurs radiatives partielles et totales par la capture des neutrons de resonance

    Energy Technology Data Exchange (ETDEWEB)

    Huynh, V.D. [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1965-06-01

    Radiative capture experiments by neutron time-of-flight methods have been made for following studies: distribution of partial radiative widths, effects of correlation between different radiative transitions, fluctuations of total radiative widths {gamma}{sub {gamma}} from resonance to resonance, variation of {gamma}{sub {gamma}} with number of mass and the search for the existence of potential capture. Also, some other experiments with the use of neutron capture gamma-rays spectra have been investigated. (author) [French] Par la capture des neutrons de resonance dont les energies sont selectionnees a l'aide de la technique du temps de vol, differents types d'experiences ont ete realisees concernant les etudes des distributions des largeurs radiatives partielles, des effets de correlation entre differentes voies de desexcitation, de la fluctuation des largeurs radiatives totales {gamma}{sub {gamma}} de resonance a resonance, de la variation de la quantite {gamma}{sub {gamma}} en fonction du nombre de masse et de la mise en evidence de l'existence du processus de capture potentielle. Quelques autres applications de l'emploi du spectre de rayons gamma ont egalement ete presentees. (auteur)

  20. A measurement of. Delta. sigma. sub L (np), the difference between neutron-proton total cross sections in pure longitudinal spin states

    Energy Technology Data Exchange (ETDEWEB)

    Beddo, M.E.

    1990-10-01

    A measurement off {Delta}{sigma}{sub L}(np), the difference between neutron-proton total cross sections in pure longitudinal spin states, is described. The results will help determine the isospin-zero (I = 0) scattering amplitudes, which are not well known above laboratory energies of 500 MeV, whereas the isospin-one (I = 1) amplitudes are fairly well-determined to 1 GeV. Data points were taken at the Los Alamos Meson Physics Facility (LAMPF) at Los Alamos, New Mexico, for five neutron beam energies: 484, 568, 634,720 and 788 MeV; they are the first in this energy range. Polarized neutrons were produced by charge-exchange of polarized protons on a liquid deuterium target (LD{sub 2}). Large-volume neutron counters detected the neutrons that passed through a polarized proton target. The counters subtended a range of solid angles large enough to allow extrapolation of the scattered neutrons to 0{degree}. Two modifications to the LAMPF accelerator system which were made for this work are described. They included a beam buncher,'' which modified the normal rf-time structure of the proton beam and allowed for the selection of peak-energy neutrons by time-of-flight means, and a computerized beam steering program, which reduced systematic effects due to beam motion at the LD{sub 2} target. The experimental values of {Delta}{sigma}{sub L}(np) are found to be consistent with other np data, including preliminary data from SIN and Saclay, but not with some results from Argonne which used a polarized proton beam and a polarized deuteron target. The I = 0 component was extracted from {Delta}{sigma}{sub L}(np) using existing pp data (I = 1), with the unexpected result that {Delta}{sigma}{sub L}(I = 0) was found to be essentially identical in shape to {Delta}{sigma}{sub L}(I = 1). The significance of this is not yet understood.

  1. Weakly bound structures in neutron rich Si isotopes

    International Nuclear Information System (INIS)

    Singh, D.; Saxena, G.; Yadav, H.L.

    2009-01-01

    Production of radioactive beams have facilitated the nuclear structure studies away from the line of β-stability, especially for the neutron rich drip line nuclei. Theoretical investigations of these nuclei have been carried out by using various approaches viz. few body model or clusters, shell model and mean field theories, both nonrelativistic as well as relativistic mean field (RMF). The advantage of the RMF approach, however, is that in this treatment the spin-orbit interaction is included in a natural way. This is especially advantageous for the description of drip-line nuclei for which the spin-orbit interaction plays an important role. In this communication we report briefly the results of our calculations for the Si isotopes carried out within the framework of RMF + BCS approach

  2. Neutron scatter studies of chromatin structures related to functions

    International Nuclear Information System (INIS)

    Bradbury, E.M.

    1992-01-01

    We have made considerable progress in chromatin reconstitution with very lysine rich histone H1/H5 and in understanding the dynamics of nucleosomes. A ferromagnetic fluid was developed to align biological molecules for structural studies using small-angle-neutron-scattering. We have also identified and characterized in intrinsically bent DNA region flaking the RNA polymerase I binding site of the ribosomal RNA gene in Physarum Polycephalum. Finally projects in progress are in the areas of studying the interactions of histone H4 amino-terminus peptide 1-23 and acetylated 1-23 peptide with DNA using thermal denaturation; study of GGAAT repeats found in human centromeres using high resolution Nuclear Magnetic Resonance and nuclease sentivity assay; and the role of histones and other sperm specific proteins with sperm chromatin

  3. Neutron scattering analysis of rubber carbon black composite structure

    International Nuclear Information System (INIS)

    Hjelm, R.P. Jr.; Wampler, W.A.; Gerspacher, M.

    1994-01-01

    We explore the uses of small-angle neutron scattering to dissect component form, structure and distribution in carbon black-reinforced rubber by varying the contrast of the system relative to some fluid by changing the fluid scattering-length density. This is the method of contrast variation. Contrast variation allows us to separate scattering contributions from the different components. Here, we extend our studies on high surface area (HSA) carbon black suspended in cyclohexane/deuterocyclohexane to HSA mixed with polyisoprene as a gel of ''bound'' rubber swollen with the same solvent mixtures. Contrast variation of swollen composite gels shows that there are two length scales in the gel structure. Above 1 nm fluctuations in the carbon black predominate. Interactions with elastomer hold the HSA aggregates appart. Below 1 nm the scattering is largely from the elastomer. The smooth surface structure of the carbon black is unaltered by the interactions with elastomer and appears smooth over length scales above about 1 nm. These results show that contrast variation can provide information on composite structure that is not available by other means. This information relates to the reinforcement mechanism of elastomers by carbon blacks

  4. The γ total cross section and the photon structure functions

    International Nuclear Information System (INIS)

    Alexander, G.

    1986-01-01

    A review on the current experimental status of the photon-photon total hadronic cross section as a function of energy and Q 2 is given in addition to the results obtained for the leptonic and hadronic photon structure functions. The results are discussed in terms of the point-like part of the photon and non-perturbative VDM part. It is shown that the cross section at Q 2 = 0 is well described by VDM derived models

  5. Assessment of radiation fields from neutron irradiated structural components of the 40 MW research reactor CIRUS

    International Nuclear Information System (INIS)

    Sankaranarayanan, S.; Sharma, S.K.

    1993-01-01

    The paper summarizes the results of an assessment of the radiation fields from the long-lived neutron activation products (including the decay chain products) in the various structural components of the CIRUS reactor. Special attention is given for the analysis of neutron activation of impurity elements present in the materials of the structure. 16 refs, 4 figs, 4 tabs

  6. Measurements of the total neutron cross-sections of U and UO2 below 2 eV at different temperatures

    International Nuclear Information System (INIS)

    Adib, M.; Maayouf, R.M.A.; Abdel-Kawy, A.; Ashry, A.; Abbas, Y.; Abu-Zahra, A.; Hamouda, I.

    1982-11-01

    The total neutron cross-sections of natural uranium and its oxide are measured using two time of flight spectrometers, installed in front of two of the ET-RR-1 reactor horizontal channels, and also by a neutron diffraction spectrometer. The measurements were carried out at room temperature in the energy range from 2 eV-0.002 eV and at 210 deg. C, for neutron energies below 0.005 eV. The coherent scattering cross-section of U was deduced both from the Bragg cut-offs observed in the behaviour of the total neutron cross-section of both U and UO 2 at cold neutron energies and the neutron diffraction pattern obtained at room temperature. (author)

  7. Ultracold neutrons

    International Nuclear Information System (INIS)

    Steenstrup, S.

    Briefly surveys recent developments in research work with ultracold neutrons (neutrons of very low velocity, up to 10 m/s at up to 10 -7 eV and 10 -3 K). Slow neutrons can be detected in an ionisation chamber filled with B 10 F 3 . Very slow neutrons can be used for investigations into the dipole moment of neutrons. Neutrons of large wave length have properties similar to those of light. The limit angle for total reflection is governed by the wave length and by the material. Total reflection can be used to filter ultracold neutrons out of the moderator material of a reactor. Total reflection can also be used to store ultracold neutrons but certain problems with storage have not yet been clarified. Slow neutrons can be made to lose speed in a neutron turbine, and come out as ultracold neutrons. A beam of ultracold neutrons could be used in a neutron microscope. (J.S.)

  8. Studies of the neutron single-particle structure of exotic nuclei at the HRIBF

    International Nuclear Information System (INIS)

    Thomas, J.S.; Bardayan, D.W.; Blackmon, J.C.; Cizewski, J.A.; Greife, U.; Gross, C.J.; Johnson, M.S.; Jones, K.L.; Kozub, R.L.; Liang, J.F.; Livesay, R.J.; Ma, Z.; Moazen, B.H.; Nesaraja, C.D.; Shapira, D.; Smith, M.S.

    2004-01-01

    The study of neutron single-particle strengths in neutron-rich nuclei is of interest for nuclear structure and nuclear astrophysics. The distribution of single-particle strengths constrains the effective Hamiltonian and pairing interactions and determines neutron interaction rates that are crucial for understanding the synthesis of heavy nuclei in supernovae via the rapid neutron capture process. Particularly important are the neutron single-particle levels in nuclei near closed neutron shells. Radioactive ion beams from the Holifield Radioactive Ion Beam Facility have been used to study (d,p) reactions in inverse kinematics in order to probe neutron single-particle states in exotic nuclei. The results of a measurement with a 82 Ge beam will be presented

  9. The structure of alkali silicate gel by total scattering methods

    KAUST Repository

    Benmore, C.J.

    2010-06-01

    The structure of the alkali silicate gel (ASR) collected from the galleries of Furnas Dam in Brazil was determined by a pair distribution function (PDF) analysis of high energy X-ray diffraction data. Since this method is relatively new to concrete structure analysis a detailed introduction on the PDF method is given for glassy SiO2. The bulk amorphous structure of the dam material is confirmed as no Bragg peaks are observed in the scattered intensity. The real space results show that the local structure of the amorphous material is similar to kanemite (KHSi2O5:3H2O) however the long range layer structure of the crystal is broken up in the amorphous state, so that ordering only persists of the length scale of a few polyhedra. The silicate layer structure is a much more disordered than predicted by molecular dynamics models. The X-ray results are consistent with the molecular dynamics model of Kirkpatrick et al. (2005) [1] which predicts that most of the water resides in pores within the amorphous network rather than in layers. The total scattering data provide a rigorous basis against which other models may also be tested. © 2010.

  10. The structure of alkali silicate gel by total scattering methods

    KAUST Repository

    Benmore, C.J.; Monteiro, Paulo J.M.

    2010-01-01

    The structure of the alkali silicate gel (ASR) collected from the galleries of Furnas Dam in Brazil was determined by a pair distribution function (PDF) analysis of high energy X-ray diffraction data. Since this method is relatively new to concrete structure analysis a detailed introduction on the PDF method is given for glassy SiO2. The bulk amorphous structure of the dam material is confirmed as no Bragg peaks are observed in the scattered intensity. The real space results show that the local structure of the amorphous material is similar to kanemite (KHSi2O5:3H2O) however the long range layer structure of the crystal is broken up in the amorphous state, so that ordering only persists of the length scale of a few polyhedra. The silicate layer structure is a much more disordered than predicted by molecular dynamics models. The X-ray results are consistent with the molecular dynamics model of Kirkpatrick et al. (2005) [1] which predicts that most of the water resides in pores within the amorphous network rather than in layers. The total scattering data provide a rigorous basis against which other models may also be tested. © 2010.

  11. Beta strength distributions in neutron-deficient Kr and Sr isotopes using a total absorption spectrometer

    CERN Document Server

    Maréchal, F

    2003-01-01

    Far from the line of stability, beta -decay studies are often a primary source of information on nuclear structure. The measured beta -strength distribution for a given decay can be used to verify the accuracy of our theoretical description of the parent nucleus ground state and the states populated in the daughter nucleus. Total absorption spectrometers based on large NaI crystals are well suited tools to determine the beta -strength distribution over the whole Q /sub EC/ decay window. The newly built spectrometer TAgS, dedicated to such studies, is presented and its performances and possibilities are discussed in the light of experiments performed at the ISOLDE /CERN mass separator. The resulting information on ground state deformations for the /sup 74/Kr and /sup 76/Sr isotopes are discussed. (22 refs).

  12. Determination of Total Arsenic in Seaweed Products by Neutron Activation Analysis

    OpenAIRE

    Salim, N; Santoso, M; Damayanti, S; Kartawinata, T.G

    2013-01-01

    Seaweed products are widely consumed as food nowadays. Seaweeds are known to contain arsenic due to their capability to accumulate arsenic from the environment. Arsenic is a known toxic element which naturally occurs in the environment. Ingestion of high levels of arsenic will cause several adverse health effects. Arsenic in food occurs at trace concentrations which require sensitive and selective analysis methods to perform elemental analysis on. Validated neutron activation analysis was use...

  13. Total cross-sections assessment of neutron reaction with stainless steel SUS-310 contained in various nuclear data files

    International Nuclear Information System (INIS)

    Suwoto

    2002-01-01

    The integral testing of neutron cross-sections for Stainless Steel SUS-310 contained in various nuclear data files have been performed. The shielding benchmark calculations for Stainless Steel SUS-310 has been analysed through ORNL-Broomstick Experiment calculation which performed by MAERKER, R.E. at ORNL - USA ( 1) . Assessment with JENDL-3.1, JENDL-3.2, ENDF/B-IV, ENDF/B-VI nuclear data files and data from GEEL have also been carried out. The overall calculation results SUS-310 show in a good agreement with the experimental data, although, underestimate results appear below 3 MeV for all nuclear data files. These underestimation tendencies clearly caused by presented of iron nuclide which more than half in Stainless Steel compound. The total neutron cross-sections of iron nuclide contained in various nuclear data files relatively lower on that energy ranges

  14. Structural integrity assessment based on the HFR Petten neutron beam facilities

    CERN Document Server

    Ohms, C; Idsert, P V D

    2002-01-01

    Neutrons are becoming recognized as a valuable tool for structural-integrity assessment of industrial components and advanced materials development. Microstructure, texture and residual stress analyses are commonly performed by neutron diffraction and a joint CEN/ISO Pre-Standard for residual stress analysis is under development. Furthermore neutrons provide for defects analyses, i.e. precipitations, voids, pores and cracks, through small-angle neutron scattering (SANS) or radiography. At the High Flux Reactor, 12 beam tubes have been installed for the extraction of thermal neutrons for such applications. Two of them are equipped with neutron diffractometers for residual stress and structure determination and have been extensively used in the past. Several other facilities are currently being reactivated and upgraded. These include the SANS and radiography facilities as well as a powder diffractometer. This paper summarizes the main characteristics and current status of these facilities as well as recently in...

  15. Advantages of neutron scattering for biological structure analysis

    International Nuclear Information System (INIS)

    Schoenborn, B.P.

    1975-01-01

    The advantages and disadvantages of neutron scattering for protein crystallography, scattering from oriented systems, and solution scattering are summarized. Techniques for minimizing the disadvantages are indicated

  16. Study of neutron radiation effects on MOS structures

    International Nuclear Information System (INIS)

    Vaidya, Sangeeta J.

    2003-01-01

    We have studied charge trapping in the oxide and generation of interface states due to neutrons. It is observed that neutrons, though uncharged, are capable of causing ionization and interface damage and it is significant under biased irradiation conditions. One of the important features of this work is that neutron irradiation was carried out in a nuclear reactor (swimming pool type) itself in contrast to the earlier reported work which used separate neutron sources for similar studies. To simulate real life situations, all our devices were biased during irradiation. In our belief, both of these facts gave credence to our observed experimental results. (author)

  17. Behavior of structural and target materials irradiated in spallation neutron environments

    International Nuclear Information System (INIS)

    Stubbins, J.F.; Wechsler, M.; Borden, M.

    1995-01-01

    This paper describes considerations for selection of structural and target materials for accelerator-driven neutron sources. Due to the operating constraints of proposed accelerator-driven neutron sources, the criteria for selection are different than those commonly applied to fission and fusion systems. Established irradiation performance of various alloy systems is taken into account in the selection criteria. Nevertheless, only limited materials performance data are available which specifically related to neutron energy spectra anticipated for spallation sources

  18. Behavior of structural and target materials irradiated in spallation neutron environments

    Energy Technology Data Exchange (ETDEWEB)

    Stubbins, J.F. [Univ. of Illinois, Urbana, IL (United States); Wechsler, M. [North Carolina State Univ., Raleigh, NC (United States); Borden, M. [Los Alamos National Laboratory, NM (United States)] [and others

    1995-10-01

    This paper describes considerations for selection of structural and target materials for accelerator-driven neutron sources. Due to the operating constraints of proposed accelerator-driven neutron sources, the criteria for selection are different than those commonly applied to fission and fusion systems. Established irradiation performance of various alloy systems is taken into account in the selection criteria. Nevertheless, only limited materials performance data are available which specifically related to neutron energy spectra anticipated for spallation sources.

  19. Neutron beam applications - Development of single crystal structure analysis technique using the HANARO neutron four circle diffractometer

    Energy Technology Data Exchange (ETDEWEB)

    Suh, Il Hwan; Kim, Moon Jib; Kim, Jin Gyu [Chungnam National University, Taejon (Korea)

    2000-04-01

    As the four circle diffractometer (FCD) has been set up in HANARO, it has become possible to study the single crystal structures by means of the neutron diffraction. Taking account of the geometry of the FCD, a program for the control of te FCD and neutron data acquisition operating under Windows' circumstance has been accomplished. Also, a computer program which can automatically measure the diffraction intensity data has been developed. All data obtained from the FCD are processed automatically for further work and a software for the single crystal structure analyses has been prepared. A KC1 single crystal was selected as first test sample for a structure analysis had been successfully performed on the FCD using in-house developed program and accordingly their functionings with precision were confirmed. For regular single crystal diffraction experiments, the structure analyses of chrysoberyl and Zr(Y)0{sub 1.87} single crystals were performed using both neutron and X-ray diffraction methods, and the result showed that the neutron diffraction work is superior to the X-ray one from the viewpoint of certain crystallographic information obtainable only from the former one. 24 refs., 15 figs., 15 tabs. (Author)

  20. Total and (n, 2n) neutron cross section measurements on 241Am

    International Nuclear Information System (INIS)

    Sage, C.

    2009-01-01

    Neutron induced reaction cross sections on 241 Am have been measured at the IRMM in Geel, Belgium, in the frame of a collaboration between the EC Joint Research Centres IRMM and ITU and French laboratories from CNRS and CEA. Raw material coming from the Atalante facility of CEA Marcoule has been transformed into suitable AmO 2 samples embedded in Al 2 O 3 and Y 2 O 3 matrices. The irradiations for the 241 Am(n, 2n) 240 Am reaction cross section measurement were carried out at the 7 MV Van de Graaff accelerator using the activation technique with quasi mono-energetic neutrons from 8 to 21 MeV produced via the D(d, n) 3 He and the T(d, n) 4 He reactions. The cross section was determined relative to the 27 Al(n, α) 24 Na standard cross section and was investigated for the first time above 15 MeV. The induced activity was measured off-line by standard γ-ray spectrometry using a high purity Ge detector. A special effort was made for the estimation of the uncertainties and the correlations between our experimental points. A different sample of the same isotope 241 Am has been measured in transmission and capture experiments in the resolved resonance region at the neutron ToF facility GELINA. The transmission measurement was performed in two campaigns, with an upgrade of the whole data acquisition system in between, followed by an investigation of its new performances. A preliminary analysis of the resonance parameters tends to confirm the recent evaluation to a higher value for the cross section at the bottom of the first resonances. A new design of C 6 D 6 detectors for capture measurements has been studied, but the data reduction and analysis of the measurement are not part of this work. (author) [fr

  1. High-spin structure of neutron-rich Dy isotopes

    Indian Academy of Sciences (India)

    Neutron-rich Dy isotopes; high-spin states; g-factors; cranked HFB theory. ... for 164Dy marking a clear separation in the behaviour as a function of neutron ... cipal x-axis as the cranking axis) in this mass region we have planned to make a sys-.

  2. Relativistic Processes and the Internal Structure of Neutron Stars

    International Nuclear Information System (INIS)

    Alvarez-Castillo, D. E.; Kubis, S.

    2011-01-01

    Models for the internal composition of Dense Compact Stars are reviewed as well as macroscopic properties derived by observations of relativistic processes. Modeling of pure neutron matter Neutron Stars is presented and crust properties are studied by means of a two fluid model.

  3. Structure of light neutron-rich nuclei through Coulomb dissociation

    Indian Academy of Sciences (India)

    The data analysis for Coulomb breakup of. ½ .... C (605 MeV/u) breaking up into a neutron and a .... direct break up model delivers a cross section of 107 mb for a ... separation energy for the last neutron in the even isotopes = 20 to 24 is 7 to 8 ...

  4. Scattering of 14.6 MeV neutrons from Fe and evidence for structure in the emitted neutron spectra

    International Nuclear Information System (INIS)

    Gul, K.; Anwar, M.; Ahmad, M.; Saleem, S.M.; Khan, N.A.

    1984-06-01

    Structure in the spectra of neutrons emitted from iron on bombardment with 14.6 MeV neutrons has been investigated and explained in terms of excitation of levels in iron 56. The energies of scattered neutrons have been measured by the time-of-flight technique based on the associated particle method. The observed excitations have been correlated with the reported levels in a satisfactory manner. Evidence for new excitations at 8.8 +- 0.02, 9.8 +- 0.1, 10.2 +- 0.1, 12.44 +- 0.03 and 12.52 +- 0.03 MeV has been obtained. The excitation of possible components of Ml giant resonance in iron 56 is discussed. (author)

  5. Fission Fragment Mass Distributions and Total Kinetic Energy Release of 235-Uranium and 238-Uranium in Neutron-Induced Fission at Intermediate and Fast Neutron Energies

    Energy Technology Data Exchange (ETDEWEB)

    Duke, Dana Lynn [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2015-11-12

    This Ph.D. dissertation describes a measurement of the change in mass distributions and average total kinetic energy (TKE) release with increasing incident neutron energy for fission of 235U and 238U. Although fission was discovered over seventy-five years ago, open questions remain about the physics of the fission process. The energy of the incident neutron, En, changes the division of energy release in the resulting fission fragments, however, the details of energy partitioning remain ambiguous because the nucleus is a many-body quantum system. Creating a full theoretical model is difficult and experimental data to validate existing models are lacking. Additional fission measurements will lead to higher-quality models of the fission process, therefore improving applications such as the development of next-generation nuclear reactors and defense. This work also paves the way for precision experiments such as the Time Projection Chamber (TPC) for fission cross section measurements and the Spectrometer for Ion Determination in Fission (SPIDER) for precision mass yields.

  6. The total neutron cross-sections of 151Eu, 153Eu and Eu below 1 eV

    International Nuclear Information System (INIS)

    Adib, M.; Maayouf, R.M.A.; Abdel-Kawy, A.; Ashry, A.; Hamouda, I.

    1980-12-01

    Total neutron cross-section measurements have been carried out for natural Eu and its stable isotopes in the energy range from 3 meV-1 eV. The measurements were performed using two time-of-flight spectrometers installed in front of two of the horizontal channels of the ET-RR-1 reactor. The following results have been obtained: sigmasub(α)( 151 Eu) = 9180+-150 b at 0.0253 eV; sigmasub(α)( 153 Eu) = 375+-20 b at 0.0253 eV; sigmasub(α)(Eu) = 4600+-120 b at 0.0253 eV

  7. Bulk magnetic domain structures visualized by neutron dark-field imaging

    International Nuclear Information System (INIS)

    Gruenzweig, C.; David, C.; Bunk, O.; Dierolf, M.; Frei, G.; Kuehne, G.; Schaefer, R.; Pofahl, S.; Roennow, H. M. R.; Pfeiffer, F.

    2008-01-01

    We report on how a neutron grating interferometer can yield projection images of the internal domain structure in bulk ferromagnetic samples. The image contrast relies on the ultrasmall angle scattering of unpolarized neutrons at domain wall structures in the specimen. The results show the basic domains of (110)-oriented sheets in an FeSi test sample. The obtained domain structures could be correlated with surface sensitive magneto-optical Kerr effect micrographs

  8. Bulk magnetic domain structures visualized by neutron dark-field imaging

    Science.gov (United States)

    Grünzweig, C.; David, C.; Bunk, O.; Dierolf, M.; Frei, G.; Kühne, G.; Schäfer, R.; Pofahl, S.; Rønnow, H. M. R.; Pfeiffer, F.

    2008-09-01

    We report on how a neutron grating interferometer can yield projection images of the internal domain structure in bulk ferromagnetic samples. The image contrast relies on the ultrasmall angle scattering of unpolarized neutrons at domain wall structures in the specimen. The results show the basic domains of (110)-oriented sheets in an FeSi test sample. The obtained domain structures could be correlated with surface sensitive magneto-optical Kerr effect micrographs.

  9. Evaluation of 40K in vegetables collected Malaysia by determination total potassium using neutron activation analysis

    International Nuclear Information System (INIS)

    Shafaei, M.A.; Saion, E.; Naghavi, K.; Wood, K.; Rezaee, Kh.

    2011-01-01

    Some vegetables of important nutritive requirements have been collected from Kuala Lumpur region capital of Malaysia. The vegetables were analyzed in order to determine activity concentration level of potassium using neutron activation analysis (NAA). The NAA results obtained showed the activity concentration of 40 K varied from 379 Bq/kg (Egg-plant) to 1585 Bq/kg (Spinach Red). These results are compared to other researches and are clear that the concentrations of K are relatively high in the Malaysia in compared to rather than vegetables of Pakistan and Jamaican. However, they are seen not to pose any serious internal health burden due to ingestion given the realities of vegetables choice by individuals in the study area. (author)

  10. Evaluation of body composition and nitrogen content of renal patients on chronic dialysis as determined by total body neutron activation

    International Nuclear Information System (INIS)

    Cohn, S.H.; Brennan, B.L.; Yasumura, S.; Vartsky, D.; Vaswani, A.N.; Ellis, K.J.

    1983-01-01

    Total body protein (nitrogen), body cell mass (potassium), fat, and water were measured in 15 renal patients on maintenance hemodialysis (MHD). Total body nitrogen was measured by means of prompt γ neutron activation analysis; total body water was determined with tritium labeled water; total body potassium was measured by whole body counting. The extracellular water was determined by a technique utilizing the measurement of total body chloride and plasma chloride. When compared with corresponding values of a control group of the same age, sex, and height, the protein content, body cell mass, and total body fat of the MHD patients were within the normal range. The only significant change was an increase in the extracellular water/body cell mass ratio in the male MHD patients compared to the control. The lack of significant difference of the nitrogen values of the MHD patients compared to matched controls suggests that dialysis minimizes any residual effects of uremic toxicity or protein-calorie malnutrition. These findings further suggest that there is a need to reevaluate the traditional anthropometric and biochemical standards of nutritional status for MHD patients. It was concluded that it is particularly important to measure protein stores of MHD patients with low protein intake to ascertain nutritional status. Finally, in vivo measurement of total body nitrogen and potassium for determination of body composition provides a simple, direct, and accurate assessment of the nutritional status of MHD patients

  11. Study of structure of nuclei with neutrons and nuclear data measurements for MFE

    International Nuclear Information System (INIS)

    Lane, R.O.; Grimes, S.M.

    1990-01-01

    Measurements and analysis of cross sections for neutron-induced reactions of interest to the fusion energy program have been carried out. These include neutron elastic and inelastic cross sections for 2 H, 10 B and 13 C as well as cross sections for 54 Fe and 56 Fe (n,z) reactions. Most of these data have been analyzed using either R-matrix studies or Hauser-Feshbach calculations. Details of these measurements and analyses are given. Level density measurements and low energy optical model studies for protons have been completed to improve our understanding of (n,z) reactions. Total cross section measurements have also been analyzed to obtain optical model information. Improvements to the facilities at this laboratory are also described. Modifications to the shell model code have enabled further progress to be made in studies of nuclear structure and reaction mechanisms. A description of the code and summary of the structure and level density calculations now in progress are given

  12. Neutron structure analyses and structural disorders of poly(p-phenylenebenzobisoxazole) and poly(p-phenylenebenzobisthiazole)

    International Nuclear Information System (INIS)

    Takahashi, Yasuhiro

    2001-01-01

    Poly(p-phenylenebenzobisoxazole)(PBO) and poly(p-phenylenebenzobisthiazole)(PBZT) are disordered with respect to the molecular heights. The molecular heights of PBO are disordered by 1/2 along the molecular axis, while the molecular heights of PBZT are disordered by 1/2 on the ac-plane and by every 1/5 on the bc-plane. Neutron structure analyses of both polymers were carried out for the c-projected structure in the temperature range 17 - 295K. The molecular structures of both polymers deviate from the planar structure. The crystal structures are less dependent on the temperature than the flexible polymers, polyethylene and poly(vinyl alcohol). (author)

  13. Effect of Different Structural Materials on Neutronic Performance of a Hybrid Reactor

    Science.gov (United States)

    Übeyli, Mustafa; Tel, Eyyüp

    2003-06-01

    Selection of structural material for a fusion-fission (hybrid) reactor is very important by taking into account of neutronic performance of the blanket. Refractory metals and alloys have much higher operating temperatures and neutron wall load (NWL) capabilities than low activation materials (ferritic/martensitic steels, vanadium alloys and SiC/SiC composites) and austenitic stainless steels. In this study, effect of primary candidate refractory alloys, namely, W-5Re, T111, TZM and Nb-1Zr on neutronic performance of the hybrid reactor was investigated. Neutron transport calculations were conducted with the help of SCALE 4.3 System by solving the Boltzmann transport equation with code XSDRNPM. Among the investigated structural materials, tantalum had the worst performance due to the fact that it has higher neutron absorption cross section than others. And W-5Re and TZM having similar results showed the best performance.

  14. The use of neutron scattering to determine the functional structure of glycoside hydrolase.

    Science.gov (United States)

    Nakamura, Akihiko; Ishida, Takuya; Samejima, Masahiro; Igarashi, Kiyohiko

    2016-10-01

    Neutron diffraction provides different information from X-ray diffraction, because neutrons are scattered by atomic nuclei, whereas X-rays are scattered by electrons. One of the key advantages of neutron crystallography is the ability to visualize hydrogen and deuterium atoms, making it possible to observe the protonation state of amino acid residues, hydrogen bonds, networks of water molecules and proton relay pathways in enzymes. But, because of technical difficulties, less than 100 enzyme structures have been evaluated by neutron crystallography to date. In this review, we discuss the advantages and disadvantages of neutron crystallography as a tool to investigate the functional structure of glycoside hydrolases, with some examples. Copyright © 2016 Elsevier Ltd. All rights reserved.

  15. Hadron physics and the structure of neutron stars

    International Nuclear Information System (INIS)

    Kutschera, M.

    1996-09-01

    The equation of state of hadronic matter in neutron stars is briefly reviewed. Uncertainties regarding the stiffness and composition of hadronic matter are discussed. Importance of poorly known short range interactions of nucleons and hyperons is emphasized. Condensation of meson fields and the role of subhadronic degrees of freedom is considered. Empirical constraints on the equation of state emerging from observations of neutron stars are discussed. The nature of the remnant of SN1987A is considered. (author)

  16. Single-Particle Structure of Neutron-Rich Nuclei

    International Nuclear Information System (INIS)

    Cizewski, Jolie; Jones, K.L.; Thomas, J.S.; Bardayan, Daniel W.; Blackmon, Jeff C.; Gross, Carl J.; Liang, J. Felix; Shapira, Dan; Smith, Michael Scott; Stracener, Daniel W.; Kozub, R.L.; Nesaraja, Caroline D.; Greife, U.; Livesay, Jake; Ma, Zhanwen

    2004-01-01

    Neutron transfer (d,p) reactions have been measured with rare isotope beams of 132Sn, 130Sn and 134Te accelerated to ∼4.5 MeV/u interacting with CD2 targets. Reaction protons were detected in an early implementation of the ORRUBA array of position-sensitive silicon strip detectors. Neutron excitations in the 2f7/2, 3p3/2, 3p1/2 and 2f5/2 orbitals were populated.

  17. An investigation of fossil bone mineral structure with neutron scattering

    International Nuclear Information System (INIS)

    Batdehmbehrehl, G.; Chultehm, D.; Sangaa, D.

    1999-01-01

    Using the neutron diffraction method a domination of low crystal syngonic (sp. gr. P63/m) phase Ca 5 [PO 4 ] 3 (OH, F, Cl) in the fossil dinosaur bone has been established. It is shown that the neutron diffraction method has large advantages in apatite phase of any vertebrates studies and in the case of carbonate phase x-ray method it becomes to be preferable. (author)

  18. Total neutron cross sections at energies around 20 MeV

    International Nuclear Information System (INIS)

    Morales, J.R.; Romero, J.L.; Martens, P.

    1990-09-01

    The results for measurements of total cross sections on C, Al, Mg, Cu, Ge and Pb at 17.6 and 19.8 MeV are reported. A detailed comparison is presented with previous data and with the global optical model by the Ohio group. We also discuss plans for total non elastic cross section measurements. 31 refs, 12 figs, 2 tabs

  19. Studies on fission with ALADIN. Precise and simultaneous measurement of fission yields, total kinetic energy and total prompt neutron multiplicity at GSI

    International Nuclear Information System (INIS)

    Martin, Julie-Fiona; Taieb, Julien; Chatillon, Audrey; Belier, Gilbert; Boutoux, Guillaume; Ebran, Adeline; Gorbinet, Thomas; Grente, Lucie; Laurent, Benoit; Pellereau, Eric; Alvarez-Pol, Hector; Ayyad, Yassid; Benlliure, Jose; Cortina Gil, Dolores; Caamano, Manuel; Fernandez Dominguez, Beatriz; Paradela, Carlos; Ramos, Diego; Rodriguez-Sanchez, Jose-Luis; Vargas, Jossitt; Audouin, Laurent; Tassan-Got, Laurent; Aumann, Thomas; Casarejos, Enrique; Farget, Fanny; Rodriguez-Tajes, Carme; Heinz, Andreas; Jurado, Beatriz; Kelic-Heil, Aleksandra; Kurz, Nikolaus; Nociforo, Chiara; Pietri, Stephane; Rossi, Dominic; Schmidt, Karl-Heinz; Simon, Haik; Voss, Bernd; Weick, Helmut

    2015-01-01

    A novel technique for fission studies, based on the inverse kinematics approach, is presented. Following pioneering work in the nineties, the SOFIA Collaboration has designed and built an experimental set-up dedicated to the simultaneous measurement of isotopic yields, total kinetic energies and total prompt neutron multiplicities, by fully identifying both fission fragments in coincidence, for the very first time. This experiment, performed at GSI, permits to study the fission of a wide variety of fissioning systems, ranging from mercury to neptunium, possibly far from the valley of stability. A first experiment, performed in 2012, has provided a large array of unprecedented data regarding the nuclear fission process. An excerpt of the results is presented. With this solid starter, further improvements of the experimental set-up are considered, which are consistent with the expected developments at the GSI facility, in order to measure more fission observables in coincidence. The completeness reached in the SOFIA data, permits to scrutinize the correlations between the interesting features of fission, offering a very detailed insight in this still unraveled mechanism. (orig.)

  20. Studies on fission with ALADIN. Precise and simultaneous measurement of fission yields, total kinetic energy and total prompt neutron multiplicity at GSI

    Energy Technology Data Exchange (ETDEWEB)

    Martin, Julie-Fiona; Taieb, Julien; Chatillon, Audrey; Belier, Gilbert; Boutoux, Guillaume; Ebran, Adeline; Gorbinet, Thomas; Grente, Lucie; Laurent, Benoit; Pellereau, Eric [CEA DAM Bruyeres-le-Chatel, Arpajon (France); Alvarez-Pol, Hector; Ayyad, Yassid; Benlliure, Jose; Cortina Gil, Dolores; Caamano, Manuel; Fernandez Dominguez, Beatriz; Paradela, Carlos; Ramos, Diego; Rodriguez-Sanchez, Jose-Luis; Vargas, Jossitt [Universidad de Santiago de Compostela, Santiago de Compostela (Spain); Audouin, Laurent; Tassan-Got, Laurent [CNRS/IN2P3, IPNO, Orsay (France); Aumann, Thomas [Technische Universitaet Darmstadt, Darmstadt (Germany); Casarejos, Enrique [Universidad de Vigo, Vigo (Spain); Farget, Fanny; Rodriguez-Tajes, Carme [CNRS/IN2P3, GANIL, Caen (France); Heinz, Andreas [Chalmers University of Technology, Gothenburg (Sweden); Jurado, Beatriz [CNRS/IN2P3, CENBG, Gradignan (France); Kelic-Heil, Aleksandra; Kurz, Nikolaus; Nociforo, Chiara; Pietri, Stephane; Rossi, Dominic; Schmidt, Karl-Heinz; Simon, Haik; Voss, Bernd; Weick, Helmut [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, Darmstadt (Germany)

    2015-12-15

    A novel technique for fission studies, based on the inverse kinematics approach, is presented. Following pioneering work in the nineties, the SOFIA Collaboration has designed and built an experimental set-up dedicated to the simultaneous measurement of isotopic yields, total kinetic energies and total prompt neutron multiplicities, by fully identifying both fission fragments in coincidence, for the very first time. This experiment, performed at GSI, permits to study the fission of a wide variety of fissioning systems, ranging from mercury to neptunium, possibly far from the valley of stability. A first experiment, performed in 2012, has provided a large array of unprecedented data regarding the nuclear fission process. An excerpt of the results is presented. With this solid starter, further improvements of the experimental set-up are considered, which are consistent with the expected developments at the GSI facility, in order to measure more fission observables in coincidence. The completeness reached in the SOFIA data, permits to scrutinize the correlations between the interesting features of fission, offering a very detailed insight in this still unraveled mechanism. (orig.)

  1. Atomic structure of radiation damages in FCC-metals after neutron irradiation

    International Nuclear Information System (INIS)

    Popova, E.V.; Ivchenko, V.A.; Kozlov, A.V.

