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Sample records for thermally assisted magnetic

  1. Zero field reversal probability in thermally assisted magnetization reversal

    Science.gov (United States)

    Prasetya, E. B.; Utari; Purnama, B.

    2017-11-01

    This paper discussed about zero field reversal probability in thermally assisted magnetization reversal (TAMR). Appearance of reversal probability in zero field investigated through micromagnetic simulation by solving stochastic Landau-Lifshitz-Gibert (LLG). The perpendicularly anisotropy magnetic dot of 50×50×20 nm3 is considered as single cell magnetic storage of magnetic random acces memory (MRAM). Thermally assisted magnetization reversal was performed by cooling writing process from near/almost Curie point to room temperature on 20 times runs for different randomly magnetized state. The results show that the probability reversal under zero magnetic field decreased with the increase of the energy barrier. The zero-field probability switching of 55% attained for energy barrier of 60 k B T and the reversal probability become zero noted at energy barrier of 2348 k B T. The higest zero-field switching probability of 55% attained for energy barrier of 60 k B T which corespond to magnetif field of 150 Oe for switching.

  2. Characteristics of thermally assisted magnetic recording in granular perpendicular media

    International Nuclear Information System (INIS)

    Shiino, Hirotaka; Kawana, Mayumi; Miyashita, Eiichi; Hayashi, Naoto; Watanabe, Sadayuki

    2009-01-01

    The effect of thermally assisted magnetic recording using granular perpendicular media with a single-pole-trimmed head has been investigated. A read/write experiment using a spin stand in which the media were heated by laser irradiation demonstrated that the track average amplitude strongly depends on both the position of the write head relative to the center of the laser spot in the down-track direction and on the laser power. Although the signal-to-noise ratio increased with the coercivity of the media, the increment was small; this is thought to be caused by an increase in the switching field distribution of the media with temperature. Our results suggest that the magnetic constant of the media must be optimized with respect to the temperature of writing in order for high-density thermally assisted magnetic recording to be realized

  3. Thermal effects on transducer material for heat assisted magnetic recording application

    Energy Technology Data Exchange (ETDEWEB)

    Ji, Rong, E-mail: Ji-Rong@dsi.a-star.edu.sg; Xu, Baoxi; Cen, Zhanhong; Ying, Ji Feng; Toh, Yeow Teck [Data Storage Institute, Agency for Science, Technology and Research (A-STAR), 5 Engineering Drive 1, Singapore 117608 (Singapore)

    2015-05-07

    Heat Assisted Magnetic Recording (HAMR) is a promising technology for next generation hard disk drives with significantly increased data recording capacities. In HAMR, an optical near-field transducer (NFT) is used to concentrate laser energy on a magnetic recording medium to fulfill the heat assist function. The key components of a NFT are transducer material, cladding material, and adhesion material between the cladding and the transducer materials. Since transducer materials and cladding materials have been widely reported, this paper focuses on the adhesion materials between the Au transducer and the Al{sub 2}O{sub 3} cladding material. A comparative study for two kinds of adhesion material, Ta and Cr, has been conducted. We found that Ta provides better thermal stability to the whole transducer than Cr. This is because after thermal annealing, chromium forms oxide material at interfaces and chromium atoms diffuse remarkably into the Au layer and react with Au to form Au alloy. This study also provides insights on the selection of adhesion material for HAMR transducer.

  4. Analysis of self-heating of thermally assisted spin-transfer torque magnetic random access memory

    Directory of Open Access Journals (Sweden)

    Austin Deschenes

    2016-11-01

    Full Text Available Thermal assistance has been shown to significantly reduce the required operation power for spin torque transfer magnetic random access memory (STT-MRAM. Proposed heating methods include modified material stack compositions that result in increased self-heating or external heat sources. In this work we analyze the self-heating process of a standard perpendicular magnetic anisotropy STT-MRAM device through numerical simulations in order to understand the relative contributions of Joule, thermoelectric Peltier and Thomson, and tunneling junction heating. A 2D rotationally symmetric numerical model is used to solve the coupled electro-thermal equations including thermoelectric effects and heat absorbed or released at the tunneling junction. We compare self-heating for different common passivation materials, positive and negative electrical current polarity, and different device thermal anchoring and boundaries resistance configurations. The variations considered are found to result in significant differences in maximum temperatures reached. Average increases of 3 K, 10 K, and 100 K for different passivation materials, positive and negative polarity, and different thermal anchoring configurations, respectively, are observed. The highest temperatures, up to 424 K, are obtained for silicon dioxide as the passivation material, positive polarity, and low thermal anchoring with thermal boundary resistance configurations. Interestingly it is also found that due to the tunneling heat, Peltier effect, device geometry, and numerous interfacial layers around the magnetic tunnel junction (MTJ, most of the heat is dissipated on the lower potential side of the magnetic junction. This asymmetry in heating, which has also been observed experimentally, is important as thermally assisted switching requires heating of the free layer specifically and this will be significantly different for the two polarity operations, set and reset.

  5. Monte Carlo simulation for thermal assisted reversal process of micro-magnetic torus ring with bistable closure domain structure

    Energy Technology Data Exchange (ETDEWEB)

    Terashima, Kenichi; Suzuki, Kenji; Yamaguchi, Katsuhiko, E-mail: yama@sss.fukushima-u.ac.jp

    2016-04-01

    Monte Carlo simulations were performed for temperature dependences of closure domain parameter for a magnetic micro-torus ring cluster under magnetic field on limited temperature regions. Simulation results show that magnetic field on tiny limited temperature region can reverse magnetic closure domain structures when the magnetic field is applied at a threshold temperature corresponding to intensity of applied magnetic field. This is one of thermally assisted switching phenomena through a self-organization process. The results show the way to find non-wasteful pairs between intensity of magnetic field and temperature region for reversing closure domain structure by temperature dependence of the fluctuation of closure domain parameter. Monte Carlo method for this simulation is very valuable to optimize the design of thermally assisted switching devices.

  6. Magnetization process of heat assisted magnetic recording by micro-magnetic simulation

    International Nuclear Information System (INIS)

    Shiiki, Kazuo; Motojima, Hisanori

    2010-01-01

    Magnetization reversal in a uniform magnetic field and one bit recording process by a thin film head in the heat assisted magnetic recording system of TbFeCo medium are studied by using the micro-magnetic simulation and the heat equation. The Landau-Lifsitz-Gilbert equation is solved for magnetic parameters at temperatures as the time goes by. It is found that magnetization proceeds as a progressive wave, although this behaviour may not limit the recording speed. The recording bit is expanded by the thermal fluctuation. The expansion can be suppressed as the medium thickness increases, because the thermal fluctuation is small in the thick medium. So the control of the medium thickness is important very much to achieve a high-density heat-assisted recording.

  7. Structural stability of hydrogenated amorphous carbon overcoats used in heat-assisted magnetic recording investigated by rapid thermal annealing

    KAUST Repository

    Wang, N.; Komvopoulos, K.; Rose, F.; Marchon, B.

    2013-01-01

    Ultrathin amorphous carbon (a-C) films are extensively used as protective overcoats of magnetic recording media. Increasing demands for even higher storage densities have necessitated the development of new storage technologies, such as heat-assisted magnetic recording (HAMR), which uses laser-assisted heating to record data on high-stability media that can store single bits in extremely small areas (∼1 Tbit/in.2). Because HAMR relies on locally changing the coercivity of the magnetic medium by raising the temperature above the Curie temperature for data to be stored by the magnetic write field, it raises a concern about the structural stability of the ultrathin a-C film. In this study, rapid thermal annealing (RTA) experiments were performed to examine the thermal stability of ultrathin hydrogenated amorphous carbon (a-C:H) films deposited by plasma-enhanced chemical vapor deposition. Structural changes in the a-C:H films caused by RTA were investigated by x-ray photoelectron spectroscopy, Raman spectroscopy, x-ray reflectivity, and conductive atomic force microscopy. The results show that the films exhibit thermal stability up to a maximum temperature in the range of 400-450 °C. Heating above this critical temperature leads to hydrogen depletion and sp 2 clustering. The critical temperature determined by the results of this study represents an upper bound of the temperature rise due to laser heating in HAMR hard-disk drives and the Curie temperature of magnetic materials used in HAMR hard disks. © 2013 American Institute of Physics.

  8. Influence of cooling rate in planar thermally assisted magnetic random access memory: Improved writeability due to spin-transfer-torque influence

    International Nuclear Information System (INIS)

    Chavent, A.; Ducruet, C.; Portemont, C.; Creuzet, C.; Alvarez-Hérault, J.; Vila, L.; Sousa, R. C.; Prejbeanu, I. L.; Dieny, B.

    2015-01-01

    This paper investigates the effect of a controlled cooling rate on magnetic field reversal assisted by spin transfer torque (STT) in thermally assisted magnetic random access memory. By using a gradual linear decrease of the voltage at the end of the write pulse, the STT decays more slowly or at least at the same rate as the temperature. This condition is necessary to make sure that the storage layer magnetization remains in the desired written direction during cooling of the cell. The influence of the write current pulse decay rate was investigated on two exchange biased synthetic ferrimagnet (SyF) electrodes. For a NiFe based electrode, a significant improvement in writing reproducibility was observed using a gradual linear voltage transition. The write error rate decreases by a factor of 10 when increasing the write pulse fall-time from ∼3 ns to 70 ns. For comparison, a second CoFe/NiFe based electrode was also reversed by magnetic field assisted by STT. In this case, no difference between sharp and linear write pulse fall shape was observed. We attribute this observation to the higher thermal stability of the CoFe/NiFe electrode during cooling. In real-time measurements of the magnetization reversal, it was found that Ruderman-Kittel-Kasuya-Yosida (RKKY) coupling in the SyF electrode vanishes for the highest pulse voltages that were used due to the high temperature reached during write. As a result, during the cooling phase, the final state is reached through a spin-flop transition of the SyF storage layer

  9. Stochastic simulation of thermally assisted magnetization reversal in sub-100 nm dots with perpendicular anisotropy

    International Nuclear Information System (INIS)

    Purnama, Budi; Koga, Masashi; Nozaki, Yukio; Matsuyama, Kimihide

    2009-01-01

    Thermally assisted magnetization reversal of sub-100 nm dots with perpendicular anisotropy has been investigated using a micromagnetic Langevin model. The performance of the two different reversal modes of (i) a reduced barrier writing scheme and (ii) a Curie point writing scheme are compared. For the reduced barrier writing scheme, the switching field H swt decreases with an increase in writing temperature but is still larger than that of the Curie point writing scheme. For the Curie point writing scheme, the required threshold field H th , evaluated from 50 simulation results, saturates at a value, which is not simply related to the energy barrier height. The value of H th increases with a decrease in cooling time owing to the dynamic aspects of the magnetic ordering process. Dependence of H th on material parameters and dot sizes has been systematically studied

  10. Assisted Writing in Spin Transfer Torque Magnetic Tunnel Junctions

    Science.gov (United States)

    Ganguly, Samiran; Ahmed, Zeeshan; Datta, Supriyo; Marinero, Ernesto E.

    2015-03-01

    Spin transfer torque driven MRAM devices are now in an advanced state of development, and the importance of reducing the current requirement for writing information is well recognized. Different approaches to assist the writing process have been proposed such as spin orbit torque, spin Hall effect, voltage controlled magnetic anisotropy and thermal excitation. In this work,we report on our comparative study using the Spin-Circuit Approach regarding the total energy, the switching speed and energy-delay products for different assisted writing approaches in STT-MTJ devices using PMA magnets.

  11. Thermal modeling of head disk interface system in heat assisted magnetic recording

    Energy Technology Data Exchange (ETDEWEB)

    Vemuri, Sesha Hari; Seung Chung, Pil; Jhon, Myung S., E-mail: mj3a@andrew.cmu.edu [Department of Chemical Engineering and Data Storage Systems Center, Carnegie Mellon University, 5000 Forbes Ave., Pittsburgh, Pennsylvania 15213 (United States); Min Kim, Hyung [Department of Mechanical System Engineering, Kyonggi University, Suwon, Gyeonggi-do 440-746 (Korea, Republic of)

    2014-05-07

    A thorough understanding of the temperature profiles introduced by the heat assisted magnetic recording is required to maintain the hotspot at the desired location on the disk with minimal heat damage to other components. Here, we implement a transient mesoscale modeling methodology termed lattice Boltzmann method (LBM) for phonons (which are primary carriers of energy) in the thermal modeling of the head disk interface (HDI) components, namely, carbon overcoat (COC). The LBM can provide more accurate results compared to conventional Fourier methodology by capturing the nanoscale phenomena due to ballistic heat transfer. We examine the in-plane and out-of-plane heat transfer in the COC via analyzing the temperature profiles with a continuously focused and pulsed laser beam on a moving disk. Larger in-plane hotspot widening is observed in continuously focused laser beam compared to a pulsed laser. A pulsed laser surface develops steeper temperature gradients compared to continuous hotspot. Furthermore, out-of-plane heat transfer from the COC to the media is enhanced with a continuous laser beam then a pulsed laser, while the temperature takes around 140 fs to reach the bottom surface of the COC. Our study can lead to a realistic thermal model describing novel HDI material design criteria for the next generation of hard disk drives with ultra high recording densities.

  12. Thermally assisted interlayer magnetic coupling through Ba_0_._0_5Sr_0_._9_5TiO_3 barriers

    International Nuclear Information System (INIS)

    Carreira, Santiago J.; Steren, Laura B.; Avilés Félix, Luis; Alejandro, Gabriela; Sirena, Martín

    2016-01-01

    We report on the interlayer exchange coupling across insulating barriers observed on Ni_8_0Fe_2_0/Ba_0_._0_5Sr_0_._9_5TiO_3/La_0_._6_6Sr_0_._3_3MnO_3 (Py/BST_0_._0_5/LSMO) trilayers. The coupling mechanism has been analyzed in terms of the barrier thickness, samples' substrate, and temperature. We examined the effect of MgO (MGO) and SrTiO_3 (STO) (001) single-crystalline substrates on the magnetic coupling and also on the magnetic anisotropies of the samples in order to get a deeper understanding of the magnetism of the structures. We measured a weak coupling mediated by spin-dependent tunneling phenomena whose sign and strength depend on barrier thickness and substrate. An antiferromagnetic (AF) exchange prevails for most of the samples and smoothly increases with the barrier thicknesses as a consequence of the screening effects of the BST_0_._0_5. The coupling monotonically increases with temperature in all the samples and this behavior is attributed to thermally assisted mechanisms. The magnetic anisotropy of both magnetic components has a cubic symmetry that in the case of permalloy is added to a small uniaxial component.

  13. Gelatine-assisted synthesis of magnetite nanoparticles for magnetic hyperthermia

    Energy Technology Data Exchange (ETDEWEB)

    Alves, André F.; Mendo, Sofia G. [Universidade de Lisboa, Centro de Química e Bioquímica, Faculdade de Ciências (Portugal); Ferreira, Liliana P. [Universidade de Lisboa, Biosystems and Integrative Sciences Institute, Faculdade de Ciências (Portugal); Mendonça, Maria Helena [Universidade de Lisboa, Centro de Química e Bioquímica, Faculdade de Ciências (Portugal); Ferreira, Paula [University of Aveiro, Department of Materials and Ceramic Engineering, CICECO - Aveiro Institute of Materials (Portugal); Godinho, Margarida; Cruz, Maria Margarida [Universidade de Lisboa, Biosystems and Integrative Sciences Institute, Faculdade de Ciências (Portugal); Carvalho, Maria Deus, E-mail: mdcarvalho@ciencias.ulisboa.pt [Universidade de Lisboa, Centro de Química e Bioquímica, Faculdade de Ciências (Portugal)

    2016-01-15

    Magnetite nanoparticles were synthesized by the co-precipitation method exploring the use of gelatine and agar as additives. For comparison, magnetite nanoparticles were also prepared by standard co-precipitation, by co-precipitation with the addition of a surfactant (sodium dodecyl sulphate) and by the thermal decomposition method. The structure and morphology of the synthesized nanoparticles were investigated by powder X-ray diffraction and transmission electron microscopy. Their magnetic properties were studied by SQUID magnetometry and {sup 57}Fe Mössbauer spectroscopy. The nanoparticles potential for applications in magnetic hyperthermia was evaluated through heating efficiency under alternating magnetic field. The results show that all synthesis methods produce Fe{sub 3−x}O{sub 4} nanoparticles with similar sizes. The nanoparticles synthesized in the gelatine medium display the narrowest particle size distribution, the lowest oxidation degree, one of the highest saturation magnetization values and the best hyperthermia efficiency, proving that this gelatine-assisted synthesis is an efficient, environmental friendly, and low-cost method to produce magnetite nanoparticles. Graphical Abstract: A new gelatine-assisted method is an efficient and low-cost way to synthesize magnetite nanoparticles with enhanced magnetic hyperthermia.

  14. Lubricant reflow after laser heating in heat assisted magnetic recording

    Science.gov (United States)

    Wu, Haoyu; Mendez, Alejandro Rodriguez; Xiong, Shaomin; Bogy, David B.

    2015-05-01

    In heat assisted magnetic recording (HAMR) technology for hard disk drives, the media will be heated to about 500 °C during the writing process in order to reduce its magnetic coercivity and thus allow data writing with the magnetic head transducers. The traditional lubricants such as Z-dol and Z-tetraol may not be able to perform in such harsh heating conditions due to evaporation, decomposition and thermal depletion. However, some of the lubricant depletion can be recovered due to reflow after a period of time, which can help to reduce the chance of head disk interface failure. In this study, experiments of lubricant thermal depletion and reflow were performed using a HAMR test stage for a Z-tetraol type lubricant. Various lubricant depletion profiles were generated using different laser heating conditions. The lubricant reflow process after thermal depletion was monitored by use of an optical surface analyzer. In addition, a continuum based lubrication model was developed to simulate the lubricant reflow process. Reasonably good agreement between simulations and experiments was achieved.

  15. Thermally assisted interlayer magnetic coupling through Ba{sub 0.05}Sr{sub 0.95}TiO{sub 3} barriers

    Energy Technology Data Exchange (ETDEWEB)

    Carreira, Santiago J.; Steren, Laura B. [Centro Atómico Constituyentes, San Martín, Buenos Aires 1650 (Argentina); Consejo Nacional de Investigaciones Científicas y Técnicas, Ciudad Autonoma de Buenos Aires C1425FQB (Argentina); Avilés Félix, Luis; Alejandro, Gabriela [Consejo Nacional de Investigaciones Científicas y Técnicas, Ciudad Autonoma de Buenos Aires C1425FQB (Argentina); Centro Atómico Bariloche, Bariloche, Rio Negro 8400 (Argentina); Sirena, Martín [Consejo Nacional de Investigaciones Científicas y Técnicas, Ciudad Autonoma de Buenos Aires C1425FQB (Argentina); Centro Atómico Bariloche, Bariloche, Rio Negro 8400 (Argentina); Instituto Balseiro-CNEA & Univ. Nac. de Cuyo, Bariloche, Rio Negro 8400 (Argentina)

    2016-08-08

    We report on the interlayer exchange coupling across insulating barriers observed on Ni{sub 80}Fe{sub 20}/Ba{sub 0.05}Sr{sub 0.95}TiO{sub 3}/La{sub 0.66}Sr{sub 0.33}MnO{sub 3} (Py/BST{sub 0.05}/LSMO) trilayers. The coupling mechanism has been analyzed in terms of the barrier thickness, samples' substrate, and temperature. We examined the effect of MgO (MGO) and SrTiO{sub 3} (STO) (001) single-crystalline substrates on the magnetic coupling and also on the magnetic anisotropies of the samples in order to get a deeper understanding of the magnetism of the structures. We measured a weak coupling mediated by spin-dependent tunneling phenomena whose sign and strength depend on barrier thickness and substrate. An antiferromagnetic (AF) exchange prevails for most of the samples and smoothly increases with the barrier thicknesses as a consequence of the screening effects of the BST{sub 0.05}. The coupling monotonically increases with temperature in all the samples and this behavior is attributed to thermally assisted mechanisms. The magnetic anisotropy of both magnetic components has a cubic symmetry that in the case of permalloy is added to a small uniaxial component.

  16. Magnetic Launch Assist Demonstration Test

    Science.gov (United States)

    2001-01-01

    This image shows a 1/9 subscale model vehicle clearing the Magnetic Launch Assist System, formerly referred to as the Magnetic Levitation (MagLev), test track during a demonstration test conducted at the Marshall Space Flight Center (MSFC). Engineers at MSFC have developed and tested Magnetic Launch Assist technologies. To launch spacecraft into orbit, a Magnetic Launch Assist System would use magnetic fields to levitate and accelerate a vehicle along a track at very high speeds. Similar to high-speed trains and roller coasters that use high-strength magnets to lift and propel a vehicle a couple of inches above a guideway, a launch-assist system would electromagnetically drive a space vehicle along the track. A full-scale, operational track would be about 1.5-miles long and capable of accelerating a vehicle to 600 mph in 9.5 seconds. This track is an advanced linear induction motor. Induction motors are common in fans, power drills, and sewing machines. Instead of spinning in a circular motion to turn a shaft or gears, a linear induction motor produces thrust in a straight line. Mounted on concrete pedestals, the track is 100-feet long, about 2-feet wide and about 1.5-feet high. The major advantages of launch assist for NASA launch vehicles is that it reduces the weight of the take-off, the landing gear, the wing size, and less propellant resulting in significant cost savings. The US Navy and the British MOD (Ministry of Defense) are planning to use magnetic launch assist for their next generation aircraft carriers as the aircraft launch system. The US Army is considering using this technology for launching target drones for anti-aircraft training.

  17. Magnetic Launch Assist Experimental Track

    Science.gov (United States)

    1999-01-01

    In this photograph, a futuristic spacecraft model sits atop a carrier on the Magnetic Launch Assist System, formerly known as the Magnetic Levitation (MagLev) System, experimental track at the Marshall Space Flight Center (MSFC). Engineers at MSFC have developed and tested Magnetic Launch Assist technologies that would use magnetic fields to levitate and accelerate a vehicle along a track at very high speeds. Similar to high-speed trains and roller coasters that use high-strength magnets to lift and propel a vehicle a couple of inches above a guideway, a Magnetic Launch Assist system would electromagnetically drive a space vehicle along the track. A full-scale, operational track would be about 1.5-miles long and capable of accelerating a vehicle to 600 mph in 9.5 seconds. This track is an advanced linear induction motor. Induction motors are common in fans, power drills, and sewing machines. Instead of spinning in a circular motion to turn a shaft or gears, a linear induction motor produces thrust in a straight line. Mounted on concrete pedestals, the track is 100-feet long, about 2-feet wide, and about 1.5-feet high. The major advantages of launch assist for NASA launch vehicles is that it reduces the weight of the take-off, the landing gear, the wing size, and less propellant resulting in significant cost savings. The US Navy and the British MOD (Ministry of Defense) are planning to use magnetic launch assist for their next generation aircraft carriers as the aircraft launch system. The US Army is considering using this technology for launching target drones for anti-aircraft training.

  18. Numerical analysis of thermally actuated magnets for magnetization of superconductors

    Energy Technology Data Exchange (ETDEWEB)

    Li Quan; Yan Yu; Rawlings, Colin; Coombs, Tim, E-mail: ql229@cam.ac.u [EPEC Superconductivity Group, Engineering Department, University of Cambridge, Trumpington Street. Cambridge, CB2 1PZ (United Kingdom)

    2010-06-01

    Superconductors, such as YBCO bulks, have extremely high potential magnetic flux densities, comparing to rare earth magnets. Therefore, the magnetization of superconductors has attracted broad attention and contribution from both academic research and industry. In this paper, a novel technique is proposed to magnetize superconductors. Unusually, instead of using high magnetic fields and pulses, repeatedly magnetic waves with strength of as low as rare earth magnets are applied. These magnetic waves, generated by thermally controlling a Gadolinium (Gd) bulk with a rare earth magnet underneath, travel over the flat surface of a YBCO bulk and get trapped little by little. Thus, a very small magnetic field can be used to build up a very large magnetic field. In this paper, the modelling results of thermally actuated magnetic waves are presented showing how to transfer sequentially applied thermal pulses into magnetic waves. The experiment results of the magnetization of YBCO bulk are also presented to demonstrate how superconductors are progressively magnetized by small magnetic field

  19. Numerical analysis of thermally actuated magnets for magnetization of superconductors

    International Nuclear Information System (INIS)

    Li Quan; Yan Yu; Rawlings, Colin; Coombs, Tim

    2010-01-01

    Superconductors, such as YBCO bulks, have extremely high potential magnetic flux densities, comparing to rare earth magnets. Therefore, the magnetization of superconductors has attracted broad attention and contribution from both academic research and industry. In this paper, a novel technique is proposed to magnetize superconductors. Unusually, instead of using high magnetic fields and pulses, repeatedly magnetic waves with strength of as low as rare earth magnets are applied. These magnetic waves, generated by thermally controlling a Gadolinium (Gd) bulk with a rare earth magnet underneath, travel over the flat surface of a YBCO bulk and get trapped little by little. Thus, a very small magnetic field can be used to build up a very large magnetic field. In this paper, the modelling results of thermally actuated magnetic waves are presented showing how to transfer sequentially applied thermal pulses into magnetic waves. The experiment results of the magnetization of YBCO bulk are also presented to demonstrate how superconductors are progressively magnetized by small magnetic field

  20. Lubricant depletion under various laser heating conditions in Heat Assisted Magnetic Recording (HAMR)

    Science.gov (United States)

    Xiong, Shaomin; Wu, Haoyu; Bogy, David

    2014-09-01

    Heat assisted magnetic recording (HAMR) is expected to increase the storage areal density to more than 1 Tb/in2 in hard disk drives (HDDs). In this technology, a laser is used to heat the magnetic media to the Curie point (~400-600 °C) during the writing process. The lubricant on the top of a magnetic disk could evaporate and be depleted under the laser heating. The change of the lubricant can lead to instability of the flying slider and failure of the head-disk interface (HDI). In this study, a HAMR test stage is developed to study the lubricant thermal behavior. Various heating conditions are controlled for the study of the lubricant thermal depletion. The effects of laser heating repetitions and power levels on the lubricant depletion are investigated experimentally. The lubricant reflow behavior is discussed as well.

  1. Magnetic Launch Assist System Demonstration Test

    Science.gov (United States)

    2001-01-01

    Engineers at the Marshall Space Flight Center (MSFC) have been testing Magnetic Launch Assist Systems, formerly known as Magnetic Levitation (MagLev) technologies. To launch spacecraft into orbit, a Magnetic Launch Assist system would use magnetic fields to levitate and accelerate a vehicle along a track at a very high speed. Similar to high-speed trains and roller coasters that use high-strength magnets to lift and propel a vehicle a couple of inches above a guideway, the launch-assist system would electromagnetically drive a space vehicle along the track. A full-scale, operational track would be about 1.5-miles long and capable of accelerating a vehicle to 600 mph in 9.5 seconds. This photograph shows a subscale model of an airplane running on the experimental track at MSFC during the demonstration test. This track is an advanced linear induction motor. Induction motors are common in fans, power drills, and sewing machines. Instead of spinning in a circular motion to turn a shaft or gears, a linear induction motor produces thrust in a straight line. Mounted on concrete pedestals, the track is 100-feet long, about 2-feet wide, and about 1.5- feet high. The major advantages of launch assist for NASA launch vehicles is that it reduces the weight of the take-off, the landing gear, the wing size, and less propellant resulting in significant cost savings. The US Navy and the British MOD (Ministry of Defense) are planning to use magnetic launch assist for their next generation aircraft carriers as the aircraft launch system. The US Army is considering using this technology for launching target drones for anti-aircraft training.

  2. Thermally activated magnetization reversal in magnetic tunnel junctions

    International Nuclear Information System (INIS)

    Guang-Hong, Zhou; Yin-Gang, Wang; Xian-Jin, Qi; Zi-Quan, Li; Jian-Kang, Chen

    2009-01-01

    In this paper, the magnetization reversal of the ferromagnetic layers in the IrMn/CoFe/AlO x /CoFe magnetic tunnel junction has been investigated using bulk magnetometry. The films exhibit very complex magnetization processes and reversal mechanism. Thermal activation phenomena such as the training effect, the asymmetry of reversal, the loop broadening and the decrease of exchange field while holding the film at negative saturation have been observed on the hysteresis loops of the pinned ferromagnetic layer while not on those of the free ferromagnetic layer. The thermal activation phenomena observed can be explained by the model of two energy barrier distributions with different time constants. (condensed matter: electronic structure, electrical, magnetic, and optical properties)

  3. A two-stage heating scheme for heat assisted magnetic recording

    Science.gov (United States)

    Xiong, Shaomin; Kim, Jeongmin; Wang, Yuan; Zhang, Xiang; Bogy, David

    2014-05-01

    Heat Assisted Magnetic Recording (HAMR) has been proposed to extend the storage areal density beyond 1 Tb/in.2 for the next generation magnetic storage. A near field transducer (NFT) is widely used in HAMR systems to locally heat the magnetic disk during the writing process. However, much of the laser power is absorbed around the NFT, which causes overheating of the NFT and reduces its reliability. In this work, a two-stage heating scheme is proposed to reduce the thermal load by separating the NFT heating process into two individual heating stages from an optical waveguide and a NFT, respectively. As the first stage, the optical waveguide is placed in front of the NFT and delivers part of laser energy directly onto the disk surface to heat it up to a peak temperature somewhat lower than the Curie temperature of the magnetic material. Then, the NFT works as the second heating stage to heat a smaller area inside the waveguide heated area further to reach the Curie point. The energy applied to the NFT in the second heating stage is reduced compared with a typical single stage NFT heating system. With this reduced thermal load to the NFT by the two-stage heating scheme, the lifetime of the NFT can be extended orders longer under the cyclic load condition.

  4. Magnetization reversal in single molecule magnets

    Science.gov (United States)

    Bokacheva, Louisa

    2002-09-01

    I have studied the magnetization reversal in single molecule magnets (SMMs). SMMs are Van der Waals crystals, consisting of identical molecules containing transition metal ions, with high spin and large uniaxial magnetic anisotropy. They can be considered as ensembles of identical, iso-oriented nanomagnets. At high temperature, these materials behave as superparamagnets and their magnetization reversal occurs by thermal activation. At low temperature they become blocked, and their magnetic relaxation occurs via thermally assisted tunneling or pure quantum tunneling through the anisotropy barrier. We have conducted detailed experimental studies of the magnetization reversal in SMM material Mn12-acetate (Mn12) with S = 10. Low temperature measurements were conducted using micro-Hall effect magnetometry. We performed hysteresis and relaxation studies as a function of temperature, transverse field, and magnetization state of the sample. We identified magnetic sublevels that dominate the tunneling at a given field, temperature and magnetization. We observed a crossover between thermally assisted and pure quantum tunneling. The form of this crossover depends on the magnitude and direction of the applied field. This crossover is abrupt (first-order) and occurs in a narrow temperature interval (tunneling mechanisms in Mn12.

  5. Tabletop Experimental Track for Magnetic Launch Assist

    Science.gov (United States)

    2000-01-01

    Marshall Space Flight Center's (MSFC's) Advanced Space Transportation Program has developed the Magnetic Launch Assist System, formerly known as the Magnetic Levitation (MagLev) technology that could give a space vehicle a running start to break free from Earth's gravity. A Magnetic Launch Assist system would use magnetic fields to levitate and accelerate a vehicle along a track at speeds up to 600 mph. The vehicle would shift to rocket engines for launch into orbit. Similar to high-speed trains and roller coasters that use high-strength magnets to lift and propel a vehicle a couple of inches above a guideway, a Magnetic Launch Assist system would electromagnetically propel a space vehicle along the track. The tabletop experimental track for the system shown in this photograph is 44-feet long, with 22-feet of powered acceleration and 22-feet of passive braking. A 10-pound carrier with permanent magnets on its sides swiftly glides by copper coils, producing a levitation force. The track uses a linear synchronous motor, which means the track is synchronized to turn the coils on just before the carrier comes in contact with them, and off once the carrier passes. Sensors are positioned on the side of the track to determine the carrier's position so the appropriate drive coils can be energized. MSFC engineers have conducted tests on the indoor track and a 50-foot outdoor track. The major advantages of launch assist for NASA launch vehicles is that it reduces the weight of the take-off, the landing gear, the wing size, and less propellant resulting in significant cost savings. The US Navy and the British MOD (Ministry of Defense) are planning to use magnetic launch assist for their next generation aircraft carriers as the aircraft launch system. The US Army is considering using this technology for launching target drones for anti-aircraft training.

  6. Strain and thermally induced magnetic dynamics and spin current in magnetic insulators subject to transient optical grating

    Science.gov (United States)

    Wang, Xi-Guang; Chotorlishvili, Levan; Berakdar, Jamal

    2017-07-01

    We analyze the magnetic dynamics and particularlythe spin current in an open-circuit ferromagnetic insulator irradiated by two intense, phase-locked laser pulses. The interference of the laser beams generates a transient optical grating and a transient spatio-temporal temperature distribution. Both effects lead to elastic and heat waves at the surface and into the bulk of the sample. The strain induced spin current as well as the thermally induced magnonic spin current are evaluated numerically on the basis of micromagnetic simulations using solutions of the heat equation. We observe that the thermo-elastically induced magnonic spin current propagates on a distance larger than the characteristic size of thermal profile, an effect useful for applications in remote detection of spin caloritronics phenomena. Our findings point out that exploiting strain adds a new twist to heat-assisted magnetic switching and spin-current generation for spintronic applications.

  7. 34 CFR 280.1 - What is the Magnet Schools Assistance Program?

    Science.gov (United States)

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false What is the Magnet Schools Assistance Program? 280.1... SECONDARY EDUCATION, DEPARTMENT OF EDUCATION MAGNET SCHOOLS ASSISTANCE PROGRAM General § 280.1 What is the Magnet Schools Assistance Program? The Magnet Schools Assistance Program provides grants to eligible...

  8. Robotic-assisted thermal ablation of liver tumours

    International Nuclear Information System (INIS)

    Abdullah, Basri Johan Jeet; Yeong, Chai Hong; Goh, Khean Lee; Yoong, Boon Koon; Ho, Gwo Fuang; Yim, Carolyn Chue Wai; Kulkarni, Anjali

    2015-01-01

    This study aimed to assess the technical success, radiation dose, safety and performance level of liver thermal ablation using a computed tomography (CT)-guided robotic positioning system. Radiofrequency and microwave ablation of liver tumours were performed on 20 patients (40 lesions) with the assistance of a CT-guided robotic positioning system. The accuracy of probe placement, number of readjustments and total radiation dose to each patient were recorded. The performance level was evaluated on a five-point scale (5-1: excellent-poor). The radiation doses were compared against 30 patients with 48 lesions (control) treated without robotic assistance. Thermal ablation was successfully completed in 20 patients with 40 lesions and confirmed on multiphasic contrast-enhanced CT. No procedure related complications were noted in this study. The average number of needle readjustment was 0.8 ± 0.8. The total CT dose (DLP) for the entire robotic assisted thermal ablation was 1382 ± 536 mGy.cm, while the CT fluoroscopic dose (DLP) per lesion was 352 ± 228 mGy.cm. There was no statistically significant (p > 0.05) dose reduction found between the robotic-assisted versus the conventional method. This study revealed that robotic-assisted planning and needle placement appears to be safe, with high accuracy and a comparable radiation dose to patients. (orig.)

  9. Robotic-assisted thermal ablation of liver tumours

    Energy Technology Data Exchange (ETDEWEB)

    Abdullah, Basri Johan Jeet; Yeong, Chai Hong [University of Malaya, Department of Biomedical Imaging and University of Malaya Research Imaging Centre, Faculty of Medicine, Kuala Lumpur (Malaysia); University of Malaya, Department of Internal Medicine, Faculty of Medicine, Kuala Lumpur (Malaysia); Goh, Khean Lee [University of Malaya, Department of Internal Medicine, Faculty of Medicine, Kuala Lumpur (Malaysia); Yoong, Boon Koon [University of Malaya, Department of Surgery, Faculty of Medicine, Kuala Lumpur (Malaysia); Ho, Gwo Fuang [University of Malaya, Department of Oncology, Faculty of Medicine, Kuala Lumpur (Malaysia); Yim, Carolyn Chue Wai [University of Malaya, Department of Anesthesia, Faculty of Medicine, Kuala Lumpur (Malaysia); Kulkarni, Anjali [Perfint Healthcare Corporation, Florence, OR (United States)

    2015-01-15

    This study aimed to assess the technical success, radiation dose, safety and performance level of liver thermal ablation using a computed tomography (CT)-guided robotic positioning system. Radiofrequency and microwave ablation of liver tumours were performed on 20 patients (40 lesions) with the assistance of a CT-guided robotic positioning system. The accuracy of probe placement, number of readjustments and total radiation dose to each patient were recorded. The performance level was evaluated on a five-point scale (5-1: excellent-poor). The radiation doses were compared against 30 patients with 48 lesions (control) treated without robotic assistance. Thermal ablation was successfully completed in 20 patients with 40 lesions and confirmed on multiphasic contrast-enhanced CT. No procedure related complications were noted in this study. The average number of needle readjustment was 0.8 ± 0.8. The total CT dose (DLP) for the entire robotic assisted thermal ablation was 1382 ± 536 mGy.cm, while the CT fluoroscopic dose (DLP) per lesion was 352 ± 228 mGy.cm. There was no statistically significant (p > 0.05) dose reduction found between the robotic-assisted versus the conventional method. This study revealed that robotic-assisted planning and needle placement appears to be safe, with high accuracy and a comparable radiation dose to patients. (orig.)

  10. Scaling analysis and instantons for thermally assisted tunneling and quantum Monte Carlo simulations

    Science.gov (United States)

    Jiang, Zhang; Smelyanskiy, Vadim N.; Isakov, Sergei V.; Boixo, Sergio; Mazzola, Guglielmo; Troyer, Matthias; Neven, Hartmut

    2017-01-01

    We develop an instantonic calculus to derive an analytical expression for the thermally assisted tunneling decay rate of a metastable state in a fully connected quantum spin model. The tunneling decay problem can be mapped onto the Kramers escape problem of a classical random dynamical field. This dynamical field is simulated efficiently by path-integral quantum Monte Carlo (QMC). We show analytically that the exponential scaling with the number of spins of the thermally assisted quantum tunneling rate and the escape rate of the QMC process are identical. We relate this effect to the existence of a dominant instantonic tunneling path. The instanton trajectory is described by nonlinear dynamical mean-field theory equations for a single-site magnetization vector, which we solve exactly. Finally, we derive scaling relations for the "spiky" barrier shape when the spin tunneling and QMC rates scale polynomially with the number of spins N while a purely classical over-the-barrier activation rate scales exponentially with N .

  11. Origin of coronal mass ejection and magnetic cloud: Thermal or magnetic driven?

    Science.gov (United States)

    Zhang, Gong-Liang; Wang, Chi; He, Shuang-Hua

    1995-01-01

    A fundamental problem in Solar-Terrestrial Physics is the origin of the solar transient plasma output, which includes the coronal mass ejection and its interplanetary manifestation, e.g. the magnetic cloud. The traditional blast wave model resulted from solar thermal pressure impulse has faced with challenge during recent years. In the MHD numerical simulation study of CME, the authors find that the basic feature of the asymmetrical event on 18 August 1980 can be reproduced neither by a thermal pressure nor by a speed increment. Also, the thermal pressure model fails in simulating the interplanetary structure with low thermal pressure and strong magnetic field strength, representative of a typical magnetic cloud. Instead, the numerical simulation results are in favor of the magnetic field expansion as the likely mechanism for both the asymmetrical CME event and magnetic cloud.

  12. The magnetic-nanofluid heat pipe with superior thermal properties through magnetic enhancement

    Science.gov (United States)

    2012-01-01

    This study developed a magnetic-nanofluid (MNF) heat pipe (MNFHP) with magnetically enhanced thermal properties. Its main characteristic was additional porous iron nozzle in the evaporator and the condenser to form a unique flowing pattern of MNF slug and vapor, and to magnetically shield the magnet attraction on MNF flowing. The results showed that an optimal thermal conductivity exists in the applied field of 200 Oe. Furthermore, the minor thermal performance of MNF at the condenser limited the thermal conductivity of the entire MNFHP, which was 1.6 times greater than that filled with water for the input power of 60 W. The feasibilities of an MNFHP with the magnetically enhanced heat transfer and the ability of vertical operation were proved for both a promising heat-dissipation device and the energy architecture integrated with an additional energy system. PMID:22716909

  13. Reduction of thermal expansion in Z-pinches by electron beam assisted magnetic field generation

    International Nuclear Information System (INIS)

    Heikkinen, J.A.; Karttunen, S.J.

    1989-01-01

    Weak radial expansion of a Z-pinch plasma column during its strong initial ohmic heating phase is expected when the generation of a confining magnetic field is assisted by a correctly formed electron beam pulse. Appropriate one-dimensional magnetohydrodynamic equations are numerically solved, and the observed increase of plasma radius as a function of time for various discharge parameters is compared to a normal Z-pinch discharge initiation. (author)

  14. 77 FR 67572 - Magnet Schools Assistance Program

    Science.gov (United States)

    2012-11-13

    ... DEPARTMENT OF EDUCATION 34 CFR Part 280 [Docket ID ED-2010-OII-0003] RIN 1855-AA07 Magnet Schools... amended the regulations governing the Magnet Schools Assistance Program (MSAP) to provide greater... creation of magnet schools that result in minority group enrollments in magnet and feeder schools exceeding...

  15. High-Temperature Adhesives for Thermally Stable Aero-Assist Technologies

    Science.gov (United States)

    Eberts, Kenneth; Ou, Runqing

    2013-01-01

    Aero-assist technologies are used to control the velocity of exploration vehicles (EVs) when entering Earth or other planetary atmospheres. Since entry of EVs in planetary atmospheres results in significant heating, thermally stable aero-assist technologies are required to avoid the high heating rates while maintaining low mass. Polymer adhesives are used in aero-assist structures because of the need for high flexibility and good bonding between layers of polymer films or fabrics. However, current polymer adhesives cannot withstand temperatures above 400 C. This innovation utilizes nanotechnology capabilities to address this need, leading to the development of high-temperature adhesives that exhibit high thermal conductivity in addition to increased thermal decomposition temperature. Enhanced thermal conductivity will help to dissipate heat quickly and effectively to avoid temperature rising to harmful levels. This, together with increased thermal decomposition temperature, will enable the adhesives to sustain transient high-temperature conditions.

  16. Reversal mechanisms and interactions in magnetic systems: coercivity versus switching field and thermally assisted demagnetization

    Directory of Open Access Journals (Sweden)

    Cebollada, F.

    2005-06-01

    Full Text Available In this paper we present a comparative analysis of the magnetic interactions and reversal mechanisms of two different systems: NdFeB-type alloys with grain sizes in the single domain range and Fe-SiO2 nanocomposites with Fe concentrations above and below the percolation threshold. We evidence that the use of the coercivity as the main parameter to analyse them might be misleading due to the convolution of both reversible and irreversible magnetization variations. We show that the switching field and thermally assisted demagnetization allow a better understanding of these mechanisms since they involve just irreversible magnetization changes. Specifically, the experimental analysis of the coercivity adquisition process for the NdFeB-type system suggests that the magnetization reversal is nucleated at the spin misalignments present due to intergranular exchange interactions. On the other hand, the study of the magnetic viscosity and of the isothermal remanent magnetization (IRM and direct field demagnetization (DCD remanence curves indicates that the dipolar interactions are responsible for the propagation of the switching started at individual particles.

    En este artículo presentamos un análisis comparativo de la influencia de la microestructura a través de las interacciones magnéticas en los mecanismos de inversión de la magnetización en dos sistemas diferentes: aleaciones tipo NdFeB con tamaños de grano en el rango de monodominio y nanocompuestos de Fe-SiO2 con concentraciones de Fe tanto por encima como por debajo del umbral de percolación. Ponemos de manifiesto que el uso del campo coercitivo como parámetro de análisis puede llevar a equívocos debido a la coexistencia de variaciones reversibles e irreversibles de la magnetización. También mostramos que el campo de conmutación y la desimanación térmicamente asistida permiten una mejor comprensión de dichos mecanismos ya que reflejan exclusivamente cambios irreversibles de

  17. Analysis of thermal demagnetization behavior of Nd–Fe–B sintered magnets using magnetic domain observation

    International Nuclear Information System (INIS)

    Takezawa, Masaaki; Ikeda, Soichiro; Morimoto, Yuji; Kabashima, Hisayuki

    2016-01-01

    We used magnetic domain observation to statistically observe the thermal demagnetization behavior of Nd–Fe–B sintered magnets at elevated temperatures up to 150 °C. Simultaneous magnetization reversal in a hundred adjacent grains occurred at 90 °C because of the magnetic interaction among the grains beyond grain boundaries in the Dysprosium (Dy)-free low-coercivity magnet. Conversely, simultaneous magnetization reversal in a hundred grains did not occur in the Dy-added high-coercivity magnets, and the demagnetizing ratio steadily increased with temperature. Furthermore, the addition of Dy induced high thermal stability by eliminating the simultaneous thermal demagnetization, which was caused by the magnetic interaction among the grains.

  18. Analysis of thermal demagnetization behavior of Nd–Fe–B sintered magnets using magnetic domain observation

    Energy Technology Data Exchange (ETDEWEB)

    Takezawa, Masaaki, E-mail: take@ele.kyutech.ac.jp; Ikeda, Soichiro; Morimoto, Yuji [Department of Applied Science for Integrated System Engineering, Faculty of Engineering, Kyushu Institute of Technology, 1-1 Sensui-cho, Tobata-ku, Kitakyushu, Fukuoka 804-8550 (Japan); Kabashima, Hisayuki [Mazda Motor Corporation,3-1, Shinchi, Fuchu-cho, Aki-gun Hiroshima 730-8670 (Japan)

    2016-05-15

    We used magnetic domain observation to statistically observe the thermal demagnetization behavior of Nd–Fe–B sintered magnets at elevated temperatures up to 150 °C. Simultaneous magnetization reversal in a hundred adjacent grains occurred at 90 °C because of the magnetic interaction among the grains beyond grain boundaries in the Dysprosium (Dy)-free low-coercivity magnet. Conversely, simultaneous magnetization reversal in a hundred grains did not occur in the Dy-added high-coercivity magnets, and the demagnetizing ratio steadily increased with temperature. Furthermore, the addition of Dy induced high thermal stability by eliminating the simultaneous thermal demagnetization, which was caused by the magnetic interaction among the grains.

  19. Role of magnetic resonance imaging in guiding thermal therapies. A brief technical review

    International Nuclear Information System (INIS)

    Kuroda, Kagayaki

    2007-01-01

    For a number of reasons, Magnetic Resonance Imaging (MRI) is a unique tool for interventional use. It has a spatial resolution which is independent of the wavelength of the electromagnetic field used for imaging, has various imaging parameters which are related to the physical properties of the subject; provides a superior soft-tissue contrast; provides freedom in determining the slicing or viewing angle; and it utilizes non-ionizing radiation. This technology offers assistance in therapeutic applications such as lesion identification, treatment planning, device tracking, temperature imaging and treatment evaluation. In this article, the role of MRI in assisting thermal therapy is briefly reviewed from a technical point of view. (author)

  20. Thermally and magnetically controlled superconducting rectifiers

    International Nuclear Information System (INIS)

    Mulder, G.B.J.; TenKate, H.H.J.; Krooshoop, H.J.G.; Van de Klundert, L.J.M.

    1989-01-01

    The switches of a superconducting rectifier can be controlled either magnetically or thermally. The main purpose of this paper is to point out the differences between both methods of switching and discuss the consequences for the operation of the rectifier. The discussion is illustrated by the experimental results of a rectifier which was tested with magnetically as well as thermally controlled switches. It has an input current of 30 A, an output current of more than 1 kA and an operating frequency of a few Hertz. A superconducting magnet connected to this rectifier can be energized at a rate exceeding 1 MJ/hour and an efficiency of about 97%

  1. Magnetic properties and thermal stability of MnBi/NdFeB hybrid bonded magnets

    International Nuclear Information System (INIS)

    Cao, S.; Yue, M.; Yang, Y. X.; Zhang, D. T.; Liu, W. Q.; Zhang, J. X.; Guo, Z. H.; Li, W.

    2011-01-01

    Magnetic properties and thermal stability were investigated for the MnBi/NdFeB (MnBi = 0, 20, 40, 60, 80, and 100 wt.%) bonded hybrid magnets prepared by spark plasma sintering (SPS) technique. Effect of MnBi content on the magnetic properties of the hybrid magnets was studied. With increasing MnBi content, the coercivity of the MnBi/NdFeB hybrid magnets increases rapidly, while the remanence and maximum energy product drops simultaneously. Thermal stability measurement on MnBi magnet, NdFeB magnet, and the hybrid magnet with 20 wt.% MnBi indicates that both the NdFeB magnet and the MnBi/NdFeB hybrid magnet have a negative temperature coefficient of coercivity, while the MnBi magnet has a positive one. The (BH) max of the MnBi/NdFeB magnet (MnBi = 20 wt.%) is 5.71 MGOe at 423 K, which is much higher than 3.67 MGOe of the NdFeB magnet, indicating a remarkable improvement of thermal stability.

  2. Lanthanide phosphonates: Synthesis, thermal stability and magnetic characterization

    Energy Technology Data Exchange (ETDEWEB)

    Amghouz, Z., E-mail: amghouz.uo@uniovi.es [Departamentos de Quimica Fisica y Analitica y Quimica Organica e Inorganica, Universidad de Oviedo - CINN, 33006 Oviedo (Spain); Garcia, J.R.; Garcia-Granda, S. [Departamentos de Quimica Fisica y Analitica y Quimica Organica e Inorganica, Universidad de Oviedo - CINN, 33006 Oviedo (Spain); Clearfield, A. [Department of Chemistry, Texas A and M University, College Station, TX 77842-3012 (United States); Rodriguez Fernandez, J.; Pedro, I. de [CITIMAC, Facultad de Ciencias, Universidad de Cantabria, 39005 Santander (Spain); Blanco, J.A. [Departamento de Fisica, Universidad de Oviedo, 33007 Oviedo (Spain)

    2012-09-25

    Highlights: Black-Right-Pointing-Pointer Report of the complete series of lanthanide 1,4-phenylbis(phosphonate). Black-Right-Pointing-Pointer Synthesis under conventional hydrothermal synthesis or microwave-assisted hydrothermal synthesis. Black-Right-Pointing-Pointer Cation size is the key factor for the structural and particles size variations. Black-Right-Pointing-Pointer Thermal behaviour is characterized by unusual very high thermal stability. - Abstract: Series of novel organic-inorganic hybrids materials based on trivalent lanthanides (Ln = Y, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu) and 1,4-phenylbis(phosphonate) obtained under hydrothermal conditions either by oven heat or microwave irradiation. The anhydrous compounds containing La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, and Ho, are isostructural. However, the compounds based on Y, Er, Tm, Yb, and Lu are hydrated and their structures have not yet been solved. The series of compounds are characterized by PXRD, TEM, SEM-EDX and thermal analyses (TG-MS and DSC). TEM study show a variable particles size with a minimum mean-particle size of ca. 30 nm. These compounds exhibit unusual very high thermal stability. The size of particles and the thermal stability are depending on lanthanide(III) cation features. All the investigated materials show paramagnetic behaviour. The magnetic susceptibility data follow a Curie-Weiss laws with paramagnetic effective moments in good agreement with those expected for Ln{sup 3+} free ions.

  3. Thermally-assisted Magma Emplacement Explains Restless Calderas.

    Science.gov (United States)

    Amoruso, Antonella; Crescentini, Luca; D'Antonio, Massimo; Acocella, Valerio

    2017-08-11

    Many calderas show repeated unrest over centuries. Though probably induced by magma, this unique behaviour is not understood and its dynamics remains elusive. To better understand these restless calderas, we interpret deformation data and build thermal models of Campi Flegrei caldera, Italy. Campi Flegrei experienced at least 4 major unrest episodes in the last decades. Our results indicate that the inflation and deflation of magmatic sources at the same location explain most deformation, at least since the build-up of the last 1538 AD eruption. However, such a repeated magma emplacement requires a persistently hot crust. Our thermal models show that this repeated emplacement was assisted by the thermal anomaly created by magma that was intruded at shallow depth ~3 ka before the last eruption. This may explain the persistence of the magmatic sources promoting the restless behaviour of the Campi Flegrei caldera; moreover, it explains the crystallization, re-melting and mixing among compositionally distinct magmas recorded in young volcanic rocks. Our model of thermally-assisted unrest may have a wider applicability, possibly explaining also the dynamics of other restless calderas.

  4. Upgrade of the LHC magnet interconnections thermal shielding

    Energy Technology Data Exchange (ETDEWEB)

    Musso, Andrea; Barlow, Graeme; Bastard, Alain; Charrondiere, Maryline; Deferne, Guy; Dib, Gaëlle; Duret, Max; Guinchard, Michael; Prin, Hervé; Craen, Arnaud Vande; Villiger, Gilles [CERN European Organization for Nuclear Research, Meyrin 1211, Geneva 23, CH (Switzerland); Chrul, Anna [The Henryk Niewodniczanski Institute of Nuclear Physics, Polish Academy of Sciences, ul.Radzikowskiego 152, 31-324 Krakow (Poland); Damianoglou, Dimitrios [NTUA National Technical University of Athens, Heeron Polytechniou 9, 15780 Zografou (Greece); Strychalski, Michał [Wroclaw University of Technology, Faculty of Mechanical and Power Engineering, Wyb. Wyspianskiego 27, Wroclaw, 50-370 (Poland); Wright, Loren [Lancaster University, Bailrigg, Lancaster, LA1 4YW (United Kingdom)

    2014-01-29

    The about 1700 interconnections (ICs) between the Large Hadron Collider (LHC) superconducting magnets include thermal shielding at 50-75 K, providing continuity to the thermal shielding of the magnet cryostats to reduce the overall radiation heat loads to the 1.9 K helium bath of the magnets. The IC shield, made of aluminum, is conduction-cooled via a welded bridge to the thermal shield of the adjacent magnets which is actively cooled. TIG welding of these bridges made in the LHC tunnel at installation of the magnets induced a considerable risk of fire hazard due to the proximity of the multi-layer insulation of the magnet shields. A fire incident occurred in one of the machine sectors during machine installation, but fortunately with limited consequences thanks to prompt intervention of the operators. LHC is now undergoing a 2 years technical stop during which all magnet's ICs will have to be opened to consolidate the magnet electrical connections. The IC thermal shields will therefore have to be removed and re-installed after the work is completed. In order to eliminate the risk of fire hazard when re-welding, it has been decided to review the design of the IC shields, by replacing the welded bridges with a mechanical clamping which also preserves its thermal function. An additional advantage of this new solution is the ease in dismantling for maintenance, and eliminating weld-grinding operations at removal needing radioprotection measures because of material activation after long-term operation of the LHC. This paper describes the new design of the IC shields and in particular the theoretical and experimental validation of its thermal performance. Furthermore a status report of the on-going upgrade work in the LHC is given.

  5. Upgrade of the LHC magnet interconnections thermal shielding

    Science.gov (United States)

    Musso, Andrea; Barlow, Graeme; Bastard, Alain; Charrondiere, Maryline; Chrul, Anna; Damianoglou, Dimitrios; Deferne, Guy; Dib, Gaëlle; Duret, Max; Guinchard, Michael; Prin, Hervé; Strychalski, Michał; Craen, Arnaud Vande; Villiger, Gilles; Wright, Loren

    2014-01-01

    The about 1700 interconnections (ICs) between the Large Hadron Collider (LHC) superconducting magnets include thermal shielding at 50-75 K, providing continuity to the thermal shielding of the magnet cryostats to reduce the overall radiation heat loads to the 1.9 K helium bath of the magnets. The IC shield, made of aluminum, is conduction-cooled via a welded bridge to the thermal shield of the adjacent magnets which is actively cooled. TIG welding of these bridges made in the LHC tunnel at installation of the magnets induced a considerable risk of fire hazard due to the proximity of the multi-layer insulation of the magnet shields. A fire incident occurred in one of the machine sectors during machine installation, but fortunately with limited consequences thanks to prompt intervention of the operators. LHC is now undergoing a 2 years technical stop during which all magnet's ICs will have to be opened to consolidate the magnet electrical connections. The IC thermal shields will therefore have to be removed and re-installed after the work is completed. In order to eliminate the risk of fire hazard when re-welding, it has been decided to review the design of the IC shields, by replacing the welded bridges with a mechanical clamping which also preserves its thermal function. An additional advantage of this new solution is the ease in dismantling for maintenance, and eliminating weld-grinding operations at removal needing radioprotection measures because of material activation after long-term operation of the LHC. This paper describes the new design of the IC shields and in particular the theoretical and experimental validation of its thermal performance. Furthermore a status report of the on-going upgrade work in the LHC is given.

  6. Dynamical Monte Carlo investigation of spin reversal and nonequilibrium magnetization of single-molecule magnets

    Science.gov (United States)

    Liu, Gui-Bin; Liu, Bang-Gui

    2010-10-01

    In this paper, we combine thermal effects with Landau-Zener (LZ) quantum tunneling effects in a dynamical Monte Carlo (DMC) framework to produce satisfactory magnetization curves of single-molecule magnet (SMM) systems. We use the giant spin approximation for SMM spins and consider regular lattices of SMMs with magnetic dipolar interactions (MDIs). We calculate spin-reversal probabilities from thermal-activated barrier hurdling, direct LZ tunneling, and thermal-assisted LZ tunnelings in the presence of sweeping magnetic fields. We do systematical DMC simulations for Mn12 systems with various temperatures and sweeping rates. Our simulations produce clear step structures in low-temperature magnetization curves, and our results show that the thermally activated barrier hurdling becomes dominating at high temperature near 3 K and the thermal-assisted tunnelings play important roles at intermediate temperature. These are consistent with corresponding experimental results on good Mn12 samples (with less disorders) in the presence of little misalignments between the easy axis and applied magnetic fields, and therefore our magnetization curves are satisfactory. Furthermore, our DMC results show that the MDI, with the thermal effects, have important effects on the LZ tunneling processes, but both the MDI and the LZ tunneling give place to the thermal-activated barrier hurdling effect in determining the magnetization curves when the temperature is near 3 K. This DMC approach can be applicable to other SMM systems and could be used to study other properties of SMM systems.

  7. Dynamical Monte Carlo investigation of spin reversals and nonequilibrium magnetization of single-molecule magnets

    OpenAIRE

    Liu, Gui-Bin; Liu, Bang-Gui

    2010-01-01

    In this paper, we combine thermal effects with Landau-Zener (LZ) quantum tunneling effects in a dynamical Monte Carlo (DMC) framework to produce satisfactory magnetization curves of single-molecule magnet (SMM) systems. We use the giant spin approximation for SMM spins and consider regular lattices of SMMs with magnetic dipolar interactions (MDI). We calculate spin reversal probabilities from thermal-activated barrier hurdling, direct LZ tunneling, and thermal-assisted LZ tunnelings in the pr...

  8. 75 FR 21506 - Magnet Schools Assistance Program

    Science.gov (United States)

    2010-04-26

    ... DEPARTMENT OF EDUCATION 34 CFR Part 280 RIN 1855-AA07 [Docket ID ED-2010-OII-0003] Magnet Schools Assistance Program AGENCY: Office of Innovation and Improvement, Department of Education. ACTION: Interim... in the Federal Register an interim final rule and requested comments on that rule for the Magnet...

  9. Magnetic field induced augmented thermal conduction phenomenon in magneto-nanocolloids

    International Nuclear Information System (INIS)

    Katiyar, Ajay; Dhar, Purbarun; Nandi, Tandra; Das, Sarit K.

    2016-01-01

    Magnetic field induced augmented thermal conductivity of magneto-nanocolloids involving nanoparticles, viz. Fe_2O_3, Fe_3O_4, NiO and Co_3O_4 dispersed in different base fluids have been reported. Experiments reveal the augmented thermal transport under external applied magnetic field. A maximum thermal conductivity enhancement ∼114% is attained at 7.0 vol% concentration and 0.1 T magnetic flux density for Fe_3O_4/EG magneto-nanocolloid. However, a maximum ∼82% thermal conductivity enhancement is observed for Fe_3O_4/kerosene magneto-nanocolloid for the same concentration but relatively at low magnetic flux density (∼0.06 T). Thereby, a strong effect of fluid as well as particle physical properties on the chain formation propensity, leading to enhanced conduction, in such systems is observed. Co_3O_4 nanoparticles show insignificant effect on the thermal conductivity enhancement of MNCs due to their minimal magnetic moment. A semi-empirical approach has been proposed to understand the mechanism and physics behind the thermal conductivity enhancement under external applied magnetic field, in tune with near field magnetostatic interactions as well as Neel relaxivity of the magnetic nanoparticles. Furthermore, the model is able to predict the phenomenon of enhanced thermal conductivity as a function of physical parameters and shows good agreement with the experimental observations. - Highlights: • Heat conduction in magneto-nanocolloids augments tremendously under magnetic field. • Oxide nanoparticles of Fe, Ni and Co dispersed in variant base fluids are used. • Enhancement in heat conduction is due to the formation of thermally conductive chains. • Proposed semi-empirical model shows good agreement with the experimental results.

  10. Measurement of time series variation of thermal diffusivity of magnetic fluid under magnetic field by forced Rayleigh scattering method

    Energy Technology Data Exchange (ETDEWEB)

    Motozawa, Masaaki, E-mail: motozawa.masaaki@shizuoka.ac.jp [Shizuoka University, 3-5-1 Johoku, Naka-ku, Hamamatsu-shi, Shizuoka 432-8561 (Japan); Muraoka, Takashi [Shizuoka University, 3-5-1 Johoku, Naka-ku, Hamamatsu-shi, Shizuoka 432-8561 (Japan); Motosuke, Masahiro, E-mail: mot@rs.tus.ac.jp [Tokyo University of Science, 6-3-1 Niijuku, Katsushika-ku, Tokyo 125-8585 (Japan); Fukuta, Mitsuhiro, E-mail: fukuta.mitsuhiro@shizuoka.ac.jp [Shizuoka University, 3-5-1 Johoku, Naka-ku, Hamamatsu-shi, Shizuoka 432-8561 (Japan)

    2017-04-15

    It can be expected that the thermal diffusivity of a magnetic fluid varies from time to time after applying a magnetic field because of the growth of the inner structure of a magnetic fluid such as chain-like clusters. In this study, time series variation of the thermal diffusivity of a magnetic fluid caused by applying a magnetic field was investigated experimentally. For the measurement of time series variation of thermal diffusivity, we attempted to apply the forced Rayleigh scattering method (FRSM), which has high temporal and high spatial resolution. We set up an optical system for the FRSM and measured the thermal diffusivity. A magnetic field was applied to a magnetic fluid in parallel and perpendicular to the heat flux direction, and the magnetic field intensity was 70 mT. The FRSM was successfully applied to measurement of the time series variation of the magnetic fluid from applying a magnetic field. The results show that a characteristic configuration in the time series variation of the thermal diffusivity of magnetic fluid was obtained in the case of applying a magnetic field parallel to the heat flux direction. In contrast, in the case of applying a magnetic field perpendicular to the heat flux, the thermal diffusivity of the magnetic fluid hardly changed during measurement. - Highlights: • Thermal diffusivity was measured by forced Rayleigh scattering method (FRSM). • FRSM has high temporal and high spatial resolutions for measurement. • We attempted to apply FRSM to magnetic fluid (MF). • Time series variation of thermal diffusivity of MF was successfully measured by FRSM. • Anisotropic thermal diffusivity of magnetic fluid was also successfully confirmed.

  11. Nanopatterning reconfigurable magnetic landscapes via thermally assisted scanning probe lithography

    Science.gov (United States)

    Albisetti, E.; Petti, D.; Pancaldi, M.; Madami, M.; Tacchi, S.; Curtis, J.; King, W. P.; Papp, A.; Csaba, G.; Porod, W.; Vavassori, P.; Riedo, E.; Bertacco, R.

    2016-06-01

    The search for novel tools to control magnetism at the nanoscale is crucial for the development of new paradigms in optics, electronics and spintronics. So far, the fabrication of magnetic nanostructures has been achieved mainly through irreversible structural or chemical modifications. Here, we propose a new concept for creating reconfigurable magnetic nanopatterns by crafting, at the nanoscale, the magnetic anisotropy landscape of a ferromagnetic layer exchange-coupled to an antiferromagnetic layer. By performing localized field cooling with the hot tip of a scanning probe microscope, magnetic structures, with arbitrarily oriented magnetization and tunable unidirectional anisotropy, are reversibly patterned without modifying the film chemistry and topography. This opens unforeseen possibilities for the development of novel metamaterials with finely tuned magnetic properties, such as reconfigurable magneto-plasmonic and magnonic crystals. In this context, we experimentally demonstrate spatially controlled spin wave excitation and propagation in magnetic structures patterned with the proposed method.

  12. STDAC: Solar Thermal Design Assistance Center annual report fiscal year 1994

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1994-12-31

    The Solar Thermal Design Assistance Center (STDAC) at Sandia is a resource provided by the DOE Solar Thermal Program. The STDAC`s major objective is to accelerate the use of solar thermal systems by providing direct technical assistance to users in industry, government, and foreign countries; cooperating with industry to test, evaluate, and develop renewable energy systems and components; and educating public and private professionals, administrators, and decision makers. This FY94 report highlights the activities and accomplishments of the STDAC. In 1994, the STDAC continued to provide significant direct technical assistance to domestic and international organizations in industry, government, and education, Applying solar thermal technology to solve energy problems is a vital element of direct technical assistance. The STDAC provides information on the status of new, existing, and developing solar technologies; helps users screen applications; predicts the performance of components and systems; and incorporates the experience of Sandia`s solar energy personnel and facilities to provide expert guidance. The STDAC directly enhances the US solar industry`s ability to successfully bring improved systems to the marketplace. By collaborating with Sandia`s Photovoltaic Design Assistance Center and the National Renewable Energy Laboratory the STDAC is able to offer each customer complete service in applying solar thermal technology. At the National Solar Thermal Test Facility the STDAC tests and evaluates new and innovative solar thermal technologies. Evaluations are conducted in dose cooperation with manufacturers, and the results are used to improve the product and/or quantify its performance characteristics. Manufacturers, in turn, benefit from the improved design, economic performance, and operation of their solar thermal technology. The STDAC provides cost sharing and in-kind service to manufacturers in the development and improvement of solar technology.

  13. Magnetic field induced augmented thermal conduction phenomenon in magneto-nanocolloids

    Energy Technology Data Exchange (ETDEWEB)

    Katiyar, Ajay, E-mail: ajay_cim@rediffmail.com [Research and Innovation Centre (DRDO), Indian Institute of Technology Madras Research Park, Chennai 600 113 (India); Department of Mechanical Engineering, Indian Institute of Technology Madras, Chennai 600 036 (India); Dhar, Purbarun, E-mail: purbarun@iitrpr.ac.in [Department of Mechanical Engineering, Indian Institute of Technology Madras, Chennai 600 036 (India); Nandi, Tandra, E-mail: tandra_n@rediffmail.com [Defence Materials and Stores Research and Development Establishment (DRDO), G.T. Road, Kanpur 208 013 (India); Das, Sarit K., E-mail: skdas@iitrpr.ac.in [Department of Mechanical Engineering, Indian Institute of Technology Madras, Chennai 600 036 (India)

    2016-12-01

    Magnetic field induced augmented thermal conductivity of magneto-nanocolloids involving nanoparticles, viz. Fe{sub 2}O{sub 3}, Fe{sub 3}O{sub 4}, NiO and Co{sub 3}O{sub 4} dispersed in different base fluids have been reported. Experiments reveal the augmented thermal transport under external applied magnetic field. A maximum thermal conductivity enhancement ∼114% is attained at 7.0 vol% concentration and 0.1 T magnetic flux density for Fe{sub 3}O{sub 4}/EG magneto-nanocolloid. However, a maximum ∼82% thermal conductivity enhancement is observed for Fe{sub 3}O{sub 4}/kerosene magneto-nanocolloid for the same concentration but relatively at low magnetic flux density (∼0.06 T). Thereby, a strong effect of fluid as well as particle physical properties on the chain formation propensity, leading to enhanced conduction, in such systems is observed. Co{sub 3}O{sub 4} nanoparticles show insignificant effect on the thermal conductivity enhancement of MNCs due to their minimal magnetic moment. A semi-empirical approach has been proposed to understand the mechanism and physics behind the thermal conductivity enhancement under external applied magnetic field, in tune with near field magnetostatic interactions as well as Neel relaxivity of the magnetic nanoparticles. Furthermore, the model is able to predict the phenomenon of enhanced thermal conductivity as a function of physical parameters and shows good agreement with the experimental observations. - Highlights: • Heat conduction in magneto-nanocolloids augments tremendously under magnetic field. • Oxide nanoparticles of Fe, Ni and Co dispersed in variant base fluids are used. • Enhancement in heat conduction is due to the formation of thermally conductive chains. • Proposed semi-empirical model shows good agreement with the experimental results.

  14. Thermal conductance of heat transfer interfaces for conductively cooled superconducting magnets

    International Nuclear Information System (INIS)

    Cooper, T.L.; Walters, J.D.; Fikse, T.H.

    1996-01-01

    Minimizing thermal resistances across interfaces is critical for efficient thermal performance of conductively cooled superconducting magnet systems. Thermal conductance measurements have been made for a flexible thermal coupling, designed to accommodate magnet-to-cryocooler and cryocooler-to-shield relative motion, and an interface incorporating Multilam designed as a sliding thermal connector for cryocoolers. Temperature changes were measured across each interface as a function of heat input. Thermal conductances have been calculated for each interface, and the impact of each interface on conductively cooled magnet systems will be discussed

  15. Lumped-Element Dynamic Electro-Thermal model of a superconducting magnet

    Science.gov (United States)

    Ravaioli, E.; Auchmann, B.; Maciejewski, M.; ten Kate, H. H. J.; Verweij, A. P.

    2016-12-01

    Modeling accurately electro-thermal transients occurring in a superconducting magnet is challenging. The behavior of the magnet is the result of complex phenomena occurring in distinct physical domains (electrical, magnetic and thermal) at very different spatial and time scales. Combined multi-domain effects significantly affect the dynamic behavior of the system and are to be taken into account in a coherent and consistent model. A new methodology for developing a Lumped-Element Dynamic Electro-Thermal (LEDET) model of a superconducting magnet is presented. This model includes non-linear dynamic effects such as the dependence of the magnet's differential self-inductance on the presence of inter-filament and inter-strand coupling currents in the conductor. These effects are usually not taken into account because superconducting magnets are primarily operated in stationary conditions. However, they often have significant impact on magnet performance, particularly when the magnet is subject to high ramp rates. Following the LEDET method, the complex interdependence between the electro-magnetic and thermal domains can be modeled with three sub-networks of lumped-elements, reproducing the electrical transient in the main magnet circuit, the thermal transient in the coil cross-section, and the electro-magnetic transient of the inter-filament and inter-strand coupling currents in the superconductor. The same simulation environment can simultaneously model macroscopic electrical transients and phenomena at the level of superconducting strands. The model developed is a very useful tool for reproducing and predicting the performance of conventional quench protection systems based on energy extraction and quench heaters, and of the innovative CLIQ protection system as well.

  16. Pressure-assisted thermal sterilization of soup

    Science.gov (United States)

    Shibeshi, Kidane; Farid, Mohammed M.

    2010-12-01

    The overall efficiency of an existing scale-up pressure-assisted thermal sterilization (PATS) unit was investigated with regards to inactivation of Geobacillus stearothermophilus spores suspended in pumpkin soup. The PATS unit is a double pipe heat exchanger in which the soup is pumped into its inner high pressure tube and constrained by two high pressure valves, while steam is continuously passed through the annular region to heat the content. The technology is based on pressure generation by thermal expansion of the liquid in an enclosure. In this work, the addition of an air line to push the treated liquid food out of the existing PATS unit has improved the overall quality of the treated samples, as evidenced by achieving higher log reduction of the spores. Compared with thermal processing, the application of PATS shows the potential for lowering the thermal treatment temperature, offering improved food quality.

  17. Magnetically Assisted Bilayer Composites for Soft Bending Actuators

    Directory of Open Access Journals (Sweden)

    Sung-Hwan Jang

    2017-06-01

    Full Text Available This article presents a soft pneumatic bending actuator using a magnetically assisted bilayer composite composed of silicone polymer and ferromagnetic particles. Bilayer composites were fabricated by mixing ferromagnetic particles to a prepolymer state of silicone in a mold and asymmetrically distributed them by applying a strong non-uniform magnetic field to one side of the mold during the curing process. The biased magnetic field induces sedimentation of the ferromagnetic particles toward one side of the structure. The nonhomogeneous distribution of the particles induces bending of the structure when inflated, as a result of asymmetric stiffness of the composite. The bilayer composites were then characterized with a scanning electron microscopy and thermogravimetric analysis. The bending performance and the axial expansion of the actuator were discussed for manipulation applications in soft robotics and bioengineering. The magnetically assisted manufacturing process for the soft bending actuator is a promising technique for various applications in soft robotics.

  18. Magnetically Assisted Bilayer Composites for Soft Bending Actuators.

    Science.gov (United States)

    Jang, Sung-Hwan; Na, Seon-Hong; Park, Yong-Lae

    2017-06-12

    This article presents a soft pneumatic bending actuator using a magnetically assisted bilayer composite composed of silicone polymer and ferromagnetic particles. Bilayer composites were fabricated by mixing ferromagnetic particles to a prepolymer state of silicone in a mold and asymmetrically distributed them by applying a strong non-uniform magnetic field to one side of the mold during the curing process. The biased magnetic field induces sedimentation of the ferromagnetic particles toward one side of the structure. The nonhomogeneous distribution of the particles induces bending of the structure when inflated, as a result of asymmetric stiffness of the composite. The bilayer composites were then characterized with a scanning electron microscopy and thermogravimetric analysis. The bending performance and the axial expansion of the actuator were discussed for manipulation applications in soft robotics and bioengineering. The magnetically assisted manufacturing process for the soft bending actuator is a promising technique for various applications in soft robotics.

  19. Method and device for thermal control of biological and chemical reactions using magnetic particles or magnetic beads and variable magnetic fields

    OpenAIRE

    Zilch, C.; Gerdes, W.; Bauer, J.; Holschuh, K.

    2009-01-01

    The invention relates to a method for the thermal control of at least one temperature-dependent enzymatic reaction in the presence of magnetic particles, particularly nanoparticles, or magnetic beads, in vitro by heating the magnetic beads or magnetic particles to at least one defined target temperature using alternating magnetic fields. The thermally controllable enzymatic reaction carried out with the method according to the invention is preferably a PCR reaction or another reaction for elo...

  20. Thermal conductivity of niobium single crystals in a magnetic field

    International Nuclear Information System (INIS)

    Gladun, C.; Vinzelberg, H.

    1980-01-01

    The thermal conductivity in longitudinal magnetic fields up to 5 T and in the temperature range 3.5 to 15 K is measured in two high purity niobium single crystals having residual resistivity ratios of 22700 and 19200 and orientations of the rod axis [110] and [100]. The investigations show that by means of the longitudinal magnetic field the thermal conductivity may decrease only to a limiting value. In the crystal directions [110] and [100] for the ratio of the thermal conductivity in zero field and the thermal conductivity in the saturation field the temperature-independent factors 1.92 and 1.27, respectively, are determined. With the aid of these factors the thermal conductivity in the normal state is evaluated from the measured values of thermal conductivity below Tsub(c) in the magnetic field. The different conduction and scattering mechanisms are discussed. (author)

  1. Thermal investigations of a room temperature magnetic refrigerator

    Energy Technology Data Exchange (ETDEWEB)

    Smaili, Arezki; Chiba, Younes [Ecole Nationale Polytechnique d' Alger (Algeria)], email: arezki.smaili@enp.edu.dz

    2011-07-01

    Magnetic refrigeration is a concept based on the magnetocaloric effect that some materials exhibit when the external magnetic field changes. The aim of this paper is to assess the performance of a numerical model in predicting parameters of an active magnetic regenerator refrigerator. Numerical simulations were conducted to perform a thermal analysis on an active magnetic regenerator refrigerator operating near room temperature with and without applied cooling load. Curves of temperature span, cooling capacity and thermal efficiency as functions of the operating conditions were drawn and are presented in this paper. Results showed that at fixed frequency Ql versus mf has an optimum and COP was increased with cycle frequency values. This study demonstrated that the proposed numerical model could be used to predict parameters of an active magnetic regenerator refrigerator as it provides consistent results.

  2. Study on optimization design of superconducting magnet for magnetic force assisted drug delivery system

    International Nuclear Information System (INIS)

    Fukui, S.; Abe, R.; Ogawa, J.; Oka, T.; Yamaguchi, M.; Sato, T.; Imaizumi, H.

    2007-01-01

    Analytical study on the design of the superconducting magnet for the magnetic force assisted drug delivery system is presented in this paper. The necessary magnetic field condition to reside the magnetic drug particle in the blood vessels is determined by analyzing the particle motion in the blood vessel. The design procedure of the superconducting magnet for the M-DDS is presented and some case studies are conducted. The analytical results show that the superconducting magnet to satisfy the magnetic field conduction for the M-DDS is practically feasible

  3. Magnetic Thermometer: Thermal effect on the Agglomeration of Magnetic Nanoparticles by Magnetic field

    Science.gov (United States)

    Jin, Daeseong; Kim, Hackjin

    2018-03-01

    We have investigated the agglomeration of magnetite nanoparticles in the aqueous solution under magnetic field by measuring temporal change of magnetic weight. The magnetic weight corresponds to the force due to the magnetization of magnetic materials. Superparamagnetic magnetite nanoparticles are synthesized and used in this work. When the aqueous solution of magnetite nanoparticle is placed under magnetic field, the magnetic weight of the sample jumps instantaneously by Neel and Brown mechanisms and thereafter increases steadily following a stretched exponential function as the nanoparticles agglomerate, which results from the distribution of energy barriers involved in the dynamics. Thermal motions of nanoparticles in the agglomerate perturb the ordered structure of the agglomerate to reduce the magnetic weight. Fluctuation of the structural order of the agglomerate by temperature change is much faster than the formation of agglomerate and explained well with the Boltzmann distribution, which suggests that the magnetic weight of the agglomerate works as a magnetic thermometer.

