Dielectric and Radiative Properties of Sea Foam at Microwave Frequencies: Conceptual Understanding of Foam Emissivity

OpenAIRE

Peter W. Gaiser; Magdalena D. Anguelova

2012-01-01

Foam fraction can be retrieved from space-based microwave radiometric data at frequencies from 1 to 37 GHz. The retrievals require modeling of ocean surface emissivity fully covered with sea foam. To model foam emissivity well, knowledge of foam properties, both mechanical and dielectric, is necessary because these control the radiative processes in foam. We present a physical description of foam dielectric properties obtained from the foam dielectric constant including foam skin depth; foam ...

Investigation of the microwave emission from the PRETEXT tokamak

International Nuclear Information System (INIS)

Gandy, R.F.

1981-10-01

A study of the microwave emission from the PRETEXT tokamak has been conducted. Two types of emission have been observed: electron cyclotron and electron plasma frequency. Three general emission regimes have been identified. These regimes are best classified by the dimensionless parameter α, where α = ω/sub pe//Ω/sub e/

Sensitivity Analysis of b-factor in Microwave Emission Model for Soil Moisture Retrieval: A Case Study for SMAP Mission

Directory of Open Access Journals (Sweden)

Dugwon Seo

2010-05-01

Full Text Available Sensitivity analysis is critically needed to better understand the microwave emission model for soil moisture retrieval using passive microwave remote sensing data. The vegetation b-factor along with vegetation water content and surface characteristics has significant impact in model prediction. This study evaluates the sensitivity of the b-factor, which is function of vegetation type. The analysis is carried out using Passive and Active L and S-band airborne sensor (PALS and measured field soil moisture from Southern Great Plains experiment (SGP99. The results show that the relative sensitivity of the b-factor is 86% in wet soil condition and 88% in high vegetated condition compared to the sensitivity of the soil moisture. Apparently, the b-factor is found to be more sensitive than the vegetation water content, surface roughness and surface temperature; therefore, the effect of the b-factor is fairly large to the microwave emission in certain conditions. Understanding the dependence of the b-factor on the soil and vegetation is important in studying the soil moisture retrieval algorithm, which can lead to potential improvements in model development for the Soil Moisture Active-Passive (SMAP mission.

Simultaneous emissions of X-rays and microwaves from long laboratory sparks and downward lightning leaders

Science.gov (United States)

Montanya, J.; Oscar, V. D. V.; Tapia, F. F.

2017-12-01

Since the discovery of the Terrestrial Gamma-ray Flashes more than 20 years ago, investigations on high energy emissions from natural lightning and high voltage laboratory sparks gained significant interest. X-ray emissions from lightning as well from high voltage laboratory sparks have in common the role played by negative leaders/streamers. On the other hand, negative leaders are well known to produce much more VHF and microwave radiation than positive leaders. Moreover, in previous works, microwave emissions from lightning leaders have been attributed to Bremsstrahlung process. The object of this work is to investigate if X-rays and RF microwave emissions share the same origin. We present simultaneous measurements of X-rays and microwaves in high voltage sparks and natural lightning. The instrumentation consists on a NaI(Tl) and LaBr3 scintillation detectors and two different receivers. One is fix tuned at 2.4 GHz with a bandwidth of 5.5 MHz. The second can be tuned at any frequency up to 18 GHz with different selectable bandwidths of 10 MHz, 40 MHz and 100 MHz. In the laboratory, results have shown that all the sparks presented microwave radiation before the breakdown of the gap, either X-rays were detected or not. In the cases where X-rays were identified, microwave emissions peaked at the same time (in the microsecond scale). We found that the power amplitudes of the microwave emissions are related to the applied voltage to the gap. In the same configuration, those cases where X-rays were detected microwave emissions presented higher power levels. The results suggest that in some part of the discharge electrons are very fast accelerated allowing, in some cases, to reach enought energy to produce X-rays. In the field, we have found similar results. On 13th of June of 2015 a bipolar cloud-to-ground flash struck 200 m close to the Eagle Nest instrumented tower (Spanish Pyrenees, 2536 m ASL). The flash presented four strokes and, in all of them, microwave

Venus Monitoring Camera (VMC/VEx) 1 micron emissivity and Magellan microwave properties of crater-related radar-dark parabolas and other terrains

Science.gov (United States)

Basilevsky, A. T.; Shalygina, O. S.; Bondarenko, N. V.; Shalygin, E. V.; Markiewicz, W. J.

2017-09-01

The aim of this work is a comparative study of several typical radar-dark parabolas, the neighboring plains and some other geologic units seen in the study areas which include craters Adivar, Bassi, Bathsheba, du Chatelet and Sitwell, at two depths scales: the upper several meters of the study object available through the Magellan-based microwave (at 12.6 cm wavelength) properties (microwave emissivity, Fresnel reflectivity, large-scale surface roughness, and radar cross-section), and the upper hundreds microns of the object characterized by the 1 micron emissivity resulted from the analysis of the near infra-red (NIR) irradiation of the night-side of the Venusian surface measured by the Venus Monitoring Camera (VMC) on-board of Venus Express (VEx).

[Study on the Emission Spectrum of Hydrogen Production with Microwave Discharge Plasma in Ethanol Solution].

Science.gov (United States)

Sun, Bing; Wang, Bo; Zhu, Xiao-mei; Yan, Zhi-yu; Liu, Yong-jun; Liu, Hui

2016-03-01

Hydrogen is regarded as a kind of clean energy with high caloricity and non-pollution, which has been studied by many experts and scholars home and abroad. Microwave discharge plasma shows light future in the area of hydrogen production from ethanol solution, providing a new way to produce hydrogen. In order to further improve the technology and analyze the mechanism of hydrogen production with microwave discharge in liquid, emission spectrum of hydrogen production by microwave discharge plasma in ethanol solution was being studied. In this paper, plasma was generated on the top of electrode by 2.45 GHz microwave, and the spectral characteristics of hydrogen production from ethanol by microwave discharge in liquid were being studied using emission spectrometer. The results showed that a large number of H, O, OH, CH, C2 and other active particles could be produced in the process of hydrogen production from ethanol by microwave discharge in liquid. The emission spectrum intensity of OH, H, O radicals generated from ethanol is far more than that generated from pure water. Bond of O-H split by more high-energy particles from water molecule was more difficult than that from ethanol molecule, so in the process of hydrogen production by microwave discharge plasma in ethanol solution; the main source of hydrogen was the dehydrogenation and restructuring of ethanol molecules instead of water decomposition. Under the definite external pressure and temperature, the emission spectrum intensity of OH, H, O radicals increased with the increase of microwave power markedly, but the emission spectrum intensity of CH, C2 active particles had the tendency to decrease with the increase of microwave power. It indicated that the number of high energy electrons and active particles high energy electron energy increased as the increase of microwave power, so more CH, C2 active particles were split more thoroughly.

Microfabricated Microwave-Integrated Surface Ion Trap

Science.gov (United States)

Revelle, Melissa C.; Blain, Matthew G.; Haltli, Raymond A.; Hollowell, Andrew E.; Nordquist, Christopher D.; Maunz, Peter

2017-04-01

Quantum information processing holds the key to solving computational problems that are intractable with classical computers. Trapped ions are a physical realization of a quantum information system in which qubits are encoded in hyperfine energy states. Coupling the qubit states to ion motion, as needed for two-qubit gates, is typically accomplished using Raman laser beams. Alternatively, this coupling can be achieved with strong microwave gradient fields. While microwave radiation is easier to control than a laser, it is challenging to precisely engineer the radiated microwave field. Taking advantage of Sandia's microfabrication techniques, we created a surface ion trap with integrated microwave electrodes with sub-wavelength dimensions. This multi-layered device permits co-location of the microwave antennae and the ion trap electrodes to create localized microwave gradient fields and necessary trapping fields. Here, we characterize the trap design and present simulated microwave performance with progress towards experimental results. This research was funded, in part, by the Office of the Director of National Intelligence (ODNI), Intelligence Advanced Research Projects Activity (IARPA).

Anomalous microwave emission from spinning nanodiamonds around stars

Science.gov (United States)

Greaves, J. S.; Scaife, A. M. M.; Frayer, D. T.; Green, D. A.; Mason, B. S.; Smith, A. M. S.

2018-06-01

Several interstellar environments produce anomalous microwave emission (AME), with brightness peaks at tens-of-gigahertz frequencies1. The emission's origins are uncertain; rapidly spinning nanoparticles could emit electric-dipole radiation2, but the polycyclic aromatic hydrocarbons that have been proposed as the carrier are now found not to correlate with Galactic AME signals3,4. The difficulty is in identifying co-spatial sources over long lines of sight. Here, we identify AME in three protoplanetary disks. These are the only known systems that host hydrogenated nanodiamonds5, in contrast with the very common detection of polycyclic aromatic hydrocarbons6. Using spectroscopy, the nanodiamonds are located close to the host stars, at physically well-constrained temperatures7. Developing disk models8, we reproduce the emission with diamonds 0.75-1.1 nm in radius, holding ≤1-2% of the carbon budget. Ratios of microwave emission to stellar luminosity are approximately constant, allowing nanodiamonds to be ubiquitous, but emitting below the detection threshold in many star systems. This result is compatible with the findings of similar-sized diamonds within Solar System meteorites9. As nanodiamond spectral absorption is seen in interstellar sightlines10, these particles are also a candidate for generating galaxy-scale3 AME.

Coupling the snow thermodynamic model SNOWPACK with the microwave emission model of layered snowpacks for subarctic and arctic snow water equivalent retrievals

Science.gov (United States)

Langlois, A.; Royer, A.; Derksen, C.; Montpetit, B.; Dupont, F.; GoïTa, K.

2012-12-01

Satellite-passive microwave remote sensing has been extensively used to estimate snow water equivalent (SWE) in northern regions. Although passive microwave sensors operate independent of solar illumination and the lower frequencies are independent of atmospheric conditions, the coarse spatial resolution introduces uncertainties to SWE retrievals due to the surface heterogeneity within individual pixels. In this article, we investigate the coupling of a thermodynamic multilayered snow model with a passive microwave emission model. Results show that the snow model itself provides poor SWE simulations when compared to field measurements from two major field campaigns. Coupling the snow and microwave emission models with successive iterations to correct the influence of snow grain size and density significantly improves SWE simulations. This method was further validated using an additional independent data set, which also showed significant improvement using the two-step iteration method compared to standalone simulations with the snow model.

SURFACE FILMS TO SUPPRESS FIELD EMISSION IN HIGH-POWER MICROWAVE COMPONENTS

Energy Technology Data Exchange (ETDEWEB)

Hirshfield, Jay l

2014-02-07

Results are reported on attempts to reduce the RF breakdown probability on copper accelerator structures by applying thin surface films that could suppress field emission of electrons. Techniques for application and testing of copper samples with films of metals with work functions higher than copper are described, principally for application of platinum films, since platinum has the second highest work function of any metal. Techniques for application of insulating films are also described, since these can suppress field emission and damage on account of dielectric shielding of fields at the copper surface, and on account of the greater hardness of insulating films, as compared with copper. In particular, application of zirconium oxide films on high-field portions of a 11.424 GHz SLAC cavity structure for breakdown tests are described.

Significance of agricultural row structure on the microwave emissivity of soils

Science.gov (United States)

Promes, P. M.; Jackson, T. J.; O'Neill, P. E.

1987-01-01

A series of field experiments was carried out to extend the data base available for verifying agricultural row effect models of emissivity. The row effects model was used to simulate a data base from which an algorithm could be developed to account for row effects when the scene dielectric constant and small-scale roughness are unknown. One objective of the study was to quantify the significance of row structure and to develop a practical procedure for removing the effects of periodic row structure on the microwave emissivity of a soil in order to use the emissivity values to estimate the soil moisture. A second objective was to expand the data set available for model verification through field observations using a truck-mounted 1.4-GHz microwave radiometer.

MEMLS3&a: Microwave Emission Model of Layered Snowpacks adapted to include backscattering

Directory of Open Access Journals (Sweden)

M. Proksch

2015-08-01

Full Text Available The Microwave Emission Model of Layered Snowpacks (MEMLS was originally developed for microwave emissions of snowpacks in the frequency range 5–100 GHz. It is based on six-flux theory to describe radiative transfer in snow including absorption, multiple volume scattering, radiation trapping due to internal reflection and a combination of coherent and incoherent superposition of reflections between horizontal layer interfaces. Here we introduce MEMLS3&a, an extension of MEMLS, which includes a backscatter model for active microwave remote sensing of snow. The reflectivity is decomposed into diffuse and specular components. Slight undulations of the snow surface are taken into account. The treatment of like- and cross-polarization is accomplished by an empirical splitting parameter q. MEMLS3&a (as well as MEMLS is set up in a way that snow input parameters can be derived by objective measurement methods which avoid fitting procedures of the scattering efficiency of snow, required by several other models. For the validation of the model we have used a combination of active and passive measurements from the NoSREx (Nordic Snow Radar Experiment campaign in Sodankylä, Finland. We find a reasonable agreement between the measurements and simulations, subject to uncertainties in hitherto unmeasured input parameters of the backscatter model. The model is written in Matlab and the code is publicly available for download through the following website: http://www.iapmw.unibe.ch/research/projects/snowtools/memls.html.

Microwave emission from the coronae of late-type dwarf stars

Science.gov (United States)

Linsky, J. L.; Gary, D. E.

1983-01-01

VLA microwave observations of 14 late-type dwarf and subgiant stars and binary systems are examined. In this extensive set of observations, four sources at 6 cm (Chi-1 Ori, UV Cet, YY Gem, and Wolf 630AB) were detected and low upper limits for the remaining stars were found. The microwave luminosities of the nondetected F-K dwarfs are as small as 0.01 those of the dMe stars. The detected emission is slowly variable in all cases and is consistent with gyroresonant emission from thermal electrons spiraling in magnetic fields of about 300 gauss if the source sizes are as large as R/R(asterisk) = 3-4. This would correspond to magnetic fields that are probably in the range 0.001-0.0001 gauss at the photospheric level. An alternative mechanism is gyrosynchrotron emission from a relatively small number of electrons with effective temperature.

Influence of microwave frequency electromagnetic radiation on terpene emission and content in aromatic plants.

Science.gov (United States)

Soran, Maria-Loredana; Stan, Manuela; Niinemets, Ülo; Copolovici, Lucian

2014-09-15

Influence of environmental stress factors on both crop and wild plants of nutritional value is an important research topic. The past research has focused on rising temperatures, drought, soil salinity and toxicity, but the potential effects of increased environmental contamination by human-generated electromagnetic radiation on plants have little been studied. Here we studied the influence of microwave irradiation at bands corresponding to wireless router (WLAN) and mobile devices (GSM) on leaf anatomy, essential oil content and volatile emissions in Petroselinum crispum, Apium graveolens and Anethum graveolens. Microwave irradiation resulted in thinner cell walls, smaller chloroplasts and mitochondria, and enhanced emissions of volatile compounds, in particular, monoterpenes and green leaf volatiles (GLV). These effects were stronger for WLAN-frequency microwaves. Essential oil content was enhanced by GSM-frequency microwaves, but the effect of WLAN-frequency microwaves was inhibitory. There was a direct relationship between microwave-induced structural and chemical modifications of the three plant species studied. These data collectively demonstrate that human-generated microwave pollution can potentially constitute a stress to the plants. Copyright © 2014 Elsevier GmbH. All rights reserved.

Influence of microwave frequency electromagnetic radiation on terpene emission and content in aromatic plants

Science.gov (United States)

Soran, Maria-Loredana; Stan, Manuela; Niinemets, Ülo; Copolovici, Lucian

2015-01-01

Influence of environmental stress factors on both crop and wild plants of nutritional value is an important research topic. The past research has focused on rising temperatures, drought, soil salinity and toxicity, but the potential effects of increased environmental contamination by human-generated electromagnetic radiation on plants have little been studied. Here we studied the influence of microwave irradiation at bands corresponding to wireless router (WLAN) and mobile devices (GSM) on leaf anatomy, essential oil content and volatile emissions in Petroselinum crispum, Apium graveolens and Anethum graveolens. Microwave irradiation resulted in thinner cell walls, smaller chloroplasts and mitochondria, and enhanced emissions of volatile compounds, in particular, monoterpenes and green leaf volatiles. These effects were stronger for WLAN-frequency microwaves. Essential oil content was enhanced by GSM-frequency microwaves, but the effect of WLAN-frequency microwaves was inhibitory. There was a direct relationship between microwave-induced structural and chemical modifications of the three plant species studied. These data collectively demonstrate that human-generated microwave pollution can potentially constitute a stress to the plants. PMID:25050479

Synergistic estimation of surface parameters from jointly using optical and microwave observations in EOLDAS

Science.gov (United States)

Timmermans, Joris; Gomez-Dans, Jose; Lewis, Philip; Loew, Alexander; Schlenz, Florian

2017-04-01

The large amount of remote sensing data nowadays available provides a huge potential for monitoring crop development, drought conditions and water efficiency. This potential however not been realized yet because algorithms for land surface parameter retrieval mostly use data from only a single sensor. Consequently products that combine different low-level observations from different sensors are hard to find. The lack of synergistic retrieval is caused because it is easier to focus on single sensor types/footprints and temporal observation times, than to find a way to compensate for differences. Different sensor types (microwave/optical) require different radiative transfer (RT) models and also require consistency between the models to have any impact on the retrieval of soil moisture by a microwave instrument. Varying spatial footprints require first proper collocation of the data before one can scale between different resolutions. Considering these problems, merging optical and microwave observations have not been performed yet. The goal of this research was to investigate the potential of integrating optical and microwave RT models within the Earth Observation Land Data Assimilation System (EOLDAS) synergistically to derive biophysical parameters. This system uses a Bayesian data assimilation approach together with observation operators such as the PROSAIL model to estimate land surface parameters. For the purpose of enabling the system to integrate passive microwave radiation (from an ELBARRA II passive microwave radiometer), the Community Microwave Emission Model (CMEM) RT-model, was integrated within the EOLDAS system. In order to quantify the potential, a variety of land surface parameters was chosen to be retrieved from the system, in particular variables that a) impact only optical RT (such as leaf water content and leaf dry matter), b) only impact the microwave RT (such as soil moisture and soil temperature), and c) Leaf Area Index (LAI) that impacts both

A Cherenkov-emission Microwave Source*

Science.gov (United States)

Lai, C. H.; Yoshii, J.; Katsouleas, T.; Hairapetian1, G.; Joshi, C.; Mori, W.

1996-11-01

In an unmagnetized plasma, there is no Cherenkov emission because the phase velocity vf of light is greater than c. In a magnetized plasma, the situation is completely changed. There is a rich variety of plasma modes with phase velocities vf 2 c which can couple to a fast particle. In the magnetized plasma, a fast particle, a particle beam, or even a short laser pulse excites a Cherenkov wake that has both electrostatic and electromagnetic components. Preliminary simulations indicate that at the vacuum/plasma boundary, the wake couples to a vacuum microwave with an amplitude equal to the electromagnetic component in the plasma. For a weakly magnetized plasma, the amplitude of the out-coupled radiation is approximately wc/wp times the amplitude of the wake excited in the plasma by the beam, and the frequency is approximately wp. Since plasma wakes as high as a few GeV/m are produced in current experiments, the potential for a high-power (i.e., GWatt) coherent microwave to THz source exists. In this talk, a brief overview of the scaling laws will be presented, followed by 1-D and 2-D PIC simulations. Prospects for a tuneable microwave source experiment based on this mechanism at the UCLA plasma wakefield accelerator facility will be discussed. *Work supported by AFOSR Grant #F4 96200-95-0248 and DOE Grant # DE-FG03-92ER40745. 1Now at Hughes Research Laboratories, Malibu, CA 90265

Microwave Remote Sensing Modeling of Ocean Surface Salinity and Winds Using an Empirical Sea Surface Spectrum

Science.gov (United States)

Yueh, Simon H.

2004-01-01

Active and passive microwave remote sensing techniques have been investigated for the remote sensing of ocean surface wind and salinity. We revised an ocean surface spectrum using the CMOD-5 geophysical model function (GMF) for the European Remote Sensing (ERS) C-band scatterometer and the Ku-band GMF for the NASA SeaWinds scatterometer. The predictions of microwave brightness temperatures from this model agree well with satellite, aircraft and tower-based microwave radiometer data. This suggests that the impact of surface roughness on microwave brightness temperatures and radar scattering coefficients of sea surfaces can be consistently characterized by a roughness spectrum, providing physical basis for using combined active and passive remote sensing techniques for ocean surface wind and salinity remote sensing.

Microwave emission from the coronae of late-type dwarf stars

Energy Technology Data Exchange (ETDEWEB)

Linsky, J.L.; Gary, D.E.

1983-11-15

We present VLA microwave observatios of 14 late-type dwarf and subgiant stars ad binary systems. In this extensive set of observations we detected four sources at 6 cm (chi/sup 1/ Ori, UV Cet, YY Gem, and Wolf 630AB) and found low upper limits for the remaining stars. The microwave luminosities of the nondetected F--K dwarfs are as small as 10/sup -2/ those of the dMe stars. The detected emission is slowly variable in all cases and is consistent with gyroresonant emission from thermal electrons spiralig in magnetic fields of about 300 gauss if the source sizes are as large as R/R/sub asterisk/roughly-equal3--4. This would correspond to magnetic fields that are probably in the range 10/sup 3/--10/sup 4/ gauss at the photospheric level. These photospheric field strengths are somewhat larger than have been observed so far in G--K dwarfs. An alternative mechanism is gyrosynchrotron emission from a relatively small number of electrons (only 10/sup -3/ the number of ambient electrons) with effective temperature, T/sub eff/>10/sup 8/ K. This mechanism is consistent with much smaller and presumably more realistic source sizes. Observations of YY gem dMle+dMle) at a number of phase are consistent with maximum but variable microwave flux at the same phase as miximum plage and central meridian passage of a large starspot of the secondary star. If confirmed by subsequent observations, this provides the first direct evidence that the emission process is magnetic in character on dMe stars.

Effect of a microwave field on the cascade arc light emission

NARCIS (Netherlands)

Gerasimov, N.T.; Rosado, R.J.; Schram, D.C.

1977-01-01

The effect of a pulsed microwave field on the integral light emission from the argon plasma of a DC atmospheric-pressure cascade arc is investigated experimentally. An intensive light pulse and oscillations of light emission at frequencies of the order of 10 kHz are observed. The shape and amplitude

Microwave emission from flaring magnetic loops

International Nuclear Information System (INIS)

Vlahos, L.

1980-01-01

The microwave emission from a flaring loop is considered. In particular the author examines the question: What will be the characteristics of the radio emission at centimeter wavelengths from a small compact flaring loop when the mechanism which pumps magnetic energy into the plasma in the form of heating and/or electron acceleration satisfies the conditions: (a) the magnetic energy is released in a small volume compared to the volume of the loop, and the rate at which magnetic energy is transformed into plasma energy is faster than the energy losses from the same volume. This causes a local enhancement of the temperature by as much as one or two orders of magnitude above the coronal temperature; (b) The bulk of the energy released goes into heating the plasma and heats primarily the electrons. (Auth.)

Application of microwave energy in the control of DPM, oxides of nitrogen and VOC emissions

Science.gov (United States)

Pallavkar, Sameer M.

The emissions of DPM (diesel particulate matter), NOx (oxides of nitrogen), and toxic VOCs (volatile organic compounds) from diesel engine exhaust gases and other sources such as chemical process industry and manufacturing industry have been a great environmental and health concern. Most control technologies for these emissions require elevated temperatures. The use of microwave energy as a source of heat energy, however, has not been fully explored. In this study, the microwave energy was used as the energy source in three separate emission control processes, namely, the regeneration of diesel particulate filter (DPF) for DPM control, the NOx reduction using a platinum catalyst, and the VOC destruction involving a ceramic based material. The study has demonstrated that microwave heating is an effective method in providing heat for the studied processes. The control efficiencies associated with the microwave-assisted processes have been observed to be high and acceptable. Further research, however, is required for the commercial use of these technologies.

L-Band H Polarized Microwave Emission During the Corn Growth Cycle

Science.gov (United States)

Joseph, A. T.; va der Velde, R.; O'Neill, P. E.; Kim, E.; Lang, R. H.; Gish, T.

2012-01-01

Hourly L-band (1.4 GHz) horizontally (H) polarized brightness temperatures (T(sub B))'s measured during five episodes (more than two days of continuous measurements) of the 2002 corn growth cycle are analyzed. These T(sub B)'s measurements were acquired as a part of a combined active/passive microwave field campaign, and were obtained at five incidence and three azimuth angles relative to the row direction. In support of this microwave data collection, intensive ground sampling took place once a week. Moreover, the interpretation of the hourly T(sub B)'s could also rely on the data obtained using the various automated instruments installed in the same field. In this paper, the soil moisture and temperature measured at fixed time intervals have been employed as input for the tau-omega model to reproduce the hourly T(sub B). Through the calibration of the vegetation and surface roughness parameterizations, the impact of the vegetation morphological changes on the microwave emission and the dependence of the soil surface roughness parameter, h(sub r), on soil moisture are investigated. This analysis demonstrates that the b parameter, appearing in the representation of the canopy opacity, has an angular dependence that varies throughout the growing period and also that the parameter hr increases as the soil dries in a portion of the dry-down cycle. The angular dependence of the b parameter imposes the largest uncertainty on T(sub B) simulations near senescence as the response of b to the incidence is also affected by the crop row orientation. On the other hand, the incorporation of a soil moisture dependent h(sub r) parameterization was responsible for the largest error reduction of T(sub B) simulations in the early growth cycle.

Response surface optimisation for activation of bentonite with microwave irradiation

Directory of Open Access Journals (Sweden)

Rožić Ljiljana S.

2011-01-01

Full Text Available In this study, the statistical design of the experimental method was applied on the acid activation process of bentonite with microwave irradiation. The influence of activation parameters (time, acid normality and microwave heating power on the selected process response of the activated bentonite samples was studied. The specific surface area was chosen for the process response, because the chemical, surface and structural properties of the activated clay determine and limit its potential applications. The relationship of various process parameters with the specific surface area of bentonite was examined. A mathematical model was developed using a second-order response surface model (RSM with a central composite design incorporating the above mentioned process parameters. The mathematical model developed helped in predicting the variation in specific surface area of activated bentonite with time (5-21 min, acid normality (2-7 N and microwave heating power (63-172 W. The calculated regression models were found to be statistically significant at the required range and presented little variability. Furthermore, high values of R2 (0.957 and R2 (adjusted (0.914 indicate a high dependence and correlation between the observed and the predicted values of the response. These high values also indicate that about 96% of the result of the total variation can be explained by this model. In addition, the model shows that increasing the time and acid normality improves the textural properties of bentonites, resulting in increased specific surface area. This model also can be useful for setting an optimum value of the activation parameters for achieving the maximum specific surface area. An optimum specific surface area of 142 m2g-1 was achieved with an acid normality of 5.2 N, activation time of 7.38 min and microwave power of 117 W. Acid activation of bentonite was found to occur faster with microwave irradiation than with conventional heating. Microwave

Fast surface modification by microwave assisted click reactions on silicon substrates

NARCIS (Netherlands)

Haensch, C.; Erdmenger, T.; Fijten, M.W.M.; Höppener, S.; Schubert, U.S.

2009-01-01

Microwave irradiation has been used for the chemical modification of functional monolayers on silicon surfaces. The thermal and chemical stability of these layers was tested under microwave irradiation to investigate the possibility to use this alternative heating process for the surface

Control of spontaneous emission from a microwave-field-driven four-level atom in an anisotropic photonic crystal

Science.gov (United States)

Zhang, Duo; Li, Jiahua; Ding, Chunling; Yang, Xiaoxue

2012-05-01

The spontaneous emission properties of a microwave-field-driven four-level atom embedded in anisotropic double-band photonic crystals (PCs) are investigated. We discuss the influences of the band-edge positions, Rabi frequency and detuning of the microwave field on the emission spectrum. It is found that several interesting features such as spectral-line enhancement, spectral-line suppression, spectral-line overlap, and multi-peak structures can be observed in the spectra. The proposed scheme can be achieved by use of a microwave-coupled field into hyperfine levels in rubidium atom confined in a photonic crystal. These theoretical investigations may provide more degrees of freedom to manipulate the atomic spontaneous emission.

Comparison of global cloud liquid water path derived from microwave measurements with CERES-MODIS

Science.gov (United States)

Yi, Y.; Minnis, P.; Huang, J.; Lin, B.; Ayers, K.; Sun-Mack, S.; Fan, A.

Cloud liquid water path LWP is a crucial parameter for climate studies due to the link that it provides between the atmospheric hydrological and radiative budgets Satellite-based visible infrared techniques such as the Visible Infrared Solar Split-Window Technique VISST can retrieve LWP for water clouds assumes single-layer over a variety of surfaces If the water clouds are overlapped by ice clouds the LWP of the underlying clouds can not be retrieved by such techniques However microwave techniques may be used to retrieve the LWP underneath ice clouds due to the microwave s insensitivity to cloud ice particles LWP is typically retrieved from satellite-observed microwave radiances only over ocean due to variations of land surface temperature and emissivity Recently Deeter and Vivekanandan 2006 developed a new technique for retrieving LWP over land In order to overcome the sensitivity to land surface temperature and emissivity their technique is based on a parameterization of microwave polarization-difference signals In this study a similar regression-based technique for retrieving LWP over land and ocean using Advanced Microwave Scanning Radiometer - EOS AMSR-E measurements is developed Furthermore the microwave surface emissivities are also derived using clear-sky fields of view based on the Clouds and Earth s Radiant Energy System Moderate-resolution Imaging Spectroradiometer CERES-MODIS cloud mask These emissivities are used in an alternate form of the technique The results are evaluated using independent measurements such

A CASE AGAINST SPINNING PAHS AS THE SOURCE OF THE ANOMALOUS MICROWAVE EMISSION

Energy Technology Data Exchange (ETDEWEB)

Hensley, Brandon S.; Draine, B. T. [Department of Astrophysical Sciences, Princeton University, Princeton, NJ 08544 (United States); Meisner, Aaron M., E-mail: brandon.s.hensley@jpl.nasa.gov [Berkeley Center for Cosmological Physics, Berkeley, CA 94720 (United States)

2016-08-10

We employ an all-sky map of the anomalous microwave emission (AME) produced by component separation of the microwave sky to study correlations between the AME and Galactic dust properties. We find that while the AME is highly correlated with all tracers of dust emission, the best predictor of the AME strength is the dust radiance. Fluctuations in the AME intensity per dust radiance are uncorrelated with fluctuations in the emission from polycyclic aromatic hydrocarbons (PAHs), casting doubt on the association between AME and PAHs. The PAH abundance is strongly correlated with the dust optical depth and dust radiance, consistent with PAH destruction in low density regions. We find that the AME intensity increases with increasing radiation field strength, at variance with predictions from the spinning dust hypothesis. Finally, the temperature dependence of the AME per dust radiance disfavors the interpretation of the AME as thermal emission. A reconsideration of other AME carriers, such as ultrasmall silicates, and other emission mechanisms, such as magnetic dipole emission, is warranted.

The Nanophysics of Electron Emission and Breakdown for High Power Microwave Source

Science.gov (United States)

2009-12-21

coaxial anode/collector. 3.1.2. Formation of  plasma  filaments during w‐band microwave breakdown  Regular, two-dimensional plasma ...Injection Gun ," IEEE Trans. Elec. Devices (May, 2005). 2. Booske, John H., “ Plasma physics and related challenges of millimeter-to-terahertz and...high power microwave (HPM) device technologies by establishing new physical understanding of electron emission/absorption and plasma breakdown

Enhanced field emission characteristics of boron doped diamond films grown by microwave plasma assisted chemical vapor deposition

Energy Technology Data Exchange (ETDEWEB)

Koinkar, Pankaj M. [Center for International Cooperation in Engineering Education (CICEE), University of Tokushima, 2-1 Minami-josanjima-cho, Tokushima 770-8506 (Japan); Patil, Sandip S. [Center for Advanced Studies in Materials Science and Condensed Matter Physics, Department of Physics, University of Pune, Pune 411007 (India); Kim, Tae-Gyu [Department of Nano System and Process Engineering, Pusan National University, 50 Cheonghak-ri, Samrangjin-eup, Miryang, Gyeongnam, Pusan 627-706 (Korea, Republic of); Yonekura, Daisuke [Department of Mechanical Engineering, University of Tokushima, 2-1 Minami-josanjima-cho, Tokushima 770-8506 (Japan); More, Mahendra A., E-mail: mam@physics.unipune.ac.in [Center for Advanced Studies in Materials Science and Condensed Matter Physics, Department of Physics, University of Pune, Pune 411007 (India); Joag, Dilip S. [Center for Advanced Studies in Materials Science and Condensed Matter Physics, Department of Physics, University of Pune, Pune 411007 (India); Murakami, Ri-ichi, E-mail: murakami@me.tokushima-u.ac.jp [Department of Mechanical Engineering, University of Tokushima, 2-1 Minami-josanjima-cho, Tokushima 770-8506 (Japan)

2011-01-01

Boron doped diamond films were synthesized on silicon substrates by microwave plasma chemical vapor deposition (MPCVD) technique. The effect of B{sub 2}O{sub 3} concentration varied from 1000 to 5000 ppm on the field emission characteristics was examined. The surface morphology and quality of films were characterized by scanning electron microscope (SEM) and Raman spectroscopy. The surface morphology obtained by SEM showed variation from facetted microcrystal covered with nanometric grains to cauliflower of nanocrystalline diamond (NCD) particles with increasing B{sub 2}O{sub 3} concentration. The Raman spectra confirm the formation of NCD films. The field emission properties of NCD films were observed to improve upon increasing boron concentration. The values of the onset field and threshold field are observed to be as low as 0.36 and 0.08 V/{mu}m, respectively. The field emission current stability investigated at the preset value of {approx}1 {mu}A is observed to be good, in each case. The enhanced field emission properties are attributed to the better electrical conductivity coupled with the nanometric features of the diamond films.

Control of spontaneous emission from a microwave-field-driven four-level atom in an anisotropic photonic crystal

Energy Technology Data Exchange (ETDEWEB)

Zhang, Duo, E-mail: zhangduo10@gmail.com [Wuhan National Laboratory for Optoelectronics and School of Physics, Huazhong University of Science and Technology, Wuhan 430074 (China); School of Electrical and Electronic Engineering, Wuhan Polytechnic University, Wuhan 430023 (China); Li, Jiahua, E-mail: huajia_li@163.com [Wuhan National Laboratory for Optoelectronics and School of Physics, Huazhong University of Science and Technology, Wuhan 430074 (China); Ding, Chunling; Yang, Xiaoxue [Wuhan National Laboratory for Optoelectronics and School of Physics, Huazhong University of Science and Technology, Wuhan 430074 (China)

2012-05-21

The spontaneous emission properties of a microwave-field-driven four-level atom embedded in anisotropic double-band photonic crystals (PCs) are investigated. We discuss the influences of the band-edge positions, Rabi frequency and detuning of the microwave field on the emission spectrum. It is found that several interesting features such as spectral-line enhancement, spectral-line suppression, spectral-line overlap, and multi-peak structures can be observed in the spectra. The proposed scheme can be achieved by use of a microwave-coupled field into hyperfine levels in rubidium atom confined in a photonic crystal. These theoretical investigations may provide more degrees of freedom to manipulate the atomic spontaneous emission. -- Highlights: ► Spontaneous emission properties of an atom embedded in PCs are investigated. ► Spectral-line enhancement, suppression and overlapping are observed. ► The results provide more degrees of freedom to control atomic spontaneous emission.

Control of spontaneous emission from a microwave-field-driven four-level atom in an anisotropic photonic crystal

International Nuclear Information System (INIS)

Zhang, Duo; Li, Jiahua; Ding, Chunling; Yang, Xiaoxue

2012-01-01

The spontaneous emission properties of a microwave-field-driven four-level atom embedded in anisotropic double-band photonic crystals (PCs) are investigated. We discuss the influences of the band-edge positions, Rabi frequency and detuning of the microwave field on the emission spectrum. It is found that several interesting features such as spectral-line enhancement, spectral-line suppression, spectral-line overlap, and multi-peak structures can be observed in the spectra. The proposed scheme can be achieved by use of a microwave-coupled field into hyperfine levels in rubidium atom confined in a photonic crystal. These theoretical investigations may provide more degrees of freedom to manipulate the atomic spontaneous emission. -- Highlights: ► Spontaneous emission properties of an atom embedded in PCs are investigated. ► Spectral-line enhancement, suppression and overlapping are observed. ► The results provide more degrees of freedom to control atomic spontaneous emission.

B-mode contamination by synchrotron emission from 3-yr Wilkinson Microwave Anisotropy Probe data

NARCIS (Netherlands)

Carretti, E.; Bernardi, G.; Cortiglioni, S.

2006-01-01

We study the contamination of the B-mode of the cosmic microwave background polarization (CMBP) by Galactic synchrotron in the lowest emission regions of the sky. The 22.8-GHz polarization map of the 3-yr Wilkinson Microwave Anisotropy Probe (WMAP) data release is used to identify and analyse such

Fluxon induced surface resistance and field emission in niobium films at 1.5 GHz

CERN Document Server

Benvenuti, Cristoforo; Darriulat, Pierre; Peck, M A; Valente, A M; Van't Hof, C A

2001-01-01

The surface resistance of superconducting niobium films induced by the presence of trapped magnetic flux, presumably in the form of a pinned fluxon lattice, is shown to be modified by the presence of a field emitting impurity or defect. The modification takes the form of an additional surface resistance proportional to the density of the fluxon lattice and increasing linearly with the amplitude of the microwave above a threshold significantly lower than the field emission threshold. Such an effect, a precursor of electron emission, is observed for the first time in a study using radiofrequency cavities operating at their fundamental 1.5 GHz frequency. The measured properties of the additional surface resistance severely constrain possible explanations of the observed effect. (23 refs).

Atomic hydrogen determination in medium-pressure microwave discharge hydrogen plasmas via emission actinometry

International Nuclear Information System (INIS)

Geng Zicai; Xu Yong; Yang Xuefeng; Wang Weiguo; Zhu Aimin

2005-01-01

Atomic hydrogen plays an important role in the chemical vapour deposition of functional materials, plasma etching and new approaches to the chemical synthesis of hydrogen-containing compounds. This work reports experimental determinations of atomic hydrogen in microwave discharge hydrogen plasmas formed from the TM 01 microwave mode in an ASTeX-type reactor, via optical emission spectroscopy using Ar as an actinometer. The relative intensities of the H atom Balmer lines and Ar-750.4 nm emissions as functions of input power and gas pressure have been investigated. At an input microwave power density of 13.5 W cm -3 , the approximate hydrogen dissociation fractions calculated from electron-impact excitation and quenching cross sections in the literature, decreased from ∼0.08 to ∼0.03 as the gas pressure was increased from 5 to 25 Torr. The influences of the above cross sections, and the electron and gas temperatures of the plasmas on the determination of the hydrogen dissociation fraction data have been discussed

Optimization of microwave-assisted extraction (MAP) for ginseng components by response surface methodology.

Science.gov (United States)

Kwon, Joong-Ho; Bélanger, Jacqueline M R; Paré, J R Jocelyn

2003-03-26

Response surface methodology (RSM) was applied to predict optimum conditions for microwave-assisted extraction-a MAP technology-of saponin components from ginseng roots. A central composite design was used to monitor the effect of ethanol concentration (30-90%, X(1)) and extraction time (30-270 s, X(2)) on dependent variables, such as total extract yield (Y(1)), crude saponin content (Y(2)), and saponin ratio (Y(3)), under atmospheric pressure conditions when focused microwaves were applied at an emission frequency of 2450 MHz. In MAP under pre-established conditions, correlation coefficients (R (2)) of the models for total extract yield and crude saponin were 0.9841 (p extraction conditions were predicted for each variable as 52.6% ethanol and 224.7 s in extract yield and as 77.3% ethanol and 295.1 s in crude saponins, respectively. Estimated maximum values at predicted optimum conditions were in good agreement with experimental values.

Microwave and X-Ray emission during a isentropic expansion and its application to solar bursts

International Nuclear Information System (INIS)

Piazza, L.R.

1983-01-01

The gyro-synchrotron emission in microwaves and the free-free emission in X-rays of a plasma enclosed in a cylinder coincident with a magnetic force tube were calculated for an isentropic self-similar expansion, with plane and cylindrical symmetries. This expansion model was applied to a region of the low solar corona, and the results were compared to the emission observed in some simple solar events of low intensity. The calculations show satisfactory coincidence with the events in X-rays for energies around 10 29 ergs. The solar events analyzed in microwaves, which are not the same that were studied in X-rays, in general do not fit the theoretical results. The origin of the discrepancy is probably the formulation of the processes of emission applied to the expansion. (Author) [pt

Effects of varying soil moisture contents and vegetation canopies on microwave emissions

Science.gov (United States)

Burke, H.-H. K.; Schmugge, T. J.

1982-01-01

Results of NASA airborne passive microwave scans of bare and vegetated fields for comparison with ground truth tests are discussed and a model for atmospheric scattering of radiation by vegetation is detailed. On-board radiometers obtained data at 21, 2.8, and 1.67 cm during three passes over each of 46 fields, 28 of which were bare and the others having wheat or alfalfa. Ground-based sampling included moisture in five layers down to 15 cm in addition to soil temperature. The relationships among the brightness temperature and soil moisture, as well as the surface roughness and the vegetation canopy were examined. A model was developed for the dielectric coefficient and volume scattering for a vegetation medium. L- to C-band data were found useful for retrieving soil information directly. A surface moisture content of 5-35% yielded an emissivity of 0.9-0.7. The data agreed well with a combined multilayer radiative transfer model with simple roughness correction.

Experimental studies of microwave interaction with a plasma-covered planar conducting surface

International Nuclear Information System (INIS)

Destler, W.W.; Rodgers, J.; DeGrange, J.E.; Segalov, Z.

1990-01-01

The authors present experimental studies of the reflection and absorption of microwave radiation from a plasma-covered planar conducting surface. In the experiments, microwave radiation from both highpower, short pulse (10 GHz, 100 MW, 30 ns) and low power (10 GHz, 10 mW, CW) sources is radiated at a 30 cm diameter conducting plate. A time-varying plasma is created on the surface of the conductor by 19 coaxial plasma guns embedded in the surface of the plate and discharged using a fast-rise capacitor bank. The plasma density distribution on the conducting surface is a function of time and the charging voltage on the capacitor bank. Incident and reflected microwave radiation has been measured for a wide variety of experimental conditions

DETECTION OF ANOMALOUS MICROWAVE EMISSION IN THE PLEIADES REFLECTION NEBULA WITH WILKINSON MICROWAVE ANISOTROPY PROBE AND THE COSMOSOMAS EXPERIMENT

Energy Technology Data Exchange (ETDEWEB)

Genova-Santos, R.; Rebolo, R.; Rubino-Martin, J. A.; Lopez-Caraballo, C. H.; Hildebrandt, S. R. [Instituto de Astrofisica de Canarias, C/Via Lactea s/n, E-38200 La Laguna, Tenerife (Spain)

2011-12-10

We present evidence for anomalous microwave emission (AME) in the Pleiades reflection nebula, using data from the seven-year release of the Wilkinson Microwave Anisotropy Probe and from the COSMOSOMAS (Cosmological Structures on Medium Angular Scales) experiment. The flux integrated in a 1 Degree-Sign radius around R.A. = 56.{sup 0}24, decl. = 23.{sup 0}78 (J2000) is 2.15 {+-} 0.12 Jy at 22.8 GHz, where AME is dominant. COSMOSOMAS data show no significant emission, but allow one to set upper limits of 0.94 and 1.58 Jy (99.7% confidence level), respectively, at 10.9 and 14.7 GHz, which are crucial to pin down the AME spectrum at these frequencies, and to discard any other emission mechanisms which could have an important contribution to the signal detected at 22.8 GHz. We estimate the expected level of free-free emission from an extinction-corrected H{alpha} template, while the thermal dust emission is characterized from infrared DIRBE data and extrapolated to microwave frequencies. When we deduct the contribution from these two components at 22.8 GHz, the residual flux, associated with AME, is 2.12 {+-} 0.12 Jy (17.7{sigma}). The spectral energy distribution from 10 to 60 GHz can be accurately fitted with a model of electric dipole emission from small spinning dust grains distributed in two separated phases of molecular and atomic gas, respectively. The dust emissivity, calculated by correlating the 22.8 GHz data with 100 {mu}m data, is found to be 4.36 {+-} 0.17 {mu}K (MJy sr{sup -1}){sup -1}, a value considerably lower than in typical AME clouds, which present emissivities of {approx}20 {mu}K (MJy sr{sup -1}){sup -1}, although higher than the 0.2 {mu}K (MJy sr{sup -1}){sup -1} of the translucent cloud LDN 1780, where AME has recently been claimed. The physical properties of the Pleiades nebula, in particular its low extinction A{sub V} {approx} 0.4, indicate that this is indeed a much less opaque object than those where AME has usually been studied. This fact

DETECTION OF ANOMALOUS MICROWAVE EMISSION IN THE PLEIADES REFLECTION NEBULA WITH WILKINSON MICROWAVE ANISOTROPY PROBE AND THE COSMOSOMAS EXPERIMENT

International Nuclear Information System (INIS)

Génova-Santos, R.; Rebolo, R.; Rubiño-Martín, J. A.; López-Caraballo, C. H.; Hildebrandt, S. R.

2011-01-01

We present evidence for anomalous microwave emission (AME) in the Pleiades reflection nebula, using data from the seven-year release of the Wilkinson Microwave Anisotropy Probe and from the COSMOSOMAS (Cosmological Structures on Medium Angular Scales) experiment. The flux integrated in a 1° radius around R.A. = 56. 0 24, decl. = 23. 0 78 (J2000) is 2.15 ± 0.12 Jy at 22.8 GHz, where AME is dominant. COSMOSOMAS data show no significant emission, but allow one to set upper limits of 0.94 and 1.58 Jy (99.7% confidence level), respectively, at 10.9 and 14.7 GHz, which are crucial to pin down the AME spectrum at these frequencies, and to discard any other emission mechanisms which could have an important contribution to the signal detected at 22.8 GHz. We estimate the expected level of free-free emission from an extinction-corrected Hα template, while the thermal dust emission is characterized from infrared DIRBE data and extrapolated to microwave frequencies. When we deduct the contribution from these two components at 22.8 GHz, the residual flux, associated with AME, is 2.12 ± 0.12 Jy (17.7σ). The spectral energy distribution from 10 to 60 GHz can be accurately fitted with a model of electric dipole emission from small spinning dust grains distributed in two separated phases of molecular and atomic gas, respectively. The dust emissivity, calculated by correlating the 22.8 GHz data with 100 μm data, is found to be 4.36 ± 0.17 μK (MJy sr –1 ) –1 , a value considerably lower than in typical AME clouds, which present emissivities of ∼20 μK (MJy sr –1 ) –1 , although higher than the 0.2 μK (MJy sr –1 ) –1 of the translucent cloud LDN 1780, where AME has recently been claimed. The physical properties of the Pleiades nebula, in particular its low extinction A V ∼ 0.4, indicate that this is indeed a much less opaque object than those where AME has usually been studied. This fact, together with the broad knowledge of the stellar content of this region

Spoof surface plasmon polaritons based notch filter for ultra-wideband microwave waveguide

DEFF Research Database (Denmark)

Xiao, Binggang; Li, Sheng-Hua; Xiao, Sanshui

2016-01-01

Spoof surface plasmon polaritons based notch filter for ultra-wideband microwave waveguide is proposed. Owing to subwavelength confinement, such a filter has advantage in the structure size without sacrificing the performance. The spoof SPP based notch is introduced to suppress the WLAN and satel...... and satellite communication signals. Due to planar structures proposed here, it is easy to integrate in the microwave integrated systems, which can play an important role in the microwave communication circuit and system.......Spoof surface plasmon polaritons based notch filter for ultra-wideband microwave waveguide is proposed. Owing to subwavelength confinement, such a filter has advantage in the structure size without sacrificing the performance. The spoof SPP based notch is introduced to suppress the WLAN...

Surface roughness of polyvinyl siloxane impression materials following chemical disinfection, autoclave and microwave sterilization.

Science.gov (United States)

Al Kheraif, Abdulaziz Abdullah

2013-05-01

Autoclave sterilization and microwave sterilization has been suggested as the effective methods for the disinfection of elastomeric impressions, but subjecting elastomeric impressions to extreme temperature may have adverse effects on critical properties of the elastomers. To evaluate the effect of chemical disinfection as well as autoclave and microwave sterilization on the surface roughness of elastomeric impression materials. The surface roughness of five commercially available polyvinyl siloxane impression materials (Coltene President, Affinis Perfect impression, Aquasil, 3M ESPE Express and GC Exafast) were evaluated after subjecting them to chemical disinfection, autoclaving and microwave sterilization using a Talysurf Intra 50 instrument. Twenty specimens from each material were fabricated and divided into four equal groups, three experimental and one control (n=25). The differences in the mean surface roughness between the treatment groups were recorded and statistically analyzed. No statistically significant increase in the surface roughness was observed when the specimens were subjected to chemical disinfection and autoclave sterilization, increase in roughness and discoloration was observed in all the materials when specimens were subjected to microwave sterilization. Chemical disinfection did not have a significant effect but, since it is less effective, autoclave sterilization can be considered effective and autoclaving did not show any specimen discoloration as in microwave sterilization. Microwave sterilization may be considered when impressions are used to make diagnostic casts. A significant increase in surface roughness may produce rougher casts, resulting in rougher tissue surfaces for denture and cast restorations. Autoclave sterilization of vinyl polysiloxane elastomeric impressions for 5 minutes at 134°C at 20 psi may be considered an effective method over chemical disinfection and microwave sterilization, because chemical disinfection does

Automated Hybrid Microwave Heating for Lunar Surface Solidification, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — This SBIR project addresses the need for a system that will provide automated lunar surface stabilization via hybrid microwave heating. Surface stabilization is...

Effect of microwave-assisted heating on chalcopyrite leaching of kinetics, interface temperature and surface energy

Directory of Open Access Journals (Sweden)

Tong Wen

Full Text Available The microwave-assisted leaching was a new approach to intensify the copper recovery from chalcopyrite by hydrometallurgy. In this work, the effect of microwave-assisted heating on chalcopyrite leaching of kinetics, interfacial reaction temperature and surface energy were investigated. The activation energy of chalcopyrite leaching was affected indistinctively by the microwave-assisted heating (39.1 kJ/mol compared with the conventional heating (43.9 kJ/mol. However, the boiling point of the leaching system increased through microwave-assisted heating. Because of the improved boiling point and the selective heating of microwave, the interfacial reaction temperature increased significantly, which gave rise to the increase of the leaching recovery of copper. Moreover, the surface energy of the chalcopyrite through microwave-assisted heating was also enhanced, which was beneficial to strengthen the leaching of chalcopyrite. Keywords: Microwave-assisted heating, Chalcopyrite, Leaching kinetics, Interface temperature, Surface energy

Surface modification of titanium hydride with epoxy resin via microwave-assisted ball milling

International Nuclear Information System (INIS)

Ning, Rong; Chen, Ding; Zhang, Qianxia; Bian, Zhibing; Dai, Haixiong; Zhang, Chi

2014-01-01

Highlights: • TiH 2 was modified with epoxy resin by microwave-assisted ball milling. • The epoxy ring was opened under the coupling effect of microwave and ball milling. • Microwave-assisted ball milling improved the compatibility of TiH 2 with epoxy. - Abstract: Surface modification of titanium hydride with epoxy resin was carried out via microwave-assisted ball milling and the products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermo-gravimetry (TG) and Fourier transform infrared spectroscopy (FT-IR). A sedimentation test was performed to investigate the compatibility of the modified nano titanium hydride with the epoxy resin. The results show that the epoxy resin molecules were grafted on the surface of nano titanium hydride particles during the microwave-assisted ball milling process, which led to the improvement of compatibility between the nanoparticles and epoxy resin. According to the FT-IR, the grafting site was likely to be located around the epoxy group due to the fact that the epoxy ring was opened. However, compared with microwave-assisted ball milling, the conventional ball milling could not realize the surface modification, indicating that the coupling effect of mechanical force and microwave played a key role during the process

Removal of contaminated concrete surfaces by microwave heating: Phase 1 results

International Nuclear Information System (INIS)

White, T.L.; Grubb, R.G.; Pugh, L.P.; Foster, D. Jr.; Box, W.D.

1992-01-01

Oak Ridge National Laboratory (ORNL) is developing a microwave heating process to remove radiologically contaminated surface layers from concrete. The microwave energy is directed at the concrete surface and heats the concrete and free water present in the concrete matrix. Continued heating produces steam-pressure-induced mechanical stresses that cause the concrete surface to burst. The concrete particles from this steam explosion are small enough to be removed by a vacuum system, yet less than 1% of the debris is small enough to pose an airborne contamination hazard. The first phase of this program has demonstrated reliable removal of noncontaminated concrete surfaces at frequencies of 2.45 GHz and 10.6 GHz. Continuous concrete removal rates of 1.07 cm 3 /s with 5.2 kW of 2.45.-GHz power and 2.11 cm 3 /s with 3.6 kW of 10.6-GHz power have been demonstrated. Figures-of-merit for microwave removal of concrete have been calculated to be 0.21 cm 3 /s/kW at 2.45 GHz and 0.59 cm 3 /s/kW at 10.6 GHz. The amount of concrete removed in a single pass can be controlled by choosing the frequency and power of the microwave system

Compact Microwave Fourier Spectrum Analyzer

Science.gov (United States)

Savchenkov, Anatoliy; Matsko, Andrey; Strekalov, Dmitry

2009-01-01

A compact photonic microwave Fourier spectrum analyzer [a Fourier-transform microwave spectrometer, (FTMWS)] with no moving parts has been proposed for use in remote sensing of weak, natural microwave emissions from the surfaces and atmospheres of planets to enable remote analysis and determination of chemical composition and abundances of critical molecular constituents in space. The instrument is based on a Bessel beam (light modes with non-zero angular momenta) fiber-optic elements. It features low power consumption, low mass, and high resolution, without a need for any cryogenics, beyond what is achievable by the current state-of-the-art in space instruments. The instrument can also be used in a wide-band scatterometer mode in active radar systems.

The DMRT-ML Model: Numerical Simulations of the Microwave Emission of Snowpacks Based on the Dense Media Radiative Transfer Theory

Science.gov (United States)

Brucker, Ludovic; Picard, Ghislain; Roy, Alexandre; Dupont, Florent; Fily, Michel; Royer, Alain

2014-01-01

Microwave radiometer observations have been used to retrieve snow depth and snow water equivalent on both land and sea ice, snow accumulation on ice sheets, melt events, snow temperature, and snow grain size. Modeling the microwave emission from snow and ice physical properties is crucial to improve the quality of these retrievals. It also is crucial to improve our understanding of the radiative transfer processes within the snow cover, and the snow properties most relevant in microwave remote sensing. Our objective is to present a recent microwave emission model and its validation. The model is named DMRT-ML (DMRT Multi-Layer), and is available at http:lgge.osug.frpicarddmrtml.