    2005-01-01

    Full text: Radiation clusters, formed at a neutron irradiation, are a product of evolution of cascade areas. The quantitative information about clusters can be used for verification of calculations of cascade damage ability, in particular, cascade efficiency. Data about concentration clusters and an average of the vacancies containing in them, allow to receive total of the vacancies reserved in them and to use them for comparison to results of calculations of cascade damage ability. A correctness of such comparison by that above, than below temperature of a neutron irradiation. The purpose of work was experimental studying radiation clusters formed in FCC-metals at a low temperature neutron irradiation methods of dilatometry, field ion (FIM) and transmission electronic microscopy (TEM). Radiation clusters were studied: in industrial austenite steel C0.05Crl6Nil5Mo2Mnl, irradiated in reactor Rw-2a at temperature 310 K up to fluence intermediate and fast neutrons (with E > 0,1 MeV) 6.7·l0 21 m -2 ; in a modelling material - Pt (cleanliness of 99.99 %) with the same - FCC-structure in an initial condition and after an irradiation in reactor RWW-2M at temperature 310 K up to fluence intermediate and fast neutrons (with E > 0.1 MeV) 3.5·10 22 m -2 . As a result of an irradiation of steel and pure Pt, in these materials by methods FIM and TEM many radiation clusters, the accelerated neutrons initiated by interaction with substance was revealed. It is established that these damage areas represent the depleted zones containing separate vacancies, and also small vacancy complexes, with the 'belt' interstitial atoms. The quantitative estimation of the sizes of such radiating defects is lead and their density in volume is experimentally established. So the neutron irradiation of steel at temperature 310 K up to fluence 6.7·10 21 m -2 causes formation radiation clusters which average diameter according to TEM makes 3 nanometers. Observable by methods FIM clusters have the

  2. Structure of the neutron-rich lithium isotopes in heavy-ion reactions

    International Nuclear Information System (INIS)

    Bespalova, O.V.; Galakhmatova, B.S.; Romanovskij, E.A.; Shitikova, K.V.; Burov, V.V.; Rzyanin, M.V.; Miller, H.G.; Yen, G.D.

    1993-01-01

    The structure properties, for factors, angular distributions and interaction cross sections of Li neutron-rich isotopes have been analyzed in the unified way. A good qualitative agreement with the experiment data was obtained. 20 refs.; 11 figs.; 1 tab

  3. Neutron scattering and diffraction instrument for structural study on biology in Japan

    Energy Technology Data Exchange (ETDEWEB)

    Niimura, Nobuo [Japan Atomic Energy Research Inst., Ibaraki-ken (Japan)

    1994-12-31

    Neutron scattering and diffraction instruments in Japan which can be used for structural studies in biology are briefly introduced. Main specifications and general layouts of the instruments are shown.

  4. An investigation of the structure of disordered materials by using neutron diffraction

    International Nuclear Information System (INIS)

    Petri, I.

    1999-01-01

    The structure of several semiconducting, metallic and ionic disordered materials was investigated using neutron diffraction and the results were compared with those obtained from recent ab initio molecular dynamics methods. The method of isotopic substitution was applied to measure the full set of partial structure factors, S αβ (Q), for the liquid semiconductor GeSe and the covalent network glass GeSe 2 . Their short range ordering and for GeSe 2 also the intermediate range ordering were identified and a substantial number of 'defects' such as homopolar bonds were detected in both systems. Further, the structure of liquid GeSe 2 with increasing temperature was studied at the total structure factor level. Also, changes in the topology of Ge x Se 1-x glasses in the range 0 ≤ x ≤ 0.4 were observed and investigated by measuring the total structure factors. As far as possible our results were compared with those from molecular dynamics studies. The Ge-Se system was found to serve as a sensitive test-system for these studies, giving an insight into the strengths and limitations of them. For instance, problems are found in the region of the homopolar bonds for g GeGe (r) and for the first sharp diffraction peak in the Bhatia-Thornton concentration-concentration structure factor that could not be reproduced. The structure of liquid lithium was measured and particular attention was paid to the inelasticity and resolution function corrections. The ion-ion and ion-valence electron partial structure factors were obtained and found to be in good agreement with ab initio molecular dynamics studies. The method of first order difference functions in neutron diffraction in combination with H/D substitution was applied to 2 molal solutions of Cu(ClO 4 ) 2 in perchloric acid to measure the Cu-H and, to a first order approximation, the Cu-O partial structure factor. A (4 + 1) distortion of the hydration shell around the Cu 2+ ion was measured. (author)

  5. The estimation of total body fat by inelastic neutron scattering - a geometrical feasibility study

    International Nuclear Information System (INIS)

    Lizos, F.; Kotzasarlidoou, M.; Makridou, A.; Giannopoulou, K.

    2012-01-01

    A rough quantitative representation of the basic elements in a human body is shown. It deals with a hypothetical, normal adult weighting 70 kg. It is possible to measure two basic quantities, the FFM, standing for Fat Free Mass and the FM, standing for Fat Mass. The present simulation deals with the most important aspect of the estimation of storage fat in the human body and in order to accomplish such a task, it is considered a representation of the human body, containing a uniform distribution of triacylglycerols, in a shape of cylindrical phantom. The whole process is analyzed and simulated by a geometrical model and with the aid of a computer program which takes into consideration the different attenuation for neutrons and photons, the amount of gamma radiation reaching the detector is also calculated. The net result is the determination of sensitivity for a particular set-up and by relating the out coming data to the amount of carbon; the quantity of fat is estimated. In addition, the non-uniformity is calculated, from the computer programs expressing the consistency of the system. In order to determine the storage fat, a simulation model that will enable to represent the detection of the carbon atoms in triacylglycerols was built

  6. Invisible detergents for structure determination of membrane proteins by small-angle neutron scattering

    DEFF Research Database (Denmark)

    Midtgaard, Søren Roi; Darwish, Tamim A.; Pedersen, Martin Cramer

    2018-01-01

    A novel and generally applicable method for determining structures of membrane proteins in solution via small-angle neutron scattering (SANS) is presented. Common detergents for solubilizing membrane proteins were synthesized in isotope-substituted versions for utilizing the intrinsic neutron sca...... solution structure determination of membrane proteins by SANS and subsequent data analysis available to non-specialists. This article is protected by copyright. All rights reserved....

  7. Neutrons in nuclear physics from Billiard Balls to quark-gluon structure

    International Nuclear Information System (INIS)

    Annand, J. R. M.

    2002-01-01

    Neutrons and protons are the main building blocks of atomic nuclei and neutrons have been used to probe nuclear structure since the pioneering days of nuclear physics. As strongly interacting hadrons they have a high probability of reaction and, being uncharged, they are unaffected by the nuclear Coulomb field. Neutron scattering for example has been used to determine nuclear sizes and shapes. However the strong interaction inhibits the neutron from penetrating the surface skin of the nucleus and to gain information on the interior a relatively weakly interacting probe such as a photon or electron is superior.As the energies of electron accelerators have increased, shorter distances may be probed, until at a photon momentum of ∼200 MeV/c the reduced wavelength is 1 fm, roughly the dimension of the neutron or proton. From this point one starts to become sensitive to the internal structure. Until recently most experiments have concentrated on the proton as a hydrogen target is experimentally straightforward. There is of course no free neutron target, but with an improved understanding of how nuclear binding affects the neutron embedded in deuterium or helium-3, these materials may be considered as effective neutron targets. The extra information obtained from examining an up-down-down-quark neutron, as opposed to an up-up-down-quark proton, will be vital to achieve a full understanding of the ways in which elementary quarks and gluons interact to make composite hadrons. New results from the MAMI accelerator in Germany are presented and an extension of these measurements at Jefferson Laboratory in the USA is previewed.As well as being pivotal to the development of fundamental nuclear physics, neutrons have immense technological importance. Many of the early neutron scattering experiments were driven by a need to understand nuclear fission processes for power generation or weapons production, but neutron beams have also been widely used in medicine for the treatment

  8. Structure of molten TbCl sub 3 measured by neutron diffraction

    CERN Document Server

    Martin, R A; Barnes, A C; Cuello, G J

    2002-01-01

    The total structure factor of molten TbCl sub 3 at 617 deg. C was measured by using neutron diffraction. The data are in agreement with results from previous experimental work but the use of a diffractometer having an extended reciprocal-space measurement window leads to improved resolution in real space. Significant discrepancies with the results obtained from recent molecular dynamics simulations carried out using a polarizable ion model, in which the interaction potentials were optimized to enhance agreement with previous diffraction data, are thereby highlighted. It is hence shown that there is considerable scope for the development of this model for TbCl sub 3 and for other trivalent metal halide systems spanning a wide range of ion size ratios. (letter to the editor)

  9. Effect of reactor neutron radiation and temperature on the structure of InP single crystals

    International Nuclear Information System (INIS)

    Bojko, V.M.; Kolin, N.G.; Merkurisov, D.I.; Bublik, V.T.; Voronova, M.I.; Shcherbachev, K.D.

    2006-01-01

    The structural characteristics of InP single crystals have been investigated depending on the radiation effects produced by fast and full spectrum neutrons and subsequent heat treatment. A lattice period in InP single crystals decreases under neutron irradiation. Fast neutrons make the main contribution into the change of the lattice period. Availability of the thermal neutrons initiates the formation of Sn atoms, but does not make a significant influence on the change of the lattice period. Heat treatment of the irradiated samples up to 600 deg C causes the annealing of radiation defects and recovery of the lattice period. With increasing neutron fluences a lattice period becomes even higher than before irradiation [ru

  10. Nuclear structure studies on 178Hf by means of neutron induced gamma and electron spectroscopy

    International Nuclear Information System (INIS)

    Al Mamun Imtiazul Haque.

    1985-01-01

    By means of thermal and epithermal neutron captures the nucleus 178 Hf was studied. With high-resolution spectrometers the gamma transitions and conversion electrons were measured. By the found energies, intensities, and multipolarities the level scheme of 178 Hf could be essentially improved and extended. Totally 270 secondary (from 600 gamma lines) and 39 primary gamma transitions were used in order to establish the level scheme with 66 levels in 18 rotational bands. For this 92% of all gamma intensities were used. Several new rotational bands were established. By improved gamma energies the level scheme below 2 MeV for spins between 0 and 6 is well confirmed. Moreover by the resolution of several multiplets the decay structure of the levels could be explained. The thermal neutron capture state results from the primary gamma transitions to Q n =7626.34 (23) keV. Electrical monopole transitions from several states were studied in order to determine the X(E0/E2) values. (orig./HSI) [de

  11. s- and p-wave neutron spectroscopy. Xc. Intermediate structure: 88Sr

    International Nuclear Information System (INIS)

    Malan, J.G.; Pineo, W.F.E.; Divadeenam, M.; Choi, B.H.; Bilpuch, E.G.; Newson, H.W.

    1975-01-01

    Neutron total cross section measurements of natural Sr were made from 50-875 keV using a high resolution proton beam and the 7 Li(p,n) reaction as a neutron source. These data were analyzed with the help of an R-Matrix code to extract resonance (energies and other) parameters up to about 850 keV. 2p-1h and particle-vibration doorway interpretation of the s-,p- and d-wave resonances is attempted in terms of the sum rule Σγ/subn/ 2 =γ/subd/ 2 . Predictions based on both of these models agree with the experimental results. As expected the p-wave resonances are stronger than either s- and d-wave structure. Theory accounts for the p-wave strength remarkably well. Possible location of the p-wave s.p. resonance is reproduced with a real potential and its damping due to the imaginary potential is calculated. More fragmentation of the strong p-wave doorways is observed than was expected for a compound nucleus so near 90 Zr, but a larger strength function is observed, apparently due to the p-wave giant resonance. (U.S.)

  12. Neutron total cross-sections and resonance parameters of Mo and Ta

    Indian Academy of Sciences (India)

    Linear accelerator; total cross-sections; resonance parameters; SAMMY code. ... Centre for Atomic Research, Kalpakkam 603 102, India; Pohang Accelerator Laboratory, Pohang University of Science and Technology, Pohang 790-784, Korea; Department of Physics, Kyungpook National University, Daegu 702-701, Korea ...

  13. The neutron total cross-section measurement of 56Fe and 57Fe by using Japan Proton Accelerator Research Complex facility

    International Nuclear Information System (INIS)

    Kim, Eun Ae; Shvetsov, Valery; Cho, Moo Hyun; Won, Nam Kung; Kim, Kwang Soo; Yang, Sung Chul; Lee, Man Woo; Kim, Guin Yun; Yi, Kyoung Rak; Choi, Hong Yub; Ro, Tae Ik; Mizumoto, Motoharu; Katabuchi, Tatsuya; Igashira, Masayuki

    2012-01-01

    The measurement of neutron cross section using Time-Of-Flight (TOF) method gives significant information for the nuclear data research. In the present work, the neutron total cross section of 56 Fe and 57 Fe has been measured in the energy range between 10 eV and 100 keV by using the neutron beam produced from 3-GeV proton synchrotron accelerator. The 3-GeV proton synchrotron accelerator is located at Japan Proton Accelerator Research Complex (J-PARC) facility in Tokai village. In this study, the neutron total cross section data measured by 6 Li glass scintillator detector was compared with the evaluated values of ENDF/B-VII.0

  14. The neutron total cross-section measurement of {sup 56}Fe and {sup 57}Fe by using Japan Proton Accelerator Research Complex facility

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Eun Ae; Shvetsov, Valery; Cho, Moo Hyun [Pohang University of Science and Technology, Pohang (Korea, Republic of); Won, Nam Kung [Pohang Accelerator Laboratory, Pohang (Korea, Republic of); Kim, Kwang Soo; Yang, Sung Chul; Lee, Man Woo; Kim, Guin Yun [Kyungpook National University, Daegu (Korea, Republic of); Yi, Kyoung Rak; Choi, Hong Yub; Ro, Tae Ik [Dong-A University, Pusan (Korea, Republic of); Mizumoto, Motoharu; Katabuchi, Tatsuya; Igashira, Masayuki [Tokyo Institute of Technology, Tokyo (Japan)

    2012-05-15

    The measurement of neutron cross section using Time-Of-Flight (TOF) method gives significant information for the nuclear data research. In the present work, the neutron total cross section of {sup 56}Fe and {sup 57}Fe has been measured in the energy range between 10 eV and 100 keV by using the neutron beam produced from 3-GeV proton synchrotron accelerator. The 3-GeV proton synchrotron accelerator is located at Japan Proton Accelerator Research Complex (J-PARC) facility in Tokai village. In this study, the neutron total cross section data measured by {sup 6}Li glass scintillator detector was compared with the evaluated values of ENDF/B-VII.0

  15. Neutron reflectometry

    International Nuclear Information System (INIS)

    Van Well, A.A.

    1999-01-01

    Neutron research where reflection, refraction, and interference play an essential role is generally referred to as 'neutron optics'. The neutron wavelength, the scattering length density and the magnetic properties of the material determine the critical angle for total reflection. The theoretical background of neutron reflection, experimental methods and the interpretation of reflection data are presented. (K.A.)

  16. Neutron irradiation effects in fusion or spallation structural materials: Some recent insights related to neutron spectra

    International Nuclear Information System (INIS)

    Garner, F.A.; Greenwood, L.R.

    1998-01-01

    A review is presented of recent insights on the role of transmutation in the development of radiation-induced changes in dimension or radiation-induced changes in physical or mechanical properties. It is shown that, in some materials and some neutron spectra, transmutation can significantly affect or even dominate a given property change process. When the process under study is also sensitive to displacement rate, and especially if it involves radiation-induced segregation and precipitation, it becomes much more difficult to separate the transmutation and displacement rate dependencies. This complicates the application of data derived from 'surrogate' spectra to predictions in other flux-spectra environments. It is also shown in this paper that one must be sensitive to the impact of previously -ignored 'small' variations in neutron spectra within a given reactor. In some materials these small variations have major consequences. (author)

  17. Total β-decay energies of neutron-rich zinc isotopes, A=75-80

    International Nuclear Information System (INIS)

    Lund, E.; Aleklett, K.; Fogelberg, B.; Sangariyavanish, A.

    1984-01-01

    The present investigation involves improved measurements of the Qsub(β)-values of 75-78 Zn and determinations of the total decay energies of sup(79,80)Zn which are not reported in the literature before. Also 81 Zn was detected but at the time for the experiment the ion-source was not efficient enough to yield sufficient activity for an accurate Qsub(β)-determination. (orig./HSI)

  18. Total neutron-counting plutonium inventory measurement systems (PIMS) and their potential application to near real time materials accountancy (NRTMA)

    International Nuclear Information System (INIS)

    Driscall, I.; Fox, G.H.; Orr, C.H.; Whitehouse, K.R.

    1988-01-01

    A radiometric method of determining the inventory of an operating plutonium plant is described. An array of total neutron counters distributed across the plant is used to estimate hold-up at each plant item. Corrections for the sensitivity of detectors to plutonium in adjacent plant items are achieved through a matrix approach. This paper describes our experience in design, calibration and operation of a Plutonium Inventory Measurement System (PIMS) on an oxalate precipitation plutonium finishing line. Data from a recent trial of Near-Real-Time Materials Accounting (NRTMA) using the PIMS are presented and used to illustrate its present performance and problem areas. The reader is asked to consider what role PIMS might have in future accountancy systems

  19. Chromium Fractions Changes Compared With Total-Cr As Determined by Neutron Activation Analysis Technique

    International Nuclear Information System (INIS)

    Abdel-Sabour, M.F.; Abdou, F.M.; Elwan, I.M.; Al-Salama, Y.J.

    2003-01-01

    Fifteen soil samples were chosen from different locations (five different locations at north greater Cairo, Egypt to represent different soils (alluvial and sandy) as well as different source of contaminated wastewater (sewage and industrial effluent). Using sequential extraction technique (extracting the soil with different solutions, which is designed to separate metal fractions), Cr was separated into six operationally defined fractions water soluble, exchangeable, carbonate bound, Fe-Mn oxides bound, organic bound and residual fractions. Result of soil total-Cr indicated the serious accumulation of Cr in soils subjected to prolonged irrigation with contaminated wastewater. As it could seen, total-Cr in the tested contaminated soils exceeds the permissible levels (75-100)ppm Cr by several order of magnitude particularly at the surface and subsurface layers. The highest accumulation of total Cr down to depth 60 cm was observed in case of soil E. Data showed that values of total Cr determined by NAA method were always higher than the relevant values determined either by AAS or those calculated after the sequential extraction method. T-test analysis showed the significant difference between NAA and either AAS or sequential extraction methods. Although T-test analysis showed that were significant differences between total content in soils as determined by destructive (AAS or SUM) and non-destructive (NAA) analytical techniques however, strong liner relation between NAA and other tested methods was obtained. Chromium distribution between different extractants shows that the greatest amounts are found in the residual and Occluded in Fe and Mn-Oxides fractions followed by carbonate or organic fractions. In most cases the proportion of all tested Cr-forms has increased in contaminated soil layers with higher enrichment in organically bound Cr, occluded in Fe and Mn oxides, carbonate exchangeable and soluble fractions. Results indicate that soil properties have a

  20. Nuclear structure effects on calculated fast neutron reaction cross sections

    International Nuclear Information System (INIS)

    Avrigeanu, V.

    1992-01-01

    The importance of accurate low-lying level schemes for reaction cross section calculation and need for microscopically calculated levels are proved with reference to fast neutron induced reactions in the A = 50 atomic mass range. The uses of the discrete levels both for normalization of phenomenological level density approaches and within Hauser-Feshbach calculations are discussed in this respect. (Author)

  1. Hygrothermal degradation of (3-glycidoxypropyl)trimethoxysilane films studied by neutron and X-ray reflectivity and attenuated total reflection infrared spectroscopy

    International Nuclear Information System (INIS)

    Tallant, David Robert; Garcia, Manuel Joseph; Majewski, Jaroslaw; Kent, Michael Stuart; Yim, Hyun

    2005-01-01

    Thin films of organosilanes have great technological importance in the areas of adhesion promotion, durability, and corrosion resistance. However, it is well-known that water can degrade organosilane films, particularly at elevated temperatures. In this work, X-ray and neutron reflectivity (XR and NR) were combined with attenuated total reflection infrared (ATR-IR) spectroscopy to study the chemical and structural changes within thin films of (3-glycidoxypropyl)trimethoxysilane (GPS) after exposure for various periods of time to air saturated with either D 2 O or H 2 O at 80 C. For NR and XR, ultrathin (∼100 (angstrom)) films were prepared by spin-coating. Both D 2 O and H 2 O provide neutron scattering contrast with GPS. Variations in the neutron scattering length density (SLD) profiles (a function of mass density and atomic composition) with conditioning time were measured after drying the samples out and also swelled with H 2 O or D 2 O vapor at room temperature. For samples that were dried out prior to measurement, little or no change was observed for H 2 O conditioning up to 3.5 days, but large changes were observed after 30 days of conditioning. The range of conditioning time for this structural change was narrowed to between 4 and 10 days with XR. The SLD profiles indicated that the top portion of the GPS film was transformed into a thick low-density layer after conditioning, but the bottom portion showed little structural change. A previous NR study of as-prepared GPS films involving swelling with deuterated nitrobenzene showed that the central portion of the film has much lower cross-link density than the region nearest the substrate. The present data show that the central portion also swells to a much greater extent with water and hydrolyzes more rapidly. The chemical degradation mechanism was identified by IR as hydrolysis of siloxane bonds. For ATR-IR, GPS films were prepared by dip-coating, which resulted in a greater and more variable thickness than

  2. Correlation between locally deformed structure and oxide film properties in austenitic stainless steel irradiated with neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Chimi, Yasuhiro, E-mail: chimi.yasuhiro@jaea.go.jp [Japan Atomic Energy Agency (JAEA), 2-4 Shirakata, Tokai-mura, Naka-gun, Ibaraki 319-1195 (Japan); Kitsunai, Yuji [Nippon Nuclear Fuel Development, 2163 Narita-cho, Oarai-machi, Higashi-ibaraki-gun, Ibaraki 311-1313 (Japan); Kasahara, Shigeki [Japan Atomic Energy Agency (JAEA), 2-4 Shirakata, Tokai-mura, Naka-gun, Ibaraki 319-1195 (Japan); Chatani, Kazuhiro; Koshiishi, Masato [Nippon Nuclear Fuel Development, 2163 Narita-cho, Oarai-machi, Higashi-ibaraki-gun, Ibaraki 311-1313 (Japan); Nishiyama, Yutaka [Japan Atomic Energy Agency (JAEA), 2-4 Shirakata, Tokai-mura, Naka-gun, Ibaraki 319-1195 (Japan)

    2016-07-15

    To elucidate the mechanism of irradiation-assisted stress corrosion cracking (IASCC) in high-temperature water for neutron-irradiated austenitic stainless steels (SSs), the locally deformed structures, the oxide films formed on the deformed areas, and their correlation were investigated. Tensile specimens made of irradiated 316L SSs were strained 0.1%–2% at room temperature or at 563 K, and the surface structures and crystal misorientation among grains were evaluated. The strained specimens were immersed in high-temperature water, and the microstructures of the oxide films on the locally deformed areas were observed. The appearance of visible step structures on the specimens' surface depended on the neutron dose and the applied strain. The surface oxides were observed to be prone to increase in thickness around grain boundaries (GBs) with increasing neutron dose and increasing local strain at the GBs. No penetrative oxidation was observed along GBs or along surface steps. - Highlights: • Visible step structures depend on the neutron dose and the applied strain. • Local strain at grain boundaries was accumulated with the neutron dose. • Oxide thickness increases with neutron dose and local strain at grain boundaries. • No penetrative oxidation was observed along grain boundaries or surface steps.

  3. Determination of trace elements in total particulate matter of cigarette smoke by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Mishra, U.C.; Shaikh, G.N.

    1985-01-01

    Cigarette smoke contains many trace elements hazardous for human body. Tobacco samples were analyzed for their trace element contents and the results were reported earlier. This paper presents results on the trace element content analyzed in cigarette smoke using an automatic smoking machine developed in laboratory to simulate actual smoking pattern. The trace element levels in the total particulate matter samples of the cigarette smoke collected on filter papers were measured and compared with those of cigarette smoke condensate reported in the literature. Both methods of collection give comparable results. (author)

  4. Measurement of Neutron Total Cross Sections in Support of the APT Program

    International Nuclear Information System (INIS)

    Abfalterer, W.P.; Haight, R.C.; Morgan, G.L.; Bateman, F.B.; Dietrich, F.S.; Finlay, R.W.

    1998-01-01

    The authors have completed a new set of total cross section measurements of 37 samples spanning the periodic table. The authors employed the same technique as in a previous measurement, with refinements intended to allow measurements on separated isotopes, and with improved systematic error control. The goal of the new measurement was 1% statistical accuracy in 1% energy bins with systematic errors less than 1%. This was achieved for all but the smallest samples, for which the statistical accuracy was as large as 2% in 1% bins

  5. Bone structure investigation using X-ray and neutron radiography techniques

    International Nuclear Information System (INIS)

    Kamali Moghaddam, K.; Taheri, T.; Ayubian, M.

    2008-01-01

    In this paper we report a study of the periodic variation of bone tissue humidity immediately after death using both neutron and X-ray radiography techniques. After death, bone tissue experiences sequential change over time. This change consists of organic and inorganic phase variations of the bone structure, as well as gradual reduction of the bone's water content. These variations are investigated by periodically imaging dead bone using X-ray and neutron radiography. Chemical separation techniques such as calcification and decalcification were used to separate the organic and inorganic phases of the bone. Comparison between X-ray and neutron radiographs of bone following phase separation can be potentially used to investigate the bone disease or to determine a cause of death. In our experiments, we use adult rat femur bones, and the interpretations of these results are presented based on our understanding of bone structure and images produced by neutron and X-ray photon interactions

  6. Bone structure investigation using X-ray and neutron radiography techniques

    Energy Technology Data Exchange (ETDEWEB)

    Kamali Moghaddam, K. [Nuclear Research Center (NRC), Atomic Energy Organization of Iran (AEOI), P.O. Box 11365-8486, Tehran (Iran, Islamic Republic of)], E-mail: kkamali@aeoi.org.ir; Taheri, T.; Ayubian, M. [Nuclear Research Center (NRC), Atomic Energy Organization of Iran (AEOI), P.O. Box 11365-8486, Tehran (Iran, Islamic Republic of)

    2008-01-15

    In this paper we report a study of the periodic variation of bone tissue humidity immediately after death using both neutron and X-ray radiography techniques. After death, bone tissue experiences sequential change over time. This change consists of organic and inorganic phase variations of the bone structure, as well as gradual reduction of the bone's water content. These variations are investigated by periodically imaging dead bone using X-ray and neutron radiography. Chemical separation techniques such as calcification and decalcification were used to separate the organic and inorganic phases of the bone. Comparison between X-ray and neutron radiographs of bone following phase separation can be potentially used to investigate the bone disease or to determine a cause of death. In our experiments, we use adult rat femur bones, and the interpretations of these results are presented based on our understanding of bone structure and images produced by neutron and X-ray photon interactions.

  7. Numerical Simulations of Pillar Structured Solid State Thermal Neutron Detector Efficiency and Gamma Discrimination

    Energy Technology Data Exchange (ETDEWEB)

    Conway, A; Wang, T; Deo, N; Cheung, C; Nikolic, R

    2008-06-24

    This work reports numerical simulations of a novel three-dimensionally integrated, {sup 10}boron ({sup 10}B) and silicon p+, intrinsic, n+ (PIN) diode micropillar array for thermal neutron detection. The inter-digitated device structure has a high probability of interaction between the Si PIN pillars and the charged particles (alpha and {sup 7}Li) created from the neutron - {sup 10}B reaction. In this work, the effect of both the 3-D geometry (including pillar diameter, separation and height) and energy loss mechanisms are investigated via simulations to predict the neutron detection efficiency and gamma discrimination of this structure. The simulation results are demonstrated to compare well with the measurement results. This indicates that upon scaling the pillar height, a high efficiency thermal neutron detector is possible.

  8. Proposal to extend CSEWG neutron and photon multigroup structures for wider applications

    International Nuclear Information System (INIS)

    LaBauve, R.J.; Wilson, W.B.

    1976-02-01

    The 239-group neutron multigroup structure recommended by the Codes and Formats Subcommittee of the cross section evaluation working group (CSEWG) for use in LMFBR design is not well suited for application in certain other areas, particularly thermal reactor design. This report describes a proposal for a neutron group structure consisting of 347 groups, which is an extension of the CSEWG group structure into the thermal range, and also includes more detail in other energy ranges important in LWR, HTGR, GCFR, and CTR design. Similarly, a proposed extension of the CSEWG 94-group photon multigroup structure to 103 groups is described. A subset of the neutron multigroup structure, consisting of 154 groups and for use in power reactor studies, is also presented

  9. Proposal to extend CSEWG neutron and photon multigroup structures for wider applications. [Tables

    Energy Technology Data Exchange (ETDEWEB)

    LaBauve, R.J.; Wilson, W.B.

    1976-02-01

    The 239-group neutron multigroup structure recommended by the Codes and Formats Subcommittee of the cross section evaluation working group (CSEWG) for use in LMFBR design is not well suited for application in certain other areas, particularly thermal reactor design. This report describes a proposal for a neutron group structure consisting of 347 groups, which is an extension of the CSEWG group structure into the thermal range, and also includes more detail in other energy ranges important in LWR, HTGR, GCFR, and CTR design. Similarly, a proposed extension of the CSEWG 94-group photon multigroup structure to 103 groups is described. A subset of the neutron multigroup structure, consisting of 154 groups and for use in power reactor studies, is also presented.

  10. Dependence of two-neutron momentum densities on total pair momentum

    Energy Technology Data Exchange (ETDEWEB)

    Carlson, Joseph A [Los Alamos National Laboratory; Wiringa, R B [ANL; Schiavilla, R [JEFFERSON LAB; Pieper, Steven C [ANL

    2008-01-01

    Two-nucleon momentum distributions are calculated for the ground states of {sup 3}He and {sup 4}He as a function of the nucleons' relative and total momenta. We use variational Monte Carlo wave functions derived from a realistic Hamiltonian with two- and three-nucleon potentials. The momentum distribution of pp pairs is found to be much smaller than that of pn pairs for values of the relative momentum in the range (300--500) MeV/c and vanishing total momentum. Howeer, as the totalmomentum increases to 400 MeV/c, the ratio of pp to pn pairs in this relative momentum range grows and approaches the limit 1/2 for {sup 3}He and 1/4 for {sup 4}He, corresponding to the ratio of pp to pn pairs in these nuclei. This behavior should be easily observable in two-nucleon knock-out processes, such as A(e, e'pN).

  11. Alteration of sensitivity of intratumor quiescent and total cells to γ-rays following thermal neutron irradiation with or without 10B-compound

    International Nuclear Information System (INIS)

    Masunaga, Shin-ichiro; Ono, Koji; Suzuki, Minoru; Sakurai, Yoshinori; Kobayashi, Tooru; Takagaki, Masao; Kinashi, Yuko; Akaboshi, Mitsuhiko

    2000-01-01

    Purpose: Changes in the sensitivity of intratumor quiescent (Q) and total cells to γ-rays following thermal neutron irradiation with or without 10 B-compound were examined. Methods and Materials: 5-Bromo-2'-deoxyuridine (BrdU) was injected to SCC VII tumor-bearing mice intraperitoneally 10 times to label all the proliferating (P) tumor cells. As priming irradiation, thermal neutrons alone or thermal neutrons with 10 B-labeled sodium borocaptate (BSH) or dl-p-boronophenylalanine (BPA) were administered. The tumor-bearing mice then received a series of γ-ray radiation doses, 0 through 24 h after the priming irradiation. During this period, no BrdU was administered. Immediately after the second irradiation, the tumors were excised, minced, and trypsinized. Following incubation of tumor cells with cytokinesis blocker, the micronucleus (MN) frequency in cells without BrdU labeling (= Q cells at the time of priming irradiation) was determined using immunofluorescence staining for BrdU. The MN frequency in the total (P + Q) tumor cells was determined from the tumors that were not pretreated with BrdU before the priming irradiation. To determine the BrdU-labeled cell ratios in the tumors at the time of the second irradiation, each group also included mice that were continuously administered BrdU until just before the second irradiation using mini-osmotic pumps which had been implanted subcutaneously 5 days before the priming irradiation. Results: In total cells, during the interval between the two irradiations, the tumor sensitivity to γ-rays relative to that immediately after priming irradiation decreased with the priming irradiation ranking in the following order: thermal neutrons only > thermal neutrons with BSH > thermal neutrons with BPA. In contrast, in Q cells, during that time the sensitivity increased in the following order: thermal neutrons only 10 B-compound, especially BPA, in thermal neutron irradiation causes the recruitment from the Q to P population

  12. Group constant preparation for the estimate of neutron induced damage in structural materials

    International Nuclear Information System (INIS)

    Panini, G.C.

    1996-01-01

    Neutron heating (kerma), displacement per atom cross sections (DPA), gas and γ-ray production are important parameters for the estimate of the damage produced by neutron induced nuclear reactions in the structural materials. The NJOY System for Nuclear Data Processing has been extensively used in order to compute the above quantities; here the theory, the algorithms and the connected problems are described. (author). 6 refs, 3 tabs

  13. Fundamentals and applications of neutron diffraction. Applications 7. Crystal structure analysis of fuel cell materials by means of neutron diffractometry

    International Nuclear Information System (INIS)

    Itoh, Takanori

    2010-01-01

    Perovskite oxides, which have 'A' atoms of an alkaline earth metal and/or a rare earth metal and 'B' atoms of a transition metal, have considerable potential for use in electrochemical devices such as cathodes of solid oxide fuel cells (SOFC), oxygen pumps, oxygen sensors, catalysts, and other devices such as oxygen separation membranes. The oxygen ion behavior is studied with relation performance of electrochemical devices. I have analyzed the crystal structure of SOFC materials by neutron diffraction. Using the Rietveld refinement technique, I showed that the O1(4c) and O2(8d) sites in a perovskite oxide of SOFC cathode material has different oxygen site occupancies. Furthermore, oxygen diffusion behavior is associated with temperature dependence of oxygen anisotropic atomic displacement parameters. The maximum entropy method (MEM) analysis of neutron diffraction measurements revealed nuclear scattering length distribution at high temperature by three-dimensional images in detail, therefore 1 found oxygen diffusion pass and new proton site in SOFC materials. From these results, neutron diffraction is confirmed to be very useful tool for the study of light element behavior in fuel cell materials. (author)

  14. Feasibility evaluation of a neutron grating interferometer with an analyzer grating based on a structured scintillator

    Science.gov (United States)

    Kim, Youngju; Kim, Jongyul; Kim, Daeseung; Hussey, Daniel. S.; Lee, Seung Wook

    2018-03-01

    We introduce an analyzer grating based on a structured scintillator fabricated by a gadolinium oxysulfide powder filling method for a symmetric Talbot-Lau neutron grating interferometer. This is an alternative way to analyze the Talbot self-image of a grating interferometer without using an absorption grating to block neutrons. Since the structured scintillator analyzer grating itself generates the signal for neutron detection, we do not need an additional scintillator screen as an absorption analyzer grating. We have developed and tested an analyzer grating based on a structured scintillator in our symmetric Talbot-Lau neutron grating interferometer to produce high fidelity absorption, differential phase, and dark-field contrast images. The acquired images have been compared to results of a grating interferometer utilizing a typical absorption analyzer grating with two commercial scintillation screens. The analyzer grating based on the structured scintillator enhances interference fringe visibility and shows a great potential for economical fabrication, compact system design, and so on. We report the performance of the analyzer grating based on a structured scintillator and evaluate its feasibility for the neutron grating interferometer.

  15. X-Ray and Neutron Scattering Study of the Magnetic Structure of Neodymium Metal

    DEFF Research Database (Denmark)

    Lebech, Bente; Als-Nielsen, Jens Aage; McEwen, K. A.

    1979-01-01

    A combined x-ray and neutron diffraction study has shown that the so-called "triple-q⃗" structure is not the correct model of the magnetic structure of neodymium. The x-ray data showed only the Bragg reflections originating from the double-hcp lattice. Hence, all additional reflections observed...

  16. Long life neutron generator target using deuterium pass-through structure

    Science.gov (United States)

    Alger, D. L.

    1974-01-01

    Target structure permits all deuterons, except the one-in-a-million that interacts with tritium atom to produce a neutron, to pass completely through target structure and be returned to vacuum system. Since tritium atoms are not displaced as in conventional targets, tritium population will remain unchanged while under deuteron bombardment.

  17. Composite structure of helicopter rotor blades studied by neutron- and X-ray radiography

    International Nuclear Information System (INIS)

    Balasko, M.; Veres, I.; Molnar, Gy.; Balasko, Zs.; Svab, E.

    2004-01-01

    In order to inspect the possible defects in the composite structure of helicopter rotor blades combined neutron- and X-ray radiography investigations were performed at the Budapest Research Reactor. Imperfections in the honeycomb structure, resin rich or starved areas at the core-honeycomb surfaces, inhomogeneities at the adhesive filling and water percolation at the sealing interfaces of the honeycomb sections were discovered

  18. Composite structure of helicopter rotor blades studied by neutron- and X-ray radiography

    Science.gov (United States)

    Balaskó, M.; Veres, I.; Molnár, Gy.; Balaskó, Zs.; Sváb, E.

    2004-07-01

    In order to inspect the possible defects in the composite structure of helicopter rotor blades combined neutron- and X-ray radiography investigations were performed at the Budapest Research Reactor. Imperfections in the honeycomb structure, resin rich or starved areas at the core-honeycomb surfaces, inhomogeneities at the adhesive filling and water percolation at the sealing interfaces of the honeycomb sections were discovered.

  19. Neutron Star Structure in the Presence of Conformally Coupled Scalar Fields

    Science.gov (United States)

    Sultana, Joseph; Bose, Benjamin; Kazanas, Demosthenes

    2014-01-01

    Neutron star models are studied in the context of scalar-tensor theories of gravity in the presence of a conformally coupled scalar field, using two different numerical equations of state (EoS) representing different degrees of stiffness. In both cases we obtain a complete solution by matching the interior numerical solution of the coupled Einstein-scalar field hydrostatic equations, with an exact metric on the surface of the star. These are then used to find the effect of the scalar field and its coupling to geometry, on the neutron star structure, particularly the maximum neutron star mass and radius. We show that in the presence of a conformally coupled scalar field, neutron stars are less dense and have smaller masses and radii than their counterparts in the minimally coupled case, and the effect increases with the magnitude of the scalar field at the center of the star.

  20. Membrane structure: neutron diffraction and small angle scattering studies

    International Nuclear Information System (INIS)

    Zaccai, G.