  4. Micromagnetic Simulation of Strain-Assisted Current-Induced Magnetization Switching

    Directory of Open Access Journals (Sweden)

    H. B. Huang

    2016-01-01

    Full Text Available We investigated the effect of substrate misfit strain on the current-induced magnetization switching in magnetic tunnel junctions by combining micromagnetic simulation with phase-field microelasticity theory. Our results indicate that the positive substrate misfit strain can decrease the critical current density of magnetization switching by pushing the magnetization from out-of-plane to in-plane directions, while the negative strain pushes the magnetization back to the out-of-plane directions. The magnetic domain evolution is obtained to demonstrate the strain-assisted current-induced magnetization switching.

  5. Magnetically Assisted Bilayer Composites for Soft Bending Actuators

    OpenAIRE

    Jang, Sung-Hwan; Na, Seon-Hong; Park, Yong-Lae

    2017-01-01

    This article presents a soft pneumatic bending actuator using a magnetically assisted bilayer composite composed of silicone polymer and ferromagnetic particles. Bilayer composites were fabricated by mixing ferromagnetic particles to a prepolymer state of silicone in a mold and asymmetrically distributed them by applying a strong non-uniform magnetic field to one side of the mold during the curing process. The biased magnetic field induces sedimentation of the ferromagnetic particles toward o...

  6. Controllable magnetic thermal rectification in a SMM dimmer with the Dzyaloshinskii-Moriya interaction

    Science.gov (United States)

    Xu, Ai-Hua; Liu, Juan; Luo, Bo

    2016-10-01

    Using the quantum master equation, we studied the thermally driven magnonic spin current in a single-molecule magnet (SMM) dimer with the Dzyaloshinskii-Moriya interaction (DMI). Due to the asymmetric DMI, one can observe the thermal rectifying effect in the case of the spatial symmetry coupling with the thermal reservoirs. The properties of the thermal rectification can be controlled by tuning the angle and intensity of the magnetic field. Specially, when the DM vector and magnetic field point at the specific angles, the thermal rectifying effect disappears. And this phenomenon does not depend on the intensities of DMI and magnetic field, the temperature bias and the magnetic anisotropies of the SMM.

  7. Effect of magnetic polarity on surface roughness during magnetic field assisted EDM of tool steel

    Science.gov (United States)

    Efendee, A. M.; Saifuldin, M.; Gebremariam, MA; Azhari, A.

    2018-04-01

    Electrical discharge machining (EDM) is one of the non-traditional machining techniques where the process offers wide range of parameters manipulation and machining applications. However, surface roughness, material removal rate, electrode wear and operation costs were among the topmost issue within this technique. Alteration of magnetic device around machining area offers exciting output to be investigated and the effects of magnetic polarity on EDM remain unacquainted. The aim of this research is to investigate the effect of magnetic polarity on surface roughness during magnetic field assisted electrical discharge machining (MFAEDM) on tool steel material (AISI 420 mod.) using graphite electrode. A Magnet with a force of 18 Tesla was applied to the EDM process at selected parameters. The sparks under magnetic field assisted EDM produced better surface finish than the normal conventional EDM process. At the presence of high magnetic field, the spark produced was squeezed and discharge craters generated on the machined surface was tiny and shallow. Correct magnetic polarity combination of MFAEDM process is highly useful to attain a high efficiency machining and improved quality of surface finish to meet the demand of modern industrial applications.

  8. Transport of runaway and thermal electrons due to magnetic microturbulence

    International Nuclear Information System (INIS)

    Mynick, H.E.; Strachan, J.D.

    1981-01-01

    The ratio of the runaway electron confinement to thermal electron energy confinement is derived for tokamaks where both processes are determined by free streaming along stochastic magnetic field lines. The runaway electron confinement is enhanced at high runaway electron energies due to phase averaging over the magnetic perturbations when the runaway electron drift surfaces are displaced from the magnetic surfaces. Comparison with experimental data from LT-3, Ormak, PLT, ST, and TM-3 indicates that magnetic stochasticity may explain the relative transport rates of runaways and thermal electron energy

  9. Effect of magnetic field on thermal conductivity and viscosity of a magnetic nanofluid loaded with carbon nanotubes

    Energy Technology Data Exchange (ETDEWEB)

    Shahsavar, Amin [Kermanshah University of Technology, Kermanshah (Iran, Islamic Republic of); Salimpour, Mohammad Reza; Saghafian, Mohsen [Isfahan University of Technology, Isfahan (Iran, Islamic Republic of); Shafii, M. B. [Sharif University of Technology, Tehran(Iran, Islamic Republic of)

    2016-02-15

    The present work examines experimentally the effect of magnetic field on the viscosity and thermal conductivity of a hybrid nanofluid containing tetramethylammonium hydroxide (TMAH) coated Fe{sub 3}O{sub 4} nanoparticles and Gum arabic (GA) coated carbon nanotubes (CNTs). The hybrid nanofluid was prepared by using ultrasonic dispersion method. Magnetic field was created by a pair of spaced apart magnet plates. The effect of temperature on the time variation of thermal conductivity under applied magnetic field was also investigated. According to the results of this study, viscosity of the hybrid nanofluid increases with the strength of magnetic field, while it decreases with the increase of temperature. Additionally, it is found that the hybrid nanofluid behaves as a shear thinning fluid at low shear rates while it exhibits Newtonian behavior at high shear rates. Furthermore, results show that when an external magnetic field is applied to the studied magnetic nanofluids, the thermal conductivity experiences a peak.

  10. Thermal quantum discord of spins in an inhomogeneous magnetic field

    International Nuclear Information System (INIS)

    Guo Jinliang; Mi Yingjuan; Zhang Jian; Song Heshan

    2011-01-01

    In contrast with the thermal entanglement, we study the quantum discord and classical correlation in a two-qubit Heisenberg XXZ model with an inhomogeneous magnetic field. It is shown that the effects of the external magnetic fields, including the uniform and inhomogeneous magnetic fields, on the thermal entanglement, quantum discord and classical correlation behave differently in various aspects, which depend on system temperature and model type. We can tune the inhomogeneous magnetic field to enhance the entanglement or classical correlation and meanwhile decrease the quantum discord. In addition, taking into account the inhomogeneous magnetic field, the sudden change in the behaviour of quantum discord still survives, which can detect the critical points of quantum phase transitions at finite temperature, but not for a uniform magnetic field.

  11. Production for high thermal stability NdFeB magnets

    Energy Technology Data Exchange (ETDEWEB)

    Yu, L.Q. [College of Physics Science and Technology, China University of Petroleum (East China), Dongying 257061, Shandong Province (China)], E-mail: iyy2000@163.com; Zhang, J.; Hu, S.Q.; Han, Z.D. [College of Physics Science and Technology, China University of Petroleum (East China), Dongying 257061, Shandong Province (China); Yan, M. [State Key Lab of Silicon Materials, Zhejiang University, Hangzhou 310027 (China)

    2008-04-15

    To improve sintered NdFeB magnets' thermal stability and magnetic properties, combined addition of elements Cu and Gd was investigated. It was found that with Gd addition increase to 1.0%, the temperature coefficient {alpha} improved from -0.15 to -0.05%/deg. C (maximum working temperature 120 deg. C), but the remanence and the maximum energy product linearly decreased. With addition of Cu in Gd-containing magnets the intrinsic coercivity increased greatly, and the remanence increased also because of their density improvement, and optimum Cu content was achieved at 0.2%. Microstructure analysis showed that most of the Cu distributed at grain boundaries and led to clear and smooth morphologies. Magnets with high thermal stability {alpha}=-0.05%/deg. C and magnetic properties were obtained with addition of Gd=0.8% and Cu=0.2%.

  12. Particle-in-cell simulations on spontaneous thermal magnetic field fluctuations

    Energy Technology Data Exchange (ETDEWEB)

    Simões, F. J. R. Jr.; Pavan, J. [Instituto de Física e Matemática, UFPel, Pelotas, RS (Brazil); Gaelzer, R.; Ziebell, L. F. [Instituto de Física, UFRGS, Porto Alegre, RS (Brazil); Yoon, P. H. [Institute for Physical Science and Technology, University of Maryland, College Park, Maryland 20742 (United States)

    2013-10-15

    In this paper an electromagnetic particle code is used to investigate the spontaneous thermal emission. Specifically we perform particle-in-cell simulations employing a non-relativistic isotropic Maxwellian particle distribution to show that thermal fluctuations are related to the origin of spontaneous magnetic field fluctuation. These thermal fluctuations can become seed for further amplification mechanisms and thus be considered at the origin of the cosmological magnetic field, at microgauss levels. Our numerical results are in accordance with theoretical results presented in the literature.

  13. Head-disk Interface Study for Heat Assisted Magnetic Recording (HAMR) and Plasmonic Nanolithography for Patterned Media

    Science.gov (United States)

    Xiong, Shaomin

    The magnetic storage areal density keeps increasing every year, and magnetic recording-based hard disk drives provide a very cheap and effective solution to the ever increasing demand for data storage. Heat assisted magnetic recording (HAMR) and bit patterned media have been proposed to increase the magnetic storage density beyond 1 Tb/in2. In HAMR systems, high magnetic anisotropy materials are recommended to break the superparamagnetic limit for further scaling down the size of magnetic bits. However, the current magnetic transducers are not able to generate strong enough field to switch the magnetic orientations of the high magnetic anisotropy material so the data writing is not able to be achieved. So thermal heating has to be applied to reduce the coercivity for the magnetic writing. To provide the heating, a laser is focused using a near field transducer (NFT) to locally heat a ~(25 nm)2 spot on the magnetic disk to the Curie temperature, which is ~ 400 C-600°C, to assist in the data writing process. But this high temperature working condition is a great challenge for the traditional head-disk interface (HDI). The disk lubricant can be depleted by evaporation or decomposition. The protective carbon overcoat can be graphitized or oxidized. The surface quality, such as its roughness, can be changed as well. The NFT structure is also vulnerable to degradation under the large number of thermal load cycles. The changes of the HDI under the thermal conditions could significantly reduce the robustness and reliability of the HAMR products. In bit patterned media systems, instead of using the continuous magnetic granular material, physically isolated magnetic islands are used to store data. The size of the magnetic islands should be about or less than 25 nm in order to achieve the storage areal density beyond 1 Tb/in2. However, the manufacture of the patterned media disks is a great challenge for the current optical lithography technology. Alternative lithography

  14. Interaction of supra-thermal ions with turbulence in a magnetized toroidal plasma

    International Nuclear Information System (INIS)

    Plyushchev, G.

    2009-01-01

    This thesis addresses the interaction of a supra-thermal ion beam with turbulence in the simple magnetized toroidal plasma of TORPEX. The first part of the Thesis deals with the ohmic assisted discharges on TORPEX. The aim of these discharges is the investigation of the open to closed magnetic field line transition. The relevant magnetic diagnostics were developed. Ohmic assisted discharges with a maximum plasma current up to 1 kA are routinely obtained. The equilibrium conditions on the vacuum magnetic field configuration were investigated. In the second part of the Thesis, the design of the fast ion source and detector are discussed. The accelerating electric field needed for the fast ion source was optimized. The fast ion source was constructed and commissioned. To detect the fast ions a specially designed gridded energy analyzer was used. The electron energy distribution function was obtained to demonstrate the efficiency of the detector. The experiments with the fast ion beam were conducted in different plasma regions of TORPEX. In the third part of the Thesis, numerical simulations are used to interpret the measured fast ion beam behavior. It is shown that a simple single particle equation of motion explains the beam behavior in the experiments in the absence of plasma. To explain the fast ion beam experiments with the plasma a turbulent electric field must be used. The model that takes into account this turbulent electrical field qualitatively explains the shape of the fast ion current density profile in the different plasma regions of TORPEX. The vertically elongated fast ion current density profiles are explained by a spread in the fast ion velocity distribution. The theoretically predicted radial fast ion beam spreading due to the turbulent electric field was observed in the experiment. (author)

  15. Thermal performance of the MFTF magnets

    International Nuclear Information System (INIS)

    VanSant, J.H.

    1983-01-01

    A yin-yang pair of liquid-helium (LHe) cooled, superconducting magnets were tested last year at the Lawrence Livermore National Laboratory (LLNL) as part of a series of tests with the Mirror Fusion Test Facility (MFTF). These tests were performed to determine the success of engineering design used in major systems of the MFTF and to provide a technical base for rescoping from a single-mirror facility to the large tandem-mirror configuration (MFTF-B) now under construction. The magnets were cooled, operated at their design current and magnetic field, and warmed to atmospheric temperature. In this report, we describe their thermal behavior during these tests

  16. SEISMIC DISCRIMINATION OF THERMAL AND MAGNETIC ANOMALIES IN SUNSPOT UMBRAE

    International Nuclear Information System (INIS)

    Lindsey, C.; Cally, P. S.; Rempel, M.

    2010-01-01

    Efforts to model sunspots based on helioseismic signatures need to discriminate between the effects of (1) a strong magnetic field that introduces time-irreversible, vantage-dependent phase shifts, apparently connected to fast- and slow-mode coupling and wave absorption and (2) a thermal anomaly that includes cool gas extending an indefinite depth beneath the photosphere. Helioseismic observations of sunspots show travel times considerably reduced with respect to equivalent quiet-Sun signatures. Simulations by Moradi and Cally of waves skipping across sunspots with photospheric magnetic fields of order 3 kG show travel times that respond strongly to the magnetic field and relatively weakly to the thermal anomaly by itself. We note that waves propagating vertically in a vertical magnetic field are relatively insensitive to the magnetic field, while remaining highly responsive to the attendant thermal anomaly. Travel-time measurements for waves with large skip distances into the centers of axially symmetric sunspots are therefore a crucial resource for discrimination of the thermal anomaly beneath sunspot umbrae from the magnetic anomaly. One-dimensional models of sunspot umbrae based on compressible-radiative-magnetic-convective simulations such as by Rempel et al. can be fashioned to fit observed helioseismic travel-time spectra in the centers of sunspot umbrae. These models are based on cooling of the upper 2-4 Mm of the umbral subphotosphere with no significant anomaly beneath 4.5 Mm. The travel-time reductions characteristic of these models are primarily a consequence of a Wilson depression resulting from a strong downward buoyancy of the cooled umbral medium.

  17. Thermal and structural analysis of a cryogenic conduction cooling system for a HTS NMR magnet

    Energy Technology Data Exchange (ETDEWEB)

    In, Se Hwan; Hong, Yong Jun; Yeom, Han Kil; Ko, Hyo Bong; Park, Seong Je [Korea Institute of Machinery and Materials, Daejeon (Korea, Republic of)

    2016-03-15

    The superconducting NMR magnets have used cryogen such as liquid helium for their cooling. The conduction cooling method using cryocoolers, however, makes the cryogenic cooling system for NMR magnets more compact and user-friendly than the cryogen cooling method. This paper describes the thermal and structural analysis of a cryogenic conduction cooling system for a 400 MHz HTS NMR magnet, focusing on the magnet assembly. The highly thermo-conductive cooling plates between HTS double pancake coils are used to transfer the heat generated in coils, namely Joule heating at lap splice joints, to thermal link blocks and finally the cryocooler. The conduction cooling structure of the HTS magnet assembly preliminarily designed is verified by thermal and structural analysis. The orthotropic thermal properties of the HTS coil, thermal contact resistance and radiation heat load are considered in the thermal analysis. The thermal analysis confirms the uniform temperature distribution for the present thermal design of the NMR magnet within 0.2 K. The mechanical stress and the displacement by the electromagnetic force and the thermal contraction are checked to verify structural stability. The structural analysis indicates that the mechanical stress on each component of the magnet is less than its material yield strength and the displacement is acceptable in comparison with the magnet dimension.

  18. A study: Effect of Students Peer Assisted Learning on Magnetic Field Achievement

    International Nuclear Information System (INIS)

    Mueanploy, Wannapa

    2016-01-01

    This study is the case study of Physic II Course for students of Pathumwan Institute of Technology. The purpose of this study is: 1) to develop cooperative learning method of peer assisted learning (PAL), 2) to compare the learning achievement before and after studied magnetic field lesson by cooperative learning method of peer assisted learning. The population was engineering students of Pathumwan Institute of Technology (PIT’s students) who registered Physic II Course during year 2014. The sample used in this study was selected from the 72 students who passed in Physic I Course. The control groups learning magnetic fields by Traditional Method (TM) and experimental groups learning magnetic field by method of peers assisted learning. The students do pretest before the lesson and do post-test after the lesson by 20 items achievement tests of magnetic field. The post-test higher than pretest achievement significantly at 0.01 level. (paper)

  19. Thermally-assisted Magma Emplacement Explains Restless Calderas

    Science.gov (United States)

    Amoruso, A.; Crescentini, L.; D'Antonio, M.; Acocella, V.

    2017-12-01

    Many calderas show repeated unrest over centuries. Though probably induced by magma, this unique behaviour is not understood and its dynamics remains elusive. To better understand these restless calderas, we interpret deformation data and build thermal models of Campi Flegrei, Italy, which is the best-known, yet most dangerous calderas, lying to the west of Naples and restless since the 1950s at least.Our elaboration of the geodetic data indicates that the inflation and deflation of magmatic sources at the same location explain most deformation, at least since the build-up of the last 1538 AD eruption. However, such a repeated magma emplacement requires a persistently hot crust.Our thermal models show that the repeated emplacement was assisted by the thermal anomaly created by magma that was intruded at shallow depth 3 ka before the last eruption and, in turn, contributed to maintain the thermal anomaly itself. This may explain the persistence of the magmatic sources promoting the restless behaviour of the Campi Flegrei caldera; moreover, it explains the crystallization, re-melting and mixing among compositionally distinct magmas recorded in young volcanic rocks.Available information at other calderas highlights similarities to Campi Flegrei, in the pattern and cause of unrest. All monitored restless calderas have either geodetically (Yellowstone, Aira Iwo-Jima, Askja, Fernandina and, partly, Long Valley) or geophysically (Rabaul, Okmok) detected sill-like intrusions inducing repeated unrest. Some calderas (Yellowstone, Long Valley) also show stable deformation pattern, where inflation insists on and mimics the resurgence uplift. The common existence of sill-like sources, also responsible for stable deformation patterns, in restless calderas suggests close similarities to Campi Flegrei. This suggests a wider applicability of our model of thermally-assisted sill emplacement, to be tested by future studies to better understand not only the dynamics of restless

  20. Eddy current loss calculation and thermal analysis of axial-flux permanent magnet couplers

    Directory of Open Access Journals (Sweden)

    Di Zheng

    2017-02-01

    Full Text Available A three-dimensional magnetic field analytical model of axial-flux permanent magnet couplers is presented to calculate the eddy current loss, and the prediction of the copper plate temperature under various loads is analyzed. The magnetic field distribution is calculated, and then the eddy current loss is obtained, with the magnetic field analytical model established in cylindrical coordinate. The influence of various loads on eddy current loss is analyzed. Furthermore, a thermal model of axial-flux permanent magnet couplers is established by taking the eddy current loss as the heat source, using the electromagnetic-thermal coupled method. With the help of the thermal model, the influence of various loads on copper plate temperature rise is also analyzed. The calculated results are compared with the results of finite element method and measurement. The comparison results confirm the validity of the magnetic field analytical model and thermal model.

  1. Magnetic Cellulose Nanocrystal Based Anisotropic Polylactic Acid Nanocomposite Films: Influence on Electrical, Magnetic, Thermal, and Mechanical Properties.

    Science.gov (United States)

    Dhar, Prodyut; Kumar, Amit; Katiyar, Vimal

    2016-07-20

    This paper reports a single-step co-precipitation method for the fabrication of magnetic cellulose nanocrystals (MGCNCs) with high iron oxide nanoparticle content (∼51 wt % loading) adsorbed onto cellulose nanocrystals (CNCs). X-ray diffraction (XRD), Fourier transform infrared (FTIR), and Raman spectroscopic studies confirmed that the hydroxyl groups on the surface of CNCs (derived from the bamboo pulp) acted as anchor points for the adsorption of Fe3O4 nanoparticles. The fabricated MGCNCs have a high magnetic moment, which is utilized to orient the magnetoresponsive nanofillers in parallel or perpendicular orientations inside the polylactic acid (PLA) matrix. Magnetic-field-assisted directional alignment of MGCNCs led to the incorporation of anisotropic mechanical, thermal, and electrical properties in the fabricated PLA-MGCNC nanocomposites. Thermomechanical studies showed significant improvement in the elastic modulus and glass-transition temperature for the magnetically oriented samples. Differential scanning calorimetry (DSC) and XRD studies confirmed that the alignment of MGCNCs led to the improvement in the percentage crystallinity and, with the absence of the cold-crystallization phenomenon, finds a potential application in polymer processing in the presence of magnetic field. The tensile strength and percentage elongation for the parallel-oriented samples improved by ∼70 and 240%, respectively, and for perpendicular-oriented samples, by ∼58 and 172%, respectively, in comparison to the unoriented samples. Furthermore, its anisotropically induced electrical and magnetic properties are desirable for fabricating self-biased electronics products. We also demonstrate that the fabricated anisotropic PLA-MGCNC nanocomposites could be laminated into films with the incorporation of directionally tunable mechanical properties. Therefore, the current study provides a novel noninvasive approach of orienting nontoxic bioderived CNCs in the presence of low

  2. Analysis and reduction of thermal magnetic noise in liquid-He dewar for sensitive low-field nuclear magnetic resonance measurements

    International Nuclear Information System (INIS)

    Hwang, S. M.; Yu, K. K.; Lee, Y. H.; Kang, C. S.; Kim, K.; Lee, S. J.

    2013-01-01

    For sensitive measurements of micro-Tesla nuclear magnetic resonance (μT-NMR) signal, a low-noise superconducting quantum interference device (SQUID) system is needed. We have fabricated a liquid He dewar for an SQUID having a large diameter for the pickup coil. The initial test of the SQUID system showed much higher low-frequency magnetic noise caused by the thermal magnetic noise of the aluminum plates used for the vapor-cooled thermal shield material. The frequency dependence of the noise spectrum showed that the noise increases with the decrease of frequency. This behavior could be explained from a two-layer model; one generating the thermal noise and the other one shielding the thermal noise by eddy-current shielding. And the eddy-current shielding effect is strongly dependent on the frequency through the skin-depth. To minimize the loop size for the fluctuating thermal noise current, we changed the thermal shield material into insulated thin Cu mesh. The magnetic noise of the SQUID system became flat down to 0.1 Hz with a white noise of 0.3 fT√ Hz, including the other noise contributions such as SQUID electronics and magnetically shielded room, etc, which is acceptable for low-noise μT-NMR experiments.

  3. Spin dynamics of Mn12-acetate in the thermally activated tunneling regime: ac susceptibility and magnetization relaxation

    Science.gov (United States)

    Pohjola, Teemu; Schoeller, Herbert

    2000-12-01

    In this work, we study the spin dynamics of Mn12-acetate molecules in the regime of thermally assisted tunneling. In particular, we describe the system in the presence of a strong transverse magnetic field. Similar to recent experiments, the relaxation time/rate is found to display a series of resonances; their Lorentzian shape is found to stem from the tunneling. The dynamic susceptibility χ(ω) is calculated starting from the microscopic Hamiltonian and the resonant structure manifests itself also in χ(ω). Similar to recent results reported on another molecular magnet, Fe8, we find oscillations of the relaxation rate as a function of the transverse magnetic field when the field is directed along a hard axis of the molecules. This phenomenon is attributed to the interference of the geometrical or Berry phase. We propose susceptibility experiments to be carried out for strong transverse magnetic fields to study these oscillations and for a better resolution of the sharp satellite peaks in the relaxation rates.

  4. Thermal characterization of magnetically aligned carbonyl iron/agar composites.

    Science.gov (United States)

    Diaz-Bleis, D; Vales-Pinzón, C; Freile-Pelegrín, Y; Alvarado-Gil, J J

    2014-01-01

    Composites of magnetic particles into polymeric matrices have received increasing research interest due to their capacity to respond to external magnetic or electromagnetic fields. In this study, agar from Gelidium robustum has been chosen as natural biocompatible polymer to build the matrix of the magnetic carbonyl iron particles (CIP) for their uses in biomedical fields. Heat transfer behavior of the CIP-agar composites containing different concentrations (5, 10, 15, 20, 25 and 30% w/w) of magnetically aligned and non-aligned CIP in the agar matrix was studied using photothermal radiometry (PTR) in the back-propagation emission configuration. The morphology of the CIP-agar composites with aligned and non-aligned CIP under magnetic field was also evaluated by scanning electron microscopy (SEM). The results revealed a dominant effect of CIP concentration over the alignment patterns induced by the magnetic field, which agrees with the behavior of the thermal diffusivity and thermal conductivity. Agar served as a perfect matrix to be used with CIP, and CIP-agar composites magnetically aligned at 20% CIP concentration can be considered as promising 'smart' material for hyperthermia treatments in the biomedical field. Copyright © 2013 Elsevier Ltd. All rights reserved.

  5. Thermal effects and in-plane magnetic anisotropy in thin-film recording media

    International Nuclear Information System (INIS)

    Ajan, Antony; Abarra, E.N.; Acharya, B.R.; Inomata, A.; Okamoto, I.; Shinohara, M.

    2003-01-01

    The effect of thermal activation on the in-plane magnetic anisotropy [measured as orientation ratio (OR)] of granular longitudinal magnetic recording media is investigated. Temperature and time dependent studies were made on media with different magnetic layer thicknesses. We find that OR is independent of temperature for a stable medium but shows a large increase with temperature for thermally unstable media. At low temperatures and high field sweep rates, the OR values are found to be the same, independent of the magnetic layer thickness. The unique value when thermal activation is reduced is consistent with the high population of the cobalt c axes along the texturing direction as the origin of anisotropy

  6. Thermal analysis of the LHC injection kicker magnets

    Science.gov (United States)

    Vega, L.; Abánades, A.; Barnes, M. J.; Vlachodimitropoulos, V.; Weterings, W.

    2017-07-01

    The CERN Large Hadron Collider LHC is equipped with two fast pulsed magnet systems (MKIs) that inject particle beams coming from the injector chain. Operation with high intensity beams for many hours can lead to significant beam induced heating of the ferrite yokes of the MKIs. When the ferrite exceeds the Curie temperature of 125°C it loses its magnetic properties, preventing further injection until the ferrite cools down, potentially causing a delay of several hours. Hence important upgrades of the beam-screen were implemented after Run 1 of LHC. However, the High-Luminosity (HL) LHC will be operated with significantly higher intensity beams and hence additional measures are required to limit the ferrite temperature. These magnets operate under ultra-high vacuum conditions: convection is negligible and, as a result of low emissivity of the inside of the vacuum tanks, thermal radiation is limited. A detailed study of the thermal behaviour of these magnets is reported and compared with measurements. In addition several options to improve cooling of the ferrites are presented and analysed.

  7. Nanoscale thermal transport. II. 2003–2012

    OpenAIRE

    Cahill, David G.; Braun, Paul V.; Chen, Gang; Clarke, David R.; Fan, Shanhui; Goodson, Kenneth E.; Keblinski, Pawel; King, William P.; Mahan, Gerald D.; Majumdar, Arun; Maris, Humphrey J.; Phillpot, Simon R.; Pop, Eric; Shi, Li

    2013-01-01

    A diverse spectrum of technology drivers such as improved thermal barriers, higher efficiency thermoelectric energy conversion, phase-change memory, heat-assisted magnetic recording, thermal management of nanoscale electronics, and nanoparticles for thermal medical therapies are motivating studies of the applied physics of thermal transport at the nanoscale. This review emphasizes developments in experiment, theory, and computation in the past ten years and summarizes the present status of th...

  8. Magnetically assisted bilayer composites for soft bending actuators

    NARCIS (Netherlands)

    Jang, S.H.; Na, Seon Hong; Park, Yong Lae

    2017-01-01

    This article presents a soft pneumatic bending actuator using a magnetically assisted bilayer composite composed of silicone polymer and ferromagnetic particles. Bilayer composites were fabricated by mixing ferromagnetic particles to a prepolymer state of silicone in a mold and asymmetrically

  9. Thermal stability, thermal expansion and grain-growth in exchange-coupled Fe-Pt-Ag-B bulk nanocomposite magnets

    International Nuclear Information System (INIS)

    Nicula, R.; Crisan, O.; Crisan, A.D.; Mercioniu, I.; Stir, M.; Vasiliu, F.

    2015-01-01

    Highlights: • Formation of the L10 FePt hard-magnetic phase (>90%) directly in the as-cast state. • Specific alternating hard/soft nanostructure is stable to 600 °C without grain growth. • Anisotropic and non-linear thermal expansion effects. • The FePtAgB alloy behaves like a single magnetic phase (full exchange coupling). - Abstract: Rare-earth free (RE-free) exchange coupling nanocomposite magnets are intensively studied nowadays due to their potential use in applications demanding stable high-temperature operation and corrosion resistance. In this respect, the FePt alloy system is one of the most actively addressed potential permanent magnet solutions. In FePt alloys, promising magnetic features arise from the co-existence of hard magnetic L1 0 FePt and soft magnetic L1 2 Fe 3 Pt phases emerged from the same metastable precursor. The present work deals with an in-situ temperature-resolved synchrotron radiation study of the thermal stability, thermal expansion and microstructure evolution in exchange-coupled FePtAgB alloys. The as-cast microstructural state as well as the optimized magnetic behavior are given as reference and correlated to the observed microstructural evolution with temperature. The melt-spun Fe 48 Pt 28 Ag 6 B 18 alloy ribbons were examined in situ by synchrotron X-ray powder diffraction from ambient temperature up to 600 °C. The FePt-Fe 3 Pt exchange-coupled microstructure achieved by rapid solidification is not significantly altered during the high temperature exposure. The thermal expansion of the FePt L1 0 unit cell has been found to be strongly anisotropic, being essentially an in-plane expansion which may be seen as an anisotropic invar effect. For the FePt L1 0 phase, a significant deviation from linear thermal expansion is observed at the Curie temperature T C = 477 °C. This non-linear behavior above T C is tentatively linked to a diffusion/segregation mechanism of Ag. The promising hard magnetic properties as well as the

  10. Measurement of thermal properties of magnetic nanoparticles using infrared thermal microscopy

    DEFF Research Database (Denmark)

    Kim, Jae Young; Chang, Ki Soo; Kook, Myung Ho

    2013-01-01

    Magnetic nanoparticles (MNPs) are considered promising for biomedical applications such as hyperthermia treatment and disease diagnosis owing to their distinctive thermal properties. For these applications, it is essential to screen the temperature distribution in the targeted disease site....... This study aimed to investigate and observe the thermal properties of a small amount of MNPs used as highly sensitive biomarkers for disease diagnosis by microthermography. Toward this end, we used polyacrylamide and agarose phantoms containing a small amount of MNPs (30 mg Fe-1). In phantoms, the increasing...

  11. Thermal, magnetic, and structural properties of soft magnetic FeCrNbCuSiB alloy ribbons

    International Nuclear Information System (INIS)

    Rosales-Rivera, A.; Valencia, V.H.; Quintero, D.L.; Pineda-Gomez, P.; Gomez, M.

    2006-01-01

    The thermal, magnetic and structural properties of amorphous magnetic Fe 73.5-x Cr x Nb 3 Cu 1 Si 13.5 B 9 alloy ribbons, with x=0, 2, 4, 6, 8, and 10, were studied by using differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), magneto-impedance measurements and X-ray diffraction (XRD). The ribbons exhibit ultrasoft magnetic behavior, especially giant magneto-impedance effect, GMI. A three-peak behavior was observed in GMI curves. Particular attention has been given to observation of crystallization kinetics via DSC and TGA. The primary crystallization T pcr , and Curie T c , temperatures were determined from DSC and TGA data, respectively. The effect of partial substitution of iron by Cr on the thermal and magnetic properties is discussed

  12. Microwave-assisted shingled magnetic recording simulations on an exchange-coupled composite medium

    Energy Technology Data Exchange (ETDEWEB)

    Tanaka, T., E-mail: t-tanaka@ed.kyushu-u.ac.jp [Department of Electronics, Graduate School of Information Science and Electrical Engineering, Kyushu University, Motoota 744, Nishi-ku, Fukuoka 819-0395 (Japan); Kashiwagi, S. [Department of Electronics, Graduate School of Information Science and Electrical Engineering, Kyushu University, Motoota 744, Nishi-ku, Fukuoka 819-0395 (Japan); Kanai, Y. [Department of Information and Electronics Engineering, Niigata Institute of Technology, Fujihashi 1719, Kashiwazaki, Niigata 945-1195 (Japan); Matsuyama, K. [Department of Electronics, Graduate School of Information Science and Electrical Engineering, Kyushu University, Motoota 744, Nishi-ku, Fukuoka 819-0395 (Japan)

    2016-10-15

    The potential of microwave-assisted magnetic recording combined with the shingled recording scheme has been studied by simulating read/write processes on exchange-coupled composite media focusing on recording characteristics in the cross-track direction. Microwave fields enhance writability, especially at the track edge, resulting in lower noise and higher signal-to-noise ratio (SNR), which enables higher track density in the shingled recording scheme. Read/write simulations of microwave-assisted shingled recording achieve 1.4 Mtracks/in. while retaining high SNR. Further increases in SNR and track density will require either a narrower reader or track edge noise reduction. - Highlights: • Signal recording of shingled magnetic recording using an asymmetric single pole type head combined with a microwave assistance was numerically demonstrated. • Writability is improved by microwave fields with a moderate frequency at the track edge of the shielded side, resulting in higher signal-to-noise ratio. • 1.41 Mtpi of track density is feasible for the recording scheme of shingled magnetic recording with microwave assistance.

  13. Microwave-assisted shingled magnetic recording simulations on an exchange-coupled composite medium

    International Nuclear Information System (INIS)

    Tanaka, T.; Kashiwagi, S.; Kanai, Y.; Matsuyama, K.

    2016-01-01

    The potential of microwave-assisted magnetic recording combined with the shingled recording scheme has been studied by simulating read/write processes on exchange-coupled composite media focusing on recording characteristics in the cross-track direction. Microwave fields enhance writability, especially at the track edge, resulting in lower noise and higher signal-to-noise ratio (SNR), which enables higher track density in the shingled recording scheme. Read/write simulations of microwave-assisted shingled recording achieve 1.4 Mtracks/in. while retaining high SNR. Further increases in SNR and track density will require either a narrower reader or track edge noise reduction. - Highlights: • Signal recording of shingled magnetic recording using an asymmetric single pole type head combined with a microwave assistance was numerically demonstrated. • Writability is improved by microwave fields with a moderate frequency at the track edge of the shielded side, resulting in higher signal-to-noise ratio. • 1.41 Mtpi of track density is feasible for the recording scheme of shingled magnetic recording with microwave assistance.

  14. Thermal conductivity of magnetic insulators with strong spin-orbit coupling

    Science.gov (United States)

    Stamokostas, Georgios; Lapas, Panteleimon; Fiete, Gregory A.

    We study the influence of spin-orbit coupling on the thermal conductivity of various types of magnetic insulators. In the absence of spin-orbit coupling and orbital-degeneracy, the strong-coupling limit of Hubbard interactions at half filling can often be adequately described in terms of a pure spin Hamiltonian of the Heisenberg form. However, in the presence of spin-orbit coupling the resulting exchange interaction can become highly anisotropic. The effect of the atomic spin-orbit coupling, taken into account through the effect of magnon-phonon interactions and the magnetic order and excitations, on the lattice thermal conductivity of various insulating magnetic systems is studied. We focus on the regime of low temperatures where the dominant source of scattering is two-magnon scattering to one-phonon processes. The thermal current is calculated within the Boltzmann transport theory. We are grateful for financial support from NSF Grant DMR-0955778.

  15. Magnetic structure of Fe-based amorphous and thermal annealed microwires

    International Nuclear Information System (INIS)

    Olivera, J.; Provencio, M.; Prida, V.M.; Hernando, B.; Santos, J.D.; Perez, M.J.; Gorria, P.; Sanchez, M.L.; Belzunce, F.J.

    2005-01-01

    The magnetic structure of amorphous and thermal annealed glass coated microwires is studied by thermomagnetic, DSC, and Bitter domain pattern techniques. The long-range dipolar interaction between parallel aligned microwires and the appearance of large Barkhausen jumps steps in the axially magnetized loops are discussed in terms of reversal magnetization process

  16. Spin dynamics and thermal stability in L10 FePt

    Science.gov (United States)

    Chen, Tianran; Toomey, Wahida

    Increasing the data storage density of hard drives remains one of the continuing goals in magnetic recording technology. A critical challenge for increasing data density is the thermal stability of the written information, which drops rapidly as the bit size gets smaller. To maintain good thermal stability in small bits, one should consider materials with high anisotropy energy such as L10 FePt. High anisotropy energy nevertheless implies high coercivity, making it difficult to write information onto the disk. This issue can be overcome by a new technique called heat-assisted magnetic recording, where a laser is used to locally heat the recording medium to reduce its coercivity while retaining relatively good thermal stability. Many of the microscopic magnetic properties of L10 FePt, however, have not been theoretically well understood. In this poster, I will focus on a single L10 FePt grain, typically of a few nanometers. Specifically, I will discuss its critical temperature, size effect and, in particular, spin dynamics in the writing process, a key to the success of heat-assisted magnetic recording. WCU URF16.

  17. Thermal relaxation of magnetic clusters in amorphous Hf57Fe43 alloy

    International Nuclear Information System (INIS)

    Pajic, Damir; Zadro, Kreso; Ristic, Ramir; Zivkovic, Ivica; Skoko, Zeljko; Babic, Emil

    2007-01-01

    The magnetization processes in binary magnetic/non-magnetic amorphous alloy Hf 57 Fe 43 are investigated by the detailed measurement of magnetic hysteresis loops, temperature dependence of magnetization, relaxation of magnetization and magnetic ac susceptibility, including a nonlinear term. Blocking of magnetic moments at lower temperatures is accompanied by the slow relaxation of magnetization and magnetic hysteresis loops. All of the observed properties are explained by the superparamagnetic behaviour of the single domain magnetic clusters inside the non-magnetic host, their blocking by the anisotropy barriers and thermal fluctuation over the barriers accompanied by relaxation of magnetization. From magnetic viscosity analysis based on thermal relaxation over the anisotropy barriers it is found that magnetic clusters occupy the characteristic volume from 25 up to 200 nm 3 . The validity of the superparamagnetic model of Hf 57 Fe 43 is based on the concentration of iron in the Hf 100-x Fe x system that is just below the threshold for long range magnetic ordering. This work also throws more light on the magnetic behaviour of other amorphous alloys

  18. Quantum-memory-assisted entropic uncertainty relation in a Heisenberg XYZ chain with an inhomogeneous magnetic field

    Science.gov (United States)

    Wang, Dong; Huang, Aijun; Ming, Fei; Sun, Wenyang; Lu, Heping; Liu, Chengcheng; Ye, Liu

    2017-06-01

    The uncertainty principle provides a nontrivial bound to expose the precision for the outcome of the measurement on a pair of incompatible observables in a quantum system. Therefore, it is of essential importance for quantum precision measurement in the area of quantum information processing. Herein, we investigate quantum-memory-assisted entropic uncertainty relation (QMA-EUR) in a two-qubit Heisenberg \\boldsymbol{X}\\boldsymbol{Y}\\boldsymbol{Z} spin chain. Specifically, we observe the dynamics of QMA-EUR in a realistic model there are two correlated sites linked by a thermal entanglement in the spin chain with an inhomogeneous magnetic field. It turns out that the temperature, the external inhomogeneous magnetic field and the field inhomogeneity can lift the uncertainty of the measurement due to the reduction of the thermal entanglement, and explicitly higher temperature, stronger magnetic field or larger inhomogeneity of the field can result in inflation of the uncertainty. Besides, it is found that there exists distinct dynamical behaviors of the uncertainty for ferromagnetism \\boldsymbol{}≤ft(\\boldsymbol{J}\\boldsymbol{0}\\right) chains. Moreover, we also verify that the measuring uncertainty is dramatically anti-correlated with the purity of the bipartite spin system, the greater purity can result in the reduction of the measuring uncertainty, vice versa. Therefore, our observations might provide a better understanding of the dynamics of the entropic uncertainty in the Heisenberg spin chain, and thus shed light on quantum precision measurement in the framework of versatile systems, particularly solid states.

  19. Magnetocrystalline anisotropy and its electric-field-assisted switching of Heusler-compound-based perpendicular magnetic tunnel junctions

    International Nuclear Information System (INIS)

    Bai, Zhaoqiang; Wu, Qingyun; Zeng, Minggang; Feng, Yuan Ping; Shen, Lei; Cai, Yongqing; Han, Guchang

    2014-01-01

    Employing density functional theory combined with the non-equilibrium Green's function formalism, we systematically investigate the structural, magnetic and magnetoelectric properties of the Co 2 FeAl(CFA)/MgO interface, as well as the spin-dependent transport characteristics of the CFA/MgO/CFA perpendicular magnetic tunnel junctions (p-MTJs). We find that the structure of the CFA/MgO interface with the oxygen-top FeAl termination has high thermal stability, which is protected by the thermodynamic equilibrium limit. Furthermore, this structure is found to have perpendicular magnetocrystalline anisotropy (MCA). Giant electric-field-assisted modifications of this interfacial MCA through magnetoelectric coupling are demonstrated with an MCA coefficient of up to 10 −7 erg V −1 cm. In addition, our non-collinear spin transport calculations of the CFA/MgO/CFA p-MTJ predict a good magnetoresistance performance of the device. (paper)

  20. Thermally actuated magnetization flux pump in single-grain YBCO bulk

    Energy Technology Data Exchange (ETDEWEB)

    Yan Yu; Li Quan; Coombs, T A, E-mail: yy300@cam.ac.u, E-mail: ql229@cam.ac.u, E-mail: tac1000@cam.ac.u [EPEC Superconductivity Group, Electrical Engineering Department, Cambridge University, 9 J J Thomson Avenue, Cambridge CB3 0FA (United Kingdom)

    2009-10-15

    Recent progress in material processing has proved that high temperature superconductors (HTS) have a great potential to trap large magnetic fields at cryogenic temperatures. For example, HTS are widely used in MRI scanners and in magnetic bearings. However, using traditional ways to magnetize, the YBCO will always need the applied field to be as high as the expected field on the superconductor or much higher than it, leading to a much higher cost than that of using permanent magnets. In this paper, we find a method of YBCO magnetization in liquid nitrogen that only requires the applied field to be at the level of a permanent magnet. Moreover, rather than applying a pulsed high current field on the YBCO, we use a thermally actuated material (gadolinium) as an intermedia and create a travelling magnetic field through it by changing the partial temperature so that the partial permeability is changed to build up the magnetization of the YBCO gradually after multiple pumps. The gadolinium bulk is located between the YBCO and the permanent magnet and is heated and cooled repeatedly from the outer surface to generate a travelling thermal wave inwards. In the subsequent experiment, an obvious accumulation of the flux density is detected on the surface of the YBCO bulk.

  1. Thermally actuated magnetization flux pump in single-grain YBCO bulk

    International Nuclear Information System (INIS)

    Yan Yu; Li Quan; Coombs, T A

    2009-01-01

    Recent progress in material processing has proved that high temperature superconductors (HTS) have a great potential to trap large magnetic fields at cryogenic temperatures. For example, HTS are widely used in MRI scanners and in magnetic bearings. However, using traditional ways to magnetize, the YBCO will always need the applied field to be as high as the expected field on the superconductor or much higher than it, leading to a much higher cost than that of using permanent magnets. In this paper, we find a method of YBCO magnetization in liquid nitrogen that only requires the applied field to be at the level of a permanent magnet. Moreover, rather than applying a pulsed high current field on the YBCO, we use a thermally actuated material (gadolinium) as an intermedia and create a travelling magnetic field through it by changing the partial temperature so that the partial permeability is changed to build up the magnetization of the YBCO gradually after multiple pumps. The gadolinium bulk is located between the YBCO and the permanent magnet and is heated and cooled repeatedly from the outer surface to generate a travelling thermal wave inwards. In the subsequent experiment, an obvious accumulation of the flux density is detected on the surface of the YBCO bulk.

  2. Magnetic Assisted Colloidal Pattern Formation

    Science.gov (United States)

    Yang, Ye

    Pattern formation is a mysterious phenomenon occurring at all scales in nature. The beauty of the resulting structures and myriad of resulting properties occurring in naturally forming patterns have attracted great interest from scientists and engineers. One of the most convenient experimental models for studying pattern formation are colloidal particle suspensions, which can be used both to explore condensed matter phenomena and as a powerful fabrication technique for forming advanced materials. In my thesis, I have focused on the study of colloidal patterns, which can be conveniently tracked in an optical microscope yet can also be thermally equilibrated on experimentally relevant time scales, allowing for ground states and transitions between them to be studied with optical tracking algorithms. In particular, I have focused on systems that spontaneously organize due to particle-surface and particle-particle interactions, paying close attention to systems that can be dynamically adjusted with an externally applied magnetic or acoustic field. In the early stages of my doctoral studies, I developed a magnetic field manipulation technique to quantify the adhesion force between particles and surfaces. This manipulation technique is based on the magnetic dipolar interactions between colloidal particles and their "image dipoles" that appear within planar substrate. Since the particles interact with their own images, this system enables massively parallel surface force measurements (>100 measurements) in a single experiment, and allows statistical properties of particle-surface adhesion energies to be extracted as a function of loading rate. With this approach, I was able to probe sub-picoNewton surface interactions between colloidal particles and several substrates at the lowest force loading rates ever achieved. In the later stages of my doctoral studies, I focused on studying patterns formed from particle-particle interaction, which serve as an experimental model of

  3. Spin torque oscillator for microwave assisted magnetization reversal

    Science.gov (United States)

    Taniguchi, Tomohiro; Kubota, Hitoshi

    2018-05-01

    A theoretical study is given for the self-oscillation excited in a spin torque oscillator (STO) consisting of an in-plane magnetized free layer and a perpendicularly magnetized pinned layer in the presence of a perpendicular magnetic field. This type of STO is a potential candidate for a microwave source of microwave assisted magnetization reversal (MAMR). It is, however, found that the self-oscillation applicable to MAMR disappears when the perpendicular field is larger than a critical value, which is much smaller than a demagnetization field. This result provides a condition that the reversal field of a magnetic recording bit by MAMR in nanopillar structure should be smaller than the critical value. The analytical formulas of currents determining the critical field are obtained, which indicate that a material with a small damping is not preferable to acheive a wide range of the self-oscillation applicable to MAMR, although such a material is preferable from the viewpoint of the reduction of the power consumption.

  4. Thermal activation in statistical clusters of magnetic nanoparticles

    International Nuclear Information System (INIS)

    Hovorka, O

    2017-01-01

    This article presents a kinetic Monte-Carlo study of thermally activated magnetisation dynamics in clusters of statistically distributed magnetic nanoparticles. The structure of clusters is assumed to be of fractal nature, consistently with recent observations of magnetic particle aggregation in cellular environments. The computed magnetisation relaxation decay and frequency-dependent hysteresis loops are seen to significantly depend on the fractal dimension of aggregates, leading to accelerated magnetisation relaxation and reduction in the size of hysteresis loops as the fractal dimension increases from one-dimensional-like to three-dimensional-like clusters. Discussed are implications for applications in nanomedicine, such as magnetic hyperthermia or magnetic particle imaging. (paper)

  5. Magnetically assisted intraperitoneal drug delivery for cancer chemotherapy.

    Science.gov (United States)

    Shamsi, Milad; Sedaghatkish, Amir; Dejam, Morteza; Saghafian, Mohsen; Mohammadi, Mehdi; Sanati-Nezhad, Amir

    2018-11-01

    Intraperitoneal (IP) chemotherapy has revived hopes during the past few years for the management of peritoneal disseminations of digestive and gynecological cancers. Nevertheless, a poor drug penetration is one key drawback of IP chemotherapy since peritoneal neoplasms are notoriously resistant to drug penetration. Recent preclinical studies have focused on targeting the aberrant tumor microenvironment to improve intratumoral drug transport. However, tumor stroma targeting therapies have limited therapeutic windows and show variable outcomes across different cohort of patients. Therefore, the development of new strategies for improving the efficacy of IP chemotherapy is a certain need. In this work, we propose a new magnetically assisted strategy to elevate drug penetration into peritoneal tumor nodules and improve IP chemotherapy. A computational model was developed to assess the feasibility and predictability of the proposed active drug delivery method. The key tumor pathophysiology, including a spatially heterogeneous construct of leaky vasculature, nonfunctional lymphatics, and dense extracellular matrix (ECM), was reconstructed in silico. The transport of intraperitoneally injected magnetic nanoparticles (MNPs) inside tumors was simulated and compared with the transport of free cytotoxic agents. Our results on magnetically assisted delivery showed an order of magnitude increase in the final intratumoral concentration of drug-coated MNPs with respect to free cytotoxic agents. The intermediate MNPs with the radius range of 200-300 nm yield optimal magnetic drug targeting (MDT) performance in 5-10 mm tumors while the MDT performance remains essentially the same over a large particle radius range of 100-500 nm for a 1 mm radius small tumor. The success of MDT in larger tumors (5-10 mm in radius) was found to be markedly dependent on the choice of magnet strength and tumor-magnet distance while these two parameters were less of a concern in small tumors

  6. Magnetic field approaches in dc thermal plasma modelling

    International Nuclear Information System (INIS)

    Freton, P; Gonzalez, J J; Masquere, M; Reichert, Frank

    2011-01-01

    The self-induced magnetic field has an important role in thermal plasma configurations generated by electric arcs as it generates velocity through Lorentz forces. In the models a good representation of the magnetic field is thus necessary. Several approaches exist to calculate the self-induced magnetic field such as the Maxwell-Ampere formulation, the vector potential approach combined with different kinds of boundary conditions or the Biot and Savart (B and S) formulation. The calculation of the self-induced magnetic field is alone a difficult problem and only few papers of the thermal plasma community speak on this subject. In this study different approaches with different boundary conditions are applied on two geometries to compare the methods and their limitations. The calculation time is also one of the criteria for the choice of the method and a compromise must be found between method precision and computation time. The study shows the importance of the current carrying path representation in the electrode on the deduced magnetic field. The best compromise consists of using the B and S formulation on the walls and/or edges of the calculation domain to determine the boundary conditions and to solve the vector potential in a 2D system. This approach provides results identical to those obtained using the B and S formulation over the entire domain but with a considerable decrease in calculation time.

  7. Strain-assisted current-induced magnetization reversal in magnetic tunnel junctions: A micromagnetic study with phase-field microelasticity

    International Nuclear Information System (INIS)

    Huang, H. B.; Hu, J. M.; Yang, T. N.; Chen, L. Q.; Ma, X. Q.

    2014-01-01

    Effect of substrate misfit strain on current-induced in-plane magnetization reversal in CoFeB-MgO based magnetic tunnel junctions is investigated by combining micromagnetic simulations with phase-field microelasticity theory. It is found that the critical current density for in-plane magnetization reversal decreases dramatically with an increasing substrate strain, since the effective elastic field can drag the magnetization to one of the four in-plane diagonal directions. A potential strain-assisted multilevel bit spin transfer magnetization switching device using substrate misfit strain is also proposed.

  8. Influence of coating on nanocrystalline magnetic properties during high temperature thermal ageing

    Energy Technology Data Exchange (ETDEWEB)

    Lekdim, Atef, E-mail: atef.lekdim@univ-lyon1.fr; Morel, Laurent; Raulet, Marie-Ange

    2017-05-15

    Since their birth or mergence the late 1980s, the nanocrystalline ultrasoft magnetic materials are taking a great importance in power electronic systems conception. One of the main advantages that make them more attractive nowadays is their ability to be packaged since the reduction of the magnetostrictive constant to almost zero. In aircraft applications, due to the high component compactness and to their location (for example near the jet engine), the operating temperature increases and may reach easily 200 °C and more. Consequently, the magnetic thermal ageing may occur but is, unfortunately, weakly studied. This paper focuses on the influence of the coating (packaging type) on the magnetic nanocrystalline performances during a thermal ageing. This study is based on monitoring the magnetic characteristics of two types of nanocrystalline cores (naked and coated) during a thermal activated ageing (100, 150 and 200 °C). Based on a dedicated monitoring protocol, a large magnetic characterization has been done and analyzed. Elsewhere, X-Ray Diffraction and magnetostriction measurements were carried out to support the study of the anisotropy energies evolution with ageing. This latter is discussed in this paper to explain and give hypothesis about the ageing phenomena. - Highlights: • The coating impacts drastically the magnetic properties during thermal ageing. • Irreversible ageing phenomena after the total coating breakage. • The deteriorations are related to the storage of the magnetoelastic anisotropy.

  9. Study on the effect of thermal property of metals in ultrasonic-assisted laser machining

    International Nuclear Information System (INIS)

    Lee, Hu Seung; Kim, Gun Woo; Park, Jong Eun; Cho, Sung Hak; Yang, Min Yang; Park, Jong Kweon

    2015-01-01

    The laser machining process has been proposed as an advanced process for the selective fabrication of electrodes without a mask. In this study, we adapt laser machining to metals that have different thermal properties. Based on the results, the metals exhibit a different surface morphology, heat-affected zone (HAZ), and a recast layer around the machined surface according to their thermal conductivity, boiling point, and thermal diffusivity. Then, we apply ultrasonic-assisted laser machining to remove the recast layer. The ultrasonic-assisted laser machining exhibits a better surface quality in metals with higher diffusivity than those having lower diffusivity

  10. A novel magnet focusing plate for matrix-assisted laser desorption/ionization analysis of magnetic bead-bound analytes.

    Science.gov (United States)

    Gode, David; Volmer, Dietrich A

    2013-05-15

    Magnetic beads are often used for serum profiling of peptide and protein biomarkers. In these assays, the bead-bound analytes are eluted from the beads prior to mass spectrometric analysis. This study describes a novel matrix-assisted laser desorption/ionization (MALDI) technique for direct application and focusing of magnetic beads to MALDI plates by means of dedicated micro-magnets as sample spots. Custom-made MALDI plates with magnetic focusing spots were made using small nickel-coated neodymium micro-magnets integrated into a stainless steel plate in a 16 × 24 (384) pattern. For demonstrating the proof-of-concept, commercial C-18 magnetic beads were used for the extraction of a test compound (reserpine) from aqueous solution. Experiments were conducted to study focusing abilities, the required laser energies, the influence of a matrix compound, dispensing techniques, solvent choice and the amount of magnetic beads. Dispensing the magnetic beads onto the micro-magnet sample spots resulted in immediate and strong binding to the magnetic surface. Light microscope images illustrated the homogeneous distribution of beads across the surfaces of the magnets, when the entire sample volume containing the beads was pipetted onto the surface. Subsequent MALDI analysis of the bead-bound analyte demonstrated excellent and reproducible ionization yields. The surface-assisted laser desorption/ionization (SALDI) properties of the strongly light-absorbing γ-Fe2O3-based beads resulted in similar ionization efficiencies to those obtained from experiments with an additional MALDI matrix compound. This feasibility study successfully demonstrated the magnetic focusing abilities for magnetic bead-bound analytes on a novel MALDI plate containing small micro-magnets as sample spots. One of the key advantages of this integrated approach is that no elution steps from magnetic beads were required during analyses compared with conventional bead experiments. Copyright © 2013 John Wiley

  11. Magnet system for a thermal barrier Tandem Mirror Reactor

    International Nuclear Information System (INIS)

    Kim, N.S.; Conn, R.W.

    1981-01-01

    The magnet system for a thermal barrier D-D tandem mirror reactor has been studied as part of the UCLA tandem mirror reactor design study SATYR. Three main considerations in designing the SATYR magnet system are to obtain the desired field strength variation throughout the system, to have proper space for plasma and neutron shielding, and to satisfy the MHD stability to achieve maximum central cell /beta/. Due to the importance and the complexity, the 'internal' field reversal magnet is the main concern in the entire magnet system for SATYR. Two different magnet designs, a non-uniform current density solenoid and a higher-order solenoid, are discussed. Coil levitation for the internal field reversal magnet has been analyzed

  12. Effects of assistant anode on planar inductively coupled magnetized argon plasma in plasma immersion ion implantation

    International Nuclear Information System (INIS)

    Tang, Deli; Chu, Paul K.

    2003-01-01

    The enhancement of planar radio frequency (RF) inductively coupled argon plasma is studied in the presence of an assistant anode and an external magnetic field at low pressure. The influence of the assistant anode and magnetic field on the efficiency of RF power absorption and plasma parameters is investigated. An external axial magnetic field is coupled into the plasma discharge region by an external electromagnetic coil outside the discharge chamber and an assistant cylindrical anode is inserted into the discharge chamber to enhance the plasma discharge. The plasma parameters and density profile are measured by an electrostatic Langmuir probe at different magnetic fields and anode voltages. The RF power absorption by the plasma can be effectively enhanced by the external magnetic field compared with the nonmagnetized discharge. The plasma density can be further increased by the application of a voltage to the assistant anode. Owing to the effective power absorption and enhanced plasma discharge by the assistant anode in a longitudinal magnetic field, the plasma density can be enhanced by more than a factor of two. Meanwhile, the nonuniformity of the plasma density is less than 10% and it can be achieved in a process chamber with a diameter of 600 mm

  13. Thermally tunable magnetic metamaterials at THz frequencies

    International Nuclear Information System (INIS)

    Bui, Son Tung; Nguyen, Van Dung; Bui, Xuan Khuyen; Vu, Dinh Lam; Nguyen, Thanh Tung; Lievens, Peter; Lee, YoungPak

    2013-01-01

    We investigate theoretically and numerically the tunability of the magnetic property of metamaterial in the THz region via thermal control. One component of the meta-atom is InSb, playing an important role as an alterable metal. When the temperature of the InSb stack increases from 300 to 350 K, the resonance peak of the transmission spectra shows a shift from 0.6 to 0.85 THz accompanied by a stronger magnetic behavior. The S-parameter retrieval method realizes the tunability of the negative permeability achieved in the above heating range. (paper)

  14. Spatial Inhomogeneity of Kinetic and Magnetic Dissipations in Thermal Convection

    Energy Technology Data Exchange (ETDEWEB)

    Hotta, H. [Department of Physics, Graduate School of Science, Chiba university, 1-33 Yayoi-cho, Inage-ku, Chiba, 263-8522 (Japan)

    2017-08-20

    We investigate the inhomogeneity of kinetic and magnetic dissipations in thermal convection using high-resolution calculations. In statistically steady turbulence, the injected and dissipated energies are balanced. This means that a large amount of energy is continuously converted into internal energy via dissipation. As in thermal convection, downflows are colder than upflows and the inhomogeneity of the dissipation potentially changes the convection structure. Our investigation of the inhomogeneity of the dissipation shows the following. (1) More dissipation is seen around the bottom of the calculation domain, and this tendency is promoted with the magnetic field. (2) The dissipation in the downflow is much larger than that in the upflow. The dissipation in the downflow is more than 80% of the total at maximum. This tendency is also promoted with the magnetic field. (3) Although 2D probability density functions of the kinetic and magnetic dissipations versus the vertical velocity are similar, the kinetic and magnetic dissipations are not well correlated. Our result suggests that the spatial inhomogeneity of the dissipation is significant and should be considered when modeling a small-scale strong magnetic field generated with an efficient small-scale dynamo for low-resolution calculations.

  15. Magneto-optical effects induced in a magnetic-fluid layer by thermally released supermassive magnetic monopoles

    International Nuclear Information System (INIS)

    Sofonea, V.; Vekas, L.; Hegedues, E.

    1993-01-01

    The number of photons in the optical pulse induced via magneto-optical effects by a thermally released (e.g., from old iron ores) supermassive magnetic monopole traversing a thin magnetic-fluid layer is evaluated on the basis of phenomenological models. In certain monopole search experiments, these effects could give a detectable signal of the order of tens of photons and thus it may serve as a basis for a new magnetic-monopole detection method. (orig.)

  16. Analysis of thermally induced magnetization dynamics in spin-transfer nano-oscillators

    Energy Technology Data Exchange (ETDEWEB)

    D' Aquino, M., E-mail: daquino@uniparthenope.it [Department of Technology, University of Naples ' Parthenope' , 80143 Naples (Italy); Serpico, C. [Department of Engineering, University of Naples Federico II, 80125 Naples (Italy); Bertotti, G. [Istituto Nazionale di Ricerca Metrologica 10135 Torino (Italy); Bonin, R. [Politecnico di Torino - Sede di Verres, 11029 Verres (Aosta) (Italy); Mayergoyz, I.D. [ECE Department and UMIACS, University of Maryland, College Park, MD 20742 (United States)

    2012-05-01

    The thermally induced magnetization dynamics in the presence of spin-polarized currents injected into a spin-valve-like structure used as microwave spin-transfer nano-oscillator (STNO) is considered. Magnetization dynamics is described by the stochastic Landau-Lifshitz-Slonczewski (LLS) equation. First, it is shown that, in the presence of thermal fluctuations, the spectrum of the output signal of the STNO exhibits multiple peaks at low and high frequencies. This circumstance is associated with the occurrence of thermally induced transitions between stationary states and magnetization self-oscillations. Then, a theoretical approach based on the separation of time-scales is developed to obtain a stochastic dynamics only in the slow state variable, namely the energy. The stationary distribution of the energy and the aforementioned transition rates are analytically computed and compared with the results of direct integration of the LLS dynamics, showing very good agreement.

  17. The influence of assist gas on magnetic properties of electrotechnical steel sheets cut with laser

    International Nuclear Information System (INIS)

    Gaworska-Koniarek, Dominika; Szubzda, Bronislaw; Wilczynski, Wieslaw; Drosik, Jerzy; Karas, Kazimierz

    2011-01-01

    The paper presents the influence of assist gas (air and nitrogen) during laser cutting on magnetization, magnetic permeability and loss characteristics of non-oriented electrical steels. The research was made on an non-oriented M330-50A grade electrical steels by means of single sheet tester. In order to enhance the effect of cutting and the same degradation zone on magnetic properties, strips with different width were achieved. Measurements results indicate that application of air as assist gas has more destructive effect on magnetic properties of electrical steels than nitrogen one.

  18. The influence of assist gas on magnetic properties of electrotechnical steel sheets cut with laser

    Science.gov (United States)

    Gaworska-Koniarek, Dominika; Szubzda, Bronisław; Wilczyński, Wiesław; Drosik, Jerzy; Karaś, Kazimierz

    2011-07-01

    The paper presents the influence of assist gas (air and nitrogen) during laser cutting on magnetization, magnetic permeability and loss characteristics of non-oriented electrical steels. The research was made on an non-oriented M330-50A grade electrical steels by means of single sheet tester. In order to enhance the effect of cutting and the same degradation zone on magnetic properties, strips with different width were achieved. Measurements results indicate that application of air as assist gas has more destructive effect on magnetic properties of electrical steels than nitrogen one.

  19. Low Field Magnetic and Thermal Hysteresis in Antiferromagnetic Dysprosium

    Directory of Open Access Journals (Sweden)

    Iuliia Liubimova

    2017-06-01

    Full Text Available Magnetic and thermal hysteresis (difference in magnetic properties on cooling and heating have been studied in polycrystalline Dy (dysprosium between 80 and 250 K using measurements of the reversible Villari effect and alternating current (AC susceptibility. We argue that measurement of the reversible Villari effect in the antiferromagnetic phase is a more sensitive method to detect magnetic hysteresis than the registration of conventional B(H loops. We found that the Villari point, recently reported in the antiferromagnetic phase of Dy at 166 K, controls the essential features of magnetic hysteresis and AC susceptibility on heating from the ferromagnetic state: (i thermal hysteresis in AC susceptibility and in the reversible Villari effect disappears abruptly at the temperature of the Villari point; (ii the imaginary part of AC susceptibility is strongly frequency dependent, but only up to the temperature of the Villari point; (iii the imaginary part of the susceptibility drops sharply also at the Villari point. We attribute these effects observed at the Villari point to the disappearance of the residual ferromagnetic phase. The strong influence of the Villari point on several magnetic properties allows this temperature to be ranked almost as important as the Curie and Néel temperatures in Dy and likely also for other rare earth elements and their alloys.

  20. Heat-Assisted Magnetic Recording: Fundamental Limits to Inverse Electromagnetic Design

    Science.gov (United States)

    Bhargava, Samarth

    In this dissertation, we address the burgeoning fields of diffractive optics, metals-optics and plasmonics, and computational inverse problems in the engineering design of electromagnetic structures. We focus on the application of the optical nano-focusing system that will enable Heat-Assisted Magnetic Recording (HAMR), a higher density magnetic recording technology that will fulfill the exploding worldwide demand of digital data storage. The heart of HAMR is a system that focuses light to a nano- sub-diffraction-limit spot with an extremely high power density via an optical antenna. We approach this engineering problem by first discussing the fundamental limits of nano-focusing and the material limits for metal-optics and plasmonics. Then, we use efficient gradient-based optimization algorithms to computationally design shapes of 3D nanostructures that outperform human designs on the basis of mass-market product requirements. In 2014, the world manufactured ˜1 zettabyte (ZB), ie. 1 Billion terabytes (TBs), of data storage devices, including ˜560 million magnetic hard disk drives (HDDs). Global demand of storage will likely increase by 10x in the next 5-10 years, and manufacturing capacity cannot keep up with demand alone. We discuss the state-of-art HDD and why industry invented Heat-Assisted Magnetic Recording (HAMR) to overcome the data density limitations. HAMR leverages the temperature sensitivity of magnets, in which the coercivity suddenly and non-linearly falls at the Curie temperature. Data recording to high-density hard disks can be achieved by locally heating one bit of information while co-applying a magnetic field. The heating can be achieved by focusing 100 microW of light to a 30nm diameter spot on the hard disk. This is an enormous light intensity, roughly ˜100,000,000x the intensity of sunlight on the earth's surface! This power density is ˜1,000x the output of gold-coated tapered optical fibers used in Near-field Scanning Optical Microscopes

  1. Anomalous magnetic aftereffect and thermal remagnetization in melt-spun Nd4 Fe77 B19 permanent magnets

    International Nuclear Information System (INIS)

    Mueller, K.H.; Eckert, D.; Handstein, A.; Wolf, M.; Collocott, S.; Andrikidis, C.

    1996-01-01

    Usually measurements of the magnetic after effect in permanent magnet materials are performed on the major demagnetization curve. In this investigation, however, we measured the time dependence of magnetization of the spring magnet Nd 4 Fe 77 B 19 for different magnetic pre histories. The measurements were done with SQUID magnetometers. Depending on the magnetic pre history the magnetic viscosity S can be positive as well as negative, even for the same 'coordinate' (J,H), i.e. the system does not always move directly towards the thermal equilibrium state. In particular the samples spontaneously remagnetize after being field demagnetized. The driving force for this effect may be similar as that for thermal remagnetization. For certain magnetic pre histories the magnetization J (t) depends non-monotonically on time t, i.e. it can not always be described by a formula S 1 n(1 + t/t o ). Similar effects observed for αFe, many years ago, have been called anomalous aftereffect. These observations were attributed to the reversible aftereffect associated with the diffusion of C-atoms in α-Fe. However, the reversible aftereffect is not typical for permanent magnet materials. THe anomalous aftereffect found in our investigation as well as the effects of spontaneous remagnetization will be explained in terms of magnetic interactions in the material. (author)

  2. Processing of baby food using pressure-assisted thermal sterilization (PATS) and comparison with thermal treatment

    Science.gov (United States)

    Wang, Yubin; Ismail, Marliya; Farid, Mohammed

    2017-10-01

    Currently baby food is sterilized using retort processing that gives an extended shelf life. However, this type of heat processing leads to reduction of organoleptic and nutrition value. Alternatively, the combination of pressure and heat could be used to achieve sterilization at reduced temperatures. This study investigates the potential of pressure-assisted thermal sterilization (PATS) technology for baby food sterilization. Here, baby food (apple puree), inoculated with Bacillus subtilis spores was treated using PATS at different operating temperatures, pressures and times and was compared with thermal only treatment. The results revealed that the decimal reduction time of B. subtilis in PATS treatment was lower than that of thermal only treatment. At a similar spore inactivation, the retention of ascorbic acid of PATS-treated sample was higher than that of thermally treated sample. The results indicated that PATS could be a potential technology for baby food processing while minimizing quality deterioration.

  3. Rapid magnetic hardening by rapid thermal annealing in NdFeB-based nanocomposites

    Energy Technology Data Exchange (ETDEWEB)

    Chu, K.-T.; Jin, Z Q; Chakka, Vamsi M; Liu, J P [Department of Physics, University of Texas at Arlington, Arlington, TX 76019 (United States)

    2005-11-21

    A systematic study of heat treatments and magnetic hardening of NdFeB-based melt-spun nanocomposite ribbons have been carried out. Comparison was made between samples treated by rapid thermal annealing and by conventional furnace annealing. Heating rates up to 200 K s{sup -1} were adopted in the rapid thermal processing. It was observed that magnetic hardening can be realized in an annealing time as short as 1 s. Coercivity of 10.2 kOe in the nanocomposites has been obtained by rapid thermal annealing for 1 s, and prolonged annealing did not give any increase in coercivity. Detailed results on the effects of annealing time, temperature and heating rate have been obtained. The dependence of magnetic properties on the annealing parameters has been investigated. Structural characterization revealed that there is a close correlation between magnetic hardening and nanostructured morphology. The coercivity mechanism was also studied by analysing the magnetization minor loops.

  4. Thermal and magnetic hysteresis associated with martensitic and magnetic phase transformations in Ni52Mn25In16Co7 Heusler alloy

    Science.gov (United States)

    Madiligama, A. S. B.; Ari-Gur, P.; Ren, Y.; Koledov, V. V.; Dilmieva, E. T.; Kamantsev, A. P.; Mashirov, A. V.; Shavrov, V. G.; Gonzalez-Legarreta, L.; Grande, B. H.

    2017-11-01

    Ni-Mn-In-Co Heusler alloys demonstrate promising magnetocaloric performance for use as refrigerants in magnetic cooling systems with the goal of replacing the lower efficiency, eco-adverse fluid-compression technology. The largest change in entropy occurs when the applied magnetic field causes a merged structural and magnetic transformation and the associated entropy changes of the two transformations works constructively. In this study, magnetic and crystalline phase transformations were each treated separately and the effects of the application of magnetic field on thermal hystereses associated with both structural and magnetic transformations of the Ni52Mn25In16Co7 were studied. From the analysis of synchrotron diffraction data and thermomagnetic measurements, it was revealed that the alloy undergoes both structural (from cubic austenite to a mixture of 7M &5M modulated martensite) and magnetic (ferromagnetic to a low-magnetization phase) phase transformations. Thermal hysteresis is associated with both transformations, and the variation of the thermal hystereses of the magnetic and structural transformations with applied magnetic field is significantly different. Because of the differences between the hystereses loops of the two transformations, they merge only upon heating under a certain magnetic field.

  5. Novel Magnetic-to-Thermal Conversion and Thermal Energy Management Composite Phase Change Material

    Directory of Open Access Journals (Sweden)

    Xiaoqiao Fan

    2018-05-01

    Full Text Available Superparamagnetic materials have elicited increasing interest due to their high-efficiency magnetothermal conversion. However, it is difficult to effectively manage the magnetothermal energy due to the continuous magnetothermal effect at present. In this study, we designed and synthesized a novel Fe3O4/PEG/SiO2 composite phase change material (PCM that can simultaneously realize magnetic-to-thermal conversion and thermal energy management because of outstanding thermal energy storage ability of PCM. The composite was fabricated by in situ doping of superparamagnetic Fe3O4 nanoclusters through a simple sol–gel method. The synthesized Fe3O4/PEG/SiO2 PCM exhibited good thermal stability, high phase change enthalpy, and excellent shape-stabilized property. This study provides an additional promising route for application of the magnetothermal effect.

  6. Improved magnetic properties and thermal stabilities of Pr-Nd-Fe-B sintered magnets by Hf addition

    Science.gov (United States)

    Jiang, Qingzheng; Lei, Weikai; Zeng, Qingwen; Quan, Qichen; Zhang, Lili; Liu, Renhui; Hu, Xianjun; He, Lunke; Qi, Zhiqi; Ju, Zhihua; Zhong, Minglong; Ma, Shengcan; Zhong, Zhenchen

    2018-05-01

    Nd2Fe14B-type permanent magnets have been widely applied in various fields such as wind power, voice coil motors, and medical instruments. The large temperature dependence of coercivity, however, limits their further applications. We have systematically investigated the magnetic properties, thermal stabilities and coercivity mechanisms of the (Pr0.2Nd0.8)13Fe81-xB6Hfx (x=0, 0.5) nanocrystalline magnets fabricated by a spark plasma sintering (SPS) technique. The results indicate that the influence of Hf addition is significant on magnetic properties and thermal stabilities of the (PrNd)2Fe14B-type sintered magnets. It is shown that the sample with x = 0.5 at 300 K has much higher coercivity and remanent magnetization than those counterparts without Hf. The temperature coefficients of remanence (α) and coercivity (β) of the (Pr0.2Nd0.8)13Fe81-xB6Hfx magnets are improved significantly from -0.23 %/K, -0.57 %/K for the sample at x = 0 to -0.17 %/K, -0.49 %/K for the sample at x = 0.5 in the temperature range of 300-400 K. Furthermore, it is found out that the domain wall pinning mechanism is more likely responsible for enhancing the coercivity of the (Pr0.2Nd0.8)13Fe81-xB6Hfx magnets.

  7. Micromagnetics of thermally activated switching in nonuniformly magnetized nanodots

    International Nuclear Information System (INIS)

    Torres, L.; Lopez-Diaz, L.; Moro, E.; Francisco, C. de; Alejos, O.

    2001-01-01

    Patterned magnetic elements are being proposed as media for the future ultrahigh density storage systems. The equilibrium states of different patterned magnetic dots at zero temperature have been studied in numerous micromagnetic works while in the last year some studies have begun to include the effect of temperature in the computations. In this research a stochastic dynamic micromagnetic study is carried out for rectangular magnetic dots with size 10 by 3.1 times the exchange length, patterned in a film with a thickness of 5 times the exchange length. Two kinds of nonuniform magnetized nanodots are studied in detail: those in which the state prior to the switching follows the shape of a 'C' and those following an 'S'. In both cases a field near to the zero-temperature switching field is applied and then the thermally activated switching is observed. The dependence of the switching time on temperature is analyzed. It is observed how for the 'C' configuration an Arrhenius-like behavior is obtained in a large temperature window while this is not the case for the 'S' configuration. The micromagnetic structure of the switching thermally activated modes leading to these behaviors is also studied

  8. Radial thermal diffusivity of toroidal plasma affected by resonant magnetic perturbations

    International Nuclear Information System (INIS)

    Kanno, Ryutaro; Nunami, Masanori; Satake, Shinsuke; Takamaru, Hisanori; Okamoto, Masao

    2012-04-01

    We investigate how the radial thermal diffusivity of an axisymmetric toroidal plasma is modified by effect of resonant magnetic perturbations (RMPs), using a drift kinetic simulation code for calculating the thermal diffusivity in the perturbed region. The perturbed region is assumed to be generated on and around the resonance surfaces, and is wedged in between the regular closed magnetic surfaces. It has been found that the radial thermal diffusivity χ r in the perturbed region is represented as χ r = χ r (0) {1 + c r parallel 2 >}. Here r parallel 2 > 1/2 is the strength of the RMPs in the radial directions, means the flux surface average defined by the unperturbed (i.e., original) magnetic field, χ r (0) is the neoclassical thermal diffusivity, and c is a positive coefficient. In this paper, dependence of the coefficient c on parameters of the toroidal plasma is studied in results given by the δ f simulation code solving the drift kinetic equation under an assumption of zero electric field. We find that the dependence of c is given as c ∝ ω b /ν eff m in the low collisionality regime ν eff b , where ν eff is the effective collision frequency, ω b is the bounce frequency and m is the particle mass. In case of ν eff > ω b , the thermal diffusivity χ r evaluated by the simulations becomes close to the neoclassical thermal diffusivity χ r (0) . (author)

  9. Probe branes thermalization in external electric and magnetic fields

    International Nuclear Information System (INIS)

    Ali-Akbari, M.; Ebrahim, H.; Rezaei, Z.

