Development of microfluidic devices for biomedical applications of synchrotron radiation infrared microspectroscopy

OpenAIRE

Birarda, Giovanni

2011-01-01

2009/2010 ABSTRACT DEVELOPMENT OF MICROFLUIDIC DEVICES FOR BIOMEDICAL APPLICATIONS OF SYNCHROTRON RADIATION INFRARED MICROSPECTROSCOPY by Birarda Giovanni The detection and measurement of biological processes in a complex living system is a discipline at the edge of Physics, Biology, and Engineering, with major scientific challenges, new technological applications and a great potential impact on dissection of phenomena occurring at tissue, cell, and sub cellular level. The ...

Aleurone Cell Walls of Wheat Grain: High Spatial Resolution Investigation Using Synchrotron Infrared Microspectroscopy

International Nuclear Information System (INIS)

Jamme, F.; Robert, R.; Bouchet, B.; Saulnier, L.; Dumas, P.; Guillon, F.

2008-01-01

Infrared microspectroscopy and immunolabeling techniques were employed in order to obtain deeper insight into the biochemical nature of aleurone cell walls of wheat grain. The use of a synchrotron source, thanks to its intrinsic brightness, has provided unprecedented information at the level of a few micrometers and has allowed the discrimination of various polysaccharides in cell walls. The high spectral quality obtained in the small analyzed domain has been beneficial in estimating the relative proportions of Β-glucan and arabinoxylan, through the use of principal component analysis (PCA). The highest amount of Β-glucan is found in periclinal cell walls close to the starchy endosperm. The junction regions between aleurone cells are enriched in arabinoxylan. At the early stage of wheat grain development (271 degrees D), the chemical composition along the cell walls is more heterogeneous than at the mature stage. Both synchrotron infrared microspectroscopy and immunolabeling experiments made it possible to reveal the spatial heterogeneity of the various chemical compositions of aleurone cell walls.

Recent applications and current trends in Cultural Heritage Science using synchrotron-based Fourier transform infrared micro-spectroscopy

Science.gov (United States)

Cotte, Marine; Dumas, Paul; Taniguchi, Yoko; Checroun, Emilie; Walter, Philippe; Susini, Jean

2009-09-01

Synchrotron-based Fourier transform infrared micro-spectroscopy (SR-FTIR) is one of the emerging techniques increasingly employed for Cultural Heritage analytical science. Such a technique combines the assets of FTIR spectroscopy (namely, the identification of molecular groups in various environments: organic/inorganic, crystallized/amorphous, solid/liquid/gas), with the extra potential of chemical imaging (localization of components + easier data treatment thanks to geographical correlations) and the properties of the synchrotron source (namely, high brightness, offering high data quality even with reduced dwell time and reduced spot size). This technique can be applied to nearly all kind of materials found in museum objects, going from hard materials, like metals, to soft materials, like paper, and passing through hybrid materials such as paintings and bones. The purpose is usually the identification of complex compositions in tiny, heterogeneous samples. Recent applications are reviewed in this article, together with the fundamental aspects of the infrared synchrotron source which are leading to such improvements in analytical capabilities. A recent example from the ancient Buddhist paintings from Bamiyan is detailed. Emphasis is made on the true potential offered at such large scale facilities in combining SR-FTIR microscopy with other synchrotron-based micro-imaging techniques. To cite this article: M. Cotte et al., C. R. Physique 10 (2009).

The status of the first infrared beamline at Shanghai Synchrotron Radiation Facility

International Nuclear Information System (INIS)

Ji, Te; Tong, Yajun; Zhu, Huachun; Zhang, Zengyan; Peng, Weiwei; Chen, Min; Xiao, Tiqiao; Xu, Hongjie

2015-01-01

Construction of the first infrared beamline BL01B1 at Shanghai Synchrotron Radiation Facility (SSRF) was completed at the end of 2013. The IR beamline collects both edge radiation (ER) and bending magnet radiation (BMR) from a port, providing a solid angle of 40 mrad and 20 mrad in the horizontal and vertical directions, respectively. The optical layout of the infrared beamline and the design of the extraction mirror are described in this paper. A calculation of the beam propagation has been used to optimize the parameters of the optical components. The photon flux and spatial resolution have been measured at the end-station, and the experimental results are in good agreement with the theoretical calculation

The status of the first infrared beamline at Shanghai Synchrotron Radiation Facility

Energy Technology Data Exchange (ETDEWEB)

Ji, Te; Tong, Yajun; Zhu, Huachun; Zhang, Zengyan; Peng, Weiwei; Chen, Min, E-mail: chenmin@sinap.ac.cn; Xiao, Tiqiao; Xu, Hongjie

2015-07-11

Construction of the first infrared beamline BL01B1 at Shanghai Synchrotron Radiation Facility (SSRF) was completed at the end of 2013. The IR beamline collects both edge radiation (ER) and bending magnet radiation (BMR) from a port, providing a solid angle of 40 mrad and 20 mrad in the horizontal and vertical directions, respectively. The optical layout of the infrared beamline and the design of the extraction mirror are described in this paper. A calculation of the beam propagation has been used to optimize the parameters of the optical components. The photon flux and spatial resolution have been measured at the end-station, and the experimental results are in good agreement with the theoretical calculation.

The status of the first infrared beamline at Shanghai Synchrotron Radiation Facility

Science.gov (United States)

Ji, Te; Tong, Yajun; Zhu, Huachun; Zhang, Zengyan; Peng, Weiwei; Chen, Min; Xiao, Tiqiao; Xu, Hongjie

2015-07-01

Construction of the first infrared beamline BL01B1 at Shanghai Synchrotron Radiation Facility (SSRF) was completed at the end of 2013. The IR beamline collects both edge radiation (ER) and bending magnet radiation (BMR) from a port, providing a solid angle of 40 mrad and 20 mrad in the horizontal and vertical directions, respectively. The optical layout of the infrared beamline and the design of the extraction mirror are described in this paper. A calculation of the beam propagation has been used to optimize the parameters of the optical components. The photon flux and spatial resolution have been measured at the end-station, and the experimental results are in good agreement with the theoretical calculation.

A comparison of three different ray trace programs for x-ray and infrared synchrotron beamline designs

International Nuclear Information System (INIS)

Irick, S.C.; Jung, C.R.

1997-07-01

There are a number of ray trace programs currently used for the design of synchrotron beamlines. While several of these programs have been written and used mostly within the programmer''s institution, many have also been available to the general public. This paper discusses three such programs. One is a commercial product oriented for the general optical designer (not specifically for synchrotron beamlines). One is designed for synchrotron beamlines and is free with restricted availability. Finally, one is designed for synchrotron beamlines and is used primarily in one institution. The wealth of information from general optical materials and components catalogs is readily available in the commercial program for general optical designs. This makes the design of an infrared beamline easier from the standpoint of component selection. However, this program is not easily configured for synchrotron beamline designs, particularly for a bending magnet source. The synchrotron ray trace programs offer a variety of sources, but generally are not as easy to use from the standpoint of the user interface. This paper shows ray traces of the same beamline Optikwerks, SHADOW, and RAY, and compares the results

The first synchrotron infrared beamlines at the Advanced Light Source: Spectromicroscopy and fast timing

International Nuclear Information System (INIS)

Martin, Michael C.; McKinney, Wayne R.

1999-01-01

Two recently commissioned infrared beamlines on the 1.4 bending magnet port at the Advanced Light Source, LBNL, are described. Using a synchrotron as an IR source provides three primary advantages: increased brightness, very fast light pulses, and enhanced far-IR flux. The considerable brightness advantage manifests itself most beneficially when performing spectroscopy on a microscopic length scale. Beamline (BL) 1.4.3 is a dedicated FTIR spectromicroscopy beamline, where a diffraction-limited spot size using the synchrotron source is utilized. BL 1.4.2 consists of a vacuum FTIR bench with a wide spectral range and step-scan capability. This BL makes use of the pulsed nature of the synchrotron light as well as the far-IR flux. Fast timing is demonstrated by observing the pulses from the electron bunch storage pattern at the ALS. Results from several experiments from both IR beamlines will be presented as an overview of the IR research currently being done at the ALS

A proposal for an infrared/optical beam line for the new Australian synchrotron project

International Nuclear Information System (INIS)

Creagh, D.

2002-01-01

Full text: In late 2001 the Premier of Victoria, Steve Bracks, announced that the Victorian Government would provide funding of $100,000,000 for the construction of an Australian National Synchrotron on a site on the Monash University campus. The design of the synchrotron and the tentative allocations of beamlines within the synchrotron were taken from the 'Boomerang' designs developed by Dr John Boldeman for the Australian Synchrotron Research Program. The formal administrative structure has recently been put in place. Committees such as the International Machine Advisory Committee (IMAC) and the National Scientific Advisory Committee (NSAC) have been formed and are actively pursuing the goals set down in the strategic plan. Meetings of the NSAC are held monthly, the fifteen members from all states and territories (except Tasmania and the Northern Territory) meeting to discuss how the scientific goals may be achieved. At the last meeting proposals were canvassed for the beamlines to be provided at the synchrotron. One of these beamlines is an IR/Optical Beamline, the subject of this paper. Spectroscopy, using photon energies from the infrared (IR) to the ultraviolet has long been an important analytical tool in scientific investigations. The study of the absorption and scattering (both elastic and Raman) of light by samples, and the fluorescence radiation emitted by samples, can give information about essential for the understanding of the chemical state of the sample, identifying chemical and mineral types present in a sample, and identifying changes in systems Areas of research which would benefit from the use of synchrotron radiation source include: cell biology, in particular the study of the uptake of drugs by cells; surficial processes, for example the in situ study of corrosion processes and the testing of anti-corrosion coatings; organic and inorganic nanotechnology; the study of bandgaps in quantum effect materials; mineralogy, for example determining

Transport behaviors of anionic azo dyes at interface between surfactant-modified flax shives and aqueous solution: Synchrotron infrared and adsorption studies

Energy Technology Data Exchange (ETDEWEB)

Wang, Wenxia [MOE Key Laboratory of Resources and Environmental Systems Optimization, Institute for Energy, Environment and Sustainability Research, UR-NCEPU, North China Electric Power University, Beijing, 102206 (China); Huang, Guohe, E-mail: huang@iseis.org [MOE Key Laboratory of Resources and Environmental Systems Optimization, Institute for Energy, Environment and Sustainability Research, UR-NCEPU, North China Electric Power University, Beijing, 102206 (China); An, Chunjiang; Xin, Xiaying [Institute for Energy, Environment and Sustainable Communities, University of Regina, Regina, S4S 0A2 (Canada); Zhang, Yan [MOE Key Laboratory of Resources and Environmental Systems Optimization, Institute for Energy, Environment and Sustainability Research, UR-NCEPU, North China Electric Power University, Beijing, 102206 (China); Liu, Xia [Canadian Light Source, Saskatoon, S7N 2V3 (Canada)

2017-05-31

Highlights: • Surfactant modified flax shives for removing anionic azo dyes. • The equilibrium and kinetic studies for the adsorption of anionic azo dyes. • The migration patterns of dye pollutants at flax shive-water interface. • New insights from synchrotron infrared-assisted characterization. • Potential as biomass adsorbent for the removal of dyes from wastewater. - Abstract: From the viewpoint of sustainability, biomass adsorbent has a high potential in pollution control and there is an emerging interest to investigate the behaviors of pollutants at the interface between biomass adsorbent and solution. This study investigated the performance of cetyltrimethylammonium bromide surfactant-modified flax shives (MFS) for removal of anionic azo dyes from aqueous solution. The equilibrium and kinetic analysis for the adsorption of Acid Orange 7 (AO-7), Acid Red 18 (AR-18) and Acid Black 1 (AB-1) on MFS were conducted. The surface of MFS was characterized by synchrotron infrared and SEM analysis. The absorbed amount of three anionic azo dyes varied with the change of adsorbent dosage, pH and ionic strength. The adsorption isotherm data well fit to the Langmuir model. The adsorption process followed the pseudo-second-order kinetics and the liquid film diffusion models. Thermodynamic studies indicated that the adsorption of three anionic azo dyes was spontaneous. The adsorption of AR-18 and AB-1 onto MFS was endothermic while the adsorption of AO-7 was exothermic. The results can help better understand the behaviors of organic pollutants at biomass adsorbent-water interface. They also present the potential of using MFS as a suitable adsorbent for the removal of anionic azo dyes from wastewater.

Transport behaviors of anionic azo dyes at interface between surfactant-modified flax shives and aqueous solution: Synchrotron infrared and adsorption studies

International Nuclear Information System (INIS)

Wang, Wenxia; Huang, Guohe; An, Chunjiang; Xin, Xiaying; Zhang, Yan; Liu, Xia

2017-01-01

Highlights: • Surfactant modified flax shives for removing anionic azo dyes. • The equilibrium and kinetic studies for the adsorption of anionic azo dyes. • The migration patterns of dye pollutants at flax shive-water interface. • New insights from synchrotron infrared-assisted characterization. • Potential as biomass adsorbent for the removal of dyes from wastewater. - Abstract: From the viewpoint of sustainability, biomass adsorbent has a high potential in pollution control and there is an emerging interest to investigate the behaviors of pollutants at the interface between biomass adsorbent and solution. This study investigated the performance of cetyltrimethylammonium bromide surfactant-modified flax shives (MFS) for removal of anionic azo dyes from aqueous solution. The equilibrium and kinetic analysis for the adsorption of Acid Orange 7 (AO-7), Acid Red 18 (AR-18) and Acid Black 1 (AB-1) on MFS were conducted. The surface of MFS was characterized by synchrotron infrared and SEM analysis. The absorbed amount of three anionic azo dyes varied with the change of adsorbent dosage, pH and ionic strength. The adsorption isotherm data well fit to the Langmuir model. The adsorption process followed the pseudo-second-order kinetics and the liquid film diffusion models. Thermodynamic studies indicated that the adsorption of three anionic azo dyes was spontaneous. The adsorption of AR-18 and AB-1 onto MFS was endothermic while the adsorption of AO-7 was exothermic. The results can help better understand the behaviors of organic pollutants at biomass adsorbent-water interface. They also present the potential of using MFS as a suitable adsorbent for the removal of anionic azo dyes from wastewater.

Imidazole and beta-carotene photoprotection against photodynamic therapy evaluated by synchrotron infrared microscopy

Science.gov (United States)

Bosio, Gabriela N.; Parisi, Julieta; García Einschlag, Fernando S.; Mártire, Daniel O.

2018-04-01

In order to better understand the role of β-carotene and imidazole on the Photodynamic Therapy (PDT) mechanism, synchrotron infrared microscopy was used to detect the associated intracellular biochemical modifications following the visible light irradiation of HeLa cells incubated with these compounds as typical hydrophobic and hydrophilic singlet oxygen quenchers, respectively. For this purpose, PDT was performed employing the hydrophilic sensitizer 5,10,15,20-Tetrakis (1-methyl-4-pyridinio) porphyrin tetra (p-toluenesulfonate), TMPyP, and the hydrophobic sensitizer 5-(4-Methoxycarboxyphenyl)-10,15,20-triphenyl-21H,23H-porphyrin. The single cell IR spectra of PDT-treated, PDT plus quencher-treated and control HeLa cells were recorded at the SOLEIL Synchrotron Infrared SMIS beamline targeting specifically the cell nucleus. Principal Component Analysis (PCA) was used to assess the IR spectral changes. PCA revealed that there is a frequency shift of the protein Amide I vibrational band for the assays with the TMPyP sensitizer, indicating changes in the protein secondary structures of the PDT-treated cancer cells compared to the controls. In addition, the scores in those cells treated with both quenchers appear to be similar to the controls indicating a photoprotective effect. Comparative experiments carried out with SKMEL-28 and HaCat cells showed non- significant photoprotective effects of β-carotene and imidazole.

Development and trends in synchrotron studies of ancient and historical materials

International Nuclear Information System (INIS)

Bertrand, Loïc; Cotte, Marine; Stampanoni, Marco; Thoury, Mathieu; Marone, Federica; Schöder, Sebastian

2012-01-01

Synchrotron photon-based methods are increasingly being used for the physico-chemical study of ancient and historical materials (archaeology, palaeontology, conservation sciences, palaeo-environments). In particular, parameters such as the high photon flux, the small source size and the low divergence attained at the synchrotron make it a very efficient source for a range of advanced spectroscopy and imaging techniques, adapted to the heterogeneity and great complexity of the materials under study. The continuous tunability of the source — its very extended energy distribution over wide energy domains (meV to keV) with a high intensity — is an essential parameter for techniques based on a very fine tuning of the probing energy to reach high chemical sensitivity such as XANES, EXAFS, STXM, UV/VIS spectrometry, etc. The small source size attained (a few micrometres) at least in the vertical plane leads to spatial coherence of the photon beams, giving rise in turn to a series of imaging methods already crucial to the field. This review of the existing literature shows that microfocused hard X-ray spectroscopy (absorption, fluorescence, diffraction), full-field X-ray tomography and infrared spectroscopy are the leading synchrotron techniques in the field, and presents illustrative examples of the study of ancient and historical materials for the various methods. Fast developing analytical modalities in scanning spectroscopy (STXM, macro-XRF scanning) and novel analytical strategies regarding optics, detectors and other instrumental developments are expected to provide major contributions in the years to come. Other energy domains are increasingly being used or considered such as far-infrared and ultraviolet/visible for spectroscopy and imaging. We discuss the main instrumental developments and perspectives, and their impact for the science being made on ancient materials using synchrotron techniques.

Intraocular Pressure Induced Retinal Changes Identified Using Synchrotron Infrared Microscopy.

Directory of Open Access Journals (Sweden)

Hsin-Hui Shen

Full Text Available Infrared (IR spectroscopy has been used to quantify chemical and structural characteristics of a wide range of materials including biological tissues. In this study, we examined spatial changes in the chemical characteristics of rat retina in response to intraocular pressure (IOP elevation using synchrotron infrared microscopy (SIRM, a non-destructive imaging approach. IOP elevation was induced by placing a suture around the eye of anaesthetised rats. Retinal sections were collected onto transparent CaF2 slides 10 days following IOP elevation. Using combined SIRM spectra and chemical mapping approaches it was possible to quantify IOP induced changes in protein conformation and chemical distribution in various layers of the rat retina. We showed that 10 days following IOP elevation there was an increase in lipid and protein levels in the inner nuclear layer (INL and ganglion cell layer (GCL. IOP elevation also resulted in an increase in nucleic acids in the INL. Analysis of SIRM spectra revealed a shift in amide peaks to lower vibrational frequencies with a more prominent second shoulder, which is consistent with the presence of cell death in specific layers of the retina. These changes were more substantial in the INL and GCL layers compared with those occurring in the outer nuclear layer. These outcomes demonstrate the utility of SIRM to quantify the effect of IOP elevation on specific layers of the retina. Thus SIRM may be a useful tool for the study of localised tissue changes in glaucoma and other eye diseases.

Determination of phosphorus fertilizer soil reactions by Raman and synchrotron infrared microspectroscopy.

Science.gov (United States)

Vogel, Christian; Adam, Christian; Sekine, Ryo; Schiller, Tara; Lipiec, Ewelina; McNaughton, Don

2013-10-01

The reaction mechanisms of phosphate-bearing mineral phases from sewage sludge ash-based fertilizers in soil were determined by Raman and synchrotron infrared microspectroscopy. Different reaction mechanisms in wet soil were found for calcium and magnesium (pyro-) phosphates. Calcium orthophosphates were converted over time to hydroxyapatite. Conversely, different magnesium phosphates were transformed to trimagnesium phosphate. Since the magnesium phosphates are unable to form an apatite structure, the plant-available phosphorus remains in the soil, leading to better growth results observed in agricultural pot experiments. The pyrophosphates also reacted very differently. Calcium pyrophosphate is unreactive in soil. In contrast, magnesium pyrophosphate quickly formed plant-available dimagnesium phosphate.

Synchrotron radiation sources for photobiology and ultraviolet, visible and infrared spectroscopy

International Nuclear Information System (INIS)

Sutherland, J.C.

1980-01-01

The advantages of synchrotron radiation in several types of spectroscopy, microscopy and diffraction studies are clear. The availability of synchrotron radiation will expand rapidly in the early 1980's as experimental programs start at the new generation of dedicated storage rings

PHOTOACOUSTIC SPECTROSCOPY USING A SYNCHROTRON LIGHT SOURCE

International Nuclear Information System (INIS)

JACKSON, R.S.; MICHAELIAN, K.H.; HOMES, C.C.

2001-01-01

We have investigated the use of a synchrotron as a source for infrared photoacoustic spectroscopy. A synchrotron has an intrinsically high radiance, which is beneficial when photoacoustic spectroscopy is applied to small samples, especially at long wavelengths

High-resolution far-infrared synchrotron FTIR spectrum of the ν12 band of formamide-d1 (DCONH2)

Science.gov (United States)

Tan, T. L.; Wu, Q. Y.; Ng, L. L.; Appadoo, Dominique R. T.; McNaughton, Don

2018-05-01

The spectrum of the ν12 band of formamide-d1 (DCONH2) was recorded using a synchrotron Fourier transform infrared (FTIR) spectrometer coupled to the Australian Synchrotron THz/Far-IR beamline, with an unapodized resolution of 0.00096 cm-1 in the 350-210 cm-1 region. For the first time, rovibrational constants up to five quartic and two sextic terms were derived for the v12 = 1 state through the fitting of a total of 2072 far-infrared transitions using Watson's A-reduced Hamiltonian in the Ir representation with a root-mean-square (rms) deviation of 0.000073 cm-1. The band centre of the ν12 band of DCONH2 was found to be 289.3327553(47) cm-1 although the experimental uncertainty was limited to ±0.0002 cm-1. Ground state rovibrational constants of DCONH2 up to five quartic and two sextic constants were derived from a fit of 847 ground state combination differences (GSCDs) obtained from the infrared transitions of the ν12 band, together with 6 previously reported microwave transitions, with a rms deviation of 0.000108 cm-1. The ground state rotational constants (A, B, and C) of DCONH2 were improved while the ground state centrifugal distortion constants were accurately obtained for the first time. The uncertainty of the measured infrared lines was estimated to be ±0.0002 cm-1. From the ground state rotational constants, the inertial defect of DCONH2 was calculated to be 0.0169412(11) uÅ2.

Synchrotron radiation-based Fourier-transform infrared spectromicroscopy for characterization of the protein/peptide distribution in single microspheres

Directory of Open Access Journals (Sweden)

Manli Wang

2015-05-01

Full Text Available The present study establishes a visualization method for the measurement of the distribution and localization of protein/peptide constituents within a single poly-lactide-co-glycolide (PLGA microsphere using synchrotron radiation–based Fourier-transform infrared spectromicroscopy (SR-FTIR. The representative infrared wavenumbers specific for protein/peptide (Exenatide and excipient (PLGA were identified and chemical maps at the single microsphere level were generated by measuring and plotting the intensity of these specific bands. For quantitative analysis of the distribution within microspheres, Matlab software was used to transform the map file into a 3D matrix and the matrix values specific for the drug and excipient were extracted. Comparison of the normalized SR-FTIR maps of PLGA and Exenatide indicated that PLGA was uniformly distributed, while Exenatide was relatively non-uniformly distributed in the microspheres. In conclusion, SR-FTIR is a rapid, nondestructive and sensitive detection technology to provide the distribution of chemical constituents and functional groups in microparticles and microspheres.

Synchrotron X-ray adaptative monochromator: study and realization of a prototype

International Nuclear Information System (INIS)

Dezoret, D.

1995-01-01

This work presents a study of a prototype of a synchrotron X-ray monochromator. The spectral qualities of this optic are sensitive to the heat loads which are particularly important on third synchrotron generation like ESRF. Indeed, powers generated by synchrotron beams can reach few kilowatts and power densities about a few tens watts per square millimeters. The mechanical deformations of the optical elements of the beamlines issue issue of the heat load can damage their spectral efficiencies. In order to compensate the deformations, wa have been studying the transposition of the adaptive astronomical optics technology to the x-ray field. First, we have considered the modifications of the spectral characteristics of a crystal induced by x-rays. We have established the specifications required to a technological realisation. Then, thermomechanical and technological studies have been required to transpose the astronomical technology to an x-ray technology. After these studies, we have begun the realisation of a prototype. This monochromator is composed by a crystal of silicon (111) bonded on a piezo-electric structure. The mechanical control is a loop system composed by a infrared light, a Shack-Hartmann CDD and wave front analyser. This system has to compensate the deformations of the crystal in the 5 kcV to 60 kcV energy range with a power density of 1 watt per square millimeters. (authors)

Synchrotron X-ray adaptative monochromator: study and realization of a prototype; Monochromateur adaptatif pour rayonnement X synchrotron: etude et realisation d`un prototype

Energy Technology Data Exchange (ETDEWEB)

Dezoret, D.

1995-12-12

This work presents a study of a prototype of a synchrotron X-ray monochromator. The spectral qualities of this optic are sensitive to the heat loads which are particularly important on third synchrotron generation like ESRF. Indeed, powers generated by synchrotron beams can reach few kilowatts and power densities about a few tens watts per square millimeters. The mechanical deformations of the optical elements of the beamlines issue issue of the heat load can damage their spectral efficiencies. In order to compensate the deformations, wa have been studying the transposition of the adaptive astronomical optics technology to the x-ray field. First, we have considered the modifications of the spectral characteristics of a crystal induced by x-rays. We have established the specifications required to a technological realisation. Then, thermomechanical and technological studies have been required to transpose the astronomical technology to an x-ray technology. After these studies, we have begun the realisation of a prototype. This monochromator is composed by a crystal of silicon (111) bonded on a piezo-electric structure. The mechanical control is a loop system composed by a infrared light, a Shack-Hartmann CDD and wave front analyser. This system has to compensate the deformations of the crystal in the 5 kcV to 60 kcV energy range with a power density of 1 watt per square millimeters. (authors).

Determination of Endosperm Protein Secondary Structure in Hard Wheat Breeding Lines using Synchrotron Infrared Microspectroscopy

International Nuclear Information System (INIS)

Bonwell, E.; Fisher, T.; Fritz, A.; Wetzel, D.

2008-01-01

One molecular aspect of mature hard wheat protein quality for breadmaking is the relative amount of endosperm protein in the a-helix form compared with that in other secondary structure forms including β-sheet. Modeling of a-helix and β-sheet absorption bands that contribute to the amide I band at 1650 cm-1 was applied to more than 1500 spectra in this study. The microscopic view of wheat endosperm is dominated by many large starch granules with protein in between. The spectrum produced from in situ microspectroscopy of this mixture is dominated by carbohydrate bands from the large starch granules that fill up the field. The high spatial resolution achievable with synchrotron infrared microspectroscopy enables revealing good in situ spectra of the protein located interstitially. Synchrotron infrared microspectroscopic mapping of 4 μm thick frozen sections of endosperm in the subaleurone region provides spectra from a large number of pixels. Pixels with protein-dominated spectra are sorted out from among adjacent pixels to minimize the starch absorption and scattering contributions. Subsequent data treatment to extract information from the amide I band requires a high signal to noise ratio. Although spectral interference of the carbohydrate band on the amide band is not a problem, the scattering produced by the large starch granules diminishes the signal to noise ratio throughout the spectrum. High density mapping was done on beamlines U2B and U10B at the National Synchrotron Light Source at Brookhaven National Laboratory, Upton, NY. Mapping with a single masked spot size of 5.5 μm diameter or confocal 5 μm x 5 μm spot size, respectively, on the two beamlines used produced spectra for new breeding lines under current consideration. Appropriate data treatment allows calculation of a numerical estimate of the a-helix population relative to other secondary protein structures from the position and shape of the amide I absorption band. Current breeding lines show a

Synchrotron-based FTIR spectromicroscopy: Cytotoxicity and heating considerations

Energy Technology Data Exchange (ETDEWEB)

Holman, Hoi-Ying N.; Martin, Michael C.; McKinney, Wayne R.

2002-12-13

Synchrotron radiation-based Fourier transform infrared (SR-FTIR) spectromicroscopy is a newly emerging bioanalytical and imaging tool. This unique technique provides mid-infrared (IR) spectra, hence chemical information, with high signal-to-noise at spatial resolutions as fine as 3 to 10 microns. Thus it enables researchers to locate, identify, and track specific chemical events within an individual living mammalian cell. Mid-IR photons are too low in energy (0.05 - 0.5 eV) to either break bonds or to cause ionization. In this review, we show that the synchrotron IR beam has no detectable effects on the short- and long-term viability, reproductive integrity, cell-cycle progression, and mitochondrial metabolism in living human cells, and produces only minimal sample heating (< 0.5 degrees C). These studies have established an important foundation for SR-FTIR spectromicroscopy in biological and biomedical research.

Synchrotron-based FTIR spectromicroscopy Cytotoxicity and heating considerations

CERN Document Server

Holman, H Y N; McKinney, W R

2002-01-01

Synchrotron radiation-based Fourier transform infrared (SR-FTIR) spectromicroscopy is a newly emerging bioanalytical and imaging tool. This unique technique provides mid-infrared (IR) spectra, hence chemical information, with high signal-to-noise at spatial resolutions as fine as 3 to 10 microns. Thus it enables researchers to locate, identify, and track specific chemical events within an individual living mammalian cell. Mid-IR photons are too low in energy (0.05 - 0.5 eV) to either break bonds or to cause ionization. In this review, we show that the synchrotron IR beam has no detectable effects on the short- and long-term viability, reproductive integrity, cell-cycle progression, and mitochondrial metabolism in living human cells, and produces only minimal sample heating (< 0.5 degrees C). These studies have established an important foundation for SR-FTIR spectromicroscopy in biological and biomedical research.

Transmission of infrared radiation through cylindrical waveguides

International Nuclear Information System (INIS)

Nucara, A.; Dore, P.; Calvani, P.; Cannavo', D.; Marcelli, A.

1998-01-01

Measurement of the transmittance of infrared radiation (v -1 ) through cylindrical waveguides are presented and discussed. The experimental results are compared with numerical simulations, obtained through conventional ray tracing programs. Finally, it' estimated the transmittance of a waveguide in the case of an infrared synchrotron radiation source. Are applied the results to the case of the DAΦNE collider, where a synchrotron radiation beamline for the far infrared is under construction

Biochemical profiling of rat embryonic stem cells grown on electrospun polyester fibers using synchrotron infrared microspectroscopy.

Science.gov (United States)

Doncel-Pérez, Ernesto; Ellis, Gary; Sandt, Christophe; Shuttleworth, Peter S; Bastida, Agatha; Revuelta, Julia; García-Junceda, Eduardo; Fernández-Mayoralas, Alfonso; Garrido, Leoncio

2018-06-01

Therapeutic options for spinal cord injuries are severely limited; current treatments only offer symptomatic relief and rehabilitation focused on educating the individual on how to adapt to their new situation to make best possible use of their remaining function. Thus, new approaches are needed, and interest in the development of effective strategies to promote the repair of neural tracts in the central nervous system inspired us to prepare functional and highly anisotropic polymer scaffolds. In this work, an initial assessment of the behavior of rat neural progenitor cells (NPCs) seeded on poly(3-hydroxybutyrate-co-3-hydroxyhexanoate) fiber scaffolds using synchrotron-based infrared microspectroscopy (SIRMS) is described. Combined with a modified touch imprint cytology sample preparation method, this application of SIRMS enabled the biochemical profiles of NPCs on the coated polymer fibers to be determined. The results showed that changes in the lipid and amide I-II spectral regions are modulated by the type and coating of the substrate used and the culture time. SIRMS studies can provide valuable insight into the early-stage response of NPCs to the morphology and surface chemistry of a biomaterial, and could therefore be a useful tool in the preparation and optimization of cellular scaffolds. Graphical abstract Synchrotron IR microspectroscopy can provide insight into the response of neural progenitor cells to synthetic scaffolds.

High-pressure synchrotron x-ray diffraction and infrared microspectroscopy: applications to dense hydrous phases

CERN Document Server

Liu, Z; Yang, H; Mao Ho Kwang; Hemley, R J

2002-01-01

Synchrotron x-ray diffraction (XRD) and infrared (IR) absorption spectra of hydrous and 'anhydrous' forms of phase X were measured to 30 GPa at room temperature. Three OH stretching modes were found in the hydrous phase, and surprisingly one sharp OH mode was observed in the previously characterized anhydrous phase. All OH stretching modes soften and broaden with increasing pressure and become very weak above approx 20 GPa. XRD indicates that the crystal structure remains stable up to 30 GPa. Combining IR absorption and XRD results, the behaviour is attributed to pressure-induced distortion of the Si sub 2 O sub 7 groups and disorder of the hydrogen atoms. The bulk moduli of the hydrous and 'anhydrous' phases are in the region of 74 GPa.

Low frequency interference between short synchrotron radiation sources

Directory of Open Access Journals (Sweden)

F. Méot

2001-06-01

Full Text Available A recently developed analytical formalism describing low frequency far-field synchrotron radiation (SR is applied to the calculation of spectral angular radiation densities from interfering short sources (edge, short magnet. This is illustrated by analytical calculation of synchrotron radiation from various assemblies of short dipoles, including an “isolated” highest density infrared SR source.

Synchrotron Radiation

International Nuclear Information System (INIS)

Asfour, F.I

2000-01-01

Synchrotron light is produced by electron accelerators combined with storage rings. This light is generated over a wide spectral region; from infra-red (IR) through the visible and vacuum ultraviolet (VUV), and into the X-ray region. For relativistic electrons (moving nearly with the speed of light), most radiation is concentrated in a small cone with an opening angle of 1/gamma(some 0.1 to 1 milliradian),where gamma is the electron energy in units of rest energy (typically 10 3 -10 4 ). In synchrotron radiation sources (storage rings) highly relativistic electrons are stored to travel along a circular path for many hours. Radiation is caused by transverse acceleration due to magnetic forces(bending magnets). The radiation is emitted in pulses of 10-20 picosecond, separated by some 2 nanosecond or longer separation

Identification of copper-based green pigments in Jaume Huguet's Gothic altarpieces by Fourier transform infrared microspectroscopy and synchrotron radiation X-ray diffraction.

Science.gov (United States)

Salvadó, N; Pradell, T; Pantos, E; Papiz, M Z; Molera, J; Seco, M; Vendrell-Saz, M

2002-07-01

The scientific investigation of ancient paintings gives a unique insight into ancient painting techniques and their evolution through time and geographic location. This study deals with the identification of the green pigments used by one of the most important Catalan masters in Gothic times, Jaume Huguet. Other pigments and materials have also been characterized by means of conventional techniques such as optical microscopy, scanning electron microscopy and Fourier transform infrared spectroscopy. Synchrotron radiation X-ray diffraction has been used to produce maps of phases at a spatial resolution of 100 microm across chromatic layers.

Synchrotron radiation: its characteristics and applications

International Nuclear Information System (INIS)

Blewett, J.P.; Chasman, R.; Green, G.K.

1977-01-01

It has been known for a century that charged particles radiate when accelerated and that relativistic electrons in the energy range between 100 MeV and several GeV and constrained to travel in circular orbits emit concentrated, intense beams with broad continuous spectra that can cover the electromagnetic spectrum from infrared through hard X-rays. Recently the possible applications of this radiation have been appreciated and electron synchrotrons and electron storage rings are now being used in many centers for studies of the properties of matter in the solid, liquid and gaseous states. A brief history is presented of ''synchrotron radiation'' as it is now called. The basic properties of this radiation are described and the world-wide distribution is indicated of facilities for its production. Particular attention is given to the proposed facility at Brookhaven which will be the first major installation to be dedicated only to the production and use of synchrotron radiation. Finally, typical examples are given of applications in the areas of radiation absorption studies, techniques based on scattering of radiation, and advances based on X-ray lithography

Synchrotron FTIR Imaging For The Identification Of Cell Types Within Human Tissues

International Nuclear Information System (INIS)

Walsh, Michael J.; Pounder, F. Nell; Nasse, Michael J.; Macias, Virgilia; Kajdacsy-Balla, Andre; Hirschmugl, Carol; Bhargava, Rohit

2010-01-01

The use of synchrotron Fourier Transform Infrared spectroscopy (S-FTIR) has been shown to be a very promising tool for biomedical research. S-FTIR spectroscopy allows for the fast acquisition of infrared (IR) spectra at a spatial resolution approaching the IR diffraction limit. The development of the Infrared Environmental Imaging (IRENI) beamline at the Synchrotron Radiation Center (SRC) at the University of Wisconsin-Madison has allowed for diffraction limited imaging measurements of cells in human prostate and breast tissues. This has allowed for the identification of cell types within tissues that would otherwise not have been resolvable using conventional FTIR sources.

Preliminary studies of the effects of psychological stress on circulating lymphocytes analyzed by synchrotron radiation based-Fourier transform infrared microspectroscopy

Science.gov (United States)

Vargas-Caraveo, Alejandra; Castillo-Michel, Hiram; Mejia-Carmona, Gloria Erika; Pérez-Ishiwara, David Guillermo; Cotte, Marine; Martínez-Martínez, Alejandro

2014-07-01

Psychological stress is a condition that not only generates behavioral disorders but also disrupts homeostasis and immune activity that can exacerbate or lead to inflammatory diseases. The aim of this work was to study biochemical changes in circulating immune cells from rats under psychological stress by using vibrational spectroscopy. A stress model was used, where exposure to a stressor was repeated for 5 days. Subsequently, circulating lymphocytes were examined for their biomolecular vibrational fingerprints with synchrotron radiation based-Fourier transform infrared microspectroscopy. The results showed an increased absorption at the ester lipid region (1720-1755 cm-1) in lymphocytes from stressed rats, suggesting lipid peroxidation. Statistical significant changes in wavenumber peak position and absorbance in the nucleic acid region were also observed (915-950 cm-1 Z-DNA, 1090-1150 cm-1 symmetric stretching of Psbnd Osbnd C, 1200-1260 cm-1 asymmetric PO2 and 1570-1510 cm-1 methylated nucleotides) which suggest a reduction of transcriptional activity in lymphocytes from stressed rat. These results unravel part of the mechanisms by which psychological stress may affect the immune system leading to systemic consequences.

CIRCE: A dedicated storage ring for coherent THz synchrotron radiation

International Nuclear Information System (INIS)

Byrd, J.M.; Martin, Michael C.; McKinney, W.R.; Munson, D.V.; Nishimura, H.; Robin, D.S.; Sannibale, F.; Schlueter, R.D.; Thur, W.G.; Jung, J.Y.; Wan, W.

2003-01-01

We present the concepts for an electron storage ring dedicated to and optimized for the production of stable coherent synchrotron radiation (CSR) over the far-infrared terahertz wavelength range from 200 mm to about one cm. CIRCE (Coherent InfraRed CEnter) will be a 66 m circumference ring located on top of the ALS booster synchrotron shielding tunnel and using the existing ALS injector. This location provides enough floor space for both the CIRCE ring, its required shielding, and numerous beamlines. We briefly outline a model for CSR emission in which a static bunch distortion induced by the synchrotron radiation field is used to significantly extend the stable CSR emission towards higher frequencies. This model has been verified with experimental CSR results. We present the calculated CIRCE photon flux where a gain of 6-9 orders of magnitude is shown compared to existing far-IR sources. Additionally, the particular design of the dipole vacuum chamber has been optimized to allow an excellent transmission of these far-infrared wavelengths. We believe that the CIRCE source can be constructed for a modest cost

Synchrotron far-infrared spectroscopy of the two lowest fundamental modes of 1,1-difluoroethane

Science.gov (United States)

Wong, Andy; Thompson, Christopher D.; Appadoo, Dominique R. T.; Plathe, Ruth; Roy, Pascale; Manceron, Laurent; Barros, Joanna; McNaughton, Don

2013-08-01

The far-infrared (FIR) spectrum (50-600 cm-1) of 1,1-difluoroethane was recorded using the high-resolution infrared AILES beamline at the Soleil synchrotron. A ro-vibrational assignment was performed on the lowest wavenumber, low intensity 181 0 and 171 0 modes, yielding band centres of 224.241903 (10) cm-1 and 384.252538 (13) cm-1, respectively. A total of 965 and 2031 FIR transitions were assigned to the 181 0 and 171 0 fundamentals, respectively. Previously measured pure rotational transitions from the upper states were included into the respective fits to yield improved rotational and centrifugal distortion constants. The 182 1 hot band was observed within the fundamental band, with 369 FIR transitions assigned and co-fitted with the fundamental to give a band centre of 431.956502 (39) cm-1 for ν 18 = 2. The 182 0 overtone was observed with 586 transitions assigned and fitted to give a band centre of 431.952763 (23) cm-1 for ν 18 = 2. The difference in energy is attributed to a torsional splitting of 0.003740 (45) cm-1 in the ν 18 = 2 state. Two hot bands originating from the ν 18 = 1 and ν 17 = 1 states were observed within the 171 0 fundamental.

Atomic photoelectron-spectroscopy studies using synchrotron radiation

International Nuclear Information System (INIS)

Kobrin, P.H.

1983-02-01

Photoelectron spectroscopy combined with tunable synchrotron radiation has been used to study the photoionization process in several atomic systems. The time structure of the synchrotron radiation source at the Stanford Synchrotron Radiation Laboratory (SSRL) was used to record time-of-flight (TOF) photoelectron spectra of gaseous Cd, Hg, Ne, Ar, Ba, and Mn. The use of two TOF analyzers made possible the measurement of photoelectron angular distributions as well as branching ratios and partial cross sections

3 GeV Booster Synchrotron Conceptual Design Report

Energy Technology Data Exchange (ETDEWEB)

Wiedemann, Helmut

2009-06-02

Synchrotron light cna be produced from a relativistic particle beam circulating in a storage ring at extremely high intensity and brilliance over a large spectral region reaching from the far infrared regime to hard x-rays. The particles, either electrons or positrons, radiate as they are deflected in the fields of the storage ring bending magnets or of magnets specially optimized for the production of synchrotron light. The synchrotron light being very intense and well collimated in the forward direction has become a major tool in a large variety of research fields in physics, chemistry, material science, biology, and medicine.

FT-IR microscopical analysis with synchrotron radiation: The microscope optics and system performance

International Nuclear Information System (INIS)

Reffner, J.A.; Martoglio, P.A.; Williams, G.P.

1995-01-01

When a Fourier transform infrared (FT-IR) microspectrometer was first interfaced with the National Synchrotron Light Source (NSLS) in September 1993, there was an instant realization that the performance at the diffraction limit had increased 40-100 times. The synchrotron source transformed the IR microspectrometer into a true IR microprobe, providing high-quality IR spectra for probe diameters at the diffraction limit. The combination of IR microspectroscopy and synchrotron radiation provides a powerful new tool for molecular spectroscopy. The ability to perform IR microspectroscopy with synchrotron radiation is still under development at Brookhaven National Laboratory, but several initial studies have been completed that demonstrate the broad-ranging applications of this technology and its potential for materials characterization

FT-IR microscopical analysis with synchrotron radiation: The microscope optics and system performance

Energy Technology Data Exchange (ETDEWEB)

Reffner, J.A.; Martoglio, P.A. [Spectra-Tech, Inc., Shelton, CT (United States); Williams, G.P. [Brookhaven National Lab., Upton, NY (United States)

1995-01-01

When a Fourier transform infrared (FT-IR) microspectrometer was first interfaced with the National Synchrotron Light Source (NSLS) in September 1993, there was an instant realization that the performance at the diffraction limit had increased 40-100 times. The synchrotron source transformed the IR microspectrometer into a true IR microprobe, providing high-quality IR spectra for probe diameters at the diffraction limit. The combination of IR microspectroscopy and synchrotron radiation provides a powerful new tool for molecular spectroscopy. The ability to perform IR microspectroscopy with synchrotron radiation is still under development at Brookhaven National Laboratory, but several initial studies have been completed that demonstrate the broad-ranging applications of this technology and its potential for materials characterization.

Light source for synchrotron radiation x-ray topography study at Beijing Synchrotron Radiation Laboratory (BSRL)

International Nuclear Information System (INIS)

Zhao Jiyong; Jiang Jianhua; Tian Yulian

1992-01-01

Characteristics of the synchrotron radiation source for X-ray topography study at Beijing Synchrotron Radiation Laboratory (BSRL) is described, local geometrical resolution of topographies is discussed, and the diffracting intensities of white beam topography is given

Research by industry at the National Synchrotron Light Source

International Nuclear Information System (INIS)

1995-05-01

The world's foremost facility for research using x-rays and ultraviolet and infrared radiation, is operated by the National Synchrotron Light Source dept. This pamphlet described the participating research teams that built most of the beam lines, various techniques for studying materials, treatment of materials, and various industrial research (catalysis, pharmaceuticals, etc.)

Optimization of a coherent synchrotron radiation source in the Tera-hertz range for high-resolution spectroscopy of molecules of astrophysical interest

International Nuclear Information System (INIS)

Barros, J.

2012-01-01

Fourier Transform spectroscopy is the most used multiplex tool for high-resolution measurements in the infrared range. Its extension to the Tera-hertz domain is of great interest for spectroscopic studies of interstellar molecules. This application is however hampered by the lack of dedicated, broadband sources with a sufficient intensity and stability. In this work, Coherent Synchrotron Radiation (CSR) was used as a source for molecular spectroscopy at high resolution on the AILES infrared and Tera-hertz beamline of SOLEIL synchrotron. The beamline being optimized for far-infrared, we could characterize the properties of CSR and compare them to the incoherent synchrotron radiation. A double detection system allowed to correct the effect of the source-related instabilities, hence to significantly increase the signal-to-noise ratio. Pure rotational spectra were measured using these developments. The case of the propynal molecule, for which a refined set of rotational and centrifugal distortion constants was calculated, proves the complementarity between CSR and the classical microwave or infrared sources. (author)

Plant-based food and feed protein structure changes induced by gene-transformation, heating and bio-ethanol processing: a synchrotron-based molecular structure and nutrition research program.

Science.gov (United States)

Yu, Peiqiang

2010-11-01

Unlike traditional "wet" analytical methods which during processing for analysis often result in destruction or alteration of the intrinsic protein structures, advanced synchrotron radiation-based Fourier transform infrared microspectroscopy has been developed as a rapid and nondestructive and bioanalytical technique. This cutting-edge synchrotron-based bioanalytical technology, taking advantages of synchrotron light brightness (million times brighter than sun), is capable of exploring the molecular chemistry or structure of a biological tissue without destruction inherent structures at ultra-spatial resolutions. In this article, a novel approach is introduced to show the potential of the advanced synchrotron-based analytical technology, which can be used to study plant-based food or feed protein molecular structure in relation to nutrient utilization and availability. Recent progress was reported on using synchrotron-based bioanalytical technique synchrotron radiation-based Fourier transform infrared microspectroscopy and diffused reflectance infrared Fourier transform spectroscopy to detect the effects of gene-transformation (Application 1), autoclaving (Application 2), and bio-ethanol processing (Application 3) on plant-based food and feed protein structure changes on a molecular basis. The synchrotron-based technology provides a new approach for plant-based protein structure research at ultra-spatial resolutions at cellular and molecular levels.

Synchrotron radiation and prospects of its applications

Energy Technology Data Exchange (ETDEWEB)

Kulipanov, G; Skrinskii, A

1981-04-01

Current and prospective applications are described of synchrotron radiation resulting from the motion of high-energy electrons or positrons in a magnetic field and covering a wide spectral range from the infrared to X-ray. The advantages of the synchrotron radiation include a big source luminance, a small angular divergence, the possibility of calculating the absolute intensity and the spectral distribution of the radiation. Special storage rings are most suitable as a source. Synchrotron radiation is applied in X-ray microscopy, energy diffractometry, atomic and molecular spectroscopy, in the structural analysis of microcrystals, very rapid diffractometry of biological objects and crystals, and in Moessbauer spectroscopy. The prospective applications include uses in metrology, medicine, X-ray lithography, elemental analysis, molecular microsurgery, and in radiation technology.

Techniques for Handling and Removal of Spectral Channels in Fourier Transform Synchrotron-Based Spectra

International Nuclear Information System (INIS)

Ibrahim, Amr; Predoi-Cross, Adriana; Teillet, Philippe M.

2010-01-01

Channel spectra are a big problem for those attempting to use synchrotron-based Fourier transform spectra for spectral lineshape studies. Due to the layout of the optical system at the CLS far-infrared beamline, the synchrotron beam undergoes unavoidable multiple reflections on the steering mirrors, beam splitter, several sets of windows, and filters. We present a method for eliminating channel spectra and compare the results of our technique with other methods available in the literature.

Overview and perspective of materials characterization by using synchrotron radiation

International Nuclear Information System (INIS)

Kamitsubo, Hiromichi

2009-01-01

A peculiarity of techniques and the methods of synchrotron radiation are explained. It consists of five sections such as introduction, synchrotron radiation, interaction between X-ray and materials, analytical methods of materials using synchrotron radiation and perspective and problems. The second section described the principles of synchrotron orbit radiation, synchrotron light source, the main formulae and schematic drawing of undulator, and the synchrotron radiation facilities in Japan. The third section explained behavior of X-ray in materials, absorption, reflection, refraction and scattering of X-ray. The fourth section stated many analytical methods of materials; the surface diffractometer, powder diffractometer, high-energy X-ray diffraction, core-electron absorption spectroscopy, micro-beam diffraction, X-ray fluorescence, X-ray absorption fine structure (XAFS), and photoemission spectroscopy (PES). A characteristic feature of synchrotron radiation contains the large wave length ranges from infrared to X-ray, high directivity and brightness, linear (circular) polarization, pulsed light, good control and stability. The brightness spectra of Spring-8 and SAGA-LS, concept of synchrotron light source, undulator and wiggler, nine synchrotron radiation facilities in Japan, mass absorption coefficients of Cu and Au, and analysis of materials using synchrotron radiation are illustrated. (S.Y.)

Synchrotron radiation sources: general features and vacuum system

International Nuclear Information System (INIS)

Craievich, A.F.

1985-01-01

In the last years the electron or positron storage rings, which were until 1970 only used for high energy physics experiments, begun to be built in several countries exclusively as electromagnetic radiation source (synchrotron radiation). The sources are generally made up by injector (linear accelerator or microtron), 'booster' (synchrotron), storage ring, insertions ('Wigglers' and ondulators) and light lines. The interest by these sources are due to the high intensity, large spectrum (from infrared to the X-rays), polarization and pulsed structure of the produced radiation. For the ultra-vacuum obtainement, necessary for the functioning storage rings (p=10 -9 Torr), several special procedures are used. In Brazil the Synchrotron Radiation National Laboratory of the CNPq worked out a conceptual project of synchrotron radiation source, whose execution should begin by the construction of the several components prototypes. (L.C.) [pt

SPITZER OBSERVATIONS OF GX17+2: CONFIRMATION OF A PERIODIC SYNCHROTRON SOURCE

International Nuclear Information System (INIS)

Harrison, Thomas E.; McNamara, Bernard J.; Bornak, Jillian; Gelino, Dawn M.; Wachter, Stefanie; Rupen, Michael P.; Gelino, Christopher R.

2011-01-01

GX17+2 is a low-mass X-ray binary (LMXB) that is also a member of a small family of LMXBs known as 'Z-sources' that are believed to have persistent X-ray luminosities that are very close to the Eddington limit. GX17+2 is highly variable at both radio and X-ray frequencies, a feature common to Z-sources. What sets GX17+2 apart is its dramatic variability in the near-infrared, where it changes by ΔK ∼ 3 mag. Previous investigations have shown that these brightenings are periodic, recurring every 3.01 days. Given its high extinction (A V ≥ 9 mag), it has not been possible to ascertain the nature of these events with ground-based observations. We report mid-infrared Spitzer observations of GX17+2 which indicate a synchrotron spectrum for the infrared brightenings. In addition, GX17+2 is highly variable in the mid-infrared during these events. The combination of the large-scale outbursts, the presence of a synchrotron spectrum, and the dramatic variability in the mid-infrared suggest that the infrared brightening events are due to the periodic transit of a synchrotron jet across our line of sight. An analysis of both new, and archival, infrared observations has led us to revise the period for these events to 3.0367 days. We also present new Rossi X-Ray Timing Explorer (RXTE) data for GX17+2 obtained during two predicted infrared brightening events. Analysis of these new data, and data from the RXTE archive, indicates that there is no correlation between the X-ray behavior of this source and the observed infrared brightenings. We examine various scenarios that might produce periodic jet emission.

Synchrotron light and its uses

International Nuclear Information System (INIS)

Blewett, J.P.

1978-01-01

It was known for a century that charged particles radiate when accelerated and that relativistic electrons in the energy range between 100 MeV and several GeV and constrained to travel in circular orbits emit concentrated, intense beams with broad continuous spectra that can cover the electromagnetic spectrum from infrared through hard x-rays. Recently the possible applications of this radiation were appreciated and electron synchrotrons and electron storage rings are now being used in many centers for studies of the properties of matter in the solid, liquid and gaseous states. 10 references

Photoionization studies of atoms and molecules using synchrotron radiation

International Nuclear Information System (INIS)

Lindle, D.W.

1988-01-01

Photoionization studies of free atoms and molecules have undergone considerable development in the past decade, in large part due to the use of synchrotron radiation. The tunability of synchrotron radiation has permitted the study of photoionization processes near valence-and core-level ionization thresholds for atoms and molecules throught the Periodic Table. A general illustration of these types of study will be presented, with emphasis on a few of the more promising new directions in atomic and molecular physics being pursued with synchrotron radiation. (author) [pt

Mechanistic insights into nanotoxicity determined by synchrotron radiation-based Fourier-transform infrared imaging and multivariate analysis.

Science.gov (United States)

Riding, Matthew J; Trevisan, Júlio; Hirschmugl, Carol J; Jones, Kevin C; Semple, Kirk T; Martin, Francis L

2012-12-01

Our ability to identify the mechanisms by which carbon-based nanomaterials (CBNs) exert toxicity in cells is constrained by the lack of standardized methodologies to assay endpoint effects. Herein we describe a method of mechanistically identifying the effects of various CBN types in both prokaryotic and eukaryotic cells using multi-beam synchrotron radiation-based Fourier-transform infrared imaging (SR-FTIRI) at diffraction-limited resolution. This technique overcomes many of the inherent difficulties of assaying nanotoxicity and demonstrates exceptional sensitivity in identifying the effects of CBNs in cells at environmentally-relevant concentrations. We identify key mechanisms of nanotoxicity as the alteration of Amide and lipid biomolecules, but propose more specific bioactivity of CBNs occurs as a result of specific interactions between CBN structural conformation and cellular characteristics. Copyright © 2012 Elsevier Ltd. All rights reserved.

Singapore Synchrotron Light Source - Status, first results, program

CERN Document Server

Moser, H O; Kempson, V C; Kong, J R; Li, Z W; Nyunt, T; Qian, H J; Rossmanith, R; Tor, P H; Wilhelmi, O; Yang, P; Zheng, H W; Underhay, I J

2003-01-01

The Singapore Synchrotron Light Source is a general-purpose synchrotron radiation facility serving research organisations and industry. Beamlines active or coming up within 2002 include lithography for micro/nanofabrication, phase contrast imaging, surface science, and X-ray diffraction and absorption. An infrared spectro/microscopy beamline is expected to become operational in 2003. Further beamlines are under discussion with user groups. The Microtron Undulator Radiation Facility (MURF) is under development to provide brilliant VUV radiation and to prepare for subsequent development of an EUV and X-ray FEL.

Infrared spectroscopy with synchrotron radiation

International Nuclear Information System (INIS)

Lagarde, P.

1978-01-01

Storage rings are normally used as sources of radiation in the X-ray and the u.v. part of the spectrum. It is shown that, with a specially designed component, a storage ring like ACO at Orsay is a very powerful far-infrared source, whose advantages over classical wide band sources are reviewed. (author)

The synchrotron radiation

International Nuclear Information System (INIS)

Chevallier, P.

1994-01-01

Synchrotron Radiation is a fantastic source of electromagnetic radiation the energy spectrum of which spreads continuously from the far infrared to hard X-rays. For this reason a wide part of the scientific community, fundamentalists as well as industry, is concerned by its use. We shall describe here the main properties of this light source and give two examples of application in the field of characterization of materials: EXAFS (Extended X-Ray Absorption Fine Structure) and X-ray fluorescence. (author). 8 figs., 21 refs

Chemical changes demonstrated in cartilage by synchrotron infrared microspectroscopy in an antibody-induced murine model of rheumatoid arthritis

Science.gov (United States)

Croxford, Allyson M.; Selva Nandakumar, Kutty; Holmdahl, Rikard; Tobin, Mark J.; McNaughton, Don; Rowley, Merrill J.

2011-06-01

Collagen antibody-induced arthritis develops in mice following passive transfer of monoclonal antibodies (mAbs) to type II collagen (CII) and is attributed to effects of proinflammatory immune complexes, but transferred mAbs may react directly and damagingly with CII. To determine whether such mAbs cause cartilage damage in vivo in the absence of inflammation, mice lacking complement factor 5 that do not develop joint inflammation were injected intravenously with two arthritogenic mAbs to CII, M2139 and CIIC1. Paws were collected at day 3, decalcified, paraffin embedded, and 5-μm sections were examined using standard histology and synchrotron Fourier-transform infrared microspectroscopy (FTIRM). None of the mice injected with mAb showed visual or histological evidence of inflammation but there were histological changes in the articular cartilage including loss of proteoglycan and altered chondrocyte morphology. Findings using FTIRM at high lateral resolution revealed loss of collagen and the appearance of a new peak at 1635 cm-1 at the surface of the cartilage interpreted as cellular activation. Thus, we demonstrate the utility of synchrotron FTIRM for examining chemical changes in diseased cartilage at the microscopic level and establish that arthritogenic mAbs to CII do cause cartilage damage in vivo in the absence of inflammation.

The national synchrotron light source and its applications

Energy Technology Data Exchange (ETDEWEB)

Williams, G.P.

1989-01-01

We describe the National Synchrotron Light Source facility including its beamlines and operational characteristics. Research results on selected beamlines on the VUV ring which highlight new experimental capabilities are described since they are more relevant to the program at HESYRL. Examples chosen are spin-polarized photoemission, infra-red surface science, high resolution core level spectroscopy, X- Ray lithography, photoelectron/Auger coincidence spectroscopy and high electron momentum resolution surface studies. 7 refs., 3 figs., 3 tabs.

Synchrotron environmental laboratory (SUL) at Anka

International Nuclear Information System (INIS)

Denecke, M.A.