    1985-01-01

    The author considers a molecule in a beam of radiation of wavelength lambda. Two extreme ways are shown in which on can have many identical molecules in a sample: a crystal in which they are related to each other by the symmetry of a lattice, and complete disorder in which there is no correlation between molecules. The detailed crystallographic analysis of isomorphous replacement is examined. Neutron diffraction experiments with specific deuteration are performed to characterize interactions of cholesterol with lipid bilayers. Retinal rod outer segment disk membranes and the purple membrane of H. halobium are examined

  1. Recognition of internal structure of unknown objects with simultaneous neutron and gamma radiography

    International Nuclear Information System (INIS)

    Moghadam, K.K.; Nasseri, M.M.

    2004-01-01

    Generally speaking in customary industrial and medical radiography, there is no tendency to reveal the nature of the samples. Ordinarily, the main objective of taking a radiograph is to show the position and dimension of unknown parts, inside the test object and to determine cracks, defects, etc. Whereas in radiography many important factors such as material cross-sections and build-up factors are also involved. In this paper, by using both neutron and gamma radiography techniques, some mathematical relations were successfully generated, in order to calculate the neutron and gamma total macroscopic cross-sections of some unknown elements in the presence of the other elements. For this work, some test pieces were defined and made of lead, silver, copper, Nickel, tin, graphite and polyethylene. The neutron radiography facility at Tehran Research Reactor (TRR) was used as mixed neutron and gamma radiography source (Proceedings of the Second World Conference on Neutron Radiography, Paris, France, pp. 25-32). On testing of a correction of the above-mentioned generated relations, a new technique of simultaneous neutron and gamma radiography was also investigated

  2. Structure of Insulin: Results of joint neutron and X-ray refinement

    Energy Technology Data Exchange (ETDEWEB)

    Wlodawer, A; Savage, H; Dodson, G

    1989-02-01

    Neutron diffraction data for porcine 2Zn insulin were collected to 2.2 A resolution from a single crystal deuterated by slow exchange of mother liquor. A joint neutron/X-ray restrained-least-squares refinement was undertaken using the neutron data, as well as the 1.5 A resolution X-ray data collected previously. The final R factors were 0.182 for the X-ray data and 0.191 for the neutron data. Resulting atomic coordinates were compared with the initial X-ray model, showing a total r.m.s. shift of 0.36 A for the protein and 0.6 A for the solvent. Protonation of a number of individual amino acids was investigated by analysis of the neutron maps. No D atoms were found between the carboxylates of Glu B13 which make an intermolecular contact, suggesting nonbonded interaction rather than the predicted hydrogen bond. Amide hydrogen exchange was investigated in a refinement of their atomic occupancies. Regions of unexchanged amide groups were found in the center of the B helices. The results of this study emphasize the limited amount of information available in neutron diffraction studies of proteins at resolution lower than 2 A.

  3. Yield of Prompt Gamma Radiation in Slow-Neutron Induced Fission of 235U as a Function of the Total Fragment Kinetic Energy

    Energy Technology Data Exchange (ETDEWEB)

    Albinsson, H [Chalmers Univ. of Technology, Goeteborg (SE)

    1971-07-01

    Fission gamma radiation yields as functions of the total fragment kinetic energy were obtained for 235U thermal-neutron induced fission. The fragments were detected with silicon surface-barrier detectors and the gamma radiation with a Nal(Tl) scintillator. In some of the measurements mass selection was used so that the gamma radiation could also be measured as a function of fragment mass. Time discrimination between the fission gammas and the prompt neutrons released in the fission process was employed to reduce the background. The gamma radiation emitted during different time intervals after the fission event was studied with the help of a collimator, the position of which was changed along the path of the fission fragments. Fission-neutron and gamma-ray data of previous experiments were used for comparisons of the yields, and estimates were made of the variation of the prompt gamma-ray energy with the total fragment kinetic energy

  4. Corporate financial structure, misallocation and total factor productivity

    NARCIS (Netherlands)

    Uras, R.B.

    2014-01-01

    This paper studies the quantitative relevance of the cross-sectional dispersion of corporate financial structure in explaining the intra-industry allocation efficiency of productive factors. I solve a heterogeneous firms model with financial constraints and distortions to the marginal rental-rate of

  5. Space-time structure of neutron and X-ray sources in a plasma focus

    International Nuclear Information System (INIS)

    Bostick, W.H.; Nardi, V.; Prior, W.

    1977-01-01

    Systematic measurements with paraffin collimators of the neutron emission intensity have been completed on a plasma focus with a 15-20 kV capacitor bank (hollow centre electrode; discharge period T approximately 8 μs; D 2 filling at 4-8 torr). The space resolution was 1 cm or better. These data indicate that at least 70% of the total neutron yield originates within hot-plasma regions where electron beams and high-energy D beams (approximately > 0.1-1 MeV) are produced. The neutron source is composed of several (approximately > 1-10) space-localized sources of different intensity, each with a duration approximately less than 5 ns (FWHM). Localized neutron sources and hard (approximately > 100 keV) X-ray sources have the same time multiplicity and are usually distributed in two groups over a time interval 40-400 ns long. By the mode of operation used by the authors one group of localized sources (Burst II) is observed 200-400 ns after the other group (Burst I) and its space distribution is broader than for Burst I. The maximum intensity of a localized source of neutrons in Burst I is much higher than the maximum intensity in Burst II. Secondary reactions T(D,n) 4 He (from the tritium produced only by primary reactions in the same discharge; no tritium was used in filling the discharge chamber) are observed in a time coincidence with the strongest D-D neutron pulse of Burst I. The neutron signal from a localized source with high intensity has a relatively long tail of small amplitude (area tail approximately less than 0.2 X area peak). This tail can be generated by the D-D reactions of the unconfined part of an ion beam in the cold plasma. Complete elimination of scattered neutrons on the detector was achieved in these measurements. (author)

  6. Nuclear structure for the crust of neutron stars and exotic nuclei

    International Nuclear Information System (INIS)

    Goegelein, Peter

    2007-01-01

    In this work the Skyrme Hartree-Fock and Relativistic Hartree--Fock approaches have been considered to describe the structure of nuclear systems ranging from finite nuclei, structures in the crust of neutron stars to homogeneous matter. Effects of pairing correlations and finite temperature are also taken into account. The numerical procedure in the cubic box is described for the Skyrme Hartree-Fock as well as the relativistic Hartree-Fock approach. And finally, results for the crust of neutron stars and exotic nuclei are presented and discussed. (orig.)

  7. Structure investigations on Portland cement paste by small angle neutron scattering

    International Nuclear Information System (INIS)

    Dragolici, C.A.; Lin, A.

    2004-01-01

    Hydrated Portland cement is a very complex material. Cement paste consists of many crystalline and non-crystalline phases in various ranges of sizes (μm and nm scale). The crystalline phases are embedded in amorphous phases of hydration products. We investigated the structural changes of hydrating phases in a time interval up to 18 days, at Budapest Neutron Center's SANS spectrometer. The small angle neutron scattering of Portland cements prepared with a various water-to-cement ratios, gave us information about the microstructure changes in the material. Fractals were a suitable way for structure modelling. Some comments regarding the opportunity of using the most common models are pointed out. (authors)

  8. Nuclear structure for the crust of neutron stars and exotic nuclei

    Energy Technology Data Exchange (ETDEWEB)

    Goegelein, Peter

    2007-07-01

    In this work the Skyrme Hartree-Fock and Relativistic Hartree--Fock approaches have been considered to describe the structure of nuclear systems ranging from finite nuclei, structures in the crust of neutron stars to homogeneous matter. Effects of pairing correlations and finite temperature are also taken into account. The numerical procedure in the cubic box is described for the Skyrme Hartree-Fock as well as the relativistic Hartree-Fock approach. And finally, results for the crust of neutron stars and exotic nuclei are presented and discussed. (orig.)

  9. Molecular structure and correlations in liquid D-2-propanol through neutron diffraction

    International Nuclear Information System (INIS)

    Sahoo, A.; Sarkar, S.; Joarder, R.N.; Krishna, P.S.R.

    2003-01-01

    Like t-butanol, 2-propanol molecules are quite big with substantial amount of asymmetry in the structure and so the analysis of the neutron diffraction data is tricky. A modified method of analysis, similar to one for liquid t-butanol, enables extraction of the detailed molecular conformation and intermolecular correlations through neutron diffraction. The pre-peak in the structure function, a signature of chain molecular association together with partially identified inter-molecular correlations yield some information about the nature of possible H-bonded molecular clusters in the liquid state. (author)

  10. Crystal structure solution of hydrides containing natEu from neutron powder diffraction data

    International Nuclear Information System (INIS)

    Kohlmann, H.

    1999-01-01

    Complete text of publication follows. The location of hydrogen in crystal structures of metal hydrides usually requires neutron diffraction data. Some elements, however, show excessively high absorption cross sections, σ a , for neutrons, thus making this technique seemingly impractical. Therefore no complete, refined crystal structure data of europium hydrides (σ a ( nat Eu) = .4530 barns at λ = 179.8 pm [1]) have been reported so far. It is shown that the absorption can be reduced to a value reasonable for neutron diffraction experiments by taking advantage of the wavelength dependence of σ a combined with the use of annular samples at advanced diffractometers. Neutron powder diffraction data on several nat Eu containing deuterides suitable for the ab initio crystal structure solution and refinement have been taken at D20 and D4 (ILL, Grenoble). The crystal chemistry of these europium hydrides, among them the two new compounds EuMg 2 H 6 and EuMgH 4 [2], is discussed. (author) [1] V.F. Sears, Neutron News 1992, 3, 26-37.; [2] H. Kohlmann, F. Gingl, T. Hansen, K. Yvon, Angew. Chem. Int. Ed. Eng. 1999, 38, accepted

  11. Influence of coated particle structure in thermal neutron spectrum energy range

    Energy Technology Data Exchange (ETDEWEB)

    Hansen, U; Teuchert, E

    1971-02-15

    The heterogenity due to lumping the fuel in coated particles affects the thermal neutron spectrum. A calculation model is discussed which, apart from some simplifying assumptions about the statistical distribution, allows a rigorous computation of effective cross sections for all nuclides of the heterogeneous medium. It is based on an exact computation of the neutron penetration probability through coating and kernel. The model is incorporated in a THERMOS-code providing a double heterogeneous cell calculation, which can be repeated automatically at different time steps in the depletion code system MAFIA-V.S.O.P.. A discussion of the effects of the coated particle structure is given by a comparison of calculations for heterogeneous and homogeneous fuel zones in pebble bed reactor elements. This is performed for enriched UO{sub 2} fuel and for a ThO{sub 2}-PuO{sub 2} mixture in the grains. Depending on the energy dependent total sigmas in the kernels the changes of the cross sections are ranging from 0.1% up to 45%. The influence on the spectrum averaged sigmas of the nuclides in the fresh UO{sub 2} fuel is lower than 1%. For the emerging {sup 240}Pu it increases up to 3.3% during irradiation. For the ThO{sub 2}-PuO{sub 2} fuel the averaged sigmas of the isotopes vary from 0.5% to 5.7% depending on the state of irradiation. Correspondingly there is an influence on the plutonium isotopic composition, on breeding ratios, and on the tilt of k{sub eff} during burnup which will be discussed in detail.

  12. Total body calcium by neutron activation analysis in normals and osteoporotic populations: a discriminator of significant bone mass loss

    International Nuclear Information System (INIS)

    Ott, S.M.; Murano, R.; Lewellen, T.K.; Nelp, W.B.; Chesnut, C.M.

    1983-01-01

    Measurements of total body calcium by neutron activation (TBC) in 94 normal individuals and 86 osteoporotic patients are reported. The ability of TBC to discriminate normal from osteoporotic females was evaluated with decision analysis. Bone mineral content (BMC) by single-photon absorptiometry was also measured. TBC was higher in males (range 826 to 1363 gm vs 537 to 1054 in females) and correlated with height in all normals. In females over age 55 there was a negative correlation with age. Thus, for normals an algorithm was derived to allow comparison between measured TBC and that predicted by sex, age, and height (TBCp). In the 28 normal females over age 55, the TBC was 764 +/- 115 gm vs. 616 +/- 90 in the osteoporotics. In 63 of the osteoporotic females an estimated height, from tibial length, was used to predict TBC. In normals the TBC/TBCp ratio was 1.00 +/- 0.12, whereas in osteoporotic females it was 0.80 +/- 0.12. A receiver operating characteristic curve showed better discrimination of osteoporosis with TBC/TBCp than with wrist BMC. By using Bayes' theorem, with a 25% prevalence of osteoporosis (estimate for postmenopausal women), the posttest probability of disease was 90% when the TBC/TBCp ratio was less than 0.84. The authors conclude that a low TBC/TBCp ratio is very helpful in determining osteoporosis

  13. Study of the molecular structure and dynamics of bakelite with neutron cross section measurements; Estudo da estrutura e da dinamica moleculares da baquelite atraves de medidas de secoes de choque para neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Voi, D L

    1990-06-01

    The molecular structure and dynamics of calcined bakelite were studied with neutron transmission and scattering cross section measurements. The total cross sections determined were correlated with data obtained with infra-red spectroscopy, elemental analysis and other techniques to get the probable molecular formulae of bakelite. The total cross section determined showed a deviation smaller than 5% from the literature values. The frequency distribution as well as overall experimental results allowed to suggest a structural model like polycyclic hydrocarbons for bakelite calcined at 800{sup 0} C. (F.E.). 65 refs, 31 figs, 5 tabs.

  14. The recovery of bone marrow derived GM-CFU in baboons unilaterally exposed to a total body LD50/30d mixed neutron-gamma irradiation

    International Nuclear Information System (INIS)

    Herodin, F.; Orfeuvre, H.; Janodet, D.; Mestries, J.C.; Fatome, M.

    1990-01-01

    The unilateral exposure of baboons to a total body LD 50/30d mixed neutron/gamma irradiation was characterized to be non uniform in dose distribution. The pattern of recovery of granulocyte-macrophage progenitors in bone marrow samples collected from entrance and exit sides respectively is consistent with this observed heterogeneity [fr

  15. Tagged spectator deep-inelastic scattering off the deuteron as a tool to study neutron structure

    International Nuclear Information System (INIS)

    Cosyn, W.; Sargsian, M.

    2016-01-01

    We give an overview of a model to describe deep-inelastic scattering (DIS) off the deuteron with a spectator proton (e+d → e'+X+p s ), based on the virtual nucleon approximation (VNA). The model accounts for the final-state interactions (FSI) of the DIS debris with the spectator proton. Values of the rescattering cross section are obtained by fits to high-momentum spectator data. By using the so-called 'pole extrapolation' method, free neutron structure functions can be obtained by extrapolating low-momentum spectator proton data to the on-shell neutron pole. We apply this method to the BONuS data set and find a surprising Bjorken x dependence, indicating a possible rise of the neutron to proton structure function ratio at high x. (authors)

  16. Neutrons production of very low energy by filtration through graphite and measurement of total cross sections; Production de neutrons de tres basse energie par filtration a travers du graphite et mesure de sections efficaces totales

    Energy Technology Data Exchange (ETDEWEB)

    Ertaud, A; Beauge, R [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1953-07-01

    In this report, we done on the reactor of Chatillon analogous experiences to those of Fermi in Argonne. The temperature of the neutrons filtered ba a more or less thickness of graphite is measured by the method of absorption. This method permits the production and the study of a very low energy neutron beam. (M.B.) [French] Dans ce rapport, nous avons repris sur la pile de Chatillon des experiences analogues a celles de FERMI a Argonne. La temperature des neutrons filtree par une epaisseur plus ou moins grande de graphite est mesuree par la methode d'absorption. Cette methode permettant la production et l'etude d'un faisceau de neutron de tres basse energie. (M.B.)

  17. Neutron activation behavior of NET/ITER divertor structural materials

    International Nuclear Information System (INIS)

    Smid, I.; Weimann, G.; Kny, E.; Kneringer, G.; Reheis, N.

    1995-01-01

    The post-activation behavior of the materials carbon, TZM (99.3 % Mo) and Mo.41Re, as well as of high temperature brazes suitable for their joining after irradiation with 14 MeV neutrons has been evaluated. The activity, dose rate and energy generation after exposure to an ignited fusion plasma is presented for various time steps after shutdown. The impact of the activity and the afterheat production on the handling and storage conditions of retired divertor components is simulated, the required protection for maintenance is discussed. Further the temperature of stored divertor elements after a full time operation in NET was calculated. No major afterheat production will occur and thus no special cooling is to be provided after approximately one month. Taking into account convection and radiation the equilibrium temperature of vertically stored environment/aircooled divertor elements is predicted to be approximately 100 degree C. (author)

  18. Determination of human and Sprague-Dawley rat trimethylseleonium ion and total selenium urine concentrations from endogenous body selenium pool by neutron activation analysis

    International Nuclear Information System (INIS)

    Blotcky, A.J.; Claassen, J.P.; Rack, E.P.

    1992-01-01

    This study determined trimethylselenonium ion [TMSe,(CH 3 ) 3 Se + ] and total organic selenium cationic species urinary excretion values for healthy human subjects and Sprague-Dawley rats fed regular diets. The only source of TMSe was from the endogenous selenium body pool. Total selenium concentration in urine was determined by instrumental neutron activation analysis. TMSe and total selenium cationic species concentrations and percent of total selenium urine excretion were determined by chemical neutron activation analysis and coupled anion-cation exchange chromatography and anion-exchange chromatography, respectively. Within experimental error, mean values for TMSe and cationic species as percent selenium were comparable for both human subjects and Sprague-Dawley rats. This study suggested that TMSe excreated in urine by healthy human subjects and Sprague-Dawley rats fed a normal diet is not a minor but a general metabolite of selenium ingested in a normal diet. (author) 27 refs.; 1 fig.; 2 tabs

  19. Structural and optical properties improvements of PVP/gelatin blends induced by neutron irradiation

    Science.gov (United States)

    Basha, Mohammad Ahmad-Fouad; Hassan, Mohamed Ahmed

    2018-05-01

    Blends of polyvinylpyrrolidone and gelatin were prepared in three different concentrations to study the modifications in their structural and optical properties induced by neutron irradiations with different neutron fluence values from 108 up to 1011 neutron/cm2. X-ray spectroscopy revealed that the irradiation has induced a recrystallization phenomenon in the studied blends and the crystallinity index increased by increasing the neutron fluence due to the breaking of the crystallites. Fourier-transform infrared spectroscopy came to confirm the existence of interactions between interchain groups and a higher compatibility for the irradiated blends. The irradiation induced defects inside the material were responsible for the change in their optical and structural properties. The creation of free radicals or ions inside the conduction bands has led to the increase in the number of carriers on localized states; this has caused the increase in optical conductivity of the irradiated blends as a result of decreasing the energy gaps by increasing the neutron fluence. Results may widen the applications of the gelatin based blends to include optoelectronic devices, organic light emitting devices, solar selective and anti-reflectance bio-coatings, optical organic glass and lenses.

  20. Neutron star evolution and the structure of matter at high density

    International Nuclear Information System (INIS)

    Soyeur, Madeleine.

    1981-09-01

    The structure and properties of neutron stars are determined by the state of cold nuclear matter at high density. In order to investigate the behavior of matter inside neutron stars, observables sensitive to their internal structure have to be calculated and confronted to observations. The thermal radiation of neutron stars seems to be a good candidate to be such observable. It can be shown that the neutrino luminosity of neutron stars, responsible for their cooling in the early stages of their evolution is strongly dependent on possible phase transitions to superfluid nucleons, to pion condensation or to quark matter. The specific heat of matter is also not the same in the various phases expected at high density and is particularly sensitive to the nucleon superfluidity. At present, both the theoretical estimates and the observations of the thermal properties of neutron stars are still quite preliminary. In particular, large uncertainties due to possible reheating mechanisms and magnetic field effects make the theoretical interpretation of the steady radiation of pulsars quite difficult

  1. Evaluation of apoptosis and micronucleation induced by reactor neutron beams with two different cadmium ratios in total and quiescent cell populations within solid tumors

    International Nuclear Information System (INIS)

    Masunaga, Shin-ichiro; Ono, Koji; Sakurai, Yoshinori; Takagaki, Masao; Kobayashi, Tooru; Kinashi, Yuko; Suzuki, Minoru

    2001-01-01

    Purpose: Response of quiescent (Q) and total tumor cells in solid tumors to reactor neutron beam irradiation with two different cadmium (Cd) ratios was examined in terms of micronucleus (MN) frequency and apoptosis frequency, using four different tumor cell lines. Methods and Materials: C57BL mice bearing EL4 tumors, C3H/He mice bearing SCC VII or FM3A tumors, and Balb/c mice bearing EMT6/KU tumors received 5-bromo-2'-deoxyuridine (BrdU) continuously for 5 days via implanted mini-osmotic pumps to label all proliferating (P) cells. Thirty min after i.p. injection of sodium borocaptate- 10 B (BSH), or 3 h after oral administration of p-boronophenylalanine- 10 B (BPA), the tumors were irradiated with neutron beams. The tumors without 10 B-compound administration were irradiated with neutron beams or γ-rays. This neutron beam irradiation was performed using neutrons with two different Cd ratios. The tumors were then excised, minced, and trypsinized. The tumor cell suspensions thus obtained were incubated with cytochalasin-B (a cytokinesis blocker), and the MN frequency in cells without BrdU labeling (=Q cells) was determined using immunofluorescence staining for BrdU. Meanwhile, for apoptosis assay, 6 h after irradiation, tumor cell suspensions obtained in the same manner were fixed, and the apoptosis frequency in Q cells was also determined with immunofluorescence staining for BrdU. The MN and apoptosis frequencies in total (P+Q) tumor cells were determined from the tumors that were not pretreated with BrdU. Results: Without 10 B-compounds, the sensitivity difference between total and Q cells was reduced by neutron beam irradiation. Under our particular neutron beam irradiation condition, relative biological effectiveness (RBE) of neutrons was larger in Q cells than in total cells, and the RBE values were larger for low Cd-ratio than high Cd-ratio neutrons. With 10 B-compounds, both frequencies were increased for each cell population, especially for total cells. BPA

  2. Fission fragment yields and total kinetic energy release in neutron-induced fission of235,238U,and239Pu

    Science.gov (United States)

    Tovesson, F.; Duke, D.; Geppert-Kleinrath, V.; Manning, B.; Mayorov, D.; Mosby, S.; Schmitt, K.

    2018-03-01

    Different aspects of the nuclear fission process have been studied at Los Alamos Neutron Science Center (LANSCE) using various instruments and experimental techniques. Properties of the fragments emitted in fission have been investigated using Frisch-grid ionization chambers, a Time Projection Chamber (TPC), and the SPIDER instrument which employs the 2v-2E method. These instruments and experimental techniques have been used to determine fission product mass yields, the energy dependent total kinetic energy (TKE) release, and anisotropy in neutron-induced fission of U-235, U-238 and Pu-239.

  3. Total cross-section measurements on aluminium, carbon, fluorine and hydrogen for d, d reaction neutrons using the coincidence method (1963); Mesure de la section efficace totale de l'aluminium, du carbone, du fluor et de l'hydrogene pour des neutrons de la reaction d, d par la methode des coincidences (1963)

    Energy Technology Data Exchange (ETDEWEB)

    Ambrosino, G; Sorriaux, A [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1964-07-01

    The experiment described consists in the measurement of the total cross-section of various materials: aluminium, carbon, fluorine and hydrogen, for mono-energetic 2.77 MeV neutrons obtained from the d,d reaction. The measurement is carried out by transmission. The neutrons are detected by means of a plastic scintillator mounted on a 56 AVP photomultiplier, and are isolated from all secondary phenomena (background noise, scattered neutrons) by coincidence with helium 3. which particles are associated to the neutrons from the reaction {sup 2}{sub 1}D ({sup 2}{sub 1}D, n) {sup 3}{sub 2}H The helium 3 particles are detected by a PN junction diode used with inverted polarisation. An absorption exponential has been traced out using measurements made on seven aluminium bars. The accuracy of the total cross-section measurements is about 10{sup -2}. (authors) [French] L'experience exposee dans ce rapport consiste en la mesure des sections efficaces totales de differents materiaux: aluminium, carbone, fluor et hydrogene, pour des neutrons monoenergetiques de 2,77 MeV, obtenus par la reaction d,d. La mesure est faite par transmission. Les neutrons sont detectes par un scintillateur plastique monte sur un photomultiplicateur 56 AVP, et sont separes de tout phenomene secondaire (bruit de fond, neutrons diffuses) par coincidence avec les helium 3, particules associees aux neutrons de la reaction {sup 2}{sub 1}D ({sup 2}{sub 1}D, n) {sup 3}{sub 2}H Les helium 3 sont detectes par une diode a jonction PN utilisee en polarisation inverse. Une exponentielle d'absorption a ete tracee a partir de mesures faites sur sept barreaux d'aluminium. La precision des mesures des sections efficaces totales est de l'ordre de 10{sup -2}. (auteurs)

  4. The shell structure effects in neutron cross section calculation by a ...

    African Journals Online (AJOL)

    The role of the shell structure properties of the nucleus in the calculation of neutron-induced reaction cross-section data based on nuclear reaction theory has been investigated. In this investigation, measured, evaluated and calculated (n.p) reaction cross-section data on la spherical nucleus (i.e. 112Sn) and a deformed ...

  5. Crystalline structure in the confined-deconfined mixed phase: Neutron stars as an example

    International Nuclear Information System (INIS)

    Glendenning, N.K.

    1996-01-01

    We review the differences in first order phase transition of single and multi-component systems, and then discuss the crystalline structure expected to exist in the mixed confined deconfined phase of hadronic matter. The particular context of neutron stars is chosen for illustration. The qualitative results are general and apply for example to the vapor-liquid transition in subsaturated asymmetric nuclear matter

  6. Structure of orthorhombic SrZrO/sub 3/ by neutron powder diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Ahtee, A; Ahtee, M [Helsinki Univ. (Finland). Dept. of Physics; Glazer, A M [Cambridge Univ. (UK). Cavendish Lab.; Hewat, A W [Institut Max von Laue - Paul Langevin, 38 - Grenoble (France)

    1976-12-15

    The room-temperature structure of SrZrO/sub 3/ has been established by neutron powder-profile refinement. The space group is Pbnm and SrZrO/sub 3/ is isostructural with other perovskites, such as CaTiO/sub 3/.

  7. Structure of unilamellar vesicles: Numerical analysis based on small-angle neutron scattering data

    International Nuclear Information System (INIS)

    Zemlyanaya, E. V.; Kiselev, M. A.; Zbytovska, J.; Almasy, L.; Aswal, V. K.; Strunz, P.; Wartewig, S.; Neubert, R.

    2006-01-01

    The structure of polydispersed populations of unilamellar vesicles is studied by small-angle neutron scattering for three types of lipid systems, namely, single-, two-and four-component vesicular systems. Results of the numerical analysis based on the separated-form-factor model are reported

  8. Neutron diffraction analysis of the structure of rod photoreceptor membranes in intact retinas

    Energy Technology Data Exchange (ETDEWEB)

    Yaeger, M; Schoenborn, B; Engelman, D; Moore, P; Stryer, L

    1980-01-01

    Neutron diffraction data have been collected from samples containing ten dark-adapted Rana catesbiana bullfrog retinas in 100, 80, 60, 40, and 30% D/sub 2/O Ringer's solution using a step-scanning Soller slit diffractometer. Diffraction was also recorded from retinas equilibrated in D/sub 2/O solutions with varying osmolarity. Rocking curve experiments demonstrated that the rods are disoriented in a cylindrically symmetrical fashion. Structure factor amplitudes were obtained using semi-automated curve-fitting procedures, and phases were obtained by interpreting the D/sub 2/O-H/sub 2/O and osmotic Patterson maps. In D/sub 2/O Ringer's solution the first four structure factors are -353 +- 25, 246 +- 19, 434 +- 13 and 383 +- 19. Neutron scattering density profiles were calculated to 75 A resolution using these structure factors. These neutron diffraction data are consistent with the view that the lipid bilayer is a major structural motif of the rod outer segment disc membrane. Neutron Fourier syntheses in different mixtures of D/sub 2/O and H/sub 2/O indicate that the intradisc and extradisc spaces are predominantly aqueous, consistent with the increase in the intradisc and extradisc volumes as the Ringer's solution is made more hypotomic. In isotonic Ringer's solution, the thicknesses of the intradisc and extradisc spaces are about 36 A and 160 A, respectively, and the center-to-center separation between the 50 A thick lipid bilayer is 88 A.

  9. Small-Angle Neutron Scattering Study of Structural Changes in Temperature-Sensitive Microgel Colloids

    NARCIS (Netherlands)

    Stieger, M.A.; Richtering, W.; Pedersen, J.S.; Lindner, P.

    2004-01-01

    The structure of temperature-sensitive poly(N-isopropylacrylamide) microgels in dilute suspension was investigated by means of small-angle neutron scattering. A direct modeling expression for the scattering intensity distribution was derived which describes very well the experimental data at all

  10. Laser-spectroscopy studies of the nuclear structure of neutron-rich radium

    Science.gov (United States)

    Lynch, K. M.; Wilkins, S. G.; Billowes, J.; Binnersley, C. L.; Bissell, M. L.; Chrysalidis, K.; Cocolios, T. E.; Goodacre, T. Day; de Groote, R. P.; Farooq-Smith, G. J.; Fedorov, D. V.; Fedosseev, V. N.; Flanagan, K. T.; Franchoo, S.; Garcia Ruiz, R. F.; Gins, W.; Heinke, R.; Koszorús, Á.; Marsh, B. A.; Molkanov, P. L.; Naubereit, P.; Neyens, G.; Ricketts, C. M.; Rothe, S.; Seiffert, C.; Seliverstov, M. D.; Stroke, H. H.; Studer, D.; Vernon, A. R.; Wendt, K. D. A.; Yang, X. F.

    2018-02-01

    The neutron-rich radium isotopes, Ra-233222, were measured with Collinear Resonance Ionization Spectroscopy (CRIS) at the ISOLDE facility, CERN. The hyperfine structure of the 7 s2S10→7 s 7 p P31 transition was probed, allowing measurement of the magnetic moments, quadrupole moments, and changes in mean-square charge radii. These results are compared to existing literature values, and the new moments and change in mean-square charge radii of 231Ra are presented. Low-resolution laser spectroscopy of the very neutron-rich 233Ra has allowed the isotope shift and relative charge radius to be determined for the first time.

  11. Analysis of Crystallographic Structure of a Japanese Sword by the Pulsed Neutron Transmission Method

    Science.gov (United States)

    Kino, K.; Ayukawa, N.; Kiyanagi, Y.; Uchida, T.; Uno, S.; Grazzi, F.; Scherillo, A.

    We measured two-dimensional transmission spectra of pulsed neutron beams for a Japanese sword sample. Atom density, crystalline size, and preferred orientation of crystals were obtained using the RITS code. The position dependence of the atomic density is consistent with the shape of the sample. The crystalline size is very small and shows position dependence, which is understood by the unique structure of Japanese swords. The preferred orientation has strong position dependence. Our study shows the usefulness of the pulsed neutron transmission method for cultural metal artifacts.

  12. Preliminary assessment of the activation of the IFMIF accelerator structure by deuterons and neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Gomes, Itacil C. [Argonne National Lab., IL (United States); Bruhwiler, David L. [Northrop Grumman Corp., Princeton, NJ (United States). Advanced Systems and Technology

    1997-12-01

    This paper presents a preliminary analysis of the IFMF (International Fusion Materials Irradiation Facility) accelerator structure activation by deuterons and neutrons. The main objective of this study is to identify the source terms and to quantify the radioactivity levels at different positions in the accelerator vault. The MCNP code is used to perform radiation transport analysis, the RACC activation code is used for neutron activation analysis, and the cross section library of the LAHET code is used to generate the cross section for the deuteron interaction with the inside surfaces of the accelerator. (author). 10 refs., 5 figs.

  13. Thermal structure of accreting neutron stars and strange stars

    International Nuclear Information System (INIS)

    Miralda-Escude, J.; Paczynski, B.; Haensel, P.

    1990-01-01

    Steady-state models of accreting neutron stars and strange stars are presented, and their properties as a function of accretion rate are analyzed. The models have steady-state envelopes, with stationary hydrogen burning taken into account, the helium shell flashes artificially suppressed, and the crust with a large number of secondary heat sources. The deep interiors are almost isothermal and are close to thermal equilibrium. A large number of models were calculated for many values of the accretion rates, with ordinary, pion-condensed, and strange cores, with and without secondary heat sources in the crust, and with the heavy element content of the accreting matter in the range Z = 0.0002-0.02. All models show a similar pattern of changes as the accretion rate is varied. For low accretion rates, the hydrogen burning shell is unstable; for intermediate rates, the hydrogen burning shell is stable, but helium burning is not; for high rates, the two shell sources burn together and are unstable. 60 refs

  14. Relativistic structure, stability, and gravitational collapse of charged neutron stars

    International Nuclear Information System (INIS)

    Ghezzi, Cristian R.

    2005-01-01

    Charged stars have the potential of becoming charged black holes or even naked singularities. We present a set of numerical solutions of the Tolman-Oppenheimer-Volkov equations that represents spherical charged compact stars in hydrostatic equilibrium. The stellar models obtained are evolved forward in time integrating the Einstein-Maxwell field equations. We assume an equation of state of a neutron gas at zero temperature. The charge distribution is taken as being proportional to the rest mass density distribution. The set of solutions present an unstable branch, even with charge-to-mass ratios arbitrarily close to the extremum case. We perform a direct check of the stability of the solutions under strong perturbations and for different values of the charge-to-mass ratio. The stars that are in the stable branch oscillate and do not collapse, while models in the unstable branch collapse directly to form black holes. Stars with a charge greater than or equal to the extreme value explode. When a charged star is suddenly discharged, it does not necessarily collapse to form a black hole. A nonlinear effect that gives rise to the formation of a shell of matter (in supermassive stars), is negligible in the present simulations. The results are in agreement with the third law of black hole thermodynamics and with the cosmic censorship conjecture

  15. Liquid structure of vanadium tetrachloride from neutron diffraction study

    International Nuclear Information System (INIS)

    Gopala Rao, R.V.; Satpathy, B.M.

    1982-01-01

    Assuming the separation of the intermolecular scattering function into the radial and angular parts and using Egelstaff et al's orientational model for tetrachlorides, the structure of liquid vanadium tetrachloride has been studied. It has been observed that such a separation is approximate for this liquid and the introduction of a third correction term is required to account for the molecular structure function. The chlorine-chlorine partial structure and effective angle-averaged intermolecular chlorine-chlorine potential in the liquid has been evaluated. Without taking the third correction term, introduced to generate theoretically the molecular structure function, the centre structure function has been obtained in an approximate way from the experimentally observed molecular structure function and from it the centre radial distribution function, centre direct correlation function and the angle-averaged vanadium-vanadium effective potential has been evaluated. (author)

  16. PREFACE: Structure and dynamics determined by neutron and x-ray scattering Structure and dynamics determined by neutron and x-ray scattering

    Science.gov (United States)

    Müller-Buschbaum, Peter

    2011-06-01

    Neutron and x-ray scattering have emerged as powerful methods for the determination of structure and dynamics. Driven by emerging new, powerful neutron and synchrotron radiation sources, the continuous development of new instrumentation and novel scattering techniques gives rise to exciting possibilities. For example, in situ observations become possible via a high neutron or x-ray flux at the sample and, as a consequence, morphological transitions with small time constants can be detected. This special issue covers a broad range of different materials from soft to hard condensed matter. Hence, different material classes such as colloids, polymers, alloys, oxides and metals are addressed. The issue is dedicated to the 60th birthday of Professor Winfried Petry, scientific director of the Research Neutron Source Heinz Maier-Leibnitz (FRM-II), Germany, advisor at the physics department for the Bayerische Elite-Akademie, chair person of the Arbeitsgemeinschaft Metall- und Materialphysik of the German Physical Society (DPG) and a member of the professional council of the German Science Foundation (Deutsche Forschungsgemeinschaft, DFG). We would like to acknowledge and thank all contributors for their submissions, which made this special issue possible in the first place. Moreover, we would like to thank the staff at IOP Publishing for helping us with the administrative aspects and for coordinating the refereeing process, and Valeria Lauter for the beautiful cover artwork. Finally, to the readers, we hope that you find this special issue a valuable resource that provides insights into the present possibilities of neutron and x-ray scattering as powerful tools for the investigation of structure and dynamics. Structure and dynamics determined by neutron and x-ray scattering contents In situ studies of mass transport in liquid alloys by means of neutron radiography F Kargl, M Engelhardt, F Yang, H Weis, P Schmakat, B Schillinger, A Griesche and A Meyer Magnetic spin

  17. Developments of the neutron scattering analysis method for the determination of magnetic structures

    Energy Technology Data Exchange (ETDEWEB)

    Park, Je-Geun; Chung, Jae Gwan; Park, Jung Hwan; Kong, Ung Girl [Inha Univ., Incheon (Korea); So, Ji Yong [Seoul National University, Seoul(Korea)

    2001-04-01

    Neutron diffraction is up to now almost the only and very important experimental method of determining the magnetic structure of materials. Unlike the studies of crystallographic structure, however to use neutron diffraction for magnetic structure determination is not easily accessible to non-experts because of the complexity of magnetic group theory: which is very important in the magnetic structure analysis. With the recent development of computer code for magnetic group, it is now time to rethink of these difficulties. In this work, we have used the computer code of the magnetic group (Mody-2) and Fullprof refinement program in order to study the magnetic structure of YMnO{sub 3} and other interesting materials. YMnO{sub 3} forms in the hexagonal structure and show both ferroelectric and antiferromagnetic phase transitions. Since it was recently found that YMnO{sub 3} can be used as a nonvolatile memory device, there has been many numbers of applied research on this material. We used neutron diffraction to determine the magnetic structure, and, in particular, to investigate the correlation between the order parameters of the ferroelectric and antiferromagnetic phase transitions. From this study, we have demonstrated that with a proper use of the computer code of the magnetic group one can overcome most of difficulties arising from the magnetic group theory. 4 refs., 8 figs., 5 tabs. (Author)

  18. Nuclear structure far from stability: the neutron-rich 69-79Cu isotopes

    International Nuclear Information System (INIS)

    Franchoo, Serge

    2015-01-01

    Far from stability, the nuclear structure that is predicted by the shell model is evolving. Old magic numbers disappear, while new ones appear. Our understanding of the underlying nuclear force that drives these changes is still incomplete. After a short overview across the nuclear chart, we discuss the strength functions of the shell-model orbitals in the neutron-rich copper isotopes towards the 78 Ni doubly-magic nucleus. These were measured in a 72 Zn(d, 3 He) 71 Cu proton pick-up reaction in inverse kinematics with a radioactive beam at the Ganil laboratory in France. We also present the latest results from a 80 Zn(p,2p) 79 Cu knockout experiment at Riken in Japan, leading to selective population of hole states in 79 Cu. Our findings show that the Z=28 shell gap in the neutron-rich copper isotopes is surprisingly steady against the addition of neutrons beyond N=40. (author)

  19. Effects of deformations and orientations on neutron-halo structure of light-halo nuclei

    International Nuclear Information System (INIS)

    Sawhney, Gudveen; Gupta, Raj K.; Sharma, Manoj K.