    2014-01-01

    We study thermalization on rotating probe branes in AdS 5 ×S 5 background in the presence of constant external electric and magnetic fields. In the AdS/CFT framework this corresponds to thermalization in the flavour sector in field theory. The horizon appears on the worldvolume of the probe brane due to its rotation in one of the sphere directions. For both electric and magnetic fields the behaviour of the temperature is independent of the probe brane dimension. We also study the open string metric and the fluctuations of the probe brane in such a set-up. We show that the temperatures obtained from open string metric and observed by the fluctuations are larger than the one calculated from the induced metric

  10. Thermal effect on magnetic parameters of high-coercivity cobalt ferrite

    Energy Technology Data Exchange (ETDEWEB)

    Chagas, E. F., E-mail: efchagas@fisica.ufmt.br; Ponce, A. S.; Prado, R. J.; Silva, G. M. [Instituto de Física, Universidade Federal de Mato Grosso, 78060-900 Cuiabá-MT (Brazil); Bettini, J. [Laboratório Nacional de Nanotecnologia, Centro Nacional de Pesquisa em Energia e Materiais, 13083-970 Campinas (Brazil); Baggio-Saitovitch, E. [Centro Brasileiro de Pesquisas Físicas, Rua Xavier Sigaud 150 Urca. Rio de Janeiro (Brazil)

    2014-07-21

    We prepared very high-coercivity cobalt ferrite nanoparticles synthesized by a combustion method and using short-time high-energy mechanical milling to increase strain and the structural defects density. The coercivity (H{sub C}) of the milled sample reached 3.75 kOe—a value almost five times higher than that obtained for the non-milled material (0.76 kOe). To investigate the effect of the temperature on the magnetic behavior of the milled sample, we performed a thermal treatment on the milled sample at 300, 400, and 600 °C for 30 and 180 min. We analyzed the changes in the magnetic behavior of the nanoparticles due to the thermal treatment using the hysteresis curves, Williamson-Hall analysis, and transmission electron microscopy. The thermal treatment at 600 °C causes decreases in the microstructural strain and density of structural defects resulting in a significant decrease in H{sub C}. Furthermore, this thermal treatment increases the size of the nanoparticles and, as a consequence, there is a substantial increase in the saturation magnetization (M{sub S}). The H{sub C} of the samples treated at 600 °C for 30 and 180 min were 2.24 and 1.93 kOe, respectively, and the M{sub S} of these same samples increased from 57 emu/g to 66 and 70 emu/g, respectively. The H{sub C} and the M{sub S} are less affected by the thermal treatment at 300 and 400 °C.

  11. Gap-mode-assisted light-induced switching of sub-wavelength magnetic domains

    Science.gov (United States)

    Scheunert, G.; McCarron, R.; Kullock, R.; Cohen, S. R.; Rechav, K.; Kaplan-Ashiri, I.; Bitton, O.; Hecht, B.; Oron, D.

    2018-04-01

    Creating sub-micron hotspots for applications such as heat-assisted magnetic recording (HAMR) is a challenging task. The most common approach relies on a surface-plasmon resonator (SPR), whose design dictates the size of the hotspot to always be larger than its critical dimension. Here, we present an approach which circumvents known geometrical restrictions by resorting to electric field confinement via excitation of a gap-mode (GM) between a comparatively large Gold (Au) nano-sphere (radius of 100 nm) and the magnetic medium in a grazing-incidence configuration. Operating a λ=785 nm laser, sub-200 nm hot spots have been generated and successfully used for GM-assisted magnetic switching on commercial CoCrPt perpendicular magnetic recording media at laser powers and pulse durations comparable to SPR-based HAMR. Lumerical electric field modelling confirmed that operating in the near-infrared regime presents a suitable working point where most of the light's energy is deposited in the magnetic layer, rather than in the nano-particle. Further, modelling is used for predicting the limits of our method which, in theory, can yield sub-30 nm hotspots for Au nano-sphere radii of 25-50 nm for efficient heating of FePt recording media with a gap of 5 nm.

  12. Thermal diffusivity of diamond nanowires studied by laser assisted atom probe tomography

    Science.gov (United States)

    Arnoldi, L.; Spies, M.; Houard, J.; Blum, I.; Etienne, A.; Ismagilov, R.; Obraztsov, A.; Vella, A.

    2018-04-01

    The thermal properties of single-crystal diamond nanowires (NWs) have been calculated from first principles but have never been measured experimentally. Taking advantage of the sharp geometry of samples analyzed in a laser assisted atom probe, this technique is used to measure the thermal diffusivity of a single NW at low temperature (ab-initio calculations and confirms that thermal diffusivity in nanoscale samples is lower than in bulk samples. The results impact the design and integration of diamond NWs and nanoneedles in nanoscale devices for heat dissipation.

  13. Computational micromagnetics: prediction of time dependent and thermal properties

    International Nuclear Information System (INIS)

    Schrefl, T.; Scholz, W.; Suess, Dieter; Fidler, J.

    2001-01-01

    Finite element modeling treats magnetization processes on a length scale of several nanometers and thus gives a quantitative correlation between the microstructure and the magnetic properties of ferromagnetic materials. This work presents a novel finite element/boundary element micro-magnetics solver that combines a wavelet-based matrix compression technique for magnetostatic field calculations with a BDF/GMRES method for the time integration of the Gilbert equation of motion. The simulations show that metastable energy minima and nonuniform magnetic states within the grains are important factors in the reversal dynamics at finite temperature. The numerical solution of the Gilbert equation shows how reversed domains nucleate and expand. The switching time of submicron magnetic elements depends on the shape of the elements. Elements with slanted ends decrease the overall reversal time, as a transverse demagnetizing field suppresses oscillations of the magnetization. Thermal activated processes can be included adding a random thermal field to the effective magnetic field. Thermally assisted reversal was studied for CoCrPtTa thin-film media

  14. The Solar Thermal Design Assistance Center report of its activities and accomplishments in Fiscal Year 1993

    Energy Technology Data Exchange (ETDEWEB)

    Menicucci, D.F.

    1994-03-01

    The Solar Thermal Design Assistance Center (STDAC) at Sandia National Laboratories is a resource provided by the US Department of Energy`s Solar Thermal Program. Its major objectives are to accelerate the use of solar thermal systems through (a) direct technical assistance to users, (b) cooperative test, evaluation, and development efforts with private industry, and (c) educational outreach activities. This report outlines the major activities and accomplishments of the STDAC in Fiscal Year 1993. The report also contains a comprehensive list of persons who contacted the STDAC by telephone for information or technical consulting.

  15. Magnetic nanocomposites based on phosphorus-containing polymers—structural characterization and thermal analysis

    Science.gov (United States)

    Alosmanov, R. M.; Szuwarzyński, M.; Schnelle-Kreis, J.; Matuschek, G.; Magerramov, A. M.; Azizov, A. A.; Zimmermann, R.; Zapotoczny, S.

    2018-04-01

    Fabrication of magnetic nanocomposites containing iron oxide nanoparticles formed in situ within a phosphorus-containing polymer matrix as well as its structural characterization and its thermal degradation is reported here. Comparative structural studies of the parent polymer and nanocomposites were performed using FTIR spectroscopy, x-ray diffraction, and atomic force microscopy. The results confirmed the presence of dispersed iron oxide magnetic nanoparticles in the polymer matrix. The formed composite combines the properties of porous polymer carriers and magnetic particles enabling easy separation and reapplication of such polymeric carriers used in, for example, catalysis or environmental remediation. Studies on thermal degradation of the composites revealed that the process proceeds in three stages while a significant influence of the embedded magnetic particles on that process was observed in the first two stages. Magnetic force microscopy studies revealed that nanocomposites and its calcinated form have strong magnetic properties. The obtained results provide a comprehensive characterization of magnetic nanocomposites and the products of their calcination that are important for their possible applications as sorbents (regeneration conditions, processing temperature, disposal, etc).

  16. Thermal analysis of the cryocooled superconducting magnet for the liquid helium-free hybrid magnet

    International Nuclear Information System (INIS)

    Ishizuka, Masayuki; Hamajima, Takataro; Itou, Tomoyuki; Sakuraba, Junji; Nishijima, Gen; Awaji, Satoshi; Watanabe, Kazuo

    2010-01-01

    The liquid helium-free hybrid magnet, which consists of an outer large bore cryocooled superconducting magnet and an inner water-cooled resistive magnet, was developed for magneto-science in high fields. The characteristic features of the cryogen-free outsert superconducting magnet are described in detail in this paper. The superconducting magnet cooled by Gifford-McMahon cryocoolers, which has a 360 mm room temperature bore in diameter, was designed to generate high magnetic fields up to 10 T. The hybrid magnet has generated the magnetic field of 27.5 T by combining 8.5 T generation of the cryogen-free superconducting magnet with 19 T generation of the water-cooled resistive magnet. The superconducting magnet was composed of inner Nb 3 Sn coils and outer NbTi coils. In particular, inner Nb 3 Sn coils were wound using high-strength CuNi-NbTi/Nb 3 Sn wires in consideration of large hoop stress. Although the cryocooled outsert superconducting magnet achieved 9.5 T, we found that the outsert magnet has a thermal problem to generate the designed maximum field of 10 T in the hybrid magnet operation. This problem is associated with unexpected AC losses in Nb 3 Sn wires.

  17. HELIOSEISMIC HOLOGRAPHY OF SIMULATED SUNSPOTS: MAGNETIC AND THERMAL CONTRIBUTIONS TO TRAVEL TIMES

    Energy Technology Data Exchange (ETDEWEB)

    Felipe, T. [Departamento de Astrofísica, Universidad de La Laguna, E-38205 La Laguna, Tenerife (Spain); Braun, D. C.; Crouch, A. D. [NorthWest Research Associates, Colorado Research Associates, Boulder, CO 80301 (United States); Birch, A. C., E-mail: tobias@iac.es [Max-Planck-Institut für Sonnensystemforschung, Justus-von-Liebig-Weg 3, D-37077 Göttingen (Germany)

    2016-10-01

    Wave propagation through sunspots involves conversion between waves of acoustic and magnetic character. In addition, the thermal structure of sunspots is very different than that of the quiet Sun. As a consequence, the interpretation of local helioseismic measurements of sunspots has long been a challenge. With the aim of understanding these measurements, we carry out numerical simulations of wave propagation through sunspots. Helioseismic holography measurements made from the resulting simulated wavefields show qualitative agreement with observations of real sunspots. We use additional numerical experiments to determine, separately, the influence of the thermal structure of the sunspot and the direct effect of the sunspot magnetic field. We use the ray approximation to show that the travel-time shifts in the thermal (non-magnetic) sunspot model are primarily produced by changes in the wave path due to the Wilson depression rather than variations in the wave speed. This shows that inversions for the subsurface structure of sunspots must account for local changes in the density. In some ranges of horizontal phase speed and frequency there is agreement (within the noise level in the simulations) between the travel times measured in the full magnetic sunspot model and the thermal model. If this conclusion proves to be robust for a wide range of models, it would suggest a path toward inversions for sunspot structure.

  18. HELIOSEISMIC HOLOGRAPHY OF SIMULATED SUNSPOTS: MAGNETIC AND THERMAL CONTRIBUTIONS TO TRAVEL TIMES

    International Nuclear Information System (INIS)

    Felipe, T.; Braun, D. C.; Crouch, A. D.; Birch, A. C.

    2016-01-01

    Wave propagation through sunspots involves conversion between waves of acoustic and magnetic character. In addition, the thermal structure of sunspots is very different than that of the quiet Sun. As a consequence, the interpretation of local helioseismic measurements of sunspots has long been a challenge. With the aim of understanding these measurements, we carry out numerical simulations of wave propagation through sunspots. Helioseismic holography measurements made from the resulting simulated wavefields show qualitative agreement with observations of real sunspots. We use additional numerical experiments to determine, separately, the influence of the thermal structure of the sunspot and the direct effect of the sunspot magnetic field. We use the ray approximation to show that the travel-time shifts in the thermal (non-magnetic) sunspot model are primarily produced by changes in the wave path due to the Wilson depression rather than variations in the wave speed. This shows that inversions for the subsurface structure of sunspots must account for local changes in the density. In some ranges of horizontal phase speed and frequency there is agreement (within the noise level in the simulations) between the travel times measured in the full magnetic sunspot model and the thermal model. If this conclusion proves to be robust for a wide range of models, it would suggest a path toward inversions for sunspot structure.

  19. Ordering and thermal excitations in dipolar coupled single domain magnet arrays (Presentation Recording)

    Science.gov (United States)

    Östman, Erik; Arnalds, Unnar; Kapaklis, Vassilios; Hjörvarsson, Björgvin

    2015-09-01

    For a small island of a magnetic material the magnetic state of the island is mainly determined by the exchange interaction and the shape anisotropy. Two or more islands placed in close proximity will interact through dipolar interactions. The state of a large system will thus be dictated by interactions at both these length scales. Enabling internal thermal fluctuations, e.g. by the choice of material, of the individual islands allows for the study of thermal ordering in extended nano-patterned magnetic arrays [1,2]. As a result nano-magnetic arrays represent an ideal playground for the study of physical model systems. Here we present three different studies all having used magneto-optical imaging techniques to observe, in real space, the order of the systems. The first study is done on a square lattice of circular islands. The remanent magnetic state of each island is a magnetic vortex structure and we can study the temperature dependence of the vortex nucleation and annihilation fields [3]. The second are long chains of dipolar coupled elongated islands where the magnetization direction in each island only can point in one of two possible directions. This creates a system which in many ways mimics the Ising model [4] and we can relate the correlation length to the temperature. The third one is a spin ice system where elongated islands are placed in a square lattice. Thermal excitations in such systems resemble magnetic monopoles [2] and we can investigate their properties as a function of temperature and lattice parameters. [1] V. Kapaklis et al., New J. Phys. 14, 035009 (2012) [2] V. Kapaklis et al., Nature Nanotech 9, 514(2014) [3] E. Östman et al.,New J. Phys. 16, 053002 (2014) [4] E. Östman et al.,Thermal ordering in mesoscopic Ising chains, In manuscript.

  20. Efficient Solar-Thermal Energy Harvest Driven by Interfacial Plasmonic Heating-Assisted Evaporation.

    Science.gov (United States)

    Chang, Chao; Yang, Chao; Liu, Yanming; Tao, Peng; Song, Chengyi; Shang, Wen; Wu, Jianbo; Deng, Tao

    2016-09-07

    The plasmonic heating effect of noble nanoparticles has recently received tremendous attention for various important applications. Herein, we report the utilization of interfacial plasmonic heating-assisted evaporation for efficient and facile solar-thermal energy harvest. An airlaid paper-supported gold nanoparticle thin film was placed at the thermal energy conversion region within a sealed chamber to convert solar energy into thermal energy. The generated thermal energy instantly vaporizes the water underneath into hot vapors that quickly diffuse to the thermal energy release region of the chamber to condense into liquids and release the collected thermal energy. The condensed water automatically flows back to the thermal energy conversion region under the capillary force from the hydrophilic copper mesh. Such an approach simultaneously realizes efficient solar-to-thermal energy conversion and rapid transportation of converted thermal energy to target application terminals. Compared to conventional external photothermal conversion design, the solar-thermal harvesting device driven by the internal plasmonic heating effect has reduced the overall thermal resistance by more than 50% and has demonstrated more than 25% improvement of solar water heating efficiency.

  1. Predicting thermal history a-priori for magnetic nanoparticle hyperthermia of internal carcinoma

    Science.gov (United States)

    Dhar, Purbarun; Sirisha Maganti, Lakshmi

    2017-08-01

    This article proposes a simplistic and realistic method where a direct analytical expression can be derived for the temperature field within a tumour during magnetic nanoparticle hyperthermia. The approximated analytical expression for thermal history within the tumour is derived based on the lumped capacitance approach and considers all therapy protocols and parameters. The present method is simplistic and provides an easy framework for estimating hyperthermia protocol parameters promptly. The model has been validated with respect to several experimental reports on animal models such as mice/rabbit/hamster and human clinical trials. It has been observed that the model is able to accurately estimate the thermal history within the carcinoma during the hyperthermia therapy. The present approach may find implications in a-priori estimation of the thermal history in internal tumours for optimizing magnetic hyperthermia treatment protocols with respect to the ablation time, tumour size, magnetic drug concentration, field strength, field frequency, nanoparticle material and size, tumour location, and so on.

  2. Thermal Analysis of NR Composite with MWCNTs Aligned in a Magnetic Field

    Directory of Open Access Journals (Sweden)

    Jin Xu

    2015-01-01

    Full Text Available We got the aligned carbon tube in the rubber matrix through magnetic field. TEM shows that Fe3O4 is symmetrically coated on the outer surface of MWCNTs. Diffraction peaks corresponding to Fe3O4 cubic crystal also appeared in the X-ray diffraction spectra. Thermal conductivity of composites increases by filling the appropriate content of carbon tube. If the magnetic field is larger and the direction time is longer, a greater thermal conductivity of composites can be obtained.

  3. Thermal fluctuations and critical behavior in a magnetized, anisotropic plasma

    International Nuclear Information System (INIS)

    Hazeltine, R. D.; Mahajan, S. M.

    2013-01-01

    Thermal fluctuations in a magnetized, anisotropic plasma are studied by applying standard methods, based on the Einstein rule, to the known thermodynamic potential of the system. It is found in particular that magnetic fluctuations become critical when the anisotropy p ∥ −p ⊥ changes sign. By examining the critical region, additional insight on the equations of state for near-critical anisotropic plasma is obtained

  4. Use of fusion-welding techniques in fabrication of a superconducting-magnet thermal-shield system

    International Nuclear Information System (INIS)

    Dalder, E.N.C.; Berkey, J.H.; Chang, Y.; Johnson, G.L.; Lathrop, G.H.; Podesta, D.L.; Van Sant, J.H.

    1983-01-01

    Success of the thermal shield system was demonstrated by the results of acceptance tests performed with the magnet and all its ancillary equipment. During these tests the thermal shield system was: (1) thermally cycled several times from 300 0 K to 77 0 K; (2) pressure cycled several times from 0 to 5 atmospheres; (3) operated for more than 500 hours at 77 0 K and in a vacuum environment of less than 10 - 5 torr; (4) operated in a magnetic field up to 6.0 Telsa; (5) exposed to a rapidly collapsing magnetic field of more than 250 gauss per second; (6) drained of all LN 2 in a few minutes, without any weld failures. The successful (and relatively problem free) operation of the magnet system validates the choice of the welding processes used, as well as their execution in both shop and field environments

  5. THE INFLUENCE OF THERMAL EVOLUTION IN THE MAGNETIC PROTECTION OF TERRESTRIAL PLANETS

    Energy Technology Data Exchange (ETDEWEB)

    Zuluaga, Jorge I.; Bustamante, Sebastian; Cuartas, Pablo A. [Instituto de Fisica-FCEN, Universidad de Antioquia, Calle 67 No. 53-108, Medellin (Colombia); Hoyos, Jaime H., E-mail: jzuluaga@fisica.udea.edu.co, E-mail: sbustama@pegasus.udea.edu.co, E-mail: p.cuartas@fisica.udea.edu.co, E-mail: jhhoyos@udem.edu.co [Departamento de Ciencias Basicas, Universidad de Medellin, Carrera 87 No. 30-65, Medellin (Colombia)

    2013-06-10

    Magnetic protection of potentially habitable planets plays a central role in determining their actual habitability and/or the chances of detecting atmospheric biosignatures. Here we develop a thermal evolution model of potentially habitable Earth-like planets and super-Earths (SEs). Using up-to-date dynamo-scaling laws, we predict the properties of core dynamo magnetic fields and study the influence of thermal evolution on their properties. The level of magnetic protection of tidally locked and unlocked planets is estimated by combining simplified models of the planetary magnetosphere and a phenomenological description of the stellar wind. Thermal evolution introduces a strong dependence of magnetic protection on planetary mass and rotation rate. Tidally locked terrestrial planets with an Earth-like composition would have early dayside magnetopause distances between 1.5 and 4.0 R{sub p} , larger than previously estimated. Unlocked planets with periods of rotation {approx}1 day are protected by magnetospheres extending between 3 and 8 R{sub p} . Our results are robust in comparison with variations in planetary bulk composition and uncertainties in other critical model parameters. For illustration purposes, the thermal evolution and magnetic protection of the potentially habitable SEs GL 581d, GJ 667Cc, and HD 40307g were also studied. Assuming an Earth-like composition, we found that the dynamos of these planets are already extinct or close to being shut down. While GL 581d is the best protected, the protection of HD 40307g cannot be reliably estimated. GJ 667Cc, even under optimistic conditions, seems to be severely exposed to the stellar wind, and, under the conditions of our model, has probably suffered massive atmospheric losses.

  6. Processing of magnetically anisotropic MnBi particles by surfactant assisted ball milling

    Energy Technology Data Exchange (ETDEWEB)

    Kanari, K. [Department of Physics, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Sarafidis, C., E-mail: hsara@physics.auth.gr [Department of Physics, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Gjoka, M.; Niarchos, D. [INN, NCSR Demokritos, Athens 15310 (Greece); Kalogirou, O. [Department of Physics, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece)

    2017-03-15

    MnBi particles are obtained from bulk MnBi using mechanochemical processing. The structure and magnetic properties of the MnBi particles are investigated by means of X-ray diffraction analysis, scanning electron microscopy and magnetometry. Surfactant assisted high energy ball milling results to the samples’ degradation even after one hour of milling. In the case of surfactant assisted low energy ball milling the increase of ball milling duration decreases the average particle size while the particles seem to be more separated. The saturation magnetization (M{sub s}) was found to decrease for large milling times beginning from 61 Am{sup 2}/kg, while the coercivity (μ{sub 0}H{sub c}) increases with the increase of ball milling duration up to 35 min where it reaches 1.62 T and thereafter it decreases. - Highlights: • Effect of surfactants in processing of MnBi. • Magnetization degradation due to air storage and due to processing. • Coercivity of 1.6 T in epoxy resin oriented material.

  7. Computer Assisted Instruction (Cain) For Nuclear Magnetic Resonance Spectroscopy

    International Nuclear Information System (INIS)

    Jaturonrusmee, Wasna; Arthonvorakul, Areerat; Assateranuwat, Adisorn

    2005-10-01

    A computer assisted instruction program for nuclear magnetic resonance spectroscopy was developed by using Author ware 5.0, Adobe Image Styler 1.0, Adobe Photo shop 7.0 and Flash MX. The contents included the basic theory of 1H and 13C nuclear magnetic resonance (NMR) spectroscopy, the instrumentation of NMR spectroscopy, the two dimensional (2D) NMR spectroscopy and the interpretation of NMR spectra. The program was also provided examples, and exercises, with emphasis on NMR spectra interpretation to determine the structure of unknown compounds and solutions for self study. The questionnaire from students showed that they were very satisfied with the software

  8. Experimental investigation on the thermal performance of heat pipe-assisted phase change material based battery thermal management system

    International Nuclear Information System (INIS)

    Wu, Weixiong; Yang, Xiaoqing; Zhang, Guoqing; Chen, Kai; Wang, Shuangfeng

    2017-01-01

    Highlights: • A heat pipe assisted phase change material based battery thermal management system is proposed. • The proposed system is compact and efficient from a view of practical application. • Cycling conditions are experimentally simulated for practical working environment. • The proposed system presents better thermal performance in comparison to other systems. • Combining forced air convection with heat pipe further enhances the cooling effect. - Abstract: In this paper, a heat pipe-assisted phase change material (PCM) based battery thermal management (BTM) system is designed to fulfill the comprehensive energy utilization for electric vehicles and hybrid electric vehicles. Combining the large heat storage capacity of the PCM with the excellent cooling effect of heat pipe, the as-constructed heat pipe-assisted PCM based BTM is feasible and effective with a relatively longer operation time and more suitable temperature. The experimental results show that the temperature maldistribution of battery module can be influenced by heat pipes when they are activated under high discharge rates of the batteries. Moreover, with forced air convection, the highest temperature could be controlled below 50 °C even under the highest discharge rate of 5C and a more stable and lower temperature fluctuation is obtained under cycling conditions. Meanwhile, the effectiveness of further increasing air velocity (i.e., more fan power consumption) is limited when the highest temperature continues to reduce at a lower rate due to the phase transition process of PCM. These results are expected to provide insights into the design and optimization of BTM systems.

  9. Phason thermal transport of three-helix state in insulating chiral magnets

    Science.gov (United States)

    Tatara, Gen

    2018-06-01

    Thermal dynamics of the three-helix state in a chiral magnet is studied based on a phason representation. Although phason representation is convenient for intuitive description, it is not straightforwardly compatible with microscopic linear response calculation of transport phenomena, because it is a (semi)macroscopic picture obtained by a coarse graining. By separating the slow phason mode and fast magnon mode, we show that phason thermal dynamics is driven by thermal magnon flow via the spin-transfer effect. The magnon and phason velocities are calculated by use of thermal vector potential formalism.

  10. Heat-Assisted Multiferroic Solid-State Memory.

    Science.gov (United States)

    Lepadatu, Serban; Vopson, Melvin M

    2017-08-25

    A heat-assisted multiferroic solid-state memory design is proposed and analysed, based on a PbNbZrSnTiO₃ antiferroelectric layer and Ni 81 Fe 19 magnetic free layer. Information is stored as magnetisation direction in the free layer of a magnetic tunnel junction element. The bit writing process is contactless and relies on triggering thermally activated magnetisation switching of the free layer towards a strain-induced anisotropy easy axis. A stress is generated using the antiferroelectric layer by voltage-induced antiferroelectric to ferroelectric phase change, and this is transmitted to the magnetic free layer by strain-mediated coupling. The thermally activated strain-induced magnetisation switching is analysed here using a three-dimensional, temperature-dependent magnetisation dynamics model, based on simultaneous evaluation of the stochastic Landau-Lifshitz-Bloch equation and heat flow equation, together with stochastic thermal fields and magnetoelastic contributions. The magnetisation switching probability is calculated as a function of stress magnitude and maximum heat pulse temperature. An operating region is identified, where magnetisation switching always occurs, with stress values ranging from 80 to 180 MPa, and maximum temperatures normalised to the Curie temperature ranging from 0.65 to 0.99.

  11. The dependence of critical current density of GdFeCo layer on composition of thermally assisted STT-RAM

    Science.gov (United States)

    Dai, B.; Zhu, J.; Liu, K.; Yang, L.; Han, J.

    2017-07-01

    Amorphous rare earth-transitional metal (RETM) GdFeCo memory layer with RE- and TM-rich compositions was fabricated in stacks of GdFeCo (10 nm)/Cu (3 nm)/[Co(0.2 nm)/Pd(0.4 nm)]6. Their magnetic properties and spin transfer torque (STT) switching of magnetization were investigated. The maximum magneto-resistance (MR) was around 0.24% for the TM-rich Gd21.4 (Fe90Co10)78.6 memory layer and was -0.03% for the RE-rich Gd29.0 (Fe90Co10)71.0 memory layer. The critical current densities Jc to switch the GdFeCo memory layers are in the range of 1.4 × 107 A/cm2-4.5 × 107 A/cm2. The dependence of critical current density Jc and effective anisotropy constant Keff on Gd composition were also investigated. Both Jc and Keff have maximum values in the Gd composition range from 21-29 at.%, suitable for thermally assisted STT-RAM for storage density exceeding Gb/inch2.

  12. Review and summary of Solar Thermal Conversion Program planning assistance

    Energy Technology Data Exchange (ETDEWEB)

    1975-06-01

    The Solar Thermal Conversion Program comprises a major part of the national solar energy program which must be continuously reviewed and modified where necessary. Modifications are typically required to reflect technical achievements and uncertainties which arise from within the program or from other technical programs, changes in budgets available for supporting the program as well as internal program funding priorities, changing goals such as through acceleration or stretch-out of the program schedule, significant organizational changes involving responsible governmental agencies, the introduction of new project management support contractors, and required budget or schedule changes occurring within individual projects that make up the Solar Thermal Conversion Program. The Aerospace Corporation has provided data to assist in planning, review, coordination, and documentation of the overall Solar Thermal Conversion Program. The Solar Thermal Conversion Program Plan is described in detail. Sections 2.0 through 5.0 cover the discussion and detail planning covering the objectives, justification, basic and alternative plans, budgets, and schedules for the Solar Thermal sub-unit portion of the Solar Electric Applications effort. Appendices B1, B2, and B3 include the March 21, March 28, and April 5, 1975, Program Plan submissions of the complete Solar Electric Applications effort. In Appendix B the Solar Thermal, Solar Photovoltaic, Wind Energy, and Ocean Thermal sub-unit texts have been condensed and formatted for integration in the overall ERDA budget package. (WHK)

  13. Thermal control for the MFTF magnet

    International Nuclear Information System (INIS)

    Vansant, J.H.; Russ, R.M.

    1980-01-01

    The external dimensions of the Yin-Yang magnet of the Mirror Fusion Test Facility will be 7.8 by 8.5 by 8.5 m, and it will weigh approximately 300 tons. More than 8000 liters of circulating liquid helium will be required to maintain the nearly 50 km of superconductor at below 5.0 K while the latter carries almost 6000 A in a magnetic field of up to nearly 7.7 T. This paper describes several features of the thermal control plans for the Yin-Yang: (1) the proposed cooldown and warmup schedules for the MFTF and the procedure for regenerating external cooling surfaces (2) the design of an external quench resistor based on an estimate of the superconductor's maximum temperature and (3) the use of a computer model of liquid helium circulation in choosing pipe size for the liquid helium lines

  14. Thermal Stability of Magnetic Compass Sensor for High Accuracy Positioning Applications

    OpenAIRE

    Van-Tang PHAM; Dinh-Chinh NGUYEN; Quang-Huy TRAN; Duc-Trinh CHU; Duc-Tan TRAN

    2015-01-01

    Using magnetic compass sensors in angle measurements have a wide area of application such as positioning, robot, landslide, etc. However, one of the most phenomenal that affects to the accuracy of the magnetic compass sensor is the temperature. This paper presents two thermal stability schemes for improving performance of a magnetic compass sensor. The first scheme uses the feedforward structure to adjust the angle output of the compass sensor adapt to the variation of the temperature. The se...

  15. Thermal conductivity of a quantum spin-1/2 antiferromagnetic chain with magnetic impurities

    International Nuclear Information System (INIS)

    Zviagin, A.A.

    2008-01-01

    We present an exact theory that describes how magnetic impurities change the behavior of the thermal conductivity for the integrable Heisenberg antiferromagnetic quantum spin-1/2 chain. Single magnetic impurities and a large concentration of impurities with similar values of the couplings to the host chain (a weak disorder) do not change the linear-in-temperature low-T behavior of the thermal conductivity: Only the slope of that behavior becomes smaller, compared to the homogeneous case. The strong disorder in the distribution of the impurity-host couplings produces more rapid temperature growth of the thermal conductivity, compared to the linear-in-T dependence of the homogeneous chain and the chain with weak disorder. Recent experiments on the thermal conductivity in inhomogeneous quasi-one-dimensional quantum spin systems manifest qualitative agreement with our results

  16. Magnetic islands in tokamaks induced by thermal filamentation

    International Nuclear Information System (INIS)

    Dubois, M.A.; Mohamed-Benkadda, M.S.

    1991-11-01

    The thermal instability of filamentation is revisited in the fully nonlinear regime of a system of cool magnetic island chains, taking into account: the different transport processes inside and outside island cores, and a realistic temperature dependence of radiative losses. This mechanism is found to be a plausible candidate to explain the anomalous electron energy transport

  17. The role of MFM signal in mark size measurement in probe-based magnetic recording on CoNi/Pt multilayers

    NARCIS (Netherlands)

    Zhang, Li; Bain, James A.; Zhu, Jian-Gang; Abelmann, Leon; Onoue, T.

    2007-01-01

    A method of heat-assisted magnetic recording (HAMR) potentially suitable for probe-based storage systems is characterized. Magnetic marks were formed by a scanning tunneling microscopy (STM)-based thermal magnetic mechanism on a perpendicular CoNi/Pt multilayered film. Magnetic force microscopy

  18. Static magnetism and thermal switching in randomly oriented L10 FePt thin films

    Science.gov (United States)

    Lisfi, A.; Pokharel, S.; Alqarni, A.; Akioya, O.; Morgan, W.; Wuttig, M.

    2018-05-01

    Static magnetism and thermally activated magnetic relaxation were investigated in granular FePt films (20 nm-200 nm thick) with random magnetic anisotropy through hysteresis loop, torque curve and magnetization time dependence measurements. While the magnetism of thicker film (200 nm thick) is dominated by a single switching of the ordered L10 phase, thinner film (20 nm) displays a double switching, which is indicative of the presence of the disordered cubic phase. The pronounced behavior of double switching in thinner film suggests that the film grain boundary is composed of soft cubic magnetic phase. The magnetic relaxation study reveals that magnetic viscosity S of the films is strongly dependent on the external applied field and exhibits a maximum value (12 kAm) around the switching field and a vanishing behavior at low (1 kOe) and large (12 kOe) fields. The activation volume of the thermal switching was found to be much smaller than the physical volume of the granular structure due to the incoherent rotation mode of the magnetization reversal mechanism, which is established to be domain wall nucleation.

  19. Magnetic and thermal properties of amorphous TbFeCo alloy films

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Ke, E-mail: K.Wang@hqu.edu.cn; Dong, Shuo; Huang, Ya; Qiu, Yuzhen

    2017-07-15

    Highlights: • Significant increase in magnetization is observed in TbFeCo upon crystallization. • The crystallization temperature is determined in the range between 400 and 450 °C. • The activation barriers for structural changes are obtained successfully. • Better thermal stability against crystallization and oxidation is demonstrated in FeCo-rich sample than Tb-rich type. - Abstract: Amorphous TbFeCo material with perpendicular magnetic anisotropy is currently attracting more attention for potential applications in spintronic devices and logic memories. We systematically investigate magnetic, structural, thermal, optical and electrical properties of TbFeCo alloy films. It shows out-of-plane easy axis of the films turns into in-plane orientation after annealing. Significant increase in saturation magnetization in the temperature range between 400 and 450 °C is revealed by thermomagnetic measurements. The occurrence of crystallization and oxidation at high temperatures is confirmed by X-ray diffraction measurements. Pronounced changes in optical reflectance and sheet resistance are observed with temperature, in line with structural relaxation and change. The activation barriers for crystallization and oxidation are determined to be 1.01 eV and 0.83 eV, respectively, for FeCo-rich and Tb-rich samples. Better thermal stability against crystallization and oxidation is demonstrated in the FeCo-rich sample than the Tb-rich type. Our results provide some useful information for the alloy used in device fabrication.

  20. Magnetic field assisted Fenton reactions for the enhanced degradation of methyl blue

    Institute of Scientific and Technical Information of China (English)

    Xiao Long Hao; Lu Yi Zou; Guang Sheng Zhang; Yi Bo Zhang

    2009-01-01

    Magnetic field was tentatively introduced into Fenton reactions system for the degradation and discoloration of methyl blue as the represent of organic chemical dye, which was a bio-refractory organic pollutant in industry wastewater. It was found that under optimal Fenton reaction conditions, with the assistant of magnetic field in Fenton reactions, the degradation rate of methyl blue, the decomposition rate of H2O2 and the conversion rate of Fe2+ were accelerated, the extent of them would be improved by the increase of magnetic field intensity. Meanwhile, the mineralization of methyl blue (CODcr) was improved by over 10% with magnetic fiold.

  1. The influence of the magnetic state on the thermal expansion in 1:2 rare earth intermetallic compounds

    International Nuclear Information System (INIS)

    Gratz, E.; Lindbaum, A.

    1994-01-01

    The attempt is made to demonstrate on some selected rare earth intermetallics the influence of the magnetic state on the thermal expansion. Using the X-ray powder diffraction method we investigated the thermal expansion of some selected nonmagnetic compounds (YAl 2 , YNi 2 and YCo 2 ) and some magnetic RE (rare earth) - cobalt compounds (RCo 2 ) in the temperature range from 4 up to 450 K. All these compounds crystallize in the C15-type structure (cubic Laves phase structure). By comparing the nonmagnetic Y-based compounds we could show that there is an enhanced contribution of the 3d electrons to the thermal expansion in YCo 2 . In the magnetic RCo 2 compounds the induced 3d magnetism gives rise to large volume anomalies at the magnetic ordering temperature T c . Below T c there is in addition a distortion of the cubic unit cell due to the interaction of the magnetically ordered RE ions with the anisotropic crystal field.The thermal expansion of the orthorhombic TmCu 2 , GdCu 2 and YCu 2 compounds has also been investigated for comparison. The influence of the crystal field on the thermal expansion in TmCu 2 in the paramagnetic range (TmCu 2 orders magnetically at T N =6.3 K) has been determined by comparing the thermal expansion of the nonmagnetic YCu 2 with that of TmCu 2 . The data thus obtained are compared with a theoretical model. GdCu 2 , for which the influence of the crystal field can be neglected, has been investigated in order to study the influence of the exchange interaction in the magnetically ordered state (below 42 K). ((orig.))

  2. Thermal chiral vortical and magnetic waves: New excitation modes in chiral fluids

    Energy Technology Data Exchange (ETDEWEB)

    Kalaydzhyan, Tigran, E-mail: tigran@caltech.edu [Department of Physics, University of Illinois, 845 W Taylor Street, Chicago, IL 60607 (United States); Jet Propulsion Laboratory, 4800 Oak Grove Dr, M/S 298, Pasadena, CA 91109 (United States); Murchikova, Elena [TAPIR, California Institute of Technology, MC 350-17, Pasadena, CA 91125 (United States)

    2017-06-15

    In certain circumstances, chiral (parity-violating) medium can be described hydrodynamically as a chiral fluid with microscopic quantum anomalies. Possible examples of such systems include strongly coupled quark–gluon plasma, liquid helium {sup 3}He-A, neutron stars and the Early Universe. We study first-order hydrodynamics of a chiral fluid on a vortex background and in an external magnetic field. We show that there are two previously undiscovered modes describing heat waves propagating along the vortex and magnetic field. We call them the Thermal Chiral Vortical Wave and Thermal Chiral Magnetic Wave. We also identify known gapless excitations of density (chiral vortical and chiral magnetic waves) and transverse velocity (chiral Alfvén wave). We demonstrate that the velocity of the chiral vortical wave is zero, when the full hydrodynamic framework is applied, and hence the wave is absent and the excitation reduces to the charge diffusion mode. We also comment on the frame-dependent contributions to the obtained propagation velocities.

  3. Characterization for Ceramic-coated magnets using E-beam and thermal annealing methods

    International Nuclear Information System (INIS)

    Kim, Hyug Jong; Kim, Hee Gyu; Kang, In Gu; Kim, Min Wan; Yang, Ki Ho; Lee, Byung Cheol; Choi, Byung Ho

    2009-01-01

    Hard magnet was usually used by coating SiO 2 ceramic thick films followed by the thermal annealing process. In this work, the alternative annealing process for NdFeB magnets using e-beam sources(1∼2 MeV, 50∼400 kGy) was investigated. NdFeB magnets was coated with ceramic thick films using the spray method. The optimal annealing parameter for e-beam source reveals to be 1 MeV and 300 kGy. The sample prepared at 1 MeV and 300 kGy was characterized by the analysis of the surface morphology, film hardness, adhesion and chemical stability. The mechanical property of thick film, especially film hardness, is better than that of thermal annealed samples at 180 .deg. C. As a result, e-beam annealing process will be one of candidate and attractive heat treatment process. In future, manufacturing process will be carried out in cooperation with the magnet company

  4. Thermal chiral vortical and magnetic waves: New excitation modes in chiral fluids

    International Nuclear Information System (INIS)

    Kalaydzhyan, Tigran; Murchikova, Elena

    2017-01-01

    In certain circumstances, chiral (parity-violating) medium can be described hydrodynamically as a chiral fluid with microscopic quantum anomalies. Possible examples of such systems include strongly coupled quark–gluon plasma, liquid helium "3He-A, neutron stars and the Early Universe. We study first-order hydrodynamics of a chiral fluid on a vortex background and in an external magnetic field. We show that there are two previously undiscovered modes describing heat waves propagating along the vortex and magnetic field. We call them the Thermal Chiral Vortical Wave and Thermal Chiral Magnetic Wave. We also identify known gapless excitations of density (chiral vortical and chiral magnetic waves) and transverse velocity (chiral Alfvén wave). We demonstrate that the velocity of the chiral vortical wave is zero, when the full hydrodynamic framework is applied, and hence the wave is absent and the excitation reduces to the charge diffusion mode. We also comment on the frame-dependent contributions to the obtained propagation velocities.

  5. Thermal chiral vortical and magnetic waves: New excitation modes in chiral fluids

    Directory of Open Access Journals (Sweden)

    Tigran Kalaydzhyan

    2017-06-01

    Full Text Available In certain circumstances, chiral (parity-violating medium can be described hydrodynamically as a chiral fluid with microscopic quantum anomalies. Possible examples of such systems include strongly coupled quark–gluon plasma, liquid helium 3He-A, neutron stars and the Early Universe. We study first-order hydrodynamics of a chiral fluid on a vortex background and in an external magnetic field. We show that there are two previously undiscovered modes describing heat waves propagating along the vortex and magnetic field. We call them the Thermal Chiral Vortical Wave and Thermal Chiral Magnetic Wave. We also identify known gapless excitations of density (chiral vortical and chiral magnetic waves and transverse velocity (chiral Alfvén wave. We demonstrate that the velocity of the chiral vortical wave is zero, when the full hydrodynamic framework is applied, and hence the wave is absent and the excitation reduces to the charge diffusion mode. We also comment on the frame-dependent contributions to the obtained propagation velocities.

  6. Evaluation of airborne thermal, magnetic, and electromagnetic characterization technologies

    Energy Technology Data Exchange (ETDEWEB)

    Josten, N.E.

    1992-03-01

    The identification of Buried Structures (IBS) or Aerial Surveillance Project was initiated by the US Department of Energy (DOE) Office of Technology Development to demonstrate airborne methods for locating and identifying buried waste and ordnance at the Idaho National Engineering Laboratory (INEL). Two technologies were demonstrated: (a) a thermal infrared imaging system built by Martin Marietta Missile Systems and (b) a magnetic and electromagnetic (EM) geophysical surveying system operated by EBASCO Environmental. The thermal system detects small differences in ground temperature caused by uneven heating and cooling of the ground by the sun. Waste materials on the ground can be detected when the temperature of the waste is different than the background temperature. The geophysical system uses conventional magnetic and EM sensors. These sensors detect disturbances caused by magnetic or conductive waste and naturally occurring magnetic or conductive features of subsurface soils and rock. Both systems are deployed by helicopter. Data were collected at four INEL sites. Tests at the Naval Ordnance Disposal Area (NODA) were made to evaluate capabilities for detecting ordnance on the ground surface. Tests at the Cold Simulated Waste Demonstration Pit were made to evaluate capabilities for detecting buried waste at a controlled site, where the location and depth of buried materials are known. Tests at the Subsurface Disposal Area and Stationary Low-Power Reactor-1 burial area were made to evaluate capabilities for characterizing hazardous waste at sites that are typical of DOE buried waste sites nationwide.

  7. Evaluation of airborne thermal, magnetic, and electromagnetic characterization technologies

    International Nuclear Information System (INIS)

    Josten, N.E.

    1992-03-01

    The identification of Buried Structures (IBS) or Aerial Surveillance Project was initiated by the US Department of Energy (DOE) Office of Technology Development to demonstrate airborne methods for locating and identifying buried waste and ordnance at the Idaho National Engineering Laboratory (INEL). Two technologies were demonstrated: (a) a thermal infrared imaging system built by Martin Marietta Missile Systems and (b) a magnetic and electromagnetic (EM) geophysical surveying system operated by EBASCO Environmental. The thermal system detects small differences in ground temperature caused by uneven heating and cooling of the ground by the sun. Waste materials on the ground can be detected when the temperature of the waste is different than the background temperature. The geophysical system uses conventional magnetic and EM sensors. These sensors detect disturbances caused by magnetic or conductive waste and naturally occurring magnetic or conductive features of subsurface soils and rock. Both systems are deployed by helicopter. Data were collected at four INEL sites. Tests at the Naval Ordnance Disposal Area (NODA) were made to evaluate capabilities for detecting ordnance on the ground surface. Tests at the Cold Simulated Waste Demonstration Pit were made to evaluate capabilities for detecting buried waste at a controlled site, where the location and depth of buried materials are known. Tests at the Subsurface Disposal Area and Stationary Low-Power Reactor-1 burial area were made to evaluate capabilities for characterizing hazardous waste at sites that are typical of DOE buried waste sites nationwide

  8. Thermal equilibrium of pure electron plasmas across a central region of magnetic surfaces

    Science.gov (United States)

    Hahn, Michael; Pedersen, Thomas Sunn

    2009-06-01

    Measurements of the equilibria of plasmas created by emission from a biased filament located off the magnetic axis in the Columbia Non-neutral Torus (CNT) [T. S. Pedersen, J. P. Kremer, R. G. Lefrancois et al., Fusion Sci. Technol. 50, 372 (2006)] show that such plasmas have equilibrium properties consistent with the inner surfaces being in a state of cross-surface thermal equilibrium. Numerical solutions to the equilibrium equation were used to fit the experimental data and demonstrate consistency with cross-surface thermal equilibrium. Previous experiments in CNT showed that constant temperatures across magnetic surfaces are characteristic of CNT plasmas, implying thermal confinement times much less than particle confinement times. These results show that when emitting off axis there is a volume of inner surfaces where diffusion into that region is balanced by outward transport, producing a Boltzmann distribution of electrons. When combined with the low thermal energy confinement time this is a cross-surface thermal equilibrium.

  9. Thermal equilibrium of pure electron plasmas across a central region of magnetic surfaces

    International Nuclear Information System (INIS)

    Hahn, Michael; Pedersen, Thomas Sunn

    2009-01-01

    Measurements of the equilibria of plasmas created by emission from a biased filament located off the magnetic axis in the Columbia Non-neutral Torus (CNT) [T. S. Pedersen, J. P. Kremer, R. G. Lefrancois et al., Fusion Sci. Technol. 50, 372 (2006)] show that such plasmas have equilibrium properties consistent with the inner surfaces being in a state of cross-surface thermal equilibrium. Numerical solutions to the equilibrium equation were used to fit the experimental data and demonstrate consistency with cross-surface thermal equilibrium. Previous experiments in CNT showed that constant temperatures across magnetic surfaces are characteristic of CNT plasmas, implying thermal confinement times much less than particle confinement times. These results show that when emitting off axis there is a volume of inner surfaces where diffusion into that region is balanced by outward transport, producing a Boltzmann distribution of electrons. When combined with the low thermal energy confinement time this is a cross-surface thermal equilibrium.

  10. Physical principles of microwave assisted magnetic recording

    International Nuclear Information System (INIS)

    Rivkin, Kirill; Benakli, Mourad; Yin, Huaqing; Tabat, Ned

    2014-01-01

    While the basic physics of Microwave Assisted Magnetization Reversal (MAMR) phenomenon is well established both theoretically and experimentally, its application in a practical magnetic recording environment was so far studied primarily with the help of micromagnetic recording models. In this work, we instead attempt to use analytical formulation and simple numerical models to understand the main challenges as well as benefits that are associated with such a system. It appears that the main difference between the previously introduced theory [G. Bertotti et al., Phys. Rev. Lett. 86, 724 (2001); K. Rivkin et al., Appl. Phys. Lett. 92, 153104 (2008); S. Okamoto et al., J. Appl. Phys. 107, 123914 (2010).] and recording environment is that both the RF and DC magnetic fields are applied at a substantial angle to the anisotropy axis. While the associated symmetry breaking prevents one from describing the reversal process explicitly, it is possible to approximate the solutions well enough to satisfactorily match numerical models both in the case of wire and Spin Torque Oscillator generated RF fields. This approach allows for physical explanation of various effects associated with MAMR such as high gradient of writeable anisotropy and reduction of track width, and offers a clear guidance regarding future optimization of MAMR recording.

  11. Physical principles of microwave assisted magnetic recording

    Energy Technology Data Exchange (ETDEWEB)

    Rivkin, Kirill; Benakli, Mourad; Yin, Huaqing [Seagate Technology, Edina, Minnesota 55435 (United States); Tabat, Ned [Semaphore Scientific Inc., Chanhassen, Minnesota 55317 (United States)

    2014-06-07

    While the basic physics of Microwave Assisted Magnetization Reversal (MAMR) phenomenon is well established both theoretically and experimentally, its application in a practical magnetic recording environment was so far studied primarily with the help of micromagnetic recording models. In this work, we instead attempt to use analytical formulation and simple numerical models to understand the main challenges as well as benefits that are associated with such a system. It appears that the main difference between the previously introduced theory [G. Bertotti et al., Phys. Rev. Lett. 86, 724 (2001); K. Rivkin et al., Appl. Phys. Lett. 92, 153104 (2008); S. Okamoto et al., J. Appl. Phys. 107, 123914 (2010).] and recording environment is that both the RF and DC magnetic fields are applied at a substantial angle to the anisotropy axis. While the associated symmetry breaking prevents one from describing the reversal process explicitly, it is possible to approximate the solutions well enough to satisfactorily match numerical models both in the case of wire and Spin Torque Oscillator generated RF fields. This approach allows for physical explanation of various effects associated with MAMR such as high gradient of writeable anisotropy and reduction of track width, and offers a clear guidance regarding future optimization of MAMR recording.

  12. Electron thermal confinement in a partially stochastic magnetic structure

    Science.gov (United States)

    Morton, L. A.; Young, W. C.; Hegna, C. C.; Parke, E.; Reusch, J. A.; Den Hartog, D. J.

    2018-04-01

    Using a high-repetition-rate Thomson scattering diagnostic, we observe a peak in electron temperature Te coinciding with the location of a large magnetic island in the Madison Symmetric Torus. Magnetohydrodynamic modeling of this quasi-single helicity plasma indicates that smaller adjacent islands overlap with and destroy the large island flux surfaces. The estimated stochastic electron thermal conductivity ( ≈30 m 2/s ) is consistent with the conductivity inferred from the observed Te gradient and ohmic heating power. Island-shaped Te peaks can result from partially stochastic magnetic islands.

  13. Thermally driven magnon transport in the magnetic insulator Yttrium Iron Garnet

    International Nuclear Information System (INIS)

    Agrawal, Milan

    2014-01-01

    carried out. The first direct measurement of the spatial distribution of the magnon and the phonon temperatures in the YIG film, subject to a lateral thermal gradient, is realized by developing a novel technique to measure the local magnetization in the magnetic film using Brillouin light scattering (BLS) spectroscopy. The findings reveal a close correspondence between the spatial dependencies of magnon and phonon temperatures which represents the strong interaction between the magnon and the phonon subsystems. Subsequently, the findings are utilized to understand the origin of the transverse spin Seebeck effect (SSE), where a spin current flowing perpendicularly to the heat currents or the temperature gradient is generated. The results emphasize on the formulation of the concept of spectral non-uniformity of magnon temperature to explain the transverse spin Seebeck effect with contemporary theories. The outcomes provide a new direction for a deeper theoretical investigation on the origin of the spin Seebeck effect. In order to unfold the origin of the spin Seebeck effect as well as to develop industrial applications, the knowledge about the timescales of the effect is essential. In this thesis, very first measurements of the temporal evolution of the longitudinal spin Seebeck effect, where the spin current flows parallel to the heat current, are carried out on a YIGPlatinum (Pt) heterostructure. Here, the high spin-orbital coupling material Pt is employed to measure the spin current via the inverse spin Hall effect. Two heating techniques, laser irradiation and microwave heating, are utilized to perform the time-resolved measurements of the longitudinal spin Seebeck effect. The advantages of these heating techniques over the conventional heating methods are explored as well. The time-resolved measurements on the longitudinal spin Seebeck effect reveal that this effect takes place on a sub-microsecond timescale. Further, these measurements assist in understanding the

  14. Experiment-based thermal micromagnetic simulations of the magnetization reversal for ns-range clocked nanomagnetic logic

    Science.gov (United States)

    Ziemys, Grazvydas; Breitkreutz-v. Gamm, Stephan; Csaba, Gyorgy; Schmitt-Landsiedel, Doris; Becherer, Markus

    2017-05-01

    Extensive thermal micromagnetic simulations, based on experimental data and parameters, were performed to investigate the magnetization reversal in Co/Pt nanomagnets with locally reduced perpendicular anisotropy on the nanosecond range. The simulations were supported by experimental data gained on manufactured Co/Pt nanomagnets, as used in nanomagnetic logic. It is known that magnetization reversal is governed by two mechanisms. At pulse lengths longer than 100 ns, thermal activation dominates the magnetization reversal processes and follows the common accepted Arrhenius law. For pulse lengths shorter than 100 ns, the dynamic reversal dominates. With the help of thermal micro-magnetic simulations we found out that the point where the both mechanisms meet is determined by the damping constant α of the multilayer film stack. The optimization of ferromagnetic multilayer film stacks enables higher clocking rates with lower power consumption and, therefore, further improve the performance of pNML.

  15. Thermal and mechanical effects of quenches on Nb3Sn high field hadron collider magnets

    International Nuclear Information System (INIS)

    Ryuji, Yamada

    2001-01-01

    Thermal and its resulting mechanical stress due to quenches inside short and long epoxy impregnated Nb 3 Sn high field magnets are studied with a quench simulation program, Kuench, and ANSYS program. For the protection of a long high field magnet, we have to use heaters to dump the stored energy uniformly inside the magnet, after detection of a spontaneous quench. The time delay of starting a forced quench with heaters, is estimated using ANSYS. Using this information, the thermal distribution in two-dimensional magnet cross section is studied. First a one meter model magnet with a dump resistor is used to estimate the effects and then a 10 meter long magnet is studied. The two-dimensional temperature distributions in the magnet cross sections are recorded every 5 ms, and visually displayed. With this visual animation displays we can understand intuitively the thermal and quench propagation in 2-dimensional field. The quenching cables get heated locally much more than the surrounding material and non-quenching conductor cables. With a one meter magnet with a dump resistor of 30 mOmega, typically only the quench starting cables and its neighbor cables get heated up to 100 K without significant effects from the heaters. With a10 meter magnet, heaters cause the quenches to most of the conductor blocks. The quench initiating cables get up to 250 to 300 K in 100 ms, but the surrounding and wedges are not heated up significantly. This causes the excessive stress in the quenching conductors and in their insulation material locally. The stress and strain in the conductor as well as in the insulation become excessive, and they are studied using the ANSYS stress analysis, using Von Mises criterion. It is concluded that for the one meter magnet with the presented cross section and configuration, the thermal effects due to the quench is tolerable. But we need much more quench study and improvements in the design for the extended ten meter long magnet [1

  16. Multimaterial magnetically assisted 3D printing of composite materials

    Science.gov (United States)

    Kokkinis, Dimitri; Schaffner, Manuel; Studart, André R.

    2015-10-01

    3D printing has become commonplace for the manufacturing of objects with unusual geometries. Recent developments that enabled printing of multiple materials indicate that the technology can potentially offer a much wider design space beyond unusual shaping. Here we show that a new dimension in this design space can be exploited through the control of the orientation of anisotropic particles used as building blocks during a direct ink-writing process. Particle orientation control is demonstrated by applying low magnetic fields on deposited inks pre-loaded with magnetized stiff platelets. Multimaterial dispensers and a two-component mixing unit provide additional control over the local composition of the printed material. The five-dimensional design space covered by the proposed multimaterial magnetically assisted 3D printing platform (MM-3D printing) opens the way towards the manufacturing of functional heterogeneous materials with exquisite microstructural features thus far only accessible by biological materials grown in nature.

  17. Construction of high current density SC magnets and their thermal stability

    International Nuclear Information System (INIS)

    Ishibashi, K.; Katase, A.; Kobayashi, M.; Wake, M.; Suzuki, K.

    1979-07-01

    Pancake type solenoid magnets are constructed which have a similar cooling characteristics to a pulsed dipole magnet for a synchrotron. A metal inpregnated braided cable is used to test a long sample of the cable. The detailed performances of the magnets and cable are examined with respect to achieved fields, training effect and ac losses. The stability theories which have been proposed so far are not adequate to these high current density magnets, so that a new method is developed to estimate the magnet stability. The minimum energy of thermal disturbances (MQE) which causes a quenching is measured by experiment and is compared with the calculation. The calculated values of MQE are in good agreement with the experimental results. The performance of the pancake magnet is discussed on the basis of MQE. (author)

  18. Research Update: Utilizing magnetization dynamics in solid-state thermal energy conversion

    Directory of Open Access Journals (Sweden)

    Stephen R. Boona

    2016-10-01

    Full Text Available We review the spin-Seebeck and magnon-electron drag effects in the context of solid-state energy conversion. These phenomena are driven by advective magnon-electron interactions. Heat flow through magnetic materials generates magnetization dynamics, which can strongly affect free electrons within or adjacent to the magnetic material, thereby producing magnetization-dependent (e.g., remnant electric fields. The relative strength of spin-dependent interactions means that magnon-driven effects can generate significantly larger thermoelectric power factors as compared to classical thermoelectric phenomena. This is a surprising situation in which spin-based effects are larger than purely charge-based effects, potentially enabling new approaches to thermal energy conversion.

  19. Magnetic field-assisted electrochemical discharge machining

    International Nuclear Information System (INIS)

    Cheng, Chih-Ping; Mai, Chao-Chuang; Wu, Kun-Ling; Hsu, Yu-Shan; Yan, Biing-Hwa

    2010-01-01

    Electrochemical discharge machining (ECDM) is an effective unconventional method for micromachining in non-conducting materials, such as glass, quartz and some ceramics. However, since the spark discharge performance becomes unpredictable as the machining depth increases, it is hard to achieve precision geometry and efficient machining rate in ECDM drilling. One of the main factors for this is the lack of sufficient electrolyte flow in the narrow gap between the tool and the workpiece. In this study a magnetohydrodynamic (MHD) convection, which enhances electrolyte circulation has been applied to the ECDM process in order to upgrade the machining accuracy and efficiency. During electrolysis in the presence of a magnetic field, the Lorenz force induces the charged ions to form a MHD convection. The MHD convection then forces the electrolyte into movement, thus enhancing circulation of electrolyte. Experimental results show that the MHD convection induced by the magnetic field can effectively enhance electrolyte circulation in the micro-hole, which contributes to higher machining efficiency. Micro-holes in glass with a depth of 450 µm are drilled in less than 20 s. At the same time, better electrolyte circulation can prevent deterioration of gas film quality with increasing machining depth, while ensuring stable electrochemical discharge. The improvement in the entrance diameter thus achieved was 23.8% while that in machining time reached 57.4%. The magnetic field-assisted approach proposed in the research does not require changes in the machining setup or electrolyte but has proved to achieve significant enhancement in both accuracy and efficiency of ECDM.

  20. Thermal damage control of dye-assisted laser tissue welding: effect of dye concentration

    Science.gov (United States)

    Xie, Hua; Buckley, Lisa A.; Prahl, Scott A.; Shaffer, Brian S.; Gregory, Kenton W.

    2001-05-01

    Successful laser-assisted tissue welding was implemented to provide proper weld strength with minimized tissue thermal injury. We investigated and compared the weld strengths and morphologic changes in porcine small intestinal submucose (SIS) and porcine ureteral tissues with various concentration of indocyanine green (ICG) and with a solid albumin sheet. The study showed that the tissues were welded at lower ICG concentration (0.05 mM) with minimized tissue thermal damage using an 800-nm wavelength diode laser.

  1. Technical assistance for development of thermally conductive nitride filler for epoxy molding compounds

    Energy Technology Data Exchange (ETDEWEB)

    Ryu, Ho Jin; Song, Kee Chan; Jung, In Ha

    2005-07-15

    Technical assistance was carried out to develop nitride filler for thermally conductive epoxy molding compounds. Carbothermal reduction method was used to fabricate silicon nitride powder from mixtures of silica and graphite powders. Microstructure and crystal structure were observed by using scanning electron microscopy and x-ray diffraction technique. Thermal properties of epoxy molding compounds containing silicon nitride were measured by using laser flash method. Fabrication process of silicon nitride nanowire was developed and was applied to a patent.

  2. Electrostatic Self-Assembly of Au Nanoparticles onto Thermosensitive Magnetic Core-Shell Microgels for Thermally Tunable and Magnetically Recyclable Catalysis.

    Science.gov (United States)

    Liu, Guoqiang; Wang, Daoai; Zhou, Feng; Liu, Weimin

    2015-06-01

    A facile route to fabricate a nanocomposite of Fe3O4@poly[N-isopropylacrylamide (NIPAM)-co-2-(dimethylamino)ethyl methacrylate (DMAEMA)]@Au (Fe3O4@PND@Au) is developed for magnetically recyclable and thermally tunable catalysis. The negatively charged Au nanoparticles with an average diameter of 10 nm are homogeneously loaded onto positively charged thermoresponsive magnetic core-shell microgels of Fe3O4@poly(NIPAM-co-DMAEMA) (Fe3O4@PND) through electrostatic self-assembly. This type of attachment offers perspectives for using charged polymeric shell on a broad variety of nanoparticles to immobilize the opposite-charged nanoparticles. The thermosensitive PND shell with swollen or collapsed properties can be as a retractable Au carrier, thereby tuning the aggregation or dispersion of Au nanoparticles, which leads to an increase or decrease of catalytic activity. Therefore, the catalytic activity of Fe3O4@PND@Au can be modulated by the volume transition of thermosensitive microgel shells. Importantly, the mode of tuning the aggregation or dispersion of Au nanoparticles using a thermosensitive carrier offers a novel strategy to adjust and control the catalytic activity, which is completely different with the traditional regulation mode of controlling the diffusion of reactants toward the catalytic Au core using the thermosensitive poly(N-isopropylacrylamide) network as a nanogate. Concurrent with the thermally tunable catalysis, the magnetic susceptibility of magnetic cores enables the Fe3O4@PND@Au nanocomposites to be capable of serving as smart nanoreactors for thermally tunable and magnetically recyclable catalysis. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  3. A multi-functional testing instrument for heat assisted magnetic recording media

    International Nuclear Information System (INIS)

    Yang, H. Z.; Chen, Y. J.; Leong, S. H.; An, C. W.; Ye, K. D.; Hu, J. F.; Yin, M. J.

    2014-01-01

    With recent developments in heat assisted magnetic recording (HAMR), characterization of HAMR media is becoming very important. We present a multi-functional instrument for testing HAMR media, which integrates HAMR writing, reading, and a micro-magneto-optic Kerr effect (μ-MOKE) testing function. A potential application of the present instrument is to make temperature dependent magnetic property measurement using a pump-probe configuration. In the measurement, the media is heated up by a heating (intense) beam while a testing (weak) beam is overlapped with the heating beam for MOKE measurement. By heating the media with different heating beam power, magnetic measurements by MOKE at different temperatures can be performed. Compared to traditional existing tools such as the vibrating sample magnetometer, the present instrument provides localized and efficient heating at the measurement spot. The integration of HAMR writing and μ-MOKE system can also facilitate a localized full investigation of the magnetic media by potential correlation of HAMR head independent write/read performance to localized magnetic properties

  4. Investigating spin-transfer torques induced by thermal gradients in magnetic tunnel junctions by using micro-cavity ferromagnetic resonance

    Science.gov (United States)

    Cansever, H.; Narkowicz, R.; Lenz, K.; Fowley, C.; Ramasubramanian, L.; Yildirim, O.; Niesen, A.; Huebner, T.; Reiss, G.; Lindner, J.; Fassbender, J.; Deac, A. M.

    2018-06-01

    Similar to electrical currents flowing through magnetic multilayers, thermal gradients applied across the barrier of a magnetic tunnel junction may induce pure spin-currents and generate ‘thermal’ spin-transfer torques large enough to induce magnetization dynamics in the free layer. In this study, we describe a novel experimental approach to observe spin-transfer torques induced by thermal gradients in magnetic multilayers by studying their ferromagnetic resonance response in microwave cavities. Utilizing this approach allows for measuring the magnetization dynamics on micron/nano-sized samples in open-circuit conditions, i.e. without the need of electrical contacts. We performed first experiments on magnetic tunnel junctions patterned into 6  ×  9 µm2 ellipses from Co2FeAl/MgO/CoFeB stacks. We conducted microresonator ferromagnetic resonance (FMR) under focused laser illumination to induce thermal gradients in the layer stack and compared them to measurements in which the sample was globally heated from the backside of the substrate. Moreover, we carried out broadband FMR measurements under global heating conditions on the same extended films the microstructures were later on prepared from. The results clearly demonstrate the effect of thermal spin-torque on the FMR response and thus show that the microresonator approach is well suited to investigate thermal spin-transfer-driven processes for small temperatures gradients, far below the gradients required for magnetic switching.

  5. Electric-field assisted switching of magnetization in perpendicularly magnetized (Ga,Mn)As films at high temperatures

    Science.gov (United States)

    Wang, Hailong; Ma, Jialin; Yu, Xueze; Yu, Zhifeng; Zhao, Jianhua

    2017-01-01

    The electric-field effects on the magnetism in perpendicularly magnetized (Ga,Mn)As films at high temperatures have been investigated. An electric-field as high as 0.6 V nm-1 is applied by utilizing a solid-state dielectric Al2O3 film as a gate insulator. The coercive field, saturation magnetization and magnetic anisotropy have been clearly changed by the gate electric-field, which are detected via the anomalous Hall effect. In terms of the Curie temperature, a variation of about 3 K is observed as determined by the temperature derivative of the sheet resistance. In addition, electrical switching of the magnetization assisted by a fixed external magnetic field at 120 K is demonstrated, employing the gate-controlled coercive field. The above experimental results have been attributed to the gate voltage modulation of the hole density in (Ga,Mn)As films, since the ferromagnetism in (Ga,Mn)As is carrier-mediated. The limited modulation magnitude of magnetism is found to result from the strong charge screening effect introduced by the high hole concentration up to 1.10  ×  1021 cm-3, while the variation of the hole density is only about 1.16  ×  1020 cm-3.

  6. Reduced thermal budget processing of Y-Ba-Cu-O films by rapid isothermal processing assisted metalorganic chemical vapor deposition

    International Nuclear Information System (INIS)

    Singh, R.; Sinha, S.; Hsu, N.J.; Ng, J.T.C.; Chou, P.; Thakur, R.P.S.; Narayan, J.

    1991-01-01

    Metalorganic chemical vapor deposition (MOCVD) has the potential of emerging as a viable technique to fabricate ribbons, tapes, coated wires, and the deposition of films of high-temperature superconductors, and related materials. As a reduced thermal budget processing technique, rapid isothermal processing (RIP) based on incoherent radiation as the source of energy can be usefully coupled to conventional MOCVD. In this paper we report on the deposition and characterization of high quality superconducting thin films of Y-Ba-Cu-O (YBCO) on yttrium stabilized zirconia substrates by RIP assisted MOCVD. Using O 2 gas as the source of oxygen, YBCO films deposited initially at 600 degree C for 1 min and at 745 degree C for 25 min followed by deposition at 780 degree C for 45 s are primarily c-axis oriented and zero resistance is observed at 89--90 K. The zero magnetic field current density at 53 and 77 K are 1.2x10 6 and 3x10 5 A/cm 2 , respectively. By using a mixture of N 2 O and O 2 as the oxygen source substrate temperature was further reduced in the deposition of YBCO films. The films deposited initially at 600 degree C for 1 min and than at 720 degree C for 30 min are c-axis oriented and with zero resistance being observed at 91 K. The zero magnetic field current densities at 53 and 77 K are 3.4x10 6 and 1.2x10 6 A/cm 2 , respectively. To the best of our knowledge this is the highest value of critical current density, J c for films deposited by MOCVD at a substrate temperature as low as 720 degree C. It is envisioned that high energy photons from the incoherent light source and the use of a mixture of N 2 O and O 2 as the oxygen source, assist chemical reactions and lower overall thermal budget for processing of these films

  7. Thermal analysis and microstructure of hexaperrite based magnet composite with natural rubber matrix

    International Nuclear Information System (INIS)

    Sudirman; Ridwan; Jamilah; Trijono, Waluyo

    2000-01-01

    Thermal and microstructure analyse of hexa ferrite based on composite magnets with natural rubber matrix have been done to investigate their performance. Such magnets play an important role in the toy and house-hold industries because of their suitable magnetic properties, low cost, lightness and flexibility. The composite magnets were synthesized by blending the ferrite powder and natural rubber at composition 30%-70% rubber volume. The microstructure and thermal behaviour of the composite were examined by using SEM and OTA/TGA. The result show that the natural rubber swelling is optimally at 181,17 o C, which is the recommended top condition for blending. The performance magnet composite is limited by the change of natural rubber properties which decompose at temperature around 400 o C. In the decomposition process, the natural rubber molecule trapped in a composite system based on BaM is more difficult are more compared to the composite system based on SrM because the BaM system particle microstructure and its distribution more homogeneous

  8. Synthesis, thermal and magnetic properties of RE-diborides

    Energy Technology Data Exchange (ETDEWEB)

    Novikov, V.V., E-mail: vvnovikov@mail.ru [Training-Research Center ' Bryansk Physical Laboratory' , Petrovsky Bryansk State University, 14, Bezhitskaya St, 241036 Bryansk (Russian Federation); Matovnikov, A.V. [Training-Research Center ' Bryansk Physical Laboratory' , Petrovsky Bryansk State University, 14, Bezhitskaya St, 241036 Bryansk (Russian Federation); Volkova, O.S. [Lomonosov Moscow State University, GSP-1, Leninskie Gory, 119991 Moscow (Russian Federation); Vasil' ev, A.N., E-mail: vasil@mig.phys.msu.ru [Lomonosov Moscow State University, GSP-1, Leninskie Gory, 119991 Moscow (Russian Federation)

    2017-04-15

    Techniques of synthesis of RE diborides (RB{sub 2}) are developed (R=Tb, Dy, Ho, Er, Lu). Temperature dependence of magnetisation, a heat capacity, a lattice parameters of diborides in the range of 2–300 K are measured. According to joint calorimetric and X-ray research the analysis of a phonon component of a heat capacity and thermal expansion of RE-diborides is carried out by Debye-Einstein's models, the parameters of the model are determined. The change of magnetisation of the ferromagnetic RB{sub 2} compounds with growth of temperature caused by violation of ordering in the system of the atomic magnetic moments is compared with the change of entropy of a magnetic subsystem calculated from calorimetric data. Analytical expansion for calculation of a magnetic component of a heat capacity by RB{sub 2} magnetisation data at the temperatures of 2–300 K is obtained. - Highlights: • 1 Techniques of synthesis of RE diborides (RB{sub 2}) are developed (R=Tb, Dy, Ho, Er, Lu). • 2 Temperature dependence of magnetisation of diborides at 2–300 K is determined. • 3 Calculation method of RB{sub 2} magnetic heat capacity from magnetic data is obtained.

  9. The thermal stability of magnetically exchange coupled MnBi/FeCo composites at electric motor working temperature

    Science.gov (United States)

    Cheng, Ye; Wang, Hongying; Li, Zhigang; Liu, Wanhui; Bao, Ilian

    2018-04-01

    The magnetically exchange coupled MnBi/FeCo composites were synthesized through a magnetic self-assembly process. The MnBi/FeCo composites were then hot pressed in a magnetic field to form magnets. The thermal stability of the magnets were tested by annealing at electric motor working temperature of 200 °C for 20, 40 and 60 h, respectively. It was found that after heating for 20 h, there was negligible change in its hysteresis loop. However, when the heating time was increased 40 and 60 h, the magnetic hysteresis loops presented two-phase magnetic behaviors, and the maximum energy products of the magnet were decreased. This research showed that the magnetically exchange coupled MnBi/FeCo composites had low thermal stability at electric motor working temperature.

  10. Noise spectroscopy of CoFeB/MgO/CoFeB magnetic tunnel junctions in the presence of thermal gradients

    Energy Technology Data Exchange (ETDEWEB)

    Liebing, N. [Physikalisch-Technische Bundesanstalt, Bundesallee 100, d-38116 Braunschweig (Germany); Serrano-Guisan, S., E-mail: santiago.serrano-guisan@inl.int [International Iberian Nanotechnology Laboratory, Avenida Mestre Jose Veiga, 4715-330 Braga (Portugal); Rott, K.; Reiss, G. [University of Bielefeld, Department of Physics, Univesitätesstr. 25, d-33615 Bielefeld (Germany); Schumacher, H.W., E-mail: hans.w.schumacher@ptb.de [Physikalisch-Technische Bundesanstalt, Bundesallee 100, d-38116 Braunschweig (Germany)

    2016-02-15

    We present experimental data of the precessional dynamics of the free layer of CoFeB/MgO/CoFeB based magnetic tunnel junctions (MTJ) in the presence of thermal gradients across the MTJ. The free layer precession is investigated by noise spectroscopy. Thermal gradients of the order of tens of mK/nm across the MTJ are generated by electrical heating. Without applied thermal gradients we find spin transfer torque modified magnetization precession. With increasing thermal gradients we generally observe a decrease of the precession frequency which could be related to an increasing overall free layer temperature. However an asymmetry of the line width behavior for parallel and antiparallel orientation points towards additional effects beyond thermal activation. This could be a hint for the modification of the precessional dynamics in magnetic tunnel junctions by thermal spin torques. - Highlights: • Thermal gradients induced magnetization dynamics on MTJ structures are explored. • Magnetic noise spectroscopy is carried out to study the efficiency of such effects. • A decrease of resonance frequency is observed at both MTJ states for large ∇T. • An asymmetric linewidth behavior is observed for both MTJ states under ∇T. • Additional thermal effects beyond thermal activation must be considered.

  11. Rapid microwave-assisted regeneration of magnetic carbon nanotubes loaded with p-nitrophenol

    International Nuclear Information System (INIS)

    Cui, Chunyue; Zheng, Qingzhu; Han, Yanhe; Xin, Yanjun

    2015-01-01

    Highlights: • Magnetic CNTs material was successfully synthesized. • Magnetic CNTs have high fast adsorption rate and adsorption capacity. • Magnetic CNTs can be easily separated from the water by external magnetic field. • Magnetic CNTs can be recycled by MW irradiation regeneration. - Abstract: A novel magnetic carbon nanotubes (CNTs) adsorbent with good sorption, magnetic separability, and microwave (MW) regeneration properties was prepared successfully using thermal decomposition. The magnetic CNTs were characterized using transmission electron microscopy, energy dispersive X-ray, nitrogen adsorption (Brunauer–Emmett–Teller surface area), and X-ray diffraction and their magnetic properties were measured using a vibrating sample magnetometer. Magnetic nanoparticles (≈10 nm diameter) were dispersed uniformly on the CNTs with a magnetic CNTs surface area of 146.7 m 2 g −1 and a saturation magnetization of 21.11 emu g −1 . When the magnetic CNTs were used in the sorption of p-nitrophenol, the equilibrium time was 20 min and the sorption isotherms fit the Freundlich isotherm well. The spent magnetic CNTs could be separated magnetically and be regenerated by MW irradiation. After six adsorption and MW regeneration cycles (at 850 W for 180 s), the adsorption capacity of the magnetic CNTs was higher than that of the virgin magnetic CNTs with a low carbon loss

  12. Magnetic Properties Studies on Thermal Aged Fe-Cu Alloys for the Simulation of Radiation Damage

    Energy Technology Data Exchange (ETDEWEB)

    Lee, C. K.; Kishore, M.B.; Park, D. G. [KAERI, Daejeon (Korea, Republic of); Son, De Rac. [Hannam University, Daejeon (Korea, Republic of)

    2016-05-15

    We evaluated the changes in magnetic properties due to cold rolling and thermal ageing of a Fe-1%Cu model alloy in this study. Initially, the alloy was 10% cold rolled, and isothermally aged at 400 .deg. C for 1, 10, 100 and 1000 hr. The samples were prepared at various thermal aging conditions and all the conditions were interpreted. The hysteresis loops, Magnetic Barkhausen noise (BN). The change of magnetic properties can be interpreted in terms of the domain wall motion and dislocation dynamics associated with copper rich precipitates (CRPs).The results were interpreted in terms of ageing time dependence of the precipitates evolution such as the volume fraction and size distribution. In order to evaluate the radiation embrittlement of RPV steel, A Cold rolled Fe-Cu model Alloy was prepared, The prepared samples were thermally aged by annealing at 400 .deg. C for various times, the magnetic properties of the annealed samples were measured, The Barkhausen noise and BH Loop shows a considerable trend corresponding to the Ageing time. The magnetic properties were interpreted and correlated to the CRPs formed through annealing process.

  13. Magnetic and thermal properties of amorphous TbFeCo alloy films

    Science.gov (United States)

    Wang, Ke; Dong, Shuo; Huang, Ya; Qiu, Yuzhen

    2017-07-01

    Amorphous TbFeCo material with perpendicular magnetic anisotropy is currently attracting more attention for potential applications in spintronic devices and logic memories. We systematically investigate magnetic, structural, thermal, optical and electrical properties of TbFeCo alloy films. It shows out-of-plane easy axis of the films turns into in-plane orientation after annealing. Significant increase in saturation magnetization in the temperature range between 400 and 450 °C is revealed by thermomagnetic measurements. The occurrence of crystallization and oxidation at high temperatures is confirmed by X-ray diffraction measurements. Pronounced changes in optical reflectance and sheet resistance are observed with temperature, in line with structural relaxation and change. The activation barriers for crystallization and oxidation are determined to be 1.01 eV and 0.83 eV, respectively, for FeCo-rich and Tb-rich samples. Better thermal stability against crystallization and oxidation is demonstrated in the FeCo-rich sample than the Tb-rich type. Our results provide some useful information for the alloy used in device fabrication.

  14. Mercury's thermal history and the generation of its magnetic field

    International Nuclear Information System (INIS)

    Schubert, G.; Ross, M.N.; Stevenson, D.J.; Spohn, T.

    1988-01-01

    Thermal history of Mercury's interior is examined using the model of Stevenson et al. (1983), extended to include the effects of tidal heating in Mercury's solid inner core. The implications of Mercury's thermal history for the source of the planet's magnetic field are discussed. It is shown that the major results of this model are similar to the results obtained with the Stevenson et al. model, except for the addition of inner-core tidal dissipation. It is concluded that the extended model properly characterizes Mercury's internal structure and thermal history, and that the criteria for dynamo generation are not properly satisfied. Alternative explanations, including the possibility of a weak thermoelectric dynamo, are examined

  15. The Pulse Thermal Processing of NdFeB-Based Nanocomposite Magnets

    Energy Technology Data Exchange (ETDEWEB)

    Jin, Z. Q. [University of Texas; Wang, Z. L. [Georgia Institute of Technology; Liu, J. P. [University of Texas; Kadolkar, Puja [ORNL; Ott, Ronald D [ORNL

    2006-01-01

    Pulse-thermal processing (PTP) based on high-density plasma arc lamp technology has been utilized to crystallize melt-spun NdFeB-based amorphous ribbons to form magnetic nanocomposites consisting of Nd{sub 2}Fe{sub 14}B and {alpha}-Fe phases. After applying suitable pulses, the NdFeB-based ribbons were developed with hard magnetic properties. The highest coercivity can be obtained for ribbons with a thickness of 40 {micro}m after PTP treatments consisting of a 400 A pulse for 0.25 s for ten times. The correlation between PTP parameters and magnetic properties indicates that PTP is an effective approach to control the structure and properties of nanostructured magnetic materials.