2002-01-01

) speciation methods, applications of micro-focusing for studies on heterogeneous systems and imaging techniques as well as synchrotron infrared spectroscopy are planned to be available. (author)

Biosorption of malachite green onto Haematococcus pluvialis observed through synchrotron-FTIR microspectroscopy.

Science.gov (United States)

Liu, J H; Zhang, L; Zha, D C; Chen, L Q; Chen, X X; Qi, Z M

2018-06-28

Microalgae have emerged as promising biosorbents for the treatment of malachite green in wastewater. However, the underlying mechanism for the biosorption of malachite green onto microalgae is still unclear and needs further intensive study. In this work, synchrotron Fourier-transform infrared (synchrotron-FTIR) microspectroscoy in combination with biochemical assay is employed to evaluate malachite green removal efficiency (95.2%, 75.6% and 66.5%) by three stages of Haematococcus pluvialis. Meanwhile, the various vital changes of algal cells including lipids, proteins, polysaccharides and carotenoids, is distinguished and quantified in situ. This study illustrates that synchrotron-FTIR microspectroscopy is an effective and powerful tool to scrutinize the mechanism for the interactions between the malachite green dye and microalgal cells and it even provides an effective and none-invasive new approach to screen potentially proper biosorbents for the removal of dyes from wastewater. This article is protected by copyright. All rights reserved. This article is protected by copyright. All rights reserved.

Towards a table-top synchrotron based on supercontinuum generation

DEFF Research Database (Denmark)

Petersen, Christian Rosenberg; Moselund, Peter M.; Huot, Laurent

2018-01-01

Recently, high brightness and broadband supercontinuum (SC) sources reaching far into the infrared (IR) have emerged with the potential to rival traditional broadband sources of IR radiation. Here, the brightness of these IR SC sources is compared with that of synchrotron IR beamlines and Si...

MICROANALYSIS OF MATERIALS USING SYNCHROTRON RADIATION.

Energy Technology Data Exchange (ETDEWEB)

JONES,K.W.; FENG,H.

2000-12-01

High intensity synchrotron radiation produces photons with wavelengths that extend from the infrared to hard x rays with energies of hundreds of keV with uniquely high photon intensities that can be used to determine the composition and properties of materials using a variety of techniques. Most of these techniques represent extensions of earlier work performed with ordinary tube-type x-ray sources. The properties of the synchrotron source such as the continuous range of energy, high degree of photon polarization, pulsed beams, and photon flux many orders of magnitude higher than from x-ray tubes have made possible major advances in the possible chemical applications. We describe here ways that materials analyses can be made using the high intensity beams for measurements with small beam sizes and/or high detection sensitivity. The relevant characteristics of synchrotron x-ray sources are briefly summarized to give an idea of the x-ray parameters to be exploited. The experimental techniques considered include x-ray fluorescence, absorption, and diffraction. Examples of typical experimental apparatus used in these experiments are considered together with descriptions of actual applications.

Planning study for advanced national synchrotron-radiation facilities

International Nuclear Information System (INIS)

1984-01-01

A new generation of synchrotron-radiation sources based on insertion devices offers gains in photon-beam brilliance as large as the gains that present-day synchrotron sources provided over conventional sources. This revolution in synchrotron capability and its impact on science and technology will be as significant as the original introduction of synchrotron radiation. This report recommends that insertion-device technology be pursued as our highest priority, both through the full development of insertion-device potential on existing machines and through the building of new facilities

A preliminary study of synchrotron light sources for x-ray lithography

International Nuclear Information System (INIS)

Hoffmann, C.R.; Bigham, C.B.; Ebrahim, N.A.; Sawicki, J.A.; Taylor, T.

1989-02-01

A preliminary study of synchrotron light sources has been made, primarily oriented toward x-ray lithography. X-ray lithography is being pursued vigorously in several countries, with a goal of manufacturing high-density computer chips (0.25 μm feature sizes), and may attain commercial success in the next decade. Many other applications of soft x-rays appear worthy of investigation as well. The study group visited synchrotron radiation facilities and had discussions with members of the synchrotron radiation community, particularly Canadians. It concluded that accelerator technology for a conventional synchrotron light source appropriate for x-ray lithography is well established and is consistent with skills and experience at Chalk River Nuclear Laboratories. Compact superconducting systems are being developed also. Their technical requirements overlap with capabilities at Chalk River. (32 refs)

ANKA - new horizons with synchrotron radiation

International Nuclear Information System (INIS)

Hagelstein, M.; Czolk, R.

2001-01-01

ANKA GmbH operates a state-of-the-art electron storage ring (2.5 GeV energy, 400 mA maximum current) for the production of high-intensity synchrotron radiation. The produced 'superlight' ranges from the hard X-ray to the infrared region of the electromagnetic spectrum. To use the light for microfabrication and analysis a number of modern, high quality production and experimental facilities exist on this circular (diameter about 35 m) synchrotron radiation sources. The experimental facilities are consolidated by a young, experienced and highly motivated team of experts. For the patterning of polymers by deep X-ray lithography three end-stations (so-called beamlines) are available. For analytical tasks five beamlines are established where different experiments can be made based on X-ray methods such as X-ray absorption, diffraction and fluorescence spectroscopy as well as IR-spectroscopy. (orig.)

Longitudinal tracking studies for a high intensity proton synchrotron

International Nuclear Information System (INIS)

Lessner, E.; Cho, Y.; Harkay, K.; Symon, K.

1995-01-01

Results from longitudinal tracking studies for a high intensity proton synchrotron designed for a 1-MW spallation source are presented. The machine delivers a proton beam of 0.5 mA time-averaged current at a repetition rate of 30 Hz. The accelerator is designed to have radiation levels that allow hands-on-maintenance. However, the high beam intensity causes strong space charge fields whose effects may lead to particle loss and longitudinal instabilities. The space charge fields modify the particle distribution, distort the stable bucket area and reduce the rf linear restoring force. Tracking simulations were conducted to analyze the space charge effects on the dynamics of the injection and acceleration processes and means to circumvent them. The tracking studies led to the establishment of the injected beam parameters and rf voltage program that minimized beam loss and longitudinal instabilities. Similar studies for a 10-GeV synchrotron that uses the 2-GeV synchrotron as its injector are also discussed

Advanced development of catalysts by using the high-brilliance synchrotron radiation in SPring-8

International Nuclear Information System (INIS)

2006-10-01

The advanced development of catalysts by using the high-brilliance synchrotron radiation in SPring-8 is described: (1) the industrial use of SPring-8, (2) the analytical methods of catalyst using SPring-8 (XAFS, powder X-ray diffraction, thin film X-ray scattering, X-ray imaging, infrared analysis, X-ray fluorescence analysis, and photoelectron spectroscopy etc.), (3) the history of synchrotron radiation and catalyst investigations, (4) the new advanced measuring methods of catalyst using synchrotron radiation (various X-ray spectroscopic methods, and application of XAFS to highly-disperse systems of catalyst), and (5) the new advanced development of catalysts using synchrotron radiation and its applications (motor-car catalysts, light catalysts, fuel cells, nanotechnology, and trace amounts of catalyst in wastes). (M.H.)

Structural evolution in the isothermal crystallization process of the molten nylon 10/10 traced by time-resolved infrared spectral measurements and synchrotron SAXS/WAXD measurements

International Nuclear Information System (INIS)

Tashiro, Kohji; Nishiyama, Asami; Tsuji, Sawako; Hashida, Tomoko; Hanesaka, Makoto; Takeda, Shinichi; Weiyu, Cao; Reddy, Kummetha Raghunatha; Masunaga, Hiroyasu; Sasaki, Sono; Takata, Masaki; Ito, Kazuki

2009-01-01

The structural evolution in the isothermal crystallization process of nylon 10/10 from the melt has been clarified concretely on the basis of the time-resolved infrared spectral measurement as well as the synchrotron wide-angle and small-angle X-ray scattering measurements. Immediately after the temperature jump from the melt to the crystallization point, the isolated domains consisting of the hydrogen-bonded random coils were formed in the melt, as revealed by Guinier plot of SAXS data and the infrared spectral data. With the passage of time these domains approached each other with stronger correlation as analyzed by Debye-Bueche equation. These domains transformed finally to the stacked crystalline lamellae, in which the conformationally-regularized methylene segments of the CO sides were connected each other by stronger intermolecular hydrogen bonds to form the crystal lattice.

Synchrotron light beam and a synchrotron light experiment facility

International Nuclear Information System (INIS)

Ando, Masami

1980-01-01

In the National Laboratory for High Energy Physics, about two years ago, the requirements of synchrotron light beam in respective measuring instruments were discussed. Then, also the arrangement (lattice) of a storage ring, the nature of synchrotron light beam, a synchrotron light experiment facility and the arrangement of the beam lines were studied. During the period of two years since then, due to the changes in the circumstances, the design of the lattice was altered. Accordingly, the arrangement of the beam lines and of measuring instruments were largely changed. At this point, the results of discussions in various meetings are described, though they may still be subject to future changes, with due consideration to beam, environment and beam lines required for the design of the measuring instruments: (1) storage ring and synchrotron light beam, (2) requirements on small beam size and beam stability, (3) a synchrotron light experiment facility. (J.P.N.)

Luminosity dependence in the ratio of X-ray to infrared emission of QSOs

International Nuclear Information System (INIS)

Worrall, D.M.

1987-01-01

The correlation of X-ray and near-infrared luminosity is studied for a sample of radio-quiet QSOs. The X-ray to infrared ratio is found to decrease as the infrared luminosity increases. No preference is found between the correlations of X-ray luminosity with optical or infrared luminosity. This implies that optical and infrared emission are equally good predictors of X-ray emission. Source models which directly link infrared and X-ray emission are discussed, and a preference is found for a specific synchrotron self-Compton model. This model predicts the correct luminosity dependence of the X-ray to infrared ratio if certain conditions apply. 55 references

A dedicated storage ring for Far-IR coherent synchrotron radiation at the ALS

International Nuclear Information System (INIS)

Barry, W.C.; Baptist, K.M.; Benjegerdes, R.J.; Biocca, A.K.; Byrd, J.M.; Byrne, W.E.; Cambie, D.; Chin, M.J.; Harkins, J.P.; Kwiatkowski, S.; Li, D.; Marks, S.; Martin, M.C.; McKinney, W.R.; Munson, D.V.; Nishimura, H.; Paterson, J.A.; Plate, D.W.; Rex, K.R.; Robin, D.S.; Rossi, S.L.; Sannibale, F.; Scarvie, T.; Schlueter, R.D.; Steier, C.A.; Stover, G.D.; Thur, W.G.; Jung, J.Y.; Zbasnik, J.P.

2002-01-01

We present the concepts for a storage ring dedicated to and optimized for the production of stable coherent synchrotron radiation (CSR) over the far-infrared wavelength range from about 200 microns to 1 mm

Synchrotron-based X-ray microscopic studies for bioeffects of nanomaterials.

Science.gov (United States)

Zhu, Ying; Cai, Xiaoqing; Li, Jiang; Zhong, Zengtao; Huang, Qing; Fan, Chunhai

2014-04-01

There have been increasing interests in studying biological effects of nanomaterials, which are nevertheless faced up with many challenges due to the nanoscale dimensions and unique chemical properties of nanomaterials. Synchrotron-based X-ray microscopy, an advanced imaging technology with high spatial resolution and excellent elemental specificity, provides a new platform for studying interactions between nanomaterials and living systems. In this article, we review the recent progress of X-ray microscopic studies on bioeffects of nanomaterials in several living systems including cells, model organisms, animals and plants. We aim to provide an overview of the state of the art, and the advantages of using synchrotron-based X-ray microscopy for characterizing in vitro and in vivo behaviors and biodistribution of nanomaterials. We also expect that the use of a combination of new synchrotron techniques should offer unprecedented opportunities for better understanding complex interactions at the nano-biological interface and accounting for unique bioeffects of nanomaterials. Synchrotron-based X-ray microscopy is a non-destructive imaging technique that enables high resolution spatial mapping of metals with elemental level detection methods. This review summarizes the current use and perspectives of this novel technique in studying the biology and tissue interactions of nanomaterials. Copyright © 2014 Elsevier Inc. All rights reserved.

Diffuse Scattering of the Conduction Electrons of a Metallic Substrate by an Adsorbate: an Experimental Study Using Synchrotron Infrared Radiation

International Nuclear Information System (INIS)

Hein, M.; Otto, A.; Dumas, P.; Williams, G. P.

1999-01-01

Due to its intrinsic high brightness, high stability, and proportionality to the stored electron beam current, synchrotrons IR spectroscopy has revealed itself as an unique tool to experimentally test a physical phenomenon occurring at metallic interfaces, the theory for which was motivated by previous observations. Any adsorbate induces inelastic scattering of the conduction electrons, which causes a broadband IR reflectance change, and was predicted to induce a concomitant DC resistivity change. By choosing a well ordered single crystal thin film of Cu(111), we have checked that the DC resistivity change, and the asymptotic limit of the IR reflectance change are linearly dependent, but independent of the nature of the adsorbate. Coadsorption experiments which have been used to modify the induced density of states at the Fermi level, have further demonstrated that the friction coefficient, which is responsible for the elastic scattering phenomenon, is chemically specific. This article describes the use of synchrotron radiation as an absolute source and its application to the study of dynamics of adsorbates on surfaces

Initial scientific uses of coherent synchrotron radiation inelectron storage rings

Energy Technology Data Exchange (ETDEWEB)

Basov, D.N.; Feikes, J.; Fried, D.; Holldack, K.; Hubers, H.W.; Kuske, P.; Martin, M.C.; Pavlov, S.G.; Schade, U.; Singley, E.J.; Wustefeld, G.

2004-11-23

The production of stable, high power, coherent synchrotron radiation at sub-terahertz frequency at the electron storage ring BESSY opens a new region in the electromagnetic spectrum to explore physical properties of materials. Just as conventional synchrotron radiation has been a boon to x-ray science, coherent synchrotron radiation may lead to many new innovations and discoveries in THz physics. With this new accelerator-based radiation source we have been able to extend traditional infrared measurements down into the experimentally poorly accessible sub-THz frequency range. The feasibility of using the coherent synchrotron radiation in scientific applications was demonstrated in a series of experiments: We investigated shallow single acceptor transitions in stressed and unstressed Ge:Ga by means of photoconductance measurements below 1 THz. We have directly measured the Josephson plasma resonance in optimally doped Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8} for the first time and finally we succeeded to confine the sub-THz radiation for spectral near-field imaging on biological samples such as leaves and human teeth.

Analytical research using synchrotron radiation based techniques

International Nuclear Information System (INIS)

Jha, Shambhu Nath

2015-01-01

There are many Synchrotron Radiation (SR) based techniques such as X-ray Absorption Spectroscopy (XAS), X-ray Fluorescence Analysis (XRF), SR-Fourier-transform Infrared (SRFTIR), Hard X-ray Photoelectron Spectroscopy (HAXPS) etc. which are increasingly being employed worldwide in analytical research. With advent of modern synchrotron sources these analytical techniques have been further revitalized and paved ways for new techniques such as microprobe XRF and XAS, FTIR microscopy, Hard X-ray Photoelectron Spectroscopy (HAXPS) etc. The talk will cover mainly two techniques illustrating its capability in analytical research namely XRF and XAS. XRF spectroscopy: XRF spectroscopy is an analytical technique which involves the detection of emitted characteristic X-rays following excitation of the elements within the sample. While electron, particle (protons or alpha particles), or X-ray beams can be employed as the exciting source for this analysis, the use of X-ray beams from a synchrotron source has been instrumental in the advancement of the technique in the area of microprobe XRF imaging and trace level compositional characterisation of any sample. Synchrotron radiation induced X-ray emission spectroscopy, has become competitive with the earlier microprobe and nanoprobe techniques following the advancements in manipulating and detecting these X-rays. There are two important features that contribute to the superb elemental sensitivities of microprobe SR induced XRF: (i) the absence of the continuum (Bremsstrahlung) background radiation that is a feature of spectra obtained from charged particle beams, and (ii) the increased X-ray flux on the sample associated with the use of tunable third generation synchrotron facilities. Detection sensitivities have been reported in the ppb range, with values of 10 -17 g - 10 -14 g (depending on the particular element and matrix). Keeping in mind its demand, a microprobe XRF beamline has been setup by RRCAT at Indus-2 synchrotron

Infrared absorption of human breast tissues in vitro

Energy Technology Data Exchange (ETDEWEB)

Liu Chenglin [Department of Physics, Surface Physics Laboratory (National Key laboratory), Synchrotron Radiation Research Center, Fudan University, Shanghai 200433 (China); Physics Department of Yancheng Teachers' College, Yancheng 224002 (China); Zhang Yuan [Department of Physics, Surface Physics Laboratory (National Key laboratory), Synchrotron Radiation Research Center, Fudan University, Shanghai 200433 (China); Yan Xiaohui [Department of Physics, Surface Physics Laboratory (National Key laboratory), Synchrotron Radiation Research Center, Fudan University, Shanghai 200433 (China); Zhang Xinyi [Department of Physics, Surface Physics Laboratory (National Key laboratory), Synchrotron Radiation Research Center, Fudan University, Shanghai 200433 (China) and Shanghai Research Center of Acupuncture and Meridian, Pudong, Shanghai 201203 (China)]. E-mail: xy-zhang@fudan.edu.cn; Li Chengxiang [National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230029 (China); Yang Wentao [Cancer Hospital, Medical Center, Fudan University, Shanghai 200032 (China); Shi Daren [Cancer Hospital, Medical Center, Fudan University, Shanghai 200032 (China)

2006-07-15

The spectral characteristics of human breast tissues in normal status and during different cancerous stages have been investigated by synchrotron radiation based Fourier transform infrared (SR-FTIR) absorption spectroscopy. Thanks to the excellent synchrotron radiation infrared (IR) source, higher resolving power is achieved in SR-FTIR absorption spectra than in conventional IR absorption measurements. Obvious variations in IR absorption spectrum of breast tissues were found as they change from healthy to diseased, or say in progression to cancer. On the other hand, some specific absorption peaks were found in breast cancer tissues by SR-FTIR spectroscopic methods. These spectral characteristics of breast tissue may help us in early diagnosis of breast cancer.

A study on growth and pyrolysis characteristics of microalgae using Thermogravimetric Analysis-Infrared Spectroscopy and synchrotron Fourier Transform Infrared Spectroscopy.

Science.gov (United States)

Li, Fanghua; Srivatsa, Srikanth Chakravartula; Batchelor, Warren; Bhattacharya, Sankar

2017-04-01

This two-part study firstly investigated Tetraselmis suecica grown in different CO 2 (0.04-15%v/v) concentration through indoor and outdoor cultivation systems. A high CO 2 concentration led to a high lipid content, and low nitrogen and oxygen content, which are desirable for transport fuel production. Pyrolysis characteristics were investigated by TG-IR and synchrotron IR microscopy. The results show Tetraselmis suecica grown in 10%CO 2 had the highest decomposition rate corresponding to more volatile products produced during the main thermal cracking stage and derived from protein-and lipid-corresponding functional groups. Moreover, a high reaction temperature and CO 2 concentration resulted in a low retention of surface functional groups. The nitrogen functional groups initially decomposed at a temperature range of 250-300°C and still remained at 550°C, while the lipid-corresponding functional groups completely disappeared at a temperature range of 400-500°C. Besides, the decomposition of chemical components followed the order of carbohydrate, protein and lipid. Copyright © 2017 Elsevier Ltd. All rights reserved.

European Synchrotron Radiation Facility

International Nuclear Information System (INIS)

Buras, B.

1985-01-01

How a European Synchrotron Radiation Facility has developed into a detailed proposal recently accepted as the basis for construction of the facility at Grenoble is discussed. In November 1977, the General Assembly of the European Science Foundation (ESF) approved the report of the ESF working party on synchrotron radiation entitled Synchrotron Radiation - a Perspective View for Europe. This report contained as one of its principal recommendations that work should commence on a feasibility study for a European synchrotron radiation laboratory having a dedicated hard X-ray storage ring and appropriate advanced instrumentation. In order to prepare a feasibility study the European Science Foundation set up the Ad-hoc Committee on Synchrotron Radiation, which in turn formed two working groups: one for the machine and another for instrumentation. This feasibility study was completed in 1979 with the publication of the Blue Book describing in detail the so called 1979 European Synchrotron Radiation Facility. The heart of the facility was a 5 GeV electron storage ring and it was assumed that mainly the radiation from bending magnets will be used. The facility is described

Coherent Synchrotron Radiation: Theory and Simulations

International Nuclear Information System (INIS)

Novokhatski, Alexander

2012-01-01

The physics of coherent synchrotron radiation (CSR) emitted by ultra-relativistic electron bunches, known since the last century, has become increasingly important with the development of high peak current free electron lasers and shorter bunch lengths in storage rings. Coherent radiation can be described as a low frequency part of the familiar synchrotron radiation in bending magnets. As this part is independent of the electron energy, the fields of different electrons of a short bunch can be in phase and the total power of the radiation will be quadratic with the number of electrons. Naturally the frequency spectrum of the longitudinal electron distribution in a bunch is of the same importance as the overall electron bunch length. The interest in the utilization of high power radiation from the terahertz and far infrared region in the field of chemical, physical and biological processes has led synchrotron radiation facilities to pay more attention to the production of coherent radiation. Several laboratories have proposed the construction of a facility wholly dedicated to terahertz production using the coherent radiation in bending magnets initiated by the longitudinal instabilities in the ring. Existing synchrotron radiation facilities also consider such a possibility among their future plans. There is a beautiful introduction to CSR in the 'ICFA Beam Dynamics Newsletter' N 35 (Editor C. Biscari). In this paper we recall the basic properties of CSR from the theory and what new effects, we can get from the precise simulations of the coherent radiation using numerical solutions of Maxwell's equations. In particular, transverse variation of the particle energy loss in a bunch, discovered in these simulations, explains the slice emittance growth in bending magnets of the bunch compressors and transverse de-coherence in undulators. CSR may play same the role as the effect of quantum fluctuations of synchrotron radiation in damping rings. It can limit the minimum

Synchrotron radiation

International Nuclear Information System (INIS)

Knotek, M.L.

1987-01-01

Synchrotron radiation has had a revolutionary effect on a broad range of scientific studies, from physics, chemistry and metallurgy to biology, medicine and geoscience. The situation during the last decade has been one of very rapid growth, there is a great vitality to the field and a capability has been given to a very broad range of scientific disciplines which was undreamed of just a decade or so ago. Here we will discuss some of the properties of synchrotron radiation that makes it so interesting and something of the sources in existence today including the National Synchrotron Light Source (NSLS). The NSLS is one of the new facilities built specifically for synchrotron radiation research and the model that was developed there for involvement of the scientific community is a good one which provides some good lessons for these facilities and others

Applications of synchrotron radiation to Chemical Engineering Science: Workshop report

International Nuclear Information System (INIS)

1991-07-01

This report contains extended abstracts that summarize presentations made at the Workshop on Applications of Synchrotron Radiation to Chemical Engineering Science held at Argonne National Laboratory (ANL), Argonne, IL, on April 22--23, 1991. The talks emphasized the application of techniques involving absorption fluorescence, diffraction, and reflection of synchrotron x-rays, with a focus on problems in applied chemistry and chemical engineering, as well as on the use of x-rays in topographic, tomographic, and lithographic procedures. The attendees at the workshop included experts in the field of synchrotron science, scientists and engineers from ANL, other national laboratories, industry, and universities; and graduate and undergraduate students who were enrolled in ANL educational programs at the time of the workshop. Talks in the Plenary and Overview Session described the status of and special capabilities to be offered by the Advanced Photon Source (APS), as well as strategies and opportunities for utilization of synchrotron radiation to solve science and engineering problems. Invited talks given in subsequent sessions covered the use of intense infrared, ultraviolet, and x-ray photon beams (as provided by synchrotrons) in traditional and nontraditional areas of chemical engineering research related to electrochemical and corrosion science, catalyst development and characterization, lithography and imaging techniques, and microanalysis

Applications of synchrotron radiation to Chemical Engineering Science: Workshop report

Energy Technology Data Exchange (ETDEWEB)

1991-07-01

This report contains extended abstracts that summarize presentations made at the Workshop on Applications of Synchrotron Radiation to Chemical Engineering Science held at Argonne National Laboratory (ANL), Argonne, IL, on April 22--23, 1991. The talks emphasized the application of techniques involving absorption fluorescence, diffraction, and reflection of synchrotron x-rays, with a focus on problems in applied chemistry and chemical engineering, as well as on the use of x-rays in topographic, tomographic, and lithographic procedures. The attendees at the workshop included experts in the field of synchrotron science, scientists and engineers from ANL, other national laboratories, industry, and universities; and graduate and undergraduate students who were enrolled in ANL educational programs at the time of the workshop. Talks in the Plenary and Overview Session described the status of and special capabilities to be offered by the Advanced Photon Source (APS), as well as strategies and opportunities for utilization of synchrotron radiation to solve science and engineering problems. Invited talks given in subsequent sessions covered the use of intense infrared, ultraviolet, and x-ray photon beams (as provided by synchrotrons) in traditional and nontraditional areas of chemical engineering research related to electrochemical and corrosion science, catalyst development and characterization, lithography and imaging techniques, and microanalysis.

Synchrotron x-ray reflectivity study of oxidation/passivation of copper and silicon

International Nuclear Information System (INIS)

Chu, Y.; Nagy, Z.; Parkhutik, V.; You, H.

1999-01-01

Synchrotron x-ray-scattering technique studies of copper and silicon electrochemical interfaces are reported. These two examples illustrate the application of synchrotron x-ray techniques for oxidation, passivation, and dissolution of metals and semiconductors

Synchrotron x-ray reflectivity study of oxidation/passivation of copper and silicon.

Energy Technology Data Exchange (ETDEWEB)

Chu, Y.; Nagy, Z.; Parkhutik, V.; You, H.

1999-07-21

Synchrotron x-ray-scattering technique studies of copper and silicon electrochemical interfaces are reported. These two examples illustrate the application of synchrotron x-ray techniques for oxidation, passivation, and dissolution of metals and semiconductors.

Study of beam dynamics at cooler synchrotron TARN-II

International Nuclear Information System (INIS)

Watanabe, S.; Katayama, T.; Watanabe, T.; Yoshizawa, M.; Tomizawa, M.; Chida, K.; Arakaki, Y.; Noda, K.; Kanazawa, M.

1992-08-01

Several kinds of beam diagnostic instruments, have been developed at cooler-synchrotron TARN-II. These are intended to study beam dynamics at low beam current of several microamperes and then have high sensitivity of good S/N ratio. In addition, the acceleration system, especially low level RF system, has been improved to attain the maximum beam energy. With the successful performance of these instrumentations, the study of beam dynamics are presently being carried out. For example, the synchrotron acceleration of the light ions was achieved up to 220 MeV/u without any beam loss. (author)

Chemistry with synchrotron radiation

International Nuclear Information System (INIS)

Preses, J.; Grover, J.R.; White, M.G.; Kvick, A.

1990-01-01

An accidental by-product of high-energy physics, synchrotron radiation, has emerged as one of the most powerful tools for the understanding of chemical reactions. Advances made by using synchrotron radiation in physical chemistry are reviewed herein. Descriptions of experiments exploiting the many ways that synchrotron radiation can be manipulated are presented. These manipulations include intensification of the radiation and compression or shifting of its spectral structure. Combinations of the use of synchrotron radiation, which provides access to very short wavelengths and is, at the same time, continuously and easily tunable, with laser radiation, which offers much higher resolution and much more intense radiation per pulse, but is difficult to tune in the ultraviolet region of the spectra, gives the chemist a way to map a molecule's potential energy curve, to note the lengths and strengths of chemical bonds, and to predict and explain novel reactions of more complex molecules. The use of diffraction of x-rays to study the spacing of atoms in crystals is discussed. Various applications of synchrotron radiation to studies of the fluorescence of hydrocarbons and to the chiral dichroism studies of other natural products like DNA and RNA are described. Methods for enhancing synchrotron light sources by insertion devices, such as wigglers and undulators, that increase the available photo flux and construction of new sources of synchrotron radiation are mentioned

Synchrotron radiation infrared microspectroscopy to assess the activity of vancomycin against endocarditis vegetation bacteria.

Science.gov (United States)

Batard, Eric; Jamme, Frédéric; Montassier, Emmanuel; Bertrand, Dominique; Caillon, Jocelyne; Potel, Gilles; Dumas, Paul

2011-06-01

Infrared microspectroscopy was used to show that vancomycin alters infrared spectra of endocarditis vegetation bacteria, and that vancomycin effects on bacterial biochemical contents are unevenly distributed between peripheral and central areas of bacterial masses. Infrared microspectroscopy is useful to study the activity of antibacterial agents against bacteria in tissues. Copyright © 2011 Elsevier B.V. All rights reserved.

Monochromatization of synchrotron radiation for studies in photoelectron spectroscopy

International Nuclear Information System (INIS)

Murty, P.S.

1981-01-01

Synchrotron radiation provides a tunable photon source which bridges the wavelength gap between HeI and AlKsub(α) radiation sources in photoelectron spectroscopy. The essential component for using synchrotron radiation is a monochromator. Some design features of the monochromators fabricated at Stanford, U.S.A., and Orsay, France, are described. The Stanford monochromator is a silicon crystal monochromator yielding 8 keV X-ray beam and is used with SPEAR storage ring facility, while the Orsay monochromator is a grazing incidence grating monochromator used for UPS studies. (M.G.B.)

Infrared Photometric Study of Wolf–Rayet Galaxies

Science.gov (United States)

Chen, P. S.; Yang, X. H.; Liu, J. Y.; Shan, H. G.

2018-01-01

We collected observational data on 781 Wolf–Rayet (WR) galaxies from the literature to photometrically study their infrared properties measured by the 2MASS, WISE, IRAS, AKARI, and Herschel missions. It is found that in the 1–5 μm range the radiations of WR galaxies are dominated by the free–free emissions from the stellar winds and the circumstellar dust from the late-type stars in the host galaxy. In the 5–22 μm range, the radiation of WR galaxies is dominated by the free–free emissions and the synchrotron radiation from the central active galactic nucleus (AGN; but not always present). In the 22–140 μm range, the radiations of WR galaxies are dominated by the free–free emissions and the star formation/starburst activities. In the 250–500 μm range, the radiation of WR galaxies is dominated by the free–free emissions. In addition, the comparison with the non-WR galaxies is made. It is shown that some star formation WR galaxies have redder near-infrared colors than non-WR star-forming galaxies probably due to the gas emission in the near-infrared. In the 2–5 μm region WR galaxies have redder colors due to the thermal emission from circumstellar dust of late-type stars and the enhanced gas emission. In the 5–22 μm region, both WR galaxies and non-WR galaxies have similar behavior, indicative of having similar free–free emission as the dominant radiation. In the 25–140 μm region, both types of galaxies also have similar behavior, indicative of having free–free emission from the stellar winds or the thermal radiation from the starburst/star formation as the dominant radiation.

RAPID INFRARED VARIABILITY OF THREE RADIO-LOUD NARROW-LINE SEYFERT 1 GALAXIES: A VIEW FROM THE WIDE-FIELD INFRARED SURVEY EXPLORER

Energy Technology Data Exchange (ETDEWEB)

Jiang Ning; Zhou Hongyan; Wang Tinggui; Dong Xiaobo; Jiang Peng [Key Laboratory for Research in Galaxies and Cosmology, University of Science and Technology of China, Chinese Academy of Science, Hefei, Anhui 230026 (China); Ho, Luis C. [The Observatories of the Carnegie Institution for Science, 813 Santa Barbara Street, Pasadena, CA 91101 (United States); Yuan Weimin [National Astronomical Observatories, Chinese Academy of Sciences, Beijing 100012 (China); Ji Tuo; Tian Qiguo, E-mail: jnac@mail.ustc.edu.cn [Polar Research Institute of China, 451 Jinqiao Road, Pudong, Shanghai 200136 (China)

2012-11-10

Using newly released data from the Wide-field Infrared Survey Explorer, we report the discovery of rapid infrared variability in three radio-loud narrow-line Seyfert 1 galaxies (NLS1s) selected from the 23 sources in the sample of Yuan et al. J0849+5108 and J0948+0022 clearly show intraday variability, while J1505+0326 has a longer measurable timescale within 180 days. Their variability amplitudes, corrected for measurement errors, are {approx}0.1-0.2 mag. The detection of intraday variability restricts the size of the infrared-emitting region to {approx}10{sup -3} pc, significantly smaller than the scale of the torus but consistent with the base of a jet. The three variable sources are exceptionally radio-loud, have the highest radio brightness temperature among the whole sample, and all show detected {gamma}-ray emission in Fermi/LAT observations. Their spectral energy distributions resemble those of low-energy-peaked blazars, with a synchrotron peak around infrared wavelengths. This result strongly confirms the view that at least some radio-loud NLS1s are blazars with a relativistic jet close to our line of sight. The beamed synchrotron emission from the jet contributes significantly to and probably dominates the spectra in the infrared and even optical bands.

Synchrotron radiation research

International Nuclear Information System (INIS)

Markus, N.

1995-01-01

In the many varied application fields of accelerators, synchrotron radiation ranks as one of the most valuable and widely useful tools. Synchrotron radiation is produced in multi-GeV electron synchrotrons and storage rings, and emerges tangentially in a narrow vertical fan. Synchrotron radiation has been used extensively for basic studies and, more recently, for applied research in the chemical, materials, biotechnology and pharmaceutical industries. Initially, the radiation was a byproduct of high energy physics laboratories but the high demand soon resulted in the construction of dedicated electron storage rings. The accelerator technology is now well developed and a large number of sources have been constructed, with energies ranging from about 1.5 to 8 GeV including the 6 GeV European Synchrotron Radiation Facility (ESRF) source at Grenoble, France. A modern third-generation synchrotron radiation source has an electron storage ring with a complex magnet lattice to produce ultra-low emittance beams, long straights for 'insertion devices', and 'undulator' or 'wiggler' magnets to generate radiation with particular properties. Large beam currents are necessary to give high radiation fluxes and long beam lifetimes require ultra high vacuum systems. Industrial synchrotron radiation research programmes use either Xray diffraction or spectroscopy to determine the structures of a wide range of materials. Biological and pharmaceutical applications study the functions of various proteins. With this knowledge, it is possible to design molecules to change protein behaviour for pharmaceuticals, or to configure more active proteins, such as enzymes, for industrial processes. Recent advances in molecular biology have resulted in a large increase in protein crystallography studies, with researchers using crystals which, although small and weakly diffracting, benefit from the high intensity. Examples with commercial significance include the study of

Using a non-invasive technique in nutrition: synchrotron radiation infrared microspectroscopy spectroscopic characterization of oil seeds treated with different processing conditions on molecular spectral factors influencing nutrient delivery.

Science.gov (United States)

Zhang, Xuewei; Yu, Peiqiang

2014-07-02

Non-invasive techniques are a key to study nutrition and structure interaction. Fourier transform infrared microspectroscopy coupled with a synchrotron radiation source (SR-IMS) is a rapid, non-invasive, and non-destructive bioanalytical technique. To understand internal structure changes in relation to nutrient availability in oil seed processing is vital to find optimal processing conditions. The objective of this study was to use a synchrotron-based bioanalytical technique SR-IMS as a non-invasive and non-destructive tool to study the effects of heat-processing methods and oil seed canola type on modeled protein structure based on spectral data within intact tissue that were randomly selected and quantify the relationship between the modeled protein structure and protein nutrient supply to ruminants. The results showed that the moisture heat-related processing significantly changed (pprocessing by dry heating. The moisture heating increased (p0.05) in the protein spectral profile between the raw and dry-heated canola tissue and between yellow- and brown-type canola tissue. The results indicated that different heat processing methods have different impacts on the protein inherent structure. The protein intrinsic structure in canola seed tissue was more sensitive and more response to the moisture heating in comparison to the dry heating. These changes are expected to be related to the nutritive value. However, the current study is based on limited samples, and more large-scale studies are needed to confirm our findings.

Synchrotrons: biomedical applications of the most versatile radiation source of all

International Nuclear Information System (INIS)

Lewis, R.

2003-01-01

Synchrotrons are the brightest and most versatile sources of radiation that have ever been devised. The spectrum extends from the infra-red to hard X-rays and the application range is just as wide. Applications range from radiotherapy to archaeology and from genomics to mineral identification. For a property of particle accelerators that was for many years seen as a problem, the transformation has been remarkable. There are now more than 50 synchrotron facilities worldwide and the number is still growing rapidly. Some 25 years after the first dedicated machines came into operation, Australia is about to enter the field with a national facility being built at Monash University in Melbourne. The largest impact of synchrotrons has been in the X-ray region of the spectrum where the performance gain over conventional sources is many orders of magnitude. In fact synchrotrons are the only significant improvement in X-ray production since the rotating anode was first marketed in 1929. The possibilities opened up by the availability of monochromatic, tightly collimated beams of enormous intensity has impacted on practically every area of science. Following a brief overview of synchrotron radiation production, the various prominent techniques that synchrotron radiation has made possible will be reviewed. Particular emphasis will be placed on the biomedical applications which include; 1. advanced imaging techniques exploiting X-ray phase contrast 2. radiotherapy using microbeams 3. structural biology 4. elemental, chemical and molecular structure mapping of live wet samples

Recent research in flaxseed (oil seed) on molecular structure and metabolic characteristics of protein, heat processing-induced effect and nutrition with advanced synchrotron-based molecular techniques.

Science.gov (United States)

Doiron, Kevin J; Yu, Peiqiang

2017-01-02

Advanced synchrotron radiation-based infrared microspectroscopy is able to reveal feed and food structure feature at cellular and molecular levels and simultaneously provides composition, structure, environment, and chemistry within intact tissue. However, to date, this advanced synchrotron-based technique is still seldom known to food and feed scientists. This article aims to provide detailed background for flaxseed (oil seed) protein research and then review recent progress and development in flaxseed research in ruminant nutrition in the areas of (1) dietary inclusion of flaxseed in rations; (2) heat processing effect; (3) assessing dietary protein; (4) synchrotron-based Fourier transform infrared microspectroscopy as a tool of nutritive evaluation within cellular and subcellular dimensions; (5) recent synchrotron applications in flaxseed research on a molecular basis. The information described in this paper gives better insight in flaxseed research progress and update.

Synchrotron light

International Nuclear Information System (INIS)

2001-01-01

'Synchrotron Light' is an interactive and detailed introduction to the physics and technology of the generation of coherent radiation from accelerators as well as to its widespread high-tech applications in science, medicine and engineering. The topics covered are the interaction of light and matter, the technology of synchrotron light sources, spectroscopy, imaging, scattering and diffraction of X-rays, and applications to materials science, biology, biochemistry, medicine, chemistry, food and pharmaceutical technology. All synchrotron light facilities are introduced with their home-page addresses. 'Synchrotron Light' provides an instructive and comprehensive multimedia learning tool for students, experienced practitioners and novices wishing to apply synchrotron radiation in their future work. Its multiple-entry points permit an easy exploration of the CD-Rom according to the users knowledge and interest. 2-D and 3-D animations and virtual reconstruction with computer-generated images guide visitors into the scientific and technical world of a synchrotron and into the applications of synchrotron radiation. This bilingual (English and French) CD-Rom can be used for self-teaching and in courses at various levels in physics, chemistry, engineering, and biology. (author)

Synchrotron-radiation research

International Nuclear Information System (INIS)

Cunningham, J.E.

1982-01-01

The use of radiation from synchrotron sources has started a renaissance in materials, physics, chemistry, and biology. Synchrotron radiation has advantages over conventional x rays in that its source brightness is a thousand times greater throughout a continuous energy spectrum, and resonances are produced with specific electron energy levels. Two major synchrotron radiation sources are operated by DOE: the Stanford Synchrotron Radiation Laboratory at SLAC, and the National Synchrotron Light Source at Brookhaven

Analysis of peripheral thermal damage after laser irradiation of dentin using polarized light microscopy and synchrotron radiation infrared spectromicroscopy

Science.gov (United States)

Dela Rosa, Alfredo; Sarma, Anupama V.; Le, Charles Q.; Jones, Robert S.; Fried, Daniel

2004-05-01

It is necessary to minimize peripheral thermal damage during laser irradiation, since thermal damage to collagen and mineral compromises the bond strength to restorative materials in dentin and inhibits healing and osteointegration in bone. The overall objective of this study was to test the hypothesis that lasers resonant to the specific absorption of water, collagen, and hydroxyapatite with pulse durations less than the thermal relaxation times at each respective laser wavelength will efficiently remove dentin with minimal peripheral thermal damage. Precise incisions were produced in 3 x 3 mm2 blocks of human dentin using CO2 (9.6 μm), Er:YSGG (2.79 μm), and Nd:YAG (355 nm) lasers with and without a computer controlled water spray. Polarization-sensitive optical coherence tomography was used to obtain optical cross-sections of each incision to determine the rate and efficiency of ablation. The peripheral thermal damage zone around each incision was analyzed using polarized light microscopy (PLM) and Synchrotron-Radiation Fourier Transform Infrared Spectro-microscopy (SR-FTIR). Thermally induced chemical changes to both mineral and the collagen matrix was observed with SR-FTIR with a 10-μm spatial resolution and those changes were correlated with optical changes observed with PLM. Minimal (alveolar bone.

Spatio-temporal dynamics of relativistic electron bunches during the micro bunching instability: study of the Synchrotron Soleil and UVSOR storage rings

International Nuclear Information System (INIS)

Roussel, Eleonore

2014-01-01

Relativistic electron bunches circulating in storage rings are used to produce intense radiation from far-infrared to X-rays. However, above a density threshold value, the interaction between the electron bunch and its own radiation can lead to a spatio-temporal instability called micro bunching instability. This instability is characterized by a strong emission of coherent THz radiation (typically 105 times stronger than the classical synchrotron radiation) which is a signature of the presence of microstructures (at mm scale) in the electron bunch. This instability is known to be a fundamental limitation of the operation of synchrotron light sources at high beam current. In this thesis, we have focused on this instability from a nonlinear dynamics point of view by combining experimental studies carried out at the Synchrotron Soleil and UVSOR storage rings with numerical studies mainly based on the Vlasov-Fokker-Planck equation. In a first step, due to the very indirect nature of the experimental observations, we have sought to deduce information on the microstructure wavenumber either by looking at the temporal evolution of the THz signal emitted during the instability or by studying the response of the electron bunch to a laser perturbation. In a second step, we have achieved direct, real time observations of the microstructures dynamics through two new, very different, detection techniques: a thin-film superconductor-based detector at UVSOR, and a spectrally-encoded electro-optic detection technique at Soleil. These new available experimental observations have allowed severe comparisons with the theoretical models. (author)

Toward optimal spatial and spectral quality in widefield infrared spectromicroscopy of IR labelled single cells.

Science.gov (United States)

Mattson, Eric C; Unger, Miriam; Clède, Sylvain; Lambert, François; Policar, Clotilde; Imtiaz, Asher; D'Souza, Roshan; Hirschmugl, Carol J

2013-10-07

Advancements in widefield infrared spectromicroscopy have recently been demonstrated following the commissioning of IRENI (InfraRed ENvironmental Imaging), a Fourier Transform infrared (FTIR) chemical imaging beamline at the Synchrotron Radiation Center. The present study demonstrates the effects of magnification, spatial oversampling, spectral pre-processing and deconvolution, focusing on the intracellular detection and distribution of an exogenous metal tris-carbonyl derivative 1 in a single MDA-MB-231 breast cancer cell. We demonstrate here that spatial oversampling for synchrotron-based infrared imaging is critical to obtain accurate diffraction-limited images at all wavelengths simultaneously. Resolution criteria and results from raw and deconvoluted images for two Schwarzschild objectives (36×, NA 0.5 and 74×, NA 0.65) are compared to each other and to prior reports for raster-scanned, confocal microscopes. The resolution of the imaging data can be improved by deconvolving the instrumental broadening that is determined with the measured PSFs, which is implemented with GPU programming architecture for fast hyperspectral processing. High definition, rapidly acquired, FTIR chemical images of respective spectral signatures of the cell 1 and shows that 1 is localized next to the phosphate- and Amide-rich regions, in agreement with previous infrared and luminescence studies. The infrared image contrast, localization and definition are improved after applying proven spectral pre-processing (principal component analysis based noise reduction and RMie scattering correction algorithms) to individual pixel spectra in the hyperspectral cube.

3D spectral imaging with synchrotron Fourier transform infrared spectro-microtomography

Science.gov (United States)

Michael C. Martin; Charlotte Dabat-Blondeau; Miriam Unger; Julia Sedlmair; Dilworth Y. Parkinson; Hans A. Bechtel; Barbara Illman; Jonathan M. Castro; Marco Keiluweit; David Buschke; Brenda Ogle; Michael J. Nasse; Carol J. Hirschmugl

2013-01-01

We report Fourier transform infrared spectro-microtomography, a nondestructive three-dimensional imaging approach that reveals the distribution of distinctive chemical compositions throughout an intact biological or materials sample. The method combines mid-infrared absorption contrast with computed tomographic data acquisition and reconstruction to enhance chemical...

Synchrotron radiation

CERN Document Server

Kunz, C

1974-01-01

The production of synchrotron radiation as a by-product of circular high-energy electron (positron) accelerators or storage rings is briefly discussed. A listing of existing or planned synchrotron radiation laboratories is included. The following properties are discussed: spectrum, collimation, polarization, and intensity; a short comparison with other sources (lasers and X-ray tubes) is also given. The remainder of the paper describes the experimental installations at the Deutsches Elektronen-Synchrotron (DESY) and DORIS storage rings, presents a few typical examples out of the fields of atomic, molecular, and solid-state spectroscopy, and finishes with an outlook on the use of synchrotron radiation in molecular biology. (21 refs).

Molecular photoemission studies using synchrotron radiation

International Nuclear Information System (INIS)

Truesdale, C.M.

1983-04-01

The angular distributions of photoelectrons and Auger electrons were measured by electron spectroscopy using synchrotron radiation. The experimental results are compared with theoretical calculations to interpret the electronic behavior of photoionization for molecular systems

Detection and spectral measurements of coherent synchrotron radiation at FLASH

International Nuclear Information System (INIS)

Behrens, Christopher

2010-02-01

The operation of high-gain free-electron laser (FEL) underlies tremendous demands on high quality electron beams with high peak currents. At the Free-Electron-Laser in Hamburg (FLASH), two magnetic bunch compressors are used to compress the electron bunches longitudinally. In the bunch compressor magnets, these short electron bunches generate coherent synchrotron radiation (CSR). This CSR contains information on the longitudinal bunch profile, which is relevant for driving an FEL. In order to investigate coherent synchrotron radiation at the second bunch compressor BC3 at FLASH, a new setup behind the last dipole was installed. For the detection of coherent synchrotron radiation, which is emitted in the infrared regime, pyroelectric detectors were used. These pyroelectric detectors have been calibrated at the free-electron laser FELIX in the wavelength range from 5 μm to 110 μm. For characterisation of the emitted radiation, a transverse scanning device was used to measure the transverse intensity distribution. Various transmission filters were used to obtain additional information about the spectral content. In order to get spectral information with high resolution over a wide wavelength range, a rotating mirror spectrometer using reflective blazed gratings was installed. Using this spectrometer, the first spectral measurements of coherent synchrotron radiation at FLASH in a wavelength range from 10 μm to 160 μm were done. (orig.)

Detection and spectral measurements of coherent synchrotron radiation at FLASH

Energy Technology Data Exchange (ETDEWEB)

Behrens, Christopher

2010-02-15

The operation of high-gain free-electron laser (FEL) underlies tremendous demands on high quality electron beams with high peak currents. At the Free-Electron-Laser in Hamburg (FLASH), two magnetic bunch compressors are used to compress the electron bunches longitudinally. In the bunch compressor magnets, these short electron bunches generate coherent synchrotron radiation (CSR). This CSR contains information on the longitudinal bunch profile, which is relevant for driving an FEL. In order to investigate coherent synchrotron radiation at the second bunch compressor BC3 at FLASH, a new setup behind the last dipole was installed. For the detection of coherent synchrotron radiation, which is emitted in the infrared regime, pyroelectric detectors were used. These pyroelectric detectors have been calibrated at the free-electron laser FELIX in the wavelength range from 5 {mu}m to 110 {mu}m. For characterisation of the emitted radiation, a transverse scanning device was used to measure the transverse intensity distribution. Various transmission filters were used to obtain additional information about the spectral content. In order to get spectral information with high resolution over a wide wavelength range, a rotating mirror spectrometer using reflective blazed gratings was installed. Using this spectrometer, the first spectral measurements of coherent synchrotron radiation at FLASH in a wavelength range from 10 {mu}m to 160 {mu}m were done. (orig.)

Studies of Lear antiproton deceleration: radiofrequency quadripole or synchrotron

International Nuclear Information System (INIS)

Iazzourene, F.

1987-06-01

The aim of this work is to study a radiofrequency quadrupole (RFQ) and a synchrotron as decelerating systems for antiprotons extracted from the Low Energy Antiproton Ring (LEAR) at CERN. Antiprotons at energies lower than those available from LEAR are need by some experiments, eg. the measurement of the mass difference between protons and antiprotons with 10 -9 accuracy, using a Smith and Princeton spectrometer, and the measurement of gravitation on the antiprotons, using a trap. Depending on the LEAR performances, one can conclude that the RFQ is suitable for the experiment on the gravitation, and the synchrotron, owing to its electron cooling system, is a better solution for the experiment on the mass difference measurement, because of the very small acceptance of the spectrometer [fr

Photoemission studies using laboratory and synchrotron sources

International Nuclear Information System (INIS)

Phase, D.M.

2012-01-01

Synchrotron radiation sources, providing intense, polarized and stable beams of ultra violet soft and hard X-ray photons, are having great impact on physics, chemistry, biology materials science and other areas research. In particular synchrotron radiation has revolutionized photoelectron spectroscopy by enhancing its capabilities for investigating the electronic properties of solids. The first Indian synchrotron storage ring, Indus- 1 is in operation at RRCAT, Indore. The UGC-DAE CSR with the help of university scientist had designed and developed an angle integrated photoelectron spectroscopy (PES) beamline on this 450 MeV storage ring. A storage ring of this kind is most suitable for investigation in the energy range from few electron volts to around five hundred electron volts. In this lecture we will describe the details of PES beamline and its experimental station. Till date the different university users carried out photoemission measurements on variety of samples. Some of the spectra recorded by users will be presented in order to show the capability of this beamline. In the later part we will report a review of our recent research work carried out on dilute magnetic thin films using this beamline. (author)

Synchrotron Environmental Science-I Workshop Report

International Nuclear Information System (INIS)

1999-01-01

Attendees of the Synchrotrons Environmental Science 1 (SES-1) workshop represented a broad spectrum of environmental science research areas and expertise in all of the current synchrotrons techniques (X-ray scattering and diffraction, X-ray absorption spectroscopy, and two- and three-dimensional X-ray imaging). These individuals came together to discuss current measurement obstacles in environmental research and, more specifically, ways to overcome such obstacles by applying synchrotrons radiation techniques. Significant obstacles in measurement affect virtually all of the research issues described. Attendees identified synchrotrons approaches of potential value in their research. A number of the environmental research studies discussed are currently being addressed with some success by synchrotron-based approaches. Nevertheless, improvements in low-Z measurement capabilities are needed to facilitate the use of synchrotrons radiation methodologies in environmental research

Synchrotron Environmental Science-I Workshop Report.

Energy Technology Data Exchange (ETDEWEB)

NONE

1999-07-08

Attendees of the Synchrotrons Environmental Science 1 (SES-1) workshop represented a broad spectrum of environmental science research areas and expertise in all of the current synchrotrons techniques (X-ray scattering and diffraction, X-ray absorption spectroscopy, and two- and three-dimensional X-ray imaging). These individuals came together to discuss current measurement obstacles in environmental research and, more specifically, ways to overcome such obstacles by applying synchrotrons radiation techniques. Significant obstacles in measurement affect virtually all of the research issues described. Attendees identified synchrotrons approaches of potential value in their research. A number of the environmental research studies discussed are currently being addressed with some success by synchrotron-based approaches. Nevertheless, improvements in low-Z measurement capabilities are needed to facilitate the use of synchrotrons radiation methodologies in environmental research.

Synchrotron radiation in Australia

International Nuclear Information System (INIS)

Garrett, R.F.

2002-01-01

Full text: Synchrotron radiation research in Australia is entering a new era with the commencement of the Australian synchrotron project, which will construct a 3 GeV third generation synchrotron facility at Monash University in Victoria. To date Australian scientists have used overseas facilities, primarily those managed by the Australian Synchrotron Research Program in Japan and the USA. A fast developing and maturing Australian synchrotron user program has developed around these overseas facilities. The field of synchrotron radiation and its importance to a wide range of research will be introduced and Australia's current involvement and facilities will be described. The current status and technical specifications of the Australian synchrotron will be presented. Copyright (2002) Australian X-ray Analytical Association Inc

SYNCHROTRON HEATING BY A FAST RADIO BURST IN A SELF-ABSORBED SYNCHROTRON NEBULA AND ITS OBSERVATIONAL SIGNATURE

International Nuclear Information System (INIS)

Yang, Yuan-Pei; Dai, Zi-Gao; Zhang, Bing

2016-01-01

Fast radio bursts (FRBs) are mysterious transient sources. If extragalactic, as suggested by their relative large dispersion measures, their brightness temperatures must be extremely high. Some FRB models (e.g., young pulsar model, magnetar giant flare model, or supra-massive neutron star collapse model) suggest that they may be associated with a synchrotron nebula. Here we study a synchrotron-heating process by an FRB in a self-absorbed synchrotron nebula. If the FRB frequency is below the synchrotron self-absorption frequency of the nebula, electrons in the nebula would absorb FRB photons, leading to a harder electron spectrum and enhanced self-absorbed synchrotron emission. In the meantime, the FRB flux is absorbed by the nebula electrons. We calculate the spectra of FRB-heated synchrotron nebulae, and show that the nebula spectra would show a significant hump in several decades near the self-absorption frequency. Identifying such a spectral feature would reveal an embedded FRB in a synchrotron nebula

SYNCHROTRON HEATING BY A FAST RADIO BURST IN A SELF-ABSORBED SYNCHROTRON NEBULA AND ITS OBSERVATIONAL SIGNATURE

Energy Technology Data Exchange (ETDEWEB)

Yang, Yuan-Pei; Dai, Zi-Gao [School of Astronomy and Space Science, Nanjing University, Nanjing 210093 (China); Zhang, Bing, E-mail: zhang@physics.unlv.edu [Department of Physics and Astronomy, University of Nevada, Las Vegas, NV 89154 (United States)

2016-03-01

Fast radio bursts (FRBs) are mysterious transient sources. If extragalactic, as suggested by their relative large dispersion measures, their brightness temperatures must be extremely high. Some FRB models (e.g., young pulsar model, magnetar giant flare model, or supra-massive neutron star collapse model) suggest that they may be associated with a synchrotron nebula. Here we study a synchrotron-heating process by an FRB in a self-absorbed synchrotron nebula. If the FRB frequency is below the synchrotron self-absorption frequency of the nebula, electrons in the nebula would absorb FRB photons, leading to a harder electron spectrum and enhanced self-absorbed synchrotron emission. In the meantime, the FRB flux is absorbed by the nebula electrons. We calculate the spectra of FRB-heated synchrotron nebulae, and show that the nebula spectra would show a significant hump in several decades near the self-absorption frequency. Identifying such a spectral feature would reveal an embedded FRB in a synchrotron nebula.

Fast synchrotron X-ray tomography study of the rod packing structures

Energy Technology Data Exchange (ETDEWEB)

Zhang Xiaodan; Xia Chengjie; Sun Haohua; Wang Yujie [Department of Physics, Shanghai Jiao Tong University, 800 Dong Chuan Road, Shanghai 200240 (China)

2013-06-18

We present a fast synchrotron X-ray tomography study of the packing structures of rods under tapping. Utilizing the high flux of the X-rays generated from the third-generation synchrotron source, we can complete a tomography scan within several seconds, after which the three-dimensional (3D) packing structure can be obtained for the subsequent structural analysis. Due to the high-energy nature of the X-ray beam, special image processing steps including image phase-retrieval has been implemented. Overall, this study suggests the possibility of acquiring statistically significant static packing structures within a reasonable time scale using high-intensity X-ray sources.

Experimental studies on coherent synchrotron radiation at an emittance exchange beam line

Science.gov (United States)

Thangaraj, J. C. T.; Thurman-Keup, R.; Ruan, J.; Johnson, A. S.; Lumpkin, A. H.; Santucci, J.

2012-11-01

One of the goals of the Fermilab A0 photoinjector is to investigate experimentally the transverse to longitudinal emittance exchange (EEX) principle. Coherent synchrotron radiation in the emittance exchange line could limit the performance of the emittance exchanger at short bunch lengths. In this paper, we present experimental and simulation studies of the coherent synchrotron radiation (CSR) in the emittance exchange line at the A0 photoinjector. We report on time-resolved CSR studies using a skew-quadrupole technique. We also demonstrate the advantages of running the EEX with an energy-chirped beam.

JHF synchrotrons

Energy Technology Data Exchange (ETDEWEB)

NONE

1999-03-01

The Japan Hadron Facility (JHF) consists of two synchrotrons and an injector linac. First, we will present a brief review of the specifications and lattice of the synchrotrons; one is 3 GeV booster and the other is 50 GeV main ring. Secondly, some detailed results of design study will be discussed, together with the present status of the R and D programs in progress. Among them, an estimate of beam loss is one of critical issues in beam dynamics. The development of a high gradient RF cavity is also crucial for a high intensity machine. (author)

Synchrotron white beam topographic studies of gallium arsenide crystals

International Nuclear Information System (INIS)

Wierzchowski, W.; Wieteska, K.; Graeff, W.

1997-01-01

A series of samples cut out from different types of gallium arsenide crystals with low dislocation density were studied by means of white beam synchrotron topography. The investigation was performed with transmission and black-reflection projection methods and transmission section method. Some of topographs in transmission geometry provided a very high sensitivity suitable for revealing small precipitates. The transmission section images significantly differed depending on the wavelength and absorption. In some cases a distinct Pendelloesung fringes and fine details of dislocation and precipitates images were observed. It was possible to reproduce the character of these images by means of numerical simulation based on integration of Takagi-Taupin equations. Due to more convenient choice of radiation, synchrotron back-reflection projection topography provided much better visibility of dislocations than analogous realized with conventional X-ray sources. (author)

Multiple scattering in synchrotron studies of disordered materials

International Nuclear Information System (INIS)

Poulsen, H.F.; Neuefeind, J.