    2013-01-01

    The availability of radioactive nuclear beams have enabled to study the structure of nuclei far from the stability line, which in turn led to the discovery of neutron-halo nuclei. These nuclei, located near the neutron drip-line exhibit a high probability of presence of one or two loosely bound neutrons at a large distance from the rest of nucleons. The fragmentation behavior is studied for 13 cases of 1n-halo nuclei, which include 11 Be, 14 B, 15 C, 17 C, 19 C, 22 N, 22 O, 23 O, 24 O, 24 F, 26 F, 29 Ne and 31 Ne, using the cluster-core model (CCM) extended to include the deformations and orientations of nuclei

  20. Magnetic structure of the swedenborgite CaBa (Co3Fe ) O7 derived by unpolarized neutron diffraction and spherical neutron polarimetry

    Science.gov (United States)

    Qureshi, N.; Díaz, M. T. Fernández; Chapon, L. C.; Senyshyn, A.; Schweika, W.; Valldor, M.

    2018-02-01

    We present a study that combines polarized and unpolarized neutrons to derive the magnetic structure of the swedenborgite compound CaBa (Co3Fe ) O7. Integrated intensities from a standard neutron diffraction experiment and polarization matrices from spherical neutron polarimetry have been simultaneously analyzed revealing a complex order, which differs from the usual spin configurations on a kagome lattice. We find that the magnetic structure is well described by a combination of two one-dimensional representations corresponding to the magnetic superspace symmetry P 21' , and it consists of spins rotating around an axis close to the [110] direction. Due to the propagation vector q =(1/3 00 ) , this modulation has cycloidal and helicoidal character rendering this system a potential multiferroic. The resulting spin configuration can be mapped onto the classical √{3 }×√{3 } structure of a kagome lattice, and it indicates an important interplay between the kagome and the triangular layers of the crystal structure.

  1. The electronic band structures of gadolinium chalcogenides: a first-principles prediction for neutron detecting.

    Science.gov (United States)

    Li, Kexue; Liu, Lei; Yu, Peter Y; Chen, Xiaobo; Shen, D Z

    2016-05-11

    By converting the energy of nuclear radiation to excited electrons and holes, semiconductor detectors have provided a highly efficient way for detecting them, such as photons or charged particles. However, for detecting the radiated neutrons, those conventional semiconductors hardly behave well, as few of them possess enough capability for capturing these neutral particles. While the element Gd has the highest nuclear cross section, here for searching proper neutron-detecting semiconductors, we investigate theoretically the Gd chalcogenides whose electronic band structures have never been characterized clearly. Among them, we identify that γ-phase Gd2Se3 should be the best candidate for neutron detecting since it possesses not only the right bandgap of 1.76 eV for devices working under room temperature but also the desired indirect gap nature for charge carriers surviving longer. We propose further that semiconductor neutron detectors with single-neutron sensitivity can be realized with such a Gd-chalcogenide on the condition that their crystals can be grown with good quality.

  2. A Unified Equation of State on a Microscopic Basis : Implications for Neutron Stars Structure and Cooling

    Science.gov (United States)

    Burgio, G. F.

    2018-03-01

    We discuss the structure of Neutron Stars by modelling the homogeneous nuclear matter of the core by a suitable microscopic Equation of State, based on the Brueckner-Hartree-Fock many-body theory, and the crust, including the pasta phase, by the BCPM energy density functional which is based on the same Equation of State. This allows for a uni ed description of the Neutron Star matter over a wide density range. A comparison with other uni ed approaches is discussed. With the same Equation of State, which features strong direct Urca processes and using consistent nuclear pairing gaps as well as effective masses, we model neutron star cooling, in particular the current rapid cooldown of the neutron star Cas A. We nd that several scenarios are possible to explain the features of Cas A, but only large and extended proton 1 S 0 gaps and small neutron 3 PF 2 gaps can accommodate also the major part of the complete current cooling data.

  3. Investigation of neutron radiation effects in structural materials for CTR use

    International Nuclear Information System (INIS)

    Wiffen, F.W.

    1975-01-01

    Neutron irradiation of structural materials in the high-flux region of a Controlled Thermonuclear Reactor (CTR), especially in the first wall of the reactor, will result in swelling due to cavity formation and loss of ductility through both lattice hardening and the effect of transmutation-produced helium on the fracture mode. The intensity and relative importance of the effects will be a strong function of the material and reactor operating conditions. A consideration of the effects of the 14 MeV D-T fusion neutrons, based on calculated damage response, on the sparse available data from high-energy neutron irradiation, and on an intuitive understanding of past radiation effects experimentation, suggests that although the 14 MeV neutrons will produce damage at a higher rate than lower-energy neutrons, there is no basis for anticipating different forms of damage. Irradiation experiments designed to evaluate materials for CTR service must be conducted in a number of facilities. Used in a well-coordinated evaluation program, the combined results from all available irradiation facilities will lead to an understanding of the radiation effects that will occur in CTRs. The experimental program will involve three distinct phases: (a) correlation experiments, (b) screening studies, and (c) qualification and design data generation. Each of these phases will evaluate a number of physical and mechanical properties. The end result of this program will be the qualification of a few materials for CTR use

  4. Study of the structure of light neutron rich nucleus with the Tonnerre array

    International Nuclear Information System (INIS)

    Pietri, St.

    2003-06-01

    This work concern the technical development made on the multidetector TONNERRE and the study of the 34 Si nucleus by a complete beta-neutron-gamma spectroscopy. In the first part various tests performed on modules of the detector in the 'Centre d'Etude de Bruyere le Chatel' are presented. A modification of the embassies of the photomultipliers tubes allows to gain more than 50% in the neutron efficiency and to obtain a threshold lower than 300 keV for the neutron energy. A complete C++ simulation of the neutron propagation in the array was carried out. It explains that the slow component of the light output of the scintillator may be responsible of the shape of the time-of-flight spectrum. The second part of these report presents the experiment devoted to the study of the structure of the 34 Si from the beta decay of the 34 Al. It was performed at the GANIL facility using the TONNERRE array and germanium of ENOGAM. The 34 Al was produced by projectile fragmentation of a 36 S beam of 50 MeV/A in a target of 9 Be. A complete beta scheme of the 34 Al is proposed. Eight neutron lines following the 34 Al decay were observed for the first time. Finally we suggest that a monopolar transition could occur in the 34 Si nucleus signing a O + 2 state at 2133 keV. (author)

  5. Symmetry analysis in neutron diffraction studies of magnetic structures. IV

    International Nuclear Information System (INIS)

    Izyumov, Yu.A.; Naish, V.E.; Petrov, S.B.

    1979-01-01

    By analyzing the exchange Hamiltonian, the authors develop the technique of determining the magnetic structures liable to occur in a crystal. The technique rests on Bertaut's idea that the exchange eigenfunction corresponds to some magnetic structure. A technically simple and efficient method of diagonalizing the exchange matrix is worked out using the devices of space group representation theory. A method is presented to find the magnetic structures with equal exchange energy (exchange multiplets). The occcurrence of exchange multiplets results from the additional invariance of the exchange Hamiltonian under rotation of all the spins. The degeneracy within the exchange multiplet may be the reason why some magnetic structures arise not according to one irreducible representation of the space group. The theory is illustrated with reference to an example of the magnetic structure of spinels. (Auth.)

  6. Crystal structure of barium hydride, determined by neutron diffraction experiments on BaD2

    International Nuclear Information System (INIS)

    Bronger, W.; Scha Chi-Chien; Mueller, P.

    1987-01-01

    A reinvestigation of the structure of BaH 2 and BaD 2 was performed on powdered samples by X-ray- and neutron diffraction experiments. It is shown, that the hydrogen positions correspond with those found in calcium deuteride and not with those proposed in the literature. The classification of barium hydride in the PbCl 2 structure type is discussed. (author)

  7. Measurement of the spin dependent structure functions of proton and neutron

    International Nuclear Information System (INIS)

    Rith, K.

    1989-01-01

    Recent results from the EMC experiment on the spin dependent structure function g 1 p (x) of the proton are discussed. They suggest that the nucleon spin does not originate from quark spins but rather from angular orbital momentum and gluon contributions. A proposed experiment at HERA is presented which will allow a very accurate measurement of the spin dependent structure functions and their integrals of both proton and neutron and a precise test of the Bjorken sum rule. (orig.)

  8. Structural design study of tritium breeding blanket with a lead layer as a neutron multiplier

    International Nuclear Information System (INIS)

    Iida, Hiromasa; Kitamura, Kazunori; Minato, Akio; Sakamoto, Hiroki; Yamamoto, Takashi

    1980-12-01

    Thermal and structural design study of a tritium breeding blanket with a lead layer for a International Tokamak Reactor (INTOR) is carried out. Tube in shell type blanket with a lead layer is found to be promising. The volume fraction of structural material in the lead layer can be small enough to keep the neutron multiplication effect of lead. Reasonable value of shell effect is attainable due to lead layer in the front part of the blanket. (author)

  9. Nuclear structure studies via neutron interactions. Progress report, 1 July 1994--30 June 1995

    International Nuclear Information System (INIS)

    Carlton, R.F.

    1995-01-01

    Neutron total cross section measurements of 122 Sn has been analyzed over the energy range 0.013 to 0.310 MeV. The R - matrix analysis has resulted in resonance and average parameters which provide for a complete representation of the neutron entrance the s 1/2 , p 1/2 , and p 3/2 contributions. The s - and p - neutron strength functions have been determined to be 0.123 ± 0.023 and 2.0 ± 0.200, respectively (in units of 10 -4 ). Limits are placed on level spacings and strength functions for the individual partial wave components. The s - wave potential scattering radius has been determined to be 6.3 ± 0.1 fm. Average scattering functions, deduced from the average parameters, have been used to determine the real well depth of an optical model potential which reproduces these functions. We find, as have others, that the real well depth is parity dependent. Two computer codes were developed: (1) a minimization program for finding parameters of a dispersive optical model which reproduce the high resolution data of the ORELA facility, and (2) an X-windows graphical user interface has been developed to permit interactive resonance analysis of the neutron total cross section data using analysis-and-minimization codes developed previously. These will contribute to the more routine analysis of ORELA data

  10. Equation of state of dense nuclear matter and neutron star structure from nuclear chiral interactions

    Science.gov (United States)

    Bombaci, Ignazio; Logoteta, Domenico

    2018-02-01

    Aims: We report a new microscopic equation of state (EOS) of dense symmetric nuclear matter, pure neutron matter, and asymmetric and β-stable nuclear matter at zero temperature using recent realistic two-body and three-body nuclear interactions derived in the framework of chiral perturbation theory (ChPT) and including the Δ(1232) isobar intermediate state. This EOS is provided in tabular form and in parametrized form ready for use in numerical general relativity simulations of binary neutron star merging. Here we use our new EOS for β-stable nuclear matter to compute various structural properties of non-rotating neutron stars. Methods: The EOS is derived using the Brueckner-Bethe-Goldstone quantum many-body theory in the Brueckner-Hartree-Fock approximation. Neutron star properties are next computed solving numerically the Tolman-Oppenheimer-Volkov structure equations. Results: Our EOS models are able to reproduce the empirical saturation point of symmetric nuclear matter, the symmetry energy Esym, and its slope parameter L at the empirical saturation density n0. In addition, our EOS models are compatible with experimental data from collisions between heavy nuclei at energies ranging from a few tens of MeV up to several hundreds of MeV per nucleon. These experiments provide a selective test for constraining the nuclear EOS up to 4n0. Our EOS models are consistent with present measured neutron star masses and particularly with the mass M = 2.01 ± 0.04 M⊙ of the neutron stars in PSR J0348+0432.

  11. Mixing of alcohol and water molecules studied by neutron probe. Structure and dynamics

    International Nuclear Information System (INIS)

    Yoshida, Koji

    2001-01-01

    Structure of water/alcohol mixing solution was studied by three methods such as an isotope-exchanged neutron scattering method, RISM (Reference Interaction Site Model) integral equation and a neutron spin echo method. The principle of methods, experiments and results were reported. The results of experiments of water/tert-butyl alcohol (TBA) solution by the isotope-exchange neutron scattering method showed TBA molecule associated with each other through end methyl group. Especially this effect was the largest at x TBA = 0.06 and decreased with increasing the concentration of TBA. However, hydrogen bonding of TBA was very rare at x TBA = 0.06. By the partial radial distribution function obtained from RISM integral equation, it indicated that the structure of pure TBA became chain structure by hydrogen bond but changed to the structure contacted directly each hydrophobic group with increasing the concentration of water. Water/2-butoxyethanol (BE) mixing solution was measured by a neutron spin echo method. The activation energy of the diffusion coefficients obtained agreed to the energy of hydrogen bonding. The temperature response of diffusion coefficients showed the inverse of the experimental results obtained by the dynamic light scattering method. The difference between two measurement methods was different time scale and space scale. Namely, the object of the neutron scattering method is nano meter and nano second, but one of light scattering method many times over. It was proved from the above results that there was the cluster consisted of the same kind of molecule in the homogeneous two components solution, but the cluster was not stable and constantly exchanged with molecule, where the production and decay of the cluster is repeated at about nano sec. (S.Y.)

  12. Pasta Structures of Quark-Hadron Phase Transition in Proto-Neutron Stars

    International Nuclear Information System (INIS)

    Yasutake, Nobutoshi; Maruyama, Toshiki; Tatsumi, Toshitaka

    2011-01-01

    We study the quark-hadron mixed phase in proto-neutron stars with the finite-size effects. In the calculations of pasta structures appeared in the mixed phase, the Gibbs conditions require the pressure balance and chemical equilibrium between two phases besides the thermal equilibrium. We find that the region of the mixed phase is limited due to thermal instability. Moreover, we study the effects of neutrinos to the pasta structures. As a result, we find that the existence of neutrinos make the pasta structures unstable, too. These characteristic features of the hadron-quark mixed phase should be important for the middle stage of the evolutions of proto-neutron stars.

  13. Formation of glassy carbon structure and its change under neutron irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Kurolenkin, E.I.; Lopato, Yu.S.; Virgil' ev, Yu.S.; Khakimova, D.K.; Aksenov, S.I.

    1981-01-01

    The changes of glassy carbon structure, which is prepared of phenol-formaldehyde and furfurol-phenol-formaldehyde resins in the process of irradiation with 5.3x10/sup 20/ cm/sup -2/ neutron fluence with the energy E>0.18 MeV in the temperature range of 90-540 deg C are studied. It is established the irradiation results in the shrinkage of the samples. The compression of the samples increases with the irradiation temperature and neutron fluence. The thermal annealing does not result in the restoration of the volume of samples. The sample shrinkage, caused by more compact package of globular structures and the destruction of film structures, decrease gas permeability of glassy carbon.

  14. Neutron radiography for the characterization of porous structure in degraded building stones

    International Nuclear Information System (INIS)

    Barone, G; Mazzoleni, P; Raneri, S; Crupi, V; Longo, F; Majolino, D; Venuti, V; Teixeira, J

    2014-01-01

    As it is well known, the porous structure of stones can change due to different degradation processes that modify the characteristics of freshly quarried blocks. Their knowledge is fundamental for predicting the behavior of stones and the efficacy of conservative treatments. In this context, neutron radiography is a useful tool not only to visualize the structure of porous materials, but also to evaluate the degree of degradation and surface modifications resulting from weathering processes. Furthermore, since thermal neutrons suffer a strong attenuation by hydrogen, this technique is effective in order to investigate the amount of absorbed water in building materials. In the present work, we report a neutron radiography investigation of limestones cropping out in the South-Eastern Sicily and widely used as building stones in Baroque monuments of the Noto Valley. The analyzed samples have been submitted to cyclic salt crystallization that simulate degradation processes acting in exposed stones of buildings. The obtained results demonstrate the interest of neutron radiography to better understand deterioration processes in limestones and to acquire information useful for restoration projects

  15. [Studies of nuclear structure using neutrons and charged particles

    International Nuclear Information System (INIS)

    1989-01-01

    This report contains brief discussions on nuclear research done at Triangle Universities Nuclear Laboratory. The major categories covered are: Fundamental symmetries in the nucleus; Dynamics in very light nuclei; D states in light nuclei; Nucleon-nucleus interactions; Nuclear structure and reactions; and Instrumentation and development

  16. Structure of neutron-rich isotopes of boron and carbon at the limits of stability

    International Nuclear Information System (INIS)

    Leblond, Sylvain

    2015-01-01

    The unbound nuclei 18 B and 21 C have been studied in an experiment undertaken at the RIBF-RIKEN using the recently commissioned SAMURAI spectrometer and NEBULA neutron array. The two systems were probed using single-neutron and single and two-proton knockout from secondary beams of 22 C, 22 N, et 23 O respectively in the case of 21 C and 19 B, 19 C and 20 N for 18 B. The invariant mass spectra were reconstructed from the momentum of the fragment ( 17 B, 20 C) and neutron. In order to interpret the results a complete simulation of the experimental setup was utilised. The analysis procedures as well as the calibrations were verified through a measurement of the well-known ground state of 16 B. In the case of 18 B three states were observed: an s-wave virtual state (as ≤ -50 fm), an l=2 resonance at E r =0.77 ± 0.09 MeV and an l=0 resonance at E r = 1.6 ± 0.6 MeV. These results suggest that the low-lying level structure of 18 B is governed by a competition between the neutron 2s 1/2 and 1d 5/2 configurations. In the case of 21 C resonances were observed at E r = 0.8 ± 0.15 MeV (l = 0) and E r = 1.5 ±0.1 MeV (l=2), a result which confirms predictions of an inversion of the 5/2 + and 1/2 + levels. Finally an analysis of the momentum distributions for 18 B and 21 C produced in single-neutron knockout was carried out. The results indicate that the valence neutrons 19 B and 22 C are in mixed (2s 1/2 ) 2 and (1d 5/2 ) 2 configurations. (author)

  17. Neutron diffraction instruments at the BR2 reactor and their use in the study of crystal and magnetic structures

    International Nuclear Information System (INIS)

    Legrand, E.

    1977-01-01

    The study of structural properties of condensed matted is frequently performed by means of methods based on X-ray, electron or neutron scattering. In many particular cases, the latter technique offers definite advantages which are mainly based on the following characteristics of neutron-matter interaction: The large penetration depth for neutrons in matter (with the exception of a few elements), which allow the study of large samples and the use of wavelengths from 0.5 to 5A, and even to 10 A; the absence of an atomic form factor; the irregular dependence of the scattering length for the different elements as a function of their atomic number; the large cross section for magnetic scattering; the energy of thermal neutrons which allows the direct measuremtment of the enrgy exchange between the neutrons and the scatterer. Three of the four neutron diffraction instruments for solid state research, installed at the BR2 reactor, are described in detail. (author)

  18. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2013-01-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, nanostructures investigated by small-angle neutron scattering, structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic neutron scattering, strongly correlated electrons, polymer dynamics, applications of neutron scattering. (HSI)

  19. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2012-01-01

    The following topics are dealt with: Neutron scattering in contemporary research, neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  20. A search for fine structure of the time-of-flight spectrum of the fission neutrons of 252Cf

    International Nuclear Information System (INIS)

    Scobie, J.; Scott, R.D.; Feather, N.; Vass, D.G.

    1977-01-01

    A standard time-of-flight arrangement, in which start pulses were supplied by fission fragments and stop pulses by neutrons, has been employed in an attempt to check recent claims of the existence of fine structures in the time-of-flight spectrum of the fission neutrons of 252 Cf. This structure, in the form of spikes with tails towards longer times, has been attributed to the emission of neutrons of short delay (with half-lives of a few to a hundred or so nanoseconds) in the fission process. It has not been possible to find any convincing evidence for the existence of such structure. (author)

  1. Neutron irradiation effects on silicon detectors structure, electrical and mechanical characteristics

    International Nuclear Information System (INIS)

    Rabinovich, E.; Golan, G.; Axelevich, A.; Inberg, A.; Oksman, M.; Rosenwaks, I.; Lubarsky, G.; Seidman, A.; Croitoru, N.; Rancoita, P.G.; Rattaggi, M.

    1999-01-01

    Neutron irradiation effects on (p-n) and Schottky-junction silicon detectors were studied. It was shown that neutron interactions with monocrystalline silicon create specific types of microstructure defects with morphology differing according to the level of neutron fluences (Φ). The isolated dislocation loops, formed by interstitial atoms were observed in microstructure images for 10 10 ≤ Φ ≤ 10 12 n/cm 2 . A strong change in the dislocation loops density and a cluster formation was observed for Φ ≥ 10 13 n/cm 2 . A drastic silicon damage was found for fluences over 10 14 n/cm 2 . These fluences created zones enriched with all types of dislocations, covering more than 50 % of the total surface area. A mechanical fragility appeared in that fluence range in a form of microcracks. 10 14 n/cm 2 appears to be a critical value of neutron irradiation because of the radiation damage described above and because the characteristics I f -V f of silicon detectors can be differentiated from those obtained at low fluences. (A.C.)

  2. The magnetic structure of GdNi2B2C investigated by neutron powder diffraction

    International Nuclear Information System (INIS)

    Barcza, A.; Rotter, M.; Doerr, M.; Beuneu, B.

    2005-01-01

    Full text: The group of ReT 2 B 2 C (Re=rare earth, T=transition metal) shows a very interesting interplay between magnetism and superconductivity due to the rare earth metals. In this work the magnetism of GdNi 2 B 2 C was studied with neutron diffraction. Previous investigations with x-ray diffraction methods have determined the crystal structure as a body centered tetragonal structure (I 4/mmm). Hot neutrons were used for the diffraction experiment, because the absorption cross section of Gd is significantly smaller for short wavelengths. The investigated compound orders magnetically at TN=19.5 K, and so the experiment was carried out at two temperatures, namely 30 K and 2.2 K. The results show a incommensurate spin structure with a propagation vector of (0.55 0 0). To confirm this results additional simulations of the spin structure were done based on the Standard Model of rare earth magnetism. A neutron diffraction pattern was calculated using the McPhase program package and is compared to the experimental data. (author)

  3. Neutron transport in structural materials and shielding design

    International Nuclear Information System (INIS)

    Salvatores, M.

    1979-01-01

    In this paper recent development in integral Benchmark experiments and their analysis is reviewed. The main problems related to data and method assesment are also briefly reviewed. In particular, the basic data processing and multigroup structure optimization and the effects of the basic data uncertainty evaluation are stressed. The representativity of an integral experiment from the designer point of view is indicated. Moreover a procedure to deduce design oriented bias factors is outlined. Cross section adjustments are indicated as a useful tool to reduce these bias factors and their uncertainties

  4. On the atomic structure of liquid Ni-Si alloys: a neutron diffraction study

    Science.gov (United States)

    Gruner, S.; Marczinke, J.; Hennet, L.; Hoyer, W.; Cuello, G. J.

    2009-09-01

    The atomic structure of the liquid NiSi and NiSi2 alloys is investigated by means of neutron diffraction experiments with isotopic substitution. From experimental data-sets obtained using four Ni isotopes, partial structure factors and pair correlation functions are obtained by applying a reverse Monte Carlo modelling approach. Both alloys were found to exhibit a strong tendency to hetero-coordination within the first coordination shell. In particular, covalent Si-Si bonds with somewhat greater distances seem to influence the structure of the liquid NiSi alloy.

  5. On the atomic structure of liquid Ni-Si alloys: a neutron diffraction study

    Energy Technology Data Exchange (ETDEWEB)

    Gruner, S; Marczinke, J; Hoyer, W [Institute of Physics, Chemnitz University of Technology, D-09107 Chemnitz (Germany); Hennet, L [CNRS-CEMHTI, University of Orleans, F-45071 Orleans (France); Cuello, G J, E-mail: sascha.gruner@physik.tu-chemnitz.d [Institute Laue-Langevin, PO Box 156, F-38042 Grenoble (France)

    2009-09-23

    The atomic structure of the liquid NiSi and NiSi{sub 2} alloys is investigated by means of neutron diffraction experiments with isotopic substitution. From experimental data-sets obtained using four Ni isotopes, partial structure factors and pair correlation functions are obtained by applying a reverse Monte Carlo modelling approach. Both alloys were found to exhibit a strong tendency to hetero-coordination within the first coordination shell. In particular, covalent Si-Si bonds with somewhat greater distances seem to influence the structure of the liquid NiSi alloy.

  6. Neutron powder diffraction and theory-aided structure refinement of rubidium and cesium ureate

    Energy Technology Data Exchange (ETDEWEB)

    Sterri, Kjersti B.; Deringer, Volker L.; Houben, Andreas; Jacobs, Philipp [RWTH Aachen Univ. (Germany). Inst. of Inorganic Chemistry; Kumar, Chogondahalli M.N. [Forschungszentrum Juelich GmbH, Juelich Centre for Neutron Science (JCNS), Outstation at SNS, Oak Ridge National Laboratory, Oak Ridge, TN (United States); Oak Ridge National Laboratory, TN (United States). Chemical and Engineering Materials Div.; Dronskowski, Richard [RWTH Aachen Univ. (Germany). Inst. of Inorganic Chemistry; RWTH Aachen Univ. (Germany). Juelich-Aachen Research Alliance (JARA-HPC)

    2016-08-01

    Urea (CN{sub 2}H{sub 4}O) is a fundamental biomolecule whose derivatives are abundant throughout chemistry. Among the latter, rubidium ureate (RbCN{sub 2}H{sub 3}O) and its cesium analog (CsCN{sub 2}H{sub 3}O) have been described only very recently and form the first structurally characterized salts of deprotonated urea. Here, we report on a neutron diffraction study on the aforementioned alkaline-metal ureates, which affords the positions for all hydrogen atoms (including full anisotropic displacement tensors) and thus allows us to gain fundamental insights into the hydrogen-bonding networks in the title compounds. The structure refinements of the experimental neutron data proceeded successfully using starting parameters from ab initio simulations of atomic positions and anisotropic displacement parameters. Such joint experimental-theoretical refinement procedures promise significant practical potential in cases where complex solids (organic, organometallic, framework materials) are studied by powder diffraction.

  7. Experimental model for neutron scattering in disordered systems: static structure factor determination of mode-softening

    International Nuclear Information System (INIS)

    Siegel, E.

    1982-01-01

    The generalized-disorder collective-boson mode-softening universality-principle (GDCBMSUP) for collective-boson mode dispersion in disordered systems (liquids, quantum liquids, glasses, powders, disordered magnets, plasmas...), a unified qualitative and semi-qualitative and semi-quantitative descriptive prescription for treating the properties of very differently disordered systems, is directly dependent upon a measurement (or calculation) of the static structure factor S(k) determined from a frequency average of the dynamic structure factor S(k,w), a multiple of the inelastic differential neutron scattering cross section d 2 sigma/dwdOMEGA. The prescription for this principle is given and, because of its universal applicability to disordered systems of any type with any type and/or degree of disorder, the neutron scattering determination of S(k) takes on renewed importance

  8. Structure investigations on Portland cement paste by small angle neutron scattering

    International Nuclear Information System (INIS)

    Dragolici, C. A.; Len, A.

    2003-01-01

    Portland cement pastes consist of many crystalline and non-crystalline phases in various ranges of sizes (nm and mm scale). The crystalline phases are embedded in amorphous phases of the hydration products. We investigated the structural changes of hydrating phases in the time interval of 1-30 days at Budapest Neutron Center's SANS diffractometer. The small angle neutron scattering of Portland cements prepared with a water-to-cement ratio from 0,3 to 0,8 gave us information about the microstructure changes in the material. Fractals were a suitable way for structure modelling. The variation of fractals size depending on the preparation-to-measurement time interval and water-to-cement ratio could be observed. (authors)

  9. Correlation between potential well structure and neutron production in inertial electrostatic confinement fusion

    International Nuclear Information System (INIS)

    Ohnishi, M.; Yamamoto, Y.; Yoshikawa, K.; Sato, K.H.

    1997-01-01

    The electrostatic potential well in inertial electrostatic confinement (IEC) is studied using two approaches. First, the equilibrium potential profile is obtained by solving the charge neutrality condition, i.e. n i n e , assuming the appropriate distribution functions for the ions and the electrons. The formation of a double well structure is demonstrated, with a depth depending upon the ratio between the focus radii of the electrons and the ions. The correlations between the well depth and the volume integrated neutron production due to deuterium-deuterium (DD) reactions are obtained. Second, in order to study the stability of the well, the dynamic behaviours of the potential well are calculated by performing time advancing numerical simulations on the basis of the particle in cell method. Single, double and triple wells, depending on the amount of injected ion current, are observed to be formed for ions with a monoenergetic distribution. The well in the centre of the multiwell structure is unstable and oscillates with a periods much longer than the inverse ion plasma frequency. A double well structure can be formed even for ions with a spread out energy distribution when the ion current is larger than the threshold value. The time averaged neutron production by DD fusion events is proportional to a power of the ion current involved in forming the double well structure. The results strongly suggest that the high neutron production rate should be attributed to not only the well depth but also the unstable behaviour of the potential, i.e. the intermittent peaking of the density in the centre region. A numerical simulation reveals that IEC possesses a favourable dependence of fusion reactions on the injected ion current for the application to a neutron source or a fusion reactor. (author). 9 refs, 9 figs

  10. Small angle neutron scattering form polymer melts: structural investigation and phase behaviour

    International Nuclear Information System (INIS)

    Ertugrul, O.

    2004-01-01

    The Small-Angle Neutron Scattering (SANS) techniques have been used to study the structural properties and phase behavior of polymer melts. A model based on Random Phase Approximation (RPA) is proposed to predict the experimental data. By fitting the model to data we could be able to obtain radius of gyration (a measure of size of a polymer) and phase transition for the sample. (author)

  11. Structure of neutron-rich nuclei around the N = 50 shell-gap closure

    Science.gov (United States)

    Faul, T.; Duchêne, G.; Thomas, J.-C.; Nowacki, F.; Huyse, M.; Van Duppen, P.

    2010-04-01

    The structure of neutron-rich nuclei in the vicinity of 78Ni have been investigated via the β-decay of 71,73,75Cu isotopes (ISOLDE, CERN). Experimental results have been compared with shell-model calculations performed with the ANTOINE code using a large (2p3/21f5/22p1/21g9/2) valence space and a 56/28Ni28 core.

  12. Ab initio simulations and neutron scattering studies of structure and dynamics in PdH

    International Nuclear Information System (INIS)

    Totolici, I.E.

    2001-07-01

    The work presented in this PhD thesis is concerned with the interpretation of the neutron scattering measurements from the palladium hydrogen system by means of ab initio electronic structure calculations. The motivation of performing such calculations was due to recent neutron scattering studies on this system that showed a strong directional dependence to the dynamical structure factor together with a complex dependence on energy. Here we attempt to describe the origin of these features by ab initio simulations of the dynamical structure factor. The method assumes an adiabatic separation of the motion of the proton and palladium atoms. The proton wave functions are calculated by a direct solution of the associated single-particle Schroedinger equation using a plane wave basis set method and a mapping of the adiabatic surface. The Fourier components of the adiabatic potential are obtained from LDA pseudopotential calculations. Using Fermi's golden rule within the Born approximation we were then able to calculate the dynamical structure factor, S(Q,ω), for exciting the proton from its ground state to various excited states as a function of the magnitude and direction of the scattering wave vector. The results are in agreement with the inelastic neutron scattering spectra and allow us to identify the origin of previous inexplicable features, in particular the strong directional dependence to the experimental data. The method was extended to investigate the expansion of the equilibrium lattice constant as a function of the H isotope when the zero-point energy of the proton/deuterium is explicitly taken into account in the relaxation process. The results we obtained predicted a bigger lattice constant for the hydride, as expected. Furthermore, other complex ab initio calculations were carried out in order to describe the origin of the large optic dispersion, seen previously in the coherent neutron scattering data. Our calculated dispersion proved to be in good

  13. Above-threshold structure in {sup 244}Cm neutron-induced fission cross section

    Energy Technology Data Exchange (ETDEWEB)

    Maslov, V.M. [Radiation Physics and Chemistry Problems Inst., Minsk-Sosny (Belarus)

    1997-03-01

    The quasi-resonance structure appearing above the fission threshold in neutron-induced fission cross section of {sup 244}Cm(n,f) is interpreted. It is shown to be due to excitation of few-quasiparticle states in fissioning {sup 245}Cm and residual {sup 244}Cm nuclides. The estimate of quasiparticle excitation thresholds in fissioning nuclide {sup 245}Cm is consistent with pairing gap and fission barrier parameters. (author)

  14. Structure of polyacrylic acid and polymethacrylic acid solutions : a small angle neutron scattering study

    OpenAIRE

    Moussaid , A.; Schosseler , F.; Munch , J.; Candau , S.

    1993-01-01

    The intensity scattered from polyacrylic acid and polymethacrylic acid solutions has been measured by small angle neutron scattering experiemnts. The influence of polymer concentration, ionization degree, temperature and salt content has been investigated. Results are in qualitative agreement with a model which predicts the existence of microphases in the unstable region of the phase diagram. Quantitative comparison with the theory is performed by fitting the theoretical structure factor to t...

  15. Strongly correlated electron systems and neutron scattering. Magnetism, superconductivity, structural phase transition

    Energy Technology Data Exchange (ETDEWEB)

    Katano, Susumu [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    1998-03-01

    Neutron scattering experiments in our group on strongly correlated electron systems are reviewed Metal-insulator transitions caused by structural phase transitions in (La{sub 1-x}Sr{sub x}) MnO{sub 3}, a novel magnetic transition in the CeP compound, correlations between antiferromagnetism and superconductivity in UPd{sub 2}Al{sub 3} and so forth are discussed. Here, in this note, the phase transition of Mn-oxides was mainly described. (author)

  16. The structure of molecular liquids. Neutron diffraction and molecular dynamics simulations

    International Nuclear Information System (INIS)

    Bianchi, L.

    2000-05-01

    Neutron diffraction (ND) measurements on liquid methanol (CD 3 OD, CD 3 O(H/D), CD 3 OH) under ambient conditions were performed to obtain the distinct (intra- + inter-molecular), G dist (r) and inter-molecular, G inter (r) radial distribution functions (rdfs) for the three samples. The H/D substitution on hydroxyl-hydrogen (Ho) has been used to extract the partial distribution functions, G XHo (r) (X=C, O, and H - a methyl hydrogen) and G XX (r) at both the distinct and inter-molecular levels from the difference techniques of ND. The O-Ho bond length, which has been the subject of controversy in the past, is found purely from the distinct partial distribution function, G XHo (r) to be 0.98 ± 0.01 A. The C-H distance obtained from the distinct G XX (r) partial is 1.08 ± 0.01 A. These distances determined by fitting an intra-molecular model to the total distinct structure functions are 0.961 ± 0.001 A and 1.096 ± 0.001 A, respectively. The inter-molecular G XX (r) function, dominated by contributions from the methyl groups, apart from showing broad oscillations extending up to ∼14 A is featureless, mainly because of cancellation effects from six contributing pairs. The Ho-Ho partial pair distribution function (pdf), g HoHo (r), determined from the second order difference, shows that only one other Ho atom can be found within a mean Ho-Ho separation of 2.36 A. The average position of the O-Ho hydrogen bond determined for the first time purely from experimental inter-molecular G XHo (r) partial distribution function is found to be at 1.75 ± 0.03 A. The experimental structural results at the partial distribution level are compared with those obtained from molecular dynamics (MD) simulations performed in NVE ensemble by using both 3- and 6-site force field models for the first time in this study. The MD simulations with both the models reproduce the ND rdfs rather well. However, discrepancies begin to appear between the simulated and the experimental partial

  17. Neutron total cross-section of hydrogenous and deuterated 1- and 2-propanol and n-butanol measured using the VESUVIO spectrometer

    Science.gov (United States)

    Rodríguez Palomino, L. A.; Dawidowski, J.; Márquez Damián, J. I.; Cuello, G. J.; Romanelli, G.; Krzystyniak, M.

    2017-10-01

    This work presents the total cross sections of a set of normal and deuterated alcohols (hydrogenous 1- and 2-propanol and n-butanol, 1-propanol(OD) and fully deuterated 2-propanol and n-butanol), measured at spectrometer VESUVIO (ISIS spallation neutron source, United Kingdom). Granada's Synthetic Model was applied to describe those systems and a satisfactory agreement with the measured total cross section was achieved in the range of energies from 10-3 to 100 eV. The input parameters of the model were determined from the essential features of the vibrational spectra of the atoms that compose the systems, which were studied using Molecular Dynamics.

  18. Structural characterisation of 1- and 2-dimensional transition metal polymers using powder neutron diffraction

    International Nuclear Information System (INIS)

    James, M.

    1999-01-01

    Powder neutron diffraction provides an alternate technique for the structural study of transition metal polymers and finds utility over standard X-ray methods in two significant ways. Firstly, due to a different instrument geometry, preferred orientation effects are removed from the system. The second advantage gained by utilising neutrons is that H atoms in the sample contribute much more to the nuclear scattering of the diffraction profile - allowing their atomic position to be accurately determined. In X-ray diffraction studies, where H atoms typically account for only ∼3-5% of the scattering from the sample, it is essentially impossible to refine their position in the molecular structure. The structures of several transition metal polymers have been determined using neutrons from the HIFAR reactor at ANSTO and the Powder Diffractometers HRPD and MRPD, along with Rietveld refinement methods. The 1-dimensional polymer dibromobis(thiazole)nickel(II) illustrated in the paper is characteristic of these types of systems which are comprised of transition metal centres bridged by halogen atoms with pendant amine side groups

  19. On neutron stars and gravitation

    International Nuclear Information System (INIS)

    Castagnino, M.A.