  16. Thermal neutron moderating device

    International Nuclear Information System (INIS)

    Takigami, Hiroyuki.

    1995-01-01

    In a thermal neutron moderating device, superconductive coils for generating magnetic fields capable of applying magnetic fields vertical to the longitudinal direction of a thermal neutron passing tube, and superconductive coils for magnetic field gradient for causing magnetic field gradient in the longitudinal direction of the thermal neutron passing tube are disposed being stacked at the outside of the thermal neutron passing tube. When magnetic field gradient is present vertically to the direction of a magnetic moment, thermal neutrons undergo forces in the direction of the magnetic field gradient in proportion to the magnetic moment. Then, the magnetic moment of the thermal neutrons is aligned with the direction vertical to the passing direction of the thermal neutrons, to cause the magnetic field gradient in the passing direction of the thermal neutrons. The speed of the thermal neutrons can be optionally selected and the wavelength can freely be changed by applying forces to the thermal neutrons and changing the extent and direction of the magnetic field gradient. Superconductive coils are used as the coils for generating magnetic fields and the magnetic field gradient in order to change extremely high energy of the thermal neutrons. (N.H.)

  17. Effects on heat transfer of multiphase magnetic fluid due to circular magnetic field over a stretching surface with heat source/sink and thermal radiation

    Directory of Open Access Journals (Sweden)

    A. Zeeshan

    Full Text Available The purpose of the current article is to explore the boundary layer heat transport flow of multiphase magnetic fluid with solid impurities suspended homogeneously past a stretching sheet under the impact of circular magnetic field. Thermal radiation effects are also taken in account. The equations describing the flow of dust particles in fluid along with point dipole are modelled by employing conservation laws of mass, momentum and energy, which are then converted into non-linear coupled differential equations by mean of similarity approach. The transformed ODE’s are tackled numerically with the help of efficient Runga-Kutta method. The influence of ferromagnetic interaction parameter, viscous dissipation, fluid-particle interaction parameter, Eckert number, Prandtl number, thermal radiation parameter and number of dust particles, heat production or absorption parameter with the two thermal process namely, prescribed heat flux (PHF or prescribed surface temperature (PST are observed on temperature and velocity profiles. The value of skin-friction coefficient and Nusselt number are calculated for numerous physical parameters. Present results are correlated with available for a limited case and an excellent agreement is found. Keywords: Ferromagnetic interaction parameter, Dusty magnetic fluid, stretching sheet, Magnetic dipole, Heat source/sink, Thermal radiation

  18. Repair effect on patterned CoFeB-based magnetic tunneling junction using rapid thermal annealing

    International Nuclear Information System (INIS)

    Wu, K.-M.; Wang, Y.-H.; Chen, Wei-Chuan; Yang, S.-Y.; Shen, Kuei-Hung; Kao, M.-J.; Tsai, M.-J.; Kuo, C.-Y.; Wu, J.-C.; Horng, Lance

    2007-01-01

    Rapid thermal treatment without applying magnetic field reconstructing magnetic property of Co 60 Fe 20 B 20 was studied through magnetoresistance (R-H) measurement. In this paper, we report that the switching behaviors of CoFeB were obviously improved through rapid thermal annealing for only a brief 5 min. The squareness and reproduction of minor R-H loops were enhanced from 100 deg. C to 250 deg. C . Tunneling magnetoresistance (TMR) that is about 35% in the as-etched cells increases up to 44% after 250 deg. C rapid annealing and still shows about 25% TMR even after 400 deg. C treating. Therefore, repair purpose annealing is some what different from crystallizing purpose annealing. Applying magnetic field during repair annealing was not necessary. Brief thermal treatment improves CoFeB switching behavior indeed, and causes less damage at high temperature

  19. Many particle magnetic dipole-dipole and hydrodynamic interactions in magnetizable stent assisted magnetic drug targeting

    International Nuclear Information System (INIS)

    Cregg, P.J.; Murphy, Kieran; Mardinoglu, Adil; Prina-Mello, Adriele

    2010-01-01

    The implant assisted magnetic targeted drug delivery system of Aviles, Ebner and Ritter is considered both experimentally (in vitro) and theoretically. The results of a 2D mathematical model are compared with 3D experimental results for a magnetizable wire stent. In this experiment a ferromagnetic, coiled wire stent is implanted to aid collection of particles which consist of single domain magnetic nanoparticles (radius ∼10nm). In order to model the agglomeration of particles known to occur in this system, the magnetic dipole-dipole and hydrodynamic interactions for multiple particles are included. Simulations based on this mathematical model were performed using open source C++ code. Different initial positions are considered and the system performance is assessed in terms of collection efficiency. The results of this model show closer agreement with the measured in vitro experimental results and with the literature. The implications in nanotechnology and nanomedicine are based on the prediction of the particle efficiency, in conjunction with the magnetizable stent, for targeted drug delivery.

  20. Optically Detected Magnetic Resonance and Thermal Activation Spectroscopy Study of Organic Semiconductors

    International Nuclear Information System (INIS)

    Chang-Hwan Kim

    2003-01-01

    Organic electronic materials are a new class of emerging materials. Organic light emitting devices (OLEDs) are the most promising candidates for future flat panel display technologies. The photophysical characterization is the basic research step one must follow to understand this new class of materials and devices. The light emission properties are closely related to the transport properties of these materials. The objective of this dissertation is to probe the relation between transport and photophysical properties of organic semiconductors. The transport characteristics were evaluated by using thermally stimulated current and thermally stimulated luminescence techniques. The photoluminescence detected magnetic resonance and photoluminescence quantum yield studies provide valuable photophysical information on this class of materials. OLEDs are already in the market. However, detailed studies on the degradation mechanisms are still lacking. Since both optically detected magnetic resonance and thermal activation spectroscopy probe long-lived defect-related states in organic semiconductors, the combined study generates new insight on the OLED operation and degradation mechanisms

  1. Optically Detected Magnetic Resonance and Thermal Activation Spectroscopy Study of Organic Semiconductors

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Chang-Hwan [Iowa State Univ., Ames, IA (United States)

    2003-01-01

    Organic electronic materials are a new class of emerging materials. Organic light emitting devices (OLEDs) are the most promising candidates for future flat panel display technologies. The photophysical characterization is the basic research step one must follow to understand this new class of materials and devices. The light emission properties are closely related to the transport properties of these materials. The objective of this dissertation is to probe the relation between transport and photophysical properties of organic semiconductors. The transport characteristics were evaluated by using thermally stimulated current and thermally stimulated luminescence techniques. The photoluminescence detected magnetic resonance and photoluminescence quantum yield studies provide valuable photophysical information on this class of materials. OLEDs are already in the market. However, detailed studies on the degradation mechanisms are still lacking. Since both optically detected magnetic resonance and thermal activation spectroscopy probe long-lived defect-related states in organic semiconductors, the combined study generates new insight on the OLED operation and degradation mechanisms.

  2. Thermal properties of a large-bore cryocooled 10 T superconducting magnet for a hybrid magnet

    International Nuclear Information System (INIS)

    Ishizuka, M.; Hamajima, T.; Itou, T.; Sakuraba, J.; Nishijima, G.; Awaji, S.; Watanabe, K.

    2010-01-01

    A cryocooled 10 T superconducting magnet with a 360 mm room temperature bore has been developed for a hybrid magnet. The superconducting magnet cooled by four Gifford-McMahon cryocoolers has been designed to generate a magnetic field of 10 T. Since superconducting wires composed of coils were subjected to large hoop stress over 150 MPa and Nb 3 Sn superconducting wires particularly showed a low mechanical strength due to those brittle property, Nb 3 Sn wires strengthened by NbTi-filaments were developed for the cryocooled superconducting magnet. We have already reported that the hybrid magnet could generate the resultant magnetic field of 27.5 T by adding 8.5 T from the superconducting magnet and 19 T from a water-cooled Bitter resistive magnet, after the water-cooled resistive magnet was inserted into the 360 mm room temperature bore of the cryocooled superconducting magnet. When the hybrid magnet generated the field of 27.5 T, it achieved the high magnetic-force field (B x ∂Bz/∂z) of 4500 T 2 /m, which was useful for magneto-science in high fields such as materials levitation research. In this paper, we particularly focus on the cause that the cryocooled superconducting magnet was limited to generate the designed magnetic field of 10 T in the hybrid magnet operation. As a result, it was found that there existed mainly two causes as the limitation of the magnetic field generation. One was a decrease of thermal conductive passes due to exfoliation from the coil bobbin of the cooling flange. The other was large AC loss due to both a thick Nb 3 Sn layer and its large diameter formed on Nb-barrier component in Nb 3 Sn wires.

  3. A new application and experimental validation of moulding technology for ferrite magnet assisted synchronous reluctance machine

    DEFF Research Database (Denmark)

    Wu, Qian; Lu, Kaiyuan; Rasmussen, Peter Omand

    2016-01-01

    This paper introduces a new application of moulding technology to the installation of ferrite magnet material into the rotor flux barriers of Ferrite Magnet Assisted Synchronous Reluctance Machine (FASynRM). The feasibility of this application with respect to manufacturing process and motor...

  4. Improvement of the magnetic property, thermal stability and corrosion resistance of the sintered Nd-Fe-B magnets with Dy{sub 80}Al{sub 20} addition

    Energy Technology Data Exchange (ETDEWEB)

    Zhou, Beibei; Li, Xiangbin; Liang, Xiaolin [School of Physics and Technology, Wuhan University, Wuhan, Hubei (China); Yan, Gaolin, E-mail: gaolinyan@whu.edu.cn [School of Physics and Technology, Wuhan University, Wuhan, Hubei (China); Chen, Kan; Yan, Aru [Zhejiang Province Key Laboratory of Magnetic Materials and Application Technology, Key Laboratory of Magnetic Materials and Devices, Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo, Zhejiang (China)

    2017-05-01

    To improve the coercivity and thermal stability of the Nd-Fe-B sintered magnets simultaneously, the Dy{sub 80}Al{sub 20} (at%) powders with low melting point were introduced into the Nd-Fe-B magnets. Additionally, the magnetic properties, microstructure and thermal stability of the sintered magnets with different amounts of Dy{sub 80}Al{sub 20} were investigated. By adding a small amount of Dy{sub 80}Al{sub 20}, the coercivity was significantly increased from 12.72 to 21.75 kOe. As indicated by the microstructure analysis, a well-developed core-shell structure was formed in the magnets with the addition of Dy{sub 80}Al{sub 20}. The improvement of magnetic properties could be attributed to the refined and uniform matrix phase, continuous grain boundaries and a (Nd, Dy){sub 2}Fe{sub 14}B hardening shell surrounding the matrix phase grains. With the addition of 0–4 wt% Dy{sub 80}Al{sub 20} powder, the reversible temperature coefficients of remanence (α) and coercivity (β) of the magnets could be improved from −0.117 to −0.108%/°C and −0.74 to −0.66%/°C in the range of 20–100 °C, respectively. Additionally, the irreversible loss of magnetic flux (hirr) decreased sharply as Dy{sub 80}Al{sub 20} powder was added. The results of temperature-dependent magnetic properties suggest that, the thermal stability of the magnets was effectively improved with the intergranular addition of Dy{sub 80}Al{sub 20} alloy. Also, the corrosion resistance was found to be improved through small addition of Dy{sub 80}Al{sub 20} powders This was partly due to the stability enhancement of the (Pr, Nd)-rich intergranular phase by Dy{sub 80}Al{sub 20}. - Highlights: • We successfully introduced the Dy{sub 80}Al{sub 20} alloy into the Nd-Fe-B magnets. • The magnetic properties and thermal stability of the Nd-Fe-B magnets were improved. • The corrosion resistance of the Nd-Fe-B magnets were improved.

  5. Nanoscale thermal transport. II. 2003-2012

    Science.gov (United States)

    Cahill, David G.; Braun, Paul V.; Chen, Gang; Clarke, David R.; Fan, Shanhui; Goodson, Kenneth E.; Keblinski, Pawel; King, William P.; Mahan, Gerald D.; Majumdar, Arun; Maris, Humphrey J.; Phillpot, Simon R.; Pop, Eric; Shi, Li

    2014-03-01

    A diverse spectrum of technology drivers such as improved thermal barriers, higher efficiency thermoelectric energy conversion, phase-change memory, heat-assisted magnetic recording, thermal management of nanoscale electronics, and nanoparticles for thermal medical therapies are motivating studies of the applied physics of thermal transport at the nanoscale. This review emphasizes developments in experiment, theory, and computation in the past ten years and summarizes the present status of the field. Interfaces become increasingly important on small length scales. Research during the past decade has extended studies of interfaces between simple metals and inorganic crystals to interfaces with molecular materials and liquids with systematic control of interface chemistry and physics. At separations on the order of ˜ 1 nm , the science of radiative transport through nanoscale gaps overlaps with thermal conduction by the coupling of electronic and vibrational excitations across weakly bonded or rough interfaces between materials. Major advances in the physics of phonons include first principles calculation of the phonon lifetimes of simple crystals and application of the predicted scattering rates in parameter-free calculations of the thermal conductivity. Progress in the control of thermal transport at the nanoscale is critical to continued advances in the density of information that can be stored in phase change memory devices and new generations of magnetic storage that will use highly localized heat sources to reduce the coercivity of magnetic media. Ultralow thermal conductivity—thermal conductivity below the conventionally predicted minimum thermal conductivity—has been observed in nanolaminates and disordered crystals with strong anisotropy. Advances in metrology by time-domain thermoreflectance have made measurements of the thermal conductivity of a thin layer with micron-scale spatial resolution relatively routine. Scanning thermal microscopy and thermal

  6. Enhanced performance of thermal-assisted electron field emission based on barium oxide nanowire

    Energy Technology Data Exchange (ETDEWEB)

    Cui, Yunkang [Department of Mathematics and Physics, Nanjing Institute of technology, Nanjing, 211167 (China); Chen, Jing, E-mail: chenjingmoon@gmail.com [School of Electronic Science & Engineering, Southeast University, Nanjing, 210096 (China); Zhang, Yuning; Zhang, Xiaobing; Lei, Wei; Di, Yunsong [School of Electronic Science & Engineering, Southeast University, Nanjing, 210096 (China); Zhang, Zichen, E-mail: zz241@ime.ac.cn [Integrated system for Laser applications Group, Institute of Microelectronics of Chinese Academy of Sciences, 100029, Beijing (China)

    2017-02-28

    Highlights: • A possible mechanism for thermal-assisted electric field was demonstrated. • A new path for the architecture of the novel nanomaterial and methodology for its potential application in the field emission device area was provided. • The turn-on field, the threshold field and the field emission current density were largely related to the temperature of the cathode. • The relationship between the work function of emitter material and the temperature of emitter was found. - Abstract: In this paper, thermal-assisted field emission properties of barium oxide (BaO) nanowire synthesized by a chemical bath deposition method were investigated. The morphology and composition of BaO nanowire were characterized by field emission scanning electron microscopy (FESEM), high resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SED), X-ray diffraction (XRD), and energy dispersive X-ray spectrometer (EDX) respectively. The turn-on field, threshold field and the emission current density could be affected relatively due to the thermal-assisted effect when the electric field was applied, in the meanwhile, the turn-on field for BaO nanowire was measured to be decreased from 1.12 V/μm to 0.66 V/μm when the temperature was raised from 293 K to 593 K, whereas for the threshold field was found to decrease from 3.64 V/μm to 2.12 V/μm. The improved performance was demonstrated due to the reduced work function of the BaO nanowire as the agitation temperature increasing, leading to the higher probability of electrons tunneling through the energy barrier and enhancement of the field emission properties of BaO emitters.

  7. Enhanced performance of thermal-assisted electron field emission based on barium oxide nanowire

    International Nuclear Information System (INIS)

    Cui, Yunkang; Chen, Jing; Zhang, Yuning; Zhang, Xiaobing; Lei, Wei; Di, Yunsong; Zhang, Zichen

    2017-01-01

    Highlights: • A possible mechanism for thermal-assisted electric field was demonstrated. • A new path for the architecture of the novel nanomaterial and methodology for its potential application in the field emission device area was provided. • The turn-on field, the threshold field and the field emission current density were largely related to the temperature of the cathode. • The relationship between the work function of emitter material and the temperature of emitter was found. - Abstract: In this paper, thermal-assisted field emission properties of barium oxide (BaO) nanowire synthesized by a chemical bath deposition method were investigated. The morphology and composition of BaO nanowire were characterized by field emission scanning electron microscopy (FESEM), high resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SED), X-ray diffraction (XRD), and energy dispersive X-ray spectrometer (EDX) respectively. The turn-on field, threshold field and the emission current density could be affected relatively due to the thermal-assisted effect when the electric field was applied, in the meanwhile, the turn-on field for BaO nanowire was measured to be decreased from 1.12 V/μm to 0.66 V/μm when the temperature was raised from 293 K to 593 K, whereas for the threshold field was found to decrease from 3.64 V/μm to 2.12 V/μm. The improved performance was demonstrated due to the reduced work function of the BaO nanowire as the agitation temperature increasing, leading to the higher probability of electrons tunneling through the energy barrier and enhancement of the field emission properties of BaO emitters.

  8. Atom interferometry in space: Thermal management and magnetic shielding

    Energy Technology Data Exchange (ETDEWEB)

    Milke, Alexander; Kubelka-Lange, André; Gürlebeck, Norman, E-mail: norman.guerlebeck@zarm.uni-bremen.de; Rievers, Benny; Herrmann, Sven [Center of Applied Space Technology and Microgravity (ZARM), University Bremen, Am Fallturm, 28359 Bremen (Germany); Schuldt, Thilo [DLR Institute for Space Systems, Robert-Hooke-Str. 7, 28359 Bremen (Germany); Braxmaier, Claus [Center of Applied Space Technology and Microgravity (ZARM), University Bremen, Am Fallturm, 28359 Bremen (Germany); DLR Institute for Space Systems, Robert-Hooke-Str. 7, 28359 Bremen (Germany)

    2014-08-15

    Atom interferometry is an exciting tool to probe fundamental physics. It is considered especially apt to test the universality of free fall by using two different sorts of atoms. The increasing sensitivity required for this kind of experiment sets severe requirements on its environments, instrument control, and systematic effects. This can partially be mitigated by going to space as was proposed, for example, in the Spacetime Explorer and Quantum Equivalence Principle Space Test (STE-QUEST) mission. However, the requirements on the instrument are still very challenging. For example, the specifications of the STE-QUEST mission imply that the Feshbach coils of the atom interferometer are allowed to change their radius only by about 260 nm or 2.6 × 10{sup −4} % due to thermal expansion although they consume an average power of 22 W. Also Earth's magnetic field has to be suppressed by a factor of 10{sup 5}. We show in this article that with the right design such thermal and magnetic requirements can indeed be met and that these are not an impediment for the exciting physics possible with atom interferometers in space.

  9. Radiation- and phonon-bottleneck--induced tunneling in the Fe8 single-molecule magnet

    Science.gov (United States)

    Bal, M.; Friedman, Jonathan R.; Chen, W.; Tuominen, M. T.; Beedle, C. C.; Rumberger, E. M.; Hendrickson, D. N.

    2008-04-01

    We measure magnetization changes in a single crystal of the single-molecule magnet Fe8 when exposed to intense, short (spin dynamics, allowing observation of thermally assisted resonant tunneling between spin states at the 100 ns time scale. Detailed numerical simulations quantitatively reproduce the data and yield a spin-phonon relaxation time T1~40 ns.

  10. Thermal stability analysis and modelling of advanced perpendicular magnetic tunnel junctions

    Science.gov (United States)

    Van Beek, Simon; Martens, Koen; Roussel, Philippe; Wu, Yueh Chang; Kim, Woojin; Rao, Siddharth; Swerts, Johan; Crotti, Davide; Linten, Dimitri; Kar, Gouri Sankar; Groeseneken, Guido

    2018-05-01

    STT-MRAM is a promising non-volatile memory for high speed applications. The thermal stability factor (Δ = Eb/kT) is a measure for the information retention time, and an accurate determination of the thermal stability is crucial. Recent studies show that a significant error is made using the conventional methods for Δ extraction. We investigate the origin of the low accuracy. To reduce the error down to 5%, 1000 cycles or multiple ramp rates are necessary. Furthermore, the thermal stabilities extracted from current switching and magnetic field switching appear to be uncorrelated and this cannot be explained by a macrospin model. Measurements at different temperatures show that self-heating together with a domain wall model can explain these uncorrelated Δ. Characterizing self-heating properties is therefore crucial to correctly determine the thermal stability.

  11. Magnetic, thermal and luminescence properties in room-temperature nanosecond electron-irradiated various metal oxide nanopowders

    Science.gov (United States)

    Sokovnin, S. Yu; Balezin, M. E.; Il’ves, V. G.

    2018-03-01

    By means of pulsed electron beam evaporation in vacuum of targets non-magnetic, in bulk state, Al2O3 and YSZ (ZrO2-8% Y2O3) oxides, magnetic nanopowders (NPs) with a high specific surface were produced. The NPs were subsequently irradiated in air by electrons with energy of 700 keV, using a URT-1 accelerator for 15 and 30 minutes. The magnetic, thermal, and pulsed cathodoluminescence (PCL) characteristics of NPs were measured before and after irradiation. It was established that the electron irradiation non-monotonically changes the magnetization of the pristine samples. To the contrary, a clear correlation between the intensity of PCL and the irradiation doses is found in the oxides. There was a decrease in the intensity of PCL after irradiation. Luminescent and thermal properties reflect the transformation of structural defects in NPs more strongly after the exposure to a pulsed electron beam in comparison with corresponding changes of the NPs magnetic response.

  12. Wiggler magnetic field assisted third harmonic generation in expanding clusters

    Science.gov (United States)

    Vij, Shivani

    2018-04-01

    A simple theoretical model is constructed to study the wiggler magnetic field assisted third harmonic generation of intense short pulse laser in a cluster in its expanding phase. The ponderomotive force of laser causes density perturbations in cluster electron density which couples with wiggler magnetic field to produce a nonlinear current that generates transverse third harmonic. An intense short pulse laser propagating through a gas embedded with atomic clusters, converts it into hot plasma balls via tunnel ionization. Initially, the electron plasma frequency inside the clusters ω pe > \\sqrt{3}{ω }1 (with ω 1 being the frequency of the laser). As the cluster expands under Coulomb force and hydrodynamic pressure, ω pe decreases to \\sqrt{3}{ω }1. At this time, there is resonant enhancement in the efficiency of the third harmonic generation. The efficiency of third harmonic generation is enhanced due to cluster plasmon resonance and by phase matching due to wiggler magnetic field. The effect of cluster size on the expansion rate is studied to observe that the clusters of different radii would expand differently. The impact of laser intensity and wiggler magnetic field on the efficiency of third harmonic generation is also explored.

  13. Evolution of free volume in ultrasoft magnetic FeZrN films during thermal annealing

    NARCIS (Netherlands)

    Chechenin, NG; van Veen, A; Schut, H; Chezan, AR; Boerma, DO; Vystavel, T; De Hosson, JTM; DeHaven, PW; Field, DP; Harkness, SD; Sutliff, JA; Szpunar, JA; Tang, L; Thomson, T; Vaudin, MD

    2002-01-01

    The thermal stability of nanocrystalline ultra-soft magnetic (Fe98Zr2)(1-x)N-x films with x=0.10-0.25 was studied using high-resolution transmission electron microscopy (HRTEM), positron beam analysis (PBA) and thermal desorption spectrometry (TDS). The results demonstrate that grain growth during

  14. Thermal performance analysis of a direct-expansion solar-assisted heat pump water heater

    International Nuclear Information System (INIS)

    Kong, X.Q.; Zhang, D.; Li, Y.; Yang, Q.M.

    2011-01-01

    A direct-expansion solar-assisted heat pump water heater (DX-SAHPWH) is described, which can supply hot water for domestic use during the whole year. The system mainly employs a bare flat-plate collector/evaporator with a surface area of 4.2 m 2 , an electrical rotary-type hermetic compressor, a hot water tank with the volume of 150 L and a thermostatic expansion valve. R-22 is used as working fluid in the system. A simulation model based on lumped and distributed parameter approach is developed to predict the thermal performance of the system. Given the structure parameters, meteorological parameters, time step and final water temperature, the numerical model can output operational parameters, such as heat capacity, system COP and collector efficiency. Comparisons between the simulation results and the experimental measurements show that the model is able to give satisfactory predictions. The effect of various parameters, including solar radiation, ambient temperature, wind speed and compressor speed, has been analyzed on the thermal performance of the system. -- Highlights: ► A direct-expansion solar-assisted heat pump water heater (DX-SAHPWH) is described. ► A simulation model based on lumped and distributed parameter approach is developed to predict the thermal performance of the system. ► The numerical model can output operational parameters, such as heat capacity, system COP and collector efficiency. ► Comparisons between the simulation results and the experimental measurements show that the model is able to give satisfactory predictions. ► The effect of various parameters has been analyzed on the thermal performance of the system.

  15. Synthesis, characterization, temperature dependent electrical and magnetic properties of Ca{sub 3}Co{sub 4}O{sub 9} by a starch assisted sol–gel combustion method

    Energy Technology Data Exchange (ETDEWEB)

    Agilandeswari, K.; Ruban Kumar, A., E-mail: arubankumar@vit.ac.in

    2014-09-01

    In this present work we discussed the synthesis of pure Ca{sub 3}Co{sub 4}O{sub 9} ceramic powder by a starch assisted sol–gel combustion method. The products were characterized by powder X-ray diffraction (XRD), thermogravimetric and differential thermal analyses (TGA–DTA), Fourier transformation infrared spectroscopy (FTIR), scanning electron microscope (SEM) and UV–visible diffuse reflectance spectroscopy (DRS). X-ray diffraction pattern confirmed the formation of single phase Ca{sub 3}Co{sub 4}O{sub 9} at a sintering temperature of 1073 K, and it is also confirmed in the thermal analysis. SEM images indicate the presence of diffused microporous sphere like morphology and the grain sizes are in the range of 150–300 nm. Optical properties of Ca{sub 3}Co{sub 4}O{sub 9} ceramic show a band gap at an energy level of 2.10 eV. A maximum electrical resistivity of 0.002 mΩ cm was exhibited by Ca{sub 3}Co{sub 4}O{sub 9} that was decreased to 0.0012 mΩ cm, when the temperature increased from 300 K to 473 K. Dielectric studies were conducted at various temperatures from room temperature to 673 K and the results indicate that the space charge polarization contributes to the conduction mechanism. It also shows that the dielectric relaxation with activation energy is 0.96 eV. The magnetic properties as a function of temperature represent the ferri-paramagnetic phase transition at above 50 K. M–H curve shows the hysteresis loop with saturation magnetization (M{sub s}) and confirms the presence of soft magnetic materials. - Highlights: • Ca{sub 3}Co{sub 4}O{sub 9} has not yet been reported by this starch assisted sol–gel combustion method. • SEM image shows microporous sphere like morphology. • The optical and dielectric properties of Ca{sub 3}Co{sub 4}O{sub 9} sample were studied. • Temperature dependent magnetic property has been studied for Ca{sub 3}Co{sub 4}O{sub 9}. It behaves as a soft magnetic material at 5 K.

  16. Coupled granular/continuous medium for thermally stable perpendicular magnetic recording

    International Nuclear Information System (INIS)

    Sonobe, Y.; Weller, D.; Ikeda, Y.; Takano, K.; Schabes, M.E.; Zeltzer, G.; Do, H.; Yen, B.K.; Best, M.E.

    2001-01-01

    We studied coupled granular/continuous (CGC) perpendicular media consisting of a continuous multilayer structure and a granular layer. The addition of Co/Pt multilayers decreased the nucleation field from 200 to -1800 Oe and increased the squareness from 0.9 to 1.0. The moment decay at room temperature was significantly reduced from -4.8% to -0.05% per decade. At elevated temperatures, strong exchange coupling between a granular layer and a continuous layer is needed for thermal stability. The exchange-coupled continuous layer reduces thermal demagnetization as it effectively increases the grain size, tightens the grain distribution, and prevents the reversal of individual grains. Magnetic Force Microscope image showed a larger magnetic cluster size for the CGC structure. Compared to the CoCr 18 Pt 12 medium, the CGC medium had 2.3 dB higher output. However, the noise for the CGC medium increased with the recording density, while the noise for the CoCr 18 Pt 12 medium remained constant from 4 to 15 kfc/mm. Further optimization and noise reduction are still required for future high density recording

  17. Coupled granular/continuous medium for thermally stable perpendicular magnetic recording

    Science.gov (United States)

    Sonobe, Y.; Weller, D.; Ikeda, Y.; Takano, K.; Schabes, M. E.; Zeltzer, G.; Do, H.; Yen, B. K.; Best, M. E.

    2001-10-01

    We studied coupled granular/continuous (CGC) perpendicular media consisting of a continuous multilayer structure and a granular layer. The addition of Co/Pt multilayers decreased the nucleation field from 200 to -1800 Oe and increased the squareness from 0.9 to 1.0. The moment decay at room temperature was significantly reduced from -4.8% to -0.05% per decade. At elevated temperatures, strong exchange coupling between a granular layer and a continuous layer is needed for thermal stability. The exchange-coupled continuous layer reduces thermal demagnetization as it effectively increases the grain size, tightens the grain distribution, and prevents the reversal of individual grains. Magnetic Force Microscope image showed a larger magnetic cluster size for the CGC structure. Compared to the CoCr 18Pt 12 medium, the CGC medium had 2.3 dB higher output. However, the noise for the CGC medium increased with the recording density, while the noise for the CoCr 18Pt 12 medium remained constant from 4 to 15 kfc/mm. Further optimization and noise reduction are still required for future high density recording.

  18. Nanoscale thermal transport. II. 2003–2012

    International Nuclear Information System (INIS)

    Cahill, David G.; Braun, Paul V.; Chen, Gang; Clarke, David R.; Fan, Shanhui; Goodson, Kenneth E.; Keblinski, Pawel; King, William P.; Mahan, Gerald D.; Majumdar, Arun; Maris, Humphrey J.; Phillpot, Simon R.; Pop, Eric; Shi, Li

    2014-01-01

    A diverse spectrum of technology drivers such as improved thermal barriers, higher efficiency thermoelectric energy conversion, phase-change memory, heat-assisted magnetic recording, thermal management of nanoscale electronics, and nanoparticles for thermal medical therapies are motivating studies of the applied physics of thermal transport at the nanoscale. This review emphasizes developments in experiment, theory, and computation in the past ten years and summarizes the present status of the field. Interfaces become increasingly important on small length scales. Research during the past decade has extended studies of interfaces between simple metals and inorganic crystals to interfaces with molecular materials and liquids with systematic control of interface chemistry and physics. At separations on the order of ∼1 nm, the science of radiative transport through nanoscale gaps overlaps with thermal conduction by the coupling of electronic and vibrational excitations across weakly bonded or rough interfaces between materials. Major advances in the physics of phonons include first principles calculation of the phonon lifetimes of simple crystals and application of the predicted scattering rates in parameter-free calculations of the thermal conductivity. Progress in the control of thermal transport at the nanoscale is critical to continued advances in the density of information that can be stored in phase change memory devices and new generations of magnetic storage that will use highly localized heat sources to reduce the coercivity of magnetic media. Ultralow thermal conductivity—thermal conductivity below the conventionally predicted minimum thermal conductivity—has been observed in nanolaminates and disordered crystals with strong anisotropy. Advances in metrology by time-domain thermoreflectance have made measurements of the thermal conductivity of a thin layer with micron-scale spatial resolution relatively routine. Scanning thermal microscopy and

  19. Anomalous Thermal Conductivity and Magnetic Torque Response in the Honeycomb Magnet α -RuCl3

    Science.gov (United States)

    Leahy, Ian A.; Pocs, Christopher A.; Siegfried, Peter E.; Graf, David; Do, S.-H.; Choi, Kwang-Yong; Normand, B.; Lee, Minhyea

    2017-05-01

    We report on the unusual behavior of the in-plane thermal conductivity κ and torque τ response in the Kitaev-Heisenberg material α -RuCl3 . κ shows a striking enhancement with linear growth beyond H =7 T , where magnetic order disappears, while τ for both of the in-plane symmetry directions shows an anomaly at the same field. The temperature and field dependence of κ are far more complex than conventional phonon and magnon contributions, and require us to invoke the presence of unconventional spin excitations whose properties are characteristic of a field-induced spin-liquid phase related to the enigmatic physics of the Kitaev model in an applied magnetic field.

  20. Photon-assisted tunneling in a Fe-8 single-molecule magnet

    OpenAIRE

    Sorace, L.; Wernsdorfer, W.; Thirion, C.; Barra, A. L.; Pacchioni, M.; Mailly, D.; Barbara, B.

    2003-01-01

    The low temperature spin dynamics of a Fe8 Single-Molecule Magnet was studied under circularly polarized electromagnetic radiation allowing us to establish clearly photon-assisted tunneling. This effect, while linear at low power, becomes highly non-linear above a relatively low power threshold. This non-linearity is attributed to the nature of the coupling of the sample to the thermostat.These results are of great importance if such systems are to be used as quantum computers.

  1. Photon-assisted tunneling in a Fe8 single-molecule magnet

    Science.gov (United States)

    Sorace, L.; Wernsdorfer, W.; Thirion, C.; Barra, A.-L.; Pacchioni, M.; Mailly, D.; Barbara, B.

    2003-12-01

    The low-temperature spin dynamics of a Fe8 single-molecule magnet was studied under circularly polarized electromagnetic radiation allowing us to establish clearly photon-assisted tunneling. This effect, while linear at low power, becomes highly nonlinear above a relatively low-power threshold. Heating due to phonon emission, spin-spin interactions, and coherent emission/absorption of photons might lead to the observed nonlinearity. These results are of importance if such systems are to be used as quantum computers.

  2. Damping Dependence of Reversal Magnetic Field on Co-based Nano-Ferromagnetic with Thermal Activation

    Directory of Open Access Journals (Sweden)

    Nadia Ananda Herianto

    2015-02-01

    Full Text Available Currently, hard disk development has used HAMR technology that applies heat to perpendicular media until near Curie temperature, then cools it down to room temperature. The use of HAMR technology is significantly influence by Gilbert damping constants. Damping affects the magnetization reversal and coercivity field. Simulation is used to evaluate magnetization reversal by completing Landau-Lifshitz-Gilbert explicit equation. A strong ferromagnetic cobalt based material with size 50×50×20 nm3 is used which parameters are anisotropy materials 3.51×106 erg/cm3, magnetic saturation 5697.5 G, exchange constant 1×10-7 erg/cm, and various Gilbert damping from 0.09 to 0.5. To observe the thermal effect, two schemes are used which are Reduced Barrier Writing and Curie Point Writing. As a result, materials with high damping is able to reverse the magnetizations faster and reduce the energy barrier. Moreover, it can lower the minimum field to start the magnetizations reversal, threshold field, and probability rate. The heating near Curie temperature has succeeded in reducing the reversal field to 1/10 compared to writing process in absence of thermal field.

  3. Effect of magnetic field on the growth of Be films prepared by thermal evaporation

    International Nuclear Information System (INIS)

    Li, Kai; Luo, Bing-chi; Tan, Xiu-lan; Zhang, Ji-qiang; Wu, Wei-dong; Liu, Ying

    2014-01-01

    Highlights: • The Be films were prepared on Si (1 0 0) substrates with and without a magnetic field by thermal evaporation, respectively. • The grain diameter in the Be film transited from 300 nm to 18 nm by application of the magnetic field. • The surface roughness of the Be film decreased from 61 nm to 3 nm by application of the magnetic field. • The Be film grown with the magnetic field was easily oxidized due to its refined grains and the oxidation was gradually decreased with increasing the etching depth in the film. - Abstract: Grain refinement of beryllium deposits is studied as a significant subject for beryllium capsule in the Inertial Confinement Fusion project. The Be films were prepared on the Si (1 0 0) substrates by thermal evaporation with and without a magnetic field, respectively. The two separate groups of prepared Be films were characterized. The results showed the grain diameter in the Be film transited from 300 nm to 18 nm and the surface roughness of the Be film decreased from 61 nm to 3 nm by application of the magnetic field during the deposition process of Be coating. However, the Be film grown with the magnetic field was easily oxidized in comparison with that grown without magnetic field due to the refined grains, and the oxidation was gradually decreased with the increase of etching depth in the Be film. The reason for grain refinement of Be film was also qualitatively described

  4. Removal of Iron Oxide Scale from Feed-water in Thermal Power Plant by Using Magnetic Separation

    Science.gov (United States)

    Nakanishi, Motohiro; Shibatani, Saori; Mishima, Fumihito; Akiyama, Yoko; Nishijima, Shigehiro

    2017-09-01

    One of the factors of deterioration in thermal power generation efficiency is adhesion of the scale to inner wall in feed-water system. Though thermal power plants have employed All Volatile Treatment (AVT) or Oxygen Treatment (OT) to prevent scale formation, these treatments cannot prevent it completely. In order to remove iron oxide scale, we proposed magnetic separation system using solenoidal superconducting magnet. Magnetic separation efficiency is influenced by component and morphology of scale which changes their property depending on the type of water treatment and temperature. In this study, we estimated component and morphology of iron oxide scale at each equipment in the feed-water system by analyzing simulated scale generated in the pressure vessel at 320 K to 550 K. Based on the results, we considered installation sites of the magnetic separation system.

  5. Combined effect of magnetic field and thermal dispersion on a non-darcy mixed convection

    KAUST Repository

    El-Amin, Mohamed

    2011-05-21

    This paper is devoted to investigate the influences of thermal dispersion and magnetic field on a hot semi-infinite vertical porous plate embedded in a saturated Darcy-Forchheimer-Brinkman porous medium. The coefficient of thermal diffusivity has been assumed to be the sum of the molecular diffusivity and the dynamic diffusivity due to mechanical dispersion. The effects of transverse magnetic field parameter (Hartmann number Ha), Reynolds number Re (different velocities), Prandtl number Pr (different types of fluids) and dispersion parameter on the wall shear stress and the heat transfer rate are discussed. © 2011 Science Press, Institute of Engineering Thermophysics, CAS and Springer-Verlag Berlin Heidelberg.

  6. Combined effect of magnetic field and thermal dispersion on a non-darcy mixed convection

    KAUST Repository

    El-Amin, Mohamed; Sun, Shuyu

    2011-01-01

    This paper is devoted to investigate the influences of thermal dispersion and magnetic field on a hot semi-infinite vertical porous plate embedded in a saturated Darcy-Forchheimer-Brinkman porous medium. The coefficient of thermal diffusivity has been assumed to be the sum of the molecular diffusivity and the dynamic diffusivity due to mechanical dispersion. The effects of transverse magnetic field parameter (Hartmann number Ha), Reynolds number Re (different velocities), Prandtl number Pr (different types of fluids) and dispersion parameter on the wall shear stress and the heat transfer rate are discussed. © 2011 Science Press, Institute of Engineering Thermophysics, CAS and Springer-Verlag Berlin Heidelberg.

  7. Purification of condenser water in thermal power station by superconducting magnetic separation

    International Nuclear Information System (INIS)

    Ha, D.W.; Kwon, J.M.; Baik, S.K.; Lee, Y.J.; Han, K.S.; Ko, R.K.; Sohn, M.H.; Seong, K.C.

    2011-01-01

    Magnetic separation using cryo-cooled Nb-Ti superconducting magnet was applied for the purification of condenser water. Iron oxides in condenser water were effectively removed by superconducting magnetic separation. The effect of magnetic field strength and filter size was determined. Thermal power station is made up of a steam turbine and a steam condenser which need a lot of water. The water of steam condenser should be replaced, since scales consisting of iron oxide mainly are accumulated on the surface of condenser pipes as it goes. Superconducting high gradient magnetic separation (HGMS) system has merits to remove paramagnetic substance like iron oxides because it can generate higher magnetic field strength than electromagnet or permanent magnet. In this paper, cryo-cooled Nb-Ti superconducting magnet that can generate up to 6 T was used for HGMS systems. Magnetic filters were designed by the analysis of magnetic field distribution at superconducting magnets. The result of X-ray analysis showed contaminants were mostly α-Fe 2 O 3 (hematite) and γ-Fe 2 O 3 (maghemite). The higher magnetic field was applied up to 6 T, the more iron oxides were removed. As the wire diameter of magnetic filter decreased, the turbidity removal of the sample was enhanced.

  8. Magnetism and thermal evolution of the terrestrial planets

    International Nuclear Information System (INIS)

    Stevenson, D.J.; Spohn, T.; Schubert, G.

    1983-01-01

    The absence in the cases of Venus and Mars of the substantial intrinsic magnetic fields of the earth and Mercury is considered, in light of thermal history calculations which suggest that, while the cores of Mercury and the earth are continuing to freeze, the cores of Venus and Mars may still be completely liquid. It is noted that completely fluid cores, lacking intrinsic heat sources, are not likely to sustain thermal convection for the age of the solar system, but cool to a subadiabatic, conductive state that cannot maintain a dynamo because of the gravitational energy release and the chemically driven convection that accompany inner core growth. The models presented include realistic pressure- and composition-dependent freezing curves for the core, and material parameters are chosen so that correct present-day values of heat outflow, upper mantle temperature and viscosity, and inner core radius, are obtained for the earth. 116 references

  9. Magnetism and thermal evolution of the terrestrial planets

    Science.gov (United States)

    Stevenson, D. J.; Spohn, T.; Schubert, G.

    1983-01-01

    The absence in the cases of Venus and Mars of the substantial intrinsic magnetic fields of the earth and Mercury is considered, in light of thermal history calculations which suggest that, while the cores of Mercury and the earth are continuing to freeze, the cores of Venus and Mars may still be completely liquid. It is noted that completely fluid cores, lacking intrinsic heat sources, are not likely to sustain thermal convection for the age of the solar system, but cool to a subadiabatic, conductive state that cannot maintain a dynamo because of the gravitational energy release and the chemically driven convection that accompany inner core growth. The models presented include realistic pressure- and composition-dependent freezing curves for the core, and material parameters are chosen so that correct present-day values of heat outflow, upper mantle temperature and viscosity, and inner core radius, are obtained for the earth.

  10. Hysteresis in magnetic materials: the role of structural disorder, thermal relaxation, and dynamic effects

    International Nuclear Information System (INIS)

    Bertotti, G.; Basso, V.; Beatrice, C.; LoBue, M.; Magni, A.; Tiberto, P.

    2001-01-01

    An overview is given of the present understanding of hysteresis phenomena in magnetic materials. The problem is addressed from three approximate viewpoints: the connection between rate-independent hysteresis and micromagnetics; the modifications brought into this picture by thermal relaxation effects; the role of rate-dependent magnetization mechanisms, like eddy-current-damped domain wall motion

  11. Improving the performance of nickel-coated fluorine-doped tin oxide thin films by magnetic-field-assisted laser annealing

    Energy Technology Data Exchange (ETDEWEB)

    Li, Bao-jia, E-mail: li_bjia@126.com [School of Materials Science and Engineering, Jiangsu University, Zhenjiang 212013 (China); Jiangsu Provincial Key Laboratory of Center for Photon Manufacturing Science and Technology, Jiangsu University, Zhenjiang 212013 (China); Huang, Li-jing [School of Materials Science and Engineering, Jiangsu University, Zhenjiang 212013 (China); Jiangsu Provincial Key Laboratory of Center for Photon Manufacturing Science and Technology, Jiangsu University, Zhenjiang 212013 (China); Ren, Nai-fei [Jiangsu Provincial Key Laboratory of Center for Photon Manufacturing Science and Technology, Jiangsu University, Zhenjiang 212013 (China); School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013 (China); Kong, Xia; Cai, Yun-long; Zhang, Jie-lu [Jiangsu Tailong Reduction Box Co. Ltd., Taixing 225400 (China)

    2015-10-01

    Highlights: • Ni/FTO films were prepared by sputtering Ni layers on commercial FTO glass. • The as-prepared Ni/FTO films underwent magnetic-field-assisted laser annealing. • Magnetic field and laser fluence were crucial for improving quality of the films. • All Ni/FTO films displayed enhanced compactness after magnetic laser annealing. • Magnetic laser annealing using a fluence of 0.9 J/cm{sup 2} led to the best film quality. - Abstract: Nickel-coated fluorine-doped tin oxide (Ni/FTO) thin films were prepared by sputtering Ni layers on commercial FTO glass. The as-prepared Ni/FTO films underwent nanosecond pulsed laser annealing in an external magnetic field (0.4 T). The effects of the presence of magnetic field and laser fluence on surface morphology, crystal structure and photoelectric properties of the films were investigated. All the films displayed enhanced compactness after magnetic-field-assisted laser annealing. It was notable that both crystallinity and grain size of the films gradually increased with increasing laser fluence from 0.6 to 0.9 J/cm{sup 2}, and then decreased slightly with an increase in laser fluence to 1.1 J/cm{sup 2}. As a result, the film obtained by magnetic-field-assisted laser annealing using a fluence of 0.9 J/cm{sup 2} had the best overall photoelectric property with an average transmittance of 81.2%, a sheet resistance of 5.5 Ω/sq and a figure of merit of 2.27 × 10{sup −2} Ω{sup −1}, outperforming that of the film obtained by pure laser annealing using the same fluence.

  12. Thermal deposition of intact tetrairon(III) single-molecule magnets in high-vacuum conditions.

    Science.gov (United States)

    Margheriti, Ludovica; Mannini, Matteo; Sorace, Lorenzo; Gorini, Lapo; Gatteschi, Dante; Caneschi, Andrea; Chiappe, Daniele; Moroni, Riccardo; de Mongeot, Francesco Buatier; Cornia, Andrea; Piras, Federica M; Magnani, Agnese; Sessoli, Roberta

    2009-06-01

    A tetrairon(III) single-molecule magnet is deposited using a thermal evaporation technique in high vacuum. The chemical integrity is demonstrated by time-of-flight secondary ion mass spectrometry on a film deposited on Al foil, while superconducting quantum interference device magnetometry and alternating current susceptometry of a film deposited on a kapton substrate show magnetic properties identical to the pristine powder. High-frequency electron paramagnetic resonance spectra confirm the characteristic behavior for a system with S = 5 and a large Ising-type magnetic anisotropy. All these results indicate that the molecules are not damaged during the deposition procedure keeping intact the single-molecule magnet behavior.

  13. Thermal and particle size distribution effects on the ferromagnetic resonance in magnetic fluids

    International Nuclear Information System (INIS)

    Marin, C.N.

    2006-01-01

    Thermal and particle size distribution effects on the ferromagnetic resonance of magnetic fluids were theoretically investigated, assuming negligible interparticle interactions and neglecting the viscosity of the carrier liquid. The model is based on the usual approach for the ferromagnetic resonance description of single-domain magnetic particle systems, which was amended in order to take into account the finite particle size effect, the particle size distribution and the orientation mobility of the particles within the magnetic fluid. Under these circumstances the shape of the resonance line, the resonance field and the line width are found to be strongly affected by the temperature and by the particle size distribution of magnetic fluids

  14. An Overview of the Thermal Calculation and the Cooling Technology for Active Magnetic Bearing

    Science.gov (United States)

    Zhang, Li; Yu, Meiyun; Luo, Yanyan; Liu, Jun; Ren, Yafeng

    2017-10-01

    The cooling process of AMB is that the energy loss is sent out to the outside world when the system is operating. The energy loss transfers to the surrounding medium in the form of heat, which leads to raise the temperature of system components and influences the performance of the system. So it is necessary to study the internal loss of the magnetic bearing system and thermal calculation method. Three kinds of thermal calculation methods are compared, which is important for the design and calculation of cooling. At the same time, the cooling way, the cooling method, and the cooling system is summarized on the basis of cooling technology of active magnetic bearing, and the design method of the cooling system is studied. But for the active magnetic bearing system, when designing the cooling system, heat dissipation of the motor can not be ignored. It is important not only for the performance of the active magnetic bearing system and stable operation, and but also for the improvement of the cooling technology.

  15. Thermally Assisted Macroscopic Quantum Resonance on a Single-Crystal of Mn12-ac

    Science.gov (United States)

    Lionti, F.; Thomas, L.; Ballou, R.; Wernsdorfer, W.; Barbara, B.; Sulpice, A.; Sessoli, R.; Gatteschi, D.

    1997-03-01

    Magnetization measurements have been performed on a single mono-crystal of the molecule Mn12-acetate (L. Thomas, F. Lionti, R. Ballou, R. Sessoli, D. Gatteschi and B. Barbara, Nature, 383, 145 (1996).). Steps were observed in the hysteresis loop for values of the applied field at which level crossings of the collective spin states of each manganese clusters take place. The influence of quartic terms is taken into account. At these fields, the magnetization relaxes at short time scales, being otherwise essentially blocked. This novel behavior is interpreted in terms of resonant quantum tunneling of the magnetization from thermally activated energy levels. Hysteresis loop measurements performed for different field orientations and ac-susceptibility experiments, confirm general trends of this picture.

  16. Numerical study of finned heat pipe-assisted thermal energy storage system with high temperature phase change material

    International Nuclear Information System (INIS)

    Tiari, Saeed; Qiu, Songgang; Mahdavi, Mahboobe

    2015-01-01

    Highlights: • A finned heat pipe-assisted latent heat thermal energy storage system is studied. • The effects of heat pipes spacing and fins geometrical features are investigated. • Smaller heat pipes spacing and longer fins improve the melting rate. • The optimal heat pipe and fin arrangements are determined. - Abstract: In the present study, the thermal characteristics of a finned heat pipe-assisted latent heat thermal energy storage system are investigated numerically. A transient two-dimensional finite volume based model employing enthalpy-porosity technique is implemented to analyze the performance of a thermal energy storage unit with square container and high melting temperature phase change material. The effects of heat pipe spacing, fin length and numbers and the influence of natural convection on the thermal response of the thermal energy storage unit have been studied. The obtained results reveal that the natural convection has considerable effect on the melting process of the phase change material. Increasing the number of heat pipes (decreasing the heat pipe spacing) leads to the increase of melting rate and the decrease of base wall temperature. Also, the increase of fin length results in the decrease of temperature difference within the phase change material in the container, providing more uniform temperature distribution. It was also shown that number of the fins does not have a significant effect on the performance of the system

  17. The influence of the solid thermal conductivity on active magnetic regenerators

    DEFF Research Database (Denmark)

    Nielsen, Kaspar Kirstein; Engelbrecht, Kurt

    2012-01-01

    The influence of the thermal conductivity of the regenerator solid on the performance of a flat plate active magnetic regenerator (AMR) is investigated using an established numerical AMR model. The cooling power at different (fixed) temperature spans is used as a measure of the performance...... for a range of thermal conductivities, operating frequencies, a long and short regenerator, and finally a regenerator with a low and a high number of transfer units (NTU) regenerator. In this way the performance is mapped out and the impact of the thermal conductivity of the solid is probed. Modeling shows...... that under certain operating conditions, the AMR cycle is sensitive to the solid conductivity. It is found that as the operating frequency is increased it is not only sufficient to have a high NTU regenerator but the regenerator performance will also benefit from increased thermal conductivity in the solid...

  18. Ultrasonic-assisted synthesis and strepavidin conjugation of amino-magnetic nanoparticles

    International Nuclear Information System (INIS)

    Liu Li; Jiao Qinghua; Peng Cheng; He Shijiang; Wang Lihua

    2008-01-01

    MNPs are widely used in biotechnology, magnetic resonance imaging, catalysis and other areas. In this paper, we propose a simple, quick, inexpensive and efficient way to prepare amino-MNPs with sonication-assisted process. The amino-MNPs prepared by hydrolyzing TEOS and APS were characterized by SEM, TEM and FTIR. Conjugation of SA and amino-MNPs was also studied. The biotin bound capacity of prepared SA coated amino-MNPs was 1.824 nmol/mg, which well meet the need of biological application. (authors)

  19. Kinetics and thermodynamics of the thermal inactivation and chaperone assisted folding of zebrafish dihydrofolate reductase.

    Science.gov (United States)

    Thapliyal, Charu; Jain, Neha; Rashid, Naira; Chaudhuri Chattopadhyay, Pratima

    2018-01-01

    The maintenance of thermal stability is a major issue in protein engineering as many proteins tend to form inactive aggregates at higher temperatures. Zebrafish DHFR, an essential protein for the survival of cells, shows irreversible thermal unfolding transition. The protein exhibits complete unfolding and loss of activity at 50 °C as monitored by UV-Visible, fluorescence and far UV-CD spectroscopy. The heat induced inactivation of zDHFR follows first-order kinetics and Arrhenius law. The variation in the value of inactivation rate constant, k with increasing temperatures depicts faster inactivation at elevated temperatures. We have attempted to study the chaperoning ability of a shorter variant of GroEL (minichaperone) and compared it with that of conventional GroEL-GroES chaperone system. Both the chaperone system prevented the aggregation and assisted in refolding of zDHFR. The rate of thermal inactivation was significantly retarded in the presence of chaperones which indicate that it enhances the thermal stability of the enzyme. As minichaperone is less complex, and does not require high energy co-factors like ATP, for its function as compared to conventional GroEL-GroES system, it can act as a very good in vitro as well as in vivo chaperone model for monitoring assisted protein folding phenomenon. Copyright © 2017 Elsevier Inc. All rights reserved.

  20. A Conduction-Cooled Superconducting Magnet System-Design, Fabrication and Thermal Tests

    DEFF Research Database (Denmark)

    Song, Xiaowei (Andy); Holbøll, Joachim; Wang, Qiuliang

    2015-01-01

    A conduction-cooled superconducting magnet system with an operating current of 105.5 A was designed, fabricated and tested for material processing applications. The magnet consists of two coaxial NbTi solenoid coils with an identical vertical height of 300 mm and is installed in a high-vacuumed c......A conduction-cooled superconducting magnet system with an operating current of 105.5 A was designed, fabricated and tested for material processing applications. The magnet consists of two coaxial NbTi solenoid coils with an identical vertical height of 300 mm and is installed in a high......-vacuumed cryostat. A two-stage GM cryocooler with a cooling power of 1.5 W at 4.2 K in the second stage is used to cool the system from room temperature to 4.2 K. In this paper, the detailed design, fabrication, thermal analysis and tests of the system are presented....

  1. Review and evaluation of extractants for strontium removal using magnetically assisted chemical separation

    International Nuclear Information System (INIS)

    Bauer, C.B.; Rogers, R.D.

    1995-11-01

    A literature review on extractants for strontium removal was initially performed at Northern Illinois University to assess their potential in magnetically assisted chemical separation. A series of potential strontium extractants was systematically evaluated there using radioanalytical methods. Initial experiments were designed to test the uptake of strontium from nitric acid using several samples of magnetic extractant particles that were coated with various crown ether ligands. High partition coefficient (K d ) values for stimulant tank waste were obtained. Further studies demonstrated that the large partitioning was due to uncoated particles

  2. Review and evaluation of extractants for strontium removal using magnetically assisted chemical separation

    Energy Technology Data Exchange (ETDEWEB)

    Bauer, C.B.; Rogers, R.D. [Northern Illinois Univ., De Kalb, IL (United States). Dept. of Chemistry; Nunez, L.; Ziemer, M.D.; Pleune, T.T.; Vandegrift, G.F. [Argonne National Lab., IL (United States)

    1995-11-01

    A literature review on extractants for strontium removal was initially performed at Northern Illinois University to assess their potential in magnetically assisted chemical separation. A series of potential strontium extractants was systematically evaluated there using radioanalytical methods. Initial experiments were designed to test the uptake of strontium from nitric acid using several samples of magnetic extractant particles that were coated with various crown ether ligands. High partition coefficient (K{sub d}) values for stimulant tank waste were obtained. Further studies demonstrated that the large partitioning was due to uncoated particles.

  3. Thermally activated magnetization reversal in monatomic magnetic chains on surfaces studied by classical atomistic spin-dynamics simulations

    International Nuclear Information System (INIS)

    Bauer, David S G; Mavropoulos, Phivos; Bluegel, Stefan; Lounis, Samir

    2011-01-01

    We analyse the spontaneous magnetization reversal of supported monatomic chains of finite length due to thermal fluctuations via atomistic spin-dynamics simulations. Our approach is based on the integration of the Landau-Lifshitz equation of motion of a classical spin Hamiltonian in the presence of stochastic forces. The associated magnetization lifetime is found to obey an Arrhenius law with an activation barrier equal to the domain wall energy in the chain. For chains longer than one domain wall width, the reversal is initiated by nucleation of a reversed magnetization domain primarily at the chain edge followed by a subsequent propagation of the domain wall to the other edge in a random-walk fashion. This results in a linear dependence of the lifetime on the chain length, if the magnetization correlation length is not exceeded. We studied chains of uniaxial and triaxial anisotropy and found that a triaxial anisotropy leads to a reduction of the magnetization lifetime due to a higher reversal attempt rate, even though the activation barrier is not changed.

  4. A 3D Dynamic Lumped Parameter Thermal Network of Air-Cooled YASA Axial Flux Permanent Magnet Synchronous Machine

    Directory of Open Access Journals (Sweden)

    Abdalla Hussein Mohamed

    2018-03-01

    Full Text Available To find the temperature rise for high power density yokeless and segmented armature (YASA axial flux permanent magnet synchronous (AFPMSM machines quickly and accurately, a 3D lumped parameter thermal model is developed and validated experimentally and by finite element (FE simulations on a 4 kW YASA machine. Additionally, to get insight in the thermal transient response of the machine, the model accounts for the thermal capacitance of different machine components. The model considers the stator, bearing, and windage losses, as well as eddy current losses in the magnets on the rotors. The new contribution of this work is that the thermal model takes cooling via air channels between the magnets on the rotor discs into account. The model is parametrized with respect to the permanent magnet (PM angle ratio, the PM thickness ratio, the air gap length, and the rotor speed. The effect of the channels is incorporated via convection equations based on many computational fluid dynamics (CFD computations. The model accuracy is validated at different values of parameters by FE simulations in both transient and steady state. The model takes less than 1 s to solve for the temperature distribution.

  5. In situ generated gas bubble-assisted modulation of the morphologies, photocatalytic, and magnetic properties of ferric oxide nanostructures synthesized by thermal decomposition of iron nitrate

    International Nuclear Information System (INIS)

    Tong Guoxiu; Guan Jianguo; Xiao Zhidong; Huang Xing; Guan Yao

    2010-01-01

    Ferric oxide (Fe 2 O 3 ) complex nanoarchitectures with high BET specific surface area, superior photocatalytic activity and modulated magnetic properties are facilely synthesized via controlled thermal decomposition of iron(III) nitrate nonahydrate. The products are characterized by X-ray diffraction, Fourier-transforming infrared spectra, field-emission scanning electron microscope, field-emission high-resolution transmission electron microscope, and nitrogen physisorption and micrometrics analyzer. The corresponding photocatalytic activity and static magnetic properties are also evaluated by measuring the photocatalytic degradation of Rhodamine B aqueous solution under visible light illumination and vibrating sample magnetometer, respectively. Simply tuning the decomposition temperature can conveniently modulate the adsorbing/desorbing behaviors of the in situ generated gases on the nucleus surfaces, and consequently the crystalline structures and morphologies of the Fe 2 O 3 complex nanoarchitectures. The as-prepared Fe 2 O 3 complex nanoarchitectures show strong crystal structure and/or morphology-dependent photocatalytic and magnetic performances. The Fe 2 O 3 complex nanoarchitectures with high specific surface area and favorable crystallization are found to be beneficial for improving the photocatalytic activity. This work not only reports a convenient and low-cost decomposition procedure and a novel formation mechanism of complex nanoarchitectures but also provides an efficient route to enhance catalytic and magnetic properties of Fe 2 O 3 .

  6. In-syringe-stirring: A novel approach for magnetic stirring-assisted dispersive liquid–liquid microextraction

    International Nuclear Information System (INIS)

    Horstkotte, Burkhard; Suárez, Ruth; Solich, Petr; Cerdà, Víctor

    2013-01-01

    Graphical abstract: -- Highlights: •We propose a new automatic magnetic stirring assisted dispersive liquid–liquid microextraction. •It allows the extraction of aluminum from seawater and freshwater samples within less than 4 min. •The method was applicable to the natural samples. -- Abstract: For the first time, the use of a magnetic stirrer within the syringe of an automated syringe pump and the resulting possible analytical applications are described. A simple instrumentation following roughly the one from sequential injection analyzer systems is used in combination with an adaptor, which is placed onto the barrel of a glass syringe. Swirling around the longitudinal axis of the syringe and holding two strong neodymium magnets, it causes a rotating magnetic field and serves as driver for a magnetic stirring bar placed inside of the syringe. In a first study it was shown that this approach leads to a sealed but also automatically adaptable reaction vessel, the syringe, in which rapid and homogeneous mixing of sample with the required reagents within short time can be carried out. In a second study in-a-syringe magnetic stirring-assisted dispersive liquid–liquid microextraction (MSA-DLLME) was demonstrated by the application of the analyzer system to fluorimetric determination of aluminum in seawater samples using lumogallion. A linear working range up to 1.1 μmol L −1 and a limit of detection of 6.1 nmol L −1 were found. An average recovery of 106.0% was achieved for coastal seawaters with a reproducibility of 4.4%. The procedure lasted 210 s including syringe cleaning and only 150 μL of hexanol and 4.1 mL of sample were required

  7. Flat super-oscillatory lens for heat-assisted magnetic recording with sub-50 nm resolution.

    Science.gov (United States)

    Yuan, Guanghui; Rogers, Edward T F; Roy, Tapashree; Shen, Zexiang; Zheludev, Nikolay I

    2014-03-24

    Heat-assisted magnetic recording (HAMR) is a future roadmap technology to overcome the superparamagnetic limit in high density magnetic recording. Existing HAMR schemes depend on a simultaneous magnetic stimulation and light-induced local heating of the information carrier. To achieve high-density recorded data, near-field plasmonic transducers have been proposed as light concentrators. Here we suggest and investigate in detail an alternative approach exploiting a far-field focusing device that can focus light into sub-50 nm hot-spots in the magnetic recording layer using a laser source operating at 473 nm. It is based on a recently introduced super-oscillatory flat lens improved with the use of solid immersion, giving an effective numerical aperture as high as 4.17. The proposed solution is robust and easy to integrate with the magnetic recording head thus offering a competitive advantage over plasmonic technology.

  8. Thermal Stability and Magnetic Properties of Polyvinylidene Fluoride/Magnetite Nanocomposites

    OpenAIRE

    Ouyang, Zen-Wei; Chen, Erh-Chiang; Wu, Tzong-Ming

    2015-01-01

    This work describes the thermal stability and magnetic properties of polyvinylidene fluoride (PVDF)/magnetite nanocomposites fabricated using the solution mixing technique. The image of transmission electron microscopy for PVDF/magnetite nanocomposites reveals that the 13 nm magnetite nanoparticles are well distributed in PVDF matrix. The electroactive β-phase and piezoelectric responses of PVDF/magnetite nanocomposites are increased as the loading of magnetite nanoparticles increases. The pi...

  9. Thermal Sunyaev-Zel'dovich effect in the intergalactic medium with primordial magnetic fields

    Science.gov (United States)

    Minoda, Teppei; Hasegawa, Kenji; Tashiro, Hiroyuki; Ichiki, Kiyotomo; Sugiyama, Naoshi

    2017-12-01

    The presence of ubiquitous magnetic fields in the universe is suggested from observations of radiation and cosmic ray from galaxies or the intergalactic medium (IGM). One possible origin of cosmic magnetic fields is the magnetogenesis in the primordial universe. Such magnetic fields are called primordial magnetic fields (PMFs), and are considered to affect the evolution of matter density fluctuations and the thermal history of the IGM gas. Hence the information of PMFs is expected to be imprinted on the anisotropies of the cosmic microwave background (CMB) through the thermal Sunyaev-Zel'dovich (tSZ) effect in the IGM. In this study, given an initial power spectrum of PMFs as P (k )∝B1Mpc 2knB , we calculate dynamical and thermal evolutions of the IGM under the influence of PMFs, and compute the resultant angular power spectrum of the Compton y -parameter on the sky. As a result, we find that two physical processes driven by PMFs dominantly determine the power spectrum of the Compton y -parameter; (i) the heating due to the ambipolar diffusion effectively works to increase the temperature and the ionization fraction, and (ii) the Lorentz force drastically enhances the density contrast on small scale just after the recombination epoch. These facts result in making the anisotropies of the CMB temperature on small scales, and we find that the signal goes up to 10 μ K2 around ℓ˜106 with B1 Mpc=0.1 nG and nB=0.0 . Therefore, CMB measurements on such small scales may provide a hint for the existence of the PMFs.

  10. Optimisation of applied field pulses for microwave assisted magnetic recording

    Directory of Open Access Journals (Sweden)

    Simon John Greaves

    2017-05-01

    Full Text Available Grains in a recording medium experience field pulses from a write head during recording. In general, a short head field rise time and a square pulse shape have been viewed as optimal. This work investigates the optimum field pulse shape for microwave assisted magnetic recording on single layer and ECC media. A square pulse was found to give the best recording performance on single layer media, but an initially negative field pulse increasing at a constant rate was more suitable for ECC media.

  11. Numerical and experimental investigations of coupled electromagnetic and thermal fields in superconducting accelerator magnets

    International Nuclear Information System (INIS)

    Mierau, Anna

    2013-01-01

    The new international facility for antiproton and ion research FAIR will be built in Darmstadt (Germany). The existing accelerator facility of GSI Helmholtzzentrum for Heavy Ion Research will serve as a pre-accelerator for the new facility. FAIR will provide high-energy antiproton and ion beams with unprecedented intensity and quality for fundamental research of states of matter and the evolution of the universe. The central component of FAIR's accelerator and storage rings complex is a double-ring accelerator consisting of two heavy ion synchrotrons SIS100 and SIS300. The SIS100 is the primary accelerator of FAIR. The desired beam properties of SIS100 require a design of the machine much more challenging than the conventional design of existing proton and ion synchrotrons. The key technical components of each synchrotron are the special electromagnets, which allow guiding the charged particles on their orbits in the synchrotron during the acceleration processes. For a stable operation of the SIS100's the magnets have to produce extremely homogeneous magnetic fields. Furthermore, the SIS100 high-intensity ion beam modes, for example with U 28+ ions, require an ultra-high vacuum in the beam pipe of the synchrotron, which can be generated effectively only at low temperatures below 15 K. Due to the field quality requirements for the magnets, the properties of the dynamic vacuum in the beam pipe but also in order to minimise future operating costs, fast ramped superconducting magnets will be used to guide the beam in SIS100. These magnets have been developed at GSI within the framework of the FAIR project. Developing a balanced design of a superconducting accelerator magnet requires a sound understanding of the interaction between its thermal and electromagnetic fields. Of special importance in this case are the magnetic field properties such as the homogeneity of the static magnetic field in the aperture of the magnet, and the dynamic heat losses of the whole magnet

  12. Thermal spin current generation and spin transport in Pt/magnetic-insulator/Py heterostructures

    Science.gov (United States)

    Chen, Ching-Tzu; Safranski, Christopher; Krivorotov, Ilya; Sun, Jonathan

    Magnetic insulators can transmit spin current via magnon propagation while blocking charge current. Furthermore, under Joule heating, magnon flow as a result of the spin Seeback effect can generate additional spin current. Incorporating magnetic insulators in a spin-orbit torque magnetoresistive memory device can potentially yield high switching efficiencies. Here we report the DC magneto-transport studies of these two effects in Pt/magnetic-insulator/Py heterostructures, using ferrimagnetic CoFexOy (CFO) and antiferromagnet NiO as the model magnetic insulators. We observe the presence and absence of the inverse spin-Hall signals from the thermal spin current in Pt/CFO/Py and Pt/NiO/Py structures. These results are consistent with our spin-torque FMR linewidths in comparison. We will also report investigations into the magnetic field-angle dependence of these observations.

  13. Large-scale magnetic fields, curvature fluctuations, and the thermal history of the Universe

    International Nuclear Information System (INIS)

    Giovannini, Massimo

    2007-01-01

    It is shown that gravitating magnetic fields affect the evolution of curvature perturbations in a way that is reminiscent of a pristine nonadiabatic pressure fluctuation. The gauge-invariant evolution of curvature perturbations is used to constrain the magnetic power spectrum. Depending on the essential features of the thermodynamic history of the Universe, the explicit derivation of the bound is modified. The theoretical uncertainty in the constraints on the magnetic energy spectrum is assessed by comparing the results obtained in the case of the conventional thermal history with the estimates stemming from less conventional (but phenomenologically allowed) post-inflationary evolutions

  14. Influence of thermal debinding on the final properties of Fe–Si soft magnetic alloys for metal injection molding (MIM)

    Energy Technology Data Exchange (ETDEWEB)

    Páez-Pavón, A.; Jiménez-Morales, A. [Dpto. Ciencia e Ing. de materiales e Ing. Química, Universidad Carlos III de Madrid, 28911 Leganés, Madrid (Spain); Santos, T.G. [UNIDEMI, Departamento de Engenharia Mecânica e Industrial, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa, 2829-516 Caparica (Portugal); Quintino, L. [Instituto Superior Técnico, Universidade de Lisboa, 1049-001 Lisboa (Portugal); Torralba, J.M. [Dpto. Ciencia e Ing. de materiales e Ing. Química, Universidad Carlos III de Madrid, 28911 Leganés, Madrid (Spain)

    2016-10-15

    Metal injection molding (MIM) may be used to produce soft magnetic materials with optimal mechanical and magnetic properties. Unlike other techniques, MIM enables the production of complex and small Fe–Si alloy parts with silicon contents greater than 3% by weight. In MIM process development, it is critical to design a proper debinding cycle not only to ensure complete removal of the binder system but also to obtain improved properties in the final part. This work is a preliminary study on the production of Fe-3.8Si soft magnetic parts by MIM using pre-alloyed powders and a non-industrialized binder. Two different heating rates during thermal debinding were used to study their effect on the final properties of the part. The final properties of the sintered parts are related to thermal debinding. It has been demonstrated that the heating rate during thermal debinding has a strong influence on the final properties of Fe–Si soft magnetic alloys. - Highlights: • The properties of MIM Fe-Si alloy are influenced by the debinding heating rate. • The slow debinding led to a lower porosity, lower oxygen content and grain growth. • The magnetization of the sintered samples improved after a slow thermal debinding.

  15. Single axis controlled hybrid magnetic bearing for left ventricular assist device: hybrid core and closed magnetic circuit.

    Science.gov (United States)

    da Silva, Isaias; Horikawa, Oswaldo; Cardoso, Jose R; Camargo, Fernando A; Andrade, Aron J P; Bock, Eduardo G P

    2011-05-01

    In previous studies, we presented main strategies for suspending the rotor of a mixed-flow type (centrifugal and axial) ventricular assist device (VAD), originally presented by the Institute Dante Pazzanese of Cardiology (IDPC), Brazil. Magnetic suspension is achieved by the use of a magnetic bearing architecture in which the active control is executed in only one degree of freedom, in the axial direction of the rotor. Remaining degrees of freedom, excepting the rotation, are restricted only by the attraction force between pairs of permanent magnets. This study is part of a joint project in development by IDPC and Escola Politecnica of São Paulo University, Brazil. This article shows advances in that project, presenting two promising solutions for magnetic bearings. One solution uses hybrid cores as electromagnetic actuators, that is, cores that combine iron and permanent magnets. The other solution uses actuators, also of hybrid type, but with the magnetic circuit closed by an iron core. After preliminary analysis, a pump prototype has been developed for each solution and has been tested. For each prototype, a brushless DC motor has been developed as the rotor driver. Each solution was evaluated by in vitro experiments and guidelines are extracted for future improvements. Tests have shown good results and demonstrated that one solution is not isolated from the other. One complements the other for the development of a single-axis-controlled, hybrid-type magnetic bearing for a mixed-flow type VAD. © 2011, Copyright the Authors. Artificial Organs © 2011, International Center for Artificial Organs and Transplantation and Wiley Periodicals, Inc.

  16. Thermal and magnetic behavior of Angustifolia Kunth bamboo fibers covered with Fe3O4 particles

    International Nuclear Information System (INIS)

    Calvo, S.; Arias, N.P.; Giraldo, O.; Rosales-Rivera, A.; Moscoso, O.

    2012-01-01

    Several Angustifolia Kunth bamboo fibers, which have been previously treated with an alkaline solution, were coated with magnetite particles. The coating of the fibers was achieved by an in-situ co-precipitation method with Fe 2+ and Fe 3+ in NaOH or NH 4 OH. The fibers were evaluated by chemical analysis using atomic absorption (A.A.) technique, structural characterization by X-ray diffraction (XRD), thermal stability with thermo-gravimetric analysis (TGA) in nitrogen at temperature range between 23 °C and 800 °C and magnetic behavior using vibrating sample magnetometry (VSM) applying a magnetic field between -27 KOe and 27 KOe at room temperature. We found that the thermal stability and magnetization depend of the synthesis method used to cover the Angustifolia Kunth bamboo fibers. In addition, an improved magnetic response was observed when NaOH solution is used to generate the magnetite coating on the fiber surface.

  17. Investigating the Plasma-Assisted and Thermal Catalytic Dry Methane Reforming for Syngas Production: Process Design, Simulation and Evaluation

    Directory of Open Access Journals (Sweden)

    Evangelos Delikonstantis

    2017-09-01

    Full Text Available The growing surplus of green electricity generated by renewable energy technologies has fueled research towards chemical industry electrification. By adapting power-to-chemical concepts, such as plasma-assisted processes, cheap resources could be converted into fuels and base chemicals. However, the feasibility of those electrified processes at large scale has not been investigated yet. Thus, the current work strives to compare, for first time in the literature, plasma-assisted production of syngas, from CH4 and CO2 (dry methane reforming, with thermal catalytic dry methane reforming. Specifically, both processes are conceptually designed to deliver syngas suitable for methanol synthesis (H2/CO ≥ 2 in mole. The processes are simulated in the Aspen Plus process simulator where different process steps are investigated. Heat integration and equipment cost estimation are performed for the most promising process flow diagrams. Collectively, plasma-assisted dry methane reforming integrated with combined steam/CO2 methane reforming is an effective way to deliver syngas for methanol production. It is more sustainable than combined thermal catalytic dry methane reforming with steam methane reforming, which has also been proposed for syngas production of H2/CO ≥ 2; in the former process, 40% more CO2 is captured, while 38% less H2O is consumed per mol of syngas. Furthermore, the plasma-assisted process is less complex than the thermal catalytic one; it requires higher amount of utilities, but comparable capital investment.

  18. Simulation of adiabatic thermal beams in a periodic solenoidal magnetic focusing field

    Directory of Open Access Journals (Sweden)

    T. J. Barton

    2012-12-01

    Full Text Available Self-consistent particle-in-cell simulations are performed to verify earlier theoretical predictions of adiabatic thermal beams in a periodic solenoidal magnetic focusing field [K. R. Samokhvalova, J. Zhou, and C. Chen, Phys. Plasmas 14, 103102 (2007PHPAEN1070-664X10.1063/1.2779281; J. Zhou, K. R. Samokhvalova, and C. Chen, Phys. Plasmas 15, 023102 (2008PHPAEN1070-664X10.1063/1.2837891]. In particular, results are obtained for adiabatic thermal beams that do not rotate in the Larmor frame. For such beams, the theoretical predictions of the rms beam envelope, the conservations of the rms thermal emittances, the adiabatic equation of state, and the Debye length are verified in the simulations. Furthermore, the adiabatic thermal beam is found be stable in the parameter regime where the simulations are performed.

  19. submitter Thermal, Hydraulic, and Electromagnetic Modeling of Superconducting Magnet Systems

    CERN Document Server

    Bottura, L

    2016-01-01

    Modeling techniques and tailored computational tools are becoming increasingly relevant to the design and analysis of large-scale superconducting magnet systems. Efficient and reliable tools are useful to provide an optimal forecast of the envelope of operating conditions and margins, which are difficult to test even when a prototype is available. This knowledge can be used to considerably reduce the design margins of the system, and thus the overall cost, or increase reliability during operation. An integrated analysis of a superconducting magnet system is, however, a complex matter, governed by very diverse physics. This paper reviews the wide spectrum of phenomena and provides an estimate of the time scales of thermal, hydraulic, and electromagnetic mechanisms affecting the performance of superconducting magnet systems. The analysis is useful to provide guidelines on how to divide the complex problem into building blocks that can be integrated in a design and analysis framework for a consistent multiphysic...

  20. Magnetization strucrure of thermal vent on island arc from vector magnetic anomlies using AUV

    Science.gov (United States)

    Isezaki, N.; Matsuo, J.; Sayanagi, K.

