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Sample records for temperature tensile properties

  1. Elevated temperature tensile properties of borated 304 stainless steel

    International Nuclear Information System (INIS)

    Stephens, J.J.; Sorenson, K.B.; McConnell, P.

    1993-01-01

    This paper presents a comparison of the tensile properties of Powder Metallurgy (PM) 'Grade A' material with that of the conventional IM 'Grade B' material for two selected Types (i.e., boron contents) as defined by the ASTM A887 specification: Types 304B5 and 304B7. Tensile properties have been generated for these materials at temperatures ranging from room temperature to 400degC (752degF). The data at higher temperatures are required for ASME Code Case purposes, since the use temperature of a basket under 'worst case' cask conditions may be as high as 343degC (650degF), due to self-heating by the activated fuel elements. We will also discuss the current status of efforts aimed at obtaining an ASME Boiler and Pressure Vessel Code Case for selected grades of borated stainless steel covered by the ASTM A887 specification. (J.P.N.)

  2. Temperature dependency of tensile properties of GFRP composite for wind turbine blades

    Energy Technology Data Exchange (ETDEWEB)

    Huh, Yong Hak; Kim, Jong Il; Kim, Dong Jin; Lee, Gun Chang [Korea Research Institute of Standards and Science, Daejeon (Korea, Republic of)

    2012-09-15

    In this study, the temperature dependency of the tensile properties of a glass fiber reinforced plastic (GFRP) used in wind turbine blades was examined. The tensile strength, elastic modulus, and Poisson's ratio of the tensile specimen manufactured from uniaxial (0 .deg.) and triaxial (0/{+-}45.deg) laminate composite plates were measured at four different testing temperatures-room temperature, -30 .deg. C, -50 .deg. C, and 60 .deg. C. It was found that the tensile strengths and elastic moduli of the uniaxial laminates were greater than those of the triaxial laminates over the testing temperature range. The tensile strength of the two laminates was significantly dependent on the testing temperature, while the dependency of the elastic modulus on the temperature was insignificant. Furthermore, it could be considered that the Poisson's ratio changed slightly with a change in the testing temperature.

  3. Temperature dependency of tensile properties of GFRP composite for wind turbine blades

    International Nuclear Information System (INIS)

    Huh, Yong Hak; Kim, Jong Il; Kim, Dong Jin; Lee, Gun Chang

    2012-01-01

    In this study, the temperature dependency of the tensile properties of a glass fiber reinforced plastic (GFRP) used in wind turbine blades was examined. The tensile strength, elastic modulus, and Poisson's ratio of the tensile specimen manufactured from uniaxial (0 .deg.) and triaxial (0/±45.deg) laminate composite plates were measured at four different testing temperatures-room temperature, -30 .deg. C, -50 .deg. C, and 60 .deg. C. It was found that the tensile strengths and elastic moduli of the uniaxial laminates were greater than those of the triaxial laminates over the testing temperature range. The tensile strength of the two laminates was significantly dependent on the testing temperature, while the dependency of the elastic modulus on the temperature was insignificant. Furthermore, it could be considered that the Poisson's ratio changed slightly with a change in the testing temperature

  4. Properties of aluminum alloys tensile, creep, and fatigue data at high and low temperatures

    CERN Document Server

    1999-01-01

    This book compiles more than 300 tables listing typical average properties of a wide range of aluminum alloys. The individual test results were compiled, plotted in various ways, and analyzed. The average values from the tensile and creep tests were then normalized to the published typical room-temperature tensile properties of the respective alloys for easy comparison. This extensive project was done by Alcoa Laboratories over a period of several years. The types of data presented include: Typical Mechanical Properties of Wrought and Cast Aluminum Alloys at Various Temperatures, including tensile properties at subzero temperatures, at temperature after various holding times at the test temperature, and at room temperature after exposure at various temperatures for various holding times; creep rupture strengths for various times at various temperatures; stresses required to generate various amounts of creep in various lengths of time; rotating-beam fatigue strengths; modulus of elasticity as a function of t...

  5. Tensile properties of commercially pure vanadium from room temperature to 1200 degree C

    International Nuclear Information System (INIS)

    Henshall, G.A.; Torres, S.G.

    1993-12-01

    The tensile properties of vanadium are sensitive to interstitial impurity content, on grain size and strain rate. Thus, it is problematic to use published tensile data for materials potentially varying in these quantities. This investigation was undertaken to fully characterize the tensile properties of the commercially pure vanadium used at Lawrence Livermore. Both sheet and rod stock were tested in vacuum from ambient temperature to 1200C at strain rates 6.67 x 10 -5 to 6.67 x 10 -2 s -1 . The results of these experiments show that vanadium behaves in a manner typical of many bcc metals containing interstitial impurities. Local peaks in yield stress and ultimate tensile stress vs temperature curves are observed at intermediate temperatures. Serrated yielding also is observed in some temperature ranges. Changes in strain rate within the quasi-static regime have a relatively small, predictable effect. The rod and sheet stock have similar properties, except that the lower yield stress of the rod is less than that of the sheet over most of the temperature range studied. No plateau in yield strength vs temperature curve was observed for the rod. In both forms, and for all temperatures, vanadium is ductile. The elongation to failure reaches a minimum of approximately 35% at a temperature of 500C and a maximum of approximately 140% at 1200C

  6. Tensile properties of unirradiated PCA from room temperature to 7000C

    International Nuclear Information System (INIS)

    Braski, D.N.; Maziasz, P.J.

    1983-01-01

    The tensile properties of Prime Candidate Alloy (PCA) austenitic stainless steel after three different thermomechanical treatments were determined from room temperature to 700 0 C. The solution-annealed PCA had the lowest strength and highest ductility, while the reverse was true for the 25%-cold-worked material. The PCA containing titanium-rich MC particles fell between the other two heats. The cold-worked PCA had nearly the same tensile properties as cold-worked type 316 stainless steel. Both alloys showed ductility minima at 300 0 C

  7. Size and temperature dependence of the tensile mechanical properties of zinc blende CdSe nanowires

    International Nuclear Information System (INIS)

    Fu, Bing; Chen, Na; Xie, Yiqun; Ye, Xiang; Gu, Xiao

    2013-01-01

    The effect of size and temperature on the tensile mechanical properties of zinc blende CdSe nanowires is investigated by all atoms molecular dynamic simulation. We found the ultimate tensile strength and Young's modulus will decrease as the temperature and size of the nanowire increase. The size and temperature dependence are mainly attributed to surface effect and thermally elongation effect. High reversibility of tensile behavior will make zinc blende CdSe nanowires suitable for building efficient nanodevices.

  8. Microstructure and tensile properties of tungsten at elevated temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Shen, Tielong [Laboratory for Nuclear Materials, Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); Institute of Modern Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); Dai, Yong, E-mail: yong.dai@psi.ch [Laboratory for Nuclear Materials, Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); Lee, Yongjoong [European Spallation Source, Tunavägen 24, 223 63 Lund (Sweden)

    2016-01-15

    In order to support the development of the 5 MW spallation target for the European Spallation Source, the effect of fabrication process on microstructure, ductile-to-brittle transition temperature (DBTT), tensile and fracture behaviour of powder-metallurgy pure tungsten materials has been investigated. A hot-rolled (HR) tungsten piece of 12 mm thickness and a hot-forged (HF) piece of about 80 mm thickness were used to simulate the thin and thick blocks in the target. The two tungsten pieces were characterized with metallography analysis, hardness measurement and tensile testing. The HR piece exhibits an anisotropic grain structure with an average size of about 330 × 140 × 40 μm in rolling, long transverse and short transverse (thickness) directions. The HF piece possesses a bimodal grain structure with about 310 × 170 × 70 μm grain size in deformed part and about 25 μm sized grains remained from sintering process. Hardness (HV0.2) of the HR piece is slightly greater than that of the HF one. The ductility of the HR tungsten specimens is greater than that of the HF tungsten. For the HF tungsten piece, specimens with small grains in gauge section manifest lower ductility but higher strength. The DBTT evaluated from the tensile results is 250–300 °C for the HR tungsten and about 350 °C for the HF tungsten. - Highlights: • This work was conducted to support the development of the 5 MW spallation target for the European Spallation Source. • The effect of fabrication process on microstructure, ductile-to-brittle transition temperature and tensile behaviour was studied with hot-rolled and hot-forged tungsten. • The tungsten materials were characterized with metallography analysis, hardness measurement and tensile test in a temperature range of 25–500 °C. • The results indicate that the HR tungsten has better mechanical properties in terms of greater ductility and lower ductile-to-brittle transition temperature.

  9. The temperature dependence of the tensile properties of thermally treated Alloy 690 tubing

    International Nuclear Information System (INIS)

    Harrod, D.L.; Gold, R.E.; Larsson, B.; Bjoerkman, G.

    1992-01-01

    Tensile tests were run in air on full tube cross-sections of 22.23 mm OD by 1.27 mm wall thickness Alloy 690 steam generator production tubes from ten (10) heats of material at eight (8) temperatures between room temperature and 760 degrees C. The tubing was manufactured to specification requirements consistent with the EPRI guidelines for Alloy 690 tubing. The room temperature stress-strain curves are described quite well by the Voce equation. Ductile fracture by dimpled rupture was observed at all test temperatures. The elevated temperature tensile properties are compared with design data given in the ASME Code

  10. Effect of test temperature on tensile and fatigue properties of nickel-base heat-resistant alloys

    International Nuclear Information System (INIS)

    Tsuji, Hirokazu; Nakajima, Hajime

    1987-01-01

    A series of tensile and strain controlled low-cycle fatigue tests were conducted at temperatures ranging from RT to 900 0 C on a nickel-base heat-resistant alloy, Hastelloy XR-II, which is one of the candidate alloys for applications in the process heating high-temperature gas-cooled reactor (HTGR). Fatigue tests at room temperature and all tensile tests were conducted in air, while fatigue tests at and above 400 0 C were conducted in the simulated HTGR helium environment. In those tests the effect of test temperature on tensile and fatigue properties was investigated. The ductility minimum point was observed near 600 0 C, while tensile and fatigue strengths decreased with increasing test temperature. The fatigue lives estimated with the method proposed by Manson were compatible with the experimental results under the given conditions. For the specimens fatigued at and above 700 0 C, the percentage of the intergranular fracture mode gradually increased with increasing test temperature. (orig.)

  11. Tensile Deformation Temperature Impact on Microstructure and Mechanical Properties of AISI 316LN Austenitic Stainless Steel

    Science.gov (United States)

    Xiong, Yi; He, Tiantian; Lu, Yan; Ren, Fengzhang; Volinsky, Alex A.; Cao, Wei

    2018-03-01

    Uniaxial tensile tests were conducted on AISI 316LN austenitic stainless steel from - 40 to 300 °C at a rate of 0.5 mm/min. Microstructure and mechanical properties of the deformed steel were investigated by optical, scanning and transmission electron microscopies, x-ray diffraction, and microhardness testing. The yield strength, ultimate tensile strength, elongation, and microhardness increase with the decrease in the test temperature. The tensile fracture morphology has the dimple rupture feature after low-temperature deformations and turns to a mixture of transgranular fracture and dimple fracture after high-temperature ones. The dominating deformation microstructure evolves from dislocation tangle/slip bands to large deformation twins/slip bands with temperature decrease. The deformation-induced martensite transformation can only be realized at low temperature, and its quantity increases with the decrease in the temperature.

  12. Thermal properties of graphene under tensile stress

    Science.gov (United States)

    Herrero, Carlos P.; Ramírez, Rafael

    2018-05-01

    Thermal properties of graphene display peculiar characteristics associated to the two-dimensional nature of this crystalline membrane. These properties can be changed and tuned in the presence of applied stresses, both tensile and compressive. Here, we study graphene monolayers under tensile stress by using path-integral molecular dynamics (PIMD) simulations, which allows one to take into account quantization of vibrational modes and analyze the effect of anharmonicity on physical observables. The influence of the elastic energy due to strain in the crystalline membrane is studied for increasing tensile stress and for rising temperature (thermal expansion). We analyze the internal energy, enthalpy, and specific heat of graphene, and compare the results obtained from PIMD simulations with those given by a harmonic approximation for the vibrational modes. This approximation turns out to be precise at low temperatures, and deteriorates as temperature and pressure are increased. At low temperature, the specific heat changes as cp˜T for stress-free graphene, and evolves to a dependence cp˜T2 as the tensile stress is increased. Structural and thermodynamic properties display non-negligible quantum effects, even at temperatures higher than 300 K. Moreover, differences in the behavior of the in-plane and real areas of graphene are discussed, along with their associated properties. These differences show up clearly in the corresponding compressibility and thermal expansion coefficient.

  13. Influences of hot-isostatic-pressing temperature on microstructure, tensile properties and tensile fracture mode of Inconel 718 powder compact

    International Nuclear Information System (INIS)

    Chang, Litao; Sun, Wenru; Cui, Yuyou; Yang, Rui

    2014-01-01

    Inconel 718 powders have been hot-isostatic-pressed (HIPed) at representative temperatures to investigate the variations in microstructure, tensile properties and tensile fracture mode of the powder compact. Microstructure of the powder compacts were characterized by optical microscopy (OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and so on. The results showed that the interdendritic precipitates inherited from the powders were partially retained in the powder compacts when the powders were HIPed at or below 1210 °C but were eliminated when HIPed at and above 1260 °C. The grain size uniformity of the powder compacts first increases and then decreases with increasing HIPing temperature. Prior particle boundaries (PPBs) were observed in the powder compacts HIPed at and below 1260 °C but was eliminated when HIPed at 1275 °C. The PPBs were decorated with carbide particles, the amount of the carbide particles at the PPBs decreases with increasing HIPing temperature. Most of the PPBs were pinned by the carbide particles in the compacts HIPed at 1140 °C. When the HIPing temperature was increased to 1210 °C and 1260 °C, a large number of PPBs de-pinned and moved beyond the pinning carbide particles, leading to grain growth and leaving carbide particles at the site of the original PPBs within the new grains. With increasing HIPing temperature, the 0.2% yield strength of the powder compacts at 650 °C decreases, the tensile elongation increases, and the tensile fracture mode changed from inter-particle dominant fracture to fully dimple ductile fracture

  14. Influences of hot-isostatic-pressing temperature on microstructure, tensile properties and tensile fracture mode of Inconel 718 powder compact

    Energy Technology Data Exchange (ETDEWEB)

    Chang, Litao [Institute of Metal Research, Chinese Academy of Sciences, Shenyang (China); University of Chinese Academy of Sciences, Beijing (China); Sun, Wenru; Cui, Yuyou [Institute of Metal Research, Chinese Academy of Sciences, Shenyang (China); Yang, Rui, E-mail: ryang@imr.ac.cn [Institute of Metal Research, Chinese Academy of Sciences, Shenyang (China)

    2014-04-01

    Inconel 718 powders have been hot-isostatic-pressed (HIPed) at representative temperatures to investigate the variations in microstructure, tensile properties and tensile fracture mode of the powder compact. Microstructure of the powder compacts were characterized by optical microscopy (OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and so on. The results showed that the interdendritic precipitates inherited from the powders were partially retained in the powder compacts when the powders were HIPed at or below 1210 °C but were eliminated when HIPed at and above 1260 °C. The grain size uniformity of the powder compacts first increases and then decreases with increasing HIPing temperature. Prior particle boundaries (PPBs) were observed in the powder compacts HIPed at and below 1260 °C but was eliminated when HIPed at 1275 °C. The PPBs were decorated with carbide particles, the amount of the carbide particles at the PPBs decreases with increasing HIPing temperature. Most of the PPBs were pinned by the carbide particles in the compacts HIPed at 1140 °C. When the HIPing temperature was increased to 1210 °C and 1260 °C, a large number of PPBs de-pinned and moved beyond the pinning carbide particles, leading to grain growth and leaving carbide particles at the site of the original PPBs within the new grains. With increasing HIPing temperature, the 0.2% yield strength of the powder compacts at 650 °C decreases, the tensile elongation increases, and the tensile fracture mode changed from inter-particle dominant fracture to fully dimple ductile fracture.

  15. Tensile properties and fracture mechanism of IN-100 superalloy in high temperature range

    Directory of Open Access Journals (Sweden)

    Milan T. Jovanović

    2017-06-01

    Full Text Available Tensile properties and fracture mechanism of a polycrystalline IN-100 superalloy have been investigated in the range from room temperature to 900°C. Optical microscopy (OM and transmission electron microscopy (TEM applying replica technique were used for microstructural investigation, whereas scanning electron microscopy (SEM was utilized for fracture study. High temperature tensile tests were carried out in vacuumed chamber. Results show that strength increases up to 700°C, and then sharply decreases with further increase in temperature. Elongation increases very slowly (6-7.5% till 500°C, then decreases to 4.5% at 900°C. Change in elongation may be ascribed to a change of fracture mechanism. Appearance of a great number of microvoids prevails up to 500°C resulting in a slow increase of elongation, whereas above this temperature elongation decrease is correlated with intergranular crystallographic fracture and fracture of carbides.

  16. Effects of Elevated Temperature Treatment on Compositions and Tensile Properties of Several Kinds of Basalt Fibers

    Directory of Open Access Journals (Sweden)

    CHEN Jing

    2017-06-01

    Full Text Available Five kinds of domestic basalt fibers were studied for the changes of chemical compositions, physical properties and tensile properties of these fibers before and after 200-800℃ treatment in air atmosphere and in nitrogen atmosphere. These works were done mainly by means of X-ray fluorescence spectrometry and fiber monofilament tensile testing methods in order to understand the elevated temperature resistance of basalt fiber. The experimental results show that the surface of basalt fibers becomes smoother with slightly smaller in diameter and mass reduction at the same time, due to the removal of fiber surface treatment agent after elevated temperature treatment in air atmosphere. Mass fractions of SiO2 and Al2O3 decrease while mass fractions of FeO+Fe2O3, CaO and MgO increase, among which the mass fraction of FeO+Fe2O3 increase the most with the maximum increase of 21%. The monofilament tensile strength of basalt fiber is reduced after 200℃ treatment and the maximum strength retention percentage is 98.3%. The monofilament tensile strength reduces evidently after 400℃ treatment and the maximum strength retention percentage is 64.6%. Moreover, the strength retention percentages of five kinds of basalt fibers are all less than 20% after 800℃ treatment. In addition, the fiber elongation at break decreases with the increase of treating temperature and the elastic modulus increases. Compared with that in air atmosphere, strength retention rate of basalt fiber is higher and tensile properties are more stable in nitrogen atmosphere.

  17. High temperature tensile properties and fracture characteristics of bimodal 12Cr-ODS steel

    International Nuclear Information System (INIS)

    Chauhan, Ankur; Litvinov, Dimitri; Aktaa, Jarir

    2016-01-01

    This article describes the tensile properties and fracture characteristics of a 12Cr oxide dispersion strengthened (ODS) ferritic steel with unique elongated bimodal grain size distribution. The tensile tests were carried out at four different temperatures, ranging from room temperature to 700 °C, at a nominal strain rate of 10"−"3 s"−"1. At room temperature the material exhibits a high tensile strength of 1294 MPa and high yield strength of 1200 MPa. At 700 °C, the material still exhibits relatively high tensile strength of 300 MPa. The total elongation-to-failure exceeds 18% over the whole temperature range and has a maximum value of 29% at 600 °C. This superior ductility is attributed to the material's bimodal grain size distribution. In comparison to other commercial, as well as experimental, ODS steels, the material shows an excellent compromise between strength and ductility. The fracture surface studies reveal a change in fracture behavior from a mixed mode fracture at room temperature to fully ductile fracture at 600 °C. At 700 °C, the fracture path changes from intragranular to intergranular fracture, which is associated with a reduced ductility. - Highlights: • The steel has a unique elongated bimodal grain size distribution. • The steel shows an excellent compromise between strength and ductility. • Superior ductility in comparison to other commercial and experimental ODS steels. • Fracture behavior changes from mixed mode fracture at room temperature to fully ductile fracture at 600 °C. • Fracture path changes from intragranular to intergranular fracture at 700 °C.

  18. Microstructure, tensile properties and fracture behavior of high temperature Al–Si–Mg–Cu cast alloys

    Energy Technology Data Exchange (ETDEWEB)

    Mohamed, A.M.A., E-mail: madel@uqac.ca [Center for Advanced Materials, Qatar University, Doha (Qatar); Department of Metallurgical and Materials Engineering, Faculty of Petroleum and Mining Engineering, Suez Canal University, Box 43721, Suez (Egypt); Samuel, F.H. [Université du Québec à Chicoutimi, Chicoutimi, QC, Canada G7H 2B1 (Canada); Al Kahtani, Saleh [Industrial Engineering Program, Mechanical Engineering Department, College of Engineering, Salman bin Abdulaziz University, Al Kharj (Saudi Arabia)

    2013-08-10

    The high temperature tensile behavior of 354 aluminum cast alloy was investigated in the presence of Zr and Ni. The cast alloys were given a solutionizing treatment followed by artificial aging at 190 °C for 2 h. High temperature tensile tests were conducted at various temperatures from 25 °C to 300 °C. Optical microscopy and electron probe micro-analyzer were used to study the microstructure of different intermetallic phases formed. The fractographic observations of fracture surface were analyzed by scanning electron microscopy to understand the fracture mechanism. The results revealed that the intermetallics phases of (Al, Si){sub 3}(Zr, Ti), Al{sub 3}CuNi and Al{sub 9}NiFe are the main feature in the microstructures of alloys with Zr and Ni additions. The results also indicated that the tensile strength of alloy decreases with an increase in temperature. The combined addition of 0.2 wt% Zr and 0.2 wt% Ni leads to a 30% increase in the tensile properties at 300 °C compared to the base alloy. Zr and Ni bearing phases played a vital role in the fracture mechanism of the alloys studied.

  19. Microstructure, tensile properties and fracture behavior of high temperature Al–Si–Mg–Cu cast alloys

    International Nuclear Information System (INIS)

    Mohamed, A.M.A.; Samuel, F.H.; Al Kahtani, Saleh

    2013-01-01

    The high temperature tensile behavior of 354 aluminum cast alloy was investigated in the presence of Zr and Ni. The cast alloys were given a solutionizing treatment followed by artificial aging at 190 °C for 2 h. High temperature tensile tests were conducted at various temperatures from 25 °C to 300 °C. Optical microscopy and electron probe micro-analyzer were used to study the microstructure of different intermetallic phases formed. The fractographic observations of fracture surface were analyzed by scanning electron microscopy to understand the fracture mechanism. The results revealed that the intermetallics phases of (Al, Si) 3 (Zr, Ti), Al 3 CuNi and Al 9 NiFe are the main feature in the microstructures of alloys with Zr and Ni additions. The results also indicated that the tensile strength of alloy decreases with an increase in temperature. The combined addition of 0.2 wt% Zr and 0.2 wt% Ni leads to a 30% increase in the tensile properties at 300 °C compared to the base alloy. Zr and Ni bearing phases played a vital role in the fracture mechanism of the alloys studied

  20. High Temperature Tensile Properties of Unirradiated and Neutron Irradiated 20 Cr-35 Ni Austenitic Steel

    Energy Technology Data Exchange (ETDEWEB)

    Roy, R B; Solly, B

    1966-12-15

    The tensile properties of an unirradiated and neutron irradiated (at 40 deg C) 20 % Cr, 35 % Ni austenitic steel have been studied at 650 deg C, 750 deg C and 820 deg C. The tensile elongation and mode of fracture (transgranular) of unirradiated specimens tested at room temperature and 650 deg C are almost identical. At 750 deg C and 820 deg C the elongation decreases considerably and a large part of the total elongation is non-uniform. Furthermore, the mode of fracture at these temperatures is intergranular and microscopic evidence suggests that fracture is caused by formation and linkup of grain boundary cavities. YS and UTS decrease monotonically with temperature. Irradiated specimens show a further decrease in ductility and an increase in the tendency to grain boundary cracking. Irradiation has no significant effect on the YS, but the UTS are reduced. The embrittlement of the irradiated specimens is attributed to the presence of He and Li atoms produced during irradiation and the possible mechanisms are discussed. Prolonged annealing of irradiated and unirradiated specimens at 650 deg C appears to have no significant effect on tensile properties.

  1. The elevated temperature tensile properties of S-200E commercially pure beryllium

    International Nuclear Information System (INIS)

    Henshall, G.A.; Torres, S.G.; Hanafee, J.E.

    1995-01-01

    The tensile properties of commercially pure beryllium are sensitive to temperature, impurity content, texture, grain size, and prior processing. Therefore, tensile tests have been conducted using the commercially pure S-200E Be commonly employed at Lawrence Livermore National Laboratory. These experiments were performed at temperatures ranging from 300 to 1100 degrees C in the longitudinal and transverse orientations at the quasi-static strain rate of 5.5 x 10 -4 s -1 . The results of these experiments reveal that the stress-strain curve is smooth, ie. without yield points or serrations, over the entire temperature range studied. The yield stress (YS) and ultimate tensile stress (UTS) decrease monotonically with increasing temperature. Similar strengths were measured for both the longitudinal and transverse orientations, with the latter exhibiting slightly lower YS and UTS values. The measured failure elongation (e f ) vs. temperature curve is complex due to the competing effects of increasing basal-plane fracture stress with increasing temperature combined with the presence of hot shortness at intermediate temperatures. The latter is believed to be caused, at least partially, by the presence of free aluminum impurities at the grain boundaries. This hypothesis is supported by the measured increase in e f at 700 degrees C following a 100-hr anneal at 750 degrees C, which would remove free Al from the grain boundaries. Texture also was found to influence e f . The favorable orientation of the basal planes for initiation and propagation of cleavage cracks in longitudinal specimens results in a significantly decreased failure elongation compared with the transverse orientation. The effects of testing temperature and specimen orientation on the reduction in area were found to be similar to those described for e f

  2. Low temperature tensile properties and stress corrosion cracking resistance in the super duplex stainless steels weldments

    International Nuclear Information System (INIS)

    Lee, Jeung Woo; Sung, Jang Hyun; Lee, Sung Keun

    1998-01-01

    Low temperature tensile properties and SCC resistances of super duplex stainless steels and their weldments are investigated. Tensile strengths increase remarkably with decreasing test temperature, while elongations decrease steeply at -196 .deg. C after showing peak or constant value down to -100 .deg. C. Owing to the low tensile deformation of weld region, elongations of welded specimen decrease in comparison to those of unwelded specimen. The welded tensile specimen is fractured through weld region at -196 .deg. C due to the fact that the finely dispersed ferrite phase in the austenite matrix increases an opportunity to supply the crack propagation path through the brittle ferrite phase at low temperature. The stress corrosion cracking initiates preferentially at the surface ferrite phase of base metal region and propagates through ferrite phase. When the corrosion crack meets with the fibrously aligned austenite phase to the tensile direction, the ferrite phase around austenite continues to corrode. Eventually, fracture of the austenite phase begins without enduring the tensile load. The addition of Cu+W to the super duplex stainless steel deteriorates the SCC resistance in boiling MgCl 2 solution, possibly due to the increment of pits in the ferrite phase and reduction of N content in the austenite phase

  3. HIGH TEMPERATURE TENSILE PROPERTIES OF NEW FE-CR-MN DEVELOPED STEEL

    OpenAIRE

    M. Mahmoudiniya; Sh. Kheirandish; M. Asadi Asadabad

    2017-01-01

    Nowadays, Ni-free austenitic stainless steels are being developed rapidly and high price of nickel is one of the most important motivations for this development. At present research a new FeCrMn steel was designed and produced based on Fe-Cr-Mn-C system. Comparative studies on microstructure and high temperature mechanical properties of  new steel and AISI 316 steel were done. The results showed that new FeCrMn developed steel has single austenite phase microstructure, and its tensile st...

  4. Study of Tensile Properties and Deflection Temperature of Polypropylene/Subang Pineapple Leaf Fiber Composites

    Science.gov (United States)

    Hafizhah, R.; Juwono, A. L.; Roseno, S.

    2017-05-01

    The development of eco-friendly composites has been increasing in the past four decades because the requirement of eco-friendly materials has been increasing. Indonesia has a lot of natural fiber resources and, pineapple leaf fiber is one of those fibers. This study aimed to determine the influence of weight fraction of pineapple leaf fibers, that were grown at Subang, to the tensile properties and the deflection temperature of polypropylene/Subang pineapple leaf fiber composites. Pineapple leaf fibers were pretreated by alkalization, while polypropylene pellets, as the matrix, were extruded into sheets. Hot press method was used to fabricate the composites. The results of the tensile test and Heat Deflection Temperature (HDT) test showed that the composites that contained of 30 wt.% pineapple leaf fiber was the best composite. The values of tensile strength, modulus of elasticity and deflection temperature were (64.04 ± 3.91) MPa; (3.98 ± 0.55) GPa and (156.05 ± 1.77) °C respectively, in which increased 187.36%, 198.60%, 264.72% respectively from the pristine polypropylene. The results of the observation on the fracture surfaces showed that the failure modes were fiber breakage and matrix failure.

  5. Ultra-high temperature tensile properties of ODS steel claddings under severe accident conditions

    Energy Technology Data Exchange (ETDEWEB)

    Yano, Y., E-mail: yano.yasuhide@jaea.go.jp [Japan Atomic Energy Agency, 4002, Narita-cho, Oarai-machi, Ibaraki, 311-1393 (Japan); Tanno, T.; Oka, H.; Ohtsuka, S.; Inoue, T.; Kato, S.; Furukawa, T.; Uwaba, T.; Kaito, T. [Japan Atomic Energy Agency, 4002, Narita-cho, Oarai-machi, Ibaraki, 311-1393 (Japan); Ukai, S.; Oono, N. [Materials Science and Engineering, Faculty of Engineering, Hokkaido University, N13, W-8, Kita-ku, Sapporo, Hokkaido, 060-8628 (Japan); Kimura, A. [Institute of Advanced Energy, Kyoto University, Gokasho, Uji, Kyoto 611-0011 (Japan); Hayashi, S. [Tokyo Institute of Technology, 2-12-1, Ookayama, Meguro-ku, Tokyo 152-8550 (Japan); Torimaru, T. [Nippon Nuclear Fuel Development Co., Ltd., 2163, Narita-cho, Oarai-machi, Ibaraki, 311-1313 (Japan)

    2017-04-15

    Ultra-high temperature ring tensile tests were performed to investigate the tensile behavior of oxide dispersion strengthened (ODS) steel claddings and wrapper materials under severe accident conditions with temperatures ranging from room temperature to 1400 °C which is close to the melting point of core materials. The experimental results showed that the tensile strength of 9Cr-ODS steel claddings was highest in the core materials at ultra-high temperatures of 900–1200 °C, but there was significant degradation in the tensile strength of 9Cr-ODS steel claddings above 1200 °C. This degradation was attributed to grain boundary sliding deformation with γ/δ transformation, which is associated with reduced ductility. By contrast, the tensile strength of recrystallized 12Cr-ODS and FeCrAl-ODS steel claddings retained its high value above 1200 °C, unlike the other tested materials.

  6. Ultra-high temperature tensile properties of ODS steel claddings under severe accident conditions

    Science.gov (United States)

    Yano, Y.; Tanno, T.; Oka, H.; Ohtsuka, S.; Inoue, T.; Kato, S.; Furukawa, T.; Uwaba, T.; Kaito, T.; Ukai, S.; Oono, N.; Kimura, A.; Hayashi, S.; Torimaru, T.

    2017-04-01

    Ultra-high temperature ring tensile tests were performed to investigate the tensile behavior of oxide dispersion strengthened (ODS) steel claddings and wrapper materials under severe accident conditions with temperatures ranging from room temperature to 1400 °C which is close to the melting point of core materials. The experimental results showed that the tensile strength of 9Cr-ODS steel claddings was highest in the core materials at ultra-high temperatures of 900-1200 °C, but there was significant degradation in the tensile strength of 9Cr-ODS steel claddings above 1200 °C. This degradation was attributed to grain boundary sliding deformation with γ/δ transformation, which is associated with reduced ductility. By contrast, the tensile strength of recrystallized 12Cr-ODS and FeCrAl-ODS steel claddings retained its high value above 1200 °C, unlike the other tested materials.

  7. Temperature and Pressure Dependences of the Elastic Properties of Tantalum Single Crystals Under Tensile Loading: A Molecular Dynamics Study

    Science.gov (United States)

    Li, Wei-bing; Li, Kang; Fan, Kan-qi; Zhang, Da-xing; Wang, Wei-dong

    2018-04-01

    Atomistic simulations are capable of providing insights into physical mechanisms responsible for mechanical properties of the transition metal of Tantalum (Ta). By using molecular dynamics (MD) method, temperature and pressure dependences of the elastic properties of Ta single crystals are investigated through tensile loading. First of all, a comparative study between two types of embedded-atom method (EAM) potentials is made in term of the elastic properties of Ta single crystals. The results show that Ravelo-EAM (Physical Review B, 2013, 88: 134101) potential behaves well at different hydrostatic pressures. Then, the MD simulation results based on the Ravelo-EAM potential show that Ta will experience a body-centered-cubic (BCC) to face-centered-cubic (FCC) phase transition before fracture under tensile loading at 1 K temperature, and model size and strain rate have no obvious effects on tensile behaviors of Ta. Next, from the simulation results at the system temperature from 1 to 1500 K, it can be derived that the elastic modulus of E 100 linearly decrease with the increasing temperature, while the yielding stress decrease with conforming a quadratic polynomial formula. Finally, the pressure dependence of the elastic properties is performed from 0 to 140 GPa and the observations show that the elastic modulus increases with the increasing pressure overall.

  8. Effect of irradiation on the tensile properties of niobium-base alloys

    International Nuclear Information System (INIS)

    Grossbeck, M.L.; Heestand, R.L.; Atkin, S.D.

    1986-11-01

    The alloys Nb-1Zr and PWC-11 (Nb-1Zr-0.1C) were selected as prime candidate alloys for the SP-100 reactor. Since the mechanical properties of niobium alloys irradiated to end-of-life exposure levels of about 2 x 10 26 neutrons/m 2 (E > 0.1 MeV) at temperatures above 1300 K were not available, an irradiation experiment (B-350) in EBR-II was conducted. Irradiation creep, impact properties, bending fatigue, and tensile properties were investigated; however, only tensile properties will be reported in this paper. The tensile properties were studied since they easily reveal the common irradiation phenomena of hardening and embrittlement. Most attention was directed to testing at the irradiation temperature. Further testing was conducted at lower temperatures in order to scope the behavior of the alloys in cooldown conditions

  9. HIGH TEMPERATURE TENSILE PROPERTIES OF NEW FE-CR-MN DEVELOPED STEEL

    Directory of Open Access Journals (Sweden)

    M. Mahmoudiniya

    2017-03-01

    Full Text Available Nowadays, Ni-free austenitic stainless steels are being developed rapidly and high price of nickel is one of the most important motivations for this development. At present research a new FeCrMn steel was designed and produced based on Fe-Cr-Mn-C system. Comparative studies on microstructure and high temperature mechanical properties of  new steel and AISI 316 steel were done. The results showed that new FeCrMn developed steel has single austenite phase microstructure, and its tensile strength and toughness were higher than those of 316 steel at 25, 200,350 and 500°C. In contrast with 316 steel, the new FeCrMn steel did not show strain induced transformation and dynamic strain aging phenomena during tensile tests that represented higher austenite stability of new developed steel. Lower density and higher strength of the new steel caused higher specific strength in comparison with the 316 one that can be considered as an important advantage in structural applications but in less corrosive environment

  10. Characterization of high temperature tensile and creep–fatigue properties of Alloy 800H for intermediate heat exchanger components of (V)HTRs

    Energy Technology Data Exchange (ETDEWEB)

    Kolluri, M., E-mail: kolluri@nrg.eu; Pierick, P. ten, E-mail: tenpierick@nrg.eu; Bakker, T., E-mail: t.bakker@nrg.eu

    2015-04-01

    Highlights: • High temperature tensile, creep–fatigue (C–F) properties of Alloy 800H are studied. • Strength and uniform elongation properties at 800 °C are much lower than RT values. • Strong influence of hold time and Δε{sub tot} on low cycle fatigue life was observed. • The total allowable C–F damage (D) at 800 °C decreases with the decreasing Δε{sub tot}. • Synergetic effect of C–F interactions showed stronger effect at lower Δε{sub tot} values. - Abstract: Alloy 800H is considered as a candidate material for intermediate heat exchanger (IHX) components of (very) high temperature reactors (V)HTRs. Qualification of the this alloy for the aforementioned nuclear applications requires understanding of its high temperature tensile, low-cycle fatigue behavior and creep–fatigue interactions because the IHX components suffer from combined creep–fatigue loadings resulting from thermally induced strain cycles associated with start-up and shutdown cycles. To this end, in this paper, the tensile properties of the Alloy 800H base and tungsten inert gas (TIG) welded materials are studied at three different temperatures, room temperature 21, 700 and 800 °C. Low cycle fatigue (LCF) behavior of the base material is investigated at 800 °C with no-hold time (no-HT) and hold time (HT) to study creep–fatigue interactions. The tensile test results showed substantial differences between the strength and ductility properties of the base and weld materials at all 3 temperatures, however, the trends in temperature dependence of tensile properties are similar for both base and weld materials. LCF studies with no-HT and HT showed a strong influence of HT on the low cycle fatigue life of this alloy illustrating the substantial influence of creep mechanisms at 800 °C. Finally, cumulative values of creep versus fatigue damage fractions are plotted in a creep–fatigue interaction diagram and these results are discussed with respect to the existing bi

  11. Tensile-property characterization of thermally aged cast stainless steels

    International Nuclear Information System (INIS)

    Michaud, W.F.; Toben, P.T.; Soppet, W.K.; Chopra, O.K.

    1994-02-01

    The effect of thermal aging on tensile properties of cast stainless steels during service in light water reactors has been evaluated. Tensile data for several experimental and commercial heats of cast stainless steels are presented. Thermal aging increases the tensile strength of these steels. The high-C Mo-bearing CF-8M steels are more susceptible to thermal aging than the Mo-free CF-3 or CF-8 steels. A procedure and correlations are presented for predicting the change in tensile flow and yield stresses and engineering stress-vs.-strain curve of cast stainless steel as a function of time and temperature of service. The tensile properties of aged cast stainless steel are estimated from known material information, i.e., chemical composition and the initial tensile strength of the steel. The correlations described in this report may be used for assessing thermal embrittlement of cast stainless steel components

  12. Tensile properties of unirradiated path A PCA

    International Nuclear Information System (INIS)

    Braski, D.N.; Maziasz, P.J.

    1983-01-01

    The tensile properties of PCA in the Al (solution annealed), A3 (25%-cold worked), and B2 (aged, cold worked, and reaged) conditions were determined from room temperature to 600 0 C. The tensile behavior of PCA-A1 and -A3 was generally similar to that of titanium-modified type 316 stainless steel with similar microstructures. The PCA-B2 was weaker than PCA-A3, especially above 500 0 C, but demonstrated slightly better ducility

  13. Tensile properties of orthodontic elastomeric ligatures.

    Science.gov (United States)

    Ahrari, F; Jalaly, T; Zebarjad, M

    2010-01-01

    Tensile properties of elastomeric ligatures become important when efficiency of orthodontic appliances is considered. The aim of this study was to compare tensile strength, extension to tensile strength, toughness and modulus of elasticity of elastomeric ligatures in both the as--received condition and after 28 days of immersion in the simulated oral environment. Furthermore, the changes that occurred in tensile properties of each brand of ligatures after 28 days were evaluated. Experimental-laboratory based. Elastomeric ligatures were obtained from different companies and their tensile properties were measured using Zwick testing machine in both the as-received condition and after 28 days of immersion in the simulated oral environment. The data were analyzed using independent sample t-tests, analysis of variance and Tukey tests. After 28 days, all the ligatures experienced a significant decrease in tensile strength, extension to tensile strength and toughness ( P tensile properties of different brands of ligatures in both conditions ( P tensile properties of different brands of ligatures, which should be considered during selection of these products.

  14. High temperature tensile properties of 316 stainless steel implanted with helium

    International Nuclear Information System (INIS)

    Hasegawa, Akira; Yamamoto, Norikazu; Shiraishi, Haruki

    1993-01-01

    Helium embrittlement is one of the problems in structural materials for fusion reactors. Recently, martensitic steels have been developed which have a good resistance to high-temperature helium embrittlement, but the mechanism has not yet been clarified. In this paper, tensile behaviors of helium implanted austenitic stainless steels, which are sensitive to the helium embrittlement, were studied and compared with those of martensitic steels under the same experimental conditions, and the effect of microstructure on helium embrittlement was discussed. Helium was implanted by 300 appm at 573-623 K to miniature tensile speciments of 316 austenitic steels using a cyclotron accelerator. Solution annealed (316SA) and 20% cold worked (316CW) specimens were used. Post-implantation tensile tests were carried out at 573, 873 and 973 K. Yield stress at 573 K increased with the helium implantation in 316SA and 316CW, but the yield stress changes of 316SA at 873 and 973 K were different from that of 316CW. Black-dots were observed in the as-implanted specimen and bubbles were observed in the speciments tensile-tested at 873 and 973 K. Intergranular fracture was observed at only 973 K in both of the 316SA and 316CW specimens. Therefore, cold work did not suppress the high-temperature helium embrittlement under this experimental condition. The difference in the influence of helium on type 316 steel and 9Cr martensitic steels were discussed. Test temperature change of reduction in are showed clearly that helium embrittlement did not occur in 9Cr martensitic steels but occurred in 316 austenitic steels. Fine microstructures of 9Cr martensitic steels should suppress helium embrittlement at high temperatures. (author)

  15. Tensile testing and damage analysis of woven glass-cloth/epoxy laminates at low temperature

    International Nuclear Information System (INIS)

    Kumagai, S.; Shindo, Y.; Horiguchi, K.

    2002-01-01

    In order to evaluate the tensile properties of SL-ES30 glass-cloth/epoxy laminates for superconducting magnets in fusion energy systems, tensile tests were examined both experimentally and analytically. The tensile tests were conducted in accordance with JIS K 7054 at room temperature and liquid nitrogen temperature (77 K). The general specimen geometry was a rectangular dog-bone shape with constant gage length, but with each specimen size having a different specimen width. The experimental finding provides the data for analytical modeling. The model utilizes two damage variables which are determined from experimental data. A finite element method coupled with damage was adopted for the extensional analysis. The effects of temperature, specimen geometry and gripping method on the tensile properties are examined

  16. Tensile properties and temperature-dependent yield strength prediction of GH4033 wrought superalloy

    Energy Technology Data Exchange (ETDEWEB)

    Ma, Jianzuo [State Key Laboratory of Coal Mine Disaster Dynamics and Control and College of Aerospace Engineering, Chongqing University, Chongqing 400030 (China); Li, Weiguo, E-mail: wgli@cqu.edu.cn [State Key Laboratory of Coal Mine Disaster Dynamics and Control and College of Aerospace Engineering, Chongqing University, Chongqing 400030 (China); Zhang, Xianhe; Kou, Haibo; Shao, Jiaxing; Geng, Peiji; Deng, Yong [State Key Laboratory of Coal Mine Disaster Dynamics and Control and College of Aerospace Engineering, Chongqing University, Chongqing 400030 (China); Fang, Daining [LTCS and College of Engineering, Peking University, Beijing 100871 (China)

    2016-10-31

    The tensile properties of superalloy GH4033 have been evaluated at temperatures ranging from room temperature to 1000 °C. Fracture surfaces and precipitation were observed using a field-emission scanning electron microscope (FE-SEM). The alloy mainly consisted of γ’ precipitate particles homogeneously dispersed in the γ matrix interior. The effects of dynamic strain aging and precipitation on the strength were verified. A temperature-dependent yield strength model was developed to describe the temperature and precipitation effects on the alloy's yield behaviour. The model is able to consider the effect of precipitation strengthening on the yield strength. The yield behaviour of the precipitation-strengthened superalloy was demonstrated to be adequately predictable over a wide range of temperatures. Note that this model reflects the quantitative relationship between the yield strength of the precipitation-strengthened superalloy and the temperature, the elastic modulus, the specific heat capacity at constant pressure, Poisson's ratio, the precipitate particle size and the volume fraction of the particles.

  17. Tensile Properties and Fracture Behavior of a Powder-Thixoformed 2024Al/SiCp Composite at Elevated Temperatures

    Directory of Open Access Journals (Sweden)

    Pubo Li

    2017-10-01

    Full Text Available In the present work, the tensile properties and fracture behavior of a 2024Al composite reinforced with 10 vol % SiCp and fabricated via powder thixoforming (PT were studied at temperatures ranging from 25 °C to 300 °C with a strain rate of 0.05 s−1, as well as the PT 2024 alloy. The results indicated that the tensile strengths of both the PT materials were all decreased with increasing the temperature, but the decrease rate of the composite was smaller than that of the 2024 alloy, and the composite exhibited higher tensile strength than that of the 2024 alloy at all of the employed testing temperatures due to the strengthening role of SiCp. Increasing temperature was beneficial for enhancing the ductility of materials, and the maximum elongation was reached at 250 °C. The elongation decrease over 250 °C was attributed to the cavity formation due to the debonding of the SiCp/Al interface and the fracturing of the matrix between SiCp. The fracture of the composite at room temperature initiated from the fracture of SiCp and the debonding of the SiCp/Al interface, but that at high temperatures was dominated by void nucleation and growth in the matrix besides the interface debonding.

  18. Correlation of hot-microhardness with elevated-temperature tensile properties of low activation ferritic steel

    International Nuclear Information System (INIS)

    Hsu Chenyih

    1986-01-01

    Hot microhardness and elevated temperature tensile tests have been performed on 9Cr-2.5W-0.3V-0.15C(GA3X) low activation ferritic steel at temperatures from 20 0 C to 650 0 C. The uniform elongation of the tensile test correlated well with the ductility parameter of the microhardness test. The hot-microhardness test showed a sensitive response to the softening and changes in ductility of the GA3X steel. The ultimate tensile strength and 0.2% yield strength of this steel correlated well with hot microhardness data at test temperatures up to 400 0 C using Cahoon's expressions σ uts = (H/2.9)(n/0.217) n and σ ys = (H/3)(0.1) n , respectively, where H is the diamond pyramid hardness and n is the strain hardening exponent. A 20-30% underestimate of tensile strengths were obtained using Cahoon's expressions at temperatures above 400 0 C, which is probably attributed to creep deformation and may be improved by selecting a proper loading condition during the hardness test. (orig.)

  19. Influence of processing parameters on microstructure and tensile properties of TG6 titanium alloy

    International Nuclear Information System (INIS)

    Wang Tao; Guo Hongzhen; Wang Yanwei; Yao Zekun

    2010-01-01

    Research highlights: → This paper highlights the relationships among processing parameters, microstructure and tensile properties of TG6 high temperature titanium alloy. → The microstructural evolutions under different processing parameters were studied by the quantitative metallography, and the effects of microstructure on room and high temperature tensile properties of TG6 alloy were analysed by SEM and TEM. → Linear relationships of elongation vs. volume fraction of primary α phase and ultimate tensile strength vs. thickness of lamellar α phase were determined. - Abstract: Near-isothermal forging of the TG6 titanium alloy was conducted on microprocessor-controlled 630 ton hydraulic press at the deformation temperatures ranging from 850 deg. C to 1045 deg. C, the strain rates of 0.0008 s -1 , 0.003 s -1 and 0.008 s -1 and the deformation degree from 10% to 70%, and then different double heat treatments were applied to the forged specimens. The microstructural evolutions were researched by optical microscope and the microstructural features, i.e. volume fraction of primary α phase and thickness of lamellar α phase, were measured by means of the image analysis software. The room and high temperature tensile properties were obtained for all the specimens. Effects of microstructure on the properties were analysed by scanning electronic microscope. It was found that tenslie properties depended on microstructural features strongly. The plots of ultimate tensile strength vs. thickness of α lamellae and elongation vs. volume fraction of primary α phase produced straight lines. The liner equations were determined by fitting the experimental date, respectively. Compared to other parameters, heat treatment had more influence on the tensile strength and the tensile plasticity was more sensitive to the forging temperature.

  20. Elevated-temperature tensile properties of three heats of commercially heat-treated Alloy 718

    International Nuclear Information System (INIS)

    Booker, M.K.; Booker, B.L.P.

    1980-03-01

    Three heats of commercially heat-treated alloy 718 were tensile tested over the temperature range from room temperature to 816 degree C and at nominal strain rates from 6.7 x 10 -6 to 6.7 x 10 -3 /s. We examined data for yield strength, ultimate tensile strength, uniform elongation, total elongation, and reduction in area and also inspected tensile stress-strain behavior. Yield and ultimate tensile strengths for commercially heat-treated alloy 718 decrease very gradually with temperature from room temperature up to about 600 degree C for a strain rate of 6.7 x 10 -5 /s or to about 700 degree C for a strain rate of 6.7 x 10 -4 /s. Above these temperatures the strength drops off fairly rapidly. Reduction in area and total elongation data show minimum around 700 degree C, with each ductility measure falling to 10% or less at the minimum. This minimum is more pranced and occurs at lower temperatures as strain rate decreases. Up to about 600 degree C the ductility is typically around 30%. As the temperature reaches 816 degree C the ductility again increases to perhaps 60%. The uniform elongation (plastic strain at peak load) decreases only slightly with temperature to about 500 degree C then drops off rapidly and monotonically with temperature, reaching values less than 1% at 816 degree C. At the highest test temperatures the load maximum may result, not from necking of the specimen, but from overaging of the precipitation-hardened microstructure. Stress-strain curves showed serrated deformations in the temperature range from 316 to 649 degree C, although they occur only for the faster strain rates at the supper end of this temperature range. The serrations can be quite large, involving load drops of perhaps 40 to 80 MPa. The serrations typically begin within the first 2% of deformation and continue until fracture, although exceptions were noted. 16 refs., 14 figs., 3 tabs

  1. Tensile properties of strip casting 6.5 wt% Si steel at elevated temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Li, Hao-Ze, E-mail: lhzqq83@163.com; Liu, Zhen-Yu, E-mail: zyliu@mail.neu.edu.cn

    2015-07-15

    Tensile behaviors of strip casting 6.5 wt% Si steel are tested at elevated temperatures ranging from 300 °C to 800 °C. A detailed study of the morphology of the fracture surface and the ordered phase at each deforming temperature is carried out by a scanning electron microscope and a transmission electron microscope. The results show that the deforming temperature rather than the ordered degree determines the tensile properties. As the deforming temperature increases, the stress level in the whole deforming stage continually decreases, whereas the elongation gradually increases. The ductile–brittle transition occurs around 350 °C. The elongation of 2% at 300 °C rapidly increases up to 16.4% at 350 °C and the corresponding fracture mode transforms from the complete cleavage fracture to the mixture of the very limited cleavage fracture, intergranular dimple fracture and the dimple fracture. Serrated flow is observed at 350 °C and 400 °C probably due to the occurrence of dynamic strain aging. Due to the gradually weakened grain boundary cohesion with the deforming temperature increasing, intergranular dimple pattern dominates the fracture surface at 600 °C and the elongation slowly increases from 16.4% at 350 °C to 22.8% at 600 °C. At 700 °C and 800 °C, the much more enhanced dynamic recovery, the substantially decreased stress levels which contribute to the inhibition of the intergranular dimple fracture, the much lower content of the B2 ordered phase at 700 °C, and the completely disordered state at 800 °C give rise to the dramatically improved elongations of 88.8% and 130.8%, respectively.

  2. Effects of annealing on tensile property and corrosion behavior of Ti-Al-Zr alloy

    International Nuclear Information System (INIS)

    Kim, Tae-Kyu; Choi, Byung-Seon; Jeong, Yong-Hwan; Lee, Doo-Jeong; Chang, Moon-Hee

    2002-01-01

    The effects of annealing on the tensile property and corrosion behavior of Ti-Al-Zr alloy were evaluated. The annealing in the temperature range from 500 to 800 deg. C for 1 h induced the growth of the grain and the precipitate sizes. The results of tensile tests at room temperature showed that the strengths and the ductility were almost independent of the annealing temperature. However, the results of corrosion test in an ammonia aqueous solution of pH 9.98 at 360 deg. C showed that the corrosion resistance depended on the annealing temperature, and the corrosion rate was accelerated with increasing annealing temperature. Hydrogen contents absorbed during the corrosion test of 220 days also increased with the annealing temperature. It could be attributed to the growth of Fe-rich precipitates by annealing. It is thus suggested that the lower annealing temperatures provide the better corrosion properties without degrading the tensile properties

  3. Effect of tungsten on tensile properties and flow behaviour of RAFM steel

    Energy Technology Data Exchange (ETDEWEB)

    Vanaja, J., E-mail: jvanaja@igcar.gov.in [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India); Laha, K.; Nandagopal, M. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India); Sam, Shiju [Institute for Plasma Research, Gandhinagar 382 428, Gujarat (India); Mathew, M.D.; Jayakumar, T. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India); Rajendra Kumar, E. [Institute for Plasma Research, Gandhinagar 382 428, Gujarat (India)

    2013-02-15

    Effect of tungsten in the range of 1–2 wt.% on tensile properties and flow behaviour of 9Cr–W–Ta–V Reduced Activation Ferritic–Martensitic (RAFM) steel has been investigated. The tungsten in the investigated range was found to have only minor effect on the tensile properties of the steel over the temperature range of 300–873 K and at a strain rate of 3 × 10{sup −3} s{sup −1}. The tensile flow behaviour of the RAFM steels was adequately described by the Voce’s constitutive equation. The tensile strength of the steels were predicted well from the parameters of the Voce’s constitutive equation. The Voce’s strain hardening parameter ‘n{sub v}’ was found to be quite sensitive to the tungsten content and predicted the onset of dislocation climbing process at relatively higher testing temperature with the increase in tungsten content. The equivalence between tensile and creep deformations and the influence of tungsten have been discussed.

  4. Effect of tungsten on tensile properties and flow behaviour of RAFM steel

    International Nuclear Information System (INIS)

    Vanaja, J.; Laha, K.; Nandagopal, M.; Sam, Shiju; Mathew, M.D.; Jayakumar, T.; Rajendra Kumar, E.

    2013-01-01

    Effect of tungsten in the range of 1–2 wt.% on tensile properties and flow behaviour of 9Cr–W–Ta–V Reduced Activation Ferritic–Martensitic (RAFM) steel has been investigated. The tungsten in the investigated range was found to have only minor effect on the tensile properties of the steel over the temperature range of 300–873 K and at a strain rate of 3 × 10 −3 s −1 . The tensile flow behaviour of the RAFM steels was adequately described by the Voce’s constitutive equation. The tensile strength of the steels were predicted well from the parameters of the Voce’s constitutive equation. The Voce’s strain hardening parameter ‘n v ’ was found to be quite sensitive to the tungsten content and predicted the onset of dislocation climbing process at relatively higher testing temperature with the increase in tungsten content. The equivalence between tensile and creep deformations and the influence of tungsten have been discussed

  5. Tensile properties and impact toughness of S30408 stainless steel and its welded joints at cryogenic temperatures

    Science.gov (United States)

    Ding, Huiming; Wu, Yingzhe; Lu, Qunjie; Xu, Ping; Zheng, Jinyang; Wei, Lijun

    2018-06-01

    Designing a cryogenic pressure vessel based on the mechanical properties of the austenitic stainless steel (ASS) at its cryogenic operating temperature fully utilizes the potential of the material at low temperatures, resulting in lightweight and compact products. A series of tensile tests and impact tests were carried out in a wide range of 77-293 K, to investigate the mechanical properties of S30408 base metal (BM) and welded joints (WJ) at cryogenic temperatures. As the temperature decreases, yield stress (Rp0.2) and ultimate tensile stress (Rm) increase significantly thanks to the low-temperature strengthening effects. To estimate strengths at cryogenic temperatures, quadratic polynomial model was used to accurately predict the variations of Rp0.2 and Rm from 77 K to 293 K. As an important phase in the WJ, ferrite presents a radial pattern and an inhomogeneity in the WJ's cross-section. Due to the formation of ferrite in the WJ, the WJ has higher Rp0.2 and lower Rm , Charpy absorbed energy and lateral expansion compared with the BM. Strain-induced martensite transformation is an important role influencing the deformation of ASS at low temperatures. In this study, less martensite amount was measured in the weldment zone with higher Nickel equivalents which stabilize the austenite phase at cryogenic temperatures. Additionally, due to higher ferrite content and more precipitates forming, the SAW joints has lower Rm and impact toughness than PAW + GTAW joints. To ensure the structural integrity and safety, the PAW + GTAW method should be chosen and ferrite content be controlled.

  6. Tensile properties of in situ synthesized titanium matrix composites reinforced by TiB and Nd2O3 at elevated temperature

    International Nuclear Information System (INIS)

    Geng Ke; Lu Weijie; Zhang Di; Sakata, Taokao; Mori, Hirotaro

    2003-01-01

    Titanium matrix composites reinforced with TiB and Nd 2 O 3 were prepared by a non-consumable arc-melting technology. X-ray diffraction (XRD) was used to identify the phases in the composites. Microstructures of the composites were observed by means of optical microscope (OM). There are three phases: TiB, Nd 2 O 3 and titanium matrix. TiB grows in needle shape, whereas Nd 2 O 3 grows in lath shape. Tensile properties of the composites were tested at 773, 823 and 873 K. Both the fracture surfaces and longitudinal sections of the fractured tensile specimens were comprehensively examined by scanning electron microscope (SEM). The fracture mode and fracture process at different temperatures were analyzed and explained. It shows that the tensile strength of the composites has a significant improvement at elevated temperatures compared to titanium matrix. The ductility of the composites improves with the content of neodymium and the test temperatures. The titanium composite exhibits different fracture modes at different test temperatures

  7. Effects of strain rate, test temperature and test environment on tensile properties of vandium alloys

    International Nuclear Information System (INIS)

    Gubbi, A.N.; Rowcliffe, A.F.; Eatherly, W.S.; Gibson, L.T.

    1996-01-01

    Tensile testing was carried out on SS-3 tensile specimens punched from 0.762-mm-thick sheets of the large heat of V-4Cr-4Ti and small heats of V-3Cr-3Ti and V-6Cr-6Ti. The tensile specimens were annealed at 1000 degrees for 2 h to obtain a fully recrystallized, fine grain microstructure with a grain size in the range of 10-19 μm. Room temperature tests at strain rates ranging from 10 -3 to 5 x 10 -1 /s were carried out in air; elevated temperature testing up to 700 degrees C was conducted in a vacuum better than 1 x 10 -5 torr ( -3 Pa). To study the effect of atomic hydrogen on ductility, tensile tests were conducted at room temperature in an ultra high vacuum chamber (UHV) with a hydrogen leak system

  8. Effects of strain rate, test temperature and test environment on tensile properties of vandium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Gubbi, A.N.; Rowcliffe, A.F.; Eatherly, W.S.; Gibson, L.T. [Oak Ridge National Lab., TN (United States)

    1996-10-01

    Tensile testing was carried out on SS-3 tensile specimens punched from 0.762-mm-thick sheets of the large heat of V-4Cr-4Ti and small heats of V-3Cr-3Ti and V-6Cr-6Ti. The tensile specimens were annealed at 1000{degrees} for 2 h to obtain a fully recrystallized, fine grain microstructure with a grain size in the range of 10-19 {mu}m. Room temperature tests at strain rates ranging from 10{sup {minus}3} to 5 x 10{sup {minus}1}/s were carried out in air; elevated temperature testing up to 700{degrees}C was conducted in a vacuum better than 1 x 10{sup {minus}5} torr (<10{sup {minus}3} Pa). To study the effect of atomic hydrogen on ductility, tensile tests were conducted at room temperature in an ultra high vacuum chamber (UHV) with a hydrogen leak system.

  9. The influence of temperature on the tensile properties of a super duplex stainless steel

    International Nuclear Information System (INIS)

    Girones, A.; Mateo, A.; Llanes, L.; Anglada, M

    2001-01-01

    Tensile tests, at temperatures ranging between 275 and 475 degree centigree were performed in a superduplex stainless steel EN 1.4410. The dependence of yield stress and ultimate tensile strength on temperature indicates the existence of dynamic strain aging (DSA). In order to evaluate the influence of strain rate on this phenomenon, tests were conducted at two different strain rates, both at 325 degree centigree, temperature at which DSA is maximum for this materials. The results shows that the flow stress has an inverse strain rate sensitivity which confirms the existence of DSA in the steel under study. (Author) 10 refs

  10. Mechanical Properties of Weakly Segregated Block Copolymers. 3. Influence of Strain Rate and Temperature on Tensile Properties of Poly(styrene-b-butyl methacrylate) Diblock Copolymers with Different Morphologies

    NARCIS (Netherlands)

    Weidisch, R.; Stamm, M.; Michler, G.H.; Fischer, H.R.; Jérôme, R.

    1999-01-01

    Poly(styrene-b-butyl methacrylate) diblock copolymers, PS-6-PBMA, with different morphologies are investigated with respect to the influence of strain rate and temperature on tensile properties. In the first part the mechanical properties of bicontinuous and perforated lamellar structure are

  11. Mechanical Tensile Testing of Titanium 15-3-3-3 and Kevlar 49 at Cryogenic Temperatures

    Science.gov (United States)

    James, Bryan L.; Martinez, Raul M.; Shirron, Peter; Tuttle, Jim; Galassi, Nicholas M.; Mcguinness, Daniel S.; Puckett, David; Francis, John J.; Flom, Yury

    2011-01-01

    Titanium 15-3-3-3 and Kevlar 49 are highly desired materials for structural components in cryogenic applications due to their low thennal conductivity at low temperatures. Previous tests have indicated that titanium 15-3-3-3 becomes increasingly brittle as the temperature decreases. Furthermore, little is known regarding the mechanical properties of Kevlar 49 at low temperatures, most specifically its Young's modulus. This testing investigates the mechanical properties of both materials at cryogenic temperatures through cryogenic mechanical tensile testing to failure. The elongation, ultimate tensile strength, yield strength, and break strength of both materials are provided and analyzed here.

  12. The influences of anneal temperature and cooling rate on microstructure and tensile properties of laser deposited Ti–4Al–1.5Mn titanium alloy

    International Nuclear Information System (INIS)

    Tian, X.J.; Zhang, S.Q.; Wang, H.M.

    2014-01-01

    Highlights: • We study the heat treatment parameters of laser deposited near-α titanium alloy. • Microstructure/tensile property relationships are demonstrated and discussed. • Higher cooling rate leads to finer microstructure and higher strength. • Higher anneal temperature promotes strength without ductility obviously decreased. - Abstract: As a metal near-net-shape manufacturing technology, direct laser fabrication has a great potential to reduce costs and delivery time and received an intense attention in the field of titanium alloy aerospace components fabrications. However, the laser deposited titanium alloys usually have equivalent strength and lower ductility compared to the wrought counterparts due to their lamellar microstructure. To investigate the responses of laser deposit titanium alloy Ti–4Al–1.5Mn to anneal parameters, various anneal temperatures and cooling rates were applied in this study. Microstructures were examined by Optical Microscope (OM) and Scanning Electron Microscope (SEM). Microhardness test and room temperature tensile tests were employed to evaluate the tensile properties of the as-deposited and annealed specimens. Results show that air cooling from the α + β phase region generates a microstructure composed of coarse primary α plates and fine lamellar transformed β, while water quenching produces similar but much finer microstructure. Moreover, higher cooling rate generates more area fraction of fine transformed β. With increasing anneal temperature, the ultimate tensile strength and yield strength increase for both cooling methods. Moreover, higher cooling rate leads to higher strength as expected. It is worth noting that both the strength and ductility of the laser deposited alloy improved by water quenched from the α + β duplex phase region. The improved tensile properties were mainly owing to the fine lamellar transformed β in the special bimodal microstructure

  13. Tensile behaviour of radiata pine with different moisture contents at elevated temperatures

    DEFF Research Database (Denmark)

    Pearson, Hamish; Gabbitas, Brian; Ormarsson, Sigurdur

    2012-01-01

    that moisture and temperature can play a significant role in reducing stress during drying, regardless of the drying time. Properties of wood, such as tensile elastic information at elevated temperatures, are important for mechanical design, distortion modelling and understanding the fundamental behaviour...

  14. Influence of thermal conditions on the tensile properties of basalt fiber reinforced polypropylene–clay nanocomposites

    International Nuclear Information System (INIS)

    Eslami-Farsani, Reza; Reza Khalili, S. Mohammad; Hedayatnasab, Ziba; Soleimani, Neda

    2014-01-01

    Highlights: • We studied tensile properties of basalt fiber/nanoclay-polypropylene (BF–PPCN). • Addition of nanoclay improves the yield strength and Young’s modulus of BF–PPCN. • The tensile properties of BF–PPCN are high at low temperature (−196 °C). - Abstract: In this paper, a comparative study on the tensile properties of clay reinforced polypropylene (PP) nanocomposites (PPCN) and chopped basalt fiber reinforced PP–clay nanocomposites (PPCN-B) is presented. PP matrix are filled with 1, 3 and 5 wt.% of nanoclays. The ultimate tensile strength, yield strength, Young’s modulus and toughness are measured at various temperature conditions. The thermal conditions are included the room temperature (RT), low temperature (LT) and high temperature (HT). The basal spacing of clay in the composites is measured by X-ray diffraction (XRD). Nanoscale morphology of the samples is observed by transmission electron microscopy (TEM). Addition of nanoclay improves the yield strength and Young’s modulus of PPCN and PPCN-B; however, it reduces the ultimate tensile strength. Furthermore, the addition of chopped basalt fibers to PPCN improves the Young’s modulus of the composites. The Young’s modulus and the yield strength of both PPCN and PPCN-B are significantly high at LT (−196 °C), descend at RT (25 °C) and then low at HT (120 °C)

  15. High temperature tensile testing of modified 9Cr-1Mo after irradiation with high energy protons

    International Nuclear Information System (INIS)

    Toloczko, M.B.; Hamilton, M.L.; Maloy, S.A.

    2003-01-01

    This study examines the effect of tensile test temperatures ranging from 50 to 600 deg. C on the tensile properties of a modified 9Cr-1Mo ferritic steel after high energy proton irradiation at about 35-67 deg. C to doses from 1 to 3 dpa and 9 dpa. For the specimens irradiated to doses between 1 and 3 dpa, it was observed that the yield strength and ultimate strength decreased monotonically as a function of tensile test temperature, whereas the uniform elongation (UE) remained at approximately 1% for tensile test temperatures up to 250 deg. C and then increased for tensile test temperatures up to and including 500 deg. C. At 600 deg. C, the UE was observed to be less than the values at 400 and 500 deg. C. UE of the irradiated material tensile tested at 400-600 deg. C was observed to be greater than the values for the unirradiated material at the same temperatures. Tensile tests on the 9 dpa specimens followed similar trends

  16. Experimental Analysis of Tensile Mechanical Properties of Sprayed FRP

    Directory of Open Access Journals (Sweden)

    Zhao Yang

    2016-01-01

    Full Text Available To study the tensile mechanical properties of sprayed FRP, 13 groups of specimens were tested through uniaxial tensile experiments, being analyzed about stress-strain curve, tensile strength, elastic modulus, breaking elongation, and other mechanical properties. Influencing factors on tensile mechanical properties of sprayed FRP such as fiber type, resin type, fiber volume ratio, fiber length, and composite thickness were studied in the paper too. The results show that both fiber type and resin type have an obvious influence on tensile mechanical properties of sprayed FRP. There will be a specific fiber volume ratio for sprayed FRP to obtain the best tensile mechanical property. The increase of fiber length can lead to better tensile performance, while that of composite thickness results in property degradation. The study can provide reference to popularization and application of sprayed FRP material used in structure reinforcement.

  17. Temperature Effects on Tensile and Compressive Mechanical Behaviors of C-S-H Structure via Atomic Simulation

    Directory of Open Access Journals (Sweden)

    Hao Xin

    2017-01-01

    Full Text Available An atomic scale model of amorphous calcium silicate hydrate (C-S-H with Ca/Si ratio of 1.67 is constructed. Effects of temperature on mechanical properties of C-S-H structure under tensile and compressive loading in the layered direction are investigated via molecular dynamics simulations. Results from present simulations show that (1 the tensile strength and Young’s modulus of C-S-H structure significantly decrease with the increase of the temperature; (2 the water layer plays an important role in the mechanical properties of C-S-H structure; (3 the compressive strength is stronger than tensile strength, which corresponds with the characteristic of cement paste.

  18. Measurement of tensile and fracture toughness properties using small punch test

    International Nuclear Information System (INIS)

    Chatterjee, S.; Shah Priti Kotak

    2005-05-01

    Small punch test wu carried out at room temperature on five different steels using 10 mm by 10 mm specimens of 0.4 mm thickness in a univesal testing machine. The tensile and fracture toughness properties of the five steels obtained from small punch test were compared with those obtained from the standard test method. The results (except in one steel) show that the tensile properties obtained from small punch test are in close proximity to those obtained ftom uni-axial tension test. The results also show that fracture toughness (Jic) properties obtained ftom small punch test are within ±20% of the corresponding values obtained using standard test procedures. (author)

  19. Residual Tensile Property of Plain Woven Jute Fiber/Poly(Lactic Acid) Green Composites during Thermal Cycling.

    Science.gov (United States)

    Katogi, Hideaki; Takemura, Kenichi; Akiyama, Motoki

    2016-07-14

    This study investigated the residual tensile properties of plain woven jute fiber reinforced poly(lactic acid) (PLA) during thermal cycling. Temperature ranges of thermal cycling tests were 35-45 °C and 35-55 °C. The maximum number of cycles was 10³ cycles. The quasi-static tensile tests of jute fiber, PLA, and composite were conducted after thermal cycling tests. Thermal mechanical analyses of jute fiber and PLA were conducted after thermal cycling tests. Results led to the following conclusions. For temperatures of 35-45 °C, tensile strength of composite at 10³ cycles decreased 10% compared to that of composite at 0 cycles. For temperatures of 35-55 °C, tensile strength and Young's modulus of composite at 10³ cycles decreased 15% and 10%, respectively, compared to that of composite at 0 cycles. Tensile properties and the coefficient of linear expansion of PLA and jute fiber remained almost unchanged after thermal cycling tests. From observation of a fracture surface, the length of fiber pull out in the fracture surface of composite at 10³ cycles was longer than that of composite at 0 cycles. Therefore, tensile properties of the composite during thermal cycling were decreased, probably because of the decrease of interfacial adhesion between the fiber and resin.

  20. Tensile properties of Zr-2.5 Nb pressure tube alloy between 25 and 800 degC

    International Nuclear Information System (INIS)

    Singh, R.N.; Kishore, R.; Sinha, T.K.; Banerjee, S.

    2000-10-01

    Tensile properties of zirconium-2.5 wt. % niobium pressure tube material were evaluated by uniaxial tension tests at temperatures between 25 and 800 degC and under strain-rates varying from 3.3 x 10 -5 to 3.3 x 10 -3 /s. Tests were carried out on specimens fabricated from the sections of finished (autoclaved) tubes as well as on those machined from the sections of cold worked (2 nd pilgered) tubes. Moreover, specimens fabricated from finished tubes belonging to twenty different heats were tested at 300 degC to study the heat to heat variation in tensile properties of this alloy. In order to study the effect of the crystallographic texture on the tensile properties, specimens oriented in longitudinal as well as, in transverse directions of the tubes were also tested. Results showed that both yield and ultimate tensile strengths of this alloy decreased monotonically with increasing test temperatures, with a rapid fall in strengths above a temperature of 350 degC (623 K). The tensile ductility did not change appreciably up to 400 degC (673K) but increased rapidly above this temperature. The observed results on the temperature dependence of the strength and ductility indicated the possible occurrence of dynamic strain-ageing in this alloy in the temperature range of 200-300 degC (473 to 573 K). The transverse specimens showed higher strengths and lower ductility as compared to those of the longitudinal specimens up to a temperature of 350 degC (623 K). Above 350 degC, the difference in the strengths and the ductility of the two types of the specimens, became negligibly small indicating that the texture did not appreciably influence the tensile properties of this alloy at temperatures exceeding 350 degC. The alloy developed extensive superplasticity (ductility exceeding 100 %), when tested in the temperature range of 650-800 degC. Maximum ductility values of 650 % for longitudinal and 900 % for the transverse orientation with strain-rate sensitivity (m) exceeding 0

  1. High strain rate tensile properties of annealed 2 1/4 Cr--1 Mo steel

    International Nuclear Information System (INIS)

    Klueh, R.L.; Oakes, R.E. Jr.

    1975-01-01

    The high strain rate tensile properties of annealed 2 1 / 4 Cr-1 Mo steel were determined and the tensile behavior from 25 to 566 0 C and strain rates of 2.67 x 10 -6 to 144/s were described. Above 0.1/s at 25 0 C, both the yield stress and the ultimate tensile strength increased rapidly with increasing strain rate. As the temperature was increased, a dynamic strain aging peak appeared in the ultimate tensile strength-temperature curves. The peak height was a maximum at about 350 0 C and 2.67 x 10 -6 /s. With increasing strain rate, a peak of decreased height occurred at progressively higher temperatures. The major effect of strain rate on ductility occurred at elevated temperatures, where a decrease in strain rate caused an increase in total elongation and reduction in area

  2. Microstructure and tensile properties of in situ synthesized (TiB+Y2O3)/Ti composites at elevated temperature

    International Nuclear Information System (INIS)

    Geng Ke; Lu Weijie; Zhang Di

    2003-01-01

    A novel titanium matrix composites reinforced with TiB and rare earth oxides (Y 2 O 3 ) were prepared by a non-consumable arc-melting technology. Microstructures of the composites were observed by means of optical microscope (OM) and transmission electron microscope (TEM). X-ray diffraction (XRD) was used to identify the phases in the composites. There are three phases: TiB, Y 2 O 3 and titanium matrix alloy. TiB grows in needle shape, whereas Y 2 O 3 grows from near-equiaxed shape to dendritic shape with increase of yttrium content in the composite. The interfaces between reinforcements and titanium matrix are very clear. There is no interfacial reaction. Tensile properties of the composites were tested at 773, 823 and 873 K. Both the fracture surfaces and longitudinal sections of the fractured tensile specimens were comprehensively examined by scanning electron microscope (SEM). The fracture mode and fracture process at different temperatures were analyzed and explained. The results show that the tensile strength of the composites has a significant improvement at elevated temperatures. The predominant fracture mode of composites is cleavaged at 773 and 823 K. Fracture occurs by ductile failure at 873 K

  3. Residual Tensile Strength and Bond Properties of GFRP Bars after Exposure to Elevated Temperatures

    Directory of Open Access Journals (Sweden)

    Devon S. Ellis

    2018-02-01

    Full Text Available The use of fiber reinforced polymer (FRP bars in reinforced concrete members enhances corrosion resistance when compared to traditional steel reinforcing bars. Although there is ample research available on the behavior of FRP bars and concrete members reinforced with FRP bars under elevated temperatures (due to fire, there is little published information available on their post-fire residual load capacity. This paper reports residual tensile strength, modulus of elasticity, and bond strength (to concrete of glass fiber reinforced polymer (GFRP bars after exposure to elevated temperatures of up to 400 °C and subsequent cooling to an ambient temperature. The results showed that the residual strength generally decreases with increasing temperature exposure. However, as much as 83% of the original tensile strength and 27% of the original bond strength was retained after the specimens were heated to 400 °C and then cooled to ambient temperature. The residual bond strength is a critical parameter in post-fire strength assessments of GFRP-reinforced concrete members.