    1987-01-01

    From the variational principle for the total internal energy of a neutron star and some restrictions of the form of the metric coefficients, equations of structure which are valid for every metric theory of gravitation have been found. Some simple solutions of the structure equations to find the maximum mass of a neutron star are also presented. Finally it is studied this problem using a post post-Newtonian parametrization

  20. Structure Analysis of Polymeric Nanopore Using Small Angle Neutron Scattering

    International Nuclear Information System (INIS)

    Ryu, Du Yeol; Kim, Eun Hye; Kim, Bo Kyung; Lee, Ho Yeon; Kim, Soon Cheol

    2010-05-01

    The main purpose of this project is to develop the functional nanostructures via the SANS analysis and molecular simulations, based on the synthesis of multicomponent polymer self-assembly. We will study the diffusion and transition behavior of polymers at the confined condition such as hydrostatic pressure and thin films on the surfaces where the molecular interactions are controlled. - Physical properties of the functionalized nanostructures - Structural analysis of nanostructures via SANS measurement under hydrostatic pressure - Statistical mechanics theory and molecular simulation for nanostructures - Control of the molecular interactions on the substrates by the surface modification, and the study of diffusion and transition behavior of polymers - Organization research community to resolve technical issues, which is based on SANS technology in the development of industrial materials - Academic understanding about the application of SANS technology - Establishment of competitive power internationally in the application of SANS technology - Educational effect of members through research activity - Publication in the top journals and presentation reports - Possibility of technology transfer to the industries by the application of SANS technology

  1. Effect of liposome entrapped Cu/Zn bovine superoxide dismutase in rat after total body (neutron-gamma) irradiation

    International Nuclear Information System (INIS)

    Lamproglou, I.; Martin, S.; Lambert, F.; Fontanille, P.; Fessi, H.; Puisieux, F.; Colas-Linhart, N.; Bok, B.; Fatome, M.; Martin, C.

    1998-01-01

    Our purpose was, to study in rat the effects of (neutron-gamma) exposure and of LIPSOD treatment (liposomal Cu/Zn super-oxide dismutase) on cognitive functions. Our data demonstrate that whole-body irradiation induces in Sprague-Dawley rats some cognitive dysfunction. Treatment using LIPSOD corrects in a significantly way this trend. Moreover, in sham-irradiated rats, this treatment shows an inhibitory effect. (authors)

  2. A method to compare calculated and experimental 14 MeV neutron attenuation coefficient and to determine the total removal cross-section

    International Nuclear Information System (INIS)

    Elay, A.G.

    1978-01-01

    A method to compare calculated and experimental neutron attenuation coefficients (chi) when samples are o, different geometries but the same material is proposed. The best Σ (total removal cross section) is determined by using the fact that the logarithm of the attenuation coefficient varies linearly with respect to Σ i.e. lg chi = + asub(s) Σ, where asub(s) is a parameter that characterises all the geometrical experimental conditions of the neutron source, the sample and the relative source-to-sample geometry. In order to increase the precision, samples of different geometries but the same material were used. Values of chi are determined experimentally and asub(s) calculated for these geometries. The graph of lg chi as a function of asub(s) together with a simple fit to a straight line is sufficient to determine Σ (the slope of the line). (T.G.)

  3. Investigation of the single Particle Structure of the neutron-rich Sodium Isotopes $^{27-31}\\!$Na

    CERN Document Server

    2002-01-01

    We propose to study the single particle structure of the neutron-rich isotopes $^{27-31}\\!$Na. These isotopes will be investigated via neutron pickup reactions in inverse kinematics on a deuterium and a beryllium target. Scattered beam particles and transfer products are detected in a position sensitive detector located around 0$^\\circ$. De-excitation $\\gamma$-rays emitted after an excited state has been populated will be registered by the MINIBALL Germanium array. The results will shed new light on the structure of the neutron-rich sodium isotopes and especially on the region of strong deformation around the N=20 nucleus $^{31}\\!$Na.

  4. TLD-300 detectors for separate measurement of total and gamma absorbed dose distributions of single, multiple, and moving-field neutron treatments

    International Nuclear Information System (INIS)

    Rassow, J.

    1984-01-01

    Fast neutron therapy requirements, because of the poor depth dose characteristic of present therapeutical sources, are at least as complex in treatment plans as photon therapy. The physical part of the treatment planning is very important; however, it is much more complicated than for photons or electrons owing to the need for: Separation of total and gamma absorbed dose distributions (Dsub(T) and Dsub(G)); and more stringent tissue-equivalence conditions of phantoms than in photon therapy. Therefore, methods of clinical dosimetry for the separate determination of total and gamma absorbed dose distributions in irregularly shaped (inhomogeneous) phantoms are needed. A method using TLD-300 (CaF 2 :Tm) detectors is described, which is able to give an approximate solution of the above-mentioned dosimetric requirements. The two independent doses, Dsub(T) and Dsub(G), can be calculated by an on-line computer analysis of the digitalized glow curve of TLD-300 detectors, irradiated with d(14)+Be neutrons of the cyclotron isocentric neutron therapy facility CIRCE in Essen. Results are presented for depth and lateral absorbed dose distributions (Dsub(T) and Dsub(G)) for fixed neutron beams of different field sizes compared with measurements by standard procedures (TE-TE ionization chamber, GM counter) in an A-150 phantom. The TLD-300 results for multiple and moving-field treatments (with and without wedge filters) in a patient simulating irregularly shaped (inhomogeneous) phantoms, are shown together with computer calculations of these dose distributions. The probable causes for some systematic deviations are discussed, which lead to open problems for further investigations owing to features of the detector material and the evaluation method, but mainly to differences in the composition of phantom materials used for the calculations (standard dose distributions) and TLD-300 measurements. (author)

  5. Crystal structure studies with the Paris-Edinburgh cell: Neutron scattering aspects

    Science.gov (United States)

    Loveday, J. S.; Wilson, R. M.; Nelmes, R. J.; Besson, J. M.; Klotz, S.; Hamel, G.; Hull, S.

    1994-07-01

    The count rates achieved in neutron powder diffraction experiments create difficulties for high-pressure experiments because large sample volumes (˜100 mm3) must be used. Until recently it has been difficult to build suitable pressure cells with such large volumes and hence the maximum pressure for neutron diffraction has remained at the relatively low value of 3 GPa. We have now developed a pressure cell (the Paris-Edinburgh cell) which is capable of exceeding 10 GPa with a sample volume of ˜100 mm3 for use at the U.K. spallation source ISIS. Considerable effort has been devoted to the opimization of the cell, shielding, and detector geometry to enable the best possible data to be recorded. Finite-element calculations to correct for the systematic errors introduced by the attenuation of the pressure-cell materials have been developed and tested. As a result of this work we are now able to obtain accurate structural data to ˜12 GPa and recent studies of phase IV of ND3, the behaviour of the O-D bondlength in D2O ice VIII, and the structural pressure dependence of B4C illustrate the importance of the extension of neutron-diffraction studies to such pressures.

  6. The Precision Measurement of the Neutron Spin Structure Function Using Polarized HE-3 Target

    Energy Technology Data Exchange (ETDEWEB)

    Wang, X

    2004-01-05

    Using a 48.6 GeV polarized electron beam scattering off a polarized {sup 3}He target at Stanford Linear Accelerator Centre (SLAC), they measured the neutron spin structure function g{sub 1}{sup n} over kinematic(x) ranging 0.014 < x <0.7 and 1 < Q{sup 2} < 17GeV{sup 2}. The measurement gave the integral result over the neutron spin structure function {integral}{sub 0.014}{sup 0.7} g{sub 1}{sup n}(x)dx = -0.036 {+-} 0.004(stat) {+-} 0.005(syst) at an average Q{sup 2} = 5GeV{sup 2}. Along with the proton results from SLAC E143 experiment (0.03 < x) and SMC experiment (0.014 < x < 0.03), they find the Bjorken sum rule appears to be largely saturated by the data integrated down to x of 0.014. However, they observe relatively large values for g{sub 1}{sup n} at low x. The result calls into question the usual methods (Regge theory) for extrapolating to x = 0 to find the full neutron integral {integral}{sub 0}{sup t} g{sub 1}{sup n}(x) dx, needed for testing the Quark-Parton Model (QMP).

  7. Spin structure of the neutron ({sup 3}He) and the Bjoerken sum rule

    Energy Technology Data Exchange (ETDEWEB)

    Meziani, Z.E. [Stanford Univ., CA (United States)

    1994-12-01

    A first measurement of the longitudinal asymmetry of deep-inelastic scattering of polarized electrons from a polarized {sup 3}He target at energies ranging from 19 to 26 GeV has been performed at the Stanford Linear Accelerator Center (SLAC). The spin-structure function of the neutron g{sub 1}{sup n} has been extracted from the measured asymmetries. The Quark Parton Model (QPM) interpretation of the nucleon spin-structure function is examined in light of the new results. A test of the Ellis-Jaffe sum rule (E-J) on the neutron is performed at high momentum transfer and found to be satisfied. Furthermore, combining the proton results of the European Muon Collaboration (EMC) and the neutron results of E-142, the Bjoerken sum rule test is carried at high Q{sup 2} where higher order Perturbative Quantum Chromodynamics (PQCD) corrections and higher-twist corrections are smaller. The sum rule is saturated to within one standard deviation.

  8. Measurement of the Neutron F2 Structure Function via Spectator Tagging with CLAS

    Science.gov (United States)

    Baillie, N.; Tkachenko, S.; Zhang, J.; Bosted, P.; Bültmann, S.; Christy, M. E.; Fenker, H.; Griffioen, K. A.; Keppel, C. E.; Kuhn, S. E.; Melnitchouk, W.; Tvaskis, V.; Adhikari, K. P.; Adikaram, D.; Aghasyan, M.; Amaryan, M. J.; Anghinolfi, M.; Arrington, J.; Avakian, H.; Baghdasaryan, H.; Battaglieri, M.; Biselli, A. S.; Branford, D.; Briscoe, W. J.; Brooks, W. K.; Burkert, V. D.; Carman, D. S.; Celentano, A.; Chandavar, S.; Charles, G.; Cole, P. L.; Contalbrigo, M.; Crede, V.; D'Angelo, A.; Daniel, A.; Dashyan, N.; De Vita, R.; De Sanctis, E.; Deur, A.; Dey, B.; Djalali, C.; Dodge, G.; Domingo, J.; Doughty, D.; Dupre, R.; Dutta, D.; Ent, R.; Egiyan, H.; El Alaoui, A.; El Fassi, L.; Elouadrhiri, L.; Eugenio, P.; Fedotov, G.; Fegan, S.; Fradi, A.; Gabrielyan, M. Y.; Gevorgyan, N.; Gilfoyle, G. P.; Giovanetti, K. L.; Girod, F. X.; Gohn, W.; Golovatch, E.; Gothe, R. W.; Graham, L.; Guegan, B.; Guidal, M.; Guler, N.; Guo, L.; Hafidi, K.; Heddle, D.; Hicks, K.; Holtrop, M.; Hungerford, E.; Hyde, C. E.; Ilieva, Y.; Ireland, D. G.; Ispiryan, M.; Isupov, E. L.; Jawalkar, S. S.; Jo, H. S.; Kalantarians, N.; Khandaker, M.; Khetarpal, P.; Kim, A.; Kim, W.; King, P. M.; Klein, A.; Klein, F. J.; Klimenko, A.; Kubarovsky, V.; Kuleshov, S. V.; Kvaltine, N. D.; Livingston, K.; Lu, H. Y.; MacGregor, I. J. D.; Mao, Y.; Markov, N.; McKinnon, B.; Mineeva, T.; Morrison, B.; Moutarde, H.; Munevar, E.; Nadel-Turonski, P.; Ni, A.; Niccolai, S.; Niculescu, I.; Niculescu, G.; Osipenko, M.; Ostrovidov, A. I.; Pappalardo, L.; Park, K.; Park, S.; Pasyuk, E.; Anefalos Pereira, S.; Pisano, S.; Pozdniakov, S.; Price, J. W.; Procureur, S.; Prok, Y.; Protopopescu, D.; Raue, B. A.; Ricco, G.; Rimal, D.; Ripani, M.; Rosner, G.; Rossi, P.; Sabatié, F.; Saini, M. S.; Salgado, C.; Schott, D.; Schumacher, R. A.; Seder, E.; Sharabian, Y. G.; Sober, D. I.; Sokhan, D.; Stepanyan, S.; Stepanyan, S. S.; Stoler, P.; Strauch, S.; Taiuti, M.; Tang, W.; Ungaro, M.; Vineyard, M. F.; Voutier, E.; Watts, D. P.; Weinstein, L. B.; Weygand, D. P.; Wood, M. H.; Zana, L.; Zhao, B.

    2012-04-01

    We report on the first measurement of the F2 structure function of the neutron from the semi-inclusive scattering of electrons from deuterium, with low-momentum protons detected in the backward hemisphere. Restricting the momentum of the spectator protons to ≲100MeV/c and their angles to ≳100° relative to the momentum transfer allows an interpretation of the process in terms of scattering from nearly on-shell neutrons. The F2n data collected cover the nucleon-resonance and deep-inelastic regions over a wide range of Bjorken x for 0.65neutron to proton structure function ratio F2n/F2p at 0.2≲x≲0.8 with little uncertainty due to nuclear effects.

  9. Structures of high and low density amorphous ice by neutron diffraction

    International Nuclear Information System (INIS)

    Finney, J.L.; Hallbrucker, A.; Kohl, I.; Soper, A.K.; Bowron, D.T.

    2002-01-01

    Neutron diffraction with isotope substitution is used to determine the structures of high (HDA) and low (LDA) density amorphous ice. Both 'phases' are fully hydrogen bonded, tetrahedral networks, with local order similarities between LDA and ice Ih, and HDA and liquid water. Moving from HDA, through liquid water and LDA to ice Ih, the second shell radial order increases at the expense of spatial order. This is linked to a fifth first neighbor 'interstitial' that restricts the orientations of first shell waters. This 'lynch pin' molecule which keeps the HDA structure intact has implications for the nature of the HDA-LDA transition that bear on the current metastable water debate

  10. Neutron diffraction structure investigations for expanded liquid selenium up to 14000C and 300 bar

    International Nuclear Information System (INIS)

    Edeling, M.

    1980-01-01

    The static structure factor of the expanded liquid Selenium is measured by means of the neutron diffraction for temperatures between 600 0 C and 1400 0 C and for pressures up to 300 bar. From the structure factors the pair distribution functions show that the bond length of the Selenium atoms is constant 2.37 A to 2.38 A for the whole concentration range. For temperatures above 1200 0 C the calculated intermolecular coordination number shows that the intermolecular interaction increases. (BHO)

  11. Investigation of the cluster structure in aqueous suspensions of nanodiamonds by small-angle neutron scattering

    Directory of Open Access Journals (Sweden)

    L. A. Bulavin

    2015-07-01

    Full Text Available The paper presents the results of the structural study of various types of the water-detonation nanodiamond liquid systems, which are obtained by small-angle scattering of thermal neutrons. It was shown that in the mass fraction range (0.3 - 1.8 % the experimental spectra are well described by a two-level model of unified exponential/power-law approach. The resulting structural parameters allowed us to estimate the aggregation number in the studied systems. Sizes of the nanodiamond particles and their clusters are found as well as the fractal dimension of the latter.

  12. Investigation of the cluster structure in aqueous suspensions of nanodiamonds by small-angle neutron scattering

    International Nuclear Information System (INIS)

    Bulavin, L.A.; Tomchuk, O.V.; Avdeev, M.V.

    2015-01-01

    The paper presents the results of the structural study of various types of the water-detonation nanodiamond liquid systems, which are obtained by small-angle scattering of thermal neutrons. It was shown that in the mass fraction range (0.3/1.8) % the experimental spectra are well described by a two-level model of unified exponential/power-law approach. The resulting structural parameters allowed us to estimate the aggregation number in the studied systems. Sizes of the nanodiamond particles and their clusters are found as well as the fractal dimension of the latter

  13. Structure and Spatial Distribution of Ge Nanocrystals Subjected to Fast Neutron Irradiation

    Directory of Open Access Journals (Sweden)

    Alexander N. Ionov

    2011-07-01

    Full Text Available The influence of fast neutron irradiation on the structure and spatial distribution of Ge nanocrystals (NC embedded in an amorphous SiO2 matrix has been studied. The investigation was conducted by means of laser Raman Scattering (RS, High Resolution Transmission Electron Microscopy (HR-TEM and X-ray photoelectron spectroscopy (XPS. The irradiation of Ge- NC samples by a high dose of fast neutrons lead to a partial destruction of the nanocrystals. Full reconstruction of crystallinity was achieved after annealing the radiation damage at 8000C, which resulted in full restoration of the RS spectrum. HR-TEM images show, however, that the spatial distributions of Ge-NC changed as a result of irradiation and annealing. A sharp decrease in NC distribution towards the SiO2 surface has been observed. This was accompanied by XPS detection of Ge oxides and elemental Ge within both the surface and subsurface region.

  14. Standardization of accelerator irradiation procedures for simulation of neutron induced damage in reactor structural materials

    Science.gov (United States)

    Shao, Lin; Gigax, Jonathan; Chen, Di; Kim, Hyosim; Garner, Frank A.; Wang, Jing; Toloczko, Mychailo B.

    2017-10-01

    Self-ion irradiation is widely used as a method to simulate neutron damage in reactor structural materials. Accelerator-based simulation of void swelling, however, introduces a number of neutron-atypical features which require careful data extraction and, in some cases, introduction of innovative irradiation techniques to alleviate these issues. We briefly summarize three such atypical features: defect imbalance effects, pulsed beam effects, and carbon contamination. The latter issue has just been recently recognized as being relevant to simulation of void swelling and is discussed here in greater detail. It is shown that carbon ions are entrained in the ion beam by Coulomb force drag and accelerated toward the target surface. Beam-contaminant interactions are modeled using molecular dynamics simulation. By applying a multiple beam deflection technique, carbon and other contaminants can be effectively filtered out, as demonstrated in an irradiation of HT-9 alloy by 3.5 MeV Fe ions.

  15. Using Neutron Scattering and Mercury Intrusion Techniques to Characterize Micro- and Nano-Pore Structure of Shale

    Science.gov (United States)

    Zhang, Y.; Barber, T.; Hu, Q.; Bleuel, M.

    2017-12-01

    The micro- and nano-pore structure of oil shale plays a critical role in hydrocarbon storage and migration. This study aims to characterize the pore structure of three Bakken members (i.e., upper organic-rich shale, middle silty/sandy dolomites, and lower organic-rich shale), through small and ultra-small angle neutron scattering (SANS and USANS) techniques, as well as mercury injection capillary pressure (MICP) analyses. SANS/USANS have the capabilities of measuring total porosity (connected and closed porosity) across nm-mm spectrum, not measurable than other fluid-invasion approaches, such as MICP which obtains connected porosity and pore-throat size distribution. Results from both techniques exhibit different features of upper/lower Bakken and middle Bakken, as a result of various mineral composition and organic matter contents. Middle Bakken is primarily dominated by the mineral pores, while in the upper and lower Bakken, organic pores contribute a significant portion of total porosity. A combination of USANS/SANS and MICP techniques gives a comprehensive picture of shale micro- and nano-pore structure.

  16. Neutron μstiX. Micrometer structure investigation with real space and reciprocal space crossover using neutron imaging detectors

    Energy Technology Data Exchange (ETDEWEB)

    Muehlbauer, Martin Johann

    2013-07-19

    This work is concerned with the investigation of inhomogeneities in materials with length scales of the order of micrometers by means of neutrons. In real space this is done by neutron imaging methods measuring the transmitted signal while for Ultra Small Angle Neutron Scattering (USANS) the signal of the scattered neutrons is assigned to a spatial frequency distribution in reciprocal space. The part about neutron imaging is focused on time-resolved neutron radiography on an injection nozzle similar to the ones used for modern diesel truck engines. The associated experiments have been carried out at the neutron imaging facility ANTARES at the Forschungs-Neutronenquelle Heinz Maier-Leibnitz (FRM II) of the Technische Universitaet Muenchen in Garching near Munich. Especially the demands on the detector system were high. Therefore different detection methods and detector configurations have been tested. On the one hand the detector should allow for a time resolution high enough to record the injection process lasting about 900 μs. On the other hand it needed to offer a spatial resolution sufficient to resolve the test oil inside the spray hole of a maximum diameter of less than 200 μm. An advanced aim of this work is the visualization of cavitation phenomena which may occur during the injection process inside of the spray hole. In order to operate the injector at conditions as close to reality as possible a high pressure pump supplying the injector with test oil at a pressure of 1600 bar was needed in addition to the specially developed control electronics, the recuperation tank and the exhaust gas equipment for the escaping atomized spray. A second part of the work describes USANS experiments based on the idea of Dr. Roland Gaehler and carried out at the instrument D11 at the Institut Laue-Langevin in Grenoble. For this purpose a specific multi-beam geometry was applied, where a multi-slit aperture replaced the standard source aperture and the sample aperture was

  17. Neutron μstiX. Micrometer structure investigation with real space and reciprocal space crossover using neutron imaging detectors

    International Nuclear Information System (INIS)

    Muehlbauer, Martin Johann

    2013-01-01

    This work is concerned with the investigation of inhomogeneities in materials with length scales of the order of micrometers by means of neutrons. In real space this is done by neutron imaging methods measuring the transmitted signal while for Ultra Small Angle Neutron Scattering (USANS) the signal of the scattered neutrons is assigned to a spatial frequency distribution in reciprocal space. The part about neutron imaging is focused on time-resolved neutron radiography on an injection nozzle similar to the ones used for modern diesel truck engines. The associated experiments have been carried out at the neutron imaging facility ANTARES at the Forschungs-Neutronenquelle Heinz Maier-Leibnitz (FRM II) of the Technische Universitaet Muenchen in Garching near Munich. Especially the demands on the detector system were high. Therefore different detection methods and detector configurations have been tested. On the one hand the detector should allow for a time resolution high enough to record the injection process lasting about 900 μs. On the other hand it needed to offer a spatial resolution sufficient to resolve the test oil inside the spray hole of a maximum diameter of less than 200 μm. An advanced aim of this work is the visualization of cavitation phenomena which may occur during the injection process inside of the spray hole. In order to operate the injector at conditions as close to reality as possible a high pressure pump supplying the injector with test oil at a pressure of 1600 bar was needed in addition to the specially developed control electronics, the recuperation tank and the exhaust gas equipment for the escaping atomized spray. A second part of the work describes USANS experiments based on the idea of Dr. Roland Gaehler and carried out at the instrument D11 at the Institut Laue-Langevin in Grenoble. For this purpose a specific multi-beam geometry was applied, where a multi-slit aperture replaced the standard source aperture and the sample aperture was

  18. Use of the method of neutrons moderation to the adjustment of the concrete dosage through the total humidity of the arid s

    International Nuclear Information System (INIS)

    Howland, J.; Morejon, D.; Simeon, G.; Gracia, R.; Desdin, L.; O'Reilly, V.

    1997-01-01

    The method of neutrons moderation to the fast determination was applied of the content of humidity in the fine and thick arid s. The measure values of humidity were employed in the adjustment of the Dosification of concrete by the total humidity of the arid. The obtained results indicate that the employment of this fitting method allows to get higher values of resistance to the compression and also reduces the dispersions in the concretes production. This method would permit a considerable saving of cement in comparison with the traditional method. (author) [es

  19. The structure of phosphate glass biomaterials from neutron diffraction and 31P nuclear magnetic resonance data

    International Nuclear Information System (INIS)

    Pickup, D M; Ahmed, I; Guerry, P; Knowles, J C; Smith, M E; Newport, R J

    2007-01-01

    Neutron diffraction and 31 P nuclear magnetic resonance spectroscopy were used to probe the structure of phosphate glass biomaterials of general composition (CaO) 0.5-x (Na 2 O) x (P 2 O 5 ) 0.5 (x = 0, 0.1 and 0.5). The results suggest that all three glasses have structures based on chains of Q 2 phosphate groups. Clear structural differences are observed between the glasses containing Na 2 O and CaO. The P-O bonds to bridging and non-bridging oxygens are less well resolved in the neutron data from the samples containing CaO, suggesting a change in the nature of the bonding as the field strength of the cation increases Na + → Ca 2+ . In the (CaO) 0.5 (P 2 O 5 ) 0.5 glass most of the Ca 2+ ions are present in isolated CaO x polyhedra whereas in the (Na 2 O) 0.5 (P 2 O 5 ) 0.5 glass the NaO x polyhedra share edges leading to a Na-Na correlation. The results of the structural study are related to the properties of the (CaO) 0.4 (Na 2 O) 0.1 (P 2 O 5 ) 0.5 biomaterial

  20. Analysis of Management Practices in Lagos State Tertiary Institutions through Total Quality Management Structural Framework

    Science.gov (United States)

    AbdulAzeez, Abbas Tunde

    2016-01-01

    This research investigated total quality management practices and quality teacher education in public tertiary institutions in Lagos State. The study was therefore designed to analyse management practices in Lagos state tertiary institutions through total quality management structural framework. The selected public tertiary institutions in Lagos…

  1. New developments in neutron scattering for the study of molecular systems: structure and diffusive motions

    International Nuclear Information System (INIS)

    Volino, F.

    1976-01-01

    After a short review of the main concepts concerning the neutron and its interaction with matter, the authors focus their attention on the study of molecular systems by means of neutron scattering. Instead of reviewing the subject yet again, they limit themselves to the new kind of work which can be done now, with the combined help of high flux reactors and novel instruments. As examples, a few experiments performed at the Institut Laue-Langevin in Grenoble are described: a neutron diffraction study of liquid acetonitrile using a powder diffractometer installed at the hot source; three high-resolution quasi-elastic studies of molecular motions - in an organic solid, (PAA), an organic liquid (C 3 H 6 ) and a liquid crystal (TBBA) - made by combining measurements with high and ultra-high energy resolution spectrometers installed at the cold source. The concept of elastic incoherent structure factor (EISF) is extensively used for the analysis. Finally some prospects on possible future developments are presented. (orig./HK) [de

  2. The effect of neutron irradiation on the structure and properties of carbon-carbon composite materials

    International Nuclear Information System (INIS)

    Burchell, T.D.; Eatherly, W.P.; Robbins, J.M.; Strizak, J.P.

    1991-01-01

    Carbon-based materials are an attractive choice for fusion reactor plasma facing components (PFCs) because of their low atomic number, superior thermal shock resistance, and low neutron activation. Next generation plasma fusion reactors, such as the International Thermonuclear Experimental Reactor (ITER), will require advanced carbon-carbon composite materials possessing extremely high thermal conductivity to manage the anticipated severe heat loads. Moreover, ignition machines such as ITER will produce high neutron fluxes. Consequently, the influence of neutron damage on the structure and properties of carbon-carbon composite materials must be evaluated. Data from an irradiation experiment are reported and discussed here. Fusion relevant graphite and carbon-carbon composites were irradiated in a target capsule in the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory (ORNL). A peak damage dose of 1.59 dpa at 600 degrees C was attained. The carbon materials irradiated included nuclear graphite grade H-451 and one-, two-, and three-directional carbon-carbon composite materials. Dimensional changes, thermal conductivity and strength are reported for the materials examined. The influence of fiber type, architecture, and heat treatment temperature on properties and irradiation behavior are reported. Carbon-Carbon composite dimensional changes are interpreted in terms of simple microstructural models

  3. Evaluation of toughness degradation by small punch (SP) tests for neutron irradiated structural steels

    International Nuclear Information System (INIS)

    Misawa, Toshihei; Hamaguchi, Yoshikazu; Kimura, Akihiko; Eto, Motokuni; Suzuki, Masahide; Nakajima, Nobuya.

    1992-01-01

    The small punch (SP) test as one of the useful small specimen testing technique (SSTT) has been developed to evaluate the fracture toughness, ductile-brittle transition temperature (DBTT) and tensile properties for neutron irradiated structural materials. The SP tests using the miniaturized specimens of φ3 mm TEM disk and 10 mm 2 coupon were performed for six kinds of ferritic steels of F-82, F-82H, HT-9, JFMS, 2.25-1Mo and SQV2A. It was shown that the temperature dependence of SP fracture energies with scatter in miniaturized testing can give reliable information on the DBTT by use of the statistical analysis based on the Weibull distribution. A good correlation between the DBTT of the SP tests and that of the standard CVN test has been obtained for the various nuclear ferritic steels. The SP test was performed for cryogenic austenitic steels as a way of evaluating elastic-plastic fracture toughness, J IC , on the basis of a universal empirical relationship between J IC and SP equivalent fracture strain, ε-bar qf . The SP testing using the neutron irradiated specimens of 2.25Cr-1Mo, F-82, F-82H and HT-9 steels was successfully applied and presented the neutron radiation induced changes on the DBTT, fracture toughness and tensile properties. (author)

  4. Low-energy neutron measurements in an iron calorimeter structure irradiated by 200 GeV/c hadrons

    Energy Technology Data Exchange (ETDEWEB)

    Russ, J S [Carnegie-Mellon University, Pittsburgh, PA (United States); Stevenson, G R; Fasso, A; Nielsen, M C [CERN, Geneva (Switzerland); Furetta, C; Rancoita, P G; Vismara, I [INFN, Milan (Italy)

    1989-04-21

    Of serious concern in the design of detectors for the new high-luminosity hadron-hadron colliders are the radiation damage effects on silicon and other detectors of low-energy neutrons produced by spallation evaporation or fission processes. Because of the lack of experimental information on the number of neutrons with energies between 0.1 and 10 MeV in the cascades originating from high-energy hadrons, an experiment was carried out using activation detector techniques to measure the neutron fluence in a cascade initiated by 200 GeV hadrons in acalorimeter-like iron structure. It was found that at the maximum of the cascade one produces approximately 3 neutrons per GeV of incident energy: some 70% of these are of energies between 0.1 and 5 MeV, the remainder are fairly uniformly distributed in energy between 5 and several hundred MeV. The number of albedo neutrons leaving the front face of the calorimeter structure was about 0.3 neutrons per GeV of incident energy with in energy distribution similar to those at cascade maximum These data confirm that neutron-induced damage will he of concern in the design of detectors for the new colliders and that further measurements and calculations are necessary for a correct assessment of this damage. (author)

  5. Single-neutron knockout from 20C and the structure of 19C

    Directory of Open Access Journals (Sweden)

    J.W. Hwang

    2017-06-01

    Full Text Available The low-lying unbound level structure of the halo nucleus 19C has been investigated using single-neutron knockout from 20C on a carbon target at 280 MeV/nucleon. The invariant mass spectrum, derived from the momenta of the forward going beam velocity 18C fragment and neutrons, was found to be dominated by a very narrow near threshold (Erel=0.036(1 MeV peak. Two less strongly populated resonance-like features were also observed at Erel=0.84(4 and 2.31(3 MeV, both of which exhibit characteristics consistent with neutron p-shell hole states. Comparisons of the energies, measured cross sections and parallel momentum distributions to the results of shell-model and eikonal reaction calculations lead to spin-parity assignments of 5/21+ and 1/21− for the levels at Ex=0.62(9 and 2.89(10 MeV with Sn=0.58(9 MeV. Spectroscopic factors were also deduced and found to be in reasonable accord with shell-model calculations. The valence neutron configuration of the 20C ground state is thus seen to include, in addition to the known 1s1/22 component, a significant 0d5/22 contribution. The level scheme of 19C, including significantly the 1/21− cross-shell state, is well accounted for by the YSOX shell-model interaction developed from the monopole-based universal interaction.

  6. Structure solution from powder neutron and x-ray diffraction data: getting the best of both worlds

    International Nuclear Information System (INIS)

    Hunter, B.A.

    2000-01-01

    Full text: Powder diffraction methods have traditionally been used in three main areas: phase identification and quantification, lattice parameter determination and structure refinement. Until recently structure solution has been the almost exclusive domain of single crystal diffraction methods, predominantly using x-rays. The increasing use of synchrotron and neutron sources, and the unrelenting advances in computing hardware and software means that powder methods are challenging single crystal methods as a practical method for structure solution, especially when single crystal method can not be applied. It is known that structural refinements from a known starting structure using combined X-ray and neutron data sets are capable of providing highly accurate structures. Likewise, using combined x-ray and neutron powder diffraction data in the structure solution process should also be a powerful technique, although to date no one is pursuing this methodology. This paper present examples of solutions to the problem. Namely we are using high resolution powder X-ray and neutron methods to solve the structures of molecular materials and minerals, then refining the structures using both sets of data. In this way we exploit the advantages of both methods while minimising the disadvantages. We present our solution for a small amino acid structure, a metalorganic and a mineral structure

  7. Determination of the total amount of organically bound chlorine, bromine and iodine in environmental samples by instrumental neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Gether, J; Lunde, G [Central Institute for Industrial Research, Oslo (Norway); Steinnes, E [Institutt for Atomenergi, Kjeller (Norway)

    1979-07-01

    The determination of chlorine, bromine and iodine present as non-polar, hydrophobic hydrocarbons in environmental samples is reported. The organohalogen compounds are seprated from water into an organic phase by on-site liquid-liquid extraction, and form biological material by procedures based on lipid phase extraction and codistillation. After removal of inorganic halides by washing with water and concentration of the sample by evaporation of the solvent, the resulting extracts are analyzed for their chlorine, bromine and iodine contents by instrumental neutron activation analysus. Strict attention is paid to the possibility of contamination in every step of the procedure. Background values in routine analysis are approximately 100-200 ng of chlorine, <5 ng of bromine and <3 ng of iodine.

  8. Analysis of Challenges for Management Education in India Using Total Interpretive Structural Modelling

    Science.gov (United States)

    Mahajan, Ritika; Agrawal, Rajat; Sharma, Vinay; Nangia, Vinay

    2016-01-01

    Purpose: The purpose of this paper is to identify challenges for management education in India and explain their nature, significance and interrelations using total interpretive structural modelling (TISM), an innovative version of Warfield's interpretive structural modelling (ISM). Design/methodology/approach: The challenges have been drawn from…

  9. Small angle neutron and x-ray scattering studies of self-assembled nano structured materials

    International Nuclear Information System (INIS)

    Choi, Sung Min

    2009-01-01

    Full text: Small angle neutron and x-ray scattering are very powerful techniques to investigate nano structured materials. In this presentation, examples of nano structured materials investigated by neutron and x-ray scattering will be presented. Part I: The unique anisotropic physical properties of columnar discotic liquid crystals (DLCs) have attracted considerable interest for their potential applications as electronic devices. For many practical applications, however, it is crucial to obtain uniaxially oriented and highly ordered columnar superstructures of DLC molecules covering macroscopic area. Here, we present a simple and straight-forward approach to fabricate uniaxially oriented and highly ordered columnar superstructures of cobalt octa(n-decylthio) porphyrazine (CoS 1 0), a discotic supra-molecule, in bulk and on substrates [1] over a macroscopic length scale, utilizing an applied magnetic field and the interaction of CoS 1 0 with an OTS-functionalized substrate. The details of the oriented and ordered columnar nano-structures are investigated by SANS and GISAXS. Part II: Self-assembly of one-dimensional (1D) nanoparticles with metallic or semiconducting properties into highly ordered superstructures using various interactions has been of great interest as a route towards materials with new functionalities. Here, we report a new phase diagram of negatively charged 1D nanoparticle (cROD) and cationic liposome (CL) complexes in water which exhibit three different highly ordered phases [2]. Small angle neutron and x-ray scattering measurements show that the cROD-CL complexes exhibit three different highly ordered phases, intercalated lamellar, doubly intercalated lamellar and centered rectangular phases, depending on particle curvature and electrostatic interactions. The new phase diagram can be used to understand and design new highly ordered self-assemblies of 1D nanoparticles in soft matter which provide new functionalities. (author)

  10. Effect of ion-beam gettering on the GaAs transistor structure parameters under neutron irradiation

    International Nuclear Information System (INIS)

    Obolenskij, S.V.; Skupov, V.D.

    2000-01-01

    It is established that the neutron irradiation negative effect on the parameters of the field transistors with the Schottky shut-off on the basis of the epitaxial gallium arsenide is essentially reduced when the argon ions are preliminary implanted into structure on the substrate side. The above effect is explained through remotely controlled gettering by ion irradiation of admixtures and defects in the transistor active areas related with origination of deep levels under the neutron fluence [ru

  11. Structure around the island of inversion with single-neutron knockout reactions at GANIL

    CERN Document Server

    Fernández-Domínguez, B; Patterson, N; Thomas, J S; Orr, N; Chartier, M; Catford, W; Achouri, N L; Angélique, J-C; Ashwood, N I; Banu, A; Bastin,B; Brown, J; Borcea, R; Franchoo, S; Freer, M; Gaudefroy, L; Laurent, B; Labiche, M; Lemmon, R C; Negoita, F; Paschalis, S; Paul, E S; Petri, M; Roussel-Chomaz, P; Staniou, M; Taylor, M J; Trache, L

    2010-01-01

    The nuclear structure of the 31Mg nucleus has been studied with the singleneutron knockout reaction. We report on the preliminary results of an experiment performed with the EXOGAM array coupled, for the first time, to the SPEG spectrometer at GANIL.We present a provisional result for the inclusive single-neutron knockout cross section of σinc= 90(5) mb. Preliminary exclusive cross sections for the measured bound states, including the ground state, are also presented. Finally, preliminary longitudinal momentum distributions for the ground state and first excited state are also shown. These results are compared to Monte Carlo Shell-Model calculations in the sd-pf region.

  12. Software of structure experiMents in a neutron time-of-flight diffractometer

    International Nuclear Information System (INIS)

    Balagurov, A.M.; Dlouga, M.; Zlokazov, V.B.; Mironova, G.M.

    1978-01-01

    A set of programs is discussed to be used in diffraction experiment in a neutron time-of-flight diffractometer. The DIFRAT program, which processes spectra of poly and monocrystals, locates all spectrum maxima and assesses their width on the basis of given experimental data and elementary cell parameters. Accurate location of maxima, evaluation of their area and width is done by the IREAK program. The most important feature of this program is a capability to set an experimental model of maxima patterns. The EXPDAT program is developed to investigate structural characteristics of a sample. It calculates corrections for absorbtion and extinction

  13. Neutron and X-ray Scattering Study of Structure and Dynamics of Condensed Matters

    Science.gov (United States)

    Fujii, Yasuhiko

    In this article, I have reviewed a series of research on a various phase transitions such as (1) structural phase transitions of perovskite compounds driven by soft phonons, (2) pressure-induced molecular dissociation and metallization observed in solid halogens, and (3) the “Devil's Flower” type phase diagram observed in two compounds with frustrating interactions. Also commented is on the so-called “Small Science at Large Facility” typically symbolized by neutron and synchrotron radiation experiments like the present research.

  14. Deuteron A(Q2) structure function and the neutron electric form factor

    International Nuclear Information System (INIS)

    Platchkov, S.; Amroun, A.; Auffret, S.; Cavedon, J.M.; Dreux, P.; Duclos, J.; Frois, B.; Goutte, D.; Hachemi, H.; Martino, J.