    2012-04-01

    The geomagnetic anomaly measured by a scalar magnetometer,such as a proton precession magnetometer cannot be defined its direction, then it does not satisfy the Laplace's equation. Therefore physical formula describing the relation between magnetic field and magnetization cannot be established.Because the difference between results obtained from scalar data and from vector data is very significant, we must use vector magnetic field data for magnetization analyses to get the more reliable and exact solutions. The development program of fundamental tools for exploration of deep seabed resources started with the financial support of the Ministry of Education, Culture, Sports, Science & Technology (MEXT) in 2008 and will end in 2012. In this project, we are developing magnetic exploration tools for seabed resources using AUV (Autonomous Underwater Vehicle) and other deep-towed vehicles to measure not the scalar magnetic field but the vector magnetic field in order to estimate magnetization structure below the sea-floor exactly and precisely. We conducted AUV magnetic survey in 2010 at the thermal area called Hakurei deposit in the Bayonnaise submarine caldera at the southern end of Izu island arc, about 400km south of Tokyo. We analyzed the observed vector magnetic fields to get the vector magnetic anomaly Fields using the method of Isezaki(1984). We inverted these vector magnetic anomaly fields to magnetization structure. CONCLUSIONS 1.The scalar magnetic field TIA (Total Intensity Anomaly) has no physical formula describing the relation between M (Magnetization) and TIA because TIA does not satisfy the Laplace's equation. Then it is impossible to estimate M from TIA. 2.Anlyses of M using TIA have been done so far under assumption TIA=PTA (Projected Total Anomay on MF (Main Geomagnetic Field)), however, which caused the analysis error due to ɛT= TIA - PTA . 3.We succeeded to measure the vector magnetic anomaly fields using AUV despite the severe magnetic noises

  1. Investigation of Thermal and Vacuum Transients on the LHC Prototype Magnet String

    CERN Document Server

    Cruikshank, P; Riddone, G; Tavian, L

    1996-01-01

    The prototype magnet string, described in a companion paper, is a full-scale working model of a 50-m length of the future Large Hadron Collider (LHC), CERN's new accelerator project, which will use high-field superconducting magnets operating below 2 K in superfluid helium. As such, it provides an excellent test bed for practising standard operating modes of LHC insulation vacuum and cryogenics, as well as for experimentally assessing accidental behaviour and failure modes, and thus verifying design calculations. We present experimental investigation of insulation vacuum pumpdown, magnet forced-flow cooldown and warmup, and evolution of residual vacuum pressures and temperatures in natural warmup, as well as catastrophic loss of insulation vacuum. In all these transient modes, experimental results are compared with simulated behaviour, using a non-linear, one-dimensional thermal model of the magnet string.

  2. Microwave-Assisted Synthesis of CuFe2O4 Nanoparticles and Starch-Based Magnetic Nanocomposites

    Directory of Open Access Journals (Sweden)

    Gh. Nabiyouni

    2013-06-01

    Full Text Available Magnetic CuFe2O4 nanoparticles were synthesized by a facile microwave-assisted reaction between Cu(NO32 and Fe(NO33. The magnetic nanoparticles were added to starch to make magnetic polymeric nanocomposite. The nanoparticles and nanocomposites were characterized using X-ray diffraction and scanning electron microscopy. The magnetic properties of the samples were investigated using an alternating gradient force magnetometer (AGFM. The copper ferrite nanoparticles exhibited ferromagnetic behavior at room temperature, with a saturation magnetization of 29emu/g and a coercivity of 136 Oe. The distribution of the CuFe2O4 nanoparticles into the polymeric matrixes decreases the coercivity (136 Oe to 66 Oe. The maximum coercivity of 82 Oe was found for 15% of CuFe2O4 distributed to the starch matrix.

  3. Anisotropic electrical, thermal and magnetic properties of Al{sub 13}Ru{sub 4} decagonal quasicrystalline approximant

    Energy Technology Data Exchange (ETDEWEB)

    Wencka, Magdalena [Polish Academy of Sciences, Poznan (Poland). Inst. of Molecular Physics; Vrtnik, Stanislav; Kozelj, Primoz; Dolinsek, Janez [Ljubljana Univ. (Slovenia). Faculty of Mathematics and Physics; Jozef Stefan Institute, Ljubljana (Slovenia); Jaglicic, Zvonko [Ljubljana Univ. (Slovenia). Inst. of Mathematics, Physics and Mechanics; Gille, Peter [Muenchen Univ. (Germany). Crystallography Section

    2017-09-01

    We present measurements of the anisotropic electrical and thermal transport coefficients (the electrical resistivity, the thermoelectric power, the thermal conductivity), the magnetization and the specific heat of the Al{sub 13}Ru{sub 4} monoclinic approximant to the decagonal quasicrystal, in comparison to the isostructural Al{sub 13}Fe{sub 4}. The electrical and thermal transport parameters of Al{sub 13}Ru{sub 4} were found to exhibit significant anisotropy, qualitatively similar to that found previously in the Al{sub 13}Fe{sub 4} (P. Popcevic, et al., Phys. Rev. B 2010, 81, 184203). The crystallographic b direction, corresponding to the stacking direction of the (a,c) atomic planes, is the most conducting direction for the electricity and heat. The thermopower is strongly anisotropic with a complicated temperature dependence, exhibiting maxima, minima, crossovers and sign change. The electronic density of states (DOS) at the Fermi energy is reduced to 35% of the DOS of Al metal. The magnetic susceptibility is diamagnetic and the diamagnetism is by a factor of 2 stronger for the magnetic field along the stacking b direction.

  4. Controllable deposition of gadolinium doped ceria electrolyte films by magnetic-field-assisted electrostatic spray deposition

    International Nuclear Information System (INIS)

    Ksapabutr, Bussarin; Chalermkiti, Tanapol; Wongkasemjit, Sujitra; Panapoy, Manop

    2013-01-01

    This paper describes a simple and low-temperature approach to fabrication of dense and crack-free gadolinium doped ceria (GDC) thin films with controllable deposition by a magnetic-field-assisted electrostatic spray deposition technique. The influences of external permanent magnets on the deposition of GDC films were investigated. The coating area deposited using two magnets with the same pole arrangement decreased in comparison with the case of no magnets, whereas the largest deposition area was obtained in the system of the opposite poles. Analysis of as-deposited films at 450 °C indicated the formation of uniform, smooth and dense thin films with a single-phase fluorite structure. The films produced in the system using same poles were thicker, smaller in crystallite size and smoother than those fabricated under other conditions. Additionally, the GDC film deposited using the same pole arrangement showed the maximum in electrical conductivity of about 2.5 × 10 −2 S/cm at a low operating temperature of 500 °C. - Highlights: • Magnetic-field-assisted electrostatic spray allows a controllable coating. • Dense, crack-free thin films were obtained at low process temperature of 450 °C. • Control of deposition, thickness and uniformity is easy to achieve simultaneously. • Films from the same pole were thicker, smaller in crystal size and smoother. • The maximum conductivity of doped ceria film was 2.5 × 10 −2 S/cm at 500 °C

  5. Modelling of bulk superconductor magnetization

    International Nuclear Information System (INIS)

    Ainslie, M D; Fujishiro, H

    2015-01-01

    This paper presents a topical review of the current state of the art in modelling the magnetization of bulk superconductors, including both (RE)BCO (where RE = rare earth or Y) and MgB 2 materials. Such modelling is a powerful tool to understand the physical mechanisms of their magnetization, to assist in interpretation of experimental results, and to predict the performance of practical bulk superconductor-based devices, which is particularly important as many superconducting applications head towards the commercialization stage of their development in the coming years. In addition to the analytical and numerical techniques currently used by researchers for modelling such materials, the commonly used practical techniques to magnetize bulk superconductors are summarized with a particular focus on pulsed field magnetization (PFM), which is promising as a compact, mobile and relatively inexpensive magnetizing technique. A number of numerical models developed to analyse the issues related to PFM and optimise the technique are described in detail, including understanding the dynamics of the magnetic flux penetration and the influence of material inhomogeneities, thermal properties, pulse duration, magnitude and shape, and the shape of the magnetization coil(s). The effect of externally applied magnetic fields in different configurations on the attenuation of the trapped field is also discussed. A number of novel and hybrid bulk superconductor structures are described, including improved thermal conductivity structures and ferromagnet–superconductor structures, which have been designed to overcome some of the issues related to bulk superconductors and their magnetization and enhance the intrinsic properties of bulk superconductors acting as trapped field magnets. Finally, the use of hollow bulk cylinders/tubes for shielding is analysed. (topical review)

  6. Magnetic properties of thermally reduced graphene oxide decorated with PtNi nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Huízar-Félix, A.M. [Universidad Autónoma de Nuevo León, UANL, Facultad de Ingeniería Mecánica y Eléctrica, FIME, Ave. Pedro de Alba s/n, Ciudad Universitaria, C.P.66455 San Nicolás de los Garza, N.L. (Mexico); Departamento de Electricidad y Electrónica, Universidad del País Vasco (UPV/EHU), 48940 Leioa (Spain); BC Materials, Basque Centre for Materials, Applications and Nanostructures, 48160 Derio (Spain); Cruz-Silva, R. [Research Center for Exotic NanoCarbon, Shinshu University, 4-17-1 Wakasato, Nagano 380-8553 (Japan); Barandiarán, J.M. [Departamento de Electricidad y Electrónica, Universidad del País Vasco (UPV/EHU), 48940 Leioa (Spain); BC Materials, Basque Centre for Materials, Applications and Nanostructures, 48160 Derio (Spain); García-Gutiérrez, D.I. [Universidad Autónoma de Nuevo León, UANL, Facultad de Ingeniería Mecánica y Eléctrica, FIME, Ave. Pedro de Alba s/n, Ciudad Universitaria, C.P.66455 San Nicolás de los Garza, N.L. (Mexico); Orue, I. [SGIKER Medidas Magnéticas, Facultad de Ciencia y Tecnología, Universidad del País Vasco (UPV/EHU), 48940 Leioa (Spain); and others

    2016-09-05

    Nanocomposites of reduced graphene oxide (RGO) with PtNi nanoparticles were obtained by in situ thermal reduction of a physical mixture of GO and metallic precursors. RGO and PtNiRGO nanocomposites were studied by differential thermal analysis and thermogravimetry, Fourier transform infrared spectroscopy (FTIR), powder X-ray diffraction (XRD), as well as scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The method presented here is a one-step thermal reduction procedure that allows the deposition of bimetallic PtNi nanoparticles with tetragonal crystalline structure and particle size ranging from 3 nm to 30 nm on RGO. The magnetic properties of the RGO and PtNiRGO nanocomposites were measured by vibrating sample magnetometry, which revealed that the RGO exhibited diamagnetism at room temperature and paramagnetism at temperatures below 10 K. PtNiRGO nanocomposites show hysteresis and ferromagnetic ordering at room temperature with a Curie temperature of 658 K. In addition, its magnetic properties at low temperature were strongly influenced by the paramagnetic contribution of RGO and the morphology of the bimetallic nanoparticles. - Highlights: • Simultaneous synthesis method for growth of PtNi nanoparticles on RGO. • Microstructural features of PtNiRGO nanocomposite were studied with extensive characterization. • Diamagnetic behavior of RGO and ferromagnetic ordering for PtNiRGO nanocomposite.

  7. Ultrasound-assisted fabrication of a biocompatible magnetic hydroxyapatite.

    Science.gov (United States)

    Zhou, Gang; Song, Wei; Hou, Yongzhao; Li, Qing; Deng, Xuliang; Fan, Yubo

    2014-10-01

    This work describes the fabrication and characterization of a biocompatible magnetic hydroxyapatite (HA) using an ultrasound-assisted co-precipitation method. X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and transmission electron microscopy (TEM) were used to characterize the structure and chemical composition of the produced samples. The M-H loops of synthesized materials were traced using a vibrating sample magnetometer (VSM) and the biocompatibility was evaluated by cell culture and MTT (3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide) assay. Furthermore, in vivo histopathological examinations were used to evaluate the potential toxicological effects of Fe₃O₄-HA composites on kidney of SD rats injected intraperitoneally with Fe₃O₄-HA particles. The results showed that magnetic iron oxide particles first replace OH ions of HA, which are parallel to the c axis, and then enter the HA crystal lattice which produces changes in the crystal surface of HA. Chemical bond interaction was observed between PO₄³⁻ groups of HA and iron ions of Fe₃O₄. The saturation magnetization (MS ) of Fe₃O₄-HA composites was 46.36 emu/g obtained from VSM data. Cell culture and MTT assays indicated that HA could affect the growth and proliferation of HEK-293 cells. This Fe₃O₄-HA composite produced no negative effects on cell morphology, viability, and proliferation and exhibited remarkable biocompatibility. Moreover, no inflammatory cell infiltration was observed in kidney histopathology slices. Therefore, this study succeeds to develop a Fe₃O₄-HA composite as a prospective biomagnetic material for future applications. © 2013 Wiley Periodicals, Inc.

  8. Start-up assist by magnetized plasma flow injection in TPE-RX reversed-field pinch

    Energy Technology Data Exchange (ETDEWEB)

    Asai, T. [College of Science and Technology, Nihon University, 1-8 Kanda-Surugadai, Chiyoda-ku, Tokyo 101-8308 (Japan)]. E-mail: asai@phys.cst.nihon-u.ac.jp; Nagata, M. [Graduate School of Engineering, University of Hyogo, Himeji (Japan); Koguchi, H. [National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba (Japan); Hirano, Y. [National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba (Japan); Sakakita, H. [National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba (Japan); Yambe, K. [National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba (Japan); Kiyama, S. [National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba (Japan)

    2006-11-15

    A reversed-field pinch (RFP) start-up assisted by a magnetized plasma flow injection was demonstrated for the first time on a TPE-RX machine. This sequence of experiments aimed to establish a new method of ionization, gas-fill and helicity injection in the start-up phase of an RFP. In this start-up method, magnetized and well-ionized plasma is formed by a magnetized coaxial plasma gun and injected into the torus chamber as an initial pre-ionized plasma for RFP formation. In the initial experiments, attenuated density pump-out and comparatively slow decay of the toroidal flux and plasma current were observed as evidence of its being an effective start-up method.

  9. Structural Design and Thermal Analysis for Thermal Shields of the MICE Coupling Magnets

    International Nuclear Information System (INIS)

    Green, Michael A.; Pan, Heng; Liu, X.K.; Wang, Li; Wu, Hong; Chen, A.B.; Guo, X.L.

    2009-01-01

    A superconducting coupling magnet made from copper matrix NbTi conductors operating at 4 K will be used in the Muon Ionization Cooling Experiment (MICE) to produce up to 2.6 T on the magnet centerline to keep the muon beam within the thin RF cavity indows. The coupling magnet is to be cooled by two cryocoolers with a total cooling capacity of 3 W at 4.2 K. In order to keep a certain operating temperature margin, the most important is to reduce the heat leakage imposed on cold surfaces of coil cold mass assembly. An ntermediate temperature shield system placed between the coupling coil and warm vacuum chamber is adopted. The shield system consists of upper neck shield, main shields, flexible connections and eight supports, which is to be cooled by the first stage cold heads of two ryocoolers with cooling capacity of 55 W at 60 K each. The maximum temperature difference on the shields should be less than 20 K, so the thermal analyses for the shields with different thicknesses, materials, flexible connections for shields' cooling and structure design for heir supports were carried out. 1100 Al is finally adopted and the maximum temperature difference is around 15 K with 4 mm shield thickness. The paper is to present detailed analyses on the shield system design.

  10. Thermal Stability of Magnetic Compass Sensor for High Accuracy Positioning Applications

    Directory of Open Access Journals (Sweden)

    Van-Tang PHAM

    2015-12-01

    Full Text Available Using magnetic compass sensors in angle measurements have a wide area of application such as positioning, robot, landslide, etc. However, one of the most phenomenal that affects to the accuracy of the magnetic compass sensor is the temperature. This paper presents two thermal stability schemes for improving performance of a magnetic compass sensor. The first scheme uses the feedforward structure to adjust the angle output of the compass sensor adapt to the variation of the temperature. The second scheme increases both the temperature working range and steady error performance of the sensor. In this scheme, we try to keep the temperature of the sensor is stable at the certain value (e.g. 25 oC by using a PID (proportional-integral-derivative controller and a heating/cooling generator. Many experiment scenarios have implemented to confirm the effectivity of these solutions.

  11. The thermal expansion of hard magnetic materials of the Nd-Fe-B system

    Science.gov (United States)

    Savchenko, Igor; Kozlovskii, Yurii; Samoshkin, Dmitriy; Yatsuk, Oleg

    2017-10-01

    The results of dilatometric measurement of the thermal expansion of hard magnetic materials brands N35M, N35H and N35SH containing as a main component the crystalline phase of Nd2Fe14B type are presented. The temperature range from 200 to 750 K has been investigated by the method of dilatometry with an error of 1.5-2×10-7 K-1. The approximation dependences of the linear thermal expansion coefficient have been obtained. The character of changes of the thermal coefficient of linear expansion in the region of the Curie point has been specified, its critical indices and critical amplitudes have been defined.

  12. Creation of Magnetic Fields by Electrostatic and Thermal Fluctuations

    International Nuclear Information System (INIS)

    Saleem, Hamid

    2009-01-01

    It is pointed out that the electrostatic and thermal fluctuations are the main source of magnetic fields in unmagnetized inhomogeneous plasmas. The unmagnetized inhomogeneous plasmas can support a low frequency electromagnetic ion wave as a normal mode like Alfven wave of magnetized plasmas. But this is a coupled mode produced by the mixing of longitudinal and transverse components of perturbed electric field due to density inhomogeneity. The ion acoustic wave does not remain electrostatic in non-uniform plasmas. On the other hand, a low frequency electrostatic wave can also exist in the pure electron plasmas and it couples with ion acoustic wave when ions are dynamic. These waves can become unstable when density and temperature gradients are parallel to each other as can be the case of laser plasmas and is the common situation in stellar cores. The main instability condition for the electrostatic and electromagnetic modes is the same (2/3)κ n T (where κ n and κ T are inverse of the scale lengths of gradients of density and electron temperature, respectively). This indicates that the electrostatic and magnetic field fluctuations are strongly coupled in unmagnetized nonuniform plasmas.

  13. Thermal and magnetic properties of ternary mixed Ising nanoparticles with core–shell structure: Effective-field theory approach

    International Nuclear Information System (INIS)

    Kantar, Ersin; Keskin, Mustafa

    2014-01-01

    We propose a ternary Ising spins (1/2, 1, 3/2) model to investigate the thermal and magnetic properties of magnetic nanoparticles with core–shell structure within the framework of the effective-field theory with correlations. The center site of the core is occupied by σ=±1/2 spin, while those surrounding the center site are occupied by S=±1, 0 spins and the shell sites are occupied by m=±1/2,±3/2 spins. Thermal behaviors of the core and shell magnetizations, susceptibilities and internal energies as well as total magnetization are examined. In order to confirm the stability of the solutions we also investigate the free energy of the system. According to the values of Hamiltonian parameters, the system undergoes first- and second-order phase transitions. Phase diagrams are calculated and discussed in detail. We find that the system exhibits a tricritical point, reentrant and five different type (Q, P, R, S and W) of compensation behaviors that strongly depend on interaction parameters. The results are in good agreement with some experimental and theoretical results. - Highlights: • Thermal and magnetic properties of ternary Ising nanoparticles are studied. • Phase diagrams within the EFT with correlations are calculated and discussed. • The effects of the exchange interactions and crystal field have been studied. • Reentrant phenomena and compensation behaviors have been found

  14. Thermal and magnetic properties of ternary mixed Ising nanoparticles with core–shell structure: Effective-field theory approach

    Energy Technology Data Exchange (ETDEWEB)

    Kantar, Ersin [Department of Physics, Erciyes University, 38039 Kayseri (Turkey); Institute of Science, Erciyes University, 38039 Kayseri (Turkey); Keskin, Mustafa, E-mail: keskin@erciyes.edu.tr [Department of Physics, Erciyes University, 38039 Kayseri (Turkey)

    2014-01-15

    We propose a ternary Ising spins (1/2, 1, 3/2) model to investigate the thermal and magnetic properties of magnetic nanoparticles with core–shell structure within the framework of the effective-field theory with correlations. The center site of the core is occupied by σ=±1/2 spin, while those surrounding the center site are occupied by S=±1, 0 spins and the shell sites are occupied by m=±1/2,±3/2 spins. Thermal behaviors of the core and shell magnetizations, susceptibilities and internal energies as well as total magnetization are examined. In order to confirm the stability of the solutions we also investigate the free energy of the system. According to the values of Hamiltonian parameters, the system undergoes first- and second-order phase transitions. Phase diagrams are calculated and discussed in detail. We find that the system exhibits a tricritical point, reentrant and five different type (Q, P, R, S and W) of compensation behaviors that strongly depend on interaction parameters. The results are in good agreement with some experimental and theoretical results. - Highlights: • Thermal and magnetic properties of ternary Ising nanoparticles are studied. • Phase diagrams within the EFT with correlations are calculated and discussed. • The effects of the exchange interactions and crystal field have been studied. • Reentrant phenomena and compensation behaviors have been found.

  15. Simulations of planar non-thermal plasma assisted ignition at atmospheric pressure

    KAUST Repository

    Casey, Tiernan A.

    2016-10-21

    The opportunity for ignition assistance by a pulsed applied voltage is investigated in a canonical one-dimensional configuration. An incipient ignition kernel, formed by localized energy deposition into a lean mixture of methane and air at atmospheric pressure, is subjected to sub-breakdown electric fields (E/N ≈ 100 Td) by a DC potential applied across the domain, resulting in non-thermal behavior of the plasma formed during the discharge. A two-fluid approach is employed to couple thermal neutrals and ions to the non-thermal electrons. A two-temperature plasma mechanism describing gas phase combustion, excitation of neutral species, and high-energy electron kinetics is employed to account for non-thermal effects. Charged species transported from the ignition zone drift rapidly through the domain, augmenting the magnitude of the electric field in the fresh gas during the pulse through a dynamic-electrode effect, which results in an increase in the energy of the electrons in the fresh mixture with increasing time. Enhanced fuel and oxidizer decomposition due to electron impact dissociation and interaction with excited neutrals generate a pool of radicals, mostly O and H, in the fresh gas ahead of the flame\\'s preheat zone. In the configuration considered, the effect of the nanosecond pulse is to increase the mass of fuel burned at equivalent times relative to the unsupported ignition through enhanced radical generation, resulting in an increased heat release rate in the immediate aftermath of the pulse.

  16. Electrical, thermal and magnetic behaviour of the metallic glass Fe80B20 in the crystallization process

    International Nuclear Information System (INIS)

    Isalgue, A.; Cusido, J.A.

    1986-01-01

    The thermal, electrical DC conductivity and magnetic properties have been studied in the crystallization process of the metallic glass Fe 80 B 20 (Metglass 2605) induced by heat treatment. The electrical and thermal conductivity, the coercive force and the remanence are strongly affected with the crystallization of the glass. Two steps can be dicerned from the magnetic measurements; the differences between the two steps are interpreted in the basis of the ''spherulite-type'', grown of Fe 3 B in the first crystallization step and the aparition of Fe 2 B in the second step. (author)

  17. A thermal model for czochralski silicon crystal growth with an axial magnetic field

    Science.gov (United States)

    Hjellming, L. N.

    1990-07-01

    This paper presents a thermal model for molten silicon in a Czochralski crystal puller system with an applied uniform axial magnetic field. The melt depth is treated as continually decreasing, which affects the thermal environment of the melt and crystal. The radiative heat loss and the input heat flux are treated as functions of time, with a constraint placed on the heat lost to the crystal from the melt. As the melt motion reaches a steady state rapidly, the temperature and flow fields are treated as instantaneously steady at each melt depth. The heat transport is a mixture of conduction and convection, and by considering the crystal and crucible to be rotating with the same angular velocity, the flows driven by buoyancy and thermocapillarity are isolated and provide the convective heat transport in the melt for the range of magnetic field strengths 0.2 ≤ B ≤ 1.0T.

  18. Evidence for thermally assisted threshold switching behavior in nanoscale phase-change memory cells

    International Nuclear Information System (INIS)

    Le Gallo, Manuel; Athmanathan, Aravinthan; Krebs, Daniel; Sebastian, Abu

    2016-01-01

    In spite of decades of research, the details of electrical transport in phase-change materials are still debated. In particular, the so-called threshold switching phenomenon that allows the current density to increase steeply when a sufficiently high voltage is applied is still not well understood, even though there is wide consensus that threshold switching is solely of electronic origin. However, the high thermal efficiency and fast thermal dynamics associated with nanoscale phase-change memory (PCM) devices motivate us to reassess a thermally assisted threshold switching mechanism, at least in these devices. The time/temperature dependence of the threshold switching voltage and current in doped Ge 2 Sb 2 Te 5 nanoscale PCM cells was measured over 6 decades in time at temperatures ranging from 40 °C to 160 °C. We observe a nearly constant threshold switching power across this wide range of operating conditions. We also measured the transient dynamics associated with threshold switching as a function of the applied voltage. By using a field- and temperature-dependent description of the electrical transport combined with a thermal feedback, quantitative agreement with experimental data of the threshold switching dynamics was obtained using realistic physical parameters

  19. Positioning and aligning CNTs by external magnetic field to assist localised epoxy cure

    Directory of Open Access Journals (Sweden)

    Ariu G.

    2016-01-01

    Full Text Available This work focuses on the generation of conductive networks through the localised alignment of nano fillers, such as multi-walled carbon nanotubes (MWCNTs. The feasibility of alignment and positioning of functionalised MWCNTs by external DC magnetic fields was investigated. The aim of this manipulation is to enhance resin curing through AC induction heating due to hysteresis losses from the nanotubes. Experimental analyses focused on in-depth assessment of the nanotube functionalisation, processing and characterisation of magnetic, rheological and cure kinetics properties of the MWCNT solution. The study has shown that an external magnetic field has great potential for positioning and alignment of CNTs. The study demonstrated potential for creating well-ordered architectures with an unprecedented level of control of network geometry. Magnetic characterisation indicated cobalt-plated nanotubes to be the most suitable candidate for magnetic alignment due to their high magnetic sensitivity. Epoxy/metal-plated CNT nanocomposite systems were validated by thermal analysis as induction heating mediums. The curing process could therefore be optimised by the use of dielectric resins. This study offers a first step towards the proof of concept of this technique as a novel repair technology.

  20. Positioning and aligning CNTs by external magnetic field to assist localised epoxy cure

    Science.gov (United States)

    Ariu, G.; Hamerton, I.; Ivanov, D.

    2016-01-01

    This work focuses on the generation of conductive networks through the localised alignment of nano fillers, such as multi-walled carbon nanotubes (MWCNTs). The feasibility of alignment and positioning of functionalised MWCNTs by external DC magnetic fields was investigated. The aim of this manipulation is to enhance resin curing through AC induction heating due to hysteresis losses from the nanotubes. Experimental analyses focused on in-depth assessment of the nanotube functionalisation, processing and characterisation of magnetic, rheological and cure kinetics properties of the MWCNT solution. The study has shown that an external magnetic field has great potential for positioning and alignment of CNTs. The study demonstrated potential for creating well-ordered architectures with an unprecedented level of control of network geometry. Magnetic characterisation indicated cobalt-plated nanotubes to be the most suitable candidate for magnetic alignment due to their high magnetic sensitivity. Epoxy/metal-plated CNT nanocomposite systems were validated by thermal analysis as induction heating mediums. The curing process could therefore be optimised by the use of dielectric resins. This study offers a first step towards the proof of concept of this technique as a novel repair technology.

  1. Micromagnetic modeling for heat-assisted magnetic recording

    International Nuclear Information System (INIS)

    Li Zhenghua; Wei Dan; Wei Fulin

    2008-01-01

    Heat-assisted magnetic recording (HAMR) is one of the candidate systems beyond the perpendicular recording technology. Here, a micromagnetic model and a heat transfer model are introduced to study the heating and cooling processes in the HAMR media; then, by integration of the SPT head and the laser heating source, the recording performance is simulated and investigated on a single track at an area density of 1 Tb/in 2 . In the HAMR system, the temperature in the medium under the laser wave guide is increased by heating, and decreased by air bearing and heat conduction when the write process really occurred. The target of this study is to find the proper design of the head-laser assembly for optimum recording. It is found that the proper distance between the laser wave guide and the head's main pole rear/front edge is only 41.4/1.4 nm for optimum recording performance

  2. Thermal aging of melt-spun NdFeB magnetic powder in hydrogen

    Science.gov (United States)

    Pinkerton, Frederick E.; Balogh, Michael P.; Ellison, Nicole; Foto, Aldo; Sechan, Martin; Tessema, Misle M.; Thompson, Margarita P.

    2016-11-01

    High energy product neodymium-iron-boron (NdFeB) magnets are the premier candidate for demanding electrified vehicle traction motor applications. Injection molded (IM) or compression molded (CM) magnets made using NdFeB powders are promising routes to improve motor efficiency, cost, and manufacturability. However, IM and CM NdFeB magnets are susceptible to substantial thermal aging losses at motor operating temperatures when exposed to the automatic transmission fluid (ATF) used as a lubricant and cooling medium. The intrinsic coercivity Hci of NdFeB IM and CM magnets degrades by as much as 18% when aged for 1000 h in ATF at 150 °C, compared to a 3% loss when aged in air. Here we report aging studies of rapidly quenched NdFeB powder in air, ATF, and H2 gas. Expansion of the NdFeB crystal lattice in both ATF and H2 identified hydrogen dissociated from the ATF during aging and diffused into the primary NdFeB phase as the probable cause of the coercivity loss of IM and CM magnets.

  3. Reduction of Thermal Loss in HTS Windings by Using Magnetic Flux Deflection

    Science.gov (United States)

    Tsuzuki, K.; Miki, M.; Felder, B.; Koshiba, Y.; Izumi, M.; Umemoto, K.; Aizawa, K.; Yanamoto, T.

    Efforts on the generation of intensified magnetic flux have been made for the optimized shape of HTS winding applications. This contributes to the high efficiency of the rotating machines using HTS windings. Heat generation from the HTS windings requires to be suppressed as much as possible, when those coils are under operation with either direct or alternative currents. Presently, the reduction of such thermal loss generated by the applied currents on the HTS coils is reported with a magnetic flux deflection system. The HTS coils are fixed together with flattened magnetic materials to realize a kind of redirection of the flux pathway. Eventually, the magnetic flux density perpendicular to the tape surface (equivalent to the a-b plane) of the HTS tape materials is reduced to the proximity of the HTS coil. To verify the new geometry of the surroundings of the HTS coils with magnetic materials, a comparative study of the DC coil voltage was done for different applied currents in prototype field-pole coils of a ship propulsion motor.

  4. Ultrasound assisted, thermally activated persulfate oxidation of coal tar DNAPLs.

    Science.gov (United States)

    Peng, Libin; Wang, Li; Hu, Xingting; Wu, Peihui; Wang, Xueqing; Huang, Chumei; Wang, Xiangyang; Deng, Dayi

    2016-11-15

    The feasibility of ultrasound assisted, thermally activated persulfate for effective oxidation of twenty 2-6 ringed coal tar PAHs in a biphasic tar/water system and a triphasic tar/soil/water system were investigated and established. The results indicate that ultrasonic assistance, persulfate and elevated reaction temperature are all required to achieve effective oxidation of coal tar PAHs, while the heating needed can be provided by ultrasonic induced heating as well. Further kinetic analysis reveals that the oxidation of individual PAH in the biphasic tar/water system follows the first-order kinetics, and individual PAH oxidation rate is primary determined by the mass transfer coefficients, tar/water interfacial areas, the aqueous solubility of individual PAH and its concentration in coal tar. Based on the kinetic analysis and experimental results, the contributions of ultrasound, persulfate and elevated reaction temperature to PAHs oxidation were characterized, and the effects of ultrasonic intensity and oxidant dosage on PAHs oxidation efficiency were investigated. In addition, the results indicate that individual PAH degradability is closely related to its reactivity as well, and the high reactivity of 4-6 ringed PAHs substantially improves their degradability. Copyright © 2016 Elsevier B.V. All rights reserved.

  5. Morphology and magnetic properties of CeCo5 submicron flakes prepared by surfactant-assisted high-energy ball milling

    International Nuclear Information System (INIS)

    Zhang, J.J.; Gao, H.M.; Yan, Y.; Bai, X.; Su, F.; Wang, W.Q.; Du, X.B.

    2012-01-01

    CeCo 5 permanent magnetic alloy has been processed by surfactant assisted high energy ball milling. Heptane and oleic acid were used as the solvent and surfactant, respectively. The amount of surfactant used was 50% by weight of the starting powder. The produced particles were deposited on a piece of copper (4 mm in length and width) under a magnetic field of 27 kOe applied along the copper surface and immobilized by ethyl α-cyanoacrylate. Scanning electron microscope pictures show that the particles are flakes, several μm in length and width and tens of nm in thickness. X-ray diffraction patterns and magnetic measurements prove that the flakes are crystalline with c-axes magnetic anisotropy. The easy magnetization axis is oriented perpendicular to the surface of the flake. A maximum coercivity of 3.3 kOe was obtained for the sample milled for 40 min. - Highlights: ► CeCo 5 permanent magnetic alloy has been processed by surfactant assisted high energy ball milling (HEBM). ► The particles show a flake-like morphology with several μm in length and width and tens nm in thickness. ► The flakes are crystallographic and magnetic anisotropic and the c-axes, also the easy magnetization directions are oriented perpendicular to the surface of the flake. ► Maximum coercivity of 3.3 kOe has been obtained for the sample milled for 40 min.

  6. Spin-Orbit Torque-Assisted Switching in Magnetic Insulator Thin Films with Perpendicular Magnetic Anisotropy

    Science.gov (United States)

    Wu, Mingzhong

    As an in-plane charge current flows in a heavy metal film with spin-orbit coupling, it produces a torque that can induce magnetization switching in a neighboring ferromagnetic metal film. Such spin-orbit torque (SOT)-induced switching has been studied extensively in recent years and has shown higher efficiency than switching using conventional spin-transfer torque. This presentation reports the SOT-assisted switching in heavy metal/magnetic insulator systems.1 The experiments made use of Pt/BaFe12O19 bi-layered structures. Thanks to its strong spin-orbit coupling, Pt has been widely used to produce pure spin currents in previous studies. BaFe12O19 is an M-type barium hexagonal ferrite and is often referred as BaM. It is one of the few magnetic insulators with strong magneto-crystalline anisotropy and shows an effective uniaxial anisotropy field of about 17 kOe. It's found that the switching response in the BaM film strongly depends on the charge current applied to the Pt film. When a constant magnetic field is applied in the film plane, the charge current in the Pt film can switch the normal component of the magnetization (M⊥) in the BaM film between the up and down states. The current also dictates the up and down states of the remnant magnetization when the in-plane field is reduced to zero. When M⊥ is measured by sweeping an in-plane field, the response manifests itself as a hysteresis loop, which evolves in a completely opposite manner if the sign of the charge current is flipped. When the coercivity is measured by sweeping an out-of-plane field, its value can be reduced or increased by as much as about 500 Oe if an appropriate charge current is applied. 1. P. Li, T. Liu, H. Chang, A. Kalitsov, W. Zhang, G. Csaba, W. Li, D. Richardson, A. Demann, G. Rimal, H. Dey, J. S. Jiang, W. Porod, S. Field, J. Tang, M. C. Marconi, A. Hoffmann, O. Mryasov, and M. Wu, Nature Commun. 7:12688 doi: 10.1038/ncomms12688 (2016).

  7. Thermally assisted nanosecond laser generation of ferric nanoparticles

    Science.gov (United States)

    Kurselis, K.; Kozheshkurt, V.; Kiyan, R.; Chichkov, B.; Sajti, L.

    2018-03-01

    A technique to increase nanosecond laser based production of ferric nanoparticles by elevating temperature of the iron target and controlling its surface exposure to oxygen is reported. High power near-infrared laser ablation of the iron target heated up to 600 °C enhances the particle generation efficiency by more than tenfold exceeding 6 μg/J. Temporal and thermal dependencies of the particle generation process indicate correlation of this enhancement with the oxidative processes that take place on the iron surface during the per spot interpulse delay. Nanoparticles, produced using the heat-assisted ablation technique, are examined using scanning electron and transmission electron microscopy confirming the presence of 1-100 nm nanoparticles with an exponential size distribution that contain multiple randomly oriented magnetite nanocrystallites. The described process enables the application of high power lasers and facilitates precise, uniform, and controllable direct deposition of ferric nanoparticle coatings at the industry-relevant rates.

  8. The thermal expansion of hard magnetic materials of the Nd-Fe-B system

    Directory of Open Access Journals (Sweden)

    Savchenko Igor

    2017-01-01

    Full Text Available The results of dilatometric measurement of the thermal expansion of hard magnetic materials brands N35M, N35H and N35SH containing as a main component the crystalline phase of Nd2Fe14B type are presented. The temperature range from 200 to 750 K has been investigated by the method of dilatometry with an error of 1.5-2×10-7 K-1. The approximation dependences of the linear thermal expansion coefficient have been obtained. The character of changes of the thermal coefficient of linear expansion in the region of the Curie point has been specified, its critical indices and critical amplitudes have been defined.

  9. Linear and nonlinear stability of a thermally stratified magnetically driven rotating flow in a cylinder.

    Science.gov (United States)

    Grants, Ilmars; Gerbeth, Gunter

    2010-07-01

    The stability of a thermally stratified liquid metal flow is considered numerically. The flow is driven by a rotating magnetic field in a cylinder heated from above and cooled from below. The stable thermal stratification turns out to destabilize the flow. This is explained by the fact that a stable stratification suppresses the secondary meridional flow, thus indirectly enhancing the primary rotation. The instability in the form of Taylor-Görtler rolls is consequently promoted. These rolls can only be excited by finite disturbances in the isothermal flow. A sufficiently strong thermal stratification transforms this nonlinear bypass instability into a linear one reducing, thus, the critical value of the magnetic driving force. A weaker temperature gradient delays the linear instability but makes the bypass transition more likely. We quantify the non-normal and nonlinear components of this transition by direct numerical simulation of the flow response to noise. It is observed that the flow sensitivity to finite disturbances increases considerably under the action of a stable thermal stratification. The capabilities of the random forcing approach to identify disconnected coherent states in a general case are discussed.

  10. The effect of thermal conductivity of the tool electrode in spark-assisted chemical engraving gravity-feed micro-drilling

    International Nuclear Information System (INIS)

    Mousa, M; Allagui, A; Ng, H D; Wüthrich, R

    2009-01-01

    Spark-assisted chemical engraving (SACE) is a non-traditional micro-machining technology based on electrochemical discharge phenomena. In SACE gravity-feed micro-drilling, various parameters including the thermal properties of the tool electrode play a significant role in the process. Based on a series of experiments using tool electrodes with different thermal properties, the effect in SACE gravity-feed micro-drilling is discussed. It is demonstrated that machining with higher thermal conductivity tool electrodes results in faster machining during the discharge regime and slower machining during the hydrodynamic regime of SACE gravity-feed micro-drilling

  11. 2D resistivity imaging and magnetic survey for characterization of thermal springs: A case study of Gergedi thermal springs in the northwest of Wonji, Main Ethiopian Rift, Ethiopia

    Science.gov (United States)

    Abdulkadir, Yahya Ali; Eritro, Tigistu Haile

    2017-09-01

    Electrical resistivity imaging and magnetic surveys were carried out at Gergedi thermal springs, located in the Main Ethiopian Rift, to characterize the geothermal condition of the area. The area is geologically characterized by alluvial and lacustrine deposits, basaltic lava, ignimbrites, and rhyolites. The prominent structural feature in this part of the Main Ethiopian Rift, the SW -NE trending structures of the Wonji Fault Belt System, crosse over the study area. Three lines of imaging data and numerous magnetic data, encompassing the active thermal springs, were collected. Analysis of the geophysical data shows that the area is covered by low resistivity response regions at shallow depths which resulted from saline moisturized soil subsurface horizon. Relatively medium and high resistivity responses resulting from the weathered basalt, rhyolites, and ignimbrites are also mapped. Qualitative interpretation of the magnetic data shows the presence of structures that could act as pathways for heat and fluids manifesting as springs and also characterize the degree of thermal alteration of the area. Results from the investigations suggest that the Gergedi thermal springs area is controlled by fault systems oriented parallel and sub-parallel to the main tectonic lines of the Main Ethiopian Rift.

  12. Environmental Assisted Fatigue Evaluation of Direct Vessel Injection Piping Considering Thermal Stratification

    International Nuclear Information System (INIS)

    Kim, Taesoon; Lee, Dohwan

    2016-01-01

    As the environmentally assisted fatigue (EAF) due to the primary water conditions is to be a critical issue, the fatigue evaluation for the components and pipes exposed to light water reactor coolant conditions has become increasingly important. Therefore, many studies to evaluate the fatigue life of the components and pipes in LWR coolant environments on fatigue life of materials have been conducted. Among many components and pipes of nuclear power plants, the direct vessel injection piping is known to one of the most vulnerable pipe systems because of thermal stratification occurred in that systems. Thermal stratification occurs because the density of water changes significantly with temperature. In this study, fatigue analysis for DVI piping using finite element analysis has been conducted and those results showed that the results met design conditions related with the environmental fatigue evaluation of safety class 1 pipes in nuclear power plants. Structural and fatigue integrity for the DVI piping system that thermal stratification occurred during the plant operation has conducted. First of all, thermal distribution of the piping system is calculated by computational fluid dynamic analysis to analyze the structural integrity of that piping system. And the fatigue life evaluation considering environmental effects was carried out. Our results showed that the DVI piping system had enough structural integrity and fatigue life during the design lifetime of 60 years

  13. Polymer-assisted iron oxide magnetic nanoparticle immobilized keratinase

    Energy Technology Data Exchange (ETDEWEB)

    Konwarh, Rocktotpal; Karak, Niranjan [Advanced Polymer and Nanomaterial Laboratory, Department of Chemical Sciences, Tezpur University, Tezpur-784028, Assam (India); Rai, Sudhir Kumar; Mukherjee, Ashis Kumar [Department of Molecular Biology and Biotechnology, Tezpur University, Tezpur-784028, Assam (India)], E-mail: karakniranjan@yahoo.com

    2009-06-03

    Nanotechnology holds the prospect for avant-garde changes to improve the performance of materials in various sectors. The domain of enzyme biotechnology is no exception. Immobilization of industrially important enzymes onto nanomaterials, with improved performance, would pave the way to myriad application-based commercialization. Keratinase produced by Bacillus subtilis was immobilized onto poly(ethylene glycol)-supported Fe{sub 3}O{sub 4} superparamagnetic nanoparticles. The optimization process showed that the highest enzyme activity was noted when immobilized onto cyanamide-activated PEG-assisted MNP prepared under conditions of 25 deg. C and pH 7.2 of the reaction mixture before addition of H{sub 2}O{sub 2} (3% w/w), 2% (w/v) PEG{sub 6000} and 0.062:1 molar ratio of PEG to FeCl{sub 2}{center_dot}4H{sub 2}O. Further statistical optimization using response surface methodology yielded an R{sup 2} value that could explain more than 94% of the sample variations. Along with the magnetization studies, the immobilization of the enzyme onto the PEG-assisted MNP was characterized by UV, XRD, FTIR and TEM. The immobilization process had resulted in an almost fourfold increase in the enzyme activity over the free enzyme. Furthermore, the immobilized enzyme exhibited a significant thermostability, storage stability and recyclability. The leather-industry-oriented application of the immobilized enzyme was tested for the dehairing of goat-skin.

  14. Polymer-assisted iron oxide magnetic nanoparticle immobilized keratinase

    International Nuclear Information System (INIS)

    Konwarh, Rocktotpal; Karak, Niranjan; Rai, Sudhir Kumar; Mukherjee, Ashis Kumar

    2009-01-01

    Nanotechnology holds the prospect for avant-garde changes to improve the performance of materials in various sectors. The domain of enzyme biotechnology is no exception. Immobilization of industrially important enzymes onto nanomaterials, with improved performance, would pave the way to myriad application-based commercialization. Keratinase produced by Bacillus subtilis was immobilized onto poly(ethylene glycol)-supported Fe 3 O 4 superparamagnetic nanoparticles. The optimization process showed that the highest enzyme activity was noted when immobilized onto cyanamide-activated PEG-assisted MNP prepared under conditions of 25 deg. C and pH 7.2 of the reaction mixture before addition of H 2 O 2 (3% w/w), 2% (w/v) PEG 6000 and 0.062:1 molar ratio of PEG to FeCl 2 ·4H 2 O. Further statistical optimization using response surface methodology yielded an R 2 value that could explain more than 94% of the sample variations. Along with the magnetization studies, the immobilization of the enzyme onto the PEG-assisted MNP was characterized by UV, XRD, FTIR and TEM. The immobilization process had resulted in an almost fourfold increase in the enzyme activity over the free enzyme. Furthermore, the immobilized enzyme exhibited a significant thermostability, storage stability and recyclability. The leather-industry-oriented application of the immobilized enzyme was tested for the dehairing of goat-skin.

  15. Polymer-assisted iron oxide magnetic nanoparticle immobilized keratinase

    Science.gov (United States)

    Konwarh, Rocktotpal; Karak, Niranjan; Rai, Sudhir Kumar; Mukherjee, Ashis Kumar

    2009-06-01

    Nanotechnology holds the prospect for avant-garde changes to improve the performance of materials in various sectors. The domain of enzyme biotechnology is no exception. Immobilization of industrially important enzymes onto nanomaterials, with improved performance, would pave the way to myriad application-based commercialization. Keratinase produced by Bacillus subtilis was immobilized onto poly(ethylene glycol)-supported Fe3O4 superparamagnetic nanoparticles. The optimization process showed that the highest enzyme activity was noted when immobilized onto cyanamide-activated PEG-assisted MNP prepared under conditions of 25 °C and pH 7.2 of the reaction mixture before addition of H2O2 (3% w/w), 2% (w/v) PEG6000 and 0.062:1 molar ratio of PEG to FeCl2·4H2O. Further statistical optimization using response surface methodology yielded an R2 value that could explain more than 94% of the sample variations. Along with the magnetization studies, the immobilization of the enzyme onto the PEG-assisted MNP was characterized by UV, XRD, FTIR and TEM. The immobilization process had resulted in an almost fourfold increase in the enzyme activity over the free enzyme. Furthermore, the immobilized enzyme exhibited a significant thermostability, storage stability and recyclability. The leather-industry-oriented application of the immobilized enzyme was tested for the dehairing of goat-skin.

  16. Thermal, structural and magnetic properties of some zinc phosphate glasses doped with manganese ions

    International Nuclear Information System (INIS)

    Pascuta, Petru; Bosca, Maria; Borodi, Gheorghe; Culea, Eugen

    2011-01-01

    Research highlights: → MnO) x .(P 2 O 5 ) 40 .(ZnO) 60-x glasses (0 ≤ x ≤ 20 mol%) were prepared by the melt-quenching technique. → The DTA data indicate a good thermal stability of the studied glasses. → EPR spectra shows isolated Mn 2+ ions in octahedral symmetric sites or to associated ones when the Mn 2+ ions are involved in dipole-dipole and/or superexchange interactions. → The magnetic susceptibility data revealed superexchange magnetic interactions involving manganese ions, antiferromagnetically coupled for the sample containing 20 mol% MnO. - Abstract: (MnO) x .(P 2 O 5 ) 40 .(ZnO) 60-x glasses containing different concentrations of MnO ranging from 0 to 20 mol% were prepared by the melt-quenching technique. The samples had a fixed P 2 O 5 content of 40 mol% and the MnO:ZnO ratio was varied. The thermal, structural and magnetic properties of these glasses were investigated by means of differential thermal analysis (DTA), electron paramagnetic resonance (EPR) and magnetic susceptibility measurements. Compositional dependence of the glass transition (T g ), crystallization (T p ) and melting temperatures were determined by DTA investigations. From the dependence of the T g on the heating rate (a), the activation energy of the glass transition (E g ) was calculated. The fragility index (F) for the studied glasses was determined to see whether these materials are obtained from kinetically strong-glass-forming (KS) or kinetically fragile-glass forming (KF) liquids. The EPR spectra of the studied glasses revealed absorptions centered at g ∼ 2.0, 3.3 and 4.3. The compositional variations of the intensity and line width of these absorption lines was interpreted in terms of the variation in the concentration of the Mn 2+ and Mn 3+ ions in the glass and the interaction between the manganese ions. EPR and magnetic susceptibility data reveal that both Mn 2+ and Mn 3+ ions are present in the studied glasses, their relative concentration being dependent on

  17. Protection Heater Design Validation for the LARP Magnets Using Thermal Imaging

    CERN Document Server

    Marchevsky, M; Cheng, D W; Felice, H; Sabbi, G; Salmi, T; Stenvall, A; Chlachidze, G; Ambrosio, G; Ferracin, P; Izquierdo Bermudez, S; Perez, J C; Todesco, E

    2016-01-01

    Protection heaters are essential elements of a quench protection scheme for high-field accelerator magnets. Various heater designs fabricated by LARP and CERN have been already tested in the LARP high-field quadrupole HQ and presently being built into the coils of the high-field quadrupole MQXF. In order to compare the heat flow characteristics and thermal diffusion timescales of different heater designs, we powered heaters of two different geometries in ambient conditions and imaged the resulting thermal distributions using a high-sensitivity thermal video camera. We observed a peculiar spatial periodicity in the temperature distribution maps potentially linked to the structure of the underlying cable. Two-dimensional numerical simulation of heat diffusion and spatial heat distribution have been conducted, and the results of simulation and experiment have been compared. Imaging revealed hot spots due to a current concentration around high curvature points of heater strip of varying cross sections and visuali...

  18. Thermal convection in a closed cavity in zero-gravity space conditions with stationary magnetic forces

    International Nuclear Information System (INIS)

    Lyubimova, T; Mailfert, A

    2013-01-01

    The paper deals with the investigation of thermo-magnetic convection in a paramagnetic liquid subjected to a non-uniform magnetic field in weightlessness conditions. Indeed, in zero-g space conditions such as realized in International Space Station (ISS), or in artificial satellite, or in free-flight space vessels, the classical thermo-gravitational convection in fluid disappears. In any cases, it may be useful to restore the convective thermal exchange inside fluids such as liquid oxygen. In this paper, the restoration of heat exchange by the way of creation of magnetic convection is numerically studied.

  19. Observation of thermal quench induced by runaway electrons in magnetic perturbation

    Science.gov (United States)

    Cheon, MunSeong; Seo, Dongcheol; Kim, Junghee

    2018-04-01

    Experimental observations in Korea Superconducting Tokamak Advanced Research (KSTAR) plasmas show that a loss of pre-disruptive runaway electrons can induce a rapid radiative cooling of the plasma, by generating impurity clouds from the first wall. The synchrotron radiation image shows that the loss of runaway electrons occurs from the edge region when the resonant magnetic perturbation is applied on the plasma. When the impact of the runaway electrons on the wall is strong enough, a sudden drop of the electron cyclotron emission (ECE) signal occurs with the characteristic plasma behaviors such as the positive spike and following decay of the plasma current, Dα spike, big magnetic fluctuation, etc. The visible images at this runaway loss show an evidence of the generation of impurity cloud and the following radiative cooling. When the runaway beam is located on the plasma edge, thermal quenches are expected to occur without global destruction of the magnetic structure up to the core.

  20. Tidal Heating of Earth-like Exoplanets around M Stars: Thermal, Magnetic, and Orbital Evolutions.

    Science.gov (United States)

    Driscoll, P E; Barnes, R

    2015-09-01

    The internal thermal and magnetic evolution of rocky exoplanets is critical to their habitability. We focus on the thermal-orbital evolution of Earth-mass planets around low-mass M stars whose radiative habitable zone overlaps with the "tidal zone," where tidal dissipation is expected to be a significant heat source in the interior. We develop a thermal-orbital evolution model calibrated to Earth that couples tidal dissipation, with a temperature-dependent Maxwell rheology, to orbital circularization and migration. We illustrate thermal-orbital steady states where surface heat flow is balanced by tidal dissipation and cooling can be stalled for billions of years until circularization occurs. Orbital energy dissipated as tidal heat in the interior drives both inward migration and circularization, with a circularization time that is inversely proportional to the dissipation rate. We identify a peak in the internal dissipation rate as the mantle passes through a viscoelastic state at mantle temperatures near 1800 K. Planets orbiting a 0.1 solar-mass star within 0.07 AU circularize before 10 Gyr, independent of initial eccentricity. Once circular, these planets cool monotonically and maintain dynamos similar to that of Earth. Planets forced into eccentric orbits can experience a super-cooling of the core and rapid core solidification, inhibiting dynamo action for planets in the habitable zone. We find that tidal heating is insignificant in the habitable zone around 0.45 (or larger) solar-mass stars because tidal dissipation is a stronger function of orbital distance than stellar mass, and the habitable zone is farther from larger stars. Suppression of the planetary magnetic field exposes the atmosphere to stellar wind erosion and the surface to harmful radiation. In addition to weak magnetic fields, massive melt eruption rates and prolonged magma oceans may render eccentric planets in the habitable zone of low-mass stars inhospitable for life.

  1. Nd-Fe-B/Sm-M/Nd-M (M = Fe, Co, Ti, Cu, Zr) hybrid magnets with improved thermal stability

    Science.gov (United States)

    Grigoras, M.; Lostun, M.; Urse, M.; Borza, F.; Chiriac, H.; Lupu, N.

    2018-02-01

    Hybrid magnets of Nd12Fe82B6(2:14:1-phase)/Nd9.4Fe59Co25.3Ti6.3(3:29-phase) and Nd12Fe82B6/Sm11.1Co65.8Fe8.9Cu10.7Zr3.5(2:17-phase) with different weight ratio have been prepared by spark plasma sintering pressing technique from ball-milled powders obtained from melt-spun ribbons. Influence of the ratio between the two phases on the magnetic properties and thermal stability of the hybrid magnets was studied. It has been found that the ratio has a remarkable influence, especially on the thermal stability of the bulk magnets. However, the magnetic properties of such type of hybrid magnets result not only from the type and ratio of components but also from the interaction between them. It was found that in NdFeB/3:29 hybrid magnets with 15% content of 3:29-phase, the temperature coefficients of remanence (α) and of coercivity (β) are improved from -0.095 to -0.082 (%/°C) and from -0.57 to -0.47 (%/°C), respectively, as compared to the Nd2Fe14B single-phase counterpart. While for the NdFeB/2:17 hybrid magnets the content of 2:17-phase is not significantly influencing the temperature coefficient of induction (α), the temperature coefficient of °C (β) increases up to -0.41 (%/°C) for 10% content of 2:17-phase. The increase in the reversible temperature coefficients of hybrid magnets indicate a remarkable improvement of their thermal stability.

  2. Escape from metastable magnetic states: New results on Mn_12 acetate

    Science.gov (United States)

    Kent, Andrew D.

    2000-03-01

    The crossover from thermally assisted to pure quantum tunneling has been studied in Mn_12 acetate molecular crystals using micro-Hall effect magnetometry [1]. Several new features, intrinsic to the magnetization relaxation of this material, have been found. First, magnetic hysteresis measurements have been used to accurately identify the energy levels important to the magnetic relaxation (the ``escape levels’’) as a function of the magnetic field and temperature (0.3 to 3 K) [2]. These results indicate that the escape levels can change either smoothly or abruptly with temperature, depending upon the magnetic field magnitude and orientation. Second, relaxation experiments show evidence for a pure quantum relaxation regime at low temperature (Chudnovsky and D. A. Garanin, Phys. Rev. Lett. 79, 4469 (1997)

  3. Effects of Toroidal Magnetic Fields on the Thermal Instability of Thin ...

    Indian Academy of Sciences (India)

    With this assumption, we obtain a general thermal instability criterion for magne- tized thin disks, i.e.,. = 2 − 5βgas − 4(1 + n)βmag − 6 fadv. + 8 fadvβgas + (8 + 4n) fadvβmag > 0, where βgas, βmag and fadv are the ratio of gas pressure to total pressure, the ratio of magnetic pressure to total pressure, and the advection factor ...

  4. Discharging process of a finned heat pipe–assisted thermal energy storage system with high temperature phase change material

    International Nuclear Information System (INIS)

    Tiari, Saeed; Qiu, Songgang; Mahdavi, Mahboobe

    2016-01-01

    Highlights: • The discharging process of a latent heat thermal energy storage system is studied. • The thermal energy storage system is assisted by finned heat pipes. • The influences of heat pipe spacing and fins geometrical features are studied. • Smaller heat pipe spacing enhances the solidification rate. • Better heat pipe and fin arrangements are determined. - Abstract: This paper presents the results of a numerical study conducted to investigate the discharging process of a latent heat thermal energy storage system assisted by finned heat pipes. A two-dimensional finite volume based numerical model along with enthalpy-porosity technique is employed to simulate the phase change of storage media during the discharging mode. The thermal energy storage system in this study consists of a square container, finned heat pipes, and potassium nitrate (KNO 3 ) as the phase change material. The charging process of the same thermal energy storage system was reported in an early paper by the authors. This paper reports the results of discharging process of the thermal energy storage system. The influences of heat pipe spacing, fin geometry and quantities as well as the effects of natural convection heat transfer on the thermal performance of the storage system were studied. The results indicate that the phase change material solidification process is hardly affected by the natural convection. Decreasing the heat pipe spacing results in faster discharging process and higher container base wall temperature. Increasing the fins length does not change the discharging time but yields higher base wall temperature. Using more fins also accelerates the discharging process and increases the container base wall temperature.

  5. Thermal decomposition of synthetic antlerite prepared by microwave-assisted hydrothermal method

    Energy Technology Data Exchange (ETDEWEB)

    Koga, Nobuyoshi [Chemistry Laboratory, Graduate School of Education, Hiroshima University, 1-1-1 Kagamiyama, Higashi-Hiroshima 739-8524 (Japan)], E-mail: nkoga@hiroshima-u.ac.jp; Mako, Akira; Kimizu, Takaaki; Tanaka, Yuu [Chemistry Laboratory, Graduate School of Education, Hiroshima University, 1-1-1 Kagamiyama, Higashi-Hiroshima 739-8524 (Japan)

    2008-01-30

    Copper(II) hydroxide sulfate was synthesized by a microwave-assisted hydrothermal method from a mixed solution of CuSO{sub 4} and urea. Needle-like crystals of ca. 20-30 {mu}m in length precipitated by irradiating microwave for 1 min were characterized as Cu{sub 3}(OH){sub 4}SO{sub 4} corresponding to mineral antlerite. The reaction pathway and kinetics of the thermal decomposition of the synthetic antlerite Cu{sub 3}(OH){sub 4}SO{sub 4} were investigated by means of thermoanalytical techniques complemented by powder X-ray diffractometry and microscopic observations. The thermal decomposition of Cu{sub 3}(OH){sub 4}SO{sub 4} proceeded via two separated reaction steps of dehydroxylation and desulfation to produce CuO, where crystalline phases of Cu{sub 2}OSO{sub 4} and CuO appeared as the intermediate products. The kinetic characteristics of the respective steps were discussed in comparison with those of the synthetic brochantite Cu{sub 4}(OH){sub 6}SO{sub 4} reported previously.

  6. Development of a procedure for forming assisted thermal joining of tubes

    Science.gov (United States)

    Chen, Hui; Löbbe, Christian; Staupendahl, Daniel; Tekkaya, A. Erman

    2018-05-01

    With the demand of lightweight design in the automotive industry, not only the wall-thicknesses of tubular components of the chassis or spaceframe are continuously decreased. Also the thicknesses of exhaust system parts are reduced to save material and mass. However, thinner tubular parts bring about additional challenges in joining. Welding or brazing methods, which are utilized in joining tubes with specific requirements concerning leak tightness, are sensitive to the gap between the joining partners. Furthermore, a large joining area is required to ensure the durability of the joint. The introduction of a forming step in the assembled state prior to thermal joining can define and control the gap for subsequent brazing or welding. The mechanical pre-joint resulting from the previously described calibration step also results in easier handling of the tubes prior to thermal joining. In the presented investigation, a spinning process is utilized to produce force-fit joints of varying lengths and diameter reduction and form-fit joints with varying geometrical attributes. The spinning process facilitates a high formability and geometrical flexibility, while at the achievable precision is high and the process forces are low. The strength of the joints is used to evaluate the joint quality. Finally, a comparison between joints produced by forming with subsequent brazing and original tube is conducted, which presents the high performance of the developed procedure for forming assisted thermal joining.

  7. Experimental Investigation of A Heat Pipe-Assisted Latent Heat Thermal Energy Storage System

    Science.gov (United States)

    Tiari, Saeed; Mahdavi, Mahboobe; Qiu, Songgang

    2016-11-01

    In the present work, different operation modes of a latent heat thermal energy storage system assisted by a heat pipe network were studied experimentally. Rubitherm RT55 enclosed by a vertical cylindrical container was used as the Phase Change Material (PCM). The embedded heat pipe network consisting of a primary heat pipe and an array of four secondary heat pipes were employed to transfer heat to the PCM. The primary heat pipe transports heat from the heat source to the heat sink. The secondary heat pipes transfer the extra heat from the heat source to PCM during charging process or retrieve thermal energy from PCM during discharging process. The effects of heat transfer fluid (HTF) flow rate and temperature on the thermal performance of the system were investigated for both charging and discharging processes. It was found that the HTF flow rate has a significant effect on the total charging time of the system. Increasing the HTF flow rate results in a remarkable increase in the system input thermal power. The results also showed that the discharging process is hardly affected by the HTF flow rate but HTF temperature plays an important role in both charging and discharging processes. The authors would like to acknowledge the financial supports by Temple University for the project.

  8. Optimized design of a high-power-density PM-assisted synchronous reluctance machine with ferrite magnets for electric vehicles

    Directory of Open Access Journals (Sweden)

    Liu Xiping

    2017-06-01

    Full Text Available This paper proposes a permanent magnet (PM-assisted synchronous reluctance machine (PMASynRM using ferrite magnets with the same power density as rareearth PM synchronous motors employed in Toyota Prius 2010. A suitable rotor structure for high torque density and high power density is discussed with respect to the demagnetization of ferrite magnets, mechanical strength and torque ripple. Some electromagnetic characteristics including torque, output power, loss and efficiency are calculated by 2-D finite element analysis (FEA. The analysis results show that a high power density and high efficiency of PMASynRM are obtained by using ferrite magnets.

  9. Application of a thermally assisted mechanical dewatering process to biomass

    Energy Technology Data Exchange (ETDEWEB)

    Mahmoud, A.; Arlabosse, P. [Universite de Toulouse, Mines Albi, CNRS, Campus Jarlard, F-81013 Albi cedex 09 (France); Ecole des Mines Albi, Centre RAPSODEE, Campus Jarlard, F-81013 Albi (France); Fernandez, A. [Universite de Toulouse, INSA, UPS, INP, LISBP, 135 Avenue de Rangueil, F-31400 Toulouse (France); INRA, UMR792 Ingenierie des Systemes Biologiques et des Procedes, CNRS, UMR5504, F-31400 Toulouse (France)

    2011-01-15

    Thermally assisted mechanical dewatering (TAMD) is a new process for energy-efficient liquid/solids separation which enhances conventional-device efficiency. The main idea of this process is to supply a flow of heat in mechanical dewatering processes to favour the reduction of the liquid content. This is not a new idea but the proposed combination, especially the chosen operating conditions (T < 100 C and P < 3000 kPa) constitutes an original approach and a significant energy saving since the liquid is kept in liquid state. Response surface methodology was used to evaluate the effects of the processing parameters of TAMD on the final dry solids content, which is a fundamental dewatering parameter and an excellent indicator of the extent of TAMD. In this study, a two-factor central composite design was used to establish the optimum conditions for the TAMD of alfalfa biomass. Experiments were carried out on a laboratory compression cell. Experiments showed that the dewatering enhancement results only from thermal effects. With a moderate heat supply (T{sub piston} = 80 C), the dry solid content of the press cake can reach 66%, compared to 36% at ambient temperature. A significant regression model, describing changes on final dry solids content with respect to independent variables, was established with determination coefficient, R{sup 2}, greater than 88%. With an energy consumption of less than 150 kWh/m{sup 3}, the use of the TAMD process before a thermal drying process leads to an energy saving of at least 30% on the overall separation chain. (author)

  10. Synthesis of magnetic microtubes decorated with nanowires and cells

    Science.gov (United States)

    Pomar, C. Diaz; Martinho, H.; Ferreira, F. F.; Goia, T. S.; Rodas, A. C. D.; Santos, S. F.; Souza, J. A.

    2018-04-01

    Antiferromagnetic and ferrimagnetic microtubes decorated with nanowires have been obtained during thermal oxidation process, which was assisted by in situ electrical resistivity measurements. The synthesis route including heat treatment and electrical current along with growth mechanism are presented. This simple method and the ability to tune in the magnetic moment of the obtained microtubes going from a nonmagnetic-like to a large magnetization saturation open an avenue for interesting applications. In vitro experiments involving adherence, migration, and proliferation of fibroblasts cell culture on the surface of the microtubes indicated the absence of cytotoxicity for this material. We have also calculated both torque and driving magnetic force for these microtubes with nanowires and cells as a function of external magnetic field gradient which were found to be robust opening the possibility for magnetic bio micro-robot device fabrication and application in biotechnology.

  11. Effect of magnetic and thermal properties of iron oxide nanoparticles (IONs) in nitrile butadiene rubber (NBR) latex

    International Nuclear Information System (INIS)

    Ong, Hun Tiar; Julkapli, Nurhidayatullaili Muhd; Hamid, Sharifah Bee Abd; Boondamnoen, O.; Tai, Mun Foong

    2015-01-01

    Nitrile butadiene rubber (NBR) gloves are one of the most important personal protective equipments but they are possible to tear off and contaminate food or pharmaceutical and healthcare products during manufacturing and packaging process. High tendency of torn glove remaining in food or products due to white or light flesh-coloured glove is not easy to be detected by naked eyes. In this paper, iron oxide nanoparticles (IONs) selected as additive for NBR to improve its detectability by mean of magnetic properties. IONs synthesized via precipitation method and compounded with NBR latex before casting on petri dish. The properties of IONs were investigated by X-ray Diffractometry (XRD), Transmission Electron Microscope (TEM), Raman Spectroscopy and Vibrating Sample Magnetometer (VSM). Meanwhile NBR/IONs composites were studied by Thermogravimetry Analysis (TGA), Differential Scanning Calorimetry (DSC) and Vibrating Sample Magnetometer (VSM). It observed that, synthesized IONs shows of 25.28 nm crystallite with 25.86 nm semipherical (changed as) shape. Meanwhile, Magnetite and maghemite phase are found in range of 670 cm −1 and 700 cm −1 respectively, which it contributes magnetization saturation of 73.96 emu/g at 10,000 G by VSM. Thermal stability and magnetic properties were increased with incorporating IONs into NBR latex up to 20 phr. NBR/IONs 5 phr has the optimum thermal stability, lowest glass transition temperature (−14.83 °C) and acceptable range of magnetization saturation (3.83 emu/g at 10,000 G) to form NBR gloves with magnetic detectability. - Highlights: • We synthesized IONs with high magnetization saturation (M s ). • High M s of IONs were incorporated into NBR latex in order to induce magnetic properties in the NBR composite. • Introduction of IONs into NBR latex would improve thermal properties. • The produced NBR/IONs 5 phr composite exceeded the minimum magnetic moment sensor of the detector. • They have high potential for the

  12. Effect of magnetic and thermal properties of iron oxide nanoparticles (IONs) in nitrile butadiene rubber (NBR) latex

    Energy Technology Data Exchange (ETDEWEB)

    Ong, Hun Tiar; Julkapli, Nurhidayatullaili Muhd; Hamid, Sharifah Bee Abd, E-mail: sharifahbee@um.edu.my; Boondamnoen, O.; Tai, Mun Foong

    2015-12-01

    Nitrile butadiene rubber (NBR) gloves are one of the most important personal protective equipments but they are possible to tear off and contaminate food or pharmaceutical and healthcare products during manufacturing and packaging process. High tendency of torn glove remaining in food or products due to white or light flesh-coloured glove is not easy to be detected by naked eyes. In this paper, iron oxide nanoparticles (IONs) selected as additive for NBR to improve its detectability by mean of magnetic properties. IONs synthesized via precipitation method and compounded with NBR latex before casting on petri dish. The properties of IONs were investigated by X-ray Diffractometry (XRD), Transmission Electron Microscope (TEM), Raman Spectroscopy and Vibrating Sample Magnetometer (VSM). Meanwhile NBR/IONs composites were studied by Thermogravimetry Analysis (TGA), Differential Scanning Calorimetry (DSC) and Vibrating Sample Magnetometer (VSM). It observed that, synthesized IONs shows of 25.28 nm crystallite with 25.86 nm semipherical (changed as) shape. Meanwhile, Magnetite and maghemite phase are found in range of 670 cm{sup −1} and 700 cm{sup −1} respectively, which it contributes magnetization saturation of 73.96 emu/g at 10,000 G by VSM. Thermal stability and magnetic properties were increased with incorporating IONs into NBR latex up to 20 phr. NBR/IONs 5 phr has the optimum thermal stability, lowest glass transition temperature (−14.83 °C) and acceptable range of magnetization saturation (3.83 emu/g at 10,000 G) to form NBR gloves with magnetic detectability. - Highlights: • We synthesized IONs with high magnetization saturation (M{sub s}). • High M{sub s} of IONs were incorporated into NBR latex in order to induce magnetic properties in the NBR composite. • Introduction of IONs into NBR latex would improve thermal properties. • The produced NBR/IONs 5 phr composite exceeded the minimum magnetic moment sensor of the detector. • They have high

  13. Freely oriented portable superconducting magnet

    Science.gov (United States)

    Schmierer, Eric N [Los Alamos, NM; Prenger, F Coyne [Los Alamos, NM; Hill, Dallas D [Los Alamos, NM

    2010-01-12

    A freely oriented portable superconducting magnet is disclosed. Coolant is supplied to the superconducting magnet from a repository separate from the magnet, enabling portability of the magnet. A plurality of support assemblies structurally anchor and thermally isolate the magnet within a thermal shield. A plurality of support assemblies structurally anchor and thermally isolate the thermal shield within a vacuum vessel. The support assemblies restrain movement of the magnet resulting from energizing and cooldown, as well as from changes in orientation, enabling the magnet to be freely orientable.

  14. Morphology and magnetic properties of CeCo{sub 5} submicron flakes prepared by surfactant-assisted high-energy ball milling

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, J.J.; Gao, H.M.; Yan, Y.; Bai, X.; Su, F.; Wang, W.Q. [State key Laboratory for Superhard Materials and Department of Physics, Jilin University, Changchun 130012 (China); Du, X.B., E-mail: duxb@jlu.edu.cn [State key Laboratory for Superhard Materials and Department of Physics, Jilin University, Changchun 130012 (China)

    2012-10-15

    CeCo{sub 5} permanent magnetic alloy has been processed by surfactant assisted high energy ball milling. Heptane and oleic acid were used as the solvent and surfactant, respectively. The amount of surfactant used was 50% by weight of the starting powder. The produced particles were deposited on a piece of copper (4 mm in length and width) under a magnetic field of 27 kOe applied along the copper surface and immobilized by ethyl {alpha}-cyanoacrylate. Scanning electron microscope pictures show that the particles are flakes, several {mu}m in length and width and tens of nm in thickness. X-ray diffraction patterns and magnetic measurements prove that the flakes are crystalline with c-axes magnetic anisotropy. The easy magnetization axis is oriented perpendicular to the surface of the flake. A maximum coercivity of 3.3 kOe was obtained for the sample milled for 40 min. - Highlights: Black-Right-Pointing-Pointer CeCo{sub 5} permanent magnetic alloy has been processed by surfactant assisted high energy ball milling (HEBM). Black-Right-Pointing-Pointer The particles show a flake-like morphology with several {mu}m in length and width and tens nm in thickness. Black-Right-Pointing-Pointer The flakes are crystallographic and magnetic anisotropic and the c-axes, also the easy magnetization directions are oriented perpendicular to the surface of the flake. Black-Right-Pointing-Pointer Maximum coercivity of 3.3 kOe has been obtained for the sample milled for 40 min.

  15. Gonioscopy-assisted Transluminal Trabeculotomy (GATT): Thermal Suture Modification With a Dye-stained Rounded Tip.

    Science.gov (United States)

    Grover, Davinder S; Fellman, Ronald L

    2016-06-01

    To describe a novel technique for thermally marking the tip of a suture, in preparation for a gonioscopy-assisted transluminal trabeculotomy. One patient was used as an example for this technique. Technique report. The authors introduce a modification of a novel surgical procedure (GATT) in which a suture is marked and thermally blunted allowing a proper visualization while performing an ab interno, minimally invasive, circumferential 360-degree suture trabeculotomy. The authors have previously reported on the GATT surgery with the use of an illuminated microcatheter, which allowed for visualization of the tip of the catheter as it circumnavigated Schlemm canal. This modification allows for similar visualization of the tip of the suture, however, is much more cost-effective while still maintaining similar safety.

  16. Laser assisted crystallization of ferromagnetic amorphous ribbons: A multimodal characterization and thermal model study

    Energy Technology Data Exchange (ETDEWEB)

    Katakam, Shravana; Santhanakrishnan, S.; Smith, Casey; Banerjee, Rajarshi; Dahotre, Narendra B. [Laboratory of Laser Materials Processing and Synthesis Department of Materials Science and Engineering University of North Texas, Denton, Texas 76207 (United States); Devaraj, Arun; Bowden, Mark; Thevuthasan, Suntharampillai [William R. Wiley Environmental Molecular Sciences Laboratory, Pacific Northwest National Laboratory, Richland, Washington 99352 (United States); Ramanujan, R. V. [Schhol of Materials Science and Engineering Nanyang Technological University, Singapore 639798 (Singapore)

    2013-11-14

    This paper focuses on laser-based de-vitrification of amorphous soft magnetic Fe-Si-B ribbons and its consequent influence on the magnetic properties. Laser processing resulted in a finer scale of crystallites due to rapid heating and cooling during laser annealing compared to conventional furnace annealing process. A significant increase in saturation magnetization is observed for laser-annealed ribbons compared to both as-received and furnace annealed samples coupled with an increase in coercivity compared to the as received samples. The combined effect of thermal histories and stresses developed during laser annealing results in the formation of nano-crystalline phase along the laser track. The phase evolution is studied by micro-XRD and TEM analysis. Solute partitioning and compositional variation within the phases are obtained by Local Electrode Atom probe analysis. The evolution of microstructure is rationalized using a Finite Element based heat transfer multi-physics model.

  17. Spin-wave thermal population as temperature probe in magnetic tunnel junctions

    Energy Technology Data Exchange (ETDEWEB)

    Le Goff, A., E-mail: adrien.le-goff@u-psud.fr; Devolder, T. [Institut d' Electronique Fondamentale, CNRS, Univ. Paris-Sud, Université Paris-Saclay, 91405 Orsay (France); Nikitin, V. [SAMSUNG Electronics Corporation, 601 McCarthy Blvd Milpitas, California 95035 (United States)

    2016-07-14

    We study whether a direct measurement of the absolute temperature of a Magnetic Tunnel Junction (MTJ) can be performed using the high frequency electrical noise that it delivers under a finite voltage bias. Our method includes quasi-static hysteresis loop measurements of the MTJ, together with the field-dependence of its spin wave noise spectra. We rely on an analytical modeling of the spectra by assuming independent fluctuations of the different sub-systems of the tunnel junction that are described as macrospin fluctuators. We illustrate our method on perpendicularly magnetized MgO-based MTJs patterned in 50 × 100 nm{sup 2} nanopillars. We apply hard axis (in-plane) fields to let the magnetic thermal fluctuations yield finite conductance fluctuations of the MTJ. Instead of the free layer fluctuations that are observed to be affected by both spin-torque and temperature, we use the magnetization fluctuations of the sole reference layers. Their much stronger anisotropy and their much heavier damping render them essentially immune to spin-torque. We illustrate our method by determining current-induced heating of the perpendicularly magnetized tunnel junction at voltages similar to those used in spin-torque memory applications. The absolute temperature can be deduced with a precision of ±60 K, and we can exclude any substantial heating at the spin-torque switching voltage.

  18. Mechanical and thermal measurements on a 11 m long beam screen in the LHC Magnet Test String during RUN 3A

    CERN Document Server

    Artoos, K; Kos, N

    1999-01-01

    Two eleven meter long beam screens were installed in the third dipole of the LHC Magnet Test String. Instrumentation was used to measure the mechanical and thermal behaviour of the screens during thermal transients and quenches. The horizontal deformation, angular displacement, heating of the screen as a result of the quench induced eddy currents and relative longitudinal displacement between beam screen and magnet end were measured.

  19. Computer-assisted training in the thermal production department

    International Nuclear Information System (INIS)

    Felgines, R.