The morphology of the Anomalous Microwave Emission in the Planck 2015 data release

Energy Technology Data Exchange (ETDEWEB)

Hausegger, Sebastian von; Liu, Hao, E-mail: s.vonhausegger@nbi.dk, E-mail: liuhao@nbi.dk [The Niels Bohr Institute and Discovery Center, Blegdamsvej 17, 2100 Copenhagen Ø (Denmark)

2015-08-01

We calculate weighted mosaic correlations between the recently published Planck 2015 foreground maps— both anomalous microwave emission (AME) maps, free-free emission, synchrotron radiation and thermal dust emission. The weighting coefficients are constructed taking account of the signal-to-error ratio given by the data product. Positive correlation is found for AME compared with thermal dust emission as well as synchrotron radiation. We find AME and free-free emission tending to be anti-correlated, however, when investigating different scales, their relationship appears to be more complex. We argue that dust particles responsible for AME are pushed out of hot zones in the interstellar medium (ISM)

Microwave surface resistance of bulk YBa2Cu3O6+x material

Science.gov (United States)

Fathy, A.; Kalokitis, D.; Belohoubek, E.; Sundar, H. G. K.; Safari, A.

1988-10-01

Superconducting Y-Ba-Cu-O samples were prepared by conventional solid-state reaction. The microwave surface resistance of 1:2:3 compound superconductor material was measured in a special disk resonator structure at 10 GHz. At liquid-nitrogen temperatures the microwave surface resistance is comparable to that of Au. At lower temperature (~10 K) the surface resistance is an order of magnitude lower than that of Au at the same temperature.

A Prototype Physical Database for Passive Microwave Retrievals of Precipitation over the US Southern Great Plains

Science.gov (United States)

Ringerud, S.; Kummerow, C. D.; Peters-Lidard, C. D.

2015-01-01

An accurate understanding of the instantaneous, dynamic land surface emissivity is necessary for a physically based, multi-channel passive microwave precipitation retrieval scheme over land. In an effort to assess the feasibility of the physical approach for land surfaces, a semi-empirical emissivity model is applied for calculation of the surface component in a test area of the US Southern Great Plains. A physical emissivity model, using land surface model data as input, is used to calculate emissivity at the 10GHz frequency, combining contributions from the underlying soil and vegetation layers, including the dielectric and roughness effects of each medium. An empirical technique is then applied, based upon a robust set of observed channel covariances, extending the emissivity calculations to all channels. For calculation of the hydrometeor contribution, reflectivity profiles from the Tropical Rainfall Measurement Mission Precipitation Radar (TRMM PR) are utilized along with coincident brightness temperatures (Tbs) from the TRMM Microwave Imager (TMI), and cloud-resolving model profiles. Ice profiles are modified to be consistent with the higher frequency microwave Tbs. Resulting modeled top of the atmosphere Tbs show correlations to observations of 0.9, biases of 1K or less, root-mean-square errors on the order of 5K, and improved agreement over the use of climatological emissivity values. The synthesis of these models and data sets leads to the creation of a simple prototype Tb database that includes both dynamic surface and atmospheric information physically consistent with the land surface model, emissivity model, and atmospheric information.

Modeling the Anomalous Microwave Emission with Spinning Nanoparticles: No PAHs Required

Energy Technology Data Exchange (ETDEWEB)

Hensley, Brandon S. [Jet Propulsion Laboratory, California Institute of Technology, 4800 Oak Grove Drive, Pasadena, CA 91109 (United States); Draine, B. T., E-mail: brandon.s.hensley@jpl.nasa.gov [Department of Astrophysical Sciences, Princeton University, Princeton, NJ 08544 (United States)

2017-02-20

In light of recent observational results indicating an apparent lack of correlation between the anomalous microwave emission (AME) and mid-infrared emission from polycyclic aromatic hydrocarbons, we assess whether rotational emission from spinning silicate and/or iron nanoparticles could account for the observed AME without violating observational constraints on interstellar abundances, ultraviolet extinction, and infrared emission. By modifying the SpDust code to compute the rotational emission from these grains, we find that nanosilicate grains could account for the entirety of the observed AME, whereas iron grains could be responsible for only a fraction, even for extreme assumptions on the amount of interstellar iron concentrated in ultrasmall iron nanoparticles. Given the added complexity of contributions from multiple grain populations to the total spinning dust emission, as well as existing uncertainties due to the poorly constrained grain size, charge, and dipole moment distributions, we discuss generic, carrier-independent predictions of spinning dust theory and observational tests that could help identify the AME carrier(s).

Rain detection over land surfaces using passive microwave satellite data

NARCIS (Netherlands)

Bauer, P.; Burose, D.; Schulz, J.

2002-01-01

An algorithm is presented for the detection of surface rainfall using passive microwave measurements by satellite radiometers. The technique consists of a two-stage approach to distinguish precipitation signatures from other effects: (1) Contributions from slowly varying parameters (surface type and

ANOMALOUS MICROWAVE EMISSION IN H ii REGIONS: IS IT REALLY ANOMALOUS? THE CASE OF RCW 49

Energy Technology Data Exchange (ETDEWEB)

Paladini, Roberta [Infrared Processing Analysis Center, California Institute of Technology, 770 South Wilson Ave., Pasadena, CA 91125 (United States); Ingallinera, Adriano; Agliozzo, Claudia; Umana, Grazia; Trigilio, Corrado [Osservatorio Astrofisico di Catania, Via S. Sofia 78, I-95123 Catania Italy (Italy); Tibbs, Christopher T. [Scientific Support Office, Directorate of Science and Robotic Exploration,European Space Research and Technology Centre (ESA/ESTEC), Keplerlaan 1, 2201 AZ, Noordwijk (Netherlands); Noriega-Crespo, Alberto [Space Telescope Science Institute, 3700 San Martin Drive, Baltimore, MD 21218 (United States); Dickinson, Clive [Jodrell Bank Centre for Astrophysics, Alan Turing Building, School of Physics and Astronomy, The University of Manchester, Oxford Road, Manchester M13 9PL (United Kingdom)

2015-11-01

The detection of an excess of emission at microwave frequencies with respect to the predicted free–free emission has been reported for several Galactic H ii regions. Here, we investigate the case of RCW 49, for which the Cosmic Background Imager tentatively (∼3σ) detected Anomalous Microwave Emission (AME) at 31 GHz on angular scales of 7′. Using the Australia Telescope Compact Array, we carried out a multi-frequency (5, 19, and 34 GHz) continuum study of the region, complemented by observations of the H109α radio recombination line. The analysis shows that: (1) the spatial correlation between the microwave and IR emission persists on angular scales from 3.′4 to 0.″4, although the degree of the correlation slightly decreases at higher frequencies and on smaller angular scales; (2) the spectral indices between 1.4 and 5 GHz are globally in agreement with optically thin free–free emission, however, ∼30% of these are positive and much greater than −0.1, consistent with a stellar wind scenario; and (3) no major evidence for inverted free–free radiation is found, indicating that this is likely not the cause of the Anomalous Emission in RCW 49. Although our results cannot rule out the spinning dust hypothesis to explain the tentative detection of AME in RCW 49, they emphasize the complexity of astronomical sources that are very well known and studied, such as H ii regions, and suggest that, at least in these objects, the reported excess of emission might be ascribed to alternative mechanisms such as stellar winds and shocks.

Characterization of microwave plasma in a multicusp using 2D emission based tomography: Bessel modes and wave absorption

Science.gov (United States)

Rathore, Kavita; Bhattacharjee, Sudeep; Munshi, Prabhat

2017-06-01

A tomographic method based on the Fourier transform is used for characterizing a microwave plasma in a multicusp (MC), in order to obtain 2D distribution of plasma emissions, plasma (electron) density (Ne) and temperature (Te). The microwave plasma in the MC is characterized as a function of microwave power, gas pressure, and axial distance. The experimentally obtained 2D emission profiles show that the plasma emissions are generated in a circular ring shape. There are usually two bright rings, one at the plasma core and another near the boundary. The experimental results are validated using a numerical code that solves Maxwell's equations inside a waveguide filled with a plasma in a magnetic field, with collisions included. It is inferred that the dark and bright circular ring patterns are a result of superposition of Bessel modes (TE11 and TE21) of the wave electric field inside the plasma filled MC, which are in reasonable agreement with the plasma emission profiles. The tomographically obtained Ne and Te profiles indicate higher densities in the plasma core (˜1010 cm-3) and enhanced electron temperature in the ECR region (˜13 eV), which are in agreement with earlier results using a Langmuir probe and optical emission spectroscopy (OES) diagnostics.

Investigation of the delay time distribution of high power microwave surface flashover

Science.gov (United States)

Foster, J.; Krompholz, H.; Neuber, A.

2011-01-01

Characterizing and modeling the statistics associated with the initiation of gas breakdown has proven to be difficult due to a variety of rather unexplored phenomena involved. Experimental conditions for high power microwave window breakdown for pressures on the order of 100 to several 100 torr are complex: there are little to no naturally occurring free electrons in the breakdown region. The initial electron generation rate, from an external source, for example, is time dependent and so is the charge carrier amplification in the increasing radio frequency (RF) field amplitude with a rise time of 50 ns, which can be on the same order as the breakdown delay time. The probability of reaching a critical electron density within a given time period is composed of the statistical waiting time for the appearance of initiating electrons in the high-field region and the build-up of an avalanche with an inherent statistical distribution of the electron number. High power microwave breakdown and its delay time is of critical importance, since it limits the transmission through necessary windows, especially for high power, high altitude, low pressure applications. The delay time distribution of pulsed high power microwave surface flashover has been examined for nitrogen and argon as test gases for pressures ranging from 60 to 400 torr, with and without external UV illumination. A model has been developed for predicting the discharge delay time for these conditions. The results provide indications that field induced electron generation, other than standard field emission, plays a dominant role, which might be valid for other gas discharge types as well.

Low-noise heterodyne receiver for electron cyclotron emission imaging and microwave imaging reflectometry

Energy Technology Data Exchange (ETDEWEB)

Tobias, B., E-mail: bjtobias@pppl.gov [Princeton Plasma Physics Laboratory, Princeton, New Jersey 08543 (United States); Domier, C. W.; Luhmann, N. C.; Luo, C.; Mamidanna, M.; Phan, T.; Pham, A.-V.; Wang, Y. [University of California at Davis, Davis, California 95616 (United States)

2016-11-15

The critical component enabling electron cyclotron emission imaging (ECEI) and microwave imaging reflectometry (MIR) to resolve 2D and 3D electron temperature and density perturbations is the heterodyne imaging array that collects and downconverts radiated emission and/or reflected signals (50–150 GHz) to an intermediate frequency (IF) band (e.g. 0.1–18 GHz) that can be transmitted by a shielded coaxial cable for further filtering and detection. New circuitry has been developed for this task, integrating gallium arsenide (GaAs) monolithic microwave integrated circuits (MMICs) mounted on a liquid crystal polymer (LCP) substrate. The improved topology significantly increases electromagnetic shielding from out-of-band interference, leads to 10× improvement in the signal-to-noise ratio, and dramatic cost savings through integration. The current design, optimized for reflectometry and edge radiometry on mid-sized tokamaks, has demonstrated >20 dB conversion gain in upper V-band (60-75 GHz). Implementation of the circuit in a multi-channel electron cyclotron emission imaging (ECEI) array will improve the diagnosis of edge-localized modes and fluctuations of the high-confinement, or H-mode, pedestal.

THE LOCAL DUST FOREGROUNDS IN THE MICROWAVE SKY. I. THERMAL EMISSION SPECTRA

International Nuclear Information System (INIS)

Dikarev, Valeri; Preuss, Oliver; Solanki, Sami; Krueger, Harald; Krivov, Alexander

2009-01-01

Analyses of the cosmic microwave background (CMB) radiation maps made by the Wilkinson Microwave Anisotropy Probe (WMAP) have revealed anomalies not predicted by the standard inflationary cosmology. In particular, the power of the quadrupole moment of the CMB fluctuations is remarkably low, and the quadrupole and octopole moments are aligned mutually and with the geometry of the solar system. It has been suggested in the literature that microwave sky pollution by an unidentified dust cloud in the vicinity of the solar system may be the cause for these anomalies. In this paper, we simulate the thermal emission by clouds of spherical homogeneous particles of several materials. Spectral constraints from the WMAP multi-wavelength data and earlier infrared observations on the hypothetical dust cloud are used to determine the dust cloud's physical characteristics. In order for its emissivity to demonstrate a flat, CMB-like wavelength dependence over the WMAP wavelengths (3 through 14 mm), and to be invisible in the infrared light, its particles must be macroscopic. Silicate spheres of several millimeters in size and carbonaceous particles an order of magnitude smaller will suffice. According to our estimates of the abundance of such particles in the zodiacal cloud and trans-Neptunian belt, yielding the optical depths of the order of 10 -7 for each cloud, the solar system dust can well contribute 10 μK (within an order of magnitude) in the microwaves. This is not only intriguingly close to the magnitude of the anomalies (about 30 μK), but also alarmingly above the presently believed magnitude of systematic biases of the WMAP results (below 5 μK) and, to an even greater degree, of the future missions with higher sensitivities, e.g., Planck.

Characterization of near-infrared nonmetal atomic emission from an atmospheric helium microwave-induced plasma using a Fourier transform spectrophotometer

International Nuclear Information System (INIS)

Hubert, J.; Van Tra, H.; Chi Tran, K.; Baudais, F.L.

1986-01-01

A new approach for using Fourier transform spectroscopy (FTS) for the detection of atomic emission from an atmospheric helium plasma has been developed and the results obtained are described. Among the different types of plasma source available, the atmospheric pressure microwave helium plasma appears to be an efficient excitation source for the determination of nonmetal species. The more complete microwave plasma emission spectra of Cl, Br, I, S, O, P, C, N, and He in the near-infrared region were obtained and their corrected relative emission intensities are reported. This makes qualitative identification simple, and aids in the quantitative analysis of atomic species. The accuracy of the emission wavelengths obtained with the Fourier transform spectrophotometer was excellent and the resolution provided by the FTS allowed certain adjacent emission lines to be adequate for analytical applications

Multifrequency passive microwave remote sensing of soil moisture and roughness

International Nuclear Information System (INIS)

Paloscia, S.; Pampaloni, P.; Chiarantini, L.; Coppo, P.; Gagliani, S.; Luzi, G.

1993-01-01

The accuracy achievable in the surface soil moisture measurement of rough bare and vegetated soils, typical of the Italian landscape, has been investigated by using microwave experimental data collected by means of a multi-band sensor package (L, X, Ka and infrared bands). The thickness of soil that mainly affects the emission at the three microwave frequencies has been assessed. The sensitivity of L band emission to the moisture content of a soil layer about 5 cm thick has been confirmed, as well as the attenuation effect due to the surface roughness and presence of vegetation. A correction criterion based on the sensitivity to roughness and crop parameters of the highest frequencies (X and Ka bands) is proposed in order to increase the precision in soil moisture measurements

Assimilation of Feng-Yun-3B satellite microwave humidity sounder data over land

Science.gov (United States)

Chen, Keyi; Bormann, Niels; English, Stephen; Zhu, Jiang

2018-03-01

The ECMWF has been assimilating Feng-Yun-3B (FY-3B) satellite microwave humidity sounder (MWHS) data over ocean in an operational forecasting system since 24 September 2014. It is more difficult, however, to assimilate microwave observations over land and sea ice than over the open ocean due to higher uncertainties in land surface temperature, surface emissivity and less effective cloud screening. We compare approaches in which the emissivity is retrieved dynamically from MWHS channel 1 [150 GHz (vertical polarization)] with the use of an evolving emissivity atlas from 89 GHz observations from the MWHS onboard NOAA and EUMETSAT satellites. The assimilation of the additional data over land improves the fit of short-range forecasts to other observations, notably ATMS (Advanced Technology Microwave Sounder) humidity channels, and the forecast impacts are mainly neutral to slightly positive over the first five days. The forecast impacts are better in boreal summer and the Southern Hemisphere. These results suggest that the techniques tested allow for effective assimilation of MWHS/FY-3B data over land.

Spoof surface plasmon polaritons based notch filter for ultra-wideband microwave waveguide

DEFF Research Database (Denmark)

Xiao, Binggang; Li, Sheng-Hua; Xiao, Sanshui

2016-01-01

Spoof surface plasmon polaritons based notch filter for ultra-wideband microwave waveguide is proposed. Owing to subwavelength confinement, such a filter has advantage in the structure size without sacrificing the performance. The spoof SPP based notch is introduced to suppress the WLAN and satel......Spoof surface plasmon polaritons based notch filter for ultra-wideband microwave waveguide is proposed. Owing to subwavelength confinement, such a filter has advantage in the structure size without sacrificing the performance. The spoof SPP based notch is introduced to suppress the WLAN...

Planck intermediate results: XVII. Emission of dust in the diffuse interstellar medium from the far-infrared to microwave frequencies

DEFF Research Database (Denmark)

Bartlett, J.G.; Cardoso, J.-F.; Delabrouille, J.

2014-01-01

H-atom. The dust temperature is observed to be anti-correlated with the dust emissivity and opacity. We interpret this result as evidence of dust evolution within the diffuse ISM. The mean dust opacity is measured to be (7.1 ± 0.6) × 10-27 cm2 H-1 × (v/353 GHz) 1.53 ± 0.03for 100 ≤ v ≤ 353 GHz......The dust-Hi correlation is used to characterize the emission properties of dust in the diffuse interstellar medium (ISM) from far infrared wavelengths to microwave frequencies. The field of this investigation encompasses the part of the southern sky best suited to study the cosmic infrared...... and microwave backgrounds. We cross-correlate sky maps from Planck, the Wilkinson Microwave Anisotropy Probe (WMAP), and the diffuse infrared background experiment (DIRBE), at 17 frequencies from 23 to 3000 GHz, with the Parkes survey of the 21 cm line emission of neutral atomic hydrogen, over a contiguous area...

Microwave and plasma-assisted modification of composite fiber surface topography

Science.gov (United States)

Paulauskas, Felix L [Knoxville, TN; White, Terry L [Knoxville, TN; Bigelow, Timothy S [Knoxville, TN

2003-02-04

The present invention introduces a novel method for producing an undulated surface on composite fibers using plasma technology and microwave radiation. The undulated surface improves the mechanical interlocking of the fibers to composite resins and enhances the mechanical strength and interfacial sheer strength of the composites in which they are introduced.

Electrical Characteristics of Carbon Nanotubes by Plasma and Microwave Surface Treatments

Energy Technology Data Exchange (ETDEWEB)

Cho, Sangjin; Lee, Soonbo; Boo, Jinhyo [Sungkyunkwan Univ., Suwon (Korea, Republic of); Shrestha, Shankar Prasad [Tribhuvan Univ., Kathmandu (Nepal)

2014-03-15

The plasma and microwave surface treatments of carbon nanotubes that loaded on plastic substrates were carried out with expecting a change of carbon nanotube dispersion by increasing treatment time. The microwave treatment process was undergone by commercial microwave oven (800 W). The electrical property was measured by hall measurement and resistance was increased by increasing O{sub 2} flow rate of plasma, suggesting an improvement of carbon nanotube dispersion and a possibility of controlling the resistances of carbon nanotubes by plasma surface treatment. The resistance was increased in both polyethylene terephthalate and polyimide substrates by increasing O{sub 2} flow rate. Resistance changes only slightly with different O{sub 2} flow treatment in measure rho for all polyimide samples. Sheet resistance is lowest in polyimide substrate not due to high carbon nanotube loading but due to tendency to remain in elongated structure. O{sub 2} or N{sub 2} plasma treatments on both polyethylene terephthalate and polyimide substrates lead to increase in sheet resistance.

Electrical Characteristics of Carbon Nanotubes by Plasma and Microwave Surface Treatments

International Nuclear Information System (INIS)

Cho, Sangjin; Lee, Soonbo; Boo, Jinhyo; Shrestha, Shankar Prasad

2014-01-01

The plasma and microwave surface treatments of carbon nanotubes that loaded on plastic substrates were carried out with expecting a change of carbon nanotube dispersion by increasing treatment time. The microwave treatment process was undergone by commercial microwave oven (800 W). The electrical property was measured by hall measurement and resistance was increased by increasing O 2 flow rate of plasma, suggesting an improvement of carbon nanotube dispersion and a possibility of controlling the resistances of carbon nanotubes by plasma surface treatment. The resistance was increased in both polyethylene terephthalate and polyimide substrates by increasing O 2 flow rate. Resistance changes only slightly with different O 2 flow treatment in measure rho for all polyimide samples. Sheet resistance is lowest in polyimide substrate not due to high carbon nanotube loading but due to tendency to remain in elongated structure. O 2 or N 2 plasma treatments on both polyethylene terephthalate and polyimide substrates lead to increase in sheet resistance

L-Band Microwave Emission of Soil Freeze-Thaw Process in the Third Pole Environment

NARCIS (Netherlands)

Zheng, Donghai; van der Velde, R.; Su, Z.; Zeng, Y.

2017-01-01

Soil freeze-thaw transition monitoring is essential for quantifying climate change and hydrologic dynamics over cold regions, for instance, the Third Pole. We investigate the L-band (1.4 GHz) microwave emission characteristics of soil freeze-thaw cycle via analysis of tower-based brightness

Ultralow field emission from thinned, open-ended, and defected carbon nanotubes by using microwave hydrogen plasma processing

Energy Technology Data Exchange (ETDEWEB)

Deng, Jian-Hua, E-mail: jhdeng1983@163.com [College of Physics and Materials Science, Tianjin Normal University, Tianjin 300387 (China); Cheng, Lin; Wang, Fan-Jie; Yu, Bin; Li, Guo-Zheng; Li, De-Jun [College of Physics and Materials Science, Tianjin Normal University, Tianjin 300387 (China); Cheng, Guo-An [Key Laboratory of Beam Technology and Material Modification of Ministry of Education, Beijing Normal University, Beijing 100875 (China)

2015-01-01

Graphical abstract: Thinned, open-ended, and defected carbon nanotubes were prepared by using hydrogen plasma processing. The processed carbon nanotubes have far better field emission performance than that of the pristine ones. - Highlights: • CVD prepared CNT arrays were processed by microwave hydrogen plasma. • Thinned, open-ended, and defected CNTs were obtained. • Processed CNTs have far better field emission performance than the pristine ones. • Processed CNTs have applicable emission stability after being perfectly aged. - Abstract: Ultralow field emission is achieved from carbon nanotubes (CNTs) by using microwave hydrogen plasma processing. After the processing, typical capped CNT tips are removed, with thinned, open-ended, and defected CNTs left. Structural analyses indicate that the processed CNTs have more SP{sup 3}-hybridized defects as compared to the pristine ones. The morphology of CNTs can be readily controlled by adjusting microwave powers, which change the shape of CNTs by means of hydrogen plasma etching. Processed CNTs with optimal morphology are found to have an ultralow turn-on field of 0.566 V/μm and threshold field of 0.896 V/μm, much better than 0.948 and 1.559 V/μm of the as-grown CNTs, respectively. This improved FE performance is ascribed to the structural changes of CNTs after the processing. The thinned and open-ended shape of CNTs can facilitate electron tunneling through barriers and additionally, the increased defects at tube walls can serve as new active emission sites. Furthermore, our plasma processed CNTs exhibit excellent field emission stability at a large emission current density of 10.36 mA/cm{sup 2} after being perfectly aged, showing promising prospects in applications as high-performance vacuum electron sources.

Effect of Repeated Microwave Disinfection on Surface Hardness and Dimensional Accuracy of Two Dental Stone Materials

Directory of Open Access Journals (Sweden)

Mahmood Robati Anaraki

2015-01-01

Full Text Available There is controversial evidence in relation to the effect of microwave on mechanical properties of stone casts. The present study was designed to evaluate the effect of repeated microwave disinfection on surface hardness and dimensional accuracy of dental stone. In this in vitro study, 48 cylindrical stone samples were prepared using two products of type IV stone to assess surface hardness and 48 impressions were taken from a model and poured by these stones to assess the dimensional accuracy. The evaluation of the samples was carried out consequently by a micro-hardness tester and a digital caliper after the stone samples were exposed to 7 consecutive rounds of 900 watts (W microwave irradiation for five minutes each time after cooling. Data were analyzed by t-test and ANOVA. According to the obtained results, multiple disinfections of the stone casts by microwave do not negatively affect their surface hardness and dimensional accuracy.   Key words: Dental stone; Dimensional accuracy; Hardness; Microwave

[Impact of microwave dealing with the cutting surface on the hepatocellular carcinoma recurrence after hepatectomy].

Science.gov (United States)

Wu, Zhengshan; Wang, Xing; Wang, Dong; Fan, Ye; Li, Donghua; Kong, Lianbao; Wang, Xuehao; Wang, Ke

2015-12-01

To explore the impact of microwave dealing with cutting surface on perioperative liver function recovery and recurrence and metastasis after hepatectomy for HCC. Clinical data of 133 patients with HCC from March 2009 to November 2010 were retrospectively analyzed. They were divided into the conventional surgery group (66 cases) and microwave treatment group (67 cases). A domestic ECO-100 microwave knife was inserted into the liver cutting surface 0.5 cm from the cutting edge, and repeated multi-point burning with an average time of 25 minutes in the microwave treatment group. Then the perioperative liver function recovery and recurrence and metastasis in the two groups were compared. The operation time of conventional surgery group was (158.0 ± 31.0) minutes, and that of microwave treatment group was significantly longer (181.0 ± 28.0) minutes (P=0.027). There were no significant differences in the liver function recovery between the two groups (P>0.05). There were 6 cases of recurrence and metastasis after 6 months and 9 cases after 12 months in the microwave treatment group, while there were 15 cases of recurrence and metastasis after 6 months and 20 cases after 12 months in the conventional surgery group, showing a significant difference (P=0.034 and 0.022, respectively). Microwave dealing with the cutting surface has no significant effect on perioperative liver function recovery in hepatectomy. However, microwave treatment can reduce the in situ recurrence in HCC patients within the first year after surgery, indicating a good clinical application value.

The MIDAS experiment: A prototype for the microwave emission of Ultra-High Energy Cosmic Rays

International Nuclear Information System (INIS)

Monasor, M.; Alekotte, I.; Alvarez-Muniz, J.; Berlin, A.; Bertou, X.; Bodgan, M.; Bohacova, M.; Bonifazi, C.; Carvalho, W.; Mello Neto, J.R.T. de; Genat, J.F.; Facal San Luis, P.; Mills, E.; Rouille d'Orfeuil, B.; Wayne, S.; Reyes, L.C.; Santos, E.M.; Privitera, P.; Williams, C.; Zas, E.

2011-01-01

Recent measurements suggest that extensive air showers initiated by ultra-high energy cosmic rays (UHECR) emit signals in the microwave band of the electromagnetic spectrum caused by the collisions of the free-electrons with the atmospheric neutral molecules in the plasma produced by the passage of the shower. Such emission is isotropic and could allow the detection of air showers with 100% duty cycle and a calorimetric-like energy measurement, a significant improvement over current detection techniques. We have built MIDAS (MIcrowave Detection of Air Showers), a prototype of microwave detector, which consists of a 4.5 m diameter antenna with a cluster of 53 feed-horns in the 4 GHz range. The details of the prototype and first results will be presented.

Surface and Bulk Characteristics of Cesium Iodide (CsI) coated Carbon (C) Fibers for High Power Microwave (HPM) Field Emission Cathodes

Science.gov (United States)

Vlahos, Vasilios; Morgan, Dane; Booske, John H.; Shiffler, Don

2008-11-01

CsI coated C fibers [1] are promising field emission cathodes for HPM applications. Ab initio computational modeling has shown that atomically-thin CsI coatings reduce the work function of C substrates by a surface dipole mechanism [2]. Characterization measurements of the composition and morphology of the CsI-coated C fibers are underway for determining the properties and characteristics of the following important regions of the fiber: (i) the surface on the tip of the fiber where the majority of electron emission is believed to occur, (ii) the surface covering the body of the fiber and its role on the emission properties of the system, and (iii) the interior volume of the fiber and its effects on the CsI surface re-supply process and rate. The results will be interpreted in terms of surface electronic properties and theoretical electron emission models. [1]D. Shiffler, et al., Phys. Plasmas 11 (2004) 1680. [2]V.Vlahos et al., Appl. Phys. Lett. 91 (2007) 144102.

NOAA JPSS Microwave Integrated Retrieval System (MIRS) Advanced Technology Microwave Sounder (ATMS) Precipitation and Surface Products from NDE

Data.gov (United States)

National Oceanic and Atmospheric Administration, Department of Commerce — This dataset contains two-dimensional precipitation and surface products from the JPSS Microwave Integrated Retrieval System (MIRS) using sensor data from the...

Pushbroom microwave radiometer results from HAPEX-MOBILHY

International Nuclear Information System (INIS)

Nichols, W.E.; Cuenca, R.H.; Schmugge, T.J.; Wang, J.R.

1993-01-01

The NASA C-130 remote sensing aircraft was in Toulouse, France from 25 May through 4 July 1986, for participation in the HAPEX-MOBILHY program. Spectral and radiometric data were collected by C-130 borne sensors in the visible, infrared, and microwave wavelengths. These data provided information on the spatial and temporal variations of surface parameters such as vegetation indices, surface temperature, and surface soil moisture. The Pushbroom Microwave Radiometer (PBMR) was used to collect passive microwave brightness temperature data. This four-beam sensor operates at the 21-cm wavelength, providing cross-track coverage approximately 1.2 times the aircraft altitude. Observed brightness temperatures for the period were high, ranging from above 240 K about 290 K. Brightness temperature images appeared to correspond well to spatial and temporal soil moisture variation. Previous research has demonstrated that an approximately linear relationship exists between the surface emissivity and surface soil moisture. For these data, however, regression analysis did not indicate a strong linear relationship (r 2 = 0.32 and r 2 = 0.42 respectively) because of the limited range of soil moisture conditions encountered and the small number of ground measurements. When results from wetter soil conditions encountered in another experiment were included, the regression improved dramatically. Based on similar research with the PBMR and an understanding of the ground data collection program, this result was examined to produce recommendations for improvements to future passive microwave research and data collection programs. Examples of surface soil moisture maps generated with PBMR data are presented which appear to be representative of the actual soil moisture conditions

Observations of the Polarisation of the Anomalous Microwave Emission: A Review

Directory of Open Access Journals (Sweden)

J. A. Rubiño-Martín

2012-01-01

Full Text Available The observational status of the polarisation of the anomalous microwave emission (AME is reviewed, both for individual compact Galactic regions as well as for the large-scale Galactic emission. There are six Galactic regions with existing polarisation constraints in the relevant range of 10–40 GHz: four dust clouds (Perseus, ρ Ophiuchi, LDN1622, and Pleiades and two HII regions (LPH96 and the Helix nebula. These constraints are discussed in detail and are complemented by deriving upper limits on the polarisation of the AME for those objects without published WMAP constraints. For the case of large-scale emission, two recent works, based on WMAP data, are reviewed. Currently, the best constraints on the fractional polarisation of the AME, at frequencies near the peak of the emission (i.e., 20–30 GHz, are at the level of ~1% (95.4% confidence level. Finally, we compare these constraints with the predictions of some theoretical AME models and discuss the possible impact of polarised AME on future primordial B-mode experiments.

A Prognostic Methodology for Precipitation Phase Detection using GPM Microwave Observations —With Focus on Snow Cover

Science.gov (United States)

Takbiri, Z.; Ebtehaj, A.; Foufoula-Georgiou, E.; Kirstetter, P.

2017-12-01

Improving satellite retrieval of precipitation requires increased understanding of its passive microwave signature over different land surfaces. Passive microwave signals over snow-covered surfaces are notoriously difficult to interpret because they record both emission from the land below and absorption/scattering from the liquid/ice crystals. Using data from the Global Precipitation Measurement (GPM) core satellite, we demonstrate that the microwave brightness temperatures of rain and snowfall shifts from a scattering to an emission regime from summer to winter, due to expansion of the less emissive snow cover underneath. We present evidence that the combination of low- (10-19 GHz) and high-frequency (89-166 GHz) channels provides the maximum amount of information for snowfall detection. The study also examines a prognostic nearest neighbor matching method for the detection of precipitation and its phase from passive microwave observations using GPM data. The nearest neighbor uses the weighted Euclidean distance metric to search through an a priori database that is populated with coincident GPM radiometer and radar data as well as ancillary snow cover fraction. The results demonstrate prognostic capabilities of the proposed method in detection of terrestrial snowfall. At the global scale, the average probability of hit and false alarm reaches to 0.80 and remains below 0.10, respectively. Surprisingly, the results show that the snow cover may help to better detect precipitation as the detection rate of terrestrial precipitation is increased from 0.75 (no snow cover) to 0.84 (snow-covered surfaces). For solid precipitation, this increased rate of detection is larger than its liquid counterpart by almost 8%. The main reasons are found to be related to the multi-frequency capabilities of the nearest neighbor matching that can properly isolate the atmospheric signal from the background emission and the fact that the precipitation can exhibit an emission-like (warmer

Recent Improvements in Retrieving Near-Surface Air Temperature and Humidity Using Microwave Remote Sensing

Science.gov (United States)

Roberts, J. Brent

2010-01-01

Detailed studies of the energy and water cycles require accurate estimation of the turbulent fluxes of moisture and heat across the atmosphere-ocean interface at regional to basin scale. Providing estimates of these latent and sensible heat fluxes over the global ocean necessitates the use of satellite or reanalysis-based estimates of near surface variables. Recent studies have shown that errors in the surface (10 meter)estimates of humidity and temperature are currently the largest sources of uncertainty in the production of turbulent fluxes from satellite observations. Therefore, emphasis has been placed on reducing the systematic errors in the retrieval of these parameters from microwave radiometers. This study discusses recent improvements in the retrieval of air temperature and humidity through improvements in the choice of algorithms (linear vs. nonlinear) and the choice of microwave sensors. Particular focus is placed on improvements using a neural network approach with a single sensor (Special Sensor Microwave/Imager) and the use of combined sensors from the NASA AQUA satellite platform. The latter algorithm utilizes the unique sampling available on AQUA from the Advanced Microwave Scanning Radiometer (AMSR-E) and the Advanced Microwave Sounding Unit (AMSU-A). Current estimates of uncertainty in the near-surface humidity and temperature from single and multi-sensor approaches are discussed and used to estimate errors in the turbulent fluxes.

Kinetic computer modeling of microwave surface-wave plasma production

International Nuclear Information System (INIS)

Ganachev, Ivan P.

2004-01-01

Kinetic computer plasma modeling occupies an intermediate position between the time consuming rigorous particle dynamic simulation and the fast but rather rough cold- or warm-plasma fluid models. The present paper reviews the kinetic modeling of microwave surface-wave discharges with accent on recent kinetic self-consistent models, where the external input parameters are reduced to the necessary minimum (frequency and intensity of the applied microwave field and pressure and geometry of the discharge vessel). The presentation is limited to low pressures, so that Boltzmann equation is solved in non-local approximation and collisional electron heating is neglected. The numerical results reproduce correctly the bi-Maxwellian electron energy distribution functions observed experimentally. (author)

Temporal observations of surface soil moisture using a passive microwave sensor

International Nuclear Information System (INIS)

Jackson, T.J.; O'Neill, P.

1987-01-01

A series of 10 aircraft flights was conducted over agricultural fields to evaluate relationships between observed surface soil moisture and soil moisture predicted using passive microwave sensor observations. An a priori approach was used to predict values of surface soil moisture for three types of fields: tilled corn, no-till corn with soybean stubble, and idle fields with corn stubble. Acceptable predictions were obtained for the tilled corn fields, while poor results were obtained for the others. The source of error is suspected to be the density and orientation of the surface stubble layer; however, further research is needed to verify this explanation. Temporal comparisons between observed, microwave predicted, and soil water-simulated moisture values showed similar patterns for tilled well-drained fields. Divergences between the observed and simulated measurements were apparent on poorly drained fields. This result may be of value in locating and mapping hydrologic contributing areas

Microwave off-gas treatment apparatus and process

Science.gov (United States)

Schulz, Rebecca L.; Clark, David E.; Wicks, George G.

2003-01-01

The invention discloses a microwave off-gas system in which microwave energy is used to treat gaseous waste. A treatment chamber is used to remediate off-gases from an emission source by passing the off-gases through a susceptor matrix, the matrix being exposed to microwave radiation. The microwave radiation and elevated temperatures within the combustion chamber provide for significant reductions in the qualitative and quantitative emissions of the gas waste stream.

Controlled fabrication of the strong emission YVO4:Eu3+ nanoparticles and nanowires by microwave assisted chemical synthesis

International Nuclear Information System (INIS)

Huong, Tran Thu; Vinh, Le Thi; Phuong, Ha Thi; Khuyen, Hoang Thi; Anh, Tran Kim; Tu, Vu Duc; Minh, Le Quoc

2016-01-01

In this report, we are presenting the controlled fabrication results of the strong emission YVO 4 : Eu 3+ nanoparticles and nanowires by microwave which is assisted chemical synthesis. The effects of incorporated synthesis conditions such as microwave irradiated powers, pH values and concentration of chemical composition on properties of nanomaterials are also investigated to obtain the controllable size and homogenous morphology. Morphological and optical properties of YVO 4 : Eu 3+ prepared products which have been characterized by X-ray diffraction (XRD), field emission micrcroscopy (FESEM) and photoluminescence spectroscopy. As based from result of synthesized samples, we found that the changing of pH values, microwave irradiated powers and chemical composition rise to change reform the size and shape of materials from nanoparticles (diameter about 20 nm) to wires shape (with about 500÷800 nm length and 10÷20 nm width). The photoluminescence (PL) spectroscopy measurements of YVO 4 : Eu 3+ nanostructure materials under UV excitation showed that: the strong luminescence in red region with narrow lines corresponding to the intra-4f transitions of 5 D 0 – 7 F j (j=1, 2, 3, and 4) of Eu 3+ ions with the highest luminescence intensity of 5 D 0 → 7 F 2 transition. - Highlights: • The strong emission YVO 4 :Eu 3+ nanostructure materials were successfully synthesized by microwave assisted chemical synthesis. • The size, morphology and luminescence of the YVO 4 :Eu 3+ nanostructure materials can be controlled by the solution pH, microwave irradiated powers and chemical composition. • These YVO 4 :Eu 3+ nanostructure materials above can potentially applied in various fields of application, especially in luminescent labeling and visualization in biomedical application.

Use of AMSR-E microwave satellite data for land surface characteristics and snow cover variation

Directory of Open Access Journals (Sweden)

Mukesh Singh Boori

2016-12-01

Full Text Available This data article contains data related to the research article entitled “Global land cover classification based on microwave polarization and gradient ratio (MPGR” [1] and “Microwave polarization and gradient ratio (MPGR for global land surface phenology” [2]. This data article presents land surface characteristics and snow cover variation information from sensors like EOS Advanced Microwave Scanning Radiometer (AMSR-E. This data article use the HDF Explorer, Matlab, and ArcGIS software to process the pixel latitude, longitude, snow water equivalent (SWE, digital elevation model (DEM and Brightness Temperature (BT information from AMSR-E satellite data to provide land surface characteristics and snow cover variation data in all-weather condition at any time. This data information is useful to discriminate different land surface cover types and snow cover variation, which is turn, will help to improve monitoring of weather, climate and natural disasters.

Planck intermediate results. XV. A study of anomalous microwave emission in Galactic clouds

DEFF Research Database (Denmark)

Ade, P. A. R.; Aghanim, N.; Alves, Marie-Helene

2014-01-01

radiation field, G0. Modelling of this trend suggests that both radiative and collisional excitation are important for the spinning dust emission. The most significant AME regions tend to have relatively less ionized gas (free-free emission), although this could be a selection effect. The infrared excess......Anomalous microwave emission (AME) is believed to be due to electric dipole radiation from small spinning dust grains. The aim of this paper is a statistical study of the basic properties of AME regions and the environment in which they emit. We used WMAP and Planck maps, combined with ancillary...... for the AME regions. The AME regions tend to be associated with cooler dust in the range 14−20 K and an average emissivity index, βd, of +1.8, while the non-AME regions are typically warmer, at 20−27 K. In agreement with previous studies, the AME emissivity appears to decrease with increasing column density...

Electron emission at the rail surface

International Nuclear Information System (INIS)

Thornhill, L.; Battech, J.

1991-01-01

In this paper the authors examine the processes by which current is transferred from the cathode rail to the plasma armature in an arc-driven railgun. Three electron emission mechanisms are considered, namely thermionic emission, field-enhanced thermionic emission (or Schottky emission), and photoemission. The author's calculations show that the dominant electron emission mechanism depends, to a great extent, on the work function of the rail surface, the rail surface temperature, the electric field at the rail surface, and the effective radiation temperature of the plasma. For conditions that are considered to be typical of a railgun armature, Schottky emission is the dominant electron emission mechanism, providing current densities on the order of 10 9 A/m 2

Preparation of High Surface Area Activated Carbon from Spent Phenolic Resin by Microwave Heating and KOH Activation

Science.gov (United States)

Cheng, Song; Zhang, Libo; Zhang, Shengzhou; Xia, Hongying; Peng, Jinhui

2018-01-01

The spent phenolic resin is as raw material for preparing high surface area activated carbon (HSAAC) by microwave-assisted KOH activation. The effects of microwave power, activation duration and impregnation ratio (IR) on the iodine adsorption capability and yield of HSAAC were investigated. The surface characteristics of HSAAC were characterized by nitrogen adsorption isotherms, FTIR, SEM and TEM. The operating variables were optimized utilizing the response surface methodology (RSM) and were identified to be microwave power of 700 W, activation duration of 15 min and IR of 4, corresponding to a yield of 51.25 % and an iodine number of 2,384 mg/g. The pore structure parameters of the HSAAC, i. e., Brunauer-Emmett-Teller (BET) surface area, total pore volume, and average pore diameter were estimated to be 4,269 m2/g, 2.396 ml/g and 2.25 nm, respectively, under optimum conditions. The findings strongly support the feasibility of microwave-assisted KOH activation for preparation of HSAAC from spent phenolic resin.

Effect of plasma formation on electron pinching and microwave emission in a virtual cathode oscillator

International Nuclear Information System (INIS)

Yatsuzuka, M.; Nakayama, M.; Nobuhara, S.; Young, D.; Ishihara, O.

1996-01-01

Time and spatial evolutions of anode and cathode plasmas in a vircator diode were observed with a streak camera. A cathode plasma appeared immediately after the rise of a beam current and was followed by an anode plasma typically after about 30 ns. Both plasmas expanded with almost the same speed of order of 104 m/s. The anode plasma was confirmed as a hydrogen plasma with an optical filter for H β line and study of anode-temperature rise. Electron beam pinching immediately followed by microwave emission was observed at the beam current less than the critical current for diode pinching in the experiment and the simulation. The electron beam current in the diode region is well characterized by the electron space-charge-limited current in bipolar flow with the expanding plasmas between the anode-cathode gap. As a result, electron bombardment produced the anode plasma, which made the electron beam strongly pinched, resulting in virtual cathode formation and microwave emission. (author). 5 figs., 5 refs

Surface motion and confinement potential for a microwave confined corona

International Nuclear Information System (INIS)

Ensley, D.L.

1979-07-01

Approximate time dependent solutions for surface velocities and potentials are given for a plane polarized microwave field confining a hot, over-dense plasma corona. Steady state solutions to Poissons' equation can be applied to the time dependent case, provided transit time effects are included. The product of ion pressure and potential wave (surface) velocity gives an average heating rate approx. 7/32 NKT 0 V/sub theta/ directly to the ions

Extreme ultraviolet spectroscopy of low pressure helium microwave driven discharges

Science.gov (United States)

Espinho, Susana; Felizardo, Edgar; Tatarova, Elena; Alves, Luis Lemos

2016-09-01

Surface wave driven discharges are reliable plasma sources that can produce high levels of vacuum and extreme ultraviolet radiation (VUV and EUV). The richness of the emission spectrum makes this type of discharge a possible alternative source in EUV/VUV radiation assisted applications. However, due to challenging experimental requirements, publications concerning EUV radiation emitted by microwave plasmas are scarce and a deeper understanding of the main mechanisms governing the emission of radiation in this spectral range is required. To this end, the EUV radiation emitted by helium microwave driven plasmas operating at 2.45 GHz has been studied for low pressure conditions. Spectral lines from excited helium atoms and ions were detected via emission spectroscopy in the EUV/VUV regions. Novel data concerning the spectral lines observed in the 23 - 33 nm wavelength range and their intensity behaviour with variation of the discharge operational conditions are presented. The intensity of all the spectral emissions strongly increases with the microwave power delivered to the plasma up to 400 W. Furthermore, the intensity of all the ion spectral emissions in the EUV range decreases by nearly one order of magnitude as the pressure was raised from 0.2 to 0.5 mbar. Work funded by FCT - Fundacao para a Ciencia e a Tecnologia, under Project UID/FIS/50010/2013 and grant SFRH/BD/52412/2013 (PD-F APPLAuSE).

Operational features and microwave characteristics of the Vircator II experiment

International Nuclear Information System (INIS)

Price, D.; Fittinghoff, O.; Benford, J.; Sze, H.; Woo, W.

1988-01-01

The Vircator II oscillating virtual-cathode microwave source operates with diode voltages between 600 and 800 kV and diode current between 50 and 120 kA. Maximal microwave output power between 200 and 500 MW is achieved when the diode aspect ratio, cathode surface, charge voltage, and extraction coupling are arranged to simultaneously 1) maximize diode voltage, 2) satisfy magnetic insulation criteria, 3) avoid nonuniform or unstable electron emission, and 4) optimize microwave transmission from the virtual cathode to the launching antenna. Broad-band radiation between 0.4 and 5.5 GHz is generated. The central frequency follows the beam plasma frequency. It is tuned by varying the current density with anode-cathode (A-K) gap adjustments

Effect of vegetation on soil moisture sensing observed from orbiting microwave radiometers

International Nuclear Information System (INIS)

Wang, J.R.

1985-01-01

The microwave radiometric measurements made by the Skylab 1.4 GHz radiometer and by the 6.6 GHz and 10.7 GHz channels of the Nimbus-7 Scanning Multichannel Microwave Radiometer were analyzed to study the large-area soil moisture variations of land surfaces. Two regions in Texas, one with sparse and the other with dense vegetation covers, were selected for the study. The results gave a confirmation of the vegetation effect observed by ground-level microwave radiometers. Based on the statistics of the satellite data, it was possible to estimate surface soil moisture in about five different levels from dry to wet conditions with a 1.4 GHz radiometer, provided that the biomass of the vegetation cover could be independently measured. At frequencies greater than about 6.6 GHz, the radiometric measurements showed little sensitivity to moisture variation for vegetation-covered soils. The effects of polarization in microwave emission were studied also. (author)

New Approach for Monitoring Seismic and Volcanic Activities Using Microwave Radiometer Data

Science.gov (United States)

Maeda, Takashi; Takano, Tadashi

Interferograms formed from the data of satellite-borne synthetic aperture radar (SAR) enable us to detect slight land-surface deformations related to volcanic eruptions and earthquakes. Currently, however, we cannot determine when land-surface deformations occurred with high time resolution since the time lag between two scenes of SAR used to form interferograms is longer than the recurrent period of the satellite carrying it (several tens of days). In order to solve this problem, we are investigating new approach to monitor seismic and vol-canic activities with higher time resolution from satellite-borne sensor data, and now focusing on a satellite-borne microwave radiometer. It is less subject to clouds and rainfalls over the ground than an infrared spectrometer, so more suitable to observe an emission from land sur-faces. With this advantage, we can expect that thermal microwave energy by increasing land surface temperatures is detected before a volcanic eruption. Additionally, laboratory experi-ments recently confirmed that rocks emit microwave energy when fractured. This microwave energy may result from micro discharges in the destruction of materials, or fragment motions with charged surfaces of materials. We first extrapolated the microwave signal power gener-ated by rock failures in an earthquake from the experimental results and concluded that the microwave signals generated by rock failures near the land surface are strong enough to be detected by a satellite-borne radiometer. Accordingly, microwave energy generated by rock failures associated with a seismic activity is likely to be detected as well. However, a satellite-borne microwave radiometer has a serious problem that its spatial res-olution is too coarse compared to SAR or an infrared spectrometer. In order to raise the possibility of detection, a new methodology to compensate the coarse spatial resolution is es-sential. Therefore, we investigated and developed an analysis method to detect local

Bidirectional reflectance distribution function modeling of one-dimensional rough surface in the microwave band

International Nuclear Information System (INIS)

Guo Li-Xin; Gou Xue-Yin; Zhang Lian-Bo

2014-01-01

In this study, the bidirectional reflectance distribution function (BRDF) of a one-dimensional conducting rough surface and a dielectric rough surface are calculated with different frequencies and roughness values in the microwave band by using the method of moments, and the relationship between the bistatic scattering coefficient and the BRDF of a rough surface is expressed. From the theory of the parameters of the rough surface BRDF, the parameters of the BRDF are obtained using a genetic algorithm. The BRDF of a rough surface is calculated using the obtained parameter values. Further, the fitting values and theoretical calculations of the BRDF are compared, and the optimization results are in agreement with the theoretical calculation results. Finally, a reference for BRDF modeling of a Gaussian rough surface in the microwave band is provided by the proposed method. (electromagnetism, optics, acoustics, heat transfer, classical mechanics, and fluid dynamics)

The Contribution of Galactic Free-Free Emission to Anistropies in the Cosmic Microwave Background Found by the Saskatoon Experiment

Science.gov (United States)

Simonetti, John H.; Dennison, Brian; Topasna, Gregory A.

1996-02-01

We made a sensitive, wide-field H alpha image of the north celestial polar region. Using this image, we constrain the contribution of irregularities in interstellar free-free emission to the degree-scale anisotropies in the cosmic microwave background detected in recent observations at Saskatoon by the Princeton group. The analysis of the H alpha image mimics the Saskatoon data analysis: the resulting signal is the strength of irregularities sampled with the Saskatoon beam (i.e., degree-scale) along the 85 deg declination circle. We found no such irregularities that could be attributed to H alpha emission. The implied upper bound on the rms variation in free-free brightness temperature is less than 4.6 mu K at 27.5 GHz. The observed cosmic microwave background anisotropies are much larger. Therefore, the contribution of irregularities in interstellar free-free emission to the observed anisotropies is negligible.

Effect of plasma formation on electron pinching and microwave emission in a virtual cathode oscillator

Energy Technology Data Exchange (ETDEWEB)

Yatsuzuka, M; Nakayama, M; Nobuhara, S [Himeji Institute of Technology (Japan); Young, D; Ishihara, O [Texas Tech Univ., Lubbock, TX (United States)

1997-12-31

Time and spatial evolutions of anode and cathode plasmas in a vircator diode were observed with a streak camera. A cathode plasma appeared immediately after the rise of a beam current and was followed by an anode plasma typically after about 30 ns. Both plasmas expanded with almost the same speed of order of 104 m/s. The anode plasma was confirmed as a hydrogen plasma with an optical filter for H{sub {beta}} line and study of anode-temperature rise. Electron beam pinching immediately followed by microwave emission was observed at the beam current less than the critical current for diode pinching in the experiment and the simulation. The electron beam current in the diode region is well characterized by the electron space-charge-limited current in bipolar flow with the expanding plasmas between the anode-cathode gap. As a result, electron bombardment produced the anode plasma, which made the electron beam strongly pinched, resulting in virtual cathode formation and microwave emission. (author). 5 figs., 5 refs.

Microwave sintering of ZnO nanopowders and characterization for gas sensing

International Nuclear Information System (INIS)

Bai Zikui; Xie Changsheng; Zhang Shunping; Xu Weilin; Xu Jie

2011-01-01

Thick film gas sensors based on ZnO nanopowders were fabricated by using microwave sintering. The surface and cross section morphologies were characterized by field-emission scanning electron microscopy (FE-SEM). The stability of the microstructure was studied by impedance spectroscopy. The results showed that the shape of the nanoparticles was not changed through microwave sintering, and the thick films had the more dense microstructures than that by muffle oven sintering. The resistance-temperature characteristic and the responses to toluene, methanol and formaldehyde revealed that the microwave sintering technique could effectively control the growth of ZnO nanoparticles, realize the uniform sintering of thick film, gain the stable microstructure and improve the response of sensor. In addition, the formative mechanism of the thick film microstructure was proposed according to microwave sintering mechanism.

Surface modification of plasmonic nanostructured materials with thiolated oligonucleotides in 10 seconds using selective microwave heating

International Nuclear Information System (INIS)

Abel, B.; Aslan, K.

2012-01-01

This study demonstrates the proof-of-principle of rapid surface modification of plasmonic nanostructured materials with oligonucleotides using low power microwave heating. Due to their interesting optical and electronic properties, silver nanoparticle films (SNFs, 2 nm thick) deposited onto glass slides were used as the model plasmonic nanostructured materials. Rapid surface modification of SNFs with oligonucleotides was carried out using two strategies (1) Strategy 1: for ss-oligonucleotides, surface hybridization and (2) Strategy 2: for ds-oligonucleotides, solution hybridization, where the samples were exposed to 10, 15, 30 and 60 seconds microwave heating. To assess the efficacy of our new rapid surface modification technique, identical experiments carried out without the microwave heating (i.e., conventional method), which requires 24 hours for the completion of the identical steps. It was found that SNFs can be modified with ss- and ds-oligonucleotides in 10 seconds, which typically requires several hours of incubation time for the chemisorption of thiol groups on to the planar metal surface using conventional techniques. (Copyright copyright 2012 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

A passive and active microwave-vector radiative transfer (PAM-VRT) model

International Nuclear Information System (INIS)

Yang, Jun; Min, Qilong

2015-01-01

A passive and active microwave vector radiative transfer (PAM-VRT) package has been developed. This fast and accurate forward microwave model, with flexible and versatile input and output components, self-consistently and realistically simulates measurements/radiation of passive and active microwave sensors. The core PAM-VRT, microwave radiative transfer model, consists of five modules: gas absorption (two line-by-line databases and four fast models); hydrometeor property of water droplets and ice (spherical and nonspherical) particles; surface emissivity (from Community Radiative Transfer Model (CRTM)); vector radiative transfer of successive order of scattering (VSOS); and passive and active microwave simulation. The PAM-VRT package has been validated against other existing models, demonstrating good accuracy. The PAM-VRT not only can be used to simulate or assimilate measurements of existing microwave sensors, but also can be used to simulate observation results at some new microwave sensors. - Highlights: • A novel microwave vector radiative transfer model is developed. • It can simulate passive and active microwave radiative transfer simultaneously. • It can be applied to simulate measurements for different types of viewing geometry. • The accuracy of this model has been validated against other existing models

Controlled fabrication of the strong emission YVO{sub 4}:Eu{sup 3+} nanoparticles and nanowires by microwave assisted chemical synthesis

Energy Technology Data Exchange (ETDEWEB)

Huong, Tran Thu, E-mail: tthuongims@gmail.com [Institute of Materials Science, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet Road, Cau Giay District, Hanoi (Viet Nam); Vinh, Le Thi [Institute of Materials Science, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet Road, Cau Giay District, Hanoi (Viet Nam); Department of Chemistry, Hanoi University of Mining and Geology (Viet Nam); Phuong, Ha Thi [Institute of Materials Science, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet Road, Cau Giay District, Hanoi (Viet Nam); Department of Chemistry, Hanoi University of Medicine (Viet Nam); Khuyen, Hoang Thi [Institute of Materials Science, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet Road, Cau Giay District, Hanoi (Viet Nam); Anh, Tran Kim [Institute of Materials Science, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet Road, Cau Giay District, Hanoi (Viet Nam); Duy Tan University, 14/25 Quang Trung, Da Nang (Viet Nam); Tu, Vu Duc [Institute of Materials Science, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet Road, Cau Giay District, Hanoi (Viet Nam); Physics, National Chung Cheng University, 168 University Road, Min-Hsiung, Chia-Yi 62102, Taiwan (China); Minh, Le Quoc [Institute of Materials Science, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet Road, Cau Giay District, Hanoi (Viet Nam); Duy Tan University, 14/25 Quang Trung, Da Nang (Viet Nam)

2016-05-15

In this report, we are presenting the controlled fabrication results of the strong emission YVO{sub 4}: Eu{sup 3+} nanoparticles and nanowires by microwave which is assisted chemical synthesis. The effects of incorporated synthesis conditions such as microwave irradiated powers, pH values and concentration of chemical composition on properties of nanomaterials are also investigated to obtain the controllable size and homogenous morphology. Morphological and optical properties of YVO{sub 4}: Eu{sup 3+} prepared products which have been characterized by X-ray diffraction (XRD), field emission micrcroscopy (FESEM) and photoluminescence spectroscopy. As based from result of synthesized samples, we found that the changing of pH values, microwave irradiated powers and chemical composition rise to change reform the size and shape of materials from nanoparticles (diameter about 20 nm) to wires shape (with about 500÷800 nm length and 10÷20 nm width). The photoluminescence (PL) spectroscopy measurements of YVO{sub 4}: Eu{sup 3+} nanostructure materials under UV excitation showed that: the strong luminescence in red region with narrow lines corresponding to the intra-4f transitions of {sup 5}D{sub 0}–{sup 7}F{sub j} (j=1, 2, 3, and 4) of Eu{sup 3+} ions with the highest luminescence intensity of {sup 5}D{sub 0}→{sup 7}F{sub 2} transition. - Highlights: • The strong emission YVO{sub 4}:Eu{sup 3+} nanostructure materials were successfully synthesized by microwave assisted chemical synthesis. • The size, morphology and luminescence of the YVO{sub 4}:Eu{sup 3+} nanostructure materials can be controlled by the solution pH, microwave irradiated powers and chemical composition. • These YVO{sub 4}:Eu{sup 3+} nanostructure materials above can potentially applied in various fields of application, especially in luminescent labeling and visualization in biomedical application.

Microwave remote sensing: Active and passive. Volume 2 - Radar remote sensing and surface scattering and emission theory

Science.gov (United States)

Ulaby, F. T.; Moore, R. K.; Fung, A. K.

1982-01-01

The fundamental principles of radar backscattering measurements are presented, including measurement statistics, Doppler and pulse discrimination techniques, and associated ambiguity functions. The operation of real and synthetic aperture sidelooking airborne radar systems is described, along with the internal and external calibration techniques employed in scattering measurements. Attention is given to the physical mechanisms responsible for the scattering emission behavior of homogeneous and inhomogeneous media, through a discussion of surface roughness, dielectric properties and inhomogeneity, and penetration depth. Simple semiempirical models are presented. Theoretical models involving greater mathematical sophistication are also given for extended ocean and bare soil surfaces, and the more general case of a vegetation canopy over a rough surface.

Secondary electron emission from textured surfaces

Science.gov (United States)

Huerta, C. E.; Patino, M. I.; Wirz, R. E.

2018-04-01

In this work, a Monte Carlo model is used to investigate electron induced secondary electron emission for varying effects of complex surfaces by using simple geometric constructs. Geometries used in the model include: vertical fibers for velvet-like surfaces, tapered pillars for carpet-like surfaces, and a cage-like configuration of interlaced horizontal and vertical fibers for nano-structured fuzz. The model accurately captures the secondary electron emission yield dependence on incidence angle. The model shows that unlike other structured surfaces previously studied, tungsten fuzz exhibits secondary electron emission yield that is independent of primary electron incidence angle, due to the prevalence of horizontally-oriented fibers in the fuzz geometry. This is confirmed with new data presented herein of the secondary electron emission yield of tungsten fuzz at incidence angles from 0-60°.

Development of a modified two-scale electromagnetic model simulating both active and passive microwave measurements: Comparison to data remotely sensed over the ocean

Science.gov (United States)

Boukabara, S. A.; Eymard, L.; Guillou, C.; Lemaire, D.; Sobieski, P.; Guissard, A.

2002-08-01

Spaceborne microwave remote sensing allows the determination of oceanic and atmospheric parameters. Operational payloads such as ERS-1 and ERS-2 and TOPEX/Poseidon as well as missions such as Jason (from NASA-Centre National d'Etudes) or Envisat (from the European Space Agency), have contained or contain paired microwave instruments looking at the nadir direction. This combination consists of microwave radiometers and a radar-altimeter. For the frequencies chosen in oceanographic satellite payloads, the active mode signal is mostly dependent on the surface state through its reflectivity and thus used for the near-surface wind speed retrieval. The active mode can also be attenuated by the atmosphere. On the other hand, the passive mode is related to the surface emissivity and the atmospheric radiation through the radiative transfer equation. Until now, the oceanic and atmospheric parameters have been retrieved separately, the latter being used to correct radar measurements. However, the reflectivity and the emissivity of a target are not independent quantities; hence the synergistic use of these two kinds of microwave measurements should allow one to improve the retrieval quality of the sea and atmosphere parameters. For this purpose, a unified model has been developed for the simulation of both the microwave backscattering coefficient σ° (active measurement) and the microwave emissivity, an important factor for the brightness temperature TB simulation, for every configuration (incidence angles, frequency, polarizations), taking into account the fact that the reflectivity and the emissivity are complementary to unity. The atmospheric absorption is computed following a widely used model from the literature. This paper gives a description and a first attempt of validation of this approach through a comparison with real data. The performance of the model is assessed by comparing the simulations to both brightness temperatures and backscattering coefficients from ERS

Electron emission mechanism of carbon fiber cathode

International Nuclear Information System (INIS)

Liu Lie; Li Limin; Wen Jianchun; Wan Hong

2005-01-01

Models of electron emission mechanism are established concerning metal and carbon fiber cathodes. Correctness of the electron emission mechanism was proved according to micro-photos and electron scanning photos of cathodes respectively. The experimental results and analysis show that the surface flashover induces the electron emission of carbon fiber cathode and there are electron emission phenomena from the top of the carbon and also from its side surface. In addition, compared with the case of the stainless steel cathode, the plasma expansion velocity for the carbon fiber cathode is slower and the pulse duration of output microwave can be widened by using the carbon fiber cathode. (authors)

A model for atmospheric brightness temperatures observed by the special sensor microwave imager (SSM/I)

Science.gov (United States)

Petty, Grant W.; Katsaros, Kristina B.

1989-01-01

A closed-form mathematical model for the atmospheric contribution to microwave the absorption and emission at the SSM/I frequencies is developed in order to improve quantitative interpretation of microwave imagery from the Special Sensor Microwave Imager (SSM/I). The model is intended to accurately predict upwelling and downwelling atmospheric brightness temperatures at SSM/I frequencies, as functions of eight input parameters: the zenith (nadir) angle, the integrated water vapor and vapor scale height, the integrated cloud water and cloud height, the effective surface temperature, atmospheric lapse rate, and surface pressure. It is shown that the model accurately reproduces clear-sky brightness temperatures computed by explicit integration of a large number of radiosonde soundings representing all maritime climate zones and seasons.

Electron Density in Atmospheric Pressure Microwave Surface Wave Discharges

International Nuclear Information System (INIS)

Jasinski, M.; Zakrzewski, Z.; Mizeraczyk, J.

2008-01-01

In this paper, we present results of the spectroscopic measurements of the electron density in a microwave surface wave sustained discharges in Ar and Ne at atmospheric pressure. The discharge in the form of a plasma column was generated inside a quartz tube cooled with a dielectric liquid. The microwave power delivered to the discharge via rectangular waveguide was applied in the range of 200-1500 W. In all investigations presented in this paper, the gas flow rate was relatively low (0.5 l/min), so the plasma column was generated in the form of a single filament, and the lengths of the upstream and downstream plasma columns were almost the same. The electron density in the plasma columns was determined using the method based on the Stark broadening of H β spectral line, including plasma region inside the waveguide which was not investigated earlier

Variability of emissivity and surface temperature over a sparsely vegetated surface

International Nuclear Information System (INIS)

Humes, K.S.; Kustas, W.P.; Moran, M.S.; Nichols, W.D.; Weltz, M.A.

1994-01-01

Radiometric surface temperatures obtained from remote sensing measurements are a function of both the physical surface temperature and the effective emissivity of the surface within the band pass of the radiometric measurement. For sparsely vegetated areas, however, a sensor views significant fractions of both bare soil and various vegetation types. In this case the radiometric response of a sensor is a function of the emissivities and kinetic temperatures of various surface elements, the proportion of those surface elements within the field of view of the sensor, and the interaction of radiation emitted from the various surface components. In order to effectively utilize thermal remote sensing data to quantify energy balance components for a sparsely vegetated area, it is important to examine the typical magnitude and degree of variability of emissivity and surface temperature for such surfaces. Surface emissivity measurements and ground and low-altitude-aircraft-based surface temperature measurements (8-13 micrometer band pass) made in conjunction with the Monsoon '90 field experiment were used to evaluate the typical variability of those quantities during the summer rainy season in a semiarid watershed. The average value for thermal band emissivity of the exposed bare soil portions of the surface was found to be approximately 0.96; the average value measured for most of the varieties of desert shrubs present was approximately 0.99. Surface composite emissivity was estimated to be approximately 0.98 for both the grass-dominated and shrub-dominated portions of the watershed. The spatial variability of surface temperature was found to be highly dependent on the spatial scale of integration for the instantaneous field of view (IFOV) of the instrument, the spatial scale of the total area under evaluation, and the time of day

Microwave assisted in situ synthesis of Ag–NaCMC films and their reproducible surface-enhanced Raman scattering signals

International Nuclear Information System (INIS)

Jiang, Tao; Li, Junpeng; Zhang, Li; Wang, Binbing; Zhou, Jun

2014-01-01

Graphical abstract: Two kinds of Ag–NaCMC films for surface-enhanced Raman scattering (SERS) were prepared by conventional heating and microwave assisted in situ reduction methods without any additional capping or reducing agents. A relatively narrow and symmetric surface plasmon resonance band was observed in the absorption spectra of the films fabricated by the microwave assisted in situ reduction method. More uniform silver nanoparticles (NPs) implied by the symmetric absorption spectrum were further confirmed by the scanning electron microscopy images. After the simulation of the E-field intensity distribution around the silver NPs in NaCMC film, the Raman scattering enhancement factors (EFs) of these films were then investigated with 4-mercaptobenzoic acid molecule as a SERS reporter. Improved reproducibility of SERS signal was obtained in the microwave assisted synthesized Ag–NaCMC film, although it maintained an EF as only 1.11 × 10 8 . The reproducible SERS signal of the Ag–NaCMC film is particularly attractive and this microwave assisted in situ reduction method is suitable for the production of excellent substrate for biosensor application. - Highlights: • The synthesis of Ag–NaCMC films was successfully fulfilled by a low-cost microwave method. • More uniform silver nanoparticles were observed in Ag–NaCMC film synthesized by microwave. • Improved reproducibility of SERS signal was obtained in microwave synthesized Ag–NaCMC film. - Abstract: Two kinds of Ag–NaCMC films for surface-enhanced Raman scattering (SERS) were prepared by conventional heating and microwave assisted in situ reduction methods without any additional capping or reducing agents. A relatively narrow and symmetric surface plasmon resonance band was observed in the absorption spectra of the films fabricated by the microwave assisted in situ reduction method. More uniform silver nanoparticles (NPs) implied by the symmetric absorption spectrum were further confirmed by

Microwave heating of arginine yields highly fluorescent nanoparticles

International Nuclear Information System (INIS)

Philippidis, Aggelos; Stefanakis, Dimitrios; Anglos, Demetrios; Ghanotakis, Demetrios

2013-01-01

Brightly fluorescent nanoparticles were produced via a single-step, single-precursor procedure based on microwave heating of an aqueous solution of the amino acid arginine. Key structural and optical properties of the resulting Arg nanoparticles, Arg-dots, are reported and discussed with emphasis on the pH dependence of their fluorescence emission. The surface of the Arg-dots was functionalised through coupling to folic acid, opening up ways for connecting fluorescent nanoparticles to cancer cells. The generality and versatility of the microwave heating procedure was further demonstrated by the synthesis of different types of carbon nanoparticles, such as CE-dots, that were produced by use of citric acid and ethanolamine as precursors and compared to the Arg-dots.

Microwave discharges in capillary tubes

International Nuclear Information System (INIS)

Dervisevic, Emil

1984-01-01

This research thesis aims at being a contribution to the study of microwave discharge by a surface wave, and more precisely focusses on the discharge in capillary tubes filled with argon. The author first present theoretical models which describe, on the one hand, the propagation of the surface wave along the plasma column, and, on the other hand, longitudinal and radial profiles of the main discharge characteristics. The second part addresses the study of the influence of parameters (gas pressure and tube radius) on discharge operation and characteristics. Laws of similitude as well as empirical relationships between argon I and argon II emission line intensities, electron density, and electric field in the plasma have been established [fr

A theoretical study on the use of microwaves in reducing energy consumption for an endothermic reaction: Role of metal coated bounding surface

International Nuclear Information System (INIS)

Bhattacharya, Madhuchhanda; Basak, Tanmay

2013-01-01

This work presents a theoretical analysis on savings of energy during an endothermic reaction under microwave heating compared to conventional heating and shows the use of metal coated bounding surface to enhance the energy savings in otherwise low saving zones. Main thrust of this work is the quantification of energy savings for various probable microwave heating scenarios that may arise either due to varying reactor dimension (2L) over thin, intermediate and thick regimes or due to varying dielectric properties of the reactor. The analysis considers detailed transport equations in conjunction with Helmholtz equation for microwave propagation within a semiinfinite batch reactor. Simulations show that use of microwave can significantly save energy (as high as 60%) depending on reactor configuration. Simulations also show efficient use of metal coated bounding surface to enhance energy savings for reactors with 2L/λ eff = 0.5n−0.25, where n = 1, 2, 3… and λ eff is wavelength of microwave within the reactor. The enhancement is found to be 2 and 1.5 times at 2L/λ eff = 0.25 and 0.75, respectively. Various regions of efficient use of metal coated bounding surface for different microwave heating scenarios have been identified in a series of master curves. - Highlights: • This work simulates chemical reaction under microwave radiation using detailed model. • Simulations are presented in presence or absence of metal coated bounding surface. • Savings of energy under microwave have been analyzed for various probable scenarios. • Simulations show significant savings of energy under microwave heating. • Simulations show the potential of metal coated bounding surface to further enhance energy savings

Modeling the Observed Microwave Emission from Shallow Multi-Layer Tundra Snow Using DMRT-ML

Directory of Open Access Journals (Sweden)

Nastaran Saberi

2017-12-01

Full Text Available The observed brightness temperatures (Tb at 37 GHz from typical moderate density dry snow in mid-latitudes decreases with increasing snow water equivalent (SWE due to volume scattering of the ground emissions by the overlying snow. At a certain point, however, as SWE increases, the emission from the snowpack offsets the scattering of the sub-nivean emission. In tundra snow, the Tb slope reversal occurs at shallower snow thicknesses. While it has been postulated that the inflection point in the seasonal time series of observed Tb V 37 GHz of tundra snow is controlled by the formation of a thick wind slab layer, the simulation of this effect has yet to be confirmed. Therefore, the Dense Media Radiative Transfer Theory for Multi Layered (DMRT-ML snowpack is used to predict the passive microwave response from airborne observations over shallow, dense, slab-layered tundra snow. Airborne radiometer observations coordinated with ground-based in situ snow measurements were acquired in the Canadian high Arctic near Eureka, NT, in April 2011. The DMRT-ML was parameterized with the in situ snow measurements using a two-layer snowpack and run in two configurations: a depth hoar and a wind slab dominated pack. With these two configurations, the calibrated DMRT-ML successfully predicted the Tb V 37 GHz response (R correlation of 0.83 when compared with the observed airborne Tb footprints containing snow pits measurements. Using this calibrated model, the DMRT-ML was applied to the whole study region. At the satellite observation scale, observations from the Advanced Microwave Scanning Radiometer-Earth Observing System (AMSR-E over the study area reflected seasonal differences between Tb V 37 GHz and Tb V 19 GHz that supports the hypothesis of the development of an early season volume scattering depth hoar layer, followed by the growth of the late season emission-dominated wind slab layer. This research highlights the necessity to consider the two

The EUMETSAT OSI SAF near 50 GHz sea ice emissivity model

Directory of Open Access Journals (Sweden)

Rasums T. Tonboe

2013-02-01

Full Text Available A sea ice thermal microwave emission model for 50 GHz was developed under EUMETSAT's Ocean and Sea Ice Satellite Application Facility (OSI SAF programme. The model is based on correlations between the surface brightness temperature at 18, 36 and 50 GHz. The model coefficients are estimated using simulated data from a combined thermodynamic and emission model. The intention with the model is to provide a first guess sea ice surface emissivity estimate for atmospheric temperature sounding applications in the troposphere in numerical weather prediction (NWP models assimilating Advanced Microwave Sounding Unit (AMSU and Special Sensor Microwave Imager/Sounder (SSMIS data. The spectral gradient ratio is defined as the difference over the sum of the SSMIS brightness temperatures at 18 and 36 GHz vertical linear polarisation (GR1836. The GR1836 is related to the emissivity at the atmospheric temperature sounding channels at around 50 GHz. Furthermore, the brightness temperatures and the polarisation ratio (PR at the neighbouring 18, 36 and 50 GHz channels are highly correlated. Both the gradient ratio at 18 and 36 GHz and the PR at 36 GHz measured by SSMIS are input into the model predicting the 50 GHz emissivity for horizontal and vertical linear polarisations and incidence angles between 0° and 60° The simulated emissivity is compared to the emissivity derived with alternative methods. The fit to real AMSU observations is investigated using the different emissivity estimates for simulating the observations with atmospheric data from a regional weather prediction model.

Microwave radiation mechanism in a pulse-laser-irradiated Cu foil target revisited

International Nuclear Information System (INIS)

Chen Ziyu; Li Jianfeng; Li Jun; Peng Qixian

2011-01-01

The microwave radiation mechanism in a Cu-based foil target irradiated by an intense laser pulse has been investigated. Microwave emission in the frequency range 0.5-4 GHz has been observed from a 200 ps laser pulse of intensity about 10 12 W cm -2 normally incident on the target surface. The total microwave power and energy emitted from the interaction were found to be about 0.4 W and 2 nJ, respectively, corresponding to an efficiency of coupling laser energy to microwave energy of 2x10 -8 . The result agrees well with quadrupole radiation calculated based on a circuit model of a laser plasma, which indicates that the radiative process can be explained by magnetic dipole or electric quadrupole radiation from the laser-produced symmetric poloidal current distribution at the plasma-target interface.

Microwave radiation mechanism in a pulse-laser-irradiated Cu foil target revisited

Energy Technology Data Exchange (ETDEWEB)

Chen Ziyu; Li Jianfeng; Li Jun; Peng Qixian, E-mail: ziyuch@gmail.com [Institute of Fluid Physics, China Academy of Engineering Physics, Mianyang 621900 (China)

2011-05-01

The microwave radiation mechanism in a Cu-based foil target irradiated by an intense laser pulse has been investigated. Microwave emission in the frequency range 0.5-4 GHz has been observed from a 200 ps laser pulse of intensity about 10{sup 12} W cm{sup -2} normally incident on the target surface. The total microwave power and energy emitted from the interaction were found to be about 0.4 W and 2 nJ, respectively, corresponding to an efficiency of coupling laser energy to microwave energy of 2x10{sup -8}. The result agrees well with quadrupole radiation calculated based on a circuit model of a laser plasma, which indicates that the radiative process can be explained by magnetic dipole or electric quadrupole radiation from the laser-produced symmetric poloidal current distribution at the plasma-target interface.

Quantitative sub-surface and non-contact imaging using scanning microwave microscopy

International Nuclear Information System (INIS)

Gramse, Georg; Kasper, Manuel; Hinterdorfer, Peter; Brinciotti, Enrico; Rankl, Christian; Kienberger, Ferry; Lucibello, Andrea; Marcelli, Romolo; Patil, Samadhan B.; Giridharagopal, Rajiv

2015-01-01

The capability of scanning microwave microscopy for calibrated sub-surface and non-contact capacitance imaging of silicon (Si) samples is quantitatively studied at broadband frequencies ranging from 1 to 20 GHz. Calibrated capacitance images of flat Si test samples with varying dopant density (10 15 –10 19 atoms cm −3 ) and covered with dielectric thin films of SiO 2 (100–400 nm thickness) are measured to demonstrate the sensitivity of scanning microwave microscopy (SMM) for sub-surface imaging. Using standard SMM imaging conditions the dopant areas could still be sensed under a 400 nm thick oxide layer. Non-contact SMM imaging in lift-mode and constant height mode is quantitatively demonstrated on a 50 nm thick SiO 2 test pad. The differences between non-contact and contact mode capacitances are studied with respect to the main parameters influencing the imaging contrast, namely the probe tip diameter and the tip–sample distance. Finite element modelling was used to further analyse the influence of the tip radius and the tip–sample distance on the SMM sensitivity. The understanding of how the two key parameters determine the SMM sensitivity and quantitative capacitances represents an important step towards its routine application for non-contact and sub-surface imaging. (paper)

Surface-electronic-state effects in electron emission from the Be(0001) surface

International Nuclear Information System (INIS)

Archubi, C. D.; Gravielle, M. S.; Silkin, V. M.

2011-01-01

We study the electron emission produced by swift protons impinging grazingly on a Be(0001) surface. The process is described within a collisional formalism using the band-structure-based (BSB) approximation to represent the electron-surface interaction. The BSB model provides an accurate description of the electronic band structure of the solid and the surface-induced potential. Within this approach we derive both bulk and surface electronic states, with these latter characterized by a strong localization at the crystal surface. We found that such surface electronic states play an important role in double-differential energy- and angle-resolved electron emission probabilities, producing noticeable structures in the electron emission spectra.

Surface-electronic-state effects in electron emission from the Be(0001) surface

Energy Technology Data Exchange (ETDEWEB)

Archubi, C. D. [Instituto de Astronomia y Fisica del Espacio, casilla de correo 67, sucursal 28, C1428EGA, Buenos Aires (Argentina); Gravielle, M. S. [Instituto de Astronomia y Fisica del Espacio, casilla de correo 67, sucursal 28, C1428EGA, Buenos Aires (Argentina); Departamento de Fisica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Buenos Aires (Argentina); Silkin, V. M. [Donostia International Physics Center, E-20018 San Sebastian (Spain); Departamento de Fisica de Materiales, Facultad de Ciencias Quimicas, Universidad del Pais Vasco, Apartado 1072, E-20080 San Sebastian (Spain); IKERBASQUE, Basque Foundation for Science, E-48011 Bilbao (Spain)

2011-07-15

We study the electron emission produced by swift protons impinging grazingly on a Be(0001) surface. The process is described within a collisional formalism using the band-structure-based (BSB) approximation to represent the electron-surface interaction. The BSB model provides an accurate description of the electronic band structure of the solid and the surface-induced potential. Within this approach we derive both bulk and surface electronic states, with these latter characterized by a strong localization at the crystal surface. We found that such surface electronic states play an important role in double-differential energy- and angle-resolved electron emission probabilities, producing noticeable structures in the electron emission spectra.

An evaluation of microwave-assisted fusion and microwave-assisted acid digestion methods for determining elemental impurities in carbon nanostructures using inductively coupled plasma optical emission spectrometry

KAUST Repository

Patole, Shashikant P.

2015-10-21

It is common for as-prepared carbon nanotube (CNT) and graphene samples to contain remnants of the transition metals used to catalyze their growth; contamination may also leave other trace elemental impurities in the samples. Although a full quantification of impurities in as-prepared samples of carbon nanostructures is difficult, particularly when trace elements are intercalated or encapsulated within a protective layer of graphitic carbon, reliable information is essential for reasons such as quantifying the adulteration of physico-chemical properties of the materials and for evaluating environmental issues. Here, we introduce a microwave-based fusion method to degrade single- and double-walled CNTs and graphene nanoplatelets into a fusion flux thereby thoroughly leaching all metallic impurities. Subsequent dissolution of the fusion product in diluted hydrochloric and nitric acid allowed us to identify their trace elemental impurities using inductively coupled plasma optical emission spectrometry. Comparisons of the results from the proposed microwave-assisted fusion method against those of a more classical microwave-assisted acid digestion approach suggest complementarity between the two that ultimately could lead to a more reliable and less costly determination of trace elemental impurities in carbon nanostructured materials. Graphical abstract A method for the complete digestion of carbon nanostructures has been demonstrated. Photographs (on the left side) show zirconium crucibles containing SWCNTs with flux of Na2CO3 and K2CO3, before and after microwave fusion; (on the right side) the appearance of the final solutions containing dissolved samples, from microwave-assisted fusion and microwave-assisted acid digestion. These solutions were used for determining the trace elemental impurities by ICP‒OES.

Modeling microwave/electron-cloud interaction

International Nuclear Information System (INIS)

Mattes, M; Sorolla, E; Zimmermann, F

2013-01-01

Starting from the separate codes BI-RME and ECLOUD or PyECLOUD, we are developing a novel joint simulation tool, which models the combined effect of a charged particle beam and of microwaves on an electron cloud. Possible applications include the degradation of microwave transmission in telecommunication satellites by electron clouds; the microwave-transmission techniques being used in particle accelerators for the purpose of electroncloud diagnostics; the microwave emission by the electron cloud itself in the presence of a magnetic field; and the possible suppression of electron-cloud formation in an accelerator by injecting microwaves of suitable amplitude and frequency. A few early simulation results are presented. (author)

Characterization of an Atmospheric-Pressure Argon Plasma Generated by 915 MHz Microwaves Using Optical Emission Spectroscopy

Directory of Open Access Journals (Sweden)

Robert Miotk

2017-01-01

Full Text Available The paper presents the investigations of an atmospheric-pressure argon plasma generated at 915 MHz microwaves using the optical emission spectroscopy (OES. The 915 MHz microwave plasma was inducted and sustained in a waveguide-supplied coaxial-line-based nozzleless microwave plasma source. The aim of presented investigations was to estimate parameters of the generated plasma, that is, excitation temperature of electrons Texc, temperature of plasma gas Tg, and concentration of electrons ne. Assuming that excited levels of argon atoms are in local thermodynamic equilibrium, Boltzmann method allowed in determining the Texc temperature in the range of 8100–11000 K. The temperature of plasma gas Tg was estimated by comparing the simulated spectra of the OH radical to the measured one in LIFBASE program. The obtained Tg temperature ranged in 1200–2800 K. Using a method based on Stark broadening of the Hβ line, the concentration of electrons ne was determined in the range from 1.4 × 1015 to 1.7 × 1015 cm−3, depending on the power absorbed by the microwave plasma.

Spatially resolved emission spectroscopic investigation of microwave-induced reactive low-power plasma jets

International Nuclear Information System (INIS)

Arnold, Thomas; Grabovski, Sergey; Schindler, Axel; Wagner, Hans-Erich

2004-01-01

A microwave-induced Ar/SF 6 plasma jet is characterized by means of optical emission spectroscopy. Rotational temperatures from unresolved N 2 bands and excitation temperatures from Fe lines as well as electron densities (H β Stark broadening) have been estimated along the plasma jet axis using a side-on configuration. The SF 6 gas flow rate and chamber pressure were varied from 10 to 250 sccm and 20 to 500 mbar, respectively. Three characteristic jet regions have been observed: the plasma ignition zone, followed by the gas mixing zone and a relaxing zone

Field Measurements of PCB emissions from Building Surfaces Using a New Portable Emission Test Cell

DEFF Research Database (Denmark)

Lyng, Nadja; Haven, Rune; Gunnarsen, Lars Bo

2016-01-01

The purpose of the study was to measure PCB-emission rates from indoor surfaces on-site in contaminated buildings using a newly developed portable emission test cell. Emission rates were measured from six different surfaces; three untreated surfaces and three remediated surfaces in a contaminated...

Modulation of surface structure and catalytic properties of cerium oxide nanoparticles by thermal and microwave synthesis techniques

Energy Technology Data Exchange (ETDEWEB)

He, Jian [College of Pharmacy, Third Military Medical University, Chongqing 400038 (China); Zhou, Lan; Liu, Jie; Yang, Lu; Zou, Ling; Xiang, Junyu; Dong, Shiwu [School of Biomedical Engineering, Third Military Medical University, Chongqing 400038 (China); Yang, Xiaochao, E-mail: xcyang@tmmu.edu.cn [School of Biomedical Engineering, Third Military Medical University, Chongqing 400038 (China)

2017-04-30

Highlights: • The CNPs synthesized by microwave irradiation have more reactive hot spots than that synthesized by convective heating. • The CNPs synthesized by microwave irradiation exhibited higher SOD activity than that synthesized by convective heating. • The CNPs synthesized by microwave irradiation heating could better protect cells from oxidative stress. - Abstract: Cerium oxide nanoparticles (CNPs) have been intensively explored for biomedical applications in recent few years due to the versatile enzyme mimetic activities of the nanoparticles. However, the control of CNPs quality through the optimization of synthesis conditions remains largely unexplored as most of the previous studies only focus on utilizing the catalytic activities of the nanoparticles. In the present study, CNPs with size about 5 nm were synthesized by thermal decomposition method using traditional convective heating and recently developed microwave irradiation as heating source. The quality of CNPs synthesized by the two heating manner was evaluated. The CNPs synthesized by convective heating were slightly smaller than that synthesized by microwave irradiation heating. The cores of the CNPs synthesized by the two heating manner have similar crystal structure. While the surface subtle structures of the CNPs synthesized by two heating manner were different. The CNPs synthesized by microwave irradiation have more surface reactive hot spot than that synthesized by convective heating as the nanoparticles responded more actively to the redox environment variation. This difference resulted in the higher superoxide dismutase (SOD) mimetic activity of CNPs synthesized by microwave irradiation heating than that of the convective heating. Preliminary experiments indicated that the CNPs synthesized by microwave irradiation heating could better protect cells from oxidative stress due to the higher SOD mimetic activity of the nanoparticles.

Modulation of surface structure and catalytic properties of cerium oxide nanoparticles by thermal and microwave synthesis techniques

International Nuclear Information System (INIS)

He, Jian; Zhou, Lan; Liu, Jie; Yang, Lu; Zou, Ling; Xiang, Junyu; Dong, Shiwu; Yang, Xiaochao

2017-01-01

Highlights: • The CNPs synthesized by microwave irradiation have more reactive hot spots than that synthesized by convective heating. • The CNPs synthesized by microwave irradiation exhibited higher SOD activity than that synthesized by convective heating. • The CNPs synthesized by microwave irradiation heating could better protect cells from oxidative stress. - Abstract: Cerium oxide nanoparticles (CNPs) have been intensively explored for biomedical applications in recent few years due to the versatile enzyme mimetic activities of the nanoparticles. However, the control of CNPs quality through the optimization of synthesis conditions remains largely unexplored as most of the previous studies only focus on utilizing the catalytic activities of the nanoparticles. In the present study, CNPs with size about 5 nm were synthesized by thermal decomposition method using traditional convective heating and recently developed microwave irradiation as heating source. The quality of CNPs synthesized by the two heating manner was evaluated. The CNPs synthesized by convective heating were slightly smaller than that synthesized by microwave irradiation heating. The cores of the CNPs synthesized by the two heating manner have similar crystal structure. While the surface subtle structures of the CNPs synthesized by two heating manner were different. The CNPs synthesized by microwave irradiation have more surface reactive hot spot than that synthesized by convective heating as the nanoparticles responded more actively to the redox environment variation. This difference resulted in the higher superoxide dismutase (SOD) mimetic activity of CNPs synthesized by microwave irradiation heating than that of the convective heating. Preliminary experiments indicated that the CNPs synthesized by microwave irradiation heating could better protect cells from oxidative stress due to the higher SOD mimetic activity of the nanoparticles.

Emission, absorption and group delay of microwaves in the atmosphere in relation to water vapour content over the Indian subcontinent

Science.gov (United States)

Sen, A. K.; Gupta, A. K. D.; Karmakar, P. K.; Barman, S. D.; Bhattacharya, A. B.; Purkait, N.; Gupta, M. K. D.; Sehra, J. S.

1985-01-01

The advent of satellite communication for global coverage has apparently indicated a renewed interest in the studies of radio wave propagation through the atmosphere, in the VHF, UHF and microwave bands. The extensive measurements of atmosphere constituents, dynamics and radio meterological parameters during the Middle Atmosphere Program (MAP) have opened up further the possibilities of studying tropospheric radio wave propagation parameters, relevant to Earth/space link design. The three basic parameters of significance to radio propagation are thermal emission, absorption and group delay of the atmosphere, all of which are controlled largely by the water vapor content in the atmosphere, particular at microwave bands. As good emitters are also good absorbers, the atmospheric emission as well as the absorption attains a maximum at the frequency of 22.235 GHz, which is the peak of the water vapor line. The group delay is practically independent of frequency in the VHF, UHF and microwave bands. However, all three parameters exhibit a similar seasonal dependence originating presumably from the seasonal dependence of the water vapor content. Some of the interesting results obtained from analyses of radiosonde data over the Indian subcontinent collected by the India Meteorological Department is presented.

Localised Microwave Bursts During ELMs on MAST

Directory of Open Access Journals (Sweden)

Freethy Simon

2015-01-01

Full Text Available Bursts of microwave emission are observed during ELM events on the Mega Ampère Spherical Tokamak. In agreement with observations on other machines, these bursts are up to 3 orders of magnitude more intense than the thermal background, but are electron cyclotron in nature. The peak in microwave emission is ~20μ before the peak in midplane Dα emission. Using the Synthetic Aperture Microwave Imaging radiometer, we are able to demonstrate that these bursts are often highly spatially localised and preferentially occur at the tokamak midplane. It is hypothesised that the localisation is a result of Doppler resonance broadening for electron Bernstein waves and the high perpendicular electron energies could be the result of pitch angle scattering in high collisionality regions of the plasma.

Study on anti-emission materials for non-emitting grid applications in microwave power tubes

International Nuclear Information System (INIS)

Jiang, J.; Jiang, B.Y.; Ren, C.X.; Zhang, F.M.; Feng, T.; Wang, X.; Liu, X.H.; Zou, S.C.

2006-01-01

Hafnium and platinum were deposited onto molybdenum grids by ion-beam assisted deposition method. Electron-emission characteristics from molybdenum grids with Hf and Pt films, which were contaminated by active electron-emission substances (Ba, BaO) of the cathode, were measured using analogous diode method. The surfaces of grids were analyzed by X-ray diffraction. The results revealed that the reaction between BaO and Hf formed BaHfO 3 compound, which greatly reduced the accumulation of BaO on the surface and accordingly decreased grid emission. In contrast, Ba were formed by the decomposition of BaO on the surface of Pt film under high temperature and re-evaporated from its surface, which reduced the active electron-emission substances on the surface of the grid and effectively restrained grid emission. Their mechanisms for grid-emission suppression are discussed and a good method to develop new grid-coating materials is suggested

Microwave radiation is effective at disinfecting dental stone surfaces without changing their physical properties.

Science.gov (United States)

Bona, Ariel José; Amaral-Brito, Mauro Gustavo; Rodrigues, José Augusto; Peruzzo, Daiane Cristina; França, Fabiana Mantovani Gomes

2017-01-01

The aims of this study were to evaluate the effectiveness of different microwave radiation regimens for disinfection of type IV dental stone surfaces and to assess the influence of these regimens on surface roughness and dimensional change following disinfection. Three hundred cylindrical (20 × 2-mm) test specimens were made in type IV stone and divided into subgroups of 20 according to the microorganisms tested (Staphylococcus aureus, Escherichia coli, or Candida albicans) and the 900-W microwave radiation protocol (cycles of 3, 5, or 7 minutes; a positive control; or a negative control). To test physical changes, 80 test specimens were made with the same dimensions except that they had 2 parallel and symmetrical indentations measuring 8 × 4 mm. These specimens were divided into 4 subgroups of 20 each (a subgroup for each radiation time and a negative control). The mean dimensional change and roughness data were analyzed by mixed models for repeated measures and Tukey-Kramer tests. Disinfection was analyzed with descriptive statistics. For E coli and C albicans, all radiation times proved effective at sterilizing the test specimens. For S aureus, sterilization was achieved with 5 and 7 minutes of exposure; however, colonies were observed in 10 Petri dishes (50%) exposed to 3 minutes of microwave radiation. No statistically significant difference in dimensional change or surface roughness was observed for any radiation regimen (P > 0.05).

Increased field-emission site density from regrown carbon nanotube films

International Nuclear Information System (INIS)

Wang, Y.Y.; Gupta, S.; Liang, M.; Nemanich, R.J.

2005-01-01

Electron field-emission properties of as-grown, etched, and regrown carbon nanotube thin films were investigated. The aligned carbon nanotube films were deposited by the microwave plasma-assisted chemical vapor deposition technique. The surface of the as-grown film contained a carbon nanotube mat of amorphous carbon and entangled nanotubes with some tubes protruding from the surface. Hydrogen plasma etching resulted in the removal of the surface layer, and regrowth on the etched surface displayed the formation of a new carbon nanotube mat. The emission site density and the current-voltage dependence of the field emission from all of the samples were analyzed. The results showed that the as-grown sample had a few strong emission spots and a relatively high emission current density (∼20 μA/cm 2 at 1 V/μm), while the regrown sample exhibited a significantly increased emission site density

Evaluating superconductors for microwave applications

International Nuclear Information System (INIS)

Hammond, B.; Bybokas, J.

1989-01-01

It is becoming increasingly obvious that some of the earliest applications for high Tc superconductors will be in the microwave market. While this is a major opportunity for the superconductor community, it also represents a significant challenge. At DC or low frequencies a superconductor can be easily characterized by simple measurements of resistivity and magnetic susceptibility versus temperature. These parameters are fundamental to superconductor characterization and various methods exist for measuring them. The only valid way to determine the microwave characteristics of a superconductor is to measure it at microwave frequencies. It is for this reason that measuring microwave surface resistance has emerged as one of the most demanding and telling tests for materials intended for high frequency applications. In this article, the theory of microwave surface resistance is discussed. Methods for characterizing surface resistance theoretically and by practical implementation are described

Theoretical insight into ArO2 surface-wave microwave discharges

OpenAIRE

2010-01-01

Abstract A zero-dimensional kinetic model has been developed to investigate the coupled electron and heavy-particle kinetics in Ar-O 2 surface-wave microwave discharges generated in long cylindrical tubes, such as those launched with a surfatron or a surfaguide. The model has been validated by comparing the calculated electron temperature and species densities with experimental data available in the literature for different discharge conditions. Systematic studies have been carried out for...

Visualization of the microwave beam generated by a plasma relativistic microwave amplifier

Energy Technology Data Exchange (ETDEWEB)

Alekseev, I. S.; Ivanov, I. E.; Strelkov, P. S., E-mail: strelkov@fpl.gpi.ru [Russian Academy of Science, Prokhorov General Physics Institute (Russian Federation); Tarakanov, V. P., E-mail: karat@msk.su [Russian Academy of Sciences, Joint Institute for High Temperatures (Russian Federation); Ulyanov, D. K. [Russian Academy of Science, Prokhorov General Physics Institute (Russian Federation)

2017-03-15

A method based on the detection of emission of a dielectric screen with metal microinclusions in open air is applied to visualize the transverse structure of a high-power microwave beam. In contrast to other visualization techniques, the results obtained in this work provide qualitative information not only on the electric field strength, but also on the structure of electric field lines in the microwave beam cross section. The interpretation of the results obtained with this method is confirmed by numerical simulations of the structure of electric field lines in the microwave beam cross section by means of the CARAT code.

OPTIMIZATION OF MICROWAVE AND AIR DRYING CONDITIONS OF QUINCE (CYDONIA OBLONGA, MILLER USING RESPONSE SURFACE METHODOLOGY

Directory of Open Access Journals (Sweden)

Cem Baltacioglu

2015-03-01

Full Text Available Effects of slice thickness of quince (Cydonia oblonga Miller , microwave incident power and air drying temperature on antioxidant activity and total phenolic content of quince were investigated during drying in microwave and air drying. Optimum conditions were found to be: i for microwave drying, 285 W and 4.14 mm thick (maximum antioxidant activity and 285 W and 6.85 mm thick (maximum total phenolic content, and ii for air drying, 75 ºC and 1.2 mm thick (both maximum antioxidant activity and total phenolic content. Drying conditions were optimized by using the response surface methodology. 13 experiments were carried out considering incident microwave powers from 285 to 795 W, air temperature from 46 to 74 ºC and slice thickness from 1.2 to 6.8 mm.

Photoelectric emission from negative-electron-affinity diamond (111) surfaces: Exciton breakup versus conduction-band emission

International Nuclear Information System (INIS)

Bandis, C.; Pate, B.B.

1995-01-01

We have recently reported that bound electron-hole pairs (Mott-Wannier excitons) are the dominant source of photoelectron emission from specially prepared [''as-polished'' C(111)-(1x1):H] negative-electron-affinity diamond surfaces for near-band-gap excitation up to 0.5 eV above threshold [C. Bandis and B. B. Pate, Phys. Rev. Lett. 74, 777 (1995)]. It was found that photoexcited excitons transport to the surface, break up, and emit their electron. In this paper, we extend the study of exciton-derived emission to include partial yield (constant final-state) analysis as well as angular distribution measurements of the photoelectric emission. In addition, we find that exciton-derived emission does not always dominate. Photoelectric emission properties of the in situ ''rehydrogenated'' (111)-(1x1):H diamond surface are characteristically different than emission observed from the as-polished (111)-(1x1):H surface. The rehydrogenated surface has additional downward band bending as compared to the as-polished surface. In confirmation of the assignment of photoelectric yield to exciton breakup emission, we find a significant enhancement of the total electron yield when the downward band bending of the hydrogenated surface is increased. The functional form of the observed total electron yield demonstrates that, in contrast to the as-polished surface, conduction-band electrons are a significant component of the observed photoelectric yield from the in situ hydrogenated (111)-(1x1):H surface. Furthermore, electron emission characteristics of the rehydrogenated surface confirms our assignment of a Fan phonon-cascade mechanism for thermalization of excitons

Space-Charge-Limited Emission Models for Particle Simulation

Science.gov (United States)

Verboncoeur, J. P.; Cartwright, K. L.; Murphy, T.

2004-11-01

Space-charge-limited (SCL) emission of electrons from various materials is a common method of generating the high current beams required to drive high power microwave (HPM) sources. In the SCL emission process, sufficient space charge is extracted from a surface, often of complicated geometry, to drive the electric field normal to the surface close to zero. The emitted current is highly dominated by space charge effects as well as ambient fields near the surface. In this work, we consider computational models for the macroscopic SCL emission process including application of Gauss's law and the Child-Langmuir law for space-charge-limited emission. Models are described for ideal conductors, lossy conductors, and dielectrics. Also considered is the discretization of these models, and the implications for the emission physics. Previous work on primary and dual-cell emission models [Watrous et al., Phys. Plasmas 8, 289-296 (2001)] is reexamined, and aspects of the performance, including fidelity and noise properties, are improved. Models for one-dimensional diodes are considered, as well as multidimensional emitting surfaces, which include corners and transverse fields.

Investigation of the Surface Filamentary Discharge in Focus of Microwave Radiation

Science.gov (United States)

2010-08-01

microwave radiation 5a. CONTRACT NUMBER ISTC Registration No: 3784 5b. GRANT NUMBER 5c. PROGRAM ELEMENT NUMBER 6. AUTHOR(S) Dr. Kirill...NUMBER(S) ISTC 07-7011 12. DISTRIBUTION/AVAILABILITY STATEMENT Approved for public release; distribution is unlimited. (approval given by local...contract to the International Science and Technology Center ( ISTC ), Moscow Project ISTC # 3784p (077011) Investigation of the surface filamentary

Partial microwave-assisted wet digestion of animal tissue using a baby-bottle sterilizer for analyte determination by inductively coupled plasma optical emission spectrometry

International Nuclear Information System (INIS)

Matos, Wladiana O.; Menezes, Eveline A.; Gonzalez, Mario H.; Costa, Leticia M.; Trevizan, Lilian C.; Nogueira, Ana Rita A.

2009-01-01

A procedure for partial digestion of bovine tissue is proposed using polytetrafluoroethylene (PTFE) micro-vessels inside a baby-bottle sterilizer under microwave radiation for multi-element determination by inductively coupled plasma optical emission spectrometry (ICP OES). Samples were directly weighed in laboratory-made polytetrafluoroethylene vessels. Nitric acid and hydrogen peroxide were added to the uncovered vessels, which were positioned inside the baby-bottle sterilizer, containing 500 mL of water. The hydrogen peroxide volume was fixed at 100 μL. The system was placed in a domestic microwave oven and partial digestion was carried out for the determination of Ca, Cu, Fe, Mg, Mn and Zn by inductively coupled plasma optical emission spectrometry. The single-vessel approach was used in the entire procedure, to minimize contamination in trace analysis. Better recoveries and lower residual carbon content (RCC) levels were obtained under the conditions established through a 2 4-1 fractional factorial design: 650 W microwave power, 7 min digestion time, 50 μL nitric acid and 50 mg sample mass. The digestion efficiency was ascertained according to the residual carbon content determined by inductively coupled plasma optical emission spectrometry. The accuracy of the proposed procedure was checked against two certified reference materials.

Source analysis of spaceborne microwave radiometer interference over land

Science.gov (United States)

Guan, Li; Zhang, Sibo

2016-03-01

Satellite microwave thermal emissions mixed with signals from active sensors are referred to as radiofrequency interference (RFI). Based on Advanced Microwave Scanning Radiometer-Earth Observing System (AMSR-E) observations from June 1 to 16, 2011, RFI over Europe was identified and analyzed using the modified principal component analysis algorithm in this paper. The X band AMSR-E measurements in England and Italy are mostly affected by the stable, persistent, active microwave transmitters on the surface, while the RFI source of other European countries is the interference of the reflected geostationary TV satellite downlink signals to the measurements of spaceborne microwave radiometers. The locations and intensities of the RFI induced by the geostationary TV and communication satellites changed with time within the observed period. The observations of spaceborne microwave radiometers in ascending portions of orbits are usually interfered with over European land, while no RFI was detected in descending passes. The RFI locations and intensities from the reflection of downlink radiation are highly dependent upon the relative geometry between the geostationary satellite and the measuring passive sensor. Only these fields of view of a spaceborne instrument whose scan azimuths are close to the azimuth relative to the geostationary satellite are likely to be affected by RFI.

Thermal measurement a requirement for monolithic microwave integrated circuit design

OpenAIRE

Hopper, Richard; Oxley, C. H.

2008-01-01

The thermal management of structures such as Monolithic Microwave Integrated Circuits (MMICs) is important, given increased circuit packing densities and RF output powers. The paper will describe the IR measurement technology necessary to obtain accurate temperature profiles on the surface of semiconductor devices. The measurement procedure will be explained, including the device mounting arrangement and emissivity correction technique. The paper will show how the measurement technique has be...

FTIR Emission spectroscopy of surfaces

Science.gov (United States)

Van Woerkom, P. C. M.

A number of vibrational spectroscopic techniques are available For the study of surfaces, such as ATR, IR reflection-absorption, IR emission, etc. Infrared emission is hardly used, although interesting applications are possible now due to the high sensitivity of Fourier transform IR (FTIR) spectrometers. Two examples, where infrared emission measurements are very fruitful, will be given. One is the investigation of the curing behaviour of organic coatings, the other is the in situ study of heterogeneously catalyzed reactions. Undoubtedly, infrared emission measurements offer a number of specific advantages in some cases. Especially the less critical demands on the sample preparation are important.

Retrieval of total water vapour in the Arctic using microwave humidity sounders

Science.gov (United States)

Cristian Scarlat, Raul; Melsheimer, Christian; Heygster, Georg

2018-04-01

Quantitative retrievals of atmospheric water vapour in the Arctic present numerous challenges because of the particular climate characteristics of this area. Here, we attempt to build upon the work of Melsheimer and Heygster (2008) to retrieve total atmospheric water vapour (TWV) in the Arctic from satellite microwave radiometers. While the above-mentioned algorithm deals primarily with the ice-covered central Arctic, with this work we aim to extend the coverage to partially ice-covered and ice-free areas. By using modelled values for the microwave emissivity of the ice-free sea surface, we develop two sub-algorithms using different sets of channels that deal solely with open-ocean areas. The new algorithm extends the spatial coverage of the retrieval throughout the year but especially in the warmer months when higher TWV values are frequent. The high TWV measurements over both sea-ice and open-water surfaces are, however, connected to larger uncertainties as the retrieval values are close to the instrument saturation limits.This approach allows us to apply the algorithm to regions where previously no data were available and ensures a more consistent physical analysis of the satellite measurements by taking into account the contribution of the surface emissivity to the measured signal.

Microwave plasma induced surface modification of diamond-like carbon films

Science.gov (United States)

Rao Polaki, Shyamala; Kumar, Niranjan; Gopala Krishna, Nanda; Madapu, Kishore; Kamruddin, Mohamed; Dash, Sitaram; Tyagi, Ashok Kumar

2017-12-01

Tailoring the surface of diamond-like carbon (DLC) film is technically relevant for altering the physical and chemical properties, desirable for useful applications. A physically smooth and sp3 dominated DLC film with tetrahedral coordination was prepared by plasma-enhanced chemical vapor deposition technique. The surface of the DLC film was exposed to hydrogen, oxygen and nitrogen plasma for physical and chemical modifications. The surface modification was based on the concept of adsorption-desorption of plasma species and surface entities of films. Energetic chemical species of microwave plasma are adsorbed, leading to desorbtion of the surface carbon atoms due to energy and momentum exchange. The interaction of such reactive species with DLC films enhanced the roughness, surface defects and dangling bonds of carbon atoms. Adsorbed hydrogen, oxygen and nitrogen formed a covalent network while saturating the dangling carbon bonds around the tetrahedral sp3 valency. The modified surface chemical affinity depends upon the charge carriers and electron covalency of the adsorbed atoms. The contact angle of chemically reconstructed surface increases when a water droplet interacts either through hydrogen or van dear Waals bonding. These weak interactions influenced the wetting property of the DLC surface to a great extent.

Microwave plasma initiated graft copolymerization modification of monomers onto PTFE surface

International Nuclear Information System (INIS)

Guan Weishu; Wen Yunjian; Fang Yan; Yin Yongxiang

1996-02-01

A graft copolymerization modification technique of monomers onto polytetrafluoroethylene (PTFE) surface initiated by a 2.45 GHz non-equilibrium microwave plasma has been investigated. Standard X-Ray Photoelectron Spectroscopy (XPS), Attenuated Total Reflectance-Fourier Transform Infrared Spectroscopy (ATR-FTIR), Scanning Electron Microscopy (sEM) and wetting techniques were used for examination and analysis of samples. Considerable changes in chemical structure, composition and in morphology of grafted surface of PTFE were found. Results showed the occurrence of noticeable defluorination and cross-linked structure on grafted surface, and indicated that different kinds and contents of oxygen-containing functional groups were introduced into the surface of PTFE. Wetting and adhesion experiment of the sample proved that significant improvements in hydrophilicity and adhesion of surface were exhibited. These results confirmed the success of grafting. (8 refs., 7 figs., 1 tab.)

Fluxon induced resistance and field emission

CERN Document Server

Calatroni, Sergio; Darriulat, Pierre; Peck, M A; Valente, A M; Van't Hof, C A

2000-01-01

The surface resistance of superconducting niobium films induced by the presence of trapped magnetic flux, presumably in the form of a pinned fluxon lattice, is shown to be modified by the presence of a field emitting impurity or defect. The modification takes the form of an additional surface resistance proportional to the density of the fluxon lattice and increasing linearly with the amplitude of the microwave above a threshold significantly lower than the field emission threshold. Such an effect, precursor of electron emission, is observed here for the first time in a study using radiofrequency cavities operated at their fundamental 1.5 GHz frequency. The measured properties of the additional surface resistance severely constrain possible explanations of the observed effect.

Microwave-induced activation of additional active edge sites on the MoS2 surface for enhanced Hg0 capture

Science.gov (United States)

Zhao, Haitao; Mu, Xueliang; Yang, Gang; Zheng, Chengheng; Sun, Chenggong; Gao, Xiang; Wu, Tao

2017-10-01

In recent years, significant effort has been made in the development of novel materials for the removal of mercury from coal-derived flue gas. In this research, microwave irradiation was adopted to induce the creation of additional active sites on the MoS2 surface. The results showed that Hg0 capture efficiency of the adsorbent containing MoS2 nanosheets being microwave treated was as high as 97%, while the sample prepared via conventional method only showed an efficiency of 94% in its first 180 min testing. After the adsorbent was treated by microwave irradiation for 3 more times, its mercury removal efficiency was still noticeably higher than that of the sample prepared via conventional method. Characterization of surface structure of the MoS2 containing material together with DFT study further revealed that the (001) basal planes of MoS2 crystal structure were cracked into (100) edge planes (with an angle of approximately 75°) under microwave treatment, which subsequently resulted in the formation of additional active edge sites on the MoS2 surface and led to the improved performance on Hg0 capture.

Planck intermediate results XXXI. Microwave survey of Galactic supernova remnants

DEFF Research Database (Denmark)

Arnaud, M.; Ashdown, M.; Atrio-Barandela, F.

2016-01-01

The all-sky Planck survey in 9 frequency bands was used to search for emission from all 274 known Galactic supernova remnants. Of these, 16 were detected in at least two Planck frequencies. The radio-through-microwave spectral energy distributions were compiled to determine the mechanism for micr......The all-sky Planck survey in 9 frequency bands was used to search for emission from all 274 known Galactic supernova remnants. Of these, 16 were detected in at least two Planck frequencies. The radio-through-microwave spectral energy distributions were compiled to determine the mechanism...... for microwave emission. In only one case, IC 443, is there high-frequency emission clearly from dust associated with the supernova remnant. In all cases, the low-frequency emission is from synchrotron radiation. As predicted for a population of relativistic particles with energy distribution that extends...

Surface spectral emissivity derived from MODIS data

Science.gov (United States)

Chen, Yan; Sun-Mack, Sunny; Minnis, Patrick; Smith, William L.; Young, David F.

2003-04-01

Surface emissivity is essential for many remote sensing applications including the retrieval of the surface skin temperature from satellite-based infrared measurements, determining thresholds for cloud detection and for estimating the emission of longwave radiation from the surface, an important component of the energy budget of the surface-atmosphere interface. In this paper, data from the Terra MODIS (MODerate-resolution Imaging Spectroradiometer) taken at 3.7, 8.5, 10.8, 12.0 micron are used to simultaneously derive the skin temperature and the surface emissivities at the same wavelengths. The methodology uses separate measurements of the clear-sky temperatures that are determined by the CERES (Clouds and Earth's Radiant Energy System) scene classification in each channel during the daytime and at night. The relationships between the various channels at night are used during the day when solar reflectance affects the 3.7 micron data. A set of simultaneous equations is then solved to derive the emissivities. Global results are derived from MODIS. Numerical weather analyses are used to provide soundings for correcting the observed radiances for atmospheric absorption. These results are verified and will be available for remote sensing applications.

Microwave Radiometry in Remote Sensing

DEFF Research Database (Denmark)

Gudmandsen, Preben

1982-01-01

Microwave radiometry has shown its capabilities of observing and monitoring large-scale geophysical observables from space. Examples are sea surface temperature and surface wind over the ocean, sea ice extent, concentration and category and snow cover extent and water content. At low microwave fr...

Model of thermal fatigue of a copper surface under the action of high-power microwaves

Science.gov (United States)

Kuzikov, S. V.; Plotkin, M. E.

2007-10-01

The accelerating structures of modern supercolliders, as well as the components of high-power microwave electron devices operated in strong cyclic electromagnetic fields should have long lifetimes. Along with the electric breakdown, the surfaces of these microwave components deteriorate and their lifetimes decrease due to thermal strains and subsequent mechanical loads on the surface metal layer. The elementary theory of thermal fatigue was developed in the 1970s. In particular, a model of metal as a continuous medium was considered. Within the framework of this model, thermal fatigue is caused by the strains arising between the hot surface layer and the cold internal layer of the metal. However, this theory does not describe all the currently available experimental data. In particular, the notion of “safe temperature” of the heating, i.e., temperature at which the surface is not destroyed during an arbitrarily long series of pulses, which was proposed in the theoretical model, is in poor agreement with the experiment performed in the Stanford Linear Accelerator Center (SLAC, USA). In this work, the thermal-fatigue theory is developed on the basis of consideration of the copper polycrystalline structure. The necessity to take it into account was demonstrated by the results of the SLAC experiment, in which a change in the mutual orientation of copper grains and the formation of cracks at their boundaries was recorded for the first time. The developed theory makes it possible to use the experimental data to refine the coefficients in the obtained formulas for the lifetime of the metal surface and to predict the number of microwave pulses before its destruction as a function of the radiation power, the surface-temperature increase at the pulse peak, and the pulse duration.

Evolution of the near-UV emission spectrum associated with the reduction process in microwave iron making.

Science.gov (United States)

Matsubara, Akihiro; Takayama, Sadatsugu; Okajima, Shigeki; Sato, Motoyasu

2008-01-01

The structure of the emission spectrum in the near-UV range (240 nm-310 nm) changes drastically from the continuous spectrum to a discrete line spectrum with increasing sample temperature during the carbothermic reduction of magnetite in a 2.45 GHz microwave multimode furnace. The continuous spectrum can be assigned as a cathodoluminescence of magnetite. The dynamic evolution of the spectrum from continuous to discrete represents the progress of the reduction from magnetite to iron.

Design of a portable optical emission tomography system for microwave induced compact plasma for visible to near-infrared emission lines

Energy Technology Data Exchange (ETDEWEB)

Rathore, Kavita, E-mail: kavira@iitk.ac.in, E-mail: pmunshi@iitk.ac.in, E-mail: sudeepb@iitk.ac.in; Munshi, Prabhat, E-mail: kavira@iitk.ac.in, E-mail: pmunshi@iitk.ac.in, E-mail: sudeepb@iitk.ac.in [Nuclear Engineering and Technology Programme, Indian Institute of Technology Kanpur, Kanpur (India); Bhattacharjee, Sudeep, E-mail: kavira@iitk.ac.in, E-mail: pmunshi@iitk.ac.in, E-mail: sudeepb@iitk.ac.in [Department of Physics, Indian Institute of Technology Kanpur, Kanpur 208016 (India)

2016-03-15

A new non-invasive diagnostic system is developed for Microwave Induced Plasma (MIP) to reconstruct tomographic images of a 2D emission profile. A compact MIP system has wide application in industry as well as research application such as thrusters for space propulsion, high current ion beams, and creation of negative ions for heating of fusion plasma. Emission profile depends on two crucial parameters, namely, the electron temperature and density (over the entire spatial extent) of the plasma system. Emission tomography provides basic understanding of plasmas and it is very useful to monitor internal structure of plasma phenomena without disturbing its actual processes. This paper presents development of a compact, modular, and versatile Optical Emission Tomography (OET) tool for a cylindrical, magnetically confined MIP system. It has eight slit-hole cameras and each consisting of a complementary metal–oxide–semiconductor linear image sensor for light detection. The optical noise is reduced by using aspheric lens and interference band-pass filters in each camera. The entire cylindrical plasma can be scanned with automated sliding ring mechanism arranged in fan-beam data collection geometry. The design of the camera includes a unique possibility to incorporate different filters to get the particular wavelength light from the plasma. This OET system includes selected band-pass filters for particular argon emission 750 nm, 772 nm, and 811 nm lines and hydrogen emission H{sub α} (656 nm) and H{sub β} (486 nm) lines. Convolution back projection algorithm is used to obtain the tomographic images of plasma emission line. The paper mainly focuses on (a) design of OET system in detail and (b) study of emission profile for 750 nm argon emission lines to validate the system design.

Measurement of the sea surface wind speed and direction by an airborne microwave radar altimeter

Energy Technology Data Exchange (ETDEWEB)

Nekrassov, A. [GKSS-Forschungszentrum Geesthacht GmbH (Germany). Inst. fuer Hydrophysik

2001-07-01

A pilot needs operational information about wind over sea as well as wave height to provide safety of a hydroplane landing on water. Near-surface wind speed and direction can be obtained with an airborne microwave scatterometer, radar designed for measuring the scatter characteristics of a surface. Mostly narrow-beam antennas are applied for such wind measurement. Unfortunately, a microwave narrow-beam antenna has considerable size that hampers its placing on flying apparatus. In this connection, a possibility to apply a conventional airborne radar altimeter as a scatterometer with a nadir-looking wide-beam antenna in conjunction with Doppler filtering for recovering the wind vector over sea is discussed, and measuring algorithms of sea surface wind speed and direction are proposed. The obtained results can be used for creation of an airborne radar system for operational measurement of the sea roughness characteristics and for safe landing of a hydroplane on water. (orig.)

Investigation of graft copolymerization modification of PTFE surface using microwave plasma

International Nuclear Information System (INIS)

Wen Yunjian; Guan Weishu; Fang Yan; Ying Yongxiang

1995-03-01

Investigation of graft copolymerization modification of PTFE surface with kind of one or another reactive monomers was performed by using non-equilibrium microwave plasma at 2.45 GHz under various operating conditions. Untreated clean samples and grafted samples were examined and analyzed with different surface analytical techniques such as X-Ray Photoelectron Spectroscopy (XPS), Attenuated Total Reflectance-Fourier Transform Infrared Spectroscopy (ATR-FTIR) and Scanning Electron Microscopy (SEM). The results showed that the occurrence of noticeable de-fluorination and cross linking on grafted surface, and different polar groups and content of oxygen-containing were introduced into the grafted surface of PTFE. Fibriform hetero-structure layer was also formed. These results confirmed the success of graft and indicated that the hydrophilicity of the grafted surface is excellent and a significant improvement in adhesion characteristics has been achieved. The experiments revealed that the changes in surface properties are correlated closely to the changes in chemical structure, composition and morphology. (8 figs., 1 refs.)

The influence of microwave irradiation on rocks for microwave-assisted underground excavation

Directory of Open Access Journals (Sweden)

Ferri Hassani

2016-02-01

Full Text Available Demand is growing for explosive-free rock breakage systems for civil and mining engineering, and space industry applications. This paper highlights the work being undertaken in the Geomechanics Laboratory of McGill University to make a real application of microwave-assisted mechanical rock breakage to full-face tunneling machines and drilling. Comprehensive laboratory tests investigated the effect of microwave radiation on temperature profiles and strength reduction in hard rocks (norite, granite, and basalt for a range of exposure times and microwave power levels. The heating rate on the surface of the rock specimens linearly decreased with distance between the sample and the microwave antenna, regardless of microwave power level and exposure time. Tensile and uniaxial compressive strengths were reduced with increasing exposure time and power level. Scanning electron micrographs (SEMs highlighted fracture development in treated basalt. It was concluded that the microwave power level has a strong positive influence on the amount of heat damage induced to the rock surface. Numerical simulations of electric field intensity and wave propagation conducted with COMSOL Multiphysics® software generated temperature profiles that were in close agreement with experimental results.

Calibration of an integrated land surface process and radiobrightness (LSP/R) model during summertime

Science.gov (United States)

Judge, Jasmeet; England, Anthony W.; Metcalfe, John R.; McNichol, David; Goodison, Barry E.

2008-01-01

In this study, a soil vegetation and atmosphere transfer (SVAT) model was linked with a microwave emission model to simulate microwave signatures for different terrain during summertime, when the energy and moisture fluxes at the land surface are strong. The integrated model, land surface process/radiobrightness (LSP/R), was forced with weather and initial conditions observed during a field experiment. It simulated the fluxes and brightness temperatures for bare soil and brome grass in the Northern Great Plains. The model estimates of soil temperature and moisture profiles and terrain brightness temperatures were compared with the observed values. Overall, the LSP model provides realistic estimates of soil moisture and temperature profiles to be used with a microwave model. The maximum mean differences and standard deviations between the modeled and the observed temperatures (canopy and soil) were 2.6 K and 6.8 K, respectively; those for the volumetric soil moisture were 0.9% and 1.5%, respectively. Brightness temperatures at 19 GHz matched well with the observations for bare soil, when a rough surface model was incorporated indicating reduced dielectric sensitivity to soil moisture by surface roughness. The brightness temperatures of the brome grass matched well with the observations indicating that a simple emission model was sufficient to simulate accurate brightness temperatures for grass typical of that region and surface roughness was not a significant issue for grass-covered soil at 19 GHz. Such integrated SVAT-microwave models allow for direct assimilation of microwave observations and can also be used to understand sensitivity of microwave signatures to changes in weather forcings and soil conditions for different terrain types.

A semiconductor nanowire Josephson junction microwave laser

Science.gov (United States)

Cassidy, Maja; Uilhoorn, Willemijn; Kroll, James; de Jong, Damaz; van Woerkom, David; Nygard, Jesper; Krogstrup, Peter; Kouwenhoven, Leo

We present measurements of microwave lasing from a single Al/InAs/Al nanowire Josephson junction strongly coupled to a high quality factor superconducting cavity. Application of a DC bias voltage to the Josephson junction results in photon emission into the cavity when the bias voltage is equal to a multiple of the cavity frequency. At large voltage biases, the strong non-linearity of the circuit allows for efficient down conversion of high frequency microwave photons down to multiple photons at the fundamental frequency of the cavity. In this regime, the emission linewidth narrows significantly below the bare cavity linewidth to 50%. The junction-cavity coupling and laser emission can be tuned rapidly via an external gate, making it suitable to be integrated into a scalable qubit architecture as a versatile source of coherent microwave radiation. This work has been supported by the Netherlands Organisation for Scientific Research (NWO/OCW), Foundation for Fundamental Research on Matter (FOM), European Research Council (ERC), and Microsoft Corporation Station Q.

Electron emission during multicharged ion-metal surface interactions

International Nuclear Information System (INIS)

Zeijlmans van Emmichoven, P.A.; Havener, C.C.; Hughes, I.G.; Overbury, S.H.; Robinson, M.T.; Zehner, D.M.; Meyer, F.W.

1992-01-01

The electron emission during multicharged ion-metal surface interactions will be discussed. The interactions lead to the emission of a significant number of electrons. Most of these electrons have energies below 30 eV. For incident ions with innershell vacancies the emission of Auger electrons that fill these vacancies has been found to occur mainly below the surface. We will present recently measured electron energy distributions which will be used to discuss the mechanisms that lead to the emission of Auger and of low-energy electrons

Advances in microwaves 7

CERN Document Server

Young, Leo

2013-01-01

Advances in Microwaves, Volume 7 covers the developments in the study of microwaves. The book discusses the effect of surface roughness on the propagation of the TEM mode, as well as the voltage breakdown of microwave antennas. The text also describes the theory and design considerations of single slotted-waveguide linear arrays and the techniques and theories that led to the achievement of wide bandwidths and ultralow noise temperatures for communication applications. The book will prove invaluable to microwave engineers.

Recent Advancements in Microwave Imaging Plasma Diagnostics

International Nuclear Information System (INIS)

Park, H.; Chang, C.C.; Deng, B.H.; Domier, C.W.; Donni, A.J.H.; Kawahata, K.; Liang, C.; Liang, X.P.; Lu, H.J.; Luhmann, N.C. Jr.; Mase, A.; Matsuura, H.; Mazzucato, E.; Miura, A.; Mizuno, K.; Munsat, T.; Nagayama, K.; Nagayama, Y.; Pol, M.J. van de; Wang, J.; Xia, Z.G.; Zhang, W-K.

2002-01-01

Significant advances in microwave and millimeter wave technology over the past decade have enabled the development of a new generation of imaging diagnostics for current and envisioned magnetic fusion devices. Prominent among these are revolutionary microwave electron cyclotron emission imaging (ECEI), microwave phase imaging interferometers, imaging microwave scattering and microwave imaging reflectometer (MIR) systems for imaging electron temperature and electron density fluctuations (both turbulent and coherent) and profiles (including transport barriers) on toroidal devices such as tokamaks, spherical tori, and stellarators. The diagnostic technology is reviewed, and typical diagnostic systems are analyzed. Representative experimental results obtained with these novel diagnostic systems are also presented

Granularity effect on microwave surface resistance in high-Tc YBa2Cu3O7-x bulk and thin film superconductor

International Nuclear Information System (INIS)

Swarup, Ram; Gupta, A.K.

2001-01-01

We report the effect of variation of Josephson coupling strength in YBa 2 Cu 3 O 7-x (YBCO) superconductor due to grain enlargement, grain orientation and magnetic field on microwave surface resistance (R s ). The coupling strength in the bulk samples has been increased by increasing the sample density from 4.4 to 5.3 g/cm 3 , whereas in thin films, the same could be increased by increasing the c-axis orientation of the grains. The value of R s (10 GHz, 65 K) in bulk samples has been found to decrease from 52 to 4 mΩ with the increase of the coupling strength from 0.06 to 0.43 and in thin films from 930 to 600 μΩ with increase of the coupling strength from 0.92 to 2.43. The effect of grain decoupling on microwave surface resistance was studied under dc and microwave magnetic fields. The surface resistance increases gradually with the application of dc and microwave magnetic fields due to grain decoupling and finally gets saturated beyond a certain critical field. (author)

Surface renewal as a significant mechanism for dust emission

Directory of Open Access Journals (Sweden)

J. Zhang

2016-12-01

Full Text Available Wind tunnel experiments of dust emissions from different soil surfaces are carried out to better understand dust emission mechanisms. The effects of surface renewal on aerodynamic entrainment and saltation bombardment are analyzed in detail. It is found that flow conditions, surface particle motions (saltation and creep, soil dust content and ground obstacles all strongly affect dust emission, causing its rate to vary over orders of magnitude. Aerodynamic entrainment is highly effective, if dust supply is unlimited, as in the first 2–3 min of our wind tunnel runs. While aerodynamic entrainment is suppressed by dust supply limits, surface renewal through the motion of surface particles appears to be an effective pathway to remove the supply limit. Surface renewal is also found to be important to the efficiency of saltation bombardment. We demonstrate that surface renewal is a significant mechanism affecting dust emission and recommend that this mechanism be included in future dust models.

Evidence of Convective Redistribution of Carbon Monoxide in Aura Tropospheric Emission Sounder (TES) and Microwave Limb Sounder (MLS) Observations

Science.gov (United States)

Manyin, Michael; Douglass, Anne; Schoeberl, Mark

2010-01-01

Vertical convective transport is a key element of the tropospheric circulation. Convection lofts air from the boundary layer into the free troposphere, allowing surface emissions to travel much further, and altering the rate of chemical processes such as ozone production. This study uses satellite observations to focus on the convective transport of CO from the boundary layer to the mid and upper troposphere. Our hypothesis is that strong convection associated with high rain rate regions leads to a correlation between mid level and upper level CO amounts. We first test this hypothesis using the Global Modeling Initiative (GMI) chemistry and transport model. We find the correlation is robust and increases as the precipitation rate (the strength of convection) increases. We next examine three years of CO profiles from the Tropospheric Emission Sounder (TES) and Microwave Limb Sounder (MLS) instruments aboard EOS Aura. Rain rates are taken from the Tropical Rainfall Measuring Mission (TRMM) 3B-42 multi-satellite product. Again we find a correlation between mid-level and upper tropospheric CO, which increases with rain rate. Our result shows the critical importance of tropical convection in coupling vertical levels of the troposphere in the transport of trace gases. The effect is seen most clearly in strong convective regions such as the Inter-tropical Convergence Zone.

A bare ground evaporation revision in the ECMWF land-surface scheme: evaluation of its impact using ground soil moisture and satellite microwave data

Directory of Open Access Journals (Sweden)

C. Albergel

2012-10-01

Full Text Available In situ soil moisture data from 122 stations across the United States are used to evaluate the impact of a new bare ground evaporation formulation at ECMWF. In November 2010, the bare ground evaporation used in ECMWF's operational Integrated Forecasting System (IFS was enhanced by adopting a lower stress threshold than for the vegetation, allowing a higher evaporation. It results in more realistic soil moisture values when compared to in situ data, particularly over dry areas. Use was made of the operational IFS and offline experiments for the evaluation. The latter are based on a fixed version of the IFS and make it possible to assess the impact of a single modification, while the operational analysis is based on a continuous effort to improve the analysis and modelling systems, resulting in frequent updates (a few times a year. Considering the field sites with a fraction of bare ground greater than 0.2, the root mean square difference (RMSD of soil moisture is shown to decrease from 0.118 m³ m⁻³ to 0.087 m³ m⁻³ when using the new formulation in offline experiments, and from 0.110 m³ m⁻³ to 0.088 m³ m⁻³ in operations. It also improves correlations. Additionally, the impact of the new formulation on the terrestrial microwave emission at a global scale is investigated. Realistic and dynamically consistent fields of brightness temperature as a function of the land surface conditions are required for the assimilation of the SMOS data. Brightness temperature simulated from surface fields from two offline experiments with the Community Microwave Emission Modelling (CMEM platform present monthly mean differences up to 7 K. Offline experiments with the new formulation present drier soil moisture, hence simulated brightness temperature with its surface fields are larger. They are also closer to SMOS remotely sensed brightness temperature.

Phase 2 microwave concrete decontamination results

International Nuclear Information System (INIS)

White, T.L.; Foster, D. Jr.; Wilson, C.T.; Schaich, C.R.

1995-01-01

The authors report on the results of the second phase of a four-phase program at Oak Ridge National Laboratory to develop a system to decontaminate concrete using microwave energy. The microwave energy is directed at the concrete surface through the use of an optimized wave guide antenna, or applicator, and this energy rapidly heats the free water present in the interstitial spaces of the concrete matrix. The resulting steam pressure causes the surface to burst in much the same way popcorn pops in a home microwave oven. Each steam explosion removes several square centimeters of concrete surface that are collected by a highly integrated wave guide and vacuum system. The authors call this process the microwave concrete decontamination, or MCD, process. In the first phase of the program the principle of microwaves concrete removal concrete surfaces was demonstrated. In these experiments, concrete slabs were placed on a translator and moved beneath a stationary microwave system. The second phase demonstrated the ability to mobilize the technology to remove the surfaces from concrete floors. Area and volume concrete removal rates of 10.4 cm 2 /s and 4.9 cm 3 /S, respectively, at 18 GHz were demonstrated. These rates are more than double those obtained in Phase 1 of the program. Deeper contamination can be removed by using a longer residence time under the applicator to create multiple explosions in the same area or by taking multiple passes over previously removed areas. Both techniques have been successfully demonstrated. Small test sections of painted and oil-soaked concrete have also been removed in a single pass. Concrete with embedded metal anchors on the surface has also been removed, although with some increased variability of removal depth. Microwave leakage should not pose any operational hazard to personnel, since the observed leakage was much less than the regulatory standard

X-radiation /E greater than 10 keV/, H-alpha and microwave emission during the impulsive phase of solar flares.

Science.gov (United States)

Vorpahl, J. A.

1972-01-01

A study has been made of the variation in hard (E greater than 10 keV) X-radiation, H-alpha and microwave emission during the impulsive phase of solar flares. Analysis shows that the rise-time in the 20-30-keV X-ray spike depends on the electron hardness. The impulsive phase is also marked by an abrupt, very intense increase in H-alpha emission in one or more knots of the flare. Properties of these H-alpha kernels include: (1) a luminosity several times greater than the surrounding flare, (2) an intensity rise starting about 20-30 sec before, peaking about 20-25 sec after, and lasting about twice as long as the hard spike, (3) a location lower in the chromosphere than the remaining flare, (4) essentially no expansion prior to the hard spike, and (5) a position within 6000 km of the boundary separating polarities, usually forming on both sides of the neutral line near both feet of the same tube of force. Correspondingly, impulsive microwave events are characterized by: (1) great similarity in burst structure with 20-32 keV X-rays but only above 5000 MHz, (2) typical low frequency burst cutoff between 1400-3800 MHz, and (3) maximum emission above 7500 MHz.

The microwave and H-alpha sources of the 1992 January 13 flare

Science.gov (United States)

Wang, H.; Gary, D. E.; Zirin, H.; Kosugi, T.; Schwartz, R. A.; Linford, G.

1995-01-01

We compare X-ray, microwave and H-alpha observations for the 1992 January 13 limb flare. The soft and hard X-ray images of the flare have been studied thoroughly by Masuda et al. (1994) with Yohkoh SXT and HXT images. We find that during the hard X-ray emission peak there is no H-alpha brightening on the disk nor at the limb, so the main ribbons of this flare must be beyond the limb. The microwave source maintains a fixed distance about 10 arcsecs from the optical limb in the frequency range 2.8-14.0 GHz. We interpret this limit in source position as due to the presence of a microwave limb that extends higher than the white-light limb -- to a height of 7300 +/- 1500 km. We believe that the high-frequency microwave emissions are occulted by this extended limb, while the soft and hard X-ray emissions are able to pass through largely unaffected. We also believe, however, that the hard X-ray footpoints are also partially occulted by the photospheric limb, despite the appearance of 'footpoint sources' in HXT data shown by Masuda et al. The smooth X-ray and microwave time profiles, microwave-rich emission relative to hard X-rays, and progressive hard X-ray spectral hardening through the flare peak are all characteristics that we interpret as being a direct result of the occultation of footpoint emission.

[Experimental study on spectra of compressed air microwave plasma].

Science.gov (United States)

Liu, Yong-Xi; Zhang, Gui-Xin; Wang, Qiang; Hou, Ling-Yun

2013-03-01

Using a microwave plasma generator, compressed air microwave plasma was excited under 1 - 5 atm pressures. Under different pressures and different incident microwave power, the emission spectra of compressed air microwave plasma were studied with a spectra measuring system. The results show that continuum is significant at atmospheric pressure and the characteristic will be weakened as the pressure increases. The band spectra intensity will be reduced with the falling of the incident microwave power and the band spectra were still significant. The experimental results are valuable to studying the characteristics of compressed air microwave plasma and the generating conditions of NO active groups.

Effect of microwave (24 GHz) radiation treatment on impurity photoluminescence of CdTe:Cl single crystals

International Nuclear Information System (INIS)

Red'ko, R.A.; Budzulyak, S.I.; Vakhnyak, N.D.; Demchina, L.A.; Korbutyak, D.V.; Konakova, R.V.; Lotsko, A.P.; Okhrimenko, O.B.; Berezovskaya, N.I.; Bykov, Yu.V.; Egorov, S.V.; Eremeev, A.G.

2016-01-01

Effect of microwave radiation (24 GHz) on transformation of impurity-defect complexes in CdTe:Cl single crystals within the spectral range 1.3–1.5 eV was studied using the low-temperature (T=2 K) photoluminescence (PL) technique. The shapes of donor–acceptor pairs (DAP) and Y PL bands were studied in detail. The Huang–Rhys factor was calculated for the DAP luminescence depending on microwave radiation treatment. The increase of the distance between the DAP components responsible for emission at 1.455 eV and the quenching of Y-band due to microwave irradiation were observed. The method to decrease the amount of extended defects in near-surface layers of CdTe:Cl single crystals has been proposed.

Surface scanning through a cylindrical tank of coupling fluid for clinical microwave breast imaging exams

International Nuclear Information System (INIS)

Pallone, Matthew J.; Meaney, Paul M.; Paulsen, Keith D.

2012-01-01

Purpose: Microwave tomographic image quality can be improved significantly with prior knowledge of the breast surface geometry. The authors have developed a novel laser scanning system capable of accurately recovering surface renderings of breast-shaped phantoms immersed within a cylindrical tank of coupling fluid which resides completely external to the tank (and the aqueous environment) and overcomes the challenges associated with the optical distortions caused by refraction from the air, tank wall, and liquid bath interfaces. Methods: The scanner utilizes two laser line generators and a small CCD camera mounted concentrically on a rotating gantry about the microwave imaging tank. Various calibration methods were considered for optimizing the accuracy of the scanner in the presence of the optical distortions including traditional ray tracing and image registration approaches. In this paper, the authors describe the construction and operation of the laser scanner, compare the efficacy of several calibration methods—including analytical ray tracing and piecewise linear, polynomial, locally weighted mean, and thin-plate-spline (TPS) image registrations—and report outcomes from preliminary phantom experiments. Results: The results show that errors in calibrating camera angles and position prevented analytical ray tracing from achieving submillimeter accuracy in the surface renderings obtained from our scanner configuration. Conversely, calibration by image registration reliably attained mean surface errors of less than 0.5 mm depending on the geometric complexity of the object scanned. While each of the image registration approaches outperformed the ray tracing strategy, the authors found global polynomial methods produced the best compromise between average surface error and scanner robustness. Conclusions: The laser scanning system provides a fast and accurate method of three dimensional surface capture in the aqueous environment commonly found in microwave

Field emission from the surface of highly ordered pyrolytic graphite

Energy Technology Data Exchange (ETDEWEB)

Knápek, Alexandr, E-mail: knapek@isibrno.cz [Institute of Scientific Instruments of the ASCR, v.v.i., Královopolská 147, Brno (Czech Republic); Sobola, Dinara; Tománek, Pavel [Department of Physics, FEEC, Brno University of Technology, Technická 8, Brno (Czech Republic); Pokorná, Zuzana; Urbánek, Michal [Institute of Scientific Instruments of the ASCR, v.v.i., Královopolská 147, Brno (Czech Republic)

2017-02-15

Highlights: • HOPG shreds were created and analyzed in the UHV conditions. • Current-voltage measurements have been done to confirm electron tunneling, based on the Fowler-Nordheim theory. • Surface was characterized by other surface evaluation methods, in particular by: SNOM, SEM and AFM. - Abstract: This paper deals with the electrical characterization of highly ordered pyrolytic graphite (HOPG) surface based on field emission of electrons. The effect of field emission occurs only at disrupted surface, i.e. surface containing ripped and warped shreds of the uppermost layers of graphite. These deformations provide the necessary field gradients which are required for measuring tunneling current caused by field electron emission. Results of the field emission measurements are correlated with other surface characterization methods such as scanning near-field optical microscopy (SNOM) or atomic force microscopy.

Field emission from the surface of highly ordered pyrolytic graphite

International Nuclear Information System (INIS)

Knápek, Alexandr; Sobola, Dinara; Tománek, Pavel; Pokorná, Zuzana; Urbánek, Michal

2017-01-01

Highlights: • HOPG shreds were created and analyzed in the UHV conditions. • Current-voltage measurements have been done to confirm electron tunneling, based on the Fowler-Nordheim theory. • Surface was characterized by other surface evaluation methods, in particular by: SNOM, SEM and AFM. - Abstract: This paper deals with the electrical characterization of highly ordered pyrolytic graphite (HOPG) surface based on field emission of electrons. The effect of field emission occurs only at disrupted surface, i.e. surface containing ripped and warped shreds of the uppermost layers of graphite. These deformations provide the necessary field gradients which are required for measuring tunneling current caused by field electron emission. Results of the field emission measurements are correlated with other surface characterization methods such as scanning near-field optical microscopy (SNOM) or atomic force microscopy.

Microwave Resonators and Filters

Science.gov (United States)

2015-12-22

1 Microwave Resonators and Filters Daniel E. Oates MIT Lincoln Laboratory 244 Wood St. Lexington, MA 02478 USA Email: oates@ll.mit.edu...explained in other chapters, the surface resistance of superconductors at microwave frequencies can be as much as three orders of magnitude lower than the...resonators and filters in the first edition of this handbook (Z.-Y. Shen 2003) discussed the then state of the art of microwave frequency applications

The microwave surface impedance of MgB2 thin films

International Nuclear Information System (INIS)

Purnell, A J; Zhukov, A A; Nurgaliev, T; Lamura, G; Bugoslavsky, Y; Lockman, Z; MacManus-Driscoll, J L; Zhai, H Y; Christen, H M; Paranthaman, M P; Lowndes, D H; Jo, M H; Blamire, M G; Hao, Ling; Gallop, J C; Cohen, L F

2003-01-01

In this paper we present the results of measurements of the microwave surface impedance of a powder sample and two films of MgB 2 . The powder sample has a T c = 39 K and the films have T c = 29 K and 38 K. These samples show different temperature dependences of the field penetration depth. Over a period of six months, the film with T c = 38 K degraded to a T c of 35 K. We compare the results on all samples with data obtained elsewhere and discuss the implications as far as is possible at this stage

Application of response surface methodology for optimization of parameters for microwave heating of rare earth carbonates

Science.gov (United States)

Yin, Shaohua; Lin, Guo; Li, Shiwei; Peng, Jinhui; Zhang, Libo

2016-09-01

Microwave heating has been applied in the field of drying rare earth carbonates to improve drying efficiency and reduce energy consumption. The effects of power density, material thickness and drying time on the weight reduction (WR) are studied using response surface methodology (RSM). The results show that RSM is feasible to describe the relationship between the independent variables and weight reduction. Based on the analysis of variance (ANOVA), the model is in accordance with the experimental data. The optimum experiment conditions are power density 6 w/g, material thickness 15 mm and drying time 15 min, resulting in an experimental weight reduction of 73%. Comparative experiments show that microwave drying has the advantages of rapid dehydration and energy conservation. Particle analysis shows that the size distribution of rare earth carbonates after microwave drying is more even than those in an oven. Based on these findings, microwave heating technology has an important meaning to energy-saving and improvement of production efficiency for rare earth smelting enterprises and is a green heating process.

Microwave power coupling in a surface wave excited plasma

Directory of Open Access Journals (Sweden)

Satyananda Kar

2015-01-01

Full Text Available In recent decades, different types of plasma sources have been used for various types of plasma processing, such as, etching and thin film deposition. The critical parameter for effective plasma processing is high plasma density. One type of high density plasma source is Microwave sheath-Voltage combination Plasma (MVP. In the present investigation, a better design of MVP source is reported, in which over-dense plasma is generated for low input microwave powers. The results indicate that the length of plasma column increases significantly with increase in input microwave power.

Photoinduced spin polarization and microwave technology

International Nuclear Information System (INIS)

Antipov, Sergey; Poluektov, Oleg; Schoessow, Paul; Kanareykin, Alexei; Jing, Chunguang

2013-01-01

We report here on studies of optically pumped active microwave media based on various fullerene derivatives, with an emphasis on the use of these materials in microwave electronics. We have investigated a class of optically excited paramagnetic materials that demonstrate activity in the X-band as candidate materials. We found that a particular fullerene derivative, Phenyl-C 61 -butyric acid methyl ester (PCBM), produced the largest electron paramagnetic resonance (EPR) emission signal compared to other organic compounds that have been suggested for use as microwave active materials. We also studied the effects of concentration, temperature, solvent etc. on the activity of the material. In these experiments, EPR studies using a commercial spectrometer were followed up by measurements of an RF signal reflected from a resonator loaded with the PCBM-based material. The activity was directly demonstrated through the change in the quality factor and RF coupling between the resonator and waveguide feed. At the inception of these experiments the primary interest was the development of a microwave PASER. The PASER (particle acceleration by stimulated emission of radiation [1]) is a novel acceleration concept that is based on the direct energy transfer from an active medium to a charged particle beam. While the previous work on the PASER has emphasized operations at infrared or visible wavelengths, operating in the microwave regime has significant advantages in terms of the less stringent quality requirements placed on the electron beam provided an appropriate microwave active medium can be found. This paper is focused on our investigation of the possibility of a PASER operating in the microwave frequency regime [2] using active paramagnetic materials. While a high level of gain for PCBM was demonstrated compared to other candidate materials, dielectric losses and quenching effects were found to negatively impact its performance for PASER applications. We present results on

Great microwave bursts and hard X-rays from solar flares

International Nuclear Information System (INIS)

Wiehl, H.J.; Batchelor, D.A.; Crannell, C.J.; Dennis, B.R.; Price, P.N.

1983-06-01

The microwave and hard X-ray charateristics of 13 solar flares that produced microwave fluxes greater than 500 Solar Flux Units were analyzed. These Great Microwave Bursts were observed in the frequency range from 3 to 35 GHz at Berne, and simultaneous hard X-ray observations were made in the energy range from 30 to 500 keV with the Hard X-Ray Burst Spectrometer on the Solar Maximum Mission spacecraft. The principal aim of this analysis is to determine whether or not the same distribution of energetic electrons can explain both emissions. Correlations were found between respective temporal characteristics and, for the first time, between microwave and hard X-ray spectral characteristics. A single-temperature and a multi-temperature model from the literature were tested for consistency with the coincident X-ray and microwave spectra at microwave burst maximum. Four events are inconsistent with both of the models tested, and neither of the models attempts to explain the high-frequency part of the microwave spectrum. A model in which the emissions above and below the peak frequency originate in two different parts of a diverging magnetic loop is proposed. With this model the entire microwave spectrum of all but one of the events is explained

Optical emission spectroscopy for quantification of ultraviolet radiations and biocide active species in microwave argon plasma jet at atmospheric pressure

Energy Technology Data Exchange (ETDEWEB)

Wattieaux, G., E-mail: gaetan.wattieaux@laplace.univ-tlse.fr; Yousfi, M.; Merbahi, N.

2013-11-01

This work deals with absorption and mainly emission spectrometry of a microwave induced surfatron plasma jet launched in ambient air and using an Argon flow carrier gas. The Ar flow rate varies between 1 and 3 L/min and the microwave power between 40 and 60 W. The analysis of the various spectra has led to the determination of the ozone and atomic oxygen concentrations, ultraviolet (UV) irradiance separating UVA, UVB and UVC, gas temperature, plasma electron density and excitation temperature. Most of these diagnostics are spatially resolved along the plasma jet axis. It is shown more particularly that rotational temperature obtained from OH(A-X) spectra ranges between 800 K to 1000 K while the apparent temperature of the plasma jet remains lower than about 325 K which is compatible with biocide treatment without significant thermal effect. The electron density reaches 1.2 × 10{sup 14} cm{sup −3}, the excitation temperature is about 4000 K, the UVC radiation represents only 5% of the UV radiations emitted by the device, the ozone concentration is found to reach 88 ± 27 ppm in the downstream part of the plasma jet at a distance of 30 mm away from the quartz tube outlet of the surfatron and the atomic oxygen concentration lies between 10 and 80 ppm up to a distance of 20 mm away from the quartz tube outlet. Ozone is identified as the main germicidal active species produced by the device since its concentration is in accordance with bacteria inactivation durations usually reported using such plasma devices. Human health hazard assessment is carried out all along this study since simple solutions are reminded to respect safety standards for exposures to ozone and microwave leakage. In this study, an air extraction unit is used and a Faraday cage is set around the quartz tube of the surfatron and the plasma jet. These solutions should be adopted by users of microwave induced plasma in open air conditions because according to the literature, this is not often the

Optical emission spectroscopy for quantification of ultraviolet radiations and biocide active species in microwave argon plasma jet at atmospheric pressure

International Nuclear Information System (INIS)

Wattieaux, G.; Yousfi, M.; Merbahi, N.

2013-01-01

This work deals with absorption and mainly emission spectrometry of a microwave induced surfatron plasma jet launched in ambient air and using an Argon flow carrier gas. The Ar flow rate varies between 1 and 3 L/min and the microwave power between 40 and 60 W. The analysis of the various spectra has led to the determination of the ozone and atomic oxygen concentrations, ultraviolet (UV) irradiance separating UVA, UVB and UVC, gas temperature, plasma electron density and excitation temperature. Most of these diagnostics are spatially resolved along the plasma jet axis. It is shown more particularly that rotational temperature obtained from OH(A-X) spectra ranges between 800 K to 1000 K while the apparent temperature of the plasma jet remains lower than about 325 K which is compatible with biocide treatment without significant thermal effect. The electron density reaches 1.2 × 10 14 cm −3 , the excitation temperature is about 4000 K, the UVC radiation represents only 5% of the UV radiations emitted by the device, the ozone concentration is found to reach 88 ± 27 ppm in the downstream part of the plasma jet at a distance of 30 mm away from the quartz tube outlet of the surfatron and the atomic oxygen concentration lies between 10 and 80 ppm up to a distance of 20 mm away from the quartz tube outlet. Ozone is identified as the main germicidal active species produced by the device since its concentration is in accordance with bacteria inactivation durations usually reported using such plasma devices. Human health hazard assessment is carried out all along this study since simple solutions are reminded to respect safety standards for exposures to ozone and microwave leakage. In this study, an air extraction unit is used and a Faraday cage is set around the quartz tube of the surfatron and the plasma jet. These solutions should be adopted by users of microwave induced plasma in open air conditions because according to the literature, this is not often the case

First detection of nonflare microwave emissions from the coronae of single late-type dwarf stars

Science.gov (United States)

Gary, D. E.; Linsky, J. L.

1981-01-01

Results are presented of a search for nonflare microwave radiation from the coronae of nearby late-type dwarf stars comparable to the sun: single stars without evidence for either a large wind or circumstellar envelope. The observing program consisted of flux measurements of six stars over a 24-h period with the VLA in the C configuration at a wavelength of 6 cm with 50 MHz bandwidth. Positive detections at 6 cm were made for Chi 1 Ori (0.6 mJy) and the flare star UV Cet (1.55 mJy), and upper limits were obtained for the stars Pi 1 UMa, Xi Boo A, 70 Oph A and Epsilon Eri. It is suggested that Chi 1 Ori, and possibly UV Cet, represent the first detected members of a new class of radio sources which are driven by gyroresonance emission, i.e. cyclotron emission from nonrelativistic Maxwellian electrons.

Response surface methodology applied to the study of the microwave-assisted synthesis of quaternized chitosan.

Science.gov (United States)

dos Santos, Danilo Martins; Bukzem, Andrea de Lacerda; Campana-Filho, Sérgio Paulo

2016-03-15

A quaternized derivative of chitosan, namely N-(2-hydroxy)-propyl-3-trimethylammonium chitosan chloride (QCh), was synthesized by reacting glycidyltrimethylammonium chloride (GTMAC) and chitosan (Ch) in acid medium under microwave irradiation. Full-factorial 2(3) central composite design and response surface methodology (RSM) were applied to evaluate the effects of molar ratio GTMAC/Ch, reaction time and temperature on the reaction yield, average degree of quaternization (DQ) and intrinsic viscosity ([η]) of QCh. The molar ratio GTMAC/Ch was the most important factor affecting the response variables and RSM results showed that highly substituted QCh (DQ = 71.1%) was produced at high yield (164%) when the reaction was carried out for 30min. at 85°C by using molar ratio GTMAC/Ch 6/1. Results showed that microwave-assisted synthesis is much faster (≤30min.) as compared to conventional reaction procedures (>4h) carried out in similar conditions except for the use of microwave irradiation. Copyright © 2015 Elsevier Ltd. All rights reserved.

A LAST LOOK AT THE MICROWAVE HAZE/BUBBLES WITH WMAP

Energy Technology Data Exchange (ETDEWEB)

Dobler, Gregory, E-mail: dobler@kitp.ucsb.edu [Kavli Institute for Theoretical Physics, University of California, Santa Barbara Kohn Hall, Santa Barbara, CA 93106 (United States)

2012-05-01

The microwave 'haze' was first discovered with the initial release of the full sky data from the Wilkinson Microwave Anisotropy Probe (WMAP). It is diffuse emission toward the center of our Galaxy with spectral behavior that makes it difficult to categorize as any of the previously known emission mechanisms at those wavelengths. With now seven years of WMAP data publicly available, we have learned much about the nature of the haze, and with the release of data from the Fermi Gamma-Ray Space Telescope and the discovery of the gamma-ray haze/bubbles, we have had a spectacular confirmation of its existence at other wavelengths. As the WMAP mission winds down and the Planck mission prepares to release data, I take a last look at what WMAP has to tell us about the origin of this unique Galactic feature. Much like the gamma rays, the microwave haze/bubbles is/are elongated in latitude with respect to longitude by a factor of roughly two, and at high latitudes, the microwave emission cuts off sharply above {approx}35 Degree-Sign (compared to {approx}50 Degree-Sign in the gammas). The hard spectrum of electrons required to generate the microwave synchrotron is consistent with that required to generate gamma-ray emission via inverse Compton scattering, though it is likely that these signals result from distinct regions of the spectrum ({approx}10 GeV for the microwaves and {approx}1 TeV for the gammas). While there is no evidence for significant haze polarization in the seven-year WMAP data, I demonstrate explicitly that it is unlikely such a signal would be detectable above the noise.

Prediction of Backscatter and Emissivity of Snow at Millimeter Wavelengths.

Science.gov (United States)

1980-01-01

AD-AI16 9A MASSACHUISETTS IMST OF TECH CAMBRIDGE RESEARCH LAB OF-ETC F/6 17/9 PREDICTION OF BACKSCATTER AND EMISSIVITY OF SNOW AT MILLETER --ETC(U...emitting media such as snow. The emissivity in the Ray- leigh- Jeans approximation is then the microwave brightness tempera- ture T divided by an effective...resistivity, and thermal tempera- ture. Jean et al. (Reference 125) compared a theoretical expression for the total apparent temperature of a smooth surface

The Barrier Properties of PET Coated DLC Film Deposited by Microwave Surface-Wave PECVD

Science.gov (United States)

Yin, Lianhua; Chen, Qiang

2017-12-01

In this paper we report the investigation of diamond-like carbon (DLC) deposited by microwave surface-wave plasma enhanced chemical vapor deposition (PECVD) on the polyethylene terephthalate (PET) web for the purpose of the barrier property improvement. In order to characterize the properties of DLC coatings, we used several substrates, silicon wafer, glass, and PET web and KBr tablet. The deposition rate was obtained by surface profiler based on the DLC deposited on glass substrates; Fourier transform infrared spectroscope (FTIR) was carried out on KBr tablets to investigate chemical composition and bonding structure; the morphology of the DLC coating was analyzed by atomic force microscope (AFM) on Si substrates. For the barrier properties of PET webs, we measured the oxygen transmission rate (OTR) and water vapor transmission rate (WVTR) after coated with DLC films. We addressed the film barrier property related to process parameters, such as microwave power and pulse parameter in this work. The results show that the DLC coatings can greatly improve the barrier properties of PET webs.

Microwave radiometric measurements of soil moisture in Italy

Directory of Open Access Journals (Sweden)

G. Macelloni

2003-01-01

Full Text Available Within the framework of the MAP and RAPHAEL projects, airborne experimental campaigns were carried out by the IFAC group in 1999 and 2000, using a multifrequency microwave radiometer at L, C and X bands (1.4, 6.8 and 10 GHz. The aim of the experiments was to collect soil moisture and vegetation biomass information on agricultural areas to give reliable inputs to the hydrological models. It is well known that microwave emission from soil, mainly at L-band (1.4 GHz, is very well correlated to its moisture content. Two experimental areas in Italy were selected for this project: one was the Toce Valley, Domodossola, in 1999, and the other, the agricultural area of Cerbaia, close to Florence, where flights were performed in 2000. Measurements were carried out on bare soils, corn and wheat fields in different growth stages and on meadows. Ground data of soil moisture (SMC were collected by other research teams involved in the experiments. From the analysis of the data sets, it has been confirmed that L-band is well related to the SMC of a rather deep soil layer, whereas C-band is sensitive to the surface SMC and is more affected by the presence of surface roughness and vegetation, especially at high incidence angles. An algorithm for the retrieval of soil moisture, based on the sensitivity to moisture of the brightness temperature at C-band, has been tested using the collected data set. The results of the algorithm, which is able to correct for the effect of vegetation by means of the polarisation index at X-band, have been compared with soil moisture data measured on the ground. Finally, the sensitivity of emission at different frequencies to the soil moisture profile was investigated. Experimental data sets were interpreted by using the Integral Equation Model (IEM and the outputs of the model were used to train an artificial neural network to reproduce the soil moisture content at different depths. Keywords: microwave radiometry, soil moisture

Microwave Plasma System: PVA Tepla 300

Data.gov (United States)

Federal Laboratory Consortium — Description:CORAL Name: Microwave AsherA tool using microwave oxygen plasma to remove organics on the surfacesSpecifications / Capabilities:Frequency: 2.45 GHzPower:...

Comparing land surface phenology derived from satellite and GPS network microwave remote sensing.

Science.gov (United States)

Jones, Matthew O; Kimball, John S; Small, Eric E; Larson, Kristine M

2014-08-01

The land surface phenology (LSP) start of season (SOS) metric signals the seasonal onset of vegetation activity, including canopy growth and associated increases in land-atmosphere water, energy and carbon (CO2) exchanges influencing weather and climate variability. The vegetation optical depth (VOD) parameter determined from satellite passive microwave remote sensing provides for global LSP monitoring that is sensitive to changes in vegetation canopy water content and biomass, and insensitive to atmosphere and solar illumination constraints. Direct field measures of canopy water content and biomass changes desired for LSP validation are generally lacking due to the prohibitive costs of maintaining regional monitoring networks. Alternatively, a normalized microwave reflectance index (NMRI) derived from GPS base station measurements is sensitive to daily vegetation water content changes and may provide for effective microwave LSP validation. We compared multiyear (2007-2011) NMRI and satellite VOD records at over 300 GPS sites in North America, and their derived SOS metrics for a subset of 24 homogenous land cover sites to investigate VOD and NMRI correspondence, and potential NMRI utility for LSP validation. Significant correlations (P<0.05) were found at 276 of 305 sites (90.5 %), with generally favorable correspondence in the resulting SOS metrics (r (2)=0.73, P<0.001, RMSE=36.8 days). This study is the first attempt to compare satellite microwave LSP metrics to a GPS network derived reflectance index and highlights both the utility and limitations of the NMRI data for LSP validation, including spatial scale discrepancies between local NMRI measurements and relatively coarse satellite VOD retrievals.

Joining of thermoplastic substrates by microwaves

Science.gov (United States)

Paulauskas, Felix L.; Meek, Thomas T.

1997-01-01

A method for joining two or more items having surfaces of thermoplastic material includes the steps of depositing an electrically-conductive material upon the thermoplastic surface of at least one of the items, and then placing the other of the two items adjacent the one item so that the deposited material is in intimate contact with the surfaces of both the one and the other items. The deposited material and the thermoplastic surfaces contacted thereby are then exposed to microwave radiation so that the thermoplastic surfaces in contact with the deposited material melt, and then pressure is applied to the two items so that the melted thermoplastic surfaces fuse to one another. Upon discontinuance of the exposure to the microwave energy, and after permitting the thermoplastic surfaces to cool from the melted condition, the two items are joined together by the fused thermoplastic surfaces. The deposited material has a thickness which is preferably no greater than a skin depth, .delta..sub.s, which is related to the frequency of the microwave radiation and characteristics of the deposited material in accordance with an equation.

Non-self-sustained microwave discharge and the concept of a microwave air jet engine

International Nuclear Information System (INIS)

Batanov, G M; Gritsinin, S I; Kossyi, I A

2002-01-01

A new type of microwave discharge - near-surface non-self-sustained discharge (NSND) - has been realized and investigated. A physical model of this discharge is presented. For the first time NSND application for microwave air jet engines has been proposed. Measurements under laboratory conditions modelling the microwave air jet engine operation shows the qualitative agreement between the model of NSND and actual processes near the target irradiated by a powerful microwave beam. Characteristic dependences of recoil momentum of target on the background pressure and microwave pulse duration obtained in experiments are presented. Measured cost of thrust produced by the NSND is no more than 3.0 kW N -1 , which is close to the predicted values

[Study on friction and wear properties of dental zirconia ceramics processed by microwave and conventional sintering methods].

Science.gov (United States)

Guoxin, Hu; Ying, Yang; Yuemei, Jiang; Wenjing, Xia

2017-04-01

This study evaluated the wear of an antagonist and friction and wear properties of dental zirconia ceramic that was subjected to microwave and conventional sintering methods. Ten specimens were fabricated from Lava brand zirconia and randomly assigned to microwave and conventional sintering groups. A profile tester for surface roughness was used to measure roughness of the specimens. Wear test was performed, and steatite ceramic was used as antagonist. Friction coefficient curves were recorded, and wear volume were calculated. Finally, optical microscope was used to observe the surface morphology of zirconia and steatite ceramics. Field emission scanning electron microscopy was used to observe the microstructure of zirconia. Wear volumes of microwave and conventionally sintered zirconia were (6.940±1.382)×10⁻², (7.952±1.815) ×10⁻² mm³, respectively. Moreover, wear volumes of antagonist after sintering by the considered methods were (14.189±4.745)×10⁻², (15.813±3.481)×10⁻² mm³, correspondingly. Statistically significant difference was not observed in the wear resistance of zirconia and wear volume of steatite ceramic upon exposure to two kinds of sintering methods. Optical microscopy showed that ploughed surfaces were apparent in zirconia. The wear surface of steatite ceramic against had craze, accompanied by plough. Scanning electron microscopy showed that zirconia was sintered compactly when subjected to both conventional sintering and microwave methods, whereas grains of zirconia sintered by microwave alone were smaller and more uniform. Two kinds of sintering methods are successfully used to produce dental zirconia ceramics with similar friction and wear properties.
.

Microwave surface resistance of YBa2Cu3O/sub 6.9/ superconducting films

International Nuclear Information System (INIS)

Martens, J.S.; Beyer, J.B.; Ginley, D.S.

1988-01-01

The microwave surface resistance of an YBa 2 Cu 3 O/sub 6.9/ superconducting thick film was measured over the range 7.0--16.7 GHz at 77 K. This was done by placing a sample in a TE 01 /sub n/ wavemeter cavity and observing the change in selectivity of the cavity. The material's surface resistance is of the same order of magnitude as that of silver at 77 K from 8 to 12 GHz and improves about another order at 4.2 K. The power-law behavior of surface resistance with frequency is probably close to quadratic. This is similar to the behavior of low critical temperature superconductors

Current in heavy-current planar diode with discrete emission surface

International Nuclear Information System (INIS)

Belomyttsev, S.Ya.; Korovin, S.D.; Pegel', I.V

1999-01-01

Dependence of current in a high-current planar diode on the size of emission centres was studied. Essential effect of emission surface microstructure on the current value in the planar diode was demonstrated. It was determined that if the distance between the emitter essentially exceeded their size then current dependence on the ratio of size to the value of the diode gap was an exponential function with 3/2 index. Current dependence on voltage obeyed the exponential law with 3/2 index up to higher voltage values in the planar diode with discrete emission surface in contrast to the case of a planar diode with homogeneous emission surface [ru

Use of microwave remote sensing in salinity estimation

International Nuclear Information System (INIS)

Singh, R.P.; Kumar, V.; Srivastav, S.K.

1990-01-01

Soil-moisture interaction and the consequent liberation of ions causes the salinity of waters. The salinity of river, lake, ocean and ground water changes due to seepage and surface runoff. We have studied the feasibility of using microwave remote sensing for the estimation of salinity by carrying out numerical calculations to study the microwave remote sensing responses of various models representative of river, lake and ocean water. The results show the dependence of microwave remote sensing responses on the salinity and surface temperature of water. The results presented in this paper will be useful in the selection of microwave sensor parameters and in the accurate estimation of salinity from microwave remote sensing data

Induction of stress volatiles and changes in essential oil content and composition upon microwave exposure in the aromatic plant Ocimum basilicum

Energy Technology Data Exchange (ETDEWEB)

Lung, Ildikó [National Institute for Research and Development of Isotopic and Molecular Technologies, 67-103 Donat Street, Cluj-Napoca 400293 (Romania); Soran, Maria-Loredana, E-mail: loredana.soran@itim-cj.ro [National Institute for Research and Development of Isotopic and Molecular Technologies, 67-103 Donat Street, Cluj-Napoca 400293 (Romania); Opriş, Ocsana; Truşcă, Mihail Radu Cătălin [National Institute for Research and Development of Isotopic and Molecular Technologies, 67-103 Donat Street, Cluj-Napoca 400293 (Romania); Niinemets, Ülo [Institute of Agricultural and Environmental Sciences, Estonian University of Life Sciences, 1 Kreutzwaldi Street, Tartu 51014 (Estonia); Copolovici, Lucian [Institute of Agricultural and Environmental Sciences, Estonian University of Life Sciences, 1 Kreutzwaldi Street, Tartu 51014 (Estonia); Institute of Technical and Natural Sciences Research-Development of “Aurel Vlaicu” University, 2 Elena Drăgoi Street, Arad 310330 (Romania)

2016-11-01

Exposure to sustained low intensity microwaves can constitute a stress for the plants, but its effects on plant secondary chemistry are poorly known. We studied the influence of GSM and WLAN-frequency microwaves on emissions of volatile organic compounds and content of essential oil in the aromatic plant Ocimum basilicum L. hypothesizing that microwave exposure leads to enhanced emissions of stress volatiles and overall greater investment in secondary compounds. Compared to the control plants, microwave irradiation led to decreased emissions of β-pinene, α-phellandrene, bornyl acetate, β-myrcene, α-caryophyllene and benzaldehyde, but increased emissions of eucalyptol, estragole, caryophyllene oxide, and α-bergamotene. The highest increase in emission, 21 times greater compared to control, was observed for caryophyllene oxide. The irradiation resulted in increases in the essential oil content, except for the content of phytol which decreased by 41% in the case of GSM-frequency, and 82% in the case of WLAN-frequency microwave irradiation. The strongest increase in response to WLAN irradiation, > 17 times greater, was observed for hexadecane and octane contents. Comparisons of volatile compositions by multivariate analyses demonstrated a clear separation of different irradiance treatments, and according to the changes in the volatile emissions, the WLAN-frequency irradiation represented a more severe stress than the GSM-frequency irradiation. Overall, these results demonstrating important modifications in the emission rates, essential oil content and composition indicate that microwave irradiation influences the quality of herbage of this economically important spice plant. - Highlights: • Microwave irradiation represents a stress for the plants. • Microwave exposure leads to enhanced emissions of stress volatiles. • O. basilicum irradiation with microwaves increases the essential oil content. • Microwave pollution can constitute a threat to the

Induction of stress volatiles and changes in essential oil content and composition upon microwave exposure in the aromatic plant Ocimum basilicum

International Nuclear Information System (INIS)

Lung, Ildikó; Soran, Maria-Loredana; Opriş, Ocsana; Truşcă, Mihail Radu Cătălin; Niinemets, Ülo; Copolovici, Lucian

2016-01-01

Exposure to sustained low intensity microwaves can constitute a stress for the plants, but its effects on plant secondary chemistry are poorly known. We studied the influence of GSM and WLAN-frequency microwaves on emissions of volatile organic compounds and content of essential oil in the aromatic plant Ocimum basilicum L. hypothesizing that microwave exposure leads to enhanced emissions of stress volatiles and overall greater investment in secondary compounds. Compared to the control plants, microwave irradiation led to decreased emissions of β-pinene, α-phellandrene, bornyl acetate, β-myrcene, α-caryophyllene and benzaldehyde, but increased emissions of eucalyptol, estragole, caryophyllene oxide, and α-bergamotene. The highest increase in emission, 21 times greater compared to control, was observed for caryophyllene oxide. The irradiation resulted in increases in the essential oil content, except for the content of phytol which decreased by 41% in the case of GSM-frequency, and 82% in the case of WLAN-frequency microwave irradiation. The strongest increase in response to WLAN irradiation, > 17 times greater, was observed for hexadecane and octane contents. Comparisons of volatile compositions by multivariate analyses demonstrated a clear separation of different irradiance treatments, and according to the changes in the volatile emissions, the WLAN-frequency irradiation represented a more severe stress than the GSM-frequency irradiation. Overall, these results demonstrating important modifications in the emission rates, essential oil content and composition indicate that microwave irradiation influences the quality of herbage of this economically important spice plant. - Highlights: • Microwave irradiation represents a stress for the plants. • Microwave exposure leads to enhanced emissions of stress volatiles. • O. basilicum irradiation with microwaves increases the essential oil content. • Microwave pollution can constitute a threat to the

Electron emission during multicharged ion-surface interactions

International Nuclear Information System (INIS)

Zeijlmans van Emmichoven, P.A.; Havener, C.C.; Meyer, F.W.; Zehner, D.M.

1990-01-01

Recent measurements of electron spectra for slow multicharged N ion-surface collisions are presented. The emphasis is on potential emission, i.e. the electron emission related to the neutralization of the ions. When using N ions that carry a K shell vacancy into the collision, characteristic K Auger electron emission from the projectiles is observed, as well as, for specific surfaces, target atom Auger transitions (resulting from vacancy transfer). Measurements of the intensity of these Auger transitions as a function of the time the ions spend above the surface can serve as a useful probe of the timescales characterizing the relevant neutralization processes. This technique is elucidated with the help of some computer simulations. It is shown that neutralization timescales required in the atomic ladder picture, in which neutralization takes place by resonant capture followed by purely intra-atomic Auger transitions, are too long to explain our experimental results. The introduction of additional neutralization/de-excitation mechanisms in the simulations leads to much better agreement with the experiments

Arrays of surface-normal electroabsorption modulators for the generation and signal processing of microwave photonics signals

NARCIS (Netherlands)

Noharet, Bertrand; Wang, Qin; Platt, Duncan; Junique, Stéphane; Marpaung, D.A.I.; Roeloffzen, C.G.H.

2011-01-01

The development of an array of 16 surface-normal electroabsorption modulators operating at 1550nm is presented. The modulator array is dedicated to the generation and processing of microwave photonics signals, targeting a modulation bandwidth in excess of 5GHz. The hybrid integration of the

Closed vessels microwave digestion method for uranium analysis of soils using alpha-spectroscopy

International Nuclear Information System (INIS)

Salar Amoli, H.; Barker, J.; Flowers, A.

2007-01-01

This paper describes our development of an accurate determination of uranium by alpha spectrometry using various kinds of sample digestion methods. The sample preparation techniques employed an acid digestion with HNO 3 , and microwave oven digestion either by HNO 3 or by combination of HNO 3 and HF. The samples were obtained from surface and in depth(40 cm) soils from residential area. An extraction chromatography column has been used to separate the uranium from interference matrix and elements. Results show that the microwave method significantly speeds up the analysis time, reduces the volume of acids used and eliminates a large fraction of acid vapour emission. Compared with the uranium recoveries it was shown that microwave HNO 3 +HF achieved greater recovery (83%) than microwave HNO 3 (78%), while less obtained by HNO 3 digestion using hot plate (75%). Various kind of digestion methods have been applied (24 times) for two kind of soil sample . The reproducibility was acceptable and the average precision (coefficient of variation) was between 4 to 5. No significant differences between the precision of the methods have been observed. Acid volume required for the microwave procedures are a fraction of 5 times lower and the analysis time 6 times lower than traditional digestion by hot plate technique. (author)

Infrared and microwave properties of polypyrrole/multi-walled carbon nanotube composites

Energy Technology Data Exchange (ETDEWEB)

Gao, Qi; Wang, Yongsheng, E-mail: yshwang@bjtu.edu.cn; He, Dawei, E-mail: dwhe@bjtu.edu.cn; Gao, Lei; Zhou, Yikang; Fu, Ming

2014-08-01

This study analyses the formation of polypyrrole/multi-walled carbon nanotube (PPy/MWCNT) composite materials using chemical oxidation with varying amounts of MWCNTs added. The samples are characterized by scanning electron microscopy, Fourier transform infrared emission spectroscopy, a four-probe method, and infrared thermal imaging using electromagnetic parameters. According to the test results, it is seen that the formation of PPy with the addition of MWCNTs can affect the material’s infrared properties and increase the material’s microwave return losses (up to −19 dB). This production procedure can also make the peak frequency of the microwave return losses adjustable, and the composite’s infrared and microwave performance becomes compatible and adjustable. - Highlights: • A one step in-situ synthesis method of PPy/MWCNT polymerization is proposed. • The composites were used for infrared camouflage and for their microwave properties. • The microwave return losses and infrared emissivity of the composites are adjustable. • The mechanism relies on changes in the composites’ conductivity.

Infrared and microwave properties of polypyrrole/multi-walled carbon nanotube composites

International Nuclear Information System (INIS)

Gao, Qi; Wang, Yongsheng; He, Dawei; Gao, Lei; Zhou, Yikang; Fu, Ming

2014-01-01

This study analyses the formation of polypyrrole/multi-walled carbon nanotube (PPy/MWCNT) composite materials using chemical oxidation with varying amounts of MWCNTs added. The samples are characterized by scanning electron microscopy, Fourier transform infrared emission spectroscopy, a four-probe method, and infrared thermal imaging using electromagnetic parameters. According to the test results, it is seen that the formation of PPy with the addition of MWCNTs can affect the material’s infrared properties and increase the material’s microwave return losses (up to −19 dB). This production procedure can also make the peak frequency of the microwave return losses adjustable, and the composite’s infrared and microwave performance becomes compatible and adjustable. - Highlights: • A one step in-situ synthesis method of PPy/MWCNT polymerization is proposed. • The composites were used for infrared camouflage and for their microwave properties. • The microwave return losses and infrared emissivity of the composites are adjustable. • The mechanism relies on changes in the composites’ conductivity

The surface emissions trap: a new approach in indoor air purification.

Science.gov (United States)

Markowicz, Pawel; Larsson, Lennart

2012-11-01

A new device for stopping or reducing potentially irritating or harmful emissions from surfaces indoors is described. The device is a surface emissions trap prototype and consists of an adsorbent sheet with a semipermeable barrier surrounded by two thin nonwoven layers. The trap may be applied directly at the source of the emissions e.g. at moisture-affected floors and walls, surfaces contaminated by chemical spills etc. This results in an immediate stop or reduction of the emitting pollutants. The trap has a very low water vapor resistance thus allowing drying of wet surfaces. In laboratory experiments typically 98% reduction of air concentrations of volatile organic compounds and a virtually total reduction of mold particle-associated mycotoxins was observed. The surface emissions trap may represent a convenient and efficient way of restoring indoor environments polluted by microbial and other moisture-associated emissions. Copyright © 2012 Elsevier B.V. All rights reserved.

TiO2-coated mesoporous carbon: conventional vs. microwave-annealing process.

Science.gov (United States)

Coromelci-Pastravanu, Cristina; Ignat, Maria; Popovici, Evelini; Harabagiu, Valeria

2014-08-15

The study of coating mesoporous carbon materials with titanium oxide nanoparticles is now becoming a promising and challenging area of research. To optimize the use of carbon materials in various applications, it is necessary to attach functional groups or other nanostructures to their surface. The combination of the distinctive properties of mesoporous carbon materials and titanium oxide is expected to be applied in field emission displays, nanoelectronic devices, novel catalysts, and polymer or ceramic reinforcement. But, their synthesis is still largely based on conventional techniques, such as wet impregnation followed by chemical reduction of the metal nanoparticle precursors, which takes time and money. The thermal heating based techniques are time consuming and often lack control of particle size and morphology. Hence, since there is a growing interest in microwave technology, an alternative way of power input into chemical reactions through dielectric heating is the use of microwaves. This work is focused on the advantages of microwave-assisted synthesis of TiO2-coated mesoporous carbon over conventional thermal heating method. The reviewed studies showed that the microwave-assisted synthesis of such composites allows processes to be completed within a shorter reaction time allowing the nanoparticles formation with superior properties than that obtained by conventional method. Copyright © 2014 Elsevier B.V. All rights reserved.

Influence of the magnetic field in the time evolution of the solar explosion radiation in X-ray and microwaves

International Nuclear Information System (INIS)

Costa, J.E.R.

1983-01-01

It has been made a theoretical development, sel-consistent with recent models for the explosive source, applied to time delays of peak emission at different microwave frequencies, and between microwaves and hard X-ray emission. A working hipothesis has been assumed with the adoption of a growing magnetic field during the solar flare explosion, and therefore contributing to a growth in microwave emission, differential in frequency, producing delays of maximum emission towards lower microwave frequencies, and delays of microwave maximum emission with respect to hard X-rays. It has been found that these delays are consistent with a growth in the magnetic field of about 14% by assuming both thermal and non-thermal models. This variation in magnetic field has been associated to movements of thermal sources downwards in the solar atmosphere, and it has been found that the estimated velocities of displacement were consistent compared to characteristic velocities of anomalous conduction fronts of thermal models. (Author) [pt

Analysis of parameter and interaction between parameter of the microwave assisted transesterification process of coconut oil using response surface methodology

Science.gov (United States)

Hidayanti, Nur; Suryanto, A.; Qadariyah, L.; Prihatini, P.; Mahfud, Mahfud

2015-12-01

A simple batch process was designed for the transesterification of coconut oil to alkyl esters using microwave assisted method. The product with yield above 93.225% of alkyl ester is called the biodiesel fuel. Response surface methodology was used to design the experiment and obtain the maximum possible yield of biodiesel in the microwave-assisted reaction from coconut oil with KOH as the catalyst. The results showed that the time reaction and concentration of KOH catalyst have significant effects on yield of alkyl ester. Based on the response surface methodology using the selected operating conditions, the time of reaction and concentration of KOH catalyst in transesterification process were 150 second and 0.25%w/w, respectively. The largest predicted and experimental yield of alkyl esters (biodiesel) under the optimal conditions are 101.385% and 93.225%, respectively. Our findings confirmed the successful development of process for the transesterification reaction of coconut oil by microwave-assisted heating, which is effective and time-saving for alkyl ester production.

Synthetic Aperture Microwave Imaging (SAMI) of the plasma edge on NSTX-U

Science.gov (United States)

Vann, Roddy; Taylor, Gary; Brunner, Jakob; Ellis, Bob; Thomas, David

2016-10-01

The Synthetic Aperture Microwave Imaging (SAMI) system is a unique phased-array microwave camera with a +/-40° field of view in both directions. It can image cut-off surfaces corresponding to frequencies in the range 10-34.5GHz; these surfaces are typically in the plasma edge. SAMI operates in two modes: either imaging thermal emission from the plasma (often modified by its interaction with the plasma edge e.g. via BXO mode conversion) or ``active probing'' i.e. injecting a broad beam at the plasma surface and imaging the reflected/back-scattered signal. SAMI was successfully pioneered on the Mega-Amp Spherical Tokamak (MAST) at Culham Centre for Fusion Energy. SAMI has now been installed and commissioned on the National Spherical Torus Experiment Upgrade (NSTX-U) at Princeton Plasma Physics Laboratory. The firmware has been upgraded to include real-time digital filtering, which enables continuous acquisition of the Doppler back-scattered active probing data. In this poster we shall present SAMI's analysis of the plasma edge on NSTX-U including measurements of the edge pitch angle on NSTX-U using SAMI's unique 2-D Doppler-backscattering capability.

Rough surface mitigates electron and gas emission

International Nuclear Information System (INIS)

Molvik, A.

2004-01-01

Heavy-ion beams impinging on surfaces near grazing incidence (to simulate the loss of halo ions) generate copious amounts of electrons and gas that can degrade the beam. We measured emission coefficients of η e (le) 130 and η 0 ∼ 10 4 respectively, with 1 MeV K + incident on stainless steel. Electron emission scales as η e ∝ 1/cos(θ), where θ is the ion angle of incidence relative to normal. If we were to roughen a surface by blasting it with glass beads, then ions that were near grazing incidence (90 o ) on smooth surface would strike the rims of the micro-craters at angles closer to normal incidence. This should reduce the electron emission: the factor of 10 reduction, Fig. 1(a), implies an average angle of incidence of 62 o . Gas desorption varies more slowly with θ (Fig. 1(b)) decreasing a factor of ∼2, and along with the electron emission is independent of the angle of incidence on a rough surface. In a quadrupole magnet, electrons emitted by lost primary ions are trapped near the wall by the magnetic field, but grazing incidence ions can backscatter and strike the wall a second time at an azimuth where magnetic field lines intercept the beam. Then, electrons can exist throughout the beam (see the simulations of Cohen, HIF News 1-2/04). The SRIM (TRIM) Monte Carlo code predicts that 60-70% of 1 MeV K + ions backscatter when incident at 88-89 o from normal on a smooth surface. The scattered ions are mostly within ∼10 o of the initial direction but a few scatter by up to 90 o . Ion scattering decreases rapidly away from grazing incidence, Fig. 1(c ). At 62 deg. the predicted ion backscattering (from a rough surface) is 3%, down a factor of 20 from the peak, which should significantly reduce electrons in the beam from lost halo ions. These results are published in Phys. Rev. ST - Accelerators and Beams

Synthesis of Graphite Oxide with Different Surface Oxygen Contents Assisted Microwave Radiation

Directory of Open Access Journals (Sweden)

Adriana Ibarra-Hernández

2018-02-01

Full Text Available Graphite oxide is synthesized via oxidation reaction using oxidant compounds that have lattice defects by the incorporation of unlike functional groups. Herein, we report the synthesis of the graphite oxide with diverse surface oxygen content through three (B, C, D different modified versions of the Hummers method assisted microwave radiation compared with the conventional graphite oxide sample obtained by Hummers method (A. These methods allow not only the production of graphite oxide but also reduced graphene oxide, without undergoing chemical, thermal, or mechanical reduction steps. The values obtained of C/O ratio were ~2, 3.4, and ~8.5 for methodologies C, B, and D, respectively, indicating the presence of graphite oxide and reduced graphene oxide, according to X-ray photoelectron spectroscopy. Raman spectroscopy of method D shows the fewest structural defects compared to the other methodologies. The results obtained suggest that the permanganate ion produces reducing species during graphite oxidation. The generation of these species is attributed to a reversible reaction between the permanganate ion with π electrons, ions, and radicals produced after treatment with microwave radiation.

TRMM MICROWAVE IMAGER (TMI) WENTZ OCEAN PRODUCTS V3

Data.gov (United States)

National Aeronautics and Space Administration — The TRMM Microwave Imager (TMI) is a 5-channel, dual-polarized, passive microwave radiometer. Microwave radiation is emitted by the Earth's surface and by water...

One-step microwave plasma enhanced chemical vapor deposition (MW-PECVD) for transparent superhydrophobic surface

Science.gov (United States)

Thongrom, Sukrit; Tirawanichakul, Yutthana; Munsit, Nantakan; Deangngam, Chalongrat

2018-02-01

We demonstrate a rapid and environmental friendly fabrication technique to produce optically clear superhydrophobic surfaces using poly (dimethylsiloxane) (PDMS) as a sole coating material. The inert PDMS chain is transformed into a 3-D irregular solid network through microwave plasma enhanced chemical vapor deposition (MW-PECVD) process. Thanks to high electron density in the microwave-activated plasma, coating can be done in just a single step with rapid deposition rate, typically much shorter than 10 s. Deposited layers show excellent superhydrophobic properties with water contact angles of ∼170° and roll-off angles as small as ∼3°. The plasma-deposited films can be ultrathin with thicknesses under 400 nm, greatly diminishing the optical loss. Moreover, with appropriate coating conditions, the coating layer can even enhance the transmission over the entire visible spectrum due to a partial anti-reflection effect.

Photon emission produced by particle-surface collisions

International Nuclear Information System (INIS)

White, C.W.; Tolk, N.H.

1976-02-01

Visible, ultraviolet, and infrared optical emission results from low-energy (20 eV-10 keV) particle-surface collisions. Several distinct kinds of collision induced optical radiation are discussed which provide fundamental information on particle-solid collision processes. Line radiation arises from excited states of sputtered surface constituents and backscattered beam particles. This radiation uniquely identifies the quantum state of sputtered or reflected particles, provides a method for identifying neutral atoms sputtered from the surface, and serves as the basis for a sensitive surface analysis technique. Broadband radiation from the bulk of the solid is attributed to the transfer of projectile energy to the electrons in the solid. Continuum emission observed well in front of transition metal targets is believed to arise from excited atom clusters (diatomic, triatomic, etc.) ejected from the solid in the sputtering process. Application of sputtered atom optical radiation for surface and depth profile analysis is demonstrated for the case of submonolayer quantities of chromium on silicon and aluminum implanted in SiO 2

Application of microwave to drying and blanching of tomatoes

International Nuclear Information System (INIS)

Ando, Y.; Orikasa, T.; Shiina, T.; Sotome, I.; Isobe, S.; Muramatsu, Y.; Tagawa, A.

2010-01-01

The applicability of microwave to the drying and blanching of tomatoes was examined. The changes of the drying rate and surface color were first measured and compared between drying by hot air (50degC) or microwave at three radiation powers. The drying rates using a microwave were higher than that using hot air. Both a constant-rate drying period and a falling-rate drying period were observed for each microwave radiation power. Compared to hot air drying, microwave drying resulted in an increase in lightness which is a preferable quality of tomatoes. Next, the changes in temperature, nutrients and surface color were measured and compared between blanching by microwave or boiling water. Microwave blanching required less time, resulted in higher retention of nutrients (ascorbic acid and lycopene) and caused less change in color in comparison with boiling water blanching. These results suggest that a microwave could be applied to drying and blanching tomatoes

Temporal Arctic longwave surface emissivity feedbacks in the Community Earth System Model

Science.gov (United States)

Kuo, C.; Feldman, D.; Huang, X.; Flanner, M.; Yang, P.; Chen, X.

2017-12-01

We have investigated how the inclusion of realistic and consistent surface emissivity in both land-surface and atmospheric components of the CESM coupled-climate model affects a wide range of climate variables. We did this by replacing the unit emissivity values in RRTMG_LW for water, fine-grained snow, and desert scenes with spectral emissivity values, and by replacing broadband emissivity values in surface components with the Planck-curve weighted counterparts. We find that this harmonized treatment of surface emissivity within CESM can be important for reducing high-latitude temperature biases. We also find that short-term effects of atmospheric dynamics and spectral information need to be considered to understand radiative effects in higher detail, and are possible with radiative kernels computed for every grid and time point for the entire model integration period. We find that conventional climatological feedback calculations indicate that sea-ice emissivity feedback is positive in sign, but that the radiative effects of the difference in emissivity between frozen and unfrozen surfaces exhibit seasonal dependence. Furthermore, this seasonality itself exhibits meridional asymmetry due to differences in sea-ice response to climate forcing between the Arctic and the Antarctic. In the Arctic, this seasonal, temporally higher order analysis exhibits increasing outgoing surface emissivity radiative response in a warming climate. While the sea-ice emissivity feedback and seasonal sea-ice emissivity radiative response amplitudes are a few percent of surface albedo feedbacks, the feedback analysis methods outlined in this work demonstrate that spatially and temporally localized feedback analysis can give insight into the mechanisms at work on those scales which differ in amplitude and sign from conventional climatological analyses. We note that the inclusion of this realistic physics leads to improved agreement between CESM model results and Arctic surface

Continuous microwave flow synthesis of mesoporous hydroxyapatite

International Nuclear Information System (INIS)

Akram, Muhammad; Alshemary, Ammar Z.; Goh, Yi-Fan; Wan Ibrahim, Wan Aini; Lintang, Hendrik O.; Hussain, Rafaqat

2015-01-01

We have successfully used continuous microwave flow synthesis (CMFS) technique for the template free synthesis of mesoporous hydroxyapatite. The continuous microwave flow reactor consisted of a modified 2.45 GHz household microwave, peristaltic pumps and a Teflon coil. This cost effective and efficient system was exploited to produce semi-crystalline phase pure nano-sized hydroxyapatite. Effect of microwave power, retention time and the concentration of reactants on the phase purity, degree of crystallinity and surface area of the final product was studied in detail. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) were used to study the phase purity and composition of the product, while transmission electron microscopy (TEM) was used to study the effect of process parameters on the morphology of hydroxyapatite. The TEM analysis confirmed the formation of spherical particles at low microwave power; however the morphology of the particles changed to mesoporous needle and rod-like structure upon exposing the reaction mixture to higher microwave power and longer retention time inside the microwave. The in-vitro ion dissolution behavior of the as synthesized hydroxyapatite was studied by determining the amount of Ca 2+ ion released in SBF solution. - Highlights: • Continuous microwave flow synthesis method was used to prepare hydroxyapatite. • Increase in microwave power enhanced the degree of crystallinity. • TEM images confirmed the presence of mesopores on the surface of HA

Continuous microwave flow synthesis of mesoporous hydroxyapatite

Energy Technology Data Exchange (ETDEWEB)

Akram, Muhammad; Alshemary, Ammar Z.; Goh, Yi-Fan; Wan Ibrahim, Wan Aini [Department of Chemistry, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor (Malaysia); Lintang, Hendrik O. [Centre for Sustainable Nanomaterials (CSNano), Ibnu Sina Institute for Scientific and Industrial Research, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor (Malaysia); Hussain, Rafaqat, E-mail: rafaqat@kimia.fs.utm.my [Centre for Sustainable Nanomaterials (CSNano), Ibnu Sina Institute for Scientific and Industrial Research, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor (Malaysia)

2015-11-01

We have successfully used continuous microwave flow synthesis (CMFS) technique for the template free synthesis of mesoporous hydroxyapatite. The continuous microwave flow reactor consisted of a modified 2.45 GHz household microwave, peristaltic pumps and a Teflon coil. This cost effective and efficient system was exploited to produce semi-crystalline phase pure nano-sized hydroxyapatite. Effect of microwave power, retention time and the concentration of reactants on the phase purity, degree of crystallinity and surface area of the final product was studied in detail. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) were used to study the phase purity and composition of the product, while transmission electron microscopy (TEM) was used to study the effect of process parameters on the morphology of hydroxyapatite. The TEM analysis confirmed the formation of spherical particles at low microwave power; however the morphology of the particles changed to mesoporous needle and rod-like structure upon exposing the reaction mixture to higher microwave power and longer retention time inside the microwave. The in-vitro ion dissolution behavior of the as synthesized hydroxyapatite was studied by determining the amount of Ca{sup 2+} ion released in SBF solution. - Highlights: • Continuous microwave flow synthesis method was used to prepare hydroxyapatite. • Increase in microwave power enhanced the degree of crystallinity. • TEM images confirmed the presence of mesopores on the surface of HA.

Satellite passive microwave rain measurement techniques for land and ocean

Science.gov (United States)

Spencer, R. W.

1985-01-01

Multiseasonal rainfall was found to be measurable over land with satellite passive microwave data, based upon comparisons between Nimbus 7 Scanning Multichannel Microwave Radiometer (SMME) brightness temperatures (T sub B) and operational WSR-57 radar rain rates. All of the SMMR channels (bipolarized 37, 21, 18, 10.7, and 6.6. GHz T sub B) were compared to radar reflectivities for 25 SMMR passes and 234 radar scans over the U.S. during the spring, summer, and fall of 1979. It was found that the radar rain rates were closely related to the difference between 37 and 21 GHz T sub B. This result is due to the volume scattering effects of precipitation which cause emissivity decreases with frequency, as opposed to emissive surfaces (e.g., water) whose emissivities increase with frequency. Two frequencies also act to reduce the effects of thermometric temperature variations on T sub B to a miminum. During summer and fall, multiple correlation coefficients of 0.80 and 0.75 were obtained. These approach the limit of correlation that can be expected to exist between two very different data sources, especially in light of the errors attributable to manual digitization of PPI photographs of variable quality from various operational weather radar not calibrated for research purposes. During the spring, a significantly lower (0.63) correlation was found. This poorer performance was traced to cases of wet, unvegetated soil being sensed at the lower frequencies through light rain, partly negating the rain scattering signal.

Microwave hematoma detector

Science.gov (United States)

Haddad, Waleed S.; Trebes, James E.; Matthews, Dennis L.

2001-01-01

The Microwave Hematoma Detector is a non-invasive device designed to detect and localize blood pooling and clots near the outer surface of the body. While being geared towards finding sub-dural and epi-dural hematomas, the device can be used to detect blood pooling anywhere near the surface of the body. Modified versions of the device can also detect pneumothorax, organ hemorrhage, atherosclerotic plaque in the carotid arteries, evaluate perfusion (blood flow) at or near the body surface, body tissue damage at or near the surface (especially for burn assessment) and be used in a number of NDE applications. The device is based on low power pulsed microwave technology combined with a specialized antenna, signal processing/recognition algorithms and a disposable cap worn by the patient which will facilitate accurate mapping of the brain and proper function of the instrument. The invention may be used for rapid, non-invasive detection of sub-dural or epi-dural hematoma in human or animal patients, detection of hemorrhage within approximately 5 cm of the outer surface anywhere on a patient's body.

Incorporation of Passive Microwave Brightness Temperatures in the ECMWF Soil Moisture Analysis

Directory of Open Access Journals (Sweden)

Joaquín Muñoz-Sabater

2015-05-01

Full Text Available For more than a decade, the European Centre for Medium-Range Weather Forecasts (ECMWF has used in-situ observations of 2 m temperature and 2 m relative humidity to operationally constrain the temporal evolution of model soil moisture. These observations are not available everywhere and they are indirectly linked to the state of the surface, so under various circumstances, such as weak radiative forcing or strong advection, they cannot be used as a proxy for soil moisture reinitialization in numerical weather prediction. Recently, the ECMWF soil moisture analysis has been updated to be able to account for the information provided by microwave brightness temperatures from the Soil Moisture and Ocean Salinity (SMOS mission of the European Space Agency (ESA. This is the first time that ECMWF uses direct information of the soil emission from passive microwave data to globally adjust the estimation of soil moisture by a land-surface model. This paper presents a novel version of the ECMWF Extended Kalman Filter soil moisture analysis to account for remotely sensed passive microwave data. It also discusses the advantages of assimilating direct satellite radiances compared to current soil moisture products, with a view to an operational implementation. A simple assimilation case study at global scale highlights the potential benefits and obstacles of using this new type of information in a global coupled land-atmospheric model.

Microwave-assisted efficient conjugation of nanodiamond and paclitaxel.

Science.gov (United States)

Hsieh, Yi-Han; Liu, Kuang-Kai; Sulake, Rohidas S; Chao, Jui-I; Chen, Chinpiao

2015-01-01

Nanodiamond has recently received considerable attention due to the various possible applications in medical field such as drug delivery and bio-labeling. For this purpose suitable and effective surface functionalization of the diamond material are required. A versatile and reproducible surface modification method of nanoscale diamond is essential for functionalization. We introduce the input of microwave energy to assist the functionalization of nanodiamond surface. The feasibility of such a process is illustrated by comparing the biological assay of ND-paclitaxel synthesized by conventional and microwave irradiating. Using a microwave we manage to have approximately doubled grafted molecules per nanoparticle of nanodiamond. Copyright © 2015 Elsevier Ltd. All rights reserved.

Microwave based method of monitoring crack formation

International Nuclear Information System (INIS)

Aman, Sergej; Aman, Alexander; Majcherek, Soeren; Hirsch, Soeren; Schmidt, Bertram

2014-01-01

The formation of cracks in glass particles was monitored by application of linearly polarized microwaves. The breakage behavior of glass spheres coated with a thin gold layer of about 50 nm, i.e. a thickness that is lower than the microwave penetration depth, was tested. In this way the investigation of fracture behavior of electronic circuits was simulated. A shielding current was induced in the gold layer by the application of microwaves. During the crack formation the distribution of this current changed abruptly and a scattered microwave signal appeared at the frequency of the incident microwaves. The time behavior of the scattered signal reflects the microscopic processes occurring during the fracture of the specimen. The duration of the increasing signal corresponds to the crack formation time in the tested specimen. This time was estimated as particle size divided by crack development speed in glass. An intense emission of electrons occurs during the formation of cracks. Due to this, coherent Thomson scattering of microwaves by emitted electrons becomes significant with a delay of a few microseconds after the initial phase of crack formation. In this time the intensity of the microwave signal increases. (paper)

Pyrolysis of methane by microwaves. Pt. 1

International Nuclear Information System (INIS)

Avni, R.; Winefordner, J.D.; Nickel, H.

1975-04-01

The pyrolysis of methane and mixtures of argon-methane by microwaves (2,450 MHz) was investigated. The microwave plasma diagnostic study was performed using electrical probes, namely, the double floating probe technique. Parameters such as electric field strength and current densities were measured and from their relationship the electron temperature, electric conductivity, electron and ion densities were evaluated as function of gas pressure, microwave power input and distance of the probe from the microwave cavity. Various spectroscopic techniques were used for the measurement of temperatures in the microwave plasma; the 'reversal temperature' by measuring the intensities of the electronic vibrational bands of CN and OH molecules and 'rotational temperature' from the measured intensities of rotational OH lines. The 'rotational' as well as the 'reversal temperature' were found to be identical and this temperature was assumed to be the temperature of the gas in the microwave plasma. Energy balance calculation, based upon the electrical energy input and thermal losses, were performed in order to determine if steady state conditions existed in the microwave plasma. Emission and absorption spectroscopy were used for determining the active species formed in the pyrolysis of methane and also of mixtures of CH 4 -Ar, by the microwave plasma. (orig.) [de

Growth, microstructure, and field-emission properties of synthesized diamond film on adamantane-coated silicon substrate by microwave plasma chemical vapor deposition

International Nuclear Information System (INIS)

Tiwari, Rajanish N.; Chang Li

2010-01-01

Diamond nucleation on unscratched Si surface is great importance for its growth, and detailed understanding of this process is therefore desired for many applications. The pretreatment of the substrate surface may influence the initial growth period. In this study, diamond films have been synthesized on adamantane-coated crystalline silicon {100} substrate by microwave plasma chemical vapor deposition from a gaseous mixture of methane and hydrogen gases without the application of a bias voltage to the substrates. Prior to adamantane coating, the Si substrates were not pretreated such as abraded/scratched. The substrate temperature was ∼530 deg. C during diamond deposition. The deposited films are characterized by scanning electron microscopy, Raman spectrometry, x-ray diffraction, and x-ray photoelectron spectroscopy. These measurements provide definitive evidence for high-crystalline quality diamond film, which is synthesized on a SiC rather than clean Si substrate. Characterization through atomic force microscope allows establishing fine quality criteria of the film according to the grain size of nanodiamond along with SiC. The diamond films exhibit a low-threshold (55 V/μm) and high current-density (1.6 mA/cm 2 ) field-emission (FE) display. The possible mechanism of formation of diamond films and their FE properties have been demonstrated.

Correlation between galactic HI and the cosmic microwave background

International Nuclear Information System (INIS)

Land, Kate; Slosar, Anze

2007-01-01

We revisit the issue of a correlation between the atomic hydrogen gas in our local galaxy and the cosmic microwave background, a detection of which has been claimed in some literature. We cross correlate the 21-cm emission of galactic atomic hydrogen as traced by the Leiden/Argentine/Bonn Galactic Hi survey with the 3-year cosmic microwave background data from the Wilkinson microwave anisotropy probe. We consider a number of angular scales, masks, and Hi velocity slices and find no statistically significant correlation

Microwave-derived soil moisture over Mediterranean land uses: from ground-based radiometry to SMOS first observations

Science.gov (United States)

Saleh, Kauzar; Antolín, Carmen; Juglea, Silvia; Kerr, Yann; Millán-Scheiding, Cristina; Novello, Nathalie; Pardé, Mickael; Wigneron, Jean-Pierre; Zribi, Mehrez; López-Baeza, Ernesto

2010-05-01

This communication will present the main results of a series of airborne and ground-based experiments conducted at the Valencia Anchor Station (VAS) site for the implementation of the SMOS emission model L-MEB (L-band Microwave Emission model of the Biosphere, Wigneron et al., 2007), and will evaluate the performance of L-MEB against SMOS measurements. The L-MEB model has been implemented in the context of the SMOS mission and through numerous radiometry experiments over different land uses. Within L-MEB, each land use is characterised by model parameterisations that are used to describe the radiative transfer at L-band. They describe, for instance, the attenuation properties of different canopies, or the effect of soil roughness on the surface emission. In recent years, the Valencia Anchor Station site (VAS) has hosted various radiometry experiments. These were performed at different scales, from the plot scale to the regional scale (up to 50 km), using ground-based and airborne-based radiometry. The main results are discussed in this communication, and some preliminary comparisons with SMOS measurements are presented. 1) Ground-based experiments. MELBEX-I was a ground-radiometry experiment run in 2005 using the L-band radiometer EMIRAD over a plot of shrub land. We will present results from this experiment (Cano et al., 2009), that highlighted a constant (and small) contribution of Mediterranean shrub land to the overall emission, and investigated the role of exposed rocks in the surface emission. MELBEX-II was a ground-radiometry experiment run in 2007 using the EMIRAD L-band radiometer over a plot of vineyards throughout the whole vegetation cycle. Vineyards are the main land use at the VAS site, therefore parameterisations for vineyards are key for the validation of SMOS data at VAS. This communication will discuss, in particular, estimates of microwave surface roughness throughout the crop year, and changes in the canopy microwave properties throughout the

Photoelectron emission from metal surfaces by ultrashort laser pulses

International Nuclear Information System (INIS)

Faraggi, M. N.; Gravielle, M. S.; Silkin, V. M.

2006-01-01

Electron emission from metal surfaces produced by short laser pulses is studied within the framework of the distorted-wave formulation. The proposed approach, named surface-Volkov (SV) approximation, makes use of the band-structure based (BSB) model and the Volkov phase to describe the interaction of the emitted electron with the surface and the external electric field, respectively. The BSB model provides a realistic representation of the surface, based on a model potential that includes the main features of the surface band structure. The SV method is applied to evaluate the photoelectron emission from the valence band of Al(111). Angular and energy distributions are investigated for different parameters of the laser pulse, keeping in all cases the carrier frequency larger than the plasmon one

A microwave resonator for limiting depth sensitivity for electron paramagnetic resonance spectroscopy of surfaces.

Science.gov (United States)

Sidabras, Jason W; Varanasi, Shiv K; Mett, Richard R; Swarts, Steven G; Swartz, Harold M; Hyde, James S

2014-10-01

A microwave Surface Resonator Array (SRA) structure is described for use in Electron Paramagnetic Resonance (EPR) spectroscopy. The SRA has a series of anti-parallel transmission line modes that provides a region of sensitivity equal to the cross-sectional area times its depth sensitivity, which is approximately half the distance between the transmission line centers. It is shown that the quarter-wave twin-lead transmission line can be a useful element for design of microwave resonators at frequencies as high as 10 GHz. The SRA geometry is presented as a novel resonator for use in surface spectroscopy where the region of interest is either surrounded by lossy material, or the spectroscopist wishes to minimize signal from surrounding materials. One such application is in vivo spectroscopy of human finger-nails at X-band (9.5 GHz) to measure ionizing radiation dosages. In order to reduce losses associated with tissues beneath the nail that yield no EPR signal, the SRA structure is designed to limit depth sensitivity to the thickness of the fingernail. Another application, due to the resonator geometry and limited depth penetration, is surface spectroscopy in coating or material science. To test this application, a spectrum of 1.44 μM of Mg(2+) doped polystyrene 1.1 mm thick on an aluminum surface is obtained. Modeling, design, and simulations were performed using Wolfram Mathematica (Champaign, IL; v. 9.0) and Ansys High Frequency Structure Simulator (HFSS; Canonsburg, PA; v. 15.0). A micro-strip coupling circuit is designed to suppress unwanted modes and provide a balanced impedance transformation to a 50 Ω coaxial input. Agreement between simulated and experimental results is shown.

A microwave resonator for limiting depth sensitivity for electron paramagnetic resonance spectroscopy of surfaces

Energy Technology Data Exchange (ETDEWEB)

Sidabras, Jason W.; Varanasi, Shiv K.; Hyde, James S. [Department of Biophysics, Medical College of Wisconsin, Milwaukee, Wisconsin 53211 (United States); Mett, Richard R. [Department of Biophysics, Medical College of Wisconsin, Milwaukee, Wisconsin 53211 (United States); Department of Physics and Chemistry, Milwaukee School of Engineering, Milwaukee, Wisconsin 53202 (United States); Swarts, Steven G. [Department of Radiation Oncology, University of Florida, Gainesville, Florida, 32610 (United States); Swartz, Harold M. [Department of Radiology, Geisel Medical School at Dartmouth, Hanover, New Hampshire 03755 (United States)

2014-10-15

A microwave Surface Resonator Array (SRA) structure is described for use in Electron Paramagnetic Resonance (EPR) spectroscopy. The SRA has a series of anti-parallel transmission line modes that provides a region of sensitivity equal to the cross-sectional area times its depth sensitivity, which is approximately half the distance between the transmission line centers. It is shown that the quarter-wave twin-lead transmission line can be a useful element for design of microwave resonators at frequencies as high as 10 GHz. The SRA geometry is presented as a novel resonator for use in surface spectroscopy where the region of interest is either surrounded by lossy material, or the spectroscopist wishes to minimize signal from surrounding materials. One such application is in vivo spectroscopy of human finger-nails at X-band (9.5 GHz) to measure ionizing radiation dosages. In order to reduce losses associated with tissues beneath the nail that yield no EPR signal, the SRA structure is designed to limit depth sensitivity to the thickness of the fingernail. Another application, due to the resonator geometry and limited depth penetration, is surface spectroscopy in coating or material science. To test this application, a spectrum of 1.44 μM of Mg{sup 2+} doped polystyrene 1.1 mm thick on an aluminum surface is obtained. Modeling, design, and simulations were performed using Wolfram Mathematica (Champaign, IL; v. 9.0) and Ansys High Frequency Structure Simulator (HFSS; Canonsburg, PA; v. 15.0). A micro-strip coupling circuit is designed to suppress unwanted modes and provide a balanced impedance transformation to a 50 Ω coaxial input. Agreement between simulated and experimental results is shown.

Electron emission from insulator surfaces by ultra-short laser pulses

Energy Technology Data Exchange (ETDEWEB)

Acuna, M; Gravielle, M S, E-mail: mario@iafe.uba.a, E-mail: msilvia@iafe.uba.a [Institutes de AstronomIa y Fisica del Espacio, Casilla de Correo 67, Sucursal 28, 1428 Buenos Aires (Argentina)

2009-11-01

Photoelectron emission from insulator surfaces induced by ultra-short laser pulses is studied within a time-dependent distorted wave method. The proposed approach combines the Volkov phase, which takes into account the laser interaction, with a simple representation of the unperturbed surface states, given by the Tight-binding method. The model is applied to evaluate the photoelectron emission from a LiF(001) surface, finding effects of interference produced by the crystal lattice.

Determination of the mineral compositions of in six beans by microwave digestion with inductively coupled plasma atomic emission spectrometry

International Nuclear Information System (INIS)

Yan, Q.; Yang, L.; Chen, S.; Liu, X.; Ma, X.

2012-01-01

In the study, microwave digestion procedure optimized was applied for digesting beans. Nineteen mineral element concentrations were determined by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES). The result indicated detection limits for the 19 elements were less than 0.0998, and relative standard deviations were 1.01% - 5.02% for all the elements, and recoveries were 90.89% - 104.55% by adding standard recovery experiment. The study showed the beans selected were abundant in mineral element contents in human nutrition, determination mineral element contents by ICP-AES with microwave digestion technology were a lot of merits of small environmental pollution, fast and accurate determination result, which could satisfy the examination request of bean samples. The results provided evidence that the six beans were a good source of K, P, Mg and Ca. This study is to give important reference value to people due to individual differences by adjusting the dietary to complement the different mineral elements. (author)

Calibration methods for ECE systems with microwave sources

International Nuclear Information System (INIS)

Tubbing, B.J.D.; Kissel, S.E.

1987-01-01

The authors investigated the feasibility of two methods for calibration of electron cyclotron emission (ECE) systems, both based on the use of a microwave source. In the first method -called the Antenna Pattern Integration (API) method - the microwave source is scanned in space, so as to simulate a large - area - blackbody -source. In the second method -called the Untuned Cavity (UC) method -an untuned cavity, fed by the microwave source, is used to simulate a blackbody. For both methods, the hardware required to perform partly automated calibrations was developed. The microwave based methods were compared with a large area blackbody calibration on two different ECE systems, a Michelson interferometer and a grating polychromator. The API method was found to be more successful than the UC method. (author)

Spectral emissivity of surface blackbody calibrators

DEFF Research Database (Denmark)

Clausen, Sønnik

2007-01-01

The normal spectral emissivity of commercial infrared calibrators is compared with measurements of anodized aluminum samples and grooved aluminum surfaces coated with Pyromark. Measurements performed by FTIR spectroscopy in the wavelength interval from 2 to 20 mu m and at temperatures between 5...

Microwave and pulsed power engineering

International Nuclear Information System (INIS)

Hofer, W.W.

1984-01-01

The Microwave and Pulsed Power Engineering Thrust Area is responsible for developing the short-term and long-term engineering resources required to support the growing microwave and pulsed power engineering requirements of several LLNL Programs. The responsibility of this Thrust Area is to initiate applicable research and development projects and to provide capabilities and facilities to permit engineers involved in these and other programs to make significant contributions. In this section, the principal projects are described: dielectric failure prediction using partial discharge analysis, coating dielectrics to increase surface flashover potential, and the microwave generator experiment

Microwave detection of air showers with the MIDAS experiment

International Nuclear Information System (INIS)

Privitera, Paolo; Alekotte, I.; Alvarez-Muniz, J.; Berlin, A.; Bertou, X.; Bogdan, M.; Bohacova, M.; Bonifazi, C.; Carvalho, W.R.; Mello Neto, J.R.T. de; Facal San Luis, P.; Genat, J.F.; Hollon, N.; Mills, E.; Monasor, M.; Reyes, L.C.; Rouille d'Orfeuil, B.; Santos, E.M.; Wayne, S.; Williams, C.

2011-01-01

Microwave emission from Extensive Air Showers could provide a novel technique for ultra-high energy cosmic rays detection over large area and with 100% duty cycle. We describe the design, performance and first results of the MIDAS (MIcrowave Detection of Air Showers) detector, a 4.5 m parabolic dish with 53 feeds in its focal plane, currently installed at the University of Chicago.

Modelling the passive microwave signature from land surfaces: a review of recent results and application to the SMOS & SMAP soil moisture retrieval algorithms

Science.gov (United States)

Two passive microwave missions are currently operating at L-band to monitor surface soil moisture (SM) over continental surfaces. The SMOS sensor, based on an innovative interferometric technology enabling multi-angular signatures of surfaces to be measured, was launched in November 2009....

Global Warming and the Microwave Background

Directory of Open Access Journals (Sweden)

Robitaille P.-M.

2009-04-01

Full Text Available In the work, the importance of assigning the microwave background to the Earth is ad- dressed while emphasizing the consequences for global climate change. Climate mod- els can only produce meaningful forecasts when they consider the real magnitude of all radiative processes. The oceans and continents both contribute to terrestrial emis- sions. However, the extent of oceanic radiation, particularly in the microwave region, raises concerns. This is not only since the globe is covered with water, but because the oceans themselves are likely to be weaker emitters than currently believed. Should the microwave background truly be generated by the oceans of the Earth, our planet would be a much less efficient emitter of radiation in this region of the electromagnetic spectrum. Furthermore, the oceans would appear unable to increase their emissions in the microwave in response to temperature elevation, as predicted by Stefan’s law. The results are significant relative to the modeling of global warming.

Terahertz emission from semi-insulating GaAs with octadecanthiol-passivated surface

International Nuclear Information System (INIS)

Wu, Xiaojun; Xu, Xinlong; Lu, Xinchao; Wang, Li

2013-01-01

Terahertz (THz) emission from octadecanthiol (ODT) passivated (1 0 0) surface of the semi-insulating GaAs was measured, and compared with those from the native oxidized and the fresh surfaces. It was shown that the self-assembled ODT monolayer can stabilize the GaAs (1 0 0) surface, and maintain a THz surface emission 1.4 times as efficient as the native oxidized surface under equal conditions. Surface passivation can reduce the built-in electric field in the depletion region of the GaAs (1 0 0), resulting in the suppression of the THz radiation to a different extent. Oxidation of GaAs surface reduces the THz amplitude mainly in the low-frequency region. These results indicate that GaAs can be made a more effective THz source by choosing molecular passivation technique. Conversely, the THz emission features such as polarity, amplitude, and phase from molecule-passivated surfaces may be used to characterize the attached molecules.

The microwave effects on the properties of alumina at high frequencies of microwave sintering

International Nuclear Information System (INIS)

Sudiana, I. Nyoman; Ngkoimani, La Ode; Usman, Ida; Mitsudo, Seitaro; Sako, Katsuhide; Inagaki, Shunsuke; Aripin, H.

2016-01-01

Microwave sintering of materials has attracted much research interest because of its significant advantages (e.g. reduced sintering temperatures and soaking times) over the conventional heating. Most researchers compared processes that occurred during the microwave and conventional heating at the same temperature and time. The enhancements found in the former method are indicated as a 'non-thermal effect' which is usually used for explaining the phenomena in microwave processing. Numerous recent studies have been focused on the effect to elucidate the microwave interaction mechanism with materials. Moreover, recent progress on microwave sources such as gyrotrons has opened the possibility for processing materials by using a higher microwave frequency. Therefore, the technology is expected to exhibit a stronger non-thermal effect. This paper presents results from a series of experiments to study the non-thermal effect on microwave sintered alumina. Sintering by using a wide rage of microwave frequencies up to 300 GHz as well as a conventional furnace was carried out. The linear shrinkages of samples for each sintering method were measured. Pores and grains taken from scanning electron microstructure (SEM) images of cut surfaces were also examined. The results of a comparative study of the shrinkages and microstructure evolutions of the sintered samples under annealing in microwave heating systems and in an electric furnace were analyzed. A notably different behavior of the shrinkages and microstructures of alumina after being annealed was found. The results suggested that microwave radiations provided an additional force for mass transports. The results also indicated that the sintering process depended on microwave frequencies.

The microwave effects on the properties of alumina at high frequencies of microwave sintering

Energy Technology Data Exchange (ETDEWEB)

Sudiana, I. Nyoman, E-mail: sudiana75@yahoo.com; Ngkoimani, La Ode; Usman, Ida [Department of Physics, Faculty of Mathematic and Natural Science, Halu Oleo University, Kampus Bumi Tridharma Anduonohu, Kendari 93232 (Indonesia); Mitsudo, Seitaro; Sako, Katsuhide; Inagaki, Shunsuke [Research Center for Development of Far-Infrared Region, University of Fukui, 3-9-1 Bunkyo, Fukui-shi 910-8507 (Japan); Aripin, H. [Center for Material Processing and Renewable Energy, Faculty of Learning Teacher and Education Science, Siliwangi University, Jl. Siliwangi 24 Tasikmalaya 46115, West Java (Indonesia)

2016-03-11

Microwave sintering of materials has attracted much research interest because of its significant advantages (e.g. reduced sintering temperatures and soaking times) over the conventional heating. Most researchers compared processes that occurred during the microwave and conventional heating at the same temperature and time. The enhancements found in the former method are indicated as a 'non-thermal effect' which is usually used for explaining the phenomena in microwave processing. Numerous recent studies have been focused on the effect to elucidate the microwave interaction mechanism with materials. Moreover, recent progress on microwave sources such as gyrotrons has opened the possibility for processing materials by using a higher microwave frequency. Therefore, the technology is expected to exhibit a stronger non-thermal effect. This paper presents results from a series of experiments to study the non-thermal effect on microwave sintered alumina. Sintering by using a wide rage of microwave frequencies up to 300 GHz as well as a conventional furnace was carried out. The linear shrinkages of samples for each sintering method were measured. Pores and grains taken from scanning electron microstructure (SEM) images of cut surfaces were also examined. The results of a comparative study of the shrinkages and microstructure evolutions of the sintered samples under annealing in microwave heating systems and in an electric furnace were analyzed. A notably different behavior of the shrinkages and microstructures of alumina after being annealed was found. The results suggested that microwave radiations provided an additional force for mass transports. The results also indicated that the sintering process depended on microwave frequencies.

Surface nanostructuring in the carbon–silicon(100) system upon microwave plasma treatment

Energy Technology Data Exchange (ETDEWEB)

Yafarov, R. K., E-mail: pirpc@yandex.ru; Shanygin, V. Ya. [Russian Academy of Sciences, Kotel’nikov Institute of Radio Engineering and Electronics, Saratov Branch (Russian Federation)

2017-04-15

The study is concerned with the physical and chemical processes and the mechanisms of the effect of plasma preparation of a surface on the systematic features of condensation and surface phase transformations during the formation of Si–C mask domains on p-Si(100) crystals by the deposition of submonolayer C coatings in the microwave plasma of low-pressure ethanol vapors. It is shown that, at short durations of the deposition of carbon onto silicon wafers with a natural-oxide coating at a temperature of 100°C, the formation of domains is observed. The lateral dimensions of the domains lie in the range from 10–15 to 200 nm, and the heights of ridges produced by the plasma chemical etching of silicon through the mask domain coatings vary in the range from 40 to 80 nm.

Microwave second-harmonic response of ceramic MgB2 samples

International Nuclear Information System (INIS)

Agliolo Gallitto, A.; Bonsignore, G.; Li Vigni, M.

2005-01-01

Nonlinear microwave response of different ceramic MgB 2 samples has been investigated by the technique of second-harmonic emission. The second-harmonic signal has been investigated as a function of temperature, DC magnetic field and input microwave power. The attention has mainly been devoted to the response at low magnetic fields, where nonlinear processes arising from motion of Abrikosov fluxons are ineffective. The results show that different mechanisms are responsible for the nonlinear response in the different ranges of temperature. At low temperatures, the nonlinear response is due to processes involving weak links. At temperatures close to T c , a further contribution to the harmonic emission is present; it can be ascribed to modulation of the order parameter by the microwave field and gives rise to a peak in the temperature dependence of the harmonic signal

Application of a plane-stratified emission model to predict the effects of vegetation in passive microwave radiometry

Directory of Open Access Journals (Sweden)

K. Lee

2002-01-01

Full Text Available This paper reports the application to vegetation canopies of a coherent model for the propagation of electromagnetic radiation through a stratified medium. The resulting multi-layer vegetation model is plausibly realistic in that it recognises the dielectric permittivity of the vegetation matter, the mixing of the dielectric permittivities for vegetation and air within the canopy and, in simplified terms, the overall vertical distribution of dielectric permittivity and temperature through the canopy. Any sharp changes in the dielectric profile of the canopy resulted in interference effects manifested as oscillations in the microwave brightness temperature as a function of canopy height or look angle. However, when Gaussian broadening of the top and bottom of the canopy (reflecting the natural variability between plants was included within the model, these oscillations were eliminated. The model parameters required to specify the dielectric profile within the canopy, particularly the parameters that quantify the dielectric mixing between vegetation and air in the canopy, are not usually available in typical field experiments. Thus, the feasibility of specifying these parameters using an advanced single-criterion, multiple-parameter optimisation technique was investigated by automatically minimizing the difference between the modelled and measured brightness temperatures. The results imply that the mixing parameters can be so determined but only if other parameters that specify vegetation dry matter and water content are measured independently. The new model was then applied to investigate the sensitivity of microwave emission to specific vegetation parameters. Keywords: passive microwave, soil moisture, vegetation, SMOS, retrieval

Negative secondary ion emission from oxidized surfaces

International Nuclear Information System (INIS)

Gnaser, H.; Kernforschungsanlage Juelich G.m.b.H.

1984-01-01

The emission of negative secondary ions from 23 elements was studied for 10 keV O 2 + and 10 keV In + impact at an angle of incidence of 45 0 . Partial oxidation of the sample surfaces was achieved by oxygen bombardment and/or by working at a high oxygen partial pressure. It was found that the emission of oxide ions shows an element-characteristic pattern. For the majority of the elements investigated these features are largely invariant against changes of the surface concentration of oxygen. For the others admission of oxygen strongly changes the relative intensities of oxide ions: a strong increase of MO 3 - signals (M stands for the respective element) is accompanied by a decrease of MO - and M - intensities. Different primary species frequently induce changes of both the relative and the absolute negative ion intensities. Carbon - in contrast to all other elements - does not show any detectable oxide ion emission but rather intense cluster ions Csub(n) - (detected up to n=12) whose intensities oscillate in dependence on n. (orig./RK)

Indonesia sea surface temperature from TRMM Microwave Imaging (TMI) sensor

Science.gov (United States)

Marini, Y.; Setiawan, K. T.

2018-05-01

We analysis the Tropical Rainfall Measuring Mission's (TRMM) Microwave Imager (TMI) data to monitor the sea surface temperature (SST) of Indonesia waters for a decade of 2005-2014. The TMI SST data shows the seasonal and interannual SST in Indonesian waters. In general, the SST average was highest in March-May period with SST average was 29.4°C, and the lowest was in June – August period with the SST average was 28.5°C. The monthly SST average fluctuation of Indonesian waters for 10 years tends to increase. The lowest SST average of Indonesia occurred in August 2006 with the SST average was 27.6° C, while the maximum occurred in May 2014 with the monthly SST average temperature was 29.9 ° C.

Rapid growth of ZnO hexagonal prism crystals by direct microwave heating

Institute of Scientific and Technical Information of China (English)

ZHU Zhenqi; ZHOU Jian; LIU Guizhen; REN Zhiguo

2008-01-01

ZnO hexagonal prism crystals were synthesized from ZnO powders by microwave heating in a short time (within 20 min) without any metal catalyst or transport agent.Zinc oxide raw materials were made by evaporating from the high-temperature zone in an enclosure atmosphere and crystals were grown on the self-source substrate.The inherent asymmetry in microwave heating provides the temperature gradient for crystal growth.Substrate and temperature distribution in the oven show significant effects on the growth of the ZnO crystal.The morphologies demonstrate that these samples are pure hexagonal prism crystals with maximum 80 μm in diameter and 600 μm in length,which possess a well faceted end and side surface.X-ray diffraction (XRD) reveals that these samples are pure crystals.The photoluminescence (PL) exhibits strong ultraviolet emission at room temperature,indicating potential applications for short-wave light-emitting photonic devices.

The Python Sky Model: software for simulating the Galactic microwave sky

Science.gov (United States)

Thorne, B.; Dunkley, J.; Alonso, D.; Næss, S.

2017-08-01

We present a numerical code to simulate maps of Galactic emission in intensity and polarization at microwave frequencies, aiding in the design of cosmic microwave background experiments. This python code builds on existing efforts to simulate the sky by providing an easy-to-use interface and is based on publicly available data from the WMAP (Wilkinson Microwave Anisotropy Probe) and Planck satellite missions. We simulate synchrotron, thermal dust, free-free and anomalous microwave emission over the whole sky, in addition to the cosmic microwave background, and include a set of alternative prescriptions for the frequency dependence of each component, for example, polarized dust with multiple temperatures and a decorrelation of the signals with frequency, which introduce complexity that is consistent with current data. We also present a new prescription for adding small-scale realizations of these components at resolutions greater than current all-sky measurements. The usefulness of the code is demonstrated by forecasting the impact of varying foreground complexity on the recovered tensor-to-scalar ratio for the LiteBIRD satellite. The code is available at: https://github.com/bthorne93/PySM_public.

Preparation of silica nanoparticles through microwave-assisted acid-catalysis.

Science.gov (United States)

Lovingood, Derek D; Owens, Jeffrey R; Seeber, Michael; Kornev, Konstantin G; Luzinov, Igor

2013-12-16

Microwave-assisted synthetic techniques were used to quickly and reproducibly produce silica nanoparticle sols using an acid catalyst with nanoparticle diameters ranging from 30-250 nm by varying the reaction conditions. Through the selection of a microwave compatible solvent, silicic acid precursor, catalyst, and microwave irradiation time, these microwave-assisted methods were capable of overcoming the previously reported shortcomings associated with synthesis of silica nanoparticles using microwave reactors. The siloxane precursor was hydrolyzed using the acid catalyst, HCl. Acetone, a low-tan δ solvent, mediates the condensation reactions and has minimal interaction with the electromagnetic field. Condensation reactions begin when the silicic acid precursor couples with the microwave radiation, leading to silica nanoparticle sol formation. The silica nanoparticles were characterized by dynamic light scattering data and scanning electron microscopy, which show the materials' morphology and size to be dependent on the reaction conditions. Microwave-assisted reactions produce silica nanoparticles with roughened textured surfaces that are atypical for silica sols produced by Stöber's methods, which have smooth surfaces.

Facile conversion of bulk metal surface to metal oxide single-crystalline nanostructures by microwave irradiation: Formation of pure or Cr-doped hematite nanostructure arrays

International Nuclear Information System (INIS)

Cho, Seungho; Jeong, Haeyoon; Lee, Kun-Hong

2010-01-01

We report a method for converting the surfaces of bulk metal substrates (pure iron or stainless steel) to metal oxide (hematite or Cr-doped hematite) nanostructures using microwave irradiation. When microwave radiation (2.45 GHz, single-mode) was applied to a metal substrate under the flow of a gas mixture containing O 2 and Ar, metal oxide nanostructures formed and entirely covered the substrate. The nanostructures were single crystalline, and the atomic ratios of the substrate metals were preserved in the nanostructures. When a pure iron sheet was used as a substrate, hematite nanowires (1000 W microwave radiation) or nanosheets (1800 W microwave radiation) formed on the surface of the substrate. When a SUS410 sheet was used as a substrate, slightly curved rod-like nanostructures were synthesized. The oxidation states of Fe and Cr in these nanorods were Fe 3+ and Cr 3+ . Quantitative analyses revealed an average Fe/Cr atomic ratio of 9.2, nearly identical to the ratio of the metals in the SUS410 substrate.

Plasma upflows and microwave emission in hot supra-arcade structure associated with AN M1.6 limb flare

International Nuclear Information System (INIS)

Kim, S.; Shibasaki, K.; Bain, H.-M.; Cho, K.-S.

2014-01-01

We have investigated a supra-arcade structure associated with an M1.6 flare, which occurred on the south-east limb on 2010 November 4. It is observed in EUV with the Atmospheric Imaging Assembly (AIA) on board the Solar Dynamics Observatory, microwaves at 17 and 34 GHz with the Nobeyama Radioheliograph (NoRH), and soft X-rays of 8-20 keV with RHESSI. Interestingly, we found exceptional properties of the supra-arcade thermal plasma from the AIA 131 Å and the NoRH: (1) plasma upflows along large coronal loops and (2) enhancing microwave emission. RHESSI detected two soft X-ray sources, a broad one in the middle of the supra-arcade structure and a bright one just above the flare-arcade. We estimated the number density and thermal energy for these two source regions during the decay phase of the flare. In the supra-arcade source, we found that there were increases of the thermal energy and the density at the early and last stages, respectively. On the contrary, the density and thermal energy of the source on the top of the flare-arcade decreases throughout. The observed upflows imply that there is continuous energy supply into the supra-arcade structure from below during the decay phase of the flare. It is hard to explain by the standard flare model in which the energy release site is located high in the corona. Thus, we suggest that a potential candidate of the energy source for the hot supra-arcade structure is the flare-arcade, which has exhibited a predominant emission throughout.

An experimental study of electron transfer and emission during particle-surface interactions

International Nuclear Information System (INIS)

McGrath, C.T.

2000-09-01

A new coincidence technique has been developed and used to study the secondary electron emission that arises during the interaction of ions with surfaces. This coincidence technique allows the secondary electron emission statistics due to the impact of singly, doubly and multiply charged ions on surfaces to be measured in coincidence with reflected particles, in specific charge states and with specific post-collision trajectories. This system has been used to study the impact of 8 keV H + ions on polycrystalline copper and aluminium targets. Under these conditions the potential emission contribution is negligible and the electron emission is almost entirely due to kinetic emission processes. The sub-surface contribution to the observed electron emission has been isolated using two newly developed models. These models provide valuable information about the depth and amount of surface penetration and on the probability for subsequent electron transport to the surface. The impact of 2 - 100 keV Xe q+ (q = 1 - 10) ions on polycrystalline copper has also been studied using this system. From the subsequent data the potential and kinetic contributions to secondary electron emission have been separated using a previously established model for potential emission. The resulting kinetic emission yield increases with increasing ion impact energy, consistent with current concepts on quasimolecular ionisation. For ions impacting at large incident angles evidence for sub-surface emission has also been observed. The degree of penetration increases with ion impact energy, consistent with current concepts on this effect. The formation of H - ions from incident H + ions has also been studied by measuring the secondary electron emission statistics in coincidence with reflected particles in specific final charge states. This preliminary data is consistent with a two-step process of Auger neutralisation followed by resonant electron capture to the affinity level. However this mechanism

FeNi3/indium tin oxide (ITO) composite nanoparticles with excellent microwave absorption performance and low infrared emissivity

International Nuclear Information System (INIS)

Fu, Li-Shun; Jiang, Jian-Tang; Zhen, Liang; Shao, Wen-Zhu

2013-01-01

Highlights: ► Electrical conductivity and infrared emissivity can be controlled by ITO content. ► The infrared emissivity is the lowest when the mole ratio of In:Sn in sol is 9:1. ► The permittivity in microwave band can be controlled by the electrical conductivity. ► EMA performance is significantly influenced by the content of ITO phase. ► FeNi 3 /ITO composite particles are suitable for both infrared and radar camouflage. - Abstract: FeNi 3 /indium tin oxide (ITO) composite nanoparticles were synthesized by a self-catalyzed reduction method and a sol–gel process. The dependence of the content of ITO phase with the mole ratios of In:Sn of different sols was investigated. The relation between the electrical conductivity, infrared emissivity of FeNi 3 /ITO composite nanoparticles and the content of ITO phase was discussed. Electromagnetic wave absorption (EMA) performance of products was evaluated by using transmission line theory. It was found that EMA performance including the intensity and the location of effective band is significantly dependent on the content of ITO phase. The low infrared emissivity and superior EMA performance of FeNi 3 /ITO composite nanoparticles can be both achieved when the mole ratio of In:Sn in sol is 9:1.

Optimizing the conditions for the microwave-assisted direct liquefaction of Ulva prolifera for bio-oil production using response surface methodology

International Nuclear Information System (INIS)

Liu, Junhai; Zhuang, Yingbin; Li, Yan; Chen, Limei; Guo, Jingxue; Li, Demao; Ye, Naihao

2013-01-01

Microwave-assisted direct liquefaction (MADL) of Ulva prolifera was performed in ethylene glycol (EG) using sulfuric acid (H 2 SO 4 ) as a catalyst. Response Surface Methodology (RSM) based on central composite rotatable design (CCRD) was employed to optimize the conditions of three independent variables (catalyst content, solvent-to-feedstock ratio and temperature) for the liquefaction yield. And the bio-oil was analyzed by elementary analysis, Fourier transform infrared spectroscopic analysis (FT-IR) and gas chromatography–mass spectrometry (GC–MS). The maximum liquefaction yield was 93.17%, which was obtained under a microwave power of 600 W for 30 min at 165 °C with a solvent-to-feedstock ratio of 18.87:1 and 4.93% sulfuric acid. The bio-oil was mainly composed of phthalic acid esters, alkenes and a fatty acid methyl ester with a long chain from C 16 to C 20 . - Highlights: • Ulva prolifera was converted to bio-oil through microwave-assisted direct liquefaction. • Response surface methodology was used to optimize the liquefaction technology. • A maximum liquefaction rate of 93.17 wt% bio-oil was obtained. • The bio-oil was composed of carboxylic acids and esters

Loads due to stray microwave radiation in ITER

Energy Technology Data Exchange (ETDEWEB)

Oosterbeek, Johan W. [ITER Organization, Route de Vinon-sur-Verdon, CS 90 046, 13067 St. Paul Lez Durance Cedex (France); Eindhoven University of Technology, P.O. Box 513, 5600 AZ Eindhoven (Netherlands); Udintsev, Victor S.; Gandini, Franco [ITER Organization, Route de Vinon-sur-Verdon, CS 90 046, 13067 St. Paul Lez Durance Cedex (France); Hirsch, Matthias; Laqua, Heinrich P. [Max-Planck-Institut für Plasmaphysik, EURATOM Association, Teilinstitut Greifswald, D-17489 Greifswald (Germany); Maassen, Nick [Eindhoven University of Technology, P.O. Box 513, 5600 AZ Eindhoven (Netherlands); Ma, Yunxing; Polevoi, Alexei; Sirinelli, Antoine; Vayakis, George; Walsh, Mike J. [ITER Organization, Route de Vinon-sur-Verdon, CS 90 046, 13067 St. Paul Lez Durance Cedex (France)

2015-10-15

High-power microwaves generated by gyrotrons will be extensively used in ITER for a variety of purposes such as assisting plasma breakdown, plasma heating, current drive, tearing mode suppression and as a probing beam for the Collective Thomson Scattering diagnostic. In a number of these schemes absorption of the microwaves by the plasma will not be full and in some cases there could be no absorption at all. This may result in a directed beam with a high microwave power flux or – depending on location and plasma conditions – an approximately isotropic microwave power field. The contribution of electron cyclotron emission to these power densities is briefly discussed. Exposure to in-vessel components leads to absorption by metals and ceramics. In this paper microwave power densities are estimated and, following a brief review of absorption, thermal loads on in-vessel components are assessed. The paper is concluded by a discussion of the current approach to control such loads.

Is X-ray emissivity constant on magnetic flux surfaces?

International Nuclear Information System (INIS)

Granetz, R.S.; Borras, M.C.

1997-01-01

Knowledge of the elongations and shifts of internal magnetic flux surfaces can be used to determine the q profile in elongated tokamak plasmas. X-ray tomography is thought to be a reasonable technique for independently measuring internal flux surface shapes, because it is widely believed that X-ray emissivity should be constant on a magnetic flux surface. In the Alcator C-Mod tokamak, the X-ray tomography diagnostic system consists of four arrays of 38 chords each. A comparison of reconstructed X-ray contours with magnetic flux surfaces shows a small but consistent discrepancy in the radial profile of elongation. Numerous computational tests have been performed to verify these findings, including tests of the sensitivity to calibration and viewing geometry errors, the accuracy of the tomography reconstruction algorithms, and other subtler effects. We conclude that the discrepancy between the X-ray contours and the magnetic flux surfaces is real, leading to the conclusion that X-ray emissivity is not exactly constant on a flux surface. (orig.)

Optimization of dynamic-microwave assisted enzymatic hydrolysis extraction of total ginsenosides from stems and leaves of panax ginseng by response surface methodology.

Science.gov (United States)

Wang, Xiao-Yan; Ren, Hui

2018-03-21

Ginseng stems and leaves (GSAL) are abundant in ginsenosides compounds. For efficient utilization of GSAL and the enhancement of total ginsenosides (TG) compound yields in GSAL, TG from GSAL were extracted, using dynamic-microwave assisted extraction coupled with enzymatic hydrolysis (DMAE-EH) method. The extraction process has been simulated and its main influencing factors such as ethanol concentration, microwave temperature, microwave time and pump flow rate have been optimized by response surface methodology coupled with a Box-Behnken design(BBD). The experimental results indicated that optimal extraction conditions of TG from GSAL were as follows: ethanol concentration of 75%, microwave temperature of 60°C, microwave time of 20 min and pump flow rate of 38 r/min. After experimental verification, the experimental yields of TG was 60.62 ± 0.85 mg g -1 , which were well agreement with the predicted by the model. In general, the present results demonstrated that DMAE-EH method was successfully used to extract total ginsenosides in GSAL.

Global Occurrence and Emission of Rotaviruses to Surface Waters

Directory of Open Access Journals (Sweden)

Nicholas M. Kiulia

2015-05-01

Full Text Available Group A rotaviruses (RV are the major cause of acute gastroenteritis in infants and young children globally. Waterborne transmission of RV and the presence of RV in water sources are of major public health importance. In this paper, we present the Global Waterborne Pathogen model for RV (GloWPa-Rota model to estimate the global distribution of RV emissions to surface water. To our knowledge, this is the first model to do so. We review the literature to estimate three RV specific variables for the model: incidence, excretion rate and removal during wastewater treatment. We estimate total global RV emissions to be 2 × 1018 viral particles/grid/year, of which 87% is produced by the urban population. Hotspot regions with high RV emissions are urban areas in densely populated parts of the world, such as Bangladesh and Nigeria, while low emissions are found in rural areas in North Russia and the Australian desert. Even for industrialized regions with high population density and without tertiary treatment, such as the UK, substantial emissions are estimated. Modeling exercises like the one presented in this paper provide unique opportunities to further study these emissions to surface water, their sources and scenarios for improved management.

Snow water equivalent monitoring retrieved by assimilating passive microwave observations in a coupled snowpack evolution and microwave emission models over North-Eastern Canada

Science.gov (United States)

Royer, A.; Larue, F.; De Sève, D.; Roy, A.; Vionnet, V.; Picard, G.; Cosme, E.

2017-12-01

Over northern snow-dominated basins, the snow water equivalent (SWE) is of primary interest for spring streamflow forecasting. SWE retrievals from satellite data are still not well resolved, in particular from microwave (MW) measurements, the only type of data sensible to snow mass. Also, the use of snowpack models is challenging due to the large uncertainties in meteorological input forcings. This project aims to improve SWE prediction by assimilation of satellite brightness temperature (TB), without any ground-based observations. The proposed approach is the coupling of a detailed multilayer snowpack model (Crocus) with a MW snow emission model (DMRT-ML). The assimilation scheme is a Sequential Importance Resampling Particle filter, through ensembles of perturbed meteorological forcings according to their respective uncertainties. Crocus simulations driven by operational meteorological forecasts from the Canadian Global Environmental Multiscale model at 10 km spatial resolution were compared to continuous daily SWE measurements over Québec, North-Eastern Canada (56° - 45°N). The results show a mean bias of the maximum SWE overestimated by 16% with variations up to +32%. This observed large variability could lead to dramatic consequences on spring flood forecasts. Results of Crocus-DMRT-ML coupling compared to surface-based TB measurements (at 11, 19 and 37 GHz) show that the Crocus snowpack microstructure described by sticky hard spheres within DMRT has to be scaled by a snow stickiness of 0.18, significantly reducing the overall RMSE of simulated TBs. The ability of assimilation of daily TBs to correct the simulated SWE is first presented through twin experiments with synthetic data, and then with AMSR-2 satellite time series of TBs along the winter taking into account atmospheric and forest canopy interferences (absorption and emission). The differences between TBs at 19-37 GHz and at 11-19 GHz, in vertical polarization, were assimilated. This assimilation

Improving surface-enhanced Raman scattering effect using gold-coated hierarchical polystyrene bead substrates modified with postgrowth microwave treatment.

Science.gov (United States)

Yuen, Clement; Zheng, Wei; Huang, Zhiwei

2008-01-01

We report a novel postgrowth microwave heating implementation by selectively modifying hierarchical polystyrene (PS) bead substrates coated with gold (Au) films to effectively improve the surface-enhanced Raman scattering (SERS) effect on the analytes. The SERS signal of probe molecule rhodamine 6G (Rh 6G) on the microwave-treated Au-PS substrates can be improved by 10-fold, while the detection limit of Rh 6G in concentration can be enhanced by two orders of magnitude compared to the as-growth substrates. The high-quality SERS spectrum of saliva can also be acquired using the modified substrates, demonstrating the potential for the realization of the high-performance SERS substrates for biomedical applications.

Mineral distribution in rice: Measurement by Microwave Plasma Atomic Emission Spectroscopy (MP-AES)

International Nuclear Information System (INIS)

Ramos, Nerissa C.; Ramos, R.G.A.; Quirit, L.L.; Arcilla, C.A.

2015-01-01

Microwave Plasma Atomic Emission Spectroscopy (MP-AES) is a new technology with comparable performance and sensitivity to Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES). Both instrument use plasma as the energy source that produces atomic and ionic emission lines. However, MP-AES uses nitrogen as the plasma gas instead of argon which is an additional expense for ICP-OES. Thus, MP-AES is more economical. This study quantified six essential minerals (Se, Zn, Fe, Cu, Mn and K) in rice using MP-AES. Hot plate digestion was used for sample extraction and the detection limit for each instrument was compared with respect to the requirement for routine analysis in rice. Black, red and non-pigmented rice samples were polished in various intervals to determine the concentration loss of minerals. The polishing time corresponds to the structure of the rice grains such as outer bran layer (0 to 15), inner bran layer (15 to 30), outer endosperm layer (30 to 45), and middle endosperm layer (45 to 60). Results of MP-AES analysis showed that black rice had all essential materials (except K) in high concentration at the outer bran layer. The red and non-pigmented rice samples on the other hand, contained high levels of Se, Zn, Fe, and Mn in the whole bran portion. After 25 seconds, the mineral concentrations remained constant. The concentration of Cu however, gave consistent value in all polishing intervals, hence Cu might be located in the inner endosperm layer. Results also showed that K was uniformly distributed in all samples where 5% loss was consistently observed for every polishing interval. Therefore, the concentration of K was also affected by polishing time. Thus, the new MP-AES technology with comparable performance to ICP-OES is a promising tool for routine analysis in rice. (author)

Discussion on Microwave-Matter Interaction Mechanisms by In Situ Observation of "Core-Shell" Microstructure during Microwave Sintering.

Science.gov (United States)

Liu, Wenchao; Xu, Feng; Li, Yongcun; Hu, Xiaofang; Dong, Bo; Xiao, Yu

2016-02-23

This research aims to deepen the understanding of the interaction mechanisms between microwave and matter in a metal-ceramic system based on in situ synchrotron radiation computed tomography. A special internal "core-shell" microstructure was discovered for the first time and used as an indicator for the interaction mechanisms between microwave and matter. Firstly, it was proved that the microwave magnetic field acted on metal particles by way of inducing an eddy current in the surface of the metal particles, which led to the formation of a "core-shell" microstructure in the metal particles. On this basis, it was proposed that the ceramic particles could change the microwave field and open a way for the microwave, thereby leading to selective heating in the region around the ceramic particles, which was verified by the fact that all the "core-shell" microstructure was located around ceramic particles. Furthermore, it was indicated that the ceramic particles would gather the microwaves, and might lead to local heating in the metal-ceramic contact region. The focusing of the microwave was proved by the quantitative analysis of the evolution rate of the "core-shell" microstructure in a different region. This study will help to reveal the microwave-matter interaction mechanisms during microwave sintering.

Dependence of the microwave surface resistance of superconducting niobium on the magnitude of the rf field

Energy Technology Data Exchange (ETDEWEB)

Romanenko, A.; Grassellino, A. [Fermi National Accelerator Laboratory, Batavia, Illinois 60510 (United States)

2013-06-24

Utilizing difference in temperature dependencies we decoupled Bardeen-Cooper-Schrieffer (BCS) and residual components of the microwave surface resistance of superconducting niobium at all rf fields up to B{sub rf}{approx}115 mT. We reveal that the residual resistance decreases with field at B{sub rf} Less-Than-Or-Equivalent-To 40 mT and strongly increases in chemically treated niobium at B{sub rf}>80 mT. We find that BCS surface resistance is weakly dependent on field in the clean limit, whereas a strong and peculiar field dependence emerges after 120 Degree-Sign C vacuum baking.

GREENER SYNTHESIS OF HETEROCYCLIC COMPOUNDS USING MICROWAVE IRRADIATION

Science.gov (United States)

An introduction of our interest in the microwave-assisted greener synthesis of a variety of heterocyclic compounds will be presented. It involves microwave (MW) exposure of neat reactants (undiluted) catalyzed by the surfaces of recyclable mineral supports, such as alumina, sili...

The Passive Microwave Remote Sensing of Soil Moisture: the Effect of Tilled Row Structure

Science.gov (United States)

Wang, J. R.; Newton, R. W.; Rouse, J. W.

1979-01-01

The tilled rowstructure is known to be one of the important factors affecting the observations of the microwave emission from a natural surface. Measurements of this effect were carried out with both I and X band radiometers mounted on a mobile truck on a bare 40 m x 45 m row tilled field. The soil moisture content during the measurements ranged from approximately 10 percent to approximately 30 percent by dry weight. The results of these measurements showed that the variations of the antenna temperatures with incident angle theta changed with the azimuthal angle a measured from the row direction. A numerical calculation based on a composite surface roughness was made and found to predict the observed features within the model's limit of accuracy. It was concluded that the difference between the horizontally and vertically polarized temperatures was due to the change in the local angle of field emission within the antenna field of view caused by the large scale row structure.

High power microwave emission and diagnostics of microsecond electron beams

Energy Technology Data Exchange (ETDEWEB)

Gilgenbach, R; Hochman, J M; Jayness, R; Rintamaki, J I; Lau, Y Y; Luginsland, J; Lash, J S [Univ. of Michigan, Ann Arbor, MI (United States). Intense Electron Beam Interaction Lab.; Spencer, T A [Air Force Phillips Lab., Kirtland AFB, NM (United States)

1997-12-31

Experiments were performed to generate high power, long-pulse microwaves by the gyrotron mechanism in rectangular cross-section interaction cavities. Long-pulse electron beams are generated by MELBA (Michigan Electron Long Beam Accelerator), which operates with parameters: -0.8 MV, 1-10 kA, and 0.5-1 microsecond pulse length. Microwave power levels are in the megawatt range. Polarization control is being studied by adjustment of the solenoidal magnetic field. Initial results show polarization power ratios up to a factor of 15. Electron beam dynamics (V{sub perp}/V{sub par}) are being measured by radiation darkening on glass plates. Computer modeling utilizes the MAGIC Code for electromagnetic waves and a single electron orbit code that includes a distribution of angles. (author). 4 figs., 4 refs.

Microwave-assisted hydrothermal synthesis of lead zirconate fine powders

Directory of Open Access Journals (Sweden)

Apinpus Rujiwatra

2011-01-01

Full Text Available A rapid synthesis of lead zirconate fine powders by microwave-assisted hydrothermal technique is reported. The influences of type of lead precursor, concentration of potassium hydroxide mineraliser, applied microwave power and irradiation time are described. The synthesised powders were characterised by powder X-ray diffraction, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopic microanalysis and light scattering technique. The merits of the microwave application in reducing reaction time and improving particle mono-dispersion and size uniformity as well as the drawbacks, viz. low purity of the desired phase and increasing demand of mineraliser, are discussed in relation to conventional heating method.

Isotherms clustering in cosmic microwave background

International Nuclear Information System (INIS)

Bershadskii, A.

2006-01-01

Isotherms clustering in cosmic microwave background (CMB) has been studied using the 3-year WMAP data on cosmic microwave background radiation. It is shown that the isotherms clustering could be produced by the baryon-photon fluid turbulence in the last scattering surface. The Taylor-microscale Reynolds number of the turbulence is estimated directly from the CMB data as Re λ ∼10 2

Removal of concrete layers from biological shields by microwaves

International Nuclear Information System (INIS)

Wace, P.F.; Harker, A.H.; Hills, D.L.

1990-01-01

A comprehensive literature review has been carried out, to provide information for an experimental programme and equipment design. Mathematical modelling of the microwave and power fields in a concrete block, both steel reinforced and unreinforced, subjected to a microwave attack at two frequencies, has been carried out and estimates of the likely temperature rise with time obtained. A method of launching microwaves into concrete has been established from theoretical considerations and from the findings of the literature review. Equipment for laboratory trials has been designed and assembled using an 896 MHz, 25 kW microwave generator. Reinforced concrete blocks, 0.6 m in dimension and representing the concrete in a Magnox reactor biological shield, have been attacked at different power levels and the surface removed to the depth of the reinforcing steel (100 mm). Outline proposals for the design of a remotely operated prototype microwave machine for stripping the surface of large concrete test panels have been prepared. (author)

Microwave effective surface impedance of structures including a high-Tc superconducting film

International Nuclear Information System (INIS)

Hartemann, P.

1992-01-01

The microwave effective surface impedances of different stacks made of high-temperature superconducting films, dielectric materials and bulk normal metals were computed. The calculations were based on the two-fluid model of superconductors and the conventional transmission line theory. These effective impedances are compared to the calculated intrinsic surface impedances of the stacked superconducting films. The considered superconducting material has been the oxide YBa 2 Cu 3 O 7 epitaxially grown on crystalline substrates (MgO, LaAlO 3 , SrTiO 3 ), the film thickness ranging from a few nm to 1μm. Discrepancies between the effective surface resistances or reactances and the corresponding intrinsic values were determined at 10 GHz for non resonant or resonant structures. At resonance the surface resistance discrepancy exhibits a sharp peak which reaches 10 4 or more in relative value according to the geometry and the used materials. Obviously the effective surface reactance shows also huge variations about the resonance and may be negative. Moreover geometries allowing to obtain an effective resistance smaller than the film intrinsic value have been found. The effects of the resonance phenomenon on the electromagnetic wave reflectivity and reflection phase shift are investigated. Therefore the reported theoretical results demonstrate that the effective surface impedance of YBCO films with a thickness smaller than 500 nm can be very different from the intrinsic film impedance according to the structures. (Author). 3 refs., 10 figs., 2 tabs

Electron field emission for ultrananocrystalline diamond films

Energy Technology Data Exchange (ETDEWEB)

Krauss, A. R.; Auciello, O.; Ding, M. Q.; Gruen, D. M.; Huang, Y.; Zhirnov, V. V.; Givargizov, E. I.; Breskin, A.; Chechen, R.; Shefer, E. (and others)

2001-03-01

Ultrananocrystalline diamond (UNCD) films 0.1--2.4 {mu}m thick were conformally deposited on sharp single Si microtip emitters, using microwave CH{sub 4}--Ar plasma-enhanced chemical vapor deposition in combination with a dielectrophoretic seeding process. Field-emission studies exhibited stable, extremely high (60--100 {mu}A/tip) emission current, with little variation in threshold fields as a function of film thickness or Si tip radius. The electron emission properties of high aspect ratio Si microtips, coated with diamond using the hot filament chemical vapor deposition (HFCVD) process were found to be very different from those of the UNCD-coated tips. For the HFCVD process, there is a strong dependence of the emission threshold on both the diamond coating thickness and Si tip radius. Quantum photoyield measurements of the UNCD films revealed that these films have an enhanced density of states within the bulk diamond band gap that is correlated with a reduction in the threshold field for electron emission. In addition, scanning tunneling microscopy studies indicate that the emission sites from UNCD films are related to minima or inflection points in the surface topography, and not to surface asperities. These data, in conjunction with tight binding pseudopotential calculations, indicate that grain boundaries play a critical role in the electron emission properties of UNCD films, such that these boundaries: (a) provide a conducting path from the substrate to the diamond--vacuum interface, (b) produce a geometric enhancement in the local electric field via internal structures, rather than surface topography, and (c) produce an enhancement in the local density of states within the bulk diamond band gap.

CuO urchin-nanostructures synthesized from a domestic hydrothermal microwave method

International Nuclear Information System (INIS)

Keyson, D.; Volanti, D.P.; Cavalcante, L.S.; Simoes, A.Z.; Varela, J.A.; Longo, E.

2008-01-01

This letter reports the synthesis of CuO urchin-nanostructures by a simple and novel hydrothermal microwave method. The formation and growth of urchin-nanostructures is mainly affected by the addition of polyethylene glycol (PEG). The hierarchical malachite particles are uniform spheres with a diameter of 0.7-1.9 μm. CuO urchin-nanostructures were characterized by X-ray diffraction (XRD), field-emission scanning electron microscopy (FEG-SEM) and nitrogen adsorption (BET). The specific surface area of the CuO nanostructured microspheres was about 170.5 m 2 /g. A possible mechanism for the formation of such CuO urchin-nanostructures is proposed

Sea Surface Salinity and Wind Retrieval Algorithm Using Combined Passive-Active L-Band Microwave Data

Science.gov (United States)

Yueh, Simon H.; Chaubell, Mario J.

2011-01-01

Aquarius is a combined passive/active L-band microwave instrument developed to map the salinity field at the surface of the ocean from space. The data will support studies of the coupling between ocean circulation, the global water cycle, and climate. The primary science objective of this mission is to monitor the seasonal and interannual variation of the large scale features of the surface salinity field in the open ocean with a spatial resolution of 150 kilometers and a retrieval accuracy of 0.2 practical salinity units globally on a monthly basis. The measurement principle is based on the response of the L-band (1.413 gigahertz) sea surface brightness temperatures (T (sub B)) to sea surface salinity. To achieve the required 0.2 practical salinity units accuracy, the impact of sea surface roughness (e.g. wind-generated ripples and waves) along with several factors on the observed brightness temperature has to be corrected to better than a few tenths of a degree Kelvin. To the end, Aquarius includes a scatterometer to help correct for this surface roughness effect.

Enhancement of adhesion between carbon nanotubes and polymer substrates using microwave irradiation

International Nuclear Information System (INIS)

Shim, Hyung Cheoul; Kwak, Yoon Keun; Han, Chang-Soo; Kim, Soohyun

2009-01-01

This paper reports the enhancement of adhesive strength between single-walled carbon nanotubes (SWNTs) and polymer substrates using microwave irradiation of 0-5 min duration at 2.45 GHz and 800 W. Field emission scanning electron microscopy images, ultraviolet-visible data and four-point probe sheet resistance measurement data indicate that microwave irradiation is effective for enhancement of adhesion between SWNTs and polymer substrates. SWNTs could be locally welded onto a polymer substrate due to their active response to microwave irradiation.

Ultrafast Formation of ZnO Nanorods via Seed-Mediated Microwave Assisted Hydrolysis Process

International Nuclear Information System (INIS)

Tan, S T; Yahaya, M; Yap, C C; Umar, A A; Salleh, M M

2013-01-01

One dimensional (1D) zinc oxide, ZnO nanostructures have shown promising results for usage in photodiode and optoelectronic device due to their high surface area. Faster and conventional method for synthesis ZnO nanorods has become an attention for researcher today. In this paper, ZnO nanorods have been successfully synthesized via two-step process, namely alcothermal seeding and seed-mediated microwave hydrolysis process. In typical process, the ZnO nanoseeds were grown in the growth solution that contained equimolar (0.04 M) of zinc nitrate hexahydrate, Zn (NO 3 ).6H 2 O and hexamethylenetetramine, HMT. The growth process was carried inside the inverted microwave within 5- 20 s. The effect of growth parameters (i.e. concentration, microwave power, time reaction) upon the modification of ZnO morphology was studied. ZnO nanostructures were characterized by Field emission scanning electron microscope (FESEM) and X-ray diffraction (XRD). The densities of nanorods were evaluated by the Image J analysis. It was found that the morphology (e.g. shape and size) of nanostructures has changed drastically with the increment of growth solution concentration. The density of ZnO nanorods was proven to increase with the increasing of reaction time and microwave power. We hypothesize that the microwave power might enhance the rate of nucleation and promote the faster nanostructure growth as compared with the normal heating condition due to the superheating phenomenon. This method might promote a new and faster alternative way in nanostructure growth which can be applied in currently existing application.

Ultrafast Formation of ZnO Nanorods via Seed-Mediated Microwave Assisted Hydrolysis Process

Science.gov (United States)

Tan, S. T.; Umar, A. A.; Yahaya, M.; Yap, C. C.; Salleh, M. M.

2013-04-01

One dimensional (1D) zinc oxide, ZnO nanostructures have shown promising results for usage in photodiode and optoelectronic device due to their high surface area. Faster and conventional method for synthesis ZnO nanorods has become an attention for researcher today. In this paper, ZnO nanorods have been successfully synthesized via two-step process, namely alcothermal seeding and seed-mediated microwave hydrolysis process. In typical process, the ZnO nanoseeds were grown in the growth solution that contained equimolar (0.04 M) of zinc nitrate hexahydrate, Zn (NO3).6H2O and hexamethylenetetramine, HMT. The growth process was carried inside the inverted microwave within 5- 20 s. The effect of growth parameters (i.e. concentration, microwave power, time reaction) upon the modification of ZnO morphology was studied. ZnO nanostructures were characterized by Field emission scanning electron microscope (FESEM) and X-ray diffraction (XRD). The densities of nanorods were evaluated by the Image J analysis. It was found that the morphology (e.g. shape and size) of nanostructures has changed drastically with the increment of growth solution concentration. The density of ZnO nanorods was proven to increase with the increasing of reaction time and microwave power. We hypothesize that the microwave power might enhance the rate of nucleation and promote the faster nanostructure growth as compared with the normal heating condition due to the superheating phenomenon. This method might promote a new and faster alternative way in nanostructure growth which can be applied in currently existing application.

Spectrum of the Anomalous Microwave Emission in the North Celestial Pole with WMAP 7-Year Data

Directory of Open Access Journals (Sweden)

Anna Bonaldi

2012-01-01

Full Text Available We estimate the frequency spectrum of the diffuse anomalous microwave emission (AME on the North Celestial Pole (NCP region of the sky with the Correlated Component Analysis (CCA component separation method applied to WMAP 7-yr data. The NCP is a suitable region for this analysis because the AME is weakly contaminated by synchrotron and free-free emission. By modeling the AME component as a peaked spectrum we estimate the peak frequency to be 21.7±0.8 GHz, in agreement with previous analyses which favored νp < 23 GHz. The ability of our method to correctly recover the position of the peak is verified through simulations. We compare the estimated AME spectrum with theoretical spinning dust models to constrain the hydrogen density nH. The best results are obtained with densities around 0.2–0.3 cm−3, typical of warm ionised medium (WIM to warm neutral medium (WNM conditions. The degeneracy with the gas temperature prevents an accurate determination of nH, especially for low hydrogen ionization fractions, where densities of a few cm−3 are also allowed.

Polarization of Magnetic Dipole Emission and Spinning Dust Emission from Magnetic Nanoparticles

OpenAIRE

Hoang, Thiem; Lazarian, A.

2015-01-01

Magnetic dipole emission (MDE) from interstellar magnetic nanoparticles is an important Galactic foreground in the microwave frequencies, and its polarization level may pose great challenges for achieving reliable measurements of cosmic microwave background (CMB) B-mode signal. To obtain theoretical constraints on the polarization of MDE, we first compute the degree of alignment of big silicate grains incorporated with magnetic inclusions. We find that, in realistic conditions of the interste...

Integrated Advanced Microwave Sounding Unit-A (AMSU-A). Engineering Test Report: Radiated Emissions and SARR, SARP, DCS Receivers, Link Frequencies EMI Sensitive Band Test Results, AMSU-A1, S/N 109

Science.gov (United States)

Valdez, A.

2000-01-01

This is the Engineering Test Report, Radiated Emissions and SARR, SARP, DCS Receivers, Link Frequencies EMI Sensitive Band Test Results, AMSU-A1, S/N 109, for the Integrated Advanced Microwave Sounding Unit-A (AMSU-A).

Microwave alkaline roasting-water dissolving process for germanium extraction from zinc oxide dust and its analysis by response surface methodology (RSM)

Science.gov (United States)

Wang, Wankun; Wang, Fuchun; Lu, Fanghai

2017-12-01

Microwave alkaline roasting-water dissolving process was proposed to improve the germanium (Ge) extraction from zinc oxide (ZnO) dust. The effects of important parameters were investigated and the process conditions were optimized using response surface methodology (RSM). The Ge extraction is consistent with the linear polynomial model type. Alkali-material ratio, microwave heating temperature and leaching temperature are the significant factors for this process. The optimized conditions are obtained as follows, alkali-material ratio of 0.9 kg/kg, aging time of 1.12 day, microwave heating at 658 K for 10 min, liquid-solid ratio of 4.31 L/kg, leaching temperature at 330 K, leaching time of 47 min with the Ge extraction about 99.38%. It is in consistence with the predictive value of 99.31%. Compared to the existed alkaline roasting process heated by electric furnace in literature, the alkaline roasting temperature and holding time. It shows a good prospect on leaching Ge from ZnO dust with microwave alkaline roasting-water dissolving process.

A comparative study of different processing methods and microwave surface conductivity of 1-2-3 superconducting ceramics

International Nuclear Information System (INIS)

Sundar, H.G.K.; Wilson, C.; Horzog, D.

1988-01-01

Superconducting YBa/sub 2/Cu/sub 3/O/sub 6+x/ samples were made from powders prepared by different routes: solid state reaction, amorphous citrate and Pechini method. The powders produced by solid state reaction were milled to different degrees, calcined and sintered. Samples were also hot pressed at 875 C and subsequently annealed at different temperatures to regain the superconducting phase. In order to compare the amount of residual carbonate in the final materials prepared by solid state and liquid mix methods, XPS spectra were taken on as calcined powder and on material sintered at different temperatures. To our surprise, the amount of carbonate was quite small in both the methods, but this amount increased with sintering temperature. The microwave surface conductivity of 1-2-3 superconducting material was measured in a disk resonator configuration. At liquid nitrogen temperatures the microwave conductivity was comparable to that of gold and improved with decreasing temperature. At --10K the conductivity was two orders of magnitude greater than that of gold at the same temperature. The surface conductivity of samples obtained by Pechini method was much better than that obtained by solid state method

Hard X-ray emission from accretion shocks around galaxy clusters

Science.gov (United States)

Kushnir, Doron; Waxman, Eli

2010-02-01

We show that the hard X-ray (HXR) emission observed from several galaxy clusters is consistent with a simple model, in which the nonthermal emission is produced by inverse Compton scattering of cosmic microwave background photons by electrons accelerated in cluster accretion shocks: The dependence of HXR surface brightness on cluster temperature is consistent with that predicted by the model, and the observed HXR luminosity is consistent with the fraction of shock thermal energy deposited in relativistic electrons being lesssim0.1. Alternative models, where the HXR emission is predicted to be correlated with the cluster thermal emission, are disfavored by the data. The implications of our predictions to future HXR observations (e.g. by NuStar, Simbol-X) and to (space/ground based) γ-ray observations (e.g. by Fermi, HESS, MAGIC, VERITAS) are discussed.

Hard X-ray emission from accretion shocks around galaxy clusters

Energy Technology Data Exchange (ETDEWEB)

Kushnir, Doron; Waxman, Eli, E-mail: doron.kushnir@weizmann.ac.il, E-mail: eli.waxman@weizmann.ac.il [Physics Faculty, Weizmann Institute of Science, PO Box 26, Rehovot (Israel)

2010-02-01

We show that the hard X-ray (HXR) emission observed from several galaxy clusters is consistent with a simple model, in which the nonthermal emission is produced by inverse Compton scattering of cosmic microwave background photons by electrons accelerated in cluster accretion shocks: The dependence of HXR surface brightness on cluster temperature is consistent with that predicted by the model, and the observed HXR luminosity is consistent with the fraction of shock thermal energy deposited in relativistic electrons being ∼<0.1. Alternative models, where the HXR emission is predicted to be correlated with the cluster thermal emission, are disfavored by the data. The implications of our predictions to future HXR observations (e.g. by NuStar, Simbol-X) and to (space/ground based) γ-ray observations (e.g. by Fermi, HESS, MAGIC, VERITAS) are discussed.

Hard X-ray emission from accretion shocks around galaxy clusters

International Nuclear Information System (INIS)

Kushnir, Doron; Waxman, Eli

2010-01-01

We show that the hard X-ray (HXR) emission observed from several galaxy clusters is consistent with a simple model, in which the nonthermal emission is produced by inverse Compton scattering of cosmic microwave background photons by electrons accelerated in cluster accretion shocks: The dependence of HXR surface brightness on cluster temperature is consistent with that predicted by the model, and the observed HXR luminosity is consistent with the fraction of shock thermal energy deposited in relativistic electrons being ∼<0.1. Alternative models, where the HXR emission is predicted to be correlated with the cluster thermal emission, are disfavored by the data. The implications of our predictions to future HXR observations (e.g. by NuStar, Simbol-X) and to (space/ground based) γ-ray observations (e.g. by Fermi, HESS, MAGIC, VERITAS) are discussed

Field emission and high voltage cleaning of particulate contaminants on extended metallic surfaces

International Nuclear Information System (INIS)

Tan, J.; Bonin, B.; Safa, H.

1996-01-01

The vacuum insulation properties of extended metallic surfaces depends strongly on their cleanliness. The usual technique to reduce electronic field emission from such surfaces consists in exposing them to very high electric fields during limited periods of time. This kind of processing also reduces the occurrence of vacuum breakdown. The processing of the surface is generally believed to be due to a thermomechanical destruction of the emitting sites, initiated by the emission itself. Comparison of the electric forces vs adherence forces which act on dust particles lying on the surface shows that the processing could also be due simply to the mechanical removal of the dust particles, with a subsequent reduction of field emission from the contaminated surface. (author)

Influence of the density of the microwave plasma in the nitridation of the AISI 4140 steel

International Nuclear Information System (INIS)

Chirino O, S.; Camps C, E.; Escobar A, L.; Mejia H, J.A.

2004-01-01

A source of microwaves plasma type ECR was used to modify those mechanical properties of the surface of steel pieces AISI 4140. The experiments were carried out in a range of pressure among 4 X 10 -4 and 7 X 10 -4 Torr using one mixture of gases 60/40 hydrogen / nitrogen and an incident power of the microwaves of 400 W. Previous to the treatment of the samples, the plasma was studied using one Langmuir probe to determine the temperature of the electrons and the density of the plasma, the species excited in the plasma were determined by means of Optical emission spectroscopy. All the samples were treated during 50 min in a regime of low temperature (- 250 C), and the surface hardness it was increased up of 100% of their initial value, with a depth of penetration of the nitrogen of 4.5 μ m. The biggest hardness and depth of penetration of the nitrogen were obtained when the biggest density in the plasma was used to carry out the experiments. (Author)

Effects of fibre-form nanostructures on particle emissions from a tungsten surface in plasmas

International Nuclear Information System (INIS)

Takamura, S.; Miyamoto, T.; Ohno, N.

2012-01-01

The effects of fibre-form nanostructure of a tungsten surface on both electron emission and sputtering in helium/argon plasmas are represented. Generally, a nano-fibre forest, the so-called ‘fuzz’, made of tungsten with helium gas inside is found to have the tendency of suppressing the particle emission substantially. The electron emission comes from the impact of high-energy primary electrons. In addition, a deeply biased tungsten target, which inhibits the influx of even energetic primary electrons, seems to produce an electron emission, and it may be suppressed on the way to nanostructure formation on the surface of the W target. Such an emission process is discussed here. The sputtering yield of the He-damaged tungsten surface with the fibre-form nanostructure depends on the surface morphology while the sputtering itself changes the surface morphology, so that the time evolutions of sputtering yield from the W surface with an originally well-developed nanostructure are found to show a minimum in sputtering yield, which is about a half for the fresh nanostructured tungsten and roughly one-fifth of the yield for the original flat normal tungsten surface. The surface morphology at that time is, for the first time, made clear with field emission scanning electron microscopy observation. The physical mechanism for the appearance of such a minimum in sputtering yield is discussed. (paper)

Trends in the Microwave-Assisted Synthesis of Metal Oxide Nanoparticles Supported on Carbon Nano tubes and Their Applications

International Nuclear Information System (INIS)

Motshekga, S.C.; Pillai, S.K.; Ray, S.S.; Motshekga, S.C.; Ray, S.S.; Jalama, K.; Krause, Rui.W.M.

2012-01-01

The study of coating carbon nano tubes with metal/oxides nanoparticles is now becoming a promising and challenging area of research. To optimize the use of carbon nano tubes in various applications, it is necessary to attach functional groups or other nano structures to their surface. The combination of the distinctive properties of carbon nano tubes and metal/oxides is expected to be applied in field emission displays, nano electronic devices, novel catalysts, and polymer or ceramic reinforcement. The synthesis of these composites is still largely based on conventional techniques, such as wet impregnation followed by chemical reduction of the metal nanoparticle precursors. These techniques based on thermal heating can be time consuming and often lack control of particle size and morphology. Hence, there is interest in microwave technology recently, where using microwaves represents an alternative way of power input into chemical reactions through dielectric heating. This paper covers the synthesis and applications of carbon-nano tube-coated metal/oxides nanoparticles prepared by a microwave-assisted method. The reviewed studies show that the microwave-assisted synthesis of the composites allows processes to be completed within a shorter reaction time with uniform and well-dispersed nanoparticle formation.

Recent Trends in the Microwave-Assisted Synthesis of Metal Oxide Nanoparticles Supported on Carbon Nanotubes and Their Applications

Directory of Open Access Journals (Sweden)

Sarah C. Motshekga

2012-01-01

Full Text Available The study of coating carbon nanotubes with metal/oxides nanoparticles is now becoming a promising and challenging area of research. To optimize the use of carbon nanotubes in various applications, it is necessary to attach functional groups or other nanostructures to their surface. The combination of the distinctive properties of carbon nanotubes and metal/oxides is expected to be applied in field emission displays, nanoelectronic devices, novel catalysts, and polymer or ceramic reinforcement. The synthesis of these composites is still largely based on conventional techniques, such as wet impregnation followed by chemical reduction of the metal nanoparticle precursors. These techniques based on thermal heating can be time consuming and often lack control of particle size and morphology. Hence, there is interest in microwave technology recently, where using microwaves represents an alternative way of power input into chemical reactions through dielectric heating. This paper covers the synthesis and applications of carbon-nanotube-coated metal/oxides nanoparticles prepared by a microwave-assisted method. The reviewed studies show that the microwave-assisted synthesis of the composites allows processes to be completed within a shorter reaction time with uniform and well-dispersed nanoparticle formation.

Effect of surface morphology and densification on the infrared emissivity of C/SiC composites

International Nuclear Information System (INIS)

Wang, Fuyuan; Cheng, Laifei; Zhang, Qing; Zhang, Litong

2014-01-01

Highlights: • The cauliflower-like microstructure improved the infrared emissivity multiply. • The infrared emissivity decreased continually with the improving surface flatness. • The densification process boosted the infrared emissivity. - Abstract: The effects of surface morphology and densification on the infrared emissivity of 2D C/SiC composites were investigated in 6–16 μm from 1000 °C to 1600 °C. As the sample surface was polished, the reflection and scattering for the electromagnetic waves of thermal radiation were reduced, causing a sustained decrease in the infrared emissivity. The space-variant polarizations caused by the cauliflower-like microstructure were enervated in the smooth surface, which enhanced the reduction trendy in the infrared emissivity. In densification process, the increasing SiC content and the growing amount of the cauliflower-like microstructure on sample surface improved the infrared emissivity of C/SiC composites, while the decreasing porosity decreased it. Due to the greater positive effects on the thermal radiation during the densification process, the infrared emissivity of C/SiC composites increased successively with density

Effect of surface morphology and densification on the infrared emissivity of C/SiC composites

Energy Technology Data Exchange (ETDEWEB)

Wang, Fuyuan, E-mail: wangfy1986@gmail.com; Cheng, Laifei; Zhang, Qing, E-mail: zhangqing@nwpu.edu.cn; Zhang, Litong

2014-09-15

Highlights: • The cauliflower-like microstructure improved the infrared emissivity multiply. • The infrared emissivity decreased continually with the improving surface flatness. • The densification process boosted the infrared emissivity. - Abstract: The effects of surface morphology and densification on the infrared emissivity of 2D C/SiC composites were investigated in 6–16 μm from 1000 °C to 1600 °C. As the sample surface was polished, the reflection and scattering for the electromagnetic waves of thermal radiation were reduced, causing a sustained decrease in the infrared emissivity. The space-variant polarizations caused by the cauliflower-like microstructure were enervated in the smooth surface, which enhanced the reduction trendy in the infrared emissivity. In densification process, the increasing SiC content and the growing amount of the cauliflower-like microstructure on sample surface improved the infrared emissivity of C/SiC composites, while the decreasing porosity decreased it. Due to the greater positive effects on the thermal radiation during the densification process, the infrared emissivity of C/SiC composites increased successively with density.

Effect of metallic and hyperbolic metamaterial surface on electric and magnetic dipole emission

DEFF Research Database (Denmark)

Ni, Xingjie; Naik, Gururaj V.; Kildishev, Alexander V.

2010-01-01

Spontaneous emission patterns of electric and magnetic dipoles on different material surfaces were studied numerically and experimentally. The results show the modified behavior of electric and magnetic dipoles on metallic and HMM surfaces.......Spontaneous emission patterns of electric and magnetic dipoles on different material surfaces were studied numerically and experimentally. The results show the modified behavior of electric and magnetic dipoles on metallic and HMM surfaces....

Multimodel Surface Temperature Responses to Removal of U.S. Sulfur Dioxide Emissions

Science.gov (United States)

Conley, A. J.; Westervelt, D. M.; Lamarque, J.-F.; Fiore, A. M.; Shindell, D.; Correa, G.; Faluvegi, G.; Horowitz, L. W.

2018-03-01

Three Earth System models are used to derive surface temperature responses to removal of U.S. anthropogenic SO2 emissions. Using multicentury perturbation runs with and without U.S. anthropogenic SO2 emissions, the local and remote surface temperature changes are estimated. In spite of a temperature drift in the control and large internal variability, 200 year simulations yield statistically significant regional surface temperature responses to the removal of U.S. SO2 emissions. Both local and remote surface temperature changes occur in all models, and the patterns of changes are similar between models for northern hemisphere land regions. We find a global average temperature sensitivity to U.S. SO2 emissions of 0.0055 K per Tg(SO2) per year with a range of (0.0036, 0.0078). We examine global and regional responses in SO4 burdens, aerosol optical depths (AODs), and effective radiative forcing (ERF). While changes in AOD and ERF are concentrated near the source region (United States), the temperature response is spread over the northern hemisphere with amplification of the temperature increase toward the Arctic. In all models, we find a significant response of dust concentrations, which affects the AOD but has no obvious effect on surface temperature. Temperature sensitivity to the ERF of U.S. SO2 emissions is found to differ from the models' sensitivity to radiative forcing of doubled CO2.

Space-Based Diagnosis of Surface Ozone Sensitivity to Anthropogenic Emissions

Science.gov (United States)

Martin, Randall V.; Fiore, Arlene M.; VanDonkelaar, Aaron

2004-01-01

We present a novel capability in satellite remote sensing with implications for air pollution control strategy. We show that the ratio of formaldehyde columns to tropospheric nitrogen dioxide columns is an indicator of the relative sensitivity of surface ozone to emissions of nitrogen oxides (NO(x) = NO + NO2) and volatile organic compounds (VOCs). The diagnosis from these space-based observations is highly consistent with current understanding of surface ozone chemistry based on in situ observations. The satellite-derived ratios indicate that surface ozone is more sensitive to emissions of NO(x) than of VOCs throughout most continental regions of the Northern Hemisphere during summer. Exceptions include Los Angeles and industrial areas of Germany. A seasonal transition occurs in the fall when surface ozone becomes less sensitive to NOx and more sensitive to VOCs.

Integrated Advanced Microwave Sounding Unit-A (AMSU-A). Engineering Test Report: Radiated Emissions and SARR, SARP, DCS Receivers, Link Frequencies EMI Sensitive Band Test Results, AMSU-A1, S/N 108 2

Science.gov (United States)

Valdez, A.

2000-01-01

This is the Engineering Test Report, Radiated Emissions and SARR, SARP, DCS Receivers, Link Frequencies EMI Sensitive Band Test Results, AMSU-A1 SIN 108, for the Integrated Advanced Microwave Sounding Unit-A (AMSU-A).

Microwave surface impedance of MgB2 thin film

International Nuclear Information System (INIS)

Jin, B B; Klein, N; Kang, W N; Kim, Hyeong-Jin; Choi, Eun-Mi; Lee, Sung-I K; Dahm, T; Maki, K

2003-01-01

The microwave surface impedance Z s = R s + jωμ 0 λ was measured with dielectric resonator techniques for two c-axis-oriented MgB 2 thin films. The temperature dependence of the penetration depth λ measured with a sapphire resonator at 17.93 GHz can be well fitted from 5 K close to T c by the standard BCS integral expression assuming the reduced energy gap Δ(0)/kT c to be as low as 1.13 and 1.03 for the two samples. From these fits the penetration depth at zero temperatures was determined to be 102 nm and 107 nm, respectively. The results clearly indicate the s-wave nature of the order parameter. The temperature dependence of surface resistance R s , measured with a rutile dielectric resonator, shows an exponential behaviour below about T c /2 with a reduced energy gap being consistent with the one determined from the λ data. The R s value at 4.2 K was found to be as low as 19 μΩ at 7.2 GHz, which is comparable with that of a high-quality high-temperature thin film of YBa 2 Cu 3 O 7 . A higher-order mode at 17.9 GHz was employed to determine the frequency f dependence of R s ∝ f n(T) . Our results revealed a decrease of n with increasing temperature ranging from n = 2 below 8 K to n 1 from 13 to 34 K

Application of a sawtooth surface to accelerator beam chambers with low electron emission rate

International Nuclear Information System (INIS)

Suetsugu, Y.; Tsuchiya, M.; Nishidono, T.; Kato, N.; Satoh, N.; Endo, S.; Yokoyama, T.

2003-01-01

One of the latest problems in positron or proton accelerators is a single-beam instability due to an electron cloud around the beam. The instability, for an example, causes a beam size blow up of the positron beam and deteriorates the performance of the electron-positron collider. the seed of the electron cloud is the electrons emitted from the surface of the beam chamber, which consists of electrons due to the synchrotron radiation (photoelectrons) and sometimes those multiplied by the multipactoring. Suppressing the electron emission from the surface is, therefore, an essential way to cure the instability. Here a rough surface with a sawtooth structure (sawtooth surface) is proposed to reduce the electron emission from the surface of the beam chamber. A new rolling-tap method is developed for this study to make the sawtooth surface in a circular beam chamber with a length of several meters. The first experiment using a test chamber at a photon beam line of the KEK Photon Factory verifies its validity. The photoelectron emission from the sawtooth surface reduces by one order of magnitude compared to the usual smooth surface. In the second experiment under a bunched positron beam in the KEK B-Factory, however, the electron emission is comparable to that of a smooth surface and the behavior is quite different from the previous one. The reason is that the beam field excites the multipactoring of electrons and the decrease of the photoelectron emission by the sawtooth surface is wiped out. The sawtooth surface will be effective to reduce the electron emission under the situation with external magnetic fields or without strong beam fields where the electron multipactoring hardly occurs

Heat transfer within a concrete slab applying the microwave decontamination process

International Nuclear Information System (INIS)

Li, W.; Ebadian, M.A.; White, T.L.; Grubb, R.G.

1993-01-01

Decontamination of a radioactive contaminated concrete surface is a new technology for the treatment of radioactive waste. In this paper, concrete decontamination using microwave technology is investigated theoretically. A plane wave assumption of microwave propagation has been employed to estimate the microwave field and power dissipation within the concrete. A one-dimensional, unsteady heat conduction model with microwave heat dissipation resulting from microwave-material interaction has been used to evaluate frequency, steel reinforcement within the concrete, and thermal boundary conditions are also considered in the present model. Four commonly used microwave frequencies of 0.896, 2.45, 10.6, and 18.0 GHz have been utilized in the analysis. The results revealed that as the microwave frequency increases to, or higher than 10.6 GHz, the microwave power dissipation shifts toward the front surface of the concrete. Furthermore, it was observed that use of a higher frequency microwave could reduce power intensity requirements needed to raise the temperature difference or thermal stress to the same value in the same period of time. It was found that the presence of reinforcing steel mesh causes part of the microwave energy to be blocked and reflected. Thus, the temperature or thermal stress of the concrete increases before the reinforcement, and decreases after the reinforcement. 16 refs., 6 figs., 3 tabs

IDENTIFYING THE RADIO BUBBLE NATURE OF THE MICROWAVE HAZE

Energy Technology Data Exchange (ETDEWEB)

Dobler, Gregory, E-mail: dobler@kitp.ucsb.edu [Kavli Institute for Theoretical Physics, University of California, Santa Barbara Kohn Hall, Santa Barbara, CA 93106 (United States)

2012-11-20

Using seven-year data from the Wilkinson Microwave Anisotropy Probe, I identify a sharp 'edge' in the microwave haze at high southern Galactic latitude (-55 Degree-Sign < b < -35 Degree-Sign ) that is spatially coincident with the southern edge of the 'Fermi haze/bubbles'. This finding proves conclusively that the edge in the gamma rays is real (and not a processing artifact), demonstrates explicitly that the microwave haze and the gamma-ray bubbles are indeed the same structure observed at multiple wavelengths, and strongly supports the interpretation of the microwave haze as a separate component of Galactic synchrotron (likely generated by a transient event) as opposed to a simple variation of the spectral index of disk synchrotron. In addition, combining these data sets allows for the first determination of the magnetic field within a radio bubble using microwaves and gamma rays by taking advantage of the fact that the inverse Compton gamma rays are primarily generated by scattering of cosmic microwave background photons at these latitudes, thus minimizing uncertainty in the target radiation field. Assuming uniform volume emissivity, I find that the magnetic field within the southern Galactic microwave/gamma-ray bubble is {approx}5 {mu}G above 6 kpc off of the Galactic plane.

Sensitive measurement of fluctuations in the cosmic microwave background

Energy Technology Data Exchange (ETDEWEB)

Davies, R D; Watson, R A; Daintree, E J; Hopkins, J; Lasenby, A N; Beckman, J; Sanchez-Almeida, J; Rebolo, R

1987-04-02

Extensive high sensitivity observations of the cosmic microwave background have been made on an angular scale of 8/sup 0/ covering a substantial fraction of the northern sky. An observed anisotropy in the sky emission at a level of ..delta..T/T = 3.7 x 10/sup -5/ has been detected (T is temperature). This level should strictly be interpreted as an upper limit to the cosmic microwave background fluctuations. It is possibly the direct imprint of density perturbations in the early Universe.

Sensitive measurement of fluctuations in the cosmic microwave background

International Nuclear Information System (INIS)

Davies, R.D.; Watson, R.A.; Daintree, E.J.; Hopkins, J.; Lasenby, A.N.

1987-01-01

Extensive high sensitivity observations of the cosmic microwave background have been made on an angular scale of 8 0 covering a substantial fraction of the northern sky. An observed anisotropy in the sky emission at a level of ΔT/T = 3.7 x 10 -5 has been detected (T is temperature). This level should strictly be interpreted as an upper limit to the cosmic microwave background fluctuations. It is possibly the direct imprint of density perturbations in the early Universe. (author)

Passive microwave remote sensing of soil moisture

International Nuclear Information System (INIS)

Jackson, T.J.; Schmugge, T.J.

1986-01-01

Microwave remote sensing provides a unique capability for direct observation of soil moisture. Remote measurements from space afford the possibility of obtaining frequent, global sampling of soil moisture over a large fraction of the Earth's land surface. Microwave measurements have the benefit of being largely unaffected by cloud cover and variable surface solar illumination, but accurate soil moisture estimates are limited to regions that have either bare soil or low to moderate amounts of vegetation cover. A particular advantage of passive microwave sensors is that in the absence of significant vegetation cover soil moisture is the dominant effect on the received signal. The spatial resolutions of passive microwave soil moisture sensors currently considered for space operation are in the range 10–20 km. The most useful frequency range for soil moisture sensing is 1–5 GHz. System design considerations include optimum choice of frequencies, polarizations, and scanning configurations, based on trade-offs between requirements for high vegetation penetration capability, freedom from electromagnetic interference, manageable antenna size and complexity, and the requirement that a sufficient number of information channels be available to correct for perturbing geophysical effects. This paper outlines the basic principles of the passive microwave technique for soil moisture sensing, and reviews briefly the status of current retrieval methods. Particularly promising are methods for optimally assimilating passive microwave data into hydrologic models. Further studies are needed to investigate the effects on microwave observations of within-footprint spatial heterogeneity of vegetation cover and subsurface soil characteristics, and to assess the limitations imposed by heterogeneity on the retrievability of large-scale soil moisture information from remote observations

Integrated Advanced Microwave Sounding Unit-A (AMSU-A). Engineering Test Report: Radiated Emissions and SARR, SARP, DCS Receivers, Link Frequencies EMI Sensitive Band Test Results, AMSU-A2, S/N 108, 08

Science.gov (United States)

Valdez, A.

2000-01-01

This is the Engineering Test Report, Radiated Emissions and SARR, SARP, DCS Receivers, Link Frequencies EMI Sensitive Band Test Results, AMSU-A2, S/N 108, for the Integrated Advanced Microwave Sounding Unit-A (AMSU-A).

Production of atmospheric pressure microwave plasma with dielectric half-mirror resonator and its application to polymer surface treatment

Science.gov (United States)

Sasai, Kensuke; Keyamura, Kazuki; Suzuki, Haruka; Toyoda, Hirotaka

2018-06-01

For the surface treatment of a polymer tube, a ring-shaped atmospheric pressure microwave plasma (APMP) using a coaxial waveguide is studied. In this APMP, a dielectric plate is used not only as a partial mirror for cavity resonation but also for the precise alignment of the discharge gap for ring-shaped plasma production. The optimum position of the dielectric plate is investigated by electromagnetic wave simulation. On the basis of simulation results, a ring-shaped plasma with good uniformity along the ring is produced. The coaxial APMP is applied to the surface treatment of ethylene tetrafluoroethylene. A very fast surface modification within 3 s is observed.

Fundamental properties of secondary negative ion emission by sputtering

International Nuclear Information System (INIS)

Shimizu, Toshiki; Tsuji, Hiroshi; Ishikawa, Junzo

1989-01-01

The report describes some results obtained from preliminary experiments on secondary negative ion emission from a cesiated surface by Xe-ion beam sputtering, which give the production probability. A measuring system is constructed for secondary negative ion emission. The system consists of a microwave ion source with a lens, a sputtering target holder with a heater, a cesium oven, a limiting aperture with a substrate for deposition, a negative-ion extractor and lens, and a ExB type mass separator. Observations are made on the dependence of negative ion current on cesium supply, dependence of negative ion current on target temperature, and negative ion production probability. The cesium supply and the target temperature are found to strongly influence the negative ion emission. By controlling these factors, the optimum condition for secondary negative ion emission is achieved with a minimum surface work function. The production probability of the negative ion is found to be very high, about 20% for carbon. Therefore, the secondary negative ion emission is considered a useful and highly efficient method to obtain high current ion beams. The constant in the Rasser's theoretical equation is experimentally determined to be 4.1 x 10 -4 eV sec/m. (N.K.)

Effects of Microwave Radiation on Oil Recovery

Science.gov (United States)

Esmaeili, Abdollah

2011-12-01

A variety of oil recovery methods have been developed and applied to mature and depleted reservoirs in order to improve the efficiency. Microwave radiation oil recovery method is a relatively new method and has been of great interest in the recent years. Crude oil is typically co-mingled with suspended solids and water. To increase oil recovery, it is necessary to remove these components. The separation of oil from water and solids using gravitational settling methods is typically incomplete. Oil-in-water and oil-water-solid emulsions can be demulsified and separated into their individual layers by microwave radiation. The data also show that microwave separation is faster than gravity separation and can be faster than conventional heating at many conditions. After separation of emulsion into water and oil layers, water can be discharged and oil is collected. High-frequency microwave recycling process can recover oil and gases from oil shale, residual oil, drill cuttings, tar sands oil, contaminated dredge/sediments, tires and plastics with significantly greater yields and lower costs than are available utilizing existing known technologies. This process is environmentally friendly, fuel-generating recycler to reduce waste, cut emissions, and save energy. This paper presents a critical review of Microwave radiation method for oil recovery.

Microwave-induced direct spin-flip transitions in mesoscopic Pd/Co heterojunctions

Science.gov (United States)

Pietsch, Torsten; Egle, Stefan; Keller, Martin; Fridtjof-Pernau, Hans; Strigl, Florian; Scheer, Elke

2016-09-01

We experimentally investigate the effect of resonant microwave absorption on the magneto-conductance of tunable Co/Pd point contacts. At the interface a non-equilibrium spin accumulation is created via microwave absorption and can be probed via point contact spectroscopy. We interpret the results as a signature of direct spin-flip excitations in Zeeman-split spin-subbands within the Pd normal metal part of the junction. The inverse effect, which is associated with the emission of a microwave photon in a ferromagnet/normal metal point contact, can also be detected via its unique signature in transport spectroscopy.

Microwave-induced direct spin-flip transitions in mesoscopic Pd/Co heterojunctions

International Nuclear Information System (INIS)

Pietsch, Torsten; Egle, Stefan; Keller, Martin; Fridtjof-Pernau, Hans; Strigl, Florian; Scheer, Elke

2016-01-01

We experimentally investigate the effect of resonant microwave absorption on the magneto-conductance of tunable Co/Pd point contacts. At the interface a non-equilibrium spin accumulation is created via microwave absorption and can be probed via point contact spectroscopy. We interpret the results as a signature of direct spin-flip excitations in Zeeman-split spin-subbands within the Pd normal metal part of the junction. The inverse effect, which is associated with the emission of a microwave photon in a ferromagnet/normal metal point contact, can also be detected via its unique signature in transport spectroscopy. (paper)

FeNi{sub 3}/indium tin oxide (ITO) composite nanoparticles with excellent microwave absorption performance and low infrared emissivity

Energy Technology Data Exchange (ETDEWEB)

Fu, Li-Shun; Jiang, Jian-Tang [School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001 (China); Zhen, Liang, E-mail: lzhen@hit.edu.cn [School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001 (China); MOE Key Laboratory of Micro-systems and Micro-structures Manufacturing, Harbin Institute of Technology, Harbin 150080 (China); Shao, Wen-Zhu [School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001 (China)

2013-03-01

Highlights: Black-Right-Pointing-Pointer Electrical conductivity and infrared emissivity can be controlled by ITO content. Black-Right-Pointing-Pointer The infrared emissivity is the lowest when the mole ratio of In:Sn in sol is 9:1. Black-Right-Pointing-Pointer The permittivity in microwave band can be controlled by the electrical conductivity. Black-Right-Pointing-Pointer EMA performance is significantly influenced by the content of ITO phase. Black-Right-Pointing-Pointer FeNi{sub 3}/ITO composite particles are suitable for both infrared and radar camouflage. - Abstract: FeNi{sub 3}/indium tin oxide (ITO) composite nanoparticles were synthesized by a self-catalyzed reduction method and a sol-gel process. The dependence of the content of ITO phase with the mole ratios of In:Sn of different sols was investigated. The relation between the electrical conductivity, infrared emissivity of FeNi{sub 3}/ITO composite nanoparticles and the content of ITO phase was discussed. Electromagnetic wave absorption (EMA) performance of products was evaluated by using transmission line theory. It was found that EMA performance including the intensity and the location of effective band is significantly dependent on the content of ITO phase. The low infrared emissivity and superior EMA performance of FeNi{sub 3}/ITO composite nanoparticles can be both achieved when the mole ratio of In:Sn in sol is 9:1.

Microwave-assisted aqueous synthesis of transition metal ions doped ZnSe/ZnS core/shell quantum dots with tunable white-light emission

Energy Technology Data Exchange (ETDEWEB)

Zhang, Jie [Laboratory of Advanced Materials, Fudan University, Shanghai 200438 (China); Chen, Qiuhang; Zhang, Wanlu; Mei, Shiliang; He, Liangjie; Zhu, Jiatao [Engineering Research Center of Advanced Lighting Technology, Ministry of Education, Institute for Electric Light Sources, Fudan University, Shanghai 200433 (China); Chen, Guoping [School of Information Science and Technology, Fudan University, Shanghai 200433 (China); Guo, Ruiqian, E-mail: rqguo@fudan.edu.cn [Engineering Research Center of Advanced Lighting Technology, Ministry of Education, Institute for Electric Light Sources, Fudan University, Shanghai 200433 (China)

2015-10-01

Highlights: • ZnSe-based QDs were formed via a microwave-assisted aqueous approach. • The stabilizer, ZnS coats and UV irradiation played a role in the PL enhancement. • Tunable white-light-emitting Mn:ZnSe QDs and Cu,Mn:ZnSe/ZnS QDs were synthesized. • The formation mechanism of Cu,Mn:ZnSe QDs was clarified. • The corresponding CIE color coordinates of different PL spectra were obtained. - Abstract: Synthesis of bright white-light emitting Mn and Cu co-doped ZnSe/ZnS core/shell quantum dots (QDs) (Cu,Mn:ZnSe/ZnS) was reported. Water-soluble ZnSe-based QDs with Mn and Cu doping were prepared using a versatile hot-injection method in aqueous solution with a microwave-assisted approach. Influence of the Se/S ratio, stabilizer, refluxing time and the concentration of Cu/Mn dopant ions on the particle size and photoluminescence (PL) were investigated. The as-prepared QDs in the different stages of growth were characterized by X-ray powder diffractometer (XRD), high-resolution transmission electron microscopy (HRTEM), UV–visible (UV–vis) spectrophotometer, and fluorescence spectrophotometer. It is found that these ZnSe-based QDs synthesized under mild conditions exhibit emission in the range of 390–585 nm. The PL quantum yield (QY) of the as-prepared water-soluble ZnSe QDs can be up to 24.3% after the UV-irradiation treatment. The band-gap emission of ZnSe is effectively restrained through Mn and Cu doping. The refluxing time influences the doping of not only Mn, but also Cu, which leads to the best refluxing time of Mn:ZnSe and the red-shift of the emission of Cu:ZnSe d-dots. Co-doping induced white-light emission (WLE) from Cu,Mn:ZnSe/ZnS core/shell QDs were obtained, which can offer the opportunity for future-generation white-light emitting diodes (LEDs)

Emissivity Measurements of Foam-Covered Water Surface at L-Band for Low Water Temperatures

Directory of Open Access Journals (Sweden)

En-Bo Wei

2014-11-01

Full Text Available For a foam-covered sea surface, it is difficult to retrieve sea surface salinity (SSS with L-band brightness temperature (1.4 GHz because of the effect of a foam layer with wind speeds stronger than 7 m/s, especially at low sea surface temperature (SST. With foam-controlled experiments, emissivities of a foam-covered water surface at low SST (−1.4 °C to 1.7 °C are measured for varying SSS, foam thickness, incidence angle, and polarization. Furthermore, a theoretical model of emissivity is introduced by combining wave approach theory with the effective medium approximation method. Good agreement is obtained upon comparing theoretical emissivities with those of experiments. The results indicate that foam parameters have a strong influence on increasing emissivity of a foam-covered water surface. Increments of experimental emissivities caused by foam thickness of 1 cm increase from about 0.014 to 0.131 for horizontal polarization and 0.022 to 0.150 for vertical polarization with SSS increase and SST decrease. Contributions of the interface between the foam layer and water surface to the foam layer emissivity increments are discussed for frequencies between 1 and 37 GHz.

Effect of microwave irradiation on selective heating behavior and magnetic separation characteristics of Panzhihua ilmenite

International Nuclear Information System (INIS)

Zhao, Wei; Chen, Jin; Chang, Xiaodong; Guo, Shenghui; Srinivasakannan, C.; Chen, Guo; Peng, Jinhui

2014-01-01

Highlights: • Microwave irradiation can be applied effectively and efficiently to the irradiation processes of Panzhihua ilmenite. • The mineral processing properties of microwave treated ilmenite were generally as good as or better than that of initial ilmenite. • The microwave selective heating characteristics of the different minerals and compounds, and the thermal stresses were caused by the uniform heat rate disturbed under microwave irradiation. - Abstract: The influences of microwave irradiation on the surface characteristics of Panzhihua ilmenite were systematically investigated. The crystal structures, surface morphology and surface chemical functional groups of ilmenite were characterized before and after microwave irradiation and magnetic separation for different microwave treatment times by using various methods, such as XRD, SEM, and FT-IR, respectively. XRD analysis showed that the microwave treated ilmenite has the strongest peaks of phase more than that of raw samples, indicates that the crystalline compound of ilmenite increased with the microwave irradiation time. SEM analysis showed the micro-cracking appeared at many grain boundaries of ilmenite after being pretreated by microwave treatment. The separations of ilmenite from gangue minerals were completed and the micro-fissure within ilmenite minerals were also formed, which could be attributed to the microwave selective heating characteristics of the different minerals and compounds, and the thermal stresses were caused by the uniform heat rate disturbed under microwave irradiation. The mineral processing results showed that the magnetic separation characteristics and properties of microwave treated ilmenite samples were better than that of microwave untreated ilmenite samples. It was concluded that microwave irradiation can be applied effectively and efficiently to the irradiation processes of Panzhihua ilmenite

Ion induced optical emission for surface and depth profile analysis

International Nuclear Information System (INIS)

White, C.W.

1977-01-01

Low-energy ion bombardment of solid surfaces results in the emission of infrared, visible, and ultraviolet radiation produced by inelastic ion-solid collision processes. The emitted optical radiation provides important insight into low-energy particle-solid interactions and provides the basis for an analysis technique which can be used for surface and depth profile analysis with high sensitivity. The different kinds of collision induced optical radiation emitted as a result of low-energy particle-solid collisions are reviewed. Line radiation arising from excited states of sputtered atoms or molecules is shown to provide the basis for surface and depth profile analysis. The spectral characteristics of this type of radiation are discussed and applications of the ion induced optical emission technique are presented. These applications include measurements of ion implant profiles, detection sensitivities for submonolayer quantities of impurities on elemental surfaces, and the detection of elemental impurities on complex organic substrates

White light emission from fluorescent SiC with porous surface

DEFF Research Database (Denmark)

Lu, Weifang; Ou, Yiyu; Fiordaliso, Elisabetta Maria

2017-01-01

We report for the frst time a NUV light to white light conversion in a N-B co-doped 6H-SiC (fuorescent SiC) layer containing a hybrid structure. The surface of fuorescent SiC sample contains porous structures fabricated by anodic oxidation method. After passivation by 20nm thick Al2O3, the photol......We report for the frst time a NUV light to white light conversion in a N-B co-doped 6H-SiC (fuorescent SiC) layer containing a hybrid structure. The surface of fuorescent SiC sample contains porous structures fabricated by anodic oxidation method. After passivation by 20nm thick Al2O3...... the bulk fuorescent SiC layer. A high color rendering index of 81.1 has been achieved. Photoluminescence spectra in porous layers fabricated in both commercial n-type and lab grown N-B co-doped 6H-SiC show two emission peaks centered approximately at 460nm and 530nm. Such bluegreen emission phenomenon can......, the photoluminescence intensity from the porous layer was signifcant enhanced by a factor of more than 12. Using a porous layer of moderate thickness (~10µm), high-quality white light emission was realized by combining the independent emissions of blue-green emission from the porous layer and yellow emission from...

Carbon dioxide emission from raised bog surface after peat extraction

Directory of Open Access Journals (Sweden)

Turbiak Janusz

2017-12-01

Full Text Available Research on CO2 emission from a raised bog after completion of peat extraction was performed in 2011–2013. CO2 emissions were determined by the chamber method. Twenty years after the termination of peat extraction, the bog surface was almost entirely devoid of plants. CO2 emission from the bog varied depending on temperature and water conditions and was 418 mg·m−2·h−1 on average during the research period. CO2 losses on the raised bog were on average 19.7 Mg·ha−1·year−1 during the research period which corresponded to a carbon loss of 5.37 Mg·ha−1·year−1 or mineralisation of 9.6 Mg·ha−1·year−1 of organic mass of 56% carbon content. It is possible to reduce organic mass losses and CO2 emission to the atmosphere from the bog surface after peat extraction has been terminated by reconstruction of initial water conditions, i.e. retaining a high ground water level and restoration of aquatic plant communities.

Microwave-induced electrostatic etching: generation of highly reactive magnesium for application in Grignard reagent formation.

Science.gov (United States)

van de Kruijs, Bastiaan H P; Dressen, Mark H C L; Meuldijk, Jan; Vekemans, Jef A J M; Hulshof, Lumbertus A

2010-04-07

A detailed study regarding the influence of microwave irradiation on the formation of a series of Grignard reagents in terms of rates and selectivities has revealed that these heterogeneous reactions may display a beneficial microwave effect. The interaction between microwaves and magnesium turnings generates violent electrostatic discharges. These discharges on magnesium lead to melting of the magnesium surface, thus generating highly active magnesium particles. As compared to conventional operation the microwave-induced discharges on the magnesium surface lead to considerably shorter initiation times for the insertion of magnesium in selected substrates (i.e. halothiophenes, halopyridines, octyl halides, and halobenzenes). Thermographic imaging and surface characterization by scanning electron microscopy showed that neither selective heating nor a "specific" microwave effect was causing the reduction in initiation times. This novel and straightforward initiation method eliminates the use of toxic and environmentally adverse initiators. Thus, this initiation method limits the formation of by-products. We clearly demonstrated that microwave irradiation enables fast Grignard reagent formation. Therefore, microwave technology is promising for process intensification of Grignard based coupling reactions.

A comparison of optical and microwave scintillometers with eddy covariance derived surface heat fluxes

KAUST Repository

Yee, Mei Sun

2015-11-01

Accurate measurements of energy fluxes between land and atmosphere are important for understanding and modeling climatic patterns. Several methods are available to measure heat fluxes, and scintillometers are becoming increasingly popular because of their ability to measure sensible (. H) and latent (. LvE) heat fluxes over large spatial scales. The main motivation of this study was to test the use of different methods and technologies to derive surface heat fluxes.Measurements of H and LvE were carried out with an eddy covariance (EC) system, two different makes of optical large aperture scintillometers (LAS) and two microwave scintillometers (MWS) with different frequencies at a pasture site in a semi-arid environment of New South Wales, Australia. We used the EC measurements as a benchmark. Fluxes derived from the EC system and LAS systems agreed (R2>0.94), whereas the MWS systems measured lower H (bias ~60Wm-2) and larger LvE (bias ~65Wm-2) than EC. When the scintillometers were compared against each other, the two LASs showed good agreement of H (R2=0.98), while MWS with different frequencies and polarizations led to different results. Combination of LAS and MWS measurements (i.e., two wavelength method) resulted in performance that fell in between those estimated using either LAS or MWS alone when compared with the EC system. The cause for discrepancies between surface heat fluxes derived from the EC system and those from the MWS systems and the two-wavelength method are possibly related to inaccurate assignment of the structure parameter of temperature and humidity. Additionally, measurements from MWSs can be associated with two values of the Bowen ratio, thereby leading to uncertainties in the estimation of the fluxes. While only one solution has been considered in this study, when LvE was approximately less than 200Wm-2, the alternate solution may be more accurate. Therefore, for measurements of surface heat fluxes in a semi-arid or dry environment, the

Au-controlled enhancement of photoluminescence of NiS nanostructures synthesized via a microwave-assisted hydrothermal technique

International Nuclear Information System (INIS)

Linganiso, Ella Cebisa; Mwakikunga, Bonex Wakufwa; Mhlanga, Sabelo Dalton; Coville, Neil John

2014-01-01

Nickel sulphide (NiS) nanostructures decorated with gold (Au) nanoparticles (NPs) were synthesized via a microwave-assisted hydrothermal technique. Binary phase NiS (α and β) crystalline nanostructures, bare, and decorated with Au NPs were obtained and confirmed by X-ray diffraction (XRD) studies. TEM analysis revealed that the NiS nanostructures were of various shapes. A quantum confinement effect was confirmed by the blue shift PL emissions and high optical energy band gap observed for the as-synthesized sample. A threefold light emission enhancement due to Au NP coatings was obtained when Au metal NP decoration concentrations was varied from 1% to 10%. These enhancements were attributed to the surface plasmon resonance (SPR) excitation of the surface decorated metal NPs which results in an increased rate of spontaneous emission. The PL enhancement factor was observed to vary at different NiS emissions as well as with the size of the Au NPs. The effect of metal NP decoration on the PL emission of NiS is to the best of our knowledge, presented for the first time. - Highlights: • Binary phase NiS decorated with gold nanoparticles. • Quantum confinement effect confirmed by PL analysis. • PL enhancement depending more on particle size distribution. • Effect of gold on NiS PL is to the best of our knowledge reported for the first time

Surface modification and stability of detonation nanodiamonds in microwave gas discharge plasma

International Nuclear Information System (INIS)

Stanishevsky, Andrei V.; Walock, Michael J.; Catledge, Shane A.

2015-01-01

Graphical abstract: - Highlights: • Single and binary gas plasma modification of nanodiamond powders studied. • Temperature-dependent effect of N 2 and N 2 /H 2 plasma reported for the first time. • Role of H 2 in H 2 /N 2 and H 2 /O 2 plasma modification of nanodiamond discussed. - Abstract: Detonation nanodiamonds (DND), with low hydrogen content, were exposed to microwave plasma generated in pure H 2 , N 2 , and O 2 gases and their mixtures, and investigated using X-ray diffraction (XRD), Fourier Transform Infrared (FTIR), Raman, and X-ray photoelectron spectroscopies. Considerable alteration of the DND surface was observed under the plasma conditions for all used gases, but the diamond structure of the DND particle core was preserved in most cases. The stabilizing effect of H 2 in H 2 /N 2 and H 2 /O 2 binary gas plasmas on the DND structure and the temperature-dependent formation of various CNH x surface groups in N 2 and H 2 /N 2 plasmas were observed and discussed for the first time. DND surface oxidation and etching were the main effects of O 2 plasma, whereas the N 2 plasma led to DND surfaces rich in amide groups below 1073 K and nitrile groups at higher temperatures. Noticeable graphitization of the DND core structure was detected only in N 2 plasma when the substrate temperature was above 1103 K.

Sliding wear studies of microwave clad versus unclad surface of stainless steel 304

Directory of Open Access Journals (Sweden)

Akshata M. K.

2018-01-01

Full Text Available Small and large scale (gas power plant, hydro power plant, automobile industries are suffering by failure of component. Sometimes, it is also observed that the component which was failed due to these reasons are very much costly and replacement of those also very difficult due to the complex geometry. By using Microwave hybrid heating, WC-12Co based clads were developed on austenitic stainless steel (SS304. Microwave clads were developed by introducing the preplaced, preheated powder for a duration of 15 min to microwave radiation at 2.45GHz frequency and 900 W power in domestic microwave applicator. By using optical microscope and scanning electron microscope (SEM, the developed clads were characterized. By using pin-on-disk, wear performance of the WC-12Co based clads and unclad samples were tested. It is observed that developed clad samples performed superior wear resistance than unclad samples.

Combining Passive Microwave Sounders with CYGNSS information for improved retrievals: Observations during Hurricane Harvey

Science.gov (United States)

Schreier, M. M.

2017-12-01

The launch of CYGNSS (Cyclone Global Navigation Satellite System) has added an interesting component to satellite observations: it can provide wind speeds in the tropical area with a high repetition rate. Passive microwave sounders that are overpassing the same region can benefit from this information, when it comes to the retrieval of temperature or water profiles: the uncertainty about wind speeds has a strong impact on emissivity and reflectivity calculations with respect to surface temperature. This has strong influences on the uncertainty of retrieval of temperature and water content, especially under extreme weather conditions. Adding CYGNSS information to the retrieval can help to reduce errors and provide a significantly better sounder retrieval. Based on observations during Hurricane Harvey, we want to show the impact of CYGNSS data on the retrieval of passive microwave sensors. We will show examples on the impact on the retrieval from polar orbiting instruments, like the Advanced Technology Microwave Sounder (ATMS) and AMSU-A/B on NOAA-18 and 19. In addition we will also show the impact on retrievals from HAMSR (High Altitude MMIC Sounding Radiometer), which was flying on the Global Hawk during the EPOCH campaign. We will compare the results with other observations and estimate the impact of additional CYGNSS information on the microwave retrieval, especially on the impact in error and uncertainty reduction. We think, that a synergetic use of these different data sources could significantly help to produce better assimilation products for forecast assimilation.

Microwave-assisted fibrous decoration of mPE surface utilizing Aloe vera extract for tissue engineering applications.

Science.gov (United States)

Balaji, Arunpandian; Jaganathan, Saravana Kumar; Supriyanto, Eko; Muhamad, Ida Idayu; Khudzari, Ahmad Zahran Md

2015-01-01

Developing multifaceted, biocompatible, artificial implants for tissue engineering is a growing field of research. In recent times, several works have been reported about the utilization of biomolecules in combination with synthetic materials to achieve this process. Accordingly, in this study, the ability of an extract obtained from Aloe vera, a commonly used medicinal plant in influencing the biocompatibility of artificial material, is scrutinized using metallocene polyethylene (mPE). The process of coating dense fibrous Aloe vera extract on the surface of mPE was carried out using microwaves. Then, several physicochemical and blood compatibility characterization experiments were performed to disclose the effects of corresponding surface modification. The Fourier transform infrared spectrum showed characteristic vibrations of several active constituents available in Aloe vera and exhibited peak shifts at far infrared regions due to aloe-based mineral deposition. Meanwhile, the contact angle analysis demonstrated a drastic increase in wettability of coated samples, which confirmed the presence of active components on glazed mPE surface. Moreover, the bio-mimic structure of Aloe vera fibers and the influence of microwaves in enhancing the coating characteristics were also meticulously displayed through scanning electron microscopy micrographs and Hirox 3D images. The existence of nanoscale roughness was interpreted through high-resolution profiles obtained from atomic force microscopy. And the extent of variations in irregularities was delineated by measuring average roughness. Aloe vera-induced enrichment in the hemocompatible properties of mPE was established by carrying out in vitro tests such as activated partial thromboplastin time, prothrombin time, platelet adhesion, and hemolysis assay. In conclusion, the Aloe vera-glazed mPE substrate was inferred to attain desirable properties required for multifaceted biomedical implants.

Cosmic microwave background science at commercial airline altitudes

Science.gov (United States)

Feeney, Stephen M.; Gudmundsson, Jon E.; Peiris, Hiranya V.; Verde, Licia; Errard, Josquin

2017-07-01

Obtaining high-sensitivity measurements of degree-scale cosmic microwave background (CMB) polarization is the most direct path to detecting primordial gravitational waves. Robustly recovering any primordial signal from the dominant foreground emission will require high-fidelity observations at multiple frequencies, with excellent control of systematics. We explore the potential for a new platform for CMB observations, the Airlander 10 hybrid air vehicle, to perform this task. We show that the Airlander 10 platform, operating at commercial airline altitudes, is well suited to mapping frequencies above 220 GHz, which are critical for cleaning CMB maps of dust emission. Optimizing the distribution of detectors across frequencies, we forecast the ability of Airlander 10 to clean foregrounds of varying complexity as a function of altitude, demonstrating its complementarity with both existing (Planck) and ongoing (C-BASS) foreground observations. This novel platform could play a key role in defining our ultimate view of the polarized microwave sky.

A Degree-Scale Measurement of the Anisotropy in the Cosmic Microwave Background

Science.gov (United States)

Wollack, Ed; Jarosik, Norm; Netterfield, Barth; Page, Lyman; Wilkinson, David

1995-01-01

We report the detection of anisotropy in the microwave sky at 3O GHz and at l deg angular scales. The most economical interpretation of the data is that the fluctuations are intrinsic to the cosmic microwave background. However, galactic free-free emission is ruled out with only 90% confidence. The most likely root-mean-squared amplitude of the fluctuations, assuming they are described by a Gaussian auto-correlation function with a coherence angle of 1.2 deg, is 41(+16/-13) (mu)K. We also present limits on the anisotropy of the polarization of the cosmic microwave background.

Diminished Mercury Emission From Water Surfaces by Duckweed (Lemna minor)

Science.gov (United States)

Wollenberg, J. L.; Peters, S. C.

2007-12-01

Aquatic plants of the family Lemnaceae (generally referred to as duckweeds) are a widely distributed type of floating vegetation in freshwater systems. Under suitable conditions, duckweeds form a dense vegetative mat on the water surface, which reduces light penetration into the water column and decreases the amount of exposed water surface. These two factors would be expected to reduce mercury emission by limiting a) direct photoreduction of Hg(II), b) indirect reduction via coupled DOC photooxidation-Hg(II) reduction, and c) gas diffusion across the water-air interface. Conversely, previous studies have demonstrated transpiration of Hg(0) by plants, so it is therefore possible that the floating vegetative mat would enhance emission via transpiration of mercury vapor. The purpose of this experiment was to determine whether duckweed limits mercury flux to the atmosphere by shading and the formation of a physical barrier to diffusion, or whether it enhances emission from aquatic systems via transpiration of Hg(0). Deionized water was amended with mercury to achieve a final concentration of approximately 35 ng/L and allowed to equilibrate prior to the experiment. Experiments were conducted in rectangular polystyrene flux chambers with measured UV-B transmittance greater than 60% (spectral cutoff approximately 290 nm). Light was able to penetrate the flux chamber from the sides as well as the top throughout the experiment, limiting the effect of shading by duckweed on the water surface. Flux chambers contained 8L of water with varying percent duckweed cover, and perforated plastic sheeting was used as an abiotic control. Exposures were conducted outside on days with little to no cloud cover. Real time mercury flux was measured using atomic absorption (Mercury Instruments UT-3000). Total solar and ultraviolet radiation, as well as a suite of meteorological parameters, were also measured. Results indicate that duckweed diminishes mercury emission from the water surface

Depressed emission between magnetic arcades near a sunspot

Science.gov (United States)

Ryabov, B. I.; Shibasaki, K.

The locations of the depressed emission in microwaves, EUV and soft X-rays are compared with each other and with the location of the plasma outflow in the active region (AR) 8535 on the Sun. We found that two open-field regions overlap the regions of depressed emission near the AR's sunspot. These two open-field regions are simulated with the potential-field source-surface (PFSS) model under radial distances of RSS = 1.8 R⊙ and RSS = 2.5 R⊙. Each open-field region is located between the arcades of the loops of the same magnetic polarity. The former open-field region covers the region of the plasma outflow, which is thus useful for the tests on connection to the heliosphere. The utmost microwave depression of the intensity in the ordinary mode (the Very Large Array 15 GHz observations) also overlaps the region of the plasma outflow and thus indicates this outflow. The lasting for eight days depression in soft X-rays and the SOHO EIT 2.84× 10-8 m images are attributed to the evacuation of as hot coronal plasma as T≥ 2× 106 K from the extended in height (``open") magnetic structures. We conclude that the AR 8535 presents the sunspot atmosphere affected by the large-scale magnetic fields.

Microwave Pretreatment for Thiourea Leaching for Gold Concentrate

Directory of Open Access Journals (Sweden)

Nag-Choul Choi

2017-10-01

Full Text Available In this research, we studied the use of microwave pretreatment to enhance the efficiency of Au leaching from gold concentrate. The gold concentrate was pretreated using microwaves with different irradiation time. The sample temperature was increased up to 950 °C by the microwave irradiation. A scanning electron microscope-energy dispersive spectrometer showed the evolution of microcracks and the reduction of sulfur on the mineral surface. X-ray diffraction data also showed the mineral phase shift from pyrite to hematite or pyrrhotite. A leaching test was conducted for the microwave-treated and untreated gold concentrates using thiourea. Although the thiourea leaching recovered 80% of Au from the untreated concentrate, from the treated concentration, the Au could be recovered completely. Au leaching efficiency increased as the microwave irradiation time increased, as well as with a higher composition of thiourea.

Synthesis of N-graphene using microwave plasma-based methods

Science.gov (United States)

Dias, Ana; Tatarova, Elena; Henriques, Julio; Dias, Francisco; Felizardo, Edgar; Abrashev, Miroslav; Bundaleski, Nenad; Cvelbar, Uros

2016-09-01

In this work a microwave atmospheric plasma driven by surface waves is used to produce free-standing graphene sheets (FSG). Carbonaceous precursors are injected into a microwave plasma environment, where decomposition processes take place. The transport of plasma generated gas-phase carbon atoms and molecules into colder zones of plasma reactor results in carbon nuclei formation. The main part of the solid carbon is gradually carried from the ``hot'' plasma zone into the outlet plasma stream where carbon nanostructures assemble and grow. Subsequently, the graphene sheets have been N-doped using a N2-Ar large-scale remote plasma treatment, which consists on placing the FSG on a substrate in a remote zone of the N2-Ar plasma. The samples were treated with different compositions of N2-Ar gas mixtures, while maintaining 1 mbar pressure in the chamber and a power applied of 600 W. The N-doped graphene sheets were characterized by scanning and by high-resolution transmission electron microscopy, X-ray photoelectron spectroscopy and Raman spectroscopy. Plasma characterization was also performed by optical emission spectroscopy. Work partially funded by Portuguese FCT - Fundacao para a Ciencia e a Tecnologia, under grant SFRH/BD/52413/2013 (PD-F APPLAuSE).

Generalized model of the microwave auditory effect

International Nuclear Information System (INIS)

Yitzhak, N M; Ruppin, R; Hareuveny, R

2009-01-01

A generalized theoretical model for evaluating the amplitudes of the sound waves generated in a spherical head model, which is irradiated by microwave pulses, is developed. The thermoelastic equation of motion is solved for a spherically symmetric heating pattern of arbitrary form. For previously treated heating patterns that are peaked at the sphere centre, the results reduce to those presented before. The generalized model is applied to the case in which the microwave absorption is concentrated near the sphere surface. It is found that, for equal average specific absorption rates, the sound intensity generated by a surface localized heating pattern is comparable to that generated by a heating pattern that is peaked at the centre. The dependence of the induced sound pressure on the shape of the microwave pulse is explored. Another theoretical extension, to the case of repeated pulses, is developed and applied to the interpretation of existing experimental data on the dependence of the human hearing effect threshold on the pulse repetition frequency.

Low-cost microwave radiometry for remote sensing of soil moisture

Science.gov (United States)

Chikando, Eric Ndjoukwe

2007-12-01

Remote sensing is now widely regarded as a dominant means of studying the Earth and its surrounding atmosphere. This science is based on blackbody theory, which states that all objects emit broadband electromagnetic radiation proportional to their temperature. This thermal emission is detectable by radiometers---highly sensitive receivers capable of measuring extremely low power radiation across a continuum of frequencies. In the particular case of a soil surface, one important parameter affecting the emitted radiation is the amount of water content or, soil moisture. A high degree of precision is required when estimating soil moisture in order to yield accurate forecasting of precipitations and short-term climate variability such as storms and hurricanes. Rapid progress within the remote sensing community in tackling current limitations necessitates an awareness of the general public towards the benefits of the science. Information about remote sensing instrumentation and techniques remain inaccessible to many higher-education institutions due to the high cost of instrumentation and the current general inaccessibility of the science. In an effort to draw more talent within the field, more affordable and reliable scientific instrumentation are needed. This dissertation introduces the first low-cost handheld microwave instrumentation fully capable of surface soil moisture studies. The framework of this research is two-fold. First, the development of a low-cost handheld microwave radiometer using the well-known Dicke configuration is examined. The instrument features a super-heterodyne architecture and is designed following a microwave integrated circuit (MIC) system approach. Validation of the instrument is performed by applying it to various soil targets and comparing measurement results to gravimetric technique measured data; a proven scientific method for determining volumetric soil moisture content. Second, the development of a fully functional receiver RF front

Surface magnetism studied by polarized light emission after He+ scattering

NARCIS (Netherlands)

Manske, J; Dirska, M; Lubinski, G; Schleberger, M; Narmann, A; Hoekstra, R

Surface magnetism is studied by means of an ion beam of low energy (2-15 keV) scattered off the surface under grazing incidence conditions. During the scattering, a small fraction of the ions is neutralized into excited states which decay subsequently by light emission. The circular polarization of

Continuous microwave flow synthesis of mesoporous hydroxyapatite.

Science.gov (United States)

Akram, Muhammad; Alshemary, Ammar Z; Goh, Yi-Fan; Wan Ibrahim, Wan Aini; Lintang, Hendrik O; Hussain, Rafaqat

2015-11-01

We have successfully used continuous microwave flow synthesis (CMFS) technique for the template free synthesis of mesoporous hydroxyapatite. The continuous microwave flow reactor consisted of a modified 2.45GHz household microwave, peristaltic pumps and a Teflon coil. This cost effective and efficient system was exploited to produce semi-crystalline phase pure nano-sized hydroxyapatite. Effect of microwave power, retention time and the concentration of reactants on the phase purity, degree of crystallinity and surface area of the final product was studied in detail. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) were used to study the phase purity and composition of the product, while transmission electron microscopy (TEM) was used to study the effect of process parameters on the morphology of hydroxyapatite. The TEM analysis confirmed the formation of spherical particles at low microwave power; however the morphology of the particles changed to mesoporous needle and rod-like structure upon exposing the reaction mixture to higher microwave power and longer retention time inside the microwave. The in-vitro ion dissolution behavior of the as synthesized hydroxyapatite was studied by determining the amount of Ca(2+) ion released in SBF solution. Copyright © 2015 Elsevier B.V. All rights reserved.

An evaluation of microwave-assisted fusion and microwave-assisted acid digestion methods for determining elemental impurities in carbon nanostructures using inductively coupled plasma optical emission spectrometry

KAUST Repository

Patole, Shashikant P.; Simõ es, Filipa; Yapici, Tahir; Warsama, Bashir H.; Anjum, Dalaver H.; Da Costa, Pedro M. F. J.

2015-01-01

A method for the complete digestion of carbon nanostructures has been demonstrated. Photographs (on the left side) show zirconium crucibles containing SWCNTs with flux of Na2CO3 and K2CO3, before and after microwave fusion; (on the right side) the appearance of the final solutions containing dissolved samples, from microwave-assisted fusion and microwave-assisted acid digestion. These solutions were used for determining the trace elemental impurities by ICP‒OES.

Use of IRI to Model the Effect of Ionosphere Emission on Earth Remote Sensing at L-Band

Science.gov (United States)

Abraham, Saji; LeVine, David M.

2004-01-01

Microwave remote sensing in the window at 1.413 GHz (L-band) set aside for passive use only is important for monitoring sea surface salinity and soil moisture. These parameters are important for understanding ocean dynamics and energy exchange between the surface and atmosphere, and both NASA and ESA plan to launch satellite sensors to monitor these parameters at L-band (Aquarius, Hydros and SMOS). The ionosphere is an important source of error for passive remote sensing at this frequency. In addition to Faraday rotation, emission from the ionosphere is also a potential source of error at L-band. As an aid for correcting for emission, a regression model is presented that relates ionosphere emission to the integrated electron density (TEC). The goal is to use TEC from sources such as TOPEX, JASON or GPS to obtain estimates of emission over the oceans where the electron density profiles needed to compute emission are not available. In addition, data will also be presented to evaluate the use of the IRI for computing emission over the ocean.

Microwave-assisted activation for electroless nickel plating on PMMA microspheres

Energy Technology Data Exchange (ETDEWEB)

Chen, Yen-Chung [Graduate School of Defense Science, Chung Cheng Institute of Technology, National Defense University, Tao-Yuan, Taiwan 335 (China); Materials and Electro-optics Research Division, Chung Shan Institute of Science and Technology, Tao-Yuan, Taiwan 325 (China); Liu, Robert Lian-Huey [Graduate School of Defense Science, Chung Cheng Institute of Technology, National Defense University, Tao-Yuan, Taiwan 335 (China); Department of Chemical and Materials Engineering, Minghsin University of Science and Technology, Hsinchu Taiwan 304 (China); Chen, Xin-Liang [Graduate School of Defense Science, Chung Cheng Institute of Technology, National Defense University, Tao-Yuan, Taiwan 335 (China); Shu, Hsiou-Jeng [Materials and Electro-optics Research Division, Chung Shan Institute of Science and Technology, Tao-Yuan, Taiwan 325 (China); Ger, Ming-Der, E-mail: mingderger@gmail.com [Department of Chemical and Materials Engineering, Chung Cheng Institute of Technology, National Defense University, Tao-Yuan, Taiwan 335 (China)

2011-05-15

A novel microwave-assisted activation method for electroless plating on PMMA microspheres is presented in this study. When the microwave irradiation was applied during the activation step, the amount of the Pd species adsorbed on PMMA surfaces was much higher than that of sample pretreated with a conventional activation process without microwave irradiation. With this activation method, it was also shown that the adsorbed Pd species with a size of 4-6 nm were uniformly distributed on the surfaces of the PMMA microspheres, thus a smooth and uniform nickel-phosphorus coating on the PMMA microspheres was obtained by subsequent electroless plating. The samples after each step were characterized by XPS, TEM, ICP and SEM.

Microwave generation and frequency conversion using intense relativistic electron beams

International Nuclear Information System (INIS)

Buzzi, J.M.; Doucet, H.J.; Etlicher, B.

1977-01-01

Some aspects of the microwave generation and frequency conversion by relativistic electron beams are studied. Using an electron synchrotron maser, the excitation of microwaves by an annular relativistic electron beam propagating through a circular wave guide immersed in a longitudinal magnetic field is analyzed. This theoretical model is somewhat more realistic than the previous one because the guiding centers are not on the wave guide axis. Microwave reflection is observed on a R.E.B. front propagating into a gas filled waveguide. The frequency conversion from the incident X-band e.m. waves and the reflected Ka band observed signal is consistent with the Doppler model for β = 0.7. This value agrees with the average beam front velocity as measured from time-of-flight using two B/sub theta/ probes. The reflection is found to occur during the current rise time. With a low impedance device (2 Ω, 400 keV) a GW X-band emission has been observed using thin anodes and a gas filled waveguide. This emission is probably due to the self-fields of the beam and could be used as a diagnostic

Field emission from vertically aligned few-layer graphene

International Nuclear Information System (INIS)

Malesevic, Alexander; Kemps, Raymond; Vanhulsel, Annick; Chowdhury, Manish Pal; Volodin, Alexander; Van Haesendonck, Chris

2008-01-01

The electric field emission behavior of vertically aligned few-layer graphene was studied in a parallel plate-type setup. Few-layer graphene was synthesized in the absence of any metallic catalyst by microwave plasma enhanced chemical vapor deposition with gas mixtures of methane and hydrogen. The deposit consists of nanostructures that are several micrometers wide, highly crystalline stacks of four to six atomic layers of graphene, aligned vertically to the substrate surface in a high density network. The few-layer graphene is found to be a good field emitter, characterized by turn-on fields as low as 1 V/μm and field amplification factors up to several thousands. We observe a clear dependence of the few-layer graphene field emission behavior on the synthesis parameters: Hydrogen is identified as an efficient etchant to improve field emission, and samples grown on titanium show lower turn-on field values and higher amplification factors when compared to samples grown on silicon

In Situ Spectroscopic Analysis of the Carbothermal Reduction Process of Iron Oxides during Microwave Irradiation

Directory of Open Access Journals (Sweden)

Jun Fukushima

2018-01-01

Full Text Available The effects of microwave plasma induction and reduction on the promotion of the carbothermal reduction of iron oxides (α-Fe2O3, γ-Fe2O3, and Fe3O4 are investigated using in situ emission spectroscopy measurements during 2.45 GHz microwave processing, and the plasma discharge (such as CN and N2 is measured during microwave E-field irradiation. It is shown that CN gas or excited CN molecules contribute to the iron oxide reduction reactions, as well as to the thermal reduction. On the other hand, no plasma is generated during microwave H-field irradiation, resulting in thermal reduction. Magnetite strongly interacts with the microwave H-field, and the reduction reaction is clearly promoted by microwave H-field irradiation, as well as thermal reduction reaction.

The AMY experiment: Microwave emission from air shower plasmas

Directory of Open Access Journals (Sweden)

Alvarez-Muñiz J.

2016-01-01

Full Text Available You The Air Microwave Yield (AMY experiment investigate the molecular bremsstrahlung radiation emitted in the GHz frequency range from an electron beam induced air-shower. The measurements have been performed at the Beam Test Facility (BTF of Frascati INFN National Laboratories with a 510 MeV electron beam in a wide frequency range between 1 and 20 GHz. We present the apparatus and the results of the tests performed.

On-line digestion in a focused microwave-assisted oven for elements determination in orange juice by inductively coupled plasma optical emission spectrometry

Directory of Open Access Journals (Sweden)

Fili Sabrina P.

2003-01-01

Full Text Available A flow injection system coupled to focused microwave-assisted oven was used for on-line orange juice sample digestion for determination of Ca, Cu, Fe, K, Mg, Mn, Na, P, and Zn by inductively coupled plasma optical emission spectrometry. The reactor coil was a PTFE tube (4.0 m long and 1.6 mm i.d. positioned into the commercial glass tube of the focused microwave oven. Aliquots of 500 muL of sample and 1000 muL of reagent (80% v/v HNO3 were mixed in a confluence and carried out to the reactor coil by air carrier. The relative standard deviation for five replicates of sample was lower than 5.0%. Good recoveries varying from 91 to 111% were obtained for added concentrations of the interest elements. The results obtained using the proposed digestion system are in agreement with those obtained for total digestion at the 95% confidence level. With this on-line digestion system was possible to carry out 12 samples h-1, minimizing contamination, saving consumption of samples and reagent and low residue generation.

Microwave-assisted green synthesis of superparamagnetic nanoparticles using fruit peel extracts: surface engineering, T2 relaxometry, and photodynamic treatment potential

Directory of Open Access Journals (Sweden)

Bano S

2016-08-01

Full Text Available Shazia Bano,1–3 Samina Nazir,2 Alia Nazir,1 Saeeda Munir,3 Tariq Mahmood,2 Muhammad Afzal,1 Farzana Latif Ansari,4 Kehkashan Mazhar3 1Department of Physics, The Islamia University of Bahawalpur, Bahawalpur, 2Nanosciences and Technology Department, National Centre for Physics, 3Institute of Biomedical and Genetic Engineering (IBGE, 4Pakistan Council for Science and Technology, Islamabad, Pakistan Abstract: Superparamagnetic iron oxide nanoparticles (SPIONs have the potential to be used as multimodal imaging and cancer therapy agents due to their excellent magnetism and ability to generate reactive oxygen species when exposed to light. We report the synthesis of highly biocompatible SPIONs through a facile green approach using fruit peel extracts as the biogenic reductant. This green synthesis protocol involves the stabilization of SPIONs through coordination of different phytochemicals. The SPIONs were functionalized with polyethylene glycol (PEG-6000 and succinic acid and were extensively characterized by X-ray diffraction analysis, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopy, atomic force microscopy, Rutherford backscattering spectrometry, diffused reflectance spectroscopy, fluorescence emission, Fourier-transform infrared spectroscopy, ultraviolet-visible spectroscopy, and magnetization analysis. The developed SPIONs were found to be stable, almost spherical with a size range of 17–25 nm. They exhibited excellent water dispersibility, colloidal stability, and relatively high R2 relaxivity (225 mM-1 s-1. Cell viability assay data revealed that PEGylation or carboxylation appears to significantly shield the surface of the particles but does not lead to improved cytocompatibility. A highly significant increase of reactive oxygen species in light-exposed samples was found to play an important role in the photokilling of human cervical epithelial malignant carcinoma (HeLa cells. The bio-SPIONs developed

Field emission characteristics of SnO2/CNT composite prepared by microwave assisted wet impregnation

CSIR Research Space (South Africa)

Kesavan Pillai, Sreejarani

2012-01-01

Full Text Available SnO2/CNT composites were prepared by microwave assisted wet impregnation at 60 °C. The process was optimized by varying the microwave power and reaction time. Raman analysis showed the typical features of the rutile phase of as-synthesized SnO2...

Detection of defects on the metal surface using the modulated microwave

International Nuclear Information System (INIS)

Joo, Gwang Tae; Jeong, Sung Hae; Song, Ki Young; Kim, Jin Ouk

1996-01-01

The defects on the metal surface, like as ended circular pressed hole, penetrated circular drilled hole and linear hollow lane(ended linear crack), are tested by method of reflection, transmission, fixed carrier frequency and mod-demodulation techniques using microwave horn antenna and rectangular waveguide on 9.2 GHz carrier and 3 kHz modulation frequency. In the cases of ended circular hole and penetrated hole defects, the magnitude of reflection signals changed extremely, and the results on the defects' sizes are enlarge d by about 2.5 times at the ended hole and decreased by about 75% at the penetrate d hole. And in the cases of linear hollow lane, depths are 0.45 mm, 1.2 mm and 2.4 mm, the measured results on average increasing rate of detected reflection signals according to crack widths are 0.46 mV/mm, 0.32 mV/mm and 0.23 mV/mm each, for length of lane 150 mm.

Graphene oxide reduction by microwave heating

International Nuclear Information System (INIS)

Longo, Angela; Carotenuto, Gianfranco

2016-01-01

The possibility to prepare thermal reduced graphene oxide (Tr-GO) colloidal suspensions by microwave heating of graphene oxide (GO) suspensions in N-methyl-2-pyrrolidone (NMP) has been investigated. According to transmission electron microscopy (TEM) and absorption and emission spectroscopy characterization, such a type of thermal reduction does not lead to graphene quantum dots formation because only mono-functional oxygen-containing groups are removed.

Graphene oxide reduction by microwave heating

Energy Technology Data Exchange (ETDEWEB)

Longo, Angela; Carotenuto, Gianfranco [Institute for Polymers, Composites, and Biomaterials, National Research Council, Piazzale Enrico Fermi 1, 80055 Portici (Italy)

2016-05-18

The possibility to prepare thermal reduced graphene oxide (Tr-GO) colloidal suspensions by microwave heating of graphene oxide (GO) suspensions in N-methyl-2-pyrrolidone (NMP) has been investigated. According to transmission electron microscopy (TEM) and absorption and emission spectroscopy characterization, such a type of thermal reduction does not lead to graphene quantum dots formation because only mono-functional oxygen-containing groups are removed.

Effect of surface contaminants on the light emission spectrum of LiF TLDs

International Nuclear Information System (INIS)

Abhold, M.E.

1987-01-01

Recent results show the differences between the light emissions spectra from LiF Thermoluminescent Dosimeters (TLDs) for gamma vs. alpha irradiations to be due to contaminants on the surface of the TLD. The light emission spectrum for thermal neutron irradiations was observed to be identical to that for a Cs-137 gamma irradiation in Harshaw TLD-100. Further experiments with surface treatments on TLD-100 indicate trace contaminants introduced by the standard methanol cleansing rinse in reagent grade methanol to have a substantial effect on the light emission spectrum for Am-241 alpha irradiations

Surface functionalization of microwave plasma-synthesized silica nanoparticles for enhancing the stability of dispersions

Science.gov (United States)

Sehlleier, Yee Hwa; Abdali, Ali; Schnurre, Sophie Marie; Wiggers, Hartmut; Schulz, Christof

2014-08-01

Gas phase-synthesized silica nanoparticles were functionalized with three different silane coupling agents (SCAs) including amine, amine/phosphonate and octyltriethoxy functional groups and the stability of dispersions in polar and non-polar dispersing media such as water, ethanol, methanol, chloroform, benzene, and toluene was studied. Fourier transform infrared spectroscopy showed that all three SCAs are chemically attached to the surface of silica nanoparticles. Amine-functionalized particles using steric dispersion stabilization alone showed limited stability. Thus, an additional SCA with sufficiently long hydrocarbon chains and strong positively charged phosphonate groups was introduced in order to achieve electrosteric stabilization. Steric stabilization was successful with hydrophobic octyltriethoxy-functionalized silica nanoparticles in non-polar solvents. The results from dynamic light scattering measurements showed that in dispersions of amine/phosphonate- and octyltriethoxy-functionalized silica particles are dispersed on a primary particle level. Stable dispersions were successfully prepared from initially agglomerated nanoparticles synthesized in a microwave plasma reactor by designing the surface functionalization.

A microwave powered sensor assembly for microwave ovens

DEFF Research Database (Denmark)

2016-01-01

The present invention relates to a microwave powered sensor assembly for micro- wave ovens. The microwave powered sensor assembly comprises a microwave antenna for generating an RF antenna signal in response to microwave radiation at a predetermined excitation frequency. A dc power supply circuit...... of the microwave powered sensor assembly is operatively coupled to the RF antenna signal for extracting energy from the RF antenna signal and produce a power supply voltage. A sensor is connected to the power supply voltage and configured to measure a physical or chemical property of a food item under heating...... in a microwave oven chamber....

Microwave engineering

CERN Document Server

Pozar, David M

2012-01-01

The 4th edition of this classic text provides a thorough coverage of RF and microwave engineering concepts, starting from fundamental principles of electrical engineering, with applications to microwave circuits and devices of practical importance.  Coverage includes microwave network analysis, impedance matching, directional couplers and hybrids, microwave filters, ferrite devices, noise, nonlinear effects, and the design of microwave oscillators, amplifiers, and mixers. Material on microwave and RF systems includes wireless communications, radar, radiometry, and radiation hazards. A large

Microwave radiometric detection of thermal asymmetry of varicocele

International Nuclear Information System (INIS)

Felderman, T.P.; Shaeffer, J.; El-Mahdi, A.M.; Carr, K.L.; Stecker, J.F. Jr.

1985-01-01

Varicocele, a varicose enlargement of the veins in the spermatic cord, is found in 21-39% of men being evaluated for infertility. Thermometric detection of this condition was attempted by microwave radiometry as well as by contact thermometry using thermistor probes. The inguinal and scrotal regions of 44 male subject and inguinal regions of 11 female subjects were studied. Substantially different thermal patterns were obtained by thermistors (surface temperature) and microwave radiometry (subsurface temperature). There was a correlation between left scrotal varicocele and a temperature elevation of the left spermatic cord using microwave radiometry. This thermal defect appeared to be corrected following surgery

Surface modification and stability of detonation nanodiamonds in microwave gas discharge plasma

Energy Technology Data Exchange (ETDEWEB)

Stanishevsky, Andrei V., E-mail: astan@uab.edu; Walock, Michael J.; Catledge, Shane A.

2015-12-01

Graphical abstract: - Highlights: • Single and binary gas plasma modification of nanodiamond powders studied. • Temperature-dependent effect of N{sub 2} and N{sub 2}/H{sub 2} plasma reported for the first time. • Role of H{sub 2} in H{sub 2}/N{sub 2} and H{sub 2}/O{sub 2} plasma modification of nanodiamond discussed. - Abstract: Detonation nanodiamonds (DND), with low hydrogen content, were exposed to microwave plasma generated in pure H{sub 2}, N{sub 2}, and O{sub 2} gases and their mixtures, and investigated using X-ray diffraction (XRD), Fourier Transform Infrared (FTIR), Raman, and X-ray photoelectron spectroscopies. Considerable alteration of the DND surface was observed under the plasma conditions for all used gases, but the diamond structure of the DND particle core was preserved in most cases. The stabilizing effect of H{sub 2} in H{sub 2}/N{sub 2} and H{sub 2}/O{sub 2} binary gas plasmas on the DND structure and the temperature-dependent formation of various CNH{sub x} surface groups in N{sub 2} and H{sub 2}/N{sub 2} plasmas were observed and discussed for the first time. DND surface oxidation and etching were the main effects of O{sub 2} plasma, whereas the N{sub 2} plasma led to DND surfaces rich in amide groups below 1073 K and nitrile groups at higher temperatures. Noticeable graphitization of the DND core structure was detected only in N{sub 2} plasma when the substrate temperature was above 1103 K.

Microwave plasma chemical synthesis of nanocrystalline carbon film structures and study their properties

Science.gov (United States)

Bushuev, N.; Yafarov, R.; Timoshenkov, V.; Orlov, S.; Starykh, D.

2015-08-01

The self-organization effect of diamond nanocrystals in polymer-graphite and carbon films is detected. The carbon materials deposition was carried from ethanol vapors out at low pressure using a highly non-equilibrium microwave plasma. Deposition processes of carbon film structures (diamond, graphite, graphene) is defined. Deposition processes of nanocrystalline structures containing diamond and graphite phases in different volume ratios is identified. The solid film was obtained under different conditions of microwave plasma chemical synthesis. We investigated the electrical properties of the nanocrystalline carbon films and identified it's from various factors. Influence of diamond-graphite film deposition mode in non-equilibrium microwave plasma at low pressure on emission characteristics was established. This effect is justified using the cluster model of the structure of amorphous carbon. It was shown that the reduction of bound hydrogen in carbon structures leads to a decrease in the threshold electric field of emission from 20-30 V/m to 5 V/m. Reducing the operating voltage field emission can improve mechanical stability of the synthesized film diamond-graphite emitters. Current density emission at least 20 A/cm2 was obtained. Nanocrystalline carbon film materials can be used to create a variety of functional elements in micro- and nanoelectronics and photonics such as cold electron source for emission in vacuum devices, photonic devices, cathodoluminescent flat display, highly efficient white light sources. The obtained graphene carbon net structure (with a net size about 6 μm) may be used for the manufacture of large-area transparent electrode for solar cells and cathodoluminescent light sources

Vacuum ultraviolet emission spectrum measurement of a microwave-discharge hydrogen-flow lamp in several configurations: Application to photodesorption of CO ice

Energy Technology Data Exchange (ETDEWEB)

Chen, Y.-J.; Wu, C.-Y. R. [Space Sciences Center and Department of Physics and Astronomy, University of Southern California, Los Angeles, CA 90089-1341 (United States); Chuang, K.-J.; Chu, C.-C.; Yih, T.-S. [Department of Physics, National Central University, Jhongli City, Taoyuan County 32054, Taiwan (China); Muñoz Caro, G. M. [Centro de Astrobiología, INTA-CSIC, Torrejón de Ardoz, E-28850 Madrid (Spain); Nuevo, M. [NASA Ames Research Center, Moffett Field, CA 94035 (United States); Ip, W.-H., E-mail: yujung@usc.edu [Graduate Institute of Astronomy, National Central University, Jhongli City, Taoyuan County 32049, Taiwan (China)

2014-01-20

We report measurements of the vacuum ultraviolet (VUV) emission spectra of a microwave-discharge hydrogen-flow lamp (MDHL), a common tool in astrochemistry laboratories working on ice VUV photoprocessing. The MDHL provides hydrogen Ly-α (121.6 nm) and H{sub 2} molecular emission in the 110-180 nm range. We show that the spectral characteristics of the VUV light emitted in this range, in particular the relative proportion of Ly-α to molecular emission bands, strongly depend on the pressure of H{sub 2} inside the lamp, the lamp geometry (F type versus T type), the gas used (pure H{sub 2} versus H{sub 2} seeded in He), and the optical properties of the window used (MgF{sub 2} versus CaF{sub 2}). These different configurations are used to study the VUV irradiation of CO ice at 14 K. In contrast to the majority of studies dedicated to the VUV irradiation of astrophysical ice analogs, which have not taken into consideration the emission spectrum of the MDHL, our results show that the processes induced by photons in CO ice from a broad energy range are different and more complex than the sum of individual processes induced by monochromatic sources spanning the same energy range, as a result of the existence of multistate electronic transitions and discrepancy in absorption cross sections between parent molecules and products in the Ly-α and H{sub 2} molecular emission ranges.

Vacuum ultraviolet emission spectrum measurement of a microwave-discharge hydrogen-flow lamp in several configurations: Application to photodesorption of CO ice

International Nuclear Information System (INIS)

Chen, Y.-J.; Wu, C.-Y. R.; Chuang, K.-J.; Chu, C.-C.; Yih, T.-S.; Muñoz Caro, G. M.; Nuevo, M.; Ip, W.-H.

2014-01-01

We report measurements of the vacuum ultraviolet (VUV) emission spectra of a microwave-discharge hydrogen-flow lamp (MDHL), a common tool in astrochemistry laboratories working on ice VUV photoprocessing. The MDHL provides hydrogen Ly-α (121.6 nm) and H 2 molecular emission in the 110-180 nm range. We show that the spectral characteristics of the VUV light emitted in this range, in particular the relative proportion of Ly-α to molecular emission bands, strongly depend on the pressure of H 2 inside the lamp, the lamp geometry (F type versus T type), the gas used (pure H 2 versus H 2 seeded in He), and the optical properties of the window used (MgF 2 versus CaF 2 ). These different configurations are used to study the VUV irradiation of CO ice at 14 K. In contrast to the majority of studies dedicated to the VUV irradiation of astrophysical ice analogs, which have not taken into consideration the emission spectrum of the MDHL, our results show that the processes induced by photons in CO ice from a broad energy range are different and more complex than the sum of individual processes induced by monochromatic sources spanning the same energy range, as a result of the existence of multistate electronic transitions and discrepancy in absorption cross sections between parent molecules and products in the Ly-α and H 2 molecular emission ranges.

Tunable surface plasmon instability leading to emission of radiation

Energy Technology Data Exchange (ETDEWEB)

Gumbs, Godfrey [Department of Physics and Astronomy, Hunter College of the City University of New York, 695 Park Avenue, New York, New York 10065 (United States); Donostia International Physics Center (DIPC), P de Manuel Lardizabal, 4, 20018 San Sebastian, Basque Country (Spain); Iurov, Andrii, E-mail: aiurov@chtm.unm.edu [Department of Physics and Astronomy, Hunter College of the City University of New York, 695 Park Avenue, New York, New York 10065 (United States); Center for High Technology Materials, University of New Mexico, Albuquerque, New Mexico 87106 (United States); Huang, Danhong [Air Force Research Laboratory, Space Vehicles Directorate, Kirtland Air Force Base, New Mexico 87117 (United States); Pan, Wei [Sandia National Laboratory, Albuquerque, New Mexico 87185 (United States)

2015-08-07

We propose a new approach for energy conversion from a dc electric field to tunable terahertz emission based on hybrid semiconductors by combining two-dimensional (2D) crystalline layers and a thick conducting material with possible applications for chemical analysis, security scanning, medical (single-molecule) imaging, and telecommunications. The hybrid nano-structure may consist of a single or pair of sheets of graphene, silicene, or a 2D electron gas. When an electric current is passed through a 2D layer, we discover that two low-energy plasmon branches exhibit a characteristic loop in their dispersion before they merge into an unstable region beyond a critical wave vector q{sub c}. This finite q{sub c} gives rise to a wavenumber cutoff in the emission dispersion of the surface plasmon induced instability and emission of radiation (spiler). However, there is no instability for a single driven layer far from the conductor, and the instability of an isolated pair of 2D layers occurs without a wavenumber cutoff. The wavenumber cutoff is found to depend on the conductor electron density, layer separation, distances of layers from the conductor surface, and the driving-current strength.

Interpretation of a correlation between the flux densities of extended hard x-rays and microwave solar bursts

International Nuclear Information System (INIS)

Nelson, G.J.; Stewart, R.T.

1979-01-01

In a previous paper the authors showed that for extended bursts a good correlation exists between the observed 100 keV X-ray flux density and the 3.75 or 9.4 GHz microwave flux density. They now propose a source model for the extended bursts in which the microwave emission comes from thin shells at increasing heights for decreasing frequencies. This model with reasonable parameter values gives the observed microwave spectral characteristics and also explains why the X-ray and microwave flux densities are so well correlated

Measurements and removal of substrate effects on the microwave surface impedance of YBCO films on SrTiO{sub 3}

Energy Technology Data Exchange (ETDEWEB)

Pompeo, N [Dipartimento di Fisica ' E Amaldi' and Unita CNISM, Universita Roma Tre, Via dellaVasca Navale 84, 00146 Rome (Italy); Muzzi, L [Dipartimento di Fisica ' E Amaldi' and Unita CNISM, Universita Roma Tre, Via dellaVasca Navale 84, 00146 Rome (Italy); Galluzzi, V [ENEA-Frascati, Via Enrico Fermi 45, 00044 Frascati, Rome (Italy); Marcon, R [Dipartimento di Fisica ' E Amaldi' and Unita CNISM, Universita Roma Tre, Via dellaVasca Navale 84, 00146 Rome (Italy); Silva, E [Dipartimento di Fisica ' E Amaldi' and Unita CNISM, Universita Roma Tre, Via dellaVasca Navale 84, 00146 Rome (Italy)

2007-10-15

We reconsider the problem of the measurements of the microwave complex surface impedance in thin superconducting films deposited on SrTiO{sub 3} substrates. We perform measurements of the complex surface impedance Z{sub s}' = R{sub s}'+i{delta}X{sub s}' of thin YBa{sub 2}Cu{sub 3}O{sub 7-{delta}} films deposited by laser ablation on SrTiO{sub 3} substrates. The typical oscillations due to the strong temperature variation of the SrTiO{sub 3} permittivity are confirmed in R{sub s}' and observed in {delta}X{sub s}'. The effects of the SrTiO{sub 3} substrate are evident even well below the superconducting transition temperature of YBa{sub 2}Cu{sub 3}O{sub 7-{delta}}. Similarly to previous works, we describe the overall response in terms of impedance transformations. We extend the known results by (i) considering the measurements of the imaginary part (ii) comparing the measurements to the absolute dc resistivity measured on the same sample, and (iii) suggesting a method for measuring the intrinsic thin film surface impedance by adjusting the substrate impedance. To demonstrate the feasibility of microwave measurements of intrinsic properties of films grown onto SrTiO{sub 3} substrates, we check the proposed method by measuring the field dependent surface impedance before and after removal of the substrate resonance.

Influence of Local Airflow on the Pollutant Emission from Indoor Building Surfaces

DEFF Research Database (Denmark)

Topp, Claus; Nielsen, Peter Vilhelm; Heiselberg, Per Kvols

2001-01-01

This article reports the results of an investigation, based on fundamental fluid dynamics and mass transfer theory, carried out to obtain a general understanding of the mechanisms involved in the emissions from building materials in ventilated rooms. In addition, a generally applicable method...... for the prediction of surface emissions is proposed. The work focused on the emission of vapours and gases and no particulate emissions were considered. The methods used were numerical calculations by computational fluid dynamics (CFD) and full-scale laboratory experiments. It was found that the emissions...

Nano-optomechanical system based on microwave frequency surface acoustic waves

Science.gov (United States)

Tadesse, Semere Ayalew

Cavity optomechnics studies the interaction of cavity confined photons with mechanical motion. The emergence of sophisticated nanofabrication technology has led to experimental demonstrations of a wide range of novel optomechanical systems that exhibit strong optomechanical coupling and allow exploration of interesting physical phenomena. Many of the studies reported so far are focused on interaction of photons with localized mechanical modes. For my doctoral research, I did experimental investigations to extend this study to propagating phonons. I used surface travelling acoustic waves as the mechanical element of my optomechanical system. The optical cavities constitute an optical racetrack resonator and photonic crystal nanocavity. This dissertation discusses implementation of this surface acoustic wave based optomechanical system and experimental demonstrations of important consequences of the optomechanical coupling. The discussion focuses on three important achievements of the research. First, microwave frequency surface acoustic wave transducers were co-integrated with an optical racetrack resonator on a piezoelectric aluminum nitride film deposited on an oxidized silicon substrate. Acousto-optic modulation of the resonance modes at above 10 GHz with the acoustic wavelength significantly below the optical wavelength was achieved. The phase and modal matching conditions in this paradigm were investigated for efficient optmechanical coupling. Second, the optomechanical coupling was pushed further into the sideband resolved regime by integrating the high frequency surface acoustic wave transducers with a photonic crystal nanocavity. This device was used to demonstrate optomecahnically induced transparency and absorption, one of the interesting consequences of cavity optomechanics. Phase coherent interaction of the acoustic wave with multiple nanocavities was also explored. In a related experiment, the photonic crystal nanoscavity was placed inside an acoustic

Microwave irradiation enhances kinetics of the biomimetic process of hydroxyapatite nanocomposites

International Nuclear Information System (INIS)

Guha, Avijit; Nayar, Suprabha; Thatoi, H N

2010-01-01

In situ synthesized hydroxyapatite-poly(vinyl) alcohol nanocomposite was subjected to microwave irradiation, post synthesis. Interestingly, the aging time of 1 week required for the normal biomimetic process was reduced to 1 h post microwave irradiation, as characterized by x-ray powder diffraction and transmission electron microscopy. The surface topography shows the tendency of tubules to cross-link with the help of microwave energy. The microwave energy seems to provide a directional pull to the polymer chains which could have led to an enhancement of the kinetics of phase formation. (communication)

A microwave resonance dew-point hygrometer

Science.gov (United States)

Underwood, R. J.; Cuccaro, R.; Bell, S.; Gavioso, R. M.; Madonna Ripa, D.; Stevens, M.; de Podesta, M.

2012-08-01

We report the first measurements of a quasi-spherical microwave resonator used as a dew-point hygrometer. In conventional dew-point hygrometers, the condensation of water from humid gas flowing over a mirror is detected optically, and the mirror surface is then temperature-controlled to yield a stable condensed layer. In our experiments we flowed moist air from a humidity generator through a quasi-spherical resonator and detected the onset of condensation by measuring the frequency ratio of selected microwave modes. We verified the basic operation of the device over the dew-point range 9.5-13.5 °C by comparison with calibrated chilled-mirror hygrometers. These tests indicate that the microwave method may allow a quantitative estimation of the volume and thickness of the water layer which is condensed on the inner surface of the resonator. The experiments reported here are preliminary due to the limited time available for the work, but show the potential of the method for detecting not only water but a variety of other liquid or solid condensates. The robust all-metal construction should make the device appropriate for use in industrial applications over a wide range of temperatures and pressures.

A microwave resonance dew-point hygrometer

International Nuclear Information System (INIS)

Underwood, R J; Bell, S; Stevens, M; De Podesta, M; Cuccaro, R; Gavioso, R M; Ripa, D Madonna

2012-01-01

We report the first measurements of a quasi-spherical microwave resonator used as a dew-point hygrometer. In conventional dew-point hygrometers, the condensation of water from humid gas flowing over a mirror is detected optically, and the mirror surface is then temperature-controlled to yield a stable condensed layer. In our experiments we flowed moist air from a humidity generator through a quasi-spherical resonator and detected the onset of condensation by measuring the frequency ratio of selected microwave modes. We verified the basic operation of the device over the dew-point range 9.5–13.5 °C by comparison with calibrated chilled-mirror hygrometers. These tests indicate that the microwave method may allow a quantitative estimation of the volume and thickness of the water layer which is condensed on the inner surface of the resonator. The experiments reported here are preliminary due to the limited time available for the work, but show the potential of the method for detecting not only water but a variety of other liquid or solid condensates. The robust all-metal construction should make the device appropriate for use in industrial applications over a wide range of temperatures and pressures. (paper)

High temperature superconducting YBCO microwave filters

Science.gov (United States)

Aghabagheri, S.; Rasti, M.; Mohammadizadeh, M. R.; Kameli, P.; Salamati, H.; Mohammadpour-Aghdam, K.; Faraji-Dana, R.

2018-06-01

Epitaxial thin films of YBCO high temperature superconductor are widely used in telecommunication technology such as microwave filter, antenna, coupler and etc., due to their lower surface resistance and lower microwave loss than their normal conductor counterparts. Thin films of YBCO were fabricated by PLD technique on LAO substrate. Transition temperature and width were 88 K and 3 K, respectively. A filter pattern was designed and implemented by wet photolithography method on the films. Characterization of the filter at 77 K has been compared with the simulation results and the results for a made gold filter. Both YBCO and gold filters show high microwave loss. For YBCO filter, the reason may be due to the improper contacts on the feedlines and for gold filter, low thickness of the gold film has caused the loss increased.

Observation of a Short Period Quasi-periodic Pulsation in Solar X-Ray, Microwave, and EUV Emissions

Energy Technology Data Exchange (ETDEWEB)

Kumar, Pankaj; Cho, Kyung-Suk [Korea Astronomy and Space Science Institute (KASI), Daejeon, 305-348 (Korea, Republic of); Nakariakov, Valery M., E-mail: pankaj@kasi.re.kr [Centre for Fusion, Space and Astrophysics, Department of Physics, University of Warwick, CV4 7AL (United Kingdom)

2017-02-10

This paper presents the multiwavelength analysis of a 13 s quasi-periodic pulsation (QPP) observed in hard X-ray (12–300 keV) and microwave (4.9–34 GHz) emissions during a C-class flare that occurred on 2015 September 21. Atmospheric Image Assembly (AIA) 304 and 171 Å images show an emerging loop/flux tube (L1) moving radially outward, which interacts with the preexisting structures within the active region (AR). The QPP was observed during the expansion of and rising motion of L1. The Nobeyama Radioheliograph microwave images in 17/34 GHz channels reveal a single radio source that was co-spatial with a neighboring loop (L2). In addition, using AIA 304 Å images, we detected intensity oscillations in the legs of L2 with a period of about 26 s. A similar oscillation period was observed in the GOES soft X-ray flux derivative. This oscillation period seems to increase with time. We suggest that the observed QPP is most likely generated by the interaction between L2 and L3 observed in the AIA hot channels (131 and 94 Å). The merging speed of loops L2 and L3 was ∼35 km s{sup −1}. L1 was destroyed possibly by its interaction with preexisting structures in the AR, and produced a cool jet with the speed of ∼106–118 km s{sup −1} associated with a narrow CME (∼770 km s{sup −1}). Another mechanism of the QPP in terms of a sausage oscillation of the loop (L2) is also possible.

Speciation analysis of organomercurial compounds in Fish Tissue by capillary gas chromatography coupled to microwave-induced plasma atomic emission detection

Directory of Open Access Journals (Sweden)

Dorfe Díaz

Full Text Available This paper describes a novel approach for analysis of mercury speciation in fish using gas chromatography coupled with microwave-induced plasma optical emission spectrometry (GC-MIP-OES in surfatron resonant cavity. Sample treatment was based on quantitative leaching of mercury species from fish tissue with ultrasound-assisted acid-toluene extraction. The extracted mercury species analyzed with GC-MIP-OES attained detection limits of 5 and 9 pg for methylmercury (MeHg and ethylmercury (EtHg, respectively. A complete chromatogram could be completed in 1.5 min. MeHg values obtained with GC-MIP-OES were matched with organic mercury values obtained with selective reduction cold vapour- atomic absorption spectrometry (CV-AAS.

The use of design of experiments for the evaluation of the production of surface rich activated carbon from sewage sludge via microwave and conventional pyrolysis

International Nuclear Information System (INIS)

Simões dos Reis, Glaydson; Wilhelm, Michaela; Silva, Thamires Canuto de Almeida; Rezwan, Kurosch; Sampaio, Carlos Hoffmann; Lima, Eder Claudio; Guelli Ulson de Souza, Selene M.A.

2016-01-01

Highlights: • Using of DOE for preparation of AC by conventional and microwave pyrolysis. • The significant parameters in producing activated carbon were investigated. • Conventional pyrolysis AC had better textural development than microwave AC. • Temperature and holding time had significant influence on the S_B_E_T. • Reduction of production cost of activated carbon. - Abstract: Experimental design and response surface methodology were used for the preparation and comparison of activated carbon produced from sewage sludge by two types of pyrolysis: conventional furnace and microwave. The preparation method was performed following a full fractional factorial design (2"3), including pyrolysis temperature or power radiation, holding time and chemical activation agent, and specific surface area (S_B_E_T) of prepared activated carbon. The influence of these factors on the S_B_E_T of obtained carbon was investigated using an analysis of variance. Samples made by conventional pyrolysis showed overall higher S_B_E_T values than samples synthesised by the microwave method. The optimum parameters for the preparation of activated carbon using the conventional pyrolysis have been identified as: pyrolysis temperature of 500 °C, holding time of 15 min, and a ratio of ZnCl_2:sludge of 0.5. Microwave pyrolysis is found to be optimal when operating at 980 W for 12 min. Under these conditions, S_B_E_T values of 679 and 501 m"2g"−"1, respectively, have been obtained. The analysis of nitrogen adsorption/desorption isotherms revealed the presence of micro and mesopores in the activated carbon. The most important significant factor, according statistical analysis, in the variance in S_B_E_T for the conventional pyrolysis samples were the pyrolysis temperature and interaction between pyrolysis temperature, holding time and ratio of ZnCl_2:sludge were the most important factors. The highest impact parameters for the microwave method were found for the interaction

Optimization of microwave-assisted extraction for anthocyanins, polyphenols, and antioxidants from raspberry (Rubus Coreanus Miq.) using response surface methodology.

Science.gov (United States)

Teng, Hui; Lee, Won Young; Choi, Yong Hee

2013-09-01

Anthocyanins (Acys), polyphenols, and antioxidants were extracted from raspberry (Rubus Coreanus Miq.) using a highly efficient microwave-assisted extraction technique. Different solvents, including methanol, ethanol, and acetone, were tested. The colors of the extracts varied from light yellow to purple red or dark red. SEM and other nutrient analyses verified that ethanol was the most favorable medium for the microwave-assisted extraction of raspberry due to its high output and low toxicity. Effects of process parameters, including microwave power, irradiation time, and solvent concentration, were investigated through response surface methodology. Canonical analysis estimated that the highest total Acys content, total polyphenols content, and antioxidant activity of raspberry were 17.93 mg cyanidin-3-O-glucoside equivalents per gram dry weight, 38.57 mg gallic acid equivalents per gram dry weight, and 81.24%, respectively. The polyphenol compositions of raspberry extract were identified by HPLC with diode array detection, and nine kinds of polyphenols were identified and quantified, revealing that chlorogenic acid, syringic acid, and rutin are the major polyphenols contained in raspberry fruits. Compared with other fruits and vegetables, raspberry contains higher Acy and polyphenol contents with stronger antioxidant activity, suggesting that raspberry fruits are a good source of natural food colorants and antioxidants. © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Surface charge compensation for a highly charged ion emission microscope

International Nuclear Information System (INIS)

McDonald, J.W.; Hamza, A.V.; Newman, M.W.; Holder, J.P.; Schneider, D.H.G.; Schenkel, T.

2003-01-01

A surface charge compensation electron flood gun has been added to the Lawrence Livermore National Laboratory (LLNL) highly charged ion (HCI) emission microscope. HCI surface interaction results in a significant charge residue being left on the surface of insulators and semiconductors. This residual charge causes undesirable aberrations in the microscope images and a reduction of the Time-Of-Flight (TOF) mass resolution when studying the surfaces of insulators and semiconductors. The benefits and problems associated with HCI microscopy and recent results of the electron flood gun enhanced HCI microscope are discussed

Microwave Atmospheric-Pressure Sensor

Science.gov (United States)

Flower, D. A.; Peckham, G. E.; Bradford, W. J.

1986-01-01

Report describes tests of microwave pressure sounder (MPS) for use in satellite measurements of atmospheric pressure. MPS is multifrequency radar operating between 25 and 80 GHz. Determines signal absorption over vertical path through atmosphere by measuring strength of echoes from ocean surface. MPS operates with cloud cover, and suitable for use on current meteorological satellites.

Microplasmas ignited and sustained by microwaves

Science.gov (United States)

Hopwood, Jeffrey; Hoskinson, Alan R.; Gregório, José

2014-12-01

The challenges and benefits of microwave-induced microdischarges are reviewed. Transmission lines, resonators and surface wave launchers may be used for coupling microwave power to very small plasmas. Fortunately, microplasmas are typically much smaller than the wavelength of microwaves, and the electromagnetic problem may be treated electrostatically within the plasma. It is possible to trap electrons within small discharge gaps if the amplitude of electron oscillation is smaller than the plasma size. Typically occurring above 0.3 GHz, this condition results in lower breakdown fields than are required by direct current or radio frequency systems. Trapping of electrons also decreases the electrode potential to only tens of volts and makes the plasma density invariant in time. The steady-state microplasma produces electron densities of up to 1015 cm-3 in argon but the electrons are not in equilibrium with the low gas temperatures (500-1000 K). Microwave discharges are compared with other forms of microplasma and guidelines for device selection are recommended. Scale-up of microplasmas using array concepts are presented followed by some exciting new applications.

Optimization of formulation of soy-cakes baked in infrared-microwave combination oven by response surface methodology.

Science.gov (United States)

Şakıyan, Özge

2015-05-01

The aim of present work is to optimize the formulation of a functional cake (soy-cake) to be baked in infrared-microwave combination oven. For this optimization process response surface methodology was utilized. It was also aimed to optimize the processing conditions of the combination baking. The independent variables were the baking time (8, 9, 10 min), the soy flour concentration (30, 40, 50 %) and the DATEM (diacetyltartaric acid esters of monoglycerides) concentration (0.4, 0.6 and 0.8 %). The quality parameters that were examined in the study were specific volume, weight loss, total color change and firmness of the cake samples. The results were analyzed by multiple regression; and the significant linear, quadratic, and interaction terms were used in the second order mathematical model. The optimum baking time, soy-flour concentration and DATEM concentration were found as 9.5 min, 30 and 0.72 %, respectively. The corresponding responses of the optimum points were almost comparable with those of conventionally baked soy-cakes. So it may be declared that it is possible to produce high quality soy cakes in a very short time by using infrared-microwave combination oven.

Bayesian Analysis of the Cosmic Microwave Background

Science.gov (United States)

Jewell, Jeffrey

2007-01-01

There is a wealth of cosmological information encoded in the spatial power spectrum of temperature anisotropies of the cosmic microwave background! Experiments designed to map the microwave sky are returning a flood of data (time streams of instrument response as a beam is swept over the sky) at several different frequencies (from 30 to 900 GHz), all with different resolutions and noise properties. The resulting analysis challenge is to estimate, and quantify our uncertainty in, the spatial power spectrum of the cosmic microwave background given the complexities of "missing data", foreground emission, and complicated instrumental noise. Bayesian formulation of this problem allows consistent treatment of many complexities including complicated instrumental noise and foregrounds, and can be numerically implemented with Gibbs sampling. Gibbs sampling has now been validated as an efficient, statistically exact, and practically useful method for low-resolution (as demonstrated on WMAP 1 and 3 year temperature and polarization data). Continuing development for Planck - the goal is to exploit the unique capabilities of Gibbs sampling to directly propagate uncertainties in both foreground and instrument models to total uncertainty in cosmological parameters.

Synthesis of zinc aluminate with high surface area by microwave hydrothermal method applied in the transesterification of soybean oil (biodiesel)

International Nuclear Information System (INIS)

Quirino, M.R.; Oliveira, M.J.C.; Keyson, D.; Lucena, G.L.; Oliveira, J.B.L.; Gama, L.

2016-01-01

Highlights: • ZnAl_2O_4 spinel was synthesized by the microwave hydrothermal method in only 15 or 30 min. • The powders show high specific surface area. • ZAT_b15 showed activity of 52.22% for the conversion of soybean oil into biodiesel. - Abstract: Zinc aluminate is a material with high thermal stability and high mechanical strength that, owing to these properties, is used as a catalyst or support. In this work, zinc aluminate spinel was synthesized by the microwave hydrothermal method in only 15 or 30 min at a low temperature (150 °C) without templates, using only Al(NO_3)_3·9H_2O, Zn(NO_3)_2·6H_2O, and urea as precursors and applied in the transesterification of soybean oil. X-ray diffraction analysis showed that ZnAl_2O_4 had a cubic structure without secondary phases. The nitrogen adsorption measurements (BET) revealed a high surface area (266.57 m"2 g"−"1) for the nanopowder synthesized in 15 min. This powder showed activity of 52.22% for the catalytic conversion of soybean oil into biodiesel by transesterification.

Microwave transport in EBT distribution manifolds using Monte Carlo ray-tracing techniques

International Nuclear Information System (INIS)

Lillie, R.A.; White, T.L.; Gabriel, T.A.; Alsmiller, R.G. Jr.

1983-01-01

Ray tracing Monte Carlo calculations have been carried out using an existing Monte Carlo radiation transport code to obtain estimates of the microsave power exiting the torus coupling links in EPT microwave manifolds. The microwave power loss and polarization at surface reflections were accounted for by treating the microwaves as plane waves reflecting off plane surfaces. Agreement on the order of 10% was obtained between the measured and calculated output power distribution for an existing EBT-S toroidal manifold. A cost effective iterative procedure utilizing the Monte Carlo history data was implemented to predict design changes which could produce increased manifold efficiency and improved output power uniformity

Relative impacts of worldwide tropospheric ozone changes and regional emission modifications on European surface-ozone levels

International Nuclear Information System (INIS)

Szopa, S.; Hauglustaine, D.A.

2007-01-01

Multi-scale models were applied to assess the surface ozone changes in 2030. Several emission scenarios are considered, ranging from (a) a pessimistic anthropogenic emission increase to (b) an optimistic decrease of emissions, and including (c) a realistic scenario that assumes the implementation of control legislations [CLE]. The two extreme scenarios lead respectively to homogeneous global increase and decrease of surface ozone, whereas low and inhomogeneous changes associated with a slight global increase of ozone are found for the CLE scenario. Over western Europe, for the CLE scenario, the benefit of European emission reduction is significantly counterbalanced by increasing global ozone levels. Considering warmer conditions over Europe and future emission modifications, the human health exposure to surface ozone is found to be significantly worsened. (authors)

Surface-plasmon-enhanced lasing emission based on polymer distributed feedback laser

Energy Technology Data Exchange (ETDEWEB)

Zhang, Dingke, E-mail: dingke.zhang@gmail.com, E-mail: shijianchen@gmail.com [School of Physics and Electronic Engineering, Chongqing Normal University, Chongqing 401331 (China); Chen, Shijian, E-mail: dingke.zhang@gmail.com, E-mail: shijianchen@gmail.com; Huang, Yingzhou; Zhang, Zhen [School of Physics, Chongqing University, Chongqing 401331 (China); Wang, Yanping; Ma, Dongge [State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022 (China)

2015-01-14

Optical losses associated with the metallic contacts necessary for charge injection are an obstacle to the development of electrically pumped organic lasers. In this work, we show that it is possible to overcome these losses by introducing surface plasmons (SPs) in a distributed feedback laser to enhance the lasing emission. We perform a detailed study of the SPs influence on the lasing emission. We experimentally show that enhanced lasing emission has been successfully achieved in the presence of a metal electrode. The laser emission is strongly dependent on the thickness of Ag layer. By optimizing the thickness of Ag layer, surface-plasmon-enhanced lasing emission has been achieved with much reduced thresholds and higher intensity. When the thickness of the Ag layer increases to 50 nm, the device exhibits ten-fold emission intensity and a fifth of excitation threshold comparing with Ag-free one. The finite-difference time-domain (FDTD) results show that large field intensity is built at the 4-(dicyanomethylene)-2-i-propyl-6-(1,1,7,7-tetramethyljulolidyl-9-enyl) -4H-pyran:/poly(9-vinylcarbazole)Ag interface, which could lead to a strong coupling between lasing and SPs, and consequently a much enhanced laser emission at the photon energy of around 2.02 eV (615 nm). Our FDTD simulations gave an explanation of the effects of the SPs on lasing operation in the periodic structures. The use of SPs would lead to a new class of highly efficient solid-state laser sources and provide a new path to achieve electrically pumped organic lasers.

Improving the indoor air quality by using a surface emissions trap

Science.gov (United States)

Markowicz, Pawel; Larsson, Lennart

2015-04-01

The surface emissions trap, an adsorption cloth developed for reducing emissions of volatile organic compounds and particulate matter from surfaces while allowing evaporation of moisture, was used to improve the indoor air quality of a school building with elevated air concentrations of 2-ethyl-1-hexanol. An improvement of the perceived air quality was noticed a few days after the device had been attached on the PVC flooring. In parallel, decreased air concentrations of 2-ethyl-1-hexanol were found as well as a linear increase of the amounts of the same compound adsorbed on the installed cloth as observed up to 13 months after installation. Laboratory studies revealed that the performance of the device is not affected by differences in RH (35-85%), temperature (30-40 °C) or by accelerated aging simulating up to 10 years product lifetime, and, from a blinded exposure test, that the device efficiently blocks chemical odors. This study suggests that the device may represent a fast and efficient means of restoring the indoor air quality in a building e.g. after water damage leading to irritating and potentially harmful emissions from building material surfaces indoors.

Effect of metallic and hyperbolic metamaterial surfaces on electric and magnetic dipole emission transitions

DEFF Research Database (Denmark)

Ni, X.; Naik, G. V.; Kildishev, A. V.

2011-01-01

Spontaneous emission patterns of electric and magnetic dipoles on different metallic surfaces and a hyperbolic metamaterial (HMM) surface were simulated using the dyadic Green’s function technique. The theoretical approach was verified by experimental results obtained by measuring angular......-dependent emission spectra of europium ions on top of different films. The results show the modified behavior of electric and magnetic dipoles on metallic and HMM surfaces. The results of numerical calculations agree well with experimental data....

Microwave imaging

CERN Document Server

Pastorino, Matteo

2010-01-01

An introduction to the most relevant theoretical and algorithmic aspects of modern microwave imaging approaches Microwave imaging-a technique used in sensing a given scene by means of interrogating microwaves-has recently proven its usefulness in providing excellent diagnostic capabilities in several areas, including civil and industrial engineering, nondestructive testing and evaluation, geophysical prospecting, and biomedical engineering. Microwave Imaging offers comprehensive descriptions of the most important techniques so far proposed for short-range microwave imaging-in

Modulated microwave microscopy and probes used therewith

Science.gov (United States)

Lai, Keji; Kelly, Michael; Shen, Zhi-Xun

2012-09-11

A microwave microscope including a probe tip electrode vertically positionable over a sample and projecting downwardly from the end of a cantilever. A transmission line connecting the tip electrode to the electronic control system extends along the cantilever and is separated from a ground plane at the bottom of the cantilever by a dielectric layer. The probe tip may be vertically tapped near or at the sample surface at a low frequency and the microwave signal reflected from the tip/sample interaction is demodulated at the low frequency. Alternatively, a low-frequency electrical signal is also a non-linear electrical element associated with the probe tip to non-linearly interact with the applied microwave signal and the reflected non-linear microwave signal is detected at the low frequency. The non-linear element may be semiconductor junction formed near the apex of the probe tip or be an FET formed at the base of a semiconducting tip.

Ag-protein plasmonic architectures for surface plasmon-coupled emission enhancements and Fabry-Perot mode-coupled directional fluorescence emission

Science.gov (United States)

Badiya, Pradeep Kumar; Patnaik, Sai Gourang; Srinivasan, Venkatesh; Reddy, Narendra; Manohar, Chelli Sai; Vedarajan, Raman; Mastumi, Noriyoshi; Belliraj, Siva Kumar; Ramamurthy, Sai Sathish

2017-10-01

We report the use of silver decorated plant proteins as spacer material for augmented surface plasmon-coupled emission (120-fold enhancement) and plasmon-enhanced Raman scattering. We extracted several proteins from different plant sources [Triticum aestivum (TA), Aegle marmelos (AM), Ricinus communis (RC), Jatropha curcas (JC) and Simarouba glauca (SG)] followed by evaluation of their optical properties and simulations to rationalize observed surface plasmon resonance. Since the properties exhibited by protein thin films is currently gaining research interest, we have also carried out simulation studies with Ag-protein biocomposites as spacer materials in metal-dielectric-metal planar microcavity architecture for guided emission of Fabry-Perot mode-coupled fluorescence.

On the Earth Microwave Background: Absorption and Scattering by the Atmosphere

Directory of Open Access Journals (Sweden)

Robitaille P.-M.

2007-07-01

Full Text Available The absorption and scattering of microwave radiation by the atmosphere of the Earth is considered under a steady state scenario. Using this approach, it is demonstrated that the microwave background could not have a cosmological origin. Scientific observations in the microwave region are explained by considering an oceanic source, combined with both Rayleigh and Mie scattering in the atmosphere in the absence of net absorption. Importantly, at high frequencies, Mie scattering occurs primarily with forward propagation. This helps to explain the lack of high frequency microwave background signals when radio antennae are positioned on the Earth’s surface.

Improvements in or relating to microwave heating

International Nuclear Information System (INIS)

Hardwick, W.H.; Gayler, R.

1984-01-01

The invention is concerned with microwave heating and more particularly with microwave heating to effect melting. Material is contained in a container and microwave energy is applied to melt material while a portion of the material adjacent to the internal surfaces of the container is maintained at a temperature at which it is not molten. This may be by cooling water in vessel. The invention therefore provides for ''skull'' melting in which a layer of non-molten material protects the container from molten material. Examples of materials which may be treated in accordance with the present invention are glasses and glass-like materials and precursors therefor (e.g. glasses and glass-like materials or precursors therefor containing radioactive wastes). (author)

X-ray emission in slow highly charged ion-surface collisions

International Nuclear Information System (INIS)

Watanabe, H; Abe, T; Fujita, Y; Sun, J; Takahashi, S; Tona, M; Yoshiyasu, N; Nakamura, N; Sakurai, M; Yamada, C; Ohtani, S

2007-01-01

X-rays emitted in the collisions of highly charged ions with a surface have been measured to investigate dissipation schemes of their potential energies. While 8.1% of the potential energy was dissipated in the collisions of He-like I ions with a W surface, 29.1% has been dissipated in the case of He-like Bi ions. The x-ray emissions play significant roles in the dissipation of the potential energies in the interaction of highly charged heavy ions with the surface

An introduction to microwave imaging for breast cancer detection

CERN Document Server

Conceição, Raquel Cruz; O'Halloran, Martin

2016-01-01

This book collates past and current research on one of the most promising emerging modalities for breast cancer detection. Readers will discover how, as a standalone technology or in conjunction with another modality, microwave imaging has the potential to provide reliable, safe and comfortable breast exams at low cost. Current breast imaging modalities include X- ray, Ultrasound, Magnetic Resonance Imaging, and Positron Emission Tomography. Each of these methods suffers from limitations, including poor sensitivity or specificity, high cost, patient discomfort, and exposure to potentially harmful ionising radiation. Microwave breast imaging is based on a contrast in the dielectric properties of breast tissue that exists at microwave frequencies. The book begins by considering the anatomy and dielectric properties of the breast, contrasting historical and recent studies. Next, radar-based breast imaging algorithms are discussed, encompassing both early-stage artefact removal, and data independent and adaptive ...

Ka-band microwave generation using the Smith-Purcell effect

International Nuclear Information System (INIS)

Ekdahl, C.A.; Davis, H.A.

1983-01-01

The CERETRON microwave generator concept relies on the conversion of intense relativistic electron beam (REB) energy into highpower microwave emission through the Smith-Purcell effect. We report initial results from experiments with the production of Ka-band Smith-Purcell radiation generated by a 50-kA, 2.8-MeV beam propagated through a cylindrical transmission grating with lambda 0 = 1 cm. These experiments were performed without a quasi-optical resonator, and the output was limited by breakdown of the grating and by limited access through the 90-kG magnet coil. Nevertheless, the measured power output from these initial experiments was about 7 kW in the Ka band

Effect of Er{sup 3+} ions on the phase formation and properties of In{sub 2}O{sub 3}nanostructures crystallized upon microwave heating

Energy Technology Data Exchange (ETDEWEB)

Lemos, Samantha C.S.; Romeiro, Fernanda C.; Paula, Leonardo F. de [Instituto de Química, Universidade Federal de Uberlândia, 38400-902 Uberlândia, MG (Brazil); Gonçalves, Rosana F. [UNIFESP, Universidade Federal de São Paulo, 09972-270 Diadema, SP (Brazil); Moura, Ana P. de [LIEC, Instituto de Química, Universidade Estadual Paulista, 14800-900 Araraquara, SP (Brazil); Ferrer, Mateus M.; Longo, Elson [INCTMN-UFSCar, Universidade Federal de São Carlos, 13565-905 São Carlos, SP (Brazil); Patrocinio, Antonio Otavio T. [Instituto de Química, Universidade Federal de Uberlândia, 38400-902 Uberlândia, MG (Brazil); Lima, Renata C., E-mail: rclima@ufu.br [Instituto de Química, Universidade Federal de Uberlândia, 38400-902 Uberlândia, MG (Brazil)

2017-05-15

Regular sized nanostructures of indium oxide (In{sub 2}O{sub 3}) were homogeneously grown using a facile route, i.e. a microwave-hydrothermal method combined with rapid thermal treatment in a microwave oven. The presence of Er{sup 3+} doping plays an important role in controlling the formation of cubic (bcc) and rhombohedral (rh) In{sub 2}O{sub 3} phases. The samples presented broad photoluminescent emission bands in the green-orange region, which were attributed to the recombination of electrons at oxygen vacancies. The photocatalytic activities of pure bcc-In{sub 2}O{sub 3} and a bcc-rh-In{sub 2}O{sub 3} mixture towards the UVA degradation of methylene blue (MB) were also evaluated. The results showed that Er{sup +3} doped In{sub 2}O{sub 3} exhibited the highest photocatalytic activity with a photonic efficiency three times higher than the pure oxide. The improved performance was attributed to the higher surface area, the greater concentration of electron traps due the presence of the dopant and the possible formation of heterojunctions between the cubic and rhombohedral phases. - Graphical abstract: Photodegradation curves as a function of irradiation time of the samples obtained upon rapid microwave heating. - Highlights: • Efficient and rapid microwave heating to obtain Er{sup 3+} doped In{sub 2}O{sub 3} nanostructures. • Er{sup 3+} ions doping is fundamental to stabilizing the crystalline rhombohedral phase. • Symmetry breaking induced by vacancies in the lattice leads to photoluminescence. • Surface area of doped sample was two times higher than the surface of pure oxide. • The presence of defects in the lattice structure favors photocatalytic activity.

Observations of Anomalous Microwave Emission from HII Regions

Directory of Open Access Journals (Sweden)

Clive Dickinson

2013-01-01

free-free emission from UCHII regions may be also be significant in some cases. The AME emissivity, defined as the ratio of the AME brightness to the 100 μm brightness, is comparable to the value observed in high-latitude diffuse cirrus in some regions, but is significantly lower in others. However, this value is dependent on the dust temperature. More data, both at high frequencies (>~5 GHz and high resolution (~1′ or better is required to disentangle the emission processes in such complex regions.

Photodegradation of HCFC-22 Using Microwave Discharge Electrodeless Mercury Lamp with TiO2 Photocatalyst Balls

Directory of Open Access Journals (Sweden)

Seong-Gyu Seo

2014-01-01

Full Text Available The photodegradation of chlorodifluoromethane (HCFC-22 was investigated using microwave/UV/TiO2 photocatalysts hybrid system. The microwave discharge electrodeless mercury lamp (MDEML used in this study showed mainly atomic Hg emission lines at 253.7 nm. The decomposition efficiency of HCFC-22 increased with decreasing inlet concentration and with increasing reactor residence time. The removal efficiency increased with increasing microwave power on every oxygen concentration. The highest degradation efficiency was obtained when both TiO2 balls and MDEML were used.

Converting a Microwave Oven into a Plasma Reactor: A Review

Directory of Open Access Journals (Sweden)

Victor J. Law

2018-01-01

Full Text Available This paper reviews the use of domestic microwave ovens as plasma reactors for applications ranging from surface cleaning to pyrolysis and chemical synthesis. This review traces the developments from initial reports in the 1980s to today’s converted ovens that are used in proof-of-principle manufacture of carbon nanostructures and batch cleaning of ion implant ceramics. Information sources include the US and Korean patent office, peer-reviewed papers, and web references. It is shown that the microwave oven plasma can induce rapid heterogeneous reaction (solid to gas and liquid to gas/solid plus the much slower plasma-induced solid state reaction (metal oxide to metal nitride. A particular focus of this review is the passive and active nature of wire aerial electrodes, igniters, and thermal/chemical plasma catalyst in the generation of atmospheric plasma. In addition to the development of the microwave oven plasma, a further aspect evaluated is the development of methodologies for calibrating the plasma reactors with respect to microwave leakage, calorimetry, surface temperature, DUV-UV content, and plasma ion densities.

Simultaneous determination of macro and trace elements in biological reference materials by microwave induced plasma optical emission spectrometry with slurry sample introduction

International Nuclear Information System (INIS)

Matusiewicz, Henryk; Golik, Bartosz

2004-01-01

A slurry sampling technique (SST) has been utilized for simultaneous multi-element analysis by microwave-induced plasma optical emission spectrometry (MIP-OES). Slurry samples from a spray chamber are fed directly into the microwave cavity-torch assembly (power 300 W) with no desolvation apparatus. The performance of SST-MIP-OES was demonstrated by the determination of macro (Na, K, Ca, Mg, P) and trace (Cd, Cu, Mn, Sr, Zn) elements in three biological certified reference materials using a V-groove, clog-free Babington-type nebulizer. Slurry concentrations up to 1% m/v (particles 3 (pH 1.2) containing 0.01% of Triton X-100, were used with calibration by the standard additions method. The method offers relatively good precision (R.S.D. ranged from 7 to 11%) with measured concentrations being in satisfactory agreement with certified values for NRCC TORT-1 (Lobster hepatopancreas), NRCC LUTS-1 (Lobster hepatopancreas) and IAEA-153 (Milk powder). The concentrations of Na, K, Ca, Mg, P and Cd, Cu, Mn, Sr, Zn were determined in the range 90-22 000 μg/g and 1-420 μg/g, respectively. The method could be useful as a routine procedure

A flat Universe from high-resolution maps of the cosmic microwave background radiation

Science.gov (United States)

de Bernardis P; Ade; Bock; Bond; Borrill; Boscaleri; Coble; Crill; De Gasperis G; Farese; Ferreira; Ganga; Giacometti; Hivon; Hristov; Iacoangeli; Jaffe; Lange; Martinis; Masi; Mason; Mauskopf; Melchiorri; Miglio; Montroy; Netterfield

2000-04-27

The blackbody radiation left over from the Big Bang has been transformed by the expansion of the Universe into the nearly isotropic 2.73 K cosmic microwave background. Tiny inhomogeneities in the early Universe left their imprint on the microwave background in the form of small anisotropies in its temperature. These anisotropies contain information about basic cosmological parameters, particularly the total energy density and curvature of the Universe. Here we report the first images of resolved structure in the microwave background anisotropies over a significant part of the sky. Maps at four frequencies clearly distinguish the microwave background from foreground emission. We compute the angular power spectrum of the microwave background, and find a peak at Legendre multipole Ipeak = (197 +/- 6), with an amplitude delta T200 = (69 +/- 8) microK. This is consistent with that expected for cold dark matter models in a flat (euclidean) Universe, as favoured by standard inflationary models.

Electron emission and energy loss in grazing collisions of protons with insulator surfaces

International Nuclear Information System (INIS)

Gravielle, M. S.; Miraglia, J. E.; Aldazabal, I.; Arnau, A.; Ponce, V. H.; Aumayr, F.; Lederer, S.; Winter, H.

2007-01-01

Electron emission from LiF, KCl, and KI crystal surfaces during grazing collisions of swift protons is studied using a first-order distorted-wave formalism. Owing to the localized character of the electronic structure of these surfaces, we propose a model that allows us to describe the process as a sequence of atomic transitions from different target ions. Experimental results are presented for electron emission from LiF and KI and energy loss from KI surfaces. Calculations show reasonable agreement with these experimental data. The role played by the charge of the incident particle is also investigated

Electron emission from MOS electron emitters with clean and cesium covered gold surface

DEFF Research Database (Denmark)

Nielsen, Gunver; Thomsen, Lasse Bjørchmar; Johansson, Martin

2009-01-01

MOS (metal-oxide-semiconductor) electron emitters consisting of a Si substrate, a SiO2 tunnel barrier and a Ti (1 nm)/Au(7 nm) top-electrode, with an active area of 1 cm(2) have been produced and studied with surface science techniques under UHV (ultra high vacuum) conditions and their emission...... characteristics have been investigated. It is known, that deposition of an alkali metal on the emitting surface lowers the work function and increases the emission efficiency. For increasing Cs coverages the surface has been characterized by X-ray Photoelectron Spectroscopy (XPS), Ion Scattering Spectroscopy (ISS...

FINGERPRINTS OF GALACTIC LOOP I ON THE COSMIC MICROWAVE BACKGROUND

International Nuclear Information System (INIS)

Liu, Hao; Mertsch, Philipp; Sarkar, Subir

2014-01-01

We investigate possible imprints of galactic foreground structures such as the ''radio loops'' in the derived maps of the cosmic microwave background. Surprisingly, there is evidence for these not only at radio frequencies through their synchrotron radiation, but also at microwave frequencies where emission by dust dominates. This suggests the mechanism is magnetic dipole radiation from dust grains enriched by metallic iron or ferrimagnetic molecules. This new foreground we have identified is present at high galactic latitudes, and potentially dominates over the expected B-mode polarization signal due to primordial gravitational waves from inflation

Mechanism of negative ion emission from surfaces of ferroelectrics