    1989-01-01

    We present new measurements of the deuteron A(Q 2 ) structure function in the momentum transfer region between 1 and 18 fm -2 . The accuracy of the data ranges from 2% to 6%. We investigate the sensitivity of A(Q 2 ) to the nucleon-nucleon interaction and to the neutron electric form factor G E n . Our analysis shows that below 20 fm -2 G E n can be inferred from these data with a significantly improved accuracy. The model dependence of this analysis is discussed

  15. Structure of polyacrylic acid and polymethacrylic acid solutions: a small angle neutron scattering study

    Energy Technology Data Exchange (ETDEWEB)

    Moussaid, A. (Lab. d' Ultrasons et de Dynamique des Fluides Complexes, Univ. Louis Pasteur, 67 - Strasbourg (France)); Schosseler, F. (Lab. d' Ultrasons et de Dynamique des Fluides Complexes, Univ. Louis Pasteur, 67 - Strasbourg (France)); Munch, J.P. (Lab. d' Ultrasons et de Dynamique des Fluides Complexes, Univ. Louis Pasteur, 67 - Strasbourg (France)); Candau, S.J. (Lab. d' Ultrasons et de Dynamique des Fluides Complexes, Univ. Louis Pasteur, 67 - Strasbourg (France))

    1993-04-01

    The intensity scattered from polyacrylic acid and polymethacrylic acid solutions has been measured by small angle neutron scattering experiments. The influence of polymer concentration, ionization degree, temperature and salt content has been investigated. Results are in qualitative agreement with a model which predicts the existence of microphases in the unstable region of the phase diagram. Quantitative comparison with the theory is performed by fitting the theoretical structure factor to the experimental data. For a narrow range of ionization degrees nearly quantitative agreement with the theory is found for the polyacrylic acid system. (orig.).

  16. Structure of polyacrylic acid and polymethacrylic acid solutions : a small angle neutron scattering study

    Science.gov (United States)

    Moussaid, A.; Schosseler, F.; Munch, J. P.; Candau, S. J.

    1993-04-01

    The intensity scattered from polyacrylic acid and polymethacrylic acid solutions has been measured by small angle neutron scattering experiemnts. The influence of polymer concentration, ionization degree, temperature and salt content has been investigated. Results are in qualitative agreement with a model which predicts the existence of microphases in the unstable region of the phase diagram. Quantitative comparison with the theory is performed by fitting the theoretical structure factor to the experimental data. For a narrow range of ionizaiton degrees nearly quantitative agreement with the theory is found for the polyacrylic acide system.

  17. First observation of excited structures in neutron-deficient 179Hg : evidence for multiple shape coexistence

    International Nuclear Information System (INIS)

    Kondev, F.G.; Carpenter, M.P.; Janssens, R.V.F.; Lister, C.J.; Abu Saleem, K.; Ahmad, I.; Amro, H.; Caggiano, J.; Davids, C.N.; Heinz, A.; Herskind, B.; Khoo, T.L.; Lauristen, T.; Ma, W.C.; Ressler, J.J.; Reviol, W.; Riedinger, L.L.; Sarantites, D.G.; Seweryniak, D.; Siem, S.; Sonzongni, A.A.; Varmette, P.G.; Wiedenhoever, I.

    2002-01-01

    Excited structures in the neutron-deficient nucleus 179 Hg have been established for the first time using the Gammasphere spectrometer in conjunction with the fragment mass analyzer. Competing states originating from three different minima associated with nearly spherical, oblate, and prolate deformations were found. This result can be contrasted with the situation in heavier odd-mass Hg isotopes where only two minima (oblate and prolate) have been seen. The implications of these three shapes at low spin and excitation energy are discussed in the general context of shape coexistence in this mass region.

  18. Quantitative neutron radiography using neutron absorbing honeycomb

    International Nuclear Information System (INIS)

    Tamaki, Masayoshi; Oda, Masahiro; Takahashi, Kenji; Ohkubo, Kohei; Tasaka, Kanji; Tsuruno, Akira; Matsubayashi, Masahito.

    1993-01-01

    This investigation concerns quantitative neutron radiography and computed tomography by using a neutron absorbing honeycomb collimator. By setting the neutron absorbing honeycomb collimator between object and imaging system, neutrons scattered in the object were absorbed by the honeycomb material and eliminated before coming to the imaging system, but the neutrons which were transmitted the object without interaction could reach the imaging system. The image by purely transmitted neutrons gives the quantitative information. Two honeycombs were prepared with coating of boron nitride and gadolinium oxide and evaluated for the quantitative application. The relation between the neutron total cross section and the attenuation coefficient confirmed that they were in a fairly good agreement. Application to quantitative computed tomography was also successfully conducted. The new neutron radiography method using the neutron-absorbing honeycomb collimator for the elimination of the scattered neutrons improved remarkably the quantitativeness of the neutron radiography and computed tomography. (author)

  19. Electrical Properties of MWCNT/HDPE Composite-Based MSM Structure Under Neutron Irradiation

    Science.gov (United States)

    Kasani, H.; Khodabakhsh, R.; Taghi Ahmadi, M.; Rezaei Ochbelagh, D.; Ismail, Razali

    2017-04-01

    Because of their low cost, low energy consumption, high performance, and exceptional electrical properties, nanocomposites containing carbon nanotubes are suitable for use in many applications such as sensing systems. In this research work, a metal-semiconductor-metal (MSM) structure based on a multiwall carbon nanotube/high-density polyethylene (MWCNT/HDPE) nanocomposite is introduced as a neutron sensor. Scanning electron microscopy, Fourier-transform infrared, and infrared spectroscopy techniques were used to characterize the morphology and structure of the fabricated device. Current-voltage ( I- V) characteristic modeling showed that the device can be assumed to be a reversed-biased Schottky diode, if the voltage is high enough. To estimate the depletion layer length of the Schottky contact, impedance spectroscopy was employed. Therefore, the real and imaginary parts of the impedance of the MSM system were used to obtain electrical parameters such as the carrier mobility and dielectric constant. Experimental observations of the MSM structure under irradiation from an americium-beryllium (Am-Be) neutron source showed that the current level in the device decreased significantly. Subsequently, current pulses appeared in situ I- V and current-time ( I- t) curve measurements when increasing voltage was applied to the MSM system. The experimentally determined depletion region length as well as the space-charge-limited current mechanism for carrier transport were compared with the range for protons calculated using Monte Carlo n-particle extended (MCNPX) code, yielding the maximum energy of recoiled protons detectable by the device.

  20. Structure, magnetic properties, polarized neutron diffraction, and theoretical study of a copper(II) cubane.

    Science.gov (United States)

    Aronica, Christophe; Chumakov, Yurii; Jeanneau, Erwann; Luneau, Dominique; Neugebauer, Petr; Barra, Anne-Laure; Gillon, Béatrice; Goujon, Antoine; Cousson, Alain; Tercero, Javier; Ruiz, Eliseo

    2008-01-01

    The paper reports the synthesis, X-ray and neutron diffraction crystal structures, magnetic properties, high field-high frequency EPR (HF-EPR), spin density and theoretical description of the tetranuclear CuII complex [Cu4L4] with cubane-like structure (LH2=1,1,1-trifluoro-7-hydroxy-4-methyl-5-aza-hept-3-en-2-one). The simulation of the magnetic behavior gives a predominant ferromagnetic interaction J1 (+30.5 cm(-1)) and a weak antiferromagnetic interaction J2 (-5.5 cm(-1)), which correspond to short and long Cu-Cu distances, respectively, as evidence from the crystal structure [see formulate in text]. It is in agreement with DFT calculations and with the saturation magnetization value of an S=2 ground spin state. HF-EPR measurements at low temperatures (5 to 30 K) provide evidence for a negative axial zero-field splitting parameter D (-0.25+/-0.01 cm(-1)) plus a small rhombic term E (0.025+/-0.001 cm(-1), E/D = 0.1). The experimental spin distribution from polarized neutron diffraction is mainly located in the basal plane of the CuII ion with a distortion of yz-type for one CuII ion. Delocalization on the ligand (L) is observed but to a smaller extent than expected from DFT calculations.

  1. An optimized ultra-fine energy group structure for neutron transport calculations

    International Nuclear Information System (INIS)

    Huria, Harish; Ouisloumen, Mohamed

    2008-01-01

    This paper describes an optimized energy group structure that was developed for neutron transport calculations in lattices using the Westinghouse lattice physics code PARAGON. The currently used 70-energy group structure results in significant discrepancies when the predictions are compared with those from the continuous energy Monte Carlo methods. The main source of the differences is the approximations employed in the resonance self-shielding methodology. This, in turn, leads to ambiguous adjustments in the resonance range cross-sections. The main goal of developing this group structure was to bypass the self-shielding methodology altogether thereby reducing the neutronic calculation errors. The proposed optimized energy mesh has 6064 points with 5877 points spanning the resonance range. The group boundaries in the resonance range were selected so that the micro group cross-sections matched reasonably well with those derived from reaction tallies of MCNP for a number of resonance absorbers of interest in reactor lattices. At the same time, however, the fast and thermal energy range boundaries were also adjusted to match the MCNP reaction rates in the relevant ranges. The resulting multi-group library was used to obtain eigenvalues for a wide variety of reactor lattice numerical benchmarks and also the Doppler reactivity defect benchmarks to establish its adequacy. (authors)

  2. Phenomenological study of nuclear structure of neutron-rich 88Rb isotope

    Science.gov (United States)

    Gupta, Surbhi; Gupta, Anuradha; Bharti, Arun

    2018-05-01

    A theoretical study of the nuclear structure of odd-odd 88Rb nucleus in the A ˜100 mass region is carried out by using the angular-momentum-projection technique implemented in the Projected Shell Model (PSM). The influence of the high-j orbitals, h11/2 for neutrons and g9/2 for protons on the structure of 88Rb isotope is investigated in the present case by assuming an axial symmetry in the deformed basis. For this isotope, PSM calculations are performed to obtain the yrast line and also the description of the formation of the yrast level structure from multi-quasi-particle configurations. The back-bending in moment of inertia and transition energies have also been calculated and compared with the experimental data.

  3. New structures in the continuum of 15C populated by two-neutron transfer

    International Nuclear Information System (INIS)

    Cappuzzello, F.; Rea, C.; Bonaccorso, A.; Bondì, M.; Carbone, D.; Cavallaro, M.; Cunsolo, A.; Foti, A.; Orrigo, S.E.A.; Rodrigues, M.R.D.; Taranto, G.

    2012-01-01

    The 13 C( 18 O,  16 O) 15 C reaction has been studied at 84 MeV incident energy. The ejectiles have been detected at forward angles and 15 C excitation energy spectra have been obtained up to about 20 MeV. Several known bound and resonant states of 15 C have been identified together with two unknown structures at 10.5 MeV (FWHM=2.5 MeV) and 13.6 MeV (FWHM=2.5 MeV). Calculations based on the removal of two uncorrelated neutrons from the projectile describe a significant part of the continuum observed in the energy spectra. In particular the structure at 10.5 MeV is dominated by a resonance of 15 C near the 13 C+n+n threshold. Similar structures are found in nearby nuclei such as 14 C and 11 Be.

  4. Membrane Structure Studies by Means of Small-Angle Neutron Scattering (SANS)

    International Nuclear Information System (INIS)

    Knott, R. B.

    2008-01-01

    The basic model for membrane structure--a lipid bilayer with imbedded proteins--was formulated 35 years ago, however the detailed structure is still under active investigation using a variety of physical, chemical and computational techniques. Every biologically active cell is encapsulated by a plasma membrane with most cells also equipped with an extensive intracellular membrane system. The plasma membrane is an important boundary between the cytoplasm of the cell and the external environment, and selectively isolates the cell from that environment. Passive diffusion and/or active transport mechanisms are provided for water, ions, substrates etc. which are vital for cell metabolism and viability. Membranes also facilitate excretion of substances either as useful cellular products or as waste. Despite their complexity and diverse function, plasma membranes from quite different cells have surprisingly similar compositions. A typical membrane structure consists of a phospholipid bilayer with a number of proteins scattered throughout, along with carbohydrates (glycoproteins), glycolipids and sterols. The plasma membranes of most eukaryotic cells contain approximately equal weights of lipid and protein, which corresponds to about 100 lipid molecules per protein molecule. Clearly, lipids are a major constituent and the study of their structure and function in isolation provides valuable insight into the more complex intact multicomponent membrane. The membrane bound protein is the other major constituent and is a very active area of research for a number of reasons including the fact that over 60% of modern drugs act on their receptor sites. The interaction between the protein and the supporting lipid bilayer is clearly of major importance. Neutron scattering is a powerful technique for exploring the structure of membranes, either as reconstituted membranes formed from well characterised lipids, or as intact membranes isolated from selected biological systems. A brief

  5. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner [eds.

    2010-07-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  6. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2010-01-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  7. Neutron scattering studies of nuclear and magnetic structures of YBa2(Cu1-yZny)3O6+x

    International Nuclear Information System (INIS)

    Villeneuve, R.; Mirebeau, I.; Collin, G.; Bouree, F.

    1994-01-01

    Structural effects of zinc substitution in YBCO have been studied by neutron diffraction in order to determine the substitution site of zinc atoms. Electron neutron diffraction experiments are performed on YBa 2 (Cu 1-y Zn y ) 3 O 6+x powders. Nuclear structures have been refined using the Rietveld method on powders of compositions x=1 and y ranging from 0.01 to 0.06. The results suggest a solubility limit of zinc in the copper planes at y ≅ 0.04 and zinc may start to substitute for chain copper sites for higher y values. Magnetic structure of a y=0.02 and x=0.05 powder has been studied by neutron elastic diffraction. The antiferromagnetic structure is not affected by non-magnetic zinc atoms but the ordering temperature is strongly reduced. 2 figs., 11 refs

  8. Separation and correlation of structural and magnetic roughness in a Ni thin film by polarized off-specular neutron reflectometry.

    Science.gov (United States)

    Singh, Surendra; Basu, Saibal

    2009-02-04

    Diffuse (off-specular) neutron and x-ray reflectometry has been used extensively for the determination of interface morphology in solids and liquids. For neutrons, a novel possibility is off-specular reflectometry with polarized neutrons to determine the morphology of a magnetic interface. There have been few such attempts due to the lower brilliance of neutron sources, though magnetic interaction of neutrons with atomic magnetic moments is much easier to comprehend and easily tractable theoretically. We have obtained a simple and physically meaningful expression, under the Born approximation, for analyzing polarized diffuse (off-specular) neutron reflectivity (PDNR) data. For the first time PDNR data from a Ni film have been analyzed and separate chemical and magnetic morphologies have been quantified. Also specular polarized neutron reflectivity measurements have been carried out to measure the magnetic moment density profile of the Ni film. The fit to PDNR data results in a longer correlation length for in-plane magnetic roughness than for chemical (structural) roughness. The magnetic interface is smoother than the chemical interface.

  9. Consistent analysis of collective level structure and neutron interaction data for 12C in the framework of the soft-rotator model

    International Nuclear Information System (INIS)

    Sukhovitskii, E.Sh.; Porodzinskii, Yu.V.; Iwamoto, Osamu; Chiba, Satoshi.

    1997-09-01

    A systematic analysis of nuclear structure and neutron interaction data for 12 C was carried out in the framework of the soft-rotator model. The model was firstly applied to analyze the low-lying collective level structure of the 12 C nucleus, which turned out to be very successful. The intrinsic wave function obtained in such an analysis was then used to construct the coupling potentials in the coupled-channels formalism to calculate the neutron total and scattering cross sections. The quadrupole deformation parameter obtained in the present analysis was 0.164, which was much smaller in the absolute sense than the value used in the symmetric-rotator, vibrator model employed frequently in the past, i.e., ≅0.6. When averaged over the β-vibration function, however, the present result yields an effective quadrupole strength of about the same scale as the previous studies due to softness of the 12 C wave function with respect to β 2 degree of freedom. The soft-rotator model was found to be very successful in reproducing both the structure and neutron scattering data consistently for the first time in this mass region. (author)

  10. Effects of mixed neutrontotal-body irradiation on physical activity performance of rhesus monkeys

    International Nuclear Information System (INIS)

    Franz, C.G.

    1985-01-01

    Behavioral incapacitation for a physical activity task and its relationship to emesis and survival time following exposure to ionizing radiation were evaluated in 39 male rhesus monkeys (Macaca mulatta). Subjects were trained to perform a shock avoidance activity task for 6 hr on a 10-min work/5-min rest schedule in a nonmotorized physical activity wheel. Following stabilization of performance, each subject received a single, pulsed dose of mixed neutron-γ, whole-body radiation (n/γ = 3.0) ranging between 1274 and 4862 rad. Performance testing was started 45 sec after exposure. A dose-response function for early transient incapacitation (ETI) during the first 2 hr after irradiation was fitted, and the median effective dose (ED 50 ) was calculated to be 1982 rad. Analysis done on the relationship of dose to ETI, emesis, and survival time found (a) a significant relationship between the radiation dose and the number and duration of ETIs; (b) no correlation between emesis and dose, survival time, or ETI; (c) no relation between survival time and ETI at any dose; and (d) no significant difference in survival time for dose groups between 1766 +/- 9 (SEM) and 2308 +/- 23 rad

  11. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2010-07-01

    The following topics are dealt with: Neutron sources, neutron properties and elastic scattering, correlation functions measured by scattering experiments, symmetry of crystals, applications of neutron scattering, polarized-neutron scattering and polarization analysis, structural analysis, magnetic and lattice excitation studied by inelastic neutron scattering, macromolecules and self-assembly, dynamics of macromolecules, correlated electrons in complex transition-metal oxides, surfaces, interfaces, and thin films investigated by neutron reflectometry, nanomagnetism. (HSI)

  12. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2010-01-01

    The following topics are dealt with: Neutron sources, neutron properties and elastic scattering, correlation functions measured by scattering experiments, symmetry of crystals, applications of neutron scattering, polarized-neutron scattering and polarization analysis, structural analysis, magnetic and lattice excitation studied by inelastic neutron scattering, macromolecules and self-assembly, dynamics of macromolecules, correlated electrons in complex transition-metal oxides, surfaces, interfaces, and thin films investigated by neutron reflectometry, nanomagnetism. (HSI)

  13. Extracting quantitative structural parameters for disordered polymers from neutron scattering data

    International Nuclear Information System (INIS)

    Rosi-Schwartz, B.; Mitchell, G.R.

    1995-01-01

    The organization of non-crystalline polymeric materials at a local level, namely on a spatial scale between a few and 100 A, is still unclear in many respects. The determination of the local structure in terms of the configuration and conformation of the polymer chain and of the packing characteristics of the chain in the bulk material represents a challenging problem. Data from wide-angle diffraction experiments are very difficult to interpret due to the very large amount of information that they carry, that is the large number of correlations present in the diffraction patterns.We describe new approaches that permit a detailed analysis of the complex neutron diffraction patterns characterizing polymer melts and glasses. The coupling of different computer modelling strategies with neutron scattering data over a wide Q range allows the extraction of detailed quantitative information on the structural arrangements of the materials of interest. Proceeding from modelling routes as diverse as force field calculations, single-chain modelling and reverse Monte Carlo, we show the successes and pitfalls of each approach in describing model systems, which illustrate the need to attack the data analysis problem simultaneously from several fronts. ((orig.))

  14. Structure of ionic liquid-water mixtures at interfaces: x-ray and neutron reflectometry studies

    International Nuclear Information System (INIS)

    Lauw, Yansen; Rodopoulos, Theo; Horne, Mike; Follink, Bart; Hamilton, Bill; Knott, Robert; Nelson, Andy

    2009-01-01

    Full text: Fundamental studies on the effect of water in ionic liquids are necessary since the overall performance of ionic liquids in many industrial applications is often hampered by the presence of water.[1] Based on this understanding, the surface and interfacial structures of 1-butyl-1methylpyrrolidinium trifluoromethylsulfonylimide [C4mpyr][NTf2] ionic liquid-water mixtures were probed using x-ray and neutron reflectometry techniques. At the gas-liquid surface, a thick cation+water layer was detected next to the phase boundary, followed by an increasing presence of anion towards the bulk. The overall thickness of the surface exhibits non-monotonic trends with an increasing water content, which explains similar phenomenological trends in surface tension reported in the literature.[2] At an electrified interface, the interfacial structure of pure ionic liquids probed by neutron reflectometry shows similar trends to those predicted by a mean-field model.[3] However, the presence of water within the electrical double-layer is less obvious, although it is widely known that water reduces electrochemical window of ionic liquids. To shed light on this issue, further studies are currently in progress.

  15. Determination of the Magnetic Structure of Complex anti-Perovskite Fluorides by Neutron Diffraction

    Science.gov (United States)

    Felder, Justin; Yeon, Jeongho; Zur Loye, Hans-Conrad

    An unusual family of anti-perovskite fluorides consisting of complex ions as the A, B, and X building units has been synthesized as single crystals. This family of anti-perovskites provides a unique framework to probe the magnetic properties of transition metals. Presented here is the Fe endmember of the family: [Cu(H2O)4]3[FeF6]2. The iron member exhibits complex magnetic behavior at low temperatures, which has been probed by magnetometry and neutron diffraction experiments. Presented here are the results from the anisotropic magnetometry study as well as the magnetic spin structure as determined by neutron diffraction experiments. The materials presented here represent an interesting class of perovskites that are as-yet unexplored. Given the wide range of properties possible in perovskites and related structures, it is reasonable to expect that further exploration of these materials will reveal many interesting attributes; both chemical and physical. United States Department of Energy, Office of Basic Energy Sciences, Division of Materials Sciences and Engineering, Award DE-SC0008664.

  16. The structure of the Gamow-Teller giant resonance and consequences for beta-delayed neutron spectra and element synthesis

    International Nuclear Information System (INIS)

    Klapdor, H.V.

    1976-01-01

    Recent results in β-delayed neutron emission are interpreted by structure of the Gamow-Teller giant resonance not included in the 'gross-theory' of β-decay. Inclusion of this structure of the β-decay function is important for calculations of β-decay production rates for heavy nuclides by astrophysical processes and thermonuclear explosions. (Auth.)

  17. Structure of zinc and niobium tellurite glasses by neutron and x-ray diffraction

    International Nuclear Information System (INIS)

    Hoppe, U; Yousef, E; Ruessel, C; Neuefeind, J; Hannon, A C

    2004-01-01

    Neutron and x-ray diffraction experiments of high resolving power with neutrons from a spallation source and high-energy photons from a synchrotron have been performed on compositional series of binary Zn, Nb and on mixed Zn/Nb tellurite glasses. The Te-O, Zn-O and Nb-O coordination numbers are determined by Gaussian fitting of the first-neighbour peaks in the neutron and x-ray data simultaneously. The transition of TeO 4 to TeO 3 units with increasing fraction of a second component is indicated by decreasing total Te-O coordination numbers. This transition appears different for glasses with ZnO or Nb 2 O 5 additions. Details of the Te-O peaks suggest there are two species of Te-O bonds with lengths of ∼ 0.19 and ∼ 0.21 nm. The change of their fractions shows excellent agreement with the existence of TeO 4 trigonal bipyramids and TeO 3 trigonal pyramids. All oxygen atoms from ZnO and Nb 2 O 5 are used for rupture of Te-O-Te bridges, which is accompanied with a change of nearly all participating TeO 4 to TeO 3 groups. The tendency for a TeO 4 → TeO 3 change decreases for glasses of higher second component content which is accompanied by the occurrence of TeO 4 groups with non-bridging oxygens. The Nb tellurite glasses show transition to network-forming behaviour with the formation of Nb-O-Nb bridges. The fractions of TeO 3 units of ternary Zn/Nb tellurite glasses agree with an additivity behaviour of the modifying effects of ZnO and Nb 2 O 5 additions

  18. Laser spectroscopy of cadmium isotopes: probing the nuclear structure between the neutron 50 and 82 shell closures

    CERN Multimedia

    Blaum, K; Stroke, H H; Krieger, A R

    We propose to study the isotopic chain of cadmium with high-resolution laser spectroscopy for the first time. Our goal is to determine nuclear spins, moments and root-mean-square charge radii of ground and isomeric states between the neutron 50 and 82 shell closures, contributing decisively to a better understanding of the nuclear structure in the vicinity of the doubly-magic $^{100}$Sn and $^{132}$Sn. On the neutron-rich side this is expected to shed light on a shell-quenching hypothesis and consequently on the duration of the r-process along the waiting-point nuclei below $^{130}$Cd. On the neutron-deficient side it may elucidate the role of the cadmium isotopes in the rp-process for rapidly accreting neutron stars.

  19. Structural characterization of advanced ceramics using the neutron diffractometer developed by Instituto de Pesquisas Energeticas e Nucleares (IPEN)

    International Nuclear Information System (INIS)

    Parente, C.B.R.; Mazzocchi, V.L.

    1999-01-01

    Application of neutron diffractometer at the Instituto de Pesquisas Energeticas Nucleares, Sao Paulo, Brazil, in the structural investigations of advanced ceramics was presented. Methodology of the analysis of neutron diffraction patterns was tested with BaLiF 3 single crystals and also doped with Ni 2+ or Pb 2+ ions. The same methodology was used to investigate the HTSC phases in the system Bi-Sr-Ca-Cu-O. The system Bi 1.7 Pb 0.3 Sr 2 Ca 2.2 Cu 3.5 O 10.6 was also investigated. Addition of Pb 2+ ions increased the fraction of high-T c phase 2223. Symmetry in neutron multiple diffraction patterns, obtained for aluminium single crystal, was elaborated. Crystal lattice parameter for aluminium single crystal was determined at different temperatures using neutron multiple diffraction. (author)

  20. Fluid bilayer structure determination: Joint refinement in composition space using X-ray and neutron diffraction data

    Energy Technology Data Exchange (ETDEWEB)

    White, S.H. [Univ. of California, Irvine, CA (United States); Wiener, M.C. [Univ. of California, San Francisco, CA (United States)

    1994-12-31

    Experimentally-determined structural models of fluid lipid bilayers are essential for verifying molecular dynamics simulations of bilayers and for understanding the structural consequences of peptide interactions. The extreme thermal motion of bilayers precludes the possibility of atomic-level structural models. Defining {open_quote}the structure{close_quote} of a bilayer as the time-averaged transbilayer distribution of the water and the principal lipid structural groups such as the carbonyls and double-bonds (quasimolecular fragments), one can represent the bilayer structure as a sum of Gaussian functions referred to collectively as the quasimolecular structure. One method of determining the structure is by neutron diffraction combined with exhaustive specific deuteration. This method is impractical because of the expense of the chemical syntheses and the limited amount of neutron beam time currently available. We have therefore developed the composition space refinement method for combining X-ray and minimal neutron diffraction data to arrive at remarkably detailed and accurate structures of fluid bilayers. The composition space representation of the bilayer describes the probability of occupancy per unit length across the width of the bilayer of each quasimolecular component and permits the joint refinement of X-ray and neutron lamellar diffraction data by means of a single quasimolecular structure that is fitted simultaneously to both data sets. Scaling of each component by the appropriate neutron or X-ray scattering length maps the composition-space profile to the appropriate scattering length space for comparison to experimental data. The difficulty with the method is that fluid bilayer structures are generally only marginally determined by the experimental data. This means that the space of possible solutions must be extensively explored in conjunction with a thorough analysis of errors.

  1. Fluid bilayer structure determination: Joint refinement in composition space using X-ray and neutron diffraction data

    International Nuclear Information System (INIS)

    White, S.H.; Wiener, M.C.

    1994-01-01

    Experimentally-determined structural models of fluid lipid bilayers are essential for verifying molecular dynamics simulations of bilayers and for understanding the structural consequences of peptide interactions. The extreme thermal motion of bilayers precludes the possibility of atomic-level structural models. Defining open-quote the structure close-quote of a bilayer as the time-averaged transbilayer distribution of the water and the principal lipid structural groups such as the carbonyls and double-bonds (quasimolecular fragments), one can represent the bilayer structure as a sum of Gaussian functions referred to collectively as the quasimolecular structure. One method of determining the structure is by neutron diffraction combined with exhaustive specific deuteration. This method is impractical because of the expense of the chemical syntheses and the limited amount of neutron beam time currently available. We have therefore developed the composition space refinement method for combining X-ray and minimal neutron diffraction data to arrive at remarkably detailed and accurate structures of fluid bilayers. The composition space representation of the bilayer describes the probability of occupancy per unit length across the width of the bilayer of each quasimolecular component and permits the joint refinement of X-ray and neutron lamellar diffraction data by means of a single quasimolecular structure that is fitted simultaneously to both data sets. Scaling of each component by the appropriate neutron or X-ray scattering length maps the composition-space profile to the appropriate scattering length space for comparison to experimental data. The difficulty with the method is that fluid bilayer structures are generally only marginally determined by the experimental data. This means that the space of possible solutions must be extensively explored in conjunction with a thorough analysis of errors

  2. The Effect of Structured Exercise Intervention on Intensity and Volume of Total Physical Activity

    Directory of Open Access Journals (Sweden)

    Niko Wasenius

    2014-12-01

    Full Text Available This study aimed to investigate the effects of a 12-week structured exercise intervention on total physical activity and its subcategories. Twenty-three overweight or obese middle aged men with impaired glucose regulation were randomized into a 12-week Nordic walking group, a power-type resistance training group, and a non-exercise control group. Physical activity was measured with questionnaires before the intervention (1–4 weeks and during the intervention (1–12 weeks and was expressed in metabolic equivalents of task. No significant change in the volume of total physical activity between or within the groups was observed (p > 0.050. The volume of total leisure-time physical activity (structured exercises + non-structured leisure-time physical activity increased significantly in the Nordic walking group (p 0.050 compared to the control group. In both exercise groups increase in the weekly volume of total leisure-time physical activity was inversely associated with the volume of non-leisure-time physical activities. In conclusion, structured exercise intervention did not increase the volume of total physical activity. Albeit, endurance training can increase the volume of high intensity physical activities, however it is associated with compensatory decrease in lower intensity physical activities. To achieve effective personalized exercise program, individuality in compensatory behavior should be recognised.

  3. Novel tendencies in developing small-angle neutron scattering methods for studying the structure of biological macromolecules

    International Nuclear Information System (INIS)

    Serdyuk, I.

    1995-01-01

    In recent 20 years thermal neutron scattering has been acknowledged an important instrument for structural studies in molecular biology. The methods of neutron diffraction of high resolution, which are not discussed in this paper, have already permitted to obtain a detailed representation of the course of proteolytic reactions and have arisen a number of new problems connected with the localization of water molecules and the H-D exchange. The methods of low resolution widely used due to a relative simplicity of the experiment have been successfully applied for both solving structural problems per se and investigating the changes in the structure when macromolecules perform their biological functions. The most promising are novel experimental approaches: the triple isotopic substitution method and the method of spin dynamic polarization. These methods ensure solving structural problems at a higher resolution than the dimensions of the macromolecules studied. Installation of new experimental instruments makes neutron measurements more accessible, and development of direct methods for interpretation of experimental data using the apparatus of spherical harmonics opens new possibilities for small-angle neutron scattering making it a necessary element for interpretation of diffraction data of monocrystals of intricate biological macromolecules. The paper presents a brief account of the tendencies in theoretical development and practical use of small-angle scattering for studying biological macromolecules. Special attention is given to the studies carried out in the Laboratory of Neutron Physics on a unique pulse IBR-2 reactor. (author) 14 refs

  4. Mitigation method of thermal transient stress by thermalhydraulic-structure total analysis

    International Nuclear Information System (INIS)

    Kasahara, Naoto; Jinbo, Masakazu; Hosogai, Hiromi

    2003-01-01

    This study proposes a rational evaluation and mitigation method of thermal transient loads in fast reactor components by utilizing relationships among plant system parameters and stresses induced by thermal transients of plants. A thermalhydraulic-structure total analysis procedure helps us to grasp relationship among system parameters and thermal stresses. Furthermore, it enables mitigation of thermal transient loads by adjusting system parameters. In order to overcome huge computations, a thermalhydraulic-structure total analysis code and the Design of Experiments methodology are utilized. The efficiency of the proposed mitigation method is validated through thermal stress evaluation of an intermediate heat exchanger in Japanese demonstration fast reactor. (author)

  5. Small-angle neutron scattering and molecular dynamics structural study of gelling DNA nanostars

    Energy Technology Data Exchange (ETDEWEB)

    Fernandez-Castanon, J.; Bomboi, F. [Sapienza–Università di Roma, P.le A. Moro 5, 00185 Roma (Italy); Rovigatti, L. [Rudolf Peierls C.T.P., University of Oxford, 1 Keble Road, Oxford OX1 3NP (United Kingdom); Faculty of Physics, University of Vienna, Boltzmanngasse 5, A-1090 Vienna (Austria); Zanatta, M. [Dipartimento di Fisica, Università di Perugia, Via Pascoli, 06123 Perugia (Italy); CNR-ISC, UOS Sapienza–Università di Roma, I-00186 Roma (Italy); Paciaroni, A. [Dipartimento di Fisica, Università di Perugia, Via Pascoli, 06123 Perugia (Italy); Comez, L. [Dipartimento di Fisica, Università di Perugia, Via Pascoli, 06123 Perugia (Italy); IOM-CNR, UOS Perugia c/o Dipartimento di Fisica e Geologia, Università di Perugia, Via Pascoli, 06123 Perugia (Italy); Porcar, L. [Institut Laue-Langevin, 71 Avenue des Martyrs, CS 20156, 38042 Grenoble Cedex 9 (France); Jafta, C. J. [Helmholtz-Zentrum Berlin, Hahn-Meitner-Platz 1, 14109 Berlin (Germany); Fadda, G. C. [Laboratoire Léon Brillouin, LLB, CEA Saclay, 91191 Gif-sur-Yvette Cedex (France); Bellini, T. [Department of Medical Biotechnology and Translational Medicine, Università di Milano, I-20133 Milano (Italy); Sciortino, F., E-mail: francesco.sciortino@uniroma1.it [Sapienza–Università di Roma, P.le A. Moro 5, 00185 Roma (Italy); CNR-ISC, UOS Sapienza–Università di Roma, I-00186 Roma (Italy)

    2016-08-28

    DNA oligomers with properly designed sequences self-assemble into well defined constructs. Here, we exploit this methodology to produce bulk quantities of tetravalent DNA nanostars (each one composed of 196 nucleotides) and to explore the structural signatures of their aggregation process. We report small-angle neutron scattering experiments focused on the evaluation of both the form factor and the temperature evolution of the scattered intensity at a nanostar concentration where the system forms a tetravalent equilibrium gel. We also perform molecular dynamics simulations of one isolated tetramer to evaluate the form factor numerically, without resorting to any approximate shape. The numerical form factor is found to be in very good agreement with the experimental one. Simulations predict an essentially temperature-independent form factor, offering the possibility to extract the effective structure factor and its evolution during the equilibrium gelation.

  6. Refinement of the crystal structure of malachite, Cu2(OH)2CO3, by neutron diffraction

    International Nuclear Information System (INIS)

    Zigan, F.; Joswig, W.; Schuster, H.D.; Mason, S.A.

    1977-01-01

    The crystal structure of malachite is refined (R = 0,021) with the intensity values of 635 independent neutron reflexions from a single crystal, rather free from absorption and extinction. Concerning the structural geometry, no essential deviations occur from the known results of x-ray diffraction. The thermal elongations are generally largest about the normal to the (201) layers, between which the bonding is relatively weak. In both of the (medium, bent) OH...O hydrogen bonds, the anisotropic thermal parameters, converted according to the riding model, are - with certain restrictions - in agreement with the measured infrared spectrum as well as with frequencies and directions of the proton vibration calculated from the bonding geometry on the basis of a theoretical model. (orig.) [de

  7. Pion structure function from leading neutron electroproduction and SU(2) flavor asymmetry

    Energy Technology Data Exchange (ETDEWEB)

    McKenney, Joshua R. [North Carolina State Univ., Raleigh, NC (United States); Thomas Jefferson National Accelerator Facility (TJNAF), Newport News, VA (United States); Univ. of North Carolina, Chapel Hill, NC (United States); Sato Gonzalez, Nobuo; Melnitchouk, Wally [Thomas Jefferson National Accelerator Facility (TJNAF), Newport News, VA (United States); Ji, Chueng-Ryong [North Carolina State Univ., Raleigh, NC (United States)

    2016-03-01

    We examine the efficacy of pion exchange models to simultaneously describe leading neutron electroproduction at HERA and the $\\bar{d}-\\bar{u}$ flavor asymmetry in the proton. A detailed $\\chi^2$ analysis of the ZEUS and H1 cross sections, when combined with constraints on the pion flux from Drell-Yan data, allows regions of applicability of one-pion exchange to be delineated. The analysis disfavors several models of the pion flux used in the literature, and yields an improved extraction of the pion structure function and its uncertainties at parton momentum fractions in the pion of $4 \\times 10^{-4} \\lesssim x_\\pi \\lesssim 0.05$ at a scale of $Q^2$=10 GeV$^2$. Based on the fit results, we provide estimates for leading proton structure functions in upcoming tagged deep-inelastic scattering experiments at Jefferson Lab on the deuteron with forward protons.

  8. Characterization of swollen structure of high-density polyelectrolyte brushes in salt solution by neutron reflectivity

    Energy Technology Data Exchange (ETDEWEB)

    Kobayashi, Motoyasu; Takahara, Atsushi [Institute for Materials Chemistry and Engineering, Kyushu University, 744 Motooka, Nishi-ku, Fukuoka 819-0395 (Japan); Terayama, Yuki [Graduate School of Engineering, Kyushu University (Japan); Hino, Masahiro [Reactor Research Institute, Kyoto University (Japan); Ishihara, Kazuhiko, E-mail: takahara@cstf.kyushu-u.ac.j [Graduate School of Engineering, University of Tokyo (Japan)

    2009-08-01

    Zwitterionic and cationic polyelectrolyte brushes on quartz substrate were prepared by surface-initiated atom transfer radical polymerization of 2-(methacryloyloxy)ethyl phosphorylcholine (MPC) and 2-(methacryloyloxy)ethyltrimethylammonium chloride (METAC), respectively. The effects of ionic strength on brush structure and surface properties of densely grafted polyelectrolyte brushes were analysed by neutron reflectivity (NR) measurements. NR at poly(METAC)/D{sub 2}O and poly(MPC)/D{sub 2}O interface revealed that the grafted polymer chains were fairly extended from the substrate surface, while the thickness reduction of poly(METAC) brush was observed in 5.6 M NaCl/D{sub 2}O solution due to the screening of the repulsive interaction between polycations by hydrated salt ions. Interestingly, no structural change was observed in poly(MPC) brush even in a salt solution probably due to the unique interaction properties of phosphorylcholine units.