    1985-01-01

    For many years now, in the United States and Canada, computer-assisted training (CAT) experiments have been carried out in various fields: general or professional education, student testing in universities. This method seems very promising and particularly for continuing education and for keeping industrial process operating and maintenance personnel abreast of their specialities. Thanks to the progress in data processing and remote processing with central computers, this technique is being developed in France for professional training applications. Faced with many training problems, the Thermal Production Department of EDF (Electricite de France) first conducted in 1979 a test involving a limited subset of the nuclear power station operating personnel; this course amounted to some ten hours with very limited content. It seemed promising enough, so that in 1981, a real test was launched at 4 PWR plants: DAMPIERRE, FESSENHEIM, GRAVELINES, TRICASTIN. This test which involves about 700 employees has been fruitful and we decided to generalise this system to all the French nuclear power plants (40 units of 900 and 1300 MW). (author)

  20. Thermal and magnetic behavior of Angustifolia Kunth bamboo fibers covered with Fe{sub 3}O{sub 4} particles

    Energy Technology Data Exchange (ETDEWEB)

    Calvo, S. [Laboratorio de Magnetismo y Materiales Avanzados, Facultad de Ciencias Exactas y Naturales, Universidad Nacional de Colombia, Sede Manizales, Manizales (Colombia); Arias, N.P. [Laboratorio de Materiales Nanoestructurados y Funcionales, Facultad de Ciencias Exactas y Naturales, Universidad Nacional de Colombia, Sede Manizales, Manizales (Colombia); Departamento de Ingenieria Electrica, Electronica y Computacion, Facultad de Ingenieria y Arquitectura, Universidad Nacional de Colombia, Sede Manizales, Manizales (Colombia); Giraldo, O., E-mail: ohggiraldo@hotmail.com [Laboratorio de Materiales Nanoestructurados y Funcionales, Facultad de Ciencias Exactas y Naturales, Universidad Nacional de Colombia, Sede Manizales, Manizales (Colombia); Rosales-Rivera, A.; Moscoso, O. [Laboratorio de Magnetismo y Materiales Avanzados, Facultad de Ciencias Exactas y Naturales, Universidad Nacional de Colombia, Sede Manizales, Manizales (Colombia)

    2012-08-15

    Several Angustifolia Kunth bamboo fibers, which have been previously treated with an alkaline solution, were coated with magnetite particles. The coating of the fibers was achieved by an in-situ co-precipitation method with Fe{sup 2+} and Fe{sup 3+}in NaOH or NH{sub 4}OH. The fibers were evaluated by chemical analysis using atomic absorption (A.A.) technique, structural characterization by X-ray diffraction (XRD), thermal stability with thermo-gravimetric analysis (TGA) in nitrogen at temperature range between 23 Degree-Sign C and 800 Degree-Sign C and magnetic behavior using vibrating sample magnetometry (VSM) applying a magnetic field between -27 KOe and 27 KOe at room temperature. We found that the thermal stability and magnetization depend of the synthesis method used to cover the Angustifolia Kunth bamboo fibers. In addition, an improved magnetic response was observed when NaOH solution is used to generate the magnetite coating on the fiber surface.

  1. Implant-assisted magnetic drug targeting in permeable microvessels: Comparison of two-fluid statistical transport model with experiment

    Energy Technology Data Exchange (ETDEWEB)

    ChiBin, Zhang; XiaoHui, Lin, E-mail: lxh60@seu.edu.cn; ZhaoMin, Wang; ChangBao, Wang

    2017-03-15

    In experiments and theoretical analyses, this study examines the capture efficiency (CE) of magnetic drug carrier particles (MDCPs) for implant-assisted magnetic drug targeting (IA-MDT) in microvessels. It also proposes a three-dimensional statistical transport model of MDCPs for IA-MDT in permeable microvessels, which describes blood flow by the two-fluid (Casson and Newtonian) model. The model accounts for the permeable effect of the microvessel wall and the coupling effect between the blood flow and tissue fluid flow. The MDCPs move randomly through the microvessel, and their transport state is described by the Boltzmann equation. The regulated changes and factors affecting the CE of the MDCPs in the assisted magnetic targeting were obtained by solving the theoretical model and by experimental testing. The CE was negatively correlated with the blood flow velocity, and positively correlated with the external magnetic field intensity and microvessel permeability. The predicted CEs of the MDCPs were consistent with the experimental results. Additionally, under the same external magnetic field, the predicted CE was 5–8% higher in the IA-MDT model than in the model ignoring the permeability effect of the microvessel wall. - Highlights: • A model of MDCPs for IA-MDT in permeable microvessels was established. • An experimental device was established, the CE of MDCPs was measured. • The predicted CE of MDCPs was 5–8% higher in the IA-MDT model.

  2. Magnetic graphene enabled tunable microwave absorber via thermal control

    Science.gov (United States)

    Quan, L.; Qin, F. X.; Li, Y. H.; Estevez, D.; Fu, G. J.; Wang, H.; Peng, H.-X.

    2018-06-01

    By synthesizing nitrogen-doped graphene (NG) via a facile thermal annealing method, a fine control of the amount and location of doped nitrogen as well as the oxygen-containing functional groups is achieved with varying annealing temperature. The favorable magnetic properties have been achieved for N-doped rGO samples obtained at two temperatures of all NG samples, i.e., 500 °C and 900 °C with saturation magnetization of 0.63 emu g‑1 and 0.67 emu g‑1 at 2 K, respectively. This is attributed to the optimized competition of the N-doping and reduction process at 500 °C and the dominated reduction process at 900 °C. NG obtained at 300 °C affords the best overall absorbing performance: when the absorber thickness is 3.0 mm, the maximum absorption was ‑24.6 dB at 8.51 GHz, and the absorption bandwidth was 4.89 GHz (7.55–12.44 GHz) below ‑10 dB. It owes its large absorbing intensity to the good impedance match and significant dielectric loss. The broad absorption bandwidth benefits from local fluctuations of dielectric responses contributed by competing mechanisms. Despite the significant contribution from materials loss to the absorption, the one quarter-wavelength model is found to be responsible for the reflection loss peak positions. Of particular significance is that an appropriate set of electromagnetic parameters associated with reasonable reduction is readily accessible by convenient control of annealing temperature to modulate the microwave absorbing features of graphene. Thus, NG prepared by thermal annealing promises to be a highly efficient microwave absorbent.

  3. Magnetic susceptibilities and thermal expansion of artificial graphites

    International Nuclear Information System (INIS)

    Cornuault, P.; Herpin, A.; Hering, H.; Seguin, M.; Commissariat a l'Energie Atomique, Saclay

    1960-01-01

    Starting from measurements of the magnetic susceptibility made in the two principal directions of a graphite bar, the distribution function of the normals to the carbon planes in the crystallites has been evaluated. The effect of different variation in the manufacturing process on this crystalline anisotropy has been studied. From this crystalline anisotropy we have calculated the thermal expansion coefficient possessed by a compact mass of crystallites having exactly the same orientational anisotropy as the porous body consideration. The difference between this and the observed expansion coefficient leads to the determination of the expansion of the non-graphitic part of the mass which turns out to have a negative value and is also anisotropic. We have attempted to draw some conclusions from this result. (author) [fr

  4. Performance Analysis of Permanent Magnet Motors for Electric Vehicles (EV Traction Considering Driving Cycles

    Directory of Open Access Journals (Sweden)

    Thanh Anh Huynh

    2018-05-01

    Full Text Available This paper evaluates the electromagnetic and thermal performance of several traction motors for electric vehicles (EVs. Two different driving cycles are employed for the evaluation of the motors, one for urban and the other for highway driving. The electromagnetic performance to be assessed includes maximum motor torque output for vehicle acceleration and the flux weakening capability for wide operating range under current and voltage limits. Thermal analysis is performed to evaluate the health status of the magnets and windings for the prescribed driving cycles. Two types of traction motors are investigated: two interior permanent magnet motors and one permanent magnet-assisted synchronous reluctance motor. The analysis results demonstrate the benefits and disadvantages of these motors for EV traction and provide suggestions for traction motor design. Finally, experiments are conducted to validate the analysis.

  5. Relaxation of a coherent, magnetic s–p model system coupled to one and two thermal baths and a laser pulse

    Energy Technology Data Exchange (ETDEWEB)

    Lefkidis, G. [Department of Physics and Research Center OPTIMAS, University of Kaiserslautern, Box 3049, 67653 Kaiserslautern (Germany); School of Mechanics, Civil Engineering and Architecture, Northwestern Polytechnical University, Xi’an 710072 (China); Sold, S.; Hübner, W. [Department of Physics and Research Center OPTIMAS, University of Kaiserslautern, Box 3049, 67653 Kaiserslautern (Germany)

    2017-06-15

    We study an s–p model magnetic system with a triplet ground state coupled to two temperature baths. By varying the temperatures we both generate non-thermal electronic distributions and create additional coherences in the density matrix of the system. Thus the thermally-induced magnetic response goes beyond the simple picture of majority-minority population dynamics. Furthermore, we discuss the influence of temperature induced relaxation effects on the dynamics induced by an optical perturbation for this quantum system.

  6. Thermal instabilities in magnetically confined plasmas: Solar coronal loops

    International Nuclear Information System (INIS)

    Habbal, S.R.; Rosner, R.

    1979-01-01

    The thermal stability of confined solar coronal structures (''loops'') is investigated, following both normal mode and a new, global instability analysis. We demonstrate that: (a) normal mode analysis shows modes with size scales comparable to that of loops to be unstable, but to be strongly affected by the loop boundary conditions; (b) a global analysis, based upon variation of the total loop energy losses and gains, yields loop stability conditions for global modes dependent upon the coronal loop heating process, with magnetically coupled heating processes giving marginal stability. The connection between the present analysis and the minimum flux corona of Hearn is also discussed

  7. Growth of wrinkle-free graphene on texture-controlled platinum films and thermal-assisted transfer of large-scale patterned graphene.

    Science.gov (United States)

    Choi, Jae-Kyung; Kwak, Jinsung; Park, Soon-Dong; Yun, Hyung Duk; Kim, Se-Yang; Jung, Minbok; Kim, Sung Youb; Park, Kibog; Kang, Seoktae; Kim, Sung-Dae; Park, Dong-Yeon; Lee, Dong-Su; Hong, Suk-Kyoung; Shin, Hyung-Joon; Kwon, Soon-Yong

    2015-01-27

    Growth of large-scale patterned, wrinkle-free graphene and the gentle transfer technique without further damage are most important requirements for the practical use of graphene. Here we report the growth of wrinkle-free, strictly uniform monolayer graphene films by chemical vapor deposition on a platinum (Pt) substrate with texture-controlled giant grains and the thermal-assisted transfer of large-scale patterned graphene onto arbitrary substrates. The designed Pt surfaces with limited numbers of grain boundaries and improved surface perfectness as well as small thermal expansion coefficient difference to graphene provide a venue for uniform growth of monolayer graphene with wrinkle-free characteristic. The thermal-assisted transfer technique allows the complete transfer of large-scale patterned graphene films onto arbitrary substrates without any ripples, tears, or folds. The transferred graphene shows high crystalline quality with an average carrier mobility of ∼ 5500 cm(2) V(-1) s(-1) at room temperature. Furthermore, this transfer technique shows a high tolerance to variations in types and morphologies of underlying substrates.

  8. Helium leak testing of superconducting magnets, thermal shields and cryogenic lines of SST -1

    International Nuclear Information System (INIS)

    Thankey, P.L.; Joshi, K.S.; Semwal, P.; Pathan, F.S.; Raval, D.C.; Khan, Z.; Patel, R.J.; Pathak, H.A.

    2005-01-01

    Tokamak SST - 1 is under commissioning at Institute for Plasma Research. It comprises of a toroidal doughnut shaped plasma chamber, surrounded by liquid helium cooled superconducting magnets, housed in a cryostat chamber. The cryostat has two cooling circuits, (1) liquid nitrogen cooling circuit operating at 80 K to minimize the radiation heat load on the magnets, and (2) liquid helium cooling circuit to cool magnets and cold mass support structure to 4.5 K. In this paper we describe (a) the leak testing of copper - SS joints, brazing joints, interconnecting joints of the superconducting magnets, and (b) the leak testing of the liquid nitrogen cooling circuit, comprising of the main supply header, the thermal shields, interconnecting pipes, main return header and electrical isolators. All these tests were carried out using both vacuum and sniffer methods. (author)

  9. Magnetic field-assisted synthesis of wire-like Co3O4 nanostructures: Electrochemical and photocatalytic studies

    International Nuclear Information System (INIS)

    Zhao, Xiubin; Pang, Zhanwen; Wu, Mingzai; Liu, Xiansong; Zhang, Hui; Ma, Yongqing; Sun, Zhaoqi; Zhang, Lide; Chen, Xiaoshuang

    2013-01-01

    Graphical abstract: Schematic illustration for the magnetic field-assisted growth of wire-like Co 3 O 4 nanostructure. Display Omitted Highlights: ► Co 3 O 4 nanowires are prepared by magnetic field hydrothermal reduction and annealing. ► These Co 3 O 4 nanowires possess enhanced capacitance. ► The Co 3 O 4 nanowires have a good photocatalytic activity for methyl orange. -- Abstract: Wire-like Co 3 O 4 nanostructures were prepared by the combination of magnetic field-assisted hydrothermal reduction of cobalt ions and the subsequent ambient annealing at 500 °C. X-ray diffraction (XRD) and scanning electron microscopy (SEM) were used to characterize the structure and morphological evolution of the products. The results show that the wire-like nanostructures possess diameters about 250 nm and lengths over 10 μm. The possible formation mechanism of the wire-like Co 3 O 4 nanostructures is also proposed based on the SEM results. Galvanostatic methods were used to characterize the electrochemical properties. The measurements indicate that the wire-like Co 3 O 4 nanostructures show larger discharge and charge capacities than that of spherical Co 3 O 4 nanoparticles prepared in the absence of magnetic field. In addition, the photocatalytic activity of the products was investigated by measuring the photodegradation of methyl orange solution under ultraviolet radiation, which shows that both the wire-like and spherical products have a good photocatalytic activity.

  10. Thermal electron transport in regimes with low and negative magnetic shear in Tore Supra

    International Nuclear Information System (INIS)

    Voitsekhovitch, I.; Litaudon, X.; Moreau, D.; Aniel, T.; Becoulet, A.; Erba, M.; Joffrin, E.; Kazarian-Vibert, F.; Peysson, Y.

    1997-01-01

    The magnetic shear effect on thermal electron transport is studied in a large variety of non-inductive plasmas in Tore Supra. An improved confinement in the region of low and negative shear was observed and quantified with an exponential dependence on the magnetic shear (Litaudon, et al., Fusion Energy 1996 (Proc. 16th Int. Conf. Montreal, 1996), Vol. 1, IAEA, Vienna (1997) 669). This is interpreted as a consequence of a decoupling of the global modes (Romanelli and Zonca, Phys. Fluids B 5 (1993) 4081) that are thought to be responsible for anomalous transport. This dependence is proposed in order to complete the Bohm-like L mode local electron thermal diffusivity so as to describe the transition from Bohm-like to gyroBohm transport in the plasma core. The good agreement between the predictive simulations of the different Tore Supra regimes (hot core lower hybrid enhanced performance, reversed shear plasmas and combined lower hybrid current drive and fast wave electron heating) and experimental data provides a basis for extrapolation of this magnetic shear dependence in the local transport coefficients to future machines. As an example, a scenario for non-inductive current profile optimization and control in ITER is presented. (author)

  11. Calcium-assisted reduction of cobalt ferrite nanoparticles for nanostructured iron cobalt with enhanced magnetic performance

    International Nuclear Information System (INIS)

    Qi, B.; Andrew, J. S.; Arnold, D. P.

    2017-01-01

    This paper demonstrates the potential of a calcium-assisted reduction process for synthesizing fine-grain (~100 nm) metal alloys from metal oxide nanoparticles. To demonstrate the process, an iron cobalt alloy (Fe_6_6Co_3_4) is obtained by hydrogen annealing 7-nm cobalt ferrite (CoFe_2O_4) nanoparticles in the presence of calcium granules. The calcium serves as a strong reducing agent, promoting the phase transition from cobalt ferrite to a metallic iron cobalt alloy, while maintaining high crystallinity. Magnetic measurements demonstrate the annealing temperature is the dominant factor of tuning the grain size and magnetic properties. Annealing at 700 °C for 1 h maximizes the magnetic saturation, up to 2.4 T (235 emu/g), which matches that of bulk iron cobalt.

  12. Calcium-assisted reduction of cobalt ferrite nanoparticles for nanostructured iron cobalt with enhanced magnetic performance

    Energy Technology Data Exchange (ETDEWEB)

    Qi, B. [University of Florida, Interdisciplinary Microsystems Group, Department of Electrical and Computer Engineering (United States); Andrew, J. S. [University of Florida, Department of Materials Science and Engineering (United States); Arnold, D. P., E-mail: darnold@ufl.edu [University of Florida, Interdisciplinary Microsystems Group, Department of Electrical and Computer Engineering (United States)

    2017-03-15

    This paper demonstrates the potential of a calcium-assisted reduction process for synthesizing fine-grain (~100 nm) metal alloys from metal oxide nanoparticles. To demonstrate the process, an iron cobalt alloy (Fe{sub 66}Co{sub 34}) is obtained by hydrogen annealing 7-nm cobalt ferrite (CoFe{sub 2}O{sub 4}) nanoparticles in the presence of calcium granules. The calcium serves as a strong reducing agent, promoting the phase transition from cobalt ferrite to a metallic iron cobalt alloy, while maintaining high crystallinity. Magnetic measurements demonstrate the annealing temperature is the dominant factor of tuning the grain size and magnetic properties. Annealing at 700 °C for 1 h maximizes the magnetic saturation, up to 2.4 T (235 emu/g), which matches that of bulk iron cobalt.

  13. A novel solar-assisted heat pump driven by photovoltaic/thermal collectors: Dynamic simulation and thermoeconomic optimization

    International Nuclear Information System (INIS)

    Calise, Francesco; Dentice d'Accadia, Massimo; Figaj, Rafal Damian; Vanoli, Laura

    2016-01-01

    This paper presents a dynamic simulation model and a thermo-economic analysis of a novel polygeneration system based on a solar-assisted heat pump and an adsorption chiller, both driven by PVT (photovoltaic/thermal) collectors. The aim of this work is to design and dynamically simulate a novel ultra-high efficient solar heating and cooling system. The overall plant layout is designed to supply electricity, space heating and cooling and domestic hot water for a small residential building. The system combines solar cooling, solar-assisted heat pump and photovoltaic/thermal collector technologies in a novel solar polygeneration system. In fact, the polygeneration system is based on a PVT solar field, coupled with a water-to-water electric heat pump or to an adsorption chiller. PVT collectors simultaneously produce electricity and thermal energy. During the winter, hot water produced by PVT collectors primarily supplies the evaporator of the heat pump, whereas in summer, solar energy supplies an adsorption chiller providing the required space cooling. All year long, solar thermal energy in excess is converted into DHW (domestic hot water). The system model was developed in TRNSYS environment. 1-year dynamic simulations are performed for different case studies in various weather conditions. The results are analysed on different time bases presenting energetic, environmental and economic performance data. Finally, a sensitivity analysis and a thermoeconomic optimization were performed, in order to determine the set of system design/control parameters that minimize the simple pay-back period. The results showed a total energy efficiency of the PVT of 49%, a heat pump yearly coefficient of performance for heating mode above 4 and a coefficient of performance of the adsorption chiller of 0.55. Finally, it is also concluded that system performance is highly sensitive to the PVT field area. The system is profitable when a capital investment subsidy of 50% is considered

  14. Magnetic fluctuations due to thermally excited Alfven waves

    International Nuclear Information System (INIS)

    Agim, Y.Z.; Prager, S.C.

    1990-01-01

    Magnetic fluctuations due to the thermally excited MHD waves are investigated using fluid and kinetic models to describe a stable, uniform, compressible plasma in the range above the drift wave frequency and below the ion cyclotron frequency. It is shown that the fluid model with resistivity yields spectral densities which are roughly Lorentzian, exhibit equipartition with no apparent cutoff in wavenumber space and a Bohm-type diffusion coefficient. Under certain conditions, the ensuing transport may be comparable to classical values. For a phenomenological cutoff imposed on the spectrum, the typical fluctuating-to-equilibrium magnetic field ratio is found to be of the order of 10 -10 . Physical mechanisms to obtain decay profiles of the spectra with increasing wavenumber due to dispersion and/or different forms of damping are investigated analytically in a cold fluid approximation and numerically, with a kinetic model. The mode dispersion due to the finite ion-gyrofrequency is identified as the leading effect determining the spectral profile shapes. It is found that the amplitude of fluctuations may be within a factor of the value suggested by the cold plasma model. The results from both models are presented and compared in low- and high-β regimes. 21 refs., 6 figs

  15. Complementary variational principle method applied to thermal conductivities of a plasma in a uniform magnetic field

    Energy Technology Data Exchange (ETDEWEB)

    Sehgal, A K; Gupta, S C [Punjabi Univ., Patiala (India). Dept. of Physics

    1982-12-14

    The complementary variational principles method (CVP) is applied to the thermal conductivities of a plasma in a uniform magnetic field. The results of computations show that the CVP derived results are very useful.

  16. The microstructure and magnetic properties of anisotropic polycrystalline Nd2Fe14B nanoflakes prepared by surfactant-assisted cryomilling

    International Nuclear Information System (INIS)

    Liu, Lidong; Zhang, Jian; Xia, Weixing; Du, Juan; Yan, Aru; Ping Liu, J; Li, Wei; Guo, Zhaohui

    2014-01-01

    A new method for fabricating rare-earth-transition metal nanoflakes and nanoparticles, surfactant-assisted cryomilling (SACM), was developed. The effects of milling temperature on the particle size, microstructure and magnetic performance of Nd 2 Fe 14 B nanoflakes were investigated systematically. Compared with Nd 2 Fe 14 B nanoflakes prepared by surfactant-assisted ball milling (SABM) at room temperature, the samples prepared by SACM showed more intriguing features such as smaller particle sizes, larger microstrain, smaller grain size and higher coercivity, which were ascribed to a higher defect concentration generated in the nanoflakes. The optimal coercivity of the samples prepared by SACM was about 50% higher than that of the samples milled at room temperature. It is demonstrated that SACM is an effective way to prepare rare-earth-transition metal nanoflakes with higher coercivity and smaller particle size. These findings are of importance for research on sintered magnets and high-performance nanocomposite magnets. (papers)

  17. Fundamental research on the gravity assisted heat pipe thermal storage unit (GAHP-TSU) with porous phase change materials (PCMs) for medium temperature applications

    International Nuclear Information System (INIS)

    Hu, Bo-wen; Wang, Qian; Liu, Zhen-Hua

    2015-01-01

    Highlights: • A novel gravity-assisted heat pipe thermal storage unit (GAHP-TSU) is presented and tested. • Composite granular solid–liquid PCM is piled up as the porous medium layer in GAHP-TSU. • GAHP-TSU avoids the major obstacle of low thermal conductivity of the PCM. • GAHP-TSU enables the thermal storage unit with outstanding heat transfer performance. - Abstract: In this study, a novel gravity-assisted heat pipe type thermal storage unit (GAHP-TSU) has been presented for the potential application in solar air conditioning and refrigeration systems, in which composite granular solid–liquid PCMs compounded by RT100 and high-density polyethylene with phase change temperature of 100 °C are piled up as a porous PCMs medium layer. Water is used as heat transfer fluid in the GAHP-TSU. The heat transfer mechanism of heat storage/release in the GAHP-TSU is similar to that of the gravity-assisted heat pipe, which is superior to traditional direct-contact or indirect-contact thermal storage units. The properties of start-up, heat transfer characteristics on the stages of heat absorption and release of the GAHP-TSU are studied in detailed, including necessary calculations based on heat transfer theory. The results show that the whole system is almost isothermal at the temperature over 70 °C and the heat transfer properties are excellent both for heat absorption and release stages. The GAHP-TSU device with low thermal conductivity of the PCMs is promising in potential industry applications

  18. High speed subfractional HP-motor with permanent magnets

    International Nuclear Information System (INIS)

    Hanitsch, R.; Frenzel, B.

    1998-01-01

    During the last years an increasing demand for small permanent magnet motors can be detected, especially in the fields of medical applications. For heart assist devices there is the request to have small high speed devices operating at low voltage supply with almost no overtemperature. The design of a special hollow shaft motor for the speed range of 15000..25000 rpm and a torque of 4 to 8 mNm will be outlined. The low noise requirements and the high efficiency request lead to a design with an airgap winding. A thermal analysis is also done in order to meet the conditions given by the medical specialists. The features of the prototype will be presented and also the sensorless control strategy will be outlined. Measured and calculated data show good agreement. Focus will be on the magnetic circuit and the thermal behaviour and not on the control aspects of the motor. Specific parameters demonstrate the good quality of the drive system. (orig.)

  19. Thermal plasma synthesis of Fe1−xNix alloy nanoparticles

    International Nuclear Information System (INIS)

    Raut, Suyog A.; Kanhe, Nilesh S.; Bhoraskar, S. V.; Mathe, V. L.; Das, A. K.

    2014-01-01

    Fe-Ni alloy nanoparticles are of great interest because of diverse practical applications in the fields such as magnetic fluids, high density recording media, catalysis and medicine. We report the synthesis of Fe-Ni nanoparticles via thermal plasma route. Thermal plasma assisted synthesis is a high temperature process and gives high yields of production. Here, we have used direct arc thermal plasma plume of 6kw as a source of energy at operating pressure 500 Torr. The mixture of Fe-Ni powder in required proportion (Fe 1−x Ni x ; x=0.30, 0.32, 0.34, 0.36, 0.38 and 0.40) was made to evaporate simultaneously from the graphite anode in thermal plasma reactor to form Fe-Ni bimetallic nanoparticles. The as synthesized particles were characterized by X-Ray Diffraction (XRD), Thermo-Gravimetric Analysis/Differential Scanning Calorimtry (TGA/DSC)

  20. Topological honeycomb magnon Hall effect: A calculation of thermal Hall conductivity of magnetic spin excitations

    Energy Technology Data Exchange (ETDEWEB)

    Owerre, S. A., E-mail: solomon@aims.ac.za [African Institute for Mathematical Sciences, 6 Melrose Road, Muizenberg, Cape Town 7945, South Africa and Perimeter Institute for Theoretical Physics, 31 Caroline St. N., Waterloo, Ontario N2L 2Y5 (Canada)

    2016-07-28

    Quite recently, the magnon Hall effect of spin excitations has been observed experimentally on the kagome and pyrochlore lattices. The thermal Hall conductivity κ{sup xy} changes sign as a function of magnetic field or temperature on the kagome lattice, and κ{sup xy} changes sign upon reversing the sign of the magnetic field on the pyrochlore lattice. Motivated by these recent exciting experimental observations, we theoretically propose a simple realization of the magnon Hall effect in a two-band model on the honeycomb lattice. The magnon Hall effect of spin excitations arises in the usual way via the breaking of inversion symmetry of the lattice, however, by a next-nearest-neighbour Dzyaloshinsky-Moriya interaction. We find that κ{sup xy} has a fixed sign for all parameter regimes considered. These results are in contrast to the Lieb, kagome, and pyrochlore lattices. We further show that the low-temperature dependence on the magnon Hall conductivity follows a T{sup 2} law, as opposed to the kagome and pyrochlore lattices. These results suggest an experimental procedure to measure thermal Hall conductivity within a class of 2D honeycomb quantum magnets and ultracold atoms trapped in a honeycomb optical lattice.

  1. Micromagnetic analysis of geometrically controlled current-driven magnetization switching

    Directory of Open Access Journals (Sweden)

    O. Alejos

    2017-05-01

    Full Text Available The magnetization dynamics induced by current pulses in a pair of two “S-shaped” ferromagnetic elements, each one consisting on two oppositely tilted tapered spikes at the ends of a straight section, is theoretically studied by means of micromagnetic simulations. Our results indicate that the magnetization reversal is triggered by thermal activation, which assists the current-induced domain nucleation and the propagation of domain walls. The detailed analysis of the magnetization dynamics reveals that the magnetization switching is only achieved when a single domain wall is nucleated in the correct corner of the element. In agreement with recent experimental studies, the switching is purely dictated by the shape, being independent of the current polarity. The statistical study points out that successful switching is only achieved within a narrow range of the current pulse amplitudes.

  2. Production and corrosion resistance of NdFeBZr magnets with an improved response to thermal variations during sintering

    International Nuclear Information System (INIS)

    Yu, L.Q.; Zhong, X.L.; Zhang, Y.P.; Yan, Y.G.; Zhen, Y.H.; Zakotnik, M.

    2011-01-01

    This study describes an attempt to produce NdFeB magnets that are insensitive to the sintering temperature. It was found that addition of Zr to NdFeB magnets significantly augmented the thermal stability of this magnetic material during sintering at high temperature even at industrial scale. The best sintered magnets were produced by jet-milling the powder (to achieve an average 3.4 μm particle size), and then aligned, pressed and sintered under argon at 1100 o C for 3 h followed by appropriate heat treatment. The magnetic properties of the resulting magnets were: (BH) m =403.8 kJ m -3 (±4.7 kJ m -3 ), B r =1430 mT (±9 mT) and i H c =907 kA m -1 (±12 kA m -1 ). Large grain growth, in excess of 100 μm in the Zr-free magnets, was observed during sintering at 1100 o C. This did not occur in the presence of Zr. These observations imply that the sensitivity of this class of magnets to high sintering temperatures is greatly reduced by Zr addition. Corrosion resistance of NdFeB was therefore significantly improved by the addition of small amounts of Zr. - Research highlights: →This study describes an attempt to produce NdFeB magnets that are insensitive to the sintering temperature. → It was found that addition of Zr to NdFeB magnets significantly augmented the thermal stability of this magnetic material during sintering at high temperature; even at industrial scale. → The magnetic properties of the resulting magnets were: (BH) m =403.8 kJ m -3 (±4.7 kJ m -3 ), B r =1430 mT (±9 mT) and i H c =907 kA m -1 (±12 kA m -1 ).

  3. Bounds on the entanglement attainable from unitary transformed thermal states in liquid-state nuclear magnetic resonance

    International Nuclear Information System (INIS)

    Yu, Terri M.; Brown, Kenneth R.; Chuang, Isaac L.

    2005-01-01

    The role of mixed-state entanglement in liquid-state nuclear magnetic resonance (NMR) quantum computation is not yet well understood. In particular, despite the success of quantum-information processing with NMR, recent work has shown that quantum states used in most of those experiments were not entangled. This is because these states, derived by unitary transforms from the thermal equilibrium state, were too close to the maximally mixed state. We are thus motivated to determine whether a given NMR state is entanglable - that is, does there exist a unitary transform that entangles the state? The boundary between entanglable and nonentanglable thermal states is a function of the spin system size N and its temperature T. We provide bounds on the location of this boundary using analytical and numerical methods; our tightest bound scales as N∼T, giving a lower bound requiring at least N∼22 000 proton spins to realize an entanglable thermal state at typical laboratory NMR magnetic fields. These bounds are tighter than known bounds on the entanglability of effective pure states

  4. Magnetic Thermal Ablation Using Ferrofluids: Influence of Administration Mode on Biological Effect in Different Porcine Tissues

    International Nuclear Information System (INIS)

    Bruners, Philipp; Hodenius, Michael; Baumann, Martin; Oversohl, Jessica; Guenther, Rolf W.; Schmitz-Rode, Thomas; Mahnken, Andreas H.

    2008-01-01

    The purpose of this study was to compare the effects of magnetic thermal ablation in different porcine tissues using either a singular injection or a continuous infusion of superparamagnetic iron oxide nanoparticles. In the first setting samples of three ferrofluids containing different amounts of iron (1:171, 2:192, and 3:214 mg/ml) were singularly interstitially injected into specimens of porcine liver, kidney, and muscle (n = 5). Then the specimens were exposed to an alternating magnetic field (2.86 kA/m, 190 kHz) generated by a circular coil for 5 min. In the second experimental setup ferrofluid samples were continuously interstitially infused into the tissue specimens during the exposure to the magnetic field. To measure the temperature increase two fiber-optic temperature probes with a fixed distance of 0.5 cm were inserted into the specimens along the puncture tract of the injection needle and the temperature was measured every 15 s. Finally, the specimens were dissected, the diameters of the created thermal lesions were measured, and the volumes were calculated and compared. Compared to continuous infusion, a single injection of ferrofluids resulted in smaller coagulation volumes in all tissues. Significant differences regarding coagulation volume were found in kidney and muscle specimens. The continuous infusion technique led to more elliptically shaped coagulation volumes due to larger diameters along the puncture tract. Our data show the feasibility of magnetic thermal ablation using either a single interstitial injection or continuous infusion for therapy of lesions in muscle, kidney, and liver. Continuous infusion of ferrofluids results in larger zones of necrosis compared to a single injection technique.

  5. {CoIII2DyIII2} single molecule magnet with two resolved thermal activated magnetization relaxation pathways at zero field.

    Science.gov (United States)

    Funes, Alejandro V; Carrella, Luca; Rentschler, Eva; Alborés, Pablo

    2014-02-14

    The new complex [Co(III)2Dy(III)2(OMe)2(teaH)2(Piv)6] in the {Co(III)2Dy(III)2} family, shows two well resolved thermal activated magnetization relaxation pathways under AC experiments in zero DC field. Fitted crystal field parameters suggest that the origin of these two pathways relies on two different excited mJ sub-levels.

  6. Direct observation of the thermal demagnetization of magnetic vortex structures in nonideal magnetite recorders

    DEFF Research Database (Denmark)

    Almeida, Trevor P.; Muxworthy, Adrian R.; Kovács, András

    2016-01-01

    The thermal demagnetization of pseudo-single-domain (PSD) magnetite (Fe3O4) particles, which govern the magnetic signal in many igneous rocks, is examined using off-axis electron holography. Visualization of a vortex structure held by an individual Fe3O4 particle (~250nm in diameter) during in situ...

  7. Thermal expansion and magnetic properties of benzoquinone-bridged dinuclear rare-earth complexes.

    Science.gov (United States)

    Moilanen, Jani O; Mansikkamäki, Akseli; Lahtinen, Manu; Guo, Fu-Sheng; Kalenius, Elina; Layfield, Richard A; Chibotaru, Liviu F

    2017-10-10

    The synthesis and structural characterization of two benzoquinone-bridged dinuclear rare-earth complexes [BQ(MCl 2 ·THF 3 ) 2 ] (BQ = 2,5-bisoxide-1,4-benzoquinone; M = Y (1), Dy (2)) are described. Of these reported metal complexes, the dysprosium analogue 2 is the first discrete bridged dinuclear lanthanide complex in which both metal centres reside in pentagonal bipyramidal environments. Interestingly, both complexes undergo significant thermal expansion upon heating from 120 K to 293 K as illustrated by single-crystal X-ray and powder diffraction experiments. AC magnetic susceptibility measurements reveal that 2 does not show the slow relation of magnetization in zero dc field. The absent of single-molecule behaviour in 2 arises from the rotation of the principal magnetic axis as compared to the pseudo-C 5 axis of the pentagonal bipyramidal environment as suggested by ab initio calculations. The cyclic voltammetry and chemical reduction experiments demonstrated that complexes 1 and 2 can be reduced to radical species containing [BQ 3 ˙ - ]. This study establishes efficient synthetic strategy to make bridged redox-active multinuclear lanthanide complexes with a pentagonal bipyramidal coordination environment that are potential precursors for single-molecule magnets.

  8. Microwave-assisted RAFT polymerization of well-constructed magnetic surface molecularly imprinted polymers for specific recognition of benzimidazole residues

    Science.gov (United States)

    Chen, Fangfang; Wang, Jiayu; Chen, Huiru; Lu, Ruicong; Xie, Xiaoyu

    2018-03-01

    Magnetic nanoparticles have been widely used as support core for fast separation, which could be directly separated from complicated matrices using an external magnet in few minutes. Surface imprinting based on magnetic core has shown favorable adsorption and separation performance, including good adsorption capacity, fast adsorption kinetics and special selectivity adsorption. Reversible addition-fragmentation chain transfer (RAFT) is an ideal choice for producing well-defined complex architecture with mild reaction conditions. We herein describe the preparation of well-constructed magnetic molecularly imprinted polymers (MMIPs) for the recognition of benzimidazole (BMZ) residues via the microwave-assisted RAFT polymerization. The merits of RAFT polymerization assisting with microwave heating allowed successful and more efficient preparation of well-constructed imprinted coats. Moreover, the polymerization time dramatically shortened and was just 1/24th of the time taken by conventional heating. The results indicated that a uniform nanoscale imprinted layer was formed on the Fe3O4 core successfully, and enough saturation magnetization of MMIPs (16.53 emu g-1) was got for magnetic separation. The desirable adsorption capacity (30.18 μmol g-1) and high selectivity toward template molecule with a selectivity coefficient (k) of 13.85 of MMIPs were exhibited by the adsorption isothermal assay and competitive binding assay, respectively. A solid phase extraction enrichment approach was successfully established for the determination of four BMZ residues from apple samples using MMIPs coupled to HPLC. Overall, this study provides a versatile approach for highly efficient fabrication of well-constructed MMIPs for enrichment and determination of target molecules from complicated samples.

  9. Thermal Entanglement and Critical Behavior of Magnetic Properties on a Triangulated Kagomé Lattice

    Directory of Open Access Journals (Sweden)

    N. Ananikian

    2011-01-01

    Full Text Available The equilibrium magnetic and entanglement properties in a spin-1/2 Ising-Heisenberg model on a triangulated Kagomé lattice are analyzed by means of the effective field for the Gibbs-Bogoliubov inequality. The calculation is reduced to decoupled individual (clusters trimers due to the separable character of the Ising-type exchange interactions between the Heisenberg trimers. The concurrence in terms of the three qubit isotropic Heisenberg model in the effective Ising field in the absence of a magnetic field is non-zero. The magnetic and entanglement properties exhibit common (plateau, peak features driven by a magnetic field and (antiferromagnetic exchange interaction. The (quantum entangled and non-entangled phases can be exploited as a useful tool for signalling the quantum phase transitions and crossovers at finite temperatures. The critical temperature of order-disorder coincides with the threshold temperature of thermal entanglement.

  10. Theoretical modelling of physiologically stretched vessel in magnetisable stent assisted magnetic drug targeting application

    International Nuclear Information System (INIS)

    Mardinoglu, Adil; Cregg, P.J.; Murphy, Kieran; Curtin, Maurice; Prina-Mello, Adriele

    2011-01-01

    The magnetisable stent assisted magnetic targeted drug delivery system in a physiologically stretched vessel is considered theoretically. The changes in the mechanical behaviour of the vessel are analysed under the influence of mechanical forces generated by blood pressure. In this 2D mathematical model a ferromagnetic, coiled wire stent is implanted to aid collection of magnetic drug carrier particles in an elastic tube, which has similar mechanical properties to the blood vessel. A cyclic mechanical force is applied to the elastic tube to mimic the mechanical stress and strain of both the stent and vessel while in the body due to pulsatile blood circulation. The magnetic dipole-dipole and hydrodynamic interactions for multiple particles are included and agglomeration of particles is also modelled. The resulting collection efficiency of the mathematical model shows that the system performance can decrease by as much as 10% due to the effects of the pulsatile blood circulation. - Research highlights: →Theoretical modelling of magnetic drug targeting on a physiologically stretched stent-vessel system. →Cyclic mechanical force applied to mimic the mechanical stress and strain of both stent and vessel. →The magnetic dipole-dipole and hydrodynamic interactions for multiple particles is modelled. →Collection efficiency of the mathematical model is calculated for different physiological blood flow and magnetic field strength.

  11. Thermal aging of melt-spun NdFeB magnetic powder in hydrogen

    International Nuclear Information System (INIS)

    Pinkerton, Frederick E.; Balogh, Michael P.; Ellison, Nicole; Foto, Aldo; Sechan, Martin; Tessema, Misle M.; Thompson, Margarita P.

    2016-01-01

    High energy product neodymium-iron-boron (NdFeB) magnets are the premier candidate for demanding electrified vehicle traction motor applications. Injection molded (IM) or compression molded (CM) magnets made using NdFeB powders are promising routes to improve motor efficiency, cost, and manufacturability. However, IM and CM NdFeB magnets are susceptible to substantial thermal aging losses at motor operating temperatures when exposed to the automatic transmission fluid (ATF) used as a lubricant and cooling medium. The intrinsic coercivity H ci of NdFeB IM and CM magnets degrades by as much as 18% when aged for 1000 h in ATF at 150 °C, compared to a 3% loss when aged in air. Here we report aging studies of rapidly quenched NdFeB powder in air, ATF, and H 2 gas. Expansion of the NdFeB crystal lattice in both ATF and H 2 identified hydrogen dissociated from the ATF during aging and diffused into the primary NdFeB phase as the probable cause of the coercivity loss of IM and CM magnets. - Highlights: • Injection molded NdFeB magnets age rapidly in automatic transmission fluid (ATF). • Coercivity loss is not due to direct chemical reaction between ATF and the powder. • Chemical reaction with the binder does not play a major role in aging. • Hydrogen dissociates from ATF and diffuses into Nd 2 Fe 14 B, reducing coercivity.

  12. Thermal aging of melt-spun NdFeB magnetic powder in hydrogen

    Energy Technology Data Exchange (ETDEWEB)

    Pinkerton, Frederick E., E-mail: frederick.e.pinkerton@gm.com [Chemical and Materials Systems Laboratory, General Motors Research and Development Center, Warren, MI 48092 (United States); Balogh, Michael P.; Ellison, Nicole [Chemical and Materials Systems Laboratory, General Motors Research and Development Center, Warren, MI 48092 (United States); Foto, Aldo [Element Materials Technology Wixom, Inc (United States); Sechan, Martin; Tessema, Misle M.; Thompson, Margarita P. [Powertrain Materials/Fluids/AMPPD Engineering and Labs, GFL VE/PT Materials Engineering, General Motors LLC, Pontiac, MI 48340 (United States)

    2016-11-01

    High energy product neodymium-iron-boron (NdFeB) magnets are the premier candidate for demanding electrified vehicle traction motor applications. Injection molded (IM) or compression molded (CM) magnets made using NdFeB powders are promising routes to improve motor efficiency, cost, and manufacturability. However, IM and CM NdFeB magnets are susceptible to substantial thermal aging losses at motor operating temperatures when exposed to the automatic transmission fluid (ATF) used as a lubricant and cooling medium. The intrinsic coercivity H{sub ci} of NdFeB IM and CM magnets degrades by as much as 18% when aged for 1000 h in ATF at 150 °C, compared to a 3% loss when aged in air. Here we report aging studies of rapidly quenched NdFeB powder in air, ATF, and H{sub 2} gas. Expansion of the NdFeB crystal lattice in both ATF and H{sub 2} identified hydrogen dissociated from the ATF during aging and diffused into the primary NdFeB phase as the probable cause of the coercivity loss of IM and CM magnets. - Highlights: • Injection molded NdFeB magnets age rapidly in automatic transmission fluid (ATF). • Coercivity loss is not due to direct chemical reaction between ATF and the powder. • Chemical reaction with the binder does not play a major role in aging. • Hydrogen dissociates from ATF and diffuses into Nd{sub 2}Fe{sub 14}B, reducing coercivity.

  13. Thermal Analysis on Radial Flux Permanent Magnet Generator (PMG using Finite Element Method

    Directory of Open Access Journals (Sweden)

    Hilman Syaeful A Syaeful A

    2011-05-01

    Full Text Available The main source of heat in the permanent magnet generator (PMG is the total losses which f come from winding losses, core losses and rotational losses. Total heat arising from such these losses must be properly distributed and maintained so as not to exceed the maximum allowable temperature to prevent damage to insulation on the winding and demagnetization on the permanent magnet machines. In this research, we consider thermal analysis which is occurred on the radial flux PMG by using finite element method to determine the extent to which the heat generated can be properly distributed. The simulation results show that there are no points of heat concentration or hot spot. The simulation maximum temperatures of the permanent magnet and the winding are 39.1oC and 72.5oC respectively while the experimental maximum temperature of the winding is 62oC.

  14. Effects of thermal fluctuations on non-minimal regular magnetic black hole

    International Nuclear Information System (INIS)

    Jawad, Abdul; Shahzad, M.U.

    2017-01-01

    We analyze the effects of thermal fluctuations on a regular black hole (RBH) of the non-minimal Einstein-Yang-Mill theory with gauge field of magnetic Wu-Yang type and a cosmological constant. We consider the logarithmic corrected entropy in order to analyze the thermal fluctuations corresponding to non-minimal RBH thermodynamics. In this scenario, we develop various important thermodynamical quantities, such as entropy, pressure, specific heats, Gibb's free energy and Helmholtz free energy. We investigate the first law of thermodynamics in the presence of logarithmic corrected entropy and non-minimal RBH. We also discuss the stability of this RBH using various frameworks such as the γ factor (the ratio of heat capacities), phase transition, grand canonical ensemble and canonical ensemble. It is observed that the non-minimal RBH becomes globally and locally more stable if we increase the value of the cosmological constant. (orig.)

  15. Effects of thermal fluctuations on non-minimal regular magnetic black hole

    Energy Technology Data Exchange (ETDEWEB)

    Jawad, Abdul [COMSATS Institute of Information Technology, Department of Mathematics, Lahore (Pakistan); Shahzad, M.U. [COMSATS Institute of Information Technology, Department of Mathematics, Lahore (Pakistan); University of Central Punjab, CAMS, UCP Business School, Lahore (Pakistan)

    2017-05-15

    We analyze the effects of thermal fluctuations on a regular black hole (RBH) of the non-minimal Einstein-Yang-Mill theory with gauge field of magnetic Wu-Yang type and a cosmological constant. We consider the logarithmic corrected entropy in order to analyze the thermal fluctuations corresponding to non-minimal RBH thermodynamics. In this scenario, we develop various important thermodynamical quantities, such as entropy, pressure, specific heats, Gibb's free energy and Helmholtz free energy. We investigate the first law of thermodynamics in the presence of logarithmic corrected entropy and non-minimal RBH. We also discuss the stability of this RBH using various frameworks such as the γ factor (the ratio of heat capacities), phase transition, grand canonical ensemble and canonical ensemble. It is observed that the non-minimal RBH becomes globally and locally more stable if we increase the value of the cosmological constant. (orig.)

  16. Structure and magnetism of SmCo5 nanoflakes prepared by surfactant-assisted ball milling with different ball sizes

    International Nuclear Information System (INIS)

    Nie, Junwu; Han, Xianghua; Du, Juan; Xia, Weixing; Zhang, Jian; Guo, Zhaohui; Yan, Aru; Li, Wei; Ping Liu, J.

    2013-01-01

    Anisotropic magnetic SmCo 5 nanoflakes have been fabricated by surfactant-assisted ball milling (SABM) using hardened steel balls of one of the following sizes: 4, 6.5, 9.5 and 12.7 mm in diameters. The magnetic properties of SmCo 5 particles prepared by SABM with different milling ball sizes in diameters were investigated systematically. It was showed that the nanoflakes milled by amount of small size balls had a higher coercivity and lower anisotropy, i.e., worse grain orientation although in a short milling time while the nanoflakes prepared with same weight of big balls tend to have a lower coercivity, better grain orientation. The coercivity mechanism of the nanoflake was studied and it was mainly dominated with the domain-wall pinning. The SEM analysis shows that the morphology of nanoflakes prepared with different ball sizes are almost the same when the balls to powder weight ratio is fixed. The different magnetic properties caused by different ball sizes are mainly due to the different microstructure changes, i.e, grain refinement and c-axis orientation, which are demonstrated by X-ray diffraction (XRD) analysis and transmission electron microscope (TEM). Based on the experiments above, a combined milling process was suggested and done to improve magnetic properties as your need. - Highlights: • We fabricated anisotropic magnetic SmCo 5 nanoflakes by surfactant-assisted ball milling (SABM). • We investigated the magnetic properties of SmCo 5 particles systematically. It was showed that the coercivity, high or low, and grain orientation, good or bad, were influenced strongly by balls size. The different magnetisms caused by different ball sizes is mainly due to the different microstructure changes. • The coercivity mechanism of the nanoflake was studied and it was mainly dominated with the domain-wall pinning

  17. Magnetic properties evolution of a high permeability nanocrystalline FeCuNbSiB during thermal ageing

    Science.gov (United States)

    Lekdim, Atef; Morel, Laurent; Raulet, Marie-Ange

    2017-07-01

    It is found to be one of the major issues while designing an aircraft, mass and volume have to be reduced in order to achieve energy efficiency. This leads to a high compactness of the electrical components which enables them to withstand at high temperatures. The magnetic components which are responsible for the electrical energy conversion, therefore exposed to high temperatures in working conditions. Their thermal ageing becomes a serious problem and deserves a particular attention. The FeCuNbSiB nanocrystalline materials have been selected for this ageing study because they are used in power electronic systems very frequently. The objective of the study is based on monitoring the magnetic characteristics under the condition of several continuous thermal ageing (100, 150, 200 and 240 °C). An important, experimental work of magnetic characterization is being done through a specific monitoring protocol and X-ray diffraction (XRD) along with magnetostriction measurements was carried out to support the study of the evolution of the anisotropy energies with aging. The latter is discussed in this paper to explain and give the hypothesis about the aging phenomena. Contribution to the topical issue "Electrical Engineering Symposium (SGE 2016)", edited by Adel Razek

  18. Chiral charge erasure via thermal fluctuations of magnetic helicity

    International Nuclear Information System (INIS)

    Long, Andrew J.; Sabancilar, Eray

    2016-01-01

    We consider a relativistic plasma of fermions coupled to an Abelian gauge field and carrying a chiral charge asymmetry, which might arise in the early Universe through baryogenesis. It is known that on large length scales, λ≳1/(αμ_5), the chiral anomaly opens an instability toward the erasure of chiral charge and growth of magnetic helicity. Here the chemical potential μ_5 parametrizes the chiral asymmetry and α is the fine-structure constant. We study the process of chiral charge erasure through the thermal fluctuations of magnetic helicity and contrast with the well-studied phenomenon of Chern-Simons number diffusion. Through the fluctuation-dissipation theorem we estimate the amplitude and time scale of helicity fluctuations on the length scale λ, finding δ H∼λT and τ∼αλ"3T"2 for a relativistic plasma at temperature T. We argue that the presence of a chiral asymmetry allows the helicity to grow diffusively for a time t∼T"3/(α"5μ_5"4) until it reaches an equilibrium value H∼μ_5T"2/α, and the chiral asymmetry is partially erased. If the chiral asymmetry is small, μ_5< T/α, this avenue for chiral charge erasure is found to be slower than the chiral magnetic effect for which t∼T/(α"3μ_5"2). This mechanism for chiral charge erasure can be important for the hypercharge sector of the Standard Model as well as extensions including U(1) gauge interactions, such as asymmetric dark matter models.

  19. Role of field-induced nanostructures, zippering and size polydispersity on effective thermal transport in magnetic fluids without significant viscosity enhancement

    Science.gov (United States)

    Vinod, Sithara; Philip, John

    2017-12-01

    Magnetic nanofluids or ferrofluids exhibit extraordinary field dependant tunable thermal conductivity (k), which make them potential candidates for microelectronic cooling applications. However, the associated viscosity enhancement under an external stimulus is undesirable for practical applications. Further, the exact mechanism of heat transport and the role of field induced nanostructures on thermal transport is not clearly understood. In this paper, through systematic thermal, rheological and microscopic studies in 'model ferrofluids', we demonstrate for the first time, the conditions to achieve very high thermal conductivity to viscosity ratio. Highly stable ferrofluids with similar crystallite size, base fluid, capping agent and magnetic properties, but with slightly different size distributions, are synthesized and characterized by X-ray diffraction, small angle X-ray scattering, transmission electron microscopy, dynamic light scattering, vibrating sample magnetometer, Fourier transform infrared spectroscopy and thermo-gravimetry. The average hydrodynamic diameters of the particles were 11.7 and 10.1 nm and the polydispersity indices (σ), were 0.226 and 0.151, respectively. We observe that the system with smaller polydispersity (σ = 0.151) gives larger k enhancement (130% for 150 G) as compared to the one with σ = 0.226 (73% for 80 G). Further, our results show that dispersions without larger aggregates and with high density interfacial capping (with surfactant) can provide very high enhancement in thermal conductivity, with insignificant viscosity enhancement, due to minimal interfacial losses. We also provide experimental evidence for the effective heat conduction (parallel mode) through a large number of space filling linear aggregates with high aspect ratio. Microscopic studies reveal that the larger particles act as nucleating sites and facilitate lateral aggregation (zippering) of linear chains that considerably reduces the number density of space

  20. THE EFFECT OF ELECTRON THERMAL PRESSURE ON THE OBSERVED MAGNETIC HELICITY IN THE SOLAR WIND

    Energy Technology Data Exchange (ETDEWEB)

    Markovskii, S. A.; Vasquez, Bernard J.; Smith, Charles W., E-mail: sergei.markovskii@unh.edu, E-mail: bernie.vasquez@unh.edu, E-mail: charles.smith@unh.edu [Space Science Center, University of New Hampshire, Durham, NH 03824 (United States)

    2016-12-20

    Statistical analysis of magnetic helicity spectra in the solar wind at 1 au is carried out. A large database of the solar wind intervals assembled from Wind spacecraft magnetic and plasma data is used. The effect of the electron thermal pressure on the wavenumber position of the helicity signature, i.e., the peak of the spectrum, is studied. The position shows a statistically significant dependence on both the electron and proton pressures. However, the strongest dependence is seen when the two pressures are summed. These findings confirm that the generation of the magnetic helicity is associated with an increasing compressibility of the turbulent fluctuations at smaller kinetic scales. It is argued that instrumental artifacts do not contribute to the helicity signature.

  1. Thermal and microstructural analysis of an aluminium A356 alloy solidified by magnetic agitation

    International Nuclear Information System (INIS)

    Bustos, O; Ordonez, S; Jarami, Dario; Colas, R

    2008-01-01

    A magnetic agitation device was designed using a permanently rotating magnetic field, in order to study the effect of applying a variable magnetic field to agitate cast metals during the solidification process. The procedure used to verify the machine's functioning involved smelting and casting a predefined amount of A356 alloy in the device with and without the application of the magnetic field and then characterizing the material obtained with standard procedures of metallographic analysis. The results obtained show that the application of a permanently rotating magnetic field produces a destruction of the cast dendritic structure. This is explained by the fact that a magnetic field that varies over time induces a f.e.m. in a fluid conductor that becomes an increased convective transport through the Lorentz force. This work also studied the kinetics of solidification. The alloy was heated to 680 o C and was cast in molds preheated to 200 o C. Tests were carried out with and without the application of magnetic agitation. The cooling curves were recorded to evaluate the effect of the magnetic agitation on the alloy's form of solidification. The thermal analysis of the cooling curves shows a decrease in the temperatures under which the formation of dendrites from the primary phase as well as from the eutectic Al-Si phase begins when a magnetic field is imposed. A series of intermetallic AlFeSi type compounds appear in these alloys, which display noticeable refining and redistribution from the magnetic agitation (au)

  2. Magnetic Nanoparticle-Assisted Tunable Optical Patterns from Spherical Cholesteric Liquid Crystal Bragg Reflectors

    Directory of Open Access Journals (Sweden)

    Yali Lin

    2017-11-01

    Full Text Available Cholesteric liquid crystals (CLCs exhibit selective Bragg reflections of circularly polarized (CP light owing to their spontaneous self-assembly abilities into periodic helical structures. Photonic cross-communication patterns could be generated toward potential security applications by spherical cholesteric liquid crystal (CLC structures. To endow these optical patterns with tunability, we fabricated spherical CLC Bragg reflectors in the shape of microshells by glass-capillary microfluidics. Water-soluble magnetofluid with Fe3O4 nanoparticles incorporated in the inner aqueous core of CLC shells is responsible for the non-invasive transportable capability. With the aid of an external magnetic field, the reflection interactions between neighboring microshells and microdroplets were identified by varying the mutual distance in a group of magnetically transportable and unmovable spherical CLC structures. The temperature-dependent optical reflection patterns were investigated in close-packed hexagonal arrangements of seven CLC microdroplets and microshells with inverse helicity handedness. Moreover, we demonstrated that the magnetic field-assisted assembly of microshells array into geometric figures of uppercase English letters “L” and “C” was successfully achieved. We hope that these findings can provide good application prospects for security pattern designs.

  3. Magnetic Nanoparticle-Assisted Tunable Optical Patterns from Spherical Cholesteric Liquid Crystal Bragg Reflectors.

    Science.gov (United States)

    Lin, Yali; Yang, Yujie; Shan, Yuwei; Gong, Lingli; Chen, Jingzhi; Li, Sensen; Chen, Lujian

    2017-11-08

    Cholesteric liquid crystals (CLCs) exhibit selective Bragg reflections of circularly polarized (CP) light owing to their spontaneous self-assembly abilities into periodic helical structures. Photonic cross-communication patterns could be generated toward potential security applications by spherical cholesteric liquid crystal (CLC) structures. To endow these optical patterns with tunability, we fabricated spherical CLC Bragg reflectors in the shape of microshells by glass-capillary microfluidics. Water-soluble magnetofluid with Fe₃O₄ nanoparticles incorporated in the inner aqueous core of CLC shells is responsible for the non-invasive transportable capability. With the aid of an external magnetic field, the reflection interactions between neighboring microshells and microdroplets were identified by varying the mutual distance in a group of magnetically transportable and unmovable spherical CLC structures. The temperature-dependent optical reflection patterns were investigated in close-packed hexagonal arrangements of seven CLC microdroplets and microshells with inverse helicity handedness. Moreover, we demonstrated that the magnetic field-assisted assembly of microshells array into geometric figures of uppercase English letters "L" and "C" was successfully achieved. We hope that these findings can provide good application prospects for security pattern designs.

  4. Effects of Anisotropic Thermal Conductivity and Lorentz Force on the Flow and Heat Transfer of a Ferro-Nanofluid in a Magnetic Field

    Directory of Open Access Journals (Sweden)

    Yubai Li

    2017-07-01

    Full Text Available In this paper, we study the effects of the Lorentz force and the induced anisotropic thermal conductivity due to a magnetic field on the flow and the heat transfer of a ferro-nanofluid. The ferro-nanofluid is modeled as a single-phase fluid, where the viscosity depends on the concentration of nanoparticles; the thermal conductivity shows anisotropy due to the presence of the nanoparticles and the external magnetic field. The anisotropic thermal conductivity tensor, which depends on the angle of the applied magnetic field, is suggested considering the principle of material frame indifference according to Continuum Mechanics. We study two benchmark problems: the heat conduction between two concentric cylinders as well as the unsteady flow and heat transfer in a rectangular channel with three heated inner cylinders. The governing equations are made dimensionless, and the flow and the heat transfer characteristics of the ferro-nanofluid with different angles of the magnetic field, Hartmann number, Reynolds number and nanoparticles concentration are investigated systematically. The results indicate that the temperature field is strongly influenced by the anisotropic behavior of the nanofluids. In addition, the magnetic field may enhance or deteriorate the heat transfer performance (i.e., the time-spatially averaged Nusselt number in the rectangular channel depending on the situations.

  5. Simultaneous microwave-assisted synthesis, characterization, thermal stability, and antimicrobial activity of cellulose/AgCl nanocomposites

    International Nuclear Information System (INIS)

    Li, Shu-Ming; Fu, Lian-Hua; Ma, Ming-Guo; Zhu, Jie-Fang; Sun, Run-Cang; Xu, Feng

    2012-01-01

    By means of a simultaneous microwave-assisted method and a simple chemical reaction, cellulose/AgCl nanocomposites have been successfully synthesized using cellulose solution and AgNO 3 in N,N-dimethylacetamide (DMAc) solvent. The cellulose solution was firstly prepared by the dissolution of the microcrystalline cellulose and lithium chloride (LiCl) in DMAc. DMAc acts as both a solvent and a microwave absorber. LiCl was used as the reactant to fabricate AgCl crystals. The effects of the heating time and heating temperature on the products were studied. This method is based on the simultaneous formation of AgCl nanoparticles and precipitation of the cellulose, leading to a homogeneous distribution of AgCl nanoparticles in the cellulose matrix. The experimental results confirmed the formation of cellulose/AgCl nanocomposites with high-purity, good thermal stability and antimicrobial activity. This rapid, green and environmentally friendly microwave-assisted method opens a new window to the high value-added applications of biomass. -- Highlights: ► Cellulose/AgCl nanocomposites have been synthesized by microwave method. ► Effect of heating temperature on the nanocomposites was researched. ► Thermal stability of the nanocomposites was investigated. ► Cellulose/AgCl nanocomposites had good antimicrobial activity. ► This method is based on the simultaneous formation of AgCl and cellulose.

  6. Magnetic properties of nanocrystalline CoFe{sub 2}O{sub 4} synthesized by thermal plasma in large scale

    Energy Technology Data Exchange (ETDEWEB)

    Nawale, A.B.; Kanhe, N.S. [Department of Physics, University of Pune, Pune 411007 (India); Patil, K.R. [Center for Materials Characterizations, National Chemical Laboratory, Dr. Hommi Bhabha Road, Pashan, Pune 411008 (India); Reddy, V.R.; Gupta, A. [UGC-DAE Consortium for Scientific Research, Indore Centre, University Campus, Khandwa Road, Indore 452 017 (India); Kale, B.B. [Center for Materials for Electronics Technology, Department of Information Technology, Government of India, Panchawati, Off Pashan Road, Pune 411008 (India); Bhoraskar, S.V. [Department of Physics, University of Pune, Pune 411007 (India); Mathe, V.L., E-mail: vlmathe@physics.unipune.ac.in [Department of Physics, University of Pune, Pune 411007 (India); Das, A.K. [Laser and Plasma Technology Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085 (India)

    2012-12-14

    The paper reports the large scale synthesis of nanoparticles of CoFe{sub 2}O{sub 4} using thermal plasma reactor by gas phase condensation method. The yield of formation was found to be around 15 g h{sup -1}. The magnetic properties of CoFe{sub 2}O{sub 4}, synthesized at different reactor powers, were investigated in view of studying the effect of operating parameters of plasma reactor on the structural reorganization leading to the different cation distribution. The values of saturation magnetization, coercivity and remanent magnetization were found to be influenced by input power in thermal plasma. Although the increase in saturation magnetization was marginal (61 emu g{sup -1} to 70 emu g{sup -1}) with increasing plasma power; a significant increase in the coercivity (552 Oe to 849 Oe) and remanent magnetization (16 emu g{sup -1} to 26 emu g{sup -1}) were also noticed. The Moessbauer spectra showed mixed spinel structure and canted spin order for the as synthesized nanoparticles. The detailed analysis of cation distribution using the Moessbauer spectroscopy and X-ray photoelectron spectroscopy leads to the conclusion that the sample synthesized at an optimized power shows the different site selective states. -- Highlights: Black-Right-Pointing-Pointer A rapid synthesis method for synthesizing magnetic nanoparticles of cobalt ferrite. Black-Right-Pointing-Pointer The average particle size ranges between 25 and 40 nm; as revealed by the FESEM analysis. Black-Right-Pointing-Pointer Magnetic properties are influenced by different operating parameters.

  7. Manufacture and testing of the CTB&SBB thermal shield for the ITER magnet feeder system

    Energy Technology Data Exchange (ETDEWEB)

    Lu, Kun; Liu, Chen; Song, Yuntao; Feng, Hansheng; Ding, Kaizhong, E-mail: kzding@ipp.ac.cn; Wang, Tanbin; Ji, Hui

    2015-10-15

    The system of International Thermonuclear Experimental Reactor (ITER) feeders is responsible for the power, helium cooling, and instrumentation of the magnets of the coil terminal box and S-bend box (CTB&SBB) thermal shield outside the cryostat. An 80-K rectangular Al thermal shield is hung inside the CTB&SBB to reduce the thermal radiation heat loads of 4.5-K helium. The American Society of Interventional Pain Physicians (ASIPP) will supply all the 31 sets of feeders for ITER. A manufactured prototype of CTB&SBB thermal shield is first quality-tested before the commencement of the series production. First, a detailed configuration of the rectangular Al thermal shield is presented in this article. The paper also presents more information on the manufacturing process of the thermal shield, especially the welding process, the procedure for ensuring good weld quality, and the use of a specially designed tool to ensure <5-mm deformation on such a 7.3-m-long thermal shield during welding. In addition, the cold test and results, including the cooling process with 13-bar and 17.5-g/s 80-K He gas, and the temperature distribution on different panels of the thermal shield are presented. The whole process of manufacture and testing lays a good foundation for the series production of the thermal shield.

  8. Morphology and magnetic properties of CeCo5 submicron flakes prepared by surfactant-assisted high-energy ball milling

    Science.gov (United States)

    Zhang, J. J.; Gao, H. M.; Yan, Y.; Bai, X.; Su, F.; Wang, W. Q.; Du, X. B.

    2012-10-01

    CeCo5 permanent magnetic alloy has been processed by surfactant assisted high energy ball milling. Heptane and oleic acid were used as the solvent and surfactant, respectively. The amount of surfactant used was 50% by weight of the starting powder. The produced particles were deposited on a piece of copper (4 mm in length and width) under a magnetic field of 27 kOe applied along the copper surface and immobilized by ethyl α-cyanoacrylate. Scanning electron microscope pictures show that the particles are flakes, several μm in length and width and tens of nm in thickness. X-ray diffraction patterns and magnetic measurements prove that the flakes are crystalline with c-axes magnetic anisotropy. The easy magnetization axis is oriented perpendicular to the surface of the flake. A maximum coercivity of 3.3 kOe was obtained for the sample milled for 40 min.

  9. Effect of magnetic and thermal properties of iron oxide nanoparticles (IONs) in nitrile butadiene rubber (NBR) latex

    Science.gov (United States)

    Ong, Hun Tiar; Julkapli, Nurhidayatullaili Muhd; Hamid, Sharifah Bee Abd; Boondamnoen, O.; Tai, Mun Foong

    2015-12-01

    Nitrile butadiene rubber (NBR) gloves are one of the most important personal protective equipments but they are possible to tear off and contaminate food or pharmaceutical and healthcare products during manufacturing and packaging process. High tendency of torn glove remaining in food or products due to white or light flesh-coloured glove is not easy to be detected by naked eyes. In this paper, iron oxide nanoparticles (IONs) selected as additive for NBR to improve its detectability by mean of magnetic properties. IONs synthesized via precipitation method and compounded with NBR latex before casting on petri dish. The properties of IONs were investigated by X-ray Diffractometry (XRD), Transmission Electron Microscope (TEM), Raman Spectroscopy and Vibrating Sample Magnetometer (VSM). Meanwhile NBR/IONs composites were studied by Thermogravimetry Analysis (TGA), Differential Scanning Calorimetry (DSC) and Vibrating Sample Magnetometer (VSM). It observed that, synthesized IONs shows of 25.28 nm crystallite with 25.86 nm semipherical (changed as) shape. Meanwhile, Magnetite and maghemite phase are found in range of 670 cm-1 and 700 cm-1 respectively, which it contributes magnetization saturation of 73.96 emu/g at 10,000 G by VSM. Thermal stability and magnetic properties were increased with incorporating IONs into NBR latex up to 20 phr. NBR/IONs 5 phr has the optimum thermal stability, lowest glass transition temperature (-14.83 °C) and acceptable range of magnetization saturation (3.83 emu/g at 10,000 G) to form NBR gloves with magnetic detectability.

  10. Magnetic separation as a method to assist mineralogical characterization of rocks by X-ray diffraction

    International Nuclear Information System (INIS)

    Silva, Amanda Luzia da; Oliveira, Arno Heeren de; Fernandes, Maria Lourdes Souza

    2013-01-01

    The X-ray diffraction (XRD) corresponds to one of the main techniques for characterization of structures in crystalline materials widely used in the identification of minerals in samples of geological materials such as rocks. However, the large number of mineral phases present in a rock sample can generate excess peaks in the diffractogram, and it can promote overlapping peaks and induce erroneous identification. The purpose of this study was to perform magnetic separation of minerals from rock samples in order to enable the identification of the minerals by XRD. For this magnetic separation, two samples of rock were selected: a sample of high silica content and a sample with low silica content. The magnetic separation of minerals from each sample was performed using the magnetic separator isodynamic Frantz. Posteriorly, the fractions obtained in magnetic separations were analyzed by XRD. In the sample with high silica content, it was obtained a fraction where was identified the accessory mineral epidote, which had not been identified in the total sample diffractogram. In the sample with low silica content, the magnetic separation into several mineral fractions made possible to obtain diffraction patterns with fewer peaks and peaks with higher relative intensities, which allowed its mineralogical characterization. The results showed that the mineral separation by the magnetic separator Frantz made the identification of accessory minerals by XRD and the characterization of samples which have many mineral phases possible, which proves that magnetic separation by Frantz is a method which can assist analyses by XRD. (author)

  11. Magnetic separation as a method to assist mineralogical characterization of rocks by X-ray diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Amanda Luzia da; Oliveira, Arno Heeren de; Fernandes, Maria Lourdes Souza, E-mail: amanda@igc.ufmg.br, E-mail: heeren@nuclear.ufmg.br, E-mail: amanda@igc.ufmg.br, E-mail: lurdesfernandes@ufmg.br [Universidade Federal de Minas Gerais (UFMG), Belo Horionte, MG (Brazil)

    2013-07-01

    The X-ray diffraction (XRD) corresponds to one of the main techniques for characterization of structures in crystalline materials widely used in the identification of minerals in samples of geological materials such as rocks. However, the large number of mineral phases present in a rock sample can generate excess peaks in the diffractogram, and it can promote overlapping peaks and induce erroneous identification. The purpose of this study was to perform magnetic separation of minerals from rock samples in order to enable the identification of the minerals by XRD. For this magnetic separation, two samples of rock were selected: a sample of high silica content and a sample with low silica content. The magnetic separation of minerals from each sample was performed using the magnetic separator isodynamic Frantz. Posteriorly, the fractions obtained in magnetic separations were analyzed by XRD. In the sample with high silica content, it was obtained a fraction where was identified the accessory mineral epidote, which had not been identified in the total sample diffractogram. In the sample with low silica content, the magnetic separation into several mineral fractions made possible to obtain diffraction patterns with fewer peaks and peaks with higher relative intensities, which allowed its mineralogical characterization. The results showed that the mineral separation by the magnetic separator Frantz made the identification of accessory minerals by XRD and the characterization of samples which have many mineral phases possible, which proves that magnetic separation by Frantz is a method which can assist analyses by XRD. (author)

  12. [Microsurgery assisted by intraoperative magnetic resonance imaging and neuronavigation for small lesions in deep brain].

    Science.gov (United States)

    Song, Zhi-jun; Chen, Xiao-lei; Xu, Bai-nan; Sun, Zheng-hui; Sun, Guo-chen; Zhao, Yan; Wang, Fei; Wang, Yu-bo; Zhou, Ding-biao

    2012-01-03

    To explore the practicability of resecting small lesions in deep brain by intraoperative magnetic resonance imaging (iMRI) and neuronavigator-assisted microsurgery and its clinical efficacies. A total of 42 cases with small lesions in deep brain underwent intraoperative MRI and neuronavigator-assisted microsurgery. The drifting of neuronavigation was corrected by images acquired from intraoperative MR rescanning. All lesions were successfully identified and 40 cases totally removed without mortality. Only 3 cases developed new neurological deficits post-operatively while 2 of them returned to normal neurological functions after a follow-up duration of 3 months to 2 years. The application of intraoperative MRI can effectively correct the drifting of neuronavigation and enhance the accuracy of microsurgical neuronavigation for small lesions in deep brain.

  13. A novel permanently magnetised high gradient magnetic filter using assisted capture for fine particles

    Energy Technology Data Exchange (ETDEWEB)

    Watson, J.H.P. [Univ. of Southampton (United Kingdom)

    1995-02-01

    This paper describes the structure and properties of a novel permanently magnetised magnetic filter for fine friable radioactive material. Previously a filter was described and tested. This filter was designed so that the holes in the filter are left open as capture proceeds which means the pressure drop builds up only slowly. This filter is not suitable for friable composite particles which can be broken by mechanical forces. The structure of magnetic part of the second filter has been changed so as to strongly capture particles composed of fine particles weakly bound together which tend to break when captured. This uses a principle of assisted-capture in which coarse particles aid the capture of the fine fragments. The technique has the unfortunate consequence that the pressure drop across the filter rises faster as capture capture proceeds than the filter described previously. These filters have the following characteristics: (1) No external magnet is required. (2) No external power is required. (3) Small is size and portable. (4) Easily interchangeable. (5) Can be cleaned without demagnetising.

  14. Numerical analysis of magnetic field effects on hydro-thermal behavior of a magnetic nanofluid in a double pipe heat exchanger

    Energy Technology Data Exchange (ETDEWEB)

    Shakiba, Ali, E-mail: Shakiba7858@yahoo.com [Department of Mechanical Engineering, Mazandaran Institute of Technology, Babol (Iran, Islamic Republic of); Vahedi, Khodadad, E-mail: Khvahedi@ihu.ac.ir [Department of Mechanical Engineering, Imam Hossein University, Tehran (Iran, Islamic Republic of)

    2016-03-15

    This study attempts to numerically investigate the hydro-thermal characteristics of a ferrofluid (water and 4 vol% Fe{sub 3}O{sub 4}) in a counter-current horizontal double pipe heat exchanger, which is exposed to a non-uniform transverse magnetic field with different intensities. The magnetic field is generated by an electric current going through a wire located parallel to the inner tube and between two pipes. The single phase model and the control volume technique have been used to study the flow. The effects of magnetic field have been added to momentum equation by applying C++ codes in Ansys Fluent 14. The results show that applying this kind of magnetic field causes kelvin force to be produced perpendicular to the ferrofluid flow, changing axial velocity profile and creating a pair of vortices which leads to an increase in Nusselt number, friction factor and pressure drop. Comparing the enhancement percentage of Nusselt number, friction factor and pressure drop demonstrates that the optimum value of magnetic number for Re{sub ff}=50 is between Mn=1.33×10{sup 6} and Mn=2.37×10{sup 6}. So applying non-uniform transverse magnetic field can control the flow of ferrofluid and improve heat transfer process of double pipe heat exchanger. - Highlights: • Effect of applying non-uniform transverse magnetic field on a ferrofluid for enhancing the cooling process in a double pipe heat exchanger is investigated. • Heat exchanger is exposed to a non-uniform transverse magnetic field with different intensities. • The magnetic field is generated by an electric current going through a wire located parallel to inner tube and between two pipes. • Applying this field produces kelvin force to change axial velocity profile and creating a pair of vortices increasing Nusselt number, friction factor and pressure drop.

  15. The effect of electron thermal conduction on plasma pressure gradient during reconnection of magnetic field lines

    International Nuclear Information System (INIS)

    Chu, T.K.

    1987-12-01

    The interplay of electron cross-field thermal conduction and the reconnection of magnetic field lines around an m = 1 magnetic island prior to a sawtooth crash can generate a large pressure gradient in a boundary layer adjacent to the reconnecting surface, leading to an enhanced gradient of poloidal beta to satisfy the threshold condition for ideal MHD modes. This narrow boundary layer and the short onset time of a sawtooth crash can be supported by fine-grained turbulent processes in a tokamak plasma. 11 refs

  16. Comparison of the Effectiveness of Water-Based Extraction of Substances from Dry Tea Leaves with the Use of Magnetic Field Assisted Extraction Techniques

    Directory of Open Access Journals (Sweden)

    Grzegorz Zaguła

    2017-10-01

    Full Text Available This article presents the findings of a study investigating the feasibility of using a magnetic field assisted technique for the water-based extraction of mineral components, polyphenols, and caffeine from dry black and green tea leaves. The authors present a concept of applying constant and variable magnetic fields in the process of producing water-based infusions from selected types of tea. Analyses investigating the effectiveness of the proposed technique in comparison with conventional infusion methods assessed the contents of selected mineral components—i.e., Al, Ca, Cu, K, Mg, P, S, and Zn—which were examined with the use of ICP-OES. The contents of caffeine and polyphenolic compounds were assessed using the HPLC. A changing magnetic field permitted an increased effectiveness of extraction of the mineral components, caffeine, and polyphenols. The findings support the conclusion that a changing magnetic field assisted extraction method is useful for obtaining biologically valuable components from tea infusions.

  17. Magnetic suspension of the rotor of a ventricular assist device of mixed flow type.

    Science.gov (United States)

    Horikawa, Oswaldo; de Andrade, Aron José Pazin; da Silva, Isaías; Bock, Eduardo Guy Perpetuo

    2008-04-01

    This work presents results of preliminary studies concerning application of magnetic bearing in a ventricular assist device (VAD) being developed by Dante Pazzanese Institute of Cardiology-IDPC (São Paulo, Brazil). The VAD-IDPC has a novel architecture that distinguishes from other known VADs. In this, the rotor has a conical geometry with spiral impellers, showing characteristics that are intermediate between a centrifugal VAD and an axial VAD. The effectiveness of this new type of blood pumping principle was showed by tests and by using it in heart surgery for external blood circulation. However, the developed VAD uses a combination of ball bearings and mechanical seals, limiting the life for some 10 h, making impossible its long-term use or its use as an implantable VAD. As a part of development of an implantable VAD, this work aims at the replacement of ball bearings by a magnetic bearing. The most important magnetic bearing principles are studied and the magnetic bearing developed by Escola Politécnica of São Paulo University (EPUSP-MB) is elected because of its very simple architecture. Besides presenting the principle of the EPUSP-MB, this work presents one possible alternative for applying the EPUSP-MB in the IDPC-VAD.

  18. Magnet-assisted device-level alignment for the fabrication of membrane-sandwiched polydimethylsiloxane microfluidic devices

    International Nuclear Information System (INIS)

    Lu, J-C; Liao, W-H; Tung, Y-C

    2012-01-01

    Polydimethylsiloxane (PDMS) microfluidic device is one of the most essential techniques that advance microfluidics research in recent decades. PDMS is broadly exploited to construct microfluidic devices due to its unique and advantageous material properties. To realize more functionalities, PDMS microfluidic devices with multi-layer architectures, especially those with sandwiched membranes, have been developed for various applications. However, existing alignment methods for device fabrication are mainly based on manual observations, which are time consuming, inaccurate and inconsistent. This paper develops a magnet-assisted alignment method to enhance device-level alignment accuracy and precision without complicated fabrication processes. In the developed alignment method, magnets are embedded into PDMS layers at the corners of the device. The paired magnets are arranged in symmetric positions at each PDMS layer, and the magnetic attraction force automatically pulls the PDMS layers into the aligned position during assembly. This paper also applies the method to construct a practical microfluidic device, a tunable chaotic micromixer. The results demonstrate the successful operation of the device without failure, which suggests the accurate alignment and reliable bonding achieved by the method. Consequently, the fabrication method developed in this paper is promising to be exploited to construct various membrane-sandwiched PDMS microfluidic devices with more integrated functionalities to advance microfluidics research. (paper)

  19. Antifungal activity of magnetically separable Fe3O4/ZnO/AgBr nanocomposites prepared by a facile microwave-assisted method

    Directory of Open Access Journals (Sweden)

    Abolghasem Hoseinzadeh

    2016-08-01

    Full Text Available In the present work, magnetically separable Fe3O4/ZnO/AgBr nanocomposites with different weight ratios of Fe3O4 to ZnO/AgBr were prepared by a facile microwave-assisted method. The resultant samples were characterized by X-ray diffraction (XRD, scanning electron microscopy (SEM, transmission electron microscopy (TEM, energy dispersive analysis of X-rays (EDX, and vibrating sample magnetometery (VSM. Antifungal activity of the as-prepared samples was evaluated against Fusarium graminearum and Fusarium oxysporum as two phytopathogenic fungi. Among the nanocomposites, the sample with 1:8 weight ratio of Fe3O4 to ZnO/AgBr was selected as the best nanocomposite. This nanocomposite inactivates Fusarium graminearum and Fusarium oxysporum at 120 and 60 min, respectively. Moreover, it was observed that the microwave irradiation time has considerable influence on the antifungal activity and the sample prepared by irradiation for 10 min showed the best activity. Moreover, the nanocomposite without any thermal treatment displayed the superior activity.