  4. Residual Tensile Strength and Bond Properties of GFRP Bars after Exposure to Elevated Temperatures.

    Science.gov (United States)

    Ellis, Devon S; Tabatabai, Habib; Nabizadeh, Azam

    2018-02-27

    The use of fiber reinforced polymer (FRP) bars in reinforced concrete members enhances corrosion resistance when compared to traditional steel reinforcing bars. Although there is ample research available on the behavior of FRP bars and concrete members reinforced with FRP bars under elevated temperatures (due to fire), there is little published information available on their post-fire residual load capacity. This paper reports residual tensile strength, modulus of elasticity, and bond strength (to concrete) of glass fiber reinforced polymer (GFRP) bars after exposure to elevated temperatures of up to 400 °C and subsequent cooling to an ambient temperature. The results showed that the residual strength generally decreases with increasing temperature exposure. However, as much as 83% of the original tensile strength and 27% of the original bond strength was retained after the specimens were heated to 400 °C and then cooled to ambient temperature. The residual bond strength is a critical parameter in post-fire strength assessments of GFRP-reinforced concrete members.

  5. Relationship between micro-porosity and tensile properties of 6063 alloy

    Directory of Open Access Journals (Sweden)

    Li Xiehua

    2013-01-01

    Full Text Available The micro-porosity is usually present in the as-cast microstructure, which decreases the tensile strength and ductility and therefore limit the application of cast aluminum parts. Although much work has been done to investigate the effects of various casting parameters on the formation of porosity in various aluminum alloys, up to now, little information has been available for the relationship between micro-porosity and tensile properties of 6063 alloy. In this study, the influences of size and area fraction of micro-porosity on the tensile properties and fracture behavior of 6063 aluminum alloy were investigated by means of tensile testing, optical microscopy (OM, and scanning electron microscopy (SEM. The tensile tests were conducted in air at 100 ℃, 200 ℃ and 300 ℃, respectively. Results show that the large micro-porosity with sizes between 100 μm and 800 μm located at the center and top of the ingot, while the small micro-porosity with size between 2 μm and 60 μm distributed at the edge and bottom of the ingot. The area fraction of micro-porosity at the center of the ingot is much bigger than that at the edge of the ingot. When tested at 100 ℃, with the decrease in the area fraction of micro-porosity from the top of the ingot to the bottom of the ingot, the ultimate tensile strength, yield strength and the elongation are increased from 82 to 99 MPa, 32 to 66 MPa and 7% to 11%, respectively. When the temperature is no more than 200 ℃, the strain hardening exponent decreases with an increase in the area fraction of micro-porosity; while the deviation disappears when the temperature reaches 300 ℃. The fracture mode of the alloy is greatly influenced by the size and area fraction of the micro-porosity.

  6. Residual Tensile Property of Plain Woven Jute Fiber/Poly(Lactic Acid Green Composites during Thermal Cycling

    Directory of Open Access Journals (Sweden)

    Hideaki Katogi

    2016-07-01

    Full Text Available This study investigated the residual tensile properties of plain woven jute fiber reinforced poly(lactic acid (PLA during thermal cycling. Temperature ranges of thermal cycling tests were 35–45 °C and 35–55 °C. The maximum number of cycles was 103 cycles. The quasi-static tensile tests of jute fiber, PLA, and composite were conducted after thermal cycling tests. Thermal mechanical analyses of jute fiber and PLA were conducted after thermal cycling tests. Results led to the following conclusions. For temperatures of 35–45 °C, tensile strength of composite at 103 cycles decreased 10% compared to that of composite at 0 cycles. For temperatures of 35–55 °C, tensile strength and Young’s modulus of composite at 103 cycles decreased 15% and 10%, respectively, compared to that of composite at 0 cycles. Tensile properties and the coefficient of linear expansion of PLA and jute fiber remained almost unchanged after thermal cycling tests. From observation of a fracture surface, the length of fiber pull out in the fracture surface of composite at 103 cycles was longer than that of composite at 0 cycles. Therefore, tensile properties of the composite during thermal cycling were decreased, probably because of the decrease of interfacial adhesion between the fiber and resin.

  7. High temperature tensile properties and deep drawing of fully green composites

    Directory of Open Access Journals (Sweden)

    2009-01-01

    Full Text Available In recent years, research and development of materials using biomass sources are much expected to construct a sustainable society. The so-called green composite consisting of natural fibers and biodegradable resin, is one of the most promising materials in developing biomass products. In this study, especially, we focus on the tensile deformation behavior of the green composites reinforced with ramie woven fabrics at high temperature. The results show that the fracture strain at high temperatures increases larger than that of room temperature, and initial deformation resistance of the composites seen at room temperature does not appear at high temperatures. Thus, several conditions to cause more deformability of the green composites were found. Finally, in order to utilize such deformability, Lankford-values of the green composites were clarified, and deep drawing was carried out for sheet materials made of the green composites.

  8. Statistical behavior of the tensile property of heated cotton fiber

    Science.gov (United States)

    The temperature dependence of the tensile property of single cotton fiber was studied in the range of 160-300°C using Favimat test, and its statistical behavior was interpreted in terms of structural changes. The tenacity of control cotton fiber was well described by the single Weibull distribution,...

  9. Kenaf Fibre Reinforced Polypropylene Composites: Effect of Cyclic Immersion on Tensile Properties

    Directory of Open Access Journals (Sweden)

    W. H. Haniffah

    2015-01-01

    Full Text Available This research studied the degradation of tensile properties of kenaf fibre reinforced polypropylene composites due to cyclic immersion into two different solutions, as well as comparison of the developed composites’ tensile properties under continuous and cyclic immersion. Composites with 40% and 60% fibre loadings were immersed in tap water and bleach for 4 cycles. Each cycle consisted of 3 days of immersion and 4 days of conditioning in room temperature (28°C and 55% humidity. The tensile strength and modulus of composites were affected by fibre composition, type of liquid of immersion, and number of cycles. The number of immersion cycles and conditioning caused degradation to tensile strength and modulus of kenaf fibre reinforced polypropylene composites. Continuous and cyclic immersion in bleach caused tensile strength of the composites to differ significantly whereas, for tensile modulus, the difference was insignificant in any immersion and fibre loadings. However, continuous immersion in the bleach reduced the tensile strength of composites more compared to cyclic immersion. These preliminary results suggest further evaluation of the suitability of kenaf fibre reinforced polypropylene composites for potential bathroom application where the composites will be exposed to water/liquid in cyclic manner due to discontinuous usage of bathroom.

  10. Influence of strain rate and temperature on tensile properties and flow behaviour of a reduced activation ferritic-martensitic steel

    Energy Technology Data Exchange (ETDEWEB)

    Vanaja, J., E-mail: jvanaja4@gmail.com [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India); Laha, K. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India); Sam, Shiju [Institute for Plasma Research, Gandhinagar, Gujarat (India); Nandagopal, M.; Panneer Selvi, S.; Mathew, M.D.; Jayakumar, T. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India); Rajendra Kumar, E. [Institute for Plasma Research, Gandhinagar, Gujarat (India)

    2012-05-15

    Tensile strength and flow behaviour of a Reduced Activation Ferritic-Martensitic (RAFM) steel (9Cr-1W-0.06Ta-0.22V-0.08C) have been investigated over a temperature range of 300-873 K at different strain rates. Tensile strength of the steel decreased with temperature and increased with strain rate except at intermediate temperatures. Negative strain rate sensitivity of flow stress of the steel at intermediate temperatures revealed the occurrence of dynamic strain ageing in the steel, even though no serrated flow was observed. The tensile flow behaviour of the material was well represented by the Voce strain hardening equation for all the test conditions. Temperature and strain rate dependence of the various parameters of Voce equation were interpreted with the possible deformation mechanisms. The equivalence between the saturation stress at a given strain rate in tensile test and steady state deformation rate at a given stress in creep test was found to be satisfied by the RAFM steel.

  11. Influence of strain rate and temperature on tensile properties and flow behaviour of a reduced activation ferritic-martensitic steel

    Science.gov (United States)

    Vanaja, J.; Laha, K.; Sam, Shiju; Nandagopal, M.; Panneer Selvi, S.; Mathew, M. D.; Jayakumar, T.; Rajendra Kumar, E.

    2012-05-01

    Tensile strength and flow behaviour of a Reduced Activation Ferritic-Martensitic (RAFM) steel (9Cr-1W-0.06Ta-0.22V-0.08C) have been investigated over a temperature range of 300-873 K at different strain rates. Tensile strength of the steel decreased with temperature and increased with strain rate except at intermediate temperatures. Negative strain rate sensitivity of flow stress of the steel at intermediate temperatures revealed the occurrence of dynamic strain ageing in the steel, even though no serrated flow was observed. The tensile flow behaviour of the material was well represented by the Voce strain hardening equation for all the test conditions. Temperature and strain rate dependence of the various parameters of Voce equation were interpreted with the possible deformation mechanisms. The equivalence between the saturation stress at a given strain rate in tensile test and steady state deformation rate at a given stress in creep test was found to be satisfied by the RAFM steel.

  12. Influence of strain rate and temperature on tensile properties and flow behaviour of a reduced activation ferritic–martensitic steel

    International Nuclear Information System (INIS)

    Vanaja, J.; Laha, K.; Sam, Shiju; Nandagopal, M.; Panneer Selvi, S.; Mathew, M.D.; Jayakumar, T.; Rajendra Kumar, E.

    2012-01-01

    Tensile strength and flow behaviour of a Reduced Activation Ferritic–Martensitic (RAFM) steel (9Cr–1W–0.06Ta–0.22V–0.08C) have been investigated over a temperature range of 300–873 K at different strain rates. Tensile strength of the steel decreased with temperature and increased with strain rate except at intermediate temperatures. Negative strain rate sensitivity of flow stress of the steel at intermediate temperatures revealed the occurrence of dynamic strain ageing in the steel, even though no serrated flow was observed. The tensile flow behaviour of the material was well represented by the Voce strain hardening equation for all the test conditions. Temperature and strain rate dependence of the various parameters of Voce equation were interpreted with the possible deformation mechanisms. The equivalence between the saturation stress at a given strain rate in tensile test and steady state deformation rate at a given stress in creep test was found to be satisfied by the RAFM steel.

  13. Novel development of the micro-tensile test at elevated temperature using a test structure with integrated micro-heater

    Science.gov (United States)

    Ang, W. C.; Kropelnicki, P.; Soe, Oak; Ling, J. H. L.; Randles, A. B.; Hum, A. J. W.; Tsai, J. M. L.; Tay, A. A. O.; Leong, K. C.; Tan, C. S.

    2012-08-01

    This paper describes the novel development of a micro-tensile testing method that allows testing at elevated temperatures. Instead of using a furnace, a titanium/platinum thin film micro-heater was fabricated on a conventional dog-bone-shaped test structure to heat up its gauge section locally. An infrared (IR) camera with 5 µm resolution was employed to verify the temperature uniformity across the gauge section of the test structure. With this micro-heater-integrated test structure, micro-tensile tests can be performed at elevated temperatures using any conventional tensile testing system without any major modification to the system. In this study, the tensile test of the single crystal silicon (SCS) thin film with (1 0 0) surface orientation and tensile direction was performed at room temperature and elevated temperatures, up to 300 °C. Experimental results for Young's modulus as a function of temperature are presented. A micro-sized SCS film showed a low dependence of mechanical properties on temperature up to 300 °C.

  14. Microstructure, Tensile Properties, and Corrosion Behavior of Die-Cast Mg-7Al-1Ca- xSn Alloys

    Science.gov (United States)

    Wang, Feng; Dong, Haikuo; Sun, Shijie; Wang, Zhi; Mao, Pingli; Liu, Zheng

    2018-02-01

    The microstructure, tensile properties, and corrosion behavior of die-cast Mg-7Al-1Ca- xSn ( x = 0, 0.5, 1.0, and 2.0 wt.%) alloys were studied using OM, SEM/EDS, tensile test, weight loss test, and electrochemical test. The experimental results showed that Sn addition effectively refined grains and intermetallic phases and increased the amount of intermetallic phases. Meanwhile, Sn addition to the alloys suppressed the formation of the (Mg,Al)2Ca phase and resulted in the formation of the ternary CaMgSn phase and the binary Mg2Sn phase. The Mg-7Al-1Ca-0.5Sn alloy exhibited best tensile properties at room temperature, while Mg-7Al-1Ca-1.0Sn alloy exhibited best tensile properties at elevated temperature. The corrosion resistance of studied alloys was improved by the Sn addition, and the Mg-7Al-1Ca-0.5Sn alloy presented the best corrosion resistance.

  15. Tensile properties of modified 9Cr-1Mo steel by shear punch testing and correlation with microstructures

    Energy Technology Data Exchange (ETDEWEB)

    Karthik, V., E-mail: karthik@igcar.gov.in [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, Tamil Nadu 603102 (India); Laha, K.; Parameswaran, P.; Chandravathi, K.S.; Kasiviswanathan, K.V.; Jayakumar, T.; Raj, Baldev [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, Tamil Nadu 603102 (India)

    2011-10-15

    Modified 9Cr-1Mo ferritic steel (P91) is subjected to a series of heat treatments consisting of soaking for 5 min at the selected temperatures in the range 973 K-1623 K (below Ac{sub 1} to above Ac{sub 4}) followed by oil quenching and tempering at 1033 K for 1 h to obtain different microstructural conditions. The tensile properties of the different microstructural conditions are evaluated from small volumes of material by shear punch test technique. A new methodology for evaluating yield strength, ultimate tensile strength and strain hardening exponent from shear punch test by using correlation equations without employing empirical constants is presented and validated. The changes in the tensile properties are related to the microstructural changes of the steel investigated by electron microscopic studies. The steel exhibits minimum strength and hardness when soaked between Ac{sub 1} and Ac{sub 3} (intercritical range) temperatures due to the replacement of original lath martensitic structure with subgrains. The finer martensitic microstructure produced in the steel after soaking at temperatures above Ac{sub 3} leads to a monotonic increase in hardness and strength with decreasing strain hardening exponent. For soaking temperatures above Ac{sub 4}, the hardness and strength of the steel increases marginally due to the formation of soft {delta} ferrite. - Highlights: > A methodology presented for computing tensile properties from shear punch test. > UTS and strain hardening estimated using extended analysis of blanking models. > The analysis methodology validated for different heat treated 9Cr-1Mo steel. > Changes in tensile properties of steel correlated with microstructures.

  16. Influence of the quenching rate and step-wise cooling temperatures on microstructural and tensile properties of PER72 ® Ni-based superalloy

    Directory of Open Access Journals (Sweden)

    Le Baillif Paul

    2014-01-01

    Full Text Available The PER72® grade is used as a wrought engine turbine disk, which is a critical high temperature component. During the heat treatment process, residual stresses are generated during the quench, which may lead to irreversible damages on the workpiece. The aim of this study is to better understand the mechanisms involved in the residual stress generation. Therefore, the influence of quenching conditions on the high temperature tensile properties and the multi-scale microstructure evolutions are investigated after cooling. PER72® specimens are annealed above the solvus temperature, directly on the servo-hydraulic testing machine. Three quenching rates are used: 30 ∘C/min, 120 ∘C/min, and 300 ∘C/min. For each condition, the cooling is interrupted at 1000 ∘C, 850 ∘C, 600 ∘C and 20 ∘C to perform isothermal tensile test. Specimens are post-mortem analysed. On one hand the fracture surface is investigated using SEM. On the other hand the microstructure evolution was observed and quantified at different scales using SEM directly on the bulk or after the chemical extraction of precipitation. The precipitation size and volume fraction statistics, X-Ray diffraction for the crystallography and composition of the different phases are investigated. It was shown that the testing temperature does not significantly influence the γ′ distribution of particles. Conversely, the γ′ precipitation is strongly influenced by the cooling rate. Notably, the average size, the distance between particles as well as the number density of γ′ precipitates are significantly modified by the cooling rate. Changes in tensile properties are related to microstructural.

  17. Effect of small additions of silicon, iron, and aluminum on the room-temperature tensile properties of high-purity uranium

    International Nuclear Information System (INIS)

    Ludwig, R.L.

    1983-01-01

    Eleven binary and ternary alloys of uranium and very low concentrations of iron, silicon, and aluminum were prepared and tested for room-temperature tensile properties after various heat treatments. A yield strength approximately double that of high-purity derby uranium was obtained from a U-400 ppM Si-200 ppM Fe alloy after beta solution treatment and alpha aging. Higher silicon plus iron alloy contents resulted in increased yield strength, but showed an unacceptable loss of ductility

  18. Empirical relations for tensile properties of austenitic stainless steels irradiated in mixed-spectrum reactors

    International Nuclear Information System (INIS)

    Grossbeck, M.L.

    1991-01-01

    An assessment has been made of available tensile property data relevant to the design of fusion reactors, especially near term devices expected to operate at lower temperatures than power reactors. Empirical relations have been developed for the tensile properties as a functions of irradiation temperature for neutron exposures of 10-15, 20, 30, and 50 dpa. It was found that yield strength depends little on the particular austenitic alloy and little on the helium concentration. Strength depends upon initial condition of the alloy only for exposures of less than 30 dpa. Uniform elongation was found to be more sensitive to alloy and condition. It was also more sensitive than strength to helium level. However, below 500deg C, helium only appeared to have an efect at 10-15 dpa. At higher temperatures, helium embrittlement was apparent, and its threshold temperature decreased with increasing neutron exposure level. (orig.)

  19. Tensile, swelling and morphological properties of bentonite-filled acrylonitrile butadiene rubber composites

    Science.gov (United States)

    Lotfi, Muhamad Nadhli Amin; Ismail, Hanafi; Othman, Nadras

    2017-10-01

    Tensile, swelling and morphological properties of bentonite filled acrylonitrile butadiene rubber (NBR/Bt) composites were studied. The experiments were conducted at room temperature by using two rolled mill, universal testing machine (INSTRON), and American Standard Testing Method (ASTM) D471 for compounding, tensile testing, and swelling test, respectively. Results obtained indicated that a better tensile strength, elongation at break and tensile modulus were recorded as compared to the pure NBR particularly up to 90 phr of Bt loading. However, swelling (%) exhibited the opposite trend where the liquid uptake by the composites was indirectly proportional with the increasing of Bt loading. Scanning electron microscopy (SEM) used on the tensile fractured surface of the NBR/Bt composites have shown that the fillers were well embedded in the NBR matrix, for Bt loading up to 90 phr. The agglomeration of fillers occurred for Bt loading exceeding 90 phr.

  20. Influence of quenching cooling rate on residual stress and tensile properties of 2A14 aluminum alloy forgings

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Yu-xun, E-mail: zhangyuxun198@163.com; Yi, You-ping, E-mail: yyp@csu.edu.cn; Huang, Shi-quan, E-mail: huangsqcsu@sina.com; Dong, Fei

    2016-09-30

    To balance the quenching residual stress and the mechanical properties of aluminum alloys, the influence of cooling rate on the residual stress and tensile properties was investigated by numerical simulation and quenching experiments. During the quenching experiments, 2A14 aluminum alloy samples were treated with different water temperatures (20 °C, 70 °C, 100 °C) and a step quenching process. X-ray diffraction (XRD) was used to measure the residual stress. Prior to them, the quenching sensitivity was studied. For this purpose, the time-temperature-properties (TTP) curves were measured and the alloy microstructure was observed using transmission electron microscopy (TEM). The results indicated that the mechanical properties of 2A14 aluminum alloys were mainly determined by the cooling rate within the quenching sensitive temperature range from 300 to 400 °C. Lower cooling rates reduced the tensile strength and yield strength due to a decrease amount of fine precipitates, and reduced the residual stress with the reduction of plastic strain and the degree of inhomogeneous plastic deformation. In addition, the residual stress changed faster than the tensile properties with decreasing cooling rate. Therefore, warm water (70 °C) was used to balance the residual stress and tensile properties of 140-mm-thick 2A14 aluminum alloy forgings, since it can achieve low cooling rates. Furthermore, by combining this characteristic and the material quenching sensitivity, step quenching produced similar tensile properties and lower residual stress, compared with the sample quenched in warm water (70 °C), by increasing cooling rate within quenching sensitivity range and reducing it in other ranges.

  1. Influence of quenching cooling rate on residual stress and tensile properties of 2A14 aluminum alloy forgings

    International Nuclear Information System (INIS)

    Zhang, Yu-xun; Yi, You-ping; Huang, Shi-quan; Dong, Fei

    2016-01-01

    To balance the quenching residual stress and the mechanical properties of aluminum alloys, the influence of cooling rate on the residual stress and tensile properties was investigated by numerical simulation and quenching experiments. During the quenching experiments, 2A14 aluminum alloy samples were treated with different water temperatures (20 °C, 70 °C, 100 °C) and a step quenching process. X-ray diffraction (XRD) was used to measure the residual stress. Prior to them, the quenching sensitivity was studied. For this purpose, the time-temperature-properties (TTP) curves were measured and the alloy microstructure was observed using transmission electron microscopy (TEM). The results indicated that the mechanical properties of 2A14 aluminum alloys were mainly determined by the cooling rate within the quenching sensitive temperature range from 300 to 400 °C. Lower cooling rates reduced the tensile strength and yield strength due to a decrease amount of fine precipitates, and reduced the residual stress with the reduction of plastic strain and the degree of inhomogeneous plastic deformation. In addition, the residual stress changed faster than the tensile properties with decreasing cooling rate. Therefore, warm water (70 °C) was used to balance the residual stress and tensile properties of 140-mm-thick 2A14 aluminum alloy forgings, since it can achieve low cooling rates. Furthermore, by combining this characteristic and the material quenching sensitivity, step quenching produced similar tensile properties and lower residual stress, compared with the sample quenched in warm water (70 °C), by increasing cooling rate within quenching sensitivity range and reducing it in other ranges.

  2. Tensile and electrical properties of unirradiated and irradiated Hycon 3HP{trademark} CuNiBe

    Energy Technology Data Exchange (ETDEWEB)

    Zinkle, S.J.; Eatherly, W.S. [Oak Ridge National Lab., TN (United States)

    1996-10-01

    The unirradiated tensile properties of two different heats of Hycon 3HP{trademark} CuNiBe (HT Temper) have been measured over the temperature range of 20-500{degrees}C for longitudinal and long transverse orientations. The room temperature electrical conductivity has also been measured for both heats. Both heats exhibited a very good combination of strength and conductivity at room temperature. The strength remained relatively high at all test temperatures, with a yield strength of 420-520 MPa at 500{degrees}C. However, low levels of ductility (<5% uniform elongation) were observed at test temperatures above 200-250{degrees}C, due to flow localization adjacent to grain boundaries. Fission neutron irradiation to a dose of {approximately}0.7 dpa at temperatures between 100 and 240{degrees}C produced a slight increase in strength and a significant decrease in ductility. The measured tensile elongation increased with increasing irradiation temperature, with a uniform elongation of {approximately}3.3% observed at 240{degrees}C. The electrical conductivity decreased slightly following irradiation, due to the presence of defect clusters and Ni, Zn, Co transmutation products. The data indicate that CuNiBe alloys have irradiated tensile and electrical properties comparable or superior to CuCrZr and oxide dispersion strengthened copper at temperatures <250{degrees}C, and may be suitable for certain fusion energy structural applications.

  3. Microstructure, process, and tensile property relationships in an investment cast near-γTiAl alloy

    International Nuclear Information System (INIS)

    Jones, P.E.; Porter, W.J. III.; Keller, M.M.; Eylon, D.

    1992-01-01

    The brittle nature of near-γ TiAl alloys makes fabrication difficult. This paper reports on developing near-net shape technologies, such as investment casting, for these alloys which is one of the essential approached to their commercial introduction. The near-γ TiAl alloy Ti-48Al-2Nb-2Cr (a%) is investment cast with two cooling rates. The effect of casting cooling rate on the fill and surface integrity was studied for complex shape thin walled components. Block and bar castings are hot isostatically pressed (HIP'd) and heat treated to produce duplex (lamellar + equiaxed) microstructures for mechanical property evaluation. The relationships between the casting conditions, microstructures, and tensile properties are studied. The strength and elongation below the ductile to brittle transition temperature are dependent on the casting cooling rate and section size. The tensile properties improved with faster cooling during the casting process as a result of microstructural refinement. Faster cooled castings are more fully transformed to a duplex structure during post-casting heat treatments. Above the ductile to brittle transition temperature the effect of casting cooling rate on tensile properties is less pronounced

  4. Preparation of poly (arylene ether nitrile)/NzdFeB composite film with excellent thermal properties and tensile strength

    Science.gov (United States)

    Pan, Hai; Xu, Mingzhen; Liu, Xiaobo

    2017-12-01

    PEN/NdFeB composite films were prepared by the solution casting method. The thermal properties, fracture morphology and tensile strength of the composite films were tested by DSC, TGA, SEM and electromechanical universal testing machine, respectively. The results reveal that the composite film has good thermal properties and tensile strength. Glass-transition temperature and decomposition temperatures at weight loss of 5% ot the composite films retain at 166±1 C and 462±4 C, respectively. The composite film with 5 wt.% NdFeB has the best tensile strength value for 100.5 MPa. In addition, it was found that the NdFeB filler was well dispersed in PEN matrix by SEM analysis.

  5. Influence of Cutting Temperature on the Tensile Strength of a Carbon Fiber-Reinforced Polymer

    Directory of Open Access Journals (Sweden)

    Jérémy Delahaigue

    2017-12-01

    Full Text Available Carbon fiber-reinforced plastics (CFRP have seen a significant increase in use over the years thanks to their specific properties. Despite continuous improvements in the production methods of laminated parts, a trimming operation is still necessary to achieve the functional dimensions required by engineering specifications. Laminates made of carbon fibers are very abrasive and cause rapid tool wear, and require high cutting temperatures. This creates damage to the epoxy matrix, whose glass-transition temperature is often recognized to be about 180 °C. This study aims to highlight the influence of the cutting temperature generated by tool wear on the surface finish and mechanical properties obtained from tensile tests. Trimming operations were performed on a quasi-isotropic 24-ply carbon/epoxy laminate, of 3.6 mm thickness, with a 6 flutes diamond-coated (CVD cutter. The test specimens of 6 mm and 12 mm wide were obtained by trimming. The reduced width of the coupons allowed amplification of the effect of defects on the measured properties by increasing the proportion of coupon cross-section occupied by the defects. A new tool and a tool in an advanced state of wear were used to generate different cutting temperatures. Results showed a cutting temperature of 300 °C for the new tool and 475 °C for the worn tool. The analysis revealed that the specimens machined with the new tool have no thermal damage and the cut is clean. The plies oriented at −45° presented the worst surface finish according to the failure mode of the fiber. For the worn tool, the surface was degraded and the matrix was carbonized. After cutting, observations showed a degraded resin spread on the machined surface, which reduced the surface roughness and hid the cutting defects. In support of these observations, the tensile tests showed no variation of the mechanical properties for the 12 mm-wide specimens, but did show a 10% loss in mechanical properties for the 6 mm

  6. Handbook for tensile properties of austenitic stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Kim, D. W.; Ryu, W. S.; Jang, J. S.; Kim, S. H.; Kim, W. G.; Chung, M. K.; Han, C. H. [Korea Atomic Energy Research Institute, Taejeon (Korea)

    2000-03-01

    Database system of nuclear materials has not been developed and the physical and mechanical properties of materials used in nuclear power plant are not summarized systematically in Korea. Although Korea designs nuclear power plant, many materials used in nuclear power plant are imported because we do not have database system of nuclear material yet and it was hard to select a proper material for the structural materials of nuclear power plant. To develop database system of nuclear materials, data of mechanical, corrosion, irradiation properties are needed. Of theses properties, tensile properties are tested and summarized in this report. Tensile properties of stainless steel used in nuclear reactor internal were investigated. Data between Korea Atomic Energy Research Institute and foreign laboratory were compared to determine the precision of the result. To develope database system, materials, chemical composition, heat treatment, manufacturing process, and grain size were classified. Tensile properties were tested and summarized to use input data of database system. 9 figs., 9 tabs. (Author)

  7. Surface orientation effects on bending properties of surgical mesh are independent of tensile properties.

    Science.gov (United States)

    Simon, David D; Andrews, Sharon M; Robinson-Zeigler, Rebecca; Valdes, Thelma; Woods, Terry O

    2018-02-01

    Current mechanical testing of surgical mesh focuses primarily on tensile properties even though implanted devices are not subjected to pure tensile loads. Our objective was to determine the flexural (bending) properties of surgical mesh and determine if they correlate with mesh tensile properties. The flexural rigidity values of 11 different surgical mesh designs were determined along three textile directions (machine, cross-machine, and 45° to machine; n = 5 for each) using ASTM D1388-14 while tracking surface orientation. Tensile testing was also performed on the same specimens using ASTM D882-12. Linear regressions were performed to compare mesh flexural rigidity to mesh thickness, areal mass density, filament diameter, ultimate tensile strength, and maximum extension. Of 33 mesh specimen groups, 30 had significant differences in flexural rigidity values when comparing surface orientations (top and bottom). Flexural rigidity and mesh tensile properties also varied with textile direction (machine and cross-machine). There was no strong correlation between the flexural and tensile properties, with mesh thickness having the best overall correlation with flexural rigidity. Currently, surface orientation is not indicated on marketed surgical mesh, and a single mesh may behave differently depending on the direction of loading. The lack of correlation between flexural stiffness and tensile properties indicates the need to examine mesh bending stiffness to provide a more comprehensive understanding of surgical mesh mechanical behaviors. Further investigation is needed to determine if these flexural properties result in the surgical mesh behaving mechanically different depending on implantation direction. © 2017 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 106B: 854-862, 2018. © 2017 Wiley Periodicals, Inc.

  8. The effect of temperature on compressive and tensile strengths of commonly used luting cements: an in vitro study.

    Science.gov (United States)

    Patil, Suneel G; Sajjan, Mc Suresh; Patil, Rekha

    2015-02-01

    The luting cements must withstand masticatory and parafunctional stresses in the warm and wet oral environment. Mouth temperature and the temperature of the ingested foods may induce thermal variation and plastic deformation within the cements and might affect the strength properties. The objectives of this study were to evaluate the effect of temperature on the compressive and diametral tensile strengths of two polycarboxylate, a conventional glass ionomer and a resin modified glass ionomer luting cements and, to compare the compressive strength and the diametral tensile strength of the selected luting cements at varying temperatures. In this study, standardized specimens were prepared. The temperature of the specimens was regulated prior to testing them using a universal testing machine at a crosshead speed of 1 mm/min. Six specimens each were tested at 23°C, 37°C and 50°C for both the compressive and diametral tensile strengths, for all the luting cements. All the luting cements showed a marginal reduction in their compressive and diametral tensile strengths at raised temperatures. Fuji Plus was strongest in compression, followed by Fuji I > Poly F > Liv Carbo. Fuji Plus had the highest diametral tensile strength values, followed by Poly F = Fuji I = Liv Carbo, at all temperatures. An increase in the temperature caused no significant reduction in the compressive and diametral tensile strengths of the cements evaluated. The compressive strength of the luting cements differed significantly from one another at all temperatures. The diametral tensile strength of resin modified glass ionomers differed considerably from the other cements, whereas there was no significant difference between the other cements, at all the temperatures.

  9. Ethylene propylene cable degradation during LOCA research tests: tensile properties at the completion of accelerated aging

    International Nuclear Information System (INIS)

    Bustard, L.D.

    1982-05-01

    Six ethylene-propylene rubber (EPR) insulation materials were aged at elevated temperature and radiation stress exposures common in cable LOCA qualification tests. Material samples were subjected to various simultaneous and sequential aging simulations in preparation for accident environmental exposures. Tensile properties subsequent to the aging exposure sequences are reported. The tensile properties of some, but not all, specimens were sensitive to the order of radiation and elevated temperature stress exposure. Other specimens showed more severe degradation when simultaneously exposed to radiation and elevated temperature as opposed to the sequential exposure to the same stresses. Results illustrate the difficulty in defining a single test procedure for nuclear safety-related qualification of EPR elastomers. A common worst-case sequential aging sequence could not be identified

  10. Effects of time of heatsetting on the tensile properties of ingeo (tm) poly (lactic acid) (PLA) fabric

    Energy Technology Data Exchange (ETDEWEB)

    Idumah, C.I. [School of Materials, University of Manchester, Manchester, M13 9PL (United Kingdom); Nwachukwu, A.N. [Williamson Research Centre for Molecular Environmental Sciences, School of Earth, Atmospheric and Environmental Science, University of Manchester, M13 9P (United Kingdom)

    2013-07-01

    Poly (lactic acid) is biodegradable and environmentally benign aliphatic polyester produced from the fermentation of naturally occurring and renewable resources like corn, sugar and vegetables and subsequently converted to a textile fiber through melt spinning and spun bonding. A study of the effect of time of heatsetting on tensile properties of knitted Ingeo (tm) Poly (lactic acid) fabric was investigated and reported in this paper. PLA samples were subjected to increasing heatsetting times of 15s, 30s, 40s, 60s, 90s and 240s at 1300 C using the Werner Mathis Infra red heatsetting equipment. Tensile properties were evaluated using the KES-FB (KAWABATA) fabric evaluation system. The tensile properties determined in weft and warp directions included fabric extension [%], linearity of load extension [-], tensile energy [WT] g.cm/cm2 and tensile resilience [%]. Results revealed the optimum time of heatsetting PLA yarns to attain dimensional stability was within the time range of 30-45s at heatsetting temperature of 130 0C.

  11. Effects of liquid lead on 316l tensile properties

    International Nuclear Information System (INIS)

    Ionescu, V.; Pitigoi, V.; Nitu, A.; Hororoi, M.; Voicu, F.; Cojocaru, V.

    2016-01-01

    The lead-cooled fast reactor (LFR) is one of the concepts of the Generation IV reactor systems. Compatibility of the candidate structural materials with the liquid lead is known to be one of the critical issues to allow development of the LFR reactors. In contact with the liquid metal, the mechanical integrity of the structural materials can be affected. The steel.s mechanical properties are assessed by tensile testing as a function of temperature in heavy liquid metal and in an air environment. RATEN ICN is involved in several European projects aimed to Generation IV research activities. In a first stage an Experimental Facility for Tensile Tests in Liquid Lead environment has been set up. This installation is adapted on the Instron testing machine, already existing in institute. 316L alloy is one of a candidate structural material for this type of reactor. This document presents the effect of liquid lead on tensile properties of 316L material tested in liquid lead (in static conditions) and in air environment at 500°C, without oxygen monitoring system. When solid metals are placed in contact to liquid metals and stress is applied, they may undergo abrupt brittle failure. Stress-strain curves of slow strain rate tests have been obtained in conformity with ASTM, E-8. Mechanical characteristics determined are in accordance with literature. (authors)

  12. Elevated-temperature tensile properties of 2 1/4 Cr-1 Mo steel irradiated in the EBR-II, AD-2 experiment

    International Nuclear Information System (INIS)

    Klueh, R.L.; Vitek, J.M.

    1984-01-01

    The effect of irradiated on the tensile properties of 2 1/4 Cr-1 Mo steel was determined for specimens irradiation in EBR-II at 390 to 550 0 C. Unirradiated control specimens and specimens aged for 5000 h at the irradiation temperatures were also tested. Irradiation to approximately 9 dpa at 390 0 C increased the strength and decreased the ductility compared with the unirradiated and aged specimens. Softening occurred in samples irradiated and tested at 450, 500, and 550 0 C

  13. Tensile properties and flow behavior analysis of modified 9Cr-1Mo steel clad tube material

    Science.gov (United States)

    Singh, Kanwarjeet; Latha, S.; Nandagopal, M.; Mathew, M. D.; Laha, K.; Jayakumar, T.

    2014-11-01

    The tensile properties and flow behavior of modified 9Cr-1Mo steel clad tube have been investigated in the framework of various constitutive equations for a wide range of temperatures (300-923 K) and strain rates (3 × 10-3 s-1, 3 × 10-4 s-1 and 3 × 10-5 s-1). The tensile flow behavior of modified 9Cr-1Mo steel clad tube was most accurately described by Voce equation. The variation of instantaneous work hardening rate (θ = dσ/dε) and σθ with stress (σ) indicated two stage behavior characterized by rapid decrease at low stresses (transient stage) followed by a gradual decrease in high stresses (Stage III). The variation of work hardening parameters and work hardening rate in terms of θ vs. σ and σθ vs. σ with temperature exhibited three distinct regimes. Rapid decrease in flow stress and work hardening parameters and rapid shift of θ vs. σ and σθ vs. σ towards low stresses with increase in temperature indicated dynamic recovery at high temperatures. Tensile properties of the material have been best predicted from Voce equation.

  14. Tensile properties and flow behavior analysis of modified 9Cr–1Mo steel clad tube material

    International Nuclear Information System (INIS)

    Singh, Kanwarjeet; Latha, S.; Nandagopal, M.; Mathew, M.D.; Laha, K.; Jayakumar, T.

    2014-01-01

    The tensile properties and flow behavior of modified 9Cr–1Mo steel clad tube have been investigated in the framework of various constitutive equations for a wide range of temperatures (300–923 K) and strain rates (3 × 10 −3 s −1 , 3 × 10 −4 s −1 and 3 × 10 −5 s −1 ). The tensile flow behavior of modified 9Cr–1Mo steel clad tube was most accurately described by Voce equation. The variation of instantaneous work hardening rate (θ = dσ/dε) and σθ with stress (σ) indicated two stage behavior characterized by rapid decrease at low stresses (transient stage) followed by a gradual decrease in high stresses (Stage III). The variation of work hardening parameters and work hardening rate in terms of θ vs. σ and σθ vs. σ with temperature exhibited three distinct regimes. Rapid decrease in flow stress and work hardening parameters and rapid shift of θ vs. σ and σθ vs. σ towards low stresses with increase in temperature indicated dynamic recovery at high temperatures. Tensile properties of the material have been best predicted from Voce equation

  15. Tensile properties of vanadium alloys irradiated at 390{degrees}C in EBR-II

    Energy Technology Data Exchange (ETDEWEB)

    Chung, H.M.; Tsai, H.C.; Nowicki, L.J. [Argonne National Lab., IL (United States)] [and others

    1997-08-01

    Vanadium alloys were irradiated in Li-bonded stainless steel capsules to {approx}390{degrees}C in the EBR-II X-530 experiment. This report presents results of postirradiation tests of tensile properties of two large-scale (100 and 500 kg) heats of V-4Cr-Ti and laboratory (15-30 kg) heats of boron-doped V-4Cr-4Ti, V-8Cr-6Ti, V-5Ti, and V-3Ti-1Si alloys. Tensile specimens, divided into two groups, were irradiated in two different capsules under nominally similar conditions. The 500-kg heat (No. 832665) and the 100-kg heat (VX-8) of V-4Cr-4Ti irradiated in one of the subcapsules exhibited complete loss of work-hardening capability, which was manifested by very low uniform plastic strain. In contrast, the 100-kg heat of V-4Cr-4Ti irradiated in another subcapsule exhibited good tensile properties (uniform plastic strain 2.8-4.0%). A laboratory heat of V-3Ti-1Si irradiated in the latter subcapsule also exhibited good tensile properties. These results indicate that work-hardening capability at low irradiation temperatures varies significantly from heat to heat and is influenced by nominally small differences in irradiation conditions.

  16. Tensile properties and microstructural analysis of spheroidized hydroxyapatite-poly (etheretherketone) biocomposites

    International Nuclear Information System (INIS)

    Abu Bakar, M.S.; Cheang, P.; Khor, K.A.

    2003-01-01

    Poly(etheretherketone) or PEEK, is a high performance thermoplastic possessing exceptional mechanical properties, high temperature durability, good chemical and fatigue resistance. These coupled with its ability to withstand sterilization treatment, make it a preferred material for biomedical applications. This study examines the benefit of incorporating hydroxyapatite particulates in poly(etheretherketone) for possible usage as bone analogue materials. Flame spheroidized hydroxyapatite (FSHA) were incorporated into semi-crystalline poly(etheretherketone) polymer through a series of processes comprising melt compounding, granulating and injection molding. Biocomposites with high hydroxyapatite loading of up to 40 vol.% were processed successfully using this technique. Scanning electron microscopy (SEM) revealed fair dispersion and distribution of hydroxyapatite particles within the polymer matrix. The series of composites were characterized in terms of tensile and microhardness properties. Microstructural analysis was also carried out to correlate the structure-property relationship of the composite. The dependency of tensile properties such as modulus, strength and strain to fracture as well as the micro-hardness on the volume percentage of hydroxyapatite were investigated. By varying the amount of hydroxyapatite particles in the composite, a wide range of mechanical properties were obtained. In general, the tensile modulus and microhardness increased, while strength and strain to fracture decreased correspondingly with progressive addition of hydroxyapatite particles. The composite system under investigation also exhibited mechanical properties matching those of human bone. With hydroxyapatite loading beyond 30 vol.%, the modulus were within the bounds of the human cortical bone. Findings from this study suggest that this bioactive composite system have the potential as an alternative implant material for orthopaedic application

  17. Effect of Root Moisture Content and Diameter on Root Tensile Properties

    Science.gov (United States)

    Yang, Yuanjun; Chen, Lihua; Li, Ning; Zhang, Qiufen

    2016-01-01

    The stabilization of slopes by vegetation has been a topical issue for many years. Root mechanical characteristics significantly influence soil reinforcement; therefore it is necessary to research into the indicators of root tensile properties. In this study, we explored the influence of root moisture content on tensile resistance and strength with different root diameters and for different tree species. Betula platyphylla, Quercus mongolica, Pinus tabulaeformis, and Larix gmelinii, the most popular tree species used for slope stabilization in the rocky mountainous areas of northern China, were used in this study. A tensile test was conducted after root samples were grouped by diameter and moisture content. The results showedthat:1) root moisture content had a significant influence on tensile properties; 2) slightly loss of root moisture content could enhance tensile strength, but too much loss of water resulted in weaker capacity for root elongation, and consequently reduced tensile strength; 3) root diameter had a strong positive correlation with tensile resistance; and4) the roots of Betula platyphylla had the best tensile properties when both diameter and moisture content being controlled. These findings improve our understanding of root tensile properties with root size and moisture, and could be useful for slope stabilization using vegetation. PMID:27003872

  18. Elevated temperature tensile properties of P9 steel towards ferritic steel wrapper development for sodium cooled fast reactors

    Energy Technology Data Exchange (ETDEWEB)

    Choudhary, B.K., E-mail: bkc@igcar.gov.in; Mathew, M.D.; Isaac Samuel, E.; Christopher, J.; Jayakumar, T.

    2013-11-15

    Tensile deformation and fracture behaviour of the three developmental heats of P9 steel for wrapper applications containing varying silicon in the range 0.24–0.60% have been examined in the temperature range 300–873 K. Yield and ultimate tensile strengths in all the three heats exhibited gradual decrease with increase in temperature from room to intermediate temperatures followed by rapid decrease at high temperatures. A gradual decrease in ductility to a minimum at intermediate temperatures followed by an increase at high temperatures has been observed. The fracture mode remained transgranular ductile. The steel displayed signatures of dynamic strain ageing at intermediate temperatures and dominance of recovery at high temperatures. No significant difference in the strength and ductility values was observed for varying silicon in the range 0.24–0.60% in P9 steel. P9 steel for wrapper application displayed strength and ductility values comparable to those reported in the literature.

  19. Elevated temperature tensile properties of P9 steel towards ferritic steel wrapper development for sodium cooled fast reactors

    Science.gov (United States)

    Choudhary, B. K.; Mathew, M. D.; Isaac Samuel, E.; Christopher, J.; Jayakumar, T.

    2013-11-01

    Tensile deformation and fracture behaviour of the three developmental heats of P9 steel for wrapper applications containing varying silicon in the range 0.24-0.60% have been examined in the temperature range 300-873 K. Yield and ultimate tensile strengths in all the three heats exhibited gradual decrease with increase in temperature from room to intermediate temperatures followed by rapid decrease at high temperatures. A gradual decrease in ductility to a minimum at intermediate temperatures followed by an increase at high temperatures has been observed. The fracture mode remained transgranular ductile. The steel displayed signatures of dynamic strain ageing at intermediate temperatures and dominance of recovery at high temperatures. No significant difference in the strength and ductility values was observed for varying silicon in the range 0.24-0.60% in P9 steel. P9 steel for wrapper application displayed strength and ductility values comparable to those reported in the literature.

  20. Elevated temperature tensile properties of P9 steel towards ferritic steel wrapper development for sodium cooled fast reactors

    International Nuclear Information System (INIS)

    Choudhary, B.K.; Mathew, M.D.; Isaac Samuel, E.; Christopher, J.; Jayakumar, T.

    2013-01-01

    Tensile deformation and fracture behaviour of the three developmental heats of P9 steel for wrapper applications containing varying silicon in the range 0.24–0.60% have been examined in the temperature range 300–873 K. Yield and ultimate tensile strengths in all the three heats exhibited gradual decrease with increase in temperature from room to intermediate temperatures followed by rapid decrease at high temperatures. A gradual decrease in ductility to a minimum at intermediate temperatures followed by an increase at high temperatures has been observed. The fracture mode remained transgranular ductile. The steel displayed signatures of dynamic strain ageing at intermediate temperatures and dominance of recovery at high temperatures. No significant difference in the strength and ductility values was observed for varying silicon in the range 0.24–0.60% in P9 steel. P9 steel for wrapper application displayed strength and ductility values comparable to those reported in the literature

  1. The tensile properties of alloys 800H and 617 in the range 20 to 950deg C

    International Nuclear Information System (INIS)

    Abd El-Azim, M.E.; Ennis, P.J.; Schuster, H.; Nickel, H.

    1990-01-01

    The tensile properties of Alloy 800H and Alloy 617 in the solution treated condition and after ageing or carburization have been determined for the temperature range 20 to 950deg C. It was found that ageing at 900deg C prior to testing led to an increase in strength and a decrease in ductility at test temperatures up to 700deg C. Above 700deg C, there was no significant difference between the tensile properties of solution treated and aged material. Carburization caused a severe loss of ductility in both alloys at temperatures of 20 to around 800deg C, but the ductility increased sharply at test temperatures above 800deg C, accompanied by a change in the fracture mode from fracture of the carbide particles themselves to void formation and separation at the carbide/matrix interface. The correlation between tensile properties and creep data was investigated in tests carried out at different strain rates. Reasonable agreement was found at 800 to 950deg C for Alloy 617 and at 800 to 900deg C for Alloy 800H. Strain ageing effects were observed in both alloys at some temperatures and strain rates; these effects were serrated flow, negative strain rate sensitivity, peaks in the normalized UTS-temperature curves and plateaus in the elongation-temperature curves. The experimental results were interpreted in the light of two current models for strain ageing, the dislocation-dislocation interaction model and the dislocation-solute interaction model. (orig.) [de

  2. Effect of Annealing Temperature on the Microstructure, Tensile Properties, and Fracture Behavior of Cold-Rolled High-Mn Light-Weight Steels

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Jae-Hyun; Cho, Kyung Mox [Pusan National University, Busan (Korea, Republic of); Park, Seong-Jun; Moon, Joonoh; Kang, Jun-Yun; Park, Jun-Young; Lee, Tae-Ho [Korea Institute of Materials Science, Changwon (Korea, Republic of)

    2017-05-15

    The effects of the annealing temperature on the microstructure and tensile properties of cold-rolled light-weight steels are investigated using two Fe-30Mn-xAl-0.9C alloys that contain different Al content. The initial alloy microstructure is composed of a single austenite or a mixture of austenite and ferrite depending on the nominal aluminum content. For the alloy with 9 wt%Al content, the recrystallization and grain growth of austenite occurrs depending on the annealing temperature. However, for the alloy with 11 wt%Al content, the β-Mn phase is observed after annealing for 10 min at 550~800 ℃. The β-Mn transformation kinetics is the fastest at 700 ℃. The formation of the β-Mn phase has a detrimental effect on the ductility, and this leads to significant decreases in the total elongation. The same alloy also forms κ-carbide and DO3 ordering at 550~900 ℃. The investigated alloys exhibit a fully recrystallized microstructure after annealing at 900 ℃ for 10 min, which results in a high total elongation of 25~55%with a high tensile strength of 900~1170 MPa.

  3. Woven hybrid composites: Tensile and flexural properties of oil palm-woven jute fibres based epoxy composites

    Energy Technology Data Exchange (ETDEWEB)

    Jawaid, M. [School of Industrial Technology, Universiti Sains Malaysia, 11800 Penang (Malaysia); Abdul Khalil, H.P.S., E-mail: akhalilhps@gmail.com [School of Industrial Technology, Universiti Sains Malaysia, 11800 Penang (Malaysia); Abu Bakar, A. [School of Materials and Mineral Resources Engineering, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia)

    2011-06-15

    Highlights: {yields} Woven hybrid composites show good tensile and flexural properties. {yields} Hybridization with 20% woven jute gives rise to sufficient modulus to composites. {yields} Layering pattern affect mechanical properties of hybrid composites. {yields} Statistical analysis shows that there is significant difference between composites. - Abstract: In this research, tensile and flexural performance of tri layer oil palm empty fruit bunches (EFB)/woven jute (Jw) fibre reinforced epoxy hybrid composites subjected to layering pattern has been experimentally investigated. Sandwich composites were fabricated by hand lay-up technique in a mould and cured with 105 deg. C temperatures for 1 h by using hot press. Pure EFB and woven jute composites were also fabricate for comparison purpose. Results showed that tensile and flexural properties of pure EFB composite can be improved by hybridization with woven jute fibre as extreme woven jute fibre mat. It was found that tensile and flexural properties of hybrid composite is higher than that of EFB composite but less than woven jute composite. Statistical analysis of composites done by ANOVA-one way, it showed significant differences between the results obtained. The fracture surface morphology of the tensile samples of the hybrid composites was performed by using scanning electron microscopy.

  4. Woven hybrid composites: Tensile and flexural properties of oil palm-woven jute fibres based epoxy composites

    International Nuclear Information System (INIS)

    Jawaid, M.; Abdul Khalil, H.P.S.; Abu Bakar, A.

    2011-01-01

    Highlights: → Woven hybrid composites show good tensile and flexural properties. → Hybridization with 20% woven jute gives rise to sufficient modulus to composites. → Layering pattern affect mechanical properties of hybrid composites. → Statistical analysis shows that there is significant difference between composites. - Abstract: In this research, tensile and flexural performance of tri layer oil palm empty fruit bunches (EFB)/woven jute (Jw) fibre reinforced epoxy hybrid composites subjected to layering pattern has been experimentally investigated. Sandwich composites were fabricated by hand lay-up technique in a mould and cured with 105 deg. C temperatures for 1 h by using hot press. Pure EFB and woven jute composites were also fabricate for comparison purpose. Results showed that tensile and flexural properties of pure EFB composite can be improved by hybridization with woven jute fibre as extreme woven jute fibre mat. It was found that tensile and flexural properties of hybrid composite is higher than that of EFB composite but less than woven jute composite. Statistical analysis of composites done by ANOVA-one way, it showed significant differences between the results obtained. The fracture surface morphology of the tensile samples of the hybrid composites was performed by using scanning electron microscopy.

  5. Tensile properties of irradiated TZM and tungsten

    International Nuclear Information System (INIS)

    Steichen, J.M.

    1975-04-01

    The effect of neutron irradiation on the elevated temperature tensile properties of TZM and tungsten has been experimentally determined. Specimens were irradiated at a temperature of approximately 720 0 F to fluences of 0.4 and 0.9 x 10 22 n/cm 2 (E greater than 0.1 MeV). Test parameters for both control and irradiated specimens included strain rates from 3 x 10 -4 to 1 s -1 and temperatures from 72 to 1700 0 F. The results of these tests were correlated with a rate-temperature parameter (T ln A/epsilon) to provide a concise description of material behavior over the range of deformation conditions of this study. The yield strength of the subject materials was significantly increased by decreasing temperature, increasing strain rate, and increasing fluence. Ductility was significantly reduced at any temperature or strain rate by increasing fluence. Cleavage fractures occurred in both unirradiated and irradiated specimens when the yield strength was elevated to the effective cleavage stress by temperature and/or strain rate. Neutron irradiation for the conditions of this study increased the ductile-to-brittle transition temperature of tungsten by approximately 300 0 F and TZM by approximately 420 0 F. (U.S.)

  6. Influence of heat treatment on microstructure and tensile properties of a cast Al-Cu-Si-Mn alloy

    Directory of Open Access Journals (Sweden)

    Liu Zhixue

    2013-11-01

    Full Text Available Solution and aging treatments are important approaches to improve mechanical properties and microstructure of aluminum-base alloys. In this research, a new type high strength Al-Cu-Si-Mn cast alloy was prepared. The effect of different solution and aging treatment temperatures on microstructure and mechanical properties of the Al-Cu-Si-Mn cast alloy were studied by means of microstructure observation and mechanical properties testing. Results showed that after solution treated at different temperatures for 12 h and aged at 175 ℃ for 12 h, with the increase of the solution temperature, both the tensile strength and the elongation of the alloy firstly increase and then decrease, and reach their peak values at 530 ℃. When the solution temperature is below 530 ℃, the microstructure of the alloy consists of α phase, undissolved θ phase and T phase; while when it exceeds 530 ℃, the microstructure only consists of α phase and T phase. After solution treated at 530 ℃ for 12 h and aged at different temperatures for 12 h, both the tensile strength and the elongation of the alloy firstly increase and then decrease with the increasing of temperature, and reach their peak values at 175 ℃. Therefore, the optimal heat treatment process for the alloy in this study is 12 h solution at 530 ℃ and 12 h aging at 175 ℃, and the corresponding tensile strength is 417 MPa, elongation is 4.0%.

  7. Tensile properties of four types of austenitic stainless steel welded joints

    International Nuclear Information System (INIS)

    Balladon, P.

    1990-01-01

    In the field of an LMFBR research programme on austenitic stainless steel welds in a Shared Cost Action Safety, Research Area 8, coordinated by JRC-Ispra, four cooperating laboratories (ECN, IKE/MPA, the Welding Institute and UNIREC) have been involved in the fabrication and extensive characterization of welded joints made from one plate of ICL 167 stainless steel. The materials included parent metal, four vacuum electron beam welds, one non vacuum electron beam weld, one submerged arc weld, one gas metal arc weld and one manual metal arc weld. This report summarizes the 106 tensile tests performed at room temperature and 550 0 C, including the influence of strain rate, specimen orientation and welding procedure. Main results are that electron beam welds have tensile properties close to those of parent metal with higher values of yield strength in longitudinal orientation and lower values of total elongation in transverse orientation but with a similar reduction of area, that filler metal welds own the highest values of yield strength and lowest values of ductility. Most of the welds properties are higher than the minimum specified for parent metal, except for some values of total elongation, mainly in transverse orientation. In view of using electron beam welding for production of components used in LMFBR, results obtained show that tensile properties of electron beam welds compare well to those of classical welds. (author)

  8. The influence of prior ageing on microstructure, tensile properties and hot hardness of alloy 800HT

    International Nuclear Information System (INIS)

    El-Magd, E.

    1996-01-01

    For high temperature applications especially in the construction of equipment, carbide strengthened steels are widely used because of their good mechanical properties and relatively low cost. These materials undergo microstructural changes under such service conditions which contribute greatly to the strength properties and thus play an important role in equipment design considerations. The influence of a prior thermal ageing on the tensile strength values and the hot hardness of the austenitic iron base alloy, Alloy 800HT, is examined in this work. It was therefore necessary to carry out tensile and hot hardness tests with the solution treated and overaged material at ranges between room temperature and 900 . The microstructural changes are investigated using lightmicroscopy, SEM and TEM. The changes of the material properties with thermal pretreatment conditions is studied and discussed in the context of the determined microstructural development. (orig.) [de

  9. Effects of Ce Addition and Isothermal Aging on the Elevated Temperature Tensile Properties of Mechanically Alloyed Al-Ti Alloys

    Energy Technology Data Exchange (ETDEWEB)

    Kim, JunKi; Oh, YoungMin; Kim, YongDeog; Kim, SeonJin [Hanyang Univ., Seoul (Korea, Republic of); Kim, ByungChul [KOREA ATOMIC RESEARCH INSTITUTE, TAEJON (Korea, Republic of)

    1997-05-01

    The room and elevated temperature tensile strength of mechanically alloyed Al-8wt%. Ti alloy increased by substituting Ce for Ti up to 25at.%. However, further substitution of Ce for Ti decreased the tensile strength. It was considered to be due to the decrease of volume fraction of Ce contained dispersoid. In the meantime, the decrease of tensile strength due to the isothermal aging was effectively reduced by the addition of Ce at 400 deg. C but not 510 deg. C. The activation energies for the deformation of Al-80wt.%(Ti+Ce)alloys measured at the temperature between 300 deg. C{approx}510 deg. C were about 1.3{approx}1.9 times higher than that for pure Al self-diffusion(142 kJ/mole). Thus, it was considered that the elevated temperature deformation of Al-8wt.%(Ti+Ce)alloys was governed by Orowan mechanism (author). 9 refs. 6 figs.

  10. Elevated Temperature Tensile Tests on DU–10Mo Rolled Foils

    Energy Technology Data Exchange (ETDEWEB)

    Schulthess, Jason [Idaho National Lab. (INL), Idaho Falls, ID (United States)

    2014-09-01

    Tensile mechanical properties for uranium-10 wt.% molybdenum (U–10Mo) foils are required to support modeling and qualification of new monolithic fuel plate designs. It is expected that depleted uranium-10 wt% Mo (DU–10Mo) mechanical behavior is representative of the low enriched U–10Mo to be used in the actual fuel plates, therefore DU-10Mo was studied to simplify material processing, handling, and testing requirements. In this report, tensile testing of DU-10Mo fuel foils prepared using four different thermomechanical processing treatments were conducted to assess the impact of foil fabrication history on resultant tensile properties.

  11. Tensile properties and flow behavior analysis of modified 9Cr–1Mo steel clad tube material

    Energy Technology Data Exchange (ETDEWEB)

    Singh, Kanwarjeet, E-mail: kanwar722@yahoo.com; Latha, S.; Nandagopal, M.; Mathew, M.D.; Laha, K.; Jayakumar, T.

    2014-11-15

    The tensile properties and flow behavior of modified 9Cr–1Mo steel clad tube have been investigated in the framework of various constitutive equations for a wide range of temperatures (300–923 K) and strain rates (3 × 10{sup −3} s{sup −1}, 3 × 10{sup −4} s{sup −1} and 3 × 10{sup −5} s{sup −1}). The tensile flow behavior of modified 9Cr–1Mo steel clad tube was most accurately described by Voce equation. The variation of instantaneous work hardening rate (θ = dσ/dε) and σθ with stress (σ) indicated two stage behavior characterized by rapid decrease at low stresses (transient stage) followed by a gradual decrease in high stresses (Stage III). The variation of work hardening parameters and work hardening rate in terms of θ vs. σ and σθ vs. σ with temperature exhibited three distinct regimes. Rapid decrease in flow stress and work hardening parameters and rapid shift of θ vs. σ and σθ vs. σ towards low stresses with increase in temperature indicated dynamic recovery at high temperatures. Tensile properties of the material have been best predicted from Voce equation.

  12. Microstructure and Tensile/Corrosion Properties Relationships of Directionally Solidified Al-Cu-Ni Alloys

    Science.gov (United States)

    Rodrigues, Adilson V.; Lima, Thiago S.; Vida, Talita A.; Brito, Crystopher; Garcia, Amauri; Cheung, Noé

    2018-03-01

    Al-Cu-Ni alloys are of scientific and technological interest due to high strength/high temperature applications, based on the reinforcement originated from the interaction between the Al-rich phase and intermetallic composites. The nature, morphology, size, volume fraction and dispersion of IMCs particles throughout the Al-rich matrix are important factors determining the resulting mechanical and chemical properties. The present work aims to evaluate the effect of the addition of 1wt%Ni into Al-5wt%Cu and Al-15wt%Cu alloys on the solidification rate, macrosegregation, microstructure features and the interrelations of such characteristics on tensile and corrosion properties. A directional solidification technique is used permitting a wide range of microstructural scales to be examined. Experimental growth laws relating the primary and secondary dendritic spacings to growth rate and solidification cooling rate are proposed, and Hall-Petch type equations are derived relating the ultimate tensile strength and elongation to the primary dendritic spacing. Considering a compromise between ultimate tensile strength and corrosion resistance of the examined alloys samples from both alloys castings it is shown that the samples having more refined microstructures are associated with the highest values of such properties.

  13. Elevated temperature tensile and creep behavior of a SiC fiber-reinforced titanium metal matrix composite. Final Report, 22 Dec. 1994 M.S. Thesis, 7 May 1993

    Science.gov (United States)

    Thurston, Rita J.

    1995-01-01

    In this research program, the tensile properties and creep behavior in air of (0)(sub 4), (0/90)(sub s) and (90)(sub 4) SCS-9/Beta 21S composite layups with 0.24 volume fraction fiber were evaluated. Monotonic tensile tests at 23, 482, 650 and 815 C yielded the temperature dependence of the elastic modulus, proportional limit, ultimate tensile strength and total strain at failure. At 650 C, the UTS of the (0)(sub 4) and (0/90)(sub s) layups decreases by almost 50 percent from the room temperature values, indicating that operating temperatures should be less than 650 C to take advantage of the specific tensile properties of these composites.

  14. A user's manual for managing database system of tensile property

    International Nuclear Information System (INIS)

    Ryu, Woo Seok; Park, S. J.; Kim, D. H.; Jun, I.

    2003-06-01

    This manual is written for the management and maintenance of the tensile database system for managing the tensile property test data. The data base constructed the data produced from tensile property test can increase the application of test results. Also, we can get easily the basic data from database when we prepare the new experiment and can produce better result by compare the previous data. To develop the database we must analyze and design carefully application and after that, we can offer the best quality to customers various requirements. The tensile database system was developed by internet method using Java, PL/SQL, JSP(Java Server Pages) tool

  15. Comparative study on the high-temperature tensile and creep properties of Alloy 617 base and weld metals

    International Nuclear Information System (INIS)

    Kim, Woo Gon; Hong, Sung Deok; Kim, Yong Wan; Kim, Seon Jin; Park, Jae Young; Ekaputra, I. M. W.

    2013-01-01

    This paper presents a comparative investigation on the high-temperature tensile and creep properties of Alloy 617 base metal (BM) and weld metal (WM) fabricated by a gas tungsten arc weld process. The WM had higher yield strength and lower ultimate tensile strength than the BM does; however, its elongation was significantly lower than that of the BM. The creep curve of the BM and WM was somewhat different from that of typical heat-resistance steel, and did not show a textbook creep. The WM exhibited a longer creep rupture life, lower creep rate, and lower rupture ductility than the BM. However, as the creep rupture time reached approximately 36,800 h, the creep life of the WM was expected to be almost similar to that of the BM; and after 36,800 h, its creep life was expected to be worse than the BM. Loner creep tests is needed to investigate the long-term creep life of the WM. The creep failure mode of the BM and WM was obviously an intergranular cracking of the cavity formation and growth mechanisms, although it was more evident in the WM. The BM had a more ductile fracture surface than the WM

  16. Tensile properties of latex paint films with TiO2 pigment

    Science.gov (United States)

    Hagan, Eric W. S.; Charalambides, Maria N.; Young, Christina T.; Learner, Thomas J. S.; Hackney, Stephen

    2009-05-01

    The tensile properties of latex paint films containing TiO2 pigment were studied with respect to temperature, strain-rate and moisture content. The purpose of performing these experiments was to assist museums in defining safe conditions for modern paintings held in collections. The glass transition temperature of latex paint binders is in close proximity to ambient temperature, resulting in high strain-rate dependence in typical exposure environments. Time dependence of modulus and failure strain is discussed in the context of time-temperature superposition, which was used to extend the experimental time scale. Nonlinear viscoelastic material models are also presented, which incorporate a Prony series with the Ogden or Neo-Hookean hyperelastic function for different TiO2 concentrations.

  17. Effect of test temperature and strain rate on the tensile properties of high-strength, high-conductivity copper alloys

    Energy Technology Data Exchange (ETDEWEB)

    Zinkle, S.J.; Eatherly, W.S. [Oak Ridge National Lab., TN (United States)

    1997-04-01

    The unirradiated tensile properties of wrought GlidCop AL25 (ITER grade zero, IGO) solutionized and aged CuCrZr, and cold-worked and aged and solutionized and aged Hycon 3HP{trademark} CuNiBe have been measured over the temperature range of 20-500{degrees}C at strain rates between 4 x 10{sup {minus}4} s{sup {minus}1} and 0.06 s{sup {minus}1}. The measured room temperature electrical conductivity ranged from 64 to 90% IACS for the different alloys. All of the alloys were relatively insensitive to strain rate at room temperature, but the strain rate sensitivity of GlidCop Al25 increased significantly with increasing temperature. The CuNiBe alloys exhibited the best combination of high strength and high conductivity at room temperature. The strength of CuNiBe decreased slowly with increasing temperature. However, the ductility of CuNiBe decreased rapidly with increasing temperature due to localized deformation near grain boundaries, making these alloy heats unsuitable for typical structural applications above 300{degrees}C. The strength and uniform elongation of GlidCop Al25 decreased significantly with increasing temperature at a strain rate of 1 x 10{sup {minus}3} s{sup {minus}1}, whereas the total elongation was independent of test temperature. The strength and ductility of CuCrZr decreased slowly with increasing temperature.

  18. Tensile properties of quadruple melted Zr-2.5Nb pressure tubes evaluated from pressure tube offcuts

    International Nuclear Information System (INIS)

    Shah, Priti Kotak; Dubey, J.S.; Anantharaman, S.

    2013-12-01

    Rajasthan Atomic Power Station-2 (RAPS-2) is the first Pressurised Heavy Water Reactor (PHWR) in India having quadruple melted Zr-2.5Nb pressure tubes. Front-end and back-end off-cuts of sixteen pressure tubes were selected for studying the mechanical properties in axial and transverse directions of the tube. Tension tests were carried out at room temperature and at 300℃ using miniature tensile test specimens. The report presents the experimental details and discusses the base line tensile property data for the quadruple melted pressure tubes of RAPS-2. This data will be useful for the reactor life management. (author)

  19. Elevated temperature mechanical properties of line pipe steels

    Science.gov (United States)

    Jacobs, Taylor Roth

    The effects of test temperature on the tensile properties of four line pipe steels were evaluated. The four materials include a ferrite-pearlite line pipe steel with a yield strength specification of 359 MPa (52 ksi) and three 485 MPa (70 ksi) yield strength acicular ferrite line pipe steels. Deformation behavior, ductility, strength, strain hardening rate, strain rate sensitivity, and fracture behavior were characterized at room temperature and in the temperature range of 200--350 °C, the potential operating range for steels used in oil production by the steam assisted gravity drainage process. Elevated temperature tensile testing was conducted on commercially produced as-received plates at engineering strain rates of 1.67 x 10 -4, 8.33 x 10-4, and 1.67 x 10-3 s-1. The acicular ferrite (X70) line pipe steels were also tested at elevated temperatures after aging at 200, 275, and 350 °C for 100 h under a tensile load of 419 MPa. The presence of serrated yielding depended on temperature and strain rate, and the upper bound of the temperature range where serrated yielding was observed was independent of microstructure between the ferrite-pearlite (X52) steel and the X70 steels. Serrated yielding was observed at intermediate temperatures and continuous plastic deformation was observed at room temperature and high temperatures. All steels exhibited a minimum in ductility as a function of temperature at testing conditions where serrated yielding was observed. At the higher temperatures (>275 °C) the X52 steel exhibited an increase in ductility with an increase in temperature and the X70 steels exhibited a maximum in ductility as a function of temperature. All steels exhibited a maximum in flow strength and average strain hardening rate as a function of temperature. The X52 steel exhibited maxima in flow strength and average strain hardening rate at lower temperatures than observed for the X70 steels. For all steels, the temperature where the maximum in both flow

  20. Influence of HIP pressure on tensile properties of a 14Cr ODS ferritic steel

    Energy Technology Data Exchange (ETDEWEB)

    Oksiuta, Z., E-mail: z.oksiuta@pb.edu.pl [Bialystok Technical University, Mechanical Department, Wiejska 45c, 15-351 Bialystok (Poland); Ozieblo, A.; Perkowski, K.; Osuchowski, M. [Institute of Ceramics and Building Materials, Postępu 9, 02-676 Warsaw (Poland); Lewandowska, M. [Warsaw University of Technology, Woloska 141, 02-504 Warsaw (Poland)

    2014-02-15

    Highlights: • The HIPping parameters of the 14Cr–2W–0.3Ti–0.3Y{sub 2}O{sub 3} ODS steel powder were investigated. • The density and microstructure of the tested specimens after HIPping were studied. • The mechanical properties, high temperature tensile tests, were performed. • Residual porosity was observed in all tested specimens. • HIPping pressure has negligible influence on the strength of the ODS steel however improves material ductility. - Abstract: An oxide dispersion strengthened ferritic steel with a nominal composition of Fe–14Cr–2W–0.3Ti–0.3Y{sub 2}O{sub 3} (in wt.%) was consolidated by hot isostatic pressing at 1150 °C under various pressures in the range of 185–300 MPa for 3 h. The microstructure, microhardness and high temperature tensile properties of the steel were investigated. With increasing compaction pressure the density of specimens also increased, however OM and SEM observations revealed residual porosity in all tested specimens and similar ferritic microstructure with bimodal-like grains and numerous of large oxide particles, located at the grain boundaries. Mechanical testing revealed that compaction pressure has negligible influence on the hardness and tensile strength of the ODS steel, however improves the material ductility.

  1. Influence of HIP pressure on tensile properties of a 14Cr ODS ferritic steel

    International Nuclear Information System (INIS)

    Oksiuta, Z.; Ozieblo, A.; Perkowski, K.; Osuchowski, M.; Lewandowska, M.

    2014-01-01

    Highlights: • The HIPping parameters of the 14Cr–2W–0.3Ti–0.3Y 2 O 3 ODS steel powder were investigated. • The density and microstructure of the tested specimens after HIPping were studied. • The mechanical properties, high temperature tensile tests, were performed. • Residual porosity was observed in all tested specimens. • HIPping pressure has negligible influence on the strength of the ODS steel however improves material ductility. - Abstract: An oxide dispersion strengthened ferritic steel with a nominal composition of Fe–14Cr–2W–0.3Ti–0.3Y 2 O 3 (in wt.%) was consolidated by hot isostatic pressing at 1150 °C under various pressures in the range of 185–300 MPa for 3 h. The microstructure, microhardness and high temperature tensile properties of the steel were investigated. With increasing compaction pressure the density of specimens also increased, however OM and SEM observations revealed residual porosity in all tested specimens and similar ferritic microstructure with bimodal-like grains and numerous of large oxide particles, located at the grain boundaries. Mechanical testing revealed that compaction pressure has negligible influence on the hardness and tensile strength of the ODS steel, however improves the material ductility

  2. Effect of heat treatments on the tensile and electrical properties of high-strength, high-conductivity copper alloys

    Energy Technology Data Exchange (ETDEWEB)

    Zinkle, S.J.; Eatherly, W.S. [Oak Ridge National Lab., TN (United States)

    1997-08-01

    The unirradiated tensile properties of CuCrZr produced by two different vendors have been measured following different heat treatments. Room temperature electrical resistivity measurements were also performed in order to estimate the thermal conductivity of these specimens. The thermomechanical conditions studied included solution quenched, solution quenched and aged (ITER reference heat treatment), simulated slow HIP thermal cycle ({approximately}1{degrees}C/min cooling from solutionizing temperature) and simulated fast HIP thermal cycle ({approximately}100{degrees}C/min cooling from solutionizing temperature). Specimens from the last two heat treatments were tested in both the solution-cooled condition and after subsequent precipitate aging at 475{degrees}C for 2 h. Both of the simulated HIP thermal cycles caused a pronounced decreases in the strength and electrical conductivity of CuCrZr. The tensile and electrical properties were unchanged by subsequent aging in the slow HIP thermal cycles caused a pronounced decrease in the strength and electrical conductivity of CuCrZr. The tensile and electrical properties were unchanged by subsequent aging in the slow HIP thermal cycle specimens, whereas the strength and conductivity following aging in the fast HIP thermal cycle improved to {approximately}65% of the solution quenched and aged CuCrZr values. Limited tensile and electrical resistivity measurements were also made on two new heats of Hycon 3HP CuNiBe. High strength but poor uniform and total elongations were observed at 500{degrees}C on one of these new heats of CuNiBe, similar to that observed in other heats.

  3. Effect of heat treatments on the tensile and electrical properties of high-strength, high-conductivity copper alloys

    International Nuclear Information System (INIS)

    Zinkle, S.J.; Eatherly, W.S.

    1997-01-01

    The unirradiated tensile properties of CuCrZr produced by two different vendors have been measured following different heat treatments. Room temperature electrical resistivity measurements were also performed in order to estimate the thermal conductivity of these specimens. The thermomechanical conditions studied included solution quenched, solution quenched and aged (ITER reference heat treatment), simulated slow HIP thermal cycle (∼1 degrees C/min cooling from solutionizing temperature) and simulated fast HIP thermal cycle (∼100 degrees C/min cooling from solutionizing temperature). Specimens from the last two heat treatments were tested in both the solution-cooled condition and after subsequent precipitate aging at 475 degrees C for 2 h. Both of the simulated HIP thermal cycles caused a pronounced decreases in the strength and electrical conductivity of CuCrZr. The tensile and electrical properties were unchanged by subsequent aging in the slow HIP thermal cycles caused a pronounced decrease in the strength and electrical conductivity of CuCrZr. The tensile and electrical properties were unchanged by subsequent aging in the slow HIP thermal cycle specimens, whereas the strength and conductivity following aging in the fast HIP thermal cycle improved to ∼65% of the solution quenched and aged CuCrZr values. Limited tensile and electrical resistivity measurements were also made on two new heats of Hycon 3HP CuNiBe. High strength but poor uniform and total elongations were observed at 500 degrees C on one of these new heats of CuNiBe, similar to that observed in other heats

  4. Tensile properties of interwoven hemp/PET (Polyethylene Terephthalate) epoxy hybrid composites

    Science.gov (United States)

    Ahmad, M. A. A.; Majid, M. S. A.; Ridzuan, M. J. M.; Firdaus, A. Z. A.; Amin, N. A. M.

    2017-10-01

    This paper describes the experimental investigation of the tensile properties of interwoven Hemp/PET hybrid composites. The effect of hybridization of hemp (warp) with PET fibres (weft) on tensile properties was of interest. Hemp and PET fibres were selected as the reinforcing material while epoxy resin was chosen as the matrix. The interwoven Hemp/PET fabric was used to produce hybrid composite using a vacuum infusion process. The tensile test was conducted using Universal Testing Machine in accordance to the ASTM D638. The tensile properties of the interwoven Hemp/PET hybrid composite were then compared with the neat woven hemp/epoxy composite. The results show that the strength of hemp/PET with the warp direction was increased by 8% compared to the neat woven hemp composite. This enhancement of tensile strength was due to the improved interlocking structure of interwoven Hemp/PET hybrid fabric.

  5. Selective Laser Melting Produced Ti-6Al-4V: Post-Process Heat Treatments to Achieve Superior Tensile Properties.

    Science.gov (United States)

    Ter Haar, Gerrit M; Becker, Thorsten H

    2018-01-17

    Current post-process heat treatments applied to selective laser melting produced Ti-6Al-4V do not achieve the same microstructure and therefore superior tensile behaviour of thermomechanical processed wrought Ti-6Al-4V. Due to the growing demand for selective laser melting produced parts in industry, research and development towards improved mechanical properties is ongoing. This study is aimed at developing post-process annealing strategies to improve tensile behaviour of selective laser melting produced Ti-6Al-4V parts. Optical and electron microscopy was used to study α grain morphology as a function of annealing temperature, hold time and cooling rate. Quasi-static uniaxial tensile tests were used to measure tensile behaviour of different annealed parts. It was found that elongated α'/α grains can be fragmented into equiaxial grains through applying a high temperature annealing strategy. It is shown that bi-modal microstructures achieve a superior tensile ductility to current heat treated selective laser melting produced Ti-6Al-4V samples.