  9. Neutron diffraction stress determination in W-laminates for structural divertor applications

    Directory of Open Access Journals (Sweden)

    R. Coppola

    2015-07-01

    Full Text Available Neutron diffraction measurements have been carried out to develop a non-destructive experimental tool for characterizing the crystallographic structure and the internal stress field in W foil laminates for structural divertor applications in future fusion reactors. The model sample selected for this study had been prepared by brazing, at 1085 °C, 13 W foils with 12 Cu foils. A complete strain distribution measurement through the brazed multilayered specimen and determination of the corresponding stresses has been obtained, assuming zero stress in the through-thickness direction. The average stress determined from the technique across the specimen (over both ‘phases’ of W and Cu is close to zero at −17 ± 32 MPa, in accordance with the expectations.

  10. Structure and dynamics of photosynthetic proteins studied by neutron scattering and molecular dynamic simulation

    International Nuclear Information System (INIS)

    Dellerue, Serge

    2000-01-01

    Understand the structure-dynamics-function relation in the case of proteins is essential. But few experimental techniques allow to have access to knowledge of fast internal movements of biological macromolecules. With the neutron scattering method, it has been possible to study the reorientation dynamics of side chains and of polypeptide skeleton for two proteins in terms of water or detergent and of temperature. With the use of the molecular dynamics method, essential for completing and interpreting the experimental data, it has been possible to assess the different contributions of the whole structure of proteins to the overall dynamics. It has been shown that the polypeptide skeleton presents an energy relaxation comparable to those of the side chains. Moreover, it has been explained that the protein dynamics can only be understood in terms of relaxation time distribution. (author) [fr

  11. The structure of para-toluidine by X-ray and neutron diffraction

    International Nuclear Information System (INIS)

    Bertinotti, A.L.

    1965-12-01

    The crystal and molecular structure of para-toluidine has been solved by X-ray and neutron diffraction counter techniques. The molecules are arranged in the form of infinite chains in the crystal, each molecule being linked to two neighbours by hydrogen bonds. The presence of the H bonds makes clear the difference in the melting points between para-toluidine and benzene hydrocarbons of related symmetry and molecular weight. Their direction accounts for the (001) cleavage and the growth anisotropy of crystals from supersaturated vapour phase. A structure-seeking method by computer has been elaborated, using lattice energy calculations applied to molecules treated as rigid bodies and making use of a simplex method for function minimization without calculation of derivatives. The way the available information is handled allows to increase the range of convergence, as shown in the case of para-toluidine. (author) [fr

  12. Total synthesis, structure, and oral absorption of a thiazole cyclic peptide, sanguinamide A

    DEFF Research Database (Denmark)

    Nielsen, Daniel S; Hoang, Huy N; Lohman, Rink-Jan

    2012-01-01

    The first total synthesis and three-dimensional solution structure are reported for sanguinamide A, a thiazole-containing cyclic peptide from the sea slug H. sanguineus. Solution phase fragment synthesis, solid phase fragment assembly, and solution macrocyclization were combined to give (1) in 10......% yield. Spectral properties were identical for the natural product, requiring revision of its structure from (2) to (1). Intramolecular transannular hydrogen bonds help to bury polar atoms, which enables oral absorption from the gut....

  13. Rietveld refinement of magnetic structures from pulsed-neutron-source powder-diffraction data

    International Nuclear Information System (INIS)

    Robinson, R.A.; Lawson, A.C.; Larson, A.C.; Von Dreele, R.B.; Goldstone, J.A.

    1994-01-01

    The General Structure Analysis System, GSAS, has recently been modified to include magnetic neutron- scattering cross-sections. Low-temperature diffraction data have been taken on the hexagonal noncollinear antiferromagnet UPdSn on both the HIPD and the NPD powder diffractometers ail LANSCE. The low-resolution data reveal that the magnetic structure has orthorhombic symmetry (magnetic space group P c m'c2 1 ) between 25K and 40K, and monoclinic symmetry (magnetic space group PC 1121 ) below 25K. The high-resolution data reveal that there are structural distortions with corresponding symmetry changes in each of these phases, to give chemical space groups Cmc2 1 and P2 1 , respectively, while the paramagnetic phase above 40K has space group P6 3 mc. Using GSAS, we have refined data sets from both diffractometers simultaneously, including both magnetic and structural cross-sections. Magnetoelastic coefficients for the distortions have been extracted and we have determined the sign of the coupling between the structural monoclinicity and the magnetic monoclinicity. The magnetic results from Rietveld refinement are in good agreement with model fitting to the integrated intensities of seven independent magnetic reflections and these, in turn, agree with measurements made on the same sample using the constant-wavelength reactor technique. Our results therefore validate, to some level, both the technique of using spallation sources for complicated magnetic structures and the specifics of the GSAS Rietveld code

  14. Gamma/neutron competition above the neutron separation energy in delayed neutron emitters

    Directory of Open Access Journals (Sweden)

    Valencia E.

    2014-03-01

    Full Text Available To study the β-decay properties of some well known delayed neutron emitters an experiment was performed in 2009 at the IGISOL facility (University of Jyväskylä in Finland using Total Absorption γ-ray Spectroscopy (TAGS technique. The aim of these measurements is to obtain the full β-strength distribution below the neutron separation energy (Sn and the γ/neutron competition above. This information is a key parameter in nuclear technology applications as well as in nuclear astrophysics and nuclear structure. Preliminary results of the analysis show a significant γ-branching ratio above Sn.

  15. Obtaining of total and thermal neutron flux in the carousel facility of the TRIGA MARK IPR-R1 reactor using the Monte Carlo transport method

    International Nuclear Information System (INIS)

    Guerra, Bruno Teixeira

    2011-01-01

    The IPR-R1 is a reactor type TRIGA, Mark-I model, manufactured by the General Atomic Company and installed at Nuclear Technology Development Centre (CDTN) of Brazilian Nuclear Energy Commission (CNEN), in Belo Horizonte, Brazil. It is a light water moderated and cooled, graphite-reflected, open-pool type research reactor. IPR-R1 works at 100 kW but it will be briefly licensed to operate at 250 kW. It presents low power, low pressure, for application in research, training and radioisotopes production. The fuel is an alloy of zirconium hydride and uranium enriched at 20% in 235 U. The goal this work is modelling of the IPR-R1 Research Reactor TRIGA using the codes MCNPX2.6.0 (Monte Carlo N-Particle Transport extend) and MCNP5 to the calculating the neutron flux in the carousel facility. In each simulation the sample was placed in a different position, totaling forty positions around of the reactor core. The comparison between the results obtained with experimental values from other work showing a relatively good agreement. Moreover, this methodology is a theoretical tool in validating of the experimental values and necessary for determining neutron flux which can not be accessible experimentally. (author)

  16. Total Cross-Sections of U, UO{sub 2} and ThO{sub 2} for Thermal and Subthermal Neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Beshai, S F [IAEA-fellow from Atomic Energy Establishment (Egypt)

    1966-03-15

    The total neutron cross-sections of U, UO{sub 2} and ThO{sub 2} have been measured from 0.0045 eV to 0.028 eV, using the time-of-flight technique. The samples were measured at 20 deg C. ThO{sub 2} was also measured at 750 deg C. The neutron source was the reactor Rl, Stockholm. The experimental results presented as graphs in the report show in detail the influence of Bragg scattering. The results further show that the increase of the temperature for the ThO{sub 2} sample gives an increase in the cross-section. The work also contains some calculations of the position in energy of Bragg edges for the three materials. These calculations show a very good agreement with the experiments. For uranium metal some calculations have been carried out also for the height ({sigma}{sup g}{sub hkl}) of the edges The agreement with the experiments is reasonable.

  17. An attempt of application of short lived 44K activity induced in the 44Ca(n,p)44K reaction using 14 MeV neutrons for total body calcium assessment in human subject

    International Nuclear Information System (INIS)

    Haratym, Z.; Kempisty, T.; Mikolajewski, S.; Rurarz, E.

    1999-01-01

    The status of in vivo neutron activation analysis techniques for the measurement of total body calcium in human subject is reviewed. Relevant data on the nuclear characteristics of calcium isotopes during interaction with neutrons ranging from slow up to 14 MeV neutrons are presented. Physical aspects of the measurement of in vivo total body calcium (TBCa) using 44 K activity induced in the 44 Ca(n,p) 44 K(T 1/2 =22.3 min) reaction by 14 MeV neutrons are discussed. The measurement of delayed γ-ray emitted during decay of activities induced in enriched 44 Ca, nat Ca, phantom filled with water solution of natural calcium and skeletal arm are considered. Results of measurements on the phantom and skeletal arm indicate a possibility to measure the TBCa using the 44 K activity. (author)

  18. Measurement of leakage neutron spectra from advanced blanket materials and structural materials induced by D-T neutrons. Correction for energy loss of charged particle in sample materials

    International Nuclear Information System (INIS)

    Nishio, Takashi; Kondo, Tetsuo; Takagi, Hiroyuki; Murata, Isao; Takahashi, Akito; Kokooo; Maekawa, Fujio; Ikeda, Yujiro; Takeuchi, Hiroshi

    2000-01-01

    D-T neutron benchmark experiments for LiAlO 2 , Li 2 TiO 3 , Li 2 ZrO 3 , Cu and W have been conducted at FNS of JAERI to validate five nuclear data files. The former three are promising advanced breeder materials and the latter two are important structural materials in a fusion reactor. From the results, all the nuclear data files were confirmed to be fairly reliable with respect to the prediction of neutron spectrum in the use of Li 2 TiO 3 and Cu. For LiAlO 2 and W, some large discrepancies between the experimental and calculated data were observed. For Li 2 ZrO 3 , the C/E values became very large for all the nuclear data files. (author)

  19. Structure of magnetic particles studied by small angle neutron scattering. [Magnetic colloid particles in stable liquid dispersion

    Energy Technology Data Exchange (ETDEWEB)

    Cebula, D J; Charles, S W; Popplewell, J

    1981-03-01

    The purpose of this note is to show how the use of small angle neutron scattering (SANS) can provide fundamental information on the structure of magnetic colloid particles in stable liquid dispersion. A more detailed account elaborating the use of the technique to provide fundamental information on interactions will appear later. This contribution contains some principal results on particle structure. The technique of SANS provides a very sensitive means of measuring particle size by measuring the scattered neutron intensity, I(Q), as a function of scattered wave vector, Q.

  20. A general method for computing the total solar radiation force on complex spacecraft structures

    Science.gov (United States)

    Chan, F. K.

    1981-01-01

    The method circumvents many of the existing difficulties in computational logic presently encountered in the direct analytical or numerical evaluation of the appropriate surface integral. It may be applied to complex spacecraft structures for computing the total force arising from either specular or diffuse reflection or even from non-Lambertian reflection and re-radiation.

  1. Total synthesis of the putative structure of the novel triquinane natural product isocapnellenone

    OpenAIRE

    Mehta, Goverdhan; Murthy, Sai Krishna A; Umarye, Jayant D

    2002-01-01

    A total synthesis of the ‘putative structure’ 7, attributed to the novel triquinane sesquiterpene isolated recently from two Buddelia species has been accomplished. The spectral data for 7 is a complete mismatch with those reported for the natural product and warrants a revision of the assigned structure.

  2. Total chemical synthesis and X-ray structure of kaliotoxin by racemic protein crystallography.

    Science.gov (United States)

    Pentelute, Brad L; Mandal, Kalyaneswar; Gates, Zachary P; Sawaya, Michael R; Yeates, Todd O; Kent, Stephen B H

    2010-11-21

    Here we report the total synthesis of kaliotoxin by 'one pot' native chemical ligation of three synthetic peptides. A racemic mixture of D- and L-kaliotoxin synthetic protein molecules gave crystals in the centrosymmetric space group P1 that diffracted to atomic-resolution (0.95 Å), enabling the X-ray structure of kaliotoxin to be determined by direct methods.

  3. Monitoring of concrete structures by using the 14 MeV tagged neutron beams

    International Nuclear Information System (INIS)

    Sudac, D.; Nad, K.; Obhodas, J.; Valkovic, V.

    2013-01-01

    The maintenance and repair of reinforced concrete structures, especially those submerged in the sea-water require effective inspection and monitoring techniques for assessing the state of corrosion in the reinforcement material. An underwater inspection system was developed which is able to monitor the corrosion of the reinforcement. The system is composed of a remotely operating vehicle (ROV) equipped with the sealed tube neutron generator (NG). By rotating the NG and by using the associated alpha particle technique it is possible to measure the concrete cover thickness together with the reinforcing bar diameter. The possibility of estimating the carbon and chloride contents in the concrete was investigated. Iron plates of different thickness, covered by 6 cm thick concrete block, were successfully detected and the thickness of the concrete cover was estimated. In addition, reinforcing bar of one and 3 cm in diameter were identified and measured. All measurements could be performed without cleaning the concrete surface from fouling material. -- Highlights: • An underwater inspection system was developed which is able to monitor the state of reinforcement corrosion. • The system is composed of a remotely operating vehicle (ROV) equipped with the sealed tube neutron generator (NG). • All measurements could be performed without cleaning the concrete surface from fouling material

  4. Structural design study of a proton beam window for a 1-MW spallation neutron source

    CERN Document Server

    Teraoku, T; Ishikura, S; Kaminaga, M; Maekawa, F; Meigo, S I; Terada, A

    2003-01-01

    A 1-MW spallation neutron source aiming at materials and life science researches will be constructed under the JAERI-KEK High-intensity Proton Accelerator Project (J-PARC). A proton beam passes through a proton beam window, and be injected into a target of the neutron source. The proton beam window functions as a boundary wall between a high vacuum area in the proton beam line and a helium atmosphere at about atmospheric pressure in a helium vessel which contains the target and moderators. The proton beam window is cooled by light water because high heat-density is generated in the window material by interactions with the proton beam. Then, uniformity of the water flow is requested at the window to suppress a hot-spot that causes excessive thermal stress and cooling water boiling. Also, the window has to be strong enough in its structure for inner stress due to water pressure and thermal stress due to heat generation. In this report, we propose two types of proton beam windows; one flat-type that is easy to m...

  5. Study of the structure of yrast bands of neutron-rich 114-124Pd isotopes

    Science.gov (United States)

    Chaudhary, Ritu; Devi, Rani; Khosa, S. K.

    2018-02-01

    The projected shell model calculations have been carried out in the neutron-rich 114-124Pd isotopic mass chain. The results have been obtained for the deformation systematics of E(2+1) and E(4+1)/E({2}+1) values, BCS subshell occupation numbers, yrast spectra, backbending phenomena, B( E2) transition probabilities and g-factors in these nuclei. The observed systematics of E(2+1) values and R_{42} ratios in the 114-124Pd isotopic mass chain indicate that there is a decrease of collectivity as the neutron number increases from 68 to 78. The occurrence of backbending in these nuclei as well as the changes in the calculated B( E2) transition probabilities and g -factors predict that there are changes in the structure of yrast bands in these nuclei. These changes occur at the spin where there is crossing of g-band by 2-qp bands. The predicted backbendings and predicted values of B( E2)s and g-factors in some of the isotopes need to be confirmed experimentally.

  6. Experimental determination of neutron capture cross sections of fast reactor structure materials integrated in intermediate energy spectra. Vol. 2: description of experimental structure

    International Nuclear Information System (INIS)

    Tassan, S.

    1978-01-01

    A selection of technical documents is given concerning the experimental determination of the neutron capture cross-sections of fast reactor structural materials (Fe, Cr, Ni...) integrated over the intermediate energy spectra. The experimental structure project and modifications of the reactor RB2 for this experiment, together with criticality and safety calculations, are presented

  7. ENDF/B-IV representation of the 238U total neutron cross section in the resolved resonance energy region

    International Nuclear Information System (INIS)

    de Saussure, G.; Olsen, D.K.; Perez, R.B.

    1976-01-01

    The ENDF/B-IV prescription fails to represent correctly the 238 U total (and scattering) cross section between the levels of the resolved range. It is shown how this representation can be improved by properly accounting for the contribution of levels outside the resolved region to the cross section at energies inside the resolved region, and by substituting the more precise multilevel Breit-Wigner formula for the presently used single-level formula. The importance of computing accurately the minima in the total cross section is illustrated by comparing values of the self-shielded capture resonance integral computed with ENDF/B-IV and with a more accurate cross section model

  8. The effect of the 238U neutron strength function uncertainty on resonance structure calculations in unresolved regions

    International Nuclear Information System (INIS)

    Koshcheev, V.N.; Manturov, G.N.; Sinitsa, V.V.

    1991-01-01

    The effects of the neutron strength function uncertainties on the calculated values of the self-shielding factors and energy dependence of the total and capture 238 U cross-sections in the unresolved resonance region are investigated. (author). 26 refs, 5 figs

  9. Measurements and analysis of the {sup 127}I and {sup 129}I neutron capture and total cross sections; Mesure et analyses des sections efficaces neutroniques totales et de capture radiative des iodes 127 et 129 de 0.5 eV a 100keV

    Energy Technology Data Exchange (ETDEWEB)

    Noguere, G

    2005-07-01

    Most of the experimental work on the interaction of neutrons with matter has focused on materials important to reactor physics and reactor structures. By comparison, the corresponding data for minor actinides or long-lived fission products are poor. A significant demand has developed for improved neutron cross-section data of these little-studied nuclides due to the surge of interest in the transmutation of nuclear waste. With 400 kg of {sup 129}I produced yearly in the reactors of the EU countries and a very long {beta}{sup -} half-life of 1.57 x 10{sup 7} years, iodine requires disposal strategies that will isolate this isotope from the environment for long periods of time. Therefore, {sup 129}I is potentially a key long-lived fission product for transmutation applications, since {sup 129}I transmutes in {sup 130}I after a single neutron capture and decays to {sup 130}Xe with a 12.36 h half-life. Accurate capture cross sections would help to reduce uncertainties in waste management concepts. For that purpose, Time-Of-Flight measurements covering the [0.5 eV-100 keV] energy range have been carried out at the 150 MeV pulsed neutron source GELINA of the Institute for Reference Materials and Measurements (IRMM). Two types of experiments have been performed at the IRMM, namely capture and transmission experiments. They are respectively related to the neutron capture and total cross sections. Since the PbI{sub 2} samples used in this work contain natural and radioactive iodine, extensive measurements of {sup 129}I have been carried out under the same experimental conditions as for the {sup 129}I. The data reduction process was performed with the AGS system, and the resonance parameters were extracted with the SAMMY and REFIT shape analysis codes. In a last step, the parameters have been converted into ENDF-6 format and processed with the NJOY code to produce point-wise and multigroup cross sections, as well as MCNP and ERANOS libraries. (author)

  10. Application of Neutron imaging in pore structure of hydrated wellbore cement: comparison of hydration of H20 with D2O based Portland cements

    Science.gov (United States)

    Dussenova, D.; Bilheux, H.; Radonjic, M.

    2012-12-01

    storage of the hydrogen atom. In such case, neutron tomography does not give information of the pore structure as neutrons will strongly scatter of H and the data have low count and low statistics or low neutron transmission. Hence, as the comparison and the possible tuning technique, neutron tomography measurements are performed on a Deuterium Oxide (D2O) or heavy water samples the same dimensions, cement composition, cement/liquid content and hydration time as the H2O samples. The advantage of using heavy water is that the total neutron cross-section for Deuterium is approximately four times smaller than Hydrogen's and, thus, permits better neutron transmission, i.e. better statistics. D2O does not alter cement properties or its chemical composition; therefore, the samples are almost identical. Comparison of the measurements using water and heavy water samples and the preparation of the measurement cement samples are discussed in this

  11. parity assignment of the pronounced structure in the radiative capture of neutrons by 238U below 100 keV

    International Nuclear Information System (INIS)

    Moore, M.S.; Corvi, F.; Mewissen, L.; Poortmans, F.

    1981-01-01

    Some years ago, Perez and de Saussure reported evidence for intermediate structure in the radiative capture cross sections of 238 U. More recently, these and additional data, obtained by a different experimental technique but which showed the same non-statistical behavior, were analyzed by Perez et al. Under the assumption that the structure could be attributed to doorway states in the p/sup 3/2/ neutron channel. The results of an experimental determination of the parity of the structure, using neutron capture-gamma ray spectroscopy are reported. Much of the structure below 50 keV appears to be due to s-wave interactions. The magnitude of the fluctuations is much larger than can be calculated with the usual unresolved - resonance treatment unless the average neutron and radiative-capture widths are correlated. It is shown that such an apparent correlation can arise as a result of multiple-scattering enhancement of radiative capture in the samples used, and it is concluded that the evidence for intermediate structure in the capture of neutrons by 238 U is not yet firmly established

  12. Recent SLAC measurements of the spin dependent structure functions for the proton and neutron

    International Nuclear Information System (INIS)

    Zapalac, G.

    1995-09-01

    The authors present results from SLAC experiments E142 and E143 for the spin dependent structure functions of the proton g 1 p (x, Q 2 ) and neutron g 1 n (x,Q 2 ) measured in deep inelastic scattering of polarized electrons from a polarized target. Experiment E142 measures ∫ 0 1 g 1 n (x)dx = -0.022 ± 0.011 at 2 > = 2 (GeV/c) 2 using a polarized 3 He target. Experiment E143 measures ∫ 0 1 g 1 p (x)dx = 0.129 ± 0.011 at 2 > = 3 (GeV/c) 2 using a polarized NH 3 target. These results are combined at Q 2 = 3 (GeV/c) 2 to yield ∫ 0 1 [g 1 p (x) - g 1 n (x)]dx = 0.151 ± 0.015. The Bjorken sum rule predicts 0.171 ± 0.008

  13. Structure of compensating centers in neutron irradiated n-type germanium

    International Nuclear Information System (INIS)

    Erchak, D.P.; Kosobutskij, V.S.; Stel'makh, V.F.

    1989-01-01

    Structural model of one of the main compensating defects of Ge-M1, Ge-M5, Ge-M6 in neutron irradiated (10 18 -10 20 cm -2 ) germanium, strongly alloyed (2x10 18 -3x10 19 cm -3 ) with antimony, phosphorus and arsenic respectively, is suggested. The above mentioned compensating centers are paramagnetic in a positive charge state and represent a vacancy, two nearby germanium atoms of which are replaced with two atoms of corresponding fine donor impurity. It is mainly contributed (63%- for Ge-M5 centers, 56% - for Ge-M6 centers) by orbitals of two germanium atoms neighbouring the vacancy. The angle of the bonds of each of two mentioned germanium atoms with its three neighbours and orientation of maximum electron density of hybride orbital, binding both germanium atoms, is approximately by 5 deg greater the tetrahedral one

  14. Structure of neutron star crusts from new Skyrme effective interactions constrained by chiral effective field theory

    Science.gov (United States)

    Lim, Yeunhwan; Holt, Jeremy W.

    2017-06-01

    We investigate the structure of neutron star crusts, including the crust-core boundary, based on new Skyrme mean field models constrained by the bulk-matter equation of state from chiral effective field theory and the ground-state energies of doubly-magic nuclei. Nuclear pasta phases are studied using both the liquid drop model as well as the Thomas-Fermi approximation. We compare the energy per nucleon for each geometry (spherical nuclei, cylindrical nuclei, nuclear slabs, cylindrical holes, and spherical holes) to obtain the ground state phase as a function of density. We find that the size of the Wigner-Seitz cell depends strongly on the model parameters, especially the coefficients of the density gradient interaction terms. We employ also the thermodynamic instability method to check the validity of the numerical solutions based on energy comparisons.

  15. Structure analysis of K3H(SO4)2 by neutron powder diffraction

    International Nuclear Information System (INIS)

    Murakami, Satoshi; Kuroiwa, Yoshihiro; Noda, Yukio; Nakai, Yusuke; Kamiyama, Takashi; Asano, Hajime.

    1993-01-01

    Neutron powder diffraction experiments of K 3 H(SO 4 ) 2 were carried out at KENS-HRP station in order to obtain the positional parameters of hydrogen nuclei. The data was taken at six different temperatures from room temperature to 20K. Even though K 3 H(SO 4 ) 2 contained a hydrogen atom, the structural analysis was successfully performed by using a program RIETAN. Concerning the hydrogen position, four different models give almost the same R-factor so that the state of the hydrogen nucleus is not uniquely determined. The result based on the assumption that a hydrogen nucleus occupies two sites shows that the distance of split hydrogen nuclei is shorter than the distance of hydrogen electron clouds. This result suggests that a large polarizability exists in a hydrogen atom. (author)

  16. The Small-Angle Neutron Scattering Data Analysis of the Phospholipid Transport Nanosystem Structure

    Science.gov (United States)

    Zemlyanaya, E. V.; Kiselev, M. A.; Zhabitskaya, E. I.; Aksenov, V. L.; Ipatova, O. M.; Ivankov, O. I.

    2018-05-01

    The small-angle neutron scattering technique (SANS) is employed for investigation of structure of the phospholipid transport nanosystem (PTNS) elaborated in the V.N.Orekhovich Institute of Biomedical Chemistry (Moscow, Russia). The SANS spectra have been measured at the YuMO small-angle spectrometer of IBR-2 reactor (Joint Institute of Nuclear Research, Dubna, Russia). Basic characteristics of polydispersed population of PTNS unilamellar vesicles (average radius of vesicles, polydispersity, thickness of membrane, etc.) have been determined in three cases of the PTNS concentrations in D2O: 5%, 10%, and 25%. Numerical analysis is based on the separated form factors method (SFF). The results are discussed in comparison with the results of analysis of the small-angle X-ray scattering spectra collected at the Kurchatov Synchrotron Radiation Source of the National Research Center “Kurchatov Institute” (Moscow, Russia).

  17. Effect of neutron radiation on mechanical properties of permanent near core structures

    International Nuclear Information System (INIS)

    Tavassoli, A.A.

    1988-01-01

    Several hundred specimens have been tested in order to assess the effects of low dose neutron radiation ( 0 C and ductility and toughness are primary design concerns, the changes provoked, by doses up to 1.3 dpa, in overall mechanical properties of welded joints are small. For upper core structure, where the operating temperature is about 550 0 C and fatigue and creep resistance are major design needs, the changes induced, through formation of up to about 2 appm helium, in conventional fatigue properties or fatigue with short hold times are negligible. With increasing hold time, intergranular rupture in irradiated specimens is enhanced but the limited number of tests does not allow definite conclusions to be drawn. 53 refs, 3 tabs, 9 figs

  18. A neutron diffraction study on deuterated Rochelle salt structure at - 195degC paraelectric phase

    International Nuclear Information System (INIS)

    Iwata, Yutaka; Mitani, Shigeshi; Fukui, Susumu; Shibuya, Iwao

    1989-01-01

    Neutron diffraction study on the low temperature paraelectric phase of Rochelle salt was performed using deuterated single crystal specimen. Large anisotropic thermal motions of atoms are found to be prevailing in the lower paraelectric phase. This indicates the disordering of atoms and the analysis by two-site split-atom method showed that a split atom model holds equally well with an ordinary non-split model. By connecting split positions selectively, a disordered paraelectric structure, which is composed of half-occupied units, was obtained. These units can be regarded as ones in the ferroelectric phase according to a deduction from an order-disorder phase transition scheme. A possibility of existence of the 'local disorder' of O(5)-H group in the tartrate molecule was examined by Fourier method and a result proved to be negative. Present disordered model gives better understanding to the phase transition scheme of Rochelle salt than the local disorder model case. (author)

  19. Comparison of micelle structure of glycolipids with different head groups by small angle neutron scattering

    International Nuclear Information System (INIS)

    He, Lizhong; Middelberg, Anton; Hartmann, Thorsten; Niemeyer, Bernd; Garamus, V.M.; Willumeit, Regine

    2005-01-01

    Full text: Glycolipids such as n-alkyl- beta-D-glucopyranoside and n-alkyl- beta-D-maltopyranoside can self-assemble into different structures depending on solution conditions. Their amphiphilic properties enable them to serve as biosurfactants in biology and biotechnology, especially for solubilizing membrane proteins. The physicochemical properties of glycolipids have attracted attentions from several research groups, aiming to better understand their application in biological and environmental processes. For example, small angle neutron and X-ray scattering have been used to study micelle structures formed by glycolipids. Our previous work has shown that n-octyl-beta- D-glucopyranoside and n-octyl- beta-D-maltopyranoside form micelles with different structure, suggesting an important role of the sugar head group in micelle formation. In the present work, we further compare micelle structures of n-octyl- beta-Dglucopyranoside and n-octyl- beta-D-galactopyranoside. These two glycolipids have the same hydrophobic tail and their head sugar groups differ only in the conformation with one hydroxyl group pointing to different direction. Our SANS data together with phase behaviours reported by other group have suggested that a slight alteration of head group conformation can significantly affect self-assembly of glycolipids. (authors)

  20. Measuring the Neutron and 3He Spin Structure at Low Q2

    International Nuclear Information System (INIS)

    Vince Sulkosky

    2005-01-01

    The spin structure of the nucleon has been of great interest over the past few decades. Sum rules, including the Gerasimov-Drell-Hearn (GDH), and moments of the spin structure functions are powerful tools for understanding nucleon structure. The GDH sum rule, originally derived for real photon absorption, has been generalized to nonzero Q 2 . The goal of Jefferson Lab experiment E97-110 is to perform a precise measurement of the Q 2 dependence of the generalized GDH integral and of the moments of the neutron and 3 He spin structure functions between 0.02 and 0.3 GeV 2 . This Q 2 range will allow us to test predictions of Chiral Perturbation Theory, and verify the GDH sum rule by extrapolating the integral to the real photon point. The measurement will also contribute to the understanding of nucleon resonances. The data have been taken in Hall A using a high resolution spectrometer with the addition of a septum magnet, which allowed us to access the low Q 2 region. The analysis's status, prospects and impact will be discussed

  1. The use of neutron imaging for the study of honeycomb structures in aircraft

    International Nuclear Information System (INIS)

    Hungler, P.C.; Bennett, L.G.I.; Lewis, W.J.; Brenizer, J.S.; Heller, A.K.

    2009-01-01

    Highly maneuverable aircraft, such as the CF188 Hornet, have several flight control surfaces on both the leading and the trailing edges of the wing surfaces. They are composed of composite panels constructed of aluminum honeycomb core usually covered with graphite epoxy skins. Although very light and structurally stiff, they are being compromised by water ingress. The trapped water degrades their structural integrity by interacting with the adhesive. Various studies are underway to understand the movement of water in the honeycomb core as well as to determine a method of removing the water. With a vertical neutron beam tube at Royal Military College (RMC), the component can be positioned horizontally and the pooled water in each honeycomb cell can be imaged. These images have been compared with those from a horizontal beam and thus vertical placement of the structure at Pennsylvania State University Radiation Science and Engineer Center's Breazeale reactor. Thereby, both the filet bond between the honeycomb and the skin as well as the node bond between the honeycomb cells can be studied to determine their contribution to the movement of water throughout the structure. Moreover, the exit path for water has been visualized as part of developing a drying procedure for these flight control surfaces.

  2. Analysis of the spatial structure of rigid polyphenylene dendrimers by small-angle neutron scattering

    International Nuclear Information System (INIS)

    Rosenfeldt, S.; Dingenouts, N.; Poetschke, D.; Ballauff, M.; Berresheim, A.J.; Muellen, K.; Lindner, P.; Saalwaechter, K.

    2005-01-01

    The analysis of the spatial structure of a rigid polyphenylene dendrimer G4-M of fourth generation by small-angle neutron scattering (SANS) is presented. This dendrimer is composed of phenyl units and is therefore devoid of any flexible unit. The scattering intensity of dilute solutions of the dendrimer was measured by SANS at different contrast which was adjusted by mixtures of protonated and deuterated toluene. Hence, the method of contrast variation could be applied and the data yield the scattering function extrapolated to infinite contrast. The comparison of this data with simulations demonstrates that the scaffold of the dendrimer is rigid as expected from its chemical structure. The positions of the various units setting up consecutive shells of the dendrimer are relatively well localized and the entire structure cannot be modeled in terms of spherically symmetric models. No backfolding of the terminal groups can occur and the model calculations demonstrate that higher generations of this dendritic scaffold must exhibit a dense shell and a congestion of the terminal groups. This finding is directly corroborated by recent solid-state NMR data. All results show that the rigid dendrimer investigated here presents the first example for a dendritic structure whose segment density does not have its maximum at the center. Rigid scaffolds are therefore the only way to achieve the goal of a 'dense-shell' dendrimer whereas flexible scaffolds leads invariably to the 'dense-core' case

  3. Crystal structure investigations on cation-substituted alums by X-ray and neutron diffraction

    International Nuclear Information System (INIS)

    Abdeen, A.M.

    1980-04-01

    The crystal structures of the three alums: NH 4 Al(SO 4 ) 2 .12H 2 O, (NH 3 CH 3 )Al(SO 4 ) 2 .12H 2 O and (NH 3 OH)Al(SO 4 ) 2 .12H 2 O have been determined from three-dimensional neutron diffraction data enhanced by X-ray diffraction when necessary. These compounds crystallize cubic in space group Pa3. The structures of the three alums exhibit partial occupancies of crystallographic sites for the NH 4 , (NH 3 CH 3 ) and (NH 3 OH) group atoms. This can be explained by a quantized rotation of the three groups around an axis perpendicular to the [111] direction. Some of the (SO 4 ) 2- groups in the NH 4 -alum are disordered with about 17% of the sulfate tetrahedra being in a reversed orientation around the sulfur atom. The disorder in (NH 3 CH 3 ) and (NH 3 OH)-alums is only 4,3% and 3.0% respectively. The atoms in the alum structures are held together by a system of hydrogen bonds between the water molecules and between the water molecules and the sulfate oxygen atoms. In these three structures there is a strong indication that shorter hydrogen bonds tend to be nearly linear. (orig.)

  4. The E142 SLAC experiment: measurement of the neutron gn1(x) spin structure function

    International Nuclear Information System (INIS)

    Roblin, Y.

    1995-01-01

    This thesis describes the E142 experiment which has been carried out at the Stanford Linear Accelerator (SLAC), USA, from October to December 1992. This experiment of polarized inelastic scattering of a 22.6 GeV electron beam on a polarized helium 3 target has allowed the first measurement of the neutron g n 1 (x) spin structure function. The knowledge of this structure function gives informations on the nucleon spin structure. On the other hand, the g n 1 (x) structure function integral value on the 0 2 mean value of 2 GeV 2 after some extrapolations. This value is at about two standard deviations away from the theoretical predictions of the Ellis-Jaffe rule. Thanks to the existing experimental results for the proton (E143 experiment), the Bjorken sum rule has been precisely tested and is perfectly compatible with the theoretical value. The results have allowed to estimate the nucleon spin fraction carried by the quarks. (J.S.). 86 refs., 58 figs., 13 tabs

  5. Smart nanogels at the air/water interface: structural studies by neutron reflectivity

    Science.gov (United States)

    Zielińska, Katarzyna; Sun, Huihui; Campbell, Richard A.; Zarbakhsh, Ali; Resmini, Marina

    2016-02-01

    The development of effective transdermal drug delivery systems based on nanosized polymers requires a better understanding of the behaviour of such nanomaterials at interfaces. N-Isopropylacrylamide-based nanogels synthesized with different percentages of N,N'-methylenebisacrylamide as cross-linker, ranging from 10 to 30%, were characterized at physiological temperature at the air/water interface, using neutron reflectivity (NR), with isotopic contrast variation, and surface tension measurements; this allowed us to resolve the adsorbed amount and the volume fraction of nanogels at the interface. A large conformational change for the nanogels results in strong deformations at the interface. As the percentage of cross-linker incorporated in the nanogels becomes higher, more rigid matrices are obtained, although less deformed, and the amount of adsorbed nanogels is increased. The data provide the first experimental evidence of structural changes of nanogels as a function of the degree of cross-linking at the air/water interface.The development of effective transdermal drug delivery systems based on nanosized polymers requires a better understanding of the behaviour of such nanomaterials at interfaces. N-Isopropylacrylamide-based nanogels synthesized with different percentages of N,N'-methylenebisacrylamide as cross-linker, ranging from 10 to 30%, were characterized at physiological temperature at the air/water interface, using neutron reflectivity (NR), with isotopic contrast variation, and surface tension measurements; this allowed us to resolve the adsorbed amount and the volume fraction of nanogels at the interface. A large conformational change for the nanogels results in strong deformations at the interface. As the percentage of cross-linker incorporated in the nanogels becomes higher, more rigid matrices are obtained, although less deformed, and the amount of adsorbed nanogels is increased. The data provide the first experimental evidence of structural changes

  6. Structural design study of a proton beam window for a 1-MW spallation neutron source

    Energy Technology Data Exchange (ETDEWEB)

    Teraoku, Takuji; Terada, Atsuhiko; Maekawa, Fujio; Meigo, Shin-ichiro; Kaminaga, Masanori; Ishikura, Syuichi; Hino, Ryutaro [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    2003-03-01

    A 1-MW spallation neutron source aiming at materials and life science researches will be constructed under the JAERI-KEK High-intensity Proton Accelerator Project (J-PARC). A proton beam passes through a proton beam window, and be injected into a target of the neutron source. The proton beam window functions as a boundary wall between a high vacuum area in the proton beam line and a helium atmosphere at about atmospheric pressure in a helium vessel which contains the target and moderators. The proton beam window is cooled by light water because high heat-density is generated in the window material by interactions with the proton beam. Then, uniformity of the water flow is requested at the window to suppress a hot-spot that causes excessive thermal stress and cooling water boiling. Also, the window has to be strong enough in its structure for inner stress due to water pressure and thermal stress due to heat generation. In this report, we propose two types of proton beam windows; one flat-type that is easy to manufacture, and the other, curved-type that has high stress resistivity. As a part of design study for the windows, evaluation of strength of structure and thermal hydraulic analysis were conducted. As a result, it was found that sufficient heat removal was assured with uniform water flow at the window, and stress caused by internal water pressure and thermal stress could be maintained below allowable stress values. Accordingly, it was confirmed that the proton beam window designs were feasible. (author)

  7. P-odd effects observed in the reactions with neutrons and isospin structure of weak nucleon-nucleon interaction

    International Nuclear Information System (INIS)

    Smotritskij, L.M.

    2001-01-01

    Application of resonance phase for two quasi-stationary states with similar spin and unlike parity is shown to enable to coordinate the experimentally observed signed dependence of P-odd effects in neutron reactions with the theory. The developed approach enables to obtain information on isospin structure of a weak nucleon-nucleon interaction [ru

  8. The shielding performance of multilayer composite shielding structures to 14.8 MeV fast neutrons

    International Nuclear Information System (INIS)

    Shen Zhiqiang; Kang Qing; Xu Jun; Wang Zhenggang; Lu Nan

    2014-01-01

    Cement-based round thin-layer samples mixed with 30% quality content of barite, and 20% quality content of carbide boron has Prepared, the same-diameter sliced samples of pure graphite and pure polyethylene has cut, then, samples combination and cross stack order has designed, formed four species Multilayer Composite shield structure, at last, neutron attenuation measurements has been done by experimental system of using 14.8 MeV neutrons from the 5SDH-2 accelerator and long counter composition, penetrating rate of samples and the shield structure to 14.8 MeV fast neutron has tested, and attenuation section has calculated. Results show that 14.8 MeV fast neutrons to higher penetration rates of thin layer samples, attenuation cross section of samples distinguish small between each other, must be increasing the thickness of the samples to reduce the experimental uncertainty; through composed of attenuation cross section and thickness parameters of composite structure, can more accurately predict the shielding ability of composite structures, error between calculation results and experimental results in 4%. (authors)

  9. Structure of zinc and niobium tellurite glasses by neutron and x-ray diffraction

    Science.gov (United States)

    Hoppe, U.; Yousef, E.; Rüssel, C.; Neuefeind, J.; Hannon, A. C.

    2004-03-01

    Neutron and x-ray diffraction experiments of high resolving power with neutrons from a spallation source and high-energy photons from a synchrotron have been performed on compositional series of binary Zn, Nb and on mixed Zn/Nb tellurite glasses. The Te-O, Zn-O and Nb-O coordination numbers are determined by Gaussian fitting of the first-neighbour peaks in the neutron and x-ray data simultaneously. The transition of TeO4 to TeO3 units with increasing fraction of a second component is indicated by decreasing total Te-O coordination numbers. This transition appears different for glasses with ZnO or Nb2O5 additions. Details of the Te-O peaks suggest there are two species of Te-O bonds with lengths of {\\sim }0.19 and {\\sim }0.21 nm. The change of their fractions shows excellent agreement with the existence of TeO4 trigonal bipyramids and TeO3 trigonal pyramids. All oxygen atoms from ZnO and Nb2O5 are used for rupture of Te-O-Te bridges, which is accompanied with a change of nearly all participating TeO4 to TeO3 groups. The tendency for a {\\mathrm {TeO}}_{4} \\to {\\mathrm {TeO}}_{3} change decreases for glasses of higher second component content which is accompanied by the occurrence of TeO4 groups with non-bridging oxygens. The Nb tellurite glasses show transition to network-forming behaviour with the formation of Nb-O-Nb bridges. The fractions of TeO3 units of ternary Zn/Nb tellurite glasses agree with an additivity behaviour of the modifying effects of ZnO and Nb2O5 additions. Some of these results have already been presented in thesis work: Yousef E 2003 A study of some physical properties of tellurite glass (Al-Azhar University, Assiut Egypt).

  10. Structure of molten Bi-Sb-alloys by means of neutron diffraction

    International Nuclear Information System (INIS)

    Lamparter, P.; Knoll, W.; Steeb, S.

    1976-01-01

    The structural investigations with melts can be subdivided into two groups: The first group contains molten metals and molten alloys, and one can state that the structure of molten metals and of molten alloys nowadays is rather well understood. Interference functions of molten metals may be described by a hard sphere model. This is valid also for molten alloys with statistical distribution. For the second group, namely molten non-metals and molecular melts, the interference functions as well as the pair correlation functions are very offen rather complicated and not well understood. The present study is concerned with the transition region between these two groups. It is shown that the melts of the Bi-Sb system exhibit a change from metallic to non-metallic structure. Regarding the experimental details: the experiments were done with the two-axes spectrometer D 4 at the high-flux reactor at Grenoble. The containers consisted of cylindrical quartz tubes with a wall thickness of 0.1 cm. The furnace consisted of a direct-heated vanadium tube. The wavelength of the neutrons was 0.695 A. The final result is that the structure in molten Bi-Sb-alloys consists of primitive tetrahedra with coordination number 3. There are less tetrahedra in molten Bi than in molten Sb. Also with rising temperature the number of tetrahedra decreases. It is shown how to compose the coordination numbers of two structures to get the observed coordination number. The observed values are always the mean values of the two structures. (orig./HK) [de

  11. Total scattering investigation of materials for clean energy applications: the importance of the local structure.

    Science.gov (United States)

    Malavasi, Lorenzo

    2011-04-21

    In this Perspective article we give an account of the application of total scattering methods and pair distribution function (PDF) analysis to the investigation of materials for clean energy applications such as materials for solid oxide fuel cells and lithium batteries, in order to show the power of this technique in providing new insights into the structure-property correlation in this class of materials.

  12. White light coronal structures and flattening during six total solar eclipses

    Directory of Open Access Journals (Sweden)

    B.A. Marzouk

    2016-12-01

    Flattening index is the first quantitative parameter introduced for analyses of the global structure of the solar corona. It varies with respect to the phase of the solar activity and sunspot number. In this paper we study the solar corona during the 1990, 1999, 2006, 2008, 2009 and 2012 total solar eclipses. We obtain flattening coefficients for all the six eclipses by using a new computer program. Our results are in a good agreement with published results.

  13. Structure in K--nucleon total cross sections below 1.1 GeV/c

    International Nuclear Information System (INIS)

    Carroll, A.S.; Chiang, I.; Kycia, T.F.; Li, K.K.; Mazur, P.O.; Michael, D.N.; Mockett, P.M.; Rahm, D.C.; Rubinstein, R.

    1976-01-01

    Total cross sections of K - p and K - d have been measured between 410 and 1070 MeV/c with high statistical precision. In addition to the well known Λ (1520), Λ (1820), and Σ (1769), we confirmed the presence of the Λ (1692) and the Σ (1670). We have also observed several structures which could be Y* resonances: Λ (1646), Λ (1735), Σ (1583), Σ (1608), Σ (1633), and Σ (1715)

  14. Total reflection X-ray fluorescence analysis with synchrotron radiation monochromatized by multilayer structures

    International Nuclear Information System (INIS)

    Rieder, R.; Wobrauschek, P.; Ladisich, W.; Streli, C.; Aiginger, H.; Garbe, S.; Gaul, G.; Knoechel, A.; Lechtenberg, F.

    1995-01-01

    To achieve lowest detection limits in total reflection X-ray fluorescence analysis (TXRF) synchrotron radiation has been monochromatized by a multilayer structure to obtain a relative broad energy band compared to Bragg single crystals for an efficient excitation. The energy has been set to 14 keV, 17.5 keV, 31 keV and about 55 keV. Detection limits of 20 fg and 150 fg have been achieved for Sr and Cd, respectively. ((orig.))

  15. A neutron and synchrotron investigation of the electronic structure of lanthanide zirconates

    International Nuclear Information System (INIS)

    Clements, Richard; Kennedy, Brendan; Ling, Chris; Stampfl, Anton P.J.

    2009-01-01

    Full text: The lanthanide zirconates are of interest for use in inert matrix fuels and nuclear wasteforms. A variety of studies have been performed to determine the suitability of a material as an inert matrix or wasteform. For use in these applications, the material's structure must be resistant to radiation damage and its thermal, thermodynamic and mechanical properties must be known. The structure's ability to incorporate an actinide host into the lattice vacancy must also be known. These properties may be better understood by investigating the f-electronic structure, which has historically proved difficult to model. We have undertaken a synthesis of the full range of lanthanide zirconate series using solid state techniques. We have performed neutron powder diffraction on a selection of the series in conjunction with the following measurements using synchrotron radiation: powder x-ray diffraction, VUV photoluminescence spectra, x-ray photoemission spectroscopy (XPS) and x-ray absorption near edge spectroscopy (XANES) The results are to be analysed using OFT modeling techniques. These results will be presented, along with details of the analysis and synthetic techniques used.

  16. Fractal Structures on Silica Aerogels Containing Titanium: A Small Angle Neutron Scattering Study

    International Nuclear Information System (INIS)

    Widya Sari; Dian Fitriyani; Abdul Aziz Mohamed; Noordin Ibrahim

    2009-01-01

    Full text: The fractal structure of silica aerogels containing titanium has been investigated by means of small-angle neutron scattering (SANS) technique. The SANS experiments were conducted using a 36 meter SANS BATAN spectrometer (SMARTer) in Serpong, Indonesia in the range of momentum transfer Q, 0.006 -1 ) < 0.3. The power-law for a fractal object scattering Q-D observed from all measured samples. The Fourier transform of pattern I(Q) a pair correlation model function was implemented in analyzing the structure factor from the power-law scattering profiles. The results are showing that the silica aerogels containing titanium has a mass fractal where its dimension DM is larger than the pure silica aerogels. The mass fractal dimension of silica aerogels containing titanium is relatively constant between 2.23 to 2.40 with the decrease of acid concentrations during a sol-gel process and formed a nanometer size of aggregate. Those fractal structures were simulated using a Delphi language and the results are presented in this paper. (author)

  17. Study of α-crystallin structure by small-angle neutron scattering with contrast variation

    International Nuclear Information System (INIS)

    Krivandin, A.V.; Muranov, K.O.; Polyanskij, N.B.; Ostrovskij, M.A.; Murugova, T.N.; Kuklin, A.I.; Aksenov, V.L.

    2010-01-01

    The structure of the oligomeric protein α-crystallin from the bovine eye lens has been investigated by small-angle neutron scattering (SANS) by the contrast variation method (volume fraction of D 2 O was 0, 23, 68 and 90%). Experiments were carried out on YuMO spectrometer (IBR-2 reactor, JINR). From the SANS curves the match point for α-crystallin (43% D 2 O) and its average scattering length density at this point (2.4·10 10 cm -2 ) have been obtained. The radius of gyration and distance distribution functions for α-crystallin have been calculated as well. On the basis of these calculations it was concluded that α-crystallin has a homogeneous distribution of the scattering density in domains inaccessible for water penetration and all parts of this protein undergo a uniform deuteration. The latter indicates that all α-crystallin subunits have an equal accessibility for water and presumably for some other low molecular weight substances. These conclusions on the α-crystallin structure (a homogeneous distribution of the scattering density and an equal accessibility of all subunits for low molecular weight substances) should be taken into account in the time of elaboration of α-crystallin quaternary structure models

  18. Modification of the mesoscopic structure in neutron irradiated EPDM viewed through positron annihilation spectroscopy and dynamic mechanical analysis

    International Nuclear Information System (INIS)

    Lambri, O.A.; Plazaola, F.; Axpe, E.; Mocellini, R.R.; Zelada-Lambri, G.I.; Garcia, J.A.; Matteo, C.L.; Sorichetti, P.A.

    2011-01-01

    This article focuses on the study of the mesoscopic structure in neutron irradiated EPDM both from experimental and theoretical points of view. In this work we reveal completely the modification of the mesostructure of the EPDM due to neutron irradiation, resolving volume fraction, size and distribution of the crystalline zones as a function of the irradiation dose. Positron annihilation spectroscopy and dynamic mechanical analysis techniques are applied and the results are discussed by means of new theoretical results for describing the interaction process between the crystals and amorphous zones in EPDM.

  19. Spectroscopy of 9Be and observation of neutron halo structure in the states of positive parity rotational band

    Directory of Open Access Journals (Sweden)

    Demyanova A.S.

    2014-03-01

    Full Text Available The differential cross sections of the 9Be + α inelastic scattering at 30 MeV were measured at the tandem of Tsukuba University. All the known states of 9Be up to energies ~ 12 MeV were observed and decomposed into three rotational bands, each of them having a cluster structure consisting of a 8Be core plus a valence neutron in one of the sub-shells: p3/2−, s1/2+ and p1/2−. Existence of a neutron halo in the positive parity states was confirmed.

  20. Neutron polarization

    International Nuclear Information System (INIS)

    Firk, F.W.K.

    1976-01-01

    Some recent experiments involving polarized neutrons are discussed; they demonstrate how polarization studies provide information on fundamental aspects of nuclear structure that cannot be obtained from more traditional neutron studies. Until recently, neutron polarization studies tended to be limited either to very low energies or to restricted regions at higher energies, determined by the kinematics of favorable (p, vector n) and (d, vector n) reactions. With the advent of high intensity pulsed electron and proton accelerators and of beams of vector polarized deuterons, this is no longer the case. One has entered an era in which neutron polarization experiments are now being carried out, in a routine way, throughout the entire range from thermal energies to tens-of-MeV. The significance of neutron polarization studies is illustrated in discussions of a wide variety of experiments that include the measurement of T-invariance in the β-decay of polarized neutrons, a search for the effects of meson exchange currents in the photo-disintegration of the deuteron, the determination of quantum numbers of states in the fission of aligned 235 U and 237 Np induced by polarized neutrons, and the double- and triple-scattering of fast neutrons by light nuclei

  1. Estimation of total as well as bioaccessible levels and average daily dietary intake of iodine from Japanese edible seaweeds by epithermal neutron activation analysis

    International Nuclear Information System (INIS)

    Fukushima, M.; Chatt, A.

    2012-01-01

    An epi-thermal instrumental neutron activation analysis (EINAA) method in conjunction with Compton suppression spectrometry (EINAA-CSS) was used for the determination of total iodine in eight different species of edible seaweeds from Japan. This method gave an absolute detection limit of about 2 μg. The accuracy of the method was evaluated using various reference materials and found to be generally in agreement within ±6% of the certified values. The longitudinal distributions of iodine at different growing stages in Japanese sea mustard and tangle seaweeds were investigated. For a 150-cm-high tangle, the highest concentration (5,360 mg/kg) of iodine was found at the root, then decreased slowly to 780 mg/kg in the middle portion (60-75 cm), and increased to 2,300 mg/kg at the apex. On the other hand, for a 190-cm-high sea mustard the highest levels of iodine were found both at the roots (164 mg/kg) and apex (152 mg/kg) with lower values (98 mg/kg) in the middle section. In order to estimate the bioaccessible fraction of iodine, seaweeds were digested by an in vitro enzymolysis method, dietary fibre separated from residue, and both fractions analyzed by EINAA-CSS. The average daily dietary intakes of total (0.14 mg) as well as bioaccessible fraction (0.12 mg) of iodine from the consumption of sea mustards were estimated. (author)

  2. Effect Of Soil Contamination Due To Wastewater Irrigation On Total Co As Determined By Neutron Activation And Other Conventional Analytical Techniques In Some Soils Of Egypt

    International Nuclear Information System (INIS)

    Abdel-Sabour, M. F.; Al-Salama, Y. J.

    2004-01-01

    Fifteen soil samples were chosen from different locations (five different locations at north greater Cairo, Egypt) to represent different soils (alluvial and sandy) as well as different sources of contaminated wastewater (sewage and industrial effluent). Using sequential extraction technique (extracting the soil with different solutions, which is designed to separate metal fractions), Co was separated into six operationally defined fractions: water soluble, exchangeable, carbonate bound, Fe-Mn oxides bound, organic bound and residual fractions. Moreover, total-Co in soils as determined by three analytical methods (sum of sequential extracting, Atomic Absorption Spectrometry (AAS) and neutron activation analysis (NAA) techniques) were compared. Cobalt distribution between different extractants shows that the greatest amounts are found in the residual and Occluded in Fe and Mn-Oxides fractions followed by carbonate or organic fractions. In most cases the proportion of all tested Co-forms has increased in contaminated soil layers with higher enrichment in organically bound Co, occluded in Fe and Mn oxides, carbonate exchangeable and soluble fractions. Results indicate that soil properties have a significant role on Co fractions in soil. In the mean time, soil properties are affected by pollution factors such as source of pollution and load of pollution on the studied soil. Data showed that values of total Co determined by NAA method were always higher than the relevant values determined by AAS or those calculated after the sequential extraction method. (Authors)

  3. Nuclear ``pasta'' structures in low-density nuclear matter and properties of the neutron-star crust

    Science.gov (United States)

    Okamoto, Minoru; Maruyama, Toshiki; Yabana, Kazuhiro; Tatsumi, Toshitaka

    2013-08-01

    In the neutron-star crust, nonuniform structure of nuclear matter—called the “pasta” structure—is expected. From recent studies of giant flares in magnetars, these structures might be related to some observables and physical quantities of the neutron-star crust. To investigate the above quantities, we numerically explore the pasta structure with a fully three-dimensional geometry and study the properties of low-density nuclear matter, based on the relativistic mean-field model and the Thomas-Fermi approximation. We observe typical pasta structures for fixed proton number fraction and two of them for cold catalyzed matter. We also discuss the crystalline configuration of “pasta.”

  4. Specific features of the motion of neutrons in a medium with a helical magnetic structure

    International Nuclear Information System (INIS)

    Fraerman, A. A.; Udalov, O. G.

    2007-01-01

    The specific features of the motion of neutrons in a noncoplanar magnetic field are considered by an example of the magnetization distribution in the form of a conical helix. The reflection coefficients of neutrons from holmium crystals are calculated. It is shown that, for a noncoplanar distribution of a magnetic field in a crystal, the reflection coefficient of neutrons with spin flip exhibits an additional feature

  5. Modification of chemical, optical and structural properties of Bayfol CR-6-2 using gamma and neutron irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Shehata, Mohamed M.; Radwan, Samh I.; Hassan, Amin [Atomic Energy Authority, Cairo (Egypt). Nuclear Research Centre; Waly, Sayed A. [Atomic Energy Authority, Cairo (Egypt). Second Research Reactor; Badawy, Zaynab M. [Atomic Energy Authority, Cairo (Egypt). Experimental Nuclear Physics Dept.

    2016-08-01

    The effects of gamma and neutron irradiations on the chemical, optical and structural properties of Bayfol CR-6-2 were investigated. The samples were irradiated by γ-rays from a {sup 60}Co source at various doses ranging between 16 and 900 kGy at room temperature in atmospheric air. For neutrons, an Am-Be neutron facility was used for the sample irradiation in thermal mode which had an activity of 185 GBq. Samples were irradiated with different doses of neutrons ranging from 15.7 to 564.2 mGy. The changes induced were analyzed using UV-Vis and Fourier transform infrared (FTIR) spectrometry. The results demonstrated an occurrence of oxidative degradation, resulting in the formation of carbonyl groups at 1700 cm{sup -1}. Simultaneous thermo-gravimetric investigation (TGA) has been performed on the samples of 0.3 mm thickness. The results obtained indicate that cross-linking predominates at small neutron doses and main chain scission happens at higher doses.

  6. The effect of structured triglycerides on the kinetic stability of total nutrient admixtures.

    Science.gov (United States)

    Balogh, Judit; Bubenik, Júlia; Dredán, Judit; Csempesz, Ferenc; Kiss, Dorottya; Zelkó, Romána

    2005-10-05

    The physical stability of two types of total parenteral nutrient (TPN) admixtures was studied as a function of storage time and temperature. One of them contained only structured triglycerides and the other exclusively long-chain triglycerides as lipid components. Droplet size of the mixtures was followed by photon correlation spectroscopy for 10 days. Zeta potential and dynamic surface tension measurements were carried out to evaluate the possible changes in the charge and interfacial surface tension of the emulsion droplets during the storage. pH values were monitored in order to follow the possible decomposition processes in the course of storage. Droplet size of emulsions prepared with lipids containing exclusively long-chain triglycerides showed remarkable increase after 4 days of storage in contrast with that of the mixtures containing structured lipids. The obtained results indicate that besides the advantageous metabolic effects of structured triglycerides, their application is recommended to improve the physical stability of TPN admixtures.

  7. Structures of the fractional spaces generated by the difference neutron transport operator

    International Nuclear Information System (INIS)

    Ashyralyev, Allaberen; Taskin, Abdulgafur

    2015-01-01

    The initial boundary value problem for the neutron transport equation is considered. The first, second and third order of accuracy difference schemes for the approximate solution of this problem are presented. Highly accurate difference schemes for neutron transport equation based on Padé approximation are constructed. In applications, stability estimates for solutions of difference schemes for the approximate solution of the neutron transport equation are obtained.The positivity of the neutron transport operator in Slobodeckij spaces is proved. Numerical techniques are developed and algorithms are tested on an example in MATLAB

  8. Basic research for developing the quantitative neutron radiography

    International Nuclear Information System (INIS)

    Tamaki, Masayoshi; Ikeda, Yasushi; Ohkubo, Kohei; Tasaka, Kanji; Yoneda, Kenji; Fujine, Shigenori.

    1992-01-01

    This investigation concerns the basic research and development on quantitative neutron radiography by using a honeycomb collimator which reduces the effect due to scattered neutrons in objective matter. On the observation of the hydrogenate materials such as metal hydrides, water and hydrocarbons by neutron radiography, scattered neutrons from these objectives make the quantitativeness of the neutron radiographic image lower grade. In order to improve the quantitativeness of the image, a honeycomb collimator, which is a honeycomb structure of neutron absorbing material, was introduced to the conventional neutron radiography system. By setting the neutron-absorbing honeycomb collimator between objective and imaging system, neutrons scattered in the objective were absorbed by the honeycomb material and attenuated before coming to the imaging system, but neutrons which were transmitted the objective sample without any interaction reached the imaging system and formed the image of the sample. As the image by purely transmitted neutrons is intrinsic due to the neutronic character of the sample, the image data give the quantitative information. In the present experiment, aluminum honeycomb which was coated with boron nitride was prepared and used in order to image the standard stepwise samples for the evaluation of the quantitative grade of the newly proposed neutron radiography method. From the comparison between macroscopic total cross section and the attenuation coefficient of the thermal neutron for aluminum, copper and hydrocarbons, it was confirmed that they were fairly consistent each other. It can be concluded that the newly proposed neutron radiography method using the neutron-absorbing honeycomb collimator for the elimination of the scattered neutrons improves remarkably the quantitativeness of the neutron radiography technique. (author)

  9. What can we learn about the lipid vesicle structure from the small angle neutron scattering experiment?

    International Nuclear Information System (INIS)

    Kiselev, M.A.; Zemlyanaya, E.V.; Aswal, V.K.; Neubert, R.H.H.

    2005-01-01

    Small angle neutron scattering (SANS) on the unilamellar vesicle populations (diameter of 500 and 1000 Armstrong) was used to characterize lipid vesicles from dimyristoylphosphatidylcholine (DMPC) in three phases (gel, ripple, and liquid). Parameters of vesicle populations and internal structure of the DMPC bilayer were characterized on the basis of the Separated Form Factor (SFF) model. Vesicle shape changes from about spherical in liquid phase to elliptical in ripple and gel phases for vesicles prepared via extrusion through pores with the diameter of 500 Armstrong. Parameters of the internal bilayer structure (membrane thickness, thickness of the hydrophobic core, hydration, and surface area of lipid molecule) were determined on the basis of the Hydrophobic-Hydrophilic (HH) approximation of neutron scattering length density across the bilayer ρ(x) and on the basis of the Step Function (SF) approximation of ρ(x). It was demonstrated in the framework of HH approximation that DMPC membrane thickness in the liquid phase (T = 30 deg C) depends on the membrane curvature. Vesicle population prepared via extrusion through pores with the diameter of 500 Armstrong is characterized by an average radius of 275.6 ± 0.5 Armstrong, polydispersity of 27%, membrane thickness of 47.8 ± 0.2 Armstrong, thickness of hydrophobic core of 20.5 ± 0.3 Armstrong, surface area per DMPC molecule of 61.0 ± 0.4 A 2 Armstrong, and the number of water molecules per DMPC molecule of 11.9 ± 0.3. Vesicles prepared via extrusion through pores with the diameter of 1000 Armstrong have a polydispersity of 48%, and a membrane thickness of 45.6 ± 0.2 Armstrong. SF approximation was used to describe the DMPC membrane structure in gel (T 10 deg C) and ripple (T = 20 deg C) phases. DMPC vesicles prepared via extrusion through 1000- Armstrong pores have a membrane thickness of 49.6 ± 0.5 Armstrong in the gel phase and 48.3 ± 0.6 Armstrong in the ripple phase. The dependence of the DMPC membrane

  10. Interaction of polarized neutrons with polarized La nuclei and the structure of the cross section at energies up to 20 eV

    International Nuclear Information System (INIS)

    Alfimenkov, V.P.; Mareev, Yu.D.; Novitskii, V.V.; Pikel'ner, L.B.; Skoi, V.R.

    1994-01-01

    Properties of lanthanum are investigated in an experiment on the interaction of polarized neutrons with polarized La nuclei. The total cross section for lanthanum is measured for neutron energies ranging from 0.4 to 10 eV. It is shown that one strong level below the neutron binding energy is sufficient for obtaining a good description of the lanthanum cross section in this energy range. The results on the cross section for the interaction of polarized projectiles on a polarized target confirm this conclusion. The spin of the 138 La neutron resonance at 3.0 eV is found to be J = 11 / 2 . 13 refs., 3 figs

  11. Studying magnetic structure of Bi doped Co2MnO4 cubic spinel by neutron diffraction

    International Nuclear Information System (INIS)

    Rajeevan, N.E.; Kaushik, S.D.; Kumar, Ravi

    2016-01-01

    In present work, we studied effect of Bi doped spinel Bi x Co 2-x MnO 4 (x = 0, 0.05, 0.10, 0.15 and 0.20) samples on their crystal as well as magnetic structure by employing neutron diffraction of wavelength 1.48 A using focusing crystal diffractometer of UGC-DAECSR Mumbai Centre at Dhruva, Trombay, Mumbai, India. The analysis of the neutron diffraction using Fullprof program reveals that crystal structure due to Bi doping remains intact and all the samples have been formed in the cubic spinel structure with Fd3m (space group no. 227). The lattice parameter shows the positive thermal expansion upon Bi doping across the temperature range. In order to understand the implication on the spin structure and magnetism in the detail, temperature dependent neutron diffraction study is carried out on some of the samples (x = 0, 0.1) in the series. The ND pattern of x = 0.1 at 2.9K is shown. The experimental finding in terms of modified magnetic structure upon Bi doping are discussed which are understood in terms of variation in the ferroelectric properties, bond lengths and their effect on the CoO 6 polyhedra. Furthermore, Bi substitution in Co 2 MnO 4 spinel brings in the balance of structural distortion, which affects both ferrimagnetism and ferroelectricity

  12. Measurement of the #betta#sub(μ) and anti #betta#sub(μ)-nucleon charged current total cross sections, and the ratio of #betta#sub(μ) neutron to #betta#sub(μ) proton charged current total cross-section

    International Nuclear Information System (INIS)

    Allasia, D.; Bisi, V.; Gamba, D.; Marzari-Chiesa, A.; Ramello, L.; Riccati, L.; Romero, A.; Bobisut, F.; Calimani, E.; Ciampolillo, S.; Huzita, H.; Loreti, M.; Sconza, A.; Bolognese, T.; Faccini-Turluer, M.L.; Louedec, C.; Mosca, L.; Vignaud, D.; Bonarelli, R.; Capiluppi, P.; Derkaoui, J.; Giacomelli, G.; Mandrioli, G.; Rossi, A.M.; Serra-Lugaresi, P.; Frodesen, A.G.; Halsteinslid, A.; Hornaes, A.

    1983-04-01

    This report contains an investigation performed by the Amsterdam-Bergen-Bologna-Padova-Pisa-Saclay-Torino collaboration. The total #betta#sub(μ)- and anti #betta#sub(μ)-nucleon charged current cross sections have been measured in BEBC filled with deuterium and exposed to the wide band neutrino and antineutrino beams at the CERN-SPS. Assuming a linear energy dependence for the cross sections, sigma = a Esub((anti #betta#)), the authors obtained the coefficients asub(#betta#N) = 0.60 +- 0.04 and asub(anti #betta#N) = 0.30 +- 0.02 (in units of 10 - 38 cm 2 /GeV), where the quoted error is mainly systematic. The ratio of the cross sections is sigmasub(anti #betta#N)/sigmasub(#betta#N) = 0.50 +- 0.03. They also determined the ratio of the charged current cross section for neutrino interactions on neutrons and protons R = sigmasub(#betta#n)/sigmasub(#betta#p) = 2.10 +- 0.08 (stat.) +- 0.22 (syst.). The dependence of R on the variables x, y and Esub(#betta#) is discussed. (Auth.)

  13. The Spin Structure of the Neutron Determined Using a Polarized He-3 Target

    Energy Technology Data Exchange (ETDEWEB)

    Middleton, H

    2004-01-06

    Described is a study of the internal spin structure of the neutron performed by measuring the asymmetry in spin-dependent deep inelastic scattering of polarized electrons from nuclear polarized {sup 3}He. Stanford Linear Accelerator experiment E142's sample of 400 million scattering events collected at beam energies between 19 and 26 GeV led to the most precise measurement of a nucleon spin structure function to date. The {sup 3}He target represents a major advance in polarized target technology, using the technique of spin exchange with optically pumped rubidium vapor to produce a typical {sup 3}He nuclear polarization of 34% in a 30cm long target cell with a gas density of 2.3 x 10{sup 20} cm{sup -3}. The target polarization was measured to {+-}7% using an Adiabatic Fast Passage NMR system calibrated with the thermal equilibrium polarization of the protons in a sample of water. The relatively high polarization and target thickness were the result of the development of large volume glass target cells which had inherent nuclear spin relaxation times for the {sup 3}He gas of as long as 70 hours. A target cell production procedure is presented which focuses on special glass blowing techniques to minimize surface interactions with the {sup 3}He nuclei and careful gas purification and vacuum system procedures to reduce relaxation inducing impurities.

  14. Residual stress measurements in thick structural weldments by means of neutron diffraction

    International Nuclear Information System (INIS)

    Ohms, C.; Youtsos, A.G.; Idsert, P. v.d.; Timke, T.

    2000-01-01

    Welding residual stresses in large structural components are a major concern with respect to their performance and lifetime. In large structures reasonable thermal stress relief treatment is usually impossible due to the component size. On the other hand, prediction of welding stresses by numerical modelling has not yet proven to be generally reliable, while the experimental determination of such stresses remains a demanding task. At the high flux reactor (HFR), Petten, a new residual stress diffractometer has been installed recently capable of handling of components up to 1000 kg - the large component neutron diffraction facility (LCNDF). It has facilitated residual stress measurements in two large welded components, of which results are presented here. The first component represents a bi-metallic weld in form of a pipe of 25 mm wall thickness. Three dimensional measurements of residual stress are discussed in detail. The second specimen is a 66 mm wall thickness austenitic steel nuclear piping weld. Results on relief of strain within the weld through post weld heat treatment (PWHT) are presented. Additionally results obtained earlier at former CRNL (CAN) on a section of a thick nuclear piping weld are presented in order to illustrate the variation in the reference lattice parameter trough the weld and the heat affected zone (HAZ). These results clearly show the necessity to determine the reference parameters for each location in all measurement directions by means of measurements in small coupons free of macro-stresses. (orig.)

  15. Nuclear structure studies in highly neutron-deficient (114,116)Xe

    Science.gov (United States)

    Degraaf, James Hendrick

    Lifetimes of nuclear states in 114Xe and 116Xe were measured for the first time; these nuclei represent the most neutron-deficient isotopes of xenon for which lifetimes have now been measured. The fusion-evaporation reactions 58Ni(60Ni, 2p)116Xe at 223 MeV beam energy and 58Ni(58Ni, 2p)114Xe at 215 MeV beam energy were used. Lifetimes were measured using the Recoil Distance Method (RDM) with the 8π gamma-ray spectrometer at Chalk River Laboratories. The new measurements of the B(E2;2+/to 0+) strength in these nuclei, coupled with the recent measurements for heavier xenon isotopes, are well described within the framework of the O(6) symmetry limit of the Interacting Boson Approximation. The octupole nature of the negative parity side-band was also studied, and the lifetime measurements indicate a change from a K/approx 3 structure in heavier xenon isotopes to a K/approx 0,/ 1 structure in 114Xe.

  16. Crystal structure and ion-diffusion pathway of inorganic materials through neutron diffraction

    International Nuclear Information System (INIS)

    Yashima, Masatomo

    2012-01-01

    The present brief review describes the application of neutron powder diffractometry and maximum-entropy method to the studies of crystal structure and diffusional pathways of mobile ions in ionic conducting ceramic materials. La 0.62 Li 0.16 TiO 3 and L i0.6 FePO 4 exhibit two- and one-dimensional networks of Li cation diffusional pathways, respectively. In the fluorite-structure ionic conductors such as celia solid solution Ce 0.93 Y 0.07 O 1.96 , bismuth oxide solid solution δ-Bi 1.4 Yb 0.6 O 3 and copper iodide CuI, a similar curved diffusion pathway along the directions is observed. In the cubic ABO 3 perovskite-type ionic conductor, lanthanum gallate solid solution, the mobile ions diffuse along a curved line keeping the interatomic distance between the B cation and O 2- anion. We have experimentally confirmed that the anisotropic thermal motions of the apex O2 atom and the interstitial O3 atoms are essential for the high oxygen permeability of the K 2 NiF 4 -type mixed conductor. Diffusion paths of proton are visualized along c axis in hexagonal hydroxyapatite. (author)

  17. Structure of halophilic malate dehydrogenase in multimolar KCl solutions from neutron scattering and ultracentrifugation

    International Nuclear Information System (INIS)

    Calmettes, P.

    1987-01-01

    The structure and solvent interactions of malate dehydrogenase from Halobacterium marismortui in multimolar KCl solvents are found to be similar to those in multimolar NaCl solvents reported previously (G. Zaccai, E. Wachtel and H. Eisenberg, J. Mol. Biol. 190 (1986) 97). KCl rather than NaCl is predominant in physiological medium. At salt concentrations up to about 3.0 M, the protein (a dimer of M 87000 g/mol) can be considered to occupy an invariant volume in which it is associated with about 4100 molecules of water and about 520 molecules of salt. At very low resolution, the enzyme particle appears to have a compact protein core and protruding protein parts in interaction with the water and salt components, structural features that are not observed in non-halophilic mitochondrial malate dehydrogenase. The above conclusions were drawn from the analysis of neutron scattering and ultracentrifugation data, and the complementarity of these approaches is discussed extensively. 24 refs.; 7 figs.; 4 tabs

  18. New experimental investigation of cluster structures in 10 Be and 16 C neutron-rich nuclei

    Science.gov (United States)

    Dell'Aquila, L.; Acosta, D.; Auditore, L.; Cardella, G.; De Filippo, E.; De Luca, S.; Francalanza, L.; Gnoffo, B.; Lanzalone, G.; Lombardo, I.; Martorana, N. S.; Norella, S.; Pagano, A.; Pagano, E. V.; Papa, M.; Pirrone, S.; Politi, G.; Quattrocchi, L.; Rizzo, F.; Russotto, P.; Trifirò, A.; Trimarchi, M.; Verde, G.; Vigilante, M.

    2017-11-01

    The existence of cluster structures in ^{10} Be and ^{16} C neutron-rich isotopes is investigated via projectile break-up reactions induced on polyethylene (CH _2 target. We used a fragmentation beam constituted by 55MeV/u ^{10} Be and 49MeV/u ^{16} C beams provided by the FRIBs facility at INFN-LNS. Invariant mass spectra of 4{He}+ 6 He and 6{He} + ^{10} Be breakup fragments are reconstructed by means of the CHIMERA 4π detector to investigate the presence of excited states of projectile nuclei characterized by cluster structure. In the first case, we suggest the presence of a new state in ^{10} Be at 13.5MeV. A non-vanishing yield corresponding to 20.6MeV excitation energy of ^{16} C was observed in the 6{He} + ^{10} Be cluster decay channel. To improve the results of the present analysis, a new experiment has been performed recently, taking advantage of the coupling of CHIMERA and FARCOS. In the paper we describe the data reduction process of the new experiment together with preliminary results.

  19. Studies on microphase-separated structures of block copolymers by neutron reflectivity measurement

    International Nuclear Information System (INIS)

    Torikai, Naoya; Noda, Ichiro; Matsushita, Yushu; Karim, A.; Satija, S.K.; Han, C.C.; Ebisawa, Toru.

    1996-01-01

    Segmental distributions of block copolymer chains in lamellar microphase-separated structure and those of homopolymers in block copolymer/homopolymer blends also with lamellar structures were studied by neutron reflectivity measurements. It was revealed that polystyrene and poly(2-vinylpyridine) lamellae were alternately stacked within the thin films of pure block copolymers spin-coated on silicon wafers, and they were preferentially oriented along the direction parallel to film surface. Polystyrene lamella appeared at air surfaces of the films, while poly(2-vinylpyridine) lamella did on silicon surfaces. Segment distribution at lamellar interface was well described by an error function, and the width of the lamellar interface, defined by a full-width half-maximum value of interfacial profile, was estimated to be about 4.5 nm. Segments of block chains adjacent to the chemical junction points connecting different block chains were strongly localized near the lamellar interfaces, while those on the free ends of block chains were distributed all over the lamellar microdomains with their distribution maxima at the centers of lamellae. On the other hand, it was clarified that homopolymers dissolved in the corresponding lamellar microdomains of block copolymers were also distributed throughout the microdomains with their concentration maxima at the centers of the lamellae. (author)

  20. Structure and Dynamics on Superionic Conducting Phosphate Glasses By Neutron Scattering

    International Nuclear Information System (INIS)

    Kartini, E.; Kennedy, S.J.; Itoh, K.; Arai, M.; Mezei, F.; Nakamura, M.

    2005-01-01

    Full text: A series of Neutron Diffraction and Inelastic scattering experiments have been performed on superionic conducting phosphate glasses, MX-MPO 3 (M=Ag; X=I,S) and AgI-Ag 2 S-AgPO 3 . These materials are used for solid state battery, due to high conductivity up to 10 -2 S.cm -1 at ambient temperature. The conductivity of the insulator glass AgPO 3 ∼ 10 -7 S.cm -1 . Interestingly, the structure factor S(Q) exhibits a prepeak at very low Q∼0.7 Aangstroem -1 related to the IRO ∼ 10-12 Aangstroem and the Radial Distribution Function gives an extra peak ∼ 2.8 Aangstroem -1 that corresponds to Ag-I correlation. The dynamic structure factor S(Q,ω), shows a Boson peak at low energy ∼ 2.5 meV that increases with composition and temperature. These behaviors seem to be universal for the AgI doped glasses, but the origin remains not well understood. Increasing mobility of the Ag ions, due to expansion of the phosphate network plays a dominant role on raising the ionic conductivity, prepeak and Boson peak. (authors)