  20. Mixing of nanosize particles by magnetically assisted impaction techniques

    Science.gov (United States)

    Scicolone, James V.

    approach based on use of small magnetic particles as mixing media is introduced that achieves a high-degree of mixing at scales of about a micron. The method is tested for binary mixture of alumina/silica and silica/titania. Various parameters such as processing time, size of the magnets, and magnetic particle to powder mixed ratio are considered. Experiments are carried out in batch containers in liquid and dry mediums, as well as a fluidized bed set-up. Homogeneity of Mixing (HoM), defined as the compliment of the Intensity of Segregation, was evaluated at the micron scale through field-emission scanning electron microscopy (FESEM) and the energy dispersive x-ray spectroscopy (EDS). Secondary electron images, along with elemental mappings, were used to visualize the change in agglomerate sizes. Compositional percent data of each element were obtained through an EDS spatial distribution point analysis and used to obtain quantitative analysis on the homogeneity of the mixture. The effect of magnet impaction on mixing quality was examined on the HoM of binary mixtures. The research shows that HoM improved with magnetically assisted impaction mixing techniques indicating that the HoM depends on the product of processing time with the number of magnets. In a fluidized bed set-up, MAIM not only improved dispersion, but it was also found that the magnetic particles served to break down the larger agglomerates, to reduce the minimum fluidization velocity, to delay the onset of bubbling, and to convert the fluidization behavior of ABF powder to APF. Thus MAIM techniques may be used to achieve mixing of nanopowders at a desired HoM through adjusting the number of magnets and processing time; and its inherent advantages are its simplicity, an environmentally benign operation, and reduced cost as compared with wet mixing techniques.

  1. Magnetic-field-assisted synthesis of Co{sub 3}O{sub 4} nanoneedles with superior electrochemical capacitance

    Energy Technology Data Exchange (ETDEWEB)

    Zhu, Tao; Xie, Yan; Zhang, Guoxiong; He, Zhenni; Lu, Yisheng; Guo, Haibo [Shanghai University, Department of Electronic Information Materials, School of Materials Science and Engineering (China); Lin, Chuan [GE Global Research, China Technology Center (China); Chen, Yigang, E-mail: yigangchen@shu.edu.cn [Shanghai University, Department of Electronic Information Materials, School of Materials Science and Engineering (China)

    2015-12-15

    Nanostructured Co{sub 3}O{sub 4} films have been deposited on nickel foam in a magnetic-field-assisted hydrothermal process followed by annealing in air. The magnetic field strength is varied to study its relationship with nanostructures, morphology, and electrochemical properties of the Co{sub 3}O{sub 4} electrodes. The Co{sub 3}O{sub 4} films synthesized in the weak magnetic fields consist of dispersed nanoneedles, which are different from clustered nanoneedles when the magnetic field is absent. Moreover, the magnetic fields (of several millitesla) induced substantial changes in the nanostructures and electrochemical properties of the Co{sub 3}O{sub 4} films. A possible formation mechanism of Co{sub 3}O{sub 4} nanoneedles is proposed by comparing the morphologies and nanostructures of the films synthesized with and without the magnetic fields. Among these electrodes, the optimal one has a high specific capacitance (970.8 F g{sup −1} at 0.5 A g{sup −1}), good power capability (847.5 F g{sup −1} at 6.0 A g{sup −1}), and an excellent retention ratio (93.7 % over 1000 cycles). All these impressive results demonstrate that magnetic fields may be an economic and effective tool in hydrothermal synthesis of Co{sub 3}O{sub 4} electrodes for high-performance supercapacitors.

  2. Fabrication of nano-sized magnetic tunnel junctions using lift-off process assisted by atomic force probe tip.

    Science.gov (United States)

    Jung, Ku Youl; Min, Byoung-Chul; Ahn, Chiyui; Choi, Gyung-Min; Shin, Il-Jae; Park, Seung-Young; Rhie, Kungwon; Shin, Kyung-Ho

    2013-09-01

    We present a fabrication method for nano-scale magnetic tunnel junctions (MTJs), employing e-beam lithography and lift-off process assisted by the probe tip of atomic force microscope (AFM). It is challenging to fabricate nano-sized MTJs on small substrates because it is difficult to use chemical mechanical planarization (CMP) process. The AFM-assisted lift-off process enables us to fabricate nano-sized MTJs on small substrates (12.5 mm x 12.5 mm) without CMP process. The e-beam patterning has been done using bi-layer resist, the poly methyl methacrylate (PMMA)/ hydrogen silsesquioxane (HSQ). The PMMA/HSQ resist patterns are used for both the etch mask for ion milling and the self-aligned mask for top contact formation after passivation. The self-aligned mask buried inside a passivation oxide layer, is readily lifted-off by the force exerted by the probe tip. The nano-MTJs (160 nm x 90 nm) fabricated by this method show clear current-induced magnetization switching with a reasonable TMR and critical switching current density.

  3. Energy dashboard for real-time evaluation of a heat pump assisted solar thermal system

    Science.gov (United States)

    Lotz, David Allen

    The emergence of net-zero energy buildings, buildings that generate at least as much energy as they consume, has lead to greater use of renewable energy sources such as solar thermal energy. One example is a heat pump assisted solar thermal system, which uses solar thermal collectors with an electrical heat pump backup to supply space heating and domestic hot water. The complexity of such a system can be somewhat problematic for monitoring and maintaining a high level of performance. Therefore, an energy dashboard was developed to provide comprehensive and user friendly performance metrics for a solar heat pump system. Once developed, the energy dashboard was tested over a two-week period in order to determine the functionality of the dashboard program as well as the performance of the heating system itself. The results showed the importance of a user friendly display and how each metric could be used to better maintain and evaluate an energy system. In particular, Energy Factor (EF), which is the ratio of output energy (collected energy) to input energy (consumed energy), was a key metric for summarizing the performance of the heating system. Furthermore, the average EF of the solar heat pump system was 2.29, indicating an efficiency significantly higher than traditional electrical heating systems.

  4. Thermal and structural performance of a single tube support post for the Superconducting Super Collider dipole magnet cryostat

    International Nuclear Information System (INIS)

    Boroski, W.N.; Nicol, T.H.; Ruschman, M.K.; Schoo, C.J.

    1993-07-01

    The reentrant support post currently incorporated in the Superconducting Super Collider (SSC) dipole cryostat has been shown to meet the structural and thermal requirements of the cryostat, both in prototype magnet assemblies and through component testing. However, the reentrant post design has two major drawbacks: tight dimensional control on all components, and cost driven by these tolerance constraints and a complex assembly procedure. A single tube support post has been developed as an alternative to the reentrant post design. Several prototype assemblies have been fabricated and subjected to structural testing. Compressive, tensile, and bending forces were applied to each assembly with deflection measured at several locations. A prototype support post has also been thermally evaluated in a heat leak measurement facility. Heat load to 4.2 K was measured with the intermediate post intercept operating at various temperatures while thermometers positioned along the conductive path of the post mapped thermal gradients. Results from these measurements indicate the single tube support post meets the design criteria for the SSC dipole magnet cryostat support system

  5. Thermal evolution of nanocrystalline co-sputtered Ni–Zr alloy films: Structural, magnetic and MD simulation studies

    International Nuclear Information System (INIS)

    Bhattacharya, Debarati; Rao, T.V. Chandrasekhar; Bhushan, K.G.; Ali, Kawsar; Debnath, A.; Singh, S.; Arya, A.; Bhattacharya, S.; Basu, S.

    2015-01-01

    Monophasic and homogeneous Ni 10 Zr 7 nanocrystalline alloy films were successfully grown at room temperature by co-sputtering in an indigenously developed three-gun DC/RF magnetron sputtering unit. The films could be produced with long-range crystallographic and chemical order in the alloy, thus overcoming the widely acknowledged inherent proclivity of the glass forming Ni–Zr couple towards amorphization. Crystallinity of these alloys is a desirable feature with regard to improved efficacy in applications such as hydrogen storage, catalytic activity and nuclear reactor engineering, to name a few. Thermal stability of this crystalline phase, being vital for transition to viable applications, was investigated through systematic annealing of the alloy films at 473 K, 673 K and 923 K for various durations. While the films were stable at 473 K, the effect of annealing at 673 K was to create segregation into nanocrystalline Ni (superparamagnetic) and amorphous Ni + Zr (non-magnetic) phases. Detailed analyses of the physical and magnetic structures before and after annealing were performed through several techniques effectual in analyzing stratified configurations and the findings were all consistent with each other. Polarized neutron and X-ray reflectometry, grazing incidence x-ray diffraction, time-of-flight secondary ion mass spectroscopy and X-ray photoelectron spectroscopy were used to gauge phase separation at nanometer length scales. SQUID based magnetometry was used to investigate macroscopic magnetic properties. Simulated annealing performed on this system using molecular dynamic calculations corroborated well with the experimental results. This study provides a thorough understanding of the creation and thermal evolution of a crystalline Ni–Zr alloy. - Highlights: • Nanocrystalline Ni 10 Zr 7 alloy thin films deposited successfully by co-sputtering. • Creation of a crystalline alloy in a binary system with a tendency to amorphize. • Quantitative

  6. Thermal evolution of nanocrystalline co-sputtered Ni–Zr alloy films: Structural, magnetic and MD simulation studies

    Energy Technology Data Exchange (ETDEWEB)

    Bhattacharya, Debarati, E-mail: debarati@barc.gov.in [Solid State Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Rao, T.V. Chandrasekhar; Bhushan, K.G. [Technical Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Ali, Kawsar [Material Science Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Debnath, A. [Technical Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Singh, S. [Solid State Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Arya, A. [Material Science Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Bhattacharya, S. [Technical Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Basu, S. [Solid State Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India)

    2015-11-15

    Monophasic and homogeneous Ni{sub 10}Zr{sub 7} nanocrystalline alloy films were successfully grown at room temperature by co-sputtering in an indigenously developed three-gun DC/RF magnetron sputtering unit. The films could be produced with long-range crystallographic and chemical order in the alloy, thus overcoming the widely acknowledged inherent proclivity of the glass forming Ni–Zr couple towards amorphization. Crystallinity of these alloys is a desirable feature with regard to improved efficacy in applications such as hydrogen storage, catalytic activity and nuclear reactor engineering, to name a few. Thermal stability of this crystalline phase, being vital for transition to viable applications, was investigated through systematic annealing of the alloy films at 473 K, 673 K and 923 K for various durations. While the films were stable at 473 K, the effect of annealing at 673 K was to create segregation into nanocrystalline Ni (superparamagnetic) and amorphous Ni + Zr (non-magnetic) phases. Detailed analyses of the physical and magnetic structures before and after annealing were performed through several techniques effectual in analyzing stratified configurations and the findings were all consistent with each other. Polarized neutron and X-ray reflectometry, grazing incidence x-ray diffraction, time-of-flight secondary ion mass spectroscopy and X-ray photoelectron spectroscopy were used to gauge phase separation at nanometer length scales. SQUID based magnetometry was used to investigate macroscopic magnetic properties. Simulated annealing performed on this system using molecular dynamic calculations corroborated well with the experimental results. This study provides a thorough understanding of the creation and thermal evolution of a crystalline Ni–Zr alloy. - Highlights: • Nanocrystalline Ni{sub 10}Zr{sub 7} alloy thin films deposited successfully by co-sputtering. • Creation of a crystalline alloy in a binary system with a tendency to amorphize.

  7. Tunnel magnetoresistance in thermally robust Mo/CoFeB/MgO tunnel junction with perpendicular magnetic anisotropy

    Directory of Open Access Journals (Sweden)

    B. Fang

    2015-06-01

    Full Text Available We report on tunnel magnetoresistance and electric-field effect in the Mo buffered and capped CoFeB/MgO magnetic tunnel junctions (MTJs with perpendicular magnetic anisotropy. A large tunnel magnetoresistance of 120% is achieved. Furthermore, this structure shows greatly improved thermal stability and stronger electric-field-induced modulation effect in comparison with the Ta/CoFeB/MgO-based MTJs. These results suggest that the Mo-based MTJs are more desirable for next generation spintronic devices.

  8. Preparation and characterization of magnetic carboxylated nanodiamonds for vortex-assisted magnetic solid-phase extraction of ziram in food and water samples.

    Science.gov (United States)

    Yılmaz, Erkan; Soylak, Mustafa

    2016-09-01

    A simple and rapid vortex-assisted magnetic solid phase extraction (VA-MSPE) method for the separation and preconcentration of ziram (zinc dimethyldithiocarbamate), subsequent detection of the zinc in complex structure of ziram by flame atomic absorption spectrometry (AAS) has been developed. The ziram content was calculated by using stoichiometric relationship between the zinc and ziram. Magnetic carboxylated nanodiamonds (MCNDs) as solid-phase extraction adsorbent was prepared and characterized by Fourier transform infrared (FT-IR) spectra, X-ray diffraction (XRD) spectrometry and scanning electron microscopy (SEM). These magnetic carboxylated nanodiamonds carrying the ziram could be easily separated from the aqueous solution by applying an external magnetic field; no filtration or centrifugation was necessary. Some important factors influencing the extraction efficiency of ziram such as pH of sample solution, amount of adsorbent, type and volume of eluent, extraction and desorption time and sample volume were studied and optimized. The total extraction and detection time was lower than 10min The preconcentration factor (PF), the precision (RSD, n=7), the limit of detection (LOD) and limit of quantification (LOQ) were 160, 7.0%, 5.3µgL(-1) and 17.5µgL(-1), respectively. The interference of various ions has been examined and the method has been applied for the determination of ziram in various waters, foodstuffs samples and synthetic mixtures. Copyright © 2016 Elsevier B.V. All rights reserved.

  9. Thermally assisted acoustofluidic separation of extracellular vesicles from cells

    Science.gov (United States)

    Mirtaheri, Elnaz; Dolatmoradi, Ata; Pimentel, Krystine; Bhansali, Shekhar; El-Zahab, Bilal

    2018-02-01

    Extracellular vesicles (EVs) have been gaining increasing attention given their role in communicating information between cells. Composition-based isolation of EVs is particularly of high significance as the proteomic and lipidomic characterization of their cargo could provide valuable clues to the role of EVs in mediating the biology of various conditions. This has, however, proved to be challenging as EVs, despite their abundance, are very small and difficult to be differentiated from the other constituents of host media. In addition, currently available methods like ultracentrifugation and filtration are cumbersome and capable of achieving mostly size-based separations. In this work, we demonstrate the possibility of separating submicron EV-like vesicles from cancer cells using a thermally-assisted acoustophoretic device. In a system composed of MCF-7 breast cancer cells spiked with two different types of same-size vesicles, composition-based isolation of vesicles was shown to be realizable through opposite focusing of the system's components at the node and antinodes of the overlaid ultrasonic standing wave. By proper choice of temperature in the microchannel, we were able to achieve separations with purities exceeding 93%. Furthermore, cells recovered from the channel were shown to be viable after the separation.

  10. Magnetization Switching of a Co /Pt Multilayered Perpendicular Nanomagnet Assisted by a Microwave Field with Time-Varying Frequency

    Science.gov (United States)

    Suto, Hirofumi; Kanao, Taro; Nagasawa, Tazumi; Mizushima, Koichi; Sato, Rie

    2018-05-01

    Microwave-assisted magnetization switching (MAS) is attracting attention as a method for reversing nanomagnets with a high magnetic anisotropy by using a small-amplitude magnetic field. We experimentally study MAS of a perpendicularly magnetized nanomagnet by applying a microwave magnetic field with a time-varying frequency. Because the microwave field frequency can follow the nonlinear decrease of the resonance frequency, larger magnetization excitation than that in a constant-frequency microwave field is induced, which enhances the MAS effect. The switching field decreases almost linearly as the start value of the time-varying microwave field frequency increases, and it becomes smaller than the minimum switching field in a constant-frequency microwave field. To obtain this enhancement of the MAS effect, the end value of the time-varying microwave field frequency needs to be almost the same as or lower than the critical frequency for MAS in a constant-frequency microwave field. In addition, the frequency change typically needs to take 1 ns or longer to make the rate of change slow enough for the magnetization to follow the frequency change. This switching behavior is qualitatively explained by the theory based on the macrospin model.

  11. The effects of magnetic perturbations on plasma transport or is magnetic turbulence important in tokamaks?

    International Nuclear Information System (INIS)

    Wootton, A.J.

    1993-01-01

    A test particle model is verified and then used to interpret estimates of fast electron diffusivities in terms of magnetic fluctuation levels. The implied fluctuation levels are themselves interpreted with another verified model to predict electron thermal diffusivities. If the fast electron diffusivities represent local values, then the implied associated thermal transport is too small to explain experimental values. That is, magnetic fluctuations are not important. However, if the fast electron diffusivities represent effective values across mixed good (i.e. with no magnetic fluctuations) and bad (with magnetic fluctuations) surfaces then the implied magnetic fluctuation levels can influence electron thermal transport. (author)

  12. Thermal expansion studies on low-dimensional frustrated quantum magnets. The case of κ-(BEDT-TTF)2Cu2(CN)3 and azurite

    International Nuclear Information System (INIS)

    Manna, Rudra Sekhar

    2012-01-01

    Thermal expansion measurements provide a sensitive tool for exploring a material's thermodynamic properties in condensed matter physics as they provide useful information on the electronic, magnetic and lattice properties of a material. In this thesis, thermal expansion measurements have been carried out both at ambient-pressure and under hydrostatic pressure conditions. From the materials point of view, the spin-liquid candidate κ-(BEDT-TTF) 2 Cu 2 (CN) 3 has been studied extensively as a function of temperature and magnetic field. Azurite, Cu 3 (CO 3 ) 2 (OH) 2 - a realization of a one-dimensional distorted Heisenberg chain is also studied both at ambient and hydrostatic pressure to demonstrate the proper functioning of the newly built setup ''thermal expansion under pressure''.

  13. Optomagnetic Detection of MicroRNA Based on Duplex-Specific Nuclease-Assisted Target Recycling and Multilayer Core-Satellite Magnetic Superstructures

    DEFF Research Database (Denmark)

    Tian, Bo; Ma, Jing; Qiu, Zhen

    2017-01-01

    -efficiency, and potential for bioresponsive multiplexing. Herein, we demonstrate a sensitive and rapid miRNA detection method based on optomagnetic read-out, duplex-specific nuclease (DSN)-assisted target recycling, and the use of multilayer core-satellite magnetic superstructures. Triggered by the presence of target mi...

  14. Voltage induced magnetostrictive switching of nanomagnets: Strain assisted strain transfer torque random access memory

    International Nuclear Information System (INIS)

    Khan, Asif; Nikonov, Dmitri E.; Manipatruni, Sasikanth; Ghani, Tahir; Young, Ian A.

    2014-01-01

    A spintronic device, called the “strain assisted spin transfer torque (STT) random access memory (RAM),” is proposed by combining the magnetostriction effect and the spin transfer torque effect which can result in a dramatic improvement in the energy dissipation relative to a conventional STT-RAM. Magnetization switching in the device which is a piezoelectric-ferromagnetic heterostructure via the combined magnetostriction and STT effect is simulated by solving the Landau-Lifshitz-Gilbert equation incorporating the influence of thermal noise. The simulations show that, in such a device, each of these two mechanisms (magnetostriction and spin transfer torque) provides in a 90° rotation of the magnetization leading a deterministic 180° switching with a critical current significantly smaller than that required for spin torque alone. Such a scheme is an attractive option for writing magnetic RAM cells.

  15. Voltage induced magnetostrictive switching of nanomagnets: Strain assisted strain transfer torque random access memory

    Science.gov (United States)

    Khan, Asif; Nikonov, Dmitri E.; Manipatruni, Sasikanth; Ghani, Tahir; Young, Ian A.

    2014-06-01

    A spintronic device, called the "strain assisted spin transfer torque (STT) random access memory (RAM)," is proposed by combining the magnetostriction effect and the spin transfer torque effect which can result in a dramatic improvement in the energy dissipation relative to a conventional STT-RAM. Magnetization switching in the device which is a piezoelectric-ferromagnetic heterostructure via the combined magnetostriction and STT effect is simulated by solving the Landau-Lifshitz-Gilbert equation incorporating the influence of thermal noise. The simulations show that, in such a device, each of these two mechanisms (magnetostriction and spin transfer torque) provides in a 90° rotation of the magnetization leading a deterministic 180° switching with a critical current significantly smaller than that required for spin torque alone. Such a scheme is an attractive option for writing magnetic RAM cells.

  16. Alkyl side chain on the 1-methylimidazolium ring of countercation modulating thermal and magnetic properties of metal-dithiolene complexes

    Science.gov (United States)

    Duan, Hai-Bao; Yu, Shan-Shan; Cai, Ying; Zhang, Hui

    2015-05-01

    Two low-dimensional ion-pair compounds [1,5-bis(1-methylimidazolium)pentane][Ni(mnt)2]2 (1) and [1,9-bis(1-methylimidazolium)nonane][Ni(mnt)2]2 (2) (mnt2- = maleonitriledithiolate) were designed and synthesized. The cations and anions formed mixed column along the crystallographic a-axis direction in the crystal of 1·0.5DMF. Two compounds display different thermal and magnetic behaviors. Multi-step solid to solid state phase transition was observed for 1 by DSC. 1 exhibits weak paramagnetism over the temperature range of 2-400 K and 2 shows spin gap in the low-temperature phase. Thus by changing of the alky chain length of the counter-cation allows the modulation thermal and magnetic behaviors for such system.

  17. The effect of CuAl addition on the magnetic property, thermal stability and corrosion resistance of the sintered NdFeB magnets

    Science.gov (United States)

    Liu, Y. L.; Liang, J.; He, Y. Ch.; Li, Y. F.; Wang, G. F.; Ma, Q.; Liu, F.; Zhang, Y.; Zhang, X. F.

    2018-05-01

    To improve the coercivity of the Nd-Fe-B sintered magnets, the Cu29.8Al70.2 (at.%) powders with low melting point were introduced into the Nd-Fe-B magnets. The magnetic properties, microstructure, thermal stability and corrosion behavior of the sintered magnets with different amount of Cu29.8Al70.2 (0,0.25,0.50,0.75,1.0 wt.%) were investigated. When the amount of doped Cu29.8Al70.2 was less than 0.75 wt.%, the coercivity was improved, especially that of the magnets with 0.25 wt.% Cu29.8Al70.2, markedly increased to 13.97 kOe from 12.67 kOe (without CuAl). The improvement of magnetic properties could be attributed to enhanced wettability between Nd2Fe14B phase and Nd-rich phase and decreased exchange coupling between grains, which depended on the optimization of grain boundary microstructure and their distribution by codoping Cu and Al. With the addition of 0-1.0 wt.% Cu29.8Al70.2 powders, the reversible temperature coefficients of remanence and coercivity of the magnets could be also improved. The corrosion resistances was also found to be improved through small addition of Cu29.8Al70.2 powder in 3.5 wt.% NaCl solution by electrochemical and immersion tests, which could be due to the enhancement of the Nd-rich intergranular phase by addition Cu29.8Al70.2.

  18. Nano-organocatalyst: magnetically retrievable ferrite-anchored glutathione for microwave-assisted Paal–Knorr reaction, aza-Michael addition, and pyrazole synthesis

    KAUST Repository

    Polshettiwar, Vivek; Varma, Rajender S.

    2010-01-01

    Postsynthetic Surface modification of magnetic nanoparticles by glutathione imparts desirable chemical functionality and enables the generation of catalytic sites on the surfaces of ensuing organocatalysts. In this article, we discuss the developments, unique activity, and high selectivity of nano-organocatalysts for microwave-assisted Paal-Knorr reaction, aza-Michael addition, and pyrazole synthesis. Their insoluble character Coupled with paramagnetic nature enables easy separation of these nano-catalysts from the reaction mixture using external magnet, which eliminates the requirement of catalyst filtration. Published by Elsevier Ltd.

  19. Influence of aging time of oleate precursor on the magnetic relaxation of cobalt ferrite nanoparticles synthesized by the thermal decomposition method

    International Nuclear Information System (INIS)

    Herrera, Adriana P.; Polo-Corrales, Liliana; Chavez, Ermides; Cabarcas-Bolivar, Jari; Uwakweh, Oswald N.C.; Rinaldi, Carlos

    2013-01-01

    Cobalt ferrite nanoparticles are of interest because of their room temperature coercivity and high magnetic anisotropy constant, which make them attractive in applications such as sensors based on the Brownian relaxation mechanism and probes to determine the mechanical properties of complex fluids at the nanoscale. These nanoparticles can be synthesized with a narrow size distribution by the thermal decomposition of an iron–cobalt oleate precursor in a high boiling point solvent. We studied the influence of aging time of the iron–cobalt oleate precursor on the structure, chemical composition, size, and magnetic relaxation of cobalt ferrite nanoparticles synthesized by the thermal decomposition method. The structure and thermal behavior of the iron–cobalt oleate was studied during the aging process. Infrared spectra indicated a shift in the coordination state of the oleate and iron/cobalt ions from bidentate to bridging coordination. Aging seemed to influence the thermal decomposition of the iron–cobalt oleate as determined from thermogravimmetric analysis and differential scanning calorimetry, where shifts in the temperatures corresponding to decomposition events and a narrowing of the endotherms associated with these events were observed. Aging promoted formation of the spinel crystal structure, as determined from X-ray diffraction, and influenced the nanoparticle magnetic properties, resulting in an increase in blocking temperature and magnetocrystalline anisotropy. Mossbauer spectra also indicated changes in the magnetic properties resulting from aging of the precursor oleate. Although all samples exhibited some degree of Brownian relaxation, as determined from complex susceptibility measurements in a liquid medium, aging of the iron–cobalt oleate precursor resulted in crossing of the in-phase χ′and out-of-phase χ″ components of the complex susceptibility at the frequency of the Brownian magnetic relaxation peak, as expected for nanoparticles

  20. Thermal stability of octadecylsilane hybrid silicas prepared by grafting and sol-gel methods

    International Nuclear Information System (INIS)

    Brambilla, Rodrigo; Santos, Joao H.Z. dos; Miranda, Marcia S.L.; Frost, Ray L.

    2008-01-01

    Hybrid silicas bearing octadecylsilane groups were prepared by grafting and sol-gel (SG) methods. The effect of the preparative route on the thermal stability was evaluated by means of thermal gravimetric analysis (TGA), infrared emission spectroscopy (IRES) and, complementary, by 13 C solid-state nuclear magnetic resonance ( 13 C NMR) and matrix assisted laser deionization time of flight mass spectroscopy (MALDI-TOF-MS). Silicas prepared by the grafting route seem to be slightly more stable than those produced by the sol-gel method. This behavior seems to be associated to the preparative route, since grafting affords a liquid-like conformation, while in the case of sol-gel a highly organized crystalline chain conformation was observed

  1. Microwave-assisted hydrothermal synthesis of coralloid nanostructured nickel hydroxide hydrate and thermal conversion to nickel oxide

    International Nuclear Information System (INIS)

    Lai, Teh-Long; Lai, Yuan-Lung; Yu, Jen-Wei; Shu, Youn-Yuen; Wang, Chen-Bin

    2009-01-01

    Coralloid nanostructured nickel hydroxide hydrate has been successfully synthesized by a simple microwave-assisted hydrothermal process using nickel sulfate hexahydrate as precursor and urea as hydrolysis-controlling agent. A pure coralloid nanostructured nickel oxide can be obtained from the nickel hydroxide hydrate after calcination at 400 deg. C. The thermal property, structure and morphology of samples were characterized by thermogravimetry (TG), temperature-programmed reduction (TPR), X-ray (XRD), infrared spectroscopy (IR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).

  2. Microwave-assisted hydrothermal synthesis of coralloid nanostructured nickel hydroxide hydrate and thermal conversion to nickel oxide

    Energy Technology Data Exchange (ETDEWEB)

    Lai, Teh-Long [Environmental Analysis Laboratory, Department of Chemistry, National Kaohsiung Normal University, Kaohsiung 802, Taiwan (China); Lai, Yuan-Lung [Department of Mechanical and Automation Engineering, Da-Yeh University, Changhua 515, Taiwan (China); Yu, Jen-Wei [Environmental Analysis Laboratory, Department of Chemistry, National Kaohsiung Normal University, Kaohsiung 802, Taiwan (China); Shu, Youn-Yuen, E-mail: shuyy@nknucc.nknu.edu.tw [Environmental Analysis Laboratory, Department of Chemistry, National Kaohsiung Normal University, Kaohsiung 802, Taiwan (China); Wang, Chen-Bin, E-mail: chenbin@ccit.edu.tw [Department of Applied Chemistry and Materials Science, Chung Cheng Institute of Technology, National Defense University, Tahsi, Taoyuan 335, Taiwan (China)

    2009-10-15

    Coralloid nanostructured nickel hydroxide hydrate has been successfully synthesized by a simple microwave-assisted hydrothermal process using nickel sulfate hexahydrate as precursor and urea as hydrolysis-controlling agent. A pure coralloid nanostructured nickel oxide can be obtained from the nickel hydroxide hydrate after calcination at 400 deg. C. The thermal property, structure and morphology of samples were characterized by thermogravimetry (TG), temperature-programmed reduction (TPR), X-ray (XRD), infrared spectroscopy (IR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).

  3. Thermal aspects of a superconducting coil for fusion reactor

    International Nuclear Information System (INIS)

    Yeh, H.T.

    1975-01-01

    Computer models are used to simulate both localized and extensive thermal excursions in a large superconducting magnet for fusion reactor. Conditions for the failure of fusion magnet due to thermal excursion are delineated. Designs to protect the magnet against such thermal excursion are evaluated

  4. Recent results on the giant magnetoresistance in magnetic multilayers (anisotropy, thermal variation and CCP-GMR)

    Science.gov (United States)

    Dieny, B.; Granovsky, A.; Vedyaev, A.; Ryzhanova, N.; Cowache, C.; Pereira, L. G.

    1995-12-01

    We present some recent results obtained on the electrical transport properties in magnetic multilayers. Three points are addressed. The first one is an experimental demonstration of the existence of an intrinsic anisotropy of the giant magnetoresistance (GMR). The experiments have been carried out on spin-valve samples for which there is no contribution of the usual anisotropic magnetoresistance to the observed magnetoresistance. The GMR amplitude is found to be larger (lower) in the direction perpendicular (parallel) to the sensing current. The second point concerns a quantitative analysis of the thermal variation of the CIP (current-in-plane) GMR in magnetic multilayers. This analysis is based on a semi-classical theory including the spin-intermixing due to spin-flip scattering by magnons. This approach allows quantitatively evaluation of the respective weights of the various contributions to the thermal decrease in GMR: (i) scattering by magnons in the bulk of the ferromagnetic layers; (ii) phonon scattering in the non-magnetic spacer layer; and (iii) interfacial scattering by paramagnetic interfacial layers which may form as the temperature is increased. The third point is a theoretical investigation of the CPP (current perpendicular to the plane) electrical transport through an interface between two semi-infinite metallic materials. It is shown that when a potential step U exists at such an interface, this step gives rise to an interfacial resistance proportional to U2. It also leads to the existence of large oscillations in the electric fields on both sides of the interface.

  5. Analysis of environmental effect of hybrid solar-assisted desalination cycle in Sirdarya Thermal Power Plant, Uzbekistan

    International Nuclear Information System (INIS)

    Alikulov, Khusniddin; Xuan, Tran Dang; Higashi, Osamu; Nakagoshi, Nobukazu; Aminov, Zarif

    2017-01-01

    Highlights: • A hybrid solar-assisted desalination cycle was designed and stimulated. • Maximum of 21,064.00 kW effective solar heat can be achieved. • The use of parabolic-trough collectors in the Multi Effect Distillation is potential. • The cycle can be applied in other regions with high Direct Normal Irradiation. - Abstract: This study was to investigate possible reduction of fossil fuel consumption and carbon dioxide emission in one of energy sectors of Sirdarya Thermal Power Plant (TPP), Uzbekistan. A hybrid solar-assisted desalination cycle has been designed and simulated for partially supplying saturated steam with 200 °C, 8 bar, and 32 t/h parameters to a Multi Effect Distillation (MED) process in the Sirdarya Thermal Power Plant. The outcome of the parental design model stated that maximum, 21,064.00 kW effective solar heat can be achieved, which is equivalent to 31.76 t/h of saturated steam with 200 °C and 8 bar parameters. Total saved fossil fuel in each month proved that it is possible to reduce fossil fuel (heavy oil and natural gas) consumption with 59.64, 95.24, 389.96, and 298.26 tons during available Direct Normal Irradiation (DNI) by using parabolic-trough collectors. Moreover, the above-mentioned fossil fuel savings accounted for CO_2 reduction with amounts of 182.50, 255.46, 1045.87 & 799.96 tons per each consistent month. Findings proved that integration of parabolic-trough collectors into the MED process is feasible in terms of high DNI availability and demand for retrofitting old existing heat-consuming facilities in Sirdarya Thermal Power Plant. Besides, the cycle also can be applied in other regions of Uzbekistan with high DNI for generating solar heat. Therefore, conducted study is eligible to be applied on the research site by taking into account of sufficient meteorological data and required steam parameters.

  6. Structural, magnetic and magneto-transport properties of thermally evaporated Fe/Cu multilayers

    Energy Technology Data Exchange (ETDEWEB)

    Bouziane, K.; Al-Busaidi, M.; Gismelseed, A.; Al-Rawas, A. [Physics Department, College of Science, Sultan Qabos University, P. O. Box 36, Postal Code 123, Al-Khodh, Muscat (Oman)

    2004-05-01

    Structural, magnetic and magneto-transport properties of thermally evaporated Fe/Cu multilayers (MLs) have been investigated. Although multilayered structure has been successfully obtained, a substantial interfacial roughness ranging from 0.6 nm to 1.2 nm has been determined. All Fe/Cu MLs were polycrystalline with an average grain size of about 10 nm. Fe was bcc and textured (110) whereas Cu was fcc(111). Transmission electron microscopy analysis showed that the fcc Cu layer was rather textured (110) and (100) at least in the first stage of growth of the Fe/Cu MLs. Conversion electron Moessbauer (CEMS) measurements indicated the existence of three phases. Two of them were magnetic with a dominant bcc Fe phase, followed by fcc Fe phase. The third phase was superparamagnetic. The CEMS results were explained in terms of the partial diffusion of Fe into Cu with three different zones. The small magnetoresistance (MR<0.2%) was correlated to Fe clusters located at Fe-Cu interfaces. (Abstract Copyright [2004], Wiley Periodicals, Inc.)

  7. Preparation of magnetic Ni@graphene nanocomposites and efficient removal organic dye under assistance of ultrasound

    International Nuclear Information System (INIS)

    Zhao, Chuang; Guo, Jianhui; Yang, Qing; Tong, Lei; Zhang, Jingwei; Zhang, Jiwei; Gong, Chunhong; Zhou, Jingfang; Zhang, Zhijun

    2015-01-01

    Graphical abstract: Reduced graphene oxide/Ni microspheres, being prepared under ultrasound conditions, exhibit a better removal efficiency to decolorize RhB with ultrasonic-assisted decolorization process. - Highlights: • One-step synthesis of Ni@graphene microspheres under ultrasound conditions. • During the ultrasonic process, graphene oxide was reduced and Ni nanoparticles were formed and anchored on graphene sheets. • The products exhibit excellent performance for fast and efficient removal of dye contaminants. • The nanocomposites can be easily separated from solution by a magnet. - Abstract: In this article, we report a facile one-step synthesis of Ni@graphene nanocomposite microspheres (NGs) in hydrazine hydrate solution under ultrasound conditions. During the ultrasonic process, graphene oxide (GO) was reduced effectively under mild conditions and Ni nanoparticles were simultaneously formed and anchored on graphene sheets, which act as spacers to keep the neighboring sheets separated. The target products exhibit excellent performance for fast and efficient removal of dye contaminants, rhodamine B (RhB) in aqueous solution, under assistance of ultrasound. Finally, the nanocomposites can be easily separated from solution by a magnet. Furthermore, higher content of graphene can be produced under sonication, which facilitates faster and more efficient removal of organic contaminates in the solution. The nanocomposites were also characterized by scanning electron microscopy, Raman spectroscopy, Fourier transformed infrared spectroscopy, X-ray photoelectron spectroscopy, X-ray powder diffraction and thermogravimetric analysis.

  8. Preparation of magnetic Ni@graphene nanocomposites and efficient removal organic dye under assistance of ultrasound

    Energy Technology Data Exchange (ETDEWEB)

    Zhao, Chuang; Guo, Jianhui; Yang, Qing; Tong, Lei [Key Laboratory of Ministry of Education for Special Functional Materials, Henan University, Kaifeng 475004 (China); Zhang, Jingwei, E-mail: jwzhang@henu.edu.cn [Key Laboratory of Ministry of Education for Special Functional Materials, Henan University, Kaifeng 475004 (China); Ian Wark Research Institute, University of South Australia, Mawson Lakes, SA 5095 (Australia); Zhang, Jiwei [Key Laboratory of Ministry of Education for Special Functional Materials, Henan University, Kaifeng 475004 (China); Gong, Chunhong [College of Chemistry and Chemical Engineering, Henan University, Kaifeng 475004 (China); Ian Wark Research Institute, University of South Australia, Mawson Lakes, SA 5095 (Australia); Zhou, Jingfang, E-mail: jingfang.zhou@unisa.edu.au [Ian Wark Research Institute, University of South Australia, Mawson Lakes, SA 5095 (Australia); Zhang, Zhijun [Key Laboratory of Ministry of Education for Special Functional Materials, Henan University, Kaifeng 475004 (China)

    2015-12-01

    Graphical abstract: Reduced graphene oxide/Ni microspheres, being prepared under ultrasound conditions, exhibit a better removal efficiency to decolorize RhB with ultrasonic-assisted decolorization process. - Highlights: • One-step synthesis of Ni@graphene microspheres under ultrasound conditions. • During the ultrasonic process, graphene oxide was reduced and Ni nanoparticles were formed and anchored on graphene sheets. • The products exhibit excellent performance for fast and efficient removal of dye contaminants. • The nanocomposites can be easily separated from solution by a magnet. - Abstract: In this article, we report a facile one-step synthesis of Ni@graphene nanocomposite microspheres (NGs) in hydrazine hydrate solution under ultrasound conditions. During the ultrasonic process, graphene oxide (GO) was reduced effectively under mild conditions and Ni nanoparticles were simultaneously formed and anchored on graphene sheets, which act as spacers to keep the neighboring sheets separated. The target products exhibit excellent performance for fast and efficient removal of dye contaminants, rhodamine B (RhB) in aqueous solution, under assistance of ultrasound. Finally, the nanocomposites can be easily separated from solution by a magnet. Furthermore, higher content of graphene can be produced under sonication, which facilitates faster and more efficient removal of organic contaminates in the solution. The nanocomposites were also characterized by scanning electron microscopy, Raman spectroscopy, Fourier transformed infrared spectroscopy, X-ray photoelectron spectroscopy, X-ray powder diffraction and thermogravimetric analysis.

  9. A stochastic model for magnetic dynamics in single-molecule magnets

    Energy Technology Data Exchange (ETDEWEB)

    López-Ruiz, R., E-mail: rlruiz@ifi.unicamp.br [Instituto de Física Gleb Wataghin - Universidade Estadual de Campinas, 13083-859 Campinas (SP) (Brazil); Almeida, P.T. [Instituto de Física Gleb Wataghin - Universidade Estadual de Campinas, 13083-859 Campinas (SP) (Brazil); Vaz, M.G.F. [Instituto de Química, Universidade Federal Fluminense, 24020-150 Niterói (RJ) (Brazil); Novak, M.A. [Instituto de Física - Universidade Federal do Rio de Janeiro, 21941-972 Rio de Janeiro (RJ) (Brazil); Béron, F.; Pirota, K.R. [Instituto de Física Gleb Wataghin - Universidade Estadual de Campinas, 13083-859 Campinas (SP) (Brazil)

    2016-04-01

    Hysteresis and magnetic relaxation curves were performed on double well potential systems with quantum tunneling possibility via stochastic simulations. Simulation results are compared with experimental ones using the Mn{sub 12} single-molecule magnet, allowing us to introduce time dependence in the model. Despite being a simple simulation model, it adequately reproduces the phenomenology of a thermally activated quantum tunneling and can be extended to other systems with different parameters. Assuming competition between the reversal modes, thermal (over) and tunneling (across) the anisotropy barrier, a separation of classical and quantum contributions to relaxation time can be obtained. - Highlights: • Single-molecule magnets are modeled using a simple stochastic approach. • Simulation reproduces thermally-activated tunnelling magnetization reversal features. • The time is introduced in hysteresis and relaxation simulations. • We can separate the quantum and classical contributions to decay time.

  10. Evaluation of thermal stress in the anode chamber wall of a large volume magnetic bucket ion source

    International Nuclear Information System (INIS)

    Wells, Russell; Horiike, Hiroshi; Kuriyama, Masaaki; Ohara, Yoshihiro

    1984-02-01

    Thermal stress analysis was performed on the plasma chamber of the Large Volume Magnetic Multipole Bucket Ion Source (LVB) designed for use on the JT-60 NBI system. The energy absorbed by the walls of the plasma chambers of neutral beam injectors is of the order of 1% of the accelerator electrical drain power. A previous study indicates that a moderately high heat flux, of about 600W/cm 2 , is concentrated on the magnetic field cusp lines during normal full power operation. Abnormal arc discharges during conditioning of a stainless steel LVB produced localized melting of the stainless steel at several locations near the cusps lines. The power contained in abnormal arc discharges (arc spots) was estimated from the observed melting. Thermal stress analysis was performed numerically on representative sections of the copper LVB design for both stable and abnormal arc discharge conditions. Results show that this chamber should not fail due to thermal fatigue stesses arising from normal arc discharges. However, fatigue failure may occur after several hundred to a few thousand arc spots of 30mS duration at any one location. Limited arc discharge operation of the copper bucket was performed to partially verify the chamber's durability. (author)

  11. Single crystal magnetic, dielectric and thermal studies of the relaxor ferroelectric Pb(Fe2/3W1/3)O3

    International Nuclear Information System (INIS)

    Ye, Z.G.; Sato, M.; Kita, E.; Bursill, L.A.; Schmid, H.

    1998-01-01

    The magnetic, dielectric and thermal properties of the complex perovskite Pb(Fe 2/3 W 1/3 )O 3 [PFW] have been studied on single crystals by means of a SQUID magnetometer, dielectric measurements and thermal analysis. Anomalies in the temperature dependence of the magnetization have revealed magnetic phase transitions at T N1 =350 K and T N2 =20 K. These two steps of antiferromagnetic ordering are attributed to the microstructural feature of the complex perovskite, characterized by ordered and disordered arrangements on the B-site, giving rise to a strong superexchange interaction of - Fe 3 + - O - Fe 3+ - type with a higher ordering temperature, and to a weak superexchange interaction of the B-site ordered elpasolite type - Fe 3+ + - O - W - O - Fe 3+ - with a lower Neel temperature. The low temperature antiferromagnetic phase exhibits a weak ferromagnetism. The dielectric properties of PFW show a relaxor ferroelectric behaviour with a dispersive maximum of permittivity at Tm (170 -190 K). The magnetic phase transition at T N2 =20 K results in anomalies both of the real part of permittivity and the dissipation factor, suggesting a magneto-electric coupling via magneto-structural interactions

  12. Building automation: Photovoltaic assisted thermal comfort management system for energy saving

    International Nuclear Information System (INIS)

    Khan, M Reyasudin Basir; Jidin, Razali; Shaaya, Sharifah Azwa; Pasupuleti, Jagadeesh

    2013-01-01

    Building automation plays an important key role in the means to reduce building energy consumption and to provide comfort for building occupants. It is often that air conditioning system operating features ignored in building automation which can result in thermal discomfort among building occupants. Most automation system for building is expensive and incurs high maintenance cost. Such system also does not support electricity demand side management system such as load shifting. This paper discusses on centralized monitoring system for room temperature and photovoltaic (PV) output for feasibility study of PV assisted air conditioning system in small office buildings. The architecture of the system consists of PV modules and sensor nodes located at each room. Wireless sensor network technology (WSN) been used for data transmission. The data from temperature sensors and PV modules transmitted to the host personal computer (PC) wirelessly using Zigbee modules. Microcontroller based USB data acquisition device used to receive data from sensor nodes and displays the data on PC.

  13. Building automation: Photovoltaic assisted thermal comfort management system for energy saving

    Science.gov (United States)

    Reyasudin Basir Khan, M.; Jidin, Razali; Pasupuleti, Jagadeesh; Azwa Shaaya, Sharifah

    2013-06-01

    Building automation plays an important key role in the means to reduce building energy consumption and to provide comfort for building occupants. It is often that air conditioning system operating features ignored in building automation which can result in thermal discomfort among building occupants. Most automation system for building is expensive and incurs high maintenance cost. Such system also does not support electricity demand side management system such as load shifting. This paper discusses on centralized monitoring system for room temperature and photovoltaic (PV) output for feasibility study of PV assisted air conditioning system in small office buildings. The architecture of the system consists of PV modules and sensor nodes located at each room. Wireless sensor network technology (WSN) been used for data transmission. The data from temperature sensors and PV modules transmitted to the host personal computer (PC) wirelessly using Zigbee modules. Microcontroller based USB data acquisition device used to receive data from sensor nodes and displays the data on PC.

  14. THERMAL EVOLUTION AND LIFETIME OF INTRINSIC MAGNETIC FIELDS OF SUPER-EARTHS IN HABITABLE ZONES

    International Nuclear Information System (INIS)

    Tachinami, C.; Ida, S.; Senshu, H.

    2011-01-01

    We have numerically studied the thermal evolution of different-mass terrestrial planets in habitable zones, focusing on the duration of dynamo activity to generate their intrinsic magnetic fields, which may be one of the key factors in habitability of the planets. In particular, we are concerned with super-Earths, observations of which are rapidly developing. We calculated the evolution of temperature distributions in the planetary interior using Vinet equations of state, the Arrhenius-type formula for mantle viscosity, and the astrophysical mixing-length theory for convective heat transfer modified for mantle convection. After calibrating the model with terrestrial planets in the solar system, we apply it for 0.1-10 M + rocky planets with a surface temperature of 300 K (in habitable zones) and Earth-like compositions. With the criterion of heat flux at the core-mantle boundary (CMB), the lifetime of the magnetic fields is evaluated from the calculated thermal evolution. We found that the lifetime slowly increases with planetary mass (M p ), independent of the initial temperature gap at the CMB (ΔT CMB ), but beyond the critical value M c,p (∼O(1) M + ) it abruptly declines from the mantle viscosity enhancement due to the pressure effect. We derived M c,p as a function of ΔT CMB and a rheological parameter (activation volume, V*). Thus, the magnetic field lifetime of super-Earths with M p >M p,c sensitively depends on ΔT CMB , which reflects planetary accretion, and V*, which has uncertainty at very high pressure. More advanced high-pressure experiments and first-principle simulation, as well as planetary accretion simulation, are needed to discuss the habitability of super-Earths.

  15. Reinforced carbon fiber laminates with oriented carbon nanotube epoxy nanocomposites: Magnetic field assisted alignment and cryogenic temperature mechanical properties.

    Science.gov (United States)

    He, Yuxin; Yang, Song; Liu, Hu; Shao, Qian; Chen, Qiuyu; Lu, Chang; Jiang, Yuanli; Liu, Chuntai; Guo, Zhanhu

    2018-05-01

    The epoxy nanocomposites with ordered multi-walled carbon nanotubes (MWCNTs) were used to influence the micro-cracks resistance of carbon fiber reinforced epoxy (CF/EP) laminate at 77 K, Oxidized MWCNTs functionalized with Fe 3 O 4 (Fe 3 O 4 /O-MWCNTs) with good magnetic properties were prepared by co-precipitation method and used to modify epoxy (EP) for cryogenic applications. Fe 3 O 4 /O-MWCNTs reinforced carbon fiber epoxy composites were also prepared through vacuum-assisted resin transfer molding (VARTM). The ordered Fe 3 O 4 /O-MWCNTs were observed to have effectively improved the mechanical properties of epoxy (EP) matrix at 77 K and reduce the coefficient of thermal expansion (CTE) of EP matrix. The ordered Fe 3 O 4 /O-MWCNTs also obviously improved the micro-cracks resistance of CF/EP composites at 77 K. Compared to neat EP, the CTE of ordered Fe 3 O 4 /O-MWCNTs modified CF/EP composites was decreased 37.6%. Compared to CF/EP composites, the micro-cracks density of ordered Fe 3 O 4 /O-MWCNTs modified CF/EP composites at 77 K was decreased 37.2%. Copyright © 2018 Elsevier Inc. All rights reserved.

  16. Impact of radius and skew angle on areal density in heat assisted magnetic recording hard disk drives

    Science.gov (United States)

    Cordle, Michael; Rea, Chris; Jury, Jason; Rausch, Tim; Hardie, Cal; Gage, Edward; Victora, R. H.

    2018-05-01

    This study aims to investigate the impact that factors such as skew, radius, and transition curvature have on areal density capability in heat-assisted magnetic recording hard disk drives. We explore a "ballistic seek" approach for capturing in-situ scan line images of the magnetization footprint on the recording media, and extract parametric results of recording characteristics such as transition curvature. We take full advantage of the significantly improved cycle time to apply a statistical treatment to relatively large samples of experimental curvature data to evaluate measurement capability. Quantitative analysis of factors that impact transition curvature reveals an asymmetry in the curvature profile that is strongly correlated to skew angle. Another less obvious skew-related effect is an overall decrease in curvature as skew angle increases. Using conventional perpendicular magnetic recording as the reference case, we characterize areal density capability as a function of recording position.

  17. Potential use of SERS-assisted theranostic strategy based on Fe{sub 3}O{sub 4}/Au cluster/shell nanocomposites for bio-detection, MRI, and magnetic hyperthermia

    Energy Technology Data Exchange (ETDEWEB)

    Han, Yu; Lei, Sheng-lan [Department of Biomaterials, College of Materials, Xiamen University, Xiamen 361005 (China); Lu, Jian-hua [Department of Electronic Science, College of Physical Science and Technology, Fujian Provincial Key Laboratory of Plasma and Magnetic Resonance Research, Xiamen University, Xiamen 361005 (China); He, Yuan [Department of Biomaterials, College of Materials, Xiamen University, Xiamen 361005 (China); Chen, Zhi-wei, E-mail: chenzhiwei@xmu.edu.cn [Department of Electronic Science, College of Physical Science and Technology, Fujian Provincial Key Laboratory of Plasma and Magnetic Resonance Research, Xiamen University, Xiamen 361005 (China); Ren, Lei, E-mail: renlei@xmu.edu.cn [Department of Biomaterials, College of Materials, Xiamen University, Xiamen 361005 (China); State Key Laboratory for Physical Chemistry of Solid Surfaces, Xiamen University, Xiamen 361005 (China); Fujian Collaborative Innovation Center for Exploitation and Utilization of Marine Biological Resources, Xiamen 361005 (China); Zhou, Xi [Department of Biomaterials, College of Materials, Xiamen University, Xiamen 361005 (China); Fujian Provincial Key Laboratory of Fire Retardant Materials, Xiamen University, Xiamen 361005 (China); Fujian Collaborative Innovation Center for Exploitation and Utilization of Marine Biological Resources, Xiamen 361005 (China)

    2016-07-01

    A surface-enhanced Raman scattering (SERS)-assisted theranostic strategy was designed based on a synthesized multifunctional Fe{sub 3}O{sub 4}/Au cluster/shell nanocomposite. This theranostic strategy was used for free prostate specific antigen (free-PSA) detection, magnetic resonance imaging (MRI), and magnetic hyperthermia. The lowest protein concentration detected was 1 ng mL{sup −1}, and the limit of detection (LOD) of the calculated PSA was 0.75 ng mL{sup −1}. Then, MRI was carried out to visualize the tumor cell. Lastly, magnetic hyperthermia was employed and revealed a favorable killing effect for the tumor cells. Thus, this SERS-assisted strategy based on a Fe{sub 3}O{sub 4}/Au cluster/shell nanocomposite showed great advantages in theranostic treatment. - Graphical abstract: Fe{sub 3}O{sub 4}/Au cluster/shell composite can be used for specific protein detection, magnetic resonance imaging and magnetic hyperthermia therapy. - Highlights: • We designed a SERS-assisted theranostic strategy based on the mutifunctional nanocomposites using gold shelled Fe{sub 3}O{sub 4} clusters. • Fe{sub 3}O{sub 4}/Au nanoparticles with theranostics and SERS for early diagnosis of PSA were reported for the first time. • The LOD of detection for PSA was lowed as 0.75 ng mL{sup −1}, and the total detection time was shorten to less than 1 h. • Fe{sub 3}O{sub 4} clusters had spin-spin (T{sub 2}) contrast enhancement and increased magnetic response. • Gold nanoshells supplied excellent chemical stability, biocompatibility, better heating property for magnetic hyperthermia.

  18. Thermally assisted sensor for conformity assessment of biodiesel production

    International Nuclear Information System (INIS)

    Kawano, M S; Kamikawachi, R C; Fabris, J L; Muller, M

    2015-01-01

    Although biodiesel can be intentionally tampered with, impairing its quality, ineffective production processes may also result in a nonconforming final fuel. For an incomplete transesterification reaction, traces of alcohol (ethanol or methanol) or remaining raw material (vegetable oil or animal fats) may be harmful to consumers, the environment or to engines. Traditional methods for biodiesel assessment are complex, time consuming and expensive, leading to the need for the development of new and more versatile processes for quality control. This work describes a refractometric fibre optic based sensor that is thermally assisted, developed to quantify the remaining methanol or vegetable oil in biodiesel blends. The sensing relies on a long period grating to configure an in-fibre interferometer. A complete analytical routine is demonstrated for the sensor allowing the evaluation of the biodiesel blends without segregation of the components. The results show the sensor can determine the presence of oil or methanol in biodiesel with a concentration ranging from 0% to 10% v/v. The sensor presented a resolution and standard combined uncertainty of 0.013% v/v and 0.62% v/v for biodiesel–oil samples, and 0.007% v/v and 0.22% v/v for biodiesel–methanol samples, respectively. (paper)

  19. Thermally assisted sensor for conformity assessment of biodiesel production

    Science.gov (United States)

    Kawano, M. S.; Kamikawachi, R. C.; Fabris, J. L.; Muller, M.

    2015-02-01

    Although biodiesel can be intentionally tampered with, impairing its quality, ineffective production processes may also result in a nonconforming final fuel. For an incomplete transesterification reaction, traces of alcohol (ethanol or methanol) or remaining raw material (vegetable oil or animal fats) may be harmful to consumers, the environment or to engines. Traditional methods for biodiesel assessment are complex, time consuming and expensive, leading to the need for the development of new and more versatile processes for quality control. This work describes a refractometric fibre optic based sensor that is thermally assisted, developed to quantify the remaining methanol or vegetable oil in biodiesel blends. The sensing relies on a long period grating to configure an in-fibre interferometer. A complete analytical routine is demonstrated for the sensor allowing the evaluation of the biodiesel blends without segregation of the components. The results show the sensor can determine the presence of oil or methanol in biodiesel with a concentration ranging from 0% to 10% v/v. The sensor presented a resolution and standard combined uncertainty of 0.013% v/v and 0.62% v/v for biodiesel-oil samples, and 0.007% v/v and 0.22% v/v for biodiesel-methanol samples, respectively.

  20. Magnetic Reversal and Thermal Stability of CoFeB Perpendicular Magnetic Tunnel Junction Arrays Patterned by Block Copolymer Lithography

    KAUST Repository

    Tu, Kun-Hua

    2018-04-10

    Dense arrays of pillars, with diameters of 64 and 25 nm, were made from a perpendicular CoFeB magnetic tunnel junction thin film stack using block copolymer lithography. While the soft layer and hard layer in the 64 nm pillars reverse at different fields, the reversal of the two layers in the 25 nm pillars could not be distinguished, attributed to the strong interlayer magnetostatic coupling. First order reversal curves were used to identify the steps that occur during switching, and the thermal stability and effective switching volume were determined from scan rate dependent hysteresis measurements.

  1. Dual-stage trapped-flux magnet cryostat for measurements at high magnetic fields

    Science.gov (United States)

    Islam, Zahirul; Das, Ritesh K.; Weinstein, Roy

    2015-04-14

    A method and a dual-stage trapped-flux magnet cryostat apparatus are provided for implementing enhanced measurements at high magnetic fields. The dual-stage trapped-flux magnet cryostat system includes a trapped-flux magnet (TFM). A sample, for example, a single crystal, is adjustably positioned proximate to the surface of the TFM, using a translation stage such that the distance between the sample and the surface is selectively adjusted. A cryostat is provided with a first separate thermal stage provided for cooling the TFM and with a second separate thermal stage provided for cooling sample.

  2. High field superconducting magnets

    Science.gov (United States)

    Hait, Thomas P. (Inventor); Shirron, Peter J. (Inventor)

    2011-01-01

    A superconducting magnet includes an insulating layer disposed about the surface of a mandrel; a superconducting wire wound in adjacent turns about the mandrel to form the superconducting magnet, wherein the superconducting wire is in thermal communication with the mandrel, and the superconducting magnet has a field-to-current ratio equal to or greater than 1.1 Tesla per Ampere; a thermally conductive potting material configured to fill interstices between the adjacent turns, wherein the thermally conductive potting material and the superconducting wire provide a path for dissipation of heat; and a voltage limiting device disposed across each end of the superconducting wire, wherein the voltage limiting device is configured to prevent a voltage excursion across the superconducting wire during quench of the superconducting magnet.

  3. US-LHC Magnet Database and conventions

    CERN Document Server

    Wei, J; Jain, A; Peggs, S; Pilat, F; Bottura, L; Sabbi, G L; MacKay, W W

    1999-01-01

    The US-LHC Magnet Database is designed for production-magnet quality assurance, field and alignment error impact analysis, cryostat assembly assistance, and ring installation assistance. The database consists of tables designed to store magnet field and alignment measurements data and quench data. This information will also be essential for future machine operations including local IR corrections. (7 refs).

  4. US-LHC Magnet Database and Conventions

    International Nuclear Information System (INIS)

    Wei, J.; McChesney, D.; Jain, A.; Peggs, S.; Pilat, F.; Bottura, L.; Sabbi, G.

    1999-01-01

    The US-LHC Magnet Database is designed for production-magnet quality assurance, field and alignment error impact analysis, cryostat assembly assistance, and ring installation assistance. The database consists of tables designed to store magnet field and alignment measurements data and quench data. This information will also be essential for future machine operations including local IR corrections

  5. Feeble magnetic fields generated by thermal charge fluctuations in extended metallic conductors: Implications for electric-dipole moment experiments

    International Nuclear Information System (INIS)

    Lamoreaux, S.K.

    1999-01-01

    A simple formulation for calculating the magnetic field external to an extended nonpermeable conducting body due to thermal current fluctuations within the body is developed, and is applied to a recent experimental search for the atomic electric-dipole moment (EDM) of 199 Hg. It is shown that the thermal fluctuation field is only slightly smaller in magnitude than other noise sources in that experiment. The formulation is extended to permeable bodies, and the implications for general EDM experiments are discussed. copyright 1999 The American Physical Society

  6. Iron oxide nanoparticle layer templated by polydopamine spheres: a novel scaffold toward hollow-mesoporous magnetic nanoreactors.

    Science.gov (United States)

    Huang, Liang; Ao, Lijiao; Xie, Xiaobin; Gao, Guanhui; Foda, Mohamed F; Su, Wu

    2015-01-14

    Superparamagnetic iron oxide nanoparticle layers with high packing density and controlled thickness were in situ deposited on metal-affinity organic templates (polydopamine spheres), via one-pot thermal decomposition. The as synthesized hybrid structure served as a facile nano-scaffold toward hollow-mesoporous magnetic carriers, through surfactant-assisted silica encapsulation and its subsequent calcination. Confined but accessible gold nanoparticles were successfully incorporated into these carriers to form a recyclable catalyst, showing quick magnetic response and a large surface area (642.5 m(2) g(-1)). Current nano-reactors exhibit excellent catalytic performance and high stability in reduction of 4-nitrophenol, together with convenient magnetic separability and good reusability. The integration of compact iron oxide nanoparticle layers with programmable polydopamine templates paves the way to fabricate magnetic-response hollow structures, with high permeability and multi-functionality.

  7. Influence of deuterium on the magnetic susceptibility and thermal expansion of the mixed valence compound CePd3

    International Nuclear Information System (INIS)

    Weinzierl, P.; Blaschko, O.; Fratzl, P.; Krexner, G.; Ernst, G.; Hilscher, G.

    1984-01-01

    The possibility of studying mixed valent rare earth compounds by addition of interstitially solved hydrogen is discussed. First measurements of the thermal expansion and of the magnetic susceptibility of 4 K in intermediate valent CePd 3 Dsub(0.05) are presented. (orig.) [de

  8. Effect of ballooning modes on thermal transport and magnetic field diffusion in the solar corona

    International Nuclear Information System (INIS)

    Strauss, H.R.

    1989-01-01

    Presently favored mechanisms of coronal heating: current sheet dissipation and Alfven wave resonant heating: deposit heat in thin layers. Classical thermal conduction cannot explain how heat is transported across the magnetic field. If heating occurs in thin layers, large pressure gradients can be created, which can give rise to ballooning modes. These instabilities are caused by the pressure gradient and the curvature of the magnetic field, and are stabilized by magnetic tension. The modes are broad band in wavelength and should produce turbulence. A mixing length expression for the turbulent heat transport shows that it is more than adequate to rapidly convect heat into much broader layers. Furthermore, the turbulent resistivity implies that heating occurs over most of the width of these broadened layers. The broadening also implies that much shorter time scales are required for heating. The β values in the corona suggest that 1--10 turbulent layers are formed in typical loop or arch structures. copyright American Geophysical Union 1989

  9. Magneto-thermal-acoustic differential-frequency imaging of magnetic nanoparticle with magnetic spatial localization: a theoretical prediction

    Science.gov (United States)

    Piao, Daqing

    2017-02-01

    The magneto-thermo-acoustic effect that we predicted in 2013 refers to the generation of acoustic-pressure wave from magnetic nanoparticle (MNP) when thermally mediated under an alternating magnetic field (AMF) at a pulsed or frequency-chirped application. Several independent experimental studies have since validated magneto-thermoacoustic effect, and a latest report has discovered acoustic-wave generation from MNP at the second-harmonic frequency of the AMF when operating continuously. We propose that applying two AMFs with differing frequencies to MNP will produce acoustic-pressure wave at the summation and difference of the two frequencies, in addition to the two second-harmonic frequencies. Analysis of the specific absorption dynamics of the MNP when exposed to two AMFs of differing frequencies has shown some interesting patterns of acoustic-intensity at the multiple frequency components. The ratio of the acoustic-intensity at the summation-frequency over that of the difference-frequency is determined by the frequency-ratio of the two AMFs, but remains independent of the AMF strengths. The ratio of the acoustic-intensity at the summation- or difference-frequency over that at each of the two second-harmonic frequencies is determined by both the frequency-ratio and the field-strength-ratio of the two AMFs. The results indicate a potential strategy for localization of the source of a continuous-wave magneto-thermalacoustic signal by examining the frequency spectrum of full-field non-differentiating acoustic detection, with the field-strength ratio changed continuously at a fixed frequency-ratio. The practicalities and challenges of this magnetic spatial localization approach for magneto-thermo-acoustic imaging using a simple envisioned set of two AMFs arranged in parallel to each other are discussed.

  10. Improved (0 0 1)-texture of FePt-C for heat-assisted magnetic recording media by insertion of Cr buffer layer

    Energy Technology Data Exchange (ETDEWEB)

    Shiroyama, T.; Wang, J.; Felicia, A.; Takahashi, Y.K.; Hono, K., E-mail: kazuhiro.hono@nims.go.jp

    2017-06-15

    Highlights: • Improvement of (0 0 1)-texture of prototype FePt-C granular films for heat heat assisted magnetic recording media. • Insertion of Cr buffer layer improves the crystallographic textures of the MgO underlayers, thereby reduces in-plane component in the FePt-C recording layer. • The growth in the grain size of the MgO underlayer as well as the (0 0 1)-texture of the MgO underlayer are the key factor in reducing the in-plane component in the FePt-C recording layer. - Abstract: FePt-C granular films deposited on MgO underlayers are the prototype media for heat-assisted magnetic recording. To reduce the in-plane magnetic component in the FePt-C media, we investigated the effect of Cr buffer layers on the crystallographic textures of the MgO underlayers and the resultant magnetic properties of the FePt-C layers. By growing a MgO underlayer on a Cr buffer layer, the (0 0 1) texture of the MgO underlayer is improved, on which the in-plane component of a FePt-C film is substantially reduced. We conclude that the growth in the grain size of the MgO underlayer is the key factor in reducing the in-plane component in the FePt-C recording layer.

  11. Morphologic, magnetic, and Moessbauer spectral properties of Fe75Co25 nanoparticles prepared by ultrasound-assisted electrochemistry

    International Nuclear Information System (INIS)

    Mancier, Valerie; Delplancke, J.-L.; Delwiche, Jacques; Hubin-Franskin, M.-J.; Piquer, Cristina; Rebbouh, Leila; Grandjean, Fernande

    2004-01-01

    Nanopowders of Fe 75 Co 25 alloys have been prepared by ultrasound-assisted electrochemistry. Their composition, crystallographic structure, morphology, have been studied by X-ray diffraction, transmission electron microscopy, X-ray fluorescence, and high-energy electron diffraction. The nanopowders are found to present a composition well determined by the electrolyte bath composition, they show a bcc structure. The iron and cobalt atoms exhibit a very homogeneous distribution in the particles. The magnetic properties of the nanopowders have been measured between 5 and 295 K with a vibrating sample magnetometer and their Moessbauer spectra have been obtained at 295 K. The saturation magnetization is characteristic of FeCo alloys. The magnetic behavior and transmission electron microscopy observations of the particles indicate strongly interacting particles with a radius of ca. 2-4 nm, particles which may form agglomerates of larger size. The measured average hyperfine field is situated at the maximum of the Slater-Pauling curve for the FeCo alloys

  12. MAGNETIC AND HYPERFINE CHARACTERIZATION OF THE THERMAL TRANSFORMATION CuO - Fe2O3 TO Fe3O4

    Directory of Open Access Journals (Sweden)

    Juan D. Betancur

    2018-01-01

    Full Text Available A magnetic study about the thermal transformation of hematite doped with CuO (Fe2O3 + CuO is presented. The heat treatment was carried out at a temperature of 375 ± 1 ºC, in a controlled atmosphere composed by 20% hydrogen and 80% nitrogen. Samples were characterized by Mössbauer spectroscopy at room temperature, magnetization as a function of temperature and hysteresis loops at 10K. Our results suggest that both the hyperfine fields and linewidths of the A and B sites remain essentially constant with increasing the CuO concentration, while at the same time a paramagnetic component arises, which is indicative of the appearance of a precipitate or a new phase of Fe-Cu, i.e. there is not an effective incorporation of the copper into the structure of the magnetite. The saturation magnetization falls from approximately 87 emu/g to 78 emu/g, consistent with such a paramagnetic phase. Also, an increase in the coercivity from ~576 Oe up to ~621 Oe by increasing the percentage of CuO from 2% up to 20% is observed. Such increase is also attributed to the paramagnetic phase acting as pinning center for domain walls, besides also de pinning effect due to vacancies induced by the thermal treatment. Finally, an inversion of the magnetization in the Verwey temperature is observed. The data suggest that by means of the synthesis method employed, it is possible to obtain Fe3O4 magnetite particles coexisting with precipitates of Fe-Cu, giving rise to a modification in the magnetic properties and generatingan interesting effect in the magnetization at the Verwey temperature.

  13. Transcranial magnetic stimulation assisted by neuronavigation of magnetic resonance images

    Science.gov (United States)

    Viesca, N. Angeline; Alcauter, S. Sarael; Barrios, A. Fernando; González, O. Jorge J.; Márquez, F. Jorge A.

    2012-10-01

    Technological advance has improved the way scientists and doctors can learn about the brain and treat different disorders. A non-invasive method used for this is Transcranial Magnetic Stimulation (TMS) based on neuron excitation by electromagnetic induction. Combining this method with functional Magnetic Resonance Images (fMRI), it is intended to improve the localization technique of cortical brain structures by designing an extracranial localization system, based on Alcauter et al. work.

  14. INFLUENCE OF TECHNOLOGICAL MODES OF MAGNETIC-ELECTRIC GRINDING ON MICROSTRUCTURE OF GAS-THERMAL SPRAYED NI–CR–B–SI-COATINGS

    Directory of Open Access Journals (Sweden)

    N. V. Spiridonov

    2009-01-01

    Full Text Available Influence of technological modes of magnetic-electric grinding on structural changes in a surface layer of gas-thermal sprayed coatings is investigated in the paper. The paper presents optimum modes of  coating roughing and finishing processes.

  15. The role of MFM signal in mark size measurement in probe-based magnetic recording on CoNi/Pt multilayers

    International Nuclear Information System (INIS)

    Zhang Li; Bain, James A.; Zhu Jiangang; Abelmann, Leon; Onoue, Takahiro

    2007-01-01

    A method of heat-assisted magnetic recording (HAMR) potentially suitable for probe-based storage systems is characterized. Magnetic marks were formed by a scanning tunneling microscopy (STM)-based thermal magnetic mechanism on a perpendicular CoNi/Pt multilayered film. Magnetic force microscopy (MFM) was applied to display those marks. The MFM signal is dependent of the lift-height during MFM scanning: smaller lift-height leads to higher resolution of the MFM image and a double-peak signal line, while higher lift-height leads to lower resolution and a single-peak signal line. Theoretical calculation of the magnetic field from the mark was executed. It agrees well with experiments, and demonstrates the method of mark size measurement in perpendicular media: full-width half-maximum (FWHM) of the measured MFM signal

  16. Non-thermal gamma-ray emission from delayed pair breakdown in a magnetized and photon-rich outflow

    Energy Technology Data Exchange (ETDEWEB)

    Gill, Ramandeep; Thompson, Christopher, E-mail: rgill@cita.utoronto.ca [Canadian Institute for Theoretical Astrophysics, 60 St. George Street, Toronto, ON M5S 3H8 (Canada)

    2014-12-01

    We consider delayed, volumetric heating in a magnetized outflow that has broken out of a confining medium and expanded to a high Lorentz factor (Γ ∼ 10{sup 2}-10{sup 3}) and low optical depth to scattering (τ {sub T} ∼ 10{sup –3}-10{sup –2}). The energy flux at breakout is dominated by the magnetic field, with a modest contribution from quasi-thermal gamma rays whose spectrum was calculated in Paper I. We focus on the case of extreme baryon depletion in the magnetized material, but allow for a separate baryonic component that is entrained from a confining medium. Dissipation is driven by relativistic motion between these two components, which develops once the photon compactness drops below 4 × 10{sup 3}(Y{sub e} /0.5){sup –1}. We first calculate the acceleration of the magnetized component following breakout, showing that embedded MHD turbulence provides significant inertia, the neglect of which leads to unrealistically high estimates of flow Lorentz factor. After reheating begins, the pair and photon distributions are evolved self-consistently using a one-zone kinetic code that incorporates an exact treatment of Compton scattering, pair production and annihilation, and Coulomb scattering. Heating leads to a surge in pair creation, and the scattering depth saturates at τ {sub T} ∼ 1-4. The plasma maintains a very low ratio of particle to magnetic pressure, and can support strong anisotropy in the charged particle distribution, with cooling dominated by Compton scattering. High-energy power-law spectra with photon indices in the range observed in gamma-ray bursts (GRBs; –3 < β < –3/2) are obtained by varying the ratio of heat input to the seed energy in quasi-thermal photons. We contrast our results with those for continuous heating across an expanding photosphere, and show that the latter model produces soft-to-hard evolution that is inconsistent with observations of GRBs.

  17. Ion assisted deposition of thermally evaporated Ag and Al films

    International Nuclear Information System (INIS)

    Hwangbo, C.K.; Lingg, L.J.; Lehan, J.P.; Macleod, H.A.; Makous, J.L.; Kim, S.Y.; University of Arizona, Physics Department, Tucson, Arizona 85721; Aju University, Physics Department, Suwon, Korea)

    1989-01-01

    Optical, electrical, and microstructural effects of Ar ion bombardment and Ar incorporation on thermally evaporated Ag and Al thin films are investigated. The results show that as the momentum supplied to the growing films by the bombarding ions per arriving metal atom increases, the refractive index at 632.8 nm increases and the extinction coefficient decreases, lattice spacing expands, grain size decreases, electrical resistivity increases, and trapped Ar increases slightly. In Ag films, stress reverses from tensile to compressive and in Al films compressive stress increases. In the Al films the change in optical constants can be explained by the variation in void volume. The reversal of stress from tensile to compressive in Ag films requires a threshold level of momentum. The increase in electrical resistivity is related to the decrease in grain size and increase in trapped Ar in both types of film. Many of these properties correlate well with the momentum transferred, suggesting that the momentum is an important physical parameter in describing the influence of ion beam on growing thin films and determining the characteristics of thin metal films prepared by ion assisted deposition

  18. Microwave-assisted synthesis of iron oxide nanoparticles in biocompatible organic environment

    Science.gov (United States)

    Aivazoglou, E.; Metaxa, E.; Hristoforou, E.

    2018-04-01

    The development of magnetite and maghemite particles in uniform nanometer size has triggered the interest of the research community due to their many interesting properties leading to a wide range of applications, such as catalysis, nanomedicine-nanobiology and other engineering applications. In this study, a simple, time-saving and low energy-consuming, microwave-assisted synthesis of iron oxide nanoparticles, is presented. The nanoparticles were prepared by microwave-assisted synthesis using polyethylene glycol (PEG) or PEG and β-cyclodextrin (β-CD)/water solutions of chloride salts of iron in the presence of ammonia solution. The prepared nano-powders were characterized using X-Ray Diffraction (XRD), Transition Electron Microscopy (TEM), Fourier-transform Infrared Spectroscopy (FTIR), Raman Spectroscopy, Vibrating Sample Magnetometer (VSM), X-Ray Photoelectron Spectroscopy (XPS) and Thermal analysis (TG/DSC). The produced nanoparticles are crystallized mostly in the magnetite and maghemite lattice exhibiting very similar shape and size, with indications of partial PEG coating. Heating time, microwave power and presence of PEG, are the key factors shaping the size properties of nanoparticles. The average size of particles ranges from 10.3 to 19.2 nm. The nanoparticles exhibit a faceted morphology, with zero contamination levels. The magnetic measurements indicate that the powders are soft magnetic materials with negligible coercivity and remanence, illustrating super-paramagnetic behavior.

  19. Electron-assisted magnetization tunneling in single spin systems

    Science.gov (United States)

    Balashov, Timofey; Karlewski, Christian; Märkl, Tobias; Schön, Gerd; Wulfhekel, Wulf

    2018-01-01

    Magnetic excitations of single atoms on surfaces have been widely studied experimentally in the past decade. Lately, systems with unprecedented magnetic stability started to emerge. Here, we present a general theoretical investigation of the stability of rare-earth magnetic atoms exposed to crystal or ligand fields of various symmetry and to exchange scattering with an electron bath. By analyzing the properties of the atomic wave function, we show that certain combinations of symmetry and total angular momentum are inherently stable against first or even higher-order interactions with electrons. Further, we investigate the effect of an external magnetic field on the magnetic stability.

  20. Thermomechanic equations for magnetic fluids of equilibrium magnetization

    International Nuclear Information System (INIS)

    Bashtovoy, V.G.; Berkovsky, B.M.; Vislovich, A.N.

    1988-01-01

    The main physical prerequisite for the existence of equilibrium magnetization is the assumption that nothing, except thermal motion, hinders the orientation of elementary magnetic moments along the field and that the mean value of magnetization is achieved instantaneously, i.e., within the times much shorter than the characteristic times of macroscopic processes (hydrodynamic, thermal, electromagnetic, etc.). This assumption makes it possible to consider the fluid magnetization vector M-vector at a given instant to be parallel to the vector of magnetic field intensity H-vector, which in the general form may be related as M-vector = (M/H)H-vector. Magnetization M is determined by the fluid temperature and density and by field intensity: M = M(T,rho,H). It is natural that it decreases with rising temperature and increases with the field intensity. The condition for the vectors M-vector and H-vector to be parallel is realized in a MF only for certain colloid characteristics. Nevertheless, for a wide range of problems this condition may be regarded as fulfilled and enables one to study those effects in a MF which are caused to occur by the volume magnetic force due to the interaction between equilibrium magnetization and the magnetic field

  1. High Temperature Magnetic Properties of Indirect Exchange Spring FePt/M(Cu,C/Fe Trilayer Thin Films

    Directory of Open Access Journals (Sweden)

    Anabil Gayen

    2013-01-01

    Full Text Available We report the investigation of temperature dependent magnetic properties of FePt and FePt(30/M(Cu,C/Fe(5 trilayer thin films prepared by using magnetron sputtering technique at ambient temperature and postannealed at different temperatures. L10 ordering, hard magnetic properties, and thermal stability of FePt films are improved with increasing postannealing temperature. In FePt/M/Fe trilayer, the formation of interlayer exchange coupling between magnetic layers depends on interlayer materials and interface morphology. In FePt/C/Fe trilayer, when the C interlayer thickness was about 0.5 nm, a strong interlayer exchange coupling between hard and soft layers was achieved, and saturation magnetization was enhanced considerably after using interlayer exchange coupling with Fe. In addition, incoherent magnetization reversal process observed in FePt/Fe films changes into coherent switching process in FePt/C/Fe films giving rise to a single hysteresis loop. High temperature magnetic studies up to 573 K reveal that the effective reduction in the coercivity decreases largely from 34 Oe/K for FePt/Fe film to 13 Oe/K for FePt/C(0.5/Fe film demonstrating that the interlayer exchange coupling seems to be a promising approach to improve the stability of hard magnetic properties at high temperatures, which is suitable for high-performance magnets and thermally assisted magnetic recording media.

  2. Synthesis of MnxGa1−xFe2O4 magnetic nanoparticles by thermal decomposition method for medical diagnosis applications

    International Nuclear Information System (INIS)

    Sánchez, Javier; Cortés-Hernández, Dora Alicia; Escobedo-Bocardo, José Concepción; Almanza-Robles, José Manuel; Reyes-Rodríguez, Pamela Yajaira; Jasso-Terán, Rosario Argentina; Bartolo-Pérez, Pascual; De-León-Prado, Laura Elena

    2017-01-01

    In this work, the synthesis of Mn x Ga 1−x Fe 2 O 4 (x=0–1) nanosized particles by thermal decomposition method, using tetraethylene glycol (TEG) as a reaction medium, has been performed. The crystalline structure of the inverse spinel obtained in all the cases was identified by X-ray diffraction (XRD). Vibration sample magnetometry (VSM) was used to evaluate the magnetic properties of ferrites and to demonstrate their superparamagnetic behavior and the increase of magnetization values due to the Mn 2+ ions incorporation into the FeGa 2 O 4 structure. Transmission electron microscopy, energy dispersive spectroscopy (TEM-EDS) and X-ray photoelectron spectroscopy (XPS) were used to characterize the obtained magnetic nanoparticles (MNPs). These MNPs showed a near spherical morphology, an average particle size of 5.6±1.5 nm and a TEG coating layer on their surface. In all the cases MNPs showed no response when submitted to an alternating magnetic field (AMF, 10.2 kA/m, 354 kHz) using magnetic induction tests. These results suggest that the synthesized nanoparticles can be potential candidates for their use in biomedical areas. - Highlights: • Superparamagnetic NPs of Mn x Ga 1−x Fe 2 O 4 were synthesized by thermal decomposition. • Saturation magnetization of MnGaFe 2 O 4 increases as Mn ions are increased. • Nanoparticles have a nanometric size of 5.6 nm and show no heating ability.

  3. The use of magnetite nanoparticles for implant-assisted magnetic drug targeting in thrombolytic therapy.

    Science.gov (United States)

    Kempe, Maria; Kempe, Henrik; Snowball, Ian; Wallén, Rita; Arza, Carlos Rodriguez; Götberg, Matthias; Olsson, Tommy

    2010-12-01

    Implant-assisted targeting of magnetic particles under the influence of an external magnetic field has previously been verified through mathematical modeling, in vitro studies, and in vivo studies on rat carotid arteries as a feasible method for localized drug delivery. The present study focuses on the development of nanoparticles for the treatment of in-stent thrombosis. Magnetic nanoparticles in the size-range 10-30 nm were synthesized in a one-pot procedure by precipitation of ferrous hydroxide followed by oxidation to magnetite. The nanoparticles were silanized with tetraethyl orthosilicate in the presence of triethylene glycol and/or polyethylene glycol. The surface coated magnetite nanoparticles were activated with either N-hydroxysulfosuccinimide or tresyl chloride for covalent immobilization of tissue plasminogen activator (tPA). Hysteresis loops showed saturation magnetizations of 55.8, 44.1, and 43.0 emu/g for the naked nanoparticles, the surface coated nanoparticles, and the tPA-nanoparticle conjugates, respectively. The hemolytic activity of the nanoparticles in blood was negligible. An initial in vivo biocompatibility test in pig, carried out by intravascular injection of the nanoparticles in a stented brachial artery, showed no short-term adverse effects. In vitro evaluation in a flow-through model proved that the nanoparticles were captured efficiently to the surface of a ferromagnetic coiled wire at the fluid velocities typical for human arteries. A preliminary test of the tPA-nanoparticle conjugates in a pig model suggested that the conjugates may be used for treatment of in-stent thrombosis in coronary arteries. Copyright © 2010 Elsevier Ltd. All rights reserved.

  4. Combustion characteristics and influential factors of isooctane active-thermal atmosphere combustion assisted by two-stage reaction of n-heptane

    Energy Technology Data Exchange (ETDEWEB)

    Lu, Xingcai; Ji, Libin; Ma, Junjun; Zhou, Xiaoxin; Huang, Zhen [Key Lab. for Power Machinery and Engineering of MOE, Shanghai Jiao Tong University, 200240 Shanghai (China)

    2011-02-15

    This paper presents an experimental study on the isooctane active-thermal atmosphere combustion (ATAC) which is assisted by two-stage reaction of n-heptane. The active-thermal atmosphere is created by low- and high-temperature reactions of n-heptane which is injected at intake port, and isooctane is directly injected into combustion chamber near the top dead center. The effects of isooctane injection timing, active-thermal atmosphere intensity, overall equivalence ratio, and premixed ratio on combustion characteristics and emissions are investigated. The experimental results reveal that, the isooctane ignition and combustion can be classified to thermal atmosphere combustion, active atmosphere combustion, and active-thermal atmosphere combustion respectively according to the extent of n-heptane oxidation as well as effects of isooctane quenching and charge cooling. n-Heptane equivalence ratio, isooctane equivalence ratio and isooctane delivery advance angle are major control parameters. In one combustion cycle, the isooctane ignited and burned after those of n-heptane, and then this combustion phenomenon can also be named as dual-fuel sequential combustion (DFSC). The ignition timing of the overall combustion event is mainly determined by n-heptane equivalence ratio and can be controlled in flexibility by simultaneously adjusting isooctane equivalence ratio. The isooctane ignition regime, overall thermal efficiency, and NO{sub x} emissions show strong sensitivity to the fuel delivery advance angle between 20 CA BTDC and 25 CA BTDC. (author)

  5. A new polarized neutrons method for studying depth-inhomogeneously magnetized magnetic films

    International Nuclear Information System (INIS)

    Korneev, D.A.

    1990-01-01

    The main specific features of the process of polarized thermal neutrons specular reflection from the surface of depth-inhomogeneously magnetic films are considered theoretically. It is shown how using the method of specular reflection of polarized thermal neutrons from such a films surface, one may restore the depth distribution of the local magnetization vector M-vector(z). 9 refs

  6. Photothermal investigation of local and depth dependent magnetic properties

    International Nuclear Information System (INIS)

    Pelzl, J; Meckenstock, R

    2010-01-01

    To achieve a spatially resolved measurement of magnetic properties two different photothermal approaches are used which rely on heat dissipated by magnetic resonance absorption or thermal modulation of the magnetic properties, respectively. The heat produced by modulated microwave absorption is detected by the classical photothermal methods such as photoacoustic effect and mirage effect. Examples comprise depth resolution of the magnetization of layered tapes and visualisation of magnetic excitations in ferrites. The second photothermal technique relies on the local modulation of magnetic properties by a thermal wave generated with an intensity modulated laser beam incident on the sample. This technique has a higher spatial resolution and sensitivity and has been used to characterize lateral magnetic properties of multilayers and spintronic media. To extend the lateral resolution of the ferromagnetic resonance detection into the nm-range techniques have been developed which are based on the detection of the modulated thermal microwave response by the thermal probe of an atomic force microscope (AFM) or by detection the thermal expansion of the magnetic sample in the course of the resonant microwave absorption with an AFM or tunnelling microscope. These thermal near field based techniques in ferromagnetic resonance have been successfully applied to image magnetic inhomogeneities around nano-structures and to measure the ferromagnetic resonance from magnetic nano-dots.

  7. Development of superconducting magnets for magnetically levitated trains

    International Nuclear Information System (INIS)

    Ohno, E.; Iwamoto, M.; Ogino, O.; Kawamura, T.

    1974-01-01

    Superconducting magnets will play a vital role in magnetically levitated trains, producing lift, guidance and propulsion forces. The main problems in the design are the current density of coils and the cryogenic thermal insulation. This paper describes the development of full-scale levitation magnets with length of 1.55m and width of 0.3 or 0.5m. Dynamic levitation tests using small model magnets are also presented. (author)

  8. Robust Magnetic Properties of a Sublimable Single-Molecule Magnet.

    Science.gov (United States)

    Kiefl, Evan; Mannini, Matteo; Bernot, Kevin; Yi, Xiaohui; Amato, Alex; Leviant, Tom; Magnani, Agnese; Prokscha, Thomas; Suter, Andreas; Sessoli, Roberta; Salman, Zaher

    2016-06-28

    The organization of single-molecule magnets (SMMs) on surfaces via thermal sublimation is a prerequisite for the development of future devices for spintronics exploiting the richness of properties offered by these magnetic molecules. However, a change in the SMM properties due to the interaction with specific surfaces is usually observed. Here we present a rare example of an SMM system that can be thermally sublimated on gold surfaces while maintaining its intact chemical structure and magnetic properties. Muon spin relaxation and ac susceptibility measurements are used to demonstrate that, unlike other SMMs, the magnetic properties of this system in thin films are very similar to those in the bulk, throughout the full volume of the film, including regions near the metal and vacuum interfaces. These results exhibit the robustness of chemical and magnetic properties of this complex and provide important clues for the development of nanostructures based on SMMs.

  9. Design, enhanced Thermal and Flow efficiency of a 2KW active magnetic regenerator

    DEFF Research Database (Denmark)

    Dallolio, Stefano; Eriksen, Dan; Engelbrecht, Kurt

    power of 1500 W over a temperature span of 25 K. This paper explains several details of the device, such as the design of the magnet, the regenerator housing and the flow system. In particular, this paper investigates the best geometry for the regenerator bed to achieve a thermal and mechanically...... efficient housing to be used in the AMR system. Particular attention has been given to the reduction of the parasitic losses through the regenerator housing: both heat leaks between the magnetocaloric material (MCM) and an adjacent iron ring and the surroundings through a lid on top of the regenerator...

  10. Lock-in thermography as a rapid and reproducible thermal characterization method for magnetic nanoparticles

    Energy Technology Data Exchange (ETDEWEB)

    Lemal, Philipp; Geers, Christoph; Monnier, Christophe A.; Crippa, Federica; Daum, Leopold; Urban, Dominic A.; Rothen-Rutishauser, Barbara [Adolphe Merkle Institute, University of Fribourg, Chemin des Verdiers 4, CH-1700 Fribourg (Switzerland); Bonmarin, Mathias, E-mail: mathias.bonmarin@zhaw.ch [Institute of Computational Physics, Zurich University of Applied Sciences, Technikumstrasse 9, 8400 Winterthur (Switzerland); Petri-Fink, Alke, E-mail: alke.fink@unifr.ch [Adolphe Merkle Institute, University of Fribourg, Chemin des Verdiers 4, CH-1700 Fribourg (Switzerland); Chemistry Department, University of Fribourg, Chemin du Museé 9, CH-1700 Fribourg (Switzerland); Moore, Thomas L., E-mail: thomaslee.moore@unifr.ch [Adolphe Merkle Institute, University of Fribourg, Chemin des Verdiers 4, CH-1700 Fribourg (Switzerland)

    2017-04-01

    Lock-in thermography (LIT) is a sensitive imaging technique generally used in engineering and materials science (e.g. detecting defects in composite materials). However, it has recently been expanded for investigating the heating power of nanomaterials, such as superparamagnetic iron oxide nanoparticles (SPIONs). Here we implement LIT as a rapid and reproducible method that can evaluate the heating potential of various sizes of SPIONs under an alternating magnetic field (AMF), as well as the limits of detection for each particle size. SPIONs were synthesized via thermal decomposition and stabilized in water via a ligand transfer process. Thermographic measurements of SPIONs were made by stimulating particles of varying sizes and increasing concentrations under an AMF. Furthermore, a commercially available SPION sample was included as an external reference. While the size dependent heating efficiency of SPIONs has been previously described, our objective was to probe the sensitivity limits of LIT. For certain size regimes it was possible to detect signals at concentrations as low as 0.1 mg Fe/mL. Measuring at different concentrations enabled a linear regression analysis and extrapolation of the limit of detection for different size nanoparticles. - Highlights: • A multi-sample screening assessment of magnetic nanoparticle thermal characteristics is shown via lock-in thermography. • Lower concentration limit of nanoparticle detection based on particle size is proposed. • A commercially available reference sample indicates the stability and reproducibility of LIT.

  11. Microwave assisted synthesis of Magnetically responsive composite materials

    Czech Academy of Sciences Publication Activity Database

    Šafařík, Ivo; Horská, Kateřina; Pospíšková, K.; Maděrová, Zdeňka; Šafaříková, Miroslava

    2013-01-01

    Roč. 49, č. 1 (2013), s. 213-218 ISSN 0018-9464 R&D Projects: GA ČR(CZ) GAP503/11/2263; GA MŠk LH12190 Institutional support: RVO:67179843 Keywords : magnetic materials * magnetic modification * magnetic separation * microwaves Subject RIV: EH - Ecology, Behaviour Impact factor: 1.213, year: 2013

  12. Small fan assisted air conditioner for thermal comfort and energy saving in Thailand

    International Nuclear Information System (INIS)

    Atthajariyakul, Surat; Lertsatittanakorn, Charoenporn

    2008-01-01

    From the fact that Thai people have a tolerance to high air temperature and are accustomed to high air movement from electric fans in non-air conditioned space, this paper proposes the use of small fan assisted air conditioners for human thermal comfort and energy saving in Thailand. In the study, a total 15 students were tested in a 2.5 x 3.5 x 2.5 m 3 test room equipped with a 12,000 Btu/h split type air conditioner. During the tests, the room air temperature was varied from 25, 26, 27 and 28 deg. C every 1 h. A small fan with 15 cm diameter was placed in front of each subject. In each hour, the small fan was varied to supply a small area with velocity from 0.2, 0.5, 1, 1.5 and 2 m/s. In each condition, the subjects were asked to vote for their thermal sensation. The results showed that the temperature set point could be increased up to 28 deg. C when a small fan was used to supply local air velocity from 0.5 to 2 m/s according to individual preference. This would reduce the electricity consumption of the air conditioning unit. According to the proposed method, this can save energy for office buildings in the commercial sector as high as 1959.51 GWh/year

  13. Effects of thickness and annealing condition on magnetic properties and thermal stabilities of Ta/Nd/NdFeB/Nd/Ta sandwiched films

    International Nuclear Information System (INIS)

    Liu Wen-Feng; Zhang Min-Gang; Zhang Ke-Wei; Zhang Hai-Jie; Chai Yue-Sheng; Xu Xiao-Hong

    2016-01-01

    Ta/Nd/NdFeB/Nd/Ta sandwiched films are deposited by magnetron sputtering on Si (100) substrates, and subsequently annealed in vacuum at different temperatures for different time. It is found that both the thickness of NdFeB and Nd layer and the annealing condition can affect the magnetic properties of Ta/Nd/NdFeB/Nd/Ta films. Interestingly, the thickness and annealing temperature show the relevant behaviors that can affect the magnetic properties of the film. The high coercivity of 24.1 kOe (1 Oe = 79.5775 A/m) and remanence ratio (remanent magnetization/saturation magnetization) of 0.94 can be obtained in a Ta/Nd(250 nm)/NdFeB(600 nm)/Nd(250 nm)/Ta film annealed for 3 min at 1023 K. In addition, the thermal stability of the film is also linked to the thickness of NdFeB and Nd layer and the annealing temperature as well. The excellent thermal stability can be achieved in a Ta/Nd(250 nm)/NdFeB(600 nm)/Nd(250 nm)/Ta film annealed at 1023 K. (paper)

  14. New developments in NdFeB-based permanent magnets

    International Nuclear Information System (INIS)

    Liu, Z.W.

    2011-01-01

    NdFeB based alloys have been used as permanent magnets for almost thirty years. The recent researches aim at optimizing the composition, microstructure and properties, reducing cost, and developing new processes. The demand for sintered magnet is increasing. Efforts are directed towards improving properties by controlling grain boundary diffusion, minimizing the rare earth (RE) content and also improving production yield. As for bonded magnets, to enhance remanence and energy product, nanocrystalline powders are employed. High thermal stability has been realized by mixing NdFeB with hard ferrite powders. For nanocrystalline and nano composite NdFeB based alloys, both compositional modification and microstructural optimization have been carried out. New approaches have also been proposed to prepare NdFeB magnets with idea structure. Surfactant assisted ball milling is a good top-down method to obtain nano sized hard magnetic particles and anisotropic nano flakes. Synthesis of NdFeB nanoparticles and NdFeB/Fe (Co) nano composite powders by bottom-up techniques, such as chemical reduction process and co-precipitation, has been successful very recently. To assemble nanocrystalline NdFeB powders or nanoparticles into bulk magnets, various novel consolidation processes including spark plasma sintering and high velocity press have been employed. Hot deformation can be selected as the process to achieve anisotropy in nanocrystalline magnets. (author)

  15. Hyper-resistivity and electron thermal conductivity due to destroyed magnetic surfaces in axisymmetric plasma equilibria

    Energy Technology Data Exchange (ETDEWEB)

    Weening, R. H. [Department of Radiologic Sciences, Thomas Jefferson University, 901 Walnut Street, Philadelphia, Pennsylvania 19107-5233 (United States)

    2012-06-15

    In order to model the effects of small-scale current-driven magnetic fluctuations in a mean-field theoretical description of a large-scale plasma magnetic field B(x,t), a space and time dependent hyper-resistivity {Lambda}(x,t) can be incorporated into the Ohm's law for the parallel electric field E Dot-Operator B. Using Boozer coordinates, a theoretical method is presented that allows for a determination of the hyper-resistivity {Lambda}({psi}) functional dependence on the toroidal magnetic flux {psi} for arbitrary experimental steady-state Grad-Shafranov axisymmetric plasma equilibria, if values are given for the parallel plasma resistivity {eta}({psi}) and the local distribution of any auxiliary plasma current. Heat transport in regions of plasma magnetic surfaces destroyed by resistive tearing modes can then be modeled by an electron thermal conductivity k{sub e}({psi})=({epsilon}{sub 0}{sup 2}m{sub e}/e{sup 2}){Lambda}({psi}), where e and m{sub e} are the electron charge and mass, respectively, while {epsilon}{sub 0} is the permittivity of free space. An important result obtained for axisymmetric plasma equilibria is that the {psi}{psi}-component of the metric tensor of Boozer coordinates is given by the relation g{sup {psi}{psi}}({psi}){identical_to}{nabla}{psi} Dot-Operator {nabla}{psi}=[{mu}{sub 0}G({psi})][{mu}{sub 0}I({psi})]/{iota}({psi}), with {mu}{sub 0} the permeability of free space, G({psi}) the poloidal current outside a magnetic surface, I({psi}) the toroidal current inside a magnetic surface, and {iota}({psi}) the rotational transform.

  16. Magnetically responsive enzyme powders

    Energy Technology Data Exchange (ETDEWEB)

    Pospiskova, Kristyna, E-mail: kristyna.pospiskova@upol.cz [Regional Centre of Advanced Technologies and Materials, Palacky University, Slechtitelu 11, 783 71 Olomouc (Czech Republic); Safarik, Ivo, E-mail: ivosaf@yahoo.com [Regional Centre of Advanced Technologies and Materials, Palacky University, Slechtitelu 11, 783 71 Olomouc (Czech Republic); Department of Nanobiotechnology, Institute of Nanobiology and Structural Biology of GCRC, Na Sadkach 7, 370 05 Ceske Budejovice (Czech Republic)

    2015-04-15

    Powdered enzymes were transformed into their insoluble magnetic derivatives retaining their catalytic activity. Enzyme powders (e.g., trypsin and lipase) were suspended in various liquid media not allowing their solubilization (e.g., saturated ammonium sulfate and highly concentrated polyethylene glycol solutions, ethanol, methanol, 2-propanol) and subsequently cross-linked with glutaraldehyde. Magnetic modification was successfully performed at low temperature in a freezer (−20 °C) using magnetic iron oxides nano- and microparticles prepared by microwave-assisted synthesis from ferrous sulfate. Magnetized cross-linked enzyme powders were stable at least for two months in water suspension without leakage of fixed magnetic particles. Operational stability of magnetically responsive enzymes during eight repeated reaction cycles was generally without loss of enzyme activity. Separation of magnetically modified cross-linked powdered enzymes from reaction mixtures was significantly simplified due to their magnetic properties. - Highlights: • Cross-linked enzyme powders were prepared in various liquid media. • Insoluble enzymes were magnetized using iron oxides particles. • Magnetic iron oxides particles were prepared by microwave-assisted synthesis. • Magnetic modification was performed under low (freezing) temperature. • Cross-linked powdered trypsin and lipase can be used repeatedly for reaction.

  17. Synthesis and application of magnetic deep eutectic solvents: Novel solvents for ultrasound assisted liquid-liquid microextraction of thiophene.

    Science.gov (United States)

    Khezeli, Tahere; Daneshfar, Ali

    2017-09-01

    Two novel magnetic deep eutectic solvents (MDESs), comprised of cheap and simple components named [choline chloride/phenol] [FeCl 4 ] and [choline chloride/ethylene glycol] [FeCl 4 ] were prepared and characterized by CHN elemental analysis, proton nuclear magnetic resonance ( 1 H NMR), vibrating sample magnetometery (VSM), Raman, Fourier transform-infrared (FT-IR) and UV-Vis spectrometery. The extraction efficiency of the prepared MDESs has been investigated in ultrasound assisted liquid-liquid microextraction based MDES (UALLME-MDES). Briefly, MDESs were added to n-heptan containing thiophene. Then, MDESs were dispersed in n-heptane by sonication. After that, microdroplets of MDESs were collected by a magnet and the remained concentration of thiophene in n-heptane phase was analyzed by GC-FID. The results indicated that [choline chloride/phenol] [FeCl 4 ] has higher extraction efficiency than [choline chloride/ethylene glycol] [FeCl 4 ]. This work opens a new way to the application of MDESs. Copyright © 2016 Elsevier B.V. All rights reserved.

  18. Magnetism and thermal induced characteristics of Fe{sub 2}O{sub 3} content bioceramics

    Energy Technology Data Exchange (ETDEWEB)

    Wu, Chun-Shiang; Hsi, Chi-Shiung [Department of Materials Science and Engineering, National United University, Miaoli 36003, Taiwan (China); Hsu, Fang-Chi, E-mail: fangchi@nuu.edu.tw [Department of Materials Science and Engineering, National United University, Miaoli 36003, Taiwan (China); Wang, Moo-Chin [Department of Fragrance and Cosmetics, Kaohsiung Medical University, Kaohsiung 807, Taiwan (China); Chen, Yung-Sheng [Department of Materials Science and Engineering, I-Shou University, Kaohsiung 803, Taiwan (China)

    2012-11-15

    Magnetic properties of Li{sub 2}O-MnO{sub 2}-CaO-P{sub 2}O{sub 5}-SiO{sub 2} (LMCPS) glasses doped with various amounts of Fe{sub 2}O{sub 3} were investigated. There is a dramatic change in the magnetic property of pristine LMCPS after the addition of Fe{sub 2}O{sub 3} and crystallized at 850 Degree-Sign C for 4 h. Both the electron paramagnetic resonance and magnetic susceptibility measurements showed that the glass ceramic with 4 at% Fe{sub 2}O{sub 3} exhibited the coexistence of superparamagnetism and ferromagnetism at room temperature. When the Fe{sub 2}O{sub 3} content was higher than 8 at%, the LMCPS glasses showed ferromagnetism behavior. The complex magnetic behavior is due to the distribution of (Li, Mn)ferrite particle sizes driven by the Fe{sub 2}O{sub 3} content. The thermal induced hysteresis loss of the crystallized LMCPS glass ceramics was characterized under an alternating magnetic field. The energy dissipations of the crystallized LMCPS glass ceramics were determined by the concentration and Mn/Fe ratios of Li(Mn, Fe)ferrite phase formed in the glass ceramics. - Highlights: Black-Right-Pointing-Pointer Presence of Fe{sub 2}O{sub 3} in LMCPS glass ceramic promotes the growth of (Li, Mn)ferrite. Black-Right-Pointing-Pointer The amount of Fe{sub 2}O{sub 3} determines the size of (Li,Mn)ferrite particles. Black-Right-Pointing-Pointer Room temperature superparamagnetism was obtained at 4 at% of Fe{sub 2}O{sub 3} addition. Black-Right-Pointing-Pointer In addition, Li(Mn, Fe)ferrite phase contributes to the magnetic energy loss. Black-Right-Pointing-Pointer The largest energy loss is the trade-off between the ferrite content and Mn/Fe ratio.

  19. Is There a Magnet-School Effect? A Multisite Study of MSAP-Funded Magnet Schools

    Science.gov (United States)

    Wang, Jia; Schweig, Jonathan D.; Herman, Joan L.

    2017-01-01

    Magnet schools are one of the largest sectors of choice schools in the United States. In this study, we explored the heterogeneity in magnet-school effects on student achievement by examining 24 magnet schools, funded under the Magnet Schools Assistance Program (MSAP), in 5 school districts across 4 states. The magnet effects were synthesized…

  20. Phenomenological crystal-field model of the magnetic and thermal properties of the Kondo-like system UCu2Si2

    Science.gov (United States)

    Troć, R.; Gajek, Z.; Pikul, A.; Misiorek, H.; Colineau, E.; Wastin, F.

    2013-07-01

    The transport properties described previously [Troć , Phys. Rev. BPRBMDO1098-012110.1103/PhysRevB.85.224434 85, 224434 (2012)] as well as the magnetic and thermal properties presented in this paper, observed for single-crystalline UCu2Si2, are discussed by assuming a dual (localized-itinerant) scenario. The electronic states of the localized 5f electrons in UCu2Si2 are constructed using the effective Hamiltonian known for ionic systems, allowing us to treat the Coulomb, spin-orbital, and crystal-field interactions on equal footing. The space of parameters has been restricted in the initial steps with the aid of the angular overlap model approximation. The final crystal-field parameters, obtained from the refined steps of calculations, are relatively large (in absolute values), which we attribute to the hybridization characteristic of the metallic systems on the verge of localization. The proposed crystal-field model reproduces correctly with satisfactory accuracy the magnetic and thermal properties of UCu2Si2 in agreement also with the transport properties reported previously. Considerable crystal-field splitting of the ground multiplet of 2760 K is responsible for a large anisotropy in the magnetic behavior, observed in the whole temperature range explored.

  1. One-step microwave-assisted synthesis of water-dispersible Fe3O4 magnetic nanoclusters for hyperthermia applications

    Science.gov (United States)

    Sathya, Ayyappan; Kalyani, S.; Ranoo, Surojit; Philip, John

    2017-10-01

    To realize magnetic hyperthermia as an alternate stand-alone therapeutic procedure for cancer treatment, magnetic nanoparticles with optimal performance, within the biologically safe limits, are to be produced using simple, reproducible and scalable techniques. Herein, we present a simple, one-step approach for synthesis of water-dispersible magnetic nanoclusters (MNCs) of superparamagnetic iron oxide by reducing of Fe2(SO4)3 in sodium acetate (alkali), poly ethylene glycol (capping ligand), and ethylene glycol (solvent and reductant) in a microwave reactor. The average size and saturation magnetization of the MNC's are tuned from 27 to 52 nm and 32 to 58 emu/g by increasing the reaction time from 10 to 600 s. Transmission electron microscopy images reveal that each MNC composed of large number of primary Fe3O4 nanoparticles. The synthesised MNCs show excellent colloidal stability in aqueous phase due to the adsorbed PEG layer. The highest SAR value of 215 ± 10 W/gFe observed in 52 nm size MNC at a frequency of 126 kHz and field of 63 kA/m suggest the potential use of these MNC in hyperthermia applications. This study further opens up the possibilities to develop metal ion-doped MNCs with tunable sizes suitable for various biomedical applications using microwave assisted synthesis.

  2. A predictive thermal dynamic model for parameter generation in the laser assisted direct write process

    International Nuclear Information System (INIS)

    Shang Shuo; Fearon, Eamonn; Wellburn, Dan; Sato, Taku; Edwardson, Stuart; Dearden, G; Watkins, K G

    2011-01-01

    The laser assisted direct write (LADW) method can be used to generate electrical circuitry on a substrate by depositing metallic ink and curing the ink thermally by a laser. Laser curing has emerged over recent years as a novel yet efficient alternative to oven curing. This method can be used in situ, over complicated 3D contours of large parts (e.g. aircraft wings) and selectively cure over heat sensitive substrates, with little or no thermal damage. In previous studies, empirical methods have been used to generate processing windows for this technique, relating to the several interdependent processing parameters on which the curing quality and efficiency strongly depend. Incorrect parameters can result in a track that is cured in some areas and uncured in others, or in damaged substrates. This paper addresses the strong need for a quantitative model which can systematically output the processing conditions for a given combination of ink, substrate and laser source; transforming the LADW technique from a purely empirical approach, to a simple, repeatable, mathematically sound, efficient and predictable process. The method comprises a novel and generic finite element model (FEM) that for the first time predicts the evolution of the thermal profile of the ink track during laser curing and thus generates a parametric map which indicates the most suitable combination of parameters for process optimization. Experimental data are compared with simulation results to verify the accuracy of the model.

  3. Magnetic and thermal Moessbauer effect scans: a new approach

    International Nuclear Information System (INIS)

    Pasquevich, G. A.; Zelis, P. Mendoza; Sanchez, F. H.; Fernandez van Raap, M. B.; Veiga, A.; Martinez, N.

    2006-01-01

    Moessbauer transmission recorded at fixed photon energies as a function of a given physical parameter such as temperature, external field, etc. (Moessbauer scan), is being developed as a useful quantitative tool, complementary of Moessbauer spectroscopy. Scans are performed at selected energies, suitable for the observation of a given physical property or process. It is shown that one of main advantages of this approach is the higher speed at which the external physical parameter can be swept, which allows the recording of quasi-continuous experimental response functions as well as the study of processes which occur too fast to be followed by Moessbauer spectroscopy. The applications presented here are the determination of the temperature dependence of the 57 Fe hyperfine field in FeSn 2 , the thermal evolution and nanocrystallization kinetics of amorphous Fe 73.5 Si 13.5 Cu 1 Nb 3 B 9 and the measurement of the dynamic response of Fe magnetic moments in nanocrystalline Fe 90 Zr 7 B 3 to an external ac field.

  4. Magnetically Assisted Fast Ignition

    OpenAIRE

    Wang, W.-M.; Gibbon, P.; Sheng, Z.-M.; Li, Y.-T.

    2015-01-01

    Fast ignition (FI) is investigated via integrated particle-in-cell simulation including both generation andtransport of fast electrons, where petawatt ignition lasers of 2 ps and compressed targets of a peak density of300 g cm−3 and areal density of 0.49 g cm−2 at the core are taken. When a 20 MG static magnetic field isimposed across a conventional cone-free target, the energy coupling from the laser to the core is enhancedby sevenfold and reaches 14%. This value even exceeds that obtained u...

  5. PIC Simulations of Velocity-space Instabilities in a Decreasing Magnetic Field: Viscosity and Thermal Conduction

    Science.gov (United States)

    Riquelme, Mario; Quataert, Eliot; Verscharen, Daniel

    2018-02-01

    We use particle-in-cell (PIC) simulations of a collisionless, electron–ion plasma with a decreasing background magnetic field, {\\boldsymbol{B}}, to study the effect of velocity-space instabilities on the viscous heating and thermal conduction of the plasma. If | {\\boldsymbol{B}}| decreases, the adiabatic invariance of the magnetic moment gives rise to pressure anisotropies with {p}| | ,j> {p}\\perp ,j ({p}| | ,j and {p}\\perp ,j represent the pressure of species j (electron or ion) parallel and perpendicular to B ). Linear theory indicates that, for sufficiently large anisotropies, different velocity-space instabilities can be triggered. These instabilities in principle have the ability to pitch-angle scatter the particles, limiting the growth of the anisotropies. Our simulations focus on the nonlinear, saturated regime of the instabilities. This is done through the permanent decrease of | {\\boldsymbol{B}}| by an imposed plasma shear. We show that, in the regime 2≲ {β }j≲ 20 ({β }j\\equiv 8π {p}j/| {\\boldsymbol{B}}{| }2), the saturated ion and electron pressure anisotropies are controlled by the combined effect of the oblique ion firehose and the fast magnetosonic/whistler instabilities. These instabilities grow preferentially on the scale of the ion Larmor radius, and make {{Δ }}{p}e/{p}| | ,e≈ {{Δ }}{p}i/{p}| | ,i (where {{Δ }}{p}j={p}\\perp ,j-{p}| | ,j). We also quantify the thermal conduction of the plasma by directly calculating the mean free path of electrons, {λ }e, along the mean magnetic field, finding that {λ }e depends strongly on whether | {\\boldsymbol{B}}| decreases or increases. Our results can be applied in studies of low-collisionality plasmas such as the solar wind, the intracluster medium, and some accretion disks around black holes.

  6. Thermal magnetic resonance: physics considerations and electromagnetic field simulations up to 23.5 Tesla (1GHz)

    International Nuclear Information System (INIS)

    Winter, Lukas; Oezerdem, Celal; Hoffmann, Werner; Lindt, Tessa van de; Periquito, Joao; Ji, Yiyi; Ghadjar, Pirus; Budach, Volker; Wust, Peter; Niendorf, Thoralf

    2015-01-01

    Glioblastoma multiforme is the most common and most aggressive malign brain tumor. The 5-year survival rate after tumor resection and adjuvant chemoradiation is only 10 %, with almost all recurrences occurring in the initially treated site. Attempts to improve local control using a higher radiation dose were not successful so that alternative additive treatments are urgently needed. Given the strong rationale for hyperthermia as part of a multimodal treatment for patients with glioblastoma, non-invasive radio frequency (RF) hyperthermia might significantly improve treatment results. A non-invasive applicator was constructed utilizing the magnetic resonance (MR) spin excitation frequency for controlled RF hyperthermia and MR imaging in an integrated system, which we refer to as thermal MR. Applicator designs at RF frequencies 300 MHz, 500 MHz and 1GHz were investigated and examined for absolute applicable thermal dose and temperature hotspot size. Electromagnetic field (EMF) and temperature simulations were performed in human voxel models. RF heating experiments were conducted at 300 MHz and 500 MHz to characterize the applicator performance and validate the simulations. The feasibility of thermal MR was demonstrated at 7.0 T. The temperature could be increased by ~11 °C in 3 min in the center of a head sized phantom. Modification of the RF phases allowed steering of a temperature hotspot to a deliberately selected location. RF heating was monitored using the integrated system for MR thermometry and high spatial resolution MRI. EMF and thermal simulations demonstrated that local RF hyperthermia using the integrated system is feasible to reach a maximum temperature in the center of the human brain of 46.8 °C after 3 min of RF heating while surface temperatures stayed below 41 °C. Using higher RF frequencies reduces the size of the temperature hotspot significantly. The opportunities and capabilities of thermal magnetic resonance for RF hyperthermia interventions

  7. Negative thermal expansion in functional materials: controllable thermal expansion by chemical modifications.

    Science.gov (United States)

    Chen, Jun; Hu, Lei; Deng, Jinxia; Xing, Xianran

    2015-06-07

    Negative thermal expansion (NTE) is an intriguing physical property of solids, which is a consequence of a complex interplay among the lattice, phonons, and electrons. Interestingly, a large number of NTE materials have been found in various types of functional materials. In the last two decades good progress has been achieved to discover new phenomena and mechanisms of NTE. In the present review article, NTE is reviewed in functional materials of ferroelectrics, magnetics, multiferroics, superconductors, temperature-induced electron configuration change and so on. Zero thermal expansion (ZTE) of functional materials is emphasized due to the importance for practical applications. The NTE functional materials present a general physical picture to reveal a strong coupling role between physical properties and NTE. There is a general nature of NTE for both ferroelectrics and magnetics, in which NTE is determined by either ferroelectric order or magnetic one. In NTE functional materials, a multi-way to control thermal expansion can be established through the coupling roles of ferroelectricity-NTE, magnetism-NTE, change of electron configuration-NTE, open-framework-NTE, and so on. Chemical modification has been proved to be an effective method to control thermal expansion. Finally, challenges and questions are discussed for the development of NTE materials. There remains a challenge to discover a "perfect" NTE material for each specific application for chemists. The future studies on NTE functional materials will definitely promote the development of NTE materials.

  8. Heat conduction coefficient and coefficient of linear thermal expansion of electric insulation materials for superconducting magnetic system

    International Nuclear Information System (INIS)

    Deev, V.I.; Sobolev, V.P.; Kruglov, A.B.; Pridantsev, A.I.

    1984-01-01

    Results of experimental investigation of heat conduction coefficient and coefficient of linear thermal expansion and thermal shrinkages of the STEF-1 textolite-glass widely used in superconducting magnetic systems as electric insulating and structural material are presented. Samples of two types have been died: sample axisa is perpendicular to a plae of fiberglass layers ad sample axis is parallel to a plane of fiberglass layers. Heat conduction coefficient was decreased almost a five times with temperature decrease from 300 up to 5K and was slightly dependent on a sample type. Temperature variation of linear dimensions in a sample of the first type occurs in twice as fast as compared to the sample of the second type

  9. Broadband spectroscopy of magnetic response in a nano-scale magnetic wire

    International Nuclear Information System (INIS)

    Yamaguchi, A.; Motoi, K.; Miyajima, H.; Utsumi, Y.

    2014-01-01

    We measure the broadband spectra of magnetic response in a single layered ferromagnetic nano-scale wire in order to investigate the size effect on the ferromagnetic resonance. We found that the resonance frequency difference between 300-nm- and 5-μm-wide wires was varied by about 5 GHz due to the shape anisotropy. Furthermore, we experimentally detected the magnetization precession induced by the thermal fluctuation via the rectification of a radio-frequency (rf) current by incorporating an additional direct current (dc) by using Wheatstone bridge circuit. Our investigation renders that the shape anisotropy is of great importance to control the resonance frequency and to provide thermal stability of the microwave devices. - Highlights: • We describe an experimental investigation of the magnetic response of a single layered ferromagnetic nano-scale wire. • We present the conventional broadband microwave spectroscopy with a vector network analyzer and rectifying spectroscopy obtained with a Wheatstone bridge technique. • The investigation enables us to characterize the size effect on the ferromagnetic response and also to detect the magnetization precession induced by the thermal fluctuations

  10. Low-temperature thermal expansion

    International Nuclear Information System (INIS)

    Collings, E.W.

    1986-01-01

    This chapter discusses the thermal expansion of insulators and metals. Harmonicity and anharmonicity in thermal expansion are examined. The electronic, magnetic, an other contributions to low temperature thermal expansion are analyzed. The thermodynamics of the Debye isotropic continuum, the lattice-dynamical approach, and the thermal expansion of metals are discussed. Relative linear expansion at low temperatures is reviewed and further calculations of the electronic thermal expansion coefficient are given. Thermal expansions are given for Cu, Al and Ti. Phenomenologic thermodynamic relationships are also discussed

  11. Exchange coupled CoPt/FePtC media for heat assisted magnetic recording

    Science.gov (United States)

    Dutta, Tanmay; Piramanayagam, S. N.; Ru, Tan Hui; Saifullah, M. S. M.; Bhatia, C. S.; Yang, Hyunsoo

    2018-04-01

    L10 FePtC granular media are being studied as potential future magnetic recording media and are set to be used in conjunction with heat assisted magnetic recording (HAMR) to enable recording at write fields within the range of current day recording heads. Media structures based on a FePtC storage layer and a capping layer can alleviate the switching field distribution (SFD) requirements of HAMR and reduce the noise originating from the writing process. However, the current designs suffer from SFD issues due to high temperature writing. To overcome this problem, we study a CoPt/FePtC exchange coupled composite structure, where FePtC serves as the storage layer and CoPt (with higher Curie temperature, Tc) as the capping layer. CoPt remains ferromagnetic at near Tc of FePtC. Consequently, the counter exchange energy from CoPt would reduce the noise resulting from the adjacent grain interactions during the writing process. CoPt/FePtC bilayer samples with different thicknesses of CoPt were investigated. Our studies found that CoPt forms a continuous layer at a thickness of 6 nm and leads to considerable reduction in the saturation field and its distribution.

  12. SUPPRESSION OF PARALLEL TRANSPORT IN TURBULENT MAGNETIZED PLASMAS AND ITS IMPACT ON THE NON-THERMAL AND THERMAL ASPECTS OF SOLAR FLARES

    Energy Technology Data Exchange (ETDEWEB)

    Bian, Nicolas H.; Kontar, Eduard P. [School of Physics and Astronomy, University of Glasgow, Glasgow G12 8QQ (United Kingdom); Emslie, A. Gordon, E-mail: n.bian@physics.gla.ac.uk, E-mail: emslieg@wku.edu [Department of Physics and Astronomy, Western Kentucky University, Bowling Green, KY 42101 (United States)

    2016-06-20

    The transport of the energy contained in electrons, both thermal and suprathermal, in solar flares plays a key role in our understanding of many aspects of the flare phenomenon, from the spatial distribution of hard X-ray emission to global energetics. Motivated by recent RHESSI observations that point to the existence of a mechanism that confines electrons to the coronal parts of flare loops more effectively than Coulomb collisions, we here consider the impact of pitch-angle scattering off turbulent magnetic fluctuations on the parallel transport of electrons in flaring coronal loops. It is shown that the presence of such a scattering mechanism in addition to Coulomb collisional scattering can significantly reduce the parallel thermal and electrical conductivities relative to their collisional values. We provide illustrative expressions for the resulting thermoelectric coefficients that relate the thermal flux and electrical current density to the temperature gradient and the applied electric field. We then evaluate the effect of these modified transport coefficients on the flare coronal temperature that can be attained, on the post-impulsive-phase cooling of heated coronal plasma, and on the importance of the beam-neutralizing return current on both ambient heating and the energy loss rate of accelerated electrons. We also discuss the possible ways in which anomalous transport processes have an impact on the required overall energy associated with accelerated electrons in solar flares.

  13. Thermally induced magnonic spin current, thermomagnonic torques, and domain-wall dynamics in the presence of Dzyaloshinskii-Moriya interaction

    Science.gov (United States)

    Wang, X.-G.; Chotorlishvili, L.; Guo, G.-H.; Sukhov, A.; Dugaev, V.; Barnaś, J.; Berakdar, J.

    2016-09-01

    Thermally activated domain-wall (DW) motion in magnetic insulators has been considered theoretically, with a particular focus on the role of Dzyaloshinskii-Moriya interaction (DMI) and thermomagnonic torques. The thermally assisted DW motion is a consequence of the magnonic spin current due to the applied thermal bias. In addition to the exchange magnonic spin current and the exchange adiabatic and the entropic spin transfer torques, we also consider the DMI-induced magnonic spin current, thermomagnonic DMI fieldlike torque, and the DMI entropic torque. Analytical estimations are supported by numerical calculations. We found that the DMI has a substantial influence on the size and the geometry of DWs, and that the DWs become oriented parallel to the long axis of the nanostrip. Increasing the temperature smoothes the DWs. Moreover, the thermally induced magnonic current generates a torque on the DWs, which is responsible for their motion. From our analysis it follows that for a large enough DMI the influence of DMI-induced fieldlike torque is much stronger than that of the DMI and the exchange entropic torques. By manipulating the strength of the DMI constant, one can control the speed of the DW motion, and the direction of the DW motion can be switched, as well. We also found that DMI not only contributes to the total magnonic current, but also it modifies the exchange magnonic spin current, and this modification depends on the orientation of the steady-state magnetization. The observed phenomenon can be utilized in spin caloritronics devices, for example in the DMI based thermal diodes. By switching the magnetization direction, one can rectify the total magnonic spin current.

  14. Thermal effect on structural and magnetic properties of Fe78B13Si9 annealed amorphous ribbons

    Science.gov (United States)

    Soltani, Mohamed Larbi; Touares, Abdelhay; Aboki, Tiburce A. M.; Gasser, Jean-Georges

    2017-08-01

    In the present work, we study the influence of thermal treatments on the magnetic properties of as-quenched and pre-crystallized Fe78Si9B13 after stress relaxation. The crystallization behavior of amorphous and treated Fe78Si9B13 ribbons was revisited. The measurements were carried out by means of Differential Scanning Calorimetry, by X-ray diffraction and by Vibrating Sample Magnetometer, Susceptometer and fluxmeter. Relaxed samples were heated in the resistivity device up to 700°C and annealed near the onset temperature about 420°C for respectively 1, 3, 5, 8 hours. In as-quenched samples, two transition points occur at about 505°C and 564°C but in relaxed sample, the transition points have been found about 552°C and 568°C. Kinetics of crystallization was deduced for all studied samples. Annealing of the as-purchased ribbon shows the occurrence of α-Fe and tetragonal Fe3B resulting from the crystallization of the remaining amorphous phase. The effects on magnetic properties were pointed out by relating the structural evolution of the samples. The magnetic measurements show that annealing change the saturation magnetization and the coercive magnetic field values, hence destroying the good magnetic properties of the material. The heat treatment shows that the crystallization has greatly altered the shape of the cycles and moved the magnetic saturation point of the samples. The effect of treatment on the magneto-crystalline anisotropy is also demonstrated.

  15. Animal magnetocardiography using superconducting quantum interference device gradiometers assisted with magnetic nanoparticle injection: A sensitive method for early detecting electromagnetic changes induced by hypercholesterolemia

    Science.gov (United States)

    Wu, C. C.; Hong, B. F.; Wu, B. H.; Yang, S. Y.; Horng, H. E.; Yang, H. C.; Tseng, W. Y. Isaac; Tseng, W. K.; Liu, Y. B.; Lin, L. C.; Lu, L. S.; Lee, Y. H.

    2007-01-01

    In this work, the authors used a superconducting quantum interference device (SQUID) magnetocardiography (MCG) system consisted of 64-channel low-transition-temperature SQUID gradiometers to detect the MCG signals of hepercholesterolemic rabbits. In addition, the MCG signals were recorded before and after the injection of magnetic nanoparticles into the rabbits' ear veins to investigate the effects of magnetic nanoparticles on the MCG signals. These MCG data were compared to those of normal rabbits to reveal the feasibility for early detection of the electromagnetic changes induced by hypercholesterolemia using MCG with the assistance of magnetic nanoparticle injection.

  16. Microwave-assisted synthesis of iron oxide nanoparticles in biocompatible organic environment

    Directory of Open Access Journals (Sweden)

    E. Aivazoglou

    2018-04-01

    Full Text Available The development of magnetite and maghemite particles in uniform nanometer size has triggered the interest of the research community due to their many interesting properties leading to a wide range of applications, such as catalysis, nanomedicine-nanobiology and other engineering applications. In this study, a simple, time-saving and low energy-consuming, microwave-assisted synthesis of iron oxide nanoparticles, is presented. The nanoparticles were prepared by microwave-assisted synthesis using polyethylene glycol (PEG or PEG and β-cyclodextrin (β-CD/water solutions of chloride salts of iron in the presence of ammonia solution. The prepared nano-powders were characterized using X-Ray Diffraction (XRD, Transition Electron Microscopy (TEM, Fourier-transform Infrared Spectroscopy (FTIR, Raman Spectroscopy, Vibrating Sample Magnetometer (VSM, X-Ray Photoelectron Spectroscopy (XPS and Thermal analysis (TG/DSC. The produced nanoparticles are crystallized mostly in the magnetite and maghemite lattice exhibiting very similar shape and size, with indications of partial PEG coating. Heating time, microwave power and presence of PEG, are the key factors shaping the size properties of nanoparticles. The average size of particles ranges from 10.3 to 19.2 nm. The nanoparticles exhibit a faceted morphology, with zero contamination levels. The magnetic measurements indicate that the powders are soft magnetic materials with negligible coercivity and remanence, illustrating super-paramagnetic behavior.

  17. Fluid force predictions and experimental measurements for a magnetically levitated pediatric ventricular assist device.

    Science.gov (United States)

    Throckmorton, Amy L; Untaroiu, Alexandrina; Lim, D Scott; Wood, Houston G; Allaire, Paul E

    2007-05-01

    The latest generation of artificial blood pumps incorporates the use of magnetic bearings to levitate the rotating component of the pump, the impeller. A magnetic suspension prevents the rotating impeller from contacting the internal surfaces of the pump and reduces regions of stagnant and high shear flow that surround fluid or mechanical bearings. Applying this third-generation technology, the Virginia Artificial Heart Institute has developed a ventricular assist device (VAD) to support infants and children. In consideration of the suspension design, the axial and radial fluid forces exerted on the rotor of the pediatric VAD were estimated using computational fluid dynamics (CFD) such that fluid perturbations would be counterbalanced. In addition, a prototype was built for experimental measurements of the axial fluid forces and estimations of the radial fluid forces during operation using a blood analog mixture. The axial fluid forces for a centered impeller position were found to range from 0.5 +/- 0.01 to 1 +/- 0.02 N in magnitude for 0.5 +/- 0.095 to 3.5 +/- 0.164 Lpm over rotational speeds of 6110 +/- 0.39 to 8030 +/- 0.57% rpm. The CFD predictions for the axial forces deviated from the experimental data by approximately 8.5% with a maximum difference of 18% at higher flow rates. Similarly for the off-centered impeller conditions, the maximum radial fluid force along the y-axis was found to be -0.57 +/- 0.17 N. The maximum cross-coupling force in the x direction was found to be larger with a maximum value of 0.74 +/- 0.22 N. This resulted in a 25-35% overestimate of the radial fluid force as compared to the CFD predictions; this overestimation will lead to a far more robust magnetic suspension design. The axial and radial forces estimated from the computational results are well within a range over which a compact magnetic suspension can compensate for flow perturbations. This study also serves as an effective and novel design methodology for blood pump

  18. Exchange coupling mechanism for magnetization reversal and thermal stability of Co nanoparticles embedded in a CoO matrix

    International Nuclear Information System (INIS)

    Givord, Dominique; Skumryev, Vassil; Nogues, Josep

    2005-01-01

    A model providing a semi-quantitative account of the magnetic behavior of Co nanoparticles embedded in a CoO matrix is presented. The results confirm that exchange coupling at the interface between ferromagnetic (FM) and antiferromagnetic (AFM) nanostructures could provide an extra source of magnetic anisotropy, leading to thermal stability of the FM nanoparticles. It is shown that perpendicular coupling between the AFM and FM moments may result in large coercivities. The energy barrier, which works against reversal is due to the AFM susceptibility anisotropy. The experimentally observed exchange bias is tentatively ascribed to pre-existing intrinsic canting of the AFM moments at the interface

  19. Thermal analysis of continuous and patterned multilayer films in the presence of a nanoscale hot spot

    Science.gov (United States)

    Juang, Jia-Yang; Zheng, Jinglin

    2016-10-01

    Thermal responses of multilayer films play essential roles in state-of-the-art electronic systems, such as photo/micro-electronic devices, data storage systems, and silicon-on-insulator transistors. In this paper, we focus on the thermal aspects of multilayer films in the presence of a nanoscale hot spot induced by near field laser heating. The problem is set up in the scenario of heat assisted magnetic recording (HAMR), the next-generation technology to overcome the data storage density limit imposed by superparamagnetism. We characterized thermal responses of both continuous and patterned multilayer media films using transient thermal modeling. We observed that material configurations, in particular, the thermal barriers at the material layer interfaces crucially impact the temperature field hence play a key role in determining the hot spot geometry, transient response and power consumption. With a representative generic media model, we further explored the possibility of optimizing thermal performances by designing layers of heat sink and thermal barrier. The modeling approach demonstrates an effective way to characterize thermal behaviors of micro and nano-scale electronic devices with multilayer thin film structures. The insights into the thermal transport scheme will be critical for design and operations of such electronic devices.

  20. Facile and efficient one-pot solvothermal and microwave-assisted synthesis of stable colloidal solutions of MFe2O4 spinel magnetic nanoparticles

    International Nuclear Information System (INIS)

    Solano, Eduardo; Perez-Mirabet, Leonardo; Martinez-Julian, Fernando; Guzmán, Roger; Arbiol, Jordi; Puig, Teresa; Obradors, Xavier; Yañez, Ramón; Pomar, Alberto; Ricart, Susagna; Ros, Josep

    2012-01-01

    Well-defined synthesis conditions of high quality MFe 2 O 4 (M = Mn, Fe, Co, Ni, Zn, and Cu) spinel ferrite magnetic nanoparticles, with diameters below 10 nm, have been described based on facile and efficient one-pot solvothermal or microwave-assisted heating procedures. Both methods are reproducible and scalable and allow forming concentrated stable colloidal solutions in polar solvents, but microwave-assisted heating allows reducing 15 times the required annealing time and leads to an enhanced monodispersity of the nanoparticles. Non-agglomerated nanoparticles dispersions have been achieved using a simple one-pot approach where a single compound, triethyleneglycol, behaves at the same time as solvent and capping ligand. A narrow nanoparticle size distribution and high quality crystallinity have been achieved through selected nucleation and growth conditions. High resolution transmission electron microscopy images and electron energy loss spectroscopy analysis confirm the expected structure and composition and show that similar crystal faceting has been formed in both synthetic approaches. The spinel nanoparticles behave as ferrimagnets with a high saturation magnetization and are superparamagnetic at room temperature. The influence of synthesis route on phase purity and unconventional magnetic properties is discussed in some particular cases such as CuFe 2 O 4 , CoFe 2 O 4 , and ZnFe 2 O 4 .

  1. Pathological and 3 Tesla Volumetric Magnetic Resonance Imaging Predictors of Biochemical Recurrence after Robotic Assisted Radical Prostatectomy: Correlation with Whole Mount Histopathology.

    Science.gov (United States)

    Tan, Nelly; Shen, Luyao; Khoshnoodi, Pooria; Alcalá, Héctor E; Yu, Weixia; Hsu, William; Reiter, Robert E; Lu, David Y; Raman, Steven S

    2018-05-01

    We sought to identify the clinical and magnetic resonance imaging variables predictive of biochemical recurrence after robotic assisted radical prostatectomy in patients who underwent multiparametric 3 Tesla prostate magnetic resonance imaging. We performed an institutional review board approved, HIPAA (Health Insurance Portability and Accountability Act) compliant, single arm observational study of 3 Tesla multiparametric magnetic resonance imaging prior to robotic assisted radical prostatectomy from December 2009 to March 2016. Clinical, magnetic resonance imaging and pathological information, and clinical outcomes were compiled. Biochemical recurrence was defined as prostate specific antigen 0.2 ng/cc or greater. Univariate and multivariate regression analysis was performed. Biochemical recurrence had developed in 62 of the 255 men (24.3%) included in the study at a median followup of 23.5 months. Compared to the subcohort without biochemical recurrence the subcohort with biochemical recurrence had a greater proportion of patients with a high grade biopsy Gleason score, higher preoperative prostate specific antigen (7.4 vs 5.6 ng/ml), intermediate and high D'Amico classifications, larger tumor volume on magnetic resonance imaging (0.66 vs 0.30 ml), higher PI-RADS® (Prostate Imaging-Reporting and Data System) version 2 category lesions, a greater proportion of intermediate and high grade radical prostatectomy Gleason score lesions, higher pathological T3 stage (all p <0.01) and a higher positive surgical margin rate (19.3% vs 7.8%, p = 0.016). On multivariable analysis only tumor volume on magnetic resonance imaging (adjusted OR 1.57, p = 0.016), pathological T stage (adjusted OR 2.26, p = 0.02), positive surgical margin (adjusted OR 5.0, p = 0.004) and radical prostatectomy Gleason score (adjusted OR 2.29, p = 0.004) predicted biochemical recurrence. In this cohort tumor volume on magnetic resonance imaging and pathological variables, including Gleason score

  2. Preparation, characterization, magnetic and thermal studies of some chelate polymers of first series transition metal ions

    International Nuclear Information System (INIS)

    Ukey, Vaishali V.; Juneja, H.D.; Borkar, S.D.; Ghubde, R.S.; Naz, S.

    2006-01-01

    Azelaoyl-bis-hydroxamic acid used as bis ligand for the preparation of chelate polymers of Mn(II), Co(II), Ni(II) and Zn(II). These chelate polymers have been synthesized by refluxing the metal acetate and bis ligand as 1:1 stoichiometry. In the present work, structural determination of these newly synthesized chelate polymers has been studied on the basis of elemental analyses, infrared and reflectance spectral, magnetic and thermal studies. The decomposition temperature and the order of reaction have been determined by TGA analysis. On the basis of these studies, the Zn(II) chelate polymer has tetrahedral geometry, whereas Mn(II), Co(II) and Ni(II) chelate polymers have octahedral geometry and have the thermal stability in the order Ni(II) > Mn(II) > Zn(II) > Co(II)

  3. Ultrasonic-assisted preparation of graphene oxide carboxylic acid polyvinyl alcohol polymer film and studies of thermal stability and surface resistivity.

    Science.gov (United States)

    Li, Yongshen; Li, Jihui; Li, Yuehai; Li, Yali; Song, Yunan; Niu, Shuai; Li, Ning

    2018-01-01

    In this paper, flake graphite, nitric acid and acetic anhydride are used to prepare graphene oxide carboxylic acid (GO-COOH) via an ultrasonic-assisted method, and GO-COOH and polyvinyl alcohol polymer (PVA) are used to synthesize graphene oxide carboxylic acid polyvinyl alcohol polymer (GO-COOPVA) via the ultrasonic-assisted method, and GO-COOPVA is used to manufacture graphene oxide carboxylic acid polyvinyl alcohol polymer film (GO-COOPVA film) via a solidification method, and the structure and morphology of GO-COOH, GO-COOPVA and GO-COOPVA film are characterized, and the thermal stability and surface resistivity are measured in the case of the different amount of GO-COOH. Based on the characterization and measurement, it has been successively confirmed and attested that carboxyl groups implant on 2D lattice of GO to form GO-COOH, and GO-COOH and PVA have the esterification reaction to produce GO-COOPVA, and GO-COOPVA consists of 2D lattice of GO-COOH and the chain of PVA connected in the form of carboxylic ester, and GO-COOPVA film is composed of GO-COOPVA, and the thermal stability of GO-COOPVA film obviously improves in comparison with PVA film, and the surface resistivity of GO-COOPVA film clearly decreases. Copyright © 2017 Elsevier B.V. All rights reserved.

  4. Computer-assisted imaging of the fetus with magnetic resonance imaging.

    Science.gov (United States)

    Colletti, P M

    1996-01-01

    The purpose of this paper is to review the use of magnetic resonance imaging (MRI) of the fetus and to propose future techniques and applications. Institutional review board approved MR images of the fetus were acquired in 66 patients with sonographically suspected fetal abnormalities. Axial, coronal, and sagittal short TR, short TE images were obtained. In addition, 12 studies were performed with rapid scans requiring 700-1200 ms using either GRASS or Spoiled GRASS techniques. Sequential studies demonstrating fetal motion were also performed. Three studies with 3D IR prepped GRASS were performed. These allowed for orthogonal and non-orthogonal reformatted views and 3D display. Normal fetal structures were shown with MRI, including brain, heart, liver, stomach, intestines, and bladder. Gross fetal anomalies could generally be demonstrated with MRI. MRI may give additional information to that of sonography in fetal anomalies, particularly those involving the central nervous system, and in the detection of fat, blood, and meconium. MRI of the fetus can demonstrate normal and abnormal structures. Newer techniques with faster imaging will allow for greater possibility of computer assisted manipulation of data.

  5. Surface Plasmon-Mediated Nanoscale Localization of Laser-Driven sub-Terahertz Spin Dynamics in Magnetic Dielectrics

    Science.gov (United States)

    Chekhov, Alexander L.; Stognij, Alexander I.; Satoh, Takuya; Murzina, Tatiana V.; Razdolski, Ilya; Stupakiewicz, Andrzej

    2018-05-01

    Ultrafast all-optical control of spins with femtosecond laser pulses is one of the hot topics at the crossroads of photonics and magnetism with a direct impact on future magnetic recording. Unveiling light-assisted recording mechanisms for an increase of the bit density beyond the diffraction limit without excessive heating of the recording medium is an open challenge. Here we show that surface plasmon-polaritons in hybrid metal-dielectric structures can provide spatial confinement of the inverse Faraday effect, mediating the excitation of localized coherent spin precession with 0.41 THz frequency. We demonstrate a two orders of magnitude enhancement of the excitation efficiency at the surface plasmon resonance within the 100 nm layer in dielectric garnet. Our findings broaden the horizons of ultrafast spin-plasmonics and open pathways towards non-thermal opto-magnetic recording at the nano-scale.

  6. Approximate energies and thermal properties of a position-dependent mass charged particle under external magnetic fields

    Institute of Scientific and Technical Information of China (English)

    M Eshghi; H Mehraban; S M Ikhdair

    2017-01-01

    We solve the Schr(o)dinger equation with a position-dependent mass (PDM) charged particle interacted via the superposition of the Morse-plus-Coulomb potentials and is under the influence of external magnetic and Aharonov-Bohm (AB) flux fields.The nonrelativistic bound state energies together with their wave functions are calculated for two spatially-dependent mass distribution functions.We also study the thermal quantifies of such a system.Further,the canonical formalism is used to compute various thermodynamic variables for second choosing mass by using the Gibbs formalism.We give plots for energy states as a function of various physical parameters.The behavior of the internal energy,specific heat,and entropy as functions of temperature and mass density parameter in the inverse-square mass case for different values of magnetic field are shown.

  7. Approximate energies and thermal properties of a position-dependent mass charged particle under external magnetic fields

    International Nuclear Information System (INIS)

    Eshghi, M; Mehraban, H; Ikhdair, S M

    2017-01-01

    We solve the Schrödinger equation with a position-dependent mass (PDM) charged particle interacted via the superposition of the Morse-plus-Coulomb potentials and is under the influence of external magnetic and Aharonov–Bohm (AB) flux fields. The nonrelativistic bound state energies together with their wave functions are calculated for two spatially-dependent mass distribution functions. We also study the thermal quantities of such a system. Further, the canonical formalism is used to compute various thermodynamic variables for second choosing mass by using the Gibbs formalism. We give plots for energy states as a function of various physical parameters. The behavior of the internal energy, specific heat, and entropy as functions of temperature and mass density parameter in the inverse-square mass case for different values of magnetic field are shown. (paper)

  8. Thermal convection in a toroidal duct of a liquid metal blanket. Part I. Effect of poloidal magnetic field

    International Nuclear Information System (INIS)

    Zhang, Xuan; Zikanov, Oleg

    2017-01-01

    Highlights: • 2D convection flow develops with internal heating and strong axial magnetic field. • Poloidal magnetic field suppresses turbulence at high Hartmann number. • Flow structure is dominated by large-scale counter-rotation vortices. • Effective heat transfer is maintained by surviving convection structures. - Abstract: We explore the effect of poloidal magnetic field on the thermal convection flow in a toroidal duct of a generic liquid metal blanket. Non-uniform strong heating (the Grashof number up to 10 11 ) arising from the interaction of high-speed neutrons with the liquid breeder, and strong magnetic field (the Hartmann number up to 10 4 ) corresponding to the realistic reactor conditions are considered. The study continues our earlier work , where the problem was solved for a purely toroidal magnetic field and the convection was found to result in two-dimensional turbulence and strong mixing within the duct. Here, we find that the poloidal component of the magnetic field suppresses turbulence, reduces the flow's kinetic energy and high-amplitude temperature fluctuations, and, at high values of Hartmann number, leads to a steady-state flow. At the same time, the intense mixing by the surviving convection structures remains able to maintain effective heat transfer between the liquid metal and the walls.

  9. Thermal conductivity of layered borides: The effect of building defects on the thermal conductivity of TmAlB4 and the anisotropic thermal conductivity of AlB2

    Directory of Open Access Journals (Sweden)

    X. J. Wang

    2014-04-01

    Full Text Available Rare earth metal borides have attracted great interest due to their unusual properties, such as superconductivity and f-electron magnetism. A recent discovery attributes the tunability of magnetism in rare earth aluminoborides to the effect of so-called “building defects.” In this paper, we report data for the effect of building defects on the thermal conductivities of α-TmAlB4 single crystals. Building defects reduce the thermal conductivity of α-TmAlB4 by ≈30%. At room temperature, the thermal conductivity of AlB2 is nearly a factor of 5 higher than that of α-TmAlB4. AlB2 single crystals are thermally anisotropic with the c-axis thermal conductivity nearly twice the thermal conductivity of the a-b plane. Temperature dependence of the thermal conductivity near and above room temperature reveals that both electrons and phonons contribute substantially to thermal transport in AlB2 with electrons being the dominant heat carriers.

  10. Thermal loading study for FY 1995

    International Nuclear Information System (INIS)

    1996-01-01

    This report provides the results of sensitivity analyses designed to assist the test planners in focusing their in-situ measurements on parameters that appear to be important to waste isolation. Additionally, the study provides a preliminary assessment of the feasibility of certain thermal management options. A decision on thermal loading is a critical part of the scientific and engineering basis for evaluating regulatory compliance of the potential repository for waste isolation. To show, with reasonable assurance, that the natural and engineered barriers will perform adequately under expected repository conditions (thermally perturbed) will require an integrated approach based on thermal testing (laboratory, and in-situ), natural analog observations, and analytic modeling. The Office of Civilian Radioactive Waste Management needed input to assist in the planning of the thermal testing program. Additionally, designers required information on the viability of various thermal management concepts. An approximately 18-month Thermal Loading Study was conducted from March, 1994 until September 30, 1995 to address these issues. This report documents the findings of that study. 89 refs., 71 figs., 33 tabs

  11. Magnetically assisted chemical separation (MACS) process: Preparation and optimization of particles for removal of transuranic elements

    International Nuclear Information System (INIS)

    Nunez, L.; Kaminski, M.; Bradley, C.; Buchholz, B.A.; Aase, S.B.; Tuazon, H.E.; Vandegrift, G.F.; Landsberger, S.

    1995-05-01

    The Magnetically Assisted Chemical Separation (MACS) process combines the selectivity afforded by solvent extractants with magnetic separation by using specially coated magnetic particles to provide a more efficient chemical separation of transuranic (TRU) elements, other radionuclides, and heavy metals from waste streams. Development of the MACS process uses chemical and physical techniques to elucidate the properties of particle coatings and the extent of radiolytic and chemical damage to the particles, and to optimize the stages of loading, extraction, and particle regeneration. This report describes the development of a separation process for TRU elements from various high-level waste streams. Polymer-coated ferromagnetic particles with an adsorbed layer of octyl(phenyl)-N,N-diisobutylcarbamoylmethylphosphine oxide (CMPO) diluted with tributyl phosphate (TBP) were evaluated for use in the separation and recovery of americium and plutonium from nuclear waste solutions. Due to their chemical nature, these extractants selectively complex americium and plutonium contaminants onto the particles, which can then be recovered from the solution by using a magnet. The partition coefficients were larger than those expected based on liquid[liquid extractions, and the extraction proceeded with rapid kinetics. Extractants were stripped from the particles with alcohols and 400-fold volume reductions were achieved. Particles were more sensitive to acid hydrolysis than to radiolysis. Overall, the optimization of a suitable NMCS particle for TRU separation was achieved under simulant conditions, and a MACS unit is currently being designed for an in-lab demonstration

  12. Recent investigations on refrigerants for magnetic refrigerators

    International Nuclear Information System (INIS)

    Hashimoto, T.

    1986-01-01

    In development of the magnetic refrigerator, an important problem is selection of magnetic materials as refrigerants. The main purpose of the present paper is to discuss the magnetic and thermal properties necessary for these refrigerants and to report recent investigations. Magnetic refrigerants can be expediently divided into two groups, one for the Carnottype magnetic refrigerator below 20 K and the other for the Ericsson-type refrigerator. The required physical properties of refrigerants in each type of the magnetic refrigerator are first discussed. And then, the results of recent investigations on the magnetic, thermal and magnetocaloric characters of several promising magnetic refrigerants are shown. Finally, a brief prospect of the magnetic refrigerants and refrigerators is given

  13. Magnetically responsive enzyme powders

    Czech Academy of Sciences Publication Activity Database

    Pospišková, K.; Šafařík, Ivo

    2015-01-01

    Roč. 380, APR 2015 (2015), s. 197-200 ISSN 0304-8853 R&D Projects: GA MŠk(CZ) LD13021 Institutional support: RVO:67179843 Keywords : enzyme powders * cross-linking * magnetic modification * magnetic separation * magnetic iron oxides particles * microwave-assisted synthesis Subject RIV: CE - Biochemistry Impact factor: 2.357, year: 2015

  14. A comparative study of magnetic properties of MnFe2O4 nanoparticles prepared by thermal decomposition and solvothermal methods

    Directory of Open Access Journals (Sweden)

    B Aslibeiki

    2017-09-01

    Full Text Available A comparative study of magnetic properties of MnFe2O4 ferrite nanoparticles prepared by two different methods has been reported. The first sample (S1 was synthesized by thermal decomposition of metal nitrates. And the second sample (S2 was prepared by solvothermal method using Tri-ethylene glycol (TEG. Magnetic hysteresis loops at 300 and 5 K; magnetization and AC susceptibility measurements versus temperature confirmed the effective role of TEG on the magnetic properties of nanoparticles. The results showed that, at 300 K the saturation magnetization (MS of S2 sample is 46% greater than that of S1 sample. At 5 K, the difference in MS of the samples raised to 60%. AC susceptibility measurements at different frequencies and also magnetization versus temperature under field cooling and zero field cooling processes revealed that, the TEG molecules influence the surface spins order of S2 sample. The sample S1 showed strongly interacting superspin glass state, while the sample S2 consists of weakly interacting superparamagnetic nanoparticles.

  15. Laser-assisted fabrication of materials

    CERN Document Server

    Manna, Indranil

    2013-01-01

    Laser assisted fabrication involves shaping of materials using laser as a source of heat. It can be achieved by removal of materials (laser assisted cutting, drilling, etc.), deformation (bending, extrusion), joining (welding, soldering) and addition of materials (surface cladding or direct laser cladding). This book on ´Laser assisted Fabrication’ is aimed at developing in-depth engineering concepts on various laser assisted macro and micro-fabrication techniques with the focus on application and a review of the engineering background of different micro/macro-fabrication techniques, thermal history of the treated zone and microstructural development and evolution of properties of the treated zone.

  16. Temporal behaviour of self generated magnetic field and its influence on inhibition of thermal flux in ICF plasma

    International Nuclear Information System (INIS)

    Jha, L.N.

    1989-06-01

    The self generated magnetic field of megagauss order is reported to play a crucial role in ICF target designs because of its strong influence on the transport of energy from the critical density region to the ablation layer. The inhibition of the thermal flux due to such a field, thus, affects the whole of the other phenomenon of ICF. The knowledge of the proper variation of the magnetic field may help in assigning the existing controversial value of flux limit, f. Many papers dealing with the spatial variation of such a field exist and are well documented but the study on the variation of self generated field with time is rare. Here, the spatial variation of the megagauss field generated in the corona of a wire target irradiated by a laser as well as a model to study the temporal nature of the B-field at the peak have been obtained by solving the self inhibited diffusion which is regarded as the most dominant mechanism by which the thermal transport is influenced. The field exists for about ten nanoseconds even after the laser is switched off. The ratio of the two components of the thermal conductivity is also plotted against time and shows the inhibition. So, a track on the B-field variation both in space and time is necessary to keep for at least a few nanoseconds for computation of f. (author). 19 refs, 4 figs

  17. Mass ablation and magnetic flux losses through a magnetized plasma-liner wall interface

    Science.gov (United States)

    García-Rubio, F.; Sanz, J.

    2017-07-01

    The understanding of energy and magnetic flux losses in a magnetized plasma medium confined by a cold wall is of great interest in the success of magnetized liner inertial fusion (MagLIF). In a MagLIF scheme, the fuel is magnetized and subsonically compressed by a cylindrical liner. Magnetic flux conservation is degraded by the presence of gradient-driven transport processes such as thermoelectric effects (Nernst) and magnetic field diffusion. In previous publications [Velikovich et al., Phys. Plasmas 22, 042702 (2015)], the evolution of a hot magnetized plasma in contact with a cold solid wall (liner) was studied using the classical collisional Braginskii's plasma transport equations in one dimension. The Nernst term degraded the magnetic flux conservation, while both thermal energy and magnetic flux losses were reduced with the electron Hall parameter ωeτe with a power-law asymptotic scaling (ωeτe)-1/2. In the analysis made in the present paper, we consider a similar situation, but with the liner being treated differently. Instead of a cold solid wall acting as a heat sink, we model the liner as a cold dense plasma with low thermal conduction (that could represent the cryogenic fuel layer added on the inner surface of the liner in a high-gain MagLIF configuration). Mass ablation comes into play, which adds notably differences to the previous analysis. The direction of the plasma motion is inverted, but the Nernst term still convects the magnetic field towards the liner. Magnetization suppresses the Nernst velocity and improves the magnetic flux conservation. Thermal energy in the hot plasma is lost in heating the ablated material. When the electron Hall parameter is large, mass ablation scales as (ωeτe)-3/10, while both the energy and magnetic flux losses are reduced with a power-law asymptotic scaling (ωeτe)-7/10.

  18. Experimental and numerical study of latent heat thermal energy storage systems assisted by heat pipes for concentrated solar power application

    Science.gov (United States)

    Tiari, Saeed

    A desirable feature of concentrated solar power (CSP) with integrated thermal energy storage (TES) unit is to provide electricity in a dispatchable manner during cloud transient and non-daylight hours. Latent heat thermal energy storage (LHTES) offers many advantages such as higher energy storage density, wider range of operating temperature and nearly isothermal heat transfer relative to sensible heat thermal energy storage (SHTES), which is the current standard for trough and tower CSP systems. Despite the advantages mentioned above, LHTES systems performance is often limited by low thermal conductivity of commonly used, low cost phase change materials (PCMs). Research and development of passive heat transfer devices, such as heat pipes (HPs) to enhance the heat transfer in the PCM has received considerable attention. Due to its high effective thermal conductivity, heat pipe can transport large amounts of heat with relatively small temperature difference. The objective of this research is to study the charging and discharging processes of heat pipe-assisted LHTES systems using computational fluid dynamics (CFD) and experimental testing to develop a method for more efficient energy storage system design. The results revealed that the heat pipe network configurations and the quantities of heat pipes integrated in a thermal energy storage system have a profound effect on the thermal response of the system. The optimal placement of heat pipes in the system can significantly enhance the thermal performance. It was also found that the inclusion of natural convection heat transfer in the CFD simulation of the system is necessary to have a realistic prediction of a latent heat thermal storage system performance. In addition, the effects of geometrical features and quantity of fins attached to the HPs have been studied.

  19. In-syringe magnetic-stirring-assisted liquid-liquid microextraction for the spectrophotometric determination of Cr(VI) in waters.

    Science.gov (United States)

    Henríquez, Camelia; Horstkotte, Burkhard; Solich, Petr; Cerdà, Víctor

    2013-08-01

    A fully automated method for the determination of chromate is described. It is based on the selective reaction of Cr(VI) with diphenylcarbazide in acidic media to form a colored complex of Cr(III) with the oxidation product diphenylcarbazone. The reaction was performed within the syringe of an automatic burette containing a magnetic stirrer for homogenization of the sample and the required reagents. In-syringe stirring was made possible using a specially designed driving device placed around the syringe barrel to achieve a rotating magnetic field in the syringe, forcing the stirrer to spin. In a second step, the reaction mixture in the syringe was neutralized to allow in-syringe magnetic-stirring-assisted dispersive liquid-liquid microextraction of the complex into 125 μL of n-hexanol. After phase separation by droplet flotation over 30 s, the organic phase was propelled into a coupled spectrophotometric detection cell. The entire multistep procedure including in-system standard preparation was done within 270 s. The method was used for the analysis of natural waters, achieving average analyte recovery of 103%, a limit of detection of 0.26 μg L(-1), and a repeatability of less than 4% relative standard deviation.

  20. Anisotropy of linear thermal expansion and compressibility of Y.sub.2./sub.Fe.sub.17./sub. under pressure and its correlation to magnetic structure

    Czech Academy of Sciences Publication Activity Database

    Arnold, Zdeněk; Kamarád, Jiří; Prokhnenko, Olexandr; Ritter, C.; Eto, T.; Honda, F.; Oomi, G.; Garcia-Landa, B.

    2002-01-01

    Roč. 22, - (2002), s. 175-179 ISSN 0895-7959 R&D Projects: GA ČR GA106/02/0943; GA AV ČR IAA1010018; GA MŠk ME 165 Institutional research plan: CEZ:AV0Z1010914 Keywords : intermetallic compounds * pressure effect * compressibility * thermal expansion * magnetic structure Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 0.414, year: 2002