  6. Tensile Mechanical Property of Oil Palm Empty Fruit Bunch Fiber Reinforced Epoxy Composites

    Science.gov (United States)

    Ghazilan, A. L. Ahmad; Mokhtar, H.; Shaik Dawood, M. S. I.; Aminanda, Y.; Ali, J. S. Mohamed

    2017-03-01

    Natural, short, untreated and randomly oriented oil palm empty fruit bunch fiber reinforced epoxy composites were manufactured using vacuum bagging technique with 20% fiber volume composition. The performance of the composite was evaluated as an alternative to synthetic or conventional reinforced composites. Tensile properties such as tensile strength, modulus of elasticity and Poisson’s ratio were compared to the tensile properties of pure epoxy obtained via tensile tests as per ASTM D 638 specifications using Universal Testing Machine INSTRON 5582. The tensile properties of oil palm empty fruit bunch fiber reinforced epoxy composites were lower compared to plain epoxy structure with the decrement in performances of 38% for modulus of elasticity and 61% for tensile strength.

  7. Tensile and Compressive Properties of Woven Kenaf/Glass Sandwich Hybrid Composites

    Directory of Open Access Journals (Sweden)

    Mohaiman J. Sharba

    2016-01-01

    Full Text Available Monotonic (tensile and compression properties of woven kenaf/glass reinforced unsaturated polyester sandwich hybrid composites have been experimentally investigated. Five types of composites laminates were fabricated using a combination of hand lay-up and cold press techniques, postcured for two hours at 80°C and left for 48 hours at room temperature. The hybrid composites contained fixed six layers of glass as a shell, three on each side, whereas the number of core kenaf layers was changed in three stages to get S1, S2, and S3 hybrid composites. Composites specimens with pure glass and kenaf were also fabricated for comparison. It was found that one kenaf layer replaced about 20% of total fiber weight fraction of the composite; this leads to reducing the density of final hybrid composite by 13%. Besides, in mechanical properties perspective, there are less than 1% reduction in compression strength and 40% in tensile strength when compared to pure glass composite. Generally, the results revealed that the best performance was observed in S1, which showed a good balance of all mechanical properties determined in this work.

  8. Preliminary study on tensile properties and fractography of the recycled aluminum cast product

    International Nuclear Information System (INIS)

    Hishamuddin Hussain; Mohd Harun; Hafizal Yazid; Shaiful Rizam Shamsudin; Zaiton Selamat; Mohd Shariff Sattar

    2004-01-01

    Among many mechanical properties of materials, tensile properties are probably the most frequently considered, evaluated, and referred by the industry. This paper presents the result of preliminary study regarding the tensile properties and fractography of the recycled aluminum cast product. For this purpose, three sets of specimen were prepared for tensile testing by using permanent mold casting technique. The cast products are in durable shaped tensile specimens with the gauge length of 50mm. The tensile testing was conducted in accordance with BS EN 10002-1 and ISO 6892 standards. Fracture surface analysis was also conducted to understand materials behaviour. (Author)

  9. Effect of heat treatment on microstructures and tensile properties of Ni-base superalloy M963

    International Nuclear Information System (INIS)

    He, L.Z.; Zheng, Q.; Sun, X.F.; Guan, H.R.; Hu, Z.Q.; Tieu, A.K.; Lu, C.; Zhu, H.T.

    2005-01-01

    The effect of solution treatment (ST) on tensile properties of M963 Ni-base superalloy tested at 800 deg. C has been investigated. The detailed microstructures, fracture surfaces and dislocation structures are examined through energy dispersive X-ray analysis (EDAX), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). With increasing solution treated temperature, the yield strength (YS) and ultimate tensile strength (UTS) increase, however, the elongation decreases. Microstructural observations show that the morphologies of carbide, primary γ' and re-precipitated γ' change significantly with increasing solution treated temperature. The main deformation mode is γ' by-pass when solution treated temperature is lower than 1220 deg. C, and changes to γ' shearing at 1230 deg. C. The interface of carbide with matrix is the main site of crack initiation and propagation under all testing conditions

  10. Influence of deuterium content on tensile behavior of Zr-2.5Nb pressure tube material in the temperature range of ambient to 300 degC

    International Nuclear Information System (INIS)

    Bind, A.K.; Singh, R.N.; Chakravartty, J.K.; Dhandharia, Priyesh; Ghosh, Agnish; More, Nitin S.; Chhatre, A.G.; Vijayakumar, S.

    2011-08-01

    Tensile properties of autoclaved zirconium-2.5 wt. % niobium pressure tube material were evaluated by uniaxial tension tests at temperatures between 25 and 300 degC and under strain-rates of 1.075 x 10 -4 /s. Six number of Zr-2.5Nb alloy pressure tube spools of length 130 mm were obtained from pressure tube number 19-2557-2. Five spools were polished with abrasive paper to remove the oxide layer. These spools were gaseously charged with controlled amount of deuterium. The target deuterium concentrations were 25, 50, 75, 100 and 200 wppm of hydrogen equivalent. Ten samples were machined by EDM wire cutting from every spool. The tensile specimen axis was oriented along longitudinal direction of the tube. Metallographic examination of the deuterium charged samples suggested that the deuterides were predominantly circumferential deuterides. Analysis of tensile results showed that both yield and ultimate tensile strengths of this alloy decreased monotonically with increasing test temperatures. The tensile ductility decreased marginally with increase in test temperature from ambient to 300 degC. It was also observed that both strength and ductility appear to be unaffected by deuterium content at all temperatures, thereby suggesting that at least up to 200 wppm (Heq.) of deuterium tensile properties are not influenced by deuterium. (author)

  11. Tensile properties of compressed moulded Napier/glass fibre reinforced epoxy composites

    Science.gov (United States)

    Fatinah, T. S.; Majid, M. S. Abdul; Ridzuan, M. J. M.; Hong, T. W.; Amin, N. A. M.; Afendi, M.

    2017-10-01

    This paper describes the experimental investigation of the tensile properties of compressed moulded Napier grass fibres reinforced epoxy composites. The effect of treatment 5% sodium hydroxide (NaOH) concentrated solution and hybridization of Napier with CSM E-glass fibres on tensile properties was also studied. The untreated and treated Napier fibres with 25% fibre loading were fabricated with epoxy resin by a cold press process. 7% fibre loading of CSM glass fibre was hybrid as the skin layer for 18% fibre loading of untreated Napier grass fibre. The tensile tests were conducted using Universal Testing Machine in accordance with ASTM D638. The tensile properties of the untreated Napier/epoxy composites were compared with treated Napier/epoxy and untreated Napier/CSM/epoxy composites. The results demonstrated that the tensile performance of untreated Napier fibre composites was significantly improved by both of the modification; alkali treatment and glass fibre hybridization. Napier grass fibres showed promising potentials to be used as reinforcement in the polymer based composites.

  12. Mechanical Property and Its Comparison of Superalloys for High Temperature Gas Cooled Reactor

    International Nuclear Information System (INIS)

    Kim, Woo Gon; Kim, D. W.; Ryu, W. S.; Han, C. H.; Yoon, J. H.; Chang, J.

    2005-01-01

    Since structural materials for high temperature gas cooled reactor are used during long period in nuclear environment up to 1000 .deg. C, it is important to have good properties at elevated temperature such as mechanical properties (tensile, creep, fatigue, creep-fatigue), microstructural stability, interaction between metal and gas, friction and wear, hydrogen and tritium permeation, irradiation behavior, corrosion by impurity in He. Thus, in order to select excellent materials for the high temperature gas cooled reactor, it is necessary to understand the material properties and to gather the data for them. In this report, the items related to material properties which are needed for designing the high temperature gas cooled reactor were presented. Mechanical properties; tensile, creep, and fatigue etc. were investigated for Haynes 230, Hastelloy-X, In 617 and Alloy 800H, which can be used as the major structural components, such as intermediate heat exchanger (IHX), hot duct and piping and internals. Effect of He and irradiation on these structural materials was investigated. Also, mechanical properties; physical properties, tensile properties, creep and creep crack growth rate were compared for them, respectively. These results of this report can be used as important data to select superior materials for high temperature gas reactor

  13. Thermal and tensile properties of alumina filled PET nanocomposites

    Science.gov (United States)

    Nikam, Pravin N.; Deshpande, Vineeta D.

    2018-05-01

    In the present investigation, nanocomposites of poly(ethylene terephathalate)(PET) with different content (0 to 5 wt.%) of alumina nanoparticles (n-Al2O3) were prepared by melt-extrusion technique. Morphological characterization of samples was examined by transmission electron microscopy (TEM). Morphological analysis revealed that degree of dispersion of alumina nanoparticles (ANPs) was increased at lower content (i.e. upto 2 wt.%), which observed by TEM. Thermal and tensile measurements were carried out using and differential scanning calorimetry (DSC) and universal testing machine (UTM). The thermal analysis showed that the glass transition termperature (Tg), melting temperature (Tm), crystallization temperature (Tc) of PET/alumina nanocomposites (PNCs) were higher than neat PET (PET0). The heat enthalpy (ΔHm) of crystallization for PNCs was increased compared to PET0, which indicates that degree of crystallinity of PNCs also increased compared to PET0. The half-time (t0.5) of crystallization of PNCs were decreased compared to PET0 which indicates that the incorporation of ANPs nucleate the PET molecular chains and allowing the easily crystallization during nonisothermal process. The tensile analysis revealed that the tensile elastic modulus (i.e. Young's modulus) of PNCs increased almost linearly with increasing the content of ANPs while tensile elongation at break decreased nonlinearly. The tensile strength of PNCs increased with a 1 wt.% of ANPs whereas the higher content of ANPs decreased the tensile strength.

  14. Tensile properties of V-Cr-Ti alloys after exposure in helium and low-partial-pressure oxygen environments

    Energy Technology Data Exchange (ETDEWEB)

    Natesan, K.; Soppet, W.K. [Argonne National Lab., IL (United States)

    1997-04-01

    A test program is in progress to evaluate the effect of oxygen at low pO{sub 2} on the tensile properties of V-(4-5)wt% Cr-(4-5)wt% Ti alloys. Some of the tensile specimens were precharged with oxygen at low pO{sub 2} at 500{degrees}C and reannealed in vacuum at 500{degrees}C in environments with various pO{sub 2} levels and subsequently tensile tested at room temperature. The preliminary results indicate that both approaches are appropriate for evaluating the effect of oxygen uptake on the tensile properties of the alloys. The data showed that in the relatively short-time tests conducted thus far, the maximum engineering stress slightly increased after oxygen exposure but the uniform and total elongation values exhibited significant decrease after exposure in oxygen-containing environments. The data for a specimen exposed to a helium environment were similar to those obtained in low pO{sub 2} environments.

  15. Tensile properties of V-Cr-Ti alloys after exposure in helium and low-partial-pressure oxygen environments

    International Nuclear Information System (INIS)

    Natesan, K.; Soppet, W.K.

    1997-01-01

    A test program is in progress to evaluate the effect of oxygen at low pO 2 on the tensile properties of V-(4-5)wt% Cr-(4-5)wt% Ti alloys. Some of the tensile specimens were precharged with oxygen at low pO 2 at 500 degrees C and reannealed in vacuum at 500 degrees C in environments with various pO 2 levels and subsequently tensile tested at room temperature. The preliminary results indicate that both approaches are appropriate for evaluating the effect of oxygen uptake on the tensile properties of the alloys. The data showed that in the relatively short-time tests conducted thus far, the maximum engineering stress slightly increased after oxygen exposure but the uniform and total elongation values exhibited significant decrease after exposure in oxygen-containing environments. The data for a specimen exposed to a helium environment were similar to those obtained in low pO 2 environments

  16. Tensile and impact properties of TZM and Mo-5% Re

    International Nuclear Information System (INIS)

    Filacchioni, G.; Casagrande, E.; Angelis, U. de; Santis, G. de; Ferrara, D.

    1994-01-01

    Some aspects of the mechanical behaviour of two molybdenum alloys, one belonging to the precipitation hardened sub-family (TZM) and the other is a solid solution Mo 5% rhenium-bearing alloy, have been investigated. Experimental data (tensile mechanical strength, ductility and impact properties of unirradiated materials) show that a difference in behaviour exists between the precipitation hardened and the solid solution strengthened alloy, but at the same time a serious discrepancy has been found between the present results and previously reported ductile to brittle transition temperature values for Mo alloys. ((orig.))

  17. Ageing sintered silver: Relationship between tensile behavior, mechanical properties and the nanoporous structure evolution

    Energy Technology Data Exchange (ETDEWEB)

    Gadaud, Pascal; Caccuri, Vincenzo; Bertheau, Denis [Institut Pprime, Dept. Phys. Mech. Mat., UPR CNRS 3346, ENSMA, Université de Poitiers, 1 av. Clément Ader, Téléport 2, 86961 Futuroscope – Chasseneuil (France); Carr, James [HMXIF, Materials Science Centre, The University of Manchester, M13 9PL (United Kingdom); Milhet, Xavier, E-mail: xavier.milhet@ensma.fr [Institut Pprime, Dept. Phys. Mech. Mat., UPR CNRS 3346, ENSMA, Université de Poitiers, 1 av. Clément Ader, Téléport 2, 86961 Futuroscope – Chasseneuil (France)

    2016-07-04

    Silver pastes sintering is a potential candidate for die bonding in power electronic modules. The joints, obtained by sintering, exhibit a significant pore fraction thus reducing the density of the material compared to bulk silver. This was shown to alter drastically the mechanical properties (Young's modulus, yield strength and ultimate tensile stress) at room temperature. While careful analysis of the microstructure has been reported for the as-sintered material, little is known about its quantitative evolution (pores and grains) during thermal ageing. To address this issue, sintered bulk specimens and sintered joints were aged either under isothermal conditions (125 °C up to 1500 h) or under thermal cycling (between −40 °C/+125 °C with 30 min dwell time at each temperature for 2400 cycles). Under these conditions, it is shown that the density of the material does not change but the sub-micron porosity evolves towards a broader size distribution, consistent with Oswald ripening. It is also shown that only the step at 125 °C during the non-isothermal ageing is responsible for the microstructure evolution: isothermal ageing at high temperature can be regarded as a useful tool to perform accelerated ageing tests. Tensile properties are investigated as both a function of ageing time and a function of density. It is shown that the elastic properties do not evolve with the ageing time unlike the plastic properties. This is discussed as a function of the material microstructure evolution.

  18. The effect of strain rate and temperature on the tensile behaviour of uranium 2 w/o molybdenum

    International Nuclear Information System (INIS)

    Harding, J.; Boyd, G.A.C.

    1983-01-01

    This report describes the uniaxial tensile behaviour of uranium 2 w/o molybdenum alloy over a wide range of temperature and strain rate. Specimen blanks taken from co-reduced and extruded U 2 w/o Mo rods were given one of two heat treatments. Longitudinal tensile test pieces, taken from these blanks at near surface locations were tested in the temperature range -150 deg C to +100 deg C at strain rates from quasistatic (10 -4 s -1 ) to 10 3 s -1 . To achieve this range of testing rates three machines were required: an Instron screw driven machine for rates up to 0.1 s -1 , a second specially constructed hydraulic machine for the range 0.1 s -1 to 50 s -1 and a drop weight machine for the highest strain rates. The ways in which the mechanical properties - elongation to fracture, flow stresses and ultimate tensile stress - vary with both temperature and strain rate are presented and discussed for material in both heat treatment conditions. (author)

  19. STUDY OF THE MECHANICAL PROPERTIES OF INCONEL 718 SUPERALLOY AFTER HOT TENSILE TESTS

    Directory of Open Access Journals (Sweden)

    Tarcila Sugahara

    2014-10-01

    Full Text Available This research work investigated some important mechanical properties of Inconel 718 superalloy using hot tensile tests like conventional yield strength to 0.2% strain (σe , ultimate strength (σr , and specific elongation (εu . Samples were strained to failure at temperatures of 600°C, 650°C, 700°C, 750°C, 800°C and 850°C and strain rate of 0.5 mm/min (2 × 10–4 s–1 according to ASTM E-8. The results showed higher values σe of yield strength at 700°C, this anomalous behavior can be attributed to the presence of hardening precipitates as observed in the TTT diagram of superalloy Inconel 718. Examination of the sample’s surfaces tensile fracture showed that with increasing temperature test the actuating mechanism changes from intergranular fracture to coalescence of the microcavities.

  20. Analysis/design of tensile property database system

    International Nuclear Information System (INIS)

    Park, S. J.; Kim, D. H.; Jeon, I.; Lyu, W. S.

    2001-01-01

    The data base construction using the data produced from tensile experiment can increase the application of test results. Also, we can get the basic data ease from database when we prepare the new experiment and can produce high quality result by compare the previous data. The development part must be analysis and design more specific to construct the database and after that, we can offer the best quality to customers various requirements. In this thesis, the analysis and design was performed to develop the database for tensile extension property

  1. Selective Laser Melting Produced Ti-6Al-4V: Post-Process Heat Treatments to Achieve Superior Tensile Properties

    Directory of Open Access Journals (Sweden)

    Gerrit M. Ter Haar

    2018-01-01

    Full Text Available Current post-process heat treatments applied to selective laser melting produced Ti-6Al-4V do not achieve the same microstructure and therefore superior tensile behaviour of thermomechanical processed wrought Ti-6Al-4V. Due to the growing demand for selective laser melting produced parts in industry, research and development towards improved mechanical properties is ongoing. This study is aimed at developing post-process annealing strategies to improve tensile behaviour of selective laser melting produced Ti-6Al-4V parts. Optical and electron microscopy was used to study α grain morphology as a function of annealing temperature, hold time and cooling rate. Quasi-static uniaxial tensile tests were used to measure tensile behaviour of different annealed parts. It was found that elongated α’/α grains can be fragmented into equiaxial grains through applying a high temperature annealing strategy. It is shown that bi-modal microstructures achieve a superior tensile ductility to current heat treated selective laser melting produced Ti-6Al-4V samples.

  2. Investigation of the tensile properties of continuous steel wire-reinforced gray cast iron composite

    Energy Technology Data Exchange (ETDEWEB)

    Akdemir, Ahmet [Department of Mechanical Engineering, Selcuk University, Konya (Turkey); Kus, Recai [Department of Mechanical Education, Selcuk University, Konya (Turkey); Simsir, Mehmet, E-mail: msimsir@cumhuriyet.edu.tr [Department of Metallurgical and Materials Engineering, Cumhuriyet University, Kayseri Yolu 7. Km, 58140 Sivas (Turkey)

    2011-04-25

    Research highlights: {yields} Metal matrix composite (MMC) is an important structural material. {yields} Gray cast irons as a matrix material in MMC have more advantages than other cast irons. {yields} Interface greatly determines the mechanical properties of MMC. {yields} Interface formed by diffusion of carbon atoms. {yields} While decarburizing takes place in gray cast iron, carburiszing takes place in steel near the interface. - Abstract: The aim of the present study was to improve the tensile properties of gray cast iron by reinforcing the material with a steel wire. The composite was produced by sand mold casting, and the specimens were normalized by applying heat treatments at 800 deg. C, 850 deg. C, and 900 deg. C. Tension tests were conducted on gray cast iron and composite specimens, and the microstructure of the specimens was examined with an optical microscope. The fracture surface of the tension test specimens was examined with a scanning electron microscope (SEM), and graphite-free transition regions with high degrees of hardness were observed due to the diffusion of carbon from the cast iron to the steel wire. The microstructure of the transition region (fine pearlitic phase with partially dissolved graphite flakes) and the bond quality in the transition region increased the tensile properties of cast iron composites. Also, it is concluded that the tensile properties of gray cast iron increased with an increase in the normalization temperature.

  3. Investigation of the tensile properties of continuous steel wire-reinforced gray cast iron composite

    International Nuclear Information System (INIS)

    Akdemir, Ahmet; Kus, Recai; Simsir, Mehmet

    2011-01-01

    Research highlights: → Metal matrix composite (MMC) is an important structural material. → Gray cast irons as a matrix material in MMC have more advantages than other cast irons. → Interface greatly determines the mechanical properties of MMC. → Interface formed by diffusion of carbon atoms. → While decarburizing takes place in gray cast iron, carburiszing takes place in steel near the interface. - Abstract: The aim of the present study was to improve the tensile properties of gray cast iron by reinforcing the material with a steel wire. The composite was produced by sand mold casting, and the specimens were normalized by applying heat treatments at 800 deg. C, 850 deg. C, and 900 deg. C. Tension tests were conducted on gray cast iron and composite specimens, and the microstructure of the specimens was examined with an optical microscope. The fracture surface of the tension test specimens was examined with a scanning electron microscope (SEM), and graphite-free transition regions with high degrees of hardness were observed due to the diffusion of carbon from the cast iron to the steel wire. The microstructure of the transition region (fine pearlitic phase with partially dissolved graphite flakes) and the bond quality in the transition region increased the tensile properties of cast iron composites. Also, it is concluded that the tensile properties of gray cast iron increased with an increase in the normalization temperature.

  4. The color changes and tensile properties of oxidized Ti–6A1–2Mo–1.5Cr–2Zr–2Sn–2Nb alloy

    International Nuclear Information System (INIS)

    Jia, Zhiqiang; Zeng, Weidong; Zhang, Yaowu; Shi, Chunling; Quan, Biao; Wu, Jianding

    2015-01-01

    Highlights: • The oxidized alloy exhibited notable color changes. • The color was mainly attributed to the mixing of titanium oxides. • A corresponding relation between the color and tensile properties was established. • A predicted model was proposed to characterize the diffusion of oxygen. - Abstract: The oxidation of titanium alloy at elevated temperature severely limits its property and service life. It is a common and urgent issue to assess the mechanical property of oxidized titanium component without destroying its structural integrity. In this work, the color changes and tensile properties of oxidized Ti–6A1–2Mo–1.5Cr–2Zr–2Sn–2Nb alloy with initial basket-weave microstructure were investigated in the temperature range of 100–1000 °C. It was found that the oxidized specimens exhibited brilliant and regular color changes. X-ray diffraction (XRD) analysis indicated that the color changes were mainly attributed to the mixing of colored titanium oxides in the oxidation layer (such as yellow TiO, white TiO 2 and blue Ti 2 O 3 ). It was also found that mechanical properties were significant influenced by the oxidation treatment. The specimens oxidized below 600 °C exhibited excellent strength and plasticity due to its fine basket-weave microstructure and dense oxidation layer. In the temperature range from 600 to 800 °C, the strength slightly decreased while the plasticity rose a little. The change of mechanical properties during the temperature range was mainly determined by the microstructure change. Eventually, both strength and plasticity decreased sharply when the temperature was over 800 °C, which was mainly caused by the thick oxidation layer with porous and loose microstructure. The fracture mode of tensile specimens also changed from ductile fracture (below 800 °C) to transgranular cleavage fracture (over 800 °C). On the basis of experiments, a corresponding relation between the color changes and tensile properties was

  5. The High Temperature Tensile and Creep Behaviors of High Entropy Superalloy.

    Science.gov (United States)

    Tsao, Te-Kang; Yeh, An-Chou; Kuo, Chen-Ming; Kakehi, Koji; Murakami, Hideyuki; Yeh, Jien-Wei; Jian, Sheng-Rui

    2017-10-04

    This article presents the high temperature tensile and creep behaviors of a novel high entropy alloy (HEA). The microstructure of this HEA resembles that of advanced superalloys with a high entropy FCC matrix and L1 2 ordered precipitates, so it is also named as "high entropy superalloy (HESA)". The tensile yield strengths of HESA surpass those of the reported HEAs from room temperature to elevated temperatures; furthermore, its creep resistance at 982 °C can be compared to those of some Ni-based superalloys. Analysis on experimental results indicate that HESA could be strengthened by the low stacking-fault energy of the matrix, high anti-phase boundary energy of the strengthening precipitate, and thermally stable microstructure. Positive misfit between FCC matrix and precipitate has yielded parallel raft microstructure during creep at 982 °C, and the creep curves of HESA were dominated by tertiary creep behavior. To the best of authors' knowledge, this article is the first to present the elevated temperature tensile creep study on full scale specimens of a high entropy alloy, and the potential of HESA for high temperature structural application is discussed.

  6. Effect of heat treatment on elevated temperature tensile and creep properties of the extruded Mg–6Gd–4Y–Nd–0.7Zr alloy

    Energy Technology Data Exchange (ETDEWEB)

    Yuan, Lin, E-mail: yuanlin@hit.edu.cn; Shi, Wenchao; Jiang, WenMao; Zhao, Zhe; Shan, Debin

    2016-03-21

    The light and heavy rare earth elements are added to the magnesium alloys to improve the strengths and the creep resistance. The age hardening behaviors of the extruded Mg–6Gd–4Y–Nd–0.7Zr alloy aged at 200, 225 and 250 °C were investigated. Tensile tests and creep tests of the extruded and extruded-T5 Mg–6Gd–4Y–Nd–0.7Zr were carried out at 150–300 °C. The relationship between the microstructure and the properties of the extruded-T5 Mg–6Gd–4Y–Nd–0.7Zr alloy was studied. The result shows that the extruded Mg–6Gd–4Y–Nd–0.7Zr (contained less than 10 wt% Gd) peak aged at 225 °C for 72 h has the excellent creep resistance and high strengths with the UTS more than 350 MPa from room temperature to 200 °C, which are correlative with the precipitates. The high dense and uniform distribution of β′ phase with good heat stability precipitates inhibiting the dislocation motion contributes to age hardening, accelerates the ageing hardening response and increases the creep resistance. The artificially aged (T5) at low temperature further creep tested and tensile tested at higher temperatures decreases the resistance to the dislocation motion and the grain boundary sliding, resulting in the reduction in creep properties and strengths of the extruded-T5 Mg–6Gd–4Y–Nd–0.7Zr alloy above 225 °C.

  7. The effect of strain rate and temperature on the tensile behaviour of uranium - 2sup(w)/o molybdenum

    International Nuclear Information System (INIS)

    Harding, J.; Boyd, G.A.C.

    1983-01-01

    This report describes the uniaxial tensile behaviour of uranium 2 w/o molybdenum alloy over a wide range of temperature and strain rate. Specimen blanks taken from co-reduced and extruded U2 w/o Mo rods were given one of two heat treatments. Longitudinal tensile test pieces, taken from these blanks at near surface locations were tested in the temperature range -150 deg C to +100 deg C at strain rates from quasistatic (10 -4 s -1 ) to 10 3 s -1 . To achieve this range of testing rates three machines were required: an Instron screw driven machine for rates up to 0.1 s -1 , a second specially constructed hydraulic machine for the range 0.1 s -1 to 50 s -1 and a drop weight machine for the highest strain rates. The ways in which the mechanical properties - elongation to fracture, flow stresses and ultimate tensile stress - vary with both temperature and strain rate are presented and discussed for material in both heat treatment conditions. (author)

  8. The effect of microalloying B on the High temperature mechanical properties of Ti3Al

    International Nuclear Information System (INIS)

    Newkirk, J.W.; Feldewerth, G.B.

    1989-01-01

    This paper presents a study of the effect of adding boron to Ti 3 Al on the microstructure and high temperature tensile properties. Boron caused a large grain refinement that dominated the tensile properties at all temperatures. Particles of Ti 2 B were found in all of the boron containing alloys. TiB was found only at concentrations of 0.1% B or more

  9. Build direction dependence of microstructure and high-temperature tensile property of Co–Cr–Mo alloy fabricated by electron beam melting

    International Nuclear Information System (INIS)

    Sun, Shi-Hai; Koizumi, Yuichiro; Kurosu, Shingo; Li, Yun-Ping; Matsumoto, Hiroaki; Chiba, Akihiko

    2014-01-01

    The microstructures and high-temperature tensile properties of a Co–28Cr–6Mo–0.23C–0.17N alloy fabricated by electron beam melting (EBM) with cylindrical axes deviating from the build direction by 0°, 45°, 55° and 90° were investigated. The preferred crystal orientations of the γ phase in the as-EBM-built samples with angles of 0°, 45°, 55° and 90° were near [0 0 1], [1 1 0], [1 1 1] and [1 0 0], respectively. M 23 C 6 precipitates (M = Cr, Mo or Si) were observed to align along the build direction with intervals of around 3 μm. The phase was completely transformed into a single ε-hexagonal close-packed (hcp) phase after aging treatment at 800 °C for 24 h, when lamellar colonies of M 2 N precipitates and the ε-hcp phase appeared in the matrix. Among the samples, the one built with 55° deviation had the highest ultimate tensile strength of 806 MPa at 700 °C. The relationship between the microstructure and the build direction dependence of mechanical properties suggested that the conditions of heat treatment to homogenize the microstructure throughout the height of the EBM-built object should be determined by taking into account the thermal history during the post-melt period of the EBM process, especially when the solid–solid transformation is sluggish

  10. Water absorption and its effect on the tensile properties of tapioca starch/polyvinyl alcohol bioplastics

    Science.gov (United States)

    Judawisastra, H.; Sitohang, R. D. R.; Marta, L.; Mardiyati

    2017-07-01

    Tapioca is one of the largest sources of starch and makes it suitable to be used for bioplastic material. Addition of polyvinyl alcohol (PVA) has been shown to successfully reduce the brittleness of starch bioplastic. This study aims to investigate the influence of PVA addition to water absorption behavior and its effect on the tensile properties of tapioca starch/PVA bioplastics, which are still not yet fully understood until now. The bioplastics were prepared by solution casting method at gelatinization temperature, with PVA addition from 0 to 29 wt%. Examinations were carried out by means of water absorption test, tensile test and Fourier Transform Infrared (FTIR) Spectroscopy. Increasing content of PVA, up to 29 wt%, was found to decrease the water absorption of the bioplastics, with the lowest water saturation point of 251%. This is due to the interaction between starch and PVA which reduces the free OH groups in the resulting bioplastics. Consequently, this led to a decrease in water absorption-related deterioration, i.e. tensile properties degradation of the bioplastics. The addition of 29 wt% resulted into the lowest degradation in tensile strength (6%) and stiffness (30%), while accompanied with the highest elongation increase (39%) after water immersion.

  11. THE INFLUENCES OF MELT-COMPOUNDING PARAMETERS ON THE TENSILE PROPERTIES OF LOW FILLER LOADING OF UNTREATED-MWCNTs-POLYPROPYLENE (PP NANOCOMPOSITES

    Directory of Open Access Journals (Sweden)

    M.A.MOHD SALLEH

    2008-04-01

    Full Text Available This study is to investigate the effects of addition self synthesised multi-walled carbon nanotubes (MWCNTs, to the final properties of polypropylene (PP matrix nanocomposites. The influences of melt blending parameters were evaluated, where the interrelationship between the temperatures of compounding and roller rotor speed of shearing blade parameter, to the tensile properties of fabricated composites were studied. MWCNT was synthesised in the laboratory scale; by using the floating catalyst chemical vapour deposition (FC-CVD method. Pre-compounding work is begun with de-agglomeration of MWCNT which carried out by combining the ultrasonication and mechanical stirrer means simultaneously. Carbon nanotubes produced was first verified by using SEM and TEM imaging microscopy techniques. It was later integrated with the thermoplastic PP matrix, via melt blending process through internally mixing approach. Very low weight percentage of chemically untreated MWCNT (0, 0.25, 0.50, 0.75 & 1.00 wt. % was added into PP and later was compression moulded to the thin sheet of composites film. Composites were prepared by varying the compounding temperature into three processing temperature namely 165, 175 & 185°C and also into three shearing speed of roller rotor blade, 40, 60 & 80 rpm respectively. Later, it was mechanically tested via tensile testing following the ASTM D-638 standard method. The interrelationship between each parameter of compounding to the mechanical tensile properties was tested. It was shown that, the additional of very low loading of untreated-MWCNT filler content, does give moderate effects on reinforcement to the tensile properties of composite. Different compounding parameter gives significant difference to the pattern of plot which was comparable between each other.

  12. Mechanical Properties of Commercial Carbon Fibers Using a Single Filament Tensile Test

    International Nuclear Information System (INIS)

    Joh, Han-Ik; Song, Hae Kyung; Ku, Bon-Cheol; Lee, Sungho; Kim, Ki-Young; Kang, Phil-Hyun

    2013-01-01

    In this study, mechanical properties of commercial carbon fibers were evaluated using a single filament tensile test with various fiber gauge lengths. Tensile strength increased significantly with a decreasing length of the test specimens possibly due to small defect sites. The compliance method provided more accurate moduli of the carbon fibers, removing system errors during the single filament tensile test. The Weibull modulus revealed that shorter specimens had an inhomogeneous defect distribution, leading to a higher tensile strength and its standard deviation. X-ray diffractograms of carbon fibers showed a similar crystallinity and orientation in spite of significant differences in the fiber modulus and strength, indicating that crystalline structure of the commercial carbon fibers used in the study was not attributable to the difference in their tensile properties.

  13. Reversible temper brittleness on tensile tests at room temperature

    International Nuclear Information System (INIS)

    Quadros, N.F. de; Cabral, U.Q.

    1976-01-01

    Tensile tests were carried out on unnotched test pieces at room temperature and three strain rates: 2,5x10 -4 , 2,5x10 -3 and 1,0x10 -2 s -1 in a low alloy No-Cr-Mo steel to observe the variation in its mechanical properties with the occurrence of reversible temper brittleness. The brittle samples showed a sensitivity of 50 0 C in a 48 hour heat treatment at 500 0 C. The tests showed that at the strain rate of 2,5x10 -4 s -1 there are statistically significant differences between the elongations of the material in the brittle and the nonbrittle and regenerated states. A short review of reversible temper brittleness is given and a theory suggested for the mechanism [pt

  14. Development of nanostructured SUS316L-2%TiC with superior tensile properties

    Energy Technology Data Exchange (ETDEWEB)

    Sakamoto, T., E-mail: sakamoto.tatsuaki.mm@ehime-u.ac.jp [Department of Materials Science and Biotechnology, Ehime University, Matsuyama 790-8577 (Japan); Kurishita, H.; Matsuo, S.; Arakawa, H. [International Research Center for Nuclear Materials Science, IMR, Tohoku University, Oarai, Ibaraki 311-1313 (Japan); Takahashi, S.; Tsuchida, M. [Ehime University, Matsuyama 790-8577 (Japan); Kobayashi, S.; Nakai, K. [Department of Materials Science and Biotechnology, Ehime University, Matsuyama 790-8577 (Japan); Terasawa, M. [Laboratory of Advanced Science & Technology for Industry, University of Hyogo, 3-1-2 Koto, Kamigori-cho, Hyogo 678-1205 (Japan); Yamasaki, T. [Department of Materials Science & Chemistry, Graduate School of Engineering, University of Hyogo, 2167 Shosha, Himeji, Hyogo 671-2201 (Japan); Kawai, M. [High Energy Accelerator Research Organization (KEK), Tsukuba, Ibaraki-ken 305-0801 (Japan)

    2015-11-15

    Structural materials used in radiation environments require radiation tolerance and sufficient mechanical properties in the controlled state. In order to offer SUS316L austenitic stainless steel with the assumed requirements, nanostructured SUS316L with TiC addition of 2% (SUS316L-2TiC) that is capable of exhibiting enhanced tensile ductility and flow strength sufficient for structural applications was fabricated by advanced powder metallurgical methods. The methods include MA (Mechanical Alloying), HIP (Hot Isostatic Pressing), GSMM (Grain boundary Sliding Microstructural Modification) for ductility enhancement, cold rolling at temperatures below M{sub d} (the temperature where the martensite phase occurs by plastic deformation) for phase transformation from austenite to martensite and heat treatment for reverse transformation from martensite to austenite. It is shown that the developed SUS316L-2TiC exhibits ultrafine grains with sizes of 90–270 nm, accompanied by TiC precipitates with 20–50 nm in grain interior and 70–110 nm at grain boundaries, yield strengths of 1850 to 900 MPa, tensile strengths of 1920 to 1100 MPa and uniform elongations of 0.6–21%, respectively, depending on the heat treatment temperature after rolling at −196 °C. - Highlights: • Nanostructured SUS316L-2%TiC exhibiting sufficient tensile ductility and strength is developed. • The development requires an advanced powder metallurgical route. • The route includes MA, HIP, GSMM and thermo-mechanical treatments for phase transformation. • The austenite grain sizes are 90–270 nm and TiC precipitates 20–50 nm in grain interior. • The tensile strength are 1100–1920 MPa and uniform elongation 0.6–21%.

  15. Development of nanostructured SUS316L-2%TiC with superior tensile properties

    International Nuclear Information System (INIS)

    Sakamoto, T.; Kurishita, H.; Matsuo, S.; Arakawa, H.; Takahashi, S.; Tsuchida, M.; Kobayashi, S.; Nakai, K.; Terasawa, M.; Yamasaki, T.; Kawai, M.

    2015-01-01

    Structural materials used in radiation environments require radiation tolerance and sufficient mechanical properties in the controlled state. In order to offer SUS316L austenitic stainless steel with the assumed requirements, nanostructured SUS316L with TiC addition of 2% (SUS316L-2TiC) that is capable of exhibiting enhanced tensile ductility and flow strength sufficient for structural applications was fabricated by advanced powder metallurgical methods. The methods include MA (Mechanical Alloying), HIP (Hot Isostatic Pressing), GSMM (Grain boundary Sliding Microstructural Modification) for ductility enhancement, cold rolling at temperatures below M_d (the temperature where the martensite phase occurs by plastic deformation) for phase transformation from austenite to martensite and heat treatment for reverse transformation from martensite to austenite. It is shown that the developed SUS316L-2TiC exhibits ultrafine grains with sizes of 90–270 nm, accompanied by TiC precipitates with 20–50 nm in grain interior and 70–110 nm at grain boundaries, yield strengths of 1850 to 900 MPa, tensile strengths of 1920 to 1100 MPa and uniform elongations of 0.6–21%, respectively, depending on the heat treatment temperature after rolling at −196 °C. - Highlights: • Nanostructured SUS316L-2%TiC exhibiting sufficient tensile ductility and strength is developed. • The development requires an advanced powder metallurgical route. • The route includes MA, HIP, GSMM and thermo-mechanical treatments for phase transformation. • The austenite grain sizes are 90–270 nm and TiC precipitates 20–50 nm in grain interior. • The tensile strength are 1100–1920 MPa and uniform elongation 0.6–21%.

  16. Tensile Properties of Under-Matched Weld Joints for 950 MPa Steel.

    Science.gov (United States)

    Yamamoto, Kouji; Arakawa, Toshiaki; Akazawa, Nobuki; Yamamoto, Kousei; Matsuo, Hiroki; Nakagara, Kiyoyuki; Suita, Yoshikazu

    In welding of 950 MPa-class high tensile strength steel, preheating is crucial in order to avoid cold cracks, which, however, eventually increases welding deformations. One way to decrease welding deformations is lowering preheating temperature by using under-matched weld metal. Toyota and others clarify that although breaking elongation can decrease due to plastic constraint effect under certain conditions, static tensile of under-matched weld joints is comparable to that of base metal. However, there has still been no report about joint static tensile of under-matched weld joints applied to 950 MPa-class high tensile strength steel. In this study, we aim to research tensile strength and fatigue strength of under-matched weld joints applied to 950 MPa-class high tensile steel.

  17. Fabrication, Structural Characterization and Uniaxial Tensile Properties of Novel Sintered Multi-Layer Wire Mesh Porous Plates

    Directory of Open Access Journals (Sweden)

    Liuyang Duan

    2018-01-01

    Full Text Available There is an increasing interest in developing porous metals or metallic foams for functional and structural applications. The study of the physical and mechanical properties of porous metals is very important and helpful for their application. In this paper, a novel sintered multilayer wire mesh porous plate material (WMPPs with a thickness of 0.5 mm–3 mm and a porosity of 10–35% was prepared by winding, pressing, rolling, and subsequently vacuum sintering them. The pore size and total size distribution in the as-prepared samples were investigated using the bubble point method. The uniaxial tensile behavior of the WMPPs was investigated in terms of the sintering temperature, porosity, wire diameter, and manufacturing technology. The deformation process and the failure mechanism under the tensile press was also discussed based on the appearance of the fractures (SEM figures. The results indicated that the pore size and total size distribution were closely related to the raw material used and the sintering temperature. For the WMPPs prepared by the wire mesh, the pore structures were inerratic and the vast majority of pore size was less than 10 μm. On the other hand, for the WMPPs that were prepared by wire mesh and powder, the pore structures were irregular and the pore size ranged from 0 μm–50 μm. The experimental data showed that the tensile strength of WMPPs is much higher than any other porous metals or metallic foams. Higher sintering temperatures led to coarser joints between wires and resulted in higher tensile strength. The sintering temperature decreased from 1330 °C to 1130 °C and the tensile strength decreased from 296 MPa to 164 MPa. Lower porosity means that there are more metallurgical joints and metallic frameworks resisting deformation per unit volume. Therefore, lower porosities exhibit higher tensile strength. An increase of porosity from 17.14% to 32.5% led to the decrease of the tensile strength by 90 MPa. The

  18. The tensile behavior of GH3535 superalloy at elevated temperature

    Energy Technology Data Exchange (ETDEWEB)

    Han, F.F.; Zhou, B.M.; Huang, H.F.; Leng, B.; Lu, Y.L. [Thorium Molten Salts Reactor Center, Shanghai Institute of Applied Physics, Chinese Academy of Sciences (China); Dong, J.S. [Superalloy Division, Institute of Metal Research, Chinese Academy of Sciences (China); Li, Z.J., E-mail: lizhijun@sinap.ac.cn [Thorium Molten Salts Reactor Center, Shanghai Institute of Applied Physics, Chinese Academy of Sciences (China); Zhou, X.T. [Thorium Molten Salts Reactor Center, Shanghai Institute of Applied Physics, Chinese Academy of Sciences (China)

    2016-10-01

    The tensile behavior of GH3535 alloy has been investigated at strain rates of 8.33 × 10{sup −5}/s{sup −1}–8.33 × 10{sup −3}/s{sup −1}, in the temperature range of 25–800 °C. The results showed that the ultimate tensile strength was decreased with increasing temperature and increased with rising strain rate, whereas the yield strength kept almost a constant value at the temperature range from 550 to 800 °C in all strain rates test. The formation of M{sub 12}C carbides at the grain boundary during the tension process played an important role in increasing the yield strength of the alloy at elevated temperatures. But inhomogeneous deformation at 650 °C resulted in the minimum ductility of the alloy. Additionally, various types of serrations were noticed on the stress-strain curves for the alloy tested in the temperature range of 500–800 °C. Normal Portevin-Le Chatelier (PLC) effect and positive strain rate sensitivity were observed in this alloy. Type A and A + B serrations were presented to stress-strain curves at temperatures below 650 °C, whereas type C serration was noticed when the temperature rose above 650 °C. The analysis suggested that the interactions between substitutional solutes migration and mobile dislocations were the main reason for the serrated flow behavior in this alloy. - Highlights: • The tensile behavior of GH3535 alloy at elevated temperature was studied. • The yield strength anomaly was observed in the temperature range from 550 to 800 °C. • The formation of M{sub 12}C improves the grain boundary strength to a certain extent. • Inhomogeneous deformation at 650 °C results in the ductility loss of the alloy. • The interaction between solute atoms and dislocations results in the PLC effect.

  19. Effect of thermal history on mechanical properties of polyetheretherketone below the glass transition temperature

    Science.gov (United States)

    Cebe, Peggy; Chung, Shirley Y.; Hong, Su-Don

    1987-01-01

    The effect of thermal history on the tensile properties of polyetheretherketone neat resin films was investigated at different test temperatures (125, 25, and -100) using four samples: fast-quenched amorphous (Q); quenched, then crystallized at 180 C (C180); slowly cooled (for about 16 h) from the melt (SC); and air-cooled (2-3 h) from the melt (AC). It was found that thermal history significantly affects the tensile properties of the material below the glass transition. Fast quenched amorphous films were most tough, could be drawn to greatest strain before rupture, and undergo densification during necking; at the test temperature of -100 C, these films had the best ultimate mechanical properties. At higher temperatures, the semicrystalline films AC and C180 had properties that compared favorably with the Q films. The SC films exhibited poor mechanical properties at all test temperatures.

  20. Tensile Strength of Finger Joints at Elevated Temperatures

    DEFF Research Database (Denmark)

    Nielsen, Peter C.; Olesen, Frits Bolonius

    A series of test s aimed a t establishing the effect of temperature upon the tensile strength parallel-to-grain of finger jointed laminae for glulam has been conducted in the Fire Research Laboratory at Aalborg University Centre. The objective of this report is to present the background...

  1. Development of nanostructured SUS316L-2%TiC with superior tensile properties

    Science.gov (United States)

    Sakamoto, T.; Kurishita, H.; Matsuo, S.; Arakawa, H.; Takahashi, S.; Tsuchida, M.; Kobayashi, S.; Nakai, K.; Terasawa, M.; Yamasaki, T.; Kawai, M.

    2015-11-01

    Structural materials used in radiation environments require radiation tolerance and sufficient mechanical properties in the controlled state. In order to offer SUS316L austenitic stainless steel with the assumed requirements, nanostructured SUS316L with TiC addition of 2% (SUS316L-2TiC) that is capable of exhibiting enhanced tensile ductility and flow strength sufficient for structural applications was fabricated by advanced powder metallurgical methods. The methods include MA (Mechanical Alloying), HIP (Hot Isostatic Pressing), GSMM (Grain boundary Sliding Microstructural Modification) for ductility enhancement, cold rolling at temperatures below Md (the temperature where the martensite phase occurs by plastic deformation) for phase transformation from austenite to martensite and heat treatment for reverse transformation from martensite to austenite. It is shown that the developed SUS316L-2TiC exhibits ultrafine grains with sizes of 90-270 nm, accompanied by TiC precipitates with 20-50 nm in grain interior and 70-110 nm at grain boundaries, yield strengths of 1850 to 900 MPa, tensile strengths of 1920 to 1100 MPa and uniform elongations of 0.6-21%, respectively, depending on the heat treatment temperature after rolling at -196 °C.

  2. Method for independent strain and temperature measurement in polymeric tensile test specimen using embedded FBG sensors

    DEFF Research Database (Denmark)

    Pereira, Gilmar Ferreira; McGugan, Malcolm; Mikkelsen, Lars Pilgaard

    2016-01-01

    to calculate independently the strain and temperature are presented in the article, together with a measurement resolution study. This multi-parameter measurement method was applied to an epoxy tensile specimen, tested in a unidirectional tensile test machine with a temperature controlled cabinet. A full......A novel method to obtain independent strain and temperature measurements using embedded Fibre Bragg Grating (FBG) in polymeric tensile test specimens is presented in this paper. The FBG strain and temperature cross-sensitivity was decoupled using two single mode FBG sensors, which were embedded...... of temperature, from 40 C to -10 C. The consistency of the expected theoretical results with the calibration procedure and the experimental validation shows that this proposed method is applicable to measure accurate strain and temperature in polymers during static or fatigue tensile testing. Two different...

  3. Temperature Dependence of Mechanical Properties of TRISO SiC Coatings

    International Nuclear Information System (INIS)

    Kim, Do Kyung; Park, Kwi Il; Lee, Hyeon Keun; Seong, Young Hoon; Lee, Seung Jun

    2009-04-01

    SiC coating layer has been introduced as protective layer in TRISO nuclear fuel particle of high temperature gas cooled reactor (HTGR) due to excellent mechanical stability at high temperature. It is important to study for high temperature stability in SiC coating layers, because TRISO fuel particles were operating at high temperature around 1000 .deg. C. In this study, the nanoindentation test and micro tensile test were conducted in order to measure the mechanical properties of SiC coating layers at elevated temperature. SiC coating film was fabricated on the carbon substrate using chemical vapor deposition process with different microstructures and thicknesses. Nanoindentation test was performed for the analysis of the hardness, modulus and creep properties up to 500 .deg. C. Impression creep method applied to nanoindentation and creep properties of SiC coating layers were characterized by nanoindentation creep test. The fracture strength of SiC coating layers was measured by the micro tensile method at room temperature and 500 .deg. C. From the results, we can conclude that the hardness and fracture strength are decreased with temperature and no significant change in the modulus is observed with increase in temperature. The deformation mechanism for indentation creep and creep rate changes as the testing temperature increased

  4. Tensile testing

    CERN Document Server

    2004-01-01

    A complete guide to the uniaxial tensile test, the cornerstone test for determining the mechanical properties of materials: Learn ways to predict material behavior through tensile testing. Learn how to test metals, alloys, composites, ceramics, and plastics to determine strength, ductility and elastic/plastic deformation. A must for laboratory managers, technicians, materials and design engineers, and students involved with uniaxial tensile testing. Tensile Testing , Second Edition begins with an introduction and overview of the test, with clear explanations of how materials properties are determined from test results. Subsequent sections illustrate how knowledge gained through tensile tests, such as tension properties to predict the behavior (including strength, ductility, elastic or plastic deformation, tensile and yield strengths) have resulted in improvements in materals applications. The Second Edition is completely revised and updated. It includes expanded coverage throughout the volume on a variety of ...

  5. The tensile properties of single sugar palm (Arenga pinnata) fibre

    Science.gov (United States)

    Bachtiar, D.; Sapuan, S. M.; Zainudin, E. S.; Khalina, A.; Dahlan, K. Z. M.

    2010-05-01

    This paper presents a brief description and characterization of the sugar palm fibres, still rare in the scientific community, compared to other natural fibres employed in polymeric composites. Sugar palm fibres are cellulose-based fibres extracted from the Arenga pinnata plant. The characterization consists of tensile test and the morphological examination. The average tensile properties results of fibres such as Young's modulus is equal to 3.69 GPa, tensile strength is equal to 190.29 MPa, and strain at failure is equal to 19.6%.

  6. The tensile properties of single sugar palm (Arenga pinnata) fibre

    International Nuclear Information System (INIS)

    Bachtiar, D; Sapuan, S M; Zainudin, E S; Khalina, A; Dahlan, K Z M

    2010-01-01

    This paper presents a brief description and characterization of the sugar palm fibres, still rare in the scientific community, compared to other natural fibres employed in polymeric composites. Sugar palm fibres are cellulose-based fibres extracted from the Arenga pinnata plant. The characterization consists of tensile test and the morphological examination. The average tensile properties results of fibres such as Young's modulus is equal to 3.69 GPa, tensile strength is equal to 190.29 MPa, and strain at failure is equal to 19.6%.

  7. Tensile mechanical properties of U3Si2-Al fuel plate

    International Nuclear Information System (INIS)

    Xu Yong; Hu Huawei; Zhuang Hongquan; Wang Xishu

    2003-01-01

    The fuel plate made of fuel meat, with the U 3 Si 2 -Al dispersion fuel center, and 6061 Al alloy cladding, is a new kind of fuel used in research reactors. The mechanical property data of the fuel meat is the basic data in the design of fuel group, but the mechanical property of this fuel meat has not been studied all over the world till now. In this paper, the mechanical properties of U 3 Si 2 -Al fuel meats of different sizes used in research reactors are investigated and analyzed, and at the same time the carrying capacity of tensile in different directions are also compared. In order to get more knowledge about the mechanical properties of the fuel meat, the tensile experiment has been carried out repeatedly. Considering the lower ratio of elongation and the brittleness, the microscope has been used to examine the zone of fracture after tensile test. (authors)

  8. The color changes and tensile properties of oxidized Ti–6A1–2Mo–1.5Cr–2Zr–2Sn–2Nb alloy

    Energy Technology Data Exchange (ETDEWEB)

    Jia, Zhiqiang, E-mail: jzq19841102@gmail.com [State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072 (China); Zeng, Weidong, E-mail: zengwd@nwpu.edu.cn [State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072 (China); Zhang, Yaowu [State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072 (China); Shi, Chunling [Xi’an Aircraft Industry Company LTD, 710089 (China); Quan, Biao; Wu, Jianding [State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072 (China)

    2015-08-15

    Highlights: • The oxidized alloy exhibited notable color changes. • The color was mainly attributed to the mixing of titanium oxides. • A corresponding relation between the color and tensile properties was established. • A predicted model was proposed to characterize the diffusion of oxygen. - Abstract: The oxidation of titanium alloy at elevated temperature severely limits its property and service life. It is a common and urgent issue to assess the mechanical property of oxidized titanium component without destroying its structural integrity. In this work, the color changes and tensile properties of oxidized Ti–6A1–2Mo–1.5Cr–2Zr–2Sn–2Nb alloy with initial basket-weave microstructure were investigated in the temperature range of 100–1000 °C. It was found that the oxidized specimens exhibited brilliant and regular color changes. X-ray diffraction (XRD) analysis indicated that the color changes were mainly attributed to the mixing of colored titanium oxides in the oxidation layer (such as yellow TiO, white TiO{sub 2} and blue Ti{sub 2}O{sub 3}). It was also found that mechanical properties were significant influenced by the oxidation treatment. The specimens oxidized below 600 °C exhibited excellent strength and plasticity due to its fine basket-weave microstructure and dense oxidation layer. In the temperature range from 600 to 800 °C, the strength slightly decreased while the plasticity rose a little. The change of mechanical properties during the temperature range was mainly determined by the microstructure change. Eventually, both strength and plasticity decreased sharply when the temperature was over 800 °C, which was mainly caused by the thick oxidation layer with porous and loose microstructure. The fracture mode of tensile specimens also changed from ductile fracture (below 800 °C) to transgranular cleavage fracture (over 800 °C). On the basis of experiments, a corresponding relation between the color changes and tensile properties

  9. Improvement in tensile properties of PVC–montmorillonite ...

    Indian Academy of Sciences (India)

    mechanical properties of PVC–montmorillonite materials are also currently of huge ... Its hard form can withstand a tensile stress in the order of 46–52 MPa before .... 2θ at 25 mA and 40 kV using Cu-Kα radiation. X-ray diffraction patterns of the ...

  10. Mechanical properties of graphene nanoribbons under uniaxial tensile strain

    Science.gov (United States)

    Yoneyama, Kazufumi; Yamanaka, Ayaka; Okada, Susumu

    2018-03-01

    Based on the density functional theory with the generalized gradient approximation, we investigated the mechanical properties of graphene nanoribbons in terms of their edge shape under a uniaxial tensile strain. The nanoribbons with armchair and zigzag edges retain their structure under a large tensile strain, while the nanoribbons with chiral edges are fragile against the tensile strain compared with those with armchair and zigzag edges. The fracture started at the cove region, which corresponds to the border between the zigzag and armchair edges for the nanoribbons with chiral edges. For the nanoribbons with armchair edges, the fracture started at one of the cove regions at the edges. In contrast, the fracture started at the inner region of the nanoribbons with zigzag edges. The bond elongation under the tensile strain depends on the mutual arrangement of covalent bonds with respect to the strain direction.

  11. Phase Morphology and Mechanical Properties of Cyclic Butylene Terephthalate Oligomer-Containing Rubbers: Effect of Mixing Temperature.

    Science.gov (United States)

    Halász, István Zoltán; Bárány, Tamás

    2016-08-24

    In this work, the effect of mixing temperature (T mix ) on the mechanical, rheological, and morphological properties of rubber/cyclic butylene terephthalate (CBT) oligomer compounds was studied. Apolar (styrene butadiene rubber, SBR) and polar (acrylonitrile butadiene rubber, NBR) rubbers were modified by CBT (20 phr) for reinforcement and viscosity reduction. The mechanical properties were determined in tensile, tear, and dynamical mechanical analysis (DMTA) tests. The CBT-caused viscosity changes were assessed by parallel-plate rheometry. The morphology was studied by scanning electron microscopy (SEM). CBT became better dispersed in the rubber matrices with elevated mixing temperatures (at which CBT was in partially molten state), which resulted in improved tensile properties. With increasing mixing temperature the size of the CBT particles in the compounds decreased significantly, from few hundred microns to 5-10 microns. Compounding at temperatures above 120 °C and 140 °C for NBR and SBR, respectively, yielded reduced tensile mechanical properties most likely due to the degradation of the base rubber. The viscosity reduction by CBT was more pronounced in mixes with coarser CBT dispersions prepared at lower mixing temperatures.

  12. Microstructure-Tensile Properties Correlation for the Ti-6Al-4V Titanium Alloy

    Science.gov (United States)

    Shi, Xiaohui; Zeng, Weidong; Sun, Yu; Han, Yuanfei; Zhao, Yongqing; Guo, Ping

    2015-04-01

    Finding the quantitative microstructure-tensile properties correlations is the key to achieve performance optimization for various materials. However, it is extremely difficult due to their non-linear and highly interactive interrelations. In the present investigation, the lamellar microstructure features-tensile properties correlations of the Ti-6Al-4V alloy are studied using an error back-propagation artificial neural network (ANN-BP) model. Forty-eight thermomechanical treatments were conducted to prepare the Ti-6Al-4V alloy with different lamellar microstructure features. In the proposed model, the input variables are microstructure features including the α platelet thickness, colony size, and β grain size, which were extracted using Image Pro Plus software. The output variables are the tensile properties, including ultimate tensile strength, yield strength, elongation, and reduction of area. Fourteen hidden-layer neurons which can make ANN-BP model present the most excellent performance were applied. The training results show that all the relative errors between the predicted and experimental values are within 6%, which means that the trained ANN-BP model is capable of providing precise prediction of the tensile properties for Ti-6Al-4V alloy. Based on the corresponding relations between the tensile properties predicted by ANN-BP model and the lamellar microstructure features, it can be found that the yield strength decreases with increasing α platelet thickness continuously. However, the α platelet thickness exerts influence on the elongation in a more complicated way. In addition, for a given α platelet thickness, the yield strength and the elongation both increase with decreasing β grain size and colony size. In general, the β grain size and colony size play a more important role in affecting the tensile properties of Ti-6Al-4V alloy than the α platelet thickness.

  13. Specimen alignment in an axial tensile test of thin films using direct imaging and its influence on the mechanical properties of BeCu

    International Nuclear Information System (INIS)

    Kang, Dong-Joong; Park, Jun-Hyub; Shin, Myung-Soo; Ha, Jong-Eun; Lee, Hak-Joo

    2010-01-01

    This paper proposes a new system for verification of the alignment of loading fixtures and test specimens during tensile testing of thin film with a micrometer size through direct imaging. The novel and reliable image recognition system to evaluate the misalignment between the load train and the specimen axes during tensile test of thin film was developed using digital image processing technology with CCD. The decision of whether alignment of the tensile specimen is acceptable or not is based on a probabilistic analysis through the edge feature extraction of digital imaging. In order to verify the performance of the proposed system and investigate the effect of the misalignment of the specimen on tensile properties, the tensile tests were performed as displacement control in air and at room temperature for metal thin film, the beryllium copper (BeCu) alloys. In the case of the metal thin films, bending stresses caused by misalignment are insignificant because the films are easily bent during tensile tests to eliminate the bending stresses. And it was observed that little effects and scatters on tensile properties occur by stress gradient caused by twisting at in-plane misalignment, and the effects and scatters on tensile properties are insignificant at out-of-plane misalignment, in the case of the BeCu thin film.

  14. Tensile properties of the modified 13Cr martensitic stainless steels

    Energy Technology Data Exchange (ETDEWEB)

    Mabruri, Efendi, E-mail: effe004@lipi.go.id; Anwar, Moch Syaiful, E-mail: moch.syaiful.anwar@lipi.go.id; Prifiharni, Siska, E-mail: siska.prifiharni@lipi.go.id; Romijarso, Toni B.; Adjiantoro, Bintang [Research Center for Metallurgy and Materials, Indonesian Institute of Sciences (LIPI) Kawasan Puspiptek Gd. 470 Serpong, Tangerang Selatan 15314 (Indonesia)

    2016-04-19

    This paper reports the influence of Mo and Ni on the tensile properties of the modified 13Cr martensitic stainless steels in tempered condition. Four steels with different content of Mo and Ni were prepared by induction melting followed by hot forging, quenching and tempering. The experimental results showed that the addition of about 1% and 3% Mo has a beneficial effect to increase both the tensile strength and the elongation of the steels. On the contrary, the addition of about 3% Ni into the martensitic stainless steel results in decreasing of both the tensile strength and the elongation. Among the alloys investigated the 13Cr3Mo type steel exhibited largest tensile strength of 1348 MPa and largest elongation of 12%. The observation on the tensile fractured surfaces by using scanning electron microscope supported these findings.

  15. Tensile properties of the modified 13Cr martensitic stainless steels

    International Nuclear Information System (INIS)

    Mabruri, Efendi; Anwar, Moch Syaiful; Prifiharni, Siska; Romijarso, Toni B.; Adjiantoro, Bintang

    2016-01-01

    This paper reports the influence of Mo and Ni on the tensile properties of the modified 13Cr martensitic stainless steels in tempered condition. Four steels with different content of Mo and Ni were prepared by induction melting followed by hot forging, quenching and tempering. The experimental results showed that the addition of about 1% and 3% Mo has a beneficial effect to increase both the tensile strength and the elongation of the steels. On the contrary, the addition of about 3% Ni into the martensitic stainless steel results in decreasing of both the tensile strength and the elongation. Among the alloys investigated the 13Cr3Mo type steel exhibited largest tensile strength of 1348 MPa and largest elongation of 12%. The observation on the tensile fractured surfaces by using scanning electron microscope supported these findings.

  16. Effects of Laser Energies on Wear and Tensile Properties of Biomimetic 7075 Aluminum Alloy

    Science.gov (United States)

    Yuan, Yuhuan; Zhang, Peng; Zhao, Guoping; Gao, Yang; Tao, Lixi; Chen, Heng; Zhang, Jianlong; Zhou, Hong

    2018-03-01

    Inspired by the non-smooth surface of certain animals, a biomimetic coupling unit with various sizes, microstructure, and hardness was prepared on the surface of 7075 aluminum alloy. Following experimental studies were conducted to investigate the wear and tensile properties with various laser energy inputs. The results demonstrated that the non-smooth surface with biomimetic coupling units had a positive effect on both the wear resistance and tensile property of 7075 aluminum alloy. In addition, the sample with the unit fabricated by the laser energy of 420.1 J/cm2 exhibited the most significant improvement on the wear and tensile properties owing to the minimum grain size and the highest microhardness. Also, the weight loss of the sample was one-third of the untreated one's, and the yield strength, the ultimate tensile strength, and the elongation improved by 20, 20, and 34% respectively. Moreover, the mechanisms of wear and tensile properties improvement were also analyzed.

  17. Effects of Heat-treatment on the Tensile Properties of Ti-Al-Zr Alloy

    International Nuclear Information System (INIS)

    Kim, Tae Hoon; Kang, Chang Sun; Baek, Jong Hyuk; Choi, Byoung Kwon; Jeong, Yong Hwan

    2006-01-01

    Ti-Al-Zr, titanium alloy, has been well known material as one of the candidates for heat-exchange tubes in steam generators in SMART (System integrated Modular Advanced ReacTor). But the primary circuit with the primary coolant is much different from that of commercial PWRs, i.e., an ammonia is used as a pH raising agent and the heat-exchange tubes are exposed to the primary coolant water at high temperatures and in high-pressure environments. Thus, excellent mechanical properties and corrosion resistance are required for the safe operation during the lifetime. A lot of tests were done to examine the mechanical properties of the Ti-Al-Zr alloy in the room temperature. But the test of this work is done in the more realistic condition from the viewpoint of the system characteristics for SMART design concept. Therefore, the purpose of this study is to evaluate the effects of annealing and cooling rate on the tensile properties of Ti-Al-Zr alloy at the operation temperature

  18. Tensile properties of neutron irradiated 316Ti and 15-15Ti steels

    International Nuclear Information System (INIS)

    Fissolo, A.; Levy, V.; Seran, J.L.; Maillard, A.; Royer, J.; Rabouille, O.

    1992-01-01

    This paper deals with the tensile behavior of CW316Ti and CW15-15Ti Phenix fuel pin cladding. The tensile tests were conducted on defueled tubes irradiated up to 115 dpa 3 in the 400-640 deg C temperature range. Test temperature corresponds essentially to irradiation temperature. The results emphasize that although irradiation induces a reduction of ductility, failure always occurs with significant plastic deformation even for the most irradiated clads. (author). 15 refs., 12 figs., 1 tab

  19. Tensile and fracture properties of primary heat transport system piping material

    International Nuclear Information System (INIS)

    Singh, P.K.; Chattopadhyay, J.; Kushwaha, H.S.

    1997-07-01

    The fracture mechanics calculations in leak-before-break analysis of nuclear piping system require material tensile data and fracture resistance properties in the form of J-R curve. There are large variations in fracture parameters due to variation in chemical composition and process used in making the steel components. Keeping this in view, a comprehensive program has been planned to generate the material data base for primary heat transport system piping using the specimens machined from actual pipes used in service. The material under study are SA333 Gr.6 (base as well as weld) and SA350 LF2 (base). Since the operating temperatures of 500 MWe Indian PHWR PHT system piping range from 260 degC to 304 degC the test temperature chosen are 28 degC, 200 degC, 250 degC and 300 degC. Tensile and compact tension specimens have been fabricated from actual pipe according to ASTM standard. Fracture toughness of base metal has been observed to be higher compared to weld metal in SA333 Gr.6 material for the temperature under consideration. Fracture toughness has been observed to be higher for LC orientation (notch in circumferential direction) compared to CL orientation (notch is in longitudinal direction) for the temperature range under study. Fracture toughness value decreases with increase in temperature for the materials under study. Finally, chemical analysis has been carried out to investigate the reason for high toughness of the material. It has been concluded that low percentage of carbon and nitrogen, low inclusion rating and fine grain size has enhanced the fracture toughness value

  20. Surface, structural and tensile properties of proton beam irradiated zirconium

    Energy Technology Data Exchange (ETDEWEB)

    Rafique, Mohsin; Chae, San; Kim, Yong-Soo, E-mail: yongskim@hanyang.ac.kr

    2016-02-01

    This paper reports the surface, structural and tensile properties of proton beam irradiated pure zirconium (99.8%). The Zr samples were irradiated by 3.5 MeV protons using MC-50 cyclotron accelerator at different doses ranging from 1 × 10{sup 13} to 1 × 10{sup 16} protons/cm{sup 2}. Both un-irradiated and irradiated samples were characterized using Field Emission Scanning Electron Microscope (FESEM), X-ray Diffraction (XRD) and Universal Testing Machine (UTM). The average surface roughness of the specimens was determined by using Nanotech WSxM 5.0 develop 7.0 software. The FESEM results revealed the formation of bubbles, cracks and black spots on the samples’ surface at different doses whereas the XRD results indicated the presence of residual stresses in the irradiated specimens. Williamson–Hall analysis of the diffraction peaks was carried out to investigate changes in crystallite size and lattice strain in the irradiated specimens. The tensile properties such as the yield stress, ultimate tensile stress and percentage elongation exhibited a decreasing trend after irradiation in general, however, an inconsistent behavior was observed in their dependence on proton dose. The changes in tensile properties of Zr were associated with the production of radiation-induced defects including bubbles, cracks, precipitates and simultaneous recovery by the thermal energy generated with the increase of irradiation dose.

  1. Surface, structural and tensile properties of proton beam irradiated zirconium

    Science.gov (United States)

    Rafique, Mohsin; Chae, San; Kim, Yong-Soo

    2016-02-01

    This paper reports the surface, structural and tensile properties of proton beam irradiated pure zirconium (99.8%). The Zr samples were irradiated by 3.5 MeV protons using MC-50 cyclotron accelerator at different doses ranging from 1 × 1013 to 1 × 1016 protons/cm2. Both un-irradiated and irradiated samples were characterized using Field Emission Scanning Electron Microscope (FESEM), X-ray Diffraction (XRD) and Universal Testing Machine (UTM). The average surface roughness of the specimens was determined by using Nanotech WSxM 5.0 develop 7.0 software. The FESEM results revealed the formation of bubbles, cracks and black spots on the samples' surface at different doses whereas the XRD results indicated the presence of residual stresses in the irradiated specimens. Williamson-Hall analysis of the diffraction peaks was carried out to investigate changes in crystallite size and lattice strain in the irradiated specimens. The tensile properties such as the yield stress, ultimate tensile stress and percentage elongation exhibited a decreasing trend after irradiation in general, however, an inconsistent behavior was observed in their dependence on proton dose. The changes in tensile properties of Zr were associated with the production of radiation-induced defects including bubbles, cracks, precipitates and simultaneous recovery by the thermal energy generated with the increase of irradiation dose.

  2. Grain growth behavior and high-temperature high-strain-rate tensile ductility of iridium alloy DOP-26

    International Nuclear Information System (INIS)

    McKamey, C.G.; Gubbi, A.N.; Lin, Y.; Cohron, J.W.; Lee, E.H.; George, E.P.

    1998-04-01

    This report summarizes results of studies conducted to date under the Iridium Alloy Characterization and Development subtask of the Radioisotope Power System Materials Production and Technology Program to characterize the properties of the new-process iridium-based DOP-26 alloy used for the Cassini space mission. This alloy was developed at Oak Ridge National Laboratory (ORNL) in the early 1980's and is currently used by NASA for cladding and post-impact containment of the radioactive fuel in radioisotope thermoelectric generator (RTG) heat sources which provide electric power for interplanetary spacecraft. Included within this report are data generated on grain growth in vacuum or low-pressure oxygen environments; a comparison of grain growth in vacuum of the clad vent set cup material with sheet material; effect of grain size, test temperature, and oxygen exposure on high-temperature high-strain-rate tensile ductility; and grain growth in vacuum and high-temperature high-strain-rate tensile ductility of welded DOP-26. The data for the new-process material is compared to available old-process data

  3. Effects of thermal - mechanical treatment in the creep - and tensile properties of niobium at high temperature

    International Nuclear Information System (INIS)

    Botta Filho, W.J.; Pinatti, Dyonisio G.

    1981-01-01

    Mechanical behavior of Nb at high temperature was studied based upon the samples morfology. The samples were obtainned after thermal mechanical treatment of 50mm diameter and 250mm length ingot produced by electron beam vacuum. A lot of the samples was tensile tested as a function of temperature showing small interstitials solute effect and a matrix hardened probably by substitutionals. Other lot was creep tested at homologous temperature of 0,34 and stress between 80 and 120 MPa. The results of these tests were analysed as a function of the sample morfology and showed a dependence of the percentage of recrystalization and of the grain size on the minimum creep rate. The fracture analysis showed significant effect of the oxygen content although it didn't contribute to the creep results. (Author) [pt

  4. Microstructure, Tensile and Fatigue Properties of Al-5 wt.%Mg Alloy Manufactured by Twin Roll Strip Casting

    Science.gov (United States)

    Heo, Joon-Young; Baek, Min-Seok; Euh, Kwang-Jun; Lee, Kee-Ahn

    2018-04-01

    This study investigated the microstructure, tensile and fatigue properties of Al-5 wt.%Mg alloy manufactured by twin roll strip casting. Strips cast as a fabricated (F) specimen and a specimen heat treated (O) at 400 °C/5 h were produced and compared. In the F specimen, microstructural observation discovered clustered precipitates in the center area, while in the O specimen precipitates were relatively more evenly distributed. Al, Al6(Mn, Fe), Mg2Al3 and Mg2Si phases were observed. However, most of the Mg2Al3 phase in the heat-treated O specimen was dissolved. A room temperature tensile test measured yield strength of 177.7 MPa, ultimate tensile strength of 286.1 MPa and elongation of 11.1% in the F specimen and 167.7 MPa (YS), 301.5 MPa (UTS) and 24.6% (EL) in the O specimen. A high cycle fatigue test measured a fatigue limit of 145 MPa in the F specimen and 165 MPa in the O specimen, and the O specimen achieved greater fatigue properties in all fatigue stress conditions. The tensile and fatigue fracture surfaces of the above-mentioned specimens were observed, and this study attempted to investigate the tensile and fatigue deformation behavior of strip cast Al-5 wt.%Mg based on the findings.

  5. Microstructure and elevated-temperature tensile properties of differential pressure sand cast Mg-4Y-3Nd-0.5Zr alloy

    Directory of Open Access Journals (Sweden)

    Hong-hui Liu

    2016-01-01

    Full Text Available The microstructures of an Mg-4Y-3Nd-0.5Zr alloy by differential pressure casting were investigated using scanning electron microscopy (SEM and transmission electron microscopy (TEM, and its tensile deformation behavior was measured using a Gleeble1500D themo-simulation machine in the temperature range of 200 to 400 °C at initial strain rates of 5×10-4 to 10-1 s-1. Results show that the as-cast microstructure consists of primary α-Mg phase and bone-shaped Mg5RE eutectic phase distributed along the grain boundary. The eutectic phase is dissolved into the matrix after solution treatment and subsequently precipitates during peak aging. Tensile deformation tests show that the strain rate has little effect on stress under 300 °C. Tensile stress decreases with an increase in temperature and the higher strain rate leads to an increase in stress above 300 °C. The fracture mechanism exhibits a mixed quasi-cleavage fracture at 200 °C, while the fracture above 300 °C is a ductile fracture. The dimples are melted at 400 °C with the lowest strain rate of 10-4 s-1.

  6. Characteristics of the tensile mechanical properties of fresh and dry forewings of beetles

    Energy Technology Data Exchange (ETDEWEB)

    Tuo, Wanyong [School of Civil Engineering & International Institute for Urban Systems Engineering, Southeast University, Nanjing 210096 (China); School of Civil & Architectural Engineering, Anyang Institute of Technology, Anyang 455000 (China); Chen, Jinxiang, E-mail: chenjpaper@yahoo.co.jp [School of Civil Engineering & International Institute for Urban Systems Engineering, Southeast University, Nanjing 210096 (China); Wu, Zhishen; Xie, Juan [School of Civil Engineering & International Institute for Urban Systems Engineering, Southeast University, Nanjing 210096 (China); Wang, Yong [Nantong Vocational University, Nantong, Jiangsu 226007 (China)

    2016-08-01

    Based on a tensile experiment and observations by scanning electron microscopy (SEM), this study demonstrated the characteristics of the tensile mechanical properties of the fresh and dry forewings of two types of beetles. The results revealed obvious differences in the tensile fracture morphologies and characteristics of the tensile mechanical properties of fresh and dry forewings of Cybister tripunctatus Olivier and Allomyrina dichotoma. For fresh forewings of these two types of beetles, a viscous, flow-like, polymer matrix plastic deformation was observed on the fracture surfaces, with soft morphologies and many fibers being pulled out, whereas on the dry forewings, the tensile fracture surfaces were straightforward, and there were no features resembling those found on the fresh forewings. The fresh forewings exhibited a greater fracture strain than the dry forewings, which was caused by the relative slippage of hydroxyl inter-chain bonds due to the presence of water in the fibers and proteins in the fresh forewings. Our study is the first to demonstrate the phenomenon of sudden stress drops caused by the fracturing of the lower skin because the lower skin fractured before the forewings of A. dichotoma reached their ultimate tensile strength. We also investigated the reasons underlying this phenomenon. This research provides a much better understanding of the mechanical properties of beetle forewings and facilitates the correct selection of study objects for biomimetic materials and development of the corresponding applications. - Highlights: • There is a phenomenon of sudden stress drop on the tensile stress-train curve of forewing. • The causes of the differences of mechanical properties of fresh and dry forewings are explained. • The hypothesis raised in a previous review paper is verified. • This study brings better ideas into correct understanding of the mechanical properties that the biomimetic object exhibits.

  7. Influence of additives on the microstructure and tensile properties of near-eutectic Al-10.8%Si cast alloy

    International Nuclear Information System (INIS)

    Mohamed, A.M.A.; Samuel, A.M.; Samuel, F.H.; Doty, H.W.

    2009-01-01

    The continuing quest for aluminum castings with enhanced mechanical properties for applications in the automotive industries has intensified the interest in aluminum-silicon alloys. In Al-Si alloys, the properties are influenced by the shape and distribution of the eutectic silicon particles in the matrix, as also by the iron intermetallics and copper phases that occur upon solidification. The detailed microstructure and tensile properties of as-cast and heat-treated new experimental alloy belonging to cast Al-Si near-eutectic alloys have been investigated as a function of Fe, Mn, Cu, and Mg content. Microstructural examination was carried out using optical microscopy, image analysis, and electron probe microanalysis (EPMA), wavelength dispersive spectroscopic (WDS) analysis facilities. Tensile properties upon artificial aging in the temperature range of 155-240 o C for 5 h were also investigated. The results show that the volume fraction of Fe-intermetallics increases as the iron or manganese contents increase. Compact polygonal or star-like particles form when the sludge factor is greater than 2.1. The Al 2 Cu phase was observed to dissolve almost completely during solution heat treatment of all the alloys studied, especially those containing high levels of Mg and Fe, while Al 5 Cu 2 Mg 8 Si 6 , sludge, and α-Fe phases were found to persist after solution heat treatment. The β-Al 5 (Fe,Mn)Si phase dissolved partially in Sr-modified alloys, and its dissolution became more pronounced after solution heat treatment. At 0.5% Mn, the β-Fe phase forms when the Fe content is above 0.75%, causing the tensile properties to decrease drastically. The same results are obtained when the levels of both Fe and Mn are increased beyond 0.75%, because of sludge formation. On the other hand, the tensile properties of the Cu-containing alloys are affected slightly at high levels of Mg as a result of the formation of Al 5 Cu 2 Mg 8 Si 6 which decreases the amount of free Mg

  8. Mechanical Properties and Tensile Fatigue of Graphene Nanoplatelets Reinforced Polymer Nanocomposites

    Directory of Open Access Journals (Sweden)

    Ming-Yuan Shen

    2013-01-01

    Full Text Available Graphene nanoplatelets (GNPs are novel nanofillers possessing attractive characteristics, including robust compatibility with most polymers, high absolute strength, and cost effectiveness. In this study, GNPs were used to reinforce epoxy composite and epoxy/carbon fiber composite laminates to enhance their mechanical properties. The mechanical properties of GNPs/epoxy nanocomposite, such as ultimate tensile strength and flexure properties, were investigated. The fatigue life of epoxy/carbon fiber composite laminate with GPs-added 0.25 wt% was increased over that of neat laminates at all levels of cyclic stress. Consequently, significant improvement in the mechanical properties of ultimate tensile strength, flexure, and fatigue life was attained for these epoxy resin composites and carbon fiber-reinforced epoxy composite laminates.

  9. Effect of normalization heat treatment on creep and tensile properties of modified 9Cr-1Mo steel

    International Nuclear Information System (INIS)

    Panneer Selvi, S.; Sakthivel, T.; Parameswaran, P.; Laha, K.

    2016-01-01

    Creep and tensile properties have been investigated on modified 9Cr-1Mo steel subjected to single and double normalization heat treatments. Optical, scanning and transmission electron microscopic investigation revealed the presence of refined prior austenite grain size and fine M 23 C 6 precipitates in the double normalized steel compared to the steel subjected to single normalization heat treatment. Increased creep strain and significant reduction in creep rupture life were observed with the double normalized steel in comparison with single normalized steel. Increased tensile ductility coupled with marginal decrease in tensile strength at higher test temperature was observed with double normalized steel compared to single normalized steel. It has been attributed to the presence of refined prior austenite grain size and coarsening of Nb rich MX precipitates in double normalized steel. (author)

  10. Phase Morphology and Mechanical Properties of Cyclic Butylene Terephthalate Oligomer-Containing Rubbers: Effect of Mixing Temperature

    Directory of Open Access Journals (Sweden)

    István Zoltán Halász

    2016-08-01

    Full Text Available In this work, the effect of mixing temperature (Tmix on the mechanical, rheological, and morphological properties of rubber/cyclic butylene terephthalate (CBT oligomer compounds was studied. Apolar (styrene butadiene rubber, SBR and polar (acrylonitrile butadiene rubber, NBR rubbers were modified by CBT (20 phr for reinforcement and viscosity reduction. The mechanical properties were determined in tensile, tear, and dynamical mechanical analysis (DMTA tests. The CBT-caused viscosity changes were assessed by parallel-plate rheometry. The morphology was studied by scanning electron microscopy (SEM. CBT became better dispersed in the rubber matrices with elevated mixing temperatures (at which CBT was in partially molten state, which resulted in improved tensile properties. With increasing mixing temperature the size of the CBT particles in the compounds decreased significantly, from few hundred microns to 5–10 microns. Compounding at temperatures above 120 °C and 140 °C for NBR and SBR, respectively, yielded reduced tensile mechanical properties most likely due to the degradation of the base rubber. The viscosity reduction by CBT was more pronounced in mixes with coarser CBT dispersions prepared at lower mixing temperatures.

  11. Tensile and Torsional Structural Properties of the Native Scapholunate Ligament.

    Science.gov (United States)

    Pang, Eric Quan; Douglass, Nathan; Behn, Anthony; Winterton, Matthew; Rainbow, Michael J; Kamal, Robin N

    2018-02-17

    The ideal material for reconstruction of the scapholunate interosseous ligament (SLIL) should replicate the mechanical properties of the native SLIL to recreate normal kinematics and prevent posttraumatic arthritis. The purpose of our study was to evaluate the cyclic torsional and tensile properties of the native SLIL and load to failure tensile properties of the dorsal SLIL. The SLIL bone complex was resected from 10 fresh-frozen cadavers. The scaphoid and lunate were secured in polymethylmethacrylate and mounted on a test machine that incorporated an x-y stage and universal joint, which permitted translations perpendicular to the rotation/pull axis as well as nonaxial angulations. After a 1 N preload, specimens underwent cyclic torsional testing (±0.45 N m flexion/extension at 0.5 Hz) and tensile testing (1-50 N at 1 Hz) for 500 cycles. Lastly, the dorsal 10 mm of the SLIL was isolated and displaced at 10 mm/min until failure. During intact SLIL cyclic torsional testing, the neutral zone was 29.7° ± 6.6° and the range of rotation 46.6° ± 7.1°. Stiffness in flexion and extension were 0.11 ± 0.02 and 0.12 ± 0.02 N m/deg, respectively. During cyclic tensile testing, the engagement length was 0.2 ± 0.1 mm, the mean stiffness was 276 ± 67 N/mm, and the range of displacement was 0.4 ± 0.1 mm. The dorsal SLIL displayed a 0.3 ± 0.2 mm engagement length, 240 ± 65 N/mm stiffness, peak load of 270 ± 91 N, and displacement at peak load of 1.8 ± 0.3 mm. We report the torsional properties of the SLIL. Our novel test setup allows for free rotation and translation, which reduces out-of-plane force application. This may explain our observation of greater dorsal SLIL load to failure than previous reports. By matching the natural ligament with respect to its tensile and torsional properties, we believe that reconstructions will better restore the natural kinematics of the wrist and lead to improved outcomes. Future clinical studies should aim to investigate this

  12. Influence of injection temperatures and fiberglass compositions on mechanical properties of polypropylene

    Science.gov (United States)

    Keey, Tony Tiew Chun; Azuddin, M.

    2017-06-01

    Injection molding process appears to be one of the most suitable mass and cost efficiency manufacturing processes for polymeric parts nowadays due to its high efficiency of large scale production. When down-scaling the products and components, the limits of conventional injection molding process are reached. These constraints had initiated the development of conventional injection molding process into a new era of micro injection molding technology. In this study, fiberglass reinforced polypropylenes (PP) with various glass fiber percentage materials were used. The study start with fabrication of micro tensile specimens at three different injection temperature, 260°C, 270°C and 280°C for different percentage by weight of fiberglass reinforced PP. Then evaluate the effects of various injection temperatures on the tensile properties of micro tensile specimens. Different percentage by weight of fiberglass reinforced PP were tested as well and it was found that 20% fiberglass reinforced PP possessed the greatest percentage increase of tensile strength with increasing temperatures.

  13. Elevated Temperature Properties of Commercially Available NITE-SiC/SiC Composites

    International Nuclear Information System (INIS)

    Choi, Y.B.; Hinoki, T.; Kohyama, A.

    2007-01-01

    Full text of publication follows: Continuous fiber-reinforced ceramic matrix composites (CMCs) have been expected as a new type of material having high fracture resistance up to a high temperature. In recent years, there have been extensive efforts in our research group to develop high performance SiC/SiC composites for energy applications, where improvements in mechanical properties and damage resistance by innovative new fabrication process with emphasis on interface improvement have been greatly accomplished. One of the most outstanding accomplishments is the Nano-powder Infiltration and Transient Eutectic (NITE) process using PyC coated Tyranno-SA fibers. For making SiC/SiC composites more attractive and competitive for high temperature structural components and for other industrial applications, one of the key issues is to demonstrate its reliability and safety under severe environments. Also to demonstrate the potential to produce SiC/SiC by NITE process from large scale production line at industries is very important. This paper provides fundamental database of mechanical properties and microstructure of Cera-NITE, the trade name of NITE-SiC/SiC composites. The mechanical properties were evaluated by uni-axial tensile test from room temperature to high temperatures. The tensile properties, including elastic modulus, PLS and ultimate tensile strength, are superior to those of other conventional SiC/SiC composites. The macroscopic observation of Cera-NITE indicated high density as planned with almost no-porosity and cracks. Furthermore, Cera-NITE showed outstanding microstructural uniformity. The characteristic variation coming from the sampling location was hardly observed.. Further information about database of properties and microstructure at evaluated temperature will be provided. (authors)

  14. Tensile strength of Zr-2.5 Nb pressure tubes: A statistical study

    Energy Technology Data Exchange (ETDEWEB)

    Shah, Priti Kotak, E-mail: pritik@barc.gov.in [Senior Scientist, Bhabha Atomic Research Centre, Mumbai, 400 085 (India); Dubey, J.S.; Datta, D.; Shriwastaw, R.S.; Rath, B.N.; Singh, R.N. [Senior Scientist, Bhabha Atomic Research Centre, Mumbai, 400 085 (India); Anantharaman, S. [Head, Post Irradiation Examination Division, Bhabha Atomic Research Centre, Mumbai (India); Chakravartty, J.K. [Director, Materials Group, Bhabha Atomic Research Centre, Mumbai (India)

    2015-12-15

    Highlights: • Tensile properties in axial and transverse direction for a number of Indian Zr-2.5 Nb PHWR pressure tubes. • Distribution of tensile properties of double-melted and quadruple-melted pressure tubes. • Tensile properties at front-end and back-end of the quadruple melted pressure tubes at room temperature and at 300 °C. - Abstract: In order to get an idea of the statistical variation in the tensile properties of the double-melted as well as quadruple melted Zr-2.5 Nb pressure tubes (PTs) and also the variation in tensile properties between the two ends of the pressure tubes, tension tests were carried out on around 50 pressure tube off-cuts. Longitudinal and transverse tensile specimens were prepared from these off-cuts of pressure tubes of double-melted and quadruple melted types. For quadruple melted pressure tubes the specimens were tested from both front-end and back-end off-cuts. Miniature flat tensile specimens having 1.8 mm width and 1.5 mm thickness and 7.6 mm gauge length were prepared from the pressure tube off-cuts without any flattening treatment. Tension tests were carried out in a screw-driven machine at room temperature and 300 °C for both front-end and back-end off-cuts of each of 16 pressure tubes. In general the transverse specimens showed higher yield strength (YS) and ultimate tensile strength (UTS) compared to the longitudinal specimens. Transverse specimens showed less strain hardening compared to the longitudinal specimens. The axial specimens showed higher uniform (UE) and total elongation (TE) compared to the transverse specimens. Double-melted pressure tubes showed relatively higher strength and lower elongation and larger standard deviation compared to the quadruple melted pressure tubes. Mean values of tensile properties showed that back-end off-cuts were relatively stronger and less ductile compared to the front-end off-cuts.

  15. Analysis of mechanical tensile properties of irradiated and annealed RPV weld overlay cladding

    Energy Technology Data Exchange (ETDEWEB)

    Novak, J [Czech Nuclear Society, Prague (Czech Republic)

    1994-12-31

    Mechanical tensile properties of irradiated and annealed outer layer of reactor pressure vessel weld overlay cladding, composed of Cr19Ni10Nb alloy, have been experimentally determined by conventional tensile testing and indentation testing. The constitutive properties of weld overlay cladding are then modelled with two homogenization models of the constitutive properties of elastic-plastic matrix-inclusion composites; numerical and experimental results are then compared. 10 refs., 4 figs., 4 tabs.

  16. Analysis of mechanical tensile properties of irradiated and annealed RPV weld overlay cladding

    International Nuclear Information System (INIS)

    Novak, J.

    1993-01-01

    Mechanical tensile properties of irradiated and annealed outer layer of reactor pressure vessel weld overlay cladding, composed of Cr19Ni10Nb alloy, have been experimentally determined by conventional tensile testing and indentation testing. The constitutive properties of weld overlay cladding are then modelled with two homogenization models of the constitutive properties of elastic-plastic matrix-inclusion composites; numerical and experimental results are then compared. 10 refs., 4 figs., 4 tabs

  17. High-Temperature Tensile Behaviors of Base Metal and Electron Beam-Welded Joints of Ni-20Cr-9Mo-4Nb Superalloy

    Science.gov (United States)

    Gupta, R. K.; Anil Kumar, V.; Sukumaran, Arjun; Kumar, Vinod

    2018-05-01

    Electron beam welding of Ni-20Cr-9Mo-4Nb alloy sheets was carried out, and high-temperature tensile behaviors of base metal and weldments were studied. Tensile properties were evaluated at ambient temperature, at elevated temperatures of 625 °C to 1025 °C, and at strain rates of 0.1 to 0.001 s-1. Microstructure of the weld consisted of columnar dendritic structure and revealed epitaxial mode of solidification. Weld efficiency of 90 pct in terms of strength (UTS) was observed at ambient temperature and up to an elevated temperature of 850 °C. Reduction in strength continued with further increase of test temperature (up to 1025 °C); however, a significant improvement in pct elongation is found up to 775 °C, which was sustained even at higher test temperatures. The tensile behaviors of base metal and weldments were similar at the elevated temperatures at the respective strain rates. Strain hardening exponent `n' of the base metal and weldment was 0.519. Activation energy `Q' of base metal and EB weldments were 420 to 535 kJ mol-1 determined through isothermal tensile tests and 625 to 662 kJ mol-1 through jump-temperature tensile tests. Strain rate sensitivity `m' was low ( 775 °C) is attributed to the presence of recrystallized grains. Up to 700 °C, the deformation is through slip, where strain hardening is predominant and effect of strain rate is minimal. Between 775 °C to 850 °C, strain hardening is counterbalanced by flow softening, where cavitation limits the deformation (predominantly at lower strain rate). Above 925 °C, flow softening is predominant resulting in a significant reduction in strength. Presence of precipitates/accumulated strain at high strain rate results in high strength, but when the precipitates were coarsened at lower strain rates or precipitates were dissolved at a higher temperature, the result was a reduction in strength. Further, the accumulated strain assisted in recrystallization, which also resulted in a reduction in strength.

  18. A comparison of the iraddiated tensile properties of a high-manganese austenitic steel and type 316 stainless steel

    International Nuclear Information System (INIS)

    Klueh, R.L.; Grossbeck, M.L.

    1984-01-01

    The USSR steel EP-838 is a high-manganese, low-nickel steel that also has lower chromium and molybdenum than type 316 stainless steel. Tensile specimens of 20%-cold-worked EP-838 and type 316 stainless steel were irradiated in the High Flux Isotope Reactor (HFIR) at the coolant temperature (approx.=50 0 C). A displacement damage level of 5.2 dpa was reached for the EP-838 and up to 9.5 dpa for the type 316 stainless steel. Tensile tests at room temperature and 300 0 C on the two steels indicated that the irradiation led to increased strength and decreased ductility compared to the unirradiated steels. Although the 0.2% yield stress of the type 316 stainless steel in the unirradiated condition was greater than that for the EP-838, after irradiation there was essentially no difference between the strength or ductility of the two steels. The results indicate that the replacement of the majority of the nickel by manganese and a reduction of chromium and molybdenum in an austenitic stainless steel of composition near that for type 316 stainless steel has little effect on the irradiated and unirradiated tensile properties at low temperatures. (orig.)

  19. Effects of holding pressure and process temperatures on the mechanical properties of moulded metallic parts

    DEFF Research Database (Denmark)

    Islam, Aminul; Hansen, Hans Nørgaard; Esteves, N.M.

    2013-01-01

    Metal injection moulding is gaining more and more importance over the time and needs more research to be done to understand the sensitivity of process to different process parameters. The current paper makes an attempt to better understand the effects of holding pressure and process temperatures...... on the moulded metallic parts. Stainless steel 316L is used in the investigation to produce the specimen by metal injection moulding (MIM) and multiple analyses were carried out on samples produced with different combinations of holding pressure, mould temperature and melt temperature. Finally, the parts were...... characterized to investigate mechanical properties like density, ultimate tensile strength, shrinkage etc. The results are discussed in the paper. The main conclusion from this study is unlike plastic moulding, the tensile properties of MIM parts doesn’t vary based on the flow direction of the melt, and tensile...

  20. Heat treatment effects on tensile properties of V-(4-5) wt.% Cr-(4-5) wt.% Ti alloys

    Energy Technology Data Exchange (ETDEWEB)

    Natesan, K.; Soppet, W.K. [Argonne National Lab., IL (United States)

    1997-08-01

    Effects of thermomechanical treatments on microstructures and mechanical properties are of interest for long term application of V-Cr-Ti alloys in fusion reactor systems. Influence of thermal annealing at 1050{degrees}C on stress/strain behavior, maximum engineering strength, and uniform and total elongation were evaluated. The results show that multiple annealing has minimal effect on the tensile properties of V-(4-5)Cr-(4-5)Ti alloys tested at room temperature and at 500{degrees}C.

  1. Elevated temperature tensile properties of borated 304 stainless steel: Effect of boride dispersion on strength and ductility

    International Nuclear Information System (INIS)

    Stephens, J.J.; Sorenson, K.B.; McConnell, P.

    1992-01-01

    Conventional cast and wrought (open-quotes Ingot Metallurgyclose quotes) borated 304 stainless steel has been used for a number of years in spent fuel storage applications where a combination of structural integrity and neutron criticality control are required. Similar requirements apply for materials used in transport cask baskets. However, in the high boron contents (>1.0 wt. %) which are most useful for criticality control, the conventional cast and wrought material suffers from low ductility as well as low impact toughness. The microstructural reason for these poor properties is the relatively coarse size of the boride particles in these alloys, which act as sites for crack initiation. Recently, a open-quotes premiumclose quotes grade of borated 304 stainless steel has been introduced (Strober and Smith, 1988) which is made by a Powder Metallurgy (PM) process. This material has greatly improved ductility and impact properties relative to the conventional cast and wrought product. In addition, an ASTM specification (ATSM A887) has been developed for borated stainless steel, containing 8 different material Types with respect to boron content - with the highest level (Type B7) having permissible range from 1.75 to 2.25 wt. % boron - and each Type contains two different Grades of material based on tensile and impact properties. While the ASTM specification is properties-based and does not require a specific production process for a particular grade of material, the PM material qualifies as open-quotes Grade Aclose quotes material while the conventional Ingot Metallurgy (IM) material generally qualifies as open-quotes Grade Bclose quotes material. This paper presents a comparison of the tensile properties of PM open-quotes Grade Aclose quotes material with that of the conventional IM open-quotes Grade Bclose quotes material for two selected Types (i.e., boron contents) as defined by the ASTM A887 specification: Types 304B5 and 304B7

  2. Tensile properties of cotton yarn as affected by different yarn singeing machine variables

    International Nuclear Information System (INIS)

    Tausief, M.Q.; Mahmood, N.; Iqbal, W.

    2014-01-01

    The present study endeavours to optimise the yam quality in respect of its tensile properties by choosing the best combination of the yam singeing machine variables for excellent manufacture results. This research study revealed that different values of winding speed, gas pressure and air pressure of yam singeing machine put significant effect upon the tensile properties of cotton yam after singeing. (author)

  3. Effect of phosphoric acid on the morphology and tensile properties of halloysite-polyurethane composites

    Science.gov (United States)

    Gaaz, Tayser Sumer; Luaibi, Hasan Mohammed; Al-Amiery, Ahmed A.; Kadhum, Abdul Amir H.

    2018-06-01

    The high aspect ratio of nanoscale reinforcements enhances the tensile properties of pure polymer matrix. The composites were first made by adding halloysite nanotubes (HNTs) at low weight percentages of 1, 2, and 3 wt% to thermoplastic polyurethane (TPU). Then, HNTs were phosphoric acid-treated before adding to TPU at same weight percentage to create phosphoric acid HNTs-TPU composites. The samples were fabricated using injection moulding. The HNTs-TPU composites were characterized according to the tensile properties including tensile strength, tensile strain and Young's modulus. The loading has shown its highest tensile values at 2 wt% HNTs loading and same findings are shown with the samples that treated with phosphoric acid. The tensile strength increased to reach 24.65 MPa compare with the 17.7 MPa of the neat TPU showing about 26% improvement. For the phosphoric acid-treated composites, the improvement has reached 35% compared to the neat sample. Regarding the tensile stain, the improvement was about 83% at 2 wt% HNTs loading. For Young's modulus, the results obtained in this study have shown that Young's modulus is linearly improved with either the loading content or the phosphoric acid treated achieving its highest values at 3 wt% HNTs of 14.53 MPa and 16.27 MPa for untreated and treated, respectively. FESEM results showed that HNTs were well dispersed in TPU matrix. Thus, HNTs-TPU has improved tensile properties compared with pure TPU due to the addition of nanofiller.

  4. Tensile properties of electron-beam-welded single crystals of molybdenum

    International Nuclear Information System (INIS)

    Hiraoka, Yutaka; Okada, Masatoshi; Irie, Hirosada; Fujii, Tadayuki.

    1987-01-01

    The purpose of this study is to investigate the macro- and microstructures and the tensile properties of electron-beam-welded single crystals of molybdenum. The single-crystal sheets were prepared by means of secondary recrystallization. The welding was carried out by a melt-run technique. The weld metal had the same crystallographic orientation as the base metal, and no grain boundary was observed. However, many large weld pores were formed mostly along the weld bond. The strength and ductility of the welded joints of single crystals were almost the same as those of the base metal (''annealed'' single crystals). It is concluded that the joint efficiency of molybdenum single crystals at room temperature or above was excellent and nearly 100 %. (author)

  5. The Effects of Fe-Particles on the Tensile Properties of Al-Si-Cu Alloys

    Directory of Open Access Journals (Sweden)

    Anton Bjurenstedt

    2016-12-01

    Full Text Available The effect of Fe-rich particles has been a topic for discussion in the aluminum casting industry because of the negative impact they exert on the mechanical properties. However, there are still contradictions on the effects of various morphologies of Fe-particles. In this study, microstructural characterization of tensile tested samples has been performed to reveal how unmodified and modified Fe-rich particles impact on the tensile behavior. Analysis of additions of Fe modifiers such as Mn and Cr, showed higher amounts of primary Fe-rich particles (sludge with increased porosity and, as result, degraded tensile properties. From the fracture analysis of tensile tested hot isostatic pressed (HIPed samples it could be concluded that the mechanical properties were mainly governed by the Fe-rich particles, which were fracturing through cleavage, not by the porosity.

  6. The tensile behavior of Ti36Ni49Hf15 high temperature shape memory alloy

    International Nuclear Information System (INIS)

    Wang, Y.Q.; Zheng, Y.F.; Cai, W.; Zhao, L.C.

    1999-01-01

    Recently, ternary Ti-Ni-Hf alloys have attracted great interest in the field of high temperature shape memory materials research and development. Extensive studies have been made on its manufacture process, constitutional phases, phase transformation behavior, the structure, substructure and interface structure of martensite and the precipitation behavior during ageing. Yet up to date there is no report about the fundamental mechanical properties of Ti-Ni-Hf alloys, such as the stress-strain data, the variation laws of the yield strength and elongation with the temperature. In the present study, tensile tests at various temperatures are employed to investigate the mechanical behavior of Ti-Ni-Hf alloy with different matrix structures, from full martensite to full parent phase structure, with the corresponding deformation mechanism discussed

  7. Tensile Properties of the Deep Transverse Metatarsal Ligament in Hallux Valgus

    Science.gov (United States)

    Abdalbary, Sahar Ahmed; Elshaarawy, Ehab A.A.; Khalid, Bahaa E.A.

    2016-01-01

    Abstract The deep transverse metatarsal ligament (DTML) connects the neighboring 2 metatarsal heads and is one of the stabilizers connecting the lateral sesamoid and second metatarsal head. In this study, we aimed to determine the tensile properties of the DTML in normal specimens and to compare these results with hallux valgus specimens. We hypothesized that the tensile properties of the DTML would be different between the 2 groups of specimens. The DTML in the first interspace was dissected from 12 fresh frozen human cadaveric specimens. Six cadavers had bilateral hallux valgus and the other 6 cadavers had normal feet. The initial length (L0) and cross-sectional area (A0) of the DTML were measured using a digital caliper, and tensile tests with load failure were performed using a material testing machine. There were significant between-groups differences in the initial length (L0) P = 0.009 and cross-sectional area (A0) of the DTML P = 0.007. There were also significant between-groups differences for maximum force (N) P = 0.004, maximum distance (mm) P = 0.005, maximum stress (N/mm2) P = 0.003, and maximum strain (%) P = 0.006. The DTML is an anatomical structure for which the tensile properties differ in hallux valgus. PMID:26937914

  8. Effect of cooling rate during solidification of Sn-9Zn lead-free solder alloy on its microstructure, tensile strength and ductile-brittle transition temperature

    Energy Technology Data Exchange (ETDEWEB)

    Prabhu, K.N., E-mail: prabhukn_2002@yahoo.co.in [Department of Metallurgical and Materials Engineering, National Institute of Technology Karnataka, Surathkal, Mangalore 575 025 (India); Deshapande, Parashuram; Satyanarayan [Department of Metallurgical and Materials Engineering, National Institute of Technology Karnataka, Surathkal, Mangalore 575 025 (India)

    2012-01-30

    Highlights: Black-Right-Pointing-Pointer Effect of cooling rate on tensile and impact properties of Sn-9Zn alloy was assessed. Black-Right-Pointing-Pointer Both DBTT and UTS of the solder alloy increased with increase in cooling rate. Black-Right-Pointing-Pointer An optimum cooling rate during solidification would minimize DBTT and maximize UTS. - Abstract: Solidification rate is an important variable during processing of materials, including soldering, involving solidification. The rate of solidification controls the metallurgical microstructure at the solder joint and hence the mechanical properties. A high tensile strength and a lower ductile-brittle transition temperature are necessary for reliability of solder joints in electronic circuits. Hence in the present work, the effect of cooling rate during solidification on microstructure, impact and tensile properties of Sn-9Zn lead-free solder alloy was investigated. Four different cooling media (copper and stainless steel moulds, air and furnace cooling) were used for solidification to achieve different cooling rates. Solder alloy solidified in copper mould exhibited higher cooling rate as compared to other cooling media. The microstructure is refined as the cooling rate was increased from 0.03 to 25 Degree-Sign C/s. With increase in cooling rate it was observed that the size of Zn flakes became finer and distributed uniformly throughout the matrix. Ductile-to-brittle transition temperature (DBTT) of the solder alloy increased with increase in cooling rate. Fractured surfaces of impact test specimens showed cleavage like appearance and river like pattern at very low temperatures and dimple like appearance at higher temperatures. The tensile strength of the solder alloy solidified in Cu and stainless moulds were higher as compared to air and furnace cooled samples. It is therefore suggested that the cooling rate during solidification of the solder alloy should be optimum to maximize the strength and minimize the

  9. Effect of cooling rate during solidification of Sn–9Zn lead-free solder alloy on its microstructure, tensile strength and ductile–brittle transition temperature

    International Nuclear Information System (INIS)

    Prabhu, K.N.; Deshapande, Parashuram; Satyanarayan

    2012-01-01

    Highlights: ► Effect of cooling rate on tensile and impact properties of Sn–9Zn alloy was assessed. ► Both DBTT and UTS of the solder alloy increased with increase in cooling rate. ► An optimum cooling rate during solidification would minimize DBTT and maximize UTS. - Abstract: Solidification rate is an important variable during processing of materials, including soldering, involving solidification. The rate of solidification controls the metallurgical microstructure at the solder joint and hence the mechanical properties. A high tensile strength and a lower ductile–brittle transition temperature are necessary for reliability of solder joints in electronic circuits. Hence in the present work, the effect of cooling rate during solidification on microstructure, impact and tensile properties of Sn–9Zn lead-free solder alloy was investigated. Four different cooling media (copper and stainless steel moulds, air and furnace cooling) were used for solidification to achieve different cooling rates. Solder alloy solidified in copper mould exhibited higher cooling rate as compared to other cooling media. The microstructure is refined as the cooling rate was increased from 0.03 to 25 °C/s. With increase in cooling rate it was observed that the size of Zn flakes became finer and distributed uniformly throughout the matrix. Ductile-to-brittle transition temperature (DBTT) of the solder alloy increased with increase in cooling rate. Fractured surfaces of impact test specimens showed cleavage like appearance and river like pattern at very low temperatures and dimple like appearance at higher temperatures. The tensile strength of the solder alloy solidified in Cu and stainless moulds were higher as compared to air and furnace cooled samples. It is therefore suggested that the cooling rate during solidification of the solder alloy should be optimum to maximize the strength and minimize the DBTT.

  10. A comparison of tensile properties of polyester composites reinforced with pineapple leaf fiber and pineapple peduncle fiber

    Science.gov (United States)

    Juraidi, J. M.; Shuhairul, N.; Syed Azuan, S. A.; Intan Saffinaz Anuar, Noor

    2013-12-01

    Pineapple fiber which is rich in cellulose, relatively inexpensive, and abundantly available has the potential for polymer reinforcement. This research presents a study of the tensile properties of pineapple leaf fiber and pineapple peduncle fiber reinforced polyester composites. Composites were fabricated using leaf fiber and peduncle fiber with varying fiber length and fiber loading. Both fibers were mixed with polyester composites the various fiber volume fractions of 4, 8 and 12% and with three different fiber lengths of 10, 20 and 30 mm. The composites panels were fabricated using hand lay-out technique. The tensile test was carried out in accordance to ASTM D638. The result showed that pineapple peduncle fiber with 4% fiber volume fraction and fiber length of 30 mm give highest tensile properties. From the overall results, pineapple peduncle fiber shown the higher tensile properties compared to pineapple leaf fiber. It is found that by increasing the fiber volume fraction the tensile properties has significantly decreased but by increasing the fiber length, the tensile properties will be increased proportionally. Minitab software is used to perform the two-way ANOVA analysis to measure the significant. From the analysis done, there is a significant effect of fiber volume fraction and fiber length on the tensile properties.

  11. Processing, Structural Characterization and Comparative Studies on Uniaxial Tensile Properties of a New Type of Porous Twisted Wire Material

    Directory of Open Access Journals (Sweden)

    Fei Wu

    2015-08-01

    Full Text Available A self-developed rotary multi-cutter device cuts stainless steel wire ropes into segments to fabricate twisted wires. Stainless steel porous twisted wire materials (PTWMs with a spatial composite intertexture structure are produced by the compaction and subsequent vacuum solid-phase sintering of twisted wires. The stainless steel PTWMs show two types of typical uniaxial tensile failure modes, i.e., a 45° angle fracture mode and an auxetic failure mode (the PTWMs expand along the direction perpendicular to the tension. The effects of the sintering parameters, porosities, wire diameters, and sampling direction on the tensile properties of the PTWMs are carefully investigated. By increasing the sintering temperature from 1130 °C to 1330 °C, the tensile strength of the PTWMs with 70% target porosity increased from 7.7 MPa to 28.6 MPa and the total failure goes down to 50%. When increasing the sintering time from 90 min to 150 min, the tensile strength increases from 12.4 MPa to 19.1 MPa and the total failure elongation drops to 78.6%. The tensile strength of the PTWMs increases from 28.9 MPa to 112.7 MPa with decreasing porosity from 69.5% to 46.0%, and the total failure elongation also increases from 14.8% to 40.7%. The tensile strength and the failure strain of the PTWMs with fine wires are higher than those of the PTWMs with coarse wires under the same porosity. Sampling direction has a small influence on the tensile properties of the PTWMs.

  12. Effects of grain refinement on cast structure and tensile properties of superalloy K4169 at high pouring temperature

    Directory of Open Access Journals (Sweden)

    Zi-qi Jie

    2016-03-01

    Full Text Available In order to improve the filling ability of large complex thin wall castings, the pouring temperature should be increased, but this will result in the grain coarsening. To overcome this problem, two kinds of grain refiners of Co-Fe-Nb and Cr-Fe-Nb ternary alloys, which contain high stability compound particles, were prepared. The effects of the refiners on the as-cast structures and tensile properties of the K4169 superalloy with different casting conditions were studied by analyzing specimens 110 mm long and 20 mm in diameter. Results showed that the mixture addition of the two refiners in the melt of K4169 can reduce the columnar grain region and decrease the equiaxed grain size greatly. After refinement, the amount of Laves phase decreases and its morphology changes from island to blocky structure. The carbides in the fine grain samples are fine and dispersive. Meanwhile, the porosity in specimens is decreased due to grain refinement. As a result, the yield strength, ultimate strength and the elongation of the specimens are increased. The grain refinement mechanisms are also discussed.

  13. Tensile properties of aluminized V-5Cr-5Ti alloy after exposure in air environment

    Energy Technology Data Exchange (ETDEWEB)

    Natesan, K.; Soppet, W.K. [Argonne National Lab., IL (United States)

    1997-08-01

    The objectives of this task are to (a) develop procedures to modify surface regions of V-Cr-Ti alloys in order to minimize oxygen uptake by the alloys when exposed to environments that contain oxygen, (b) evaluate the oxygen uptake of the surface-modified V-Cr-Ti alloys as a function of temperature an oxygen partial pressure in the exposure environment, (c) characterize the microstructures of oxide scales and oxygen trapped at the grain boundaries of the substrate alloys, and (d) evaluate the influence of oxygen uptake on the tensile properties of the modified alloys at room and elevated temperatures.

  14. Microstructures and Tensile Properties of Al–Cu Matrix Composites Reinforced with Nano-Sized SiCp Fabricated by Semisolid Stirring Process

    Directory of Open Access Journals (Sweden)

    Feng Qiu

    2017-02-01

    Full Text Available The nano-sized SiCp/Al–Cu composites were successfully fabricated by combining semisolid stirring with ball milling technology. Microstructures were examined by an olympus optical microscope (OM, field emission scanning electron microscope (FESEM and transmission electron microscope (TEM. Tensile properties were studied at room temperature. The results show that the α-Al dendrites of the composites were strongly refined, especially in the composite with 3 wt. % nano-sized SiCp, of which the morphology of the α-Al changes from 200 μm dendritic crystal to 90 μm much finer equiaxial grain. The strength and ductility of the composites are improved synchronously with the addition of nano-sized SiCp particles. The as-cast 3 wt. % nano-sized SiCp/Al–Cu composite displays the best tensile properties, i.e., the yield strength, ultimate tensile strength (UTS and fracture strain increase from 175 MPa, 310 MPa and 4.1% of the as-cast Al–Cu alloy to 220 MPa, 410 MPa and 6.3%, respectively. The significant improvement in the tensile properties of the composites is mainly due to the refinement of the α-Al dendrites, nano-sized SiCp strengthening, and good interface combination between the SiCp and Al–Cu alloys.

  15. Properties of Reinforced Concrete Steel Rebars Exposed to High Temperatures

    Directory of Open Access Journals (Sweden)

    İlker Bekir Topçu

    2008-01-01

    Full Text Available The deterioration of the mechanical properties of yield strength and modulus of elasticity is considered as the primary element affecting the performance of steel structures under fire. In this study, hot-rolled S220 and S420 reinforcement steel rebars were subjected to high temperatures to investigate the fire performance of these materials. It is aimed to determine the remaining mechanical properties of steel rebars after elevated temperatures. Steels were subjected to 20, 100, 200, 300, 500, 800, and 950∘C temperatures for 3 hours and tensile tests were carried out. Effect of temperature on mechanical behavior of S220 and S420 were determined. All mechanical properties were reduced due to the temperature increase of the steel rebars. It is seen that mechanical properties of S420 steel was influenced more than S220 steel at elevated temperatures.

  16. Effects of Sn addition on the microstructure and tensile properties of AX55 alloys

    Science.gov (United States)

    Qiu, K. Q.; Huang, P.

    2018-04-01

    The microstructures and tensile properties at both room and elevated temperatures for both the as-cast and as-aged Mg-5Al-5Ca (AX55) alloy with 0–2 wt% Sn addition were studied. The results indicate that the α-Mg dendrite is gradually refined and the interdendritic Al2Ca and Mg2Ca intermetallics become more connected with Sn addition. The as-cast AX55-1Sn alloy shows optimal ultimate tensile strength (UTS) at testing temperature from 25 to 225 °C. After T61 and T62 heat treatment, the eutectic-lamellar microstructure of the as-cast alloys tends to be spheroidized and distributed uniformly along the grain boundaries. While the alloys with higher Sn content show higher density of granulated and needle-shaped Al2Ca phases precipitated into α-Mg matrix, which results in the increase of UTS, yield strength (YS), elongation and microhardness with Sn addition. The morphology of CaMgSn phase can be improved by T62 treatment, which makes as-aged AX55-2.0Sn alloy exhibit a smaller decrease rate of the UTS at temperature up to 225 °C. The heat resistance of different heat-resistant magnesium alloys were compared and discussed by using the decrease rate of the UTS.

  17. Tensile and fracture toughness properties of MA957: implications to the development of nanocomposited ferritic alloys

    International Nuclear Information System (INIS)

    Alinger, M.J.; Odette, G.R.; Lucas, G.E.

    2002-01-01

    A study to explore approaches to optimizing nanocomposited ferritic alloys was carried out on dispersion strengthened mechanically alloyed (MA) MA957, in the form of extruded bar stock. Previous studies had indicated that this alloy manifested superior high temperature strength and radiation stability, but was extremely brittle in notch impact tests. Thus our objective was to develop a combination of tensile, fracture toughness and microstructural data to clarify the basis for this brittle behavior. To this end, tensile properties and fracture toughness were characterized as a function of temperature in various orientations relative to the grain and inclusion structures. This database along with extensive fractography suggests that brittleness is due to the presence of a large volume fraction of impurity alumina stringers. In orientations where the effects of the stringers are reduced, much higher toughness was observed. These results provide a path for alloy development approach to achieve high strength and toughness

  18. Tensile and fracture toughness properties of MA957: implications to the development of nanocomposited ferritic alloys

    Science.gov (United States)

    Alinger, M. J.; Odette, G. R.; Lucas, G. E.

    2002-12-01

    A study to explore approaches to optimizing nanocomposited ferritic alloys was carried out on dispersion strengthened mechanically alloyed (MA) MA957, in the form of extruded bar stock. Previous studies had indicated that this alloy manifested superior high temperature strength and radiation stability, but was extremely brittle in notch impact tests. Thus our objective was to develop a combination of tensile, fracture toughness and microstructural data to clarify the basis for this brittle behavior. To this end, tensile properties and fracture toughness were characterized as a function of temperature in various orientations relative to the grain and inclusion structures. This database along with extensive fractography suggests that brittleness is due to the presence of a large volume fraction of impurity alumina stringers. In orientations where the effects of the stringers are reduced, much higher toughness was observed. These results provide a path for alloy development approach to achieve high strength and toughness.

  19. Spectroscopic analysis of radiation-generated changes in tensile properties of a polyetherimide film

    International Nuclear Information System (INIS)

    Long, E.R. Jr.; Long, S.A.T.

    1985-05-01

    The effects of electron radiation on Ultem, a polyetherimide were studied for doses from 2 x 10 to the 9th power to 6 x 10 to the 9th power rad. Specimens were studied for tensile property testing and for electron paramagnetic resonance and infrared spectroscopic measurements of molecular structure. A Faraday cup design and a method for remote temperature measurement were developed. The spectroscopic data show that radiation caused dehydrogenation of methyl groups, rupture of main-chain ether linkage, and opening of imide rings, all to form radicals and indicate that the so-formed atomic hydrogen attached to phenyl radicals, but not to phenoxyl radicals, which would have formed hydroxyls. The observed decays of the radiation-generated phenoxyl, gem-dimethyl, and carbonyl radicals were interpreted as a combining of the radicals to form crosslinking. This crosslinking is the probable cause of the major reduction in the elongation of the tensile specimens after irradiation. Subsequent classical solubility tests indicate that the irradiation caused massive crosslinking

  20. Effects of Strain Rate and Temperature on the Mechanical Properties of Medium Manganese Steels

    Energy Technology Data Exchange (ETDEWEB)

    Rana, Radhakanta [Colorado School of Mines, Golden, CO (United States); Matlock, David K [Colorado School of Mines, Golden, CO (United States); Speer, John G [Colorado School of Mines, Golden, CO (United States); De Moor, Emmanuel [Colorado School of Mines, Golden, CO (United States)

    2016-11-16

    The effects of temperature (-60 to 100 °C) and strain rate (0.002 to 0.2 s-1) on the properties of Al-alloyed 7 and 10 wt-% Mn steels containing 34.8 and 57.3 vol-% austenite respectively were evaluated by tensile tests in isothermal liquid baths. The tensile strengths of both medium Mn steels increased with a decrease in temperature owing to the decreased austenite stability with a decrease in temperature. At lower temperatures the strength of the 10MnAl steel was highest, a consequence of the higher strain hardening rate caused by more austenite transformation to martensite with deformation. The resulting properties are assessed with a consideration of the effects of strain rate and deformation on adiabatic heating which was observed to be as high as 95o C.

  1. Tensile properties of V-Cr-Ti alloys after exposure in hydrogen-containing environments

    International Nuclear Information System (INIS)

    Natesan, K.; Soppet, W.K.

    1998-01-01

    A systematic study has been initiated at Argonne National Laboratory to evaluate the performance of several V-Cr-Ti alloys after exposure to environments containing hydrogen at various partial pressures. The goal is to correlate the chemistry of the exposure environment with hydrogen uptake in the samples and its influence on the microstructure and tensile properties of the alloys. At present, the principal effort has focused on the V-4Cr-4Ti alloy of heat identified as BL-71; however other alloys (V-5Cr-5Ti alloy of heats BL-63, and T87, plus V-4Cr-4Ti alloy from General Atomics [GA]) are also being evaluated. Other variables of interest are the effect of initial grain size on the tensile behavior of the alloys. Experiments conducted on specimens of various V-Cr-Ti alloys exposed to pH 2 levels of 0.01 and 3 x 10 -6 torr showed negligible effect of H 2 on either maximum engineering stress or uniform and total elongation. However, uniform and total elongation decreased substantially when the alloys were exposed to 1.0 torr H 2 pressure. Preliminary data from sequential exposures of the materials to low-pO 2 and several low-pH 2 environments did not reveal an adverse effect on the maximum engineering stress or on uniform and total elongation. Further, tests in H 2 environments on specimens annealed at different temperatures showed that grain-size variation by a factor of ∼2 had little or no effect on tensile properties

  2. Influence of chemical treatment on the tensile properties of kenaf fiber reinforced thermoplastic polyurethane composite

    Directory of Open Access Journals (Sweden)

    Y. A. El-Shekeil

    2012-12-01

    Full Text Available In this study, the effect of polymeric Methylene Diphenyl Diisocyanate (pMDI chemical treatment on kenaf (Hibiscus cannabinus reinforced thermoplastic polyurethane (TPU/KF was examined using two different procedures. The first consisted of treating the fibers with 4% pMDI, and the second involved 2% NaOH + 4% pMDI. The composites were characterized according to their tensile properties, Fourier Transform Infrared Spectroscopy (FTIR and Scanning Electron Microscopy (SEM. The treatment of the composite with 4% pMDI did not significantly affect its tensile properties, but the treatment with 2% NaOH + 4% pMDI significantly increased the tensile properties of the composite (i.e., 30 and 42% increases in the tensile strength and modulus, respectively. FTIR also showed that treatment with 2% NaOH + 4% pMDI led to the strongest H-bonding. Additionally, the surface morphology of specimens after tensile fracture confirmed that the composite treated with 2% NaOH + 4% pMDI had the best adhesion and wettability.

  3. Microstructure and tensile properties of Fe-40 at. pct Al alloys with C, Zr, Hf, and B additions

    Science.gov (United States)

    Gaydosh, D. J.; Draper, S. L.; Nathal, M. V.

    1989-01-01

    The influence of small additions of C, Zr, and Hf, alone or in combination with B, on the microstructure and tensile behavior of substoichiometric FeAl was investigated. Tensile properties were determined from 300 to 1100 K on powder which was consolidated by hot extrusion. All materials possessed some ductility at room temperature, although ternary additions generally reduced ductility compared to the binary alloy. Adding B to the C- and Zr-containing alloys changed the fracture mode from intergranular to transgranular and restored the ductility to approximately 5 percent elongation. Additions of Zr and Hf increased strength up to about 900 K. Fe6Al6Zr and Fe6Al6Hf precipitates, both with identical body-centered tetragonal structures, were identified as the principal second phase in these alloys. Strength decreased steadily as temperature increased above 700 K, as diffusion-assisted mechanisms became operative. Although all alloys had similar strengths at 1100 K, Hf additions significantly improved high-temperature ductility by suppressing cavitation.

  4. Effects of low doses of 14-MeV neutrons on the tensile properties of three binary copper alloys

    International Nuclear Information System (INIS)

    Heinisch, H.L.; Pintler, J.S.

    1986-12-01

    Miniature tensile specimens of high purity copper and copper alloyed respectively with five atom percent of Al, Mn, and Ni were irradiated with D-T fusion neutrons in the RTNS-II to fluences up to 1.3 x 10 18 n/cm 2 at 90 0 C. To compare fission and fusion neutron effects, some specimens were also irradiated at the same temperature to similar damage levels in the Omega West Reactor (OWR). Tensile tests were performed at room temperature, and the radiation-induced changes in tensile properties were examined as functions of displacements per atom (dpa). The irradiation-induced strengthening of Cu5%Mn is greater than that of Cu5%Al and Cu5%Ni, which behave about the same. However, all the alloys sustain less irradiation-induced strengthening by 14 MeV neutrons than pure copper, which is in contrast to the reported results of earlier work using hardness measurements. The effects of fission and fusion neutrons on the yield stress of Cu5%Al and Cu5%Ni correlate well on the basis of dpa, but the data for Cu5%Mn suggest that dpa may not be a good correlation parameter for this alloy in this fluence and temperature range

  5. Effect of helium on tensile properties of vanadium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Chung, H.M.; Billone, M.C.; Smith, D.L. [Argonne National Lab., IL (United States)

    1997-08-01

    Tensile properties of V-4Cr-4Ti (Heat BL-47), 3Ti-1Si (BL-45), and V-5Ti (BL-46) alloys after irradiation in a conventional irradiation experiment and in the Dynamic Helium Charging Experiment (DHCE) were reported previously. This paper presents revised tensile properties of these alloys, with a focus on the effects of dynamically generated helium of ductility and work-hardening capability at <500{degrees}C. After conventional irradiation (negligible helium generation) at {approx}427{degrees}C, a 30-kg heat of V-4Cr-4Ti (BL-47) exhibited very low uniform elongation, manifesting a strong susceptibility to loss of work-hardening capability. In contrast, a 15-kg heat of V-3Ti-1Si (BL -45) exhibited relatively high uniform elongation ({approx}4%) during conventional irradiation at {approx}427{degrees}C, showing that the heat is resistant to loss of work-hardening capability.

  6. Tensile properties and deformation mechanisms of a 14Cr ODS ferritic steel

    Energy Technology Data Exchange (ETDEWEB)

    Steckmeyer, A., E-mail: antonin.steckmeyer@cea.f [Service de Recherches Metallurgiques Appliquees, CEA Saclay, Gif-sur-Yvette (France); Praud, M.; Fournier, B.; Malaplate, J.; Garnier, J.; Bechade, J.L.; Tournie, I.; Tancray, A.; Bougault, A. [Service de Recherches Metallurgiques Appliquees, CEA Saclay, Gif-sur-Yvette (France); Bonnaillie, P. [Service de Recherche en Metallurgie Physique, CEA Saclay, Gif-sur-Yvette (France)

    2010-10-15

    The search for a new cladding material is part of the research studies carried out at CEA to develop a sodium-cooled fast reactor meeting the expectations of the Generation IV International Forum. In this study, the tensile properties of a ferritic oxide dispersion strengthened steel produced by hot extrusion at CEA have been evaluated. They prove the studied alloy to be as resistant as and more ductile than the other nano-reinforced alloys of literature. The effects of the strain rate and temperature on the total plastic strain of the material remind of diffusion phenomena. Intergranular damage and intergranular decohesion are clearly highlighted.

  7. Evaluation of tensile properties and water absortion of cassava starch film

    Science.gov (United States)

    Walster, R. Justin; Rozyanty, A. R.; Kahar, A. W. M.; Musa, L.; Shahnaz, S. B. S.

    2017-09-01

    Casava Starch film was prepared by casting method with different percentage of glycerol (0%, 0.5%, 1.0%, 1.5%, 2.0% and 2.5%) as plasticizer. The effect of glycerol content in starch film on mechanical and water absorption properties was studied. Results shows that the increase of glycerol content in cassava starch film had decrease the tensile strength, tensile modulus and increase the elongation of break properties. The result of water absorbency tended to increase for starch film with higher percentage of glycerol content. The incorporation of glycerol in cassava starch film had increase the water absorption ability due to increase of hydroxyl content contributed by glycerol.

  8. Tensile fracture properties of seven tropical grasses at different phenological stages

    NARCIS (Netherlands)

    Jacobs, A.A.A.; Scheper, J.A.; Benvenutti, M.A.; Gordon, I.J.; Poppi, D.P.; Elgersma, A.

    2011-01-01

    The intake of forage grasses by grazing ruminants is closely related to the mechanical fracture properties of grasses. The relationship between the tensile fracture properties of grasses and foraging behaviour is of particular importance in tropical reproductive swards composed of both stems and

  9. Some elevated temperature tensile and strain-controlled fatigue properties for a 9%Cr1Mo steel heat treated to simulate thick section material

    International Nuclear Information System (INIS)

    Sanderson, S.J.; Jacques, S.

    Current interest has been expressed in the usage of thick section 9%Cr1%Mo steel, particularly for UK Commercial Demonstration Fast Reactor (CDFR) steam generator tubeplates. This paper presents the results of some preliminary mechanical property test work on a single cast of the steel, heat treated to simulate heavy ruling sections encompassing thicknesses likely to be met in the CDFR context. The microstructures of the simulated thick section material were found to remain predominantly as tempered martensite even at the slowest transformation cooling rates used (50 deg. C/h). The effect of microstructure is reflected in the elevated temperature proof stress, tensile strength and strain-controlled fatigue endurance which were found to be comparable with the properties established for thin section normalised and tempered 9%Cr1%Mo steel. These results are extremely encouraging and, taken in conjunction with the results from other simulation work on this material, further demonstrate the potential of thick section 9%Cr1%Mo steel. (author)

  10. Swelling and tensile properties of neutron-irradiated vanadium alloys

    International Nuclear Information System (INIS)

    Loomis, B.A.; Smith, D.L.

    1990-07-01

    Vanadium-base alloys are candidates for use as structural material in magnetic fusion reactors. In comparison to other candidate structural materials (e.g., Type 316 stainless and HT-9 ferritic steels), vanadium-base alloys such as V-15Cr-5Ti and V-20Ti have intrinsically lower long-term neutron activation, neutron irradiation after-heat, biological hazard potential, and neutron-induced helium and hydrogen transmutation rates. Moreover, vanadium-base alloys can withstand a higher surface-heat, flux than steels because of their lower thermal stress factor. In addition to having these favorable neutronic and physical properties, a candidate alloy for use as structural material in a fusion reactor must have dimensional stability, i.e., swelling resistance, and resistance to embrittlement during the reactor lifetime at a level of structural strength commensurate with the reactor operating temperature and structural loads. In this paper, we present experimental results on the swelling and tensile properties of several vanadium-base alloys after irradiation at 420, 520, and 600 degree C to neutron fluences ranging from 0.3 to 1.9 x 10 27 neutrons/m 2 (17 to 114 atom displacements per atom [dpa])

  11. An Investigation on Tensile Properties of Glass Fiber/Aluminium Laminates

    Directory of Open Access Journals (Sweden)

    M. Sadighi

    2009-12-01

    Full Text Available The idea of combining low weight and good mechanical properties has led to efforts to develop a new light fiber/metal laminate (FML in the last decade. FMLs are hybrid composites consisting of alternating thin layers of metal sheets and fiber-reinforced epoxy prepregs. In this study, the effect of fiber orientation on tensile properties of this material is investigated both analytically and experimentally. An analytical constitutive model based on classical lamination theory by using Kirchhoff-Love assumption, which incorporates the elastic-plastic behavior of the aluminium alloy was applied. Test results show that fiber sheet, with zero angle in laminates, improve the tensile strength. The composite layers with different fiber orientation change specimens' mode of fracture. Good agreement is obtained between the model predictions and experimental results.

  12. Effect of grain refinement on the microstructure and tensile properties of thin 319 Al castings

    International Nuclear Information System (INIS)

    Shabani, M.J.; Emamy, M.; Nemati, N.

    2011-01-01

    The structural examinations and tensile properties of thin-section Al castings (319 Al alloy) have been investigated by applying a pattern with different cross sections (2-12 mm). Al-5Ti-1B and Al-5Zr grain refiners were added to the molten Al alloy to produce different levels of Ti (0.01%, 0.05%, 0.1% and 0.15%) and Zr (0.05%, 0.1%, 0.2%, 0.3%, 0.4% and 0.5%) in the castings. From macrostructural studies, it was found that Al-5Zr is less effective in grain refining of 319 alloy in comparison with Al-5Ti-1B master alloy. The optimum levels of grain refiners were selected for determination of tensile properties. T6 heat treatment was applied for selected specimens before tensile testing. Further structural results also showed that thinner sections are less affected by grain refiners. This observation was found to be in a good agreement with tensile test results, where tensile properties of the base and grain refined alloys did not show considerable differences in thinner sections (<6 mm).

  13. Microstructure and tensile properties of high strength duplex ferrite-martensite (DFM) steels

    International Nuclear Information System (INIS)

    Chakraborti, P.C.; Mitra, M.K.

    2007-01-01

    Duplex ferrite-martensite (DFM) steels containing 38-80% martensite of varying morphologies were developed by batch intercritical annealing of a commercial variety vanadium bearing 0.2% C-Mn steel at different temperatures. Microstructures before intercritical annealing were found to control the morphological distribution of the phase constituents of the developed DFM steels. Tensile test results revealed best strength-ductility combination for finely distributed lamellar ferrite-martensite phase aggregate containing ∼60% martensite developed from a prior martensitic structure. Taking consideration of the modified law of mechanical mixture the experimental tensile strength data of the developed DFM steels has been formulated with some success and very good estimation for tensile strengths of pure ferrite and low carbon martensite has been made from tensile strength data of DFM steels

  14. Effect of Local Post Weld Heat Treatment on Tensile Properties in Friction Stir Welded 2219-O Al Alloy

    Science.gov (United States)

    Chu, Guannan; Sun, Lei; Lin, Caiyuan; Lin, Yanli

    2017-11-01

    To improve the formability of the aluminum alloy welds and overcome the size limitation of the bulk post weld heat treatment (BPWHT) on large size friction stir welded joints, a local post weld heat treatment method (LPWHT) was proposed. In this method, the resistance heating as the moving heat source is adopted to only heat the weld seam. The temperature field of LPWHT and its influence on the mechanical properties and formability of FSW 2219-O Al alloy joints was investigated. The evaluation of the tensile properties of FSW samples was also examined by mapping the global and local strain distribution using the digital image correlation methodology. The results indicated that the formability was improved greatly after LPWHT, while the hardness distribution of the FSW joint was homogenized. The maximum elongation can reach 1.4 times that of as-welded joints with increase the strength and the strain of the nugget zone increased from 3 to 8% when annealing at 300 °C. The heterogeneity on the tensile deformation of the as-welded joints was improved by the nugget zone showing large local strain value and the reason was given according to the dimple fracture characteristics at different annealing temperatures. The tensile strength and elongation of LPWHT can reach 93.3 and 96.1% of the BPWHT, respectively. Thus, the LPWHT can be advantageous compared to the BPWHT for large size welds.

  15. Influence of thermo-mechanical treatment on the tensile properties of a modified 14Cr–15Ni stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Vijayanand, V.D., E-mail: vdvijayanand@igcar.gov.in; Laha, K.; Parameswaran, P.; Nandagopal, M.; Panneer Selvi, S.; Mathew, M.D.

    2014-10-15

    The titanium modified 14Cr–15Ni austenitic stainless steel is used as clad and wrapper material for fast breeder nuclear reactor. Thermo-mechanical treatments consisting of solution annealing at two different temperatures of 1273 and 1373 K followed by cold-work and thermal ageing have been imparted to the steel to tailor its microstructure for enhancing strength. Tensile tests have been carried out on the thermo-mechanically treated steel at nominal strain rate of 1.6 × 10{sup −4} s{sup −1} over a temperature range of 298–1073 K. The yield stress and the ultimate tensile strength of the steel increased with increase in solution treatment temperature and this has been attributed to the fine and higher density of Ti(C,N) precipitate. Tensile flow behaviour of the steel has been analysed using Ludwigson and Voce constitutive equations. The steel heat treated at higher solution temperature exhibited earlier onset of cross slip during tensile deformation. The rate of recovery at higher test temperatures was also influenced by variations in solution heat treatment temperature. In addition, dynamic recrystallization during tensile deformation at higher temperatures was profound for steel solution heat-treated at lower temperature. The differences in flow behaviour and softening mechanisms during tensile testing of the steel after different heat treated conditions have been attributed to the nature of Ti(C,N) precipitation.

  16. Influence of thermo-mechanical treatment on the tensile properties of a modified 14Cr–15Ni stainless steel

    International Nuclear Information System (INIS)

    Vijayanand, V.D.; Laha, K.; Parameswaran, P.; Nandagopal, M.; Panneer Selvi, S.; Mathew, M.D.

    2014-01-01

    The titanium modified 14Cr–15Ni austenitic stainless steel is used as clad and wrapper material for fast breeder nuclear reactor. Thermo-mechanical treatments consisting of solution annealing at two different temperatures of 1273 and 1373 K followed by cold-work and thermal ageing have been imparted to the steel to tailor its microstructure for enhancing strength. Tensile tests have been carried out on the thermo-mechanically treated steel at nominal strain rate of 1.6 × 10 −4 s −1 over a temperature range of 298–1073 K. The yield stress and the ultimate tensile strength of the steel increased with increase in solution treatment temperature and this has been attributed to the fine and higher density of Ti(C,N) precipitate. Tensile flow behaviour of the steel has been analysed using Ludwigson and Voce constitutive equations. The steel heat treated at higher solution temperature exhibited earlier onset of cross slip during tensile deformation. The rate of recovery at higher test temperatures was also influenced by variations in solution heat treatment temperature. In addition, dynamic recrystallization during tensile deformation at higher temperatures was profound for steel solution heat-treated at lower temperature. The differences in flow behaviour and softening mechanisms during tensile testing of the steel after different heat treated conditions have been attributed to the nature of Ti(C,N) precipitation

  17. Enhanced tensile properties of magnesium composites reinforced with graphene nanoplatelets

    International Nuclear Information System (INIS)

    Rashad, Muhammad; Pan, Fusheng; Hu, Huanhuan; Asif, Muhammad; Hussain, Shahid; She, Jia

    2015-01-01

    The aim of this study is to fabricate magnesium reinforced metal matrix composites using graphene nanoplatelets (GNPs) via powder metallurgy processing in order to enhance room temperature mechanical properties. The microstructural evaluation and mechanical behaviors of composite powders and extruded bulk materials were examined by X-ray diffraction (XRD), differential scanning calorimetry (DSC), Raman spectroscopy, transmission electron microscopy (TEM), scanning electron microscopy (SEM) equipped with energy-dispersive spectrometer and mechanical tests. The uniform dispersion and large specific surface area per volume of GNPs embedded in magnesium matrix led to increament in microhardness, tensile strength and fracture strains of the composites. For example, when employing the pure magnesium reinforced with 0.30 wt% GNPs, the increase of Young's modulus, yield strength, and failure strain of extruded nanocomposite was +131%, +49.5% and +74.2% respectively, compared to those of extruded materials with no GNPs additive. Additionally, mechanical properties of synthesized composites were compared with previously reported Mg–CNTs composites. It was found that GNPs outperform CNTs due their high specific surface area

  18. Enhanced tensile properties of magnesium composites reinforced with graphene nanoplatelets

    Energy Technology Data Exchange (ETDEWEB)

    Rashad, Muhammad, E-mail: rashadphy87@gmail.com [College of Materials Science and Engineering, Chongqing University, Chongqing 400044 (China); National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing 400044 (China); Pan, Fusheng, E-mail: fspan@cqu.edu.cn [College of Materials Science and Engineering, Chongqing University, Chongqing 400044 (China); National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing 400044 (China); Chongqing Academy of Science and Technology, Chongqing 401123 (China); Hu, Huanhuan [College of Materials Science and Engineering, Chongqing University, Chongqing 400044 (China); National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing 400044 (China); Asif, Muhammad [School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China); Hussain, Shahid [College of Materials Science and Engineering, Chongqing University, Chongqing 400044 (China); She, Jia [College of Materials Science and Engineering, Chongqing University, Chongqing 400044 (China); National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing 400044 (China)

    2015-04-10

    The aim of this study is to fabricate magnesium reinforced metal matrix composites using graphene nanoplatelets (GNPs) via powder metallurgy processing in order to enhance room temperature mechanical properties. The microstructural evaluation and mechanical behaviors of composite powders and extruded bulk materials were examined by X-ray diffraction (XRD), differential scanning calorimetry (DSC), Raman spectroscopy, transmission electron microscopy (TEM), scanning electron microscopy (SEM) equipped with energy-dispersive spectrometer and mechanical tests. The uniform dispersion and large specific surface area per volume of GNPs embedded in magnesium matrix led to increament in microhardness, tensile strength and fracture strains of the composites. For example, when employing the pure magnesium reinforced with 0.30 wt% GNPs, the increase of Young's modulus, yield strength, and failure strain of extruded nanocomposite was +131%, +49.5% and +74.2% respectively, compared to those of extruded materials with no GNPs additive. Additionally, mechanical properties of synthesized composites were compared with previously reported Mg–CNTs composites. It was found that GNPs outperform CNTs due their high specific surface area.

  19. Effect of native oxide layers on copper thin-film tensile properties: A reactive molecular dynamics study

    Energy Technology Data Exchange (ETDEWEB)

    Skarlinski, Michael D., E-mail: michael.skarlinski@rochester.edu [Materials Science Program, University of Rochester, Rochester, New York 14627 (United States); Quesnel, David J. [Materials Science Program, University of Rochester, Rochester, New York 14627 (United States); Department of Mechanical Engineering, University of Rochester, Rochester, New York 14627 (United States)

    2015-12-21

    Metal-oxide layers are likely to be present on metallic nano-structures due to either environmental exposure during use, or high temperature processing techniques such as annealing. It is well known that nano-structured metals have vastly different mechanical properties from bulk metals; however, difficulties in modeling the transition between metallic and ionic bonding have prevented the computational investigation of the effects of oxide surface layers. Newly developed charge-optimized many body [Liang et al., Mater. Sci. Eng., R 74, 255 (2013)] potentials are used to perform fully reactive molecular dynamics simulations which elucidate the effects that metal-oxide layers have on the mechanical properties of a copper thin-film. Simulated tensile tests are performed on thin-films while using different strain-rates, temperatures, and oxide thicknesses to evaluate changes in yield stress, modulus, and failure mechanisms. Findings indicate that copper-thin film mechanical properties are strongly affected by native oxide layers. The formed oxide layers have an amorphous structure with lower Cu-O bond-densities than bulk CuO, and a mixture of Cu{sub 2}O and CuO charge character. It is found that oxidation will cause modifications to the strain response of the elastic modulii, producing a stiffened modulii at low temperatures (<75 K) and low strain values (<5%), and a softened modulii at higher temperatures. While under strain, structural reorganization within the oxide layers facilitates brittle yielding through nucleation of defects across the oxide/metal interface. The oxide-free copper thin-film yielding mechanism is found to be a tensile-axis reorientation and grain creation. The oxide layers change the observed yielding mechanism, allowing for the inner copper thin-film to sustain an FCC-to-BCC transition during yielding. The mechanical properties are fit to a thermodynamic model based on classical nucleation theory. The fit implies that the oxidation of the

  20. Effect of low-temperature thermomechanical treatment on mechanical properties of low-alloying molybdenum alloys with carbide hardening

    International Nuclear Information System (INIS)

    Bernshtejn, L.M.; Zakharov, A.M.; Veller, M.V.

    1978-01-01

    Presented are results of testing low-temperature thermomechanical treatment of low-alloying molybdenum alloys, including quenching from 2100 deg C, 40% deformation by hydroextrusion and aging at the temperature of 1200-1400 deg C. Tensile tests at room temperature with the following processing of results have shown that low-temperature thermomechanical treatment of low-alloying molybdenum alloys of Mo-Zr-C and Mo-Zr-Nb-C systems leads to a significant increase in low-temperature mechanical properties (strength properties - by 30-35%, ductility - by 30-40%) as compared with conventional heat treatment (aging after quenching). The treatment proposed increases resistance to small, as well as large plastic deformations, and leads to a simultaneous rise of strength and plastic properties at all stages of tensile test. Alloying of the Mo-Zr-C system with niobium increases both strength and plastic characteristics as compared with alloys without niobium when testing samples, subjected to low temperature thermomechanical treatment and conventional heat treatment at room temperature

  1. High-Temperature Tensile and Tribological Behavior of Hybrid (ZrB2+Al3Zr)/AA5052 In Situ Composite

    Science.gov (United States)

    Gautam, G.; Kumar, N.; Mohan, A.; Gautam, R. K.; Mohan, S.

    2016-09-01

    During service life, components such as piston, cylinder blocks, brakes, and discs/drums, have to work under high-temperature conditions. In order to have appropriate material for such applications high-temperature studies are important. Hybrid (ZrB2+Al3Zr)/AA5052 in situ composite has been investigated from ambient to 523 K (250 °C) at an interval of 50 deg. (ZrB2+Al3Zr)/AA5052 in situ composite has been fabricated by the direct melt reaction of AA5052 alloy with zirconium and boron salts. Microstructure studies show refinement in the grain size of base alloy on in situ formation of reinforcement particles. Al3Zr particles are observed in rectangular and polyhedron shapes. It is observed from the tensile studies that ultimate tensile strength, yield strength, and percentage elongation decrease with increase in test temperature. Similar kind of behavior is also observed for flow curve properties. The tensile results have also been correlated with fractography. Wear and friction results indicate that the wear rate increases with increase in normal load, whereas coefficient of friction shows decreasing trend. With increasing test temperature, wear rate exhibits a typical phenomenon. After an initial increase, wear rate follows a decreasing trend up to 423 K (150 °C), and finally a rapid increase is observed, whereas coefficient of friction increases continuously with increase in test temperature. The mechanisms responsible for the variation of wear and friction with different temperatures have been discussed in detail with the help of worn surfaces studies under scanning electron microscope (SEM) & 3D-profilometer and debris analysis by XRD.

  2. Swelling and tensile properties of EBR-II-irradiated tantalum alloys for space reactor applications

    International Nuclear Information System (INIS)

    Grossbeck, M.L.; Wiffen, F.W.

    1985-01-01

    The tantalum alloys T-111, ASTAR-811C, Ta-10 W, and unalloyed tantalum were examined following EBR-II irradiation to a fluence of 1.7 x 10 26 neutrons/m 2 (E > 0.1 MeV) at temperatures from 650 to 950 K. Swelling was found to be negligible for all alloys; only tantalum was found to exhibit swelling, 0.36%. Tensile testing revealed that irradiated T-111 and Ta-10 W are susceptible to plastic instability, but ASTAR-811C and tantalum were not. The tensile properties of ASTAR-811C appeared adequate for current SP-100 space nuclear reactor designs. Irradiated, oxygen-doped T-111 exhibited no plastic deformation, and the abrupt failure was intergranular in nature. The absence of plastic instability in ASTAR-811C is encouraging for alloys containing carbide precipitates. These fine precipitates might prevent dislocation channeling, which leads to plastic instability in many bcc metals after irradiation. 10 refs., 13 figs., 8 tabs

  3. Effect of pre-existing shear bands on the tensile mechanical properties of a bulk metallic glass

    International Nuclear Information System (INIS)

    Cao, Q.P.; Liu, J.W.; Yang, K.J.; Xu, F.; Yao, Z.Q.; Minkow, A.; Fecht, H.J.; Ivanisenko, J.; Chen, L.Y.; Wang, X.D.; Qu, S.X.; Jiang, J.Z.

    2010-01-01

    Bulk Zr 64.13 Cu 15.75 Ni 10.12 Al 10 metallic glass has been rolled at room temperature in two different directions, and the dependences of microstructure and tensile mechanical property on the degree of deformation and rolling directions have been investigated. No deformation-induced crystallization occurs except for shear bands. Shear band formation in conjugated directions is achieved in the specimen rolled in two directions, while rolling in one direction induces shear band formation only in a single direction. Pre-existing properly spaced soft inhomogeneities can stabilize shear bands and lead to tensile plastic strain, and the efficient intersection of shear bands in conjugated directions results in work-hardening behavior, which is further confirmed by in situ tensile scanning electron microscopic observation. Based on the experimental results obtained in two different specimen geometries and finite element analysis, it is deduced that a normal-stress-modified maximum shear stress criterion rather than a shear plane criterion can describe the conditions for the formation of shear bands in uniaxial tension.

  4. Effect of long-term aging at 8150C on the tensile properties and microstructural stability of four cobalt- and nickel-base superalloys

    International Nuclear Information System (INIS)

    Hammond, J.P.

    1976-08-01

    Two heats of Haynes alloy 25 and one heat each of Haynes alloy 188, Hastelloy N, and Inconel 625 were tensile tested after aging for 11,000 h at 816 0 C. Yield strength, ultimate tensile strength, and elongation were determined 24, 316, 760, and 982 0 C and compared with typical properties for these materials in the solution annealed condition. Toughness values were determined for these materials from their engineering stress-strain curves. The long-term aging treatment degraded ductility and toughness at room temperature but, contrary to behavior expected for overaging, enhanced them over those for the solution annealed condition in tests at 760 0 C. The tensile properties of the aged superalloys were correlated with mode of fracture and the amounts, identity, and morphology of the precipitates. Aging substantially depleted the hardener tungsten from the matrix in the cobalt-base alloys

  5. The tensile properties of austenitic steel weld metals

    International Nuclear Information System (INIS)

    Wood, D.S.

    1985-01-01

    Elevated temperature tensile data on Mo containing and Mo free austenitic weld metals have been collected from French, German and UK sources and the results analysed. In the as welded condition the proof strength is significantly higher than that of wrought material and Mo containing weld metal is stronger than Mo free weld metal. The differences in UTS values are not so marked, and on average at temperatures above 400 0 the weld metal UTS is slightly lower than that of wrought material. The ductility of weld metal is significantly lower than that for wrought material. 7 refs, 2 tables, 20 figs

  6. Statistical data for the tensile properties of natural fibre composites

    Directory of Open Access Journals (Sweden)

    J.P. Torres

    2017-06-01

    Full Text Available This article features a large statistical database on the tensile properties of natural fibre reinforced composite laminates. The data presented here corresponds to a comprehensive experimental testing program of several composite systems including: different material constituents (epoxy and vinyl ester resins; flax, jute and carbon fibres, different fibre configurations (short-fibre mats, unidirectional, and plain, twill and satin woven fabrics and different fibre orientations (0°, 90°, and [0,90] angle plies. For each material, ~50 specimens were tested under uniaxial tensile loading. Here, we provide the complete set of stress–strain curves together with the statistical distributions of their calculated elastic modulus, strength and failure strain. The data is also provided as support material for the research article: “The mechanical properties of natural fibre composite laminates: A statistical study” [1].

  7. Tensile Properties and Microstructure of Inconel 718 Fabricated with Electron Beam Freeform Fabrication (EBF(sup 3))

    Science.gov (United States)

    Bird, R. Keith; Hibberd, Joshua

    2009-01-01

    Electron beam freeform fabrication (EBF3) direct metal deposition processing was used to fabricate two Inconel 718 single-bead-width wall builds and one multiple-bead-width block build. Specimens were machined to evaluate microstructure and room temperature tensile properties. The tensile strength and yield strength of the as-deposited material from the wall and block builds were greater than those for conventional Inconel 718 castings but were less than those for conventional cold-rolled sheet. Ductility levels for the EBF3 material were similar to those for conventionally-processed sheet and castings. An unexpected result was that the modulus of the EBF3-deposited Inconel 718 was significantly lower than that of the conventional material. This low modulus may be associated with a preferred crystallographic orientation resultant from the deposition and rapid solidification process. A heat treatment with a high solution treatment temperature resulted in a recrystallized microstructure and an increased modulus. However, the modulus was not increased to the level that is expected for Inconel 718.

  8. Sliding contact loading enhances the tensile properties of mesenchymal stem cell-seeded hydrogels

    Directory of Open Access Journals (Sweden)

    AH Huang

    2012-07-01

    Full Text Available The primary goal of cartilage tissue engineering is to recapitulate the functional properties and structural features of native articular cartilage. While there has been some success in generating near-native compressive properties, the tensile properties of cell-seeded constructs remain poor, and key features of cartilage, including inhomogeneity and anisotropy, are generally absent in these engineered constructs. Therefore, in an attempt to instill these hallmark properties of cartilage in engineered cell-seeded constructs, we designed and characterized a novel sliding contact bioreactor to recapitulate the mechanical stimuli arising from physiologic joint loading (two contacting cartilage layers. Finite element modeling of this bioreactor system showed that tensile strains were direction-dependent, while both tensile strains and fluid motion were depth-dependent and highest in the region closest to the contact surface. Short-term sliding contact of mesenchymal stem cell (MSC-seeded agarose improved chondrogenic gene expression in a manner dependent on both the axial strain applied and transforming growth factor-β supplementation. Using the optimized loading parameters derived from these short-term studies, long-term sliding contact was applied to MSC-seeded agarose constructs for 21 d. After 21 d, sliding contact significantly improved the tensile properties of MSC-seeded constructs and elicited alterations in type II collagen and proteoglycan accumulation as a function of depth; staining for these matrix molecules showed intense localization in the surface regions. These findings point to the potential of sliding contact to produce engineered cartilage constructs that begin to recapitulate the complex mechanical features of the native tissue.