1995-01-01

A formalism for the multiple scattering and self-absorption in synchrotron studies of disordered materials is presented. The formalism goes beyond conventionally used approximations and treat the cross sections, the beam characteristics, the state of polarization, and the electronic correction terms in full. Using hard X-rays it is shown how the simulated distributions can be directly compared to experimental data. ((orig.))

Intense, broadband, pulsed I-R source at the National Synchrotron Light Source

International Nuclear Information System (INIS)

Williams, G.P.

1984-01-01

We describe a broadband (1 μm to 1 mm) synchrotron radiation infrared source, pulsed each 20 to 180 nseconds and delivering about 10 15 photons/sec/1% bandpass into f10 optics. The source size is diffraction limited. This source is thus 100 to 1000 times brighter than a 2000 0 K black body, very stable and capable of being used for calibration

Synchrotron radiation sources

Energy Technology Data Exchange (ETDEWEB)

van Steenbergen, A.

1979-01-01

As a result of the exponential growth of the utilization of synchrotron radiation for research in the domain of the material sciences, atomic and molecular physics, biology and technology, a major construction activity has been generated towards new dedicated electron storage rings, designed optimally for synchrotron radiation applications, also, expansion programs are underway at the existing facilities, such as DORIS, SPEAR, and VEPP. In this report the basic properties of synchrotron radiation will be discussed, a short overview will be given of the existing and new facilities, some aspects of the optimization of a structure for a synchrotron radiation source will be discussed and the addition of wigglers and undulators for spectrum enhancement will be described. Finally, some parameters of an optimized synchrotron radiation source will be given.

Experimental studies on coherent synchrotron radiation at an emittance exchange beam line

Directory of Open Access Journals (Sweden)

J. C. T. Thangaraj

2012-11-01

Full Text Available One of the goals of the Fermilab A0 photoinjector is to investigate experimentally the transverse to longitudinal emittance exchange (EEX principle. Coherent synchrotron radiation in the emittance exchange line could limit the performance of the emittance exchanger at short bunch lengths. In this paper, we present experimental and simulation studies of the coherent synchrotron radiation (CSR in the emittance exchange line at the A0 photoinjector. We report on time-resolved CSR studies using a skew-quadrupole technique. We also demonstrate the advantages of running the EEX with an energy-chirped beam.

Far Infrared High Resolution Synchrotron FTIR Spectroscopy of the Low Frequency Bending Modes of Dmso

Science.gov (United States)

Cuisset, Arnaud; Smirnova, Irina; Bocquet, Robin; Hindle, Francis; Mouret, Gael; Sadovskii, Dmitrii A.; Pirali, Olivier; Roy, Pascale

2010-06-01

In addition to its importance for industrial and environmental studies, the monitoring of DiMethylSulfOxyde (DMSO, (CH_3)_2SO) concentrations is of considerable interest for civil protection. The existing high resolution gas phase spectroscopic data of DMSO only concerned the pure rotational transitions in the ground state. In the Far-IR domain, the low-frequency rovibrational transitions have never previously resolved. The high brightness of the AILES beamline of the synchrotron SOLEIL and the instrumental sensitivity provided by the multipass cell allowed to measure for the first time these transitions. 1581 A-type and C-type transitions in the ν11 band have been assigned and 25 molecular constants of Watson's s-form hamiltonian developed to degree 8 have been fitted within the experimental accuracy. The use of then synchrotron radiation has opened many possibilities for new spectroscopic studies. Together with several other recent studies, our successful measurement and analysis of DMSO convincingly demonstrates the potential of the AILES beamline for high resolution FIR spectroscopy. Thus our present work is just at the beginning of unraveling the rovibrational structure of low frequency bending and torsional vibrational states of DMSO and yielding important comprehensive structural and spectroscopic information on this molecule. L. Margules, R. A. Motienko, E. A. Alekseev, J. Demaison, J. Molec. Spectrosc., 260(23),2009 V. Typke, M. Dakkouri, J. Molec. Struct., 599(177),2001 A. Cuisset, L. Nanobashvili, I. Smirnova, R. Bocquet, F. Hindle, G. Mouret, O. Pirali, P. Roy, D. Sadovskii, Chem. Phys. Lett., accepted for publication

Characterization of the new NSLS infrared microspectroscopy beamline U10B

Energy Technology Data Exchange (ETDEWEB)

Carr, G.L.

1999-07-19

The first of several new infrared beamlines, built on a modified bending magnet port of the NSLS VUV ring, is now operational for mid-infrared microspectroscopy. The port simultaneously delivers 40 mrad by 40 mrad to two separate beamlines and spectrometer endstations designated U10A and U10B. The latter is equipped with a scanning infrared microspectrometer. The combination of this instrument and high brightness synchrotron radiation makes diffraction-limited microspectroscopy practical. This paper describes the beamline's performance and presents quantitative information on the diffraction-limited resolution.

HSC5: synchrotron radiation and neutrons for cultural heritage studies

Energy Technology Data Exchange (ETDEWEB)

Michel, Anne [Institut Neel - CNRS, 38 - Grenoble (France); Artioli, G. [Padova Univ. (Italy); Bleuet, P.; Cotte, M.; Tafforeau, P.; Susini, J. [European Synchrotron Radiation Facility, 38 - Grenoble (France); Dumas, P.; Somogyl, A. [SOLEIL Synchrotron, 91 - Gif sur Yvette (France); Cotte, M. [Centre de Recherche et de Restauration des Musees de France, UMR171, 75 - Paris (France)]|[European Synchrotron Radiation Facility, 38 - Grenoble (France); Kockelmann, W. [Science and Technology Facilities Council, Rutherford Appleton Lab. (United Kingdom); Kolar, J. [Ljubljana Univ., Morana RTD, Slovenia, Faculty of Chemistry and Chemical Technology (Slovenia); Areon, I. [Nova Gorica Univ. (Slovenia); Meden, A.; Strlie, M. [Ljubljana Univ., Faculty of Chemistry and Chemical Technology (Slovenia); Pantos, M. [Daresbury Laboratory, Warrington (United Kingdom); Vendrell, M. [Barcelona Univ., dept. of Crystallography and Mineralogy (Spain); Wess, T. [Cardiff Univ., School of Optometry and Institute of Vision (Ireland); Gunneweg, J. [Hebrew Univ., Jerusalem (Israel)

2007-07-01

Synchrotron and neutron sources offer recent and additional insight into the records of our cultural past. Over the last years, there has been an increasing demand for access to synchrotron radiation- and neutron-based techniques, and their applications in the fields of archaeological science and cultural heritage. The purpose of this Hercules Specialized Course is to give the participants an introduction to the basic principles of synchrotron radiation and neutron techniques (imaging, microscopy, diffraction, absorption and fluorescence, IR spectroscopy). The school provides cross-disciplinary examples illustrating the abilities of these techniques in a representative range of scientific cases concerning painting, archaeological artefacts, inks, pigments, fossils and the Dead Sea scrolls. This document gathers only the resumes of the lectures.

HSC5: synchrotron radiation and neutrons for cultural heritage studies

International Nuclear Information System (INIS)

Michel, Anne; Artioli, G.; Bleuet, P.; Cotte, M.; Tafforeau, P.; Susini, J.; Dumas, P.; Somogyl, A.; Cotte, M.; Kockelmann, W.; Kolar, J.; Areon, I.; Meden, A.; Strlie, M.; Pantos, M.; Vendrell, M.; Wess, T.; Gunneweg, J.

2007-01-01

Synchrotron and neutron sources offer recent and additional insight into the records of our cultural past. Over the last years, there has been an increasing demand for access to synchrotron radiation- and neutron-based techniques, and their applications in the fields of archaeological science and cultural heritage. The purpose of this Hercules Specialized Course is to give the participants an introduction to the basic principles of synchrotron radiation and neutron techniques (imaging, microscopy, diffraction, absorption and fluorescence, IR spectroscopy). The school provides cross-disciplinary examples illustrating the abilities of these techniques in a representative range of scientific cases concerning painting, archaeological artefacts, inks, pigments, fossils and the Dead Sea scrolls. This document gathers only the resumes of the lectures

Microfabrication of high quality polytetrafluoroethylene films by synchrotron radiation

International Nuclear Information System (INIS)

Yoshida, A.; Matsumoto, E.; Yamada, H.; Okada, H.; Wakahara, A.

2003-01-01

We deposited polytetrafluoroethylene (PTFE) thin films both from the PTFE target by using synchrotron radiation (SR) beam and from PTFE emulsion by spin-coat process. The X-ray diffraction analyses showed a sharp peak due to (1 0 0) PTFE crystalline part, and only C-F 2 bonding was found in Fourier transform infrared spectrophotometer spectra. From electron spectroscopy for chemical analysis measurements, no impurities were found. The fabricated PTFE films were easily etched by SR beam on the limited area of the surface on a microscale through a suitably patterned mask

Atomic physics research with synchrotron radiation

International Nuclear Information System (INIS)

Crasemann, B.; Wuilleumier, F.

1985-01-01

This chapter discusses applications of synchrotron light in atomic and molecular physics. Use of the radiation from storage rings has expanded and lent access to new areas of absorption and photoemission spectroscopy and scattering experiments. Techniques applied in connection with synchrotron radiation are discussed including absorption spectroscopy, photoelectron spectroscopy, fluorescence spectroscopy and X-ray scattering. Problem areas that are being studied by the techniques mentioned above are discussed. Synchrotron radiation has provided the means for measuring the threshold-excitation and interference effects that signal the breakdown of the two-step model of atomic excitation/deexcitation. Synchrotron radiation provides more means of excited-state photoionization measurements

Modeling Protein Structures in Feed and Seed Tissues Using Novel Synchrotron-Based Analytical Technique

International Nuclear Information System (INIS)

Yu, P.

2008-01-01

Traditional 'wet' chemical analyses usually looks for a specific known component (such as protein) through homogenization and separation of the components of interest from the complex tissue matrix. Traditional 'wet' chemical analyses rely heavily on the use of harsh chemicals and derivatization, therefore altering the native feed protein structures and possibly generating artifacts. The objective of this study was to introduce a novel and non-destructive method to estimate protein structures in feed and seeds within intact tissues using advanced synchrotron-based infrared microspectroscopy (SFTIRM). The experiments were performed at the National Synchrotron Light Source in Brookhaven National Laboratory (US Dept. of Energy, NY). The results show that with synchrotron-based SFTIRM, we are able to localize relatively 'pure' protein without destructions of the feed and seed tissues and qualify protein internal structures in terms of the proportions and ratios of a-helix, β-sheet, random coil and β-turns on a relative basis using multi-peak modeling procedures. These protein structure profile (a-helix, β-sheet, etc.) may influence protein quality and availability in animals. Several examples of feed and seeds were provided. The implications of this study are that we can use this new method to compare internal protein structures between feeds and between seed verities. We can also use this method to detect heat-induced the structural changes of protein in feeds.

Surface science station of the infrared beamline at SPring-8

International Nuclear Information System (INIS)

Sakurai, M.; Moriwaki, T.; Kimura, H.; Nishida, S.; Nanba, T.

2001-01-01

An experimental station for surface science has been constructed at the infrared beamline (BL43IR) of SPring-8, Japan. The station utilizes synchrotron radiation in the energy range of 100-20000 cm -1 to perform infrared reflection absorption spectroscopy (IRAS) of surfaces. It consists of an experimental section, a preparation chamber, gas handling equipment and a pair of focusing optics. In situ observation of vibrational spectra is possible using both IRAS and high-resolution electron energy loss spectroscopy

Science research with high-brilliance synchrotron light source

International Nuclear Information System (INIS)

Sanyal, Milan K.

2013-01-01

Synchrotron-science has changed dramatically since the development of high brilliance electron accelerator-based light sources in 1990s. In the last twenty years or so, several such facilities have come up, particularly in developed countries, as material characterizations in relevant atmosphere and protein crystallography with tiny-crystals have strong implications in industrial competitiveness. Moreover several new techniques have been developed recently over the entire spectral range of emitted light, from infra-red to high energy X-rays, which have altered our basic understanding of various materials like biomaterials, nanomaterials, soft-matter and semiconductor quantum structures. In addition, rapid development of various X-ray imaging techniques for nondestructive evaluation of compositional/structural homogeneity of engineering materials with nanometer resolution will have tremendous impact in manufacturing industries. As India becomes a developed country, it must have access to such an advanced synchrotron facility in the country that enables knowledge generation in the ever-expanding fields of design-characterization-production of advanced materials and modern medicines. Development of such state-of-the art facility will also enable us to carry out frontier-basic-research in our own country and help us to retain and bring back Indian talents to India. Here we shall discuss briefly the characteristics of a high brilliance synchrotron source and outline the nature of basic and applied science research that can be done with such a state-of-the-art facility. (author)

Observation of runaway electrons by infrared camera in J-TEXT

Energy Technology Data Exchange (ETDEWEB)

Tong, R. H.; Chen, Z. Y., E-mail: zychen@hust.edu.cn; Zhang, M.; Huang, D. W.; Yan, W.; Zhuang, G. [State Key Laboratory of Advanced Electromagnetic Engineering and Technology, School of Electrical and Electronic Engineering, Huazhong University of Science and Technology, Wuhan 430074 (China)

2016-11-15

When the energy of confined runaway electrons approaches several tens of MeV, the runaway electrons can emit synchrotron radiation in the range of infrared wavelength. An infrared camera working in the wavelength of 3-5 μm has been developed to study the runaway electrons in the Joint Texas Experimental Tokamak (J-TEXT). The camera is located in the equatorial plane looking tangentially into the direction of electron approach. The runaway electron beam inside the plasma has been observed at the flattop phase. With a fast acquisition of the camera, the behavior of runaway electron beam has been observed directly during the runaway current plateau following the massive gas injection triggered disruptions.

Molecular toxicity of triclosan and carbamazepine to green algae Chlorococcum sp.: A single cell view using synchrotron-based Fourier transform infrared spectromicroscopy.

Science.gov (United States)

Xin, Xiaying; Huang, Guohe; Liu, Xia; An, Chunjiang; Yao, Yao; Weger, Harold; Zhang, Peng; Chen, Xiujuan

2017-07-01

Although pharmaceuticals and personal care products have been used and introduced into the environment in large quantities, little information on potential ecological risks is currently available considering their effects on living organisms. We verified the feasibility of using synchrotron-based Fourier Transform Infrared (SR-FTIR) spectromicroscopy to explore in vivo toxic effects on single living Chlorococcum sp. cells. The study provided important information to achieve a better understanding of the toxic mechanism of triclosan and carbamazepine on living algae Chlorococcum sp.. Triclosan and carbamazepine had distinctive toxic effects on unicellular living algae. Most strikingly, triclosan had more dramatic toxic effects on biochemical components than carbamazepine. Triclosan can affect algae primarily by inhibiting fatty acid synthesis and causing protein aggregation. The toxicity response was irreversible at higher concentration (100.000 μM), but attenuated at lower concentration (0.391 μM) as time extended. Carbamazepine can produce hydrophobic interactions to affect the phospholipid bilayer and work on specific proteins to disfunction the cell membrane. Carbamazepine-exposed cells developed a resistance while extending exposure time. This is the first demonstration from an ecological standpoint that SR-FTIR can provide an innovative approach to reveal the toxicity of emerging pollutants in aquatic environments. Copyright © 2017 Elsevier Ltd. All rights reserved.

Basis of medical accelerator. Synchrotron

International Nuclear Information System (INIS)

Kawachi, Kiyomitsu

2014-01-01

On the synchrotron as a medical accelerator, this paper introduces the basic principle, basic techniques and the like. The accelerator, when synchrotron is adopted as an ion beam radiotherapy system, is the composite accelerator composed of ion sources, injector, and synchrotron. This paper introduces the overall structure of synchrotron, and conceptually explains the basic behavior of high-frequency waves and magnetic field of synchrotron, as well as the deflection electromagnet of medical synchrotron and the operation pattern of high-frequency acceleration system. The types of synchrotron can be classified to the function combination type and function separation type, and this paper introduces the features of each type and various types of synchrotrons. It also explains beam dynamics important for ensuring the stability of beams, with a focus on the coordinate system, vertical movement, and lateral movement. In addition, it explains the incidence and outgoing of beams that are important for properly operating the accelerator, with a focus on their techniques. (A.O.)

Microprobing the Molecular Spatial Distribution and Structural Architecture of Feed-type Sorghum Seed Tissue (Sorghum Bicolor L.) using the Synchrotron Radiation Infrared Microspectroscopy Technique

International Nuclear Information System (INIS)

Yu, P.

2011-01-01

Sorghum seed (Sorghum bicolor L.) has unique degradation and fermentation behaviours compared with other cereal grains such as wheat, barley and corn. This may be related to its cell and cell-wall architecture. The advanced synchrotron radiation infrared microspectroscopy (SR-IMS) technique enables the study of cell or living cell biochemistry within cellular dimensions. The objective of this study was to use the SR-IMS imaging technique to microprobe molecular spatial distribution and cell architecture of the sorghum seed tissue comprehensively. High-density mapping was carried out using SR-IMS on beamline U2B at the National Synchrotron Light Source (Brookhaven National Laboratory, NY, USA). Molecular images were systematically recorded from the outside to the inside of the seed tissue under various chemical functional groups and their ratios [peaks at ∼1725 (carbonyl C=O ester), 1650 (amide I), 1657 (protein secondary structure α-helix), 1628 (protein secondary structure β-sheet), 1550 (amide II), 1515 (aromatic compounds of lignin), 1428, 1371, 1245 (cellulosic compounds in plant seed tissue), 1025 (non-structural CHO, starch granules), 1246 (cellulosic material), 1160 (CHO), 1150 (CHO), 1080 (CHO), 930 (CHO), 860 (CHO), 3350 (OH and NH stretching), 2960 (CH 3 anti-symmetric), 2929 (CH 2 anti-symmetric), 2877 (CH 3 symmetric) and 2848 cm -1 (CH 2 asymmetric)]. The relative protein secondary structure α-helix to β-sheet ratio image, protein amide I to starch granule ratio image, and anti-symmetric CH 3 to CH 2 ratio image were also investigated within the intact sorghum seed tissue. The results showed unique cell architecture, and the molecular spatial distribution and intensity in the sorghum seed tissue (which were analyzed through microprobe molecular imaging) were generated using SR-IMS. This imaging technique and methodology has high potential and could be used for scientists to develop specific cereal grain varieties with targeted food and feed

Spin dynamics in electron synchrotrons

International Nuclear Information System (INIS)

Schmidt, Jan Felix

2017-01-01

Providing spin polarized particle beams with circular accelerators requires the consideration of depolarizing resonances which may significantly reduce the desired degree of polarization at specific beam energies. The corresponding spin dynamical effects are typically analyzed with numerical methods. In case of electron beams the influence of the emission of synchrotron radiation has to be taken into account. On short timescales, as in synchrotrons with a fast energy ramp or in damping rings, spin dynamics are investigated with spin tracking algorithms. This thesis presents the spin tracking code Polematrix as a versatile tool to study the impact of synchrotron radiation on spin dynamics. Spin tracking simulations have been performed based on the well established particle tracking code Elegant. The numerical studies demonstrate effects which are responsible for beam depolarization: Synchrotron side bands of depolarizing resonances and decoherence of spin precession. Polematrix can be utilized for any electron accelerator with minimal effort as it imports lattice files from the tracking programs MAD-X or Elegant. Polematrix has been published as open source software. Currently, the Electron Stretcher Accelerator ELSA at Bonn University is the only electron synchrotron worldwide providing a polarized beam. Integer and intrinsic depolarizing resonances are compensated with dedicated countermeasures during the fast energy ramp. Polarization measurements from ELSA demonstrate the particular spin dynamics of electrons and confirm the results of the spin tracking code Polematrix.

Evaluating scintillator performance in time-resolved hard X-ray studies at synchrotron light sources

International Nuclear Information System (INIS)

Rutherford, Michael E.; Chapman, David J.; White, Thomas G.; Drakopoulos, Michael; Rack, Alexander; Eakins, Daniel E.

2016-01-01

Scintillator performance in time-resolved, hard, indirect detection X-ray studies on the sub-microsecond timescale at synchrotron light sources is reviewed, modelled and examined experimentally. LYSO:Ce is found to be the only commercially available crystal suitable for these experiments. The short pulse duration, small effective source size and high flux of synchrotron radiation is ideally suited for probing a wide range of transient deformation processes in materials under extreme conditions. In this paper, the challenges of high-resolution time-resolved indirect X-ray detection are reviewed in the context of dynamic synchrotron experiments. In particular, the discussion is targeted at two-dimensional integrating detector methods, such as those focused on dynamic radiography and diffraction experiments. The response of a scintillator to periodic synchrotron X-ray excitation is modelled and validated against experimental data collected at the Diamond Light Source (DLS) and European Synchrotron Radiation Facility (ESRF). An upper bound on the dynamic range accessible in a time-resolved experiment for a given bunch separation is calculated for a range of scintillators. New bunch structures are suggested for DLS and ESRF using the highest-performing commercially available crystal LYSO:Ce, allowing time-resolved experiments with an interframe time of 189 ns and a maximum dynamic range of 98 (6.6 bits)

Evaluating scintillator performance in time-resolved hard X-ray studies at synchrotron light sources

Energy Technology Data Exchange (ETDEWEB)

Rutherford, Michael E.; Chapman, David J.; White, Thomas G. [Imperial College London, London (United Kingdom); Drakopoulos, Michael [Diamond Light Source, I12 Joint Engineering, Environmental, Processing (JEEP) Beamline, Didcot, Oxfordshire (United Kingdom); Rack, Alexander [European Synchrotron Radiation Facility, Grenoble (France); Eakins, Daniel E., E-mail: d.eakins@imperial.ac.uk [Imperial College London, London (United Kingdom)

2016-03-24

Scintillator performance in time-resolved, hard, indirect detection X-ray studies on the sub-microsecond timescale at synchrotron light sources is reviewed, modelled and examined experimentally. LYSO:Ce is found to be the only commercially available crystal suitable for these experiments. The short pulse duration, small effective source size and high flux of synchrotron radiation is ideally suited for probing a wide range of transient deformation processes in materials under extreme conditions. In this paper, the challenges of high-resolution time-resolved indirect X-ray detection are reviewed in the context of dynamic synchrotron experiments. In particular, the discussion is targeted at two-dimensional integrating detector methods, such as those focused on dynamic radiography and diffraction experiments. The response of a scintillator to periodic synchrotron X-ray excitation is modelled and validated against experimental data collected at the Diamond Light Source (DLS) and European Synchrotron Radiation Facility (ESRF). An upper bound on the dynamic range accessible in a time-resolved experiment for a given bunch separation is calculated for a range of scintillators. New bunch structures are suggested for DLS and ESRF using the highest-performing commercially available crystal LYSO:Ce, allowing time-resolved experiments with an interframe time of 189 ns and a maximum dynamic range of 98 (6.6 bits)

Broadband Correlations Provide Evidence for Synchrotron Self-Compton X-rays from the Black Hole Binary GX 339-4

International Nuclear Information System (INIS)

Coriat, M.; Corbel, S.; Buxton, M. M.; Baylin, C. D.

2009-01-01

GX 339-4 has been one of the key sources for unravelling the accretion ejection coupling in accreting stellar mass black holes. After a long period of quiescence between 1999 and 2002, GX 339-4 underwent a series of 4 outbursts that have been intensively observed by many ground based observatories (radio/infrared/optical) and satellites (X-rays). Here, we present some specific results of these broad band observational campaigns, focusing on the optical-infrared/X-ray flux correlations over the four outbursts. Thanks to our extensive data-set, we found a strong OIR/X-ray correlation over four decades with the presence of a break in the correlation index. These results seem to favour a synchrotron self-Compton origin for the X-ray emission in GX 339-4 during the hard state and could also provide an indirect detection of the break frequency in the synchrotron spectrum of the compact jets.

Synchrotron radiation

International Nuclear Information System (INIS)

Nave, C.; Quinn, P.; Blake, R.J.

1988-01-01

The paper on Synchrotron Radiation contains the appendix to the Daresbury Annual Report 1987/88. The appendix is mainly devoted to the scientific progress reports on the work at the Synchrotron Radiation Source in 1987/8. The parameters of the Experimental Stations and the index to the Scientific Reports are also included in the appendix. (U.K.)

Synchrotron radiation facilities

CERN Multimedia

1972-01-01

Particularly in the past few years, interest in using the synchrotron radiation emanating from high energy, circular electron machines has grown considerably. In our February issue we included an article on the synchrotron radiation facility at Frascati. This month we are spreading the net wider — saying something about the properties of the radiation, listing the centres where synchrotron radiation facilities exist, adding a brief description of three of them and mentioning areas of physics in which the facilities are used.

Infrared Spectroscopy Beamline Based on a Tabletop Storage Ring

OpenAIRE

Haque, Md. Monirul; Moon, Ahsa; Yamada, Hironari

2012-01-01

An optical beamline dedicated to the infrared (IR) spectroscopy has been constructed at MIRRORCLE, a tabletop storage ring. The beamline has been designed for the use of infrared synchrotron radiation (IRSR) emitted from a bending magnet of 156 mm bending radius with the acceptance angle of 355(H) × 138(V) mrad to obtain high flux. The IR emission is forced by an exactly circular optics, named photon storage ring (PhSR), placed around the electron orbit and is collected by a “magic mirror” as...

Study of spear as a dedicated source of synchrotron radiation

International Nuclear Information System (INIS)

Cerino, J.; Golde, A.; Hastings, J.; Lindau, I.; Salsburg, B.; Winick, H.; Lee, M.; Morton, P.; Garren, A.

1977-11-01

A study was made of the potential of SPEAR as a dedicated source of synchrotron radiation, based on the expectation that SPEAR will become increasingly available for this purpose as PEP, the 18-GeV colliding-beam storage ring now under construction by LBL and SLAC, becomes operational. A synchrotron radiation research program has been underway since May, 1974. Two beam ports capable of serving 9 simultaneous users are now operational. In single-beam multi-bunch operation high currents are possible (225 mA has been achieved and > approximately 300 mA is expected) and the electron beam emittance can be made smaller, resulting in higher source point brightness. Descriptions are given of SPEAR capabilities and of plans to expand the research capability by adding beam runs and by inserting wiggler magnets in SPEAR straight sections

Photoelectron and photodissociation studies of free atoms and molecules, using synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Medhurst, L.J.

1991-11-01

High resolution synchrotron radiation and Zero-Kinetic-Energy Photoelectron spectroscopy were used to study two-electron transitions in atomic systems at their ionization thresholds. Using this same technique the core-ionized mainline and satellite states of N{sub 2} and CO were studied with vibrational resolution. Vibrationally resolved synchrotron radiation was used to study the dissociation of N{sub 2}, C{sub 2}H{sub 4}, and CH{sub 3}Cl near the N 1s and C 1s thresholds. The photoelectron satellites of the argon 3s, krypton 4s and xenon 4d subshells were studied with zero kinetic energy photoelectron spectroscopy at their ionization thresholds. In all of these cases, satellites with lower binding energies are enhanced at their thresholds while those closer to the double ionization threshold are suppressed relative to their intensities at high incident light energies.

Photoelectron and photodissociation studies of free atoms and molecules, using synchrotron radiation

International Nuclear Information System (INIS)

Medhurst, L.J.

1991-11-01

High resolution synchrotron radiation and Zero-Kinetic-Energy Photoelectron spectroscopy were used to study two-electron transitions in atomic systems at their ionization thresholds. Using this same technique the core-ionized mainline and satellite states of N 2 and CO were studied with vibrational resolution. Vibrationally resolved synchrotron radiation was used to study the dissociation of N 2 , C 2 H 4 , and CH 3 Cl near the N 1s and C 1s thresholds. The photoelectron satellites of the argon 3s, krypton 4s and xenon 4d subshells were studied with zero kinetic energy photoelectron spectroscopy at their ionization thresholds. In all of these cases, satellites with lower binding energies are enhanced at their thresholds while those closer to the double ionization threshold are suppressed relative to their intensities at high incident light energies

Infrared response of YBa2Cu3O7-δ films to pulsed, broadband synchrotron radiation

International Nuclear Information System (INIS)

Carr, G.L.; Quijada, M.; Tanner, D.B.; Etemad, S.; DeRosa, F.; Venkatesan, T.; Dutta, B.; Hemmick, D.; Xi, X.

1990-01-01

We report studies of a thin high T c film operating as a fast bolometric detector of infrared radiation. The film has a response of infrared radiation. The film has a response of several mV when exposed to a 1 W, 1 ns duration broadband infrared pulse. The decay after the pulse was about 4 ns. The temperature dependence of the response accurately tracked dR/dT. A thermal model, in which the film's temperature varies relative to the substrate, provides a good description of the response. We find no evidence for other (non-bolometric) response mechanisms for temperatures near or well below T c . 13 refs., 4 figs

Space-charge calculations in synchrotrons

Energy Technology Data Exchange (ETDEWEB)

Machida, S.

1993-05-01

One obvious bottleneck of achieving high luminosity in hadron colliders, such as the Superconducting Super Collider (SSC), is the beam emittance growth, due to space-charge effects in low energy injector synchrotrons. Although space-charge effects have been recognized since the alternating-gradient synchrotron was invented, and the Laslett tune shift usually calculated to quantify these effects, our understanding of the effects is limited, especially when the Laslett tune shift becomes a large fraction of the integer. Using the Simpsons tracking code, which we developed to study emittance preservation issues in proton synchrotrons, we investigated space-charge effects in the SSC Low Energy Booster (LEB). We observed detailed dependence on parameters such as beam intensity, initial emittance, injection energy, lattice function, and longitudinal motion. A summary of those findings, as well as the tracking technique we developed for the study, are presented.

Relativistic Turbulence with Strong Synchrotron and Synchrotron-Self-Compton Cooling

Science.gov (United States)

Uzdensky, D. A.

2018-03-01

Many relativistic plasma environments in high-energy astrophysics, including pulsar wind nebulae, hot accretion flows onto black holes, relativistic jets in active galactic nuclei and gamma-ray bursts, and giant radio lobes, are naturally turbulent. The plasma in these environments is often so hot that synchrotron and inverse-Compton (IC) radiative cooling becomes important. In this paper we investigate the general thermodynamic and radiative properties (and hence the observational appearance) of an optically thin relativistically hot plasma stirred by driven magnetohydrodynamic (MHD) turbulence and cooled by radiation. We find that if the system reaches a statistical equilibrium where turbulent heating is balanced by radiative cooling, the effective electron temperature tends to attain a universal value θ = kT_e/m_e c^2 ˜ 1/√{τ_T}, where τT = neσTL ≪ 1 is the system's Thomson optical depth, essentially independent of the strength of turbulent driving and hence of the magnetic field. This is because both MHD turbulent dissipation and synchrotron cooling are proportional to the magnetic energy density. We also find that synchrotron self-Compton (SSC) cooling and perhaps a few higher-order IC components are automatically comparable to synchrotron in this regime. The overall broadband radiation spectrum then consists of several distinct components (synchrotron, SSC, etc.), well separated in photon energy (by a factor ˜ τ_T^{-1}) and roughly equal in power. The number of IC peaks is checked by Klein-Nishina effects and depends logarithmically on τT and the magnetic field. We also examine the limitations due to synchrotron self-absorption, explore applications to Crab PWN and blazar jets, and discuss links to radiative magnetic reconnection.

X-ray and synchrotron methods in studies of cultural heritage sites

Energy Technology Data Exchange (ETDEWEB)

Koval’chuk, M. V.; Yatsishina, E. B.; Blagov, A. E.; Tereshchenko, E. Yu., E-mail: elenatereschenko@yandex.ru; Prosekov, P. A.; Dyakova, Yu. A. [National Research Centre “Kurchatov Institute” (Russian Federation)

2016-09-15

X-ray and synchrotron methods that are most widely used in studies of cultural heritage objects (including archaeological sites)—X-ray diffraction analysis, X-ray spectroscopy, and visualization techniques— have been considered. The reported examples show high efficiency and informativeness of natural science studies when solving most diverse problems of archaeology, history, the study of art, museology, etc.

X-ray and synchrotron methods in studies of cultural heritage sites

International Nuclear Information System (INIS)

Koval’chuk, M. V.; Yatsishina, E. B.; Blagov, A. E.; Tereshchenko, E. Yu.; Prosekov, P. A.; Dyakova, Yu. A.

2016-01-01

X-ray and synchrotron methods that are most widely used in studies of cultural heritage objects (including archaeological sites)—X-ray diffraction analysis, X-ray spectroscopy, and visualization techniques— have been considered. The reported examples show high efficiency and informativeness of natural science studies when solving most diverse problems of archaeology, history, the study of art, museology, etc.

Synchrotron radiation from spherically accreting black holes

International Nuclear Information System (INIS)

Ipser, J.R.; Price, R.H.

1982-01-01

Spherical accretion onto a Schwartzchild black hole, of gas with frozen-in magnetic field, is studied numerically and analytically for a range of hole masses and accretion rates in which synchrotron emission is the dominant radiative mechanism. At small radii the equipartition of magnetic, kinetic, and gravitational energy is assumed to apply, and the gas is heated by dissipation of infalling magnetic energy, turbulent energy, etc. The models can be classified into three types: (a) synchrotron cooling negligible, (b) synchrotron cooling important but synchrotron self-absorption negligible, (c) synchrotron cooling and self-absorption important. In the first case gas temperatures become very high near the horizon but luminosity efficiencies (luminosity/mass-energy accretion rate) are low. In cases (b) and (c) the gas flow near the horizon is essentially isothermal and luminosity efficiencies are fairly high. The analysis and results for the isothermal cases (b) and (c) are valid only for moderate dissipative heating and synchrotron self-absorption. If self-absorption is very strong or if dissipated energy is comparable to infall energy, Comptonization effects, not included in the analysis, become important

Study of Laser Wakefield Accelerators as injectors for Synchrotron light sources

CERN Document Server

Hillenbrand, Steffen; Müller, Anke-Susanne; Jansen, Oliver; Judin, Vitali; Pukhov, Alexander

2014-01-01

Laser WakeField Accelerators (LWFA) feature short bunch lengths and high peak currents, combined with a small facility footprint. This makes them very interesting as injectors for Synchrotron light sources. Using the ANKA Synchrotron as an example, we investigate the possibility to inject a LWFA bunch into an electron storage ring. Particular emphasis is put on the longitudinal evolution of the bunch.

Photoelectron and photodissociation studies of free atoms and molecules, using synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Medhurst, Laura Jane [Univ. of California, Berkeley, CA (United States)

1991-11-01

High resolution synchrotron radiation and Zero-Kinetic-Energy Photoelectron spectroscopy were used to study two-electron transitions in atomic systems at their ionization thresholds. Using this same technique the core-ionized mainline and satellite states of N₂ and CO were studied with vibrational resolution. Vibrationally resolved synchrotron radiation was used to study the dissociation of N₂, C₂H₄, and CH₃Cl near the N 1s and C 1s thresholds. The photoelectron satellites of the argon 3s, krypton 4s and xenon 4d subshells were studied with zero kinetic energy photoelectron spectroscopy at their ionization thresholds. In all of these cases, satellites with lower binding energies are enhanced at their thresholds while those closer to the double ionization threshold are suppressed relative to their intensities at high incident light energies.

Synchrotron radiation from protons

International Nuclear Information System (INIS)

Dutt, S.K.

1992-12-01

Synchrotron radiation from protons, though described by the same equations as the radiation from electrons, exhibits a number of interesting features on account of the parameters reached in praxis. In this presentation, we shall point out some of the features relating to (i) normal synchrotron radiation from dipoles in proton machines such as the High Energy Booster and the Superconducting Super Collider; (ii) synchrotron radiation from short dipoles, and its application to light monitors for proton machines, and (iii) synchrotron radiation from undulators in the limit when, the deflection parameter is much smaller than unity. The material for this presentation is taken largely from the work of Hofmann, Coisson, Bossart, and their collaborators, and from a paper by Kim. We shall emphasize the qualitative aspects of synchrotron radiation in the cases mentioned above, making, when possible, simple arguments for estimating the spectral and angular properties of the radiation. Detailed analyses can be found in the literature

Future Synchrotron Radiation Sources

CERN Document Server

Winick, Herman

2003-01-01

Sources of synchrotron radiation (also called synchrotron light) and their associated research facilities have experienced a spectacular growth in number, performance, and breadth of application in the past two to three decades. In 1978 there were eleven electron storage rings used as light sources. Three of these were small rings, all below 500 mega-electron volts (MeV), dedicated to this purpose; the others, with energy up to 5 giga-electron volts (GeV), were used parasitically during the operation of the ring for high energy physics research. In addition, at that time synchrotron radiation from nine cyclic electron synchrotrons, with energy up to 5 GeV, was also used parasitically. At present no cyclic synchrotrons are used, while about 50 electron storage rings are in operation around the world as fully dedicated light sources for basic and applied research in a wide variety of fields. Among these fields are structural molecular biology, molecular environmental science, materials, analytic chemistry, micr...

Coronary angiography using synchrotron radiation

International Nuclear Information System (INIS)

Akatsuka, Takao; Hiranaka, Yukio; Takeda, Tohru; Hyodo, Kazuyuki.

1990-01-01

Invasive coronary angiography is the imaging technique of choice for diagnosis of ischemic heart disease. Recently, the application of synchrotron radiation in coronary angiography has been investigated in the world, with the aim of developing the noninvasive technique for visualizing the heart. In this article, backgrounds and present situation of coronary angiography using synchrotron radiation are reviewed. Firstly, visual imaging techniques of the cardiovascular system are discussed in terms of angiography and digital subtraction angiography (DSA). Conventional temporal, energy, and hybrid subtraction modes used in DSA are referred to. Secondly, the application of synchrotron radiation is presented, focusing on the property of synchrotron radiation and K-edge subtraction angiography. Two kinds of synchrotron radiation beam methods are outlined. Interpretation of image data and various subtraction procedures remain unestablished. There is much to be done before coronary angiography using synchrotron radiation comes into a clinical practice. (N.K.)

Structural studies of the lipid membranes at the Siberia-2 synchrotron radiation source

International Nuclear Information System (INIS)

Kiselev, M. A.; Ermakova, E. V.; Ryabova, N. Yu.; Nayda, O. V.; Zabelin, A. V.; Pogorely, D. K.; Korneev, V. N.; Balagurov, A. M.

2010-01-01

Lipid membranes are a subject of contemporary interdisciplinary studies at the junction of biology, biophysics, pharmacology, and bionanotechnology. The results of the structural studies of several types of lipid membranes by the lamellar and lateral diffraction of X-ray synchrotron radiation are presented. The experiments were performed at the Mediana and DICSI stations of the Siberia-2 synchrotron radiation source at the Russian Research Center Kurchatov Institute. The data obtained are compared with the results of studying lipid membranes at the small-angle scattering beamlines D22 and D24 at LURE (France) and at the A2 beamline at DESY (Germany). The parameters of the DICSI station are shown to meet the basic requirements for the structural study of lipid systems, which are of fundamental and applied interest.

Uses of synchrotron radiation

International Nuclear Information System (INIS)

Gordon, B.M.

1982-01-01

X-ray fluorescence has long been used as a technique for elemental analysis. X-ray fluorescence techniques have a number of features that make them attractive for application to biomedical samples. In the past few years synchrotron radiation x-ray sources have been developed and, because of their properties, their use can improve the sensitivity for trace element analysis by two to three orders of magnitude. Also, synchrotron radiation will make possible an x-ray microprobe with resolution in the micrometer range. The National Synchrotron Light Source (NSLS), a dedicated synchrotron radiation source recently built at Brookhaven National Laboratory, will have a facility for trace element analysis by x-ray fluorescence and will be available to all interested users

Synchrotron radiation

International Nuclear Information System (INIS)

Norman, D.; Walker, R.P.; Durham, P.J.; Ridley, P.A.

1986-01-01

The paper on synchrotron radiation is the appendix to the Daresbury (United Kingdom) annual report, 1985/86. The bulk of the volume is made up of the progress reports for the work carried out during the year under review using the Synchrotron Radiation Source (SRS) at Daresbury. The Appendix also contains: the scientific programmes at the the SRS, progress on beamlines, instrumentation and computing developments, and activities connected with accelerator development. (U.K.)

Synchrotron radiation XRF microprobe study of human bone tumor slice

International Nuclear Information System (INIS)

Huang Yuying; Zhao Limin; Wang Zhouguang; Shao Hanru; Li Guangcheng; Wu Yingrong; He Wei; Lu Jianxin; He Rongguo

1999-01-01

The experimental apparatus of X-ray fluorescence (XRF) microprobe analysis at Beijing Synchrotron Radiation Facility (BSRF) is described. Using the bovine liver as the standard reference, the minimum detection limit (MDL) of trace element was measured to determine the capability of biological sample analysis by synchrotron radiation XRF microprobe. The relative change of the content of the major or trace element in the normal and tumor part of human bone tissue slice was investigated. The experimental result relation to the clinical medicine was also discussed. (author)

Macromolecular crystallography using synchrotron radiation

International Nuclear Information System (INIS)

Bartunik, H.D.; Phillips, J.C.; Fourme, R.

1982-01-01

The use of synchrotron X-ray sources in macromolecular crystallography is described. The properties of synchrotron radiation relevant to macromolecular crystallography are examined. The applications discussed include anomalous dispersion techniques, the acquisition of normal and high resolution data, and kinetic studies of structural changes in macromolecules; protein data are presented illustrating these applications. The apparatus used is described including information on the electronic detectors, the monitoring of the incident beam and crystal cooling. (U.K.)

Initial studies of synchrotron radiation phase-contrast imaging in the field of medicine

International Nuclear Information System (INIS)

Chen Shaoliang; Zhang Xi; Peng Yifeng; Li Beilei; Cheng Aiping; Zhu Peiping; Yuan Xiqing; Huang Wanxia

2010-01-01

Recently,research on using X-ray phase information in medicine has been growing remarkably fast. Phase-contrast imaging with synchrotron radiation can reveal inner soft tissues such as tendons, cartilage, ligaments, adipose tissue, vessels and nerves without a contrast agent. We have visualized the liver, bile duct, lung, kidney, stomach and intestine, heart, blood vessel, bone and arthrosis, and tumor tissues using 'in-line' phase contrast imaging and diffraction-enhanced imaging. It is seen that the synchrotron radiation graphs show much higher resolution. This method is especially suitable for studying soft tissue structure and blood vessels. (authors)

Fast photoconductor CdTe detectors for synchrotron x-ray studies

International Nuclear Information System (INIS)

Yoo, Sung Shik; Faurie, J.P.; Huang Qiang; Rodricks, B.

1993-09-01

The Advanced Photon Source will be that brightest source of synchrotron x-rays when it becomes operational in 1996. During normal operation, the ring will be filled with 20 bunches of positrons with an interbunch spacing of 177 ns and a bunch width of 119 ps. To perform experiments with x-rays generated by positrons on these time scales one needs extremely high speed detectors. To achieve the necessary high speed, we are developing MBE-grown CdTe-base photoconductive position sensitive array detectors. The arrays fabricated have 64 pixels with a gap of 100 μm between pixels. The high speed response of the devices was tested using a short pulse laser. X-ray static measurements were performed using an x-ray tube and synchrotron radiation to study the device's response to flux and wavelength changes. This paper presents the response of the devices to some of these tests and discusses different physics aspects to be considered when designing high speed detectors

Synchrotron radiation applications in medical research

International Nuclear Information System (INIS)

Thomlinson, W.

1995-01-01

The medical projects employing synchrotron radiation as discussed in this paper are, for the most part, still in their infancies and no one can predict the direction in which they will develop. Both the basic research and applied medical programs are sure to be advanced at the new facilities coming on line, especially the ESRF and Spring- 8. However, success is not guaranteed. There is a lot of competition from advances in conventional imaging with the development of digital angiography, computed tomography, functional magnetic resonance imaging and ultrasound. The synchrotron programs will have to provide significant advantages over these modalities in order to be accepted by the medical profession. Advances in image processing and potentially the development of compact sources will be required in order to move the synchrotron developed imaging technologies into the clinical world. In any event, it can be expected that the images produced by the synchrotron technologies will establish ''gold standards'' to be targeted by conventional modalities. A lot more work needs to be done in order to bring synchrotron radiation therapy and surgery to the level of human studies and, subsequently, to clinical applications

Synchrotron power supply of TARN II

International Nuclear Information System (INIS)

Watanabe, Shin-ichi.

1991-07-01

The construction and performance of synchrotron power supply of TARN II are described. The 1.1 GeV synchrotron-cooler TARN II has been constructed at Institute for Nuclear Study, University of Tokyo. Constructed power supply for the dipole magnets is 600 V, 2500 A operated in the mode of trapezoid wave form with the repetition cycle of 0.1 Hz. The stability of magnetic field within 10 -3 and tracking error of 10 -4 have been attained with the aid of computer control system. First trial of synchrotron acceleration of He 2+ beam has been done up to 600 MeV in April, 1991. (author)

Far-infrared high resolution synchrotron FTIR spectroscopy of the ν11 bending vibrational fundamental transition of dimethylsulfoxyde

Science.gov (United States)

Cuisset, Arnaud; Nanobashvili, Lia; Smirnova, Irina; Bocquet, Robin; Hindle, Francis; Mouret, Gaël; Pirali, Olivier; Roy, Pascale; Sadovskií, Dmitrií A.

2010-05-01

We report the first successful high resolution gas phase study of the 'parallel' band of DMSO at 380 cm -1 associated with the ν11 bending vibrational mode. The spectrum was recorded with a resolution of 0.0015 cm -1 using the AILES beamline of the SOLEIL synchrotron source, the IFS 125 FTIR spectrometer and a multipass cell providing an optical path of 150 m. The rotational constants and centrifugal corrections obtained from the analysis of the resolved rotational transitions reproduce the spectrum to the experimental accuracy.

First detection of lamella-gyroid-cylinder phase transition of neat polyethylene-poly(ethylene oxide) diblock copolymers on the basis of synchrotron WAXD/SAXS and infrared/Raman spectral measurements

International Nuclear Information System (INIS)

Weiyu, Cao; Tashiro, Kohji; Hanesaka, Makoto; Takeda, Shinichi; Masunaga, Hiroyasu; Sasaki, Sono; Takata, Masaki

2009-01-01

The phase transition behaviour of polyethylene-b-poly(ethylene oxide) (PE-b-PEO) diblock copolymer with relatively short chain lengths has been studied on the basis of temperature dependent infrared and Raman spectral measurements and synchrotron WAXD/SAXS simultaneous measurements, from which the concrete structural changes were deduced successfully from the various levels of molecular chain conformation, chain packing mode and higher-order structure. The higher-order structure has been found to transform between lamella, perforated lamella, gyroid, cylinder and sphere structures. The inner structural changes occurring in the polyethylene and poly(ethylene oxide) parts have been related with these morphological changes. The morphological transition from lamella to gyroid occurs with keeping the crystalline state of polyethylene parts. This apparently curious transition can be interpreted reasonably by assuming the thermally-activated chain motion in the crystal lattice, which may play an important role as a trigger to induce the morphological change from lamella to gyroid. This idea was supported by the measurement of half-width of Raman anti-symmetric CH 2 stretching band sensitive to the thermal mobility of alkyl chains.

A Multiwavelength Study of Cygnus X-1: The First Mid-Infrared Spectroscopic Detection of Compact Jets

Science.gov (United States)

Rahoui, Farid; Lee, Julia C.; Heinz, Sebastian; Hines, Dean C.; Pottschmidt, Katja; Wilms, Joern

2011-01-01

We report on a Spitzer/IRS (mid-infrared), RXTE /PCA+HEXTE (X-ray), and Ryle (radio) simultaneous multi-wavelength study of the micro quasar Cygnus X-I, which aimed at an investigation of the origin of its mid-infrared emission. Compact jets were present in two out of three observations, and we show that they strongly contribute to the mid-infrared continuum. During the first observation, we detect the spectral break - where the transition from the optically thick to the optically thin regime takes place - at about 2.9 x 10(exp 13) Hz. We then show that the jet's optically thin synchrotron emission accounts for the Cygnus X-1's emission beyond 400 keY, although it cannot alone explain its 3-200 keV continuum. A compact jet was also present during the second observation, but we do not detect the break, since it has likely shifted to higher frequencies. In contrast, the compact jet was absent during the last observation, and we show that the 5-30 micron mid-infrared continuum of Cygnus X-I stems from the blue supergiant companion star HD 226868. Indeed, the emission can then be understood as the combination of the photospheric Raleigh-Jeans tail and the bremsstrahlung from the expanding stellar wind. Moreover, the stellar wind is found to be clumpy, with a filling factor f(sub infinity) approx.= 0.09-0.10. Its bremsstrahlung emission is likely anti-correlated to the soft X-ray emission, suggesting an anticorrelation between the mass-loss and mass-accretion rates. Nevertheless, we do not detect any mid-infrared spectroscopic evidence of interaction between the jets and the Cygnus X-1's environment and/or companion star's stellar wind.

Synchrotrons are also devoted to society

International Nuclear Information System (INIS)

Gacoin, M.P.; Cornuejols, D.; Cotte, M.; Deblay, P.; Mitchell, E.P.; McCarthy, J.; Fraissard, F.

2013-01-01

The ESRF and the SOLEIL synchrotrons are not only scientific instruments but also active players in the cultural and economic fields. This document gathers 6 short articles. The 2 first present the actions of SOLEIL and ESRS scientific teams towards the spreading of scientific knowledge in the public. The third article is dedicated to the uses of synchrotron radiation to the study of cultural objects to learn more about their fabrication, present state or the remedial actions that could be used to renovate them. The fourth and fifth articles present the contributions of ESRF and SOLEIL to the industrial world, in fact these contributions are not limited to the research field but also appear for quality assurance or the control of aging processes. Partnerships have been signed between both synchrotrons and enterprises to develop industrial products based on instrumentation or on the use of synchrotron radiation. The last article describes the procedure to have access to both facilities. (A.C.)

Optoelectronic Picosecond Detection of Synchrotron X-rays

Energy Technology Data Exchange (ETDEWEB)

Durbin, Stephen M. [Purdue Univ., West Lafayette, IN (United States)

2017-08-04

The goal of this research program was to develop a detector that would measure x-ray time profiles with picosecond resolution. This was specifically aimed for use at x-ray synchrotrons, where x-ray pulse profiles have Gaussian time spreads of 50-100 ps (FWHM), so the successful development of such a detector with picosecond resolution would permit x-ray synchrotron studies to break through the pulse width barrier. That is, synchrotron time-resolved studies are currently limited to pump-probe studies that cannot reveal dynamics faster than ~50 ps, whereas the proposed detector would push this into the physically important 1 ps domain. The results of this research effort, described in detail below, are twofold: 1) the original plan to rely on converting electronic signals from a semiconductor sensor into an optical signal proved to be insufficient for generating signals with the necessary time resolution and sensitivity to be widely applicable; and 2) an all-optical method was discovered whereby the x-rays are directly absorbed in an optoelectronic material, lithium tantalate, which can then be probed by laser pulses with the desired picosecond sensitivity for detection of synchrotron x-rays. This research program has also produced new fundamental understanding of the interaction of x-rays and optical lasers in materials that has now created a viable path for true picosecond detection of synchrotron x-rays.

Synchrotron radiation

International Nuclear Information System (INIS)

Poole, M.W.; Lea, K.R.

1982-01-01

A report is given on the work involving the Synchrotron Radiation Division of the Daresbury Laboratory during the period January 1981 - March 1982. Development of the source, beamlines and experimental stations is described. Progress reports from individual investigators are presented which reveal the general diversity and interdisciplinary nature of the research which benefits from access to synchrotron radiation and the associated facilities. Information is given on the organisation of the Division and publications written by the staff are listed. (U.K.)

National Synchrotron Light Source

International Nuclear Information System (INIS)

van Steenbergen, A.

1979-01-01

The National Synchrotron Light Source comprises two high intensity electron storage rings for the generation of intense fluxes of synchrotron radiation in the vuv wavelength domain (700 MeV e - ring) and in the x-ray wavelength domain (2.5 GeV e - ring). A description is presented of the basic facility and the characteristics of the synchrotron radiation sources. The present plans for specific beam lines will be enumerated and the planned use of beam wigglers and undulators will be discussed

Synchrotron radiation : characteristics and application in structural studies and phase transformations of materials

International Nuclear Information System (INIS)

Craievich, A.F.

1984-01-01

The main characteristics of the synchrotron radiation for studying atomic structure and phase transformations in materials are presented. Some specific applications in alloys, glass and solids are described. (E.G.) [pt

Synchrotron radiation and free electron laser activities in Novosibirsk

International Nuclear Information System (INIS)

Korchuganov, V.N.; Kulipanov, G.N.; Mezentsev, N.A.; Oreshkov, A.D.; Panchenko, V.E.; Pindyurin, V.F.; Skrinskij, A.N.; Sheromov, M.A.; Vinokurov, N.A.; Zolotarev, K.V.

1994-01-01

The results of studies realized in the Siberian synchrotron radiation centre within the frameworks of wide program of synchrotron radiation and free electron laser research are summarized. The technical information on the VEPP-2M, VEPP-3 and VEPP-4M storage rings used as synchrotron radiation sources is given. 10 refs.; 8 figs.; 12 tabs

In-Situ Synchrotron X-ray Study of the Phase and Texture Evolution of Ceria and Superconductor Films Deposited by Chemical Solution Method

DEFF Research Database (Denmark)

Yue, Zhao; Grivel, Jean-Claude; He, Dong

2012-01-01

In situ synchrotron x-ray diffraction is used to study the phase and texture formation of ceria based films and superconductor films deposited by the chemical solution method on technical substrates. Combined analysis using in situ synchrotron x-ray diffraction, thermogravimetry/differential ther......In situ synchrotron x-ray diffraction is used to study the phase and texture formation of ceria based films and superconductor films deposited by the chemical solution method on technical substrates. Combined analysis using in situ synchrotron x-ray diffraction, thermogravimetry...

A synchrotron radiation study of strontium titanate

International Nuclear Information System (INIS)

Maslen, E.N.; Spadaccini, N.; Ito, T.; Marumo, F.; Satow, Y.

1995-01-01

Electron deformation densities Δρ for SrTiO 3 have been determined from diffraction data measured using focused synchrotron radiation with λ = 0.7000 (2) A at the Photon Factory, KEK, Japan. Corrections for secondary extinction were estimated from the variation of diffraction intensity with path length, and checked from the λ-dependence of the strong intensities indicated by measurements using a weaker parallel beam with λ = 0.5000 (2) A. The 0.7 A study is more precise than earlier analyses with Mo Kα radiation. The difference density near the Ti nucleus is mildly anisotropic, and the Δρ topography is similar to those for closed-shell atoms in related perovskite structures. (orig.)

Pump-probe experiments in atoms involving laser and synchrotron radiation: an overview

International Nuclear Information System (INIS)

Wuilleumier, F J; Meyer, M

2006-01-01

The combined use of laser and synchrotron radiations for atomic photoionization studies started in the early 1980s. The strong potential of these pump-probe experiments to gain information on excited atomic states is illustrated through some exemplary studies. The first series of experiments carried out with the early synchrotron sources, from 1960 to about 1995, are reviewed, including photoionization of unpolarized and polarized excited atoms, and time-resolved laser-synchrotron studies. With the most advanced generation of synchrotron sources, a whole new class of pump-probe experiments benefiting from the high brightness of the new synchrotron beams has been developed since 1996. A detailed review of these studies as well as possible future applications of pump-probe experiments using third generation synchrotron sources and free electron lasers is presented. (topical review)

Synchrotron X-ray scattering studies at mineral-water interfaces

International Nuclear Information System (INIS)

Chiarello, R.P.; Sturchio, N.C.

1995-01-01

Synchrotron X-ray scattering techniques provide a powerful tool for the in situ study of atomic scale processes occurring at solid-liquid interfaces. We have applied these techniques to characterize and study reactions at mineral-water interfaces. Here we present two examples. The first is the characterization of the calcite (CaCO 3 ) (10 bar 14) cleavage surface, in equilibrium with deionized water, by crystal truncation rod measurements. The second is the in situ study of the heteroepitaxial growth of otavite (CdCO 3 ) on the calcite (10 bar 14) cleavage surface. The results of such studies will lead to significant progress in understanding mineral-water interface geochemistry

Rated parameters of the JINR synchrotron radiation source for the electron energy 0.7 GeV

International Nuclear Information System (INIS)

Aksenov, V.L.; Belushkin, A.V.; Meshkov, I.N.; Syresin, E.M.; Tyutyunnikov, S.I.

1998-01-01

This paper gives the first estimates of the rated parameters of the JINR compact synchrotron radiation (SR) source for the electron energy 0.7 GeV. The realization of the JINR SR source which incorporates superconducting wigglers and an undulator will make it possible to construct few channels for hard X-rays with the energy up to 10 keV. The project for the construction of the SR source is motivated by the purposes of X-ray lithography and micromechanics, the so-called LIGA process. The energy spectrum of SR from the bending magnets in the source covers the energy range from infra-red to ultra-violet. This SR can be used at several stations for investigations in the field of condensed matter physics in the infra-red region, such as studies of impurities in semiconductors, measurements of the superconducting gap, radiometry in the vacuum ultra-violet region

The pressure behaviour of actinides via synchrotron radiation

International Nuclear Information System (INIS)

Haire, R.G.; Heathman, S.; Le Bihan, T.; Lindbaum, A.

2002-01-01

Various aspects of performing high-pressure studies with radioactive f-elements using synchrotrons as sources of X-rays are discussed. For ultra-high pressures, intense well-focused beams of 10 to 30 microns in diameter and a single wavelength of 0.3 to 0.7 angstrom are desired for angle dispersive diffraction measurements. Special considerations are necessary for the studies of transuranium elements under pressure at synchrotron facilities. Normally, with these actinides the pressure cells are prepared off-site and shipped to the synchrotron for study. Approved containment techniques must be provided to assure there is not a potential for the release of sample material. The goal of these high-pressure studies is to explore the fundamental science occurring as pressure is applied to the actinide samples. One of the primary effects of pressure is to reduce interatomic distances, and the goal is to ascertain the changes in bonding and electronic nature of the system that result as atoms and electronic orbitals are forced closer together. Concepts of the science being pursued with these f-elements are outlined. A brief discussion of the behaviour of americium metal under pressure performed recently at the ESRF is provided as an example of the high-pressure research being performed with synchrotron radiation. Also discussed here is the important role synchrotrons play and the techniques/procedures employed in high-pressure studies with actinides. (authors)

Data and videos for ultrafast synchrotron X-ray imaging studies of metal solidification under ultrasound

Directory of Open Access Journals (Sweden)

Bing Wang

2018-04-01

Full Text Available The data presented in this article are related to the paper entitled ‘Ultrafast synchrotron X-ray imaging studies of microstructure fragmentation in solidification under ultrasound’ [Wang et al., Acta Mater. 144 (2018 505-515]. This data article provides further supporting information and analytical methods, including the data from both experimental and numerical simulation, as well as the Matlab code for processing the X-ray images. Six videos constructed from the processed synchrotron X-ray images are also provided.

Overview of Industrial Synchrotron Radiation Use

Science.gov (United States)

Laderman, Stephen S.

1996-03-01

Relevant, reliable and accessible synchrotron radiation methods can play an important role in industrial activities. To date, the application of synchrotron radiation based materials characterization methods by industrial concerns has followed the path of laboratory based x-ray methods: early adoption, continuous improvement, and a high degree of specialization to meet specific goals, which may change over time. Like all x-ray methods, their applicability to segments of the biotechnology, chemical, electronics, medical and metallurgical industries arises from a need to develop sophisticated processes for precisely controlling microstructures. An increasing number of those processes are being developed in ways which can, in principle, be more effectively studied if synchrotron radiation based analyses are performed. Technical limitations confined the efforts of early synchrotron radiation users to long-range research investigations. Nowadays, progress in data collection methods, analysis algorithims, accelerator performance, and worker training, have removed many constraints. However, commercial technologies are being improved at steadily higher rates, shortening the time between research, development and manufacturing and, in many cases, blurring their distinctions. Certainly, rapid rates of innovation increase the opportunities for synchrotron radiation techniques to bring competitive advantage since they can be used to shrink development times, to maintain yields and, perhaps, as part of advanced manufacturing. At the same time, rapid rates of innovation also impose stringent criteria on the reliability and timeliness of the supporting methods. Successful conventional x-ray methods have resulted from efforts to create useful new capabilities that effectively balance such forces. Currently, synchrotron radiation users throughout the world are pursuing analogous goals.

Report of the Synchrotron Radiation Vacuum Workshop

International Nuclear Information System (INIS)

Avery, R.T.

1984-06-01

The Synchrotron Radiation Vacuum Workshop was held to consider two vacuum-related problems that bear on the design of storage rings and beam lines for synchrotron radiation facilities. These problems are gas desorption from the vacuum chamber walls and carbon deposition on optical components. Participants surveyed existing knowledge on these topics and recommended studies that should be performed as soon as possible to provide more definitive experimental data on these topics. This data will permit optimization of the final design of the Advanced Light Source (ALS) and its associated beam lines. It also should prove useful for other synchrotron radiation facilities as well

Synchrotron- and focal plane array-based Fourier-transform infrared spectroscopy differentiates the basalis and functionalis epithelial endometrial regions and identifies putative stem cell regions of human endometrial glands.

Science.gov (United States)

Theophilou, Georgios; Morais, Camilo L M; Halliwell, Diane E; Lima, Kássio M G; Drury, Josephine; Martin-Hirsch, Pierre L; Stringfellow, Helen F; Hapangama, Dharani K; Martin, Francis L

2018-05-09

The cyclical process of regeneration of the endometrium suggests that it may contain a cell population that can provide daughter cells with high proliferative potential. These cell lineages are clinically significant as they may represent clonogenic cells that may also be involved in tumourigenesis as well as endometriotic lesion development. To determine whether the putative stem cell location within human uterine tissue can be derived using vibrational spectroscopy techniques, normal endometrial tissue was interrogated by two spectroscopic techniques. Paraffin-embedded uterine tissues containing endometrial glands were sectioned to 10-μm-thick parallel tissue sections and were floated onto BaF 2 slides for synchrotron radiation-based Fourier-transform infrared (SR-FTIR) microspectroscopy and globar focal plane array-based FTIR spectroscopy. Different spectral characteristics were identified depending on the location of the glands examined. The resulting infrared spectra were subjected to multivariate analysis to determine associated biophysical differences along the length of longitudinal and crosscut gland sections. Comparison of the epithelial cellular layer of transverse gland sections revealed alterations indicating the presence of putative transient-amplifying-like cells in the basalis and mitotic cells in the functionalis. SR-FTIR microspectroscopy of the base of the endometrial glands identified the location where putative stem cells may reside at the same time pointing towards ν s PO 2 - in DNA and RNA, nucleic acids and amide I and II vibrations as major discriminating factors. This study supports the view that vibration spectroscopy technologies are a powerful adjunct to our understanding of the stem cell biology of endometrial tissue. Graphical abstract ᅟ.

Synchrotron-Based X Ray and FTIR Micro-Spectroscopy for the Cultural Heritage Science at the ID21 Beamline, ESRF

International Nuclear Information System (INIS)

Cotte, M.; Radepont, M.; Pouyet, E.; Salome, M.; Susini, J.

2016-01-01

Synchrotron-based techniques are increasingly used for the study of Cultural Heritage (CH) materials. These analyses rely on light-matter interactions and can be carried out directly onto the artworks. They also benefit from the synchrotron assets and in particular from the gain in terms of lateral resolution when comparing with laboratory equipment. Thanks to the synchrotron beam high brightness and low divergence, X rays can be focused down to less than 1μm, making possible the selective analysis of various compounds in complex structures. The ID21 beamline, at the ESRF, is devoted to such high resolution microscopy, using both X ray and infrared beams. Almost all kinds of CH materials can be studied, from hard matter, such as metals, glasses, pigments, to soft matters such as varnishes, tissues, wood, paper, textile, wax… Usually, samples are prepared as transversal cross-sections in order to highlight the internal structure of the matter (corrosion patina on metals, multilayer structures in paintings…). 2D elemental mapping are generated by micro-X ray fluorescence, with low detection limit. Chemical information can be obtained both by X ray absorption spectroscopy (micro-XANES) and by infrared spectroscopy (micro-FTIR). Studies usually aim at understanding degradation mechanisms (corrosion, colour variation, formation of crust), or at identifying artistic processes (choice of pigments and binders for paintings, optical effects in glasses…). The X ray energy range at ID21 is 2-9keV, giving access to all the K-edges from P to Cu. It covers S and Cl, which are frequently implied in degradation processes, and the 3d transition metals, which enter in the composition of many artworks (being in pigments, inks, glasses or metal). The FTIR-microscope provides complementary molecular information, and is used more particularly for the analysis of organic and hybrid components. The two microscopes are independent and can be operated simultaneously. Various hardware

Synchrotron applications in wood preservation and deterioration

Science.gov (United States)

Barbara L. Illman

2003-01-01

Several non-intrusive synchrotron techniques are being used to detect and study wood decay. The techniques use high intensity synchrotron-generated X-rays to determine the atomic structure of materials with imaging, diffraction, and absorption. Some of the techniques are X-ray absorption near edge structure (XANES), X-ray fluorescence spectroscopy (XFS), X-ray...

A guide to synchrotron radiation science

CERN Document Server

Sato, Shigeru; Munro, Ian; Lodha, G S

2015-01-01

Synchrotron Radiation (SR), as a light source is now in use around the world to provide brilliant radiation from the infrared into the soft and hard X-ray regions. It is an indispensible and essential tool to establish the physic-chemical characteristics of materials and surfaces from an atomic and molecular view point. It is being applied to topics which range from mineralogy to protein crystallography, embracing research in areas from the physical to the life sciences. This new guide is a concise yet comprehensive and easily readable introduction to an expanding area of science. It presents in a readily assimilable form the basic concepts of SR science from its generation principles, through source design and operation to the principles of instruments for SR exploitation followed by a survey of its actual applications in selected research fields, including spectroscopy, diffractometry, microanalysis and chemical processing.

Contact microscopy with synchrotron radiation

International Nuclear Information System (INIS)

Panessa-Warren, B.J.

1985-10-01

Soft x-ray contact microscopy with synchrotron radiation offers the biologist and especially the microscopist, a way to morphologically study specimens that could not be imaged by conventional TEM, STEM or SEM methods (i.e. hydrated samples, samples easily damaged by an electron beam, electron dense samples, thick specimens, unstained low contrast specimens) at spatial resolutions approaching those of the TEM, with the additional possibility to obtain compositional (elemental) information about the sample as well. Although flash x-ray sources offer faster exposure times, synchrotron radiation provides a highly collimated, intense radiation that can be tuned to select specific discrete ranges of x-ray wavelengths or specific individual wavelengths which optimize imaging or microanalysis of a specific sample. This paper presents an overview of the applications of x-ray contact microscopy to biological research and some current research results using monochromatic synchrotron radiation to image biological samples. 24 refs., 10 figs

CORNELL: Synchrotron 25

International Nuclear Information System (INIS)

Anon.

1993-01-01

A recent celebration marked the twenty-fifth anniversary of the Cornell Electron Synchrotron. The major milestone in the commissioning of the synchrotron was on October 11, 1967 when Helen Edwards, Boyce McDaniel, and Maury Tigner achieved a 7 GeV beam, a worldrecord energy for electron synchrotrons at that time. Like so many advances in experimental physics, this occurred early in the morning - 3 a.m.! The transition from accelerator commissioning to high energy physics operation was extremely rapid; 7 GeV operation for data collection was routine just five weeks later. Throughout its life as a source of photon and electron beams for fixed target experiments, the synchrotron maintained energy leadership for circular electron machines. Originally designed for operation at 10 GeV, eventually it consistently provided beams for experiments at energies up to 11.6 GeV. It now operates at 5 GeV, serving as the injector for the CESR electron-positron storage ring. Robert Wilson was director of the laboratory during the design and most of the construction of the machine. He left near the end of the construction to become the first director of Fermilab and was replaced by Boyce McDaniel, who guided the laboratory from the completion of the synchrotron to the construction and early operation of CESR. Wilson recalled how the laboratory had originally proposed a 3 GeV turnkey machine to be built entirely by industry and would fit in the space previously occupied by earlier Cornell accelerators. However, members of the laboratory realized that 3 GeV would not open new physics frontiers, that the construction of the accelerator was much of the fun of doing high energy physics experiments, and that a more challenging project was needed. This led to the proposal for the 10 GeV synchrotron which was built in the ''Cornell Style'' with many of the components fabricated and nearly all of the assembly done at Cornell

CORNELL: Synchrotron 25

Energy Technology Data Exchange (ETDEWEB)

Anon.

1993-03-15

A recent celebration marked the twenty-fifth anniversary of the Cornell Electron Synchrotron. The major milestone in the commissioning of the synchrotron was on October 11, 1967 when Helen Edwards, Boyce McDaniel, and Maury Tigner achieved a 7 GeV beam, a worldrecord energy for electron synchrotrons at that time. Like so many advances in experimental physics, this occurred early in the morning - 3 a.m.! The transition from accelerator commissioning to high energy physics operation was extremely rapid; 7 GeV operation for data collection was routine just five weeks later. Throughout its life as a source of photon and electron beams for fixed target experiments, the synchrotron maintained energy leadership for circular electron machines. Originally designed for operation at 10 GeV, eventually it consistently provided beams for experiments at energies up to 11.6 GeV. It now operates at 5 GeV, serving as the injector for the CESR electron-positron storage ring. Robert Wilson was director of the laboratory during the design and most of the construction of the machine. He left near the end of the construction to become the first director of Fermilab and was replaced by Boyce McDaniel, who guided the laboratory from the completion of the synchrotron to the construction and early operation of CESR. Wilson recalled how the laboratory had originally proposed a 3 GeV turnkey machine to be built entirely by industry and would fit in the space previously occupied by earlier Cornell accelerators. However, members of the laboratory realized that 3 GeV would not open new physics frontiers, that the construction of the accelerator was much of the fun of doing high energy physics experiments, and that a more challenging project was needed. This led to the proposal for the 10 GeV synchrotron which was built in the ''Cornell Style'' with many of the components fabricated and nearly all of the assembly done at Cornell.

The Synchrotron Radiation Facility ESFR in Grenoble

International Nuclear Information System (INIS)

Haensel, R.

1994-01-01

The European Synchrotron Radiation Facility (ESFR) is the first synchrotron radiation source of the 3-th generation for Roentgen radiations.It permits a new series of experiments in the domains of physics, chemistry, materials studies, micromechanics, biology, medicine and crystallography. The main part of device represents the 850 meter storage ring of 6 GeV electrons. (MSA)

The World of Synchrotrons

Indian Academy of Sciences (India)

de Ciencias Fisicas,. Universidad Nacional. Autonoma de Mexico. Sameen Ahmed Khan. A summary of results on synchrotron radiation is presented along with notes on its properties and applications. Quantum aspects are briefly mentioned. Synchrotron radiation facilities are described briefly with a detailed coverage of ...

Study of charge-sharing in MEDIPIX3 using a micro-focused synchrotron beam

International Nuclear Information System (INIS)

Gimenez, E N; Horswell, I; Marchal, J; Sawhney, K J S; Tartoni, N; Ballabriga, R; Campbell, M; Llopart, X; Turecek, D

2011-01-01

X-ray photon-counting detectors consisting of a silicon pixel array sensor bump-bonded to a CMOS electronic readout chip offer several advantages over traditional X-ray detection technologies used for synchrotron applications. They offer high frame rate, dynamic range, count rate capability and signal-to-noise ratio. A survey of the requirements for future synchrotron detectors carried out at the Diamond Light Source synchrotron highlighted the needs for detectors with a pixel size of the order of 50μm. Reducing the pixel size leads to an increase of charge-sharing events between adjacent pixels and, therefore, to a degradation of the energy resolution and image quality of the detector. This effect was observed with MEDIPIX2, a photon-counting readout chip with a pixel size of 55μm. The latest generation of the MEDIPIX family, MEDIPIX3, is designed to overcome this charge-sharing effect in an implemented readout operating mode referred to as Charge Summing Mode. MEDIPIX3 has the same pixel size as MEDIPIX2, but it is implemented in an 8-metal 0.13μm CMOS technology which enables increased functionality per pixel. The present work focuses on the study of the charge-sharing effect when the MEDIPIX3 is operated in Charge Summing Mode compared to the conventional readout mode, referred to as Single Pixel Mode. Tests of a standard silicon photodiode array bump-bonded to MEDIPIX3 were performed in beamline B16 at the Diamond Light Source synchrotron. A monochromatic micro-focused beam of 2.9μm x 2.2μm size at 15keV was used to scan a cluster of nine pixels in order to study the charge collection and X-ray count allocation process for each readout mode, Single Pixel Mode and Charge Summing Mode. The study showed that charge-shared events were eliminated when Medipix3 was operated in Charge Summing Mode.

Combination of lasers and synchrotron radiation in studies of atomic photoionization

International Nuclear Information System (INIS)

Meyer, M.

2009-01-01

Recent experiments using the combination of conventional lasers and synchrotron radiation are presented and discussed. The controlled laser-manipulation of atoms prior to ionization by the synchrotron radiation provides an ideal experimental basis for detailed investigations of atomic photoionization. Due to the recent advances in high-resolution electron spectroscopy, it has become possible to analyze the J-resolved fine structure of the final ionic states in the photoionization of laser-excited atoms enabling thereby the determination of the specific influence of the outer electron to the ionization from inner subshells. Especially, the analysis of photoemission satellites and their relative intensities bring out directly the importance of electron correlations. Furthermore, it is shown through some examples of experiments using linearly and circularly polarized radiations, how the study of magnetic dichroisms in the photoionization opens the access to a complete description of the photoionization process, in particular to the determination of partial photoionization cross-sections.

Synchrotron light source data book

International Nuclear Information System (INIS)

Murphy, J.

1989-01-01

The ''Synchrotron Light Source Data Book'' is as its name implies a collection of data on existing and planned synchrotron light sources. The intention was to provide a compendium of tools for the design of electron storage rings as synchrotron radiation sources. The slant is toward the accelerator physicist as other booklets such as the X-ray Data Booklet, edited by D. Vaughan (LBL PUB-490), address the 'use' of synchrotron radiation. It is hoped that the booklet serves as a pocket sized reference to facilitate back of the envelope type calculations. It contains some useful formulae in 'practical units' and a brief description of many of the existing and planned light source lattices

Surface enhanced infrared spectroscopy using interacting gold nanowires

Energy Technology Data Exchange (ETDEWEB)

Neubrech, Frank; Weber, Daniel; Pucci, Annemarie [Kirchhoff-Institut fuer Physik, Heidelberg (Germany); Shen, Hong [Universite Troyes, Troyes (France); Lamy de la Chapelle, Marc [Universite Paris 13, Bobigny (France)

2009-07-01

We performed surface enhanced infrared spectroscopy (SEIRS) of molecules adsorbed on gold nanowires using synchrotron light of the ANKA IR-beamline at the Forschungszentrum Karlsruhe (Germany). Arrays of gold nanowires with interparticle spacings down to 30nm were prepared by electron beam lithography. The interparticle distance was reduced further by wet-chemically increasing the size of the gold nanowires. The growth of the wires was proofed using IR spectroscopy as well as scanning electron microscopy. After this preparation step, appropriate arrays of nanowires with an interparticle distance down to a few nanometers were selected to demonstrate the surface enhanced infrared spectroscopy of one monolayer octadecanthiol (ODT). As know from SEIRS studies using single gold nanowires, the spectral position of the antenna-like resonance in relation to the absorption bands of ODT (2850cm-1 and 2919cm-1) is crucial for both, the lineshape of the molecular vibration and the signal enhancement. In contrast to single nanowires studies, a further increase of the enhanced signals is expected due to the interaction of the electromagnetic fields of the close-by nanowires.

National Synchrotron Light Source: vacuum system for National Synchrotron Light Source

International Nuclear Information System (INIS)

Schuchman, J.C.; Godel, J.B.; Jordan, W.; Oversluizen, T.

1978-01-01

The National Synchrotron Light Source (NSLS), a 24 million dollar project under construction at Brookhaven National Laboratory (BNL), is a research facility dedicated to the production of synchrotron radiation. Synchrotron radiation is that radiation produced by the acceleration of charged particles at near the speed of light. This facility will provide a continuous spectrum of radiation from the vacuum ultraviolet to the hard x-ray range. The radiation will be highly intense, 100% polarized, extremely well collimated and will have a pulsed time structure. The radiation will be produced in two electron storage rings at energies of 700 MeV and 2.5 GeV, respectively. A maximum of one ampere at 2 GeV, or one-half ampere at 2.5 GeV, of electron beam will be stored

Study for a 6 GeV undulator based synchrotron radiation source

International Nuclear Information System (INIS)

Vignola, G.; Barton, M.; Blumberg, R.; Galayda, J.; Krinsky, S.; Luccio, A.; Pellegrini, C.; van Steenbergen, A.; Wang, J.

1985-01-01

A partial study for a 6 GeV undulator based synchrotron radiation source for production of high brightness undulator radiation, in the A region, is presented. The basic lattice adopted for the storage ring is a hybrid FODO Chasman-Green lattice, making use of gradient in the dipoles. We discuss also the e beam current limits and the injection parameters

Synchrotron-radiation experiments with recoil ions

International Nuclear Information System (INIS)

Levin, J.C.

1989-01-01

Studies of atoms, ions and molecules with synchrotron radiation have generally focused on measurements of properties of the electrons ejected during, or after, the photoionization process. Much can also be learned, however, about the atomic or molecular relaxation process by studies of the residual ions or molecular fragments following inner-shell photoionization. Measurements are reported of mean kinetic energies of highly charged argon, krypton, and xenon recoil ions produced by vacancy cascades following inner-shell photoionization using white and monochromatic synchrotron x radiation. Energies are much lower than for the same charge-state ions produced by charged-particle impact. The results may be applicable to design of future angle-resolved ion-atom collision experiments. Photoion charge distributions are presented and compared with other measurements and calculations. Related experiments with synchrotron-radiation produced recoil ion, including photoionization of stored ions and measurement of shakeoff in near-threshold excitation, are briefly discussed. 24 refs., 6 figs., 1 tab

Inverse comptonization vs. thermal synchrotron

International Nuclear Information System (INIS)

Fenimore, E.E.; Klebesadel, R.W.; Laros, J.G.

1983-01-01

There are currently two radiation mechanisms being considered for gamma-ray bursts: thermal synchrotron and inverse comptonization. They are mutually exclusive since thermal synchrotron requires a magnetic field of approx. 10 12 Gauss whereas inverse comptonization cannot produce a monotonic spectrum if the field is larger than 10 11 and is too inefficient relative to thermal synchrotron unless the field is less than 10 9 Gauss. Neither mechanism can explain completely the observed characteristics of gamma-ray bursts. However, we conclude that thermal synchrotron is more consistent with the observations if the sources are approx. 40 kpc away whereas inverse comptonization is more consistent if they are approx. 300 pc away. Unfortunately, the source distance is still not known and, thus, the radiation mechanism is still uncertain

Synchrotron radiation at Trieste

Energy Technology Data Exchange (ETDEWEB)

Anon.

1986-06-15

The fast developing field of synchrotron radiation has its origins in the mastery of storage rings in high energy physics and is a prime example of spinoff from pure science. Intense electromagnetic radiation streams off when beams of high energy electrons are bent or shaken. This synchrotron radiation was once an annoying waste of energy in particle storage rings, but now the wheel has turned full circle, with dedicated machines supplying this radiation for a wide range of science. The astonishing growth rate in this field was highlighted at an International Conference on Synchrotron Radiation, held at the International Centre for Theoretical Physics (ICTP), Trieste, Italy from 7-11 April.

Synchrotron radiation at Trieste

International Nuclear Information System (INIS)

Anon.

1986-01-01

The fast developing field of synchrotron radiation has its origins in the mastery of storage rings in high energy physics and is a prime example of spinoff from pure science. Intense electromagnetic radiation streams off when beams of high energy electrons are bent or shaken. This synchrotron radiation was once an annoying waste of energy in particle storage rings, but now the wheel has turned full circle, with dedicated machines supplying this radiation for a wide range of science. The astonishing growth rate in this field was highlighted at an International Conference on Synchrotron Radiation, held at the International Centre for Theoretical Physics (ICTP), Trieste, Italy from 7-11 April

Synchrotron Radiation in eRHIC Interaction Region

CERN Document Server

Beebe-Wang, Joanne; Montag, Christoph; Rondeau, Daniel J; Surrow, Bernd

2005-01-01

The eRHIC currently under study at BNL consists of an electron storage ring added to the existing RHIC complex. The interaction region of this facility has to provide the required low-beta focusing while accommodating the synchrotron radiation generated by beam separation close to the interaction point. In the current design, the synchrotron radiation caused by 10GeV electrons bent by low-beta triplet magnets will be guided through the interaction region and dumped 5m downstream. However, it is unavoidable to stop a fraction of the photons at the septum where the electron and ion vacuum system are separated. In order to protect the septum and minimize the backward scattering of the synchrotron radiation, an absorber and collimation system will be employed. In this paper, we first present the overview of the current design of the eRHIC interaction region with special emphasis on the synchrotron radiation. Then the initial design of the absorber and collimation system, including their geometrical and physical p...

Synchrotrons are also devoted to the society

International Nuclear Information System (INIS)

Gacoin, M.P.; Cornuejols, D.; Cotte, M.; Deblay, P.; Mitchell, E.P.; McCarthy, J.; Fraissard, F.

2013-01-01

The ESRF and the SOLEIL synchrotrons are not only scientific instruments but also active players in the cultural and economic fields. This document gathers 6 short articles. The 2 first present the actions of SOLEIL and ESRS scientific teams towards the spreading of scientific knowledge in the public. The third article is dedicated to the uses of synchrotron radiation to the study of cultural objects to learn more about their fabrication, present state or the remedial actions that could be used to renovate them. The fourth and fifth articles present the contributions of ESRF and SOLEIL to the industrial world, in fact these contributions are not limited to the research field but also appear for quality assurance or the control of aging processes. Partnerships have been signed between both synchrotrons and enterprises to develop industrial products based on instrumentation or on the use of synchrotron radiation. The last article describes the procedure to have access to both facilities. (A.C.)

Synchrotron Radiation in Biology and Medicine

International Nuclear Information System (INIS)

Pelka, J.B.

2008-01-01

This work is focused on a present status of synchrotron radiation X-ray applications in medicine and biology to imaging, diagnostics, and radio- therapy. Properties of X-ray beams generated by synchrotron sources are compared with radiation produced by classical laboratory X-ray tubes. A list of operating and planned synchrotron facilities applicable to biomedical purposes is given, together with their basic characteristics. A concise overview of typical X-ray synchrotron techniques in biology and medicine is carried out with discussion of their specific properties and examples of typical results. (author)

CHESS-the Cornell High Energy Synchrotron Source

International Nuclear Information System (INIS)

Batterman, B.W.; Cornell Univ., Ithaca, NY

1980-01-01

The Wilson Laboratory at Cornell University has done pioneering work on development of high energy synchrotrons. In the last decade, the 12 GeV synchrotron has been the most energetic electron synchrotron in the world. In 1975 plans were formulated to build a 4-8 GeV storage ring in the same tunnel as the synchrotron and to use the latter as the injector for the storage ring. This small radius (the normal bend magnets have R = 87 m), coupled with the relatively high electron energy of the storage ring, makes these magnets potent sources of synchrotron radiation. In June of 1978 the National Science Foundation funded a project to create CHESS, the Cornell High Energy Synchrotron Source. (orig./FKS)

Australian synchrotron radiation science

International Nuclear Information System (INIS)

White, J.W.

1996-01-01

Full text: The Australian Synchrotron Radiation Program, ASRP, has been set up as a major national research facility to provide facilities for scientists and technologists in physics, chemistry, biology and materials science who need access to synchrotron radiation. Australia has a strong tradition in crystallography and structure determination covering small molecule crystallography, biological and protein crystallography, diffraction science and materials science and several strong groups are working in x-ray optics, soft x-ray and vacuum ultra-violet physics. A number of groups whose primary interest is in the structure and dynamics of surfaces, catalysts, polymer and surfactant science and colloid science are hoping to use scattering methods and, if experience in Europe, Japan and USA can be taken as a guide, many of these groups will need third generation synchrotron access. To provide for this growing community, the Australian National Beamline at the Photon Factory, Tsukuba, Japan, has been established since 1990 through a generous collaboration with Japanese colleagues, the beamline equipment being largely produced in Australia. This will be supplemented in 1997 with access to the world's most powerful synchrotron x-ray source at the Advanced Photon Source, Argonne National Laboratory, USA. Some recent experiments in surface science using neutrons as well as x-rays from the Australian National Beamline will be used to illustrate one of the challenges that synchrotron x-rays may meet

Manufacturability of compact synchrotron mirrors

Science.gov (United States)

Douglas, Gary M.

1997-11-01

While many of the government funded research communities over the years have put their faith and money into increasingly larger synchrotrons, such as Spring8 in Japan, and the APS in the United States, a viable market appears to exist for smaller scale, research and commercial grade, compact synchrotrons. These smaller, and less expensive machines, provide the research and industrial communities with synchrotron radiation beamline access at a portion of the cost of their larger and more powerful counterparts. A compact synchrotron, such as the Aurora-2D, designed and built by Sumitomo Heavy Industries, Ltd. of japan (SHI), is a small footprint synchrotron capable of sustaining 20 beamlines. Coupled with a Microtron injector, with 150 MeV of injection energy, an entire facility fits within a 27 meter [88.5 ft] square floorplan. The system, controlled by 2 personal computers, is capable of producing 700 MeV electron energy and 300 mA stored current. Recently, an Aurora-2D synchrotron was purchased from SHI by the University of Hiroshima. The Rocketdyne Albuquerque Operations Beamline Optics Group was approached by SHI with a request to supply a group of 16 beamline mirrors for this machine. These mirrors were sufficient to supply 3 beamlines for the Hiroshima machine. This paper will address engineering issues which arose during the design and manufacturing of these mirrors.

Synchrotron X-Ray Footprinting on Tour

OpenAIRE

Bohon, Jen; Ralston, Corie; D'Mello, Rhijuta; Gupta, Sayan; Chance, Mark R.

2014-01-01

Synchrotron X-ray footprinting resources were investigated at a variety of beamlines and synchrotron facilities to understand their potential for a mobile general user. Results indicate that viable resources exist at each synchrotron investigated such that a prospective user need only provide a simple flow apparatus and sample handling accessories to perform this technique.

High-rate anisotropic ablation and deposition of polytetrafluoroethylene using synchrotron radiation process

International Nuclear Information System (INIS)

Inayoshi, Muneto; Ikeda, Masanobu; Hori, Masaru; Goto, Toshio; Hiramatsu, Mineo; Hiraya, Atsunari.

1995-01-01

Both anisotropic ablation and thin film formation of polytetrafluoroethylene (PTFE) were successfully demonstrated using synchrotron radiation (SR) irradiation of PTFE, that is, the SR ablation process. Anisotropic ablation by the SR irradiation was performed at an extremely high rate of 3500 μm/min at a PTFE target temperature of 200degC. Moreover, a PTFE thin film was formed at a high rate of 2.6 μm/min using SR ablation of PTFE. The chemical structure of the deposited film was similar to that of the PTFE target as determined from Fourier transform infrared absorption spectroscopy (FT-IR) analysis. (author)

Characteristics of synchrotron radiation

International Nuclear Information System (INIS)

Brown, G.S.

1984-01-01

The characteristics and production of synchrotron radiation are qualitatively discussed. The spectral properties of wigglers and undulators are briefly described. Possible applications in condensed matter physics are outlined. These include atomic and molecular studies, crystallography, impurities in solids and radiographic imaging

Synchrotron Intensity Gradients as Tracers of Interstellar Magnetic Fields

Energy Technology Data Exchange (ETDEWEB)

Lazarian, A.; Yuen, Ka Ho; Lee, Hyeseung; Cho, J. [Department of Astronomy, University of Wisconsin-Madison, 2535 Sterling Hall, 475 North Charter Street, Madison, WI 53706-1507 (United States)

2017-06-10

On the basis of the modern understanding of MHD turbulence, we propose a new way of using synchrotron radiation: using synchrotron intensity gradients (SIGs) for tracing astrophysical magnetic fields. We successfully test the new technique using synthetic data obtained with 3D MHD simulations and provide the demonstration of the practical utility of the technique by comparing the directions of magnetic fields that are obtained with PLANCK synchrotron intensity data to the directions obtained with PLANCK synchrotron polarization data. We demonstrate that the SIGs can reliably trace magnetic fields in the presence of noise and can provide detailed maps of magnetic field directions. We also show that the SIGs are relatively robust for tracing magnetic fields while the low spatial frequencies of the synchrotron image are removed. This makes the SIGs applicable to the tracing of magnetic fields using interferometric data with single-dish measurement absent. We discuss the synergy of using the SIGs together with synchrotron polarization in order to find the actual direction of the magnetic fields and quantify the effects of Faraday rotation as well as with other ways of studying astrophysical magnetic fields. We test our method in the presence of noise and the resolution effects. We stress the complementary nature of the studies using the SIG technique and those employing the recently introduced velocity gradient techniques that trace magnetic fields using spectroscopic data.

Synchrotron Intensity Gradients as Tracers of Interstellar Magnetic Fields

International Nuclear Information System (INIS)

Lazarian, A.; Yuen, Ka Ho; Lee, Hyeseung; Cho, J.

2017-01-01

On the basis of the modern understanding of MHD turbulence, we propose a new way of using synchrotron radiation: using synchrotron intensity gradients (SIGs) for tracing astrophysical magnetic fields. We successfully test the new technique using synthetic data obtained with 3D MHD simulations and provide the demonstration of the practical utility of the technique by comparing the directions of magnetic fields that are obtained with PLANCK synchrotron intensity data to the directions obtained with PLANCK synchrotron polarization data. We demonstrate that the SIGs can reliably trace magnetic fields in the presence of noise and can provide detailed maps of magnetic field directions. We also show that the SIGs are relatively robust for tracing magnetic fields while the low spatial frequencies of the synchrotron image are removed. This makes the SIGs applicable to the tracing of magnetic fields using interferometric data with single-dish measurement absent. We discuss the synergy of using the SIGs together with synchrotron polarization in order to find the actual direction of the magnetic fields and quantify the effects of Faraday rotation as well as with other ways of studying astrophysical magnetic fields. We test our method in the presence of noise and the resolution effects. We stress the complementary nature of the studies using the SIG technique and those employing the recently introduced velocity gradient techniques that trace magnetic fields using spectroscopic data.

SOFT: a synthetic synchrotron diagnostic for runaway electrons

Science.gov (United States)

Hoppe, M.; Embréus, O.; Tinguely, R. A.; Granetz, R. S.; Stahl, A.; Fülöp, T.

2018-02-01

Improved understanding of the dynamics of runaway electrons can be obtained by measurement and interpretation of their synchrotron radiation emission. Models for synchrotron radiation emitted by relativistic electrons are well established, but the question of how various geometric effects—such as magnetic field inhomogeneity and camera placement—influence the synchrotron measurements and their interpretation remains open. In this paper we address this issue by simulating synchrotron images and spectra using the new synthetic synchrotron diagnostic tool SOFT (Synchrotron-detecting Orbit Following Toolkit). We identify the key parameters influencing the synchrotron radiation spot and present scans in those parameters. Using a runaway electron distribution function obtained by Fokker-Planck simulations for parameters from an Alcator C-Mod discharge, we demonstrate that the corresponding synchrotron image is well-reproduced by SOFT simulations, and we explain how it can be understood in terms of the parameter scans. Geometric effects are shown to significantly influence the synchrotron spectrum, and we show that inherent inconsistencies in a simple emission model (i.e. not modeling detection) can lead to incorrect interpretation of the images.

50 years of synchrotrons. Early synchrotrons in Britain, and early work for CERN. - The CERN synchrotrons. Lectures

International Nuclear Information System (INIS)

Lawson, J.; Brianti, G.

1997-01-01

In the first report, 'Early synchrotrons in Britain, and early work for CERN', John Lawson gives an extended account of the material presented at the John Adams lecture, and at the same time a revised and shortened version of RAL report 97-011, which contains fuller archival references and notes. During the period covered by this report there was extensive work in Russia, where the principle of phase stability had been discovered in 1944 by Veksler. Unfortunately, all experimental work was kept secret until Veksler's talk at the first 'Atoms for Peace' conference at Geneva in August 1955. In the second lecture, 'The CERN Synchrotrons', Giorgio Brianti outlines the history of alternating-gradient synchrotrons from 1953/54 until today. In preparing this lecture he was confronted with a vast amount of material, while the time at his disposal was not even one minute per year, implying a time compression factor close to one million. Therefore, he had to exercise drastic choices, which led him to concentrate on CERN hadron synchrotrons and colliders and leave aside the Large Electron-Positron storage ring (LEP). Indeed, LEP was the subject of the John Adams Memorial Lecture in 1990, and it may be treated again in the future in connection with its energy upgrade. Even with these severe limitations, it was impossible to do justice to the number and variety of events and to the ingenuity of the people who have carved the history of CERN and of particle physics on the magnets, radiofrequency cavities, vacuum etc., and on the record performance of our machines. (orig./WL)

Preliminary study on X-ray phase contrast imaging using synchrotron radiation facility

International Nuclear Information System (INIS)

Xiong Zhuang; Wang Jianhua; Yu Yongqiang; Jiang Shiping; Chen Yang; Tian Yulian

2006-01-01

Objective: To study the methodology of X-ray phase contrast imaging using synchrotron radiation, and evaluate the quality of phase contrast images. Methods: Several experiments to obtain phase contrast images and absorption contrast images of various biological samples were conducted in Beijing Synchrotron Radiation Facility (BSRF), and then these images were interpreted to find out the difference between the two kinds of imaging methods. Results: Satisfactory phase contrast images of these various samples were obtained, and the quality of these images was superior to that obtained with absorption contrast imaging. The phase contrast formation is based on the phenomenon of fresnel diffraction which transforms phase shifts into intensity variations upon a simple act of free-space propagation, so it requires highly coherent X-rays and appropriate distance between sample and detector. This method of imaging is very useful in imaging of low-absorption objects or objects with little absorption variation, and its resolution is far higher than that of the conventional X-ray imaging. The photographs obtained showed very fine inner microstructure of the biological samples, and the smallest microstructure to be distinguished is within 30-40 μm. There is no doubt that phase contrast imaging has a practical applicability in medicine. Moreover, it improves greatly the efficiency and the resolution of the existing X-ray diagnostic techniques. Conclusions: X-ray phase contrast imaging can be performed with synchrotron radiation source and has some advantages over the conventional absorption contrast imaging. (authors)

New theoretical results in synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Bagrov, V.G. [Tomsk State University, Lenin Avenue 36, 634050 Tomsk (Russian Federation)]. E-mail: bagrov@phys.tsu.ru; Gitman, D.M. [Instituto de Fisica, Universidade de Sao Paulo, C.P. 66318, 05315-970 Sao Paulo, SP (Brazil); Tlyachev, V.B. [Tomsk Institute of High Current Electronics, Akademicheskiy Avenue 4, Tomsk (Russian Federation); Jarovoi, A.T. [Tomsk State University, Lenin Avenue 36, 634050 Tomsk (Russian Federation)

2005-11-15

One of the remarkable features of the relativistic electron synchrotron radiation is its concentration in small angle {delta}{approx}1/{gamma} (here {gamma}-relativistic factor: {gamma}=E/mc{sup 2}, E - energy, m - electron rest mass, c - light velocity) near rotation orbit plane [V.G. Bagrov, V.A. Bordovitsyn, V.G. Bulenok, V. Ya. Epp, Kinematical projection of pulsar synchrotron radiation profiles, in: Proceedings of IV ISTC Scientific Advisory Commitee Seminar on Basic Science in ISTC Aktivities, Akademgorodok, Novosibirsk, April 23-27, 2001, p. 293-300]. This theoretically predicted and experimentally confirmed feature is peculiar to total (spectrum summarized) radiating intensity. This angular distribution property has been supposed to be (at least qualitatively) conserved and for separate spectrum synchrotron radiation components. In the work of V.G. Bagrov, V.A. Bordovitsyn, V. Ch. Zhukovskii, Development of the theory of synchrotron radiation and related processes. Synchrotron source of JINR: the perspective of research, in: The Materials of the Second International Work Conference, Dubna, April 2-6, 2001, pp. 15-30 and in Angular dependence of synchrotron radiation intensity. http://lanl.arXiv.org/abs/physics/0209097, it is shown that the angular distribution of separate synchrotron radiation spectrum components demonstrates directly inverse tendency - the angular distribution deconcentration relatively the orbit plane takes place with electron energy growth. The present work is devoted to detailed investigation of this situation. For exact quantitative estimation of angular concentration degree of synchrotron radiation the definition of radiation effective angle and deviation angle is proposed. For different polarization components of radiation the dependence of introduced characteristics was investigated as a functions of electron energy and number of spectrum component.

High-pressure phases of uranium monophosphide studied by synchrotron x-ray diffraction

DEFF Research Database (Denmark)

Olsen, J. Staun; Gerward, Leif; Benedict, U.

1988-01-01

X-ray diffraction studies have been performed on UP powder for pressures up to 51 GPa using synchrotron radiation and a diamond-anvil cell. At ambient pressure UP has the rocksalt structure. The bulk modulus has been determined to B0=102(4) GPa and its pressure derivative to B0’=4.0(8). The cubic...

Spin dynamics in electron synchrotrons; Spindynamik in Elektronensynchrotronen

Energy Technology Data Exchange (ETDEWEB)

Schmidt, Jan Felix

2017-07-14

Providing spin polarized particle beams with circular accelerators requires the consideration of depolarizing resonances which may significantly reduce the desired degree of polarization at specific beam energies. The corresponding spin dynamical effects are typically analyzed with numerical methods. In case of electron beams the influence of the emission of synchrotron radiation has to be taken into account. On short timescales, as in synchrotrons with a fast energy ramp or in damping rings, spin dynamics are investigated with spin tracking algorithms. This thesis presents the spin tracking code Polematrix as a versatile tool to study the impact of synchrotron radiation on spin dynamics. Spin tracking simulations have been performed based on the well established particle tracking code Elegant. The numerical studies demonstrate effects which are responsible for beam depolarization: Synchrotron side bands of depolarizing resonances and decoherence of spin precession. Polematrix can be utilized for any electron accelerator with minimal effort as it imports lattice files from the tracking programs MAD-X or Elegant. Polematrix has been published as open source software. Currently, the Electron Stretcher Accelerator ELSA at Bonn University is the only electron synchrotron worldwide providing a polarized beam. Integer and intrinsic depolarizing resonances are compensated with dedicated countermeasures during the fast energy ramp. Polarization measurements from ELSA demonstrate the particular spin dynamics of electrons and confirm the results of the spin tracking code Polematrix.

Study of the initial processes of radiation effects using synchrotron radiation

International Nuclear Information System (INIS)

Kobayashi, Katsumi

1990-01-01

Necessity for the research of production mechanisms of molecular damages in biological system and usefulness of monochromatic soft X-ray in these studies are described. Synchrotron radiation are introduced as a strong light source with continuous spectrum. Practically, it is the only light source in soft X-ray and vacuum UV region. Development of irradiation apparatus for radiation biology and recent results using various biological systems are reviewed. (author)

Study on alumina-alumina brazing for application in vacuum chambers of proton synchrotron

International Nuclear Information System (INIS)

Yadav, D.P.; Kaul, R.; Ganesh, P.; Shiroman, Ram; Tiwari, Pragya; Sridhar, R.; Kukreja, L.M.

2013-01-01

The paper describes an experimental study to standardize vacuum brazing process to obtain satisfactory high purity alumina brazed joints for application in rapid cycle proton synchrotron machine. Two different brazing routes, adopted for making alumina-alumina brazed joints, included (i) multi-step Mo-Mn metallization and brazing with BVAg-8 alloy and (ii) advanced single-step active brazing with CuSil-ABA alloy. Brazed alumina specimens, prepared by both the routes, yielded ultra high vacuum compatible, helium leak tight and bakeable joints. Active-brazed specimens exhibited satisfactory strength values in tensile and four-point bend tests. Metallized-brazed specimens, although exhibited relatively lower tensile strength than the targeted value, displayed satisfactory flexural strength in four-point bend test. The results of the study demonstrated that active brazing is the simple and cost effective alternative to conventional metallization route for producing satisfactory brazed joints for application in rapid cycle proton synchrotron machine. (author)

Materials science and technology by synchrotron radiation

International Nuclear Information System (INIS)

Chikawa, J.

1990-01-01

In the present paper, features of the Photon Factory, a facility for synchrotron research installed at the National Laboratory for High Energy Physics in Japan, are outlined, and then the impact of the advent of synchrotron radiation is discussed in relation to its outcome during the past seven years. Prospects for future development of synchrotron radiation are also presented. The facility consists of an injector linac to accelerate electrons up to 2.5 GeV and a ring to store the accelerated electrons in a closed orbit. In the Photon Factory, a 400m-long linac has been constructed for use as injector for both the Photon Factory and the TRISTAN electron-positron collider. The storage ring is operated at the same electron energy of 2.5 GeV. The present report also describes some applications of synchrotron radiation, focusing on spectroscopy (X-ray fluorescence technique and time-resolved X-ray absorption spectroscopy), diffraction and scattering (surface structure studies and protein crystallography), and photo-chemical processing. (N.K.)

Precision synchrotron radiation detectors

International Nuclear Information System (INIS)

Levi, M.; Rouse, F.; Butler, J.

1989-03-01

Precision detectors to measure synchrotron radiation beam positions have been designed and installed as part of beam energy spectrometers at the Stanford Linear Collider (SLC). The distance between pairs of synchrotron radiation beams is measured absolutely to better than 28 /mu/m on a pulse-to-pulse basis. This contributes less than 5 MeV to the error in the measurement of SLC beam energies (approximately 50 GeV). A system of high-resolution video cameras viewing precisely-aligned fiducial wire arrays overlaying phosphorescent screens has achieved this accuracy. Also, detectors of synchrotron radiation using the charge developed by the ejection of Compton-recoil electrons from an array of fine wires are being developed. 4 refs., 5 figs., 1 tab

TIME-RESOLVED INFRARED SPECTROSCOPY IN THE U121R BEAMLINE AT THE NSLS

International Nuclear Information System (INIS)

CARR, G.L.; LAVEIGNE, J.D.; LOBO, R.P.S.M.; REITZE, D.H.; TANNER, D.B.

1999-01-01

A facility for performing time-resolved infrared spectroscopy has been developed at the NSLS, primarily at beamline U12IR. The pulsed IR light from the synchrotron is used to perform pump-probe spectroscopy. The authors present here a description of the facility and results for the relaxation of photoexcitations in both a semiconductor and superconductor

Atomic and molecular photoelectron and Auger-electron-spectroscopy studies using synchrotron radiation

International Nuclear Information System (INIS)

Southworth, S.H.

1982-01-01

Electron spectroscopy, combined with synchrotron radiation, was used to measure the angular distributions of photoelectrons and Auger electrons from atoms and molecules as functions of photon energy. The branching ratios and partial cross sections were also measured in certain cases. By comparison with theoretical calculations, the experimental results are interpreted in terms of the characteristic electronic structure and ionization dynamics of the atomic or molecular sample. The time structure of the synchrotron radiation source was used to record time-of-flight (TOF) spectra of the ejected electrons. The double-angle-TOF method for the measurement of photoelectron angular distributions is discussed. This technique offers the advantages of increased electron collection efficiency and the elimination of certain systematic errors. An electron spectroscopy study of inner-shell photoexcitation and ionization of Xe, photoelectron angular distributions from H 2 and D 2 , and photoionization cross sections and photoelectron asymmetries of the valence orbitals of NO are reported

Synchrotron Elettra. Status and perspectives

International Nuclear Information System (INIS)

Remec, I.

1992-01-01

Synchrotron radiation and the possibilities for its applications are shortly presented. Elettra, the third generation synchrotron, now under construction in Trieste, Italy, is briefly described and its main characteristics are given. Current activities in Slovenia, related to Elettra, are presented. (author) [sl

The Synchrotron Topography Project (STP) at the National Synchrotron Light Source

International Nuclear Information System (INIS)

Bilello, J.C.; Hmelo, A.B.; Liu, J.M.; Herley, P.J.; Chen, H.; Birnbaum, H.K.; Illinois Univ., Urbana; Green, R.E. Jr.

1983-01-01

The collaborators have participated in the Synchrotron Topography Project (STP) which has designed and developed instrumentation for an X-ray topography station at the National Synchrotron Light Source (NSLS) at Brookhaven National Laboratory (BNL). The two principle instruments constructed consist of a White Beam Camera (WBC) and a Multiple Crystal Camera (MCC) with high planar collimation and wide area image coverage. It is possible to perform in situ studies in a versatile environmental chamber equipped with a miniature mechanical testing stage for both the WBC and MCC systems. Real-time video imaging plus a rapid feed cassette holder for high resolution photographic plates is available for recording topographs. Provisions are made for other types of photon detection as well as spectroscopy. The facilities for the entire station have been designed for remote operation using a LSI-11/23 plus suitable interfacing. These instruments will be described briefly and the current status of the program will be reviewed. (orig.)

Synchrotron radiation

International Nuclear Information System (INIS)

Hallmeier, K.H.; Meisel, A.; Ranft, J.

1982-01-01

The physical background and the properties of synchrotron radiation are described. The radiation offers many useful applications in the fields of spectroscopy and structural investigations. Some examples are given

Evaluating scintillator performance in time-resolved hard X-ray studies at synchrotron light sources.

Science.gov (United States)

Rutherford, Michael E; Chapman, David J; White, Thomas G; Drakopoulos, Michael; Rack, Alexander; Eakins, Daniel E

2016-05-01

The short pulse duration, small effective source size and high flux of synchrotron radiation is ideally suited for probing a wide range of transient deformation processes in materials under extreme conditions. In this paper, the challenges of high-resolution time-resolved indirect X-ray detection are reviewed in the context of dynamic synchrotron experiments. In particular, the discussion is targeted at two-dimensional integrating detector methods, such as those focused on dynamic radiography and diffraction experiments. The response of a scintillator to periodic synchrotron X-ray excitation is modelled and validated against experimental data collected at the Diamond Light Source (DLS) and European Synchrotron Radiation Facility (ESRF). An upper bound on the dynamic range accessible in a time-resolved experiment for a given bunch separation is calculated for a range of scintillators. New bunch structures are suggested for DLS and ESRF using the highest-performing commercially available crystal LYSO:Ce, allowing time-resolved experiments with an interframe time of 189 ns and a maximum dynamic range of 98 (6.6 bits).

Atomic physics at high brilliance synchrotron sources: Proceedings

International Nuclear Information System (INIS)

Berry, G.; Cowan, P.; Gemmell, D.

1994-08-01

This report contains papers on the following topics: present status of SPring-8 and the atomic physics undulator beamline; recent photoabsorption measurements in the rare gases and alkalis in the 3 to 15 keV proton energy region; atomic and molecular physics at LURE; experiments on atoms, ions and small molecules using the new generation of synchrotron radiation sources; soft x-ray fluorescence spectroscopy using tunable synchrotron radiation; soft x-ray fluorescence spectroscopy excited by synchrotron radiation: Inelastic and resonant scattering near threshold; outer-shell photoionization of ions; overview of the APS BESSRC beamline development; the advanced light source: Research opportunities in atomic and molecular physics; Photoionization of the Ba + ion by 4d shell excitation; decay dynamics of inner-shell excited atoms and molecules; absorption of atomic Ca, Cr, Mn and Cu; High-resolution photoelectron studies of resonant molecular photoionization; radiative and radiationless resonant raman scattering by synchrotron radiation; auger spectrometry of atoms and molecules; some thoughts of future experiments with the new generation of storage rings; Electron spectroscopy studies of argon K-shell excitation and vacancy cascades; ionization of atoms by high energy photons; ion coincidence spectroscopy on rare gas atoms and small molecules after photoexcitation at energies of several keV; an EBIS for use with synchrotron radiation photoionization of multiply charged ions and PHOBIS; gamma-2e coincidence measurements the wave of the future in inner-shell electron spectroscopy; recoil momentum spectroscopy in ion-atom and photon-atom collisions; a study of compton ionization of helium; future perspectives of photoionization studies at high photon energies; and status report on the advanced photon source. These papers have been cataloged separately elsewhere

Australian synchrotron light source - (boomerang)

International Nuclear Information System (INIS)

Boldeman, J.

2001-01-01

The Australian National Synchrotron Light Source - (Boomerang) is to be installed at the Monash University in Victoria. This report provides some background to the proposed facility and discusses aspects of a prospective design. Recently, significant effort was devoted to refining the in principle design and a lattice providing an emittance od 18 nm rad was obtained with a distributed dispersion in the straight section of 0.29m. Exhaustive studies have been made of the economic benefits that would accrue to Australia to Australia following the installation of this facility. This design is a refinement of the design concept presented to the SRI -2000, Berlin (Boldeman, Einfeld et al), to the meeting of the 4th Asian Forum and the Preliminary Design Study presented to the Australian Synchrotron Research Program

Identification of cellulose fibres belonging to Spanish cultural heritage using synchrotron high resolution X-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Herrera, L.K.; Justo, A.; Duran, A.; Haro, M.C.J. de; Franquelo, M.L.; Perez Rodriguez, J.L. [CSIC-Seville University, Materials Science Institute of Seville, Seville (Spain)

2010-05-15

A complete characterisation of fibres used in Spanish artwork is necessary to provide a complete knowledge of these natural fibres and their stage of degradation. Textile samples employed as painting supports on canvas and one sample of unprocessed plant material were chosen for this study. All the samples were investigated by synchrotron radiation X-ray diffraction (SR-XRD). Flax and cotton have the Cellulose I structure. The values of the crystalline index (CI) were calculated for both types of fibres. The structure of Cellulose IV was associated with the unprocessed plant material. The information obtained by SR-XRD was confirmed by laboratory techniques including scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR). (orig.)

Protein Data Bank Depositions from Synchrotron Sources

International Nuclear Information System (INIS)

Jiang, J.; Sweet, R.

2004-01-01

A survey and analysis of Protein Data Bank (PDB) depositions from international synchrotron radiation facilities, based on the latest released PDB entries, are reported. The results ( ) show that worldwide, every year since 1999, more than 50% of the deposited X-ray structures have used synchrotron facilities, reaching 75% by 2003. In this web-based database, all PDB entries among individual synchrotron beamlines are archived, synchronized with the weekly PDB release. Statistics regarding the quality of experimental data and the refined model for all structures are presented, and these are analysed to reflect the impact of synchrotron sources. The results confirm the common impression that synchrotron sources extend the size of structures that can be solved with equivalent or better quality than home sources

Limitations of heavy ion synchrotron acceleration for inertial fusion

International Nuclear Information System (INIS)

Berley, D.; Danby, G.T.

1977-01-01

The potential benefits from heavy ion inertial fusion motivate the rapid development of a program to test the principle. To define the program, accelerator parameters which have not hitherto been commonly considered must be studied interactively with basic questions of space charge limitations and charge exchange. Beam lifetime and power output efficiency may ultimately lead to a linear accelerator as the choice for an ignition device. For proof of principle, however, at power levels way beyond present inertial fusion experience, synchrotrons may have applicability at lower cost. The power and energy which can be delivered by the accelerating system to the reaction chamber are limited by space charge defocussing and intra beam charge exchange scattering, both of which are beam density dependent. These put constraints on linac injector energy, synchrotron aperture, synchrotron magnetic rigidity, acceleration time, ion species and charge to mass ratio. The accelerator system considered is classical. A linear accelerator injects into a synchrotron which accelerates the ion beam to the full energy delivered to the target. The maximum energy deliverable by a synchrotron is treated in section I. The targetting parameters and the energy gained through synchrotron acceleration completely determine the synchrotron aperture. These are discussed in sections II and III. The ion range in material is treated in section IV. The problem of intrabeam scattering is considered in section V. Finally, in section VI is a discussion of examples to meet specified goals

The profile of the electron beam in the PTB synchrotron, and its influence on radiometric measurements with synchrotron radiation

International Nuclear Information System (INIS)

Kaase, H.

1976-01-01

A simple method is described to determine the beam profile in an electron synchrotron; the measured results are compared with calculated values. Moreover, the influence of synchrotron- and betatron-oscillations on synchrotron radiation measurements is discussed, and a method is given to correct this. (orig.) [de

Support for Synchrotron Access by Environmental Scientists

International Nuclear Information System (INIS)

Daly, Michael; Madden, Andrew; Palumbo, Anthony; Qafoku, N.

2006-01-01

To support ERSP-funded scientists in all aspects of synchrotron-based research at the Advanced Photon Source (APS). This support comes in one or more of the following forms: (1) writing proposals to the APS General User (GU) program, (2) providing time at MRCAT/EnviroCAT beamlines via the membership of the Molecular Environmental Science (MES) Group in MRCAT/EnviroCAT, (3) assistance in experimental design and sample preparation, (4) support at the beamline during the synchrotron experiment, (5) analysis and interpretation of the synchrotron data, and (6) integration of synchrotron experimental results into manuscripts

Apparent temperature versus true temperature of silicon crystals as a function of their thickness using infrared measurements

International Nuclear Information System (INIS)

Smither, R.K.; Fernandez, P.B.

1993-01-01

The very high intensity x-ray beams that will be present at the Advanced Photon Source and other third generation synchrotron sources will require that the first optical element in the beamline and, possibly, the second optical element as well, be cooled to remove the heat deposited by the x-ray beam. In many of the beamlines this heat will be in the 1 to 5 kW range, and any failure of the cooling system will require a quick response from safety control circuits to shut off the beam before damage is done to the optical element. In many cases, this first optical element will be a silicon diffraction crystal. Viewing the surface of objects subjected to high heat fluxes with an infrared camera or infrared sensor has proved to be a very effective method for monitoring the magnitude and distribution of surface temperatures on the object. This approach has been quite useful in studies of cooling silicon crystals in monochromators subject to high heat loads. The main drawback to this method is that single crystals of silicon are partially transparent to the infrared radiation monitored in most infrared cameras. This means that the infrared radiation emitted from the surface contains a component that comes from the interior of the crystal and that the intensity of the emitted radiation and thus the apparent temperature of the surface of the crystal depends on the thickness of the crystal and the kind of coating on the back (and/or the front) of the crystal. The apparent temperature of the crystal increases as the crystal is made thicker. A series of experiments were performed at Argonne National Laboratory to calibrate the apparent surface temperature of the crystal as measured with an infrared camera as a function of the crystal thickness and the type of coating (if any) on the back side of the crystal. A number of examples are given for data taken in synchrotron experiments with high intensity x-ray beams

Pigmented Creatine Deposits in Amyotrophic Lateral Sclerosis Central Nervous System Tissues Identified by Synchrotron Fourier Transform Infrared Microspectroscopy and X-ray Fluorescence Spectromicroscopy

Energy Technology Data Exchange (ETDEWEB)

Kastyak, M.; Szczerbowska-Boruchowska, M; Adamek, D; Tomik, B; Lankosz, M; Gough, K

2010-01-01

Amyotrophic Lateral Sclerosis (ALS) is an untreatable, neurodegenerative disease of motor neurons characterized by progressive muscle atrophy, limb paralysis, dysarthria, dysphagia, dyspnae and finally death. Large motor neurons in ventral horns of spinal cord and motor nuclei in brainstem, large pyramidal neurons of motor cortex and/or large myelinated axons of corticospinal tracts are affected. In recent synchrotron Fourier Transform Infrared microspectroscopy (sFTIR) studies of ALS CNS autopsy tissue, we discovered a small deposit of crystalline creatine, which has a crucial role in energy metabolism. We have now examined unfixed, snap frozen, post-autopsy tissue sections of motor cortex, brain stem, spinal cord, hippocampus and substantia nigra from six ALS and three non-degenerated cases with FTIR and micro-X-ray fluorescence (XRF). Heterogeneous pigmented deposits were discovered in spinal cord, brain stem and motor neuron cortex of two ALS cases. The FTIR signature of creatine has been identified in these deposits and in numerous large, non-pigmented deposits in four of the ALS cases. Comparable pigmentation and creatine deposits were not found in controls or in ALS hippocampus and substantia nigra. Ca, K, Fe, Cu and Zn, as determined by XRF, were not correlated with the pigmented deposits; however, there was a higher incidence of hot spots (Ca, Zn, Fe and Cu) in the ALS cases. The identity of the pigmented deposits remains unknown, although the absence of Fe argues against both erythrocytes and neuromelanin. We conclude that elevated creatine deposits may be indicators of dysfunctional oxidative processes in some ALS cases.

Study of III-V semiconductor band structure by synchrotron photoemission

International Nuclear Information System (INIS)

Williams, G.P.; Cerrina, F.; Anderson, J.; Lapeyre, G.J.; Smith, R.J.; Hermanson, J.; Knapp, J.A.

1982-01-01

Angle-resolved synchrotron photoemission studies of six III-V semiconductors have been carried out. For emission normal to the (110) plane of these materials, peaks in the experimental spectra were identified with the bands involved in the transitions, and the critical point energies X 3 , X 5 , and Σ 1 /sup min/, were determined. The data indicate that k perpendicular is conserved in the transitions. Comparison of the data with theoretical bands permits an evaluation of k perpendicular associated with the experimentally observed transition, and from this information the bands were plotted out

Status report of the Cornell High Energy Synchrotron Radiation Source (CHESS)

International Nuclear Information System (INIS)

Batterman, B.W.

1980-01-01

The Wilson Laboratory at Cornell University has done pioneering work on the development of high energy synchrotrons. In the last decade the 12 GeV Wilson Synchrotron was the most energetic electron synchrotron in the world. In 1975 plans were formulated at the Wilson Laboratory to build a new electron-positron storage ring to cover the range from 4-8 GeV. The storage ring was to be constructed in the same tunnel as the present synchrotron and to use the latter as an injector for the ring. A novel injection feature was to be incorporated, namely, vernier phase compression. In this scheme, positron coalesence is to be performed by compressing a 30-60 bunch positron beam by tranferring individual bunches from the storage ring to the synchrotron and stacking back into the storage ring. This procedure takes advantage of the slight circumferential difference between the storage ring and the synchrotron. Positron beams of 10 mA have been achieved in CESR at the present time. The first colliding beam studies were performed in an October 1979 two-week running period at which time CHESS, the synchrotron radiation source associated with CESR, also had its first extended experience with synchrotron light. (orig.)

Protein Data Bank depositions from synchrotron sources.

Science.gov (United States)

Jiang, Jiansheng; Sweet, Robert M

2004-07-01

A survey and analysis of Protein Data Bank (PDB) depositions from international synchrotron radiation facilities, based on the latest released PDB entries, are reported. The results (http://asdp.bnl.gov/asda/Libraries/) show that worldwide, every year since 1999, more than 50% of the deposited X-ray structures have used synchrotron facilities, reaching 75% by 2003. In this web-based database, all PDB entries among individual synchrotron beamlines are archived, synchronized with the weekly PDB release. Statistics regarding the quality of experimental data and the refined model for all structures are presented, and these are analysed to reflect the impact of synchrotron sources. The results confirm the common impression that synchrotron sources extend the size of structures that can be solved with equivalent or better quality than home sources.

Synchrotron radiation in atomic physics

International Nuclear Information System (INIS)

Crasemann, B.

1998-01-01

Much of present understanding of atomic and molecular structure and dynamics was gained through studies of photon-atom interactions. In particular, observations of the emission, absorption, and scattering of X rays have complemented particle-collision experiments in elucidating the physics of atomic inner shells. Grounded on Max von Laue's theoretical insight and the invention of the Bragg spectrometer, the field's potential underwent a step function with the development of synchrotron-radiation sources. Notably current third-generation sources have opened new horizons in atomic and molecular physics by producing radiation of wide tunability and exceedingly high intensity and polarization, narrow energy bandwidth, and sharp time structure. In this review, recent advances in synchrotron-radiation studies in atomic and molecular science are outlined. Some tempting opportunities are surveyed that arise for future studies of atomic processes, including many-body effects, aspects of fundamental photon-atom interactions, and relativistic and quantum-electrodynamic phenomena. (author)

Helical magnetized wiggler for synchrotron radiation laser

International Nuclear Information System (INIS)

Wang Mei; Park, S.Y.; Hirshfield, J.L.

1999-01-01

A helical magnetized iron wiggler has been built for a novel infrared synchrotron radiation laser (SRL) experiment. The wiggler consists of four periods of helical iron structure immersed in a solenoid field. This wiggler is to impart transverse velocity to a prebunched 6 MeV electron beam, and thus to obtain a desired high orbit pitch ratio for the SRL. Field tapering at beam entrance is considered and tested on a similar wiggler. Analytic and simulated characteristics of wigglers of this type are discussed and the performance of the fabricated wigglers is demonstrated experimentally. A 4.7 kG peak field was measured for a 6.4 mm air gap and a 5.4 cm wiggler period at a 20 kG solenoid field. The measured helical fields compare favorably with the analytical solution. This type of helical iron wigglers has the potential to be scaled to small periods with strong field amplitude

Helical magnetized wiggler for synchrotron radiation laser

CERN Document Server

Wang Mei; Hirshfield, J L

1999-01-01

A helical magnetized iron wiggler has been built for a novel infrared synchrotron radiation laser (SRL) experiment. The wiggler consists of four periods of helical iron structure immersed in a solenoid field. This wiggler is to impart transverse velocity to a prebunched 6 MeV electron beam, and thus to obtain a desired high orbit pitch ratio for the SRL. Field tapering at beam entrance is considered and tested on a similar wiggler. Analytic and simulated characteristics of wigglers of this type are discussed and the performance of the fabricated wigglers is demonstrated experimentally. A 4.7 kG peak field was measured for a 6.4 mm air gap and a 5.4 cm wiggler period at a 20 kG solenoid field. The measured helical fields compare favorably with the analytical solution. This type of helical iron wigglers has the potential to be scaled to small periods with strong field amplitude.

Synchrotron based spallation neutron source concepts

International Nuclear Information System (INIS)

Cho, Y.

1998-01-01

During the past 20 years, rapid-cycling synchrotrons (RCS) have been used very productively to generate short-pulse thermal neutron beams for neutron scattering research by materials science communities in Japan (KENS), the UK (ISIS) and the US (IPNS). The most powerful source in existence, ISIS in the UK, delivers a 160-kW proton beam to a neutron-generating target. Several recently proposed facilities require proton beams in the MW range to produce intense short-pulse neutron beams. In some proposals, a linear accelerator provides the beam power and an accumulator ring compresses the pulse length to the required ∼ 1 micros. In others, RCS technology provides the bulk of the beam power and compresses the pulse length. Some synchrotron-based proposals achieve the desired beam power by combining two or more synchrotrons of the same energy, and others propose a combination of lower and higher energy synchrotrons. This paper presents the rationale for using RCS technology, and a discussion of the advantages and disadvantages of synchrotron-based spallation sources

The Dow Chemical Company's synchrotron radiation effort - A case history

International Nuclear Information System (INIS)

Bubeck, R.A.; Bare, S.R.; DeKoven, B.M.; Heaney, M.D.; Rudolf, P.R.

1994-01-01

Synchrotron radiation is used in a broad array of technologies to study everything from molecular orientation at interfaces, through the structure of active catalyst phases. It is also a key to understanding structure-property relationships and providing fundamental information in polymers, ceramics, and other materials. The Dow Synchrotron User group, formed in 1991, has developed a long-term plan for effective utilization of synchrotron technology. The current efforts at Brookhaven National Lab. and Cornell High Energy Synchrotron Source are examined, as will the long-term commitment at the Advanced Photon Source. Current examples included are in-situ studies of polymer processing, surface and interfaces characterization, and real-time deformation studies. The APS is one of only three open-quotes Third Generationclose quotes synchrotron sources that are planned world-wide, the others being in France and Japan. With a scheduled completion date of mid-1995, the APS has remained both on-budget and ahead-of-schedule since ground-breaking in the spring of 1990. The DuPont - Northwestern University - Dow Collaborative Access Team (DND-CAT) is the first CAT to successfully pass all the necessary hurdles before beamline construction can begin. Some of the goals of the DND-CAT program are mentioned, together with the strengths of this unique collaborative effort

Preliminary studies of the quickly pulsed synchrotron involved in the Beta-Beam project; Etudes preliminaires du synchrotron rapidement pulse du projet Beta-Beam

Energy Technology Data Exchange (ETDEWEB)

Lachaize, A

2007-07-01

This study presents a quickly-pulsed synchrotron able to accelerate He{sup 6} and Ne{sup 18} beams from 100 MeV/u till 3.5 GeV (proton equivalent) The accelerator is made up of 48 bending dipoles and 42 focusing quadrupoles. The design of the HF accelerating system, the bunch injection and the correction of errors in beam dynamics are dealt with.

Synchrotron radiation

International Nuclear Information System (INIS)

Helliwell, J.R.; Walker, R.P.

1985-01-01

A detailed account of the research work associated with the Synchrotron Radiation Source at Daresbury Laboratory, United Kingdom, in 1984/85, is presented in the Appendix to the Laboratory's Annual Report. (U.K.)

Investigation of carbonates in the Sutter's Mill meteorite grains with hyperspectral infrared imaging micro-spectroscopy

Science.gov (United States)

Yesiltas, Mehmet

2018-04-01

Synchrotron-based high spatial resolution hyperspectral infrared imaging technique provides thousands of infrared spectra with high resolution, thus allowing us to acquire detailed spatial maps of chemical molecular structures for many grains in short times. Utilizing this technique, thousands of infrared spectra were analyzed at once instead of inspecting each spectrum separately. Sutter's Mill meteorite is a unique carbonaceous type meteorite with highly heterogeneous chemical composition. Multiple grains from the Sutter's Mill meteorite have been studied using this technique and the presence of both hydrous and anhydrous silicate minerals have been observed. It is observed that the carbonate mineralogy varies from simple to more complex carbonates even within a few microns in the meteorite grains. These variations, the type and distribution of calcite-like vs. dolomite-like carbonates are presented by means of hyperspectral FTIR imaging spectroscopy with high resolution. Various scenarios for the formation of different carbonate compositions in the Sutter's Mill parent body are discussed.

Iron overload of human colon adenocarcinoma cells studied by synchrotron-based X-ray techniques

NARCIS (Netherlands)

Mihucz, Victor G.; Meirer, Florian; Polgári, Zsófia; Réti, Andrea; Pepponi, Giancarlo; Ingerle, Dieter; Szoboszlai, Norbert; Streli, Christina

2016-01-01

Fast- and slow-proliferating human adenocarcinoma colorectal cells, HT-29 and HCA-7, respectively, overloaded with transferrin (Tf), Fe(III) citrate, Fe(III) chloride and Fe(II) sulfate were studied by synchrotron radiation total-reflection X-ray spectrometry (TXRF), TXRF-X-ray absorption near edge

Synchrotron X-ray fluorescence studies of a bromine-labelled cyclic RGD peptide interacting with individual tumor cells

International Nuclear Information System (INIS)

Sheridan, Erin J.; Austin, Christopher J. D.; Aitken, Jade B.; Vogt, Stefan; Jolliffe, Katrina A.; Harris, Hugh H.; Rendina, Louis M.

2013-01-01

The first example of synchrotron X-ray fluorescence imaging of cultured mammalian cells in cyclic peptide research is reported. The study reports the first quantitative analysis of the incorporation of a bromine-labelled cyclic RGD peptide and its effects on the biodistribution of endogenous elements (for example, K and Cl) within individual tumor cells. The first example of synchrotron X-ray fluorescence imaging of cultured mammalian cells in cyclic peptide research is reported. The study reports the first quantitative analysis of the incorporation of a bromine-labelled cyclic RGD peptide and its effects on the biodistribution of endogenous elements (for example, K and Cl) within individual tumor cells

Fiber structural analysis by synchrotron radiation

CERN Document Server

Kojima, J I; Kikutani, T

2003-01-01

Topics of fiber structural analysis by synchrotron radiation are explained. There are only three synchrotron radiation facilities in the world, SPring-8 (Super Photon ring-8) in Japan, APS (Advanced Photon Source) in U.S.A. and ESRF (European Synchrotron Radiation Facility) in France. Online measurement of melt spinning process of PET and Nylon6 is explained in detail. Polypropylene and PBO (poly-p-phenylenebenzobisoxazole) was measured by WAXD (Wide Angle X-ray Diffraction)/SAXS (Small Angle X-ray Scattering) at the same time. Some examples of measure of drawing process of fiber are described. The structure formation process of spider's thread was measured. Micro beam of X-ray of synchrotron facility was improved and it attained to 65nm small angle resolving power by 10 mu m beamsize. (S.Y.)

Hut clusters on Ge(001) surfaces studied by STM and synchrotron X-ray diffraction

DEFF Research Database (Denmark)

Nielsen, M.; Smilgies, D.-M.; Feidenhans'l, R.

1996-01-01

Nanoscale hut clusters formed on Ge(001) surfaces by depositing one monolayer of indium and annealing at temperatures between 350 and 500 degrees C were studied by scanning tunnelling microscopy and synchrotron X-ray diffraction. It was found that the hut clusters form regular arrays over...

Coherent synchrotron radiation by an electron linear accelerator

International Nuclear Information System (INIS)

Nakazato, T.; Oyamada, M.; Niimura, N.

1990-01-01

Coherent effects in synchrotron radiation (SR) have been observed for the first time from 180 MeV short electron bunches of 1.7 mm using the Tohoku 300 MeV Linac. The intensity of the coherent SR was about 10 5 times as strong as that of incoherent SR at wavelengths of 0.33 to 2.0 mm. This enhancement factor roughly corresponds to the number of electrons in a bunch. The SR intensity showed a quadratic dependence on the electron beam current. The radiation was mainly polarized in the orbital plane. The possibility of induced rf in a vacuum chamber was excluded experimentally. An electron linear accelerator will be applied to a strong light source from infrared to millimeter wavelengths instead of the storage rings. The bunch length of shorter than 1 mm can be observed by the spectrum measurement of coherent SR. (author)

Atomic collision experiments using pulsed synchrotron radiation

International Nuclear Information System (INIS)

Arikawa, Tatsuo; Watanabe, Tsutomu.

1982-01-01

High intensity and continuous nature of the synchrotron radiation are the properties that are fundamentally important for studies of some atomic collision experiments, and many processes have been investigated by using these characteristics. However, so far the property that the radiation is highly polarized and pulsed in time has not been exploited significantly in atomic physics. As an example of the atomic processes relevant to such polarized and pulsed features of the synchrotron radiation, collisions involving optically-allowed excited atoms and molecules will be presented. (author)

Research using synchrotron radiation at the National Synchrotron Light Source

International Nuclear Information System (INIS)

Thomlinson, W.

1982-01-01

The National Synchrotron Light Source (NSLS) is now becoming operational with synchrotron radiation experiments beginning on the 700 MeV VUV electron storage ring. Commissioning of the 2.5 GeV x-ray storage ring has also begun with the experimental program expected to begin in 1983. The current status of the experimental program and instrumentation and the plans for future developments, will be discussed. Although some early results have been obtained on VUV beam lines no attempt will be made in this paper to describe them. Instead, an overview of the beam line characteristics will be given, with an indication of those already operational. In the oral presentation some initial experimental results will be discussed

Synchrotron radiation in material science

International Nuclear Information System (INIS)

Zanotto, E.D.

1983-01-01

A brief review on the several experimental techniques (XRD, SAXS, EXAFS, IRRS, etc...) which, utilizing of synchrotron radiation can be applied in glass structural studies, is presented. The major part of these techniques can be also used for studies of other materials such as polymers, metals, etc... (L.C.) [pt

The application of synchrotron radiation to X-ray lithography

International Nuclear Information System (INIS)

Spiller, E.; Eastman, D.E.; Feder, R.; Grobman, W.D.; Gudat, W.; Topalian, J.

1976-06-01

Synchrotron radiation from the German electron synchrotron DESY in Hamburg has been used for X-ray lithograpgy. Replications of different master patterns (for magnetic bubble devices, fresnel zone plates, etc.) were made using various wavelengths and exposures. High quality lines down to 500 A wide have been reproduced using very soft X-rays. The sensitivities of X-ray resists have been evaluated over a wide range of exposures. Various critical factors (heating, radiation damage, etc.) involved with X-ray lithography using synchrotron radiation have been studied. General considerations of storage ring sources designed as radiation sources for X-ray lithography are discussed, together with a comparison with X-ray tube sources. The general conclusion is that X-ray lithography using synchrotron radiation offers considerable promise as a process for forming high quality sub-micron images with exposure times as short as a few seconds. (orig.) [de

Development of intense terahertz coherent synchrotron radiation at KU-FEL

Energy Technology Data Exchange (ETDEWEB)

Sei, Norihiro, E-mail: sei.n@aist.go.jp [Research Institute for Measurement and Analytical Instrumentation, National Institute of Advanced Industrial Science and Technology, 1-1-1 Umezono, Umezono, Tsukuba, Ibaraki 305-8568 (Japan); Zen, Heishun; Ohgaki, Hideaki [Institute for Advanced Energy, Kyoto University, Gokasho, Uji, Kyoto 611-0011 (Japan)

2016-10-01

We produced intense coherent synchrotron radiation (CSR) in the terahertz (THz) region using an S-band linac at the Kyoto University Free Electron Laser (KU-FEL), which is a mid-infrared free-electron laser facility. The CSR beam was emitted from short-pulse electron bunches compressed by a 180° arc, and was transferred to air at a large solid angle of 0.10 rad. The measured CSR energy was 55 μJ per 7 μs macropulse, and KU-FEL was one of the most powerful CSR sources in normal conducting linear accelerator facilities. The CSR spectra were measured using an uncooled pyroelectric detector and a Michelson-type interferometer designed specifically for the KU-FEL electron beam, and had a maximum at a frequency of 0.11 THz. We found that adjusting the energy slit enhanced the CSR energy and shortened the electron beam bunch length in the CSR spectra measurements. Our results demonstrated that the efficient use of the energy slit can help improve the characteristics of CSR. - Highlights: • We have developed intense coherent synchrotron radiation (CSR) at KU-FEL. • The elevation angle of the CSR was correctly measured by a new technique. • The CSR power extracted to the air was 55 μJ per 7 μs macropulse. • It was demonstrated that an energy slit was effective to improve the CSR properties.

Development of intense terahertz coherent synchrotron radiation at KU-FEL

International Nuclear Information System (INIS)

Sei, Norihiro; Zen, Heishun; Ohgaki, Hideaki

2016-01-01

We produced intense coherent synchrotron radiation (CSR) in the terahertz (THz) region using an S-band linac at the Kyoto University Free Electron Laser (KU-FEL), which is a mid-infrared free-electron laser facility. The CSR beam was emitted from short-pulse electron bunches compressed by a 180° arc, and was transferred to air at a large solid angle of 0.10 rad. The measured CSR energy was 55 μJ per 7 μs macropulse, and KU-FEL was one of the most powerful CSR sources in normal conducting linear accelerator facilities. The CSR spectra were measured using an uncooled pyroelectric detector and a Michelson-type interferometer designed specifically for the KU-FEL electron beam, and had a maximum at a frequency of 0.11 THz. We found that adjusting the energy slit enhanced the CSR energy and shortened the electron beam bunch length in the CSR spectra measurements. Our results demonstrated that the efficient use of the energy slit can help improve the characteristics of CSR. - Highlights: • We have developed intense coherent synchrotron radiation (CSR) at KU-FEL. • The elevation angle of the CSR was correctly measured by a new technique. • The CSR power extracted to the air was 55 μJ per 7 μs macropulse. • It was demonstrated that an energy slit was effective to improve the CSR properties.

The 1.3GeV electron synchrotron INS-ES

International Nuclear Information System (INIS)

Yoshida, Katsuhide

2006-01-01

The 1.3GeV electron synchrotron at Institute for Nuclear Study, University of Tokyo (INS-ES) is the first high energy accelerator in Japan. It was constructed during 1956-1961 and shut down in 1999. It had played key roles in originating high energy physics in Japan. Based upon accelerator technologies developed in the construction and the operation of INS-ES, a 12 GeV proton synchrotron was built at KEK. INS-ES was also the base to promote synchrotron radiation science in Japan and to establish Photon Factory at KEK. After 1980, it was operated mainly to deliver tagged photon beam for high energy nuclear physics. (K.Y.)

Atoms, molecules, clusters and synchrotron radiation

International Nuclear Information System (INIS)

Kui Rexi; Ju Xin

1995-01-01

The importance of synchrotron radiation, especially the third generation synchrotron radiation light source, in atomic, molecular and cluster physics is discussed and some views are presented on new methods which may become available for research in the above fields

Synchrotron-Radiation Induced X-Ray Emission (SRIXE)

Energy Technology Data Exchange (ETDEWEB)

Jones, Keith W.

1999-09-01

and increase in scientific use can be maintained for the synchrotron x-ray source. A short summary of the present state of the synchrotron radiation-induced x-ray emission (SRIXE) method is presented here. Basically, SRIXE experiments can include any that depend on the detection. of characteristic x-rays produced by the incident x-ray beam born the synchrotron source as they interact with a sample. Thus, experiments done to measure elemental composition, chemical state, crystal, structure, and other sample parameters can be considered in a discussion of SRIXE. It is also clear that the experimentalist may well wish to use a variety of complementary techniques for study of a given sample. For this reason, discussion of computed microtomography (CMT) and x-ray diffraction is included here. It is hoped that this present discussion will serve as a succinct introduction to the basic ideas of SRIXE for those not working in the field and possibly help to stimulate new types of work by those starting in the field as well as by experienced practitioners of the art. The topics covered include short descriptions of (1) the properties of synchrotron radiation, (2) a description of facilities used for its production, (3) collimated microprobe, (4) focused microprobes, (5) continuum and monoenergetic excitation, (6) detection limits, (7) quantitation, (8) applications of SRIXE, (9) computed microtomography (CMT), and (10)chemical speciation using x-ray absorption near-edge structure (XANES) and extended x-ray absorption fine structure (EXAFS). An effort has been made to cite a wide variety of work from different laboratories to show the vital nature of the field.

Synchrotron-Radiation Induced X-Ray Emission (SRIXE)

International Nuclear Information System (INIS)

Jones, Keith W.

1999-01-01

and increase in scientific use can be maintained for the synchrotron x-ray source. A short summary of the present state of the synchrotron radiation-induced x-ray emission (SRIXE) method is presented here. Basically, SRIXE experiments can include any that depend on the detection. of characteristic x-rays produced by the incident x-ray beam born the synchrotron source as they interact with a sample. Thus, experiments done to measure elemental composition, chemical state, crystal, structure, and other sample parameters can be considered in a discussion of SRIXE. It is also clear that the experimentalist may well wish to use a variety of complementary techniques for study of a given sample. For this reason, discussion of computed microtomography (CMT) and x-ray diffraction is included here. It is hoped that this present discussion will serve as a succinct introduction to the basic ideas of SRIXE for those not working in the field and possibly help to stimulate new types of work by those starting in the field as well as by experienced practitioners of the art. The topics covered include short descriptions of (1) the properties of synchrotron radiation, (2) a description of facilities used for its production, (3) collimated microprobe, (4) focused microprobes, (5) continuum and monoenergetic excitation, (6) detection limits, (7) quantitation, (8) applications of SRIXE, (9) computed microtomography (CMT), and (10)chemical speciation using x-ray absorption near-edge structure (XANES) and extended x-ray absorption fine structure (EXAFS). An effort has been made to cite a wide variety of work from different laboratories to show the vital nature of the field

Synchrotron-based intra-venous K-edge digital subtraction angiography in a pig model: A feasibility study

International Nuclear Information System (INIS)

Schueltke, Elisabeth; Fiedler, Stefan; Nemoz, Christian; Ogieglo, Lissa; Kelly, Michael E.; Crawford, Paul; Esteve, Francois; Brochard, Thierry; Renier, Michel; Requardt, Herwig; Le Duc, Geraldine; Juurlink, Bernhard; Meguro, Kotoo

2010-01-01

Background: K-edge digital subtraction angiography (KEDSA) combined with the tunability of synchrotron beam yields an imaging technique that is highly sensitive to low concentrations of contrast agents. Thus, contrast agent can be administered intravenously, obviating the need for insertion of a guided catheter to deliver a bolus of contrast agent close to the target tissue. With the high-resolution detectors used at synchrotron facilities, images can be acquired at high spatial resolution. Thus, the KEDSA appears particularly suited for studies of neurovascular pathology in animal models, where the vascular diameters are significantly smaller than in human patients. Materials and methods: This feasibility study was designed to test the suitability of KEDSA after intravenous injection of iodine-based contrast agent for use in a pig model. Four adult male pigs were used for our experiments. Neurovascular angiographic images were acquired using KEDSA with a solid state Germanium (Ge) detector at the European Synchrotron Radiation Facility (ESRF) in Grenoble, France. Results: After intravenous injection of 0.9 ml/kg iodinated contrast agent (Xenetix), the peak iodine concentrations in the internal carotid and middle cerebral arteries reached 35 mg/ml. KEDSA images in radiography mode allowed the visualization of intracranial arteries of less than 1.5 mm diameter.

Synchrotron-based intra-venous K-edge digital subtraction angiography in a pig model: a feasibility study.

Science.gov (United States)

Schültke, Elisabeth; Fiedler, Stefan; Nemoz, Christian; Ogieglo, Lissa; Kelly, Michael E; Crawford, Paul; Esteve, Francois; Brochard, Thierry; Renier, Michel; Requardt, Herwig; Le Duc, Geraldine; Juurlink, Bernhard; Meguro, Kotoo

2010-03-01

K-edge digital subtraction angiography (KEDSA) combined with the tunability of synchrotron beam yields an imaging technique that is highly sensitive to low concentrations of contrast agents. Thus, contrast agent can be administered intravenously, obviating the need for insertion of a guided catheter to deliver a bolus of contrast agent close to the target tissue. With the high-resolution detectors used at synchrotron facilities, images can be acquired at high spatial resolution. Thus, the KEDSA appears particularly suited for studies of neurovascular pathology in animal models, where the vascular diameters are significantly smaller than in human patients. This feasibility study was designed to test the suitability of KEDSA after intravenous injection of iodine-based contrast agent for use in a pig model. Four adult male pigs were used for our experiments. Neurovascular angiographic images were acquired using KEDSA with a solid state Germanium (Ge) detector at the European Synchrotron Radiation Facility (ESRF) in Grenoble, France. After intravenous injection of 0.9 ml/kg iodinated contrast agent (Xenetix), the peak iodine concentrations in the internal carotid and middle cerebral arteries reached 35 mg/ml. KEDSA images in radiography mode allowed the visualization of intracranial arteries of less than 1.5mm diameter. Copyright 2009 Elsevier Ireland Ltd. All rights reserved.

Synchrotron-based intra-venous K-edge digital subtraction angiography in a pig model: A feasibility study

Energy Technology Data Exchange (ETDEWEB)

Schueltke, Elisabeth [Departments of Surgery, University of Saskatchewan, Saskatoon, SK (Canada); Anatomy and Cell Biology, University of Saskatchewan, Saskatoon, SK (Canada); Department of Neurological Sciences, Walton Medical Centre, University of Liverpool, Liverpool L97 LJ (United Kingdom)], E-mail: e.schultke@usask.ca; Fiedler, Stefan [European Molecular Biology Laboratory (EMBL), Nottkestrasse 85, 22603 Hamburg (Germany); Nemoz, Christian [European Synchrotron Radiation Facility (ESRF), 6 rue Horowitz, 38043 Grenoble (France); Ogieglo, Lissa [Departments of Surgery, University of Saskatchewan, Saskatoon, SK (Canada); Kelly, Michael E. [Departments of Surgery, University of Saskatchewan, Saskatoon, SK (Canada); Department of Neurosurgery, Section of Cerebrovascular and Endovascular Neurosurgery, Cleveland Clinic, 9500 Euclid Avenue, Cleveland, OH (United States); Crawford, Paul [Royal Veterinary College, Hawkshead Lane, North Mymms, Hatfield, Herfordshire AL9 7TA (United Kingdom); Esteve, Francois [INSERM U836-ESRF, 6 rue Horowitz, 38043 Grenoble (France); Brochard, Thierry; Renier, Michel; Requardt, Herwig; Le Duc, Geraldine [European Synchrotron Radiation Facility (ESRF), 6 rue Horowitz, 38043 Grenoble (France); Juurlink, Bernhard [Anatomy and Cell Biology, University of Saskatchewan, Saskatoon, SK (Canada); Meguro, Kotoo [Departments of Surgery, University of Saskatchewan, Saskatoon, SK (Canada)

2010-03-15

Background: K-edge digital subtraction angiography (KEDSA) combined with the tunability of synchrotron beam yields an imaging technique that is highly sensitive to low concentrations of contrast agents. Thus, contrast agent can be administered intravenously, obviating the need for insertion of a guided catheter to deliver a bolus of contrast agent close to the target tissue. With the high-resolution detectors used at synchrotron facilities, images can be acquired at high spatial resolution. Thus, the KEDSA appears particularly suited for studies of neurovascular pathology in animal models, where the vascular diameters are significantly smaller than in human patients. Materials and methods: This feasibility study was designed to test the suitability of KEDSA after intravenous injection of iodine-based contrast agent for use in a pig model. Four adult male pigs were used for our experiments. Neurovascular angiographic images were acquired using KEDSA with a solid state Germanium (Ge) detector at the European Synchrotron Radiation Facility (ESRF) in Grenoble, France. Results: After intravenous injection of 0.9 ml/kg iodinated contrast agent (Xenetix), the peak iodine concentrations in the internal carotid and middle cerebral arteries reached 35 mg/ml. KEDSA images in radiography mode allowed the visualization of intracranial arteries of less than 1.5 mm diameter.

RF control system of the HIMAC synchrotron

International Nuclear Information System (INIS)

Kanazawa, M.; Sato, K.; Itano, A.

1992-01-01

An RF control system of the HIMAC synchrotron has been constructed. In this control system we have adopted a digital feed back system with a digital synthesizer (DS). Combining a high power system, performance of the control system have been tested in a factory (Toshiba) with a simulator circuit of the synchrotron oscillation. Following this test, We had beam acceleration test with this control system at TARN-II in INS (Institute for Nuclear Study, University of Tokyo). This paper describes the RF control system and its tested results. (author)

Present status and future plans at INS 1.3 GeV electron synchrotron

International Nuclear Information System (INIS)

Yoshida, K.

1984-01-01

The 1.3 GeV electron synchrotron at the Institute for Nuclear Study, University of Tokyo, was completed in 1961, and it was the first accelerator in Japan that was able to be used for the study on particle physics. The brief chronicle is shown. One of the purposes to construct the electron synchrotron was to train accelerator physicists for the next big project of building a high energy proton synchrotron. This project led to the foundation of the National Laboratory for High Energy Physics, and the Photon Factory was completed in 1982 there. The electron synchrotron has been continuously operated for 22 years. Meanwhile, the major components such as the injector linac, the vacuum system and the of acceleration system were renewed. By these improvement, the beam intensity and stability of the synchrotron were much improved. The circulating current is now 160 mA, and the number of accelerated electrons is 2.5 x 10 12 /sec. These are the highest values in the world. The parameters of the present synchrotron and the operational status are shown. There are five beam channels, that is, bremsstrahlung channel, tagged photon beam, fast extracted electron beam, synchrotron light channel and detector test channel. The recent activities with the INS electron synchrotron and the future plans are summarized. (Kako, I.)

Medical applications with synchrotron radiation in Japan

Energy Technology Data Exchange (ETDEWEB)

Takeda, T.; Itai, Y. [Univ. of Tsukuba, Inst. of Clinical Medicine, Tsukuba (Japan); Hyodo, K.; Ando, M. [KEK, Tsukuba (Japan); Akatsuka, T. [Yamagata Univ., Faculty of Engineering, Yamagata (Japan); Uyama, C. [National Cardiovascular Centre, Suita (Japan)

1998-05-01

In Japan, various medical applications of synchrotron X-ray imaging, such as angiography, monochromatic X-ray computed tomography (CT), radiography and radiation therapy, are being developed. In particular, coronary arteriography (CAG) is quite an important clinical application of synchrotron radiation. Using a two-dimensional imaging method, the first human intravenous CAG was carried out at KEK in May 1996; however, further improvements of image quality are required in clinical practice. On the other hand, two-dimensional aortographic CAG revealed canine coronary arteries as clearly as those on selective CAG, and coronary arteries less than 0.2 mm in diameter. Among applications of synchrotron radiation to X-ray CT, phase-contrast X-ray CT and fluorescent X-ray CT are expected to be very interesting future applications of synchrotron radiation. For actual clinical applications of synchrotron radiation, a medical beamline and a laboratory are now being constructed at SPring-8 in Harima. 55 refs.

A study on radiation shielding and safety analysis for a synchrotron radiation beamline

International Nuclear Information System (INIS)

Asano, Yoshihiro

2001-03-01

Methods of shielding design and safety analysis are presented for a beam-line of synchrotron radiation. This paper consists of the shielding and safety study of synchrotron radiation with extremely intense and low energy photon below several hundreds keV, and the study for the behavior of remarkable high-energy photons up to 8 GeV, which can creep into beam-lines. A new shielding design code, STAC8 was developed to estimate the leakage dose outside the beam line hutch (an enclosure of the beam, optical elements or experimental instruments) easily and quickly with satisfactory accuracy. The code can calculate consistently from sources of synchrotron radiation to dose equivalent outside hutches with considering the build up effect and polarization effect. Validity of the code was verified by comparing its calculations with those of Monte Carlo simulations and measurement results of the doses inside the hutch of the BL14C of Photon Factory in the High Energy Accelerator Research Organization (KEK), showing good agreements. The shielding design calculations using STAC8 were carried out to apply to the practical beam-lines with the considering polarization effect and clarified the characteristics of the typical beam-line of the third generation synchrotron radiation facility, SPring-8. In addition, the shielding calculations were compared with the measurement outside the shield wall of the bending magnet beam-line of SPring-8, and showed fairly good agreement. The new shielding problems, which have usually been neglected in shielding designs for existing synchrotron radiation facilities, are clarified through the analysis of the beam-line shielding of SPring-8. The synchrotron radiation from the SPring-8 has such extremely high-intensity involving high energy photons that the scattered synchrotron radiation from the concrete floor of the hutch, the ground shine, causes a seriously high dose. The method of effective shielding is presented. For the estimation of the gas

A study on radiation shielding and safety analysis for a synchrotron radiation beamline

Energy Technology Data Exchange (ETDEWEB)

Asano, Yoshihiro [Japan Atomic Energy Research Inst., Kansai Research Establishment, Synchrotron Radiation Research Center, Mikazuhi, Hyogo (Japan)

2001-03-01

Methods of shielding design and safety analysis are presented for a beam-line of synchrotron radiation. This paper consists of the shielding and safety study of synchrotron radiation with extremely intense and low energy photon below several hundreds keV, and the study for the behavior of remarkable high-energy photons up to 8 GeV, which can creep into beam-lines. A new shielding design code, STAC8 was developed to estimate the leakage dose outside the beam line hutch (an enclosure of the beam, optical elements or experimental instruments) easily and quickly with satisfactory accuracy. The code can calculate consistently from sources of synchrotron radiation to dose equivalent outside hutches with considering the build up effect and polarization effect. Validity of the code was verified by comparing its calculations with those of Monte Carlo simulations and measurement results of the doses inside the hutch of the BL14C of Photon Factory in the High Energy Accelerator Research Organization (KEK), showing good agreements. The shielding design calculations using STAC8 were carried out to apply to the practical beam-lines with the considering polarization effect and clarified the characteristics of the typical beam-line of the third generation synchrotron radiation facility, SPring-8. In addition, the shielding calculations were compared with the measurement outside the shield wall of the bending magnet beam-line of SPring-8, and showed fairly good agreement. The new shielding problems, which have usually been neglected in shielding designs for existing synchrotron radiation facilities, are clarified through the analysis of the beam-line shielding of SPring-8. The synchrotron radiation from the SPring-8 has such extremely high-intensity involving high energy photons that the scattered synchrotron radiation from the concrete floor of the hutch, the ground shine, causes a seriously high dose. The method of effective shielding is presented. For the estimation of the gas

Experience with synchrotron radiation sources

International Nuclear Information System (INIS)

Krinsky, S.

1987-01-01

The development of synchrotron radiation sources is discussed, emphasizing characteristics important for x-ray microscopy. Bending magnets, wigglers and undulators are considered as sources of radiation. Operating experience at the national Synchrotron Light Source on the VUV and XRAY storage rings is reviewed, with particular consideration given to achieved current and lifetime, transverse bunch dimensions, and orbit stability. 6 refs., 3 figs

Stanford Synchrotron Radiation Light Source (SSRL)

Data.gov (United States)

Federal Laboratory Consortium — The SSRL at SLAC National Accelerator Laboratory was built in 1974 to take and use for synchrotron studies the intense x-ray beams from the SPEAR storage ring that...

Electric field detection of coherent synchrotron radiation in a storage ring generated using laser bunch slicing

International Nuclear Information System (INIS)

Katayama, I.; Shimosato, H.; Bito, M.; Furusawa, K.; Adachi, M.; Zen, H.; Kimura, S.; Katoh, M.; Shimada, M.; Yamamoto, N.; Hosaka, M.; Ashida, M.

2012-01-01

The electric field of coherent synchrotron radiation (CSR) generated by laser bunch slicing in a storage ring has been detected by an electro-optic sampling method. The gate pulses for sampling are sent through a large-mode-area photonic-crystal fiber. The observed electric field profile of the CSR is in good agreement with the spectrum of the CSR observed using Fourier transform far-infrared spectrometry, indicating good phase stability in the CSR. The longitudinal density profiles of electrons modulated by laser pulses were evaluated from the electric field profile.

Coherence Inherent in an Incoherent Synchrotron Radio Source ...

Indian Academy of Sciences (India)

It is well known that synchrotron radiation mechanism does not allow MASER type coherent emission (Pacholczyk 1970). Here we show that coherence can naturally occur in a synchrotron ... cally thick region (Fig. 1), then divides the synchrotron spectrum into an incoherent. 1A thin flat circular unleavened Indian bread.

Synchrotron light sources in developing countries

Science.gov (United States)

Mtingwa, Sekazi K.; Winick, Herman

2018-03-01

We discuss the role that synchrotron light sources, such as SESAME, could play in improving the socioeconomic conditions in developing countries. After providing a brief description of a synchrotron light source, we discuss the important role that they played in the development of several economically emerging countries. Then we describe the state of synchrotron science in South Africa and that country’s leadership role in founding the African Light Source initiative. Next, we highlight a new initiative called Lightsources for Africa, the Americas & Middle East Project, which is a global initiative led by the International Union of Pure and Applied Physics and the International Union of Crystallography, with initial funding provided by the International Council for Science. Finally, we comment on a new technology called the multibend achromat that has launched a new paradigm for the design of synchrotron light sources that should be attractive for construction in developing countries.

Use of a synchrotron radiation x-ray microprobe for elemental analysis at the National Synchrotron Light Source

International Nuclear Information System (INIS)

Gordon, B.M.

1980-01-01

The National Synchrotron Light Source (NSLS) is a facility consisting of a 700 MeV and a 2.5 GeV electron storage ring and dedicated to providing synchrotron radiation in the energy range from the vacuum ultraviolet to high energy x rays. Some of the properties of synchrotron radiation that contribute to its usefulness for x-ray fluorescence are: a continuous, tunable energy spectrum, strong collimation in the horizontal plane, high polarization in the storage ring plane, and relatively low energy deposition. The highest priority is for the development of an x-ray microprobe beam line capable of trace analysis in the parts per million range with spatial resolution as low as one micrometer. An eventual capability for bulk sample analysis is also planned with sensitivities in the more favorable cases beings low as 50 parts per billion in dry biological tissue. The microprobe technique has application to a variety of fields including the geological, medical, materials and environmental sciences. Examples of investigations include multielemental trace analysis across grain boundaries for the study of diffusion and cooling processes in geological and materials sciences samples; in leukocytes and other types of individual cells for studying the relationship between trace element concentrations and disease or nutrition; and in individual particles in air pollution samples

The Australian synchrotron research program

International Nuclear Information System (INIS)

Garrett, R.F.

1998-01-01

Full text: The Australian Synchrotron Research Program (ASRP) was established in 1996 under a 5 year grant from the Australian Government, and is managed by ANSTO on behalf of a consortium of Australian universities and research organisations. It has taken over the operation of the Australian National Beamline Facility (ANBF) at the Photon Factory, and has joined two CATS at the Advanced Photon Source: the Synchrotron Radiation Instrumentation CAT (SRI-CAT) and the Consortium for Advanced Radiation Sources (CARS). The ASRP thus manages a comprehensive range of synchrotron radiation research facilities for Australian science. The ANBF is a general purpose hard X-ray beamline which has been in operation at the Photon Factory since 1993. It currently caters for about 35 Australian research teams per year. The facilities available at the ANBF will be presented and the research program will be summarised. The ASRP facilities at the APS comprise the 5 sectors operated by SRI-CAT, BioCARS and ChemMatCARS. A brief description will be given of the ASRP research programs at the APS, which will considerably broaden the scope of Australian synchrotron science

Moessbauer spectroscopy with synchrotron radiation

International Nuclear Information System (INIS)

Bergmann, U.

1994-01-01

The short pulse nature of synchrotron radiation makes it possible to perform Moessbauer spectroscopy in the time domain, i.e. instead of measuring the transmitted intensity time integrated as a function of source/absorber velocity, the intensity of the scattered radiation is measured time differential. The resulting time spectrum is essentially source independent and complications in the data analysis which are related to the radioactive source are completely removed. Furthermore, the large brightness and well defined polarization of the synchrotron radiation can, e.g., speed up the data collection and facilitate studies of polarization phenomena. To illustrate these new spectroscopic possibilities, measurements of the temperature dependence and polarization dependence of forward scattering from alpha - sup 5 sup 7 Fe nuclei are presented and discussed 26 refs., 5 figs. (author)

Synchrotron-driven spallation sources

CERN Document Server

Bryant, P J

1996-01-01

The use of synchrotrons for pulsed neutron spallation sources is an example of scientific and technological spin-off from the accelerator development for particle physics. Accelerator-driven sources provide an alternative to the continuous-flux, nuclear reactors that currently furnish the majority of neutrons for research and development. Although the present demand for neutrons can be adequately met by the existing reactors, this situation is unlikely to continue due to the increasing severity of safety regulations and the declared policies of many countries to close down their reactors within the next decade or so. Since the demand for neutrons as a research tool is, in any case,expected to grow, there has been a corresponding interest in sources that are synchrotron-driven or linac-driven with a pulse compression ring and currently several design studies are being made. These accelerator-driven sources also have the advantage of a time structure with a high peak neutron flux. The basic requirement is for a...

New developments in the application of synchrotron radiation to material science

International Nuclear Information System (INIS)

Sinha, S. K.

1999-01-01

Recent developments in the application of synchrotrons radiation to materials science are discussed, using techniques which exploit the high brilliance of the newer synchrotrons sources, such as microbeam techniques and correlation spectroscopy. These include studies of environmental systems, residual stress, slow dynamics of condensed matter systems and studies of liquid surfaces and thin magnetic films

Glass transition near the free surface studied by synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Sikorski, M.

2008-06-15

A comprehensive picture of the glass transition near the liquid/vapor interface of the model organic glass former dibutyl phthalate is presented in this work. Several surface-sensitive techniques using x-ray synchrotron radiation were applied to investigate the static and dynamic aspects of the formation of the glassy state from the supercooled liquid. The amorphous nature of dibutyl phthalate close to the free surface was confirmed by grazing incidence X-ray diffraction studies. Results from X-ray reflectivity measurements indicate a uniform electron density distribution close to the interface excluding the possibility of surface freezing down to 175 K. Dynamics on sub-{mu}m length-scales at the surface was studied with coherent synchrotron radiation via x-ray photon correlation spectroscopy. From the analysis of the dispersion relation of the surface modes, viscoelastic properties of the dibutyl phthalate are deduced. The Kelvin-Voigt model of viscoelastic media was found to describe well the properties of the liquid/vapor interface below room temperature. The data show that the viscosity at the interface matches the values reported for bulk dibutyl phthalate. The scaled relaxation rate at the surface agrees with the bulk data above 210 K. Upon approaching the glass transition temperature the free surface was observed to relax considerably faster close to the liquid/vapor interface than in bulk. The concept of higher relaxation rate at the free surface is also supported by the results of the quasielastic nuclear forward scattering experiment, during which dynamics on molecular length scales around the calorimetric glass transition temperature is studied. The data were analyzed using mode-coupling theory of the glass transition and the model of the liquid(glass)/vapor interface, predicting inhomogeneous dynamics near the surface. The quasielastic nuclear forward scattering data can be explained when the molecular mobility is assumed to decrease with the increasing

Glass transition near the free surface studied by synchrotron radiation

International Nuclear Information System (INIS)

Sikorski, M.

2008-06-01

A comprehensive picture of the glass transition near the liquid/vapor interface of the model organic glass former dibutyl phthalate is presented in this work. Several surface-sensitive techniques using x-ray synchrotron radiation were applied to investigate the static and dynamic aspects of the formation of the glassy state from the supercooled liquid. The amorphous nature of dibutyl phthalate close to the free surface was confirmed by grazing incidence X-ray diffraction studies. Results from X-ray reflectivity measurements indicate a uniform electron density distribution close to the interface excluding the possibility of surface freezing down to 175 K. Dynamics on sub-μm length-scales at the surface was studied with coherent synchrotron radiation via x-ray photon correlation spectroscopy. From the analysis of the dispersion relation of the surface modes, viscoelastic properties of the dibutyl phthalate are deduced. The Kelvin-Voigt model of viscoelastic media was found to describe well the properties of the liquid/vapor interface below room temperature. The data show that the viscosity at the interface matches the values reported for bulk dibutyl phthalate. The scaled relaxation rate at the surface agrees with the bulk data above 210 K. Upon approaching the glass transition temperature the free surface was observed to relax considerably faster close to the liquid/vapor interface than in bulk. The concept of higher relaxation rate at the free surface is also supported by the results of the quasielastic nuclear forward scattering experiment, during which dynamics on molecular length scales around the calorimetric glass transition temperature is studied. The data were analyzed using mode-coupling theory of the glass transition and the model of the liquid(glass)/vapor interface, predicting inhomogeneous dynamics near the surface. The quasielastic nuclear forward scattering data can be explained when the molecular mobility is assumed to decrease with the increasing

Injection study of the Radiance 330 synchrotron with a 1.6 MeV RFQ linac

Science.gov (United States)

Wang, F.; Flanz, J.; Hamm, R.

2012-09-01

The ProTom Radiance 330 proton radiotherapy system provides the most advanced proton delivery capability to date. It supports true three-dimensional beam scanning with dynamic energy and intensity modulation. Most of the protons extracted from the synchrotron are used to treat the patient, which results in minimal neutron background in the treatment room. The patient dose rate depends upon the number of protons injected and the acceleration cycle time. Therefore, one can boost the dose rate by increasing the beam intensity at injection. Improvements to the existing tandem accelerator injector are already underway. However, an alternative way to attain higher intensity beam is to use an RFQ linac as an injector. To this end, a novel 1.6 MeV RFQ linac has been designed to specifically satisfy the small energy acceptance limits of the synchrotron. Simulations of the beam line optics and injection matching to the synchrotron have been performed using the computer codes PARMILA and TRACE-3D to determine if an additional bunching cavity is needed. Assessments of the space charge limit at the relatively low injection energy of 1.6 MeV and RF capture simulations have also been performed. Results of these studies are presented.

Applications of synchrotron radiation in Biophysics

International Nuclear Information System (INIS)

Bemski, G.

1983-01-01

A short introduction to the generation of the synchrotron radiation is made. Following, the applications of such a radiation in biophysics with emphasis to the study of the hemoglobin molecule are presented. (L.C.) [pt

Study of charge-sharing in MEDIPIX3 using a micro-focused synchrotron beam

CERN Document Server

Gimenez, E N; Marchal, J; Turecek, D; Ballabriga, R; Tartoni, N; Campbell, M; Llopart, X; Sawhney, K J S

2011-01-01

X-ray photon-counting detectors consisting of a silicon pixel array sensor bump-bonded to a CMOS electronic readout chip offer several advantages over traditional X-ray detection technologies used for synchrotron applications. They offer high frame rate, dynamic range, count rate capability and signal-to-noise ratio. A survey of the requirements for future synchrotron detectors carried out at the Diamond Light Source synchrotron highlighted the needs for detectors with a pixel size of the order of 50 mu m. Reducing the pixel size leads to an increase of charge-sharing events between adjacent pixels and, therefore, to a degradation of the energy resolution and image quality of the detector. This effect was observed with MEDIPIX2, a photon-counting readout chip with a pixel size of 55 mu m. The lastest generation of the MEDIPIX family, MEDIPIX3, is designed to overcome this charge-sharing effect in an implemented readout operating mode referred to as Charge Summing Mode. MEDIPIX3 has the same pixel size as MEDI...

Review of third and next generation synchrotron light sources

International Nuclear Information System (INIS)

Bilderback, Donald H; Elleaume, Pascal; Weckert, Edgar

2005-01-01

Synchrotron radiation (SR) is having a very large impact on interdisciplinary science and has been tremendously successful with the arrival of third generation synchrotron x-ray sources. But the revolution in x-ray science is still gaining momentum. Even though new storage rings are currently under construction, even more advanced rings are under design (PETRA III and the ultra high energy x-ray source) and the uses of linacs (energy recovery linac, x-ray free electron laser) can take us further into the future, to provide the unique synchrotron light that is so highly prized for today's studies in science in such fields as materials science, physics, chemistry and biology, for example. All these machines are highly reliant upon the consequences of Einstein's special theory of relativity. The consequences of relativity account for the small opening angle of synchrotron radiation in the forward direction and the increasing mass an electron gains as it is accelerated to high energy. These are familiar results to every synchrotron scientist. In this paper we outline not only the origins of SR but discuss how Einstein's strong character and his intuition and excellence have not only marked the physics of the 20th century but provide the foundation for continuing accelerator developments into the 21st century

Evaluation of the synchrotron close orbit

International Nuclear Information System (INIS)

Bashmakov, Yu.A.; Karpov, V.A.

1991-01-01

The knowledge of the closed orbit position is an essential condition for the effective work of any accelerator. Therefore questions of calculations, measurements and controls have great importance. For example, during injection of particles into a synchrotron, the amplitudes of their betatron oscillations may become commensurable with the working region of the synchrotron. This makes one pay attention at the problem of formation of the optimum orbit with use of correcting optical elements. In addition, it is often necessary to calculate such an orbit at the end of the acceleration cycle when particles are deposited at internal targets or removed from the synchrotron. In this paper, the computation of the close orbit is reduced to a determination at an arbitrarily chosen azimuth of the eigenvector of the total transfer matrix of the synchrotron ring and to tracing with this vector desired orbit. The eigenvector is found as a result of an iteration

Synchrotron radiation gives insight in smaller and smaller crystals

International Nuclear Information System (INIS)

Hintsches, E.

1983-01-01

Scientists from the ''Max-Planck-Institut fuer Festkoerperforschung'' in Stuttgart have extended the method of X-ray analysis to study the structure of very small crystals. For the first time a crystal with 6 μm linear dimension has been successfully analysed using the synchrotron radiation from the DESY electron synchrotron at Hamburg. Thus this important method of analysis has been demonstrated to be usefull for structural studies of crystals, which are smaller by a factor of 20 than hitherto. (orig.) [de

Array element of a space-based synchrotron radiation detector

International Nuclear Information System (INIS)

Lee, M.W.; Commichau, S.C.; Kim, G.N.; Son, D.; Viertel, G.M.

2006-01-01

A synchrotron radiation detector (SRD) has been proposed as part of the Alpha Magnetic Spectrometer experiment on the International Space Station to study cosmic ray electrons and positrons in the TeV energy range. The SRD will identify these particles by detecting their emission of synchrotron radiation in the Earth's magnetic field. This article reports on the study of key technical parameters for the array elements which form the SRD, including the choice of the detecting medium, the sensor and the readout system

Properties of synchrotron radiation

International Nuclear Information System (INIS)

Materlik, G.

1982-01-01

This paper forms the introductory chapter to a book concerning the use of synchrotron radiation for investigation of the structure and mechanism of biological macromolecules. After a historical section, the physics of synchrotron radiation is summarized so that the most promising experiments may be extrapolated. Irradiated power and intensity, polarization and angular distribution, brilliance of a real source, and developments such as wigglers and undulators are briefly dealt with. The paper includes a tabulated compilation of proposed and operating machines in 1982, with some of their characteristics. (U.K.)

X-ray detectors for diffraction studies and their use with synchrotron radiation

International Nuclear Information System (INIS)

Milch, J.

1976-02-01

All techniques for X-ray diffraction studies on biological materials exhibit certain limitations. The characteristics of several X-ray detection systems, namely film, multiwire proportional counter and image intensified TV, are discussed and compared for application to specific biological studies. For the high count-rate situation existing at a synchrotron, it is shown that film is a good choice, but that the image intensified TV exhibits significant advantages. The details of such a system now being used at Princeton with a low intensity source are given and current results presented

Neutron and synchrotron radiation for condensed matter studies. Volume 1: theory, instruments and methods

International Nuclear Information System (INIS)

Baruchel, J.; Hodeau, J.L.; Lehmann, M.S.; Regnard, J.R.; Schlenker, C.

1993-01-01

This book provides the basic information required by a research scientist wishing to undertake studies using neutrons or synchrotron radiation at a Large Facility. These lecture notes result from 'HERCULES', a course that has been held in Grenoble since 1991 to train young scientists in these fields. They cover the production of neutrons and synchrotron radiation and describe all aspects of instrumentation. In addition, this work outlines the basics of the various fields of research pursued at these Large Facilities. It consists of a series of chapters written by experts in the particular fields. While following a progression and constituting a lecture course on neutron and x-ray scattering, these chapters can also be read independently. This first volume will be followed by two further volumes concerned with the applications to solid state physics and chemistry, and to biology and soft condensed matter properties

Multi-wavelength study of infrared galaxies

International Nuclear Information System (INIS)

Marcillac, Delphine

2005-01-01

This thesis deals with a panchromatic study of luminous infrared galaxies (LIRGs) detected at 15 microns by ISOCAM (camera aboard ISO) and at 24 microns by MIPS (camera aboard the recently launched Spitzer satellite). These galaxies are today considered to be the Rosetta Stone of galaxy evolution since they are found to be far more numerous at high redshift and it is thought that a large part of stars seen in the local universe are born in such phases. The first part of this thesis presents a new study dedicated to dust emission of distant LIRGs in the mid-infrared range. Their dust emission has been compared to those of a local sample of LIRGs in addition to the prediction of several spectral energy distributions (SEDs) built on data available in the local universe. It has been shown that distant and local LIRGs present similar mid infrared spectral energy distribution: similar PAH bumps are detected in both local and distant LIRGs, however distant LIRGs show evidence of a stronger silicate absorption at 10 microns associated silicate grains. It also shows that distant LIRG mid infrared emission can be used together with local SEDs in order to estimate the total infrared luminosity. The second part of this thesis is dedicated to the burst of star formation and to the recent star formation history of these galaxies, which is responsible for the dust emission. This study was done thanks to a combination of high resolution spectra (R=2000 in the rest frame) obtained at VLT/FORS2 and the stellar population synthesis models called GALAXEV (Bruzual and Charlot, 2003). It has been shown that the burst of star formation has a duration of about 0.1 Gyear. About 10 % of the stellar content is formed during this burst of star formation. (author) [fr

Synchrotron Applications of High Magnetic Fields

Energy Technology Data Exchange (ETDEWEB)

NONE

2006-07-01

This workshop aims at discussing the scientific potential of X-ray diffraction and spectroscopy in magnetic fields above 30 T. Pulsed magnetic fields in the range of 30 to 40 T have recently become available at Spring-8 and the ESRF (European synchrotron radiation facility). This document gathers the transparencies of the 6 following presentations: 1) pulsed magnetic fields at ESRF: first results; 2) X-ray spectroscopy and diffraction experiments by using mini-coils: applications to valence state transition and frustrated magnet; 3) R{sub 5}(Si{sub x}Ge{sub 1-x}){sub 4}: an ideal system to be studied in X-ray under high magnetic field?; 4) high field studies at the Advanced Photon Source: present status and future plans; 5) synchrotron X-ray diffraction studies under extreme conditions; and 6) projects for pulsed and steady high magnetic fields at the ESRF.

RF-knockout Extraction System for the CNAO Synchrotron

CERN Document Server

Carmignani, Nicola; Serio, Mario; Balbinot, Giovanni; Bressi, Erminia; Caldara, Michele; Pullia, Marco; Bosser, Jacques; Venchi, Giuseppe

2010-01-01

The National Centre for Oncological Hadrontherapy (CNAO) is a centre in Italy for the treatment of patients affected by tumours with proton and carbon ions beams accelerated in a synchrotron. The synchrotron extraction method is based on the use of a betatron core. This work aims to verify, through a theoretical study and a simulation, the possibility of using the RF-knockout extraction method exploiting the existing hardware. A simulation program has been written to simulate the extraction system of the synchrotron with the purpose to define the parameters of the radio frequency. Two types of radio frequencies have been compared in order to obtain a constant spill with the minimum ripple: a carrier wave with a frequency and amplitude modulation, and a gaussian narrow band noise modulated in amplitude. Results of the simulation and considerations on the kicker characteristics are presented

Shining a light on Jarosite: formation, alteration and stability studies using in situ experimental synchrotron and neutron techniques.

Science.gov (United States)

Brand, H. E. A.; Scarlett, N. V. Y.; Wilson, S. A.; Frierdich, A. J.; Grey, I. E.

2016-12-01

Jarosites and related minerals are critical to a range of mineral processing and research applications. They are used in the removal of iron species from smelting processes; they occur in metal bioleaching systems, and they are present in acid mine drainage environments. There has been a recent resurgence in interest in jarosites since their detection on Mars. In this context, the presence of jarosite has been recognised as a likely indicator of liquid water at the surface of Mars in the past & it is thought that their study will provide insight into the environmental history of Mars. Acid sulfate soils cover large areas of the Australian coastline and are likely to be a major constituent of the Martian environment. The oxidation of acid sulfate soils, coupled with potential release of heavy metals and acidic groundwaters, can have serious consequences for fragile ecosystems. Understanding these sediments will provide insight into the biogeochemical processes that affect the lifetimes of transient mineral species on Earth, and may be used to better understand soil acidification, contaminant mobility at sites affected by acid and metalliferous drainage, and even constrain past weathering and putative biosignatures on Mars. Knowledge of the behaviour of jarosite minerals under the actual conditions that they are found in is crucial to understanding their potential environmental impacts on both Earth and Mars. To this end, we are engaged in a program to study the formation, stability and alteration of natural and synthetic jarosite minerals using a complementary suite of in situ synchrotron and neutron techniques. There are 3 sections to this work that will introduce the experimental techniques and sample environments that make these measurements possible: Studying the nucleation and growth of jarosites under laboratory conditions. The experimentation consisted of time-resolved synchrotron small angle X-ray scattering and X-ray diffraction. Studying the stability of

Synchrotron radiation applications in biophysics and medicine

International Nuclear Information System (INIS)

Burattini, E.

1985-01-01

The peculiar properties of synchrotron radiation are briefly summarized. A short review on the possible applications of synchrotron radiation in two important fields like Biophysics and Medicine is presented. Details are given on experiments both in progress and carried out in many synchrotron radiation facilities, all over the world, using different techniques like X-ray absorption and fluorescence spectroscopy, X-ray fluorescence microanalysis, X-ray microscopy and digital subtraction angiography. Some news about the photon-activation therapy are briefly reported too

A multi-wavelength view of the central kiloparsec region in the luminous infrared galaxy NGC 1614

Energy Technology Data Exchange (ETDEWEB)

Herrero-Illana, Rubén; Pérez-Torres, Miguel Á.; Alberdi, Antxon; Hernández-García, Lorena [Instituto de Astrofísica de Andalucía-CSIC, P.O. Box 3004, E-18008 Granada (Spain); Alonso-Herrero, Almudena [Instituto de Física de Cantabria, CSIC-Universidad de Cantabria, E-39005 Santander (Spain); Colina, Luis [Centro de Astrobiología (INTA-CSIC), Ctra. de Torrejón a Ajalvir, km 4, E-28850 Torrejón de Ardoz, Madrid (Spain); Efstathiou, Andreas [School of Sciencies, European University Cyprus, Diogenes Street, Engomi, 1516 Nicosia (Cyprus); Miralles-Caballero, Daniel [Instituto de Física Teórica, Universidad Autónoma de Madrid, E-28049 Madrid (Spain); Väisänen, Petri [South African Astronomical Observatory, P.O. Box 9, Observatory 7935 Cape Town (South Africa); Packham, Christopher C. [Department of Physics and Astronomy, University of Texas at San Antonio, One UTSA Circle, San Antonio, TX 78249 (United States); Rajpaul, Vinesh [Department of Physics, University of Oxford, Denys Wilkinson Building, Keble Road, Oxford OX1 3RH (United Kingdom); Zijlstra, Albert A. [Jodrell Bank Centre for Astrophysics, University of Manchester, Manchester M13 9PL (United Kingdom)

2014-05-10

The Luminous Infrared Galaxy NGC 1614 hosts a prominent circumnuclear ring of star formation. However, the nature of the dominant emitting mechanism in its central ∼100 pc is still under debate. We present sub-arcsecond angular resolution radio, mid-infrared, Paα, optical, and X-ray observations of NGC 1614, aimed at studying in detail both the circumnuclear ring and the nuclear region. The 8.4 GHz continuum emission traced by the Very Large Array and the Gemini/T-ReCS 8.7 μm emission, as well as the Paα line emission, show remarkable morphological similarities within the star-forming ring, suggesting that the underlying emission mechanisms are tightly related. We used a Hubble Space Telescope/NICMOS Paα map of similar resolution to our radio maps to disentangle the thermal free-free and non-thermal synchrotron radio emission, from which we obtained the intrinsic synchrotron power law for each individual region within the central kiloparsec of NGC 1614. The radio ring surrounds a relatively faint, steep-spectrum source at the very center of the galaxy, suggesting that the central source is not powered by an active galactic nucleus (AGN), but rather by a compact (r ≲ 90 pc) starburst (SB). Chandra X-ray data also show that the central kiloparsec region is dominated by SB activity, without requiring the existence of an AGN. We also used publicly available infrared data to model-fit the spectral energy distribution of both the SB ring and a putative AGN in NGC 1614. In summary, we conclude that there is no need to invoke an AGN to explain the observed bolometric properties of the galaxy.

Materials science created by synchrotron radiation

International Nuclear Information System (INIS)

Oshima, Masaharu

2015-01-01

We survey the use of synchrotron radiation for studies on oxides. High luminosity enables the spectroscopy with high energy-resolution in soft X-ray and vacuum ultraviolet region. Element analysis is possible by examining absorption edge in the X-ray absorption spectra. Time-resolved measurements are possible due to the pulsed nature of the radiation. The radiation can bear linear or circular polarization. The feature of molecules adhered on a surface can be clarified by using linearly polarized radiation. The circularly polarized radiation, on the other hand, clarifies the magnetic structure. The structure information so far unknown can be obtained by using space- or time-coherent radiation. We show studies using synchrotron radiation on LSI gate oxide foils, variable resistance RAM, strongly correlated oxide foils, and the oxide as positive electrode of Li ion battery. (J.P.N.)

Study of moire fringes using synchrotron X-rays

International Nuclear Information System (INIS)

Yoshimura, Jun-ichi

1992-01-01

It has recently been shown that X-ray moire fringes are not exactly the projection of the intensity distribution of the wave field on the exit surface of the crystal, but do oscillate along the beam path behind the crystal. Such nonprojectiveness of moire fringes is inexplicable by the conventional understanding of moire fringes, and therefore is of interest from a fundamental viewpoint as well as practical one. In this paper the phenomena of the nonprojectiveness are described on the basis of the latest experimental data obtained by synchrotron radiation. (author)

Storage ring design of the 8 GeV synchrotron radiation facility (SPring-8)

International Nuclear Information System (INIS)

Hara, M.; Bc, S.H.; Motonaga, S.

1990-01-01

In Japan, RIKEN (Institute of Physical and Chemical Research) and JAERI (Japan Atomic Energy Research Institute) have organized a joint design team and started a design study for an 8 GeV synchrotron radiation X-ray source. This paper outlines the status of the design study for the 8 GeV highly brilliant synchrotron radiation X-ray source ring named Super Photon Ring (SPring-8). The facility consists of a main storage ring, a full-energy injector booster synchrotron and a pre-injector 1 GeV linac. The injector linac and synchrotron are laid outside the storage ring because to permit the use of the linac and synchrotron not only as an injector but also as an electron or positron beam source. The purpose of the facility is to provide stable photon beams with high brilliance in the X-ray region. The energy of the stored electrons (positrons) is fixed at 8 GeV to fulfill the required condition using conventional type insertion devices. (N.K.)

Imaging Local Chemical Microstructure of Germinated Wheat with Synchrotron Infrared Microspectroscopy

International Nuclear Information System (INIS)

Koc, H.; Wetzel, D.

2008-01-01

The spatial resolution enabled by in situ Fourier-transform infrared (FT-IR) microspectroscopy as predicted from our earlier report in Spectroscopy (1) is applied to localized chemical analysis in this vital biological process of seed germination. Germination includes several different biochemical and structural processes. Ultimately, the entire seed is consumed in sustaining the new life that results after sprouting and growth (2-4). Alpha amylase production is the standard evidence for detection of sprouted (germinated) wheat at harvest. Moist preharvest conditions can cause devastating losses and render the harvested wheat unfit for flour production. Dormancy of dry seeds following harvest retards sprouting under proper storage.

Development of the protein crystallography by synchrotron radiation

International Nuclear Information System (INIS)

Yamamoto, Masaki

2014-01-01

Since crystal structure determination of the first protein by Kendrew in 1959, protein crystallography developed into the leading role of the protein structure study by various technology developments. Especially the utilization of synchrotron radiation from the 1990s brought innovative progress of protein crystallography on the data quality and the phasing method and had expanded the samples targets including membrane proteins and suprarmolecular complexes. Here I give the outline of the history and the future prospects of the protein crystallography from the role of synchrotron radiation. (author)

New synchrotron radiation facility project. Panel on new synchrotron radiation facility project

CERN Document Server

Sato, S; Kimura, Y

2003-01-01

The project for constructing a new synchrotron radiation facility dedicated to the science in VUV (or EUV) and Soft X-ray (SX) region has been discussed for these two years at the Panel on New Synchrotron Radiation Facility Project. The Panel together with the Accelerator Design Working Group (WG), Beamline Design WG and Research Program WG suggested to the Ministry of Education, Science, Culture and Sports the construction of a 1.8 GeV electron storage ring suitable for 'Top-Up' operation and beamlines and monochromators designed for undulator radiation. The scientific programs proposed by nationwide scientists are summarized with their requirements of the characteristics of the beam. (author)

INFRARED AND RAMAN SPECTROSCOPIC STUDY OF ION ...

African Journals Online (AJOL)

Infrared and Raman spectroscopy techniques have been used to study the ionic interactions of strontium(II) and barium(II) with thiocyanate ion in liquid ammonia. A number of bands were observed in both n (CN) and n (CS) regions of infrared and Raman spectra and these were assigned to 1:1 contact ion pair, ...

Photoemission studies of clean and adsorbate covered metal surfaces using synchrotron and uv radiation sources

International Nuclear Information System (INIS)

Apai, G.R. II.

1977-09-01

Photoemission energy distribution experiments on clean metal and adsorbate-covered surfaces were performed under ultrahigh vacuum conditions by using x-ray and ultraviolet photon sources in the laboratory as well as continuously-tunable, highly polarized synchrotron radiation obtainable at the Stanford Synchrotron Radiation Laboratory (SSRL). Studies focused on two general areas: cross-section modulation in the photoemission process was studied as a function of photon energy and orbital composition. Sharp decreases in intensity of the valence bands of several transition metals (i.e., Ag, Au, and Pt) are attributed to the radial nodes in the respective wave functions. Adsorbate photoemission studies of CO adsorbed on platinum single crystals have demonstrated a very high spectral sensitivity to the 4sigma and (1π + 5sigma) peaks of CO at photon energies of 150 eV. Angle-resolved photoemission allowed determination of the orientation of CO chemisorbed on a Pt (111) or Ni(111) surface. Prelinimary results at high photon energies (approximately 150 eV) indicated scattering from the substrate which could yield chemisorption site geometries

THz near-field imaging of biological tissues employing synchrotron radiation

International Nuclear Information System (INIS)

Schade, Ulrich; Holldack, Karsten; Martin, Michael C.; Fried, Daniel

2004-01-01

Terahertz scanning near-field infrared microscopy (SNIM) below 1 THz is demonstrated. The near-field technique benefits from the broadband and highly brilliant coherent synchrotron radiation (CSR) from an electron storage ring and from a detection method based on locking onto the intrinsic time structure of the synchrotron radiation. The scanning microscope utilizes conical wave guides as near-field probes with apertures smaller than the wavelength. Different cone approaches have been investigated to obtain maximum transmittance. Together with a Martin-Puplett spectrometer the set-up enables spectroscopic mapping of the transmittance of samples well below the diffraction limit. Spatial resolution down to about lambda/40 at 2 wavenumbers (0.06 THz) is derived from the transmittance spectra of the near-field probes. The potential of the technique is exemplified by imaging biological samples. Strongly absorbing living leaves have been imaged in transmittance with a spatial resolution of 130 mu-m at about 12 wave numbers (0.36 THz). The THz near-field images reveal distinct structural differences of leaves from different plants investigated. The technique presented also allows spectral imaging of bulky organic tissues. Human teeth samples of various thicknesses have been imaged between 2 and 20 wavenumbers (between 0.06and 0.6 THz). Regions of enamel and dentin within tooth samples are spatially and spectrally resolved, and buried caries lesions are imaged through both the outer enamel and into the underlying dentin

Mid-infrared supercontinuum covering the 1.4–13.3 μm molecular fingerprint region using ultra-high NA chalcogenide step-index fibre

DEFF Research Database (Denmark)

Petersen, Christian Rosenberg; Møller, Uffe Visbech; Kubat, Irnis

2014-01-01

-power laser diodes, quantum cascade lasers and synchrotron radiation have precluded mid-infrared applications where the spatial coherence, broad bandwidth, high brightness and portability of a supercontinuum laser are all required. Here, we demonstrate experimentally that launching intense ultra-short pulses...... the potential of fibres to emit across the mid-infrared molecular ‘fingerprint region’, which is of key importance for applications such as early cancer diagnostics3, gas sensing and food quality control....

Atomic physics research with synchrotron radiation

International Nuclear Information System (INIS)

Crasemann, B.

1981-01-01

Applications of synchrotron radiation to research in high-energy atomic physics are summarized. These lie in the areas of photoelectron spectrometry, photon scattering, x-ray absorption spectroscopy, time-resolved measurements, resonance spectroscopy and threshold excitation, and future, yet undefined studies

Funding problems threaten Middle East's synchrotron

CERN Multimedia

McCabe, H

1999-01-01

Scientists will tour the Middle East to try to raise support for the Synchrotron radiation for Experimental Science and Applications in the Middle East project. The plan is to dismantle and move a decommissioned synchrotron from Berlin to the Middle East where scientists of any nationality would be able to use it (3 paragraphs).

High resolution spectroscopy of six SOCl2 isotopologues from the microwave to the far-infrared

Science.gov (United States)

Martin-Drumel, M. A.; Roucou, A.; Brown, G. G.; Thorwirth, S.; Pirali, O.; Mouret, G.; Hindle, F.; McCarthy, M. C.; Cuisset, A.

2016-02-01

Despite its potential role as an atmospheric pollutant, thionyl chloride, SOCl2, remains poorly characterized in the gas phase. In this study, the pure rotational and ro-vibrational spectra of six isotopologues of this molecule, all detected in natural abundance, have been extensively studied from the cm-wave band to the far-infrared region by means of three complementary techniques: chirped-pulse Fourier transform microwave spectroscopy, sub-millimeter-wave spectroscopy using frequency multiplier chain, and synchrotron-based far-infrared spectroscopy. Owing to the complex line pattern which results from two nuclei with non-zero spins, new, high-level quantum-chemical calculations of the hyperfine structure played a crucial role in the spectroscopic analysis. From the combined experimental and theoretical work, an accurate semi-experimental equilibrium structure (reSE) of SOCl2 has been derived. With the present data, spectroscopy-based methods can now be applied with confidence to detect and monitor this species, either by remote sensing or in situ.

Synchrotron microradiography study on acute lung injury of mouse caused by PM2.5 aerosols

International Nuclear Information System (INIS)

Tong Yongpeng; Zhang Guilin; Li Yan; Tan Mingguan; Wang Wei; Chen Jianmin; Hwu Yeukuang; Hsu, Pei-Chebg; Je, Jung Ho; Margaritondo, Giorgio; Song Weiming; Jiang, Rongfang; Jiang Zhihai

2006-01-01

In order to investigate FeSO 4 , ZnSO 4 (the two of main metal compositions of Shanghai PM 2.5 (particle matter with those aerodynamical diameter 2.5 aerosol particles, FeSO 4 , ZnSO 4 and their mixtures were instilled intratracheally into mouse lungs for experiment. By 2 days after instillation, the live mice were checked in vivo by synchrotron refractive index microradiography. In addition after extracted and examined by dissection, the right lobes of lung were fixed by formalin, then imaged by synchrotron microradiography again. Corresponding parts of those lung tissues were embedded in paraffin for histopathologic study. The synchrotron X-ray microradiographs of live mouse lung showed different lung texture changes after instilled with different toxic solutions. Hemorrhage points in lung were observed more from those mice instilled by FeSO 4 contained toxin solutions groups. Bronchial epithelial hyperplasia can be observed in ZnSO 4 contained solution-instilled groups from histopathologic analysis. It was found that the acute lung injury of mice caused by solution of PM 2.5 + FeSO 4 + ZnSO 4 was more serious than other toxin solutions. Results suggested that FeSO 4 mainly induced hemorrhage and ZnSO 4 mainly induced inflammation and bronchiolar epithelial hyperplasia in the early toxicological effects of PM 2.5

Single-mode coherent synchrotron radiation instability

Directory of Open Access Journals (Sweden)

S. Heifets

2003-06-01

Full Text Available The microwave instability driven by the coherent synchrotron radiation (CSR has been previously studied [S. Heifets and G. V. Stupakov, Phys. Rev. ST Accel. Beams 5, 054402 (2002] neglecting effect of the shielding caused by the finite beam pipe aperture. In practice, the unstable mode can be close to the shielding threshold where the spectrum of the radiation in a toroidal beam pipe is discrete. In this paper, the CSR instability is studied in the case when it is driven by a single synchronous mode. A system of equations for the beam-wave interaction is derived and its similarity to the 1D free-electron laser theory is demonstrated. In the linear regime, the growth rate of the instability is obtained and a transition to the case of continuous spectrum is discussed. The nonlinear evolution of the single-mode instability, both with and without synchrotron damping and quantum diffusion, is also studied.

National Synchrotron Light Source annual report 1988

Energy Technology Data Exchange (ETDEWEB)

Hulbert, S.; Lazarz, N.; Williams, G. (eds.)

1988-01-01

This report discusses the experiment done at the National Synchrotron Light Source. Most experiments discussed involves the use of the x-ray beams to study physical properties of solid materials. (LSP)

Application of synchrotron radiation to elemental analysis

International Nuclear Information System (INIS)

Jones, K.W.; Gordon, B.M.; Hanson, A.L.; Hastings, J.B.; Howells, M.R.; Kraner, H.W.; Chen, J.R.

1983-01-01

The use of a synchrotron storage ring as a high brightness source for production of monoergic, variable energy, and highly polarized x-ray beams promises to revolutionize the field of elemental analysis. The results of exploratory work using the Cornell synchrotron facility, CHESS, will be described. Design considerations and features of the new X-Ray Microprobe Facility now under construction at the Brookhaven National Synchrotron Light Source will be presented. This facility will be used for bulk analysis and for microanalysis with an initial spatial resolution of the order of 30 μm

Study Of Soot Growth And Nucleation By A Time-Resolved Synchrotron Radiation Based X-Ray Absorption Method

National Research Council Canada - National Science Library

Mitchell, Judith I

2001-01-01

This report results from a contract tasking University of Rennes I as follows: The contractor will perform a study of soot growth and nucleation by a time-resolved synchrotron radiation based x-ray absorption method...

Dedicated Beamline Facilities for Catalytic Research. Synchrotron Catalysis Consortium (SCC)

Energy Technology Data Exchange (ETDEWEB)

Chen, Jingguang [Columbia Univ., New York, NY; Frenkel, Anatoly [Yeshiva Univ., New York, NY (United States); Rodriguez, Jose [Brookhaven National Lab. (BNL), Upton, NY (United States); Adzic, Radoslav [Brookhaven National Lab. (BNL), Upton, NY (United States); Bare, Simon R. [UOP LLC, Des Plaines, IL (United States); Hulbert, Steve L. [Brookhaven National Lab. (BNL), Upton, NY (United States); Karim, Ayman [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Mullins, David R. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Overbury, Steve [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

2015-03-04

Synchrotron spectroscopies offer unique advantages over conventional techniques, including higher detection sensitivity and molecular specificity, faster detection rate, and more in-depth information regarding the structural, electronic and catalytic properties under in-situ reaction conditions. Despite these advantages, synchrotron techniques are often underutilized or unexplored by the catalysis community due to various perceived and real barriers, which will be addressed in the current proposal. Since its establishment in 2005, the Synchrotron Catalysis Consortium (SCC) has coordinated significant efforts to promote the utilization of cutting-edge catalytic research under in-situ conditions. The purpose of the current renewal proposal is aimed to provide assistance, and to develop new sciences/techniques, for the catalysis community through the following concerted efforts: Coordinating the implementation of a suite of beamlines for catalysis studies at the new NSLS-II synchrotron source; Providing assistance and coordination for catalysis users at an SSRL catalysis beamline during the initial period of NSLS to NSLS II transition; Designing in-situ reactors for a variety of catalytic and electrocatalytic studies; Assisting experimental set-up and data analysis by a dedicated research scientist; Offering training courses and help sessions by the PIs and co-PIs.

Synchrotron SAXS Studies of Nanostructured Materials and Colloidal Solutions: A Review

Directory of Open Access Journals (Sweden)

Craievich A.F.

2002-01-01

Full Text Available Structural characterisations using the SAXS technique in a number of nanoheterogeneous materials and liquid solutions are reviewed. The studied systems are protein (lysozyme/water solutions, colloidal ZnO particles/water sols, nanoporous NiO-based xerogels, hybrid organic-inorganic siloxane-PEG and PPG nanocomposites and PbTe semiconductor nanocrystals embedded in a glass matrix. These investigations also focus on the transformations of time-varying structures and on structural changes related to variations in temperature and composition. The reviewed investigations aim at explaining the unusual and often interesting properties of nanostructured materials and solutions. Most of the reported studies were carried out using the SAXS beamline at the National Synchrotron Light Laboratory (LNLS, Campinas, Brazil.

Hard X-ray Sources for the Mexican Synchrotron Project

International Nuclear Information System (INIS)

Reyes-Herrera, Juan

2016-01-01

One of the principal tasks for the design of the Mexican synchrotron was to define the storage ring energy. The main criteria for choosing the energy come from studying the electromagnetic spectrum that can be obtained from the synchrotron, because the energy range of the spectrum that can be obtained will determine the applications available to the users of the future light source. Since there is a public demand of hard X-rays for the experiments in the synchrotron community users from Mexico, in this work we studied the emission spectra from some hard X-ray sources which could be the best options for the parameters of the present Mexican synchrotron design. The calculations of the flux and the brightness for one Bending Magnet and four Insertion Devices are presented; specifically, for a Superconducting Bending Magnet (SBM), a Superconducting Wiggler (SCW), an In Vacuum Short Period Undulator (IV-SPU), a Superconducting Undulator (SCU) and for a Cryogenic Permanent Magnet Undulator (CPMU). Two commonly available synchrotron radiation programs were used for the computation (XOP and SRW). From the results, it can be concluded that the particle beam energy from the current design is enough to have one or more sources of hard X-rays. Furthermore, a wide range of hard X-ray region can be covered by the analyzed sources, and the choice of each type should be based on the specific characteristics of the X-ray beam to perform the experiments at the involved beamline. This work was done within the project Fomix Conacyt-Morelos ”Plan Estrategico para la construccion y operación de un Sincrotron en Morelos” (224392). (paper)

Hard X-ray Sources for the Mexican Synchrotron Project

Science.gov (United States)

Reyes-Herrera, Juan

2016-10-01

One of the principal tasks for the design of the Mexican synchrotron was to define the storage ring energy. The main criteria for choosing the energy come from studying the electromagnetic spectrum that can be obtained from the synchrotron, because the energy range of the spectrum that can be obtained will determine the applications available to the users of the future light source. Since there is a public demand of hard X-rays for the experiments in the synchrotron community users from Mexico, in this work we studied the emission spectra from some hard X-ray sources which could be the best options for the parameters of the present Mexican synchrotron design. The calculations of the flux and the brightness for one Bending Magnet and four Insertion Devices are presented; specifically, for a Superconducting Bending Magnet (SBM), a Superconducting Wiggler (SCW), an In Vacuum Short Period Undulator (IV-SPU), a Superconducting Undulator (SCU) and for a Cryogenic Permanent Magnet Undulator (CPMU). Two commonly available synchrotron radiation programs were used for the computation (XOP and SRW). From the results, it can be concluded that the particle beam energy from the current design is enough to have one or more sources of hard X-rays. Furthermore, a wide range of hard X-ray region can be covered by the analyzed sources, and the choice of each type should be based on the specific characteristics of the X-ray beam to perform the experiments at the involved beamline. This work was done within the project Fomix Conacyt-Morelos ”Plan Estrategico para la construccion y operación de un Sincrotron en Morelos” (224392).

NSLS infra-red beam line (U3) conceptual design report

Energy Technology Data Exchange (ETDEWEB)

Williams, G.P.

1984-02-09

We describe the conceptual design of an infrared (I-R) beam line on the vacuum-ultra-violet storage ring of the National Synchrotron Light Source. The beam line forms part of the Phase II expansion of the NSLS. Consistent with the implementation of the current design is the extraction of hitherto wasted radiation and the establishment of a mezzanine floor or platform to make full use of the available headroom. This means that the I-R beam line, once established, does not interfere with any existing operations on the VUV floor.

The third generation French synchrotron

International Nuclear Information System (INIS)

Anon.

1997-01-01

This short paper gives a concise presentation of the SOLEIL project of the LURE synchrotron radiation national laboratory at Orsay (France). This new accelerator is devoted to replace the DCI and Super ACO rings of first and second generation, respectively. The main research domains of this project concern: the micro-fluorescence and micro-diffraction characterization of materials, and in particular the electronic components; the study of matter in extreme conditions (high temperature and high pressure); the bio-crystallography; the study of aggregates; and the manufacturing of micro-instruments for micro-electronics or medical applications. SOLEIL will be equipped with special magnetic wigglers to obtain very high brightness sources. The source will be a 336 m circumference ring for 2.5 GeV electron storage, able to produce a large spectrum synchrotron radiation. The injection system will comprise a low energy-high current linear electron accelerator and two electron beam transport lines. The installation will be buried at a 4 m depth to ensure the environmental protection and to limit vibrations. (J.S.)

Low-luminosity Blazars in Wise: A Mid-infrared View of Unification

Science.gov (United States)

Plotkin, Richard M.; Anderson, S. F.; Brandt, W. N.; Markoff, S.; Shemmer, O.; Wu, J.

2012-01-01

We use the preliminary data release from the Wide-Field Infrared Survey Explorer (WISE) to perform the first statistical study on the mid-infrared (IR) properties of a large number ( 102) of BL Lac objects -- low-luminosity Active Galactic Nuclei (AGN) with a jet beamed toward the Earth. As expected, many BL Lac objects are so highly beamed that their jet synchrotron emission dominates their IR spectral energy distributions (SEDs), and the shape of their SEDs in the IR correlates well with SED peak frequency. In other BL Lac objects, the jet is not strong enough to completely dilute the rest of the AGN, and we do not see observational signatures of the dusty torus from these weakly beamed BL Lac objects. While at odds with simple unification, the missing torus is consistent with recent suggestions that BL Lac objects are fed by radiatively inefficient accretion flows. We discuss implications on the ``nature vs. nurture" debate for FR I and FR II galaxies, and also on the standard orientation-based AGN unification model.

Synchrotron/crystal sample preparation

Science.gov (United States)

Johnson, R. Barry

1993-01-01

The Center for Applied Optics (CAO) of the University of Alabama in Huntsville (UAH) prepared this final report entitled 'Synchrotron/Crystal Sample Preparation' in completion of contract NAS8-38609, Delivery Order No. 53. Hughes Danbury Optical Systems (HDOS) is manufacturing the Advanced X-ray Astrophysics Facility (AXAF) mirrors. These thin-walled, grazing incidence, Wolter Type-1 mirrors, varying in diameter from 1.2 to 0.68 meters, must be ground and polished using state-of-the-art techniques in order to prevent undue stress due to damage or the presence of crystals and inclusions. The effect of crystals on the polishing and grinding process must also be understood. This involves coating special samples of Zerodur and measuring the reflectivity of the coatings in a synchrotron system. In order to gain the understanding needed on the effect of the Zerodur crystals by the grinding and polishing process, UAH prepared glass samples by cutting, grinding, etching, and polishing as required to meet specifications for witness bars for synchrotron measurements and for investigations of crystals embedded in Zerodur. UAH then characterized these samples for subsurface damage and surface roughness and figure.

Towards Establishing of National Centre of Synchrotron Radiation in Poland

International Nuclear Information System (INIS)

Kolodziej, J.J.; Szymonski, M.

2004-01-01

Synchrotron radiation facilities (SRF) are established part of contemporary world research landscape. They facilitate fast advances of life, health, and physical sciences as well as development of new technologies. The extent of synchrotron radiation (SR) use has been growing up steadily for the last two decades all over the world and it is anticipated that the growth will continue in future. Growing community of SR users has generated increasing demand for the beam-time in infrared, vacuum UV and X-ray ranges. In response, many new SR facilities are now being constructed and planned, not only in large countries of strong economy but also in developing countries. It is expected that such trends will be followed in other parts of the world. No doubt, the ''cutting edge'' of research activity will continue to create the demand for beams of higher brightness, flux and photon energy but it is predictable that the increasing fraction of research done presently with laboratory radiation sources will be shifting towards small-scale SR facilities. Several hundred Polish scientists, a meaningful fraction of all SR users, take part in experiments using synchrotron sources all over the world. Many of them belong to the Polish Synchrotron Radiation Society - an active body promoting the use of SR. Present European Union priorities include knowledge, research and innovation as the key priorities and a pillar of development and stable welfare of Europe. Poland as a new member of EU will have to conform to the EU policy. The government strategy assumes a fast increase of investments in research and development sector starting from 2005. No other scientific research installations has had such major impact on advances in science an technology as the SRF. It is obvious that the time is ripe now for establishing a National Centre of Synchrotron Radiation in Poland. Recently, several Polish educational and research institutions constituted around the idea of Polish SRF. The initiative

The Australian synchrotron

International Nuclear Information System (INIS)

Farhi, R.

2005-06-01

This document recalls the historical aspects of the Australian Synchrotron which will be implemented in 2007. It presents then the objectives of this program, the specifications of the ring and the light lines. (A.L.B.)

Synchrotron radiation and structural proteomics

CERN Document Server

Pechkova, Eugenia

2011-01-01

This book presents an overview of the current state of research in both synchrotron radiation and structural proteomics from different laboratories worldwide. The book presents recent research results in the most advanced methods of synchrotron radiation analysis, protein micro- and nano crystallography, X-ray scattering and X-ray optics, coherent X-Ray diffraction, and laser cutting and contactless sample manipulation are described in details. The book focuses on biological applications and highlights important aspects such as radiation damage and molecular modeling.

Dynamic response of a typical synchrotron magnet/girder assembly

International Nuclear Information System (INIS)

Jendrzejczyk, J.A.; Smith, R.K.; Vogt, M.E.

1993-06-01

In the Advanced Photon Source, the synchrotron booster ring accelerates positrons to the required energy level of 7 GeV. The positrons are then injected into the storage ring where they continue to orbit for 10--15 h. The storage ring quadrupoles have very stringent vibration criteria that must be satisfied to ensure that beam emittance growth is within acceptable limits, viz., <10%. Because the synchrotron booster ring is not operated after particle insertion into the storage ring, its vibration response is not a critical issue relative to the performance of the storage ring beam. Nevertheless, the synchrotron pulses at a frequency of 2 Hz, and if a vibration response frequency of the synchrotron magnet/girder assembly were to coincide with the pulsation frequency or its near harmonics, large-amplitude motion could result, with the effect that it could compromise the operation of the synchrotron. Due to the complex dynamics of the synchrotron magnet/girder assembly, it is necessary to measure the dynamic response of a prototypic assembly and its components to ensure that the inherent dynamic response frequencies are not equal to 2 Hz or any near harmonics. Dynamic-response measurement of the synchrotron girder assembly and component magnets is the subject of this report

Historical development of synchrotron x-ray diffraction topography

International Nuclear Information System (INIS)

Kawado, Seiji

2011-01-01

After a short history of X-ray diffraction topography, from the early stage of laboratory X-ray topography to recent synchrotron-radiation applications, is described, the development of science and technology for the synchrotron X-ray topography and its industrial applications are reviewed in more detail. In addition, the recent trend to synchrotron topography research is clarified on the basis of several data obtained from 256 papers which have been published since 2000. (author)

Synchrotron radiation X-ray microfluorescence techniques

Indian Academy of Sciences (India)

Synchrotron X-ray imaging systems with fluorescence techniques was developed for biomedical researches in Brazilian Synchrotron Laboratory. An X-ray fluorescence microtomography system was implemented to analyse human prostate and breast samples and an X-ray microfluorescence system was implemented to ...

The synchrotron light source ROSY

International Nuclear Information System (INIS)

Einfeld, D.; Buettig, H.; Dienel, S.; Glaeser, W.; Goetz, T.; Guratzsch, H.; Hartmann, B.; Janssen, D.; Krug, H.; Linnemann, J.; Matz, W.; Murphy, J.B.; Neumann, W.; Oehme, W.; Picard, M.; Plesko, M.; Proehl, D.; Schlenk, R.; Tomassini, D.; Tyrroff, H.

1994-01-01

ROSY, a 3rd generation synchrotron light source, has been proposed to be built at the Research Center Rossendorf/Dresden in Germany. With its low emittance and optimized space for installing insertion devices ROSY will be the first synchrotron radiation source in the 3 GeV range in Europe, dedicated to materials research and industrial application. The critical wavelength of the synchrotron radiation spectra was designed to be 0.15 nm corresponding to a critical photon energy of 8.4 keV. It is proposed to use a ''modified multiple bend achromat'' (MBA) lattice in order to get a compact machine as well as a low emittance. For 3 GeV an emittance smaller than 30π nm rad can be obtained. With a fourfold symmetry and two larger straight sections within the achromatic arcs the circumference is 148 m. 23% of the circumference can be used for installing insertion devices. (orig.)

The Beamline X28C of the Center for Synchrotron Biosciences: a National Resource for Biomolecular Structure and Dynamics Experiments Using Synchrotron Footprinting

International Nuclear Information System (INIS)

Gupta, S.; Sullivan, M.; Toomey, J.; Kiselar, J.; Chance, M.

2007-01-01

Structural mapping of proteins and nucleic acids with high resolution in solution is of critical importance for understanding their biological function. A wide range of footprinting technologies have been developed over the last ten years to address this need. Beamline X28C, a white-beam X-ray source at the National Synchrotron Light Source of Brookhaven National Laboratory, functions as a platform for synchrotron footprinting research and further technology development in this growing field. An expanding set of user groups utilize this national resource funded by the National Institute of Biomedical Imaging and Bioengineering of the National Institutes of Health. The facility is operated by the Center for Synchrotron Biosciences and the Center for Proteomics of Case Western Reserve University. The facility includes instrumentation suitable for conducting both steady-state and millisecond time-resolved footprinting experiments based on the production of hydroxyl radicals by X-rays. Footprinting studies of nucleic acids are routinely conducted with X-ray exposures of tens of milliseconds, which include studies of nucleic acid folding and their interactions with proteins. This technology can also be used to study protein structure and dynamics in solution as well as protein-protein interactions in large macromolecular complexes. This article provides an overview of the X28C beamline technology and defines protocols for its adoption at other synchrotron facilities. Lastly, several examples of published results provide illustrations of the kinds of experiments likely to be successful using these approaches

A VUV photoionization organic aerosol mass spectrometric study with synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Fang Wenzheng; Lei Gong; Shan Xiaobin; Liu Fuyi [School of Nuclear Science and Technology, National Synchrotron Radiation Laboratory, University of Science and Technology of China, Anhui, Hefei 230029 (China); Wang Zhenya [Laboratory of Environmental Spectroscopy, Anhui Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Hefei 230031 (China); Sheng Liusi, E-mail: lssheng@ustc.edu.cn [School of Nuclear Science and Technology, National Synchrotron Radiation Laboratory, University of Science and Technology of China, Anhui, Hefei 230029 (China)

2011-04-15

Research highlights: {yields} A photoionization aerosol time-of-flight mass spectrometer (ATOFMS) has been developed for on-line analysis of organic compounds in aerosol particles using tunable vacuum ultraviolet (VUV) synchrotron radiation. {yields} The degree of fragmentation of molecule can be controlled either by the heater temperature or by the photon energy. {yields} The direct determination of the IEs of benzopheneone (9.07 eV), salicylic acid (8.72 eV), and urea (9.85 eV) are measured from the photoionization efficiency spectra. {yields} The species can be identified by their molecular and fragment ions weights as well as by the comparisions between their theoretical and experimental ionization energies. - Abstract: A photoionization aerosol time-of-flight mass spectrometer (ATOFMS) has been developed for on-line analysis of organic compounds in aerosol particles using tunable vacuum ultraviolet (VUV) synchrotron radiation. Aerosol particles can be sampled directly from atmospheric pressure and are focused through an aerodynamic lens assembly into the mass spectrometer. The particles are vaporized when they impact on a heater, and then the nascent vapor is softly photoionized by synchrotron radiation. The degree of fragmentation of molecule can be controlled either by the heater temperature or by the photon energy. Thus, fragment-free tunable VUV mass spectra are obtained by tuning the photon energy close to the ionization energies (IEs) of the sample molecules. The direct determination of the IEs of benzophenone (9.07 eV), salicylic acid (8.72 eV), and urea (9.85 eV) are measured from the photoionization efficiency spectra with uncertainties of {+-}50 meV. Ab initio calculations have been employed to predict the theoretical ionization energy.

Infrared studies of the monoclinic-tetragonal phase transition in Pb(Zr,Ti)O3 ceramics

International Nuclear Information System (INIS)

Guarany, C A; Pelaio, L H Z; Araujo, E B; Yukimitu, K; Moraes, J C S; Eiras, J A

2003-01-01

Recently, the observation of a new monoclinic phase in the PbZr 1-x Ti x O 3 (PZT) system in the vicinity of the morphotropic phase boundary was reported. Investigations of this new phase were reported using different techniques such as high-resolution synchrotron x-ray powder diffraction and Raman spectroscopy. In this work, the monoclinic → tetragonal phase transition in PbZr 0.50 Ti 0.50 O 3 ceramics was studied using infrared spectroscopy between 1000 and 400 cm -1 . The four possible ν 1 -stretching modes (Ti-O and Zr-O stretch) in the BO 6 octahedron in the ABO 3 structure of PZT in this region were monitored as a function of temperature. The lower-frequency mode ν 1 -(Zr-O) remains practically unaltered, while both intermediate ν 1 -(Ti-O) modes decrease linearly as temperature increases from 89 to 263 K. In contrast, the higher-frequency ν 1 -(Ti-O) and ν 1 -(Zr-O) modes present anomalous behaviour around 178 K. The singularity observed at this mode was associated with the monoclinic → tetragonal phase transition in PbZr 0.50 Ti 0.50 O 3 ceramics

Synchrotron radiation resonance Raman spectroscopy (SR3S)

International Nuclear Information System (INIS)

Hester, R.E.

1979-01-01

The use of normal Raman spectroscopy and resonance Raman spectroscopy to study the structure of molecular species and the nature of their chemical bonds is discussed. The availability of a fully tunable radiation source (the Synchrotron Radiation Source) extending into the ultraviolet raises the possibility of using synchrotron radiation resonance Raman spectroscopy as a sensitive and specific analytical probe. The pulsed nature of the SRS beam may be exploited for time-resolved resonance Raman spectroscopy and its high degree of polarization could be very helpful in the interpretation of spectra. The possibilities are considered under the headings: intensity requirements and comparison with other sources; some applications (e.g. structure of proteins; study of iron-porphyrin unit; study of chlorophylls). (U.K.)

Tracking calcification in tissue-engineered bone using synchrotron micro-FTIR and SEM.

Science.gov (United States)

Deegan, Anthony J; Cinque, Gianfelice; Wehbe, Katia; Konduru, Sandeep; Yang, Ying

2015-02-01

One novel tissue engineering approach to mimic in vivo bone formation is the use of aggregate or micromass cultures. Various qualitative and quantitative techniques, such as histochemical staining, protein assay kits and RT-PCR, have been used previously on cellular aggregate studies to investigate how these intricate arrangements lead to mature bone tissue. However, these techniques struggle to reveal spatial and temporal distribution of proliferation and mineralization simultaneously. Synchrotron-based Fourier transform infrared microspectroscopy (micro-FTIR) offers a unique insight at the molecular scale by coupling high IR sensitivity to organic matter with the high spatial resolution allowed by diffraction limited SR microbeam. This study is set to investigate the effects of culture duration and aggregate size on the dynamics and spatial distribution of calcification in engineered bone aggregates by a combination of micro-FTIR and scanning electron microscopy (SEM)/energy-dispersive X-ray spectroscopy (EDX). A murine bone cell line has been used, and small/large bone aggregates have been induced using different chemically treated culture substrates. Our findings suggest that bone cell aggregate culturing can greatly increase levels of mineralization over short culture periods. The size of the aggregates influences mineralisation rates with larger aggregates mineralizing at a faster rate than their smaller counterparts. The micro-FTIR mapping has demonstrated that mineralization in the larger aggregates initiated from the periphery and spread to the centre, whilst the smaller aggregates have more minerals in the centre at the early stage and deposited more in the periphery after further culturing, implying that aggregate size influences calcification distribution and development over time. SEM/EDX data correlates well with the micro-FTIR results for the total mineral content. Thus, synchrotron-based micro-FTIR can accurately track mineralization process

Preparation of solid-state samples of a transition metal coordination compound for synchrotron radiation photoemission studies

CERN Document Server

Crotti, C; Celestino, T; Fontana, S

2003-01-01

The aim of this research was to identify a sample preparation method suitable for the study of transition metal complexes by photoemission spectroscopy with synchrotron radiation as the X-ray source, even in the case where the compound is not evaporable. Solid-phase samples of W(CO) sub 4 (dppe) [dppe=1,2-bis(diphenylphosphino)ethane] were prepared according to different methods and their synchrotron radiation XPS spectra measured. The spectra acquired from samples prepared by spin coating show core level peaks only slightly broader than the spectrum recorded from UHV evaporated samples. Moreover, for these samples the reproducibility of the binding energy values is excellent. The dependence of the spin coating technique on parameters such as solvent and solution concentration, spinning speed and support material was studied. The same preparation method also allowed the acquisition of valence band spectra, the main peaks of which were clearly resolved. The results suggest that use of the spin coating techniqu...

Infrared studies of two dark clouds

International Nuclear Information System (INIS)

Elias, J.H.

1978-01-01

The IC5146 dark cloud complex was surveyed in the infrared in order to identify and study associated young stellar objects. Most of the objects detected in the survey appears to be field stars, predominantly late-type giants. Three young objects were detected in the survey: the BO star BD + 46 x 3474, the Ae star BD + 46 x 3471, and a previously unidentified object which appear to be a heavily obscured FU Ori star. The properties of the last two objects are examined in detail, and an attempt is made to produce reasonable models for them. It is suggested that FU Ori stars are binaries, and some consequences of this model are described. Photometry of the brighter stars in the IC5146 cluster was used to establish a distance to the cluster of 900 +- 100 pc. A near-infrared survey was also conducted of nearly 18 square degrees of the Ophiuchus dark cloud complex. Additional observations were made of selected objects found in this region, in order to identify and study the young stars associated with the cloud. These observations show that very recent star formation has been largely restricted to a small region no more than a few parsecs in extent at the center of the dark cloud complex. Most of the young stars do not appear to be main sequence stars. At least three of these objects appear to be surrounded by infrared reflection nebulae. Many of the objects studies are background K and M giants which can be used to determine the near-infrared extinction due to the dark cloud

Control circuits for the 1.3 GeV electron synchrotron

International Nuclear Information System (INIS)

Asaoka, S.; Shiino, K.; Yoshioka, M.; Norimura, K.

1980-01-01

Following control circuits for the 1.3 GeV electron synchrotron, Institute for Nuclear Study, University of Tokyo, have been designed and constructed. 1. Variable delay circuits for the timing pulse of the synchrotron. 2. An alarm circuit for sputter ion pumps. 3. A sample and hold circuit for digital display and computer control of the beam intensity. This report describes detailes of the circuits and their specificatons. (author)

Early British synchrotrons, an informal history

International Nuclear Information System (INIS)

Lawson, J.D.

1997-02-01

An historical account of the design and construction of early synchrotrons in the United Kingdom, based partly on personal reminiscences, is presented. Material is also drawn from archives at Birmingham and CERN. The document covers the period from plans for the world's first synchrotron at Malvern after the Second World War to work done at Harwell Laboratory for CERN in the period 1951-1953. (UK)

Improved mid infrared detector for high spectral or spatial resolution and synchrotron radiation use

Energy Technology Data Exchange (ETDEWEB)

Faye, Mbaye; Bordessoule, Michel; Kanouté, Brahim; Brubach, Jean-Blaise; Roy, Pascale [Synchrotron SOLEIL, L’Orme des Merisiers, F-91192 Gif-sur-Yvette (France); Manceron, Laurent [Synchrotron SOLEIL, L’Orme des Merisiers, F-91192 Gif-sur-Yvette (France); Laboratoire MONARIS, CNRS-Université Pierre et Marie Curie, UMR 8233, 4 Place Jussieu, F-75252 Paris Cedex (France)

2016-06-15

When using bright, small effective size sources, such as synchrotron radiation light beam, for broadband spectroscopy at spectral or spatial high resolution for mid-IR FTIR measurements, a marked detectivity improvement can be achieved by setting up a device matching the detector optical étendue to that of the source. Further improvement can be achieved by reducing the background unmodulated flux and other intrinsic noise sources using a lower temperature cryogen, such as liquid helium. By the combined use of cooled apertures, cold reimaging optics, filters and adapted detector polarization, and preamplification electronics, the sensitivity of a HgCdTe photoconductive IR detector can be improved by a significant factor with respect to standard commercial devices (more than one order of magnitude on average over 6–20 μm region) and the usable spectral range extended to longer wavelengths. The performances of such an optimized detector developed on the AILES Beamline at SOLEIL are presented here.

Synchrotron radiation techniques for the characterization of Nb$_{3}$Sn superconductors

CERN Document Server

Scheuerlein, C; Buta, F

2009-01-01

The high flux of high energy x-rays that can be provided through state-of-the-art high energy synchrotron beam lines has enabled a variety of new experiments with the highly absorbing Nb$_{3}$Sn superconductors. We report different experiments with Nb$_{3}$Sn strands that have been conducted at the ID15 High Energy Scattering beam line of the European Synchrotron Radiation Facility (ESRF). Synchrotron x-ray diffraction has been used in order to monitor phase transformations during in-situ reaction heat treatments prior to Nb$_{3}$Sn formation, and to monitor Nb$_{3}$Sn growth. Fast synchrotron micro-tomography was applied to study void growth during the reaction heat treatment of Internal Tin strands. The elastic strain in the different phases of fully reacted Nb$_{3}$Sn composite conductors can be measured by high resolution x-ray diffraction during in-situ tensile tests.

Infrared spectrum and compressibility of Ti3GeC2 to 51 GPa

International Nuclear Information System (INIS)

Manoun, Bouchaib; Yang, H.; Saxena, S.K.; Ganguly, A.; Barsoum, M.W.; El Bali, B.; Liu, Z.X.; Lachkar, M.

2007-01-01

Using a synchrotron radiation source and a diamond anvil cell, we measured the pressure dependence of the lattice parameters of a polycrystalline Ti 3 GeC 2 sample up to a pressure of 51 GPa. No phase transformations were observed. Like Ti 3 SiC 2 , and most other compounds belonging to the same family of ternary carbides and nitrides, the so-called MAX phases, the compressibility of Ti 3 GeC 2 along the c axis is greater than that along the a axis. The bulk modulus is 197 ± 4 GPa, with a pressure derivative of 3.4 ± 0.1. We also characterized Ti 3 GeC 2 by infrared spectroscopy; four of the five expected infrared modes were observed for this material

Propagation of synchrotron radiation through nanocapillary structures

International Nuclear Information System (INIS)

Bjeoumikhov, A.; Bjeoumikhova, S.; Riesemeier, H.; Radtke, M.; Wedell, R.

2007-01-01

The propagation of synchrotron radiation through nanocapillary structures with channel sizes of 200 nm and periods in the micrometer size has been studied experimentally. It was shown that the propagation through individual capillary channels has a mode formation character. Furthermore it was shown that during the propagation through capillary channels the coherence of synchrotron radiation is partially conserved. Interference of beams propagating through different capillary channels is observed which leads to a periodically modulated distribution of the radiation intensity in a plane far from the exit of the structure. These investigations are of high relevance for the understanding of X-ray transmission through nanocapillaries and the appearance of wave properties at this size scale

The exploitation of the Saturne synchrotron during the forth quarter of 1960; L'exploitation du synchrotron Saturne pendant le 4eme trimestre 1960

Energy Technology Data Exchange (ETDEWEB)

NONE

1961-01-15

This document reports information and data regarding the operation of the Saturne synchrotron during the fourth quarter of 1960. It addresses the machine operation (acceleration cycles, beam intensity, technical incidents, time table), hardware studies (corrector circuit under high fields, intensity increase), physics experiments (on counters, in bubble chambers, target irradiation), measures and measurements regarding the protection against radiations (comparison of irradiation levels in different areas of the synchrotron, annual evolution), the liquefactor activity (nitrogen and hydrogen consumption and production data)

Recent developments in photoelectron dynamics using synchrotron radiation

International Nuclear Information System (INIS)

Carlson, T.A.; Krause, M.O.; Taylor, J.W.; Keller, P.R.; Piancastelli, M.N.; Grimm, F.A.; Whitley, T.A.

1982-01-01

Through a collaborative effort of members of the Oak Ridge National Laboratory and Universities of Wisconsin and Tennessee, a comprehensive study of atoms and molecules using angle-resolved photoelectron spectroscopy and synchrotron radiation is underway at the Synchrotron Radiation Center, Stoughton, Wisconsin. Over 50 molecules and atoms have been investigated. These results, coupled with theory, aim at a better understanding of the dynamics of photoionization and of the wave functions that control these processes. In particular, attention is given to the following topics: metal atomic vapors, generalization of molecular orbital types, autoionization, shape resonances, core shell effects, satellite structure, and the Cooper minimum

LNLS - Brazilian Synchrotron Light Laboratory Activity Report 2005

Energy Technology Data Exchange (ETDEWEB)

NONE

2005-07-01

This activity report highlight the activities as follows: atomic local order of hafnium and silicon in dielectric films; development of bio absorbent for arsenite; insights into enzyme-substrate interaction; investigation of metastable phases in zirconia-ceria nano-ceramics by synchrotron X-ray powder diffraction; lattice distortion effects on magneto-structural phase transition of Mn As; mechanism of orbital ordering in transition-metal oxides; organic molecules in star-forming regions; spatially ordered In P dots grown on compositionally modulated In Ga P layers; structural insights into {beta}-Xylosidase from Trichoderma reesei, and surface random alloys studied by synchrotron based photoelectron diffraction.

Current status of Hiroshima Synchrotron Radiation Center

International Nuclear Information System (INIS)

Taniguchi, Masaki

2000-01-01

The Hiroshima Synchrotron Radiation Center is a common facility for both research and education in the field of synchrotron radiation science. The role of the center is to promote original research, training of young scientists, international exchange and cooperative research with neighbouring universities, public organizations and industries. (author)

National Synchrotron Light Source 2008 Activity Report

International Nuclear Information System (INIS)

Nasta, K.

2009-01-01

Funded by the U.S. Department of Energy's Office of Basic Energy Sciences, the National Synchrotron Light Source (NSLS) is a national user facility that operates two electron storage rings: X-Ray (2.8 GeV, 300 mA) and Vacuum Ultraviolet (VUV) (800 mev, 1.0A). These two rings provide intense light spanning the electromagnetic spectrum -- from very long infrared rays to ultraviolet light and super-short x-rays -- to analyze very small or highly dilute samples. The properties of this light, and the specially designed experimental stations, called beamlines, allow scientists in many diverse disciplines of research to perform experiments not possible at their own laboratories. Each year, about 2,200 scientists from more than 400 universities and companies use the NSLS for research in such diverse fields as biology, physics, chemistry, geology, medicine, and environmental and materials sciences. For example, researchers have used the NSLS to examine the minute details of computer chips, decipher the structures of viruses, probe the density of bone, determine the chemical composition of moon rocks, and reveal countless other mysteries of science. The facility has 65 operating beamlines, with 51 beamlines on the X-Ray Ring and 14 beamlines on the VUV-Infrared Ring. It runs seven days a week, 24 hours a day throughout the year, except during periods of maintenance and studies. Researchers are not charged for beam time, provided that the research results are published in open literature. Proprietary research is conducted on a full-cost-recovery basis. With close to 1,000 publications per year, the NSLS is one of the most prolific scientific facilities in the world. Among the many accolades given to its users and staff, the NSLS has won nine R and D 100 Awards for innovations ranging from a closed orbit feedback system to the first device able to focus a large spread of high-energy x-rays. In addition, a visiting NSLS researcher shared the 2003 Nobel Prize in Chemistry for

National Synchrotron Light Source 2008 Activity Report

Energy Technology Data Exchange (ETDEWEB)

Nasta,K.

2009-05-01

Funded by the U.S. Department of Energy's Office of Basic Energy Sciences, the National Synchrotron Light Source (NSLS) is a national user facility that operates two electron storage rings: X-Ray (2.8 GeV, 300 mA) and Vacuum Ultraviolet (VUV) (800 mev, 1.0A). These two rings provide intense light spanning the electromagnetic spectrum -- from very long infrared rays to ultraviolet light and super-short x-rays -- to analyze very small or highly dilute samples. The properties of this light, and the specially designed experimental stations, called beamlines, allow scientists in many diverse disciplines of research to perform experiments not possible at their own laboratories. Each year, about 2,200 scientists from more than 400 universities and companies use the NSLS for research in such diverse fields as biology, physics, chemistry, geology, medicine, and environmental and materials sciences. For example, researchers have used the NSLS to examine the minute details of computer chips, decipher the structures of viruses, probe the density of bone, determine the chemical composition of moon rocks, and reveal countless other mysteries of science. The facility has 65 operating beamlines, with 51 beamlines on the X-Ray Ring and 14 beamlines on the VUV-Infrared Ring. It runs seven days a week, 24 hours a day throughout the year, except during periods of maintenance and studies. Researchers are not charged for beam time, provided that the research results are published in open literature. Proprietary research is conducted on a full-cost-recovery basis. With close to 1,000 publications per year, the NSLS is one of the most prolific scientific facilities in the world. Among the many accolades given to its users and staff, the NSLS has won nine R&D 100 Awards for innovations ranging from a closed orbit feedback system to the first device able to focus a large spread of high-energy x-rays. In addition, a visiting NSLS researcher shared the 2003 Nobel Prize in Chemistry for

Photo absorption studies of polyatomic molecules using Indus 1 synchrotron radiation source

International Nuclear Information System (INIS)

Saraswathy, P.; Sunanda, K.; Aparna, S.; Rajashekar, B.N.; Das, N.C.

2004-06-01

The Photophysics beamline is a medium resolution beamline designed for carrying out photo absorption and fluorescence experiments using the synchrotron radiation source Indus-l. This beamline has been commissioned recently and is in operation. An experimental setup for gas phase absorption studies has been developed and installed. Absorption spectra of a few polyatomicmolecules viz. benzene, ammonia, carbon disulphide and acetone were recorded in the wavelength region 1500 -3000 A. The results from this study indicated the satisfactory performance of the beam line as well as the experimental setup. Details of the first set of absorption experiments carried out are discussed in this report. (author)

Synchrotron SAXS studies of nanostructured materials and colloidal solutions: a review

International Nuclear Information System (INIS)

Craievich, A.F.

2002-01-01

Structural characterisations using the SAXS technique in a number of nano heterogeneous materials and liquid solutions are reviewed. The studied systems are protein (lysozyme)/water solutions, colloidal Zn O particles/water sols, nano porous Ni O-based xerogels, hybrid organic-inorganic siloxane-PEG and PPG nano composites and PbTe semiconductor nano crystals embedded in a glass matrix. These investigations also focus on the transformations of time-varying structures and on structural changes related to variations in temperature and composition. The reviewed investigations aim at explaining the unusual and often interesting properties of nano structured materials and solutions. Most of the reported studies were carried out using the SAXS beamline at the National Synchrotron Light Laboratory (LNLS), Campinas, Brazil.(author)

DELSY project: status and development Dubna Electron Synchrotron

CERN Document Server

Balalykin, N; Bykovsky, V

2003-01-01

The DELSY (Dubna Electron Synchrotron) project is under development at the Joint Institute for Nuclear Research. It is based on an acceleration facility donated to the Joint Institute for Nuclear Research by the Institute for Nuclear and High Energy Physics (NIKHEF, Amsterdam). The NIKHEF accelerator facility consists of the linear electron accelerator MEA, which has an electron energy of 700 MeV, and the electron storage ring AmPS, with a maximum energy of 900 MeV and a beam current of 200 mA. There are three phases to the construction of the DELSY facility. Phase I will be accomplished with the construction of a complex of free-electron lasers covering continuously the spectrum from the far infrared down to the ultraviolet (approx 150 nm). Phase II will be accomplished with the commissioning of the storage ring DELSY. Complete commissioning of the DELSY project will take place after finishing Phase III, the construction of an X-ray free-electron laser. This phase is considered as the ultimate goal of the pr...

Microangiography in Living Mice Using Synchrotron Radiation

International Nuclear Information System (INIS)

Yuan Falei; Wang Yongting; Xie Bohua; Tang Yaohui; Guan Yongjing; Lu Haiyan; Yang Guoyuan; Xie Honglan; Du Guohao; Xiao Tiqiao

2010-01-01

Traditionally, there are no methods available to detect the fine morphologic changes of cerebrovasculature in small living animals such as rats and mice. Newly developed synchrotron radiation microangiography can achieve a fine resolution of several micrometers and had provided us with a powerful tool to study the cerebral vasculature in small animals. The purpose of this study is to identify the morphology of cerebrovasculature especially the structure of Lenticulostriate arteries (LSAs) in living mice using the synchrotron radiation source at Shanghai Synchrotron Radiation Facility (SSRF) in Shanghai, China. Adult CD-1 mice weighing 35-40 grams were anesthetized. Nonionic iodine (Omnipaque, 350 mg I /mL) was used as a contrast agent. The study was performed at the BL13W1 beam line at SSRF. The beam line was derived from a storage ring of electrons with an accelerated energy of 3.5 GeV and an average beam current of 200 mA. X-ray energy of 33.3 keV was used to produce the highest contrast image. Images were acquired every 172 ms by a x-ray camera (Photonic-Science VHR 1.38) with a resolution of 13 μm/pixel. The optimal dose of contrast agent is 100 μl per injection and the injecting rate is 33 μl/sec. The best position for imaging is to have the mouse lay on its right or left side, with ventral side facing the X-ray source. We observed the lenticulostriate artery for the first time in living mice. Our result show that there are 4 to 5 lenticulostriate branches originating from the root of middle cerebral artery in each hemisphere. LSAs have an average diameter of 43±6.8 μm. There were no differences between LSAs from the left and right hemisphere (p<0.05). These results suggest that synchrotron radiation may provide a unique tool for experimental stroke research.

Microangiography in Living Mice Using Synchrotron Radiation

Science.gov (United States)

Yuan, Falei; Wang, Yongting; Guan, Yongjing; Lu, Haiyan; Xie, Bohua; Tang, Yaohui; Xie, Honglan; Du, Guohao; Xiao, Tiqiao; Yang, Guo-Yuan

2010-07-01

Traditionally, there are no methods available to detect the fine morphologic changes of cerebrovasculature in small living animals such as rats and mice. Newly developed synchrotron radiation microangiography can achieve a fine resolution of several micrometers and had provided us with a powerful tool to study the cerebral vasculature in small animals. The purpose of this study is to identify the morphology of cerebrovasculature especially the structure of Lenticulostriate arteries (LSAs) in living mice using the synchrotron radiation source at Shanghai Synchrotron Radiation Facility (SSRF) in Shanghai, China. Adult CD-1 mice weighing 35-40 grams were anesthetized. Nonionic iodine (Omnipaque, 350 mg I /mL) was used as a contrast agent. The study was performed at the BL13W1 beam line at SSRF. The beam line was derived from a storage ring of electrons with an accelerated energy of 3.5 GeV and an average beam current of 200 mA. X-ray energy of 33.3 keV was used to produce the highest contrast image. Images were acquired every 172 ms by a x-ray camera (Photonic-Science VHR 1.38) with a resolution of 13 μm/pixel. The optimal dose of contrast agent is 100 μl per injection and the injecting rate is 33 μl/sec. The best position for imaging is to have the mouse lay on its right or left side, with ventral side facing the X-ray source. We observed the lenticulostriate artery for the first time in living mice. Our result show that there are 4 to 5 lenticulostriate branches originating from the root of middle cerebral artery in each hemisphere. LSAs have an average diameter of 43±6.8 μm. There were no differences between LSAs from the left and right hemisphere (p<0.05). These results suggest that synchrotron radiation may provide a unique tool for experimental stroke research.

Synchrotron control system of the HIMAC

International Nuclear Information System (INIS)

Takada, E.; Sato, K.; Itano, A.

1994-01-01

A structural design synopsis and the present status of the HIMAC synchrotron control system are described. The control system comprises of Timing System, (ring magnet) Power-supply Controller, Programmable Logic Controller, Static Var Compensator controller, Monitor Controller, RF control computer, Beam Transport control computer and the synchrotron main computer (denoted as CS, hereafter) that forms a local area cluster with man-machine interfacing computers, and communicates with HIMAC supervisor computer. (author)

Recent Developments in Synchrotron Moessbauer Reflectometry

Energy Technology Data Exchange (ETDEWEB)

Deak, L.; Bottyan, L.; Major, M.; Nagy, D. L. [KFKI Research Institute for Particle and Nuclear Physics (Hungary); Spiering, H. [Johannes Gutenberg Universitaet, Mainz, Institute fuer Anorganische und Analytische Chemie (Germany); Szilagyi, E.; Tancziko, F. [KFKI Research Institute for Particle and Nuclear Physics (Hungary)

2002-12-15

Synchrotron Moessbauer Reflectometry (SMR), the grazing incidence nuclear resonant scattering of synchrotron radiation, can be applied to perform depth-selective phase analysis and to determine the isotopic and magnetic structure of thin films and multilayers. Principles and methodological aspects of SMR are briefly reviewed. Off-specular SMR provides information from the lateral structure of multilayers. In anti-ferromagneticly coupled systems the size of magnetic domains can be measured.

Femtosecond infrared spectroscopy: study, development and applications

International Nuclear Information System (INIS)

Bonvalet, Adeline

1997-01-01

This work has been devoted to the development and the applications of a new technique of infrared (5-20 μm) spectroscopy allowing a temporal resolution of 100 fs. This technique relies on a source of ultrashort infrared pulses obtained by frequency mixing in a nonlinear material. In particular, the optical rectification of 12-fs visible pulses in gallium arsenide has allowed us to obtain 40-fs infrared pulses with a spectrum extending from 5 pm up to 15 μm. Spectral resolution has been achieved by Fourier transform spectroscopy, using a novel device we have called Diffracting FTIR. These developments allow to study inter-subband transitions in quantum-well structures. The inter-subband relaxation time has been measured by a pump-probe experiment, in which the sample was excited with a visible pulse, and the variations of inter-subband absorption probed with an infrared pulse. Besides, we have developed a method of coherent emission spectroscopy allowing to monitor the electric field emitted by coherent charge oscillations in quantum wells. The decay of the oscillations due to the loss of coherence between excited levels yields a direct measurement of the dephasing time between these levels. Other applications include biological macromolecules like reaction centers of photosynthetic bacteria. We have shown that we were able to monitor variations of infrared absorption of about 10 -4 optical densities with a temporal resolution of 100 fs. This would constitute a relevant tool to study the role of molecular vibrations during the primary steps of biological processes. (author) [fr

Synchrotron-based radioscopy employing spatio-temporal micro-resolution for studying fast phenomena in liquid metal foams

International Nuclear Information System (INIS)

Rack, A.; García-Moreno, F.; Baumbach, T.; Banhart, J.

2009-01-01

High-speed synchrotron-based radioscopy is applied to study a coalescence event (which lasts ∼2 ms) in situ in a liquid metal foam. Investigations of pore coalescence and individual cell wall collapse in an expanding liquid metal foam by means of X-ray radioscopy with spatio-temporal micro-resolution are reported. By using white synchrotron radiation for imaging, the rupture of a film and the subsequent merger of two neighbouring bubbles could be recorded with a time sampling rate of 40000 frames s −1 (25 µs exposure time) and a spatial sampling rate of 20 µm. The rupture time of a cell wall was found to be in the range of 300 µs. This value is in agreement with theoretical considerations which assume an inertia-dominated rupture time of cell walls in liquid metal foams

''Use of synchrotron radiation in France: present status and perspectives''

International Nuclear Information System (INIS)

Thiry, P.

1996-01-01

LURE (laboratory for the use of electromagnetic radiation) plays an important role as a research center, as a synchrotron radiation producer and as a leading pole about new light source studies. The necessity to maintain LURE at a high level of technological competitiveness implies to build a new facility called SOLEIL. This article describes the present equipment of LURE, its activity fields and draws the prospect of synchrotron radiation in France. (A.C.)

Efficiency of Synchrotron Radiation from Rotation-powered Pulsars

Energy Technology Data Exchange (ETDEWEB)

Kisaka, Shota [Department of Physics and Mathematics, Aoyama Gakuin University, Sagamihara, Kanagawa, 252-5258 (Japan); Tanaka, Shuta J., E-mail: kisaka@phys.aoyama.ac.jp, E-mail: sjtanaka@center.konan-u.ac.jp [Department of Physics, Konan University, Kobe, Hyogo, 658-8501 (Japan)

2017-03-01

Synchrotron radiation is widely considered to be the origin of the pulsed non-thermal emissions from rotation-powered pulsars in optical and X-ray bands. In this paper, we study the synchrotron radiation emitted by the created electron and positron pairs in the pulsar magnetosphere to constrain the energy conversion efficiency from the Poynting flux to the particle energy flux. We model two pair creation processes, two-photon collision, which efficiently works in young γ -ray pulsars (≲10{sup 6} year), and magnetic pair creation, which is the dominant process to supply pairs in old pulsars (≳10{sup 6} year). Using the analytical model, we derive the maximum synchrotron luminosity as a function of the energy conversion efficiency. From the comparison with observations, we find that the energy conversion efficiency to the accelerated particles should be an order of unity in the magnetosphere, even though we make a number of the optimistic assumptions to enlarge the synchrotron luminosity. In order to explain the luminosity of the non-thermal X-ray/optical emission from pulsars with low spin-down luminosity L {sub sd} ≲ 10{sup 34} erg s{sup −1}, non-dipole magnetic field components should be dominant at the emission region. For the γ -ray pulsars with L {sub sd} ≲ 10{sup 35} erg s{sup −1}, observed γ -ray to X-ray and optical flux ratios are much higher than the flux ratio between curvature and the synchrotron radiations. We discuss some possibilities such as the coexistence of multiple accelerators in the magnetosphere as suggested from the recent numerical simulation results. The obtained maximum luminosity would be useful to select observational targets in X-ray and optical bands.

X-Ray-induced Deuterium Enrichment of N-rich Organics in Protoplanetary Disks: An Experimental Investigation Using Synchrotron Light

Energy Technology Data Exchange (ETDEWEB)

Gavilan, Lisseth; Carrasco, Nathalie [LATMOS, Université Versailles St Quentin, UPMC Université Paris 06, CNRS, 11 blvd d’Alembert, F-78280 Guyancourt (France); Remusat, Laurent; Roskosz, Mathieu [IMPMC, CNRS UMR 7590, Sorbonne Universités, UPMC Université Paris 06, IRD, Muséum National d’Histoire Naturelle, CP 52, 57 rue Cuvier, Paris F-75231 (France); Popescu, Horia; Jaouen, Nicolas [SEXTANTS beamline, SOLEIL synchrotron, L’Orme des Merisiers, F-91190 Saint-Aubin (France); Sandt, Christophe [SMIS beamline, SOLEIL synchrotron, L’Orme des Merisiers, F-91190 Saint-Aubin (France); Jäger, Cornelia [Laboratory Astrophysics and Cluster Physics Group of the Max Planck Institute for Astronomy at the Friedrich Schiller University and Institute of Solid State Physics, Helmholtzweg 3, D-07743 Jena (Germany); Henning, Thomas [Max-Planck Institute for Astronomy Königstuhl 17, D-69117 Heidelberg (Germany); Simionovici, Alexandre [Institut des Sciences de la Terre, Observatoire des Sciences de l’Univers de Grenoble, BP 53, F-38041 Grenoble (France); Lemaire, Jean Louis [Institut des Sciences Moléculaires d’Orsay (ISMO), CNRS, Univ. Paris Sud, Université Paris-Saclay, F-91405 Orsay (France); Mangin, Denis, E-mail: lisseth.gavilan@latmos.ipsl.fr [Institut Jean Lamour, CNRS, Université de Lorraine, F-54011 Nancy (France)

2017-05-01

The deuterium enrichment of organics in the interstellar medium, protoplanetary disks, and meteorites has been proposed to be the result of ionizing radiation. The goal of this study is to simulate and quantify the effects of soft X-rays (0.1–2 keV), an important component of stellar radiation fields illuminating protoplanetary disks, on the refractory organics present in the disks. We prepared tholins, nitrogen-rich organic analogs to solids found in several astrophysical environments, e.g., Titan’s atmosphere, cometary surfaces, and protoplanetary disks, via plasma deposition. Controlled irradiation experiments with soft X-rays at 0.5 and 1.3 keV were performed at the SEXTANTS beamline of the SOLEIL synchrotron, and were immediately followed by ex-situ infrared, Raman, and isotopic diagnostics. Infrared spectroscopy revealed the preferential loss of singly bonded groups (N–H, C–H, and R–N≡C) and the formation of sp{sup 3} carbon defects with signatures at ∼1250–1300 cm{sup −1}. Raman analysis revealed that, while the length of polyaromatic units is only slightly modified, the introduction of defects leads to structural amorphization. Finally, tholins were measured via secondary ion mass spectrometry to quantify the D, H, and C elemental abundances in the irradiated versus non-irradiated areas. Isotopic analysis revealed that significant D-enrichment is induced by X-ray irradiation. Our results are compared to previous experimental studies involving the thermal degradation and electron irradiation of organics. The penetration depth of soft X-rays in μ m-sized tholins leads to volume rather than surface modifications: lower-energy X-rays (0.5 keV) induce a larger D-enrichment than 1.3 keV X-rays, reaching a plateau for doses larger than 5 × 10{sup 27} eV cm{sup −3}. Synchrotron fluences fall within the expected soft X-ray fluences in protoplanetary disks, and thus provide evidence of a new non-thermal pathway to deuterium fractionation of

X-Ray-induced Deuterium Enrichment of N-rich Organics in Protoplanetary Disks: An Experimental Investigation Using Synchrotron Light

Science.gov (United States)

Gavilan, Lisseth; Remusat, Laurent; Roskosz, Mathieu; Popescu, Horia; Jaouen, Nicolas; Sandt, Christophe; Jäger, Cornelia; Henning, Thomas; Simionovici, Alexandre; Lemaire, Jean Louis; Mangin, Denis; Carrasco, Nathalie

2017-05-01

The deuterium enrichment of organics in the interstellar medium, protoplanetary disks, and meteorites has been proposed to be the result of ionizing radiation. The goal of this study is to simulate and quantify the effects of soft X-rays (0.1-2 keV), an important component of stellar radiation fields illuminating protoplanetary disks, on the refractory organics present in the disks. We prepared tholins, nitrogen-rich organic analogs to solids found in several astrophysical environments, e.g., Titan’s atmosphere, cometary surfaces, and protoplanetary disks, via plasma deposition. Controlled irradiation experiments with soft X-rays at 0.5 and 1.3 keV were performed at the SEXTANTS beamline of the SOLEIL synchrotron, and were immediately followed by ex-situ infrared, Raman, and isotopic diagnostics. Infrared spectroscopy revealed the preferential loss of singly bonded groups (N-H, C-H, and R-N≡C) and the formation of sp3 carbon defects with signatures at ˜1250-1300 cm-1. Raman analysis revealed that, while the length of polyaromatic units is only slightly modified, the introduction of defects leads to structural amorphization. Finally, tholins were measured via secondary ion mass spectrometry to quantify the D, H, and C elemental abundances in the irradiated versus non-irradiated areas. Isotopic analysis revealed that significant D-enrichment is induced by X-ray irradiation. Our results are compared to previous experimental studies involving the thermal degradation and electron irradiation of organics. The penetration depth of soft X-rays in μm-sized tholins leads to volume rather than surface modifications: lower-energy X-rays (0.5 keV) induce a larger D-enrichment than 1.3 keV X-rays, reaching a plateau for doses larger than 5 × 1027 eV cm-3. Synchrotron fluences fall within the expected soft X-ray fluences in protoplanetary disks, and thus provide evidence of a new non-thermal pathway to deuterium fractionation of organic matter.

Second meeting of the Scientific Societies for the feasibility study of implantation of a synchrotron radiation national laboratory

International Nuclear Information System (INIS)

1984-01-01

Feasibility study for the implantation of a national laboratory of synchrotron radiation in Brazil is discussed by several Brazilian Scientific Societies. Problems related with cost, personnel training and machine uses are presented. (L.C.) [pt

Advances and synergy of high pressure sciences at synchrotron sources

International Nuclear Information System (INIS)

Liu, H.; Ehm, L.; Duffy, T.; Crichton, W.; Aoki, K.

2009-01-01

Introductory overview to the special issue papers on high-pressure sciences and synchrotron radiation. High-pressure research in geosciences, materials science and condensed matter physics at synchrotron sources is experiencing growth and development through synergistic efforts around the world. A series of high-pressure science workshops were organized in 2008 to highlight these developments. One of these workshops, on 'Advances in high-pressure science using synchrotron X-rays', was held at the National Synchrotron Light Source (NSLS), Brookhaven National Laboratory, USA, on 4 October 2008. This workshop was organized in honour of Drs Jingzhu Hu and Quanzhong Guo in celebration of their retirement after up to 18 years of dedicated service to the high-pressure community as beamline scientists at X17 of NSLS. Following this celebration of the often unheralded role of the beamline scientist, a special issue of the Journal of Synchrotron Radiation on Advances and Synergy of High-Pressure Sciences at Synchrotron Sources was proposed, and we were pleased to invite contributions from colleagues who participated in the workshop as well as others who are making similar efforts at synchrotron sources worldwide.

What is a synchrotron and why does Australia need one?

CERN Document Server

Nugent, K A

2002-01-01

Construction of a $157 million synchrotron will soon begin in Melbourne. The author describes what this facility means for Australian science. The Australian synchrotron is a third generation device. The facility would have the capacity to do a wide range of science and technology at the same time. A number of applications, which are the priority for the Australian synchrotron project are briefly described. The huge technological spin-offs of this knowledge have made synchrotrons an attractive proposition to state governments

Techniques for materials research with synchrotron radiation x-rays

International Nuclear Information System (INIS)

Bowen, D.K.

1983-01-01

A brief introductory survey is presented of the properties and generation of synchrotron radiation and the main techniques developed so far for its application to materials problems. Headings are:synchrotron radiation; X-ray techniques in synchrotron radiation (powder diffraction; X-ray scattering; EXAFS (Extended X-ray Absorption Fine Structure); X-ray fluorescent analysis; microradiography; white radiation topography; double crystal topography); future developments. (U.K.)

PERFORMANCE ANALYSIS OF MULTI-TURN EXTRACTION FROM THE PROTON SYNCHROTRON TO THE SUPER PROTON SYNCHROTRON

CERN Document Server

Abernethy, Samuel

2016-01-01

Within CERN's accelerator complex, the extraction from the Proton Synchrotron to the Super Proton Synchrotron has been done using the so-called ``Continuous Transfer" (CT) method since the 1970's. A new technique, known as Multi-Turn Extraction (MTE), has now been implemented and is in full operation. This report examines a holistic performance analysis of the novel technique in multiple aspects of the accelerator complex, as well as a direct comparison with its predecessor, CT, from the implementation of MTE in 2010 until the end of 2015.

X-ray and synchrotron studies of porous silicon

Energy Technology Data Exchange (ETDEWEB)

Sivkov, V. N., E-mail: svn@dm.komisc.ru [Russian Academy of Sciences, Komi Scientific Center, Ural Branch (Russian Federation); Lomov, A. A. [Russian Academy of Sciences, Physical-Technological Institute (Russian Federation); Vasil' ev, A. L. [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation); Nekipelov, S. V. [Komi State Pedagogical Institute (Russian Federation); Petrova, O. V. [Russian Academy of Sciences, Komi Scientific Center, Ural Branch (Russian Federation)

2013-08-15

The results of comprehensive studies of layers of porous silicon of different conductivity types, grown by anodizing standard Si(111) substrates in an electrolyte based on fluoric acid and ethanol with the addition of 5% of iodine and kept in air for a long time, are discussed. Measurements are performed by scanning electron microscopy, high-resolution X-ray diffraction, and ultrasoft X-ray spectroscopy using synchrotron radiation. The structural parameters of the layers (thickness, strain, and porosity) and atomic and chemical composition of the porous-silicon surface are determined. It is found that an oxide layer 1.5-2.3-nm thick is formed on the surface of the silicon skeleton. The near-edge fine structure of the Si 2p absorption spectrum of this layer corresponds to the fine structure of the 2p spectrum of well coordinated SiO{sub 2}. In this case, the fine structure in the Si 2p-edge absorption region of the silicon skeleton is identical to that of the 2p absorption spectrum of crystalline silicon.

Atomic physics with high-brightness synchrotron x-ray sources

International Nuclear Information System (INIS)

Jones, K.W.; Johnson, B.M.; Meron, M.

1985-11-01

A description of atomic physics experiments that we intend to carry out at the National Synchrotron Light Source is given. Emphasis is given to work that investigates the properties of multiply charged ions. The use of a synchrotron storage ring for highly charged heavy ions is proposed as a way to produce high current beams which will make possible experiments to study the photoexcitation and ionization of multiply charged ions for the first time. Experiments along the same lines which are feasible at the proposed Advanced Light Source are considered briefly. 7 refs., 2 figs

The Stanford Synchrotron Radiation Laboratory, 20 years of synchrotron light

International Nuclear Information System (INIS)

Cantwell, K.

1993-08-01

The Stanford Synchrotron Radiation Laboratory (SSRL) is now operating as a fully dedicated light source with low emittance electron optics, delivering high brightness photon beams to 25 experimental stations six to seven months per year. On October 1, 1993 SSRL became a Division of the Stanford Linear Accelerator Center, rather than an Independent Laboratory of Stanford University, so that high energy physics and synchrotron radiation now function under a single DOE contract. The SSRL division of SLAC has responsibility for operating, maintaining and improving the SPEAR accelerator complex, which includes the storage ring and a 3 GeV injector. SSRL has thirteen x-ray stations and twelve VUV/Soft x-ray stations serving its 600 users. Recently opened to users is a new spherical grating monochromator (SGM) and a multiundulator beam line. Circularly polarized capabilities are being exploited on a second SGM line. New YB 66 crystals installed in a vacuum double-crystal monochromator line have sparked new interest for Al and Mg edge studies. One of the most heavily subscribed stations is the rotation camera, which has been recently enhanced with a MAR imaging plate detector system for protein crystallography on a multipole wiggler. Under construction is a new wiggler-based structural molecular biology beam line with experimental stations for crystallography, small angle scattering and x-ray absorption spectroscopy. Plans for new developments include wiggler beam lines and associated facilities specialized for environmental research and materials processing

Synchrotron X-Ray Study of Melting in Submonolayer Ar and other Rare-Gas Films on Graphite

DEFF Research Database (Denmark)

McTague, J. P.; Als-Nielsen, Jens Aage; Bohr, Jakob

1982-01-01

Synchrotron x-ray diffraction studies of the (10) peak of Ar on the (001) surface of ZYX graphite show a sharp but continuous broadening of the Bragg peak with increasing temperature. Below a coverage of ∼ 1 Ar atom per six surface carbon atoms (ρ=1) the onset of this transition occurs...

Study of resonant magnet exciting system for the 3 GeV proton synchrotron

Energy Technology Data Exchange (ETDEWEB)

Koseki, Shoichiro; Zhang, Fengqing; Watanabe, Yasuhiro; Tani, Norio [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment; Adachi, Toshikazu; Someya, Hirohiko [High Energy Accelerator Research Organization, Tsukuba, Ibaraki (Japan)

2001-07-01

Exciting system for magnets of the 3 GeV Proton synchrotron is under consideration. A resonant exciting system is studied, and two type of power supply are compared. One is a parallel supply that is used generally. Another is a modified series supply. Either of them uses IGBT sinusoidal converters. Capacity of the power converter of the series supply for bending magnets becomes 28.8 MVAp. This is lager more than twice compared with the parallel supply. In the other hand, the series supply has good control performance and flexibility. More study is necessary to decide finally. (author)

Synchrotron x-ray methods in studies of thin organic film structure

International Nuclear Information System (INIS)

Gentle, I.

2002-01-01

Full text: In recent years, the study of the structures of organic films as thin as a single monolayer has been revolutionized by methods that take advantage of the characteristics of synchrotron radiation. In particular, the methods of grazing incidence X-ray diffraction (GIXD) and X-ray reflectivity have led to a number of valuable insights into structural aspects of thin films at molecular resolution. Our group has been studying films formed at the air/water interface as insoluble monolayers and subsequently transferred to solid substrates using either the vertical (Langmuir-Blodgett) or horizontal (Langmuir-Schaeffer) methods. The main aim of these experiments is to exert control over film structure in the direction parallel to the substrate surface. This is highly desirable in order to design devices that exploit the optical and electrooptical properties of functional materials, but is difficult to do. By varying the chemical structure of the film materials and controlling deposition conditions a degree of control is possible, but only using synchrotron methods can it be easily verified. We have also developed a novel method of rapidly collecting data from GIXD measurements by the application of area detection (imaging plates), which has made possible measurements of dynamic processes such as in-situ annealing. Such measurements are not possible using traditional scanning methods. One area of current interest is films composed of porphyrins as functional materials, either alone or as mixed films with fatty acids. We have been investigating ways of assembling porphyrins in such a way as to overcome the tendency to aggregate, and to produce patterning and ordered structures in the plane of the interface. Examples will be given of how film composition and deposition method affects the final structure, and of how X-ray methods can be used to elucidate both the structures and the mechanisms. Copyright (2002) Australian X-ray Analytical Association Inc

A preliminary clinic dosimetry study for synchrotron radiation therapy at SSRF

International Nuclear Information System (INIS)

Li Zhaobin; Shi Zeliang; Zhang Qing; Wang Yong; Fu Shen

2013-01-01

Synchrotron radiation (SR) represents a unique and innovative anti-cancer treatment due to its unique physical features, including high flux density, and tunable and collimated radiation generation. The aim of this work is to assess the dosimetric properties of SR in Shanghai Synchrotron Radiation Facility (SSRF) for potential applications to clinical radiation oncology. The experiments were performed with 34 and 50 keV X-rays on the BL13W biomedical beamline of SSRF and the 6 MV X-rays from ARTISTE linac for the dosimetry study. The percentage depth dose (PDD) and the surface dose of the SR X-rays and the 6 MV photon beams were performed in solid water phantom with Gafchromic EBT3 films. All curves are normalized to the maximum calculated dose, The depth of full dose buildup is about 10 μm deeper for the monoenergetic X-ray beams of 34 and 50 keV. The beam transmits through the phantom, with a linear attenuation coefficient. The profile in the horizontal plane shows that the dose distribution is uniform within the facula, while the vertical profile shows a Gaussian distribution of the dose. The penumbra is less than 0.2 mm in the horizontal profile. Gafchromic EBT film may be a useful and convenient tool for dose measurement and quality control for the high space and density resolution. It is therefore important to gain a thorough understanding about the physical features of SR before this novel technology can be applied to clinical practice. (authors)

In Situ High Resolution Synchrotron X-Ray Powder Diffraction Studies of Lithium Batteries

DEFF Research Database (Denmark)

Amri, Mahrez; Fitch, Andy; Norby, Poul

2015-01-01

allowing diffraction information to be obtained from only the active material during battery operation [2]. High resolution synchrotron x-ray powder diffraction technique has been undertaken to obtain detailed structural and compositional information during lithiation/delithiation of commercial LiFePO4...... materials [3]. We report results from the first in situ time resolved high resolution powder diffraction experiments at beamline ID22/31 at the European Synchrotron Radiation Facility, ESRF. We follow the structural changes during charge of commercial LiFePO4 based battery materials using the Rietveld...... method. Conscientious Rietveld analysis shows slight but continuous deviation of lattice parameters from those of the fully stoichiometric end members LiFePO4 and FePO4 indicating a subsequent variation of stoichiometry during cathode delithiation. The application of an intermittent current pulses during...

Operation of the Australian Store.Synchrotron for macromolecular crystallography

Energy Technology Data Exchange (ETDEWEB)

Meyer, Grischa R. [Monash University, Clayton, Victoria 3800 (Australia); Aragão, David; Mudie, Nathan J.; Caradoc-Davies, Tom T. [Australian Synchrotron, 800 Blackburn Road, Clayton, Victoria 3168 (Australia); McGowan, Sheena; Bertling, Philip J.; Groenewegen, David; Quenette, Stevan M. [Monash University, Clayton, Victoria 3800 (Australia); Bond, Charles S. [The University of Western Australia, 35 Stirling Highway, Crawley 6009, Western Australia (Australia); Buckle, Ashley M. [Monash University, Clayton, Victoria 3800 (Australia); Androulakis, Steve, E-mail: steve.androulakis@monash.edu [Monash Bioinformatics Platform, Monash University, Clayton, Victoria 3800 (Australia)

2014-10-01

The Store.Synchrotron service, a fully functional, cloud computing-based solution to raw X-ray data archiving and dissemination at the Australian Synchrotron, is described. The Store.Synchrotron service, a fully functional, cloud computing-based solution to raw X-ray data archiving and dissemination at the Australian Synchrotron, is described. The service automatically receives and archives raw diffraction data, related metadata and preliminary results of automated data-processing workflows. Data are able to be shared with collaborators and opened to the public. In the nine months since its deployment in August 2013, the service has handled over 22.4 TB of raw data (∼1.7 million diffraction images). Several real examples from the Australian crystallographic community are described that illustrate the advantages of the approach, which include real-time online data access and fully redundant, secure storage. Discoveries in biological sciences increasingly require multidisciplinary approaches. With this in mind, Store.Synchrotron has been developed as a component within a greater service that can combine data from other instruments at the Australian Synchrotron, as well as instruments at the Australian neutron source ANSTO. It is therefore envisaged that this will serve as a model implementation of raw data archiving and dissemination within the structural biology research community.

Operation of the Australian Store.Synchrotron for macromolecular crystallography

International Nuclear Information System (INIS)

Meyer, Grischa R.; Aragão, David; Mudie, Nathan J.; Caradoc-Davies, Tom T.; McGowan, Sheena; Bertling, Philip J.; Groenewegen, David; Quenette, Stevan M.; Bond, Charles S.; Buckle, Ashley M.; Androulakis, Steve

2014-01-01

The Store.Synchrotron service, a fully functional, cloud computing-based solution to raw X-ray data archiving and dissemination at the Australian Synchrotron, is described. The Store.Synchrotron service, a fully functional, cloud computing-based solution to raw X-ray data archiving and dissemination at the Australian Synchrotron, is described. The service automatically receives and archives raw diffraction data, related metadata and preliminary results of automated data-processing workflows. Data are able to be shared with collaborators and opened to the public. In the nine months since its deployment in August 2013, the service has handled over 22.4 TB of raw data (∼1.7 million diffraction images). Several real examples from the Australian crystallographic community are described that illustrate the advantages of the approach, which include real-time online data access and fully redundant, secure storage. Discoveries in biological sciences increasingly require multidisciplinary approaches. With this in mind, Store.Synchrotron has been developed as a component within a greater service that can combine data from other instruments at the Australian Synchrotron, as well as instruments at the Australian neutron source ANSTO. It is therefore envisaged that this will serve as a model implementation of raw data archiving and dissemination within the structural biology research community

Metrology of reflection optics for synchrotron radiation

International Nuclear Information System (INIS)

Takacs, P.Z.

1985-09-01

Recent years have seen an almost explosive growth in the number of beam lines on new and existing synchrotron radiation facilities throughout the world. The need for optical components to utilize the unique characteristics of synchrotron radiation has increased accordingly. Unfortunately, the technology to manufacture and measure the large, smooth, exotic optical surfaces required to focus and steer the synchrotron radiation beam has not progressed as rapidly as the operational demands on these components. Most companies do not wish to become involved with a project that requires producing a single, very expensive, aspheric optic with surface roughness and figure tolerances that are beyond their capabilities to measure. This paper will review some of the experiences of the National Synchrotron Light Source in procuring grazing incidence optical components over the past several years. We will review the specification process - how it is related to the function of the optic, and how it relates to the metrology available during the manufacturing process and after delivery to the user's laboratory. We will also discuss practical aspects of our experience with new technologies, such as single point diamond turning of metal mirrors and the use of SiC as a mirror material. Recent advances in metrology instrumentation have the potential to move the measurement of surface figure and finish from the research laboratory into the optical shop, which should stimulate growth and interest in the manufacturing of optics to meet the needs of the synchrotron radiation user community

Atomic physics and synchrotron radiation: The production and accumulation of highly charged ions

International Nuclear Information System (INIS)

Johnson, B.M.; Meron, M.; Agagu, A.; Jones, K.W.

1986-01-01

Synchrotron radiation can be used to produce highly-charged ions, and to study photoexcitation and photoionization for ions of virtually any element in the periodic table. To date, with few exceptions, atomic physics studies have been limited to rare gases and a few metal vapors, and to photoexcitation energies in the VUV region of the electromagnetic spectrum. These limitations can now be overcome using photons produced by high-brightness synchrotron storage rings, such as the x-ray ring at the National Synchrotron Light Source (NSLS) at Brookhaven. Furthermore, calculations indicate that irradiation of an ion trap with an intense energetic photon beam will result in a viable source of highly-charged ions that can be given the name PHOBIS: the PHOton Beam Ion Source. Promising results, which encourage the wider systematic use of synchrotron radiation in atomic physics research, have been obtained in recent experiments on VUV photoemission and the production and storage of multiply-charged ions. 26 refs., 4 figs., 1 tab

Synchrotron Physics and Industry: new opportunities for technology transfer

International Nuclear Information System (INIS)

Williams, P.

2002-01-01

Full text: In 1979, with the opening in the UK of the world's first dedicated synchrotron light source, the SRS, experimental science in virtually every discipline underwent what amounted to a major revolution. The unique nature of synchrotron radiation, with its intensity, brightness, polarization, time structure and energy spectrum offer an unequalled probe of matter in all its states. The decades since have seen the development of a wide range of associated experimental techniques which harness the power of this radiation, including photoemission, EXAFS, spectroscopy, imaging and, of course, protein crystallography. These in turn have been applied to studies from surface science to molecular biology. The advances using synchrotron radiation throughout the 1980s and '90s naturally had a major impact on fundamental research, particularly in unraveling the structures of large proteins and in understanding the properties of semiconductors and surfaces. Much of this work could not have been accomplished without access to one of the world's increasing number of synchrotron facilities, of which there are now approaching 100. However, industrial awareness of the opportunities afforded by the use of synchrotron radiation was restricted to the handful of major multinational corporations, primarily in Europe, the USA and Japan, whose fundamental research staff had access. While there were major programmes in certain specific areas, such as X-ray lithography for semiconductor LSI fabrication, the general level of industrial involvement was low. But today, this is changing. In protein crystallography, for example, the use of synchrotron radiation in structure determination puts the 1PX' technique on the same level as NMR in terms of its routine utility. It has become an essential tool to drug designers in biopharmaceuticals, where access to the structural data is increasingly thought of almost as a service, rather than fundamental research. Pioneering work on medical imaging

Third generation synchrotron radiation applied to materials science

International Nuclear Information System (INIS)

Kaufmann, E.N.; Yun, W.

1993-01-01

Utility of synchrotron radiation for characterization of materials and ramifications of availability of new third-generation, high-energy, high-intensity sources of synchrotron radiation are discussed. Examples are given of power of x-ray analysis techniques to be expected with these new machines

Infrared and infrared emission spectroscopic study of typical Chinese kaolinite and halloysite.

Science.gov (United States)

Cheng, Hongfei; Frost, Ray L; Yang, Jing; Liu, Qinfu; He, Junkai

2010-12-01

The structure and thermal stability between typical Chinese kaolinite and halloysite were analysed by X-ray diffraction (XRD), infrared spectroscopy, infrared emission spectroscopy (IES) and Raman spectroscopy. Infrared emission spectroscopy over the temperature range of 300-700°C has been used to characterise the thermal decomposition of both kaolinite and halloysite. Halloysite is characterised by two bands in the water bending region at 1629 and 1648 cm(-1), attributed to structural water and coordinated water in the interlayer. Well defined hydroxyl stretching bands at around 3695, 3679, 3652 and 3625 cm(-1) are observed for both kaolinite and halloysite. The 550°C infrared emission spectrum of halloysite is similar to that of kaolinite in 650-1350 cm(-1) spectral region. The infrared emission spectra of halloysite were found to be considerably different to that of kaolinite at lower temperatures. These differences are attributed to the fundamental difference in the structure of the two minerals. Copyright © 2010 Elsevier B.V. All rights reserved.

Use of synchrotron radiation in radiation biology research

International Nuclear Information System (INIS)

Yamada, Takeshi

1981-01-01

Synchrotron radiation (SR) holds great expectation as a new research tool in the new areas of material science, because it has the continuous spectral distribution from visible light to X-ray, and its intensity is 10 2 to 10 3 times as strong as that of conventional radiation sources. In the National Laboratory for High Energy Physics, a synchrotron radiation experimental facility has been constructed, which will start operation in fiscal 1982. With this SR, the photons having the wavelength in undeveloped region from vacuum ultraviolet to soft X-ray are obtained as intense mono-wavelength light. The SR thus should contribute to the elucidation of the fundamentals in the biological action of radiation. The following matters are described: synchrotron radiation, experimental facility using SR, electron storage ring, features of SR, photon factory plan and synchrotron radiation experimental facility, utilization of SR in radiation biology field. (J.P.N.)

Synchrotron radiation photoemission spectrum study on K3C60 film

Institute of Scientific and Technical Information of China (English)

李宏年; 徐亚伯; 鲍世宁; 李海洋; 何丕模; 钱海杰; 刘风琴; 奎热西·易卜拉欣

2000-01-01

K3C60 single crystal film was prepared on the cleaved (111) surface of C60 single crystal. Synchrotron radiation angle-resolved photoemission spectra were measured at normal emission with sample temperature at - 150K. Up to four subpeaks of LUMO-derived band were observed. These sub-peaks exhibit distinct energy dispersions which resemble in general the theoretical ones calculated for K3C60 at low temperature with the so-called one-dimensional disordered structure. But there is large deviation of experimental sub-band intervals from the theoretical values. This result is meaningful for the studies of the physical properties of alkali-doped C60 solids, e.g. the mechanism for superconductivity.

National Synchrotron Light Source

International Nuclear Information System (INIS)

Hulbert, S.L.; Lazarz, N.M.

1991-04-01

This report discussion research being conducted at the National Synchrotron light source. In particular, this report contains operations summaries; symposia, workshops, and projects; NSLS highlights; and abstracts of science at the NSLS

High Intensity Beam Issues in the CERN Proton Synchrotron

CERN Document Server

Aumon, Sandra; Rivkin, Leonid

This PhD work is about limitations of high intensity proton beams observed in the CERN Proton Synchrotron (PS) and, in particular, about issues at injection and transition energies. With its 53 years, the CERN PS would have to operate beyond the limit of its performance to match the future requirements. Beam instabilities driven by transverse impedance and aperture restrictions are important issues for the operation and for the High-Luminosity LHC upgrade which foresees an intensity increase delivered by the injectors. The main subject of the thesis concerns the study of a fast transverse instability occurring at transition energy. The proton beams crossing this energy range are particularly sensitive to wake forces because of the slow synchrotron motion. This instability can cause a strong vertical emittance blow-up and severe losses in less than a synchrotron period. Experimental observations show that the particles at the peak density of the beam longitudinal distribution oscillate in the vertical plane du...

Near-Infrared Spectroscopic Study of Chlorite Minerals

OpenAIRE

Min Yang; Meifang Ye; Haihui Han; Guangli Ren; Ling Han; Zhuan Zhang

2018-01-01

The mineral chemistry of twenty chlorite samples from the United States Geological Survey (USGS) spectral library and two other regions, having a wide range of Fe and Mg contents and relatively constant Al and Si contents, was studied via infrared (IR) spectroscopy, near-infrared (NIR) spectroscopy, and X-ray fluorescence (XRF) analysis. Five absorption features of the twenty samples near 4525, 4440, 4361, 4270, and 4182 cm−1 were observed, and two diagnostic features at 4440 and 4280 cm−1 we...

Inner-shell photoemission from atoms and molecules using synchrotron radiation

International Nuclear Information System (INIS)

Lindle, D.W.

1983-12-01

Photoelectron spectroscopy, in conjunction with synchrotron radiation, has been used to study inner-shell photoemission from atoms and molecules. The time structure of the synchrotron radiation permits the measurements of time-of-flight (TOF) spectra of Auger and photoelectrons, thereby increasing the electron collection efficiency. The double-angle TOF method yielded angle-resolved photoelectron intensities, which were used to determine photoionization cross sections and photoelectron angular distributions in several cases. Comparison to theoretical calculations has been made where possible to help explain observed phenomena in terms of the electronic structure and photoionization dynamics of the systems studied. 154 references, 23 figures, 7 tables

New synchrotron powder diffraction facility for long-duration experiments.

Science.gov (United States)

Murray, Claire A; Potter, Jonathan; Day, Sarah J; Baker, Annabelle R; Thompson, Stephen P; Kelly, Jon; Morris, Christopher G; Yang, Sihai; Tang, Chiu C

2017-02-01

A new synchrotron X-ray powder diffraction instrument has been built and commissioned for long-duration experiments on beamline I11 at Diamond Light Source. The concept is unique, with design features to house multiple experiments running in parallel, in particular with specific stages for sample environments to study slow kinetic systems or processes. The instrument benefits from a high-brightness X-ray beam and a large area detector. Diffraction data from the commissioning work have shown that the objectives and criteria are met. Supported by two case studies, the results from months of measurements have demonstrated the viability of this large-scale instrument, which is the world's first dedicated facility for long-term studies (weeks to years) using synchrotron radiation.

X-ray studies on electrochemical systems. Synchrotron methods for energy materials

Energy Technology Data Exchange (ETDEWEB)

Braun, Artur [Empa. Eidgenoessische Materialpruefungs- und Forschungsanstalt, Duebendorf (Switzerland)

2017-07-01

This book is your graduate level entrance into battery, fuel cell and solar cell research at synchrotron X-ray sources. Materials scientists find numerous examples for the combination of electrochemical experiments with simple and with highly complex X-ray scattering and spectroscopy methods. Physicists and chemists can link applied electrochemistry with fundamental concepts of condensed matter physics, physical chemistry and surface science.

High pressure and synchrotron radiation satellite workshop

Energy Technology Data Exchange (ETDEWEB)

Bass, J.; Guignot, N.; Morard, G.; Mezouar, M.; Andrault, D.; Bolfan-Casanova, N.; Sturhahn, W.; Daniel, I.; Reynard, B.; Simionovici, A.; Sanchez Valle, C.; Martinez, I.; Kantor, I.; Dubrovinsky, I.; Mccammon, C.; Dubrovinskaia, N.; Kurnosiv, A.; Kuznetsov, A.; Goncharenko, I.; Loubeyre, P.; Desgreniers, S.; Weck, G.; Yoo, C.S.; Iota, V.; Park, J.; Cynn, H.; Gorelli, F.; Toulemonde, P.; Machon, D.; Merlen, A.; San Miguel, A.; Amboage, M.; Aquilanti, G.; Mathon, O.; Pascarelli, S.; Itie, J.P.; Mcmillan, P.F.; Trapananti, A.; Di Cicco, A.; Panfilis, S. de; Filipponi, A.; Kreisel, J.; Bouvier, P.; Dkhil, B.; Chaabane, B.; Rosner, H.; Koudela, D.; Schwarz, U.; Handestein, A.; Hanfland, M.; Opahle, I.; Koepernik, K.; Kuzmin, M.; Mueller, K.H.; Mydosh, J.; Richter, M.; Hejny, C.; Falconi, S.; Lundegaard, L.F.; Mcmahon, M.I; Loa, I.; Syassen, K.; Wang, X.; Roth, H.; Lorenz, T.; Farber Daniel, I.; Antonangeli Daniele, I.; Krisch, M.; Badro, J.; Fiquet, G.; Occelli, F.; Mao, W.L.; Mao, H.K.; Eng, P.; Kao, C.C.; Shu, J.F.; Hemley, R.J.; Tse, J.S.; Yao, Y.; Deen, P.P.; Paolasini, I.; Braithwaite, D.; Kernavanois, N.; Lapertot, G.; Rupprecht, K.; Leupold, O.; Ponkratz, U.; Wortmann, G.; Beraud, A.; Krisch, M.; Farber, D.; Antonangeli, D.; Aracne, C.; Zarestky, J.L.; Mcqueeney, R.; Mathon, O.; Baudelet, F.; Decremps, F.; Itie, J.P.; Nataf, I.; Pascarelli, S.; Polian, A

2006-07-01

The workshop is dedicated to recent advances on science at high pressure at third generation synchrotron sources. A variety of experiments using synchrotron radiation techniques including X-ray diffraction, EXAFS (extended X-ray absorption fine structure), inelastic X-ray scattering, Compton scattering and Moessbauer spectroscopy of crystalline, liquid or amorphous samples, are reported. This document gathers the abstracts of the presentations.

X-ray fluorescence imaging with synchrotron radiation

International Nuclear Information System (INIS)

Rivers, M.L.

1987-01-01

The micro-distribution of trace elements is of great interest in fields such as geochemistry, biology and material science. The synchrotron x-ray fluorescence microprobe provides a technique to quantitatively measure trace element compositions at individual points and to construct semiquantitative two dimensional maps of trace element compositions. This paper describes an x-ray fluorescence system used at the National Synchrotron Light Source

Experimental demonstration of the KEK induction synchrotron

International Nuclear Information System (INIS)

Takayama, Ken; Torikai, Kota; Shimosaki, Yoshito; Kono, Tadaaki; Iwashita, Taiki; Arakida, Yoshio; Nakamura, Eiji; Shirakata, Masashi; Sueno, Takeshi; Wake, Masayoshi; Otsuka, Kazunori

2007-01-01

Recent progress in the KEK induction synchrotron is presented. In the recent experiment, by using a newly developed induction acceleration system instead of radio-wave acceleration devices, a single proton bunch injected from the 500 MeV Booster ring and captured by the barrier bucket created by the induction step-voltages was accelerated to 6 GeV in the KEK proton synchrotron

High pressure and synchrotron radiation satellite workshop

International Nuclear Information System (INIS)

Bass, J.; Guignot, N.; Morard, G.; Mezouar, M.; Andrault, D.; Bolfan-Casanova, N.; Sturhahn, W.; Daniel, I.; Reynard, B.; Simionovici, A.; Sanchez Valle, C.; Martinez, I.; Kantor, I.; Dubrovinsky, I.; Mccammon, C.; Dubrovinskaia, N.; Kurnosiv, A.; Kuznetsov, A.; Goncharenko, I.; Loubeyre, P.; Desgreniers, S.; Weck, G.; Yoo, C.S.; Iota, V.; Park, J.; Cynn, H.; Gorelli, F.; Toulemonde, P.; Machon, D.; Merlen, A.; San Miguel, A.; Amboage, M.; Aquilanti, G.; Mathon, O.; Pascarelli, S.; Itie, J.P.; Mcmillan, P.F.; Trapananti, A.; Di Cicco, A.; Panfilis, S. de; Filipponi, A.; Kreisel, J.; Bouvier, P.; Dkhil, B.; Chaabane, B.; Rosner, H.; Koudela, D.; Schwarz, U.; Handestein, A.; Hanfland, M.; Opahle, I.; Koepernik, K.; Kuzmin, M.; Mueller, K.H.; Mydosh, J.; Richter, M.; Hejny, C.; Falconi, S.; Lundegaard, L.F.; Mcmahon, M.I; Loa, I.; Syassen, K.; Wang, X.; Roth, H.; Lorenz, T.; Farber Daniel, I.; Antonangeli Daniele, I.; Krisch, M.; Badro, J.; Fiquet, G.; Occelli, F.; Mao, W.L.; Mao, H.K.; Eng, P.; Kao, C.C.; Shu, J.F.; Hemley, R.J.; Tse, J.S.; Yao, Y.; Deen, P.P.; Paolasini, I.; Braithwaite, D.; Kernavanois, N.; Lapertot, G.; Rupprecht, K.; Leupold, O.; Ponkratz, U.; Wortmann, G.; Beraud, A.; Krisch, M.; Farber, D.; Antonangeli, D.; Aracne, C.; Zarestky, J.L.; Mcqueeney, R.; Mathon, O.; Baudelet, F.; Decremps, F.; Itie, J.P.; Nataf, I.; Pascarelli, S.; Polian, A.

2006-01-01

The workshop is dedicated to recent advances on science at high pressure at third generation synchrotron sources. A variety of experiments using synchrotron radiation techniques including X-ray diffraction, EXAFS (extended X-ray absorption fine structure), inelastic X-ray scattering, Compton scattering and Moessbauer spectroscopy of crystalline, liquid or amorphous samples, are reported. This document gathers the abstracts of the presentations

Limitations on plasma acceleration due to synchrotron losses

International Nuclear Information System (INIS)

Barletta, W.A.; Lee, E.P.; Bonifacio, R.; De Salvo, L.

1999-01-01

In this letter we consider the effect of synchrotron radiation losses due to the betatron motion of the electron beam in its self-induced magnetic field in a plasma accelerator taking into account the charge neutralization factor. The most favorable case is where the plasma density is smaller than the beam density. The contrary regime is strongly disfavored by the synchrotron radiation loss for beams with characteristics for TeV energies. In both cases we find that upon increasing the plasma density the synchrotron losses kill the acceleration process, so that there are limitations on the maximum allowable plasma density

CIRCE, the Coherent Infrared Center at the ALS

International Nuclear Information System (INIS)

Byrd, John M.; De Santis, Stefano; Jung, Jin-Young; Li, Derun; Martin, Michael C.; McKinney, W.; Munson, Dawn; Nishimura, Hiroshi; Robin, David S.; Sannibale, Fernando; Schlueter, Ross; Venturini, Marco; Wan, Weishi; Zolotorev, Max

2004-01-01

CIRCE (Coherent InfraRed CEnter) is a proposal for a new electron storage ring to be built at the Advanced Light Source (ALS) of the Lawrence Berkeley National Laboratory (LBNL). The ring design is optimized for the generation of coherent synchrotron radiation (CSR) in the terahertz frequency range. Among others, CIRCE operation includes three interesting CSR modes: ultra stable, femtosecond laser slicing and broadband bursting. CSR allows CIRCE to generate an extremely high flux in the terahertz frequency region. The many orders of magnitude increase in the intensity over that presently achievable by conventional sources, has the potential to enable new science experiments. The characteristics of CIRCE and of the different modes of operation are described in this paper

Lung cancer and angiogenesis imaging using synchrotron radiation

International Nuclear Information System (INIS)

Liu Xiaoxia; Zhao Jun; Xu, Lisa X; Sun Jianqi; Gu Xiang; Liu Ping; Xiao Tiqiao

2010-01-01

Early detection of lung cancer is the key to a cure, but a difficult task using conventional x-ray imaging. In the present study, synchrotron radiation in-line phase-contrast imaging was used to study lung cancer. Lewis lung cancer and 4T1 breast tumor metastasis in the lung were imaged, and the differences were clearly shown in comparison to normal lung tissue. The effect of the object-detector distance and the energy level on the phase-contrast difference was investigated and found to be in good agreement with the theory of in-line phase-contrast imaging. Moreover, 3D image reconstruction of lung tumor angiogenesis was obtained for the first time using a contrast agent, demonstrating the feasibility of micro-angiography with synchrotron radiation for imaging tumor angiogenesis deep inside the body.

Simulation of space charge effects in a synchrotron

International Nuclear Information System (INIS)

Machida, Shinji; Ikegami, Masanori

1998-01-01

We have studied space charge effects in a synchrotron with multi-particle tracking in 2-D and 3-D configuration space (4-D and 6-D phase space, respectively). First, we will describe the modelling of space charge fields in the simulation and a procedure of tracking. Several ways of presenting tracking results will be also mentioned. Secondly, it is discussed as a demonstration of the simulation study that coherent modes of a beam play a major role in beam stability and intensity limit. The incoherent tune in a resonance condition should be replaced by the coherent tune. Finally, we consider the coherent motion of a beam core as a driving force of halo formation. The mechanism is familiar in linac, and we apply it in a synchrotron

Synchrotron microradiography study on acute lung injury of mouse caused by PM{sub 2.5} aerosols

Energy Technology Data Exchange (ETDEWEB)

Tong Yongpeng [Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); Zhang Guilin [Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China)]. E-mail: glzhang@sinap.ac.cn; Li Yan [Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); Tan Mingguan [Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); Wang Wei [Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); Chen Jianmin [Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800 (China); Hwu Yeukuang [Institute of Physics, Academia Sinica, Nankang, Taipei (China); Hsu, Pei-Chebg [Institute of Physics, Academia Sinica, Nankang, Taipei, Taiwan (China); Je, Jung Ho [Department of Material Science and Engineering, Pohang University of Science and Technology, Pohang (Korea, Republic of); Margaritondo, Giorgio [Faculte des sciences de base, CH-1015 Lausanne, Ecole Polytechnique Federale de Lausanne (EPFL) (Switzerland); Song Weiming [School of Public Health, Fudan University, Shanghai 200032 (China); Jiang, Rongfang [School of Public Health, Fudan University, Shanghai 200032 (China); Jiang Zhihai [School of Public Health, Fudan University, Shanghai 200032 (China)

2006-05-15

In order to investigate FeSO{sub 4}, ZnSO{sub 4} (the two of main metal compositions of Shanghai PM{sub 2.5} (particle matter with those aerodynamical diameter <2.5 {mu}m)) effects on acute lung injury, six solutions contained PM{sub 2.5} aerosol particles, FeSO{sub 4}, ZnSO{sub 4} and their mixtures were instilled intratracheally into mouse lungs for experiment. By 2 days after instillation, the live mice were checked in vivo by synchrotron refractive index microradiography. In addition after extracted and examined by dissection, the right lobes of lung were fixed by formalin, then imaged by synchrotron microradiography again. Corresponding parts of those lung tissues were embedded in paraffin for histopathologic study. The synchrotron X-ray microradiographs of live mouse lung showed different lung texture changes after instilled with different toxic solutions. Hemorrhage points in lung were observed more from those mice instilled by FeSO{sub 4} contained toxin solutions groups. Bronchial epithelial hyperplasia can be observed in ZnSO{sub 4} contained solution-instilled groups from histopathologic analysis. It was found that the acute lung injury of mice caused by solution of PM{sub 2.5} + FeSO{sub 4} + ZnSO{sub 4} was more serious than other toxin solutions. Results suggested that FeSO{sub 4} mainly induced hemorrhage and ZnSO{sub 4} mainly induced inflammation and bronchiolar epithelial hyperplasia in the early toxicological effects of PM{sub 2.5}.

X-ray diffraction studies of Pompeian wall paintings using synchrotron radiation and dedicated laboratory made systems

International Nuclear Information System (INIS)

Duran, A.; Castaing, J.; Walter, P.

2010-01-01

The full identification of artwork materials requires not only elemental analysis but also structural information of the compounds as provided by X-ray diffraction (XRD). This is easily done when taking samples (or micro-samples) from artworks. However, there is an increasing interest in performing non-destructive studies that require adapted XRD systems. Comparative study of synchrotron high-resolution X-ray powder diffraction (SR-HRPD) and laboratory non-destructive systems (portable XRD and micro-XRD) is the main objective of this work. There are no qualitative differences among the three systems as for detected phases in the Pompeian wall paintings that were studied, except in the case of minority phases which only were detected by SR-HRPD. The identified pigments were goethite, hematite, cinnabar, glauconite, Pompeian blue, together with calcite, dolomite and aragonite. Synchrotron XRD diagrams show better resolution than the others. In general, the peak widths in the diagrams obtained with the portable XRD system are similar to those obtained by micro-diffraction equipment. Factors such as residual divergence of X-ray sources, incidence angle and slit or collimator size are discussed in relation with the quality of XRD diagrams. (orig.)

THz near-field imaging of biological tissues employing synchrotron radiation (Invited Paper)

Science.gov (United States)

Schade, Ulrich; Holldack, Karsten; Martin, Michael C.; Fried, Daniel

2005-04-01

Terahertz scanning near-field infrared microscopy (SNIM) below 1 THz is demonstrated. The near-field technique benefits from the broadband and highly brilliant coherent synchrotron radiation (CSR) from an electron storage ring and from a detection method based on locking on to the intrinsic time structure of the synchrotron radiation. The scanning microscope utilizes conical waveguides as near-field probes with apertures smaller than the wavelength. Different cone approaches have been investigated to obtain maximum transmittance. Together with a Martin-Puplett spectrometer the set-up enables spectroscopic mapping of the transmittance of samples well below the diffraction limit. Spatial resolution down to about λ/40 at 2 wavenumbers (0.06 THz) is derived from the transmittance spectra of the near-field probes. The potential of the technique is exemplified by imaging biological samples. Strongly absorbing living leaves have been imaged in transmittance with a spatial resolution of 130 μm at about 12 wavenumbers (0.36 THz). The THz near-field images reveal distinct structural differences of leaves from different plants investigated. The technique presented also allows spectral imaging of bulky organic tissues. Human teeth samples of various thicknesses have been imaged between 2 and 20 wavenumbers (between 0.06 and 0.6 THz). Regions of enamel and dentin within tooth samples are spatially and spectrally resolved, and buried caries lesions are imaged through both the outer enamel and into the underlying dentin.

[The study of transpiration influence on plant infrared radiation character].

Science.gov (United States)

Ling, Jun; Zhang, Shuan-Qin; Pan, Jia-Liang; Lian, Chang-Chun; Yang, Hui

2012-07-01

Studying vegetation infrared radiation character is the base of developing infrared camouflage and concealment technology of ground military target. Accurate fusion of target and background can be achieved by simulating formation mechanism of vegetation infrared radiation character. Leaf transpiration is characteristic physiological mechanism of vegetation and one of the main factors that influence its infrared radiation character. In the present paper, physical model of leaf energy balance is set up. Based on this model the influence of plant transpiration on leaf temperature is analyzed and calculated. The daily periodic variation of transpiration, leaf temperature and infrared radiation character of typical plants such as camphor tree and holly is actually measured with porometer and infrared thermal imaging system. By contrasting plant leaf with dryness leaf, experimental data indicates that plant transpiration can regulate leaf energy balance effectively and control leaf temperature in a reasonable range and suppress deep range variation of leaf infrared radiation character.

Vacuum chambers full of ideas for the Swedish synchrotron

CERN Multimedia

Corinne Pralavorio

2016-01-01

CERN’s Vacuum, Surfaces and Coatings group has contributed to the development of vacuum chambers for the MAX IV synchrotron, which has just been officially opened in Sweden.   A section of the new 3 GeV MAX IV synchrotron at the time of installation. In the centre of the magnets you can see the vacuum chamber developed in collaboration with CERN. (Photo: Marek Grabski, MAX IV Vacuum group) On 21 June, the King and the Prime Minister of Sweden officially opened MAX IV, a brand-new synchrotron in Lund, Sweden. The summer solstice, the longest day of the year, was deliberately chosen for the ceremony: MAX IV, a cutting-edge synchrotron, will deliver the brightest X-rays ever produced to more than 2000 users. Some 1500 kilometres away, a team at CERN followed the opening ceremony with a touch of pride. The Vacuum, Surfaces and Coatings group in the Technology department (TE-VSC) participated in the construction of this new synchrotron. Its contribution lies at the very hea...

Water-induced morphology changes in BaO/?-Al2O3 NOx storage materials: an FTIR, TPD, and time-resolved synchrotron XRD study

International Nuclear Information System (INIS)

Szanyi, Janos; Kwak, Ja Hun; Kim, Do Heui; Wang, Xianqin; Chimentao, Ricardo J.; Hanson, Jonathan; Epling, William S.; Peden, Charles HF

2007-01-01

The effect of water on the morphology of BaO/Al2O3-based NOx storage materials was investigated using Fourier transform infrared spectroscopy, temperature programmed desorption, and time-resolved synchrotron X-ray diffraction techniques. The results of this multi-spectroscopy study reveal that, in the presence of water, surface Ba-nitrates convert to bulk nitrates, and water facilitates the formation of large Ba(NO3)2 particles. This process is completely reversible, i.e. after the removal of water from the storage material a significant fraction of the bulk nitrates re-convert to surface nitrates. NO2 exposure of a H2O-containing (wet) BaO/Al2O3 sample results in the formation of nitrites and bulk nitrates exclusively, i.e. no surface nitrates form. After further exposure to NO2, the nitrites completely convert to bulk nitrates. The amount of NOx taken up by the storage material is, however, essentially unaffected by the presence of water, regardless of whether the water was dosed prior to or after NO2 exposure. Based on the results of this study we are now able to explain most of the observations reported in the literature on the effect of water on NOx uptake on similar storage materials

Inauguration of Proton Synchrotron

CERN Multimedia

1960-01-01

On 5 February 1960, the Proton Synchrotron (PS) was formally inaugurated. The great Danish physicist, Niels Bohr, releases a bottle of champagne against a shielding block to launch the PS on its voyage in physics.

Evidence for quiescent synchrotron emission in the black hole X-ray transient Swift J1357.2–0933

Directory of Open Access Journals (Sweden)

Shahbaz T.

2013-12-01

Full Text Available We present high time-resolution optical and infrared observations of the edge-on black hole X-ray transient Swift J1357.2-0933. Our data taken in 2012 shows the system to be at its pre-outburst magnitude and so the system is in quiescence. In contrast to other X-ray transients, the quiescent light curves of Swift J1357.2-0933 do not show the secondary star’s ellipsoidal modulation. The optical and infrared light curves is dominated by variability with an optical fractional rms of about 20 per cent, much larger than what is observed in other systems. The quiescent ultraviolet to mid-IR spectral energy distribution in quiescence is dominated by a nonthermal component with a power–law index of −1.4, (the broad-band rms SED has a similar index which arises from optically thin synchrotron emission from a jet; the lack of a peak in the spectral energy distribution rules out advection-dominated models (based on [19].

National synchrotron light source. Activity report, October 1, 1995--September 30, 1996

Energy Technology Data Exchange (ETDEWEB)

Rothman, E.Z.; Hastings, J.B. [eds.

1997-05-01

The hard work done by the synchrotron radiation community, in collaboration with all those using large-scale central facilities during 1995, paid off in FY 1996 through the DOE`s Presidential Scientific Facilities Initiative. In comparison with the other DOE synchrotron radiation facilities, the National Synchrotron Light Source benefited least in operating budgets because it was unable to increase running time beyond 100%-nevertheless, the number of station hours was maintained. The major thrust at Brookhaven came from a 15% increase in budget which allowed the recruitment of seven staff in the beamlines support group and permitted a step increment in the funding of the extremely long list of upgrades; both to the sources and to the beamlines. During the December 1995 shutdown, the VUV Ring quadrant around U10-U12 was totally reconstructed. New front ends, enabling apertures up to 90 mrad on U10 and U12, were installed. During the year new PRTs were in formation for the infrared beamlines, encouraged by the investment the lab was able to commit from the initiative funds and by awards from the Scientific Facilities Initiative. A new PRT, specifically for small and wide angle x-ray scattering from polymers, will start work on X27C in FY 1997 and existing PRTs on X26C and X9B working on macromolecular crystallography will be joined by new members. Plans to replace aging radio frequency cavities by an improved design, originally a painfully slow six or eight year project, were brought forward so that the first pair of cavities (half of the project for the X-Ray Ring) will now be installed in FY 1997. Current upgrades to 350 mA initially and to 438 mA later in the X-Ray Ring were set aside due to lack of funds for the necessary thermally robust beryllium windows. The Scientific Facilities Initiative allowed purchase of all 34 windows in FY 1996 so that the power upgrade will be achieved in FY 1997.

Berkeley Lab's ALS generates femtosecond synchrotron radiation

CERN Document Server

Robinson, A L

2000-01-01

A team at Berkeley's Advanced Light Source has shown how a laser time-slicing technique provides a path to experiments with ultrafast time resolution. A Lawrence Berkeley National Laboratory team has succeeded in generating 300 fs pulses of synchrotron radiation at the ALS synchrotron radiation machine. The team's members come from the Materials Sciences Division (MSD), the Center for Beam Physics in the Accelerator and Fusion Research Division and the Advanced Light Source (ALS). Although this proof-of principle experiment made use of visible light on a borrowed beamline, the laser "time-slicing" technique at the heart of the demonstration will soon be applied in a new bend magnet beamline that was designed specially for the production of femtosecond pulses of X-rays to study long-range and local order in condensed matter with ultrafast time resolution. An undulator beamline based on the same technique has been proposed that will dramatically increase the flux and brightness. The use of X-rays to study the c...

Time-resolved X-ray studies using third generation synchrotron radiation sources

International Nuclear Information System (INIS)

Mills, D.M.

1991-10-01

The third generation, high-brilliance, hard x-ray, synchrotron radiation (SR) sources currently under construction (ESRF at Grenoble, France; APS at Argonne, Illinois; and SPring-8 at Harima, Japan) will usher in a new era of x-ray experimentation for both physical and biological sciences. One of the most exciting areas of experimentation will be the extension of x-ray scattering and diffraction techniques to the study of transient or time-evolving systems. The high repetition rate, short-pulse duration, high brilliance, and variable spectral bandwidth of these sources make them ideal for x-ray time-resolved studies. The temporal properties (bunch length, interpulse period, etc.) of these new sources will be summarized. Finally, the scientific potential and the technological challenges of time-resolved x-ray scattering from these new sources will be described. 13 refs., 4 figs

A synchrotron radiation study of nonlinear diffusion in Cu-Au

International Nuclear Information System (INIS)

Menon, E.S.K.; Huang, P.; Kraitchman, M.; deFontaine, D.; Hoyt, J.J.; Chow, P.

1992-01-01

This paper reports a study in which alternate layers of pure copper and gold were vapor deposited on a sodium chloride substrate, the average concentration of the films being Cu-16 at% Au and the layering periodicity (modulation wavelength) being 3.31 nm. The composition modulation gives rise to satellite diffraction peaks around the (200) Bragg reelections. Synchrotron radiation at SSRL was able to detect u to third order satellite intensity the evolution of which was measured as a function of annealing time at 515 K. although the first order satellite intensity decayed as expected exponentially with time, intensities of both second and third order satellites decreased very rapidly at first, then increased before decaying exponentially. These results are in conformity with theoretical models of satellite evolution during annealing in a one-dimensional modulated system governed by a nonlinear diffusion equation

Chemical applications of synchrotron radiation: Workshop report

International Nuclear Information System (INIS)

1989-04-01

The most recent in a series of topical meetings for Advanced Photon Source user subgroups, the Workshop on Chemical Applications of Synchrotron Radiation (held at Argonne National Laboratory, October 3-4, 1988) dealt with surfaces and kinetics, spectroscopy, small-angle scattering, diffraction, and topography and imaging. The primary objectives were to provide an educational resource for the chemistry community on the scientific research being conducted at existing synchrotron sources and to indicate some of the unique opportunities that will be made available with the Advanced Photon Source. The workshop organizers were also interested in gauging the interest of chemists in the field of synchrotron radiation. Interest expressed at the meeting has led to initial steps toward formation of a Chemistry Users Group at the APS. Individual projects are processed separately for the data bases

Chemical applications of synchrotron radiation: Workshop report

Energy Technology Data Exchange (ETDEWEB)

1989-04-01

The most recent in a series of topical meetings for Advanced Photon Source user subgroups, the Workshop on Chemical Applications of Synchrotron Radiation (held at Argonne National Laboratory, October 3-4, 1988) dealt with surfaces and kinetics, spectroscopy, small-angle scattering, diffraction, and topography and imaging. The primary objectives were to provide an educational resource for the chemistry community on the scientific research being conducted at existing synchrotron sources and to indicate some of the unique opportunities that will be made available with the Advanced Photon Source. The workshop organizers were also interested in gauging the interest of chemists in the field of synchrotron radiation. Interest expressed at the meeting has led to initial steps toward formation of a Chemistry Users Group at the APS. Individual projects are processed separately for the data bases.

Proceedings of the workshop on LAMPF II synchrotron

International Nuclear Information System (INIS)

Cooper, R.K.

1983-01-01

Topics covered at the workshop include: considerations for a staged approach to synchrotron construction; consideration of energy and cost for a kaon and/or antiproton factory; changing the transition energy in the main ring for the Fermilab antiproton beam; a lattice with 50% undispersed straight sections; bunch width considerations in a stretcher ring; a self-consistent longitudinal distribution; rapid-cycling tuned rf cavity for synchrotron use; considerations on a high-shunt impedance tunable RF cavity; rotating condensers; low extraction from the stretcher ring; an antiproton source for LAMPF II; synchrotron magnet circuit; power supply and ring magnet options; and notes for a kaon factory design

A synchrotron radiation facility for x-ray astronomy

DEFF Research Database (Denmark)

Hall, C.J.; Lewis, R.A.; Christensen, Finn Erland

1997-01-01

A proposal for an x-ray optics test facility based at a synchrotron radiation source is presented. The facility would incorporate a clean preparation area, and a large evacuable test area. The advantages of using a synchrotron as the source of the test radiation are discussed. These include the a...

Status of the National Synchrotron Light Source project

International Nuclear Information System (INIS)

Heese, R.N.

1981-01-01

The National Synchrotron Light Source is in its final stages of construction, and as the turn-on time for the 700 MeV vuv storage ring draws near, an overview of the project is presented. Emphasis is placed on the linac and booster synchrotron performance and the status of major subsystems

Photoionization and dissociative photoionization study of HFC-152a using synchrotron radiation

International Nuclear Information System (INIS)

Huang Chaoqun; Wei Lixia; Yang Bin; Yang Rui; Wang Sisheng; Shan Xiaobin; Qi Fei; Zhang Yunwu; Sheng Liusi; Hao Liqing; Zhou Shikang; Wang Zhenya

2006-01-01

Photoionization and dissociative photoionization of HFC-152a have been studied using synchrotron radiation and a reflection time-of-flight mass spectrometry (RTOF-MS). The ionization energy of parent molecule (11.94 ± 0.04 eV) and appearance potentials of various fragment ions have been determined by measuring their photoionization efficiency curves. Energies, symmetry point groups and ground electronic states of neutrals and cations of parent and its fragments have been calculated using GAUSSIAN-03 program with the G3 method. According to the theoretical and experimental results, some dissociation channels and their dissociation energies of CH 3 CHF 2 + have been analyzed. (authors)

The uses of synchrotron radiation sources for elemental and chemical microanalysis

Science.gov (United States)

Chen, J.R.; Chao, E.C.T.; Minkin, J.A.; Back, J.M.; Jones, K.W.; Rivers, M.L.; Sutton, S.R.

1990-01-01

Synchrotron radiation sources offer important features for the analysis of a material. Among these features is the ability to determine both the elemental composition of the material and the chemical state of its elements. For microscopic analysis synchrotron X-ray fluorescence (SXRF) microprobes now offer spatial resolutions of 10 ??m with minimum detection limits in the 1-10 ppm range depending on the nature of the sample and the synchrotron source used. This paper describes the properties of synchrotron radiation and their importance for elemental analysis, existing synchrotron facilities and those under construction that are optimum for SXRF microanalysis, and a number of applications including the high energy excitation of the K lines of heavy elements, microtomography, and XANES and EXAFS spectroscopies. ?? 1990.

Studies of protein structure in solution and protein folding using synchrotron small-angle x-ray scattering

Energy Technology Data Exchange (ETDEWEB)

Chen, Lingling [Stanford Univ., CA (United States)

1996-04-01

Synchrotron small angle x-ray scattering (SAXS) has been applied to the structural study of several biological systems, including the nitrogenase complex, the heat shock cognate protein (hsc70), and lysozyme folding. The structural information revealed from the SAXS experiments is complementary to information obtained by other physical and biochemical methods, and adds to our knowledge and understanding of these systems.

National Laboratory of Synchrotron Radiation: technologic potential

International Nuclear Information System (INIS)

Silva, C.E.T.G. da; Rodrigues, A.R.D.

1987-01-01

The technological or industrial developments based on the accumulated experience by research group of condensed matter physics, in Brazil, are described. The potential of a National Laboratory of Synchrotron Radiation for personnel training, absorption and adaptation of economically important technologies for Brazil, is presented. Examples of cooperations between the Laboratory and some national interprises, and some industrial applications of the synchrotron radiation are done. (M.C.K.) [pt

Synchrotron applications of pixel and strip detectors at Diamond Light Source

International Nuclear Information System (INIS)

Marchal, J.; Tartoni, N.; Nave, C.

2009-01-01

A wide range of position-sensitive X-ray detectors have been commissioned on the synchrotron X-ray beamlines operating at the Diamond Light Source in UK. In addition to mature technologies such as image-plates, CCD-based detectors, multi-wire and micro-strip gas detectors, more recent detectors based on semiconductor pixel or strip sensors coupled to CMOS read-out chips are also in use for routine synchrotron X-ray diffraction and scattering experiments. The performance of several commercial and developmental pixel/strip detectors for synchrotron studies are discussed with emphasis on the image quality achieved with these devices. Examples of pixel or strip detector applications at Diamond Light Source as well as the status of the commissioning of these detectors on the beamlines are presented. Finally, priorities and ideas for future developments are discussed.

Coherent synchrotron radiation

International Nuclear Information System (INIS)

Agoh, Tomonori

2006-01-01

This article presents basic properties of coherent synchrotron radiation (CSR) with numerical examples and introduces the reader to important aspects of CSR in future accelerators with short bunches. We show interesting features of the single bunch instability due to CSR in storage rings and discuss the longitudinal CSR field via the impedance representation. (author)

In situ study starch gelatinization under ultra-high hydrostatic pressure using synchrotron SAXS

KAUST Repository

Yang, Zhi; Gu, Qinfen; Lam, Elisa; Tian, Feng; Chaieb, Saharoui; Hemar, Yacine

2015-01-01

The gelatinization of waxy (very low amylose) corn and potato starches by high hydrostatic pressure (HHP) (up to ∼1 GPa) was investigated in situ using synchrotron small-angle X-ray scattering (SAXS) on samples held in a diamond anvil cell (DAC

Bunch heating by coherent synchrotron radiation

International Nuclear Information System (INIS)

Heifets, S.A.; Zolotorev, M.

1995-10-01

The authors discuss here effects which define the steady-state rms energy spread of a microbunch in a storage ring. It is implied that the longitudinal microwave instability is controlled by low α lattice. In this case the coherent synchrotron radiation, if exists, may be the main factor defining the bunch temperature. Another effect comes from the fact that a nonlinear momentum compaction of such lattices makes Haissinskii equation not applicable, and the coherent synchrotron radiation may effect not only bunch lengthening but the energy spread as well

HIGH-PERFORMANCE COMPUTING FOR THE STUDY OF EARTH AND ENVIRONMENTAL SCIENCE MATERIALS USING SYNCHROTRON X-RAY COMPUTED MICROTOMOGRAPHY

International Nuclear Information System (INIS)

FENG, H.; JONES, K.W.; MCGUIGAN, M.; SMITH, G.J.; SPILETIC, J.

2001-01-01

Synchrotron x-ray computed microtomography (CMT) is a non-destructive method for examination of rock, soil, and other types of samples studied in the earth and environmental sciences. The high x-ray intensities of the synchrotron source make possible the acquisition of tomographic volumes at a high rate that requires the application of high-performance computing techniques for data reconstruction to produce the three-dimensional volumes, for their visualization, and for data analysis. These problems are exacerbated by the need to share information between collaborators at widely separated locations over both local and tide-area networks. A summary of the CMT technique and examples of applications are given here together with a discussion of the applications of high-performance computing methods to improve the experimental techniques and analysis of the data

HIGH-PERFORMANCE COMPUTING FOR THE STUDY OF EARTH AND ENVIRONMENTAL SCIENCE MATERIALS USING SYNCHROTRON X-RAY COMPUTED MICROTOMOGRAPHY.

Energy Technology Data Exchange (ETDEWEB)

FENG,H.; JONES,K.W.; MCGUIGAN,M.; SMITH,G.J.; SPILETIC,J.

2001-10-12

Synchrotron x-ray computed microtomography (CMT) is a non-destructive method for examination of rock, soil, and other types of samples studied in the earth and environmental sciences. The high x-ray intensities of the synchrotron source make possible the acquisition of tomographic volumes at a high rate that requires the application of high-performance computing techniques for data reconstruction to produce the three-dimensional volumes, for their visualization, and for data analysis. These problems are exacerbated by the need to share information between collaborators at widely separated locations over both local and tide-area networks. A summary of the CMT technique and examples of applications are given here together with a discussion of the applications of high-performance computing methods to improve the experimental techniques and analysis of the data.

Sensitivities in synchrotron radiation TXRF

International Nuclear Information System (INIS)

Pianetta, P.; Baur, K.; Brennan, S.

2000-01-01

This work describes the progress we achieved at the Stanford Synchrotron Radiation Laboratory (SSRL) in improving the sensitivity for both the transition metals and light elements such as Al and Na. The transition metal work has matured to the point where a facility exists at SSRL in which semiconductor companies are able to perform industrially relevant measurements at state of the art detection limits. This facility features clean wafer handling and automated data acquisition making routine analytical measurements possible. The best sensitivity demonstrated so far is 3.4 E7 atoms/cm 2 for a 5000 second count time corresponding to 7.6 E7 atoms/cm 2 for a standard 1000 second count time. This is more than a factor of 100 better than what can be achieved with conventional TXRF systems. The detection of light elements such as Al and Na is challenging due to the presence of the h stronger Si fluorescence peak. For traditional energy-dispersive detection only the tunability of synchrotron radiation to excitation energies below the Si-K absorption edge leads to an acceptable sensitivity for Al detection which is limited by a large background due to inelastic x-ray Raman scattering. An alternative approach to overcome the Raman contribution and the strong Si fluorescence is to use a wavelength-dispersive spectrometer for fluorescence detection. The benefits of such a multilayer spectrometer over a solid state detector are its higher energy resolution and greater dynamic range. This strategy allows primary excitation above the Si K absorption edge, eliminating the background due to Raman scattering, and a gracing emission geometry to guarantee high surface sensitivity. Studies testing this concept in combination with high flux synchrotron radiation are underway and first results will be presented. (author)

Refraction-contrast bone imaging using synchrotron radiation

International Nuclear Information System (INIS)

Mori, Koichi; Sekine, Norio; Sato, Hitoshi; Shikano, Naoto; Shimao, Daisuke; Shiwaku, Hideaki; Hyodo, Kazuyuki; Oka, Hiroshi

2002-01-01

The X-ray refraction-contrast imaging using synchrotron radiation with some X-ray energies is successfully performed at B120B2 of SPring-8. The refraction-contrast images of bone samples such as human dried proximal phalanx, wrist, upper cervical vertebrae and sella turcica and as mouse proximal femur using the synchrotron X-ray are always better in image contrast and resolution than those of the absorption-contrast images using the synchrotron X-ray and/or the conventional X-ray tube. There is much likeness in the image contrast and resolution of trabeculae bone in the human dried proximal phalanx between X-ray energy of 30 keV at sample-to-film distance of 1 m and those of 40, 50 keV at those of 4,5 m, respectively. High-energy refraction-contrast imaging with suitable sample-to-film distance could reduce the exposure dose in human imaging. In the refraction-contrast imaging of human wrist, upper cervcal vertebrae, sella turcica and mouse proximal femur using the synchrotron X-ray, we can obtain better image contrast and resolution to correctly extract morphological information for diagnosis corresponding to each of the clinical field than those of the absorption-contrast images. (author)

Ultrafast molecular dynamics illuminated with synchrotron radiation

International Nuclear Information System (INIS)

Bozek, John D.; Miron, Catalin

2015-01-01

Highlights: • Ultrafast molecular dynamics probed with synchrotron radiation. • Core-excitation as probe of ultrafast dynamics through core-hole lifetime. • Review of experimental and theoretical methods in ultrafast dynamics using core-level excitation. - Abstract: Synchrotron radiation is a powerful tool for studying molecular dynamics in small molecules in spite of the absence of natural matching between the X-ray pulse duration and the time scale of nuclear motion. Promoting core level electrons to unoccupied molecular orbitals simultaneously initiates two ultrafast processes, nuclear dynamics on the potential energy surfaces of the highly excited neutral intermediate state of the molecule on the one hand and an ultrafast electronic decay of the intermediate excited state to a cationic final state, characterized by a core hole lifetime. The similar time scales of these processes enable core excited pump-probe-type experiments to be performed with long duration X-ray pulses from a synchrotron source. Recent results obtained at the PLIEADES beamline concerning ultrafast dissociation of core excited states and molecular potential energy curve mapping facilitated by changes in the geometry of the short-lived intermediate core excited state are reviewed. High brightness X-ray beams combined with state-of-the art electron and ion-electron coincidence spectrometers and highly sophisticated theoretical methods are required to conduct these experiments and to achieve a full understanding of the experimental results.

Density functional theory for prediction of far-infrared vibrational frequencies: molecular crystals of astrophysical interest

Science.gov (United States)

Ennis, C.; Auchettl, R.; Appadoo, D. R. T.; Robertson, E. G.

2017-11-01

Solid-state density functional theory code has been implemented for the structure optimization of crystalline methanol, acetaldehyde and acetic acid and for the calculation of infrared frequencies. The results are compared to thin film spectra obtained from low-temperature experiments performed at the Australian Synchrotron. Harmonic frequency calculations of the internal modes calculated at the B3LYP-D3/m-6-311G(d) level shows higher deviation from infrared experiment than more advanced theory applied to the gas phase. Importantly for the solid-state, the simulation of low-frequency molecular lattice modes closely resembles the observed far-infrared features after application of a 0.92 scaling factor. This allowed experimental peaks to be assigned to specific translation and libration modes, including acetaldehyde and acetic acid lattice features for the first time. These frequency calculations have been performed without the need for supercomputing resources that are required for large molecular clusters using comparable levels of theory. This new theoretical approach will find use for the rapid characterization of intermolecular interactions and bonding in crystals, and the assignment of far-infrared spectra for crystalline samples such as pharmaceuticals and molecular ices. One interesting application may be for the detection of species of prebiotic interest on the surfaces of Kuiper-Belt and Trans-Neptunian Objects. At such locations, the three small organic molecules studied here could reside in their crystalline phase. The far-infrared spectra for their low-temperature solid phases are collected under planetary conditions, allowing us to compile and assign their most intense spectral features to assist future far-infrared surveys of icy Solar system surfaces.

Synchrotron radiation facilities at DESY, a status report

International Nuclear Information System (INIS)

Koch, E.E.

1979-12-01

A short summary of the developments which have led to the present extensive use of Synchrotron Radiation at DESY is presented and a description of the Synchrotron Radiation facilities presently available and under development is given with emphasis on the new HASYLAB project at the storage ring DORIS. (orig.) 891 HSI/orig. 892 MKO

Fifth school on Magnetism and Synchrotron Radiation

CERN Document Server

Beaurepaire, Eric; Scheurer, Fabrice; Kappler, Jean-Paul; Magnetism and Synchrotron Radiation : New Trends

2010-01-01

Advances in the synthesis of new materials with often complex, nano-scaled structures require increasingly sophisticated experimental techniques that can probe the electronic states, the atomic magnetic moments and the magnetic microstructures responsible for the properties of these materials. At the same time, progress in synchrotron radiation techniques has ensured that these light sources remain a key tool of investigation, e.g. synchrotron radiation sources of the third generation are able to support magnetic imaging on a sub-micrometer scale. With the Fifth Mittelwihr School on Magnetism and Synchrotron Radiation the tradition of teaching the state-of-the-art on modern research developments continues and is expressed through the present set of extensive lectures provided in this volume. While primarily aimed at postgraduate students and newcomers to the field, this volume will also benefit researchers and lecturers actively working in the field.

Structural evolution of regenerated silk fibroin under shear: Combined wide- and small-angle x-ray scattering experiments using synchrotron radiation

International Nuclear Information System (INIS)

Rossle, Manfred; Panine, Pierre; Urban, Volker S.; Riekel, Christine

2004-01-01

The structural evolution of regenerated Bombyx mori silk fibroin during shearing with a Couette cell has been studied in situ by synchrotron radiation small- and wide-angle x-ray scattering techniques. An elongation of fibroin molecules was observed with increasing shear rate, followed by an aggregation phase. The aggregates were found to be amorphous with β-conformation according to infrared spectroscopy. Scanning x-ray microdiffraction with a 5 (micro)m beam on aggregated material, which had solidified in air, showed silk II reflections and a material with equatorial reflections close to the silk I structure reflections, but with strong differences in reflection intensities. This silk I type material shows up to two low-angle peaks suggesting the presence of water molecules that might be intercalated between hydrogen-bonded sheets.

Structural evolution of regenerated silk fibroin under shear: Combined wide- and small-angle x-ray scattering experiments using synchrotron radiation

Energy Technology Data Exchange (ETDEWEB)

Rossle, Manfred [European Molecular Biology Laboratory (EMBL), France; Panine, Pierre [European Synchrotron Radiation Facility (ESRF); Urban, Volker S [ORNL; Riekel, Christine [European Synchrotron Radiation Facility (ESRF)

2004-04-01

The structural evolution of regenerated Bombyx mori silk fibroin during shearing with a Couette cell has been studied in situ by synchrotron radiation small- and wide-angle x-ray scattering techniques. An elongation of fibroin molecules was observed with increasing shear rate, followed by an aggregation phase. The aggregates were found to be amorphous with {beta}-conformation according to infrared spectroscopy. Scanning x-ray microdiffraction with a 5 {micro}m beam on aggregated material, which had solidified in air, showed silk II reflections and a material with equatorial reflections close to the silk I structure reflections, but with strong differences in reflection intensities. This silk I type material shows up to two low-angle peaks suggesting the presence of water molecules that might be intercalated between hydrogen-bonded sheets.

The experimental apparatus for synchrotron radiation Moessbauer spectroscopy of BL11 in SPring-8

International Nuclear Information System (INIS)

Mitsui, T.; Kitao, S.; Zhang, X.W.; Marushita, M.; Seto, M.

2001-01-01

Synchrotron radiation Moessbauer spectroscopy (time spectrum of nuclear forward scattering and nuclear resonant inelastic scattering) enables us to study both the electronic state and lattice dynamics of a target material. Furthermore, the excellent properties of synchrotron radiation (polarization, pulse, small beam size) promise us the unique studies for material science. In order to progress in these studies, some experimental apparatuses were installed in BL11XU of SPring-8

The national synchrotron: ray of hope or ring of fire?

International Nuclear Information System (INIS)

Hollis, T.

2002-01-01

While most agree the synchrotron will be a boost for Australian science, the author reports on concerns about the cost of building and operating the project Biotech industry representatives want to know how that $100 million will be used and want to see the government's justification for pouring more than a third of its total technology budget for 2001/2 into the synchrotron. They, and the opposition, also want to know where the private money will come from to make up the balance or whether the state will ultimately have to pitch in the rest itself. Indeed, an Auditor-General's report released last week warned of the need for comprehensive financial risk management of the facility. The National Synchrotron, to be built at Monash University, will be a hollow ring of about 60 metres diameter and initially housing nine beamlines, each capable of performing independent experiments simultaneously. According to Dr Richard Garrett, director of the Australian Synchrotron Research Program (http://www.ansto.gov.au/natfac/asrp.html) projection reports had indicated the local synchrotron user community would expand from about 350 researchers today to about 1200 by the time the National Synchrotron is built, with demand steadily increasing in the years following its completion

The uses of synchrotron radiation sources for elemental and chemical microanalysis

International Nuclear Information System (INIS)

Chen, J.R.; Chao, E.C.T.; Minkin, J.A.; Back, J.M.; Jones, K.W.; Rivers, M.L.; Sutton, S.R.

1989-08-01

Synchrotron radiation sources offer important features for the analysis of a material. Among these features is the ability to determine both the elemental composition of the material and the chemical state of its elements. For microscopic analysis synchrotron x-ray fluorescence (SXRF) microprobes now offer spatial resolutions of 10μm with minimum detection limits in the 1--10 ppM range depending on the nature of the sample and the synchrotron source used. This paper describes the properties of synchrotron radiation and their importance for elemental analysis, existing synchrotron facilities and those under construction that are optimum for SXRF microanalysis, and a number of applications including the high energy excitation of the K lines of heavy elements, microtomography, and XANES and EXAFS spectroscopies. 45 refs., 8 figs., 1 tab

Synchrotron radiation laboratories at the Bonn electron accelerators. a status report

Science.gov (United States)

Hormes, J.

1987-07-01

At the Physikalisches Institut of the University in Bonn experiments with synchrotron radiation were carried out ever since 1962. At the moment (June 1986) all work takes place in the SR-laboratory at the 2.5 GeV synchrotron. A 3.5 GeV stretcher ring (ELSA) is under construction and will come into operation at the end of 1986. This accelerator will also run as a storage ring for synchrotron radiation experiments and a laboratory to be used at this machine is also under consideration. The SR experiments which are carried out in Bonn try to take advantage of the fact that we are still using a high energy synchrotron for our work. Besides basic research also applied work is done using synchrotron radiation even as a production tool for X-ray lithography.

A small-angle scattering study of bacteriophage T7 using synchrotron radiation

International Nuclear Information System (INIS)

Feigin, L.A.; Svergun, D.I.; Dembo, A.T.; Ronto, G.; Toth, K.

1989-01-01

Structure transitions in the bacterial virus T7, due to an environment of varying ionic strength, are investigated by means of synchrotron radiation small-angle scattering. Effects of radiation damages and kinetics of the structure transition are separated. Time dependencies of the structural parameters and distribution functions are obtained and characteristic features of the structure rearrangements are described. (orig.)

Tabletop synchrotron and its unique features

CERN Document Server

Yamada, H

2002-01-01

Two synchrotrons, AURORA and MIRRORCLE, were built in Ritsumeikan University. MIRRORCLE-20 is the smallest normal conduction synchrotron (15 cm orbit radius and 1.2 m outer diameter) in the world. It uses 2/3 resonance method for electron beam incidence but is not optimized for X-ray generation. MIRRORCLE-6 shall be optimized for X-ray generation. X-ray generated by MIRRORCLE shows very flat white light, rich in hard X-ray, pulse with width changeable from a few mu s to a few ms , wide radiation angle of 25 mrad at MIRRORCLE-20 and 80 mrad at MIRRORCLE-8 and high coherence. The feature such as pulsed light and high coherence is expected to new application which photon radiation cannot practice. Imaging experiments by MIRRORCLE were carried out by Cu plate, Al plate, Teflon and acryl plate. We took a photograph of insect, electric lamp, connector, and cyclotron. New X-ray generation mechanism, X-ray strength, development of tabletop synchrotron and features of X-ray beam are explained. (S.Y.)

Tabletop synchrotron and its unique features

International Nuclear Information System (INIS)

Yamada, Hironari

2002-01-01

Two synchrotrons, AURORA and MIRRORCLE, were built in Ritsumeikan University. MIRRORCLE-20 is the smallest normal conduction synchrotron (15 cm orbit radius and 1.2 m outer diameter) in the world. It uses 2/3 resonance method for electron beam incidence but is not optimized for X-ray generation. MIRRORCLE-6 shall be optimized for X-ray generation. X-ray generated by MIRRORCLE shows very flat white light, rich in hard X-ray, pulse with width changeable from a few μs to a few ms , wide radiation angle of 25 mrad at MIRRORCLE-20 and 80 mrad at MIRRORCLE-8 and high coherence. The feature such as pulsed light and high coherence is expected to new application which photon radiation cannot practice. Imaging experiments by MIRRORCLE were carried out by Cu plate, Al plate, Teflon and acryl plate. We took a photograph of insect, electric lamp, connector, and cyclotron. New X-ray generation mechanism, X-ray strength, development of tabletop synchrotron and features of X-ray beam are explained. (S.Y.)

Support for the Advanced Polymers Beamline at the National Synchrotron Light Source

Energy Technology Data Exchange (ETDEWEB)

Hsiao, Benjamin S. [State Univ. of New York (SUNY), Stonybrook, NY (United States)

2008-10-01

The primary focus of the X27C beamline is to investigate frontier polymer science and engineering problems with emphasis on real-time studies of structures, morphologies and dynamics from atomic, nanoscopic, microscopic to mesoscopic scales using simultaneous small-angle X-ray scattering (SAXS) and wide-angle X-ray diffraction (WAXD) techniques. The scientific merit of this project is as follows. Currently, many unique sample chambers for in-situ synchrotron studies, developed by the PI (B. Hsiao) and Co-PI (B. Chu), are available for general users of X27C at NSLS. These instruments include a gel/melt spinning apparatus, a continuous fiber drawing apparatus, a tensile stretching apparatus, a high pressure X-ray cell using supercritical carbon dioxide, a parallel plate strain-controlled shear stage and a dynamic rheometer for small-strain oscillatory deformation study. Based on the use of these instruments in combination with synchrotron X-rays, many new insights into the relationships between processing and structure have been obtained in recent years. The broader impact of this project is as follows. The X27C beamline is the first synchrotron facility in the United States dedicated to chemistry/materials research (with emphasis on polymers). The major benefit of this facility to the materials community is that no extensive synchrotron experience and equipment preparation are required from general users to carry out cutting-edge experiments.

Synchrotron-radiation phase-contrast imaging of human stomach and gastric cancer: in vitro studies.

Science.gov (United States)

Tang, Lei; Li, Gang; Sun, Ying-Shi; Li, Jie; Zhang, Xiao-Peng

2012-05-01

The electron density resolution of synchrotron-radiation phase-contrast imaging (SR-PCI) is 1000 times higher than that of conventional X-ray absorption imaging in light elements, through which high-resolution X-ray imaging of biological soft tissue can be achieved. For biological soft tissue, SR-PCI can give better imaging contrast than conventional X-ray absorption imaging. In this study, human resected stomach and gastric cancer were investigated using in-line holography and diffraction enhanced imaging at beamline 4W1A of the Beijing Synchrotron Radiation Facility. It was possible to depict gastric pits, measuring 50-70 µm, gastric grooves and tiny blood vessels in the submucosa layer by SR-PCI. The fine structure of a cancerous ulcer was displayed clearly on imaging the mucosa. The delamination of the gastric wall and infiltration of cancer in the submucosa layer were also demonstrated on cross-sectional imaging. In conclusion, SR-PCI can demonstrate the subtle structures of stomach and gastric cancer that cannot be detected by conventional X-ray absorption imaging, which prompt the X-ray diagnosis of gastric disease to the level of the gastric pit, and has the potential to provide new methods for the imageology of gastric cancer.

CCD detectors for X-ray synchrotron radiation application

CERN Document Server

Fedotov, M G

2000-01-01

In this paper the possibility of the application of some types of CCDs for the study of fast processes (by recording an image formed by a short flash of synchrotron radiation) is considered. The first results of model experiments are also described.

Prospects of using synchrotron radiation facilities with diamond-anvil cells

International Nuclear Information System (INIS)

Manghani, M.H.; Ming, L.C.; Jamieson, J.C.

1980-01-01

Diamond-anvil pressure cells have proven versatile and useful for conducting high pressure research in the submegabar range. The interfacing of diamond-anvil cell technology with synchrotron facilities seems a logical new step for carrying out in situ X-ray diffraction studies of materials under extreme conditions of combined high pressure and temperature. The conventional film method of X-ray diffraction has definite limitations which call for the energy dispersive analysis techniques. Various potential high pressure-temperature studies in geophysis and related fields involving the use of diamond-anvil cell, synchrotron facilities and energy dispersive techniques are exemplified. For geophysical studies the conditions prevailing in 86% of the Earth's volume are capable of being simulated completely in pressure, and partially in pressure and temperature, simultaneously. (orig.)

Simulation of AZ-PN100 resist pattern fluctuation in X-ray lithography, including synchrotron beam polarization

International Nuclear Information System (INIS)

Scheckler, E.W.; Ogawa, Taro; Tanaka, Toshihiko; Takeda, Eiji; Oizumi, Hiroaki.

1993-01-01

A new simulation model for nanometer-scale pattern fluctuation in X-ray lithography is presented and applied to a study of AZ-PN100 negative chemical amplification resist. The exposure simulation considers polarized photons from a synchrotron radiation (SR) source. Monte Carlo simulation of Auger and photoelectron generation is followed by electron scattering simulation to determine the deposited energy distribution at the nanometer scale, including beam polarization effects. An acid-catalyst random walk model simulates the post-exposure bake (PEB) step. Fourier transform infrared (FTIR) spectroscopy and developed resist thickness measurements are used to fit PEB and rate models for AZ-PN100. A polymer removal model for development simulation predicts the macroscopic resist shape and pattern roughness. The simulated 3σ linewidth variation is in excess of 24 nm. Simulation also shows a detrimental effect if the beam polarization is perpendicular to the line. Simulation assuming a theoretical ideal exposure yields a 50 nm minimum line for standard process conditions. (author)

Nuclear waste viewed in a new light; a synchrotron study of uranium encapsulated in grout

Energy Technology Data Exchange (ETDEWEB)

Stitt, C.A., E-mail: Camilla.stitt@bristol.ac.uk [Interface Analysis Centre, H. H. Wills Physics Laboratory, University of Bristol, Tyndall Avenue, Bristol BS8 1TL (United Kingdom); Hart, M., E-mail: oxford.mike@gmail.com [Diamond Light Source Limited, Harwell Science and Innovation Campus, Fermi Avenue, Didcot, Oxfordshire OX11 0QX (United Kingdom); Harker, N.J., E-mail: nicholas.harker@esrf.fr [Interface Analysis Centre, H. H. Wills Physics Laboratory, University of Bristol, Tyndall Avenue, Bristol BS8 1TL (United Kingdom); Hallam, K.R., E-mail: k.r.hallam@bristol.ac.uk [Interface Analysis Centre, H. H. Wills Physics Laboratory, University of Bristol, Tyndall Avenue, Bristol BS8 1TL (United Kingdom); MacFarlane, J., E-mail: james.macfarlane@bristol.ac.uk [Interface Analysis Centre, H. H. Wills Physics Laboratory, University of Bristol, Tyndall Avenue, Bristol BS8 1TL (United Kingdom); Banos, A., E-mail: antonis.banos@bristol.ac.uk [Interface Analysis Centre, H. H. Wills Physics Laboratory, University of Bristol, Tyndall Avenue, Bristol BS8 1TL (United Kingdom); Paraskevoulakos, C., E-mail: cp13846@bristol.ac.uk [Interface Analysis Centre, H. H. Wills Physics Laboratory, University of Bristol, Tyndall Avenue, Bristol BS8 1TL (United Kingdom); Butcher, E., E-mail: ed.j.butcher@nnl.co.uk [National Nuclear Laboratory, Seascale, Cumbria CA20 1 PG (United Kingdom); Padovani, C., E-mail: cristiano.padovani@nda.gov.uk [Radioactive Waste Management Limited (formerly the Radioactive Waste Management Directorate of the UK Nuclear Decommissioning Authority), Curie Avenue, Didcot, Oxfordshire OX11 0RH (United Kingdom); Scott, T.B., E-mail: t.b.scott@bristol.ac.uk [Interface Analysis Centre, H. H. Wills Physics Laboratory, University of Bristol, Tyndall Avenue, Bristol BS8 1TL (United Kingdom)

2015-03-21

Highlights: • Unirradiated Magnox uranium was encapsulated in grout and exposed to hydrogen. • Synchrotron X-ray tomography imaged the uranium corrosion before and after exposure. • Synchrotron X-ray powder diffraction identified the corrosion products; UH{sub 3} and UO{sub 2}. • Uranium encapsulated in grout oxidised via the anoxic U + H{sub 2}O regime. • Successful in-situ, non-invasive examination of pyrophoric and radioactive material - Abstract: How do you characterise the contents of a sealed nuclear waste package without breaking it open? This question is important when the contained corrosion products are potentially reactive with air and radioactive. Synchrotron X-rays have been used to perform micro-scale in-situ observation and characterisation of uranium encapsulated in grout; a simulation for a typical intermediate level waste storage packet. X-ray tomography and X-ray powder diffraction generated both qualitative and quantitative data from a grout-encapsulated uranium sample before, and after, deliberately constrained H{sub 2} corrosion. Tomographic reconstructions provided a means of assessing the extent, rates and character of the corrosion reactions by comparing the relative densities between the materials and the volume of reaction products. The oxidation of uranium in grout was found to follow the anoxic U + H{sub 2}O oxidation regime, and the pore network within the grout was observed to influence the growth of uranium hydride sites across the metal surface. Powder diffraction analysis identified the corrosion products as UO{sub 2} and UH{sub 3}, and permitted measurement of corrosion-induced strain. Together, X-ray tomography and diffraction provide means of accurately determining the types and extent of uranium corrosion occurring, thereby offering a future tool for isolating and studying the reactions occurring in real full-scale waste package systems.

Synchrotron radiation

International Nuclear Information System (INIS)

Pattison, P.; Quinn, P.

1990-01-01

This report details the activities in synchrotron radiation and related areas at Daresbury Laboratory during 1989/90. The number and scope of the scientific reports submitted by external users and in-house staff is a reflection of the large amount of scheduled beamtime and high operating efficiency achieved at the Synchrotron Radiation Source (SRS) during the past year. Over 4000 hours of user beam were available, equivalent to about 80% of the total scheduled time. Many of the reports collected here illustrate the increasing technical complexity of the experiments now being carried out at Daresbury. Provision of the appropriate technical and scientific infrastructure and support is a continuing challenge. The development of the Materials Science Laboratory together with the existing Biological Support Laboratory will extend the range of experiments which can be carried out on the SRS. This will particularly facilitate work in which the sample must be prepared or characterised immediately before or during an experiment. The year 1989/90 has also seen a substantial upgrade of several stations, especially in the area of x-ray optics. Many of the advantages of the High Brightness Lattice can only be exploited effectively with the use of focusing optics. As the performance of these stations improves, the range of experiments which are feasible on the SRS will be extended significantly. (author)

National Synchrotron Light Source safety-analysis report

International Nuclear Information System (INIS)

Batchelor, K.

1982-07-01

This document covers all of the safety issues relating to the design and operation of the storage rings and injection system of the National Synchrotron Light Source. The building systems for fire protection, access and egress are described together with air and other gaseous control or venting systems. Details of shielding against prompt bremstrahlung radiation and synchrotron radiation are described and the administrative requirements to be satisfied for operation of a beam line at the facility are given

Optical systems for synchrotron radiation. Lecture 2. Mirror systems

International Nuclear Information System (INIS)

Howells, M.R.

1986-02-01

The process of reflection of VUV and x-radiation is summarized. The functions of mirrors in synchrotron beamlines are described, which include deflection, filtration, power absorption, formation of a real image, focusing, and collimation. Fabrication of optical surfaces for synchrotron radiation beamlines are described, and include polishing of a near spherical surface as well as bending a cylindrical surface to toroidal shape. The imperfections present in mirrors, aberrations and surface figure inaccuracy, are discussed. Calculation of the thermal load of a mirror in a synchrotron radiation beam and the cooling of the mirror are covered briefly. 50 refs., 7 figs

Automation and Remote Synchrotron Data Collection

International Nuclear Information System (INIS)

Gilski, M.

2008-01-01

X-ray crystallography is the natural choice for macromolecular structure determination by virtue of its accuracy, speed, and potential for further speed gains, while synchrotron radiation is indispensable because of its intensity and tuneability. Good X-ray crystallographic diffraction patterns are essential and frequently this is achievable through using the few large synchrotrons located worldwide. Beamline time on these facilities have long queues, and increasing the efficiency of utilization of these facilities will help in expediting the structure determination process. Automation and remote data collection are therefore essential steps in ensuring that macromolecular structure determination becomes a very high throughput process. (author)

High pressure phases of uranium monophosphide studied by synchrotron X-ray diffraction

International Nuclear Information System (INIS)

Staun Olson, J.; Gerward, L.; Benedict, U.; Dabos, S.; Vogt, O.

1988-01-01

X-ray diffraction studies have been performed on UP powder for pressures up to 51 GPa using synchrotron radiation and a diamond anvil cell. At ambient pressure UP has the rocksalt structure. The bulk modulus has been determined to B 0 = 102(4) GPa and its pressure derivative to B 0 ' = 4.0(8). The cubic phase has been found to transform to a new phase, UP II, at about 10 GPa. UP II can be characterized by a rhombohedral Bravais lattice. UP II transforms to an orthorhombic phase, UP III, at 28 GPa. No volume change has been observed at the two transitions. The influence of the 5f electrons on the transformations is discussed. (orig.)

Application of X-ray synchrotron microscopy instrumentation in biology

International Nuclear Information System (INIS)

Gasperini, F. M.; Pereira, G. R.; Granjeiro, J. M.; Calasans-Maia, M. D.; Rossi, A. M.; Perez, C. A.; Lopes, R. T.; Lima, I.

2011-01-01

X-ray micro-fluorescence imaging technique has been used as a significant tool in order to investigate minerals contents in some kinds of materials. The aim of this study was to evaluate the elemental distribution of calcium and zinc in bone substitute materials (nano-hydroxyapatite spheres) and cortical bones through X-Ray Micro-fluorescence analysis with the increment of Synchrotron Radiation in order to evaluate the characteristics of the newly formed bone and its interface, the preexisting bone and biomaterials by the arrangement of collagen fibers and its birefringence. The elemental mapping was carried out at Brazilian Synchrotron Light Laboratory, Campinas - Sao Paulo, Brazil working at D09-XRF beam line. Based on this study, the results suggest that hydroxyapatite-based biomaterials are biocompatible, promote osteo-conduction and favored bone repair. (authors)

Synchrotron x-ray fluorescence and extended x-ray absorption fine structure analysis

International Nuclear Information System (INIS)

Chen, J.R.; Gordon, B.M.; Hanson, A.L.; Jones, K.W.; Kraner, H.W.; Chao, E.C.T.; Minkin, J.A.

1984-01-01

The advent of dedicated synchrotron radiation sources has led to a significant increase in activity in many areas of science dealing with the interaction of x-rays with matter. Synchrotron radiation provides intense, linearly polarized, naturally collimated, continuously tunable photon beams, which are used to determine not only the elemental composition of a complex, polyatomic, dilute material but also the chemical form of the elements with improved accuracy. Examples of the application of synchrotron radiation include experiments in synchrotron x-ray fluorescence (SXRF) analysis and extended x-ray absorption fine structure (EXAFS) analysis. New synchrotron radiation x-ray microprobes for elemental analysis in the parts per billion range are under construction at several laboratories. 76 references, 24 figures

On the formation of an instantaneous orbit in a synchrotron

International Nuclear Information System (INIS)

Bashmakov, Yu.A.; Karpov, V.A.

1985-01-01

In the process of injection into a synchrotron amplitudes of particle betatron oscillations can be comparable with the dimensions of the synchrotron working region, which means that special attention should be paid to the formation of the optimum instantaneous orbit. Basides, a necessity to calculate the orbit frequently arises at the end of the acceleration cycle, when particle dump onto internal targets or their extraction from the synchrotron take place. In the paper the method for calculation of particle trajectories in the synchrotron is described. According to the method the program of numerical calculation of both separate particle trajectories and closed instantaneous orbit was developed. The method suggested is based on the presentation of the accelerator magnetic structure as a sequential set of discrete elements. All the elements can be divided into the following main groups: free rectilinear gaps, rectilinear gaps with stray magnetic field, magnetic sectors, rectilinear gaps with accelerating electric field. The calculations made according to the method described have shown its high efficiency. The program developed is used for the simulation of the injection into the ''Pakhra'' synchrotron

Synchrotron radiation in art and archaeology SRA 2005

International Nuclear Information System (INIS)

Pollard, A.M.; Janssens, K.; Artioli, G.; Young, M.L.; Casadio, F.; Schnepp, S.; Marvin, J.; Dunand, D.C.; Almer, J.; Fezzaa, K.; Lee, W.K.; Haeffner, D.R.; Reguer, S.; Dillmann, Ph.; Mirambet, F.; Susini, J.; Lagarde, P.; Pradell, T.; Molera, J.; Brunetti, B.; D'acapito, F.; Maurizio, C.; Mazzoldi, P.; Padovani, S.; Sgamellotti, A.; Garges, F.; Etcheverry, M.P.; Flank, A.M.; Lagarde, P.; Marcus, M.A.; Scheidegger, A.M.; Grolimund, D.; Pallot-Frossard, I.; Smith, A.D.; Jones, M.; Gliozzo, E.; Memmi-Turbanti, I.; Molera, J.; Vendrell, M.; Mcconachie, G.; Skinner, T.; Kirkman, I.W.; Pantos, E.; Wallert, A.; Kanngiesser, B.; Hahn, O.; Wilke, M.; NekaT, B.; Malzer, W.; Erko, A.; Chalmin, E.; Vignaud, C.; Farges, F.; Susini, J.; Menu, M.; Sandstrom, M.; Cotte, M.; Kennedy, C.J.; Wess, T.J.; Muller, M.; Murphy, B.; Roberts, M.A.; Burghammer, M.; Riekel, C.; Gunneweg, J.; Pantos, E.; Dik, J.; Tafforeau, P.; Boistel, R.; Boller, E.; Bravin, A.; Brunet, M.; Chaimanee, Y.; Cloetens, P.; Feist, M.; Hoszowska, J.; Jaeger, J.J.; Kay, R.F.; Lazzari, V.; Marivaux, L.; Nel, A.; Nemoz, C.; Thibault, X.; Vignaud, P.; Zabler, S.; Sciau, P.; Goudeau, P.; Tamura, N.; Doormee, E.; Kockelmann, W.; Adriaens, A.; Ryck, I. de; Leyssens, K.; Hochleitner, B.; Schreiner, M.; Drakopoulos, M.; Snigireva, I.; Snigirev, A.; Sanchez Del Rio, M.; Martinetto, P.; Dooryhee, E.; Suarez, M.; Sodo, A.; Reyes-Valerio, C.; Haro Poniatowski, E.; Picquart, M.; Lima, E.; Reguera, E.; Gunneweg, J.; Reiche, I.; Berger, A.; Bevers, H.; Duval, A.

2005-01-01

Materials - bones, artifacts, artwork,.... - lie at the heart of both archaeology and art conservation. Synchrotron radiation techniques provide powerful ways to interrogate these records of our physical and cultural past. In this workshop we will discuss and explore the current and potential applications of synchrotron radiation science to problems in archaeology and art conservation. This document gathers the abstracts of the presentations

First turn simulations in the cooler synchrotron COSY

International Nuclear Information System (INIS)

Dinev, D.

1991-07-01

This paper is devoted to the first turn correction and related problems in particle accelerators of synchrotron type. The paper consists of two parts. The first part is a survey of the existing methods for first turn steering. The second part is entirely devoted to the first turn in the cooler synchrotron COSY which is under assembling in KFA-Julich, Germany. (orig.)

Synchrotron radiation in art and archaeology SRA 2005

Energy Technology Data Exchange (ETDEWEB)

Pollard, A M; Janssens, K; Artioli, G; Young, M L; Casadio, F; Schnepp, S; Marvin, J; Dunand, D C; Almer, J; Fezzaa, K; Lee, W K; Haeffner, D R; Reguer, S; Dillmann, Ph; Mirambet, F; Susini, J; Lagarde, P; Pradell, T; Molera, J; Brunetti, B; D' acapito, F; Maurizio, C; Mazzoldi, P; Padovani, S; Sgamellotti, A; Garges, F; Etcheverry, M P; Flank, A M; Lagarde, P; Marcus, M A; Scheidegger, A M; Grolimund, D; Pallot-Frossard, I; Smith, A D; Jones, M; Gliozzo, E; Memmi-Turbanti, I; Molera, J; Vendrell, M; Mcconachie, G; Skinner, T; Kirkman, I W; Pantos, E; Wallert, A; Kanngiesser, B; Hahn, O; Wilke, M; NekaT, B; Malzer, W; Erko, A; Chalmin, E; Vignaud, C; Farges, F; Susini, J; Menu, M; Sandstrom, M; Cotte, M; Kennedy, C J; Wess, T J; Muller, M; Murphy, B; Roberts, M A; Burghammer, M; Riekel, C; Gunneweg, J; Pantos, E; Dik, J; Tafforeau, P; Boistel, R; Boller, E; Bravin, A; Brunet, M; Chaimanee, Y; Cloetens, P; Feist, M; Hoszowska, J; Jaeger, J J; Kay, R F; Lazzari, V; Marivaux, L; Nel, A; Nemoz, C; Thibault, X; Vignaud, P; Zabler, S; Sciau, P; Goudeau, P; Tamura, N; Doormee, E; Kockelmann, W; Adriaens, A; Ryck, I de; Leyssens, K; Hochleitner, B; Schreiner, M; Drakopoulos, M; Snigireva, I; Snigirev, A; Sanchez Del Rio, M; Martinetto, P; Dooryhee, E; Suarez, M; Sodo, A; Reyes-Valerio, C; Haro Poniatowski, E; Picquart, M; Lima, E; Reguera, E; Gunneweg, J; Reiche, I; Berger, A; Bevers, H; Duval, A

2005-07-01

Materials - bones, artifacts, artwork,.... - lie at the heart of both archaeology and art conservation. Synchrotron radiation techniques provide powerful ways to interrogate these records of our physical and cultural past. In this workshop we will discuss and explore the current and potential applications of synchrotron radiation science to problems in archaeology and art conservation. This document gathers the abstracts of the presentations.

Bainitic steels behavior at different temperatures: study of cementite using neutron and synchrotron radiations

International Nuclear Information System (INIS)

Ouahab, Razane

2012-01-01

The multi-scale experimental characterization of bainitic steels has been the subject of this research. Two two-phase steels ferrite-cementite were chosen: a 16MND5 steel used to design RPW reactors (Reactor Pressurized Water) and a 2C40 steel. In order to study the mechanical behavior of each phase individually, different thermomechanical characterization tools have been considered. The originality of this work comes from the use of two techniques: in situ tensile tests combined to synchrotron radiation and nano indentation. A major interest is given to the behavior of cementite. The stresses reached in this phase were determined by two methods. First, analyzes have been performed in ferritic phase by XRD and a mixture law has been used to estimate the stress values in cementite. Then, analyzes have been carried out directly in each phase using synchrotron radiation. The results show that the mixture law is a good tool to describe the stress distribution in each phase of the studied steels. However, it may be not enough because it doesn't take into account the morphology of the carbide and highly depends on the volume fraction of the cementite: an uncertainty of ± 0.2 % can lead to stress variation of ± 1000 MPa. The local properties of cementite were also analyzed by nano indentation. The primary results have confirmed that the carbide hardness is 2-3 times greater than the hardness of the matrix [fr

Observation of high-power coherent synchrotron radiation in the THz region from the JAEA energy recovery linac

International Nuclear Information System (INIS)

Takahashi, Toshiharu; Okuda, Shuichi; Minehara, Eisuke J.; Hajima, Ryoichi; Sawamura, Masaru; Nagai, Ryoji; Kikuzawa, Nobihiro; Iijima, Hokuto; Nishitani, Tomohiro; Nishimori, Nobuyuki

2007-01-01

The energy recovery linac (ERL) is able to generate high-power coherent synchrotron radiation (CSR) in the terahertz and the millimeter-wave regions, because it produces shorter bunches than usual storage rings and a higher current than conventional linacs. The spectrum of CSR has been measured at the JAEA-ERL in the wavenumber range from 0.5 to 15 cm -1 . The detected power was 2x10 -4 W/cm -1 at 2.5 cm -1 for the average beam current of 17.7 μA. When the infrared FEL was operated with the undulator in the ERL, the CSR spectrum was shifted to the longer wavelengths because of the energy broadening of the electron beam. (author)

Synchrotron X-ray induced solution precipitation of nanoparticles

CERN Document Server

Lee, H J; Hwu, Y; Tsai, W L

2003-01-01

By irradiating a solution in electroless Ni deposition using synchrotron X-rays, Ni composite was found to nucleate homogeneously and eventually precipitate in the form of nanoparticles. The size of the nanoparticles precipitated is rather uniform (100-300 nm depending on the applied temperature). By the addition of an organic acid, well-dispersed nanoparticles could be effectively deposited on glass substrate. The hydrated electrons (e sub a sub q sup -), products of radiolysis of water molecules by synchrotron X-rays, may be responsible for the effective reduction of the metal ions, resulting in homogeneous nucleation and nanoparticle formation. Our results suggest that synchrotron X-ray can be used to induce solution precipitation of nanoparticles and therefore lead to a new method of producing nanostructured particles and coating.

Discussions for the shielding materials of synchrotron radiation beamline hutches

International Nuclear Information System (INIS)

Asano, Y.

2006-01-01

Many synchrotron radiation facilities are now under operation such as E.S.R.F., APS, and S.P.ring-8. New facilities with intermediated stored electron energy are also under construction and designing such as D.I.A.M.O.N.D., S.O.L.E.I.L., and S.S.R.F.. At these third generation synchrotron radiation facilities, the beamline shielding as well as the bulk shield is very important for designing radiation safety because of intense and high energy synchrotron radiation beam. Some reasons employ lead shield wall for the synchrotron radiation beamlines. One is narrow space for the construction of many beamlines at the experimental hall, and the other is the necessary of many movable mechanisms at the beamlines, for examples. Some cases are required to shield high energy neutrons due to stored electron beam loss and photoneutrons due to gas Bremsstrahlung. Ordinary concrete and heavy concrete are coming up to shield material of synchrotron radiation beamline hutches. However, few discussions have been performed so far for the shielding materials of the hutches. In this presentation, therefore, we will discuss the characteristics of the shielding conditions including build up effect for the beamline hutches by using the ordinary concrete, heavy concrete, and lead for shielding materials with 3 GeV and 8 GeV class synchrotron radiation source. (author)

Synchrotron radiation in transactinium research report of the workshop

Energy Technology Data Exchange (ETDEWEB)

1992-11-01

This report contains viewgraphs on the following topics. The advanced light source U8 undulator beamline, 20--300 eV; gas-phase actinide studies with synchrotron radiation; atomic structure calculations for heavy atoms; flux growth of single crystal uranium intermetallics: Extension to transuranics; x-ray absorption near-edge structure studies of actinide compounds; surface as a new stage for studying actinides: Theoretical study of the surface electronic structure of uranium; magnetic x-ray scattering experiments at resonant energies; beamline instruments for radioactive materials; the search for x-ray absorption magnetic circular dichroism in actinide materials: preliminary experiments using UFe[sub 2] and U-S; the laser plasma laboratory light source: a source of preliminary transuranic data; electron spectroscopy of heavy fermion actinide materials; study of thin layers of actinides. Present status and future use of synchrotron radiation; electronic structure and correlated-electron theory for actinide materials; and heavy fermion and kondo phenomena in actinide materials.