Sample records for surface high aspect

  1. Different methods to alter surface morphology of high aspect ratio structures

    Energy Technology Data Exchange (ETDEWEB)

    Leber, M., E-mail: [Department of Electrical and Computer Engineering, University of Utah, Salt Lake City, UT (United States); Shandhi, M.M.H. [Department of Electrical and Computer Engineering, University of Utah, Salt Lake City, UT (United States); Hogan, A. [Blackrock Microsystems, Salt Lake City, UT (United States); Solzbacher, F. [Department of Electrical and Computer Engineering, University of Utah, Salt Lake City, UT (United States); Bhandari, R.; Negi, S. [Department of Electrical and Computer Engineering, University of Utah, Salt Lake City, UT (United States); Blackrock Microsystems, Salt Lake City, UT (United States)


    Graphical abstract: Surface engineering of high aspect ratio silicon structures. - Highlights: • Multiple roughening techniques for high aspect ratio devices were investigated. • Modification of surface morphology of high aspect ratio silicon devices (1:15). • Decrease of 76% in impedance proves significant increase in surface area. - Abstract: In various applications such as neural prostheses or solar cells, there is a need to alter the surface morphology of high aspect ratio structures so that the real surface area is greater than geometrical area. The change in surface morphology enhances the devices functionality. One of the applications of altering the surface morphology is of neural implants such as the Utah electrode array (UEA) that communicate with single neurons by charge injection induced stimulation or by recording electrical neural signals. For high selectivity between single cells of the nervous system, the electrode surface area is required to be as small as possible, while the impedance is required to be as low as possible for good signal to noise ratios (SNR) during neural recording. For stimulation, high charge injection and charge transfer capacities of the electrodes are required, which increase with the electrode surface. Traditionally, researchers have worked with either increasing the roughness of the existing metallization (platinum grey, black) or other materials such as Iridium Oxide and PEDOT. All of these previously investigated methods lead to more complicated metal deposition processes that are difficult to control and often have a critical impact on the mechanical properties of the metal films. Therefore, a modification of the surface underneath the electrode's coating will increase its surface area while maintaining the standard and well controlled metal deposition process. In this work, the surfaces of the silicon micro-needles were engineered by creating a defined microstructure on the electrodes surface using several

  2. Improving surface acousto-optical interaction by high aspect ratio electrodes

    DEFF Research Database (Denmark)

    Dühring, Maria Bayard; Laude, Vincent; Khelif, Abdelkrim


    The acousto-optical interaction of an optical wave confined inside a waveguide and a surface acoustic wave launched by an interdigital transducer (IDT) at the surface of a piezoelectric material is considered. The IDT with high aspect ratio electrodes supports several acoustic modes...

  3. Dispersion and Polarization of Surface Waves Trapped in High Aspect Ratio Electrode Arrays

    DEFF Research Database (Denmark)

    Laude, Vincent; Dühring, Maria Bayard; Moubchir, Hanane


    .Phys., 90(5):2492, 2001; Appl. Phys. Lett., 89:083515, 2006.) an experimental and theoretical analysis of the transduction of SAW under a metallic array of electrodes with a large aspect ratio on a piezoelectric substrate, whereby allowing the electrode height to become larger than one wavelength...... additional results on the polarization and the dispersion of the surface waves trapped by high aspect ratio electrode arrays. A finite element model, including periodic boundary conditions along the propagation direction and a perfectly matched layer (PML) to absorb waves away from the surface...... wave vector values....

  4. Finite element analysis of surface acoustic waves in high aspect ratio electrodes

    DEFF Research Database (Denmark)

    Dühring, Maria Bayard; Laude, Vincent; Khelif, Abdelkrim


    This paper elaborates on how the finite element method is employed to model surface acoustic waves generated by high aspect ratio electrodes and their interaction with optical waves in a waveguide. With a periodic model it is shown that these electrodes act as a mechanical resonator which slows d...

  5. Jet-Surface Interaction - High Aspect Ratio Nozzle Test: Test Summary (United States)

    Brown, Clifford A.


    The Jet-Surface Interaction High Aspect Ratio Nozzle Test was conducted in the Aero-Acoustic Propulsion Laboratory at the NASA Glenn Research Center in the fall of 2015. There were four primary goals specified for this test: (1) extend the current noise database for rectangular nozzles to higher aspect ratios, (2) verify data previously acquired at small-scale with data from a larger model, (3) acquired jet-surface interaction noise data suitable for creating verifying empirical noise models and (4) investigate the effect of nozzle septa on the jet-mixing and jet-surface interaction noise. These slides give a summary of the test with representative results for each goal.

  6. Jet-Surface Interaction: High Aspect Ratio Nozzle Test, Nozzle Design and Preliminary Data (United States)

    Brown, Clifford; Dippold, Vance


    The Jet-Surface Interaction High Aspect Ratio (JSI-HAR) nozzle test is part of an ongoing effort to measure and predict the noise created when an aircraft engine exhausts close to an airframe surface. The JSI-HAR test is focused on parameters derived from the Turbo-electric Distributed Propulsion (TeDP) concept aircraft which include a high-aspect ratio mailslot exhaust nozzle, internal septa, and an aft deck. The size and mass flow rate limits of the test rig also limited the test nozzle to a 16:1 aspect ratio, half the approximately 32:1 on the TeDP concept. Also, unlike the aircraft, the test nozzle must transition from a single round duct on the High Flow Jet Exit Rig, located in the AeroAcoustic Propulsion Laboratory at the NASA Glenn Research Center, to the rectangular shape at the nozzle exit. A parametric nozzle design method was developed to design three low noise round-to-rectangular transitions, with 8:1, 12:1, and 16: aspect ratios, that minimizes flow separations and shocks while providing a flat flow profile at the nozzle exit. These designs validated using the WIND-US CFD code. A preliminary analysis of the test data shows that the actual flow profile is close to that predicted and that the noise results appear consistent with data from previous, smaller scale, tests. The JSI-HAR test is ongoing through October 2015. The results shown in the presentation are intended to provide an overview of the test and a first look at the preliminary results.

  7. Bio-nanotextured high aspect ratio micropillar arrays for high surface area energy storage devices (United States)

    Chu, S.; Gerasopoulos, K.; Ghodssi, R.


    This paper presents fabrication and characterization of bio-nanotextured hierarchical nickel oxide (NiO) supercapacitor electrodes. The hierarchical electrode structure is created through self-assembly of Tobacco mosaic viruses (TMVs) on high aspect-ratio micropillar arrays. Enhanced assembly of the bio-nanoparticles was achieved by increasing TMV solution accessibility into the deep microcavities of the pillar arrays. Electrochemical characterization of the hierarchical NiO supercapacitor electrodes revealed a 25-fold increase in charge capacity compared to a planar NiO, and demonstrated excellent cycle stability over 1500 charge/discharge cycles at 2 mA/cm2. This study leverages the unique bio-nanoscaffolds for small scale energy storage devices through further optimization of the hierarchical structures and wetting techniques for significant improvements in micro/nano scale energy storage devices.

  8. Surface tension-induced high aspect-ratio PDMS micropillars with concave and convex lens tips

    KAUST Repository

    Li, Huawei


    This paper reports a novel method for the fabrication of 3-dimensional (3D) Polydimethylsiloxane (PDMS) micropillars with concave and convex lens tips in a one-step molding process, using a CO2 laser-machined Poly(methyl methacrylate) (PMMA) mold with through holes. The PDMS micropillars are 4 mm high and have an aspect ratio of 251. The micropillars are formed by capillary force drawing up PDMS into the through hole mold. The concave and convex lens tips of the PDMS cylindrical micropillars are induced by surface tension and are controllable by changing the surface wetting properties of the through holes in the PMMA mold. This technique eliminates the requirements of expensive and complicated facilities to prepare a 3D mold, and it provides a simple and rapid method to fabricate 3D PDMS micropillars with controllable dimensions and tip shapes. © 2013 IEEE.

  9. Fabrication of high aspect ratio nanopillars and micro/nano combined structures with hydrophobic surface characteristics by injection molding (United States)

    Zhou, Mingyong; Xiong, Xiang; Jiang, Bingyan; Weng, Can


    Polymer products with micro/nano-structures have excellent mechanical and optical properties, chemical resistance, and other advantages. Injection molding is one of the most potential techniques to fabricate polymer products with micro/nano-structures artificially in large numbers. In this study, a surface approach to fabricate high aspect ratio nanopillars and micro/nano combined structures was presented. Mold insert with micropillar arrays and nanopillars on its surface was prepared by combing anodic aluminum oxide (AAO) template and etched plate. Anti-sticking modification was done on the template to realize a better demolding quality. The influences of mold temperature and polymer material on the final replication quality were investigated. The results showed that the final replication quality of high aspect ratio nanopillars was greatly improved as compared with the unprocessed template. Polymer with low elongation at break was not suitable to fabricate structures with high aspect ratio via injection molding. For polypropylene surface, the experimental results of static contact angles were almost consistent with Cassie-Baxter equation. When the mold temperature reached 178 °C, hair-like polycarbonate nanopillars were observed, resulting in an excellent hydrophobic characteristic.

  10. Biomechanical aspects of playing surfaces. (United States)

    Nigg, B M; Yeadon, M R


    The purpose of this paper is to discuss some biomechanical aspects of playing surfaces with special focus on (a) surface induced injuries, (b) methodologies used to assess surfaces and (c) findings from various sports. The paper concentrates primarily on questions related to load on the athlete's body. Data from epidemiological studies suggest strongly that the surface is an important factor in the aetiology of injuries. Injury frequencies are reported to be significantly different for different surfaces in several sports. The methodologies used to assess surfaces with respect to load or performance include material tests and tests using experimental subjects. There is only little correlation between the results of these two approaches. Material tests used in many standardized test procedures are not validated which suggests that one should exercise restraint in the interpretation of these results. Point elastic surfaces are widely studied while area elastic surfaces have received little attention to date. Questions of energy losses on sport surfaces have rarely been studied scientifically.

  11. Aspects on interactions between mid- to high latitude atmospheric circulation and some surface processes

    International Nuclear Information System (INIS)

    Byrkjedal, Oeyvind


    The Arctic is a hot topic in Climate Research. A large number of signs of a warming Arctic Climate have been identified the latest years. This is of major concern in light of the increasing atmospheric content of greenhouse gases. The climate research community projects future warming of the climate in the high latitudes as a response to increased amounts of anthropogenic release of greenhouse gases since the pre-industrial era. The overall objectives of this work has been to study the mid- and high latitude climate and climate variability, and to evaluate how well some climate processes that contribute to determine the Arctic climate and variability are represented and simulated in climate models. A new data set of storm tracks trajectories and statistics over the Northern Hemisphere for the period 1948-2002 has been developed. The variability of the cyclones extending to the Nordic Seas is studied in particular, and it is found that both the number of storms and their intensity exhibits a strong decadal and interannual variability. The ocean volume transports into and out of the Nordic Seas shows a relatively close relation to the wintertime cyclone intensity and cyclone count. To have confidence in future projections of climate, it is necessary to evaluate how the model behaves in a climate regime different from modern day. To do this two model simulations of the last glacial maximum (LGM) was performed. The reconstructions of sea surface temperatures in the Nordic Seas in LGM differ from perennial sea ice cover to having open ocean during the summer. The large scale atmospheric circulation patterns of the two different climate reconstructions are studied. It is found that the perennial sea ice cover produces a circulation pattern which may be too zonal to support the existence of the large north Eurasian ice sheets. In the case with seasonally open ocean the air masses carries larger amounts of heat and moisture towards the ice sheets and represents a larger

  12. Solid surfaces : some theoretical aspects

    International Nuclear Information System (INIS)

    Das, M.P.


    An appraisal of the current situation concerning some of the theoretical aspects of solid surfaces is presented. First of all the characterization of the surfaces that involves the surface geometry and atomic composition for both the clean and adsorbed surfaces is discussed. Under this, the methods for determining the surface structure (such as low energy electron diffraction, field electron and field ion microscopy, photo emission spectroscopy and atomic scattering) and methods for determining the surface composition by the Auger electron spectroscopy are outlined. In the second part, emphasis is on the electronic structure of the clean and adsorbed surfaces. The measurements of ultra-violet and X-ray photo electron spectra are shown to yield the information about the surface electronic structure. In this context the many body effects such as, shake-up and relaxation energy etc. are discussed. Finally the status of the theory in relation to the experiments on angular resolved and polarization dependent photo emission are presented. (auth.)

  13. Solution Process Synthesis of High Aspect Ratio ZnO Nanorods on Electrode Surface for Sensitive Electrochemical Detection of Uric Acid (United States)

    Ahmad, Rafiq; Tripathy, Nirmalya; Ahn, Min-Sang; Hahn, Yoon-Bong


    This study demonstrates a highly stable, selective and sensitive uric acid (UA) biosensor based on high aspect ratio zinc oxide nanorods (ZNRs) vertical grown on electrode surface via a simple one-step low temperature solution route. Uricase enzyme was immobilized on the ZNRs followed by Nafion covering to fabricate UA sensing electrodes (Nafion/Uricase-ZNRs/Ag). The fabricated electrodes showed enhanced performance with attractive analytical response, such as a high sensitivity of 239.67 μA cm-2 mM-1 in wide-linear range (0.01-4.56 mM), rapid response time (~3 s), low detection limit (5 nM), and low value of apparent Michaelis-Menten constant (Kmapp, 0.025 mM). In addition, selectivity, reproducibility and long-term storage stability of biosensor was also demonstrated. These results can be attributed to the high aspect ratio of vertically grown ZNRs which provides high surface area leading to enhanced enzyme immobilization, high electrocatalytic activity, and direct electron transfer during electrochemical detection of UA. We expect that this biosensor platform will be advantageous to fabricate ultrasensitive, robust, low-cost sensing device for numerous analyte detection.

  14. Aspects of high temperature superconductivity

    International Nuclear Information System (INIS)

    Deutscher, G.


    We present some remarks on special features that distinguish the phenomenology of the new high T c oxides from that of the conventional superconductors. They include a measurable width of the critical region and a high sensitivity to crystallographic defects. A consistent Landau Ginsburg interpretation is possible, with a short coherence length <15 A and a penetration depth <900 A. The latter is somewhat smaller than the currently accepted value, and implies a broad band scheme

  15. Mathematical aspects of surface water waves

    International Nuclear Information System (INIS)

    Craig, Walter; Wayne, Clarence E


    The theory of the motion of a free surface over a body of water is a fascinating subject, with a long history in both applied and pure mathematical research, and with a continuing relevance to the enterprises of mankind having to do with the sea. Despite the recent advances in the field (some of which we will hear about during this Workshop on Mathematical Hydrodynamics at the Steklov Institute), and the current focus of the mathematical community on the topic, many fundamental mathematical questions remain. These have to do with the evolution of surface water waves, their approximation by model equations and by computer simulations, the detailed dynamics of wave interactions, such as would produce rogue waves in an open ocean, and the theory (partially probabilistic) of approximating wave fields over large regions by averaged 'macroscopic' quantities which satisfy essentially kinetic equations of motion. In this note we would like to point out open problems and some of the directions of current research in the field. We believe that the introduction of new analytical techniques and novel points of view will play an important role in the future development of the area.

  16. New aspects of high energy density plasma

    International Nuclear Information System (INIS)

    Hotta, Eiki


    The papers presented at the symposium on 'New aspects of high energy density plasma' held at National Institute for Fusion Science are collected in this proceedings. The papers reflect the present status and recent progress in the experiments and theoretical works on high energy density plasma produced by pulsed power technology. The 13 of the presented papers are indexed individually. (J.P.N.)

  17. Moduli of Riemann surfaces, transcendental aspects

    International Nuclear Information System (INIS)

    Hain, R.


    These notes are an informal introduction to moduli spaces of compact Riemann surfaces via complex analysis, topology and Hodge Theory. The prerequisites for the first lecture are just basic complex variables, basic Riemann surface theory up to at least the Riemann-Roch formula, and some algebraic topology, especially covering space theory. The first lecture covers moduli in genus 0 and genus 1 as these can be understood using relatively elementary methods, but illustrate many of the points which arise in higher genus. The notes cover more material than was covered in the lectures, and sometimes the order of topics in the notes differs from that in the lectures. We have seen in genus 1 case that M 1 is the quotient Γ 1 /X 1 of a contractible complex manifold X 1 = H by a discrete group Γ 1 = SL 2 (Z). The action of Γ 1 on X 1 is said to be virtually free - that is, Γ 1 has a finite index subgroup which acts (fixed point) freely on X 1 . In this section we will generalize this to all g >= 1 - we will sketch a proof that there is a contractible complex manifold Xg, called Teichmueller space, and a group Γ g , called the mapping class group, which acts virtually freely on X g . The moduli space of genus g compact Riemann surfaces is the quotient: M g = Γ g /X g . This will imply that M g has the structure of a complex analytic variety with finite quotient singularities. Teichmueller theory is a difficult and technical subject. Because of this, it is only possible to give an overview. In this lecture, we compute the orbifold Picard group of M g for all g >= 1. Recall that an orbifold line bundle over M g is a holomorphic line bundle L over Teichmueller space X g together with an action of the mapping class group Γ g on it such that the projection L → X g is Γ g -equivariant. An orbifold section of this line bundle is a holomorphic Γ g -equivariant section X g → L of L. This is easily seen to be equivalent to fixing a level l>= 3 and considering holomorphic

  18. Technical aspects of high converter reactors

    International Nuclear Information System (INIS)


    The meeting provided an opportunity to review and discuss national R and D programs, various technical aspects of and worldwide progress in the implementation of high conversion reactors. The meeting was attended by 66 participants from 18 countries and 2 international organizations. 33 papers were presented. A separate abstract was prepared for each of these papers. Refs, figs, tabs, slides and diagram

  19. Developments in surface contamination and cleaning fundamentals and applied aspects

    CERN Document Server

    Kohli, Rajiv


    Developments in Surface Contamination and Cleaning, Vol. 1: Fundamentals and Applied Aspects, Second Edition, provides an excellent source of information on alternative cleaning techniques and methods for characterization of surface contamination and validation. Each volume in this series contains a particular topical focus, covering the key techniques and recent developments in the area. This volume forms the heart of the series, covering the fundamentals and application aspects, characterization of surface contaminants, and methods for removal of surface contamination. In addition, new cleaning techniques effective at smaller scales are considered and employed for removal where conventional cleaning techniques fail, along with new cleaning techniques for molecular contaminants. The Volume is edited by the leading experts in small particle surface contamination and cleaning, providing an invaluable reference for researchers and engineers in R&D, manufacturing, quality control, and procurement specific...

  20. Noise of Embedded High Aspect Ratio Nozzles (United States)

    Bridges, James E.


    A family of high aspect ratio nozzles were designed to provide a parametric database of canonical embedded propulsion concepts. Nozzle throat geometries with aspect ratios of 2:1, 4:1, and 8:1 were chosen, all with convergent nozzle areas. The transition from the typical round duct to the rectangular nozzle was designed very carefully to produce a flow at the nozzle exit that was uniform and free from swirl. Once the basic rectangular nozzles were designed, external features common to embedded propulsion systems were added: extended lower lip (a.k.a. bevel, aft deck), differing sidewalls, and chevrons. For the latter detailed Reynolds-averaged Navier-Stokes (RANS) computational fluid dynamics (CFD) simulations were made to predict the thrust performance and to optimize parameters such as bevel length, and chevron penetration and azimuthal curvature. Seventeen of these nozzles were fabricated at a scale providing a 2.13 inch diameter equivalent area throat." ! The seventeen nozzles were tested for far-field noise and a few data were presented here on the effect of aspect ratio, bevel length, and chevron count and penetration. The sound field of the 2:1 aspect ratio rectangular jet was very nearly axisymmetric, but the 4:1 and 8:1 were not, the noise on their minor axes being louder than the major axes. Adding bevel length increased the noise of these nozzles, especially on their minor axes, both toward the long and short sides of the beveled nozzle. Chevrons were only added to the 2:1 rectangular jet. Adding 4 chevrons per wide side produced some decrease at aft angles, but increased the high frequency noise at right angles to the jet flow. This trend increased with increasing chevron penetration. Doubling the number of chevrons while maintaining their penetration decreased these effects. Empirical models of the parametric effect of these nozzles were constructed and quantify the trends stated above." Because it is the objective of the Supersonics Project that

  1. High Aspect Ratio Plasmonic Nanotrench Structures with Large Active Surface Area for Label-Free Mid-Infrared Molecular Absorption Sensing

    DEFF Research Database (Denmark)

    Shkondin, Evgeniy; Repän, Taavi; Panah, Mohammad Esmail Aryaee


    Mid-infrared spectroscopy offers unique sensing schemes to detect target molecules thanks to the absorption of infrared light at specific wavelengths unique to chemical compositions. Due to the mismatch of the mid-infrared light wavelength on the order of micron and nanometer size molecules, the ...... may serve as a highly sensitive bio- and chemo-sensing platform for mid-infrared absorption spectroscopy....

  2. High surface area calcite (United States)

    Schultz, L. N.; Andersson, M. P.; Dalby, K. N.; Müter, D.; Okhrimenko, D. V.; Fordsmand, H.; Stipp, S. L. S.


    Calcite (CaCO3) is important in many fields—in nature, because it is a component of aquifers, oil reservoirs and prospective CO2 storage sites, and in industry, where it is used in products as diverse as paper, toothpaste, paint, plastic and aspirin. It is difficult to obtain high purity calcite with a high surface area but such material is necessary for industrial applications and for fundamental calcite research. Commercial powder is nearly always contaminated with growth inhibitors such as sugars, citrate or pectin and most laboratory synthesis methods deliver large precipitates, often containing vaterite or aragonite. To address this problem, we (i) adapted the method of carbonating a Ca(OH)2 slurry with CO2 gas to develop the first simple, cheap, safe and reproducible procedure using common laboratory equipment, to obtain calcite that reproducibly had a surface area of 14-17 m2/g and (ii) conducted a thorough characterization of the product. Scanning electron microscopy (SEM) revealed nanometer scale, rhombohedral crystals. X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and infrared spectroscopy (IR) confirmed highly crystalline, pure calcite that more closely resembles the dimensions of the biogenic calcite produced by algae in coccoliths than other methods for synthesizing calcite. We suggest that this calcite is useful when purity and high surface area are important.

  3. Injection molding of high aspect ratio sub-100 nm nanostructures

    DEFF Research Database (Denmark)

    Matschuk, Maria; Larsen, Niels B


    as described by height, width and uniformity of the nanoscopic features. Use of a mold temperature transiently above the polymer glass transition temperature (Tg) was the most important factor in increasing the replication fidelity. Surface coating of the nickel molds with a fluorocarbon-containing thin film...... with FDTS. Reduced adhesion forces are consistent with lowered friction that reduces the risk of fracturing the nanoscopic pillars during demolding. Optimized mold surface chemistry and associated injection molding conditions permitted the fabrication of square arrays of 40 nm wide and 107 nm high (aspect...

  4. Practical aspects of tritium measurement in ground and surface waters

    Energy Technology Data Exchange (ETDEWEB)

    Nitzsche, O. [Technische Univ. Bergakademie Freiberg (Germany). Inst. fuer Angewandte Physik; Hebert, D. [Technische Univ. Bergakademie Freiberg (Germany). Inst. fuer Angewandte Physik


    Tritium measurements are a powerful tool in hydrological and hydrogeological investigations for detecting mean residence times of several water reservoirs. Due to the low tritium activities in precipitation, ground and surface waters a low level measurement is necessary. Therefore often the liquid scintillation counting after an electrolytic enrichment of water is used. In this paper some practical aspects and problems of measurement are discussed and the problem of contamination in low level laboratories is shown. (orig.)

  5. Clinical Aspects of Combination of Ceramic and Acrylic Occlusal Surfaces

    Directory of Open Access Journals (Sweden)

    Z. Ozhohan


    Full Text Available The objective of the research was to develop and substantiate the methods of constructing the occlusal surfaces when manufacturing aesthetic fixed restorations through the combination of different materials. Materials and methods. The study included 65 patients with ceramic and acrylic occlusal surfaces of aesthetic fixed dental prostheses. Group I included 21 patients with a combination of ceramic and acrylic occlusal surfaces. Group II included 22 patients with a combination of ceramic occlusal surfaces. Group III included 22 patients with a combination of acrylic occlusal surfaces. The patients were observed 3, 6 and 12 months after prosthetic repair. Results. The greatest increase in the occlusal contact surface area of fixed restorations was observed in Group I, that is, when combining dental prostheses with ceramic and acrylic occlusal surfaces. Considering uneven abrasion of the occlusal surfaces, we do not recommend to combine different materials when veneering the occlusal surface of the antagonistic teeth. Conclusions. This study demonstrated the important role of the correct combination of materials when veneering the occlusal surfaces. Physical and chemical properties of materials, namely the abrasion resistance play a significant role in the long-term denture functioning. The smallest increase in the occlusal contact surface area was observed in Group II when combining ceramic occlusal surfaces. It was due to a good abrasion resistance of ceramics as compared to acrylic resin as well as the presence of the glazed layer which prevents the premature abrasion of the occlusal surfaces of the antagonistic teeth due to lower surface roughness. The combination of acrylic resin and ceramics when constructing the occlusal surfaces of fixed restorations in Group I demonstrated the highest rate of the increase in the occlusal contact surface area – 9.93%. It was due to a low hardness of acrylic resin and its high surface roughness. In


    Directory of Open Access Journals (Sweden)



    Full Text Available Surface electromyography (SEMG is a technique for detecting and recording the electrical activity of the muscles using surface electrodes. The EMG signal is used in biomechanics mainly as an indicator of the initiation of muscle activation, as an indicator of the force produced by a contracting muscle, and as an index ofthe fatigue occurring within a muscle. EMG, used as a method of investigation, can tell us if the muscle is active or not, if the muscle is more or less active, when it is on or off, how much active is it, and finally, if it fatigues.The purpose of this article is to discuss some specific EMG signal analysis aspects with emphasis on comparison type analysis and frequency fatigue analysis.

  7. High aspect ratio channels in glass and porous silicon

    International Nuclear Information System (INIS)

    Liang, H.D.; Dang, Z.Y.; Wu, J.F.; Kan, J.A. van; Qureshi, S.; Ynsa, M.D.; Torres-Costa, V.; Maira, A.; Venkatesan, T.V.; Breese, M.B.H.


    We have developed a micromachining process to produce high-aspect-ratio channels and holes in glass and porous silicon. Our process utilizes MeV proton beam irradiation of silicon using direct writing with a focused beam, followed by electrochemical etching. To increase throughput we have also developed another process for large area ion irradiation based on a radiation-resistant gold surface mask, allowing many square inches to be patterned. We present a study of the achievable channel width, depth and period and sidewall verticality for a range of channels which can be over 100 μm deep or 100 nm wide with aspect ratios up to 80. This process overcomes the difficulty of machining glass on a micro- and nanometer scale which has limited many areas of applications in different fields such as microelectronics and microfluidics.

  8. High aspect ratio channels in glass and porous silicon

    Energy Technology Data Exchange (ETDEWEB)

    Liang, H.D. [Centre for Ion Beam Applications (CIBA), Department of Physics, National University of Singapore, Singapore 117542 (Singapore); Nanoscience and Nanotechnology Initiative (NNI), National University of Singapore, Singapore 117411 (Singapore); Dang, Z.Y. [Centre for Ion Beam Applications (CIBA), Department of Physics, National University of Singapore, Singapore 117542 (Singapore); Wu, J.F. [Centre for Ion Beam Applications (CIBA), Department of Physics, National University of Singapore, Singapore 117542 (Singapore); Department of Electrical and Computer Engineering, National University of Singapore, Singapore 117583 (Singapore); Kan, J.A. van; Qureshi, S. [Centre for Ion Beam Applications (CIBA), Department of Physics, National University of Singapore, Singapore 117542 (Singapore); Ynsa, M.D.; Torres-Costa, V. [Department of Applied Physics, Universidad Autónoma de Madrid, Madrid, Campus de Cantoblanco, 28049 Madrid (Spain); Centro de Micro-Análisis de Materiales (CMAM), Universidad Autónoma de Madrid, Campus de Cantoblanco Edif. 22, Faraday 3, E-28049 Madrid (Spain); Maira, A. [Department of Applied Physics, Universidad Autónoma de Madrid, Madrid, Campus de Cantoblanco, 28049 Madrid (Spain); Venkatesan, T.V. [Nanoscience and Nanotechnology Initiative (NNI), National University of Singapore, Singapore 117411 (Singapore); Breese, M.B.H., E-mail: [Centre for Ion Beam Applications (CIBA), Department of Physics, National University of Singapore, Singapore 117542 (Singapore)


    We have developed a micromachining process to produce high-aspect-ratio channels and holes in glass and porous silicon. Our process utilizes MeV proton beam irradiation of silicon using direct writing with a focused beam, followed by electrochemical etching. To increase throughput we have also developed another process for large area ion irradiation based on a radiation-resistant gold surface mask, allowing many square inches to be patterned. We present a study of the achievable channel width, depth and period and sidewall verticality for a range of channels which can be over 100 μm deep or 100 nm wide with aspect ratios up to 80. This process overcomes the difficulty of machining glass on a micro- and nanometer scale which has limited many areas of applications in different fields such as microelectronics and microfluidics.

  9. Shape matters: synthesis and biomedical applications of high aspect ratio magnetic nanomaterials


    Fratila, Raluca M.; Rivera-Fernández, Sara; Fuente, Jesús M. de la


    High aspect ratio magnetic nanomaterials possess anisotropic properties that make them attractive for biological applications. Their elongated shape enables multivalent interactions with receptors through the introduction of multiple targeting units on their surface, thus enhancing cell internalization. Moreover, due to their magnetic anisotropy, high aspect ratio nanomaterials can outperform their spherical analogues as contrast agents for magnetic resonance imaging (MRI) applications. In th...

  10. Reusable High Aspect Ratio 3-D Nickel Shadow Mask (United States)

    Shandhi, M.M.H.; Leber, M.; Hogan, A.; Warren, D.J.; Bhandari, R.; Negi, S.


    Shadow Mask technology has been used over the years for resistless patterning and to pattern on unconventional surfaces, fragile substrate and biomaterial. In this work, we are presenting a novel method to fabricate high aspect ratio (15:1) three-dimensional (3D) Nickel (Ni) shadow mask with vertical pattern length and width of 1.2 mm and 40 μm respectively. The Ni shadow mask is 1.5 mm tall and 100 μm wide at the base. The aspect ratio of the shadow mask is 15. Ni shadow mask is mechanically robust and hence easy to handle. It is also reusable and used to pattern the sidewalls of unconventional and complex 3D geometries such as microneedles or neural electrodes (such as the Utah array). The standard Utah array has 100 active sites at the tip of the shaft. Using the proposed high aspect ratio Ni shadow mask, the Utah array can accommodate 300 active sites, 200 of which will be along and around the shaft. The robust Ni shadow mask is fabricated using laser patterning and electroplating techniques. The use of Ni 3D shadow mask will lower the fabrication cost, complexity and time for patterning out-of-plane structures. PMID:29056835

  11. High aspect ratio catalytic reactor and catalyst inserts therefor (United States)

    Lin, Jiefeng; Kelly, Sean M.


    The present invention relates to high efficient tubular catalytic steam reforming reactor configured from about 0.2 inch to about 2 inch inside diameter high temperature metal alloy tube or pipe and loaded with a plurality of rolled catalyst inserts comprising metallic monoliths. The catalyst insert substrate is formed from a single metal foil without a central supporting structure in the form of a spiral monolith. The single metal foil is treated to have 3-dimensional surface features that provide mechanical support and establish open gas channels between each of the rolled layers. This unique geometry accelerates gas mixing and heat transfer and provides a high catalytic active surface area. The small diameter, high aspect ratio tubular catalytic steam reforming reactors loaded with rolled catalyst inserts can be arranged in a multi-pass non-vertical parallel configuration thermally coupled with a heat source to carry out steam reforming of hydrocarbon-containing feeds. The rolled catalyst inserts are self-supported on the reactor wall and enable efficient heat transfer from the reactor wall to the reactor interior, and lower pressure drop than known particulate catalysts. The heat source can be oxygen transport membrane reactors.

  12. Optodynamics: dynamic aspects of laser beam-surface interaction

    International Nuclear Information System (INIS)

    Možina, J; Diaci, J


    This paper presents a synthesis of the results of our original research in the area of laser-material interaction and pulsed laser material processing with a special emphasis on the dynamic aspects of laser beam-surface interaction, which include the links between the laser material removal and the resulting material motion. In view of laser material processing, a laser beam is not only considered as a tool but also as a generator of information about the material transformation. The information is retained and conveyed by different kinds of optically induced mechanical waves. Several generation/detection schemes have been developed to extract this information, especially in the field of non-destructive material evaluation. Blast and acoustic waves, which propagate in the air surrounding the work-piece, have been studied using microphone detection as well as various setups of the laser beam deflection probe. Stress waves propagating through the work-piece have been studied using piezoelectric transducers and laser interferometers.

  13. Socioecological Aspects of High-rise Construction (United States)

    Eichner, Michael; Ivanova, Zinaida


    In this article, the authors consider the socioecological problems that arise in the construction and operation of high-rise buildings. They study different points of view on high-rise construction and note that the approaches to this problem are very different. They also analyse projects of modern architects and which attempts are made to overcome negative impacts on nature and mankind. The article contains materials of sociological research, confirming the ambivalent attitude of urban population to high-rise buildings. In addition, one of the author's sociological survey reveals the level of environmental preparedness of the university students, studying in the field of "Construction of unique buildings and structures", raising the question of how future specialists are ready to take into account socioecological problems. Conclusion of the authors: the construction of high-rise buildings is associated with huge social and environmental risks, negative impact on the biosphere and human health. This requires deepened skills about sustainable design methods and environmental friendly construction technologies of future specialists. Professor M. Eichner presents in the article his case study project results on implementation of holistic eco-sustainable construction principles for mixed-use high-rise building in the metropolis of Cairo.

  14. Injection Molding of High Aspect Ratio Nanostructures

    DEFF Research Database (Denmark)

    Matschuk, Maria; Larsen, Niels Bent

    We present a process for injection molding of 40 nm wide and >100 nm high pillars (pitch: 200 nm). We explored the effects of mold coatings and injection molding conditions on the replication quality of nanostructures in cyclic olefin copolymer. We found that optimization of molding parameters...

  15. Highly valuable microalgae: biochemical and topological aspects. (United States)

    Pignolet, Olivier; Jubeau, Sébastien; Vaca-Garcia, Carlos; Michaud, Philippe


    The past decade has seen a surge in the interest in microalgae culture for biodiesel production and other applications as renewable biofuels as an alternative to petroleum transport fuels. The development of new technologies for the culture of these photosynthetic microorganisms and improved knowledge of their biochemical composition has spurred innovation in the field of high-value biomolecules. These developments are only economically viable if all the microalgae fractions are valorized in a biorefinery strategy. Achieving this objective requires an understanding of microalgae content and the cellular localization of the main biomolecular families in order to develop efficient harvest and sequential recovery technologies. This review summarizes the state of the art in microalgae compositions and topologies using some examples of the main industrially farmed microalgae.

  16. Wakes behind surface-mounted obstacles: Impact of aspect ratio, incident angle, and surface roughness (United States)

    Tobin, Nicolas; Chamorro, Leonardo P.


    The so-called wake-moment coefficient C˜h and lateral wake deflection of three-dimensional windbreaks are explored in the near and far wake. Wind-tunnel experiments were performed to study the functional dependence of C˜h with windbreak aspect ratio, incidence angle, and the ratio of the windbreak height and surface roughness (h /z0 ). Supported with the data, we also propose basic models for the wake deflection of the windbreak in the near and far fields. The near-wake model is based on momentum conservation considering the drag on the windbreak, whereas the far-wake counterpart is based on existing models for wakes behind surface-mounted obstacles. Results show that C˜h does not change with windbreak aspect ratios of 10 or greater; however, it may be lower for an aspect ratio of 5. C˜h is found to change roughly with the cosine of the incidence angle, and to depend strongly on h /z0 . The data broadly support the proposed wake-deflection models, though better predictions could be made with improved knowledge of the windbreak drag coefficient.

  17. Optically Designed Anodised Aluminium Surfaces: Microstructural and Electrochemical Aspects

    DEFF Research Database (Denmark)

    Gudla, Visweswara Chakravarthy

    was studied in-situ in a transmission electron microscope and also ex-situ using grazing incidence X-ray diffraction. The Al-Metal oxide surface composites based on TiO2, Y2O3, and CeO2 prepared by friction stir processing were employed to generate light scattering anodised surfaces by embedding oxide...... industry. Conventional colouring techniques applied to anodised aluminium surfaces cannot generate glossy white appearing surfaces due to the fundamental differences in the interaction with visible light that is required. Surfaces appearing as perfect white are due to the scattering of visible light......This thesis presents the research work aimed at generating anodised aluminium surfaces with bright, white, and glossy decorative appearance. The aluminium surface finishing industry has been on the lookout for such surfaces due to their potential applications in aerospace, architecture, and design...

  18. Surface analysis of transition metal oxalates: Damage aspects

    Energy Technology Data Exchange (ETDEWEB)

    Chenakin, S.P., E-mail: [Université Libre de Bruxelles (ULB), Chimie-Physique des Matériaux, B-1050 Bruxelles (Belgium); Institute of Metal Physics, Nat. Acad. Sci. of Ukraine, Akad. Vernadsky Blvd. 36, 03680 Kiev (Ukraine); Szukiewicz, R. [Université Libre de Bruxelles (ULB), Chimie-Physique des Matériaux, B-1050 Bruxelles (Belgium); Barbosa, R.; Kruse, N. [Université Libre de Bruxelles (ULB), Chimie-Physique des Matériaux, B-1050 Bruxelles (Belgium); Voiland School of Chemical Engineering and Bioengineering, Washington State University, 155 Wegner Hall, Pullman, WA 99164-6515 (United States)


    Highlights: • Gas evolution from the Mn, Co, Ni and Cu oxalate hydrates in vacuum, during exposure to X-rays and after termination of X-ray irradiation is studied. • A comparative study of the damage caused by X-rays in NiC{sub 2}O{sub 4} and CuC{sub 2}O{sub 4} is carried out. • Effect of Ar{sup +} bombardment on the structure and composition of CoC{sub 2}O{sub 4} is studied. - Abstract: The behavior of transition metal oxalates in vacuum, under X-ray irradiation and low-energy Ar{sup +} ion bombardment was studied. A comparative mass-spectrometric analysis was carried out of gas evolution from the surface of Mn, Co, Ni and Cu oxalate hydrates in vacuum, during exposure to X-rays and after termination of X-ray irradiation. The rates of H{sub 2}O and CO{sub 2} liberation from the oxalates were found to be in an inverse correlation with the temperatures of dehydration and decomposition, respectively. X-ray photoelectron spectroscopy (XPS) was employed to study the X-ray induced damage in NiC{sub 2}O{sub 4} and CuC{sub 2}O{sub 4} by measuring the various XP spectral characteristics and surface composition of the oxalates as a function of time of exposure to X-rays. It was shown that Cu oxalate underwent a significantly faster degradation than Ni oxalate and demonstrated a high degree of X-ray induced reduction from the Cu{sup 2+} to the Cu{sup 1+} chemical state. 500 eV Ar{sup +} sputter cleaning of CoC{sub 2}O{sub 4} for 10 min was found to cause a strong transformation of the oxalate structure which manifested itself in an appreciable alteration of the XP core-level and valence band spectra. The analysis of changes in stoichiometry and comparison of XP spectra of bombarded oxalate with respective spectra of a reference carbonate CoCO{sub 3} implied that the bombardment-induced decomposition of CoC{sub 2}O{sub 4} gave rise to the formation of CoO-like and disordered CoCO{sub 3}-like phases.

  19. Towards a Reproducible Synthesis of High Aspect Ratio Gold Nanorods

    Directory of Open Access Journals (Sweden)

    Susanne Koeppl


    Full Text Available The seed-mediated method in presence of high concentrations of CTAB is frequently implemented in the preparation of high aspect ratio gold nanorods (i.e., nanorods with aspect ratios of 5 or more; however, the reproducibility has still been limited. We rendered the synthesis procedure simpler, decreased the susceptibility to impurities, and improved the reproducibility of the product distribution. As a result of the high aspect ratios, longitudinal plasmon absorptions were shifted up to very high absorption maxima of 1955 nm in UV-vis-NIR spectra (since this band is completely covered in aqueous solution by the strong absorption of water, the gold species were embedded in poly(vinyl alcohol films for UV-vis-NIR measurements. Finally, the directed particle growth in (110 direction leads to the conclusion that the adsorption of CTAB molecules at specific crystal faces accounts for nanorod growth and not cylindrical CTAB micelles, in agreement with other observations.

  20. Scattering and extinction from high-aspect-ratio trenches

    DEFF Research Database (Denmark)

    Roberts, Alexander Sylvester; Søndergaard, Thomas; Chirumamilla, Manohar


    We construct a semi-analytical model describing the scattering, extinction and absorption properties of a high aspect-ratio trench in a metallic film. We find that these trenches act as highly efficient scatterers of free waves. In the perfect conductor limit, which for many metals is approached...

  1. Fabrication of high aspect ratio nanocell lattices by ion beam irradiation

    International Nuclear Information System (INIS)

    Ishikawa, Osamu; Nitta, Noriko; Taniwaki, Masafumi


    Highlights: • Nanocell lattice with a high aspect ratio on InSb semiconductor surface was fabricated by ion beam irradiation. • The fabrication technique consisting of top-down and bottom-up processes was performed in FIB. • High aspect ratio of 2 was achieved in nanocell lattice with a 100 nm interval. • The intermediate-flux irradiation is favorable for fabrication of nanocell with a high aspect ratio. - Abstract: A high aspect ratio nanocell lattice was fabricated on the InSb semiconductor surface using the migration of point defects induced by ion beam irradiation. The fabrication technique consisting of the top-down (formation of voids and holes) and bottom-up (growth of voids and holes into nanocells) processes was performed using a focused ion beam (FIB) system. A cell aspect ratio of 2 (cell height/cell diameter) was achieved for the nanocell lattice with a 100 nm dot interval The intermediate-flux ion irradiation during the bottom-up process was found to be optimal for the fabrication of a high aspect ratio nanocell.

  2. Fabrication of high aspect ratio nanocell lattices by ion beam irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Ishikawa, Osamu [School of Environmental Science and Technology, Kochi University of Technology, Tosayamada, Kami, Kochi 782-8502 (Japan); Nitta, Noriko, E-mail: [School of Environmental Science and Technology, Kochi University of Technology, Tosayamada, Kami, Kochi 782-8502 (Japan); Center for Nanotechnology, Research Institute, Kochi University of Technology, Tosayamada, Kami, Kochi 782-8502 (Japan); Taniwaki, Masafumi [School of Environmental Science and Technology, Kochi University of Technology, Tosayamada, Kami, Kochi 782-8502 (Japan)


    Highlights: • Nanocell lattice with a high aspect ratio on InSb semiconductor surface was fabricated by ion beam irradiation. • The fabrication technique consisting of top-down and bottom-up processes was performed in FIB. • High aspect ratio of 2 was achieved in nanocell lattice with a 100 nm interval. • The intermediate-flux irradiation is favorable for fabrication of nanocell with a high aspect ratio. - Abstract: A high aspect ratio nanocell lattice was fabricated on the InSb semiconductor surface using the migration of point defects induced by ion beam irradiation. The fabrication technique consisting of the top-down (formation of voids and holes) and bottom-up (growth of voids and holes into nanocells) processes was performed using a focused ion beam (FIB) system. A cell aspect ratio of 2 (cell height/cell diameter) was achieved for the nanocell lattice with a 100 nm dot interval The intermediate-flux ion irradiation during the bottom-up process was found to be optimal for the fabrication of a high aspect ratio nanocell.

  3. Hydrogeological aspects of radioactive waste disposal into surface formations

    International Nuclear Information System (INIS)

    Dlouhy, Z.


    Safe disposal is discussed of radioactive wastes in geological surface formations and basic criteria are shown of the radiological protection of population from possible effects of radioactive materials diffused in the environment. Main principles are listed governing the selection of suitable localities with respect to possible interactions of the locality and the storage site with the environment. (author)

  4. Soliton surfaces associated with sigma models: differential and algebraic aspects

    International Nuclear Information System (INIS)

    Goldstein, P P; Grundland, A M; Post, S


    In this paper, we consider both differential and algebraic properties of surfaces associated with sigma models. It is shown that surfaces defined by the generalized Weierstrass formula for immersion for solutions of the CP N-1 sigma model with finite action, defined in the Riemann sphere, are themselves solutions of the Euler–Lagrange equations for sigma models. On the other hand, we show that the Euler–Lagrange equations for surfaces immersed in the Lie algebra su(N), with conformal coordinates, that are extremals of the area functional, subject to a fixed polynomial identity, are exactly the Euler–Lagrange equations for sigma models. In addition to these differential constraints, the algebraic constraints, in the form of eigenvalues of the immersion functions, are systematically treated. The spectrum of the immersion functions, for different dimensions of the model, as well as its symmetry properties and its transformation under the action of the ladder operators are discussed. Another approach to the dynamics is given, i.e. description in terms of the unitary matrix which diagonalizes both the immersion functions and the projectors constituting the model. (paper)

  5. High aspect ratio titanium nitride trench structures as plasmonic biosensor

    DEFF Research Database (Denmark)

    Shkondin, Evgeniy; Repän, Taavi; Takayama, Osamu


    High aspect ratio titanium nitride (TiN) grating structures are fabricated by the combination of deep reactive ion etching (DRIE) and atomic layer deposition (ALD) techniques. TiN is deposited at 500 ◦C on a silicon trench template. Silicon between vertical TiN layers is selectively etched...

  6. High yield polyol synthesis of round- and sharp-end silver nanowires with high aspect ratio

    Energy Technology Data Exchange (ETDEWEB)

    Nekahi, A.; Marashi, S.P.H., E-mail:; Fatmesari, D. Haghshenas


    Long silver nanowires (average length of 28 μm, average aspect ratio of 130) with uniform diameter along their length were produced by polyol synthesis of AgNO{sub 3} in ethylene glycol in the presence of PVP as preferential growth agent. Nanowires were produced with no addition of chloride salts such as NaCl or CuCl{sub 2} (or other additives such as Na{sub 2}S) which are usually used for lowering reduction rate of Ag ions by additional etchant of O{sub 2}/Cl{sup −}. Lower reduction rate was obtained by increasing the injection time of PVP and AgNO{sub 3} solutions, which was the significant factor in the formation of nanowires. Therefore, there was enough time for reduced Ag atoms to be deposited preferentially in the direction of PVP chains, resulting in high yield (the fraction of nanowires in the products) of nanowires (more than 95%) with high aspect ratio. The produced nanowires had both round- and sharp-ends with pentagonal cross section. Higher energy level of Ag atoms in borders of MTPs, which increases the dissolution rate of precipitated atoms, in addition to partial melting of MTPs at high synthesis temperatures, leads to the curving of the surfaces of exposed (111) crystalline planes in some MTPs and the formation of round-end silver nanowires. - Highlights: • Long silver nanowires with high aspect ratio of 130 were produced. • More than 95% nanowires were produced in products. • The produced nanowires had round- and sharp-ends with pentagonal cross section. • Additives were needed neither for high yield synthesis nor for round-end nanowires. • Melting and etching of MTPs in high energy borders resulted to round-end nanowires.

  7. Role of surface-reaction layer in HBr/fluorocarbon-based plasma with nitrogen addition formed by high-aspect-ratio etching of polycrystalline silicon and SiO2 stacks (United States)

    Iwase, Taku; Matsui, Miyako; Yokogawa, Kenetsu; Arase, Takao; Mori, Masahito


    The etching of polycrystalline silicon (poly-Si)/SiO2 stacks by using VHF plasma was studied for three-dimensional NAND fabrication. One critical goal is achieving both a vertical profile and high throughput for multiple-stack etching. While the conventional process consists of multiple steps for each stacked layer, in this study, HBr/fluorocarbon-based gas chemistry was investigated to achieve a single-step etching process to reduce process time. By analyzing the dependence on wafer temperature, we improved both the etching profile and rate at a low temperature. The etching mechanism is examined considering the composition of the surface reaction layer. X-ray photoelectron spectroscopy (XPS) analysis revealed that the adsorption of N-H and Br was enhanced at a low temperature, resulting in a reduced carbon-based-polymer thickness and enhanced Si etching. Finally, a vertical profile was obtained as a result of the formation of a thin and reactive surface-reaction layer at a low wafer temperature.

  8. Surface aspects of pitting and stress corrosion cracking (United States)

    Truhan, J. S., Jr.; Hehemann, R. F.


    The pitting and stress corrosion cracking of a stable austenitic stainless steel in aqueous chloride environments were investigated using a secondary ion mass spectrometer as the primary experimental technique. The surface concentration of hydrogen, oxygen, the hydroxide, and chloride ion, magnesium or sodium, chromium and nickel were measured as a function of potential in both aqueous sodium chloride and magnesium chloride environments at room temperature and boiling temperatures. It was found that, under anodic conditions, a sharp increase in the chloride concentration was observed to occur for all environmental conditions. The increase may be associated with the formation of an iron chloride complex. Higher localized chloride concentrations at pits and cracks were also detected with an electron microprobe.

  9. Asteroid Spectral Imaging Mission (ASPECT) CubeSat to characterize resources on asteroid surfaces (United States)

    Kohout, T.; Näsilä, A.; Tikka, T.; Granvik, M.; Kestilä, A.; Penttilä, A.; Kuhno, J.; Muinonen, K.; Viherkanto, K.


    ASPECT is a 3U CubeSat with a VIS-NIR spectral imager. It can characterize composition of asteroid surfaces and identify areas and objects with desired properties for sample return or in-space resource utilization.

  10. [Scanning electron microscopy (S.E.M.) aspects of intestinal mucosal surface in childhood coeliac disease]. (United States)

    Patanè, R; Bottaro, G; Ricca, O; Galasso, S


    Intestinal mucosal surface in 5 children suffered with Coeliac Disease was observed at Scanning Electron Microscopy. The comparison between two techniques of dehydration demonstrated that the Alcool-Amile Acetate dehydration reduces the technical errors to the minimum. Therefore, a better visualization allows us to recognize the surface coat, the microvillous and some mucosal functional aspects (scale off), which were previously undistinguished. There are no differences between the mucosal aspects in adult coeliac disease and childhood coelia disease.

  11. Large-Area High Aspect Ratio Plasmonic Interference Lithography Utilizing a Single High-k Mode. (United States)

    Chen, Xi; Yang, Fan; Zhang, Cheng; Zhou, Jing; Guo, L Jay


    Plasmonic lithography, which utilizes subwavelength confinement of surface plasmon polartion (SPP) waves, has the capability of breaking the diffraction limit and delivering high resolution. However, all previously reported results suffer from critical issues, such as shallow pattern depth and pattern nonuniformity even over small exposure areas, which limit the application of the technology. In this work, periodic patterns with high aspect ratios and a half-pitch of about 1/6 of the wavelength were achieved with pattern uniformity in square centimeter areas. This was accomplished by designing a special mask and photoresist (PR) system to select a single high spatial frequency mode and incorporating the PR into a waveguide configuration to ensure uniform light exposure over the entire depth of the photoresist layer. In addition to the experimental progress toward large-scale applications of plasmonic interference lithography, the general criteria of designing such an exposure system is also discussed, which can be used for nanoscale fabrication in this fashion for various applications with different requirements for wavelength, pitch, aspect ratio, and structure.

  12. Metallurgical aspects of fatigue fractured surfaces of al grain refined by some rare earth materials

    International Nuclear Information System (INIS)

    Zaid, A.I.O.


    Aluminum and aluminum alloys are widely used materials in the automobile and air craft industries due to their high strength-to-weight ratio, in addition to some other attractive characteristics e.g. corrosion resistance and high electrical and thermal conductivities. Aluminum and its alloys are normally grain refined by Ti or Ti+B to enhance their surface quality and improve their mechanical strength. Although the effect of addition of these grain refiners on the microstructure mechanical behaviour has been investigated and reported, little work has been published on the effect of the refiners on the fatigue life of aluminum and its alloys. In this paper, the effect of addition of some rare earth materials, namely Vanadium and Zirconium on the fatigue life of commercially pure aluminum grain refined by Ti or Ti+B is reported and discussed. Furthermore, metallurgical aspects of these elements on the fatigue fractured surfaces are also discussed using scanning electron microscopy, SEM. Finally, photoscans of the fractured surfaces at different fatigue stresses are presented and discussed. (author)

  13. Masks for high aspect ratio x-ray lithography

    International Nuclear Information System (INIS)

    Malek, C.K.; Jackson, K.H.; Bonivert, W.D.; Hruby, J.


    Fabrication of very high aspect ratio microstructures, as well as ultra-high precision manufacturing is of increasing interest in a multitude of applications. Fields as diverse as micromechanics, robotics, integrated optics, and sensors benefit from this technology. The scale-length of this spatial regime is between what can be achieved using classical machine tool operations and that which is used in microelectronics. This requires new manufacturing techniques, such as the LIGA process, which combines x-ray lithography, electroforming, and plastic molding

  14. A review on the wettability of dental implant surfaces I: theoretical and experimental aspects. (United States)

    Rupp, Frank; Gittens, Rolando A; Scheideler, Lutz; Marmur, Abraham; Boyan, Barbara D; Schwartz, Zvi; Geis-Gerstorfer, Jürgen


    The surface wettability of biomaterials determines the biological cascade of events at the biomaterial/host interface. Wettability is modulated by surface characteristics, such as surface chemistry and surface topography. However, the design of current implant surfaces focuses mainly on specific micro- and nanotopographical features, and is still far from predicting the concomitant wetting behavior. There is an increasing interest in understanding the wetting mechanisms of implant surfaces and the role of wettability in the biological response at the implant/bone or implant/soft tissue interface. Fundamental knowledge related to the influence of surface roughness (i.e. a quantification of surface topography) on titanium and titanium alloy surface wettability, and the different associated wetting regimes, can improve our understanding of the role of wettability of rough implant surfaces on the biological outcome. Such an approach has been applied to biomaterial surfaces only in a limited way. Focusing on titanium dental and orthopaedic implants, the present study reviews the current knowledge on the wettability of biomaterial surfaces, encompassing basic and applied aspects that include measurement techniques, thermodynamic aspects of wetting and models predicting topographical and roughness effects on the wetting behavior. Copyright © 2014 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

  15. Some aspects of the behavior of barium, bismuth and strontium on silicon surfaces studied by TXRF

    International Nuclear Information System (INIS)

    Kilian, G.; Kolbesen, B.O.; Pamler, W.; Unger, E.; Hoepfner, A.


    Current dielectric film materials (SiO 2 , SiO 2 /Si 3 N 4 ) are one of the limiting factors for the scaling of microelectronic devices in the sub-quartermicron regime, in particular regarding the storage capacitor of dynamic random access memories (DRAMs). Alternative materials comprise films with high ε such as BaSrTiO 3 (BST) or films with ferroelectric behavior such as PbZrTiO 3 (PZT) or SrBi 2 Ta 2 O 9 (SBT). In order to integrate ferroelectric and high ε films into standard CMOS technology it is necessary to investigate possible detrimental effects on performance and reliability. In case of SBT, very little is known about the effect of Ba, Bi and Sr contamination on silicon device technology. Therefore, some aspects of their adsorption, desorption and diffusion behavior at room and higher temperature in inert (N 2 ) and oxidising (O 2 ) ambient have been studied by monitoring the Ba, Bi and Sr concentrations on silicon surfaces by total reflection x-ray fluorescence analysis (TXRF). Ba and Sr are incorporated in the existing or growing oxide during RTA. If O 2 is present the growing oxide on the silicon surface forms a barrier which forces the Bi to diffuse into the bulk. Hence, cross contamination due to gas phase transport may occur in the case of Bi under N 2 atmosphere but is of no concern in the case of Ba and Sr. (author)

  16. Some aspects related to the high performance in gamma spectrometry

    International Nuclear Information System (INIS)

    Vieru, Gheorghe; Mihaiu, Ramona; Nistor, Viorica


    Full text: Gamma spectroscopy is the science (or art) of identification and/or quantification of radionuclides through gamma-ray energy spectrum analysis. It is a recognized technique, well illustrated by the following examples: environmental radioactivity monitoring, health physics personnel monitoring, reactor corrosion monitoring, nuclear materials safeguards and homeland security, as well as nuclear forensics, materials testing, nuclear medicine and radiopharmaceuticals, and industrial process monitoring. Within the Reliability and Testing Laboratory of INR Pitesti there is now available such a detector of high performance that includes all aspects related to cooling, signal processing (with a high resolution) and the dedicated software applications. At the present time, taking into account the 'nuclear renaissance' the new experimental testing laboratories require complete set-up rather than laboratories having a mixture of the old equipment. The paper presents the mechanically cooled HPGe spectrometers with an undergoing rapid evolution, which eliminate traditional intensive liquid nitrogen management. Also, there are described the digital signal processing virtually by eliminating system drift, and, at the same time, requiring recalibrations much less frequently. Another important aspect presented is related to the software applications, which cover a broad spectrum of nuclear measurement techniques. (authors)

  17. New aspects of electronic excitations at the bismuth surface: Topology, thermalization and coupling to coherent phonons

    Energy Technology Data Exchange (ETDEWEB)

    Perfetti, L., E-mail: [Laboratoire des Solides Irradiés, Ecole Polytechnique – CEA/DSM – CNRS UMR 7642, 91128 Palaiseau (France); Faure, J. [Laboratoire d’Optique Appliquée, Ecole Polytechnique – ENSTA – CNRS UMR 7639, 91761 Palaiseau (France); Papalazarou, E.; Mauchain, J.; Marsi, M.; Goerbig, M.O. [Laboratoire de Physique des Solides, CNRS UMR 8502, Université Paris-Sud, F-91405 Orsay (France); Taleb-Ibrahimi, A.; Ohtsubo, Y. [Synchrotron SOLEIL, Saint-Aubin-BP 48, F-91192 Gif sur Yvette (France)


    We review measurements of angle and time resolved photoelectron spectroscopy on the surface states of the Bi(1 1 1) surface. The work covers several aspects of these surface states, discussing the topological properties, the strong anisotropy of the spin–orbit splitting and the dynamical relaxation of photoexcited electrons. Since time resolved experiments disentagle interaction processes in real time, the reported data offer a novel perspective on the motion of charge carriers in surface states and will serve as an unuseful reference for other systems with strong spin–orbit coupling.

  18. High Yield Synthesis of Aspect Ratio Controlled Graphenic Materials from Anthracite Coal in Supercritical Fluids. (United States)

    Sasikala, Suchithra Padmajan; Henry, Lucile; Yesilbag Tonga, Gulen; Huang, Kai; Das, Riddha; Giroire, Baptiste; Marre, Samuel; Rotello, Vincent M; Penicaud, Alain; Poulin, Philippe; Aymonier, Cyril


    This paper rationalizes the green and scalable synthesis of graphenic materials of different aspect ratios using anthracite coal as a single source material under different supercritical environments. Single layer, monodisperse graphene oxide quantum dots (GQDs) are obtained at high yield (55 wt %) from anthracite coal in supercritical water. The obtained GQDs are ∼3 nm in lateral size and display a high fluorescence quantum yield of 28%. They show high cell viability and are readily used for imaging cancer cells. In an analogous experiment, high aspect ratio graphenic materials with ribbon-like morphology (GRs) are synthesized from the same source material in supercritical ethanol at a yield of 6.4 wt %. A thin film of GRs with 68% transparency shows a surface resistance of 9.3 kΩ/sq. This is apparently the demonstration of anthracite coal as a source for electrically conductive graphenic materials.

  19. Planar silicon fabrication process for high-aspect-ratio micromachined parts

    Energy Technology Data Exchange (ETDEWEB)

    Barron, C.C.; Fleming, J.G. [Sandia National Labs., Albuquerque, NM (United States). Microelectronics Development Lab.


    Surface-micromachined silicon inertial sensors are limited to relatively high-G applications in part because of the fundamental limitations on proof mass imposed by the manufacturing technology. At the same time, traditional micromolding technologies such as LIGA do not lend themselves to integration with electronics, a capability which is equally necessary for high-performance inertial sensors. The silicon micromolding processes described in this report promise to offer both larger proof masses and integrability with on-chip electronics. In Sandia`s silicon micromolding process, the proof mass is formed using a mold which is first recessed into the substrate using a deep silicon trench etch, then lined with a sacrificial or etch-stop layer, and filled with mechanical polysilicon. Since the mold is recessed into the substrate, the whole micromechanical structure can be formed, planarized, and integrated with standard silicon microelectronic circuits before the release etch. In addition, unlike surface-micromachined parts, the thickness of the molded parts is limited by the depth of the trench etch (typically 10--50 {micro}m) rather than the thickness of deposited polysilicon (typically 2 {micro}m). The fact that the high-aspect-ratio section of the device is embedded in the substrate enables the monolithic integration of high-aspect-ratio parts with surface-micromachined mechanical parts, and, in the future, also electronics. The authors anticipate that such an integrated mold/surface micromachining/electronics process will offer versatile high-aspect-ratio micromachined structures that can be batch-fabricated and monolithically integrated into complex microelectromechanical systems including high-performance inertial sensing systems.

  20. Noise Measurements of High Aspect Ratio Distributed Exhaust Systems (United States)

    Bridges, James E.


    This paper covers far-field acoustic measurements of a family of rectangular nozzles with aspect ratio 8, in the high subsonic flow regime. Several variations of nozzle geometry, commonly found in embedded exhaust systems, are explored, including bevels, slants, single broad chevrons and notches, and internal septae. Far-field acoustic results, presented previously for the simple rectangular nozzle, showed that increasing aspect ratio increases the high frequency noise, especially directed in the plane containing the minor axis of the nozzle. Detailed changes to the nozzle geometry generally made little difference in the noise, and the differences were greatest at low speed. Having an extended lip on one broad side (bevel) did produce up to 3 decibels more noise in all directions, while extending the lip on the narrow side (slant) produced up to 2 decibels more noise, primarily on the side with the extension. Adding a single, non-intrusive chevron, made no significant change to the noise, while inverting the chevron (notch) produced up to 2decibels increase in the noise. Having internal walls (septae) within the nozzle, such as would be required for structural support or when multiple fan ducts are aggregated, reduced the noise of the rectangular jet, but could produce a highly directional shedding tone from the septae trailing edges. Finally, a nozzle with both septae and a beveled nozzle, representative of the exhaust system envisioned for a distributed electric propulsion aircraft with a common rectangular duct, produced almost as much noise as the beveled nozzle, with the septae not contributing much reduction in noise.

  1. Design Concepts for Low Aspect Ratio High Pressure Turbines for High Bypass Ratio Turbofans, Phase I (United States)

    National Aeronautics and Space Administration — The proposal is to identify cycle improvements and verify structural feasibility of shrouding a low aspect ratio High Pressure Turbine(HPT) rotor designed to use...

  2. High-Luminance Road Surfaces, (United States)


    condition was changed with the decreased use of snow chains and increasing use of studded tires. The studded tires wear down the road surface in a...region, white anorthosite of a uniform and unweathered type is usable as an additive to asphalt con- crete and wear surfacing for asphalt gravel...CLASSIFICATION Of THIS PAGE(W/em Daateoo 20. Abstract (cont’d) resistance to weathering, and the degree of luminosity. Quartzites have the best wear

  3. Highly immersive virtual reality laparoscopy simulation: development and future aspects. (United States)

    Huber, Tobias; Wunderling, Tom; Paschold, Markus; Lang, Hauke; Kneist, Werner; Hansen, Christian


    Virtual reality (VR) applications with head-mounted displays (HMDs) have had an impact on information and multimedia technologies. The current work aimed to describe the process of developing a highly immersive VR simulation for laparoscopic surgery. We combined a VR laparoscopy simulator (LapSim) and a VR-HMD to create a user-friendly VR simulation scenario. Continuous clinical feedback was an essential aspect of the development process. We created an artificial VR (AVR) scenario by integrating the simulator video output with VR game components of figures and equipment in an operating room. We also created a highly immersive VR surrounding (IVR) by integrating the simulator video output with a [Formula: see text] video of a standard laparoscopy scenario in the department's operating room. Clinical feedback led to optimization of the visualization, synchronization, and resolution of the virtual operating rooms (in both the IVR and the AVR). Preliminary testing results revealed that individuals experienced a high degree of exhilaration and presence, with rare events of motion sickness. The technical performance showed no significant difference compared to that achieved with the standard LapSim. Our results provided a proof of concept for the technical feasibility of an custom highly immersive VR-HMD setup. Future technical research is needed to improve the visualization, immersion, and capability of interacting within the virtual scenario.

  4. Technological aspects of high-$T_{c}$ superconductors

    CERN Document Server

    Mamalis, A G


    The applications of the dynamic or shock-wave compaction in the area of processing of high-T/sub c/ superconducting materials are presented and discussed. The basic aspects of explosive technology and also the various features of the related experimental techniques are reported. On the other hand, the influence of the shock-wave phenomena on macro-/microstructure and physico-chemical properties of the compacted ceramic, and the quality-performance of the final superconducting component are overviewed for certain industrial applications. Finally, some basic theoretical and empirical models describing the dynamic state of the material under shock and the stress-wave propagation are also included, in order to understand the dominant compaction mechanisms. (44 refs).

  5. Fabrication of high aspect ratio micro electrode by using EDM

    International Nuclear Information System (INIS)

    Elsiti, Nagwa Mejid; Noordin, M.Y.; Alkali, Adam Umar


    The electrical discharge machining (EDM) process inherits characteristics that make it a promising micro-machining technique. Micro electrical discharge machining (micro- EDM) is a derived form of EDM, which is commonly used to manufacture micro and miniature parts and components by using the conventional electrical discharge machining fundamentals. Moving block electro discharge grinding (Moving BEDG) is one of the processes that can be used to fabricate micro-electrode. In this study, a conventional die sinker EDM machine was used to fabricate the micro-electrode. Modifications are made to the moving BEDG, which include changing the direction of movements and control gap in one electrode. Consequently current was controlled due to the use of roughing, semi-finishing and finishing parameters. Finally, a high aspect ratio micro-electrode with a diameter of 110.49μm and length of 6000μm was fabricated. (paper)

  6. Some fundamental aspects of highly reactive iron coke production

    Energy Technology Data Exchange (ETDEWEB)

    Seiji Nomura; Hidetoshi Terashima; Eiji Sato; Masaaki Naito [Nippon Steel Corporation, Chiba (Japan). Environment and Process Technology Center


    It is important to develop the production and utilization technology of highly reactive coke in order to improve the efficiency of blast furnace reactions. In this study, some fundamental aspects of highly reactive iron coke produced in a coke oven chamber were investigated. First, the effects of catalytic Fe powder addition to coal before carbonization on coke strength were investigated. The addition of Fe powder decreased the coal caking property and hence the resultant coke drum index (DI150 15). On the other hand it increased coke reactivity (JIS coke reactivity index and CRI) to a great extent. This means that the caking property of blended coals needs to be adjusted higher to produce iron coke with proper strength and high reactivity. Secondly, it was shown that the iron ore reacts with silica brick at 1200{sup o}C in a condition similar to that in a coke oven chamber. The iron ore and silica reacted to produce fayalite (2FeO{center_dot}SiO{sub 2}) and the brick was damaged. On the other hand, it was proven that the iron ore does not react with silica brick at 1100{sup o}C in the above condition. Based on this fundamental study, iron coke with proper strength and high reactivity was successfully produced in a coke oven chamber on a commercial scale by adjusting the coal blend composition and the coke oven temperature. Furthermore it was revealed that about 70% of iron in iron ore powder added to coal was reduced to metallic iron during carbonization in coke ovens.

  7. Some fundamental aspects of highly reactive iron coke production

    Energy Technology Data Exchange (ETDEWEB)

    Nomura, S.; Terashima, H.; Sato, E.; Naito, M. [Nippon Steel Corp. Ltd., Futtsu (Japan)


    The development of production and utilization technology of highly reactive coke is significant in order to improve blast furnace reaction efficiency. In this report, some fundamental aspects of highly reactive iron coke produced in a coke oven chamber were investigated. First, the effects of catalytic Fe powder addition to coal before carbonization on coke strength were investigated. The addition of Fe powder decreased coal caking property and hence resultant coke drum index (DI{sup 150}{sub 15}). On the other hand it increased coke reactivity (JIS coke reactivity index and CRI) to a great extent. This means that caking property of blended coals needs to be adjusted higher to produce the iron coke with proper strength and high reactivity. Secondly, it was shown that the iron ore reacts with silica brick at 1200{sup o}C in a condition similar to that in a coke oven chamber. The iron ore and silica reacted to produce fayalite (2FeO {center_dot}SiO{sub 2}) and the brick was damaged. On the other hand, it was proved that the iron ore does not react with silica brick at 1100{sup o}C in the above condition. Based on this fundamental study, the iron coke with proper strength and high reactivity was successfully produced in coke ovens on a commercial scale by adjusting the coal blend composition and the coke oven temperature. Furthermore it was revealed that about 70% of iron in iron ore powder added to coal was reduced to metallic iron during carbonization in coke ovens.

  8. A 3-dimensional in vitro model of epithelioid granulomas induced by high aspect ratio nanomaterials

    Directory of Open Access Journals (Sweden)

    Hurt Robert H


    Full Text Available Abstract Background The most common causes of granulomatous inflammation are persistent pathogens and poorly-degradable irritating materials. A characteristic pathological reaction to intratracheal instillation, pharyngeal aspiration, or inhalation of carbon nanotubes is formation of epithelioid granulomas accompanied by interstitial fibrosis in the lungs. In the mesothelium, a similar response is induced by high aspect ratio nanomaterials, including asbestos fibers, following intraperitoneal injection. This asbestos-like behaviour of some engineered nanomaterials is a concern for their potential adverse health effects in the lungs and mesothelium. We hypothesize that high aspect ratio nanomaterials will induce epithelioid granulomas in nonadherent macrophages in 3D cultures. Results Carbon black particles (Printex 90 and crocidolite asbestos fibers were used as well-characterized reference materials and compared with three commercial samples of multiwalled carbon nanotubes (MWCNTs. Doses were identified in 2D and 3D cultures in order to minimize acute toxicity and to reflect realistic occupational exposures in humans and in previous inhalation studies in rodents. Under serum-free conditions, exposure of nonadherent primary murine bone marrow-derived macrophages to 0.5 μg/ml (0.38 μg/cm2 of crocidolite asbestos fibers or MWCNTs, but not carbon black, induced macrophage differentiation into epithelioid cells and formation of stable aggregates with the characteristic morphology of granulomas. Formation of multinucleated giant cells was also induced by asbestos fibers or MWCNTs in this 3D in vitro model. After 7-14 days, macrophages exposed to high aspect ratio nanomaterials co-expressed proinflammatory (M1 as well as profibrotic (M2 phenotypic markers. Conclusions Induction of epithelioid granulomas appears to correlate with high aspect ratio and complex 3D structure of carbon nanotubes, not with their iron content or surface area. This model

  9. An Empirical Jet-Surface Interaction Noise Model with Temperature and Nozzle Aspect Ratio Effects (United States)

    Brown, Cliff


    An empirical model for jet-surface interaction (JSI) noise produced by a round jet near a flat plate is described and the resulting model evaluated. The model covers unheated and hot jet conditions (1 less than or equal to jet total temperature ratio less than or equal to 2.7) in the subsonic range (0.5 less than or equal to M(sub a) less than or equal to 0.9), surface lengths 0.6 less than or equal to (axial distance from jet exit to surface trailing edge (inches)/nozzle exit diameter) less than or equal to 10, and surface standoff distances (0 less than or equal to (radial distance from jet lipline to surface (inches)/axial distance from jet exit to surface trailing edge (inches)) less than or equal to 1) using only second-order polynomials to provide predictable behavior. The JSI noise model is combined with an existing jet mixing noise model to produce exhaust noise predictions. Fit quality metrics and comparisons to between the predicted and experimental data indicate that the model is suitable for many system level studies. A first-order correction to the JSI source model that accounts for the effect of nozzle aspect ratio is also explored. This correction is based on changes to the potential core length and frequency scaling associated with rectangular nozzles up to 8:1 aspect ratio. However, more work is needed to refine these findings into a formal model.

  10. Collider aspects of flavor physics at high Q

    CERN Document Server

    del Aguila, F.; Allanach, B.C.; Alwall, Johan; Andreev, Yu.; Aristizabal Sierra, D.; Bartl, A.; Beccaria, M.; Bejar, S.; Benucci, L.; Bityukov, S.; Borjanovic, I.; Bozzi, G.; Burdman, Gustavo A.; Carvalho, J.; Castro, Nuno Filipe; Clerbaux, Barbara; Carvalho De Campos, Fernando Luiz; de Gouvea, A.; Dennis, C.; Djouadi, A.; Eboli, O.J.P.; Ellwanger, U.; Fassouliotis, D.; Ferreira, P.M.; Frederix, R.; Fuks, Benjamin; Gerard, Jean-Marc; Giammanco, A.; Gninenko, Sergei; Gopalakrishna, S.; Goto, T.; Grzadkowski, B.; Guasch, J.; Hahn, T.; Heinemeyer, S.; Hektor, A.; Herquet, M.; Herrmann, B.; Hidaka, K.; Hirsch, M.K.; Hohenwarter-Sodek, K.; Hollik, W.; Hou, George W.S.; Hurth, T.; Ibarra, A.; Illana, J.; Kadastik, M.; Kalinin, S.; Karafasoulis, C.; Karagoz, Muge; Kernreiter, T.; Kirsanov, M.M.; Klasen, M.; Kou, E.; Kourkoumelis, C.; Kraml, S.; Krasnikov, N.; Krauss, F.; Kyriakis, A.; Lari, T.; Lemaitre, V.; Macorini, G.; Magro, M.B.; Majerotto, W.; Maltoni, F.; Mehdiyev, R.; Misiak, M.; Moortgat, F.; Moreau, G.; Muhlleitner, M.; Muntel, M.; Onofre, A.; Ozcan, Veysi E.; Palla, F.; Panizzi, L.; Pape, L.; Penaranda, S.; Pittau, R.; Polesello, G.; Porod, W.; Pukhov, A.; Raidal, M.; Raklev, A.R.; Rebane, L.; Renard, F.M.; Restrepo, D.; Roupas, Z.; Santos, R.; Schumann, S.; Servant, G.; Siegert, F.; Skands, Peter Z.; Slavich, P.; Sola, J.; Spira, M.; Sultansoy, Saleh; Toropin, A.; Tricomi, A.; Tseng, J.; Unel, Gokhan; Valle, J.W.F.; Veloso, F.; Ventura, Andrea; Vermisoglou, G.; Verzegnassi, C.; Villanova del Moral, Albert; Weiglein, G.; Yilmaz, M.; Working Group 1 [on Flavour in the Era of the LHC


    This review presents flavour related issues in the production and decays of heavy states at LHC, both from the experimental side and from the theoretical side. We review top quark physics and discuss flavour aspects of several extensions of the Standard Model, such as supersymmetry, little Higgs model or models with extra dimensions. This includes discovery aspects as well as measurement of several properties of these heavy states. We also present public available computational tools related to this topic.

  11. Development of a virtual probe tip with an application to high aspect ratio microscale features

    International Nuclear Information System (INIS)

    Bauza, Marcin B.; Hocken, Robert J.; Smith, Stuart T.; Woody, Shane C.


    Nondestructive measurement of microscale features remains a challenging metrology problem. For example, to assess a high aspect ratio small hole it is currently common to cut a cross section and measure the features of interest using an atomic force microscope, scanning probe microscope, or scanning electron microscope. Typically, these metrology tools may be suitable for surface finish measurement but often lack the capability for dimensional metrology. The aim of this article is to discuss the development of a high aspect-ratio microscale probe for measurement of microscale features. A 700:1 high aspect ratio probe shank is fabricated with a 7 μm diameter, and attached at one end to an oscillator. The oscillator produces a standing wave in the oscillating probe shank as opposed to conventional probes that use a microscale sphere on the end of a comparatively rigid shank. As a result of the standing wave formed in steady state vibration, the free end of the shank generates an amplitude of oscillation greater than the probe shank diameter. Thus, the probe does not require a spherical ball to serve as the contact point and simply uses the contact diameter of the free end of the vibrating shank. This methodology is referred to as a virtual probe tip. The virtual probe tip in conjunction with a nanopositioning scanner is used to measure surface profile measurements over traverse lengths of 130 μm. In this article, results from profiles of a 500 nm step height and a ruby sphere of diameter 1 mm are presented. Experiments in this article indicate the ability to repeatedly resolve surface features of less than 5 nm while maintaining bandwidths greater than 1 kHz. Furthermore, adhesion problems often encountered with micrometer scaled probes were not observed during profile measurements with this virtual probe

  12. Dense high-aspect ratio 3D carbon pillars on interdigitated microelectrode arrays

    DEFF Research Database (Denmark)

    Amato, Letizia; Heiskanen, Arto; Hansen, Rasmus


    In this work we present high-aspect ratio carbon pillars (1.4 μm in diameter and ∼11 μm in height) on top of interdigitated electrode arrays to be used for electrochemical applications. For this purpose, different types of 2D and 3D pyrolysed carbon structures were fabricated and characterised...... including surface- and microstructure, electrical and electrochemical properties. A pre-treatment of oxidised Si wafers is introduced to eliminate electrode delamination and ensure structure stability in water during long time-experiments. Additionally, a heat treatment method is reported for regeneration...... of pyrolysed carbon films with increased film resistance due to oxidation during storage....

  13. SML resist processing for high-aspect-ratio and high-sensitivity electron beam lithography (United States)

    Mohammad, Mohammad Ali; Dew, Steven K.; Stepanova, Maria


    A detailed process characterization of SML electron beam resist for high-aspect-ratio nanopatterning at high sensitivity is presented. SML contrast curves were generated for methyl isobutyl ketone (MIBK), MIBK/isopropyl alcohol (IPA) (1:3), IPA/water (7:3), n-amyl acetate, xylene, and xylene/methanol (3:1) developers. Using IPA/water developer, the sensitivity of SML was improved considerably and found to be comparable to benchmark polymethylmethacrylate (PMMA) resist without affecting the aspect ratio performance. Employing 30-keV exposures and ultrasonic IPA/water development, an aspect ratio of 9:1 in 50-nm half-pitch dense grating patterns was achieved representing a greater than two times improvement over PMMA. Through demonstration of 25-nm lift-off features, the pattern transfer performance of SML is also addressed.

  14. Evaluation of the In Vitro Effect of Gold Nanorod Aspect Ratio, Surface Charge and Chemistry on Cellular Association and Cytotoxicity (United States)



  15. High aspect ratio nanoholes in glass generated by femtosecond laser pulses with picosecond intervals (United States)

    Ahn, Sanghoon; Choi, Jiyeon; Noh, Jiwhan; Cho, Sung-Hak


    Because of its potential uses, high aspect ratio nanostructures have been interested for last few decades. In order to generate nanostructures, various techniques have been attempted. Femtosecond laser ablation is one of techniques for generating nanostructures inside a transparent material. For generating nanostructures by femtosecond laser ablation, previous studies have been attempted beam shaping such as Bessel beam and temporal tailored beam. Both methods suppress electron excitation at near surface and initiate interference of photons at certain depth. Recent researches indicate that shape of nanostructures is related with temporal change of electron density and number of self-trapped excitons. In this study, we try to use the temporal change of electron density induced by femtosecond laser pulse for generating high aspect ratio nanoholes. In order to reveal the effect of temporal change of electron density, secondary pulses are irradiated from 100 to 1000 ps after the irradiation of first pulse. Our result shows that diameter of nanoholes is increasing and depth of nanoholes is decreasing as pulse to pulse interval is getting longer. With manipulating of pulse to pulse interval, we could generate high aspect ratio nanoholes with diameter of 250-350 nm and depth of 4∼6 μm inside a glass.

  16. Collider Aspects of Flavour Physics at High Q

    Energy Technology Data Exchange (ETDEWEB)

    del Aguila, F.; Aguilar-Saavedra, J.A.; Allanach, B.C.; Alwall, J.; Andreev, Yu.; Aristizabal Sierra, D.; Bartl, A.; Beccaria, M.; Bejar, S.; Benucci, L.; Bityukov, S.; Borjanovic, I.; Bozzi, G.; Burdman, G.; Carvalho, J.; Castro, N.; Clerbaux, B.; de Campos, F.; de Gouvea, A.; Dennis, C.; Djouadi, A.; /Cambridge U., DAMTP /Louvain U., CP3 /Moscow, INR /Valencia U. /Vienna U. /Salento U. /INFN, Lecce /Barcelona, Autonoma U. /Barcelona, IFAE /INFN, Pisa /Pisa U. /Karlsruhe U. /Sao Paulo U. /LIP, Coimbra /Brussels U. /Sao Paulo U., Guaratingueta /Northwestern U. /Oxford U. /Orsay, LPT /Athens U. /Lisbon U.


    This chapter of the report of the 'Flavour in the era of LHC' workshop discusses flavor related issues in the production and decays of heavy states at LHC, both from the experimental side and from the theoretical side. We review top quark physics and discuss flavor aspects of several extensions of the Standard Model, such as supersymmetry, little Higgs model or models with extra dimensions. This includes discovery aspects as well as measurement of several properties of these heavy states. We also present public available computational tools related to this topic.

  17. Simulation and Measurement of Neuroelectrodes' Characteristics with Integrated High Aspect Ratio Nano Structures

    Directory of Open Access Journals (Sweden)

    Christoph Nick


    Full Text Available Improving the interface between electrodes and neurons has been the focus of research for the last decade. Neuroelectrodes should show small geometrical surface area and low impedance for measuring and high charge injection capacities for stimulation. Increasing the electrochemically active surface area by using nanoporous electrode material or by integrating nanostructures onto planar electrodes is a common approach to improve this interface. In this paper a simulation approach for neuro electrodes' characteristics with integrated high aspect ratio nano structures based on a point-contact-model is presented. The results are compared with experimental findings conducted with real nanostructured microelectrodes. In particular, effects of carbon nanotubes and gold nanowires integrated onto microelectrodes are described. Simulated and measured impedance properties are presented and its effects onto the transfer function between the neural membrane potential and the amplifier output signal are studied based on the point-contact-model. Simulations show, in good agreement with experimental results, that electrode impedances can be dramatically reduced by the integration of high aspect ratio nanostructures such as gold nanowires and carbon nanotubes. This lowers thermal noise and improves the signal-to-noise ratio for measuring electrodes. It also may increase the adhesion of cells to the substrate and thus increase measurable signal amplitudes.

  18. Aspects of silane coupling agents and surface conditioning in dentistry: an overview. (United States)

    Lung, Christie Ying Kei; Matinlinna, Jukka Pekka


    To give an overview of aspects of silane coupling agents and surface conditioning in dentistry. Currently, silane coupling agents are used as adhesion promoters. Silanes are effective in enhancing adhesion between resin composite and silica-based ceramics. They do not bond effectively to non-silica based dental restorative materials. Surface conditioning of non-silica based ceramics with silica coating improves the bonding. This current overview will focus on the silane coupling agents: their properties, limitations in adhesion promotion and the clinical problems with the use of silanes. It will also focus on the current surface conditioning methods as well as new surface conditioning techniques to enhance the bonding through conventional silanization approaches. Several surface conditioning methods are being used clinically to enhance the adhesion of resin composites to non-silica based restorative materials. Other approaches are under investigation. The clinical problem of using silanes in adhesion promotion is the bond degradation over time in oral environment. The current silane coupling agents are not ideal. The current silane coupling agents can fulfill the minimum requirements in clinical practice to enhance the bonding of resin composite to dental restorative materials. Developments of novel surface conditioning methods and silane coupling agents are required to address the bond durability problem. Copyright © 2012 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

  19. Improving acousto-optical interaction by high aspect ratio electrodes

    DEFF Research Database (Denmark)

    Dühring, Maria Bayard

    In recent years experiments have shown that optical waves in waveguides can be modulated by mechanical stresses from surface acoustic waves (SAW), which have most of their energy density concentrated at the surface. In these experiments the SAWs are generated in piezoelectric materials...

  20. Optimization of HNA etching parameters to produce high aspect ratio solid silicon microneedles

    International Nuclear Information System (INIS)

    Hamzah, A A; Yeop Majlis, B; Yunas, J; Dee, C F; Abd Aziz, N; Bais, B


    High aspect ratio solid silicon microneedles with a concave conic shape were fabricated. Hydrofluoric acid–nitric acid–acetic acid (HNA) etching parameters were characterized and optimized to produce microneedles that have long and narrow bodies with smooth surfaces, suitable for transdermal drug delivery applications. The etching parameters were characterized by varying the HNA composition, the optical mask's window size, the etching temperature and bath agitation. An L9 orthogonal Taguchi experiment with three factors, each having three levels, was utilized to determine the optimal fabrication parameters. Isoetch contours for HNA composition with 0% and 10% acetic acid concentrations were presented and a high nitric acid region was identified to produce microneedles with smooth surfaces. It is observed that an increase in window size indiscriminately increases the etch rate in both the vertical and lateral directions, while an increase in etching temperature beyond 35 °C causes the etching to become rapid and uncontrollable. Bath agitation and sample placement could be manipulated to achieve a higher vertical etch rate compared to its lateral counterpart in order to construct high aspect ratio microneedles. The Taguchi experiment performed suggests that a HNA composition of 2:7:1 (HF:HNO 3 :CH 3 COOH), window size of 500 µm and agitation rate of 450 RPM are optimal. Solid silicon microneedles with an average height of 159.4 µm, an average base width of 110.9 µm, an aspect ratio of 1.44, and a tip angle and diameter of 19.2° and 0.38 µm respectively were successfully fabricated. (paper)

  1. Model systems with extreme aspect ratio, tunable geometry, and surface functionality for a quantitative investigation of the Lotus effect. (United States)

    Hassel, Achim Walter; Milenkovic, Srdjan; Schürmann, Ulrich; Greve, Henry; Zaporojtchenko, Vladimir; Adelung, Rainer; Faupel, Franz


    Superhydrophobicity and superhydrophilicity of surfaces are key properties for fabrication of self-cleaning surfaces (Lotus effect). It is well known that the mechanism behind this is based on the surface roughness and surface functionalization. To obtain an understanding of the details of the underlying mechanism, a metal system based on a eutectic is suggested. In this study, a wide range tunability of its needlelike narrow size distributed nanostructure is demonstrated. The length of the needles as well as their density can be varied independently. In addition, an important parameter for the wettability, the roughness, is related directly to the growth parameters, which lead to excellent controllable and reproducible eutectic structures. Simply by varying etching time very high aspect ratios can be achieved, allowing studying the interaction of the very long needles with liquids. Moreover, the surface functionality can be tuned by RF-magnetron sputtering of PTFE onto the metal needles. As those layers can be very thin, our system allows, in principle, studying the transition from a metal to a polymer surface using submonolayers. Furthermore, the first contact angle measurements on the nanostructured and functionalized eutectic structures are presented and discussed.

  2. Diffusion of dilute gas in arrays of randomly distributed, vertically aligned, high-aspect-ratio cylinders. (United States)

    Szmyt, Wojciech; Guerra, Carlos; Utke, Ivo


    In this work we modelled the diffusive transport of a dilute gas along arrays of randomly distributed, vertically aligned nanocylinders (nanotubes or nanowires) as opposed to gas diffusion in long pores, which is described by the well-known Knudsen theory. Analytical expressions for (i) the gas diffusion coefficient inside such arrays, (ii) the time between collisions of molecules with the nanocylinder walls (mean time of flight), (iii) the surface impingement rate, and (iv) the Knudsen number of such a system were rigidly derived based on a random-walk model of a molecule that undergoes memoryless, diffusive reflections from nanocylinder walls assuming the molecular regime of gas transport. It can be specifically shown that the gas diffusion coefficient inside such arrays is inversely proportional to the areal density of cylinders and their mean diameter. An example calculation of a diffusion coefficient is delivered for a system of titanium isopropoxide molecules diffusing between vertically aligned carbon nanotubes. Our findings are important for the correct modelling and optimisation of gas-based deposition techniques, such as atomic layer deposition or chemical vapour deposition, frequently used for surface functionalisation of high-aspect-ratio nanocylinder arrays in solar cells and energy storage applications. Furthermore, gas sensing devices with high-aspect-ratio nanocylinder arrays and the growth of vertically aligned carbon nanotubes need the fundamental understanding and precise modelling of gas transport to optimise such processes.

  3. Diffusion of dilute gas in arrays of randomly distributed, vertically aligned, high-aspect-ratio cylinders

    Directory of Open Access Journals (Sweden)

    Wojciech Szmyt


    Full Text Available In this work we modelled the diffusive transport of a dilute gas along arrays of randomly distributed, vertically aligned nanocylinders (nanotubes or nanowires as opposed to gas diffusion in long pores, which is described by the well-known Knudsen theory. Analytical expressions for (i the gas diffusion coefficient inside such arrays, (ii the time between collisions of molecules with the nanocylinder walls (mean time of flight, (iii the surface impingement rate, and (iv the Knudsen number of such a system were rigidly derived based on a random-walk model of a molecule that undergoes memoryless, diffusive reflections from nanocylinder walls assuming the molecular regime of gas transport. It can be specifically shown that the gas diffusion coefficient inside such arrays is inversely proportional to the areal density of cylinders and their mean diameter. An example calculation of a diffusion coefficient is delivered for a system of titanium isopropoxide molecules diffusing between vertically aligned carbon nanotubes. Our findings are important for the correct modelling and optimisation of gas-based deposition techniques, such as atomic layer deposition or chemical vapour deposition, frequently used for surface functionalisation of high-aspect-ratio nanocylinder arrays in solar cells and energy storage applications. Furthermore, gas sensing devices with high-aspect-ratio nanocylinder arrays and the growth of vertically aligned carbon nanotubes need the fundamental understanding and precise