  9. Electronic, mechanical and dielectric properties of silicane under tensile strain

    International Nuclear Information System (INIS)

    Jamdagni, Pooja; Sharma, Munish; Ahluwalia, P. K.; Kumar, Ashok; Thakur, Anil

    2015-01-01

    The electronic, mechanical and dielectric properties of fully hydrogenated silicene i.e. silicane in stable configuration are studied by means of density functional theory based calculations. The band gap of silicane monolayer can be flexibly reduced to zero when subjected to bi-axial tensile strain, leading to semi-conducting to metallic transition, whereas the static dielectric constant for in-plane polarization increases monotonically with increasing strain. Also the EEL function show the red shift in resonance peak with tensile strain. Our results offer useful insight for the application of silicane monolayer in nano-optical and electronics devices

  10. Tensile properties of polymethyl methacrylate coated natural fabric Sterculia urens

    CSIR Research Space (South Africa)

    Jayaramudu, J

    2009-04-01

    Full Text Available stress, Young's modulus and % elongation at break were determined using a Universal Testing Machine. The effect of alkali treatment and the polymethyl methacrylate coating on tensile properties of the fabric was studied. The morphology of the fabric...

  11. Mechanical Properties of Discontinuous Precipitated Al-Zn Alloys after Drawing at Room and Cryogenic Temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Min Soo; Lee, Jehyun [Changwon National University, Changwon (Korea, Republic of); Han, Seung Zeon; Ahn, Jee Hyuk [Korea Institute of Materials Science, Changwon (Korea, Republic of); Lim, Sung Hwan [Kangwon National University, Chuncheon (Korea, Republic of); Kim, Kwang Ho [Pusan National University, Pusan (Korea, Republic of); Kim, Sang sik [Gyeongsang National University, Jinju (Korea, Republic of)

    2017-02-15

    In order to study the effect of microstructural change on the tensile properties of discontinuous precipitated Al-Zn binary alloy, four different Al-Zn alloys(25, 30, 35, 45 wt%Zn) were aged at 160 ℃ for different aging times(0, 5, 15, 30, 60, 120, 360 min) after being solution treated at 400 ℃, and successively drawn at room and cryogenic temperatures(-197 ℃). Discontinuous precipitation was formed during aging in the Al matrix(which contained more than 30 wt%Zn) in Al alloys containing more than 30 wt%Zn. The tensile strength of continuous precipitated Al-35Zn alloy decreased with increasing drawing ratio, however, the tensile strength of discontinuous precipitated Al-35Zn alloy increased with further drawing. The strength and ductility combination, 350 MPa-36%was achieved by drawning discontinuous precipitated Al-Zn alloy at room temperature. The discontinuous precipitated Al-Zn alloy drawn at cryogenic temperature showed a higher value of tensile strength, over 500 MPa, although ductility decreased.

  12. Mechanical Properties of Discontinuous Precipitated Al-Zn Alloys after Drawing at Room and Cryogenic Temperatures

    International Nuclear Information System (INIS)

    Kim, Min Soo; Lee, Jehyun; Han, Seung Zeon; Ahn, Jee Hyuk; Lim, Sung Hwan; Kim, Kwang Ho; Kim, Sang sik

    2017-01-01

    In order to study the effect of microstructural change on the tensile properties of discontinuous precipitated Al-Zn binary alloy, four different Al-Zn alloys(25, 30, 35, 45 wt%Zn) were aged at 160 ℃ for different aging times(0, 5, 15, 30, 60, 120, 360 min) after being solution treated at 400 ℃, and successively drawn at room and cryogenic temperatures(-197 ℃). Discontinuous precipitation was formed during aging in the Al matrix(which contained more than 30 wt%Zn) in Al alloys containing more than 30 wt%Zn. The tensile strength of continuous precipitated Al-35Zn alloy decreased with increasing drawing ratio, however, the tensile strength of discontinuous precipitated Al-35Zn alloy increased with further drawing. The strength and ductility combination, 350 MPa-36%was achieved by drawning discontinuous precipitated Al-Zn alloy at room temperature. The discontinuous precipitated Al-Zn alloy drawn at cryogenic temperature showed a higher value of tensile strength, over 500 MPa, although ductility decreased.

  13. Tensile properties of human collagen fibrils and fascicles are insensitive to environmental salts

    DEFF Research Database (Denmark)

    Svensson, René B; Hassenkam, Tue; Grant, Colin A

    2010-01-01

    loading direction of tendon is along its longitudinal axis. Thus, in this study, we focus on the tensile mechanical properties of two hierarchical levels from human patellar tendon, namely: individual collagen fibrils and fascicles. Investigations on collagen fibrils and fascicles were made at pH 7...... was observed at the highest phosphate-buffered saline concentration for both the fibrils and fascicles, indicating a stabilizing effect of ionic screening, but changes were much less than reported for radial compression. Due to the small magnitude of the effects, the tensile mechanical properties of collagen...

  14. Tensile Mechanical Properties and Failure Modes of a Basalt Fiber/Epoxy Resin Composite Material

    OpenAIRE

    He, Jingjing; Shi, Junping; Cao, Xiaoshan; Hu, Yifeng

    2018-01-01

    Uniaxial tensile tests of basalt fiber/epoxy (BF/EP) composite material with four different fiber orientations were conducted under four different fiber volume fractions, and the variations of BF/EP composite material failure modes and tensile mechanical properties were analyzed. The results show that when the fiber volume fraction is constant, the tensile strength, elastic modulus, and limiting strain of BF/EP composite material all decrease with increasing fiber orientation angle. When the ...

  15. Assessment of the Tensile Properties for Single Fibers

    Science.gov (United States)

    2018-02-01

    release; distribution is unlimited. 24 7. Conclusions A method for accurately characterizing the tensile material properties of single fibers...subject to any penalty for failing to comply with a collection of information if it does not display a currently valid OMB control number. PLEASE DO NOT...10. SPONSOR/MONITOR’S ACRONYM(S) 11. SPONSOR/MONITOR’S REPORT NUMBER(S) 12. DISTRIBUTION/ AVAILABILITY STATEMENT 13. SUPPLEMENTARY NOTES

  16. Influence of gamma-radiation on tensile strength properties of polytetrafluoroethylene (PTFE)

    CERN Document Server

    Gafurov, U G; Nemkova, N

    2002-01-01

    The tensile strength properties of polytetrafluoroethylene are studied at modification doses of gamma-irradiation. The main molecular process of polymer destruction is found to be the thermostimulated slippage of molecular chains. (author)

  17. Development of India-specific RAFM steel through optimization of tungsten and tantalum contents for better combination of impact, tensile, low cycle fatigue and creep properties

    Energy Technology Data Exchange (ETDEWEB)

    Laha, K., E-mail: laha@igcar.gov.in [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102, TN (India); Saroja, S.; Moitra, A.; Sandhya, R.; Mathew, M.D.; Jayakumar, T. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102, TN (India); Rajendra Kumar, E. [Institute for Plasma Research, Bhat, Gandhinagar 382 428, Gujarat (India)

    2013-08-15

    Effects of tungsten and tantalum contents on impact, tensile, low cycle fatigue and creep properties of Reduced Activation Ferritic–Martensitic (RAFM) steel were studied to develop India-specific RAFM steel. Four heats of the steel have been melted with tungsten and tantalum contents in the ranges 1–2 wt.% and 0.06–0.14 wt.% respectively. Increase in tungsten content increased the ductile-to-brittle transition temperature (DBTT), low cycle fatigue and creep strength of the steel, whereas the tensile strength was not changed significantly. Increase in tantalum content increased the DBTT and low cycle fatigue strength of the steel whereas the tensile and creep strength decreased. Detailed TEM investigations revealed enhanced microstructural stability of the steel against creep exposure on tungsten addition. The RAFM steel having 1.4 wt.% tungsten with 0.06 wt.% tantalum was found to possess optimum combination of impact, tensile, low cycle fatigue and creep properties and is considered for Indian-specific RAFM steel.

  18. Effect of solution treatment temperature and cooling rate on the mechanical properties of tungsten heavy alloy

    Energy Technology Data Exchange (ETDEWEB)

    Kumari, Anjali, E-mail: anjalikumari1261@gmail.com; Prabhu, G.; Sankaranarayana, M.; Nandy, T.K.

    2017-03-14

    The present study investigates the effect of solution treatment temperature and cooling rate on mechanical properties of a tungsten heavy alloy (89.6W-6.2Ni-1.8Fe-2.4Co). In addition to water quenching, rapid argon quenching has been attempted in this study since it is a relatively cleaner process and it can be used in conjunction with vacuum treatment. Since in these alloys, there is a possibility of incomplete dissolution of intermetallics or segregation of impurities during heat treatment, which results in scatter in the mechanical properties, it was decided that the solution treatment temperature for both water and argon quenching would be varied from 1100 to 1250 °C in order to see its effect on the microstructure and mechanical properties. Solution treatment at varying temperatures followed by water quenching resulted in tensile strength ranging from 908 to 921 MPa and % elongation varied from 19% to 26%. On the other hand, the argon quenching heat treatment resulted in tensile strength in the range of 871–955 MPa and % elongation from 9% to 25%. No significant trend with respect to solution treatment temperature on tensile properties was seen in both argon and water quenched samples. % elongation to failure and impact values of water quenched specimens were better than those of argon quenched specimens for a given solution treatment temperature. The impact values appeared to improve with increasing solution treatment temperature in water quenched condition. The properties were correlated with underlying microstructure and fractographs of the failed specimens. The study showed the argon quenching may not be appropriate for the heat treatment of heavy alloys since it results in inferior mechanical properties as compared to water quenching.

  19. Tensile Creep and Fatigue of Sylramic-iBN Melt-Infiltrated SiC Matrix Composites: Retained Properties, Damage Development, and Failure Mechanisms

    Science.gov (United States)

    Morscher, Greg; Gowayed, yasser; Miller, Robert; Ojard, Greg; Ahmad, Jalees; Santhosh, Unni; John, Reji

    2008-01-01

    An understanding of the elevated temperature tensile creep, fatigue, rupture, and retained properties of ceramic matrix composites (CMC) envisioned for use in gas turbine engine applications are essential for component design and life-prediction. In order to quantify the effect of stress, time, temperature, and oxidation for a state-of-the-art composite system, a wide variety of tensile creep, dwell fatigue, and cyclic fatigue experiments were performed in air at 1204 C for the SiC/SiC CMC system consisting of Sylramic-iBN SiC fibers, BN fiber interphase coating, and slurry-cast melt-infiltrated (MI) SiC-based matrix. Tests were either taken to failure or interrupted. Interrupted tests were then mechanically tested at room temperature to determine the residual properties. The retained properties of most of the composites subjected to tensile creep or fatigue were usually within 20% of the as-produced strength and 10% of the as-produced elastic modulus. It was observed that during creep, residual stresses in the composite are altered to some extent which results in an increased compressive stress in the matrix upon cooling and a subsequent increased stress required to form matrix cracks. Microscopy of polished sections and the fracture surfaces of specimens which failed during stressed-oxidation or after the room-temperature retained property test was performed on some of the specimens in order to quantify the nature and extent of damage accumulation that occurred during the test. It was discovered that the distribution of stress-dependent matrix cracking at 1204 C was similar to the as-produced composites at room temperature; however, matrix crack growth occurred over time and typically did not appear to propagate through thickness except at final failure crack. Failure of the composites was due to either oxidation-induced unbridged crack growth, which dominated the higher stress regime (> 179 MPa) or controlled by degradation of the fibers, probably caused by

  20. Tensile and fracture toughness test results of neutron irradiated beryllium

    Energy Technology Data Exchange (ETDEWEB)

    Chaouadi, R.; Moons, F.; Puzzolante, J.L. [Centre d`Etude de l`Energie Nucleaire, Mol (Belgium)

    1998-01-01

    Tensile and fracture toughness test results of four Beryllium grades are reported here. The flow and fracture properties are investigated by using small size tensile and round compact tension specimens. Irradiation was performed at the BR2 material testing reactor which allows various temperature and irradiation conditions. The fast neutron fluence (>1 MeV) ranges between 0.65 and 2.45 10{sup 21} n/cm{sup 2}. In the meantime, un-irradiated specimens were aged at the irradiation temperatures to separate if any the effect of temperature from irradiation damage. Test results are analyzed and discussed, in particular in terms of the effects of material grade, test temperature, thermal ageing and neutron irradiation. (author)

  1. Effect of implanted helium on tensile properties and hardness of 9% Cr martensitic stainless steels

    Science.gov (United States)

    Jung, P.; Henry, J.; Chen, J.; Brachet, J.-C.

    2003-05-01

    Hundred micrometer thick specimens of 9% Cr martensitic steels EM10 and T91 were homogeneously implanted with He 4 to concentrations up to 0.5 at.% at temperatures from 150 to 550 °C. The specimens were tensile tested at room temperature and at the respective implantation temperatures. Subsequently the fracture surfaces were analysed by scanning electron microscopy and some of the specimens were examined in an instrumented hardness tester. The implanted helium caused hardening and embrittlement which both increased with increasing helium content and with decreasing implantation temperature. Fracture surfaces showed intergranular brittle appearance with virtually no necking at the highest implantation doses, when implanted below 250 °C. The present tensile results can be scaled to tensile data after irradiation in spallation sources on the basis of helium content but not on displacement damage. An interpretation of this finding by microstructural examination is given in a companion paper [J. Nucl. Mater., these Proceedings].

  2. Ab initio elastic properties and tensile strength of crystalline hydroxyapatite.

    Science.gov (United States)

    Ching, W Y; Rulis, Paul; Misra, A

    2009-10-01

    We report elastic constant calculation and a "theoretical" tensile experiment on stoichiometric hydroxyapatite (HAP) crystal using an ab initio technique. These results compare favorably with a variety of measured data. Theoretical tensile experiments are performed on the orthorhombic cell of HAP for both uniaxial and biaxial loading. The results show considerable anisotropy in the stress-strain behavior. It is shown that the failure behavior of the perfect HAP crystal is brittle for tension along the z-axis with a maximum stress of 9.6 GPa at 10% strain. Biaxial failure envelopes from six "theoretical" loading tests show a highly anisotropic pattern. Structural analysis of the crystal under various stages of tensile strain reveals that the deformation behavior manifests itself mainly in the rotation of the PO(4) tetrahedron with concomitant movements of both the columnar and axial Ca ions. These results are discussed in the context of mechanical properties of bioceramic composites relevant to mineralized tissues.

  3. A cryogenic tensile testing apparatus for micro-samples cooled by miniature pulse tube cryocooler

    International Nuclear Information System (INIS)

    Chen, L B; Liu, S X; Gu, K X; Zhou, Y; Wang, J J

    2015-01-01

    This paper introduces a cryogenic tensile testing apparatus for micro-samples cooled by a miniature pulse tube cryocooler. At present, tensile tests are widely applied to measure the mechanical properties of materials; most of the cryogenic tensile testing apparatus are designed for samples with standard sizes, while for non-standard size samples, especially for microsamples, the tensile testing cannot be conducted. The general approach to cool down the specimens for tensile testing is by using of liquid nitrogen or liquid helium, which is not convenient: it is difficult to keep the temperature of the specimens at an arbitrary set point precisely, besides, in some occasions, liquid nitrogen, especially liquid helium, is not easily available. To overcome these limitations, a cryogenic tensile testing apparatus cooled by a high frequency pulse tube cryocooler has been designed, built and tested. The operating temperatures of the developed tensile testing apparatus cover from 20 K to room temperature with a controlling precision of ±10 mK. The apparatus configurations, the methods of operation and some cooling performance will be described in this paper. (paper)

  4. Dependence of electronic properties of germanium on the in-plane biaxial tensile strains

    Energy Technology Data Exchange (ETDEWEB)

    Yang, C.H. [State Key Laboratory of Information Photonics and Optical Communications, Beijing University of Posts and Telecommunications (BUPT), Beijing 100876 (China); Yu, Z.Y., E-mail: yuzhongyuan30@gmail.com [State Key Laboratory of Information Photonics and Optical Communications, Beijing University of Posts and Telecommunications (BUPT), Beijing 100876 (China); Liu, Y.M.; Lu, P.F. [State Key Laboratory of Information Photonics and Optical Communications, Beijing University of Posts and Telecommunications (BUPT), Beijing 100876 (China); Gao, T. [Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065 (China); Li, M.; Manzoor, S. [State Key Laboratory of Information Photonics and Optical Communications, Beijing University of Posts and Telecommunications (BUPT), Beijing 100876 (China)

    2013-10-15

    The hybrid HSE06 functional with the spin–orbit coupling effects is used to calculate the habituation of the electronic properties of Ge on the (0 0 1), (1 1 1), (1 0 1) in-plane biaxial tensile strains (IPBTSs). Our motivation is to explore the nature of electronic properties of tensile-strained Ge on different substrate orientations. The calculated results demonstrate that one of the most effective and practical approaches for transforming Ge into a direct transition semiconductor is to introduce (0 0 1) IPBTS to Ge. At 2.3% (0 0 1) IPBTS, Ge becomes a direct bandgap semiconductor with 0.53 eV band gap, in good agreement with the previous theoretical and experimental results. We find that the (1 1 1) and (1 0 1) IPBTSs are not efficient since the shear strain and inner displacement of atoms introduced by them quickly decrease the indirect gap of Ge. By investigating the dependence of valence band spin–orbit splitting on strain, we prove that the dependency relationship and the coupled ways between the valence-band states of tensile-strained Ge are closely related to the symmetry of strain tensor, i.e., the symmetry of the substrate orientation. The first- and second-order coefficients describing the dependence of indirect gap, direct gap, the valence band spin–orbit coupling splitting, and heavy-hole–light-hole splitting of Ge on IPBTSs have been obtained by the least squares polynomial fitting. These coefficients are significant to quantitatively modulate the electronic properties of Ge by tensile strain and design tensile-strained Ge devices by semiconductor epitaxial technique.

  5. Mechanical properties of aluminium–copper–lithium alloy AA2195 at cryogenic temperatures

    International Nuclear Information System (INIS)

    Nayan, Niraj; Narayana Murty, S.V.S.; Jha, Abhay K.; Pant, Bhanu; Sharma, S.C.; George, Koshy M.; Sastry, G.V.S.

    2014-01-01

    Highlights: • 4 mm thick sheet of AA2195 was imparted T87 temper. • 7% cold work to impart T87 was given by combination of cold rolling and stretching. • Mechanical properties were evaluated at RT and cryogenic temperatures. • Strength of AA2195 are superior to the conventional aluminum alloy 2219 at all temperatures. • Strength decreases with decrease in temperature whereas ductility remains unchanged. - Abstract: Tensile testing was performed on a 4 mm thick sheet of the aluminum–lithium alloy AA2195 in T87 (solution treatment + water quenching + 7% cold work + peak aging) temper which was subjected to 7% cold working by combination of cold rolling and stretching, over a temperature range from ambient to liquid hydrogen (20 K) conditions. Properties were evaluated in longitudinal as well as transverse directions to characterize anisotropy with respect to strength and ductility. Strength and ductility were compared to the conventional aluminum alloy AA2219-T87, developed for similar cryogenic applications. Decreases in test temperature led to higher strengths with little or no change in ductility. As the temperature decreases, the differences between ultimate tensile strength as well as yield strength for two different combinations of cold roll and stretch studied in the present work, narrows down and become equal at 20 K

  6. Sample selection, preparation methods, and the apparent tensile properties of silkworm (B. mori) cocoon silk.

    Science.gov (United States)

    Reed, Emily J; Bianchini, Lindsay L; Viney, Christopher

    2012-06-01

    Reported literature values of the tensile properties of natural silk cover a wide range. While much of this inconsistency is the result of variability that is intrinsic to silk, some is also a consequence of differences in the way that silk is prepared for tensile tests. Here we explore how measured mechanical properties of Bombyx mori cocoon silk are affected by two intrinsic factors (the location from which the silk is collected within the cocoon, and the color of the silk), and two extrinsic factors (the storage conditions prior to testing, and different styles of reeling the fiber). We find that extrinsic and therefore controllable factors can affect the properties more than the intrinsic ones studied. Our results suggest that enhanced inter-laboratory collaborations, that lead to standardized sample collection, handling, and storage protocols prior to mechanical testing, would help to decrease unnecessary (and complicating) variation in reported tensile properties. Copyright © 2011 Wiley Periodicals, Inc.

  7. Tensile Property of ANSI 304 Stainless Steel Weldments Subjected to Cavitation Erosion Based on Treatment of Laser Shock Processing.

    Science.gov (United States)

    Zhang, Lei; Liu, Yue-Hua; Luo, Kai-Yu; Zhang, Yong-Kang; Zhao, Yong; Huang, Jian-Yun; Wu, Xu-Dong; Zhou, Chuang

    2018-05-16

    Tensile property was one important index of mechanical properties of ANSI 304 stainless steel laser weldments subjected to cavitation erosion (CE). Laser shock processing (LSP) was utilized to strengthen the CE resistance, and the tensile property and fracture morphology were analyzed through three replicated experiment times. Results showed tensile process of treated weldments was composed of elastic deformation, plastic deformation, and fracture. The elastic limit, elastic modulus, elongation, area reduction, and ultimate tensile strength of tensile sample after CE were higher in view of LSP. In the fracture surface, the fiber zone, radiation zone and shear lip zone were generated, and those were more obvious through LSP. The number and size of pores in the fracture surface were smaller, and the fracture surface was smoother and more uniform. The dimples were elongated along the unified direction due to effects of LSP, and the elongated direction was in agreement with the crack propagation direction. Their distribution and shape were uniform with deeper depth. It could be reflected that the tensile property was improved by LSP and the CE resistance was also enhanced.

  8. Stiff and tough: a comparative study on the tensile properties of shark skin.

    Science.gov (United States)

    Creager, Shelby B; Porter, Marianne E

    2018-02-01

    In sharks, the skin is a biological composite with mineralized denticles embedded within a collagenous matrix. Swimming performance is enhanced by the dermal denticles on the skin, which have drag reducing properties produced by regional morphological variations and changes in density along the body. We used mechanical testing to quantify the effect of embedded mineralized denticles on the quasi-static tensile properties of shark skin to failure in four coastal species. We investigated regional differences in denticle density and skin properties by dissecting skin from the underlying fascia and muscle at 10 anatomical landmarks. Hourglass-shaped skin samples were extracted in the cranial to caudal orientation. Denticle density was quantified and varied significantly among both regions and species. We observed the greatest denticle densities in the cranial region of the body for the bonnethead, scalloped hammerhead, and bull sharks. Skin samples were then tested in tension until failure, stress strain curves were generated, and mechanical properties calculated. We found significant species and region effects for all three tensile mechanical properties. We report the greatest ultimate tensile strength, stiffness, and toughness near the cranial and lateral regions of the body for all 4 of the coastal species. We also report that denticle density increases with skin stiffness but decreases with toughness. Copyright © 2017 Elsevier GmbH. All rights reserved.

  9. Optimization of tensile method and specimen geometry in modified ring tensile test

    International Nuclear Information System (INIS)

    Kitano, Koji; Fuketa, Toyoshi; Sasajima, Hideo; Uetsuka, Hiroshi

    2001-03-01

    Several techniques in ring tensile test are proposed in order to evaluate mechanical properties of cladding under hoop loading condition caused by pellet/cladding mechanical interaction (PCMI). In the modified techniques, variety of tensile methods and specimen geometry are being proposed in order to limit deformation within the gauge section. However, the tensile method and the specimen geometry were not determined in the modified techniques. In the present study, we have investigated the tensile method and the specimen geometry through finite element method (FEM) analysis of specimen deformation and tensile test on specimens with various gauge section geometries. In using two-piece tensile tooling, the mechanical properties under hoop loading condition can be correctly evaluated when deformation part (gauge section) is put on the top of a half-mandrel, and friction between the specimen and the half-mandrel is reduced with Teflon tape. In addition, we have shown the optimum specimen geometry for PWR 17 by 17 type cladding. (author)

  10. Effects of Alloying Elements on Room and High Temperature Tensile Properties of Al-Si Cu-Mg Base Alloys =

    Science.gov (United States)

    Alyaldin, Loay

    In recent years, aluminum and aluminum alloys have been widely used in automotive and aerospace industries. Among the most commonly used cast aluminum alloys are those belonging to the Al-Si system. Due to their mechanical properties, light weight, excellent castability and corrosion resistance, these alloys are primarily used in engineering and in automotive applications. The more aluminum is used in the production of a vehicle, the less the weight of the vehicle, and the less fuel it consumes, thereby reducing the amount of harmful emissions into the atmosphere. The principal alloying elements in Al-Si alloys, in addition to silicon, are magnesium and copper which, through the formation of Al2Cu and Mg2Si precipitates, improve the alloy strength via precipitation hardening following heat treatment. However, most Al-Si alloys are not suitable for high temperature applications because their tensile and fatigue strengths are not as high as desired in the temperature range 230-350°C, which are the temperatures that are often attained in automotive engine components under actual service conditions. The main challenge lies in the fact that the strength of heat-treatable cast aluminum alloys decreases at temperatures above 200°C. The strength of alloys under high temperature conditions is improved by obtaining a microstructure containing thermally stable and coarsening-resistant intermetallics, which may be achieved with the addition of Ni. Zr and Sc. Nickel leads to the formation of nickel aluminide Al3Ni and Al 9FeNi in the presence of iron, while zirconium forms Al3Zr. These intermetallics improve the high temperature strength of Al-Si alloys. Some interesting improvements have been achieved by modifying the composition of the base alloy with additions of Mn, resulting in an increase in strength and ductility at both room and high temperatures. Al-Si-Cu-Mg alloys such as the 354 (Al-9wt%Si-1.8wt%Cu-0.5wt%Mg) alloys show a greater response to heat treatment as a

  11. The relationship between hardness to the tensile properties of kenaf/ unsaturated polyester composite

    Science.gov (United States)

    Ghaztar, Muhammad Mustakim Mohd; Romli, Ahmad Zafir; Ibrahim, Nik Noor Idayu Nik

    2017-12-01

    The level of fibre-matrix interaction and consolidation are essential aspects to determine the composite deformation but, less attention is given to the effect of small fibre weight increment (5 wt%), chemical treatment coalition (NaOH/ silane), fibre's length and aspect ratio to the physical and mechanical properties of the composite. Hence, this paper studies the correlation between these parameters towards hardness and tensile properties of Kenaf fibre and unsaturated polyester (UP) matrix. The study was carried out by fabricating the sample into two (2) types of fibre categories and fibre loadings and tested to determine its properties. The results showed that the hardness and tensile stress were significantly influenced by the fibre loading and dispersion of the fabricated samples. At low filler loading, the treated samples for both fibre sizes showed lower hardness property compared to the untreated samples. The chemical treatment coalition might diffuse out the pectin and hemicellulose which affect the ability of the fibre to absorb the force applied by the hardness indenter. Good fibre dispersion observed for the treated samples also resulted in the fibre-dominating composite system where the fibres were efficiently absorbed and distributed the indentation force. However, chemical treatments and good fibre dispersion contributed to the higher tensile stress of the treated fibre samples especially for smaller fibre length and aspect ratio compared to the untreated samples. At high fibre loading, treated fibre samples showed higher hardness property compared to the untreated samples since the treatment resulted in better fibre wetting by the matrix and the formation of pack structure. However, high fibre loading caused the mutual abrasion among the fibre which led to the lower tensile stress compared to the low fibre loading samples. In conclusion, by understanding the factors that influenced the reinforcing mechanism of the composite, the inconsistency of

  12. Microstructures and Mechanical Properties of Inconel 718 Alloy at Ultralow Temperatures

    Science.gov (United States)

    Yao, C. G.; Lv, H. J.; Yi, D. Q.; Meng, S.; Xiao, L. R.; Wang, B.

    2018-05-01

    The microstructures and mechanical properties of powder metallurgy Inconel 718 alloy were investigated in the temperatures range between 25 and - 253 °C. Tensile strength increased with the decrease in temperature, while the ductility first increased and then decreased. There was no significant change in impact toughness. When the temperature was - 253 °C, a zigzag stress-strain curve was observed for the alloy, owing to the interaction of dislocation glide and twinning, which effectively maintained the relatively good ductility.

  13. The effect of alkaline treatment on tensile properties of sugar palm fibre reinforced epoxy composites

    International Nuclear Information System (INIS)

    Bachtiar, D.; Sapuan, S.M.; Hamdan, M.M.

    2008-01-01

    A study on the effect of alkaline treatment on tensile properties of sugar palm fibre reinforced epoxy composites is presented in this paper. The treatment was carried out using sodium hydroxide (NaOH) solutions at two different concentrations and three different soaking times. The hydrophilic nature of sugar palm fibre makes it difficult to adhere to hydrophobic epoxy and therefore posed the problem of interfacial bonding between fibre and matrix and such treatment was needed to alleviate such problem. The composite specimens were tested for tensile property determination. Some fractured specimens were examined under scanning electron microscope (SEM) to study the microstructure of the materials. Inconsistent results were obtained for tensile strengths, which indicate that the treatment is not very effective yet to improve the interfacial bonding. However, for tensile modulus, the results are much higher than untreated fibre composite specimens, which proved the effectiveness of the treatment

  14. Effect of Deformation Temperature on Microstructure Evolution and Mechanical Properties of Low-Carbon High-Mn Steel

    Directory of Open Access Journals (Sweden)

    Adam Grajcar

    2018-01-01

    Full Text Available This work addresses the influence of deformation temperature in a range from −40°C to 200°C on the microstructure evolution and mechanical properties of a low-carbon high-manganese austenitic steel. The temperature range was chosen to cope at the time during sheet processing or car crash events. Experimental results show that yield stress and ultimate tensile strength gradually deteriorate with an increase in the tensile testing temperature. The dominant mechanism responsible for the strain hardening of steel changes as a function of deformation temperature, which is related to stacking fault energy (SFE changes. When the deformation temperature rises, twinning decreases while a role of dislocation slip increases.

  15. Effects of temperature and strain rate on the tensile behaviors of SIMP steel in static lead bismuth eutectic

    Energy Technology Data Exchange (ETDEWEB)

    Liu, Jian, E-mail: jliu12b@imr.ac.cn [Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016 (China); University of Chinese Academy of Sciences, Beijing, 100049 (China); Yan, Wei [Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016 (China); Sha, Wei [School of Planning, Architecture and Civil Engineering, Queen' s University Belfast, Belfast, BT9 5AG (United Kingdom); Wang, Wei; Shan, Yiyin [Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016 (China); Yang, Ke, E-mail: kyang@imr.ac.cn [Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016 (China)

    2016-05-15

    In order to assess the susceptibility of candidate structural materials to liquid metal embrittlement, this work investigated the tensile behaviors of ferritic-martensitic steel in static lead bismuth eutectic (LBE). The tensile tests were carried out in static lead bismuth eutectic under different temperatures and strain rates. Pronounced liquid metal embrittlement phenomenon is observed between 200 °C and 450 °C. Total elongation is reduced greatly due to the liquid metal embrittlement in LBE environment. The range of ductility trough is larger under slow strain rate tensile (SSRT) test. - Highlights: • The tensile behaviors of SIMP steel in LBE are investigated for the first time. • The SIMP is susceptible to LME at different strain rates and temperatures. • The total elongation is reduced greatly. • The ductility trough is wider under SSRT. • The tensile specimens rupture in brittle manner without obvious necking.

  16. Effects of temperature and strain rate on the tensile behaviors of SIMP steel in static lead bismuth eutectic

    International Nuclear Information System (INIS)

    Liu, Jian; Yan, Wei; Sha, Wei; Wang, Wei; Shan, Yiyin; Yang, Ke

    2016-01-01

    In order to assess the susceptibility of candidate structural materials to liquid metal embrittlement, this work investigated the tensile behaviors of ferritic-martensitic steel in static lead bismuth eutectic (LBE). The tensile tests were carried out in static lead bismuth eutectic under different temperatures and strain rates. Pronounced liquid metal embrittlement phenomenon is observed between 200 °C and 450 °C. Total elongation is reduced greatly due to the liquid metal embrittlement in LBE environment. The range of ductility trough is larger under slow strain rate tensile (SSRT) test. - Highlights: • The tensile behaviors of SIMP steel in LBE are investigated for the first time. • The SIMP is susceptible to LME at different strain rates and temperatures. • The total elongation is reduced greatly. • The ductility trough is wider under SSRT. • The tensile specimens rupture in brittle manner without obvious necking.

  17. Tensile properties of ADI material in water and gaseous environments

    Energy Technology Data Exchange (ETDEWEB)

    Rajnovic, Dragan, E-mail: draganr@uns.ac.rs [Faculty of Technical Sciences, University of Novi Sad, Trg D. Obradovića 6, 21000 Novi Sad (Serbia); Balos, Sebastian; Sidjanin, Leposava [Faculty of Technical Sciences, University of Novi Sad, Trg D. Obradovića 6, 21000 Novi Sad (Serbia); Eric Cekic, Olivera [Innovation Centre, Faculty of Mechanical Engineering, University of Belgrade, Kraljice Marije 16, 11120 Belgrade (Serbia); Grbovic Novakovic, Jasmina [Vinca Institute of Nuclear Sciences, University of Belgrade, P.O. Box 522, 11000 Belgrade (Serbia)

    2015-03-15

    Austempered ductile iron (ADI) is an advanced type of heat treated ductile iron, having comparable mechanical properties as forged steels. However, it was found that in contact with water the mechanical properties of austempered ductile irons decrease, especially their ductility. Despite considerable scientific attention, the cause of this phenomenon remains unclear. Some authors suggested that hydrogen or small atom chemisorption causes the weakening of the surface atomic bonds. To get additional reliable data of that phenomenon, in this paper, two different types of austempered ductile irons were tensile tested in various environments, such as: argon, helium, hydrogen gas and water. It was found that only the hydrogen gas and water gave a statistically significant decrease in mechanical properties, i.e. cause embrittlement. Furthermore, the fracture surface analysis revealed that the morphology of the embrittled zone near the specimen surface shares similarities to the fatigue micro-containing striation-like lines, which indicates that the morphology of the brittle zone may be caused by cyclic local-chemisorption, micro-embrittlement and local-fracture. - Highlights: • In contact with water and other liquids the ADI suddenly exhibits embrittlement. • The embrittlement is more pronounced in water than in the gaseous hydrogen. • The hydrogen chemisorption into ADI surface causes the formation of a brittle zone. • The ADI austempered at lower temperatures (300 °C) is more resistant to embrittlement.

  18. Tensile properties of V-5Cr-5Ti alloy after exposure in air environment

    Energy Technology Data Exchange (ETDEWEB)

    Natesan, K.; Soppet, W.K. [Argonne National Lab., IL (United States)

    1997-04-01

    Oxidation studies were conducted on V-5Cr-5Ti alloy specimens in an air environment to evaluate the oxygen uptake behavior of the alloy as a function of temperature and exposure time. The oxidation rates, calculated from parabolic kinetic measurements of thermogravimetric testing and confirmed by microscopic analysis of cross sections of exposed specimens, were 5, 17, and 27 {mu}m per year after exposure at 300, 400, and 500{degrees}C, respectively. Uniaxial tensile tests were conducted at room temperature and at 500{degrees}C on preoxidized specimens of the alloy to examine the effects of oxidation and oxygen migration on tensile strength and ductility. Correlations were developed between tensile strength and ductility of the oxidized alloy and microstructural characteristics such as oxide thickness, depth of hardened layer, depth of intergranular fracture zone, and transverse crack length.

  19. Preparation and tensile properties of linear low density polyethylene/rambutan peels (Nephelium chryseum Blum.) flour blends

    Science.gov (United States)

    Nadhirah, A. Ainatun.; Sam, S. T.; Noriman, N. Z.; Voon, C. H.; Samera, S. S.

    2015-05-01

    The effect of rambutan peels flour (RPF) content on the tensile properties of linear low density polyethylene filled with rambutan peel flour was studied. RPF was melt blended with linear low-density polyethylene (LLDPE). LLDPE/RPF blends were prepared by using internal mixer (brabender) at 160 °C with the flour content ranged from 0 to 15 wt%. The tensile properties were tested by using a universal testing machine (UTM) according to ASTM D638. The highest tensile strength was observed for pure LLDPE while the tensile strength LLDPE/RPF decreased gradually with the addition of rambutan peels flour content from 0% to 15%. Young's modulus of 63 µm to 250 µm rambutan peels blends with LLDPE with the fiber loading of 0 - 15 wt% increased with increasing fiber loading.

  20. Microstructure evolution and mechanical properties of a particulate reinforced magnesium matrix composites forged at elevated temperatures

    International Nuclear Information System (INIS)

    Deng, K.K.; Wu, K.; Wang, X.J.; Wu, Y.W.; Hu, X.S.; Zheng, M.Y.; Gan, W.M.; Brokmeier, H.G.

    2010-01-01

    SiCp/AZ91 magnesium matrix composite was fabricated by stir casting. The as-cast ingots were cut into cylindrical billets, and then forged at different temperatures (320, 370, 420, 470 and 520 deg. C) at a constant RAM speed of 15 mm/s with 50% reduction. The microstructure evolution of the composites during forging was investigated by optical microscope, scanning electron microscope, and transmission electron microscope. The texture of the forged composites was measured by neutron diffraction. Mechanical properties of the composite at different forging temperatures were tested by tensile tests at room temperature. It was found that a strong basal plane texture formed during forging, and the intensity of basal plane texture weakened as forging temperatures increased. The particle distribution in the composite was significantly improved by hot forging. Typical microstructures were obtained after forging at different temperatures and the composite with different microstructures offered different mechanical properties during tensile test.

  1. MICROSTRUCTURE AND TENSILE PROPERTIES OF Fe3Al-BASED ALLOYS WITH VC AND TiC ADDITIONS

    Institute of Scientific and Technical Information of China (English)

    W.L.Xu; Y.S.Sun; S.S.Ding

    2001-01-01

    Microstructure and tensile properties of Fe3Al-based alloys with additions of TiC andVC particles have been investigated.Results show that the formation of TiC particlesresults in the refinement of the macrostructure of as-cast ingots.Although the additionof VC particles does not cause significant change of the as-cast microstructure,themicrostructure of the alloy after hot-working and recrystallization has been found tobe refined.The formation of both VC and TiC particles results in the increase of yieldstrength,especially at high temperature of 600℃.

  2. Use of miniature tensile specimen and video extensometer for measurement of mechanical properties

    International Nuclear Information System (INIS)

    Kumar, Kundan; Pooleery, Arun; Madhusoodanan, K.

    2014-08-01

    Miniaturisation of the tensile test specimen below the sub-size level poses various challenges, such as conformity of specimen to various acceptance criteria as per standard test specimen, aspect ratio, minimum number of grains required in a gauge cross-section, fabrication for uniformity in metrological values, etc. Apart from these, measurement of strain over a very limited available space on the test specimen is another practical challenge. Despite these limitations, miniature specimen testing is increasingly being used worldwide these days. The driving forces behind increasing use of miniature test techniques are new material development, assuring fitness of component after in-service-inspection, low dose of radiation exposure due to smaller dimensions of test specimens etc. However, the evaluation of mechanical properties from a miniature tensile test has a greater advantage over the other miniature novel test techniques, such as small punch test, ABI, miniature fatigue and impact tests etc., as it is a direct method of measurement of mechanical properties. This report covers various aspects of miniature tensile test methodologies, which include geometrical design of specimen having gauge length of 3-5 mm, fabrication, development of special fixtures for gripping the test specimens, and use of optical method for strain measurement. The geometrical design of the specimen and its behaviour over application of tensile load has been established using FEM analysis. A good agreement between conventional and miniature test results exemplifies the potential of the miniature tensile test technique. (author)

  3. Postirradiation tensile properties of Mo and Mo alloys irradiated with 600 MeV protons

    International Nuclear Information System (INIS)

    Mueller, G.V.; Gavillet, D.; Victoria, M.; Martin, J.L.

    1994-01-01

    Tensile specimens of pure Mo and Mo-5 Re, Mo-41 Re and TZM alloys have been irradiated with 600 MeV protons in the PIREX facility at 300 and 660 K to 0.5 dpa. Results of the postirradiation tensile testing show a strong radiation hardening and a severe loss of ductility for all the materials tested at room temperature. ((orig.))

  4. Effect of elevated temperature on the tensile strength of Napier/glass-epoxy hybrid reinforced composites

    Science.gov (United States)

    Ridzuan, M. J. M.; Majid, M. S. Abdul; Afendi, M.; Firdaus, A. Z. Ahmad; Azduwin, K.

    2017-11-01

    The effects of elevated temperature on the tensile strength of Napier/glass-epoxy hybrid reinforced composites and its morphology of fractured surfaces are discussed. Napier/glass-epoxy hybrid reinforced composites were fabricated by using vacuum infusion method by arranging Napier fibres in between sheets of woven glass fibres. Napier and glass fibres were laminated with estimated volume ratios were 24 and 6 vol. %, respectively. The epoxy resin was used as matrix estimated to 70 vol. %. Specimens were tested to failure under tension at a cross-head speed of 1 mm/min using Universal Testing Machine (Instron) with a load cell 100 kN at four different temperatures of RT, 40°C, 60°C and 80°C. The morphology of fractured surface of hybrid composites was investigated by field emission scanning electron microscopy. The result shows reduction in tensile strength at elevated temperatures. The increase in the temperature activates the process of diffusion, and generates critical stresses which cause the damage at first-ply or at the centre of the hybrid plate, as a result lower the tensile strength. The observation of FESEM images indicates that the fracture mode is of evolution of localized damage, from fibre/matrix debonding, matric cracking, delamination and fibre breakage.

  5. Construction of cryogenic testing system and tensile deformation behavior of AISI 300 series stainless steels at cryogenic temperatures

    International Nuclear Information System (INIS)

    Lee, H.M.; Nahm, S.H.; Huh, Y.H.; Lee, J.J.; Bahng, G.W.

    1990-01-01

    For practical application of cryogenic engineering, development and characterization of structural materials for use at low temperatures are essential. For these purposes, a system for mechanical testing at liquid helium temperatures was developed and it was shown that the precision and accuracy of the system met the requirements of standards for materials testing machines. Using this system, tensile deformation behavior of AISI 304,316 and 310S austenitic stainless steels at cryogenic temperatures was investigated. Tests were conducted on round, tensile specimens having a 6.25mm diameter at 4,77, and 295 K and loading rate was 0.5mm/min. Serrations were observed in all alloys at 4 K. The stress-displacement curves at 77 and 4 K showed different tendency from those at 298 K. As the testing temperature decreased, ultimate strengths of 304 and 316 were largely increased compared to the increase of yield strengths, but the increase of ultimate strength of 310S was almost the same to that of yield strength. Type 310S had the highest yield strength and the lowest tensile strength at all temperatutes. These tensile characteristics were considered to be strongly affected by austenite stability.(Author)

  6. Effect of N+Cr alloying on the microstructures and tensile properties of Hadfield steel

    International Nuclear Information System (INIS)

    Chen, C.; Zhang, F.C.; Wang, F.; Liu, H.; Yu, B.D.

    2017-01-01

    The microstructures and tensile behaviors of traditional Hadfield steel, named Mn12 steel, and Hadfield steel alloyed with N+Cr, named Mn12CrN steel were studied through optical microscopy, transmission electron microscopy, and scanning electron microscopy, among others. Three different tensile strain rates of 5×10 −4 , 5×10 −3 , and 5×10 −2 s −1 were selected in the tensile test. The deformation microstructures and fracture morphologies of the two steels after fracture in the tensile test were observed to analyze the tensile deformation response to different tensile strain rates. Results showed that the grain size of Mn12CrN steel was evidently refined after alloying with N+Cr. The grain would not become abnormally coarse even with increasing austenitizing temperature. During tensile deformation, the strength and plasticity of Mn12CrN steel were superior to those of Mn12 steel at the same strain rate. With increasing the strain rate, the changes in strength and plasticity of Mn12CrN steel were less sensitive to tensile strain rate compared with Mn12 steel. The effects of grain refinement and N+Cr alloying on dynamic strain aging and deformation twining behaviors were responsible for this lack of sensitivity to strain rate.

  7. Precipitation behaviors, texture and tensile properties of an extruded Mg-7Y-1Nd-0.5Zr (wt%) alloy bar with large cross-section

    Energy Technology Data Exchange (ETDEWEB)

    Shi, Guoliang, E-mail: shigl@grinm.com; Zhang, Kui; Li, Xinggang; Li, Yongjun; Ma, Minglong; Yuan, Jiawei

    2017-02-08

    Precipitation behaviors, texture and tensile properties of an extruded Mg-7Y-1Nd-0.5Zr (wt%) (WE71) alloy bar with large cross-section of 230 mm×140 mm were investigated by hardness test, tensile test, optical microscopy (OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM), electron backscatter diffraction (EBSD), X-ray diffraction (XRD) macro-texture measurement. The bar was manufactured industrially through a procedure of “multi-direction forging (MDF)+extrusion+on-line quenching+T5 aging”. Totally different age-hardening behaviors are shown during T5 aging at 200 and 235 °C. In the first 100 h, T5 aging at 235 °C brings about 13% increases in hardness, while T5 aging at 200 °C results in 47% increase. During T5 aging at 200 °C, β′ precipitates homogeneously nucleate within the matrix with high number density; however, during T5 aging at 235 °C, β′ precipitates heterogeneously nucleate on discrete and sparse dislocations, resulting in chain-like arrangement of β′ precipitates with broad precipitate free zones in matrix. XRD macro-texture measurement illustrates that basal texture intensity of WE71 bar is much weaker than Mg-8Al-0.5Zn-0.15Mn (wt%) (AZ80) bar; the maximum basal texture intensities in the outer (O) and center (C) of WE71 bar are all about 3, while those of AZ80 bar are 17 and 14, respectively. EBSD micro-texture measurement demonstrates that the maximum texture intensities of C and O are 5.3 and 3.5, respectively. O has higher tensile properties than C because there are more un-dynamic-recrystallization (un-DRX) grains and thus larger average grain size in C. While stretching at room temperature (RT), extrusion direction (ED) in O has the best tensile properties, i.e. ultimate tensile strength (R{sub m})=368 MPa, elongation (A)=5%, and normal direction (ND) in C has the lowest tensile properties, i.e. R{sub m}=255 MPa, A=2%. While stretching at 200 °C, strength does not degrade much; ED in O still has

  8. Effect of high temperature or fire on heavy weight concrete properties

    International Nuclear Information System (INIS)

    Sakr, K.; EL-Hakim, E.

    2005-01-01

    Temperature plays an important role in the use of concrete for shielding nuclear reactors. In the present work, the effect of different durations (1, 2 and 3 h) of high temperatures (250, 500, 750 and 950 deg. C) on the physical, mechanical and radiation properties of heavy concrete was studied. The effect of fire fitting systems on concrete properties was investigated. Results showed that ilmenite concrete had the highest density, modulus of elasticity and lowest absorption percent, and it had also higher values of compressive, tensile, bending and bonding strengths than gravel or baryte concrete. Ilmenite concrete showed the highest attenuation of transmitted gamma rays. Firing (heating) exposure time was inversely proportional to mechanical properties of all types of concrete. Ilmenite concrete was more resistant to elevated temperature. Foam or air proved to be better than water as a cooling system in concrete structure exposed to high temperature because water leads to a big damage in concrete properties

  9. Tensile and creep data on type 316 stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Sikka, V. K.; Booker, B. L.P.; Booker, M. K.; McEnerney, J. W.

    1980-01-01

    This report summarizes tensile and creep data on 13 heats of type 316 stainless steel. It includes ten different product forms (three plates, four pipes, and three bars) of the reference heat tested at ORNL. Tensile data are presented in tabular form and analyzed as a function of temperature by the heat centering method. This method yielded a measure of variations within a single heat as well as among different heats. The upper and lower scatter bands developed by this method were wider at the lower temperatures than at the high temperatures (for strength properties), a trend reflected by the experimental data. The creep data on both unaged and aged specimens are presented in tabular form along with creep curves for each test. The rupture time data are compared with the ASME Code Case minimum curve at each test temperature in the range from 538 to 704{sup 0}C. The experimental rupture time data are also compared with the values predicted by using the rupture model based on elevated-temperature ultimate tensile strength. A creep ductility trend curve was developed on the basis of the reference heat data and those published in the literature on nitrogen effects. To characterize the data fully, information was also supplied on vendor, product form, fabrication method, material condition (mill-annealed vs laboratory annealed and aged), grain size, and chemical composition for various heats. Test procedures used for tensile and creep results are also discussed.

  10. Temperature Effects on the Tensile Properties of Precipitation-Hardened Al-Mg-Cu-Si Alloys

    Directory of Open Access Journals (Sweden)

    J.B. Ferguson

    2016-02-01

    Full Text Available Because the mechanical performance of precipitation-hardened alloys can be significantly altered with temperature changes, understanding and predicting the effects of temperatures on various mechanical properties for these alloys are important. In the present work, an analytical model has been developed to predict the elastic modulus, the yield stress, the failure stress, and the failure strain taking into consideration the effect of temperatures for precipitation-hardenable Al-Mg-Cu-Si Alloys (Al-A319 alloys. In addition, other important mechanical properties of Al-A319 alloys including the strain hardening exponent, the strength coefficient, and the ductility parameter can be estimated using the current model. It is demonstrated that the prediction results based on the proposed model are in good agreement with those obtained experimentally in Al-A319 alloys in the as-cast condition and after W and T7 heat treatments.

  11. Effect of High Temperature on the Tensile Behavior of CFRP and Cementitious Composites

    Science.gov (United States)

    Toutanji, Houssam A.

    1999-01-01

    Concrete and other composite manufacturing processes are continuing to evolve and become more and more suited for use in non-Earth settings such as the Moon and Mars. The fact that structures built in lunar environments would experience a range of effects from temperature extremes to bombardment by micrometeorites and that all the materials for concrete production exist on the Moon means that concrete appears to be the most feasible building material. it can provide adequate shelter from the harshness of the lunar environment and at the same time be a cost effective building material. With a return to the Moon planned by NASA to occur after the turn of the century, it will be necessary to include concrete manufacturing as one of the experiments to be conducted in one of the coming missions. Concrete's many possible uses and possibilities for manufacturing make it ideal for lunar construction. The objectives of this research are summarized as follows: i) study the possibility of concrete production on the Moon or other planets, ii) study the effect of high temperature on the tensile behavior of concrete, and iii) study the effect of high temperature on the tensile behavior of carbon fiber reinforced with inorganic polymer composites. Literature review indicates that production of concrete on the Moon or other planets is feasible using the indigenous materials. Results of this study has shown that both the tensile strength and static elastic modulus of concrete decreased with a rise in temperature from 200 to 500 C. The addition of silica fume to concrete showed higher resistance to high temperatures. Carbon fiber reinforced inorganic polymer (CFRIP) composites seemed to perform well up to 300 C. However, a significant reduction in strength was observed of about 40% at 400 C and up to 80% when the specimens were exposed to 700 C.

  12. Tensile behaviour at room and high temperatures of novel metal matrix composites based on hyper eutectic Al-Si alloys

    International Nuclear Information System (INIS)

    Valer, J.; Rodriguez, J.M.; Urcola, J.J.

    1997-01-01

    This work shows the improvement obtained on tensile stress at room and high temperatures of hyper eutectic Al-Si alloys. These alloys are produced by a combination of spray-forming, extrusion and thixoforming process, in comparison with conventional casting alloys.Al-25% Si-5%Cu. Al-25%Si-5%Cu-2%Mg and Al-30%Si-5%Cu alloys have been studied relating their microstructural parameters with tensile stress obtained and comparing them with conventional Al-20%Si. Al-36%Si and Al-50%Si alloys. Al-25%Si-5%Cu alloy-was tested before and after semi-solid forming, in order to distinguish the different behaviour of this alloy due to the different microstructure. The properties obtained with these alloys were also related to Al-SiC composites formed by similar processes. (Author) 20 refs

  13. Tensile properties of machine strength graded timber for glued laminated timber

    DEFF Research Database (Denmark)

    Boström, Lars; Hoffmeyer, Preben; Solli, Kjell-Helge

    1999-01-01

    Special setting values based on tensile properties of Norway spruce are established for four different strength grading machines. The machines included are Computermatic, Cook-Bolinder, Ersson and Dynagrade.The study shows that the yield of timber to be used in tension, such as laminations...

  14. Effect of hydrostatic pressure on the tensile properties of alpha uranium

    International Nuclear Information System (INIS)

    Chandler, E.F.

    1984-09-01

    This report examines the effect of a superimposed hydrostatic pressure on the tensile properties of four grades of rolled unalloyed alpha uranium. The materials varied in carbon content and heat treatment. The principal effect of increasing pressure is an increase in the ductility of the materials. By not heat treating the uranium after the rolling process, the interaction of carbon content on mechanical properties is almost nullified. (author)

  15. Experimental Investigations on the effect of Additive on the Tensile Properties of Fiber Glass Fabric Lamina

    Science.gov (United States)

    Nava Sai Divya, A.; Raghu Kumar, B., Dr; Lakshmi Narayana, G., Dr

    2017-09-01

    The main objective of this work is to investigate the effect of additives on tensile behaviour of fiber glass fabric at lamina level to explore an alternative skin material for the outer body of aerospace applications and machines. This experimental work investigates the effect of silica concentration in epoxy resin lapox L-12 on the tensile properties of glass fabric lamina of 4H-satin weave having 3.6 mm thickness. The lamina was prepared by using hand lay-up method and tests were conducted on it. Various tensile properties values obtained from experimentation were compared for four glass fiber lamina composites fabricated by adding the silica powder to resin bath. The effect of variations in silica concentration (0% SiO2, 5% SiO2, 10% SiO2 and 15% SiO2) on the tensile properties of prepared material revealed that maximum stiffness was obtained at 15% and yield strength at 10% SiO2 concentration in glass fiber lamina. Increasing the silica concentration beyond 10% had led to deterioration in the material properties. The experimentation that was carried out on test specimen was reasonably successful as the effect of silica powder as an additive in glass fiber lamina enhanced the mechanical properties up to certain limit. The underpinning microscopic behaviour at the source of these observations will be investigated in a follow up work.

  16. Assessment of tensile and creep data for types 304 and 316 stainless steel

    International Nuclear Information System (INIS)

    Sikka, V.K.; Booker, M.K.

    1976-01-01

    Austenitic stainless steels of types 304 and 316 are prime construction materials for nuclear fast breeder reactors and will be used in the temperature range where elevated-temperature, tensile, creep, and fatigue properties are required to calculate the design stress limits. This report examines the possible variations in such properties, using data from several sources including data from Japan and the United Kingdom. United States data were shown to contain the largest variations in both tensile and creep properties, with Japanese data the least. For a given country no distinction could be made in variations in tensile properties of types 304 and 316 stainless steels, but variations in standard error of estimate for all creep properties analyzed were significantly lower for type 316 stainless steel than corresponding variations in creep properties of type 304 stainless steel. The data from each of these countries showed the same creep rupture strength (at 10 4 h) for type 316 stainless steel; this was not true for the type 304 stainless steel. Results of the analysis performed in this paper showed that the U.S. and foreign data on types 304 and 316 stainless steels could possibly be combined for the determination of design stress intensity limits

  17. Experimental Investigation of the Effects of Concrete Alkalinity on Tensile Properties of Preheated Structural GFRP Rebar

    Directory of Open Access Journals (Sweden)

    Hwasung Roh

    2017-01-01

    Full Text Available The combined effects of preexposure to high temperature and alkalinity on the tensile performance of structural GFRP reinforcing bars are experimentally investigated. A total of 105 GFRP bar specimens are preexposed to high temperature between 120°C and 200°C and then immersed into pH of 12.6 alkaline solution for 100, 300, and 660 days. From the test results, the elastic modulus obtained at 300 immersion days is almost the same as those of 660 immersion days. For all alkali immersion days considered in the test, the preheated specimens provide slightly lower elastic modulus than the unpreheated specimens, showing only 8% maximum difference. The tensile strength decreases for all testing cases as the increase of the alkaline immersing time, regardless of the prehearing levels. The tensile strength of the preheated specimens is about 90% of the unpreheated specimen for 300 alkali immersion days. However, after 300 alkali immersion days the tensile strengths are almost identical to each other. Such results indicate that the tensile strength and elastic modulus of the structural GFRP reinforcing bars are closely related to alkali immersion days, not much related to the preheating levels. The specimens show a typical tensile failure around the preheated location.

  18. Influence of (TiC+TiB) on the microstructure and tensile properties of Ti-B20 matrix alloy

    Energy Technology Data Exchange (ETDEWEB)

    Rahoma, H.K.S. [National Key Laboratory of Science and Technology on Precision Heat Processing of Metals, Harbin Institute of Technology, Harbin 150001 (China); Chen, Y.Y., E-mail: yychen@hit.edu.cn [National Key Laboratory of Science and Technology on Precision Heat Processing of Metals, Harbin Institute of Technology, Harbin 150001 (China); State Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology, Harbin 150001 (China); Wang, X.P.; Xiao, S.L. [National Key Laboratory of Science and Technology on Precision Heat Processing of Metals, Harbin Institute of Technology, Harbin 150001 (China)

    2015-04-05

    Highlights: • After forging, the microstructure was significantly refined and uniform. • The presence of carbide and boride also led to uniform and finer precipitation of α during aging as compared to the matrix alloy. • The size of secondary α phase increased with the increase of aging temperature. This trend leads to the decrease of strength and the increase of ductility. - Abstract: A hybrid of (TiB+TiC) reinforced beta titanium matrix (Ti-B20) were produced by non-consumable arc-melting technology and hot-forging. Microstructures of the composites were observed by optical microscopy (OM), transmission electron microscope (TEM) and scanning electron microscopy (SEM). The results show that both the TiB whiskers and TiC particles tend to segregate at β boundaries. The β grain size and secondary α lath width are refined by reinforcements and aging treatment. Evolution of tensile properties shows that enhancement in yield strength and ultimate tensile strength with the addition of reinforcements, as well as the remarkable increase in the ductility can be attributed to aging treatment at 600 °C and 650 °C. The size of secondary α phase increased with the increase of aging temperature. This trend leads to the decrease of strength and the increase of ductility to get good balance of properties. The fracture mechanism of the composite can be attributed to the cracking of the reinforcements.

  19. Effect of Kevlar and carbon fibres on tensile properties of oil palm/epoxy composites

    Science.gov (United States)

    Amir, S. M. M.; Sultan, M. T. H.; Jawaid, M.; Cardona, F.; Ishak, M. R.; Yusof, M. R.

    2017-12-01

    Hybrid composites with natural and synthetic fibers have captured the interests of many researchers. In this work, Kevlar/oil palm Empty Fruit Bunch (EFB)/Kevlar and carbon/oil palm EFB hybrid/carbon composites were prepared using hand lay-up technique by keeping the oil palm EFB fiber as the core material. The tensile properties which include tensile strength, tensile modulus and elongation at break were investigated. It is observed that the tensile strength and modulus for carbon/oil palm EFB/carbon hybrid composites were much higher as compared with Kevlar/oil palm EFB/Kevlar hybrid composites. However, the elongation at break for Kevlar/oil palm EFB/Kevlar hybrid composites exhibited higher value as compared to carbon/oil palm EFB/carbon hybrid composites and oil palm EFB/epoxy composites. The tensile strength for carbon/oil palm EFB/carbon hybrid composites is 93.6 MPa and the tensile modulus for carbon/oil palm EFB/carbon hybrid composites is 6.5 GPa. The elongation at break for Kevlar/oil palm EFB/Kevlar hybrid composites is 3.6%.

  20. Tensile Properties of the Deep Transverse Metatarsal Ligament in Hallux Valgus: A CONSORT-Compliant Article.

    Science.gov (United States)

    Abdalbary, Sahar Ahmed; Elshaarawy, Ehab A A; Khalid, Bahaa E A

    2016-02-01

    The deep transverse metatarsal ligament (DTML) connects the neighboring2 metatarsal heads and is one of the stabilizers connecting the lateral sesamoid and second metatarsal head. In this study, we aimed to determine the tensile properties of the DTML in normal specimens and to compare these results with hallux valgus specimens. We hypothesized that the tensile properties of the DTML would be different between the 2 groups of specimens.The DTML in the first interspace was dissected from 12 fresh frozen human cadaveric specimens. Six cadavers had bilateral hallux valgus and the other 6 cadavers had normal feet. The initial length (L0) and cross-sectional area (A0) of the DTML were measured using a digital caliper, and tensile tests with load failure were performed using a material testing machine.There were significant between-groups differences in the initial length (L0) P = 0.009 and cross-sectional area (A0) of the DTML P = 0.007. There were also significant between-groups differences for maximum force (N) P = 0.004, maximum distance (mm) P = 0.005, maximum stress (N/mm) P = 0.003, and maximum strain (%) P = 0.006.The DTML is an anatomical structure for which the tensile properties differ in hallux valgus.

  1. The influences of deformation velocity and temperature on localized deformation of zircaloy-4 in tensile tests

    International Nuclear Information System (INIS)

    Boratto, F.J.M.

    1973-01-01

    A new parameter to describe the necking stability in zircaloy-4 during tensile tests is introduced. The parameter is defined as: s = ∂Ln (dσ/dε)/∂Ln ((1/L)dL/dt) for constant temperature, deformation and history. Measures of stress strain rate sensitivity n, reduction of the area at fracture, and deformation profiles of tensile fracture, are done. A complete description of the curve of non-uniform deformation variation with the temperature, is presented. The results are compared with existing data for pure commercially titanium. The influence of strain rate and history on s and n parameters, in the temperature range from 100-700 0 C). (author) [pt

  2. Tensile and Charpy impact properties of an ODS ferritic/martensitic steel 9Cr–1.8W–0.5Ti–0.35Y{sub 2}O{sub 3}

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Guangming; Zhou, Zhangjian, E-mail: zhouzhj@mater.ustb.edu.cn; Wang, Man; Li, Shaofu; Zou, Lei; Zhang, Liwei

    2014-04-15

    Highlights: • The tensile property and Charpy impact were tested. • Both strength and plasticity in LT direction are better than that of TL direction. • The LSE was more than 65% of the USE from absorbed energy curve. • The initiation and propagation energy at different temperatures were calculated. • High LSE and dimples on the fracture surface indicated good toughness at −60 °C. - Abstract: A 9Cr-ODS ferritic/martensitic steel with a composition of 9Cr–1.8W–0.5Ti–0.35Y{sub 2}O{sub 3} was fabricated by mechanical alloying and hot isostatic pressing, followed by hot rolling. Tensile properties were measured at room temperature (23 °C) and 700 °C in the rolling direction (LT) and the transverse direction (TL). The ultimate tensile strength (UTS) of the as-rolled samples in both directions reached 990 MPa at 23 °C, and still maintained at 260 MPa at 700 °C. The tensile strength and elongation of the rolling direction was greater than that of the transverse direction. The Charpy impact was tested from −100 to 100 °C in the LT direction. The lower shelf energy (LSE) was more than 65% of the upper shelf energy (USE). The total absorbed energy was separated into the energies for crack initiation and propagation. The propagation energy was always higher than the initiation energy in the range of temperatures tested. The ductile-to-brittle transition temperature (DBTT) of the rolled 9Cr ODS evaluated by an absorbed energy curve was about 0 °C. However, the high LSE and the fracture surface that still contained dimples at lower shelf indicated good toughness of the as-rolled 9Cr ODS steels at temperature of −60 °C.

  3. Effect of ion irradiation on tensile ductility, strength and fictive temperature in metallic glass nanowires

    International Nuclear Information System (INIS)

    Magagnosc, D.J.; Kumar, G.; Schroers, J.; Felfer, P.; Cairney, J.M.; Gianola, D.S.

    2014-01-01

    Ion irradiation of thermoplastically molded Pt 57.5 Cu 14.3 Ni 5.7 P 22.5 metallic glass nanowires is used to study the relationship between glass structure and tensile behavior across a wide range of structural states. Starting with the as-molded state of the glass, ion fluence and irradiated volume fraction are systematically varied to rejuvenate the glass, and the resulting plastic behavior of the metallic glass nanowires probed by in situ mechanical testing in a scanning electron microscope. Whereas the as-molded nanowires exhibit high strength, brittle-like fracture and negligible inelastic deformation, ion-irradiated nanowires show tensile ductility and quasi-homogeneous plastic deformation. Signatures of changes to the glass structure owing to ion irradiation as obtained from electron diffraction are subtle, despite relatively large yield strength reductions of hundreds of megapascals relative to the as-molded condition. To reconcile changes in mechanical behavior with glass properties, we adapt previous models equating the released strain energy during shear banding to a transit through the glass transition temperature by incorporating the excess enthalpy associated with distinct structural states. Our model suggests that ion irradiation increases the fictive temperature of our glass by tens of degrees – the equivalent of many orders of magnitude change in cooling rate. We further show our analytical description of yield strength to quantitatively describe literature results showing a correlation between severe plastic deformation and hardness in a single glass system. Our results highlight not only the capacity for room temperature ductile plastic flow in nanoscaled metallic glasses, but also processing strategies capable of glass rejuvenation outside of the realm of traditional thermal treatments

  4. Tensile and charpy impact properties of irradiated reduced-activation ferritic steels

    Energy Technology Data Exchange (ETDEWEB)

    Klueh, R.L.; Alexander, D.J. [Oak Ridge National Lab., TN (United States)

    1996-10-01

    Tensile tests were conducted on eight reduced-activation Cr-W steels after irradiation to 15-17 and 26-29 dpa, and Charpy impact tests were conducted on the steels irradiated to 26-29 dpa. Irradiation was in the Fast Flux Test Facility at 365{degrees}C on steels containing 2.25-12% Cr, varying amounts of W, V, and Ta, and 0.1%C. Previously, tensile specimens were irradiated to 6-8 dpa and Charpy specimens to 6-8, 15-17, and 20-24 dpa. Tensile and Charpy specimens were also thermally aged to 20000 h at 365{degrees}C. Thermal aging had little effect on the tensile behavior or the ductile-brittle transition temperature (DBTT), but several steels showed a slight increase in the upper-shelf energy (USE). After {approx}7 dpa, the strength of the steels increased and then remained relatively unchanged through 26-29 dpa (i.e., the strength saturated with fluence). Post-irradiation Charpy impact tests after 26-29 dpa showed that the loss of impact toughness, as measured by an increase in DBTT and a decrease in the USE, remained relatively unchanged from the values after 20-24 dpa, which had been relatively unchanged from the earlier irradiations. As before, the two 9Cr steels were the most irradiation resistant.

  5. Effect of N+Cr alloying on the microstructures and tensile properties of Hadfield steel

    Energy Technology Data Exchange (ETDEWEB)

    Chen, C. [State Key Laboratory of Metastable Materials Science and Technology, Yanshan University, Qinhuangdao 066004 (China); Zhang, F.C., E-mail: zfc@ysu.edu.cn [State Key Laboratory of Metastable Materials Science and Technology, Yanshan University, Qinhuangdao 066004 (China); National Engineering Research Center for Equipment and Technology of Cold Strip Rolling, Yanshan University, Qinhuangdao 066004 (China); Wang, F. [State Key Laboratory of Metastable Materials Science and Technology, Yanshan University, Qinhuangdao 066004 (China); Liu, H.; Yu, B.D. [China Railway Shanhaiguan Bridge Group Co. LTD, Qinhuangdao 066205 (China)

    2017-01-02

    The microstructures and tensile behaviors of traditional Hadfield steel, named Mn12 steel, and Hadfield steel alloyed with N+Cr, named Mn12CrN steel were studied through optical microscopy, transmission electron microscopy, and scanning electron microscopy, among others. Three different tensile strain rates of 5×10{sup −4}, 5×10{sup −3}, and 5×10{sup −2} s{sup −1} were selected in the tensile test. The deformation microstructures and fracture morphologies of the two steels after fracture in the tensile test were observed to analyze the tensile deformation response to different tensile strain rates. Results showed that the grain size of Mn12CrN steel was evidently refined after alloying with N+Cr. The grain would not become abnormally coarse even with increasing austenitizing temperature. During tensile deformation, the strength and plasticity of Mn12CrN steel were superior to those of Mn12 steel at the same strain rate. With increasing the strain rate, the changes in strength and plasticity of Mn12CrN steel were less sensitive to tensile strain rate compared with Mn12 steel. The effects of grain refinement and N+Cr alloying on dynamic strain aging and deformation twining behaviors were responsible for this lack of sensitivity to strain rate.

  6. Influence of Simulated Acid Rain Corrosion on the Uniaxial Tensile Mechanical Properties of Concrete

    Directory of Open Access Journals (Sweden)

    Ying-zi Zhang

    2012-01-01

    Full Text Available An experimental study on the uniaxial tensile property of concrete exposed to the acid rain environment was carried out. Acid rain with pH level of 1.0 was deposed by the mixture of sulfate and nitric acid solution in the laboratory. Dumbbell-shaped concrete specimens were immersed in the simulated acid rain completely. After being exposed to the deposed mixture for a certain period, uniaxial tensile test was performed on the concrete specimens. The results indicate that elastic modulus, tensile strength, and peak strain have a slight increase at the initial corrosion stage, and with the extension of corrosion process, elastic modulus and tensile strength decrease gradually, while the peak strain still increases. It is found that the compressive strength is more sensitive than the tensile strength in aggressive environment. Based on the experimental results, an equation was proposed to describe the ascending branch of the stress-strain curve of the concrete corroded by acid rain.

  7. Effect of holes on the room temperature tensile behaviors of thin wall specimens with (210) side surface of Ni-base single crystal superalloy

    Energy Technology Data Exchange (ETDEWEB)

    Zhou, Z.J.; Liu, T.; Pu, S. [Superalloys Division, Institute of Metal Research, Chinese Academy of Sciences, No. 72, Wenhua Road, Shenyang 110016 (China); Xu, H. [Materials Fatigue and Fracture Division, Institute of Metal Research, Chinese Academy of Sciences, No. 72, Wenhua Road, Shenyang 110016 (China); Wang, L., E-mail: wangli@imr.ac.cn [Superalloys Division, Institute of Metal Research, Chinese Academy of Sciences, No. 72, Wenhua Road, Shenyang 110016 (China); Lou, L.H. [Superalloys Division, Institute of Metal Research, Chinese Academy of Sciences, No. 72, Wenhua Road, Shenyang 110016 (China)

    2015-10-25

    Tensile properties of Ni-base single crystal superalloy plate specimens with and without a hole at room temperature were studied in the present paper. During the testing process, an ARAMIS system based on the digital image correlation technique and in-situ scanning electron microscopy were employed to in-situ observe the strain distribution and slip traces development on the sample surfaces. It was demonstrated that the yield stress was decreased with the appearance of a hole due to the stress concentration. The results were analyzed based on the stress and strain states of specimens and the slip traces development observed on specimen surfaces. - Graphical abstract: The strain distribution for samples without and with a hole, respectively. - Highlights: • Tensile tests of plate specimens without and with a hole were performed. • Surface strain fields were in-situ observed by ARAMIS system. • Slip traces development on sample surfaces was in-situ observed by SEM. • The hole deteriorated both the tensile strength and elongation of the samples. • Tensile strength of specimens without and with a hole was discussed respectively.

  8. Tensile Properties of Single Jersey and 1×1 Rib Knitted Fabrics Made from 100% Cotton and Cotton/Lycra Yarns

    Directory of Open Access Journals (Sweden)

    Dereje Berihun Sitotaw

    2017-01-01

    Full Text Available The tensile properties such as tensile strength which is measured as breaking force in Newton (N and elongation percent (% at break of single jersey and 1×1 rib (knitted with full needles knitted fabrics made from 100% cotton and cotton/Lycra yarns (5% Lycra yarn content in 95% combed cotton yarn are investigated in this research. The sample fabrics are conditioned for 24 hours at 20±1°C temperature and 65±2% relative humidity before testing. Ten specimens (five for lengthwise and five for widthwise have been taken from each of the two knitted structures, those made from 100% cotton and cotton/Lycra (at 95/5 percent ratio blend yarns. According to the discussion and as found from the investigations, the tensile properties of single jersey and 1×1 rib knitted fabrics made from 100% cotton and cotton/Lycra yarns are significantly different from each other and both of the knitted fabrics have high elongation percent at break with cotton/Lycra blend yarns as compared to 100% cotton yarn. Knitted fabrics made from cotton/Lycra blended yarn have low breaking force and high elongation percent at break relative to knitted fabrics made from 100% cotton yarns.

  9. Effect of helium and DPA's on tensile properties of V-5Ti and V-3Ti-1Si

    International Nuclear Information System (INIS)

    Witzenburg, W. van; Vries, E. de.

    1991-02-01

    Specimens of the alloys V-5Ti and V-3Ti-1Si were irradiated in a mixed-spectrum fission reactor in reactor grade liquid sodium to a fast neutron fluence of 3.8 x 10 25 m -2 (E>0.1 MeV), which corresponds to 6.2 dpa. Irradiation temperatures were 500, 600 and 700 deg C. Some of the specimens were pre-injected with helium to 100 appm at approx 50 deg C by means of a cyclotron. In addition, part of the specimens were doped with boron-10 to concentrations of 100 and 600 appm. Tensile testing, at temperatures equal to the irradiation temperatures and at a strain rate of 10 -4 s -1 , showed an increase in strength and reduced elongation at 500 deg C and to a lesser extent at 600 deg C. These changes are caused by displacement damage. Helium, pre-injected as well as produced by transmutation of boron-10, did not have a significant influence on the tensile properties. Cavities seen in the irradiated materials at low concentrations, were not preferentially located on grain boundaries. There was no apparent deleterious effect of lithium, which is also a transmutation product of boron-10. (author). 12 refs.; 8 figs.; 3 tabs

  10. Making High-Tensile-Strength Amalgam Components

    Science.gov (United States)

    Grugel, Richard

    2008-01-01

    Structural components made of amalgams can be made to have tensile strengths much greater than previously known to be possible. Amalgams, perhaps best known for their use in dental fillings, have several useful attributes, including room-temperature fabrication, corrosion resistance, dimensional stability, and high compressive strength. However, the range of applications of amalgams has been limited by their very small tensile strengths. Now, it has been discovered that the tensile strength of an amalgam depends critically on the sizes and shapes of the particles from which it is made and, consequently, the tensile strength can be greatly increased through suitable choice of the particles. Heretofore, the powder particles used to make amalgams have been, variously, in the form of micron-sized spheroids or flakes. The tensile reinforcement contributed by the spheroids and flakes is minimal because fracture paths simply go around these particles. However, if spheroids or flakes are replaced by strands having greater lengths, then tensile reinforcement can be increased significantly. The feasibility of this concept was shown in an experiment in which electrical copper wires, serving as demonstration substitutes for copper powder particles, were triturated with gallium by use of a mortar and pestle and the resulting amalgam was compressed into a mold. The tensile strength of the amalgam specimen was then measured and found to be greater than 10(exp 4) psi (greater than about 69 MPa). Much remains to be done to optimize the properties of amalgams for various applications through suitable choice of starting constituents and modification of the trituration and molding processes. The choice of wire size and composition are expected to be especially important. Perusal of phase diagrams of metal mixtures could give insight that would enable choices of solid and liquid metal constituents. Finally, whereas heretofore, only binary alloys have been considered for amalgams

  11. Effect of heat treatment on the elevated temperature tensile and fracture toughness behavior of Alloy 718 weldments

    International Nuclear Information System (INIS)

    Mills, W.J.

    1980-05-01

    The effect of heat treatment on the tensile and fracture toughness properties of Alloy 718 weldments was characterized at room temperature and elevated temperatures. The two heat treatments employed during this investigation were the convectional (ASTM A637) precipitation treatment and a modified treatment designed to improve the toughness of Alloy 718 welds. Weldments were also examined in the as-welded condition. The fracture toughness behavior of the Alloy 718 weldments was determined at 24, 427 and 538 degree C using both linear-elastic (K Ic ) and elastic-plastic (J Ic ) fracture mechanics concepts. Metallographic and electron fractographic examination of Alloy 718 weld fracture surfaces revealed that differences in fracture toughness behavior for the as-welded, conventional and modified conditions were associated with variations in the weld microstructure. 28 refs., 16 figs., 4 tabs

  12. STUDY ON IMPACT AND TENSILE PROPERTIES OF CONCRETE WITH COCONUT SHELL AS COARSE AGGREGATE

    OpenAIRE

    R. Ranjith*

    2017-01-01

    The mechanical properties of coconut shell aggregate concrete (CSAC) namely splitting tensile strength, impact strength have been determined and a comparison is made with conventional granite aggregate concrete (CGAC) in the 30 days short-term experimental investigation. From the test results it is observed that coconut shell aggregate concrete has considerably sufficient strength. But the splitting tensile strength of coconut shell aggregate concrete is 50 % less than that of conventional gr...

  13. FY 2017-Influence of Sodium Environment on the Tensile Properties of Advanced Alloys

    Energy Technology Data Exchange (ETDEWEB)

    Natesan, K. [Argonne National Lab. (ANL), Argonne, IL (United States); Li, Meimei [Argonne National Lab. (ANL), Argonne, IL (United States); Chen, Wei-Ying [Argonne National Lab. (ANL), Argonne, IL (United States)

    2017-08-01

    This report provides an update on the understanding of the effects of sodium exposures on tensile properties of advanced alloy 709 in support of the design and operation of structural components in sodium-cooled fast reactors (SFRs). The report is a Level 3 deliverable in FY17 (M3AT-17AN1602093), under the Work Package AT-17AN160209, “Sodium Compatibility” performed by Argonne National Laboratory (ANL), as part of Advanced Reactor Technologies Program. Three laboratory-size heats of Alloy 709 austenitic steel were investigated in liquid sodium environments at 550-650°C to understand its corrosion behaviour, microstructural evolution, and tensile properties. In addition, a commercial scale heat has been produced and hot-rolled into plates.

  14. Selective Electron Beam Manufacturing of Ti-6Al-4V Strips: Effect of Build Orientation, Columnar Grain Orientation, and Hot Isostatic Pressing on Tensile Properties

    Science.gov (United States)

    Wang, J.; Tang, H. P.; Yang, K.; Liu, N.; Jia, L.; Qian, M.

    2018-03-01

    Many novel designs for additive manufacturing (AM) contain thin-walled (≤ 3 mm) sections in different orientations. Selective electron beam melting (SEBM) is particularly suited to AM of such thin-walled titanium components because of its high preheating temperature and high vacuum. However, experimental data on SEBM of Ti-6Al-4V thin sections remains scarce because of the difficulty and high cost of producing long, thin and smooth strip tensile specimens (see Fig. 1). In this study, 80 SEBM Ti-6Al-4V strips (180 mm long, 42 mm wide, 3 mm thick) were built both vertically (V-strips) and horizontally (H-strips). Their density, microstructure and tensile properties were investigated. The V-strips showed clearly higher tensile strengths but lower elongation than the H-strips. Hot isostatic pressing (HIP) produced the same lamellar α-β microstructures in terms of the average α-lath thickness in both types of strips. The retained prior-β columnar grain boundaries after HIP showed no measurable influence on the tensile properties, irrespective of their length and orientation, because of the formation of randomly distributed fine α-laths.[Figure not available: see fulltext.

  15. Swelling and tensile properties of starch glycerol system with various crosslinking agents

    Science.gov (United States)

    Mohamed, R.; Mohd, N.; Nurazzi, N.; Siti Aisyah, M. I.; Fauzi, F. Mohd

    2017-07-01

    Brittle properties of starch had been overcome by the modification process. In this work, sago starch is being modified with variable amount of plasticiser, namely glycerol at 20 and 40% and crosslinking agent had been added to the system. The film of the modification and characterizations of the starch glycerol system with various crosslinking systems were produced by casting method. The film properties of the starch glycerol system were then characterized by tensile strength (mechanical properties) and swelling (physical properties). The modification of the starch glycerol had improved that system by increasing the tensile strength, modulus however lowering its elongation. The increasing in percentage of the water absorption and also swelling are due to the intrinsic hydroxyl groups presence from the starch and glycerol itself that can attract more water to the system. Upon crosslinking, films casted with chemicals namely, glyoxal, malonic acid, borax, PEG were characterised. It was found that, all the film of sago starch crosslinked and undergoing easy film formation. From this modification, borax and malonic acid crosslinking agent had been determined as the best crosslinking agent to the starch glycerol system.

  16. Thermal, tensile and rheological properties of low density polyethylene (LDPE) processed irradiated by gamma-ray

    International Nuclear Information System (INIS)

    Ferreto, Helio F.R.; Oliveira, Ana C.F. de; Parra, Duclerc F.; Lugao, Ademar B.

    2013-01-01

    The aim of this paper is to investigate structural changes of low density polyethylene (LDPE) modified by ionizing radiation (gamma rays). The gamma radiation process for modification of commercial polymers is a widely applied technique to promote new physical-chemical and mechanical properties. Gamma irradiation originates free radicals which can induce chain scission or recombination, providing its annihilation, branching or crosslinking. The samples were prepare in hydraulic press in temperature 180 deg C after was irradiated with gamma source of 60 Co at doses of 5, 10, 20, 50 or 100 kGy at a dose rate of 5 kGy/h in inert atmosphere. The changes in molecular structure of LDPE, after gamma irradiations were evaluated using thermogravimetric analysis (TGA) and tensile machine and oscillatory rheology. The results showed the variations of the properties depending on the dose at each atmosphere. (author)

  17. The effect of strain rate and temperature on the elevated temperature tensile flow behavior of service-exposed 2.25Cr-1Mo steel

    International Nuclear Information System (INIS)

    Girish Shastry, C.; Parameswaran, P.; Mathew, M.D.; Bhanu Sankara Rao, K.; Mannan, S.L.

    2007-01-01

    The elevated temperature tensile flow behavior of service-exposed 2.25Cr-1Mo steel has been critically examined with respect to strain rate sensitivity (m) and apparent activation energy (Q) for tensile deformation. The predominant role of forest dislocations in determining the relative flow response at true plastic strains greater than 0.01 is inferred from the profile of 'm' against flow stress. The variation of 'm' with temperature and strain is discussed based on the kinetics of dislocation generation and recovery. The decrease in Q with the increase in strain rate or temperature is attributed to the increase in recovery processes like dislocation annihilation and subcell/subgrain formation. This suggestion has been supported by transmission electron microscopy

  18. Effect of machining damage on tensile properties of beryllium

    International Nuclear Information System (INIS)

    Hanafee, J.E.

    1976-01-01

    It is well established that damage introduced at the surface of beryllium during machining operations can lower its mechanical properties. Tensile tests were conducted to illustrate this on beryllium presently being used for parts in the W79 program and similar to the new powder-processed beryllium specified for production (tentative specification MEL 76-001319). The objective of this study is to quantitatively illuminate the importance of controlling machining damage in this particular grade of powder-processed beryllium

  19. Effect of fiber content on tensile retention properties of Cellulose Microfiber Reinforced Polymer Composites for Automobile Application

    Science.gov (United States)

    Aseer, J. R.; Sankaranarayanasamy, K.

    2017-12-01

    Today, the utilization of biodegradable materials has been hogging much attention throughout the world. Due to the disposal issues of petroleum based products, there is a focus towards developing biocomposites with superior mechanical properties and degradation rate. In this research work, Hibiscus Sabdariffa (HS) fibers were used as the reinforcement for making biocomposites. The HS fibers were reinforced in the polyester resin by compression moulding method. Water absorption studies of the composite at room temperature are carried out as per ASTM D 570. Also, degradation behavior of HS/Polyester was done by soil burial method. The HS/polyester biocomposites containing 7.5 wt% of HS fiber has shown higher value of tensile strength. The tensile strength retention of the HS/Polyester composites are higher than the neat polyester composites. This value increases with increase of HS fiber loading in the composites. The results indicated that HS/polyester biocomposites can be used for making automobile components such as bumper guards etc.

  20. Effect of strain rate and notch geometry on tensile properties and fracture mechanism of creep strength enhanced ferritic P91 steel

    Science.gov (United States)

    Pandey, Chandan; Mahapatra, M. M.; Kumar, Pradeep; Saini, N.

    2018-01-01

    Creep strength enhanced ferritic (CSEF) P91 steel were subjected to room temperature tensile test for quasi-static (less than 10-1/s) strain rate by using the Instron Vertical Tensile Testing Machine. Effect of different type of notch geometry, notch depth and angle on mechanical properties were also considered for different strain rate. In quasi-static rates, the P91 steel showed a positive strain rate sensitivity. On the basis of tensile data, fracture toughness of P91 steel was also calculated numerically. For 1 mm notch depth (constant strain rate), notch strength and fracture toughness were found to be increased with increase in notch angle from 45° to 60° while the maximum value attained in U-type notch. Notch angle and notch depth has found a minute effect on P91 steel strength and fracture toughness. The fracture surface morphology was studied by field emission scanning electron microscopy (FESEM).

  1. Stress envelope of silicon carbide composites at elevated temperatures

    International Nuclear Information System (INIS)

    Nozawa, Takashi; Kim, Sunghun; Ozawa, Kazumi; Tanigawa, Hiroyasu

    2014-01-01

    To identify a comprehensive stress envelope, i.e., strength anisotropy map, of silicon carbide fiber-reinforced silicon carbide matrix composite (SiC/SiC composite) for practical component design, tensile and compressive tests were conducted using the small specimen test technique specifically tailored for high-temperature use. In-plane shear properties were, however, estimated using the off-axial tensile method and assuming that the mixed mode failure criterion, i.e., Tsai–Wu criterion, is valid for the composites. The preliminary test results indicate no significant degradation to either proportional limit stress (PLS) or fracture strength by tensile loading at temperatures below 1000 °C. A similarly good tolerance of compressive properties was identified at elevated temperatures, except for a slight degradation in PLS. With the high-temperature test data of tensile, compressive and in-plane shear properties, the stress envelopes at elevated temperatures were finally obtained. A slight reduction in the design limit was obvious at elevated temperatures when the compressive mode is dominant, whereas a negligibly small impact on the design is expected by considering the tensile loading case

  2. Stress envelope of silicon carbide composites at elevated temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Nozawa, Takashi, E-mail: nozawa.takashi67@jaea.go.jp [Japan Atomic Energy Agency, 2-166 Omotedate, Obuchi, Rokkasho, Aomori 039-3212 (Japan); Kim, Sunghun [Graduate School of Energy Science, Kyoto University, Gokasho, Uji, Kyoto 611-0011 (Japan); Ozawa, Kazumi; Tanigawa, Hiroyasu [Japan Atomic Energy Agency, 2-166 Omotedate, Obuchi, Rokkasho, Aomori 039-3212 (Japan)

    2014-10-15

    To identify a comprehensive stress envelope, i.e., strength anisotropy map, of silicon carbide fiber-reinforced silicon carbide matrix composite (SiC/SiC composite) for practical component design, tensile and compressive tests were conducted using the small specimen test technique specifically tailored for high-temperature use. In-plane shear properties were, however, estimated using the off-axial tensile method and assuming that the mixed mode failure criterion, i.e., Tsai–Wu criterion, is valid for the composites. The preliminary test results indicate no significant degradation to either proportional limit stress (PLS) or fracture strength by tensile loading at temperatures below 1000 °C. A similarly good tolerance of compressive properties was identified at elevated temperatures, except for a slight degradation in PLS. With the high-temperature test data of tensile, compressive and in-plane shear properties, the stress envelopes at elevated temperatures were finally obtained. A slight reduction in the design limit was obvious at elevated temperatures when the compressive mode is dominant, whereas a negligibly small impact on the design is expected by considering the tensile loading case.

  3. Effect of chemistry variations on the short-term rupture life and tensile properties of 20% cold-worked type 316 stainless steel

    International Nuclear Information System (INIS)

    Duncan, D.R.; Paxton, M.M.

    1977-01-01

    The effects of compositional variations on the rupture life of 20% cold-worked Type 316 stainless steel were investigated at 19-ksi (131-MPa) uniaxial tensile stress and at 1400 0 F (1033 K). Forty-nine different alloys were studied, with compositional variations from nominal in carbon, nitrogen, phosphorus, sulfur, boron, manganese, copper, silicon, molybdenum, cobalt, chromium and nickel. This alloy and cold-work level represents the duct and fuel cladding material choice for the first four core loadings of the Fast Flux Test Facility, a key element in the Liquid-Metal Fast Breeder Reactor Program. Tensile properties of four of the alloys were studied at temperatures from room temperature to 1600 0 F (1144 K). Boron, nitrogen, and molybdenum plus silicon additions significantly increased rupture life, while chromium and carbon additions decreased rupture life. Molybdenum plus silicon additions increased yield and ultimate strength and ductility at 1200 0 F (922 K) and below

  4. The Effect of Prestrain Temperature on Kinetics of Static Recrystallization, Microstructure Evolution, and Mechanical Properties of Low Carbon Steel

    Science.gov (United States)

    Akbari, Edris; Karimi Taheri, Kourosh; Karimi Taheri, Ali

    2018-05-01

    In this research, the samples of a low carbon steel sheet were rolled up to a thickness prestrain of 67% at three different temperatures consisted of room, blue brittleness, and subzero temperature. Microhardness, SEM, and tensile tests were carried out to evaluate the static recrystallization kinetics defined by the Avrami equation, microstructural evolution, and mechanical properties. It was found that the Avrami exponent is altered with change in prestrain temperature and it achieves the value of 1 to 1. 5. Moreover, it was indicated that prestraining at subzero temperature followed by annealing at 600 °C leads to considerable enhancement in tensile properties and kinetics of static recrystallization compared to room and blue brittleness temperatures. The prestraining at blue brittleness temperature followed by annealing treatment caused, however, a higher strength and faster kinetics compared with that at room temperature. It was concluded that although from the steel ductility point of view, the blue brittleness temperature is called an unsuitable temperature, but it can be used as prestraining temperature to develop noticeable combination of strength and ductility in low carbon steel.

  5. Effect of fiber orientation on tensile and impact properties of Zalacca Midrib fiber-HDPE composites by compression molding

    Science.gov (United States)

    Lasikun, Ariawan, Dody; Surojo, Eko; Triyono, Joko

    2018-02-01

    The research aims to investigate the fiber orientation effect on the tensile and impact properties of zalacca midrib fiber /HDPE composites. The composites were produced by compression molding with pressing temperature at 150°C, pressing pressure at 50 bar, and holding time of 25 minutes. The fiber orientations applied in composites were 0°, 15°, 30°, 45°, 60°, 75°, and 90°, at 10% fiber volume fraction. The samples were evaluated by using: Tensile test and Izod impact test according to ASTM D638 and ASTM D5941, respectively. The result of experiments indicate that the orientation of zalacca midrib fiber influences the characteristics of HDPE composite-zalacca midrib fiber. The composite mechanical strength decline with the increase of orientation fibers from 0° to 90°. The composite failure mode of composites are observed by Scanning Electron Microscope (SEM).

  6. The postirradiation tensile properties and microstructure of several vanadium alloys

    International Nuclear Information System (INIS)

    Braski, D.N.

    1988-01-01

    Tensile specimens of V-15Cr-5Ti, Vanstar-7, V-3Ti-1si, and V-20Ti were irradiated at 420/degrees/C in FFTF-MOTA to a damage level of 82 dpa. Helium was preimplanted to levels up to 480 appm in selected specimens using a modified tritium trick. Irradiation hardening was the dominant effect influencing the postirradiation tensile properties, and it markedly increased the yield strength and reduced the total elogation. The V-15Cr-5Ti alloy was very sensitive to helium embrittlement, but Vanstar-7 and V-3Ti-1Si were only slightly affected. Without helium, negligible swelling (<1%) were measured in V-3Ti-1Si and V-20Ti. Preimplanted helium increased swelling in V-3Ti-1Si by increasing cavity nucleation. 11 refs., 11 figs., 3 tabs

  7. Consolidation effects on tensile properties of an elemental Al matrix composite

    Energy Technology Data Exchange (ETDEWEB)

    Tang, F. [Building 4515, MS 6064, Metals and Ceramics Division, Oak Ridge National Lab, Oak Ridge, TN 37831 (United States)]. E-mail: tangf@ornl.gov; Meeks, H. [Ceracon Inc., 5150 Fairoaks Blvd. 01-330, Carmichael, CA 95628 (United States); Spowart, J.E. [UES Incorporated, AFRL/MLLM Building 655, 2230 Tenth St. Suite 1, Wright-Patterson AFB, OH 45433 (United States); Gnaeupel-Herold, T. [NIST Center for Neutron Research, 100 Bureau Dr. Stop 8562, Gaithersburg, MD 20899-8562 (United States); Prask, H. [NIST Center for Neutron Research, 100 Bureau Dr. Stop 8562, Gaithersburg, MD 20899-8562 (United States); Anderson, I.E. [Materials and Engineering Physics Program, Ames Laboratory, Iowa State University, Ames, IA 50011 (United States)

    2004-11-25

    In a simplified composite design, an unalloyed Al matrix was reinforced by spherical Al-Cu-Fe alloy particles (30 vol.%), using either commercial purity (99.7%) or high purity (99.99%) fine powders (diameter < 10 {mu}m). This composite material was consolidated by either vacuum hot pressing (VHP) or quasi-isostatic forging. The spatial distribution of reinforcement particles in both VHP and forged samples was shown to be almost the same by quantitative characterization with a multi-scale area fraction analysis technique. The tensile properties of all composite samples were tested and the forged materials showed significantly higher strength, while the elastic modulus values of all composite materials were close to the upper bound of theoretical predictions. Neutron diffraction measurements showed that there were high compressive residual stresses in the Al matrix of the forged samples and relatively low Al matrix residual stresses (predominantly compressive) in the VHP samples. By tensile tests and neutron diffraction measurements of the forged samples after annealing, it was shown that the high compressive residual stresses in the Al matrix were relieved and that tensile strength was also reduced to almost the same level as that of the VHP samples. Therefore, it was deduced that increased compressive residual stresses and enhanced dislocation densities in the forged composites raised the tensile strength to higher values than those of the VHP composites.

  8. Microstructural evolution and tensile properties of Sn-Ag-Cu mixed with Sn-Pb solder alloys

    Energy Technology Data Exchange (ETDEWEB)

    Wang Fengjiang [Department of Materials Science and Engineering and Materials Research Center, Missouri University of Science and Technology, Rolla, MO 65401 (United States); O' Keefe, Matthew [Department of Materials Science and Engineering and Materials Research Center, Missouri University of Science and Technology, Rolla, MO 65401 (United States)], E-mail: mjokeefe@mst.edu; Brinkmeyer, Brandon [Department of Materials Science and Engineering and Materials Research Center, Missouri University of Science and Technology, Rolla, MO 65401 (United States)

    2009-05-27

    The effect of incorporating eutectic Sn-Pb solder with Sn-3.0Ag-0.5Cu (SAC) Pb-free solder on the microstructure and tensile properties of the mixed alloys was investigated. Alloys containing 100, 75, 50, 25, 20, 15, 10, 5 and 0 wt% SAC, with the balance being Sn-37Pb eutectic solder alloy, were prepared and characterized. Optical and scanning electron microscopy were used to analyze the microstructures while 'mini-tensile' test specimens were fabricated and tested to determine mechanical properties at the mm length scale, more closely matching that of the solder joints. Microstructural analysis indicated that a Pb-rich phase formed and was uniformly distributed at the boundary between the Sn-rich grains or between the Sn-rich and the intermetallic compounds in the solder. Tensile results showed that mixing of the alloys resulted in an increase in both the yield and the ultimate tensile strength compared to the original solders, with the 50% SAC-50% Sn-Pb mixture having the highest measured strength. Initial investigations indicate the formation and distribution of a Pb-rich phase in the mixed solder alloys as the source of the strengthening mechanism.

  9. Measurements of the tensile and compressive properties of micro-concrete used in the Winfrith missile impact experiments

    International Nuclear Information System (INIS)

    Wilson, P.A.

    1982-10-01

    Tests to determine the tensile and compressive properties of a micro-concrete mix are described. The material is a nominally 40MPa ultimate compressive strength concrete used in impact tests with scale models in the prediction of responses in prototype concrete structures. Compressive tests were intended to give complete stress-strain relationships beyond initial failure. Tensile properties were measured by the Brazilian splitting technique and direct tension dog-bone specimens for comparison reasons. (U.K.)

  10. Tensile creep of beta phase zircaloy-2

    International Nuclear Information System (INIS)

    Burton, B.; Reynolds, G.L.; Barnes, J.P.

    1977-08-01

    The tensile creep and creep rupture properties of beta-phase zircaloy-2 are studied under vacuum in the temperature and stress range 1300-1550 K and 0.5-2 MN/m 2 . The new results are compared with previously reported uniaxial and biaxial data. A small but systematic difference is noted between the uniaxial and biaxial creep data and reasons for this discrepancy are discussed. (author)

  11. The Effect of Artificial Aging on the Tensile Properties of Alclad 24S-T and 24S-T Aluminum Alloy

    Science.gov (United States)

    Kotanchik, Joseph N.; Woods, Walter; Zender, George W.

    1943-01-01

    An experimental study was made to determine the effect of artificial aging on the tensile properties of alclad 24S-T and 24S-T aluminum-alloy sheet material. The results of the tests show that certain combinations of aging time and temperature cause a marked increase in the yield strength and a small increase in the ultimate strength; these increases are accompanied by a very large decrease in elongation. A curve is presented that shows the maximum yield strengths that can be obtained by aging this material at various combinations of time and temperature. The higher values of yield stress are obtained in material aged at relatively longer times and lower temperatures.

  12. Mechanical properties and fracture behaviour of ODS steel friction stir welds at variable temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Dawson, H., E-mail: huwdawson@gmail.com [School of Materials, University of Manchester, Manchester M13 9PL (United Kingdom); Serrano, M.; Hernandez, R. [Structural Materials Division, Technology Department, CIEMAT, Avda de la Complutense 40, 28040 Madrid (Spain); Cater, S. [Friction and Forge Processes Department, Joining Technologies Group, TWI Technology Centre (Yorkshire), Advanced Manufacturing Park, Wallis Way, Catcliffe, Rotherham S60 5TZ (United Kingdom); Jimenez-Melero, E. [School of Materials, University of Manchester, Manchester M13 9PL (United Kingdom)

    2017-05-02

    We have assessed the microstructure and the temperature-dependent mechanical behaviour of five bead-on-plate friction stir welds of Oxide Dispersion Strengthened (ODS) steel, produced using systematic changes to the tool rotation and traverse speed. Friction stir welding can potentially retain the fine dispersion of nanoparticles, and therefore also the high-temperature strength and radiation damage resistance of these materials. Tensile testing was carried out on the MA956 base material at a range of temperatures, from room temperature up to 750 °C. The mechanical properties of the welds were investigated via tensile testing at room temperature and at 500 °C, together with micro-hardness testing. The welds exhibited similar strength and ductility to the base material at both testing temperatures as welding caused a partial loss of particle strengthening, alongside an increase in grain boundary strengthening due to a greatly refined grain size in the stir zones. The micro-hardness data revealed a trend of increasing hardness with increasing tool traverse speed or decreasing rotation speed. This was attributed to the smaller grain size and lower nanoparticle number density in the welds created with these parameters. At 500 °C, the yield stress and ultimate tensile stress of the base material and the welds decreased, due to a progressive reduction in both the Orowan-type particle strengthening and the grain boundary strengthening.

  13. Effect of pressing temperature on the mechanical properties of waste styrofoam filled sawdust composite

    Science.gov (United States)

    Nasution, H.; Harahap, H.; Riani, R.; Pelawi, A. I.

    2018-02-01

    This study has investigated the effect of pressing temperature on mechanical properties of waste styrofoam composite filled with sawdust. The waste styrofoam as the matrix was mixed with sawdust as filler and maleic anhydride (6%wt) as a compatibilizer. The weight fraction ratio between matrix and filler 70:30 (wt) and wood fiber size of 100 mesh were conducted. The pressing temperatures were investigated using a hot press with temperatures varied viz. 120, 130, 150, and 170 °C. Surface modification was applied to sawdust to diminish its polarity so that it could be compatible with the non-polar waste styrofoam matrix. Composites were evaluated using Instron and impact tester machine to investigate the tensile strength and impact strength of the material, respectively. The result indicated that tensile strength has decreased with the increase of pressing temperature where the largest tensile strength is at 130 °C of 33 MPa. The same trend has occurred on impact strength, where the value has reached of 300 J/cm2 on pressing temperature of 130 °C. From scanning electron microscopy (SEM) analysis it is also confirmed that during impact test, the resistance of the composite which has been pressed at the temperature of 130 °C have given better morphology than the composite at 170 °C.

  14. Die-cast of a hypo-eutectic AL-SI alloy: influence of injection temperature on microstructure and mechanical properties

    International Nuclear Information System (INIS)

    Santos, Silvano Leal dos; Santos, Sydney Ferreira

    2014-01-01

    Die-casting is widely used for manufacturing light alloy components for automotive industry. Among others, hypo-eutectic Al-Si alloys are currently processed by die-casting. To obtain high quality die-cast components, a better understanding on the correlations between processing parameters, microstructures, and mechanical properties are of utmost importance. In this study, we investigate the effect of injection temperature of liquid metal on the microstructure and mechanical properties of Al-Si alloy EN AC 46000 (DIN designation). The injection temperatures were 579, 589, 643, and 709 deg C. As-cast components had their microstructures analyzed by X-ray diffraction, optical and scanning electron microscopy, and X-ray energy dispersive spectroscopy. The mechanical properties were examined by micro-hardness and tensile tests. It was observed that the ultimate tensile strength slightly increased with the increase of injection temperature. The same trend was observed for micro-hardness. The amount of porosity in the samples varies in a small amount for different injection temperatures. On the other hand, the microstructure of the alloys seems more refined for higher temperatures of injection. This refinement in microstructure might play a major role on the mechanical properties of the Al-Si die-cast alloy. (author)

  15. Mechanical properties of aluminium-uranium alloy and aluminium commercially pure at several temperatures

    International Nuclear Information System (INIS)

    Quadros, N.F. de.

    1976-01-01

    The mechanical properties of Ai-U (18,4 wt %) alloy with and without heat treatment were determined, and they were compared with the mechanical properties of aluminum alloy of commercial purity, AI-1100, at tempiratures of 25, 500, 550 and 600 0 C, the changes of both the yield point stress and the ultimate tensile strength as a function of temperature may be described through two emperical relationships. A fractography study was also made [pt

  16. Investigation and microstructural analyses of massive LSP impacts with coverage area on crack initiation location and tensile properties of AM50 magnesium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Luo, K.Y.; Wang, C.Y. [School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013 (China); Sun, G.F. [School of Mechanical Engineering, Southeast University, Nanjing 211189 (China); Cui, C.Y.; Sheng, J. [School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013 (China); Lu, J.Z., E-mail: blueesky2005@163.com [School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013 (China)

    2016-01-05

    The influence of massive laser shock peening (LSP) impacts with coverage area on tensile properties of AM50 magnesium alloy was investigated using MTS880-10 servo-hydraulic material testing machine system. Microstructure in the surface layer and fracture morphologies of as-machined and LSPed tensile specimens were also characterized and analyzed by scanning electron microscopy (SEM), transmission electron microscopy (TEM) and cross-sectional optical microscopy (OM). Special attention is paid to the crack initiation location as a function of LSPed coverage area in the gauge part of tensile specimen. Experimental results and analysis indicate that coverage area significantly influenced tensile properties of the tensile specimen. In addition, the grain refinement process in the top surface layer of AM50 magnesium alloy caused by massive LSP impacts is presented. Furthermore, the underlying influence mechanism of LSPed coverage area on tensile properties and crack initiation location of tensile specimen was clearly revealed.

  17. Investigation and microstructural analyses of massive LSP impacts with coverage area on crack initiation location and tensile properties of AM50 magnesium alloy

    International Nuclear Information System (INIS)

    Luo, K.Y.; Wang, C.Y.; Sun, G.F.; Cui, C.Y.; Sheng, J.; Lu, J.Z.

    2016-01-01

    The influence of massive laser shock peening (LSP) impacts with coverage area on tensile properties of AM50 magnesium alloy was investigated using MTS880-10 servo-hydraulic material testing machine system. Microstructure in the surface layer and fracture morphologies of as-machined and LSPed tensile specimens were also characterized and analyzed by scanning electron microscopy (SEM), transmission electron microscopy (TEM) and cross-sectional optical microscopy (OM). Special attention is paid to the crack initiation location as a function of LSPed coverage area in the gauge part of tensile specimen. Experimental results and analysis indicate that coverage area significantly influenced tensile properties of the tensile specimen. In addition, the grain refinement process in the top surface layer of AM50 magnesium alloy caused by massive LSP impacts is presented. Furthermore, the underlying influence mechanism of LSPed coverage area on tensile properties and crack initiation location of tensile specimen was clearly revealed.

  18. Tensile Mechanical Properties and Failure Modes of a Basalt Fiber/Epoxy Resin Composite Material

    Directory of Open Access Journals (Sweden)

    Jingjing He

    2018-01-01

    Full Text Available Uniaxial tensile tests of basalt fiber/epoxy (BF/EP composite material with four different fiber orientations were conducted under four different fiber volume fractions, and the variations of BF/EP composite material failure modes and tensile mechanical properties were analyzed. The results show that when the fiber volume fraction is constant, the tensile strength, elastic modulus, and limiting strain of BF/EP composite material all decrease with increasing fiber orientation angle. When the fiber orientation angle is constant, the tensile strength, elastic modulus, and limiting strain of BF/EP composite material all increase with increasing fiber volume fraction. A certain degree of fiber clustering appears in the epoxy resin when the basalt fiber volume fraction is >1.2%. The fiber equidistribution coefficient and clustering fiber content were used to characterize the basalt fiber clustering effect. With the increase of fiber volume fraction, the clustering fiber content gradually increased, but the fiber equidistribution coefficient decreased. Meanwhile, based on Tsai theory, a geometric model and a tensile mechanical model of the clustering fiber are established. By considering the fiber clustering effect, the BF/EP composite material tensile strength is calculated, and the calculated values are close to the experimental results.

  19. Temperature Effects on the Mechanical Properties of Candidate SNS Target Container Materials after Proton and Neutron Irradiation; TOPICAL

    International Nuclear Information System (INIS)

    Byun, T.S.

    2001-01-01

    This report presents the tensile properties of EC316LN austenitic stainless steel and 9Cr-2WVTa ferritic/martensitic steel after 800 MeV proton and spallation neutron irradiation to doses in the range 0.54 to 2.53 dpa. Irradiation temperatures were in the range 30 to 100 C. Tensile testing was performed at room temperature (20 C) and 164 C to study the effects of test temperature on the tensile properties. Test materials displayed significant radiation-induced hardening and loss of ductility due to irradiation. The EC316LN stainless steel maintained notable strain-hardening capability after irradiation, while the 9Cr-2WVTa ferritic/martensitic steel posted negative strain hardening. In the EC316LN stainless steel, increasing the test temperature from 20 C to 164 C decreased the strength by 13 to 18% and the ductility by 8 to 36%. The tensile data for the EC316LN stainless steel irradiated in spallation conditions were in line with the values in a database for 316 stainless steels for doses up to 1 dpa irradiated in fission reactors at temperatures below 200 C. However, extra strengthening induced by helium and hydrogen contents is evident in some specimens irradiated to above about 1 dpa. The effect of test temperature for the 9Cr-2WVTa ferritic/martensitic steel was less significant than for the EC316LN stainless steel. In addition, strain-hardening behaviors were analyzed for EC316LN and 316L stainless steels. The strain-hardening rate of the 316 stainless steels was largely dependent on test temperature. It was estimated that the 316 stainless steels would retain more than 1% true stains to necking at 164 C after irradiation to 5 dpa. A calculation using reduction of area (RA) measurements and stress-strain data predicted positive strain hardening during plastic instability

  20. Tensile properties of a boron/nitrogen-doped carbon nanotube–graphene hybrid structure

    Directory of Open Access Journals (Sweden)

    Kang Xia

    2014-03-01

    Full Text Available Doping is an effective approach that allows for the intrinsic modification of the electrical and chemical properties of nanomaterials. Recently, a graphene and carbon nanotube hybrid structure (GNHS has been reported, which extends the excellent properties of carbon-based materials to three dimensions. In this paper, we carried out a first-time investigation on the tensile properties of the hybrid structures with different dopants. It is found that with the presence of dopants, the hybrid structures usually exhibit lower yield strength, Young’s modulus, and earlier yielding compared to that of a pristine hybrid structure. For dopant concentrations below 2.5% no significant reduction of Young’s modulus or yield strength could be observed. For all considered samples, the failure is found to initiate at the region where the nanotubes and graphene sheets are connected. After failure, monatomic chains are normally observed around the failure region. Dangling graphene layers without the separation of a residual CNT wall are found to adhere to each other after failure with a distance of about 3.4 Å. This study provides a fundamental understanding of the tensile properties of the doped graphene–nanotube hybrid structures, which will benefit the design and also the applications of graphene-based hybrid materials.

  1. Dynamic tensile loading improves the functional properties of mesenchymal stem cell-laden nanofiber-based fibrocartilage.

    Science.gov (United States)

    Baker, Brendon M; Shah, Roshan P; Huang, Alice H; Mauck, Robert L

    2011-05-01

    Fibrocartilaginous tissues such as the meniscus serve critical load-bearing roles, relying on arrays of collagen fibers to resist tensile loads experienced with normal activity. As these structures are frequently injured and possess limited healing capacity, there exists great demand for tissue-engineered replacements. Toward recreating the structural features of these anisotropic tissues in vitro, we employ scaffolds composed of co-aligned nanofibers that direct mesenchymal stem cell (MSC) orientation and the formation of organized extracellular matrix (ECM). Concomitant with ECM synthesis, the mechanical properties of constructs increase with free-swelling culture, but ultimately failed to achieve equivalence with meniscal fibrocartilage. As mechanical forces are essential to the development and maintenance of musculoskeletal tissues, this work examined the effect of cyclic tensile loading on MSC-laden nanofibrous constructs. We hypothesized that loading would modulate the transcriptional behavior of MSCs, spur the deposition of ECM, and lead to enhancements in construct mechanical properties compared to free-swelling controls. Fiber-aligned scaffolds were seeded with MSCs and dynamically loaded daily in tension or maintained as nonloaded controls for 4 weeks. With mechanical stimulation, fibrous gene expression increased, collagen deposition increased, and the tensile modulus increased by 16% relative to controls. These results show that dynamic tensile loading enhances the maturation of MSC-laden aligned nanofibrous constructs, suggesting that recapitulation of the structural and mechanical environment of load-bearing tissues results in increases in functional properties that can be exploited for tissue engineering applications.

  2. Evaluation of mechanical and thermal properties of insulation materials for HTS power devices at liquid nitrogen temperature

    Energy Technology Data Exchange (ETDEWEB)

    Shin, Hyung Seop; Diaz, Mark Angelo [Dept. of Mechanical Design Engineering, Andong National University, Andong (Korea, Republic of)

    2017-06-15

    In superconducting power devices including power cables in which high temperature superconducting (HTS) tapes are utilized, a reliable electrical insulation should be achieved for its maximum performance. For an efficient design of HTS superconducting devices, a comparative evaluation of the mechanical and thermal propperties for various insulation materials at cryogenic temperatures is required. Especially, in the process of the property evaluation of the sheet-shaped insulation materials, anisotropy according to the machining direction should be considered because the mechanical and thermal properties are significantly influenced by the sample orientation. In this study, the cryogenic thermal and mechanical properties of various insulation material sheets such as PPLP, Cryoflex, Teflon, and Kapton were determined considering sample orientation. All samples tested at cryogenic temperature showed significantly higher tensile strength as compared with that of room temperature. The ultimate tensile strength at both temperature conditions significantly depended upon the sample orientation. The thermal properties of the insulation materials exhibited a slight difference among samples depending on the orientation: for the PPLP and Cryoflex, the CD orientation showed larger thermal contraction up to 77 K as compared to the MD one. MD samples in PPLP and Cryoflex showed a lower CTE and thermal contraction which made it more promising as an insulation material due to its comparable CTE with HTS CC tapes.

  3. Comparison of the biomechanical tensile and compressive properties of decellularised and natural porcine meniscus.

    Science.gov (United States)

    Abdelgaied, A; Stanley, M; Galfe, M; Berry, H; Ingham, E; Fisher, J

    2015-06-01

    Meniscal repair is widely used as a treatment for meniscus injury. However, where meniscal damage has progressed such that repair is not possible, approaches for partial meniscus replacement are now being developed which have the potential to restore the functional role of the meniscus, in stabilising the knee joint, absorbing and distributing stress during loading, and prevent early degenerative joint disease. One attractive potential solution to the current lack of meniscal replacements is the use of decellularised natural biological scaffolds, derived from xenogeneic tissues, which are produced by treating the native tissue to remove the immunogenic cells. The current study investigated the effect of decellularisation on the biomechanical tensile and compressive (indentation and unconfined) properties of the porcine medial meniscus through an experimental-computational approach. The results showed that decellularised medial porcine meniscus maintained the tensile biomechanical properties of the native meniscus, but had lower tensile initial elastic modulus. In compression, decellularised medial porcine meniscus generally showed lower elastic modulus and higher permeability compared to that of the native meniscus. These changes in the biomechanical properties, which ranged from less than 1% to 40%, may be due to the reduction of glycosaminoglycans (GAG) content during the decellularisation process. The predicted biomechanical properties for the decellularised medial porcine meniscus were within the reported range for the human meniscus, making it an appropriate biological scaffold for consideration as a partial meniscus replacement. Copyright © 2015 The Authors. Published by Elsevier Ltd.. All rights reserved.

  4. Developing of tensile property database system

    International Nuclear Information System (INIS)

    Park, S. J.; Kim, D. H.; Jeon, J.; Ryu, W. S.

    2002-01-01

    The data base construction using the data produced from tensile experiment can increase the application of test results. Also, we can get the basic data ease from database when we prepare the new experiment and can produce high quality result by compare the previous data. The development part must be analysis and design more specific to construct the database and after that, we can offer the best quality to customers various requirements. In this thesis, the tensile database system was developed by internet method using JSP(Java Server pages) tool

  5. Assessment of models predicting irradiation effects on tensile properties of reactor pressure vessel steels

    International Nuclear Information System (INIS)

    Pineau, L.; Landron, C.

    2015-01-01

    In this paper, an analysis of tensile data acquired as part of the French Reactor Vessel Surveillance Program (RVSP) is produced. This program contains amongst other mechanical tests, tensile tests at 20 and 300 C degrees on non irradiated base metals and at 300 C degrees only on irradiated materials. It shows that irradiation leads to an increase in the yield strength and a decrease in the strain hardening. The exploitation of tensile results has permitted to express a relationship between yield strength increase measured and fluence value, as well as between strain hardening decrease and yield strength evolution. The use of these relations in the aim at predicting evolution of tensile properties with irradiation has then permitted to propose a methodology to model entire stress-strain curves of irradiated base metal only based on the non irradiated stress-strain curve. These predictions were successfully compared with an experimental standard case. (authors)

  6. Effect of oxide films, inclusions and Fe on reproducibility of tensile properties in cast Al–Si–Mg alloys: Statistical and image analysis

    International Nuclear Information System (INIS)

    Eisaabadi B, G.; Davami, P.; Kim, S.K.; Varahram, N.; Yoon, Y.O.; Yeom, G.Y.

    2012-01-01

    Double oxide films (hereafter: oxides), inclusions and Fe-rich phases are known to be the most detrimental defects in cast Al–Si–Mg alloys. The effects of these defects on reproducibility of tensile properties in Al–7Si–0.35Mg alloy have been investigated in this study. Four different casting conditions (low oxide—low Fe, high oxide—low Fe, low oxide—high Fe and high oxide—high Fe) were studied. In each case, 30 tensile test samples were prepared by casting in a metallic mold and machining (total of 120 tensile test samples). Results of tensile test were analyzed by Weibull three-parameter and mixture analyses. The microstructure and fracture surface of samples were studied by optical and scanning electron microscopes. Total of 800 metallography images (200 images for each experiment) were taken and analyzed by image analysis software. Finally, the relationship between tensile properties and defects characteristics was discussed. According to the results, Fe (Fe-related phases) had larger negative impact on tensile properties of the alloy compared to oxides. On the other hand, Weibull analysis revealed that the scattering of tensile properties was mainly due to the presence of oxides in microstructure. Results of image analysis showed that the shape factor and number of pores were mainly controlled by oxides and Fe, respectively. Also, there was a clear relationship between Weibull modules of UTS and El% and shape factor of pores. Furthermore, tensile properties of the examined alloy showed strong dependence to the number of pores.

  7. Mechanical performance of carbon-epoxy laminates. Part II: quasi-static and fatigue tensile properties

    Directory of Open Access Journals (Sweden)

    José Ricardo Tarpani

    2006-06-01

    Full Text Available In Part II of this work, quasi-static tensile properties of four aeronautical grade carbon-epoxy composite laminates, in both the as-received and pre-fatigued states, have been determined and compared. Quasi-static mechanical properties assessed were tensile strength and stiffness, tenacity (toughness at the maximum load and for a 50% load drop-off. In general, as-molded unidirectional cross-ply carbon fiber (tape reinforcements impregnated with either standard or rubber-toughened epoxy resin exhibited the maximum performance. The materials also displayed a significant tenacification (toughening after exposed to cyclic loading, resulting from the increased stress (the so-called wear-in phenomenon and/or strain at the maximum load capacity of the specimens. With no exceptions, two-dimensional woven textile (fabric pre-forms fractured catastrophically under identical cyclic loading conditions imposed to the fiber tape architecture, thus preventing their residual properties from being determined.

  8. Tensile properties and microstructure of direct metal laser-sintered TI6AL4V (ELI alloy

    Directory of Open Access Journals (Sweden)

    Moletsane, M. G.

    2016-11-01

    Full Text Available Direct metal laser sintering (DMLS is an additive manufacturing technology used to melt metal powder by high laser power to produce customised parts, light-weight structures, or other complex objects. During DMLS, powder is melted and solidified track-by-track and layer-by-layer; thus, building direction can influence the mechanical properties of DMLS parts. The mechanical properties and microstructure of material produced by DMLS can depend on the powder properties, process parameters, scanning strategy, and building geometry. In this study, the microstructure, tensile properties, and porosity of DMLS Ti6Al4V (ELI horizontal samples were analysed. Defect analysis by CT scans in pre-strained samples was used to detect the crack formation mechanism during tensile testing of as-built and heat-treated samples. The mechanical properties of the samples before and after stress relieving are discussed.

  9. Influence of polypropylene fibres on the tensile strength and thermal properties of various densities of foamed concrete

    Science.gov (United States)

    Jhatial, Ashfaque Ahmed; Inn, Goh Wan; Mohamad, Noridah; Johnson Alengaram, U.; Mo, Kim Hung; Abdullah, Redzuan

    2017-11-01

    As almost half of the world’s population now lives in the urban areas, the raise in temperature in these areas has necessitated the development of thermal insulating material. Conventional concrete absorbs solar radiation during the daytime while releasing it at night causing raise in temperature in urban areas. The thermal conductivity of 2200 kg/m3 density conventional concrete is 1.6 W/mK. Higher the thermal conductivity value, greater the heat flow through the material. To reduce this heat transfer, the construction industry has turned to lightweight foamed concrete. Foamed concrete, due to its air voids, gives excellent thermal properties and sound absorption apart from fire-resistance and self-leveling properties. But due to limited studies on different densities of foamed concrete, the thermal properties are not understood properly thus limiting its use as thermal insulating material. In this study, thermal conductivity is determined for 1400, 1600 and 1800 kg/m3 densities of foamed concrete. 0.8% of Polypropylene fibres (PP) is used to reinforce the foamed concrete and improve the mechanical properties. Based upon the results, it was found that addition of PP fibres enhances the tensile strength and slightly reduced the thermal conductivity for lower densities, while the reverse affect was noticed in 1800 kg/m3 density.

  10. Tensile deformation behavior of AA5083-H111 at cold and warm temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Ozturk, Fahrettin; Toros, Serkan; Kilic, Suleyman [Nidge Univ. (Turkey). Dept. of Mechanical Engineering

    2010-09-15

    The effects of strain rate and temperature on the deformation behavior of hardened 5083-H111 aluminum magnesium alloy sheet were investigated by performing uniaxial tensile tests at various strain rates from 0.0083 to 0.16 s{sup -1} and temperatures from -100 to 300 C. Results from the prescribed test ranges indicate that the formability of this material at cold and warm temperatures is better than at room temperature. The improvement in formability at cold temperatures is principally due to the strain hardening of the material. However, the improvement at warm temperature and low strain rate is specifically due to the high strain rate sensitivity characteristic of the material. Results indicate that this alloy should be formed at temperatures higher than 200 C and at low strain rates. (orig.)

  11. Tensile properties of candidate structural materials for high power spallation sources at high helium contents

    Science.gov (United States)

    Jung, P.; Henry, J.; Chen, J.

    2005-08-01

    Low activation 9%Cr martensitic steels EUROFER97, pure tantalum, and low carbon austenitic stainless steel 316L were homogeneously implanted with helium to concentrations up to 5000 appm at temperatures from 70 °C to 400 °C. The specimens were tensile tested at room temperature and at the respective implantation temperatures. In all materials the helium caused an increased in strength and reduction in ductility, with both changes being generally larger at lower implantation and testing temperatures. After implantation some work hardening was retained in 316L and in tantalum, while it almost completely disappeared in EUROFER97. After tensile testing, fracture surfaces were analysed by scanning electron microscopy (SEM). Implantation caused reduction of necking, but up to concentrations of 2500 appm He fracture surface still showed transgranular ductile appearance. Completely brittle intergranular fracture was observed in tantalum at 9000 appm He and is also expected for EUROFER97 at this concentration, according to previous results on similar 9%Cr steels.

  12. Degradation in tensile properties of aromatic polymers by electron beam irradiation

    International Nuclear Information System (INIS)

    Sasuga, T.; Hayakawa, N.; Yoshida, K.; Hagiwara, M.

    1985-01-01

    Electron beam irradiation effects of ten kinds of polymers containing various aromatic rings linked by functional groups in the main chain (aromatic polymer) were studied with reference to change in tensile properties. The polymers studied were polyimides 'Kapton H', and 'UPILEX', polyetherimide 'ULTEM', polyamides 'A-Film' and 'APH-50 (nomex type paper)', poly-ether-ether-ketone 'PEEK', polyarylate 'U-Polymer', polysulphones 'Udel-Polysulphone' and 'PES', and modified poly(phenylene oxide) 'NORYL'. Irradiation was carried out by use of electron beam at a dose rate of 5 x 10 3 Gy s -1 at room temperature. The elongation at break was the most severely influenced by the irradiation and it decreased with increasing dose. The order of radiation resistivity which was evaluated from the dose required for the elongation to become 50% and 20% of the initial value was as follows: Polyimide > PEEK > polyamide > polyetherimide > polyarylate > polysulphone, poly(phenylene oxide). Based on the above experimental results, an order is proposed for the radiation stability of the aromatic repeating units composing the main chain. (author)

  13. Effect of strain rate and stress triaxiality on tensile behavior of Titanium alloy Ti-10-2-3 at elevated temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Bobbili, Ravindranadh, E-mail: ravindranadh@dmrl.drdo.in; Madhu, Vemuri

    2016-06-14

    In this study, Split hopkinson tension bar (SHTB) has been employed to investigate the dynamic tensile flow behavior of Ti-10-2-3 alloy at high strain rates and elevated temperatures. The combined effect of stress triaxiality, strain rate and temperature and on the tensile behavior of the alloy was evaluated. Johnson-Cook (J-C) constitutive and fracture models were developed based on high strain rate tensile data. A modified Johnson–Cook model was established and proved to have high accuracy. A comparative assessment has been done to confirm the accuracy of modified J–C model based on finite element method (FEM). The improved model provides better description on the influence of equivalent plastic strain rate and temperature on the plastic flow. The simulation results proved to be in good agreement with the experimental data. The fracture surfaces of specimens tested under various strain rates and temperatures were studied under scanning electron microscopy (SEM).

  14. Chemical resistance, void content and tensile properties of oil palm/jute fibre reinforced polymer hybrid composites

    International Nuclear Information System (INIS)

    Jawaid, M.; Khalil, H.P.S. Abdul; Bakar, A. Abu; Khanam, P. Noorunnisa

    2011-01-01

    Tri layer hybrid composites of oil palm empty fruit bunches (EFB) and jute fibres was prepared by keeping oil palm EFB as skin material and jute as the core material and vice versa. The chemical resistance, void content and tensile properties of oil palm EFB/Jute composites was investigated with reference to the relative weight of oil palm EFB/Jute, i.e. 4:1, the fibre loading was optimized and different layering pattern were investigated. It is found from the chemical resistance test that all the composites are resistant to various chemicals. It was observed that marked reduction in void content of hybrid composites in different layering pattern. From the different layering pattern, the tensile properties were slightly higher for the composite having jute as skin and oil palm EFB as core material. Scanning electron microscopy (SEM) was used to study tensile fracture surfaces of different composites.

  15. Hot Tensile and Fracture Behavior of 35CrMo Steel at Elevated Temperature and Strain Rate

    Directory of Open Access Journals (Sweden)

    Zhengbing Xiao

    2016-08-01

    Full Text Available To better understand the tensile deformation and fracture behavior of 35CrMo steel during hot processing, uniaxial tensile tests at elevated temperatures and strain rates were performed. Effects of deformation condition on the flow behavior, strain rate sensitivity, microstructure transformation, and fracture characteristic were characterized and discussed. The results indicated that the flow stress was sensitive to the deformation condition, and fracture occurs immediately after the peak stress level is reached, especially when the temperature is low or the strain rate is high. The strain rate sensitivity increases with the deformation temperature, which indicates that formability could improve at high temperatures. Photographs showing both the fracture surfaces and the matrix near the fracture section indicated the ductile nature of the material. However, the fracture mechanisms varied according to the deformation condition, which influences the dynamic recrystallization (DRX condition, and the DRX was accompanied by the formation of voids. For samples deformed at high temperatures or low strain rates, coalescence of numerous voids formed in the recrystallized grains is responsible for fracture, while at high strain rates or low temperatures, the grains rupture mainly by splitting because of cracks formed around the inclusions.

  16. On the effect of TiC particles on the tensile properties and on the intrinsic two way effect of NiTi shape memory alloys produced by powder metallurgy

    International Nuclear Information System (INIS)

    Johansen, K.; Voggenreiter, H.; Eggeler, G.

    1999-01-01

    The present study investigates the tensile properties of a nickel titanium (NiTi) shape memory alloy (SMA) produced by powder metallurgy (PM) with and without TiC-particles. It discusses the effect of the addition of particles on the mechanical behavior in tension and studies the intrinsic two way effect (ε 2W ) after thermomechanical training. Special emphasis is placed on the stability of ε 2W after subsequent thermal cycling. The results are discussed on the basis of an analysis of the thermomechanical data and microstructural results. The present study shows that the PM route can produce NiTi SMAs with tensile properties which match those of materials produced by classical ingot metallurgy. Adding TiC particles to NiTi SMAs alters the phase transition temperatures (PTTs) and affects the SMA performance. Adding more than ten volume percent TiC particles results in early and brittle rupture during tensile loading. (orig.)

  17. Section thickness-dependent tensile properties of squeeze cast magnesium alloy AM60

    Directory of Open Access Journals (Sweden)

    Xuezhi Zhang

    2012-05-01

    Full Text Available The development of alternative casting processes is essential for the high demand of light weight magnesium components to be used in the automotive industry, which often contain different section thicknesses. Squeeze casting with its inherent advantages has been approved for the capability of minimizing the gas porosity in magnesium alloys. For advanced engineering design of light magnesium automotive applications, it is critical to understand the effect of section thickness on mechanical properties of squeeze cast magnesium alloys. In this study, magnesium alloy AM60 with different section thicknesses of 6, 10 and 20 mm squeeze cast under an applied pressure of 30 MPa was investigated. The prepared squeeze cast AM60 specimens were tensile tested at room termperature. The results indicate that the mechanical properties including yield strength (YS, ultimate tensile strength (UTS and elongation (A decrease with an increase in section thickness of squeeze cast AM60. The microstructure analysis shows that the improvement in the tensile behavior of squeeze cast AM60 is primarily attributed to the low-gas porosity level and fine grain strucuture which result from the variation of cooling rate of different section thickness. The numerical simulation (Magmasoft? was employed to determine the solidification rates of each step, and the simulated results show that the solidification rate of the alloy decreases with an increase in the section thickness. The computed solidification rates support the experimental observation on grain structural development.

  18. Tensile Properties and Integrity of Clean Room and Low-Modulus Disposable Nitrile Gloves: A Comparison of Two Dissimilar Glove Types

    Science.gov (United States)

    Phalen, Robert N.; Wong, Weng kee

    2012-01-01

    Background: The selection of disposable nitrile exam gloves is complicated by (i) the availability of several types or formulations, (ii) product variability, and (iii) an inability of common quality control tests to detect small holes in the fingers. Differences in polymer formulation (e.g. filler and plasticizer/oil content) and tensile properties are expected to account for much of the observed variability in performance. Objectives: This study evaluated the tensile properties and integrity (leak failure rates) of two glove choices assumed to contain different amounts of plasticizers/oils. The primary aims were to determine if the tensile properties and integrity differed and if associations existed among these factors. Additional physical and chemical properties were evaluated. Methods: Six clean room and five low-modulus products were evaluated using the American Society for Testing and Materials Method D412 and a modified water-leak test to detect holes capable of passing a virus or chemical agent. Results: Significant differences in the leak failure rates and tensile properties existed between the two glove types (P ≤ 0.05). The clean room gloves were about three times more likely to have leak failures (chi-square; P = 0.001). No correlation was observed between leak failures and tensile properties. Solvent extract, an indication of added plasticizer/oil, was not associated with leak failures. However, gloves with a maximum modulus gloves were a better choice for protection against aqueous chemical or biological penetration. The observed variability between glove products indicated that glove selection cannot rely solely on glove type or manufacturer labeling. Measures of modulus and AD may aid in the selection process, in contrast with common measures of tensile strength and elongation at break. PMID:22201179

  19. Enhancing Effect of Glycerol on the Tensile Properties of Bombyx mori Cocoon Sericin Films

    Directory of Open Access Journals (Sweden)

    Liangjun Zhu

    2011-05-01

    Full Text Available An environmental physical method described herein was developed to improve the tensile properties of Bombyx mori cocoon sericin films, by using the plasticizer of glycerol, which has a nontoxic effect compared with other chemical crosslinkers. The changes in the tensile characteristics and the structure of glycerolated (0–40 wt% of glycerol sericin films were investigated. Sericin films, both in dry and wet states, showed enhanced tensile properties, which might be regulated by the addition of different concentrations of glycerol. The introduction of glycerol results in the higher amorphous structure in sericin films as evidenced by analysis of attenuated total reflection Fourier transform infrared (ATR-FTIR spectra, thermogravimetry (TGA and differential scanning calorimetry (DSC curves. Scanning Electron Microscopy (SEM observation revealed that glycerol was homogeneously blended with sericin molecules when its content was 10 wt%, while a small amount of redundant glycerol emerged on the surface of sericin films when its content was increased to 20 wt% or higher. Our results suggest that the introduction of glycerol is a novel nontoxic strategy which can improve the mechanical features of sericin-based materials and subsequently promote the feasibility of its application in tissue engineering.

  20. Structure and tensile properties of Fe-Cr model alloy strengthened by nano-scale NbC particles derived from controlled crystallization of Nb-rich clusters

    Energy Technology Data Exchange (ETDEWEB)

    Dai, Lei [College of Materials and Chemical Engineering, Three Gorges University, Yichang 443002 (China); Guo, Qianying [State Key Lab of Hydraulic Engineering Simulation and Safety, School of Material Science and Engineering, Tianjin University, Tianjin 300354 (China); Liu, Yongchang, E-mail: licmtju@163.com [State Key Lab of Hydraulic Engineering Simulation and Safety, School of Material Science and Engineering, Tianjin University, Tianjin 300354 (China); Yu, Liming; Li, Huijun [State Key Lab of Hydraulic Engineering Simulation and Safety, School of Material Science and Engineering, Tianjin University, Tianjin 300354 (China)

    2016-09-30

    This article describes the microstructural evolution and tensile properties of Fe-Cr model alloy strengthened by nano-scale NbC particles. According to the results obtained from X-ray diffraction and transmission electron microscope with Energy Dispersive Spectrometer, the bcc ultrafine grains and the disordered phase of Nb-rich nano-clusters were observed in the milled powders. The hot pressing (HP) resulted in a nearly equiaxed ferritic grains and dispersed nano-scale NbC (~8 nm) particles. The microstructure studies reveal that the formation of NbC nanoparticles is composed of nucleation and growth of the Nb-rich nano-clusters involving diffusion of their component. At room temperature the material exhibits an ultimate tensile strength of 700 MPa, yield strength of 650 MPa, and total elongation of 11.7 pct. The fracture surface studies reveal that a typical ductile fracture mode has occurred during tensile test.

  1. Tensile properties of a titanium modified austenitic stainless steel and the weld joints after neutron irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Shiba, K.; Ioka, I.; Jitsukawa, S.; Hamada, A.; Hishinuma, A. [and others

    1996-10-01

    Tensile specimens of a titanium modified austenitic stainless steel and its weldments fabricated with Tungsten Inert Gas (TIG) and Electron Beam (EB) welding techniques were irradiated to a peak dose of 19 dpa and a peak helium level of 250 appm in the temperature range between 200 and 400{degrees}C in spectrally tailored capsules in the Oak Ridge Research Reactor (ORR) and the High Flux Isotope Reactor (HFIR). The He/dpa ratio of about 13 appm/dpa is similar to the typical helium/dpa ratio of a fusion reactor environment. The tensile tests were carried out at the irradiation temperature in vacuum. The irradiation caused an increase in yield stress to levels between 670 and 800 MPa depending on the irradiation temperature. Total elongation was reduced to less than 10%, however the specimens failed in a ductile manner. The results were compared with those of the specimens irradiated using irradiation capsules producing larger amount of He. Although the He/dpa ratio affected the microstructural change, the impact on the post irradiation tensile behavior was rather small for not only base metal specimens but also for the weld joint and the weld metal specimens.

  2. Mechanical properties of Ni-base superalloys in high temperature steam environments

    International Nuclear Information System (INIS)

    Jang, Changheui; Kim, Donghoon; Sah, Injin; Lee, Ho Jung

    2015-01-01

    The effects of environmental damages on the mechanical properties of Ni-base superalloys, Alloy 617 and Haynes 230, were evaluated for VHTR-HTSE applications. Tensile tests were carried out at room temperature after ageing at 900 deg. C in vacuum, steam, and steam + 20 vol.% H2 environments up to 3 000 h. Also, creep rupture test were performed in air, steam, and steam + 20 vol.% H2 environments. The degradations such as oxidation, decarburization, and redistribution of carbides were studied in view of the interaction of materials with the environment. During the long-term ageing at 900 deg. C in vacuum, secondary phases such as M23C6 and M6C were precipitated and coarsened, which caused increase in tensile strength and decrease in ductility. For the specimens aged in steam environments, surface and internal oxides acted as preferential sites for crack initiation and consequently, decreased the tensile and creep strength. Also, the formation of decarburization region resulted in glide plane failure during tensile test and reduction in creep rupture life due to grain boundary migration and recrystallisation. During creep tests, tensile stress caused the crack and void formation in oxide layer. Consequently, fast diffusion of oxidant occurred and environmental damage were accelerated. Among the test conditions, such environmental damage was much severe in steam environments. (authors)

  3. Effects of Pouring Temperature and Electromagnetic Stirring on Porosity and Mechanical Properties of A357 Aluminum Alloy Rheo-Diecasting

    Science.gov (United States)

    Guo, An; Zhao, Junwen; Xu, Chao; Li, Hu; Han, Jing; Zhang, Xu

    2018-05-01

    Semisolid slurry of A357 aluminum alloy was prepared using a temperature-controllable electromagnetic stirrer and rheo-diecast at different temperatures. The effects of pouring temperature and electromagnetic stirring (EMS) on the porosity in rheo-diecast samples, as well as the relation between porosity and mechanical properties, were investigated. The results show that pouring temperature and EMS had minor influences on rheo-diecast microstructure but marked influence on the porosity. With decreasing slurry pouring temperature, the porosity decreased first and then increased, whereas the maximum pore ratio (ratio of shape factor to diameter of the largest pore) increased first and then decreased. The maximum pore ratio determines the level of tensile strength and elongation, and higher mechanical properties can be obtained with smaller and rounder pores in samples. The mechanical properties of the rheo-diecast samples increased linearly with increasing maximum pore ratio. The maximum pore ratio was 1.43 µm-1, and the minimum porosity level was 0.37% under EMS condition for the rheo-diecast samples obtained at a pouring temperature of 608 °C. With this porosity condition, the maximum tensile strength and elongation were achieved at 274 MPa and 4.9%, respectively. It was also revealed that EMS improves mechanical properties by reduction in porosity and an increase in maximum pore ratio.

  4. Elastic and strength properties of Hanford concrete mixes at room and elevated temperatures

    International Nuclear Information System (INIS)

    Abrams, M.S.; Gillen, M.; Campbell, D.H.

    1979-03-01

    The effects of long-term exposure to elevated temperatures on the physical properties of concrete mixes used in Hanford radioactive waste storage tanks were determined. Temperature had a significant effect on the elastic modulus of concretes. Poisson's ratio determined by the sonic method remained relatively constant. The splitting tensile strength increased rapidly up to 190 days of age. Then strength decreased to about 350 days and either leveled off or increased from that point on. Compressive strength data were erratic

  5. Tensile Properties of Open Cell Ceramic Foams

    Czech Academy of Sciences Publication Activity Database

    Dlouhý, Ivo; Řehořek, Lukáš; Chlup, Zdeněk

    2009-01-01

    Roč. 409, - (2009), s. 168-175 ISSN 1013-9826. [Fractography of Advanced Ceramics /3./. Stará Lesná, 07.09.2008-10.09.2008] R&D Projects: GA ČR(CZ) GA106/06/0724; GA ČR GD106/05/H008 Institutional research plan: CEZ:AV0Z20410507 Keywords : tensile test * ceramics foam * open porosity * tensile strength Subject RIV: JH - Ceramics, Fire-Resistant Materials and Glass

  6. Examining the influence of injection speed and mould temperature on the tensile strength of polypropylene and ABS

    DEFF Research Database (Denmark)

    Aarøe, Esben Raahede; Blaimschein, Karl Stephan; Deker, Lasse

    This report is the final task of course “41738 Experimental Plastics Technology” in the three weeks period of June 2009 at DTU, IPL. The aim of this project has been to investigate the ultimate tensile strength behaviour of two different polymers, with different structural composition, by varying...... the injection speed and the mold temperature independently while keeping all other process parameters fixed. In addition the scaling from production of large to small geometries has been investigated by doing two parallel productions and test setups of respectively injection moulded and micro injection moulded...... specimens. After production and tensile testing the specimens were examined with a microscope to underpin conclusions from the tensile test data. It was experienced that the injection speed in general increased the the tensile strength by orienting the polymeric-chains lengthwise in the specimens and thus...

  7. Material properties of oxide dispersion strengthened (ODS) ferritic steels for core materials of FBR. Tensile properties of sodium exposed and nickel diffused materials

    International Nuclear Information System (INIS)

    Kato, Shoichi; Yoshida, Eiichi

    2002-12-01

    An oxide dispersion strengthened (ODS) ferritic steel is candidate for a long-life core materials of future FBR, because of good swelling resistance and high creep strength. In this study, tensile tests were carried out the long-term extrapolation of sodium environmental effects on the mechanical properties of ODS steels. The tested heats of materials are M93, M11 and F95. The specimens were pre-exposed to sodium for 1,000 and 3,000 hours under non-stress conditions. The pre-exposure to sodium was conducted using a sodium test loop constituted by austenitic steels. For the conditions of sodium exposure test, the sodium temperature was 650 and 700degC, the oxygen concentration in sodium was about 1 ppm and sodium flow rate on the surface of specimen was less than 1x10 -4 m/seconds (nearly static). Further the specimen with the nickel diffused was prepared, which is simulate to nickel diffusing through sodium from the surface of structural stainless steels. The main results obtained were as follows; (1) The tensile strength and the fracture elongation after sodium exposure (maximum 3,000 hours) were same as that of as-received materials. If was considered that the sodium environmental effect is negligible under the condition of this study. (2) Tensile properties of nickel diffused specimens were slightly lower than that of the as-received specimens, but it remains equal to that of thermal aging specimens. (3) The change in microstructure such as a degraded layer was observed on the surface of nickel diffused specimen. In the region of the degraded layer, phase transformations from the α-phase to the γ-phase were recognized. But, the microscopic oxide particles were observed same as that of α-phase base metal. (author)

  8. Low temperature tensile deformation and acoustic emission signal characteristics of AISI 304LN stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Barat, K.; Bar, H.N. [Material Science and Technology Division, CSIR-National Metallurgical Laboratory, Jamshedpur 831007 (India); Mandal, D. [Material Processing and Technology Division, CSIR-National Metallurgical Laboratory, Jamshedpur 831007 (India); Roy, H., E-mail: himadri9504@gmail.com [NDT and Metallurgy Group, CSIR-Central Mechanical Engineering Research Institute, Durgapur 713209 (India); Sivaprasad, S.; Tarafder, S. [Material Science and Technology Division, CSIR-National Metallurgical Laboratory, Jamshedpur 831007 (India)

    2014-03-01

    This investigation examines low temperature tensile deformation behavior of AISI 304LN stainless steel along with synergistic analysis of acoustic emission signals. The tensile tests are done at a range of temperatures starting from 283 K till 223 K. The fracture surfaces of the broken specimens are investigated using scanning electron microscope. The amount of deformation induced martensite is measured using a feritscope. The obtained results reveal that with decrease in test temperature, both strength and ductility increase. The increase in strength and ductility with decreasing temperature is explained in terms of void morphologies and formation of deformation induced martensite. The rapid increment in strength and ductility at 223 K is associated with the burst of martensitic transformation at that temperature; which has been clarified from acoustic emission signals. An additional initiative has been taken to model the evolution of martensite formation from the observed cumulative emission counts using a non linear logarithmic functional form. The fitted curves from the recorded acoustic emission cumulative count data are found to be better correlated compared to earlier obtained results. However, at 223 K normal non-linear logarithmic fit is not found suitable due to presence of burst type signals at intervals, therefore; piecewise logarithmic function to model acoustic emission bursts is proposed.

  9. Effects of Temperature and Strain Rate on Tensile Deformation Behavior of 9Cr-0.5Mo-1.8W-VNb Ferritic Heat-Resistant Steel

    Science.gov (United States)

    Guo, Xiaofeng; Weng, Xiaoxiang; Jiang, Yong; Gong, Jianming

    2017-09-01

    A series of uniaxial tensile tests were carried out at different strain rate and different temperatures to investigate the effects of temperature and strain rate on tensile deformation behavior of P92 steel. In the temperature range of 30-700 °C, the variations of flow stress, average work-hardening rate, tensile strength and ductility with temperature all show three temperature regimes. At intermediate temperature, the material exhibited the serrated flow behavior, the peak in flow stress, the maximum in average work-hardening rate, and the abnormal variations in tensile strength and ductility indicates the occurrence of DSA, whereas the sharp decrease in flow stress, average work-hardening rate as well as strength values, and the remarkable increase in ductility values with increasing temperature from 450 to 700 °C imply that dynamic recovery plays a dominant role in this regime. Additionally, for the temperature ranging from 550 to 650 °C, a significant decrease in flow stress values is observed with decreasing in strain rate. This phenomenon suggests the strain rate has a strong influence on flow stress. Based on the experimental results above, an Arrhenius-type constitutive equation is proposed to predict the flow stress.

  10. Effect of Spark-Plasma-Sintering Conditions on Tensile Properties of Aluminum Matrix Composites Reinforced with Multiwalled Carbon Nanotubes (MWCNTs)

    Science.gov (United States)

    Chen, B.; Imai, H.; Umeda, J.; Takahashi, M.; Kondoh, K.

    2017-04-01

    In this study, aluminum (Al) matrix composites containing 2 wt.% multiwalled carbon nanotubes (CNTs) were fabricated by powder metallurgy using high-energy ball milling (HEBM), spark plasma sintering (SPS), and subsequent hot extrusion. The effect of SPS conditions on the tensile properties of CNT/Al composites was investigated. The results showed that composites with well-dispersed CNTs and nearly full-density CNT/Al can be obtained. During HEBM, CNTs were shortened, inserted into welded Al powder particles, bonded to Al, and still stable without CNT-Al reaction. After consolidation, Al4C3 phases formed in composites under different sintering conditions. With the increase of sintering temperature and holding time, the strength decreased. Conversely, the ductility and toughness noticeably increased. As a result, a good balance between strength (367 MPa in ultimate tensile strength) and ductility (13% in elongation) was achieved in the as-extruded CNT/Al composite sintered at 630°C with a holding time of 300 min.

  11. The Optimum Processing Parameter of Carbon Nano tubes and Thermoplastic Natural Rubber (NR/LNR/LLDPE) Composites Based on Tensile Properties

    International Nuclear Information System (INIS)

    Hazwani Halim; Syed Yusainee Syed Yahya; Sahrim Ahmad; Tarawneh, M.A.; Shamsul Bahri, A.R.

    2011-01-01

    In this study, the exact processing parameter including mixing time, rotor speed and temperature of CNTs and TPNR (NR/LNR/LLDPE) composite has been examined using tensile properties. To prepare the composite, the matrix NR/LLDPE will compatabilized using liquid natural rubber (LNR) with 40 % NR, 10 % LNR and 50 % LLDPE. Then, 2 % CNTs will be incorporated into the matrix using different processing temperature, rotor speed and mixing time. For the temperature, different temperature that used are 135, 140, 145, 150 and 155 degree and for the rotor speed 45, 50, 55, 60 and 65 rpm have been used. As for the mixing time, five different time have been investigated which is 9 min,11 min, 13 min, 15 min and 17 min. The results for Young's modulus and elongation at break show that there is the maximum increment for the composite that have been prepared using 140 degree Celsius, 55 rpm and 13 min. However when the temperature has been increased, both of these properties has been decreased. Based on these results we can conclude that the optimum processing parameter for these CNTs composite is quite similar with the composite of the matrix (TPNR) itself. (author)

  12. Characterization of Tensile Mechanical Behavior of MSCs/PLCL Hybrid Layered Sheet

    Directory of Open Access Journals (Sweden)

    Azizah Intan Pangesty

    2016-06-01

    Full Text Available A layered construct was developed by combining a porous polymer sheet and a cell sheet as a tissue engineered vascular patch. The primary objective of this study is to investigate the influence of mesenchymal stem cells (MSCs sheet on the tensile mechanical properties of porous poly-(l-lactide-co-ε-caprolactone (PLCL sheet. The porous PLCL sheet was fabricated by the solid-liquid phase separation method and the following freeze-drying method. The MSCs sheet, prepared by the temperature-responsive dish, was then layered on the top of the PLCL sheet and cultured for 2 weeks. During the in vitro study, cellular properties such as cell infiltration, spreading and proliferation were evaluated. Tensile test of the layered construct was performed periodically to characterize the tensile mechanical behavior. The tensile properties were then correlated with the cellular properties to understand the effect of MSCs sheet on the variation of the mechanical behavior during the in vitro study. It was found that MSCs from the cell sheet were able to migrate into the PLCL sheet and actively proliferated into the porous structure then formed a new layer of MSCs on the opposite surface of the PLCL sheet. Mechanical evaluation revealed that the PLCL sheet with MSCs showed enhancement of tensile strength and strain energy density at the first week of culture which is characterized as the effect of MSCs proliferation and its infiltration into the porous structure of the PLCL sheet. New technique was presented to develop tissue engineered patch by combining MSCs sheet and porous PLCL sheet, and it is expected that the layered patch may prolong biomechanical stability when implanted in vivo.

  13. An Experimental Study of the Influence of in-Plane Fiber Waviness on Unidirectional Laminates Tensile Properties

    Science.gov (United States)

    Zhao, Cong; Xiao, Jun; Li, Yong; Chu, Qiyi; Xu, Ting; Wang, Bendong

    2017-12-01

    As one of the most common process induced defects of automated fiber placement, in-plane fiber waviness and its influences on mechanical properties of fiber reinforced composite lack experimental studies. In this paper, a new approach to prepare the test specimen with in-plane fiber waviness is proposed in consideration of the mismatch between the current test standard and actual fiber trajectory. Based on the generation mechanism of in-plane fiber waviness during automated fiber placement, the magnitude of in-plane fiber waviness is characterized by axial compressive strain of prepreg tow. The elastic constants and tensile strength of unidirectional laminates with in-plane fiber waviness are calculated by off-axis and maximum stress theory. Experimental results show that the tensile properties infade dramatically with increasing magnitude of the waviness, in good agreement with theoretical analyses. When prepreg tow compressive strain reaches 1.2%, the longitudinal tensile modulus and strength of unidirectional laminate decreased by 25.5% and 57.7%, respectively.

  14. Effects of cavity surface temperature on mechanical properties of specimens with and without a weld line in rapid heat cycle molding

    International Nuclear Information System (INIS)

    Wang, Guilong; Zhao, Guoqun; Wang, Xiaoxin

    2013-01-01

    Highlights: ► Higher cavity surface temperature reduces tensile strength of non-weldline part. ► Higher cavity surface temperature increases weldline tensile strength for PS and PP. ► Higher cavity surface temperature reduces weldline tensile strength for ABS, ABS/PMMA, ABS/PMMA/nano-C a CO 3 and FRPP. ► Tensile strength is reduced more by the weldline than impact strength. ► FRPP has the lowest weld line factor than other plastics without reinforced fibers. - Abstract: Rapid heat cycle molding (RHCM) is a recently developed injection molding technology to enhance surface esthetic of the parts. By rapid heating and cooling of mold cavity surfaces in molding process, it can greatly alleviate or even eliminate the surface defects such as flow mark, weld line, glass fiber rich surface, silver mark, jetting mark, and swirl mark, and also improve gloss finish and dimensional accuracy without prolonging the molding cycle. Besides surface esthetic, mechanical property is also a very import issue for the molded plastic part. The aim of this study is focusing on the effects of the cavity surface temperature just before filling, T cs , in RHCM on the mechanical strength of the specimen with and without weld line. Six kinds of typical plastics including polystyrene (PS), polypropylene (PP), acrylonitrile butadiene styrene (ABS), acrylonitrile butadiene styrene/polymethylmethacrylate (ABS/PMMA), ABS/PMMA/nano-C a CO 3 and glass fiber reinforced polypropylene (FRPP) are used in experiments. The specimens with and without a weld line are produced with the different T cs on the developed electric-heating RHCM system. Tensile tests and notched Izod impact tests are conducted to characterize the mechanical strength of the specimens molded with different cavity surface temperatures. Simulations, differential scanning calorimetry (DSC), scanning electron microscope (SEM) and optical microscope are implemented to explain the impact mechanism of T cs on mechanical properties

  15. Study of the tensile properties of individual multicellular fibres generated by Bacillus subtilis

    Science.gov (United States)

    Ye, Xuan; Zhao, Liang; Liang, Jiecun; Li, Xide; Chen, Guo-Qiang

    2017-04-01

    Multicellular fibres formed by Bacillus subtilis (B. subtilis) are attracting interest because of their potential application as degradable biomaterials. However, mechanical properties of individual fibres remain unknown because of their small dimensions. Herein, a new approach is developed to investigate the tensile properties of individual fibres with an average diameter of 0.7 μm and a length range of 25.7-254.3 μm. Variations in the tensile strengths of fibres are found to be the result of variable interactions among pairs of microbial cells known as septa. Using Weibull weakest-link model to study this mechanical variability, we predict the length effect of the sample. Moreover, the mechanical properties of fibres are found to depend highly on relative humidity (RH), with a brittle-ductile transition occurring around RH = 45%. The elastic modulus is 5.8 GPa in the brittle state, while decreases to 62.2 MPa in the ductile state. The properties of fibres are investigated by using a spring model (RH  45%) for the time-dependent response. Loading-unloading experiments and numerical calculations demonstrate that necking instability comes from structural changes (septa) and viscoelasticity dominates the deformation of fibres at high RH.

  16. Friction Stir Welding of Low-Carbon AISI 1006 Steel: Room and High-Temperature Mechanical Properties

    Science.gov (United States)

    Shunmugasamy, Vasanth C.; Mansoor, Bilal; Ayoub, Georges; Hamade, Ramsey

    2018-03-01

    Friction stir welding (FSW) is an ecologically benign solid-state joining process. In this work, FSW of low-carbon AISI 1006 steel was carried out to study the microstructure and mechanical properties of the resulting joints at both room temperature (RT) and 200 °C. In the parameter space investigated here, a rotational tool speed and translation feed combination of 1200 rpm and 60 mm/min produced a defect-free weld with balanced mechanical properties and a superior Vickers microhardness profile compared to all other conditions and to base metal (BM). At faster translation feeds (100 and 150 mm/min), wormhole defects were observed in the weld microstructure and were attributed to higher strain rate experienced by the weld zone. Under tensile loading, welded material exhibited yield strength that was up to 86 and 91% of the BM at RT and 200 °C, respectively. On the other hand, tensile strength of welded material was nearly similar to that of the base metal at both RT and 200 °C. However, at both temperatures the tensile ductility of the welded joints was observed to be significantly lower than the BM. Annealing of the 1200 rpm and 60 mm/min FSW specimen resulted in tensile strength of 102% compared to base material and 47% increase in the strain at failure compared to the as-welded specimen. The Charpy impact values revealed up to 62 and 53% increase in the specific impact energy for the 1200 rpm and 60 mm/min welded joints as compared with the BM.

  17. Effect of dispersion hardening process on change of Rm tensile strength of EN AC-46000 alloy

    Directory of Open Access Journals (Sweden)

    J. Pezda

    2010-01-01

    Full Text Available Heat treatment of aluminum alloys is performed mainly to increase mechanical properties of the alloys. Very important issue, from improvement of mechanical properties point of view as well as economical aspects of performed treatment, is selection of a suitable parameters of solutioning and ageing operations. The paper presents results of the investigations concerning effect of the performed heat treatment on change of tensile strength of the EN AC-46000 (AlSi9Cu3 alloy. Investigated alloy was melted in electric resistance furnace. Run of crystallization is presented with making use of the thermal derivative method (ATD. This method was also implemented to determination of heat treatments’ temperature range of the alloy. Performed heat treatment resulted in growth of the Rm tensile strength. Performed tests have enabled determination of temperature and duration of solutioning and ageing operations of the investigated alloy, which would condition obtainment of improved Rm tensile strength. The tests were performed in laboratory conditions.

  18. Mechanical properties of roll extruded nuclear reactor piping

    International Nuclear Information System (INIS)

    Steichen, J.M.; Knecht, R.L.

    1975-01-01

    The elevated temperature mechanical properties of large diameter (28 inches) seamless pipe produced by roll extrusion for use as primary piping for sodium coolant in the Fast Flux Test Facility (FFTF) have been characterized. The three heats of Type 316H stainless steel piping material used exhibited consistent mechanical properties and chemical compositions. Tensile and creep-rupture properties exceeded values on which the allowable stresses for ASME Code Case 1592 on Nuclear Components in Elevated Temperature Service were based. Tensile strength and ductility were essentially unchanged by aging in static sodium at 1050 0 F for times to 10,000 hours. High strain rate tensile tests showed that tensile properties were insensitive to strain rate at temperatures to 900 0 F and that for temperatures of 1050 0 F and above both strength and ductility significantly increased with increasing strain rate. Fatigue-crack propagation properties were comparable to results obtained on plate material and no differences in crack propagation were found between axial and circumferential orientations. (U.S.)

  19. Elevated temperature mechanical properties of a rapidly solidified A1-Fe-V-Si alloy

    International Nuclear Information System (INIS)

    Mitra, S.

    1992-01-01

    Dispersion strengthened Al alloys based on the Al-Fe-V-Si quartenary system have recently been developed using rapid solidification techniques. Rapid solidification techniques which resulted in the above mentioned alloys have also been used to manufacture another commercial alloy, FVS 1212, with 37 volume % of dispersoid. The alloy has shown excellent resistance to coarsening at high temperatures and to creep deformation. Elevated temperature exposure of FVS 1212, for times up to 100 hours, resulted in a significant loss in room temperature mechanical properties only beyond 500 degrees C while 1000 hours at 425 degrees C did not result in any degradation of mechanical but no detailed study of the tensile behavior of FVS 1212 at slow strain rates and elevated temperatures has been reported to date. This paper reports that the present study was undertaken to investigate the tensile behavior of FVS 1212 from room temperature to 400 degrees C at strain rates of 6.56 x 10 - 5/sec and 6.56 x 10 -6 /sec. The study focussed on dynamic strain aging effects and strain hardening behavior, while the effect of strain rate on the flow behavior at elevated temperatures was also evaluated

  20. Solution Treatment Effect on Tensile, Impact and Fracture Behaviour of Trace Zr Added Al-12Si-1Mg-1Cu Piston Alloy

    Science.gov (United States)

    Kaiser, Md. Salim

    2018-04-01

    The effects of T6 solution treatment on tensile, impact and fracture properties of cast Al-12Si-1Mg-1Cu piston alloys with trace of zirconium were investigated. Cast alloys were given precipitation strengthening treatment having a sequence of homogenizing, solutionizing, quenching and ageing. Both cast and solutionized samples are isochronally aged for 90 min at different temperatures up to 300 °C. Tensile and impact properties of the differently processed alloys have been studied to understand the precipitation strengthening of the alloys. Fractograpy of the alloys were observed to understand the mode of fracture. It is observed that the improvement in tensile properties in the aged alloys through heat treatment is mainly attributed to the formation of the Al2Cu and Mg2Si precipitates within the Al matrix. Solution treatment improves the tensile strength for the reason that during solution treatment some alloying elements are re-dissolved to produce a solute-rich solid solution. Impact energy decreases with ageing temperature due to formation of GP zones, β' and β precipitates. The fractography shows large and small dimple structure and broken or cracked primary Si, particles. Microstructure study of alloys revealed that the solution treatment improved distribution of silicon grains. The addition of Zr produces an improvement in the tensile properties as a result of its grain refining action and grain coarsening resistance in the matrix at a higher temperature.

  1. Tensile strength and impact resistance properties of materials used in prosthetic check sockets, copolymer sockets, and definitive laminated sockets.

    Science.gov (United States)

    Gerschutz, Maria J; Haynes, Michael L; Nixon, Derek M; Colvin, James M

    2011-01-01

    Prosthetic sockets serve as the interface between people with amputations and their prostheses. Although most materials used to make prosthetic sockets have been used for many years, knowledge of these materials' properties is limited, especially after they are subjected to fabrication processes. This study evaluated tensile and impact properties of the current state-of-the-art materials used to fabricate prosthetic check sockets, copolymer sockets, and definitive laminated sockets. Thermolyn Rigid and Orfitrans Stiff check socket materials produced significantly lower tensile strength and impact resistance than polyethylene terephthalate glycol (PETG). Copolymer socket materials exhibited greater resistance to impact forces than the check socket materials but lower tensile strengths than PETG. The heated molding processes, for the check socket and copolymer materials, reduced both tensile strength and elongation at break. Definitive laminated sockets were sorted according to fabrication techniques. Nyglass material had significantly higher elongation, indicating a more ductile material than carbon-based laminations. Carbon sockets with pigmented resin had higher tensile strength and modulus at break than nonpigmented carbon sockets. Elongation at yield and elongation at break were similar for both types of carbon-based laminations. The material properties determined in this study provide a foundation for understanding and improving the quality of prosthetic sockets using current fabrication materials and a basis for evaluating future technologies.

  2. High performance thermoplastics - A review of neat resin and composite properties

    Science.gov (United States)

    Johnston, Norman J.; Hergenrother, Paul M.

    1987-01-01

    A review was made of the principal thermoplastics used to fabricate high performance composites. Neat resin tensile and fracture toughness properties, glass transition temperatures (Tg), crystalline melt temperatures (Tm) and approximate processing conditions are presented. Mechanical properties of carbon fiber composites made from many of these thermoplastics are given, including flexural, longitudinal tensile, transverse tensile and in-plane shear properties as well as short beam shear and compressive strengths and interlaminar fracture toughness.

  3. Phase Morphology and Mechanical Properties of Cyclic Butylene Terephthalate Oligomer-Containing Rubbers: Effect of Mixing Temperature

    OpenAIRE

    Hal?sz, Istv?n Zolt?n; B?r?ny, Tam?s

    2016-01-01

    In this work, the effect of mixing temperature (Tmix) on the mechanical, rheological, and morphological properties of rubber/cyclic butylene terephthalate (CBT) oligomer compounds was studied. Apolar (styrene butadiene rubber, SBR) and polar (acrylonitrile butadiene rubber, NBR) rubbers were modified by CBT (20 phr) for reinforcement and viscosity reduction. The mechanical properties were determined in tensile, tear, and dynamical mechanical analysis (DMTA) tests. The CBT-caused viscosity cha...

  4. Mechanical properties of LMR structural materials at high temperature

    International Nuclear Information System (INIS)

    Kim, D. W.; Kuk, I. H.; Ryu, W. S. and others

    1999-03-01

    Austenitic stainless is used for the structural material of liquid metal reactor (LMR) because of good mechanical properties at high temperature. Stainless steel having more resistant to temperature by adding minor element has been developing for operating the LMR at higher temperature. Of many elements, nitrogen is a prospective element to modify type 316L(N) stainless steel because nitrogen is the most effective element for solid solution and because nitrogen retards the precipitation of carbide at grain boundary. Ti, Nb, and V are added to improve creep properties by stabilizing the carbides through forming MC carbide. Testing techniques of tensile, fatigue, creep, and creep-fatigue at high temperature are difficult. Moreover, testing times for creep and creep-fatigue tests are very long up to several tens of thousands hours because creep and creep-fatigue phenomena are time-dependent damage mechanism. So, it is hard to acquire the material data for designing LMR systems during a limited time. In addition, the integrity of LMR structural materials at the end of LMR life has to be predicted from the laboratory data tested during the short term because there is no data tested during 40 years. Therefore, the effect of elements on mechanical properties at high temperature was reviewed in this study and many methods to predict the long-term behaviors of structural materials by simulated modelling equation is shown in this report. (author). 32 refs., 9 tabs., 38 figs

  5. Electrical Transport and Magnetoresistance Properties of Tensile-Strained CaMnO3 Thin Films

    Science.gov (United States)

    Ullery, Dustin; Lawson, Bridget; Zimmerman, William; Neubauer, Samuel; Chaudhry, Adeel; Hart, Cacie; Yong, Grace; Smolyaninova, Vera; Kolagani, Rajeswari

    We will present our studies of the electrical transport and magnetoresistance properties of tensile strained CaMnO3 thin films. We observe that the resistivity decreases significantly as the film thickness decreases which is opposite to what is observed in thin films of hole doped manganites. The decrease in resistivity is more pronounced in the films on (100) SrTiO3, with resistivity of the thinnest films being about 3 orders of magnitude lower than that of bulk CaMnO3. Structural changes accompanying resistivity changes cannot be fully explained as due to tensile strain, and indicate the presence of oxygen vacancies. These results also suggest a coupling between tensile strain and oxygen deficiency, consistent with predictions from models based on density functional theory calculations. We observe a change in resistance under the application of moderate magnetic field. Experiments are underway to understand the origin of the magnetoresistance and its possible relation to the tensile strain effects. We acknowledge support from: Towson Office of University Undergraduate Research, Fisher Endowment Grant and Undergraduate Research Grants from the Fisher College of Science and Mathematics, and Seed Funding Grant from the School of Emerging technologies.

  6. Influence of laboratory annealing on tensile properties and design stress intensity limits for Type 304 stainless steel

    International Nuclear Information System (INIS)

    Sikka, V.K.; Booker, M.K.

    1977-01-01

    The influence of reannealing (laboratory annealing) on yield and ultimate tensile strength values of 19 heats of type 304 stainless steel was determined. Most heats were reannealed at 1065 0 C for 0.5 hr. The reannealed properties were used to determine the influence of reannealing on time-independent design stress intensity limits (S/sub m/). The major findings are as follows: 1. Reannealing lowered the 0.2 percent yield strength versus temperature curve by approximately 42 MPa over the range from room temperature to 649 0 C. 2. The estimated S/sub m/ values for reannealed material were 24 to 28 MPa lower than the current code values. 3. Reannealing appears to influence the S/sub m/ value sufficiently to warrant the consideration of separate values of S/sub m/ in Sect. III of the Boiler and Pressure Vessel Code and Code Case 1592 for ''as-received'' and reannealed material

  7. In-Situ tensile testing of propellants in SEM: influence of temperature

    NARCIS (Netherlands)

    Di Benedetto, G.L.; Ramshorst, M.C.J.; Duvalois, W.; Hooijmeijer, P.; Heijden, A. van der

    2017-01-01

    A tensile module system placed within a Scanning Electron Microscope (SEM) was utilized to conduct insitu tensile testing of propellant samples. The tensile module system allows for real-time in-situ SEM analysis of the samples to determine the failure mechanism of the propellant material under

  8. Ion irradiation effects on tensile properties of carbon fibres

    International Nuclear Information System (INIS)

    Kurumada, A.; Ishihara, M.; Baba, S.; Aihara, J.

    2004-01-01

    Carbon/carbon composite materials have high thermal conductivity and excellent mechanical properties at high temperatures. They have been used as structural materials at high temperatures in fission and experimental fusion reactors. The changes in the microstructures and the mechanical properties due to irradiation damage must be measured for the safety design and the life assessment of the materials. The purpose of this study is to obtain a basic knowledge of the development of new carbon composite materials having high thermal conductivity and excellent resistance to irradiation damage. Five kinds of carbon fibres were selected, including a vapour growth carbon fibre (VGCF; K1100X), a polyacrylonitrile-based fibre (PAN; M55JB by Toray Corp.), two meso-phase pitch-based fibres (YS-15-60S and YS-70-60S by Nippon Graphite Fiber Corp.) and a pitch-based fibre (K13C2U by Mitsubishi Chemical Co.). They were irradiated by high-energy carbon, nickel and argon ions. Irradiation damages in the carbon fibres are expected to be uniform across the cross-section, as the diameters of the carbon fibres are about 20 μm and are sufficiently smaller than the ranges of ions. The cross-sectional areas increased due to ion irradiation, with the exception of the K1100X of VGCF. One of the reasons for the increases is the swelling of carbon basal planes due to lattice defects in the graphite interlayer. The tensile strengths and the Young's moduli decreased due to ion irradiation except for the K1100X of VGCF and the YS-15-60S of meso-phase pitch-based fibres. One of the reasons for the decreases is thought to be that the microstructures of carbon fibres are damaged in the axial direction, as ions were irradiated vertically with respect to the longitudinal direction of carbon fibres. The results of this study indicate that the VGCF and the meso-phase pitch-based carbon fibres could be useful as reinforcement fibres of new carbon composite materials having high thermal conductivity and

  9. Tensile and dimensional properties of wood strands made from plantation southern pine lumber

    Science.gov (United States)

    Qinglin Wu; Zhiyong Cai; Jong N. Lee

    2005-01-01

    Working stresses and performance of strand composite lumber largely depend upon the properties of each individual strand. Southern pine strands from plantation lumber grown in southern Louisiana were investigated in this study in order to understand strand behaviors. The effects of hot-pressing and resin application on tensile modulus, strength, and dimensional...

  10. Relationship of microstructure and tensile properties for neutron-irradiated vanadium alloys

    International Nuclear Information System (INIS)

    Loomis, B.A.; Smith, D.L.

    1990-01-01

    The microstructures in V-15Cr-5Ti, V-10Cr-5RTi, V-3Ti-1Si, V-15Ti-7.5Cr, and V-20Ti alloys were examined by transmission electron microscopy after neutron irradiation at 600 degree C to 21--84 atom displacements per atom in the Materials Open Test Assembly of the Fast Flux Test Facility. The microstructures in these irradiated alloys were analyzed to determine the radiation-produced dislocation density, precipitate number density and size, and void number density and size. The results of these analyses were used to compute increases in yield stress and swelling of the irradiated alloys. The computed increase in yield stress was compared with the increase in yield stress determined from tensile tests on these irradiated alloys. This comparison made it possible to evaluate the influence of alloy composition on the evolution of radiation-damaged microstructures and the resulting tensile properties. 11 refs

  11. Effects of gamma-ray irradiation on tensile properties of ultradrawn polyethylene

    International Nuclear Information System (INIS)

    Iida, Shozo; Sakami, Hiroshi

    1977-01-01

    The deformation of ultradrawn polyethylene was previously shown that crystalline chains were pulled out by the tension applied to tie chains which connected crystal blocks. This paper deals with the effects of γ-ray irradiation on crosslinking which prevent crystalline chains being pulled out and to improve the tensile properties. The tensile strength of high density polyethylene, drawn by a factor of 40, increased from 73 to 113 kg/mm 2 at 20 0 C and from 13 to 42 kg/mm 2 at 80 0 C with increasing irradiation dose from zero to 100 Mrad. The tensile elongation, the residual strain measured by cyclic strain test, and the rate of stress decrease by the stress relaxation measurement diminished with increasing irradiation dose. These facts showed the existence of preventive effects by crosslinks on pulling. The stress-strain relation of crosslinked polymer was calculated thermodynamically from the melting of crystalline chains accompanied by the sliding of chains, assuming that the sliding of crystalline chains was brought about by an unbalance of the tension applied to tie chains with which both sides of crystalline chains were connected. The equation of stress was derived; stress increased with increasing strain and was proportional to the Gibbs' free energy of fusion. The observed stress-strain relations obeyed the above mentioned equation. (auth.)

  12. Effect of post weld heat treatment on tensile properties and microstructure characteristics of friction stir welded armour grade AA7075-T651 aluminium alloy

    Directory of Open Access Journals (Sweden)

    P. Sivaraj

    2014-03-01

    Full Text Available This paper reports the effects of post weld heat treatments, namely artificial ageing and solution treatment followed by artificial ageing, on microstructure and mechanical properties of 12 mm thick friction stir welded joints of precipitation hardenable high strength armour grade AA7075-T651 aluminium alloy. The tensile properties, such as yield strength, tensile strength, elongation and notch tensile strength, are evaluated and correlated with the microhardness and microstructural features. The scanning electron microscope is used to characterie the fracture surfaces. The solution treatment followed by ageing heat treatment cycle is found to be marginally beneficial in improving the tensile properties of friction stir welds of AA7075-T651 aluminium alloy.

  13. Implementation of nondestructive testing and mechanical performance approaches to assess low temperature fracture properties of asphalt binders

    Directory of Open Access Journals (Sweden)

    Salman Hakimzadeh

    2017-05-01

    Full Text Available In the present work, three different asphalt binders were studied to assess their fracture behavior at low temperatures. Fracture properties of asphalt materials were obtained through conducting the compact tension [C(T] and indirect tensile [ID(T] strength tests. Mechanical fracture tests were followed by performing acoustic emissions test to determine the “embrittlement temperature” of binders which was used in evaluation of thermally induced microdamages in binders. Results showed that both nondestructive and mechanical testing approaches could successfully capture low-temperature cracking behavior of asphalt materials. It was also observed that using GTR as the binder modifier significantly improved thermal cracking resistance of PG64-22 binder. The overall trends of AE test results were consistent with those of mechanical tests. Keywords: Thermal cracking, Indirect tensile strength test, Compact tension test, Nondestructive approach, Acoustic emission test, Embrittlement temperature

  14. The effect of tungsten on the tensile and creep rupture strength of 12 CrMoV steels

    International Nuclear Information System (INIS)

    Oakes, G.; Orr, J.

    1978-01-01

    A collaborative project involving the Brown-Firth Research Laboratories, the Sheffield Laboratories of the British Steel Corporation and Tube Investments Limited has been carried out to assess the effect of a controlled tungsten addition (0.5%) on the tensile and rupture properties of 12 CrMoV steel. The results obtained indicate that 0.5% tungsten increases the tensile properties at room temperature by approximately 3% but this diminishes with increasing test temperature. The creep rupture properties of the tungsten-bearing material showed a marked short time (500-1000 hours) strength advantage over the tungsten-free material at temperatures up to 650 0 C. At longer times and higher temperatures this stress advantage was reduced considerably so that at times in the region of 10,000 to 15,000 hours it was approximately 5%. In view of the limited data generated, it was found impossible to extrapolate with confidence to longer times but there was, however, no indication that a significant strength advantage is to be anticipated at 100,000 hours for the tungsten-bearing material. (author)

  15. A comparison of the microstructure and high temperature tensile properties of a novel P/M Mo-Hf-Zr-Ta-C alloy and TZM

    International Nuclear Information System (INIS)

    Warren, J.; Reznikov, G.

    2001-01-01

    The microstructure and elevated temperature quasi-static tensile yield and ultimate strength observed in a novel, forged Mo-based alloy (Mo-0.25 Hf-0.25 Zr-0.25 Ta-0.025 C) has been analyzed and compared to a standard forged TZM composition (Mo-0.50 Ti-0.08 Zr-0.02 C). The novel material exhibits the desirable forging characteristics typical of the widely used TZM composition yet possess a higher ultimate strength and 0.2 % offset yield strength in both the stress-relieved and recrystallized conditions over a 400 o -1200 o C temperature range. The greater strength measured in the novel composition has been attributed to the combined effects of precipitation of Hf, Zr and Mo-(carbide) precipitates that strengthen the matrix in the classical Orowan fashion and improved resistance to recrystallization after high temperature exposure. Elevated temperature creep behavior, not addressed in the study presented here, will be reported on in a subsequent analysis. (author)

  16. Effect of welding process, type of electrode and electrode core diameter on the tensile property of 304L austenitic stainless steel

    Directory of Open Access Journals (Sweden)

    Akinlabi OYETUNJI

    2014-11-01

    Full Text Available The effect of welding process, type of electrode and electrode core diameter on the tensile property of AISI 304L Austenitic Stainless Steel (ASS was studied. The tensile strength property of ASS welded samples was evaluated. Prepared samples of the ASS were welded under these three various variables. Tensile test was then carried out on the welded samples. It was found that the reduction in ultimate tensile strength (UTS of the butt joint samples increases with increase in core diameter of the electrode. Also, the best electrode for welding 304L ASS is 308L stainless steel-core electrode of 3.2 mm core diameter. It is recommended that the findings of this work can be applied in the chemical, food and oil industries where 304L ASS are predominantly used.

  17. Transverse Tensile Properties of 3 Dimension-4 Directional Braided Cf/SiC Composite Based on Double-Scale Model

    Science.gov (United States)

    Niu, Xuming; Sun, Zhigang; Song, Yingdong

    2017-11-01

    In this thesis, a double-scale model for 3 Dimension-4 directional(3D-4d) braided C/SiC composites(CMCs) has been proposed to investigate mechanical properties of it. The double-scale model involves micro-scale which takes fiber/matrix/porosity in fibers tows into consideration and the unit cell scale which considers the 3D-4d braiding structure. Basing on the Micro-optical photographs of composite, we can build a parameterized finite element model that reflects structure of 3D-4d braided composites. The mechanical properties of fiber tows in transverse direction are studied by combining the crack band theory for matrix cracking and cohesive zone model for interface debonding. Transverse tensile process of 3D-4d CMCs can be simulated by introducing mechanical properties of fiber tows into finite element of 3D-4d braided CMCs. Quasi-static tensile tests of 3D-4d braided CMCs have been performed with PWS-100 test system. The predicted tensile stress-strain curve by the double scale model finds good agreement with the experimental results.

  18. Effect of cryogenic treatment on the tensile behaviour of En 52 and 21-4N valve steels at room and elevated temperatures

    International Nuclear Information System (INIS)

    Jaswin, M. Arockia; Lal, D. Mohan

    2011-01-01

    Research highlights: → Tensile behaviour of cryo-treated valve steels are investigated at elevated temperature. → En 52 and 21-4N valve steel materials are treated at - 196 o C . → Tensile strength of cryo-treated En 52 and 21-4N valve steel has improved by 8 % and 12 % respectively. → Precipitation of fine carbides through cryogenic treatment is the reason for the improved strength. -- Abstract: This experimental study investigates the effects of cryogenic treatment on the tensile behaviour of En 52 and 21-4N valve steels at room and elevated temperatures. The materials are subjected to shallow cryogenic treatment (SCT) at 193 K and deep cryogenic treatment (DCT) at 85 K and the tensile behaviour is compared with that of the conventional heat treatment (CHT). The high temperature tensile test is conducted at 673 K (400 o C) and 923 K (650 o C) for the En 52 and 21-4N valve steels respectively. The ultimate tensile strength of the En 52 and 21-4N DCT samples show an enhancement of 7.87% and 6.76% respectively, over the CHT samples tested at the elevated temperature. The average yield strength of the En 52 DCT samples has an improvement 11% than that of the CHT samples when tested at room and elevated temperatures. The deep cryogenic treatment conducted at the optimized condition shows 7.84% improvement in the tensile strength for the En 52 valve steel and 11.87% improvement for the 21-4N valve steel when compared to the strength of the samples without the cryogenic treatment. A scanning electron microscopic analysis of the fracture surface indicates the presence of dimples and microvoid coalescence on the grain facets and interfaces of the cryo-treated specimens. The fracture surface of the deep cryo-treated 21-4N valve steel specimen shows a complete intergranular fracture with deep secondary cracks between the grains. On comparing the results of the percentage elongation, the cryo-treated samples show a smaller reduction in the elongation than that of the

  19. Effect of Thermomechanical Processing on the Microstructure, Properties, and Work Behavior of a Ti50.5 Ni29.5 Pt20 High-Temperature Shape Memory Alloy

    Science.gov (United States)

    Noebe, Ronald; Draper, Susan; Gaydosh, Darrell; Garga, Anita; Lerch, Brad; Penney, Nicholas; Begelow, Glen; Padula, Santo, II; Brown, Jeff

    2006-01-01

    TiNiPt shape memory alloys are particularly promising for use as solid state actuators in environments up to 300 C, due to a reasonable balance of properties, including acceptable work output. However, one of the challenges to commercializing a viable high-temperature shape memory alloy (HTSMA) is to establish the appropriate primary and secondary processing techniques for fabrication of the material in a required product form such as rod and wire. Consequently, a Ti(50.5)Ni(29.5)Pt20 alloy was processed using several techniques including single-pass high-temperature extrusion, multiple-pass high-temperature extrusion, and cold drawing to produce bar stock, thin rod, and fine wire, respectively. The effects of heat treatment on the hardness, grain size, room temperature tensile properties, and transformation temperatures of hot- and cold-worked material were examined. Basic tensile properties as a function of temperature and the strain-temperature response of the alloy under constant load, for the determination of work output, were also investigated for various forms of the Ti(50.5)Ni(29.5)Pt20 alloy, including fine wire.

  20. Effect of post weld heat treatment on tensile properties and microstructure characteristics of friction stir welded armour grade AA7075-T651 aluminium alloy

    OpenAIRE

    Sivaraj, P.; Kanagarajan, D.; Balasubramanian, V.

    2014-01-01

    This paper reports the effects of post weld heat treatments, namely artificial ageing and solution treatment followed by artificial ageing, on microstructure and mechanical properties of 12 mm thick friction stir welded joints of precipitation hardenable high strength armour grade AA7075-T651 aluminium alloy. The tensile properties, such as yield strength, tensile strength, elongation and notch tensile strength, are evaluated and correlated with the microhardness and microstructural features....

  1. Knitting Technologies And Tensile Properties Of A Novel Curved Flat-Knitted Three-Dimensional Spacer Fabrics

    Directory of Open Access Journals (Sweden)

    Li Xiaoying

    2015-09-01

    Full Text Available This paper introduces a knitting technique for making innovative curved three-dimensional (3D spacer fabrics by the computer flat-knitting machine. During manufacturing, a number of reinforcement yarns made of aramid fibres are inserted into 3D spacer fabrics along the weft direction to enhance the fabric tensile properties. Curved, flat-knitted 3D spacer fabrics with different angles (in the warp direction were also developed. Tensile tests were carried out in the weft and warp directions for the two spacer fabrics (with and without reinforcement yarns, and their stress–strain curves were compared. The results showed that the reinforcement yarns can reduce the fabric deformation and improve tensile stress and dimensional stability of 3D spacer fabrics. This research can help the further study of 3D spacer fabric when applied to composites.

  2. Properties analysis of tensile strength, crystallinity degree and microstructure of polymer composite polypropylene-sand

    International Nuclear Information System (INIS)

    Sudirman; Karo-Karo, Aloma; Ari-Handayani; Bambang-Sugeng; Rukihati; Mashuri

    2004-01-01

    Materials modification base on polymer toward polymer composite is needed by addition of filler. Mechanical properties such as tensile strength, crystallinity degree and microstructure of polymer composite based on polypropylene with sand filler have been investigated. In this work, the polymer composite has been made by mixing the matrix of polypropylene melt flow 2 (PP MF2) or polypropylene melt flow 10 (PP MF 10) with sand filler in a labo plastomill. The composition of sand filler was varied to 10, 30, 40 and 50 % v/v, a then the composite were casted to the film sheets form. The sheets were characterized mechanically i.e tensile strength, crystallinity degree and microstructure. The result showed that the tensile strength decreased by increasing the volume fraction of sand filler, in accordance with microstructure investigation that the matrix area under zone plastic deformation (more cracks), while the filler experienced elastic deformation, so that the strength mechanism of filler did not achieved with expectation (Danusso and Tieghi theory). For filler more than 30 % of volume fraction, the tensile strength of polypropylene melt flow 10 (PP MF 10) was greater than that polypropylene melt flow 2 (PP MF2). It was caused by plasticities in PP MF 10. The tensile strength of PP MF2 was greater than that PP MF 10 for volume fraction of sand filler less than 30 %. It was caused by PP MF2 to be have more degree of crystallinity

  3. Tensile properties of neutron irradiated solid HIP 316L(N). ITER Task T214, NET deliverable GB6 ECN-5

    International Nuclear Information System (INIS)

    Van Osch, E.V.; Tjoa, G.L.; Boskeljon, J.; Van Hoepen, J.

    1998-05-01

    The tensile properties of neutron irradiated Hot Isostatically Pressed (HIP) joints of type 316L(N) stainless steel (heat PM-130) have been measured. Cylindrical tensile test specimens of 4 mm diameter were irradiated in the High Flux Reactor (HFR) in Petten, The Netherlands, simulating the first wall conditions by a combination of high displacement damage with proportional amounts of helium. The solid HIP specimens were irradiated up to a target dose level of 5 dpa at a temperature of 550K. The damage levels realized range from 3.0 to 4.1 dpa, with helium contents up to 38 appm. Post irradiation testing temperatures ranged from 300 to 700K. The report contains the experimental conditions and summarises the results, which are given in terms of engineering stresses and strains and reduction of area. The main conclusions are that the unirradiated solid-HIP material is very soft, assumingly due to the relatively large grain size. Neutron irradiation induces both hardening and reduction of ductility, similar to the behaviour of 316L(N) plate. No failures related to debonding were observed for the tests of the unirradiated samples, however one of eight tested irradiated specimens fractured in the HIP joint, showing a flat fracture surface and a low reduction of area. 6 refs

  4. Physical properties of concrete under 3-years exposure to high temperatures up to 110degC

    International Nuclear Information System (INIS)

    Nishiuchi, T.; Kanazu, T.; Ishida, H.

    1990-01-01

    Concrete structural members in a storehouse of high level radioactive wastes are designed assuming that they may be subjected to elevated temperature for a long term. So, in this study, concrete properties under temperature conditions (between 65degC-temperature limitation specified in design and 110degC-vaporing temperature of gel water in concrete) and possibility of raising this temperature limitation has been investigated from the view point of long term concrete properties. In this experiment, many properties of concrete were examined, such as compressive strength, tensile strength. Young's modulus, weight loss, pore size distribution under combined conditions (temperature conditions, mix proportions of concrete, moisture conditions). Followings are the main conclusions obtained within the limit of the experiment. 1. Compressive strength of concrete becomes smaller according as temperature becomes high, but there is little difference between the compressive strength at 65degC and 85degC. 2. Young's modulus of concrete decreases linearly according as temperature becomes higher. 3. Weight loss of concrete increases according as temperature becomes higher. 4. Judging from the decreasing rate of physical properties of concrete, it seems possible to raise temperature limitation from 65degC to 85degC. (author)

  5. Structure and tensile properties of ferro-martensitic alloys hardened by chi phase precipitation

    International Nuclear Information System (INIS)

    Alamo, A.; Aubert, H.; Laniesse, J.; Lelong, C.; Pigoury, M.; Foucher, C.

    1985-08-01

    Transformation of ferrite into austenite and of austenite into martensite, precipitation of intermetallic phases and tensile properties of the steel Cr13-Mo1.5 are studied in function of Ti additions (from 0 to 3%) and Ni additions (from 2 to 8%) for its mechanical resistance at 400-650 0 C. 12 references are given [fr

  6. Development of Embedded EM Sensors for Estimating Tensile Forces of PSC Girder Bridges

    Science.gov (United States)

    Kim, Ju-Won; Lee, Chaggil; Park, Seunghee

    2017-01-01

    The tensile force of pre-stressed concrete (PSC) girders is the most important factor for managing the stability of PSC bridges. The tensile force is induced using pre-stressing (PS) tendons of a PSC girder. Because the PS tendons are located inside of the PSC girder, the tensile force cannot be measured after construction using conventional NDT (non-destructive testing) methods. To monitor the induced tensile force of a PSC girder, an embedded EM (elasto-magnetic) sensor was proposed in this study. The PS tendons are made of carbon steel, a ferromagnetic material. The magnetic properties of the ferromagnetic specimen are changed according to the induced magnetic field, temperature, and induced stress. Thus, the tensile force of PS tendons can be estimated by measuring their magnetic properties. The EM sensor can measure the magnetic properties of ferromagnetic materials in the form of a B (magnetic density)-H (magnetic force) loop. To measure the B-H loop of a PS tendon in a PSC girder, the EM sensor should be embedded into the PSC girder. The proposed embedded EM sensor can be embedded into a PSC girder as a sheath joint by designing screw threads to connect with the sheath. To confirm the proposed embedded EM sensors, the experimental study was performed using a down-scaled PSC girder model. Two specimens were constructed with embedded EM sensors, and three sensors were installed in each specimen. The embedded EM sensor could measure the B-H loop of PS tendons even if it was located inside concrete, and the area of the B-H loop was proportionally decreased according to the increase in tensile force. According to the results, the proposed method can be used to estimate the tensile force of unrevealed PS tendons. PMID:28867790

  7. Optimization of mixing process and effect of multi-walled carbon nanotubes on tensile properties of unsaturated polyester resin in composite materials

    Energy Technology Data Exchange (ETDEWEB)

    Hoang, Van-Tho; Yum, Young-Jin [University of Ulsan, Ulsan (Korea, Republic of)

    2017-04-15

    Multi-walled carbon nanotubes (MWCNTs) were mixed with Unsaturated polyester resin (UPR) using the stir method at high temperatures. The mixing temperature and hardener ratio were optimized based on compression properties and the exothermic temperature. In the experiment, 60 °C and 1 wt.% of Methyl ethyl ketone peroxide (MEKP) were chosen for the mixing condition and catalyst concentration, respectively. MWCNTs with different weight fractions (0.05, 0.1, 0.2 and 0.3 wt.%) were dispersed to investigate the effect of MWCNTs on tensile properties of the UPR, and it was found that 0.1 wt.% of MWCNTs showed the best performance in this range of fiber weight fraction due to a higher strength (42.14 %), modulus (14.33 %) and fracture strain (37.17 %) than pure UPR. The state of dispersion and arrangement of fibers were examined by a Field emission Scanning electron microscope (FE-SEM) according to fracture surfaces. Similarly, the FE-SEM also showed better results with 0.1 wt.% of MWCNTs mixed in the UPR.

  8. Mechanical properties of 1950's vintage 304 stainless steel weldment components after low temperature neutron irradiation

    International Nuclear Information System (INIS)

    Sindelar, R.L.; Caskey, G.R. Jr.; Thomas, J.K.; Hawthorne, J.R.; Hiser, A.L.; Lott, R.A.; Begley, J.A.; Shogan, R.P.

    1991-01-01

    The reactor vessels of the nuclear production reactors at the Savannah River Site (SRS) were constructed in the 1950's from Type 304 stainless steel plates welded with Type 308 stainless steel filler using the multipass metal inert gas process. An irradiated mechanical properties database has been developed for the vessel with materials from archival primary coolant system piping irradiated at low temperatures (75 to 150 degrees C) in the State University of New York at Buffalo reactor (UBR) and the High Flux Isotope Reactor (HFIR) to doses of 0.065 to 2.1 dpa. Fracture toughness, tensile, and Charpy-V impact properties of the weldment components (base, weld, and weld heat-affected-zone (HAZ)) have been measured at temperatures of 25 degrees C and 125 degrees C in the L-C and C-L orientations for materials in both the irradiated and unirradiated conditions for companion specimens. Fracture toughness and tensile properties of specimens cut from an SRS reactor vessel sidewall with doses of 0.1 and 0.5 dpa were also measured at temperatures of 25 and 125 degrees C. The irradiated materials exhibit hardening with loss of work hardenability and a reduction in toughness relative to the unirradiated materials. The HFIR-irradiated materials show an increase in yield strength between about 20% and 190% with a concomitant tensile strength increase between about 15% to 30%. The elastic-plastic fracture toughness parameters and Charpy-V energy absorption both decrease and show only a slight sensitivity to dose. The irradiation-induced decrease in the elastic-plastic fracture toughness (J def at 1 mm crack extension) is between 20% to 65%; the range of J 1C values are 72.8 to 366 kJ/m 2 for the irradiated materials. Similarly, Charpy V-notch results show a 40% to 60% decrease in impact energies

  9. Influence of niobium addition on the high temperature mechanical properties of a centrifugally cast HP alloy

    International Nuclear Information System (INIS)

    Andrade, A.R.; Bolfarini, C.; Ferreira, L.A.M.; Vilar, A.A.A.; Souza Filho, C.D.; Bonazzi, L.H.C.

    2015-01-01

    The influence of niobium addition on the mechanical properties at high temperature of HP alloy has been investigated. Two HP alloys were centrifugally cast with a similar chemical composition differing only in the niobium content. Low strain rate high temperature tensile tests and creep-rupture tests were performed in the range of 900–1100 °C, and the results compared between the alloys. According to the results, the high temperature mechanical behavior of both alloys is controlled by several factors like solid solution, network of eutectic carbides, intradendritic precipitation and dendrite spacing. A significant increase in the mechanical properties for the HP alloy with niobium addition was found within the temperature range of 900–1050 °C. Beyond this temperature the mechanical behavior of both alloys is basically the same

  10. Mechanical properties of weakly segregated block copolymers : 1. Synergism on tensile properties of poly(styrene-b-n-butylmethacrylate) diblock copolymers

    NARCIS (Netherlands)

    Weidisch, R.; Michler, G.H.; Fischer, H.; Arnold, M.; Hofmann, S.; Stamm, M.

    1999-01-01

    Mechanical properties of poly(styrene-b-n-butylmethacrylate) diblock copolymers, PS-b-PBMA, with different lengths of the polystyrene block were investigated. The copolymers display a composition range where the tensile strength of the block copolymers exceeds the values of the corresponding

  11. Influence of mold temperature associated with glass fiber on the mechanical and thermal properties of a (PA6/GF/MMT) nanocomposite

    International Nuclear Information System (INIS)

    Damiani, Renato Adriano

    2017-01-01

    This work describes the second of a series of studies of the effects of injection molding conditions on the mechanical and thermal properties of Polyamide 6/Glass Fiber/Montmorillonite (PA6/GF/MMT) composites and was motivated by the lack of information about how the processing variables influence on the properties of three-phase composites containing fiber glass. By this time, the effects of the injection molding temperature associated with the fiber glass percentage on the mechanical and thermal properties of the composite are investigated. Some samples were processed, following a statistical experimental factorial planning, varying the mold temperature and the fiber glass percentage and maintaining 5 wt % of the MMT. The samples were submitted to tensile and flexural tests, XRD, SEM and DSC. The studies showed that an increase in the mold temperature and the fiber percentage improves the maximum tensile and flexural stresses. The increased mold temperature slows the cooling rate, which, over time, decreases the degree of crystallinity. However, there is an increase in the intercalation of the polymeric chains and the nanoclay lamellae, and the structure forms with fewer defects. (author)

  12. Influence of mold temperature associated with glass fiber on the mechanical and thermal properties of a (PA6/GF/MMT) nanocomposite

    Energy Technology Data Exchange (ETDEWEB)

    Damiani, Renato Adriano, E-mail: eng.damiani@hotmail.com [Universidade do Extremo Sul Catarinense (UNESC), Criciuma, SC (Brazil). Programa de Pos-Graduacao em Ciencias e Engenharia de Materiais; Duarte, Glaucea Warmeling; Riella, Humberto Gracher, E-mail: gwduarte@gmail.com, E-mail: huberto.riella@ufsc.br [Universidade Federal de Santa Catarina (UFSC), Florianopolis, SC (Brazil). Programa de Pos-Graduacao em Engenharia Quimica; Silva, Luciano Luiz; Mello, Josiane Maria Muneron de; Fiori, Marcio Antonio; Batiston, Eduardo Roberto, E-mail: marciofiori@gmail.com, E-mail: lucianols@unochapeco.edu.br, E-mail: josimello@unochapeco.edu.br, E-mail: erbatiston@unochapeco.edu.br [Universidade Comunitaria da Regiao de Chapeco (UNOCHAPECO), Chapeco, SC (Brazil)

    2017-01-15

    This work describes the second of a series of studies of the effects of injection molding conditions on the mechanical and thermal properties of Polyamide 6/Glass Fiber/Montmorillonite (PA6/GF/MMT) composites and was motivated by the lack of information about how the processing variables influence on the properties of three-phase composites containing fiber glass. By this time, the effects of the injection molding temperature associated with the fiber glass percentage on the mechanical and thermal properties of the composite are investigated. Some samples were processed, following a statistical experimental factorial planning, varying the mold temperature and the fiber glass percentage and maintaining 5 wt % of the MMT. The samples were submitted to tensile and flexural tests, XRD, SEM and DSC. The studies showed that an increase in the mold temperature and the fiber percentage improves the maximum tensile and flexural stresses. The increased mold temperature slows the cooling rate, which, over time, decreases the degree of crystallinity. However, there is an increase in the intercalation of the polymeric chains and the nanoclay lamellae, and the structure forms with fewer defects. (author)

  13. Effect of T6 heat treatment on tensile strength of EN AB-48000 alloy modified with strontium

    Directory of Open Access Journals (Sweden)

    J. Pezda

    2011-07-01

    Full Text Available Among alloys of non-ferrous metals, aluminum alloys have found their broadest application in foundry industry. Silumins are widely used in automotive, aviation and shipbuilding industries; as having specific gravity nearly three times lower than specific gravity of cast iron. The silumins can be characterized by high mechanical properties. To upgrade mechanical properties of a castings made from silumins one makes use of heat treatment, what leads to change of their structure and advantageously affects on mechanical properties of the silumins. In the paper are presented test results concerning effect of dispersion hardening on change of tensile strength of EN AB-48000 silumin modified with strontium. Investigated alloy was melted in electric resistance furnace. Temperature ranges of solution heat treatment and ageing heat treatment were selected on base of curves from ATD method, recorded for refined alloy and for modified alloy. The heat treatment resulted in change of Rm tensile strength, while performed investigations have enabled determination of temperatures and durations of solution heat treatment and ageing heat treatment, which precondition obtainment of the best tensile strength Rm of the investigated alloy.

  14. The determining impact of coiling temperature on the microstructure and mechanical properties of a titanium-niobium ultrahigh strength microalloyed steel: Competing effects of precipitation and bainite

    Energy Technology Data Exchange (ETDEWEB)

    Natarajan, V.V.; Challa, V.S.A. [Laboratory for Excellence in Advanced Steel Research, Materials Science and Engineering Program, Department of Metallurgical, Materials and Biomedical Engineering, 500 W. University Avenue, University of Texas at El Paso, El Paso, TX 79968 (United States); Misra, R.D.K., E-mail: dmisra2@utep.edu [Laboratory for Excellence in Advanced Steel Research, Materials Science and Engineering Program, Department of Metallurgical, Materials and Biomedical Engineering, 500 W. University Avenue, University of Texas at El Paso, El Paso, TX 79968 (United States); Sidorenko, D.M.; Mulholland, M.D.; Manohar, M.; Hartmann, J.E. [ArcelorMittal Global R& D Center, 3001 East Columbus Drive, East Chicago, IN 46312 (United States)

    2016-05-17

    We elucidate here the influence of coiling temperature on the microstructure and mechanical properties, in an ultrahigh strength titanium-niobium microalloyed steel. The objective was to underscore the impact of coiling temperature on the nature and distribution of microstructural constituents (including different phases, precipitates, and dislocation structure) that significantly contributed to differences in the yield and tensile strength of these steels. Depending on the coiling temperature, the microstructure consisted of either a combination of fine lath-type bainite and polygonal ferrite or polygonal ferrite together with the precipitation of microalloyed carbides of size ~2–10 nm in the matrix and at dislocations. The microstructure of steel coiled at lower temperature predominantly consisted of bainitic ferrite with lower yield strength compared to the steel coiled at higher temperature, and the yield to tensile strength ratio was 0.76. The steel coiled at higher temperature consisted of polygonal ferrite and extensive precipitation of carbides and was characterized by higher yield strength and with yield strength/tensile strength ratio of 0.936. The difference in the tensile strength was insignificant for the two coiling temperatures. The observed microstructure was consistent with the continuous cooling transformation diagram.

  15. Carbon nanotube modification using gum arabic and its effect on the dispersion and tensile properties of carbon nanotubes/epoxy nanocomposites.

    Science.gov (United States)

    Kim, Man Tae; Park, Ho Seok; Hui, David; Rhee, Kyong Yop

    2011-08-01

    In this study, the effects of a MWCNT treatment on the dispersion of MWCNTs in aqueous solution and the tensile properties of MWCNT/epoxy nanocomposites were investigated. MWCNTs were treated using acid and gum arabic, and MWCNT/epoxy nanocomposites were fabricated with 0.3 wt.% unmodified, oxidized and gum-treated MWCNTs. The dispersion states of the unmodified, oxidized, and Gum-treated MWCNTs were characterized in distilled water. The tensile strengths and elastic modulus of the three nanocomposites were determined and compared. The results indicated that the gum treatment produced better dispersion of the MWCNTs in distilled water and that gum-treated MWCNT/epoxy nanocomposites had a better tensile strength and elastic modulus than did the unmodified and acid-treated MWCNT/epoxy nanocomposites. Scanning electron microscope examination of the fracture surface showed that the improved tensile properties of the gum-treated MWCNT/epoxy nanocomposites were attributed to the improved dispersion of MWCNTs in the epoxy and to interfacial bonding between nanotubes and the epoxy matrix.

  16. Nonlinear and anisotropic tensile properties of graft materials used in soft tissue applications.

    Science.gov (United States)

    Yoder, Jonathon H; Elliott, Dawn M

    2010-05-01

    The mechanical properties of extracellular matrix grafts that are intended to augment or replace soft tissues should be comparable to the native tissue. Such grafts are often used in fiber-reinforced tissue applications that undergo multi-axial loading and therefore knowledge of the anisotropic and nonlinear properties are needed, including the moduli and Poisson's ratio in two orthogonal directions within the plane of the graft. The objective of this study was to measure the tensile mechanical properties of several marketed grafts: Alloderm, Restore, CuffPatch, and OrthADAPT. The degree of anisotropy and non-linearity within each graft was evaluated from uniaxial tensile tests and compared to their native tissue. The Alloderm graft was anisotropic in both the toe- and linear-region of the stress-strain response, was highly nonlinear, and generally had low properties. The Restore and CuffPatch grafts had similar stress-strain responses, were largely isotropic, had a linear-region modulus of 18MPa, and were nonlinear. OrthADAPT was anisotropic in the linear-region (131 MPA vs 47MPa in the toe-region) and was highly nonlinear. The Poisson ratio for all grafts was between 0.4 and 0.7, except for the parallel orientation of Restore which was greater than 1.0. Having an informed understanding of how the available grafts perform mechanically will allow for better assessment by the physician for which graft to apply depending upon its application. Copyright 2010 Elsevier Ltd. All rights reserved.

  17. Tensile and Creep Testing of Sanicro 25 Using Miniature Specimens

    Science.gov (United States)

    Dymáček, Petr; Jarý, Milan; Dobeš, Ferdinand; Kloc, Luboš

    2018-01-01

    Tensile and creep properties of new austenitic steel Sanicro 25 at room temperature and operating temperature 700 °C were investigated by testing on miniature specimens. The results were correlated with testing on conventional specimens. Very good agreement of results was obtained, namely in yield and ultimate strength, as well as short-term creep properties. Although the creep rupture time was found to be systematically shorter and creep ductility lower in the miniature test, the minimum creep rates were comparable. The analysis of the fracture surfaces revealed similar ductile fracture morphology for both specimen geometries. One exception was found in a small area near the miniature specimen edge that was cut by electro discharge machining, where an influence of the steel fracture behavior at elevated temperature was identified. PMID:29337867

  18. Tensile and Creep Testing of Sanicro 25 Using Miniature Specimens.

    Science.gov (United States)

    Dymáček, Petr; Jarý, Milan; Dobeš, Ferdinand; Kloc, Luboš

    2018-01-16

    Tensile and creep properties of new austenitic steel Sanicro 25 at room temperature and operating temperature 700 °C were investigated by testing on miniature specimens. The results were correlated with testing on conventional specimens. Very good agreement of results was obtained, namely in yield and ultimate strength, as well as short-term creep properties. Although the creep rupture time was found to be systematically shorter and creep ductility lower in the miniature test, the minimum creep rates were comparable. The analysis of the fracture surfaces revealed similar ductile fracture morphology for both specimen geometries. One exception was found in a small area near the miniature specimen edge that was cut by electro discharge machining, where an influence of the steel fracture behavior at elevated temperature was identified.

  19. Evaluating the Tensile Properties of Aluminum Foundry Alloys through Reference Castings-A Review.

    Science.gov (United States)

    Anilchandra, A R; Arnberg, Lars; Bonollo, Franco; Fiorese, Elena; Timelli, Giulio

    2017-08-30

    The tensile properties of an alloy can be exploited if detrimental defects and imperfections of the casting are minimized and the microstructural characteristics are optimized through several strategies that involve die design, process management and metal treatments. This paper presents an analysis and comparison of the salient characteristics of the reference dies proposed in the literature, both in the field of pressure and gravity die-casting. The specimens produced with these reference dies, called separately poured specimens, are effective tools for the evaluation and comparison of the tensile and physical behaviors of Al-Si casting alloys. Some of the findings of the present paper have been recently developed in the frame of the European StaCast project whose results are complemented here with some more recent outcomes and a comprehensive analysis and discussion.

  20. Evaluating the Tensile Properties of Aluminum Foundry Alloys through Reference Castings—A Review

    Science.gov (United States)

    Anilchandra, A.R.; Arnberg, Lars; Bonollo, Franco; Fiorese, Elena

    2017-01-01

    The tensile properties of an alloy can be exploited if detrimental defects and imperfections of the casting are minimized and the microstructural characteristics are optimized through several strategies that involve die design, process management and metal treatments. This paper presents an analysis and comparison of the salient characteristics of the reference dies proposed in the literature, both in the field of pressure and gravity die-casting. The specimens produced with these reference dies, called separately poured specimens, are effective tools for the evaluation and comparison of the tensile and physical behaviors of Al-Si casting alloys. Some of the findings of the present paper have been recently developed in the frame of the European StaCast project whose results are complemented here with some more recent outcomes and a comprehensive analysis and discussion. PMID:28867796

  1. Study of tensile test behavior of austenitic stainless steel type 347 seamless thin-walled tubes in cold worked condition

    Energy Technology Data Exchange (ETDEWEB)

    Terui, Clarice, E-mail: clarice.terui@marinha.mil.br [Centro Tecnológico da Marinha em São Paulo (CINA/CTMSP), Iperó, SP (Brazil). Centro Industrial Nuclear da Marinha; Lima, Nelson B. de, E-mail: nblima@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNE-SP), Sao Paulo, SP (Brazil)

    2017-07-01

    These austenitic stainless steel type 347 seamless thin-walled tubes are potential candidates to be used in fuel elements of nuclear power plants (as PWR - Pressurized Water Reactor). So, their metallurgical condition and mechanical properties, as the tensile strength and yield strength, normally are very restrict in demanding project and design requirements. Several full size tensile tests at room temperature and high temperature (315 deg C) were performed in these seamless tubes in cold-worked condition. The results of specified tensile and yield strengths were achieved but the elongation of the tube, in the geometry of the component, could not be measured at high temperature due to unconventional mode of rupture (helical mode without separation of parts). The average value of elongation was obtained from stress-strain curves of hot tensile tests and was around 5%. The results obtained in this research show that this behavior of the full size tensile test samples of thin-walled tube (wall thickness less than 0.5 mm) in high temperature (315°C) is due to the combination of the manufacturing process, the material (crystallographic structure and chemical composition) and the final geometry of the component. In other words, the strong crystallographic texture of material induced by tube drawing process in addition with the geometry of the component are responsible for the behavior in hot uniaxial tensile tests. (author)

  2. Tensile properties and water absorption assessment of linear low-Density Polyethylene/Poly (Vinyl Alcohol)/Kenaf composites: effect of eco-friendly coupling agent

    Science.gov (United States)

    Pang, A. L.; Ismail, H.; Abu Bakar, A.

    2018-02-01

    Linear low-density polyethylene (LLDPE)/poly (vinyl alcohol) (PVOH) filled with untreated kenaf (UT-KNF) and eco-friendly coupling agent (ECA)-treated kenaf (ECAT-KNF) were prepared using ThermoHaake internal mixer, respectively. Filler loadings of UT-KNF and ECAT-KNF used in this study are 10 and 40 parts per hundred parts of resin (phr). The effect of ECA on tensile properties and water absorption of LLDPE/PVOH/KNF composites were investigated. Field emission scanning electron microscopy (FESEM) analysis was applied to visualize filler-matrix adhesion. The results indicate LLDPE/PVOH/ECAT-KNF composites possess higher tensile strength and tensile modulus, but lower elongation at break compared to LLDPE/PVOH/UT-KNF composites. The morphological studies of tensile fractured surfaces using FESEM support the increment in tensile properties of LLDPE/PVOH/ECAT-KNF composites. Nevertheless, LLDPE/PVOH/UT-KNF composites reveal higher water absorption compared to LLDPE/PVOH/ECAT-KNF composites.

  3. Tensile Stress-Strain Results for 304L and 316L Stainless-Steel Plate at Temperature

    International Nuclear Information System (INIS)

    R. K. Blandford; D. K. Morton; S. D. Snow; T. E. Rahl

    2007-01-01

    The Idaho National Laboratory (INL) is conducting moderate strain rate (10 to 200 per second) research on stainless steel materials in support of the Department of Energy's (DOE) National Spent Nuclear Fuel Program (NSNFP). For this research, strain rate effects are characterized by comparison to quasi-static tensile test results. Considerable tensile testing has been conducted resulting in the generation of a large amount of basic material data expressed as engineering and true stress-strain curves. The purpose of this paper is to present the results of quasi-static tensile testing of 304/304L and 316/316L stainless steels in order to add to the existing data pool for these materials and make the data more readily available to other researchers, engineers, and interested parties. Standard tensile testing of round specimens in accordance with ASTM procedure A 370-03a were conducted on 304L and 316L stainless-steel plate materials at temperatures ranging from -20 F to 600 F. Two plate thicknesses, eight material heats, and both base and weld metal were tested. Material yield strength, Young's modulus, ultimate strength, ultimate strain, failure strength and failure strain were determined, engineering and true stress-strain curves to failure were developed, and comparisons to ASME Code minimums were made. The procedures used during testing and the typical results obtained are described in this paper

  4. Characterization of elevated temperature properties of heat exchanger and steam generator alloys

    International Nuclear Information System (INIS)

    Wright, J.K.; Carroll, L.J.; Cabet, C.; Lillo, T.M.; Benz, J.K.; Simpson, J.A.; Lloyd, W.R.; Chapman, J.A.; Wright, R.N.

    2012-01-01

    The Next Generation Nuclear Plant project is considering Alloy 800H and Alloy 617 for steam generator and intermediate heat exchangers. It is envisioned that a steam generator would operate with reactor outlet temperatures from 750 to 800 °C, while an intermediate heat exchanger for primary to secondary helium would operate up to an outlet temperature of 950 °C. Although both alloys are of interest due in part to their technical maturity, a number of specific properties require further characterization for design of nuclear components. Strain rate sensitivity of both alloys has been characterized and is found to be significant above 600 °C. Both alloys also exhibit dynamic strain aging, characterized by serrated flow, over a wide range of temperatures and strain rates. High temperature tensile testing of Alloy 617 and Alloy 800H has been conducted over a range of temperatures. Dynamic strain aging is a concern for these materials since it is observed to result in reduced ductility for many solid solution alloys. Creep, fatigue, and creep–fatigue properties of Alloy 617 have been measured as well, with the goal of determining the influence of the temperature, strain rate and atmosphere on the creep–fatigue life of Alloy 617. Elevated temperature properties and implications for codification of the alloys will be described.

  5. Miniature tensile test specimens for fusion reactor irradiation studies

    International Nuclear Information System (INIS)

    Klueh, R.L.

    1985-01-01

    Three miniature sheet-type tensile specimens and a miniature rod-type specimen are being used to determine irradiated tensile properties for alloy development for fusion reactors. The tensile properties of type 316 stainless steel were determined with these different specimens, and the results were compared. Reasonably good agreement was observed. However, there were differences that led to recommendations on which specimens are preferred. 4 references, 9 figures, 6 tables

  6. Effect of tungsten content on the microstructure and tensile properties of Ni–xW–6Cr alloys

    Energy Technology Data Exchange (ETDEWEB)

    Liu, Shulin [Center for Thorium Molten Salt Reactor System, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); University of Chinese Academy of Sciences, Beijing 100049 (China); Ye, Xiang-Xi, E-mail: yexiangxi@sinap.ac.cn [Center for Thorium Molten Salt Reactor System, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); Jiang, Li [Center for Thorium Molten Salt Reactor System, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); University of Chinese Academy of Sciences, Beijing 100049 (China); Cui, Chuanyong [Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016 (China); Li, Zhijun, E-mail: lizhijun@sinap.ac.cn [Center for Thorium Molten Salt Reactor System, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); Huang, Hefei; Leng, Bin [Center for Thorium Molten Salt Reactor System, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); Zhou, Xingtai, E-mail: zhouxingtai@sinap.ac.cn [Center for Thorium Molten Salt Reactor System, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China)

    2016-02-08

    Ni–xW–6Cr alloys have been considered as one of the potential structural materials for molten salt techniques, whereas their microstructure and mechanical performance have not been sufficiently studied. In this study, the microstructure and tensile deformation behavior of Ni–(10–35 wt%)W–6Cr alloys have been systematically investigated. The phase diagram calculations indicated that the solubility limit of W is 34 wt% in Ni–xW–6Cr alloy. α-W phase is formed in the matrix while the W content exceeds such limit. The fracture of the Ni–(10–35 wt%)W–6Cr alloys at room temperature is in the transgranular ductile fracture mode. The tensile properties of alloys, except for the elongation of Ni–35 wt%W–6Cr alloy, are improved with the increase of W content, which can be explained by the larger lattice distortion, the lower stack fault energy and the higher length fraction of twin boundaries (Σ3 and Σ9 type) in the Ni–(10–35 wt%)W–6Cr alloys caused by the addition of more W. The reduced elongation of the Ni–35 wt%W–6Cr alloy is ascribed to the particles in α-W phase which act as the main nucleation sites for cracking.

  7. High-temperature irradiation effects on mechnical properties of HTGR graphites

    International Nuclear Information System (INIS)

    Oku, Tatsuo; Eto, Motokuni; Fujisaki, Katsuo

    1978-04-01

    The irradiation effects on stress-strain relation, Young's modulus, tensile strength, bending strength and compressive strength of HTGR graphites were studied in irradiation temperature ranges of 200 - 300 0 C and 800 - 1400 0 C and in neutron fluences up to 7.4 x 10 20 n/cm 2 and 3 x 10 21 n/cm 2 (> 0.18 MeV). Fracture criteria and strain energy to fracture of the unirradiated and the irradiated graphites were also examined. (1) Neutron fluence dependences are similar in Young's modulus, tensile strength and bending strength. (2) The change of compressive strength and of tensile and bending strengths with neutron fluence differ; the former varies with graphite kind. (3) At lower irradiation temperatures the bending fracture strain energy decreases with increasing neutron fluence and at higher irradiation temperatures it increases. (4) The fracture criteria of graphites deviates from the constant strain energy theory (α = 0.5) and the constant strain theory (α = 1), shifting from α asymptotically equals 0.5 to α asymptotically equals 1 with increasing irradiation temperature. (auth.)

  8. High performance thermoplastics: A review of neat resin and composite properties

    Science.gov (United States)

    Johnston, Norman J.; Hergenrother, Paul M.

    1987-01-01

    A review was made of the principal thermoplastics used to fabricate high performance composites. Neat resin tensile and fracture toughness properties, glass transition temperatures (Tg), crystalline melt temperatures (Tm) and approximate processing conditions are presented. Mechanical properties of carbon fiber composites made from many of these thermoplastics are given, including flexural, longitudinal tensile, transverse tensile and in-plane shear properties as well as short beam shear and compressive strengths and interlaminar fracture toughness. Attractive features and problems involved in the use of thermo-plastics as matrices for high performance composites are discussed.

  9. Tensile behavior of irradiated manganese-stabilized stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Klueh, R.L. [Oak Ridge National Lab., TN (United States)

    1996-10-01

    Tensile tests were conducted on seven experimental, high-manganese austenitic stainless steels after irradiation up to 44 dpa in the FFTF. An Fe-20Mn-12Cr-0.25C base composition was used, to which various combinations of Ti, W, V, B, and P were added to improve strength. Nominal amounts added were 0.1% Ti, 1% W, 0.1% V, 0.005% B, and 0.03% P. Irradiation was carried out at 420, 520, and 600{degrees}C on the steels in the solution-annealed and 20% cold-worked conditions. Tensile tests were conducted at the irradiation temperature. Results were compared with type 316 SS. Neutron irradiation hardened all of the solution-annealed steels at 420, 520, and 600{degrees}C, as measured by the increase in yield stress and ultimate tensile strength. The steel to which all five elements were added to the base composition showed the least amount of hardening. It also showed a smaller loss of ductility (uniform and total elongation) than the other steels. The total and uniform elongations of this steel after irradiation at 420{degrees}C was over four times that of the other manganese-stabilized steels and 316 SS. There was much less difference in strength and ductility at the two higher irradiation temperatures, where there was considerably less hardening, and thus, less loss of ductility. In the cold-worked condition, hardening occured only after irradiation at 420{degrees}C, and there was much less difference in the properties of the steels after irradiation. At the 420{degrees}C irradiation temperature, most of the manganese-stabilized steels maintained more ductility than the 316 SS. After irradiation at 420{degrees}C, the temperature of maximum hardening, the steel to which all five of the elements were added had the best uniform elongation.

  10. Status of automated tensile machine

    International Nuclear Information System (INIS)

    Satou, M.; Hamilton, M.L.; Sato, S.; Kohyama, A.

    1992-01-01

    The objective of this work is to develop the Monbusho Automated Tensile machine (MATRON) and install and operate it at the Pacific Northwest Laboratory (PNL). The machine is designed to provide rapid, automated testing of irradiated miniature tensile specimen in a vacuum at elevated temperatures. The MATRON was successfully developed and shipped to PNL for installation in a hot facility. The original installation plan was modified to simplify the current and subsequent installations, and the installation was completed. Detailed procedures governing the operation of the system were written. Testing on irradiated miniature tensile specimen should begin in the near future

  11. Effects of Electromagnetic Stirring on the Microstructure and High-Temperature Mechanical Properties of a Hyper-eutectic Al-Si-Cu-Ni Alloy

    Science.gov (United States)

    Jang, Youngsoo; Choi, Byounghee; Kang, Byungkeun; Hong, Chun Pyo

    2015-02-01

    A liquid treatment method by electromagnetic stirring was applied to a hyper-eutectic Al-15wt pctSi-4wt pctCu-3wt pctNi alloy for the piston manufacturing with diecasting process in order to improve high-temperature mechanical properties of the piston heads. The mechanical properties, such as hardness, high-temperature tensile stress, thermal expansion, and high-temperature relative wear resistance, were estimated using the specimens taken from the liquid-treated diecast products, and the results were compared with those of a conventional metal-mold-cast piston.

  12. Effect of tempering upon the tensile properties of a nanostructured bainitic steel

    International Nuclear Information System (INIS)

    Hasan, H.S.; Peet, M.J.; Avettand-Fènoël, M-N.; Bhadeshia, H.K.D.H.

    2014-01-01

    The tensile properties of a nanostructured carbide-free bainitic steel formed at 200–250 °C are compared against those after tempering sufficiently to remove the retained austenite. Although significant ductility is observed following tempering, a comparison of tempered and untempered samples shows that it is in fact reduced when a comparison is made at identical strength. The shape of the stress–strain curves shows clear evidence that the capacity for work hardening is reduced with the loss of austenite. The nanostructure of the steel transformed at 250 °C is examined by transmission electron microscopy, to compare the as-transformed to the tempered structure. In this case after tempering at 500 °C the energy absorbed during the tensile test is lower, due to the lower strength. Reduction of strength is caused by the slight coarsening of the bainite plates, and lower dislocation density after tempering. Considering the formation of carbide particles in high strength steel, impressive ductility is exhibited even in the tempered condition

  13. Effect of tempering upon the tensile properties of a nanostructured bainitic steel

    Energy Technology Data Exchange (ETDEWEB)

    Hasan, H.S. [University of Technology, Baghdad (Iraq); Peet, M.J., E-mail: mjp54@cam.ac.uk [Department of Materials Science and Metallurgy, 27 Charles Babbage Road, Cambridge CB3 0FS (United Kingdom); Avettand-Fènoël, M-N. [Unité Matériaux Et Transformations (UMET) UMR CNRS 8207, Université, Lille 1, 59655 Villeneuve D' ASCQ (France); Bhadeshia, H.K.D.H. [Department of Materials Science and Metallurgy, 27 Charles Babbage Road, Cambridge CB3 0FS (United Kingdom)

    2014-10-06

    The tensile properties of a nanostructured carbide-free bainitic steel formed at 200–250 °C are compared against those after tempering sufficiently to remove the retained austenite. Although significant ductility is observed following tempering, a comparison of tempered and untempered samples shows that it is in fact reduced when a comparison is made at identical strength. The shape of the stress–strain curves shows clear evidence that the capacity for work hardening is reduced with the loss of austenite. The nanostructure of the steel transformed at 250 °C is examined by transmission electron microscopy, to compare the as-transformed to the tempered structure. In this case after tempering at 500 °C the energy absorbed during the tensile test is lower, due to the lower strength. Reduction of strength is caused by the slight coarsening of the bainite plates, and lower dislocation density after tempering. Considering the formation of carbide particles in high strength steel, impressive ductility is exhibited even in the tempered condition.

  14. Correlation of fracture toughness with tensile properties for irradiated 20% cold-worked 316 stainless steel

    International Nuclear Information System (INIS)

    Hamilton, M.L.; Garner, F.A.; Wolfer, W.G.

    1983-08-01

    A correlation has been developed which allows an estimate to be made of the toughness of austenitic alloys using more easily obtained tensile data. Tensile properties measured on 20% cold-worked AISI 316 specimens made from ducts and cladding irradiated in EBR-II were used to predict values for the plane strain fracture toughness according to a model originally developed by Krafft. Some microstructural examination is required to determine a parameter designated as the process zone size. In contrast to the frequently employed Hahn-Rosenfeld model, this model gives results which agree with recent experimental determinations of toughness performed in the transgranular failure regime

  15. Analysis on High Temperature Aging Property of Self-brazing Aluminum Honeycomb Core at Middle Temperature

    Directory of Open Access Journals (Sweden)

    ZHAO Huan

    2016-11-01

    Full Text Available Tension-shear test was carried out on middle temperature self-brazing aluminum honeycomb cores after high temperature aging by micro mechanical test system, and the microstructure and component of the joints were observed and analyzed using scanning electron microscopy and energy dispersive spectroscopy to study the relationship between brazing seam microstructure, component and high temperature aging properties. Results show that the tensile-shear strength of aluminum honeycomb core joints brazed by 1060 aluminum foil and aluminum composite brazing plate after high temperature aging(200℃/12h, 200℃/24h, 200℃/36h is similar to that of as-welded joints, and the weak part of the joint is the base metal which is near the brazing joint. The observation and analysis of the aluminum honeycomb core microstructure and component show that the component of Zn, Sn at brazing seam is not much affected and no compound phase formed after high temperature aging; therefore, the main reason for good high temperature aging performance of self-brazing aluminum honeycomb core is that no obvious change of brazing seam microstructure and component occurs.

  16. Influence of grain size on the tensile and creep properties of a type 316 stainless steel

    International Nuclear Information System (INIS)

    Mannan, S.L.; Samuel, K.G.; Rodriguez, P.

    The influence of grain size, on the tensile deformation behaviour in the temperature range 300-1223 K and on the creep rate at 873 and 973 K over a wide range of applied stresses, in a type 316 stainless steel has been investigated. For the tensile results, the Hall-Petch relation was found to be valid up to 1023 K. The variations of flow stress and work hardening rate with temperature and grain size have been found to be influenced by dynamic strain aging which occurs in the temperature range 523-923 K. The creep experiments revealed that grain boundaries contribute to strengthening at high stresses (180-260 MPa) at 873 K but this strengthening does not correlate with the available models which attempt to incorporate the Hall-Petch strengthening effect into creep rate equations. At 973 K the creep rate was generally constant but increased at small grain sizes and at lower stresses due to increased contribution from grain boundary sliding. The difference in the grain size effects on creep at the two temperatures is attributed to the difference in the substructures developed during creep. (author)

  17. Report on Understanding and Predicting Effects of Thermal Aging on Microstructure and Tensile Properties of Grade 91 Steel for Structural Components

    Energy Technology Data Exchange (ETDEWEB)

    Li, Meimei [Argonne National Lab. (ANL), Argonne, IL (United States); Natesan, K. [Argonne National Lab. (ANL), Argonne, IL (United States); Chen, Weiying [Argonne National Lab. (ANL), Argonne, IL (United States)

    2017-08-01

    This report provides an update on understanding and predicting the effects of long-term thermal aging on microstructure and tensile properties of G91 to corroborate the ASME Code rules in strength reduction due to elevated temperature service. The research is to support the design and long-term operation of G91 structural components in sodium-cooled fast reactors (SFRs). The report is a Level 2 deliverable in FY17 (M2AT-17AN1602017), under the Work Package AT-17AN160201, “SFR Materials Testing” performed by the Argonne National Laboratory (ANL), as part of the Advanced Reactor Technologies Program.

  18. Effect of Manufacturing Method to Tensile Properties of Hybrid Composite Reinforced by Natural (Agel Leaf Fiber) and Glass Fibers

    Science.gov (United States)

    Nugroho, A.; Abdurohman, K.; Kusmono; Hestiawan, H.; Jamasri

    2018-04-01

    This paper described the effect of different type of manufacturing method to tensile properties of hybrid composite woven agel leaf fiber and glass fiber as an alternative of LSU structure material. The research was done by using 3 ply of woven agel leaf fiber (ALF) and 3 ply of glass fiber (wr200) while the matrix was using unsaturated polyester. Composite manufacturing method used hand lay-up and vacuum bagging. Tensile test conducted with Tensilon universal testing machine, specimen shape and size according to standard size ASTM D 638. Based on tensile test result showed that the tensile strength of agel leaf fiber composite with unsaturated polyester matrix is 54.5 MPa by hand lay-up and 84.6 MPa with vacuum bagging method. From result of tensile test, hybrid fiber agel composite and glass fiber with unsaturated polyester matrix have potential as LSU structure.

  19. Novel strip-cast Mg/Al clad sheets with excellent tensile and interfacial bonding properties.

    Science.gov (United States)

    Kim, Jung-Su; Lee, Dong Ho; Jung, Seung-Pill; Lee, Kwang Seok; Kim, Ki Jong; Kim, Hyoung Seop; Lee, Byeong-Joo; Chang, Young Won; Yuh, Junhan; Lee, Sunghak

    2016-06-01

    In order to broaden industrial applications of Mg alloys, as lightest-weight metal alloys in practical uses, many efforts have been dedicated to manufacture various clad sheets which can complement inherent shortcomings of Mg alloys. Here, we present a new fabrication method of Mg/Al clad sheets by bonding thin Al alloy sheet on to Mg alloy melt during strip casting. In the as-strip-cast Mg/Al clad sheet, homogeneously distributed equi-axed dendrites existed in the Mg alloy side, and two types of thin reaction layers, i.e., γ (Mg17Al12) and β (Mg2Al3) phases, were formed along the Mg/Al interface. After post-treatments (homogenization, warm rolling, and annealing), the interfacial layers were deformed in a sawtooth shape by forming deformation bands in the Mg alloy and interfacial layers, which favorably led to dramatic improvement in tensile and interfacial bonding properties. This work presents new applications to multi-functional lightweight alloy sheets requiring excellent formability, surface quality, and corrosion resistance as well as tensile and interfacial bonding properties.

  20. Research on hardness and tensile properties of A390 alloy with tin addition

    Science.gov (United States)

    Si, Yi

    2018-03-01

    The effect of tin content on hardness and tensile properties of A390 alloys has been discussed. The microstructure of the A390 alloy with tin addition has been surveyed by OM and investigated by SEM. Research showed that β-Sn in the alloy precipitation forms were mainly small blocks and thin strips, particles within the Al2Cu network or large blocks consisting of β-Sn and Al2Cu on Al/Si interfaces or α-Al grain boundaries. Spheroidization of the primary and eutectic silicon was improved due to Sn accretion. With the augment of element tin, hardness of casting alloy is much higher than that of alloy after heat treatment. The elongation and ultimate tensile strength (UTS) were increased in Sn addition from 0 to 1%, which is attributed to the multiple action of Sn.

  1. Tensile and Compressive Responses of Ceramic and Metallic Nanoparticle Reinforced Mg Composites

    Directory of Open Access Journals (Sweden)

    Quy Bau Nguyen

    2013-05-01

    Full Text Available In the present study, room temperature mechanical properties of pure magnesium, Mg/ZrO2 and Mg/(ZrO2 + Cu composites with various compositions are investigated. Results revealed that the use of hybrid (ZrO2 + Cu reinforcements in Mg led to enhanced mechanical properties when compared to that of single reinforcement (ZrO2. Marginal reduction in mechanical properties of Mg/ZrO2 composites were observed mainly due to clustering of ZrO2 particles in Mg matrix and lack of matrix grain refinement. Addition of hybrid reinforcements led to grain size reduction and uniform distribution of hybrid reinforcements, globally and locally, in the hybrid composites. Macro- and micro- hardness, tensile strengths and compressive strengths were all significantly increased in the hybrid composites. With respect to unreinforced magnesium, failure strain was almost unchanged under tensile loading while it was reduced under compressive loading for both Mg/ZrO2 and Mg/(ZrO2 + Cu composites.

  2. A comparative study on the tensile and impact properties of Kevlar, carbon, and S-glass/epoxy composites reinforced with SiC particles

    Science.gov (United States)

    Bulut, Mehmet; Alsaadi, Mohamad; Erkliğ, Ahmet

    2018-02-01

    Present study compares the tensile and impact characteristics of Kevlar, carbon and glass fiber reinforced composites with addition of microscale silicon carbide (SiC) within the common matrix of epoxy. The variation of tensile and impact strength values was explored for different content of SiC in the epoxy resin by weight (0, 5, 10, 15 and 20 wt%). Resulting failure characteristics were identified by assisting Charpy impact tests. The influence of interfacial adhesion between particle and fiber/matrix on failure and tensile properties was discussed from obtained results and scanning electron microscopy (SEM) figures. It is concluded from results that the content of SiC particles, and fiber types used as reinforcement are major parameters those effecting on tensile and impact resistance of composites as a result of different interface strength properties between particle-matrix and particle-fiber.

  3. Microstructure and Tensile Behavior of Al8Co17Cr17Cu8Fe17Ni33 (at.%) High-Entropy Alloy

    Science.gov (United States)

    Daoud, H. M.; Manzoni, A.; Völkl, R.; Wanderka, N.; Glatzel, U.

    2013-12-01

    Microstructure evolution and tensile behavior of the high-entropy alloy Al8Co17Cr17Cu8Fe17Ni33 (at.%) are investigated at room temperature and at 500°C in the as-cast state and under different heat-treatment conditions. Detailed microstructural characterizations are carried out using optical microscopy, scanning electron microscopy, and transmission electron microscopy. The equilibrium phase evolution as a function of temperature was calculated using the Thermo-Calc software (Thermo-Calc Software, Stockholm, Sweden) integrated with TTNi-7 database. The observed majority phase is a face-centered cubic solid solution for all tested specimens. Tensile ductility at room temperature and at elevated temperature is enhanced by heat treatment at 1150°C. An embrittlement phenomenon has been observed after a heat treatment at 700°C resulting in significant degradation in tensile properties.

  4. Phase stability and tensile properties of Co-free Al0.5CrCuFeNi2 high-entropy alloys

    International Nuclear Information System (INIS)

    Ng, Chun; Guo, Sheng; Luan, Junhua; Wang, Qing; Lu, Jian; Shi, Sanqiang; Liu, C.T.

    2014-01-01

    Highlights: • The solid solution phase in the high-entropy alloy was confirmed to be metastable. • The alloy exhibited microstructural and mechanical stability against annealing. • Only as-cast alloys showed sufficient tensile plasticity. • A large variability of the measured tensile properties was recorded. • The alloys showing slip banding behavior did not necessarily have tensile ductility. -- Abstract: High-entropy alloys (HEAs) are becoming new research frontiers in the metallic materials field. The phase stability of HEAs is of critical significance, but a convincing understanding on it has been somewhat held back by the slow diffusion kinetics, which prevents the completion of diffusion assisted phase transformations toward the equilibrium state. Here a unique methodology, combining both the thermomechanical treatments and thermodynamic calculations, was employed to reveal the phase stability of HEAs, exemplified using the newly developed Al 0.5 CrCuFeNi 2 alloy. The metastable nature of the solid solution phases in this high-entropy alloy was uncovered through thermomechanical treatments induced phase transformations, and supported by the thermodynamic calculations. Meanwhile, the tensile properties for both the as-cast and thermomechanically treated alloys were measured, and correlated to their indentation behavior

  5. A study of tensile and thermal properties of 3D printed conductive ABS - ZnO composite

    Science.gov (United States)

    Aw, Y. Y.; Yeoh, C. K.; Idris, M. A.; Amali, H. K.; Aqzna, S. S.; Teh, P. L.

    2017-04-01

    Research into 3D printed composites are interesting because the properties of 3D printed components are usually insufficient for robust engineering applications. In this paper, conductive ABS - ZnO composites were successfully fabricated using a 3D printer. Tensile strength increases when filler loading increases up to 11wt%. Dynamic storage modulus of the conductive ABS-ZnO composite increases with the addition of ZnO filler, indicating stiffness enhancement of the composites. Higher loss modulus is also observed on samples with ZnO filler. Thermal conductivity increases from 0.2204 W/mK to 0.3508 W/mK when the filler concentration increases to 14wt% due to the formation of conductive network among fillers within the polymer matrix. With these promising tensile and thermal properties, the 3D printed composites are suitable to be used as automobile parts.

  6. Room Temperature Mechanical Properties of A356 Alloy with Ni Additions from 0.5 Wt to 2 Wt %

    Directory of Open Access Journals (Sweden)

    Lucia Lattanzi

    2018-03-01

    Full Text Available In recent years, the influence of Ni on high-temperature mechanical properties of casting Al alloys has been extensively examined in the literature. In the present study, room temperature mechanical properties of an A356 alloy with Ni additions from 0.5 to 2 wt % were investigated. The role of Ni-based compounds and eutectic Si particles in reinforcing the Al matrix was studied with image analysis and was then related to tensile properties and microhardness. In the as-cast condition, the formation of the 3D network is not sufficient to determine an increase of mechanical properties of the alloys since fracture propagates by cleavage through eutectic Si particles and Ni aluminides or by the debonding of brittle phases from the aluminum matrix. After T6 heat treatment the increasing amount of Ni aluminides, due to further addition of Ni to the alloy, together with their brittle behavior, leads to a decrease of yield strength, ultimate tensile strength, and Vickers microhardness. Despite the fact that Ni addition up to 2 wt % hinders spheroidization of eutectic Si particles during T6 heat treatment, it also promotes the formation of a higher number of brittle Ni-based compounds that easily promote fracture propagation.

  7. Effects of the TiC Nanoparticle on Microstructures and Tensile Properties of Selective Laser Melted IN718/TiC Nanocomposites

    Science.gov (United States)

    Yao, Xiling; Moon, Seung Ki; Lee, Bing Yang; Bi, Guijun

    2018-03-01

    The purpose of this paper is to investigate the effects of TiC nanoparticle content on microstructures and tensile properties of the IN718/TiC nanocomposites fabricated by selective laser melting (SLM). 0.5wt%, 1.0wt%, and 2.0wt% of TiC nanoparticles are added to the IN718 powders. The bulk-form IN718/TiC nanocomposites with different TiC contents are fabricated in-situ by SLM using the same process settings. The evolution of microstructures and tensile properties as the effect of changing the TiC content is studied using the optical microscopy, scanning electron microscopy, X-ray diffraction analysis, and tensile testing. The increase of TiC content refines the microstructure, promotes the formation of the cellular morphology, and reduces the size and continuity of Laves precipitates. Increasing the TiC content improves the yield strength and ultimate tensile strength but decreases the ductility. The grain refinement, dislocation bowing, dislocation punching, and the reduction in Laves precipitate contribute to the strengthening effect in the IN718/TiC nanocomposites.

  8. Effect of zirconium oxide nanoparticles addition on the optical and tensile properties of polymethyl methacrylate denture base material.

    Science.gov (United States)

    Gad, Mohammed M; Abualsaud, Reem; Rahoma, Ahmed; Al-Thobity, Ahmad M; Al-Abidi, Khalid S; Akhtar, Sultan

    2018-01-01

    Polymethyl methacrylate (PMMA) is widely used for the fabrication of removable prostheses. Recently, zirconium oxide nanoparticles (nano-ZrO 2 ) have been added to improve some properties of PMMA, but their effect on the optical properties and tensile strength are neglected. The aim of this study was to investigate the effect of nano-ZrO 2 addition on the translucency and tensile strength of the PMMA denture base material. Eighty specimens (40 dumbbell-shaped and 40 discs) were prepared out of heat-polymerized acrylic resin and divided into four groups per test (n=10). The control group for each test included unreinforced acrylic, while the test groups were reinforced with 2.5, 5, and 7.5 wt% nano-ZrO 2 . Acrylic resin was mixed according to manufacturer's instructions, packed, and processed by conventional method. After polymerization, all specimens were finished, polished, and stored in distilled water at 37°C for 48±2 hours. Tensile strength (MPa) was evaluated using the universal testing machine while the specimens' translucency was examined using a spectrophotometer. Statistical analysis was carried out by SPSS using the paired sample t -test ( p ≤0.05). A scanning electron microscope was used to analyze the morphological changes and topography of the fractured surfaces. This study showed that the mean tensile strength of the PMMA in the test groups of 2.5%NZ, 5%NZ, and 7.5%NZ was significantly higher than the control group. The tensile strength increased significantly after nano-ZrO 2 addition, and the maximum increase seen was in the 7.5%NZ group. The translucency values of the experimental groups were significantly lower than those of the control group. Within the reinforced groups, the 2.5%NZ group had significantly higher translucency values when compared to the 5%NZ and 7.5%NZ groups. The addition of nano-ZrO 2 increased the tensile strength of the denture base acrylic. The increase was directly proportional to the nano-ZrO 2 concentration. The

  9. Mechanical Properties of T650-35/AFR-PE-4 at Elevated Temperatures for Lightweight Aeroshell Designs

    Science.gov (United States)

    Whitley, Karen S.; Collins, TImothy J.

    2006-01-01

    Considerable efforts have been underway to develop multidisciplinary technologies for aeroshell structures that will significantly increase the allowable working temperature for the aeroshell components, and enable the system to operate at higher temperatures while sustaining performance and durability. As part of these efforts, high temperature polymer matrix composites and fabrication technologies are being developed for the primary load bearing structure (heat shield) of the spacecraft. New high-temperature resins and composite material manufacturing techniques are available that have the potential to significantly improve current aeroshell design. In order to qualify a polymer matrix composite (PMC) material as a candidate aeroshell structural material, its performance must be evaluated under realistic environments. Thus, verification testing of lightweight PMC's at aeroshell entry temperatures is needed to ensure that they will perform successfully in high-temperature environments. Towards this end, a test program was developed to characterize the mechanical properties of two candidate material systems, T650-35/AFR-PE-4 and T650-35/RP46. The two candidate high-temperature polyimide resins, AFR-PE-4 and RP46, were developed at the Air Force Research Laboratory and NASA Langley Research Center, respectively. This paper presents experimental methods, strength, and stiffness data of the T650-35/AFR-PE-4 material as a function of elevated temperatures. The properties determined during the research test program herein, included tensile strength, tensile stiffness, Poisson s ratio, compressive strength, compressive stiffness, shear modulus, and shear strength. Unidirectional laminates, a cross-ply laminate and two eight-harness satin (8HS)-weave laminates (4-ply and 10-ply) were tested according to ASTM standard methods at room and elevated temperatures (23, 316, and 343 C). All of the relevant test methods and data reduction schemes are outlined along with

  10. Study of the Effects of High Temperatures on the Engineering Properties of Steel 42CrMo4

    Science.gov (United States)

    Brnic, Josip; Turkalj, Goran; Canadija, Marko; Lanc, Domagoj; Brcic, Marino

    2015-02-01

    The paper presents and analyzes the experimental results of the effect of elevated temperatures on the engineering properties of steel 42CrMo4. Experimental data relating to the mechanical properties of the material, the creep resistance as well as Charpy impact energy. Temperature dependence of the mentioned properties is also shown. Some of creep curves were simulated using rheological models and an analytical equation. Finally, an assessment of fracture toughness was made that was based on experimentally determined Charpy impact energy. Based on the obtained results it is visible that the tensile strength (617 MPa) and yield strength (415 MPa) have the highest value at the room temperature while at the temperature of 700 °C (973 K) these values significantly decrease. This steel can be considered resistant to creep at 400 °C (673 K), but at higher temperatures this steel can be subjected to low levels of stress in a shorter time.

  11. The MDI-Mediated Lateral Crosslinking of Polyurethane Copolymer and the Impact on Tensile Properties and Shape Memory Effect

    International Nuclear Information System (INIS)

    Chung, Yong Chan; Chung, Hyang Mi; Choi, Jae Won; Chun, Byoung Chul

    2012-01-01

    The maximum stress and strain at break remained high and stable after MDI-mediated crosslinking. Similarly, shape recovery and shape retention tests also showed excellent and reproducible results. The MDI-mediated crosslinking was responsible for the interesting tensile and shape memory results. Therefore, it was demonstrated in this investigation that the allophanate type crosslinking, unlike previous misleading information, was possible under the mild reaction conditions. Polyurethane (PU) has long been investigated due to its excellent mechanical properties, shape memory effect, and biocompatibility, and was grafted with pendant functional groups to tailor the polymer characteristics without affecting their basic structure. Actually, polyethyleneglycol has been grafted to polyurethane to improve biocompatibility in biomedical applications, and low temperature flexibility could be improved by the pendant naphthol group grafted to PU. In the field of shape memory polyurethane, mechanical and shape memory properties could be improved by terminal crosslinking with glycerol, pentaerythritol, and dextrin. Alternatively, a flexible crosslinking method was devised to demonstrate both high mechanical strength and shape recovery

  12. Influence of the final temperature of investment healting on the tensile strength and Vickers hardness of CP Ti and Ti-6Al-4V alloy

    Directory of Open Access Journals (Sweden)

    Pedro César Garcia Oliveira

    2007-02-01

    Full Text Available The aim of the work was to evaluate the influence of the temperature of investment healting on the tensile strength and Vickers hardness of CP Ti and Ti-6Al-4V alloy casting. Were obtained for the tensile strength test dumbbell rods that were invested in the Rematitan Plus investment and casting in the Discovery machine cast. Thirty specimens were obtained, fiftten to the CP Titanium and fifteen to the Ti-6Al-4V alloy, five samples to each an of the three temperatures of investment: 430ºC (control group, 480ºC and 530ºC. The tensile test was measured by means of a universal testing machine, MTS model 810, at a strain of 1.0 mm/min. After the tensile strenght test the specimens were secctioned, embedded and polished to hardness measurements, using a Vickers tester, Micromet 2100. The means values to tensile tests to the temperatures 430ºC, 480 and 530: CP Ti (486.1 - 501.16 - 498.14 -mean 495.30 MPa and Ti-6Al-4V alloy (961.33 - 958.26 - 1005.80 - mean 975.13 MPa while for the Vickers hardness the values were (198.06, 197.85, 202.58 - mean 199.50 and (352.95, 339.36, 344.76 - mean 345.69, respectively. The values were submitted to Analysis of Variance (ANOVA and Tukey,s Test that indicate differences significant only between the materials, but not between the temperature, for both the materias. It was conclued that increase of the temperature of investment its not chance the tensile strength and the Vickers hardness of the CP Titanium and Ti-6Al-4V alloy.

  13. Novel twin-roll-cast Ti/Al clad sheets with excellent tensile properties.

    Science.gov (United States)

    Kim, Dae Woong; Lee, Dong Ho; Kim, Jung-Su; Sohn, Seok Su; Kim, Hyoung Seop; Lee, Sunghak

    2017-08-14

    Pure Ti or Ti alloys are recently spot-lighted in construction industries because they have excellent resistance to corrosions, chemicals, and climates as well as various coloring characteristics, but their wide applications are postponed by their expensiveness and poor formability. We present a new fabrication process of Ti/Al clad sheets by bonding a thin Ti sheet on to a 5052 Al alloy melt during vertical-twin-roll casting. This process has merits of reduced production costs as well as improved tensile properties. In the as-twin-roll-cast clad sheet, the homogeneously cast microstructure existed in the Al alloy substrate side, while the Ti/Al interface did not contain any reaction products, pores, cracks, or lateral delamination, which indicated the successful twin-roll casting. When this sheet was annealed at 350 °C~600 °C, the metallurgical bonding was expanded by interfacial diffusion, thereby leading to improvement in tensile properties over those calculated by a rule of mixtures. The ductility was also improved over that of 5052-O Al alloy (25%) or pure Ti (25%) by synergic effect of homogeneous deformation due to excellent Ti/Al bonding. This work provides new applications of Ti/Al clad sheets to lightweight-alloy clad sheets requiring excellent formability and corrosion resistance as well as alloy cost saving.

  14. Mechanical properties of S-65C grade beryllium at elevated temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Goods, S.H. [Sandia National Lab., Livermore, CA (United States); Dombrowski, D.E.

    1998-01-01

    Tensile property measurements and fractographic analysis of S-65C beryllium are reviewed. Tests were performed on specimens oriented in the longitudinal and transverse directions with respect to the direction of vacuum hot-pressing. Specimens were tested in air at RT, 100degC, 200degC, 300degC, 415degC and 500degC at an initial strain rate of 1.1 x 10{sup -4} sec{sup -1}. Ductility of the material was strongly affected by the test temperature, exhibiting a peak ductility at 300degC. The material displayed a yield point phenomenon which was most pronounced at this same temperature. Scanning electron microscopy was performed on the resulting fracture surfaces and observations are reported. (author)

  15. Effects of tempering temperature on microstructural evolution and mechanical properties of high-strength low-alloy D6AC plasma arc welds

    Energy Technology Data Exchange (ETDEWEB)

    Lin, Chun-Ming, E-mail: chunming@ntut.edu.tw [Department of Mechanical Engineering, National Taipei University of Technology, Taipei 10608, Taiwan (China); Lu, Chi-Hao [Department of Mechanical Engineering, National Taiwan University of Science and Technology, Taipei 10673, Taiwan (China)

    2016-10-31

    This study prepared high-strength low-alloy (HSLA) D6AC weldments using a plasma arc welding (PAW) process. The PAW weldments were then tempered at temperatures of 300 °C, 450 °C, and 600 °C for 1000 min. Microstructural characteristics of the weld in as-welded HSLA-D6AC, tempered D6AC, and tensile-tested D6AC were observed via optical microscopy (OM). We also investigated the hardness, tensile strength, and V-notched tensile strength (NTS) of the tempered specimens using a Vickers hardness tester and a universal testing machine. The fracture surfaces of the specimens were observed using a scanning electron microscope (SEM). Our results show that the mechanical properties and microstructural features of the HSLA weldments are strongly dependent on tempering temperature. An increase in tempering temperature led to a decrease in the hardness and tensile strength of the weldments but led to an increase in ductility. These effects can be attributed to the transformation of the microstructure and its effect on fracture characteristics. The specimens tempered at 300 °C and 450 °C failed in a ductile-brittle manner due to the presence of inter-lath austenite in the microstructure. After tempering at a higher temperature of 600 °C, martensite embrittlement did not occur, such that specimens failure was predominantly in a ductile manner. In the NTS specimens, an increase in tempering temperature led to a reduction in tensile strength due to notch embrittlement and the effects of grain boundary thickening and sliding. Our findings provide a valuable reference for the application of HSLA-D6AC steel in engineering and other fields.

  16. Effect of heat treatment operations on the Rm tensile strength of silumins

    Directory of Open Access Journals (Sweden)

    J. Pezda

    2010-10-01

    Full Text Available Owing to good technological properties, low weight and good corrosion resistance, aluminum-silicon alloys are widely used as a material for cast machinery components. State of macro- and microstructure of a castings manufactured from Al-Si alloys, which is determined by a shape and distribution of hardening phases, segregation of alloying constituents and impurities, as well as distribution of porosity, create conditions to obtainment of proper mechanical properties. These properties can be improved through modification of the alloy and performed heat treatment operations. The paper presents effect of modification and heat treatment process on the Rm tensile strength of a selected silumins (EN AB-AlSi9Cu3(Fe, EN AB-AlSi12CuNiMg, EN AB-AlSi17Cu1Ni1Mg. Investigated alloys were put to treatments of refining and modification, and next to heat treatment. Temperature range of the heat treatment operations was determined on base of curves from the ATD method. Obtained results illustrate registered curves of melting and solidification from the ATD method and strength tests. On base of performed initial tests one determined parameters of the heat treatment process (temperature and duration of solutionig and ageing treatments enabling obtainment of improved Rm tensile strength of the investigated alloys.

  17. High-temperature transient creep properties of CANDU pressure tubes

    International Nuclear Information System (INIS)

    Fong, R.W.L.; Chow, C.K.

    2002-06-01

    During a hypothetical large break loss-of-coolant accident (LOCA), the coolant flow would be reduced in some fuel channels and would stagnate and cause the fuel temperature to rise and overheat the pressure tube. The overheated pressure tube could balloon (creep radially) into contact with its moderator-cooled calandria tube. Upon contact, the stored thermal energy in the pressure tube is transferred to the calandria tube and into the moderator, which acts as a heat sink. For safety analyses, the modelling of fuel channel deformation behaviour during a large LOCA requires a sound knowledge of the high-temperature creep properties of Zr-2.5Nb pressure tubes. To this extent, a ballooning model to predict pressure-tube deformation was developed by Shewfelt et al., based on creep equations derived using uniaxial tensile specimens. It has been recognized, however, that there is an inherent variability in the high-temperature creep properties of CANDU pressure tubes. The variability, can be due to different tube-manufacturing practices, variations in chemical compositions, and changes in microstructure induced by irradiation during service in the reactor. It is important to quantify the variability of high-temperature creep properties so that accurate predictions on pressure-tube creep behaviour can be made. This paper summarizes recent data obtained from high-temperature uniaxial creep tests performed on specimens taken from both unirradiated (offcut) and irradiated pressure tubes, suggesting that the variability is attributed mainly to the initial differences in microstructure (grain size, shape and preferred orientation) and also from tube-to-tube variations in chemical composition, rather than due to irradiation exposure. These data will provide safety analysts with the means to quantify the uncertainties in the prediction of pressure-tube contact temperatures during a postulated large break LOCA. (author)

  18. Comparison of electromechanical properties and lattice distortions of different cuprate high temperature superconductors

    CERN Document Server

    Scheuerlein, C.; Grether, A; Rikel, M O; Hudspeth, J; Sugano, M; Ballarino, A; Bottura, L

    2016-01-01

    The electromechanical properties of different cuprate high-temperature superconductors, notably two ReBCO tapes, a reinforced and a nonreinforced Bi-2223 tape, and a Bi-2212 wire, have been studied. The axial tensile stress and strain, as well as the transverse compressive stress limits at which an irreversible critical current degradation occurs, are compared. The experimental setup has been integrated in a high-energy synchrotron beamline, and the self-field critical current and lattice parameter changes as a function of tensile stress and strain of a reinforced Bi-2223 tape have been measured simultaneously. Initially, the Bi-2223 filaments exhibit nearly linear elastic behavior up to the strain at which an irreversible degradation is observed. At 77 K, an axial Bi-2223 filament precompression of 0.09% in the composite tape and a Bi-2223 Poisson ratio ν = 0.21 have been determined.

  19. Coating of carbon nanotube fibers: variation of tensile properties, failure behavior and adhesion strength

    Directory of Open Access Journals (Sweden)

    Edith eMäder

    2015-07-01

    Full Text Available An experimental study of the tensile properties of CNT fibers and their interphasial behavior in epoxy matrices is reported. One of the most promising applications of CNT fibers is their use as reinforcement in multifunctional composites. For this purpose, an increase of the tensile strength of the CNT fibers in unidirectional composites as well as strong interfacial adhesion strength is desirable. However, the mechanical performance of the CNT fiber composites manufactured so far is comparable to that of commercial fiber composites. The interfacial properties of CNT fiber/polymer composites have rarely been investigated and provided CNT fiber/epoxy interfacial shear strength of 14.4 MPa studied by the microbond test.In order to improve the mechanical performance of the CNT fibers, an epoxy compatible coating with nano-dispersed aqueous based polymeric film formers and low viscous epoxy resin, respectively, was applied. For impregnation of high homogeneity, low molecular weight epoxy film formers and polyurethane film formers were used. The aqueous based epoxy film formers were not crosslinked and able to interdiffuse with the matrix resin after impregnation. Due to good wetting of the individual CNT fibers by the film formers, the degree of activation of the fibers was improved leading to increased tensile strength and Young’s modulus. Cyclic tensile loading and simultaneous determination of electric resistance enabled to characterize the fiber’s durability in terms of elastic recovery and hysteresis.The pull-out tests and SEM study reveal different interfacial failure mechanisms in CNT fiber/epoxy systems for untreated and film former treated fibers, on the one hand, and epoxy resin treated ones, on the other hand. The epoxy resin penetrated between the CNT bundles in the reference or film former coated fiber, forming a relatively thick CNT/epoxy composite layer and thus shifting the fracture zone within the fiber. In contrast to this

  20. Effect of sodium and strontium modifiers on microstructure and tensile properties of LM-13 Al-Si Alloy

    International Nuclear Information System (INIS)

    Tahir, Q.A.; Ikram, N.; Ahmed, R.

    2006-01-01

    During present research work LM 13 aluminium silicon alloy was prepared using high purity aluminium ingot and various master alloys of Al-Si, Al-Cu, Al-Ni, Al-Fe and Al-Mg. A gas fired crucible pit type furnace was used to prepare various heats of LM 13 alloy. Degassing procedure was carried out by using perforated bell type plunger using the degassing tablet. Modification was performed by plunging the modifier at the bottom of the crucible containing the molten metal. Three types of modifiers sodium salt, metallic sodium and strontium in the form of Al-Sr master alloy were used in order to evaluate the microstructure and tensile properties of the alloy. Degassed, unmodified and modified test samples for metallurgical testing purposes were prepared according to the standard procedures. An optical UFX-DX Nikon microscope and Hitachi S3400N scanning electron microscope were used for the observation of microstructural studies of the samples. Similarly tensile properties were determined using Autograph AG-IS series, 20KN Shimadzu Universal Tester. However hardness measurements were carried out using Shimadzu HMV micro hardness testing machine. Experimental results proved that the addition of modifiers improved the microstructures as well as the mechanical properties of the alloy. The present result also showed that sodium and strontium modifiers had almost similar beneficial effects on the microstructure but Sr-modifier showed improved tensile properties of LM 13 alloy. However, the salt method was not so effective if the same was compared to the metallic sodium and strontium modifiers. (author)

  1. Microstructure and tensile properties of selectively laser-melted and of HIPed laser-melted Ti–6Al–4V

    International Nuclear Information System (INIS)

    Qiu, Chunlei; Adkins, Nicholas J.E.; Attallah, Moataz M.

    2013-01-01

    Ti–6Al–4V samples have been prepared by selective laser melting (SLM) with varied processing conditions. Some of the samples were stress-relieved or hot isostatically pressed (HIPed). The microstructures of all samples were characterised using optical microscopy (OM), scanning electron microscopy (SEM) and X-ray diffraction (XRD) and the tensile properties measured before and after HIPing. It was found that the porosity level generally decreased with increase of laser power and laser scanning speed. Horizontally built samples were found to have a higher level of porosity than vertically built samples. The as-fabricated microstructure was dominated by columnar grains and martensites. HIPing closed the majority of the pores and also fully transformed the martensite into α and β phases. The as-fabricated microstructure exhibits very high tensile strengths but poor ductility with elongation generally smaller than 10%. The horizontally built samples show even lower elongation than vertically built samples. HIPing considerably improved ductility but led to a reduction in strength. With HIPing, the SLMed samples were found to show tensile properties comparable with those thermomechanically processed and annealed samples

  2. Applicability of Voce equation for tensile flow and work hardening behaviour of P92 ferritic steel

    International Nuclear Information System (INIS)

    Sainath, G.; Choudhary, B.K.; Christopher, J.; Isaac Samuel, E.; Mathew, M.D.

    2015-01-01

    Detailed analysis of true stress (σ)-true plastic strain (ε) data indicated that tensile flow behaviour of P92 ferritic steel can be adequately described by Voce equation at strain rates ranging from 3.16 × 10 −5 to 1.26 × 10 −3  s −1 over a temperature range 300–923 K. The steel exhibited two-stage work hardening in the variations of instantaneous work hardening rate (θ = dσ/dε) with stress. At all the strain rates, the variations in σ-ε, θ-σ and work hardening parameters associated with Voce equation with temperature exhibited three distinct temperature regimes. At intermediate temperatures, the variations in σ-ε, θ-σ and work hardening parameters with temperature and strain rate exhibited anomalous behaviour due to the occurrence of dynamic strain ageing in the steel. The shift in θ-σ towards low stresses, and rapid decrease in flow stress and work hardening parameters with increasing temperature and decreasing strain rate suggested dominance of dynamic recovery at high temperatures. - Highlights: • Tensile flow and work hardening behaviour of P92 steel has been examined. • Applicability of Voce equation to P92 steel is demonstrated. • Three temperature regimes in flow and work hardening has been observed. • Good match between predicted and the experimental tensile properties has been shown

  3. Effect of Annealing on Strain-Temperature Response under Constant Tensile Stress in Cold-Worked NiTi Thin Wire

    OpenAIRE

    Yan, Xiaojun; Van Humbeeck, Jan

    2011-01-01

    The present paper aims to understand the influence of annealing on the strain-temperature response of a cold-worked NiTi wire under constant tensile stress. It was found that transformation behavior, stress-strain relationship, and strain-temperature response of the cold-worked NiTi wire are strongly affected by the annealing temperature. Large martensitic strains can be reached even though the applied stress is below the plateau stress of the martensite phase. At all stress levels transforma...

  4. Tensile behavior and tension stiffening of reinforced concrete

    International Nuclear Information System (INIS)

    Choun, Young Sun; Seo, Jeong Moon

    2001-03-01

    For the ultimate behavior analysis of containment buildings under severe accident conditions, a clear understanding of tensile behaviors of plain and reinforced concrete is necessary. Nonlinear models for tensile behaviors of concrete are also needed. This report describe following items: tensile behaviors of plain concrete, test results of reinforced concrete panels in uniaxial and biaxial tension, tension stiffening. The tensile behaviors of reinforced concrete are significantly influenced by the properties of concrete and reinforcing steel. Thus, for a more reliable evaluation of tensile behavior and ultimate pressure capacity of a reinforced or prestressed concrete containment building, an advanced concrete model which can be considered rebar-concrete interaction effects should be developed. In additions, a crack behavior analysis method and tension stiffening models, which are based on fracture mechanics, should be developed. The model should be based on the various test data from specimens considering material and sectional properties of the containment building

  5. The Layer of Kevlar Angle-interlock Woven Fabric Effect on the Tensile Properties of Composite Materials

    Science.gov (United States)

    Xie, Wan-Chen; Guo, Xu-Yi; Yan, Tao; Zhang, Shang-Yong

    2017-09-01

    This article is based on the structure of three-dimensional angle-interlock longitudinal.The 3-layer, 5-layer, 7-layer and 9-layer of angle-interlock 3D fabrics are woven on sample weaving machine respectively with the 1500D Kevlar fiber twist filament produced by United States DuPont. At the same time, Kevlar plain weave fabric is woven, and three, five, seven and nine layers’ fabric are to be compared. In the process of VARTM composite technology, epoxy resin is matrix material, acetone is diluent, triethylene tetramine is curing agent and the five different fabrics are the reinforced materials respectively. Finally, eight different three-dimensional woven fabric composites were prepared. In this paper, the tensile properties of eight kinds of three-dimensional woven fabric composites were tested respectively.Finally, it is concluded that the five-layer angle-interlock woven fabric prepared by Kevlar fiber shows the best tensile property.

  6. Evaluation of Aluminum Alloy 2050-T84 Microstructure and Mechanical Properties at Ambient and Cryogenic Temperatures

    Science.gov (United States)

    Hafley, Robert A.; Domack, Marcia S.; Hales, Stephen J.; Shenoy, Ravi N.

    2011-01-01

    Aluminum alloy 2050 is being considered for the fabrication of cryogenic propellant tanks to reduce the mass of future heavy-lift launch vehicles. The alloy is available in section thicknesses greater than that of the incumbent aluminum alloy, 2195, which will enable designs with greater structural efficiency. While ambient temperature design allowable properties are available for alloy 2050, cryogenic properties are not available. To determine its suitability for use in cryogenic propellant tanks, tensile, compression and fracture tests were conducted on 4 inch thick 2050-T84 plate at ambient temperature and at -320degF. Various metallurgical analyses were also performed in order to provide an understanding of the compositional homogeneity and microstructure of 2050.

  7. Effect of annealing temperature on the mechanical properties of zircaloy-4 cladding

    International Nuclear Information System (INIS)

    Beauregard, R.J.; Clevinger, G.S.; Murty, K.L.

    1977-01-01

    The mechanical properties of zircaloy cladding materials are sensitive to those fabrication variables which have an effect on the preferred crystallographic orientation or texture of the finished tube. The effect of one such variable, the final annealing temperature, on various mechanical properties is examined using tube reduced zircaloy-4 fuel rod cladding annealed at temperatures from 905F to 1060F. This temperature range provides cladding with varying degrees of recrystallization including full recrystallization. Hoop creep characteristics of zircaloy cladding were studied as a function of the annealing temperature using closed-end internal pressurization tests at 750F and hoop stresses of 10, 15, 20 and 25 ksi. The critical annealing temperature at which a minimum creep strain occurs decreases as the applied stress increases. An additional test at 700F and 30 ksi hoop stress was conducted to demonstrate that the critical annealing temperature is essentially independent of the test temperature. Plausible explanations based on differing substructures developed in cold-worked stress-relieved material are forwarded. The effect of annealing temperature on the room temperature mechanical anisotropy parameters, R and P, was studied. R-parameters were determined from in situ transverse strain gage measurements in uniaxial tensile tests. P-parameters were calculated from uniaxial test data (R and yield stress) and hoop yield stress determined in biaxial, closed-end internal pressurization tests

  8. Effect of grain size on high temperature low-cycle fatigue properties of inconel 617

    International Nuclear Information System (INIS)

    Hattori, Hiroshi; Kitagawa, Masaki; Ohtomo, Akira

    1982-01-01

    The effect of grain size on the high temperature low-cycle fatigue behavior and other material strength properties of Inconel 617 was studied at 1 273 K in air. The strain controlled low-cycle fatigue tests were conducted with a symmetrical (FF type) and an asymmetrical (SF type) strain wave forms. The latter wave form was used for the evaluation of creep-fatigue interaction. The main results obtained in this study are as follows: 1) The tensile strength slightly increased with the increase of the grain diameter. On the other hand, the tensile ductility remarkabley decreased with the increase of the grain diameter. 2) The creep rupture life remarkabley increased with the increase of the grain diameter, especially at the lower stress levels. The effect of grain size on creep ductility has not detailed. 3) The low-cycle fatigue life remarkably decreased with the increase of the grain diameter, especially at the lower strain ranges. 4) The creep-fatigue life was less sensitive to the grain diameter than the fatigue life, because the grain size effects on creep and on fatigue were contrary. It is seemed that the creep-fatigue life is determined by the proportion of the creep and fatigue contribution. 5) The fatigue and creep-fatigue test results have good relations with the tensile and creep ductilities at the test temperature. (author)

  9. A novel in situ device based on a bionic piezoelectric actuator to study tensile and fatigue properties of bulk materials.

    Science.gov (United States)

    Wang, Shupeng; Zhang, Zhihui; Ren, Luquan; Zhao, Hongwei; Liang, Yunhong; Zhu, Bing

    2014-06-01

    In this work, a miniaturized device based on a bionic piezoelectric actuator was developed to investigate the static tensile and dynamic fatigue properties of bulk materials. The device mainly consists of a bionic stepping piezoelectric actuator based on wedge block clamping, a pair of grippers, and a set of precise signal test system. Tensile and fatigue examinations share a set of driving system and a set of signal test system. In situ tensile and fatigue examinations under scanning electron microscope or metallographic microscope could be carried out due to the miniaturized dimensions of the device. The structure and working principle of the device were discussed and the effects of output difference between two piezoelectric stacks on the device were theoretically analyzed. The tensile and fatigue examinations on ordinary copper were carried out using this device and its feasibility was verified through the comparison tests with a commercial tensile examination instrument.

  10. Tensile behaviour and properties of a bone analogue composite (HA, HDPE) crosslinked by gamma radiation

    International Nuclear Information System (INIS)

    Romero, G.; Smolko, Eduardo E.

    2005-01-01

    A natural composite material, hydroxyapatite (HA) and high density polyethylene (HDPE) crosslinked by ionizing radiations is been developed as a bioactive analogue material for bone replacement. Mechanical properties of the composites irradiated up to 300 kGy under tensile tests was studied. Gel content and micrographs of different composite fractures are shown. (author)

  11. Tensile properties and fracture of (α+γ) two phase stainless steel with fine grained microstructure

    International Nuclear Information System (INIS)

    Ogiyama, Hiroyuki; Tsukuda, Hitoshi; Soyama, Yoshiro

    1989-01-01

    The tensile properties and fracture of the (α+γ) two phase stainless steel with very fine γ grains were investigated. Two different microstructures with very fine γ grains can be obtianed by the thermomechanical treatments; One has both very fine γ and α grains, and the other has very fine γ and large α grains. The specimens were prepared in quenched and aged (475degC) conditions. The results obtained are as follows. The 0.2 % proof stress and tensile strength increase with the aging at 475degC for all specimens. The refinement of the γ grains plays an important role for the increase of strength in both quenched and aged conditions, and also for the ductility in the quenched condition. The refinement of α grains, however, contributes to the increase of the ductility in the aged condition. Accordingly, it is found that very good combinations of tensile strength and ductility can be achieved by the aging and the refinement of the γ and α grains (micro duplex structure). (author)

  12. Tensile and fatigue strength properties of Kevlar 29 aramid/epoxy unidirectional composites

    Energy Technology Data Exchange (ETDEWEB)

    Zweben, C.

    1981-07-22

    Static and fatigue tensile strength properties of filament wound undirectional Kevlar 29/epoxy, typical of filament wound material used in flywheel rotors, were studied. Machining techniques were developed to minimize fiber fuzzing on edges. The static modulus, normalized to 70% fiber volume fraction is 8.87 x 10/sup 6/ psi. The major Poisson's ratio is 0.37. The static composite tensile strength, normalized to 70% fiber volume fraction is 200 x 10/sup 3/ psi, corresponding to a fiber stress at failure of 286 x 10/sup 3/ psi, which is good for materials having a very high fiber volume fraction. The S-N curve for R = 0.7 was found to be quite flat. Although the techniques used in this program had previously been employed successfully to study the fatigue behavior of Kevlar 29/epoxy and Kevlar 49/epoxy unidirectional materials, we were unable to overcome the persistent problem of cohesive material failure in the tab regions. The apparent reason for this is the very low interlaminar shear strength of the filament wound material. 16 figures.

  13. Effect of porosity on the tensile properties of low ductility aluminum alloys

    Directory of Open Access Journals (Sweden)

    Gustavo Waldemar Mugica

    2004-06-01

    Full Text Available The literature contains reports of several studies correlating the porosity and mechanical properties of aluminum alloys. Most of these studies determine this correlation based on the parameter of global volumetric porosity. These reports, however, fail to separate the effects of microstructural features and porosity on alloys, though recognizing the influence of the latter on their mechanical properties. Thus, when the decrease in tensile strength due to the porosity effect is taken into account, the findings are highly contradictory. An analysis was made of the correlation between mechanical properties and global volumetric porosity and volumetric porosity in the fracture, as well as of the beta-Al5FeSi phase present in 380 aluminum alloy. Our findings indicate that mechanical properties in tension relating to global volumetric porosity lead to overestimations of the porosity effect in detriment to the mechanical properties. Moreover, the proposed models that take into account the effects of particles, both Si and beta-Al5FeSi, are unapplicable to low ductility alloys.

  14. Mechanical properties of Zr-2.5Nb pressure tube material manufactured employing forging routes for PHWR700 - Part 1: tensile behavior

    International Nuclear Information System (INIS)

    Bind, A.K.; Singh, R.N.; Sunil, Saurav; Chakravartty, J.K.; Ghosh, Agnish; Dhandharia, Priyesh; More, Nitin S.; Vijayakumar, S.; Chhatre, A.G.

    2012-01-01

    Tensile properties of Zr-2.5Nb alloy tubes produced employing forging to break the cast structure were evaluated by carrying out uni-axial tension test at temperatures between 25 and 325 degC and under strain-rate of 1.075 x 10 -4 /s for both longitudinal and transverse specimens. Both strength and elongation values were comparable for the samples obtained from front and back end of the tube. Transverse samples showed higher strength and lower uniform elongation values as compared to longitudinal samples. The yield strength of double forged material at 25 degC is higher than the PHWR700 specification of a maximum value of 586 MPa. (author)

  15. Characterization of fiber optic cables under large tensile loads

    International Nuclear Information System (INIS)

    Ogle, J.W.; Looney, L.D.; Peterson, R.T.

    1984-01-01

    Fiber optic cables designed for the Nevada Test Site (NTS) have to withstand an unusually harsh environment. Cables have been manufactured under a 6 year old DOE specification that has been slightly modified as the cable requirements are better understood. In order to better understand the cable properties a unique capability has been established at the NTS. Instrumentation has been developed to characterize the transmission properties of 1 km of fiber optic cable placed under a controlled tensile load up to 1500 lbs. The properties measured are cable tension, cable elongation, induced attenuation, attenuation vs. location, fiber strain, bandwidth, and ambient temperature. Preforming these measurements on cables from the two qualified NTS fiber optic cable manufacturers, Siecor and Andrew Corp., led to a new set of specifications

  16. Effects of irradiation at low temperature on V-4Cr-4Ti

    International Nuclear Information System (INIS)

    Alexander, D.J.; Snead, L.L.; Zinkle, S.J.

    1996-01-01

    Irradiation at low temperatures (100 to 275 degrees C) to 0.5 dpa causes significant embrittlement and changes in the subsequent room temperature tensile properties of V-4Cr-4Ti. The yield strength and microhardness at room temperature increase with increasing irradiation temperature. The tensile flow properties at room temperature show large increases in strength and a complete loss of work hardening capacity with no uniform ductility. Embrittlement, as measured by an increase in the ductile-to-brittle transition temperature, increases with increasing irradiation temperature, at least up to 275 degrees C. This embrittlement is not due to pickup of O or other interstitial solutes during the irradiation

  17. Effects of irradiation at low temperature on V-4Cr-4Ti

    Energy Technology Data Exchange (ETDEWEB)

    Alexander, D.J.; Snead, L.L.; Zinkle, S.J. [Oak Ridge National Lab., TN (United States)] [and others

    1996-10-01

    Irradiation at low temperatures (100 to 275{degrees}C) to 0.5 dpa causes significant embrittlement and changes in the subsequent room temperature tensile properties of V-4Cr-4Ti. The yield strength and microhardness at room temperature increase with increasing irradiation temperature. The tensile flow properties at room temperature show large increases in strength and a complete loss of work hardening capacity with no uniform ductility. Embrittlement, as measured by an increase in the ductile-to-brittle transition temperature, increases with increasing irradiation temperature, at least up to 275{degrees}C. This embrittlement is not due to pickup of O or other interstitial solutes during the irradiation.

  18. The effect of hot isostatic pressing on the microstructure and tensile properties of an unmodified A356-T6 cast aluminum alloy

    International Nuclear Information System (INIS)

    Ran Guang; Zhou Jingen; Wang, Q.G.

    2006-01-01

    In this paper, the effect of HIPping process on the microstructure and tensile properties of an unmodified sand cast A356-T6 aluminum alloy was studied. The microstructure and tensile fracture surfaces of the alloy were examined by transmission electron microscope (TEM), scanning electron microscope (SEM) and optical microscope. The results show that sub-grain boundaries are formed by HIPping process, and some silicon precipitates are formed at the sub-grain boundaries during aging hardening. The needle-shape precipitates are Mg 2 Si particles according to SED pattern analysis. The lattice misfit between Mg 2 Si and aluminum matrix is about 0.256% for [111] Al //[410] Mg 2 Si HIPping process significantly reduces porosity volume fraction and pore sizes and thus improves ductility. However, the tensile strength is improved very marginally due to the brittle nature of the unmodified coarse microstructure. The sub-grain boundary formed in the HIPping process has not shown significant influence on the tensile properties. For the studied alloy with large secondary dendrite arm spacing (SDAS) (above 80μm), the tensile fracture exhibits a transgranular mode (along the cell boundaries) with quasi-cleavage feature

  19. Effects of Heating Rate on the Dynamic Tensile Mechanical Properties of Coal Sandstone during Thermal Treatment

    Directory of Open Access Journals (Sweden)

    Ming Li

    2017-01-01

    Full Text Available The effects of coal layered combustion and the heat injection rate on adjacent rock were examined in the process of underground coal gasification and coal-bed methane mining. Dynamic Brazilian disk tests were conducted on coal sandstone at 800°C and slow cooling from different heating rates by means of a Split Hopkinson Pressure Bar (SHPB test system. It was discovered that thermal conditions had significant effects on the physical and mechanical properties of the sandstone including longitudinal wave velocity, density, and dynamic linear tensile strength; as the heating rates increased, the thermal expansion of the sandstone was enhanced and the damage degree increased. Compared with sandstone at ambient temperature, the fracture process of heat-treated sandstone was more complicated. After thermal treatment, the specimen had a large crack in the center and cracks on both sides caused by loading; the original cracks grew and mineral particle cracks, internal pore geometry, and other defects gradually appeared. With increasing heating rates, the microscopic fracture mode transformed from ductile fracture to subbrittle fracture. It was concluded that changes in the macroscopic mechanical properties of the sandstone were result from changes in the composition and microstructure.

  20. Tensile and Creep-Rupture Evaluation of a New Heat of Haynes Alloy 25

    International Nuclear Information System (INIS)

    Shingledecker, J.P.; Glanton, D.B.; Martin, R.L.; Sparks, B.L.; Swindeman, R.W.

    2007-01-01

    From 1999 to 2006, a program was undertaken within the Materials Science and Technology Division, formerly the Metals and Ceramics Division, of Oak Ridge National Laboratory to characterize the tensile and creep-rupture properties of a newly produced heat of Haynes alloy 25 (L-605). Tensile properties from room temperature to 1100 C were evaluated for base material and welded joints aged up to 12,000 hours at 675 C. Creep and creep-rupture tests were conducted on base metal and cross-weldments from 650 to 950 C. Pressurized tubular creep tests were conducted to evaluate multiaxial creep-rupture response of the material. Over 800,000 hours of creep test data were generated during the test program with the longest rupture tests extending beyond 38,000 hours, and the longest creep-rate experiments exceeding 40,000 hours

  1. The Effect of Corrosive Environment on Geopolymer Concrete Tensile Strength

    Directory of Open Access Journals (Sweden)

    Bayuaji Ridho

    2017-01-01

    Full Text Available This study has the purpose to explore the potential of geopolymer concrete tensile strength in particular on the effects of corrosive environments. Geopolymer concrete, concrete technology used no OPC that has advantages, one of which is durability, especially for corrosive seawater environment. In addition, geopolymer concrete with polymerization mechanism does not require large energy consumption or an environmentally friendly concept. Geopolymer concrete in this study is using a type C fly ash from PT. International Power Mitsui Operation & Maintenence Indonesia (IPMOMI Paiton. The type of alkaline activator used NaOH (14 molar and Na2SiO3. Coarse and fine aggregate used are local aggregate. Geopolymer concrete molded test specimen with dimensions of (10 × 20 cm cylinder, further heating and without heating, then maintained at room temperature and seawater up to 28 days. Then to determine the mechanical properties, the tensile strength testing is done with reference. This result of study indicates the curing of geopolymer concrete at 60 ° C for 24 hours to raise the tensile strength of geopolymer concrete.

  2. Tantalum-Addition Effect on Tensile and Creep Properties in 9Cr-0.5Mo-2W-V-Nb Steels

    International Nuclear Information System (INIS)

    Kim, Woo Gon; Kim, Sung Ho; Back, Jong Hyuk; Kim, Tae Kyu; Lee, Chan Bock

    2011-01-01

    Ferritic/martensitic steels (FMS) are being considered prospectively as cladding materials of a SFR fuel in Gen-IV nuclear systems. There are sound technical justifications for these material selections, and the adoption of the FM steels for a wide range of nuclear and non-nuclear applications has generated much industrial technology and experience. However, there are strong incentives to develop advanced materials, especially cladding, for a Gen-IV SFR. To develop an improved FM steel for the Gen-IV SFR fuel cladding in Korea, a R and D program has been progressed since 2007. Categories of materials considered in the program included 8∼12% Cr FM steels. A strong recommendation was made for the development of a high strength steel equivalent to or superior to ASTM Gr.92 steel (hereafter Gr. 92) to offset the difficulties encountered with commercial available high Cr (8∼12%) steels. Since the fuel cladding in a Gen-IV SFR would operate under higher temperatures than 600 .deg. C, contacting with liquid sodium, and be irradiated by neutrons to as high as 200dpa, the developed cladding should thus sustain both superior irradiation and temperature stabilities during its operational life. The newly developed advanced steel should also overcome severe drawbacks: mechanical properties, especially creep, are deteriorated at a higher temperature over 600 .deg. C. The aim of this study is to investigate the effect of Ta addition on the tensile and creep properties of the three alloys which are designed, manufactured and tested. Their properties are obtained and compared for developing new FM fuel cladding materials

  3. Irradiation induced tensile property change of SA 508 Cl.3 reactor pressure vessel steels

    International Nuclear Information System (INIS)

    Chi, Se-Hwan; Hong, Jun-Hwa; Kuk, Il-Hiun

    1998-01-01

    Irradiation induced tensile property change of four kinds of reactor pressure vessel steels manufactured by different steel refining process was compared based on the differences in the unirradiated and irradiated microstructure. Microvickers hardness, indentation, and miniature tensile specimen tests were conducted for mechanical property measurement and optical microscope (OM) and transmission electron microscope (TEM) were used for microstructural characterization. Specimens were 2 irradiated to a neutron fluence of 2.7x10 19 n/cm 2 (E ≥ 1 MeV) at 288 deg. C. Investigation on the unirradiated microstructures showed largely a same microstructure in that tempered acicular bainite and ferrite with bainitic phase prevailing in the unirradiated condition. Band-shaped segregations were also clearly observed except a kind of materials. A large difference in the unirradiated microstructure appeared in the grain size and carbide microstructure. Of carbide microstructures, noticeable differences were observed in the size and distribution of cementite, and bainitic lath microstructures. No noticeable changes were observed in the optical and thin film TEM microstructures after irradiation. Complicated microstructural. state of heat treated bainitic low alloy microstructure prevents easy quantification of microstructural changes due to irradiation. Apparent differences, however, were observed in the results of mechanical testing. Results of tensile testing and hardness measurement show that a steel refined by vacuum carbon deoxidation(VCD) method exhibits the highest radiation hardening behavior. Some of mechanical testing results on irradiated materials were possible to understand based on the initial microstructure, but further investigations using a wide array of sophisticated tools (for example, SANS, APFIM) are required to understand and characterize irradiation induced defects that are responsible for irradiation hardening behavior but are not revealed by

  4. Irradiation induced tensile property change of SA 508 Cl. 3 reactor pressure vessel steels

    International Nuclear Information System (INIS)

    Chi, Se Hwan; Hong, Jun Hwa; Kuk, Il Hiun

    1998-01-01

    Irradiation induced tensile property change of four kinds of reactor pressure vessel steels manufactured by different steel refining process was compared based on the differences in the miniature tensile specimen tests were conducted for mechanical property measurement and optical microscope (OM) and transmission electron microscope (TEM) were used for microstructural characterization. Specimens were irradiated to a neutron fluence of 2.7 x 10 19 n/cm 2 (E ≥ 1 MeV) at 288 deg C. Investigation on the unirradiated microstructures showed largely a same microstructure in that tempered acicular bainite and ferrite with bainitic phase prevailing in the unirradiated condition. Ban-shaped segregations were also clearly observed except a kind of materials. A large difference in the unirradiated microstructure appeared in the grain size and carbide microstructure. Of carbide microstructures, noticeable differences were observed in the size and distribution of cementite, and bainitic lath microstructures. No noticeable changes were observed in the optical and thin film TEM microstructures after irradiation. Complicated microstructural state of heat treated bainitic low alloy microstructure prevents easy quantification of microstructural changes due to irradiation. Apparent differences, however, were observed in the results of mechanical testing. Results of tensile testing and hardness measurement show that a steel refined by vacuum carbon deoxidation (VCD) method exhibits the highest radiation hardening behavior. Some of mechanical testing results on irradiated materials were possible to understand based on the initial microstructure, but further investigations using a wide array of sophisticated tools (for example, SANS, APFIM) are required to understand and characterize irradiation induced defects that are responsible for irradiation hardening behavior but are not revealed by conventional TEM. (author)

  5. Influence of adipic acid on tensile and morphology properties of linear low density polyethylene/rambutan peels flour blends

    Science.gov (United States)

    Nadhirah, A. A.; Sam, S. T.; Noriman, N. Z.; Ragunathan, S.; Ismail, H.

    2015-07-01

    This study investigate about the tensile and morphological properties of degradable polymer produced from linear low density polyethylene/rambutan peel flour (LLDPE/RPF) blends and adipic acid (AA) was used as a compatibilizer by varying the rambutan peel flour (RPF) amount from 0-25wt%. The samples were subjected to tensile and morphological tests. AA compatibilized showed higher strength compared to uncompatibilized blends. The Young's modulus for LLDPE/RPF blends increased with increasing flour content. However, the addition of adipic acid had reduced the Young's Modulus.

  6. An investigation into the room temperature mechanical properties of nanocrystalline austenitic stainless steels

    International Nuclear Information System (INIS)

    Eskandari, Mostafa; Zarei-Hanzaki, Abbas; Abedi, Hamid Reza

    2013-01-01

    Highlights: ► Strength of nanocrystalline specimens follows a trend of a remarkable rise along with a small drop in ductility in comparison to the coarse-grained one. ► Universal correlation of linear type (UTS = mτ max ) between shear punch test data and the tensile strength may be unreliable for the nanocrystalline materials. ► Actual relation between the maximum shear and ultimate tensile strength follows an empirical formula of UTS=0.013τ max 2 -25.62τ max +13049. -- Abstract: The present work has been conducted to evaluate the mechanical properties of nanostructured 316L and 301 austenitic stainless steels. The nanocrystalline structures were produced through martensite treatment which includes cold rolling followed by annealing treatment. The effect of equivalent rolling strain and annealing parameters on the room temperature mechanical behavior of the experimental alloys have been studied using the shear punch testing technique. The standard uniaxial tension tests were also carried out to adapt the related correlation factors. The microstructures and the volume fraction of phases were characterized by transmission electron microscopy and feritscopy methods, respectively. The results indicate that the strength of nanocrystalline specimens remarkably increases, but the ductility in comparison to the coarse-grained one slightly decreases. In addition the strength of nanocrystalline specimens has been increased by decreasing the annealing temperature and increasing the equivalent rolling strain. The analysis of the load–displacement data has also disclosed that the universal correlation of linear type (UTS = mτ max ) between shear punch test data and the tensile strength is somehow unreliable for the nanocrystalline materials. The results suggest that the actual relation between the maximum shear strength and ultimate tensile strength follows a second order equation of type UTS=aτ max 2 -bτ max +c.

  7. Improving High-Temperature Tensile and Low-Cycle Fatigue Behavior of Al-Si-Cu-Mg Alloys Through Micro-additions of Ti, V, and Zr

    Science.gov (United States)

    Shaha, S. K.; Czerwinski, F.; Kasprzak, W.; Friedman, J.; Chen, D. L.

    2015-07-01

    High-temperature tensile and low-cycle fatigue tests were performed to assess the influence of micro-additions of Ti, V, and Zr on the improvement of the Al-7Si-1Cu-0.5Mg (wt pct) alloy in the as-cast condition. Addition of transition metals led to modification of microstructure where in addition to conventional phases present in the Al-7Si-1Cu-0.5Mg base, new thermally stable micro-sized Zr-Ti-V-rich phases Al21.4Si4.1Ti3.5VZr3.9, Al6.7Si1.2TiZr1.8, Al2.8Si3.8V1.6Zr, and Al5.1Si35.4Ti1.6Zr5.7Fe were formed. The tensile tests showed that with increasing test temperature from 298 K to 673 K (25 °C to 400 °C), the yield stress and tensile strength of the present studied alloy decreased from 161 to 84 MPa and from 261 to 102 MPa, respectively. Also, the studied alloy exhibited 18, 12, and 5 pct higher tensile strength than the alloy A356, 354 and existing Al-Si-Cu-Mg alloy modified with additions of Zr, Ti, and Ni, respectively. The fatigue life of the studied alloy was substantially longer than those of the reference alloys A356 and the same Al-7Si-1Cu-0.5Mg base with minor additions of V, Zr, and Ti in the T6 condition. Fractographic analysis after tensile tests revealed that at the lower temperature up to 473 K (200 °C), the cleavage-type brittle fracture for the precipitates and ductile fracture for the matrix were dominant while at higher temperature fully ductile-type fracture with debonding and pull-out of cracked particles was identified. It is believed that the intermetallic precipitates containing Zr, Ti, and V improve the alloy performance at increased temperatures.

  8. Development of high temperature property database for Alloy 800H

    International Nuclear Information System (INIS)

    Yokoyama, Norio; Watanabe, Katsutoshi; Tsuji, Hirokazu; Nakajima, Hajime.

    1993-07-01

    JAERI Material Performance Database (JMPD) has been developed since 1989 in JAERI with a view to utilizing the various kinds of characteristic data of nuclear materials efficiently. Using relational database management system, PLANNER on the mainframe, the JMPD provides the retrieval supporting system, graphic and statistical analyses system. The data obtained with 7868 sets on characteristic data of metallic materials including fatigue crack growth data, etc. have been stored in the JMPD at the end of March in 1993. A ferritic superalloy, Alloy 800H is used for the structural material of the control rods of the High Temperature Engineering Test Reactor (HTTR). Thermal stress generates which might cause a severe creep damage at a reactor scram. It therefore needs to be designed with consideration on the fracture modes induced by creep deformation after neutron irradiation. The creep data (approximately 240 sets) and tensile data (approximately 100 sets) of Alloy 800H including the effects of test environment, aging treatment and neutron irradiation have been stored in the JMPD. Furthermore, using a personal computer, high temperature property database for Alloy 800H has been developed. The present report outlines the development of high temperature property database for Alloy 800H. (author)

  9. High-temperature mechanical properties and fracture mechanisms of Al–Si piston alloy reinforced with in situ TiB{sub 2} particles

    Energy Technology Data Exchange (ETDEWEB)

    Han, Gang [School of Mechanical Engineering, Beijing Institute of Technology, 5 South Zhongguancun Street, Haidian District, Beijing 100081 (China); Zhang, Weizheng, E-mail: zhangwz@bit.edu.cn [School of Mechanical Engineering, Beijing Institute of Technology, 5 South Zhongguancun Street, Haidian District, Beijing 100081 (China); Zhang, Guohua; Feng, Zengjian; Wang, Yanjun [Shandong Binzhou Bohai Piston Co., Ltd., Binzhou 256602 (China)

    2015-05-01

    In order to assess the high-temperature performance of aluminum–silicon alloy reinforced with titanium diboride particles as potential piston material, the tensile behaviors and fracture mechanisms of in situ 4 wt% TiB{sub 2}/Al–Si composite were investigated in the temperature range 25–350 °C. The tensile results revealed that the composite exhibited higher modulus than the matrix alloy at all testing temperatures, but both the matrix alloy and the composite presented similar strength levels above 200 °C. The ductility of the composite was found to be lower than that of the unreinforced matrix alloy at 25 and 200 °C, but no obvious distinction was observed at 350 °C. The effects of temperature and the presence of TiB{sub 2} particles on tensile properties of the composite had been evaluated. Fractographic morphology studies were done using scanning electron microscope, which indicated that the fracture of the composite altered from brittle to ductile mode with temperature increasing. At 25 and 200 °C, fracture was dominated by cracked silicon particles and separated TiB{sub 2} particles, while decohesion at particle–matrix interface was prevalent at 350 °C. Analysis of the fracture surfaces also showed that regions of clustered TiB{sub 2} particles were found to be the locations prone to damage in the composite at both room and high temperatures.

  10. Effects of excipients on the tensile strength, surface properties and free volume of Klucel® free films of pharmaceutical importance

    International Nuclear Information System (INIS)

    Gottnek, Mihály; Süvegh, Károly; Pintye-Hódi, Klára; Regdon, Géza

    2013-01-01

    The physicochemical properties of polymers planned to be applied as mucoadhesive films were studied. Two types of Klucel ® hydroxypropylcellulose (LF and MF) were used as film-forming polymers. Hydroxypropylcellulose was incorporated in 2 w/w% with glycerol and xylitol as excipients and lidocaine base as an active ingredient at 5, 10 or 15 w/w% of the mass of the film-forming polymer. The free volume changes of the films were investigated by positron annihilation lifetime spectroscopy, the mechanical properties of the samples were measured with a tensile strength tester and contact angles were determined to assess the surface properties of the films. It was found that the Klucel ® MF films had better physicochemical properties than those of the LF films. Klucel ® MF as a film-forming polymer with lidocaine base and both excipients at 5 w/w% exhibited physicochemical properties and good workability. The excipients proved to exert strong effects on the physicochemical properties of the tested systems and it is very important to study them intensively in preformulation studies in the pharmaceutical technology in order to utilise their benefits and to avoid any disadvantageous effects. - Highlights: • Glycerol increases, whereas xylitol decreases the free volume of both LF and MF HPC. • Both xylitol and glycerol increase the tensile strength of MF films. • The tensile strength of the MF product makes it suitable for pharmaceutical use. • The surface properties reveal a macroscopically stable film structure. • All measurements indicate a macroscopically homogeneous film structure

  11. Effect of microstructural anisotropy on the mechanical properties of K-doped tungsten rods for plasma facing components

    Energy Technology Data Exchange (ETDEWEB)

    Nogami, Shuhei, E-mail: shuhei.nogami@qse.tohoku.ac.jp; Guan, Wenhai, E-mail: wenhai.guan@jupiter.qse.tohoku.ac.jp; Fukuda, Makoto, E-mail: fukuda@jupiter.qse.tohoku.ac.jp; Hasegawa, Akira, E-mail: akira.hasegawa@qse.tohoku.ac.jp

    2016-11-01

    Highlights: • K-doping led to improve the tensile strength regardless of the test direction and temperature. • K-doping did not alter the elongation regardless of the test direction in the ductile fracture temperature range. • The ductility at lower temperature range was improved by the K-doping. • The lowest temperature of ductile fracture along both axial and radial directions decreased because of K-doping. • K-doping could suppress the influence of microstructural anisotropy on tensile properties, especially ductility, in large diameter W rods. - Abstract: The effect of microstructural anisotropy in pure tungsten (W) and potassium (K) doped W rods (20 mm in diameter) on their mechanical properties was investigated by tensile tests along the axial and radial directions at temperatures from 473 K to 1573 K and fracture analysis. K-doping led to improved tensile strength regardless of the test direction and temperature. K-doping did not alter the elongation regardless of the test direction in the temperature range showing ductile fracture. The ductility at lower temperature range was improved by the K-doping, especially in tensile tests along the radial direction. The lowest temperature of ductile fracture along both axial and radial directions decreased from 1373 K to 973 K because of K-doping. Thus, K-doping could suppress the influence of microstructural anisotropy on tensile properties, especially ductility, in large diameter W rods.

  12. Influence of heat treatments on the microstructure and tensile behaviour of selective laser melting-produced TI-6AL-4V parts

    Directory of Open Access Journals (Sweden)

    Ter Haar, Gerrit Matthys

    2016-11-01

    Full Text Available In industry, post-process heat treatments of Ti-6Al-4V are performed with the aim of improving its tensile behaviour. While heat treatments of wrought Ti6Al4V have been standardised (e.g., Aerospace Material Specification H-81200, heat treatments of selective laser melting (SLM-produced Ti-6Al-4V lacks research and understanding. Significant concern exists about SLM Ti6-Al-4V’s achievable ductility attributed to its martensitic (α’ phase. In this research, heat treatments at a range of temperatures are applied to SLM-produced Ti-6Al-4V tensile samples. Microstructural analysis (both optically and through electron backscatter diffraction was used to identify links between heat treatments and microstructure. Subsequently, uniaxial tensile tests were performed to determine the respective tensile properties of all samples. Correlations in the data show a significant loss in strength with respect to an increase in annealing temperature due to grain growth, while no noticeable trend was observed for fracture strain with regard to annealing temperatures.

  13. Effect of Controlled Cooling on Microstructure and Tensile Properties of Low C Nb-Ti-Containing HSLA Steel for Construction

    Directory of Open Access Journals (Sweden)

    Yi Fan

    2017-01-01

    Full Text Available The thermo-mechanical control processing (TMCP of low carbon (C Nb-Ti-containing HSLA steel with different cooling rates from 5 to 20 °C/s was simulated using a Gleeble 3500 system. The samples’ microstructure was characterized and the tensile properties measured. The results show that a microstructure mainly consisting of quasi-polygonal ferrite (QPF, granular bainitic ferrite (GBF, and martensite/austenite (M/A constituent formed in each sample. Furthermore, the accelerated cooling led to a significant grain refinement of the QPF and GBF, and an increase in the density of dislocations, as well as suppressed the precipitation of nanoscale particles; however, the overall yield strength (YS still increased obviously. The accelerated cooling also brought about a decrease in amount of M/A constituent acting as a mixed hard phase, which weakened the overall strain-hardening capacity of the QPF + GBF + M/A multiphase steel and simultaneously elevated yield-to-tensile strength ratio (YR. In addition, the mechanisms in dominating the influence of controlled cooling on the final microstructure and tensile properties were discussed.

  14. High-Temperature Tensile Strength of Al10Co25Cr8Fe15Ni36Ti6 Compositionally Complex Alloy (High-Entropy Alloy)

    Science.gov (United States)

    Daoud, H. M.; Manzoni, A. M.; Wanderka, N.; Glatzel, U.

    2015-06-01

    Homogenizing at 1220°C for 20 h and subsequent aging at 900°C for 5 h and 50 h of a novel Al10Co25Cr8Fe15Ni36Ti6 compositionally complex alloy (high-entropy alloy) produces a microstructure consisting of an L12 ordered γ' phase embedded in a face-centered cubic solid-solution γ matrix together with needle-like B2 precipitates (NiAl). The volume fraction of γ' phase is ~46% and of needle-like B2 precipitates database; Thermo-Calc Software, Stockholm, Sweden). The high-temperature tensile tests were carried out at room temperature, 600°C, 700°C, 800°C, and 1000°C. The tensile strength as well as the elongation to failure of both heat-treated specimens is very high at all tested temperatures. The values of tensile strength has been compared with literature data of well-known Alloy 800H and Inconel 617, and is discussed in terms of the observed microstructure.

  15. Nondestructive/in-situ evaluation of the tensile properties in industrial facilities using indentation system

    International Nuclear Information System (INIS)

    Jang, Jae Il; Choi, Yeol; Son, Dong Il; Kwon, Dong Il

    2001-01-01

    Exact reliability evaluation and lifetime prediction through the in-field diagnosis of materials properties is needed for safe usage of degraded industrial structures. But, conventional standard testing methods having destructive procedures are not applicable to in-field assessment of mechanical property. Therefore, an advanced indentation technique was proposed for simple and non-destructive testing of in-field structures and for selected testing of local range such as heat affected zone and weldment. This test measures indentation load-depth curve during indentation and analyzes the mechanical properties related to deformation and fracture. First of all, flow properties such as yield strength, tensile strength and work hardening index can be evaluated through the analysis of the deformation behavior beneath the spherical indenter. Additionally, case studies of advanced indentation techniques are introduced.

  16. Ceramic Composite Intermediate Temperature Stress-Rupture Properties Improved Significantly

    Science.gov (United States)

    Morscher, Gregory N.; Hurst, Janet B.

    2002-01-01

    Silicon carbide (SiC) composites are considered to be potential materials for future aircraft engine parts such as combustor liners. It is envisioned that on the hot side (inner surface) of the combustor liner, composites will have to withstand temperatures in excess of 1200 C for thousands of hours in oxidizing environments. This is a severe condition; however, an equally severe, if not more detrimental, condition exists on the cold side (outer surface) of the combustor liner. Here, the temperatures are expected to be on the order of 800 to 1000 C under high tensile stress because of thermal gradients and attachment of the combustor liner to the engine frame (the hot side will be under compressive stress, a less severe stress-state for ceramics). Since these composites are not oxides, they oxidize. The worst form of oxidation for strength reduction occurs at these intermediate temperatures, where the boron nitride (BN) interphase oxidizes first, which causes the formation of a glass layer that strongly bonds the fibers to the matrix. When the fibers strongly bond to the matrix or to one another, the composite loses toughness and strength and becomes brittle. To increase the intermediate temperature stress-rupture properties, researchers must modify the BN interphase. With the support of the Ultra-Efficient Engine Technology (UEET) Program, significant improvements were made as state-of-the-art SiC/SiC composites were developed during the Enabling Propulsion Materials (EPM) program. Three approaches were found to improve the intermediate-temperature stress-rupture properties: fiber-spreading, high-temperature silicon- (Si) doped boron nitride (BN), and outside-debonding BN.

  17. Oxide dispersion strengthened ferritic alloys. 14/20% chromium: effects of processing on deformation texture, recrystallization and tensile properties

    International Nuclear Information System (INIS)

    Regle, H.

    1994-01-01

    The ferritic oxide dispersion strengthened alloys are promising candidates for high temperature application materials, in particular for long life core components of advanced nuclear reactors. The aim of this work is to control the microstructure, in order to optimise the mechanical properties. The two ferritic alloys examined here, MA956 and MA957, are obtained by Mechanical Alloying techniques. They are characterised by quite anisotropic microstructure and mechanical properties. We have investigated the influence of hot and cold working processes (hot extrusion, swaging and cold-drawing) and recrystallization heat treatments on deformation textures, microstructures and tensile properties. The aim was to control the size of the grains and their anisotropic shape, using recrystallization heat treatments. After consolidation and hot extrusion, as-received materials present a extremely fine microstructure with elongated grains and a very strong (110) deformation texture with single-crystal character. At that stage of processing, recrystallization temperature are very high (1450 degrees C for MA957 alloy and 1350 degrees C for MA956 alloy) and materials develop millimetric recrystallized grains. Additional hot extrusion induce a fibre texture. Cold-drawing maintains a fibre texture, but the intensity decreases with increasing cold-work level. For both materials, the decrease of texture intensities correspond to a decrease of the recrystallization temperatures (from 1350 degrees C for a low cold-work level to 750 degrees C for 60 % cold-deformation, case of MA956 alloy) and a refinement of the grain size (from a millimetric size to less than an hundred of micrometer). Swaging develop a cyclic component where the intensity increases with increasing deformation in this case, the recrystallization temperature remains always very high and the millimetric grain size is slightly modified, even though cold-work level increases. Technologically, cold-drawing is the only way

  18. Effect of a ductility layer on the tensile strength of TiAl-based multilayer composite sheets prepared by EB-PVD

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Rubing, E-mail: zrb86411680@126.com [Department of Mechanics, School of Civil Engineering, Beijing Jiaotong University, Beijing 100044 (China); Zhang, Yaoyao [Department of Mechanics, School of Civil Engineering, Beijing Jiaotong University, Beijing 100044 (China); Liu, Qiang [Beijing Institute of Astronautical Systems Engineering, Beijing 100076 (China); Chen, Guiqing [Center for Composite Materials, Harbin Institute of Technology, Harbin 150001 (China); Zhang, Deming [Beijing General Research Institute of Mining and Metallurgy, Beijing 100044 (China)

    2014-09-15

    TiAl/Nb and TiAl/NiCoCrAl laminate composite sheets with a thickness of 0.4–0.6 mm and dimensions of 150 mm × 100 mm were successfully fabricated by electron beam physical vapor deposition. The microstructures of the sheets were examined, and their mechanical properties were compared with those of TiAl monolithic sheet produced by electron beam physical vapor deposition. Tensile testing was performed at room temperature and 750 °C, and the fracture surfaces were examined by scanning electron microscopy. Among the three microlaminate sheets, the TiAl/NiCoCrAl micro-laminate sheet had the best comprehensive properties at room temperature, and the TiAl/Nb micro-laminate sheet showed the ideal high-temperature strength and plasticity at 750 °C. The result was discussed in terms of metal strengthening mechanism. - Highlights: • TiAl-based multilayer foils was fabricated successfully by using EB-PVD method; • The tensile properties and micro-fracture morphologies of the sheet were investigated; • The deformation behavior of the multilayer foils was discussed.

  19. Comportement en fatigue et influence de la temperature sur les proprietes en traction du PLA

    Science.gov (United States)

    Menard, Claire

    Current environmental issues reduce the use of materials obtained from fossil resources. The usual plastics therefore tend to be replaced by more green polymers such as polylactic acid (PLA), a bio-based and biodegradable polymer. Knowledge on the properties of this material is essential, especially in terms of fatigue strength and influence of temperature on tensile stiffness and strength. In this study, the PLA samples are submitted to monotonic tensile tests, according to ASTM D638-10, at various temperatures between room temperature (23°C) and the glass transition temperature of the material (55-60°C). The results show a decrease of 30% of the modulus of elasticity and 60% of the tensile strength between these two temperatures. This decrease is mainly due to a significant drop in the mechanical properties beyond 50°C. In addition, tensile fatigue tests were conducted at loads rate between 40 and 80% of tensile strength, at room temperature in order to plot the Wohler curve of PLA. The ruptured specimens were finally observed with a scanning electron microscope (SEM) to analyze the failure mechanisms in fatigue of PLA.

  20. High-temperature mechanical properties of high-purity 70 mass% Cr-Fe alloy

    Energy Technology Data Exchange (ETDEWEB)

    Asahina, M.; Harima, N.; Takaki, S.; Abiko, K. [Tohoku Univ., Sendai (Japan). Inst. for Materials Research

    2002-01-16

    An ingot of high-purity 70 mass% Cr-Fe alloy was prepared by high-frequency induction melting in a high-purity argon atmosphere using a cold copper crucible. Its tensile properties such as hot-ductility and tensile strength were measured, and compared with the results for a high-purity 50 mass% Cr-Fe alloy, a high-purity 60 mass% Cr-Fe alloy and a Ni-based super-alloy. The formation of {sigma}-phase was also examined. The purity of a 70Cr-Fe alloy (70 mass% Cr-Fe alloy) ingot is more than 99.98 mass% and the total amount of gaseous impurities (C, N, O, S, H) in the 70Cr-Fe alloy is 69.9 mass ppm. The strength of the 70Cr-Fe alloy is higher than those of the 60Cr-Fe alloy and the 50Cr-Fe alloy at the temperatures between 293 and 1573 K, without decrease in ductility with increasing Cr content. The 70Cr-Fe alloy also possesses excellent high-temperature ductility. The {sigma}-phase was not observed after aging of 3.6 Ms at 873 K. Consequently, the 70Cr-Fe alloy is an excellent alloy as the base of super heat-resistant alloys. (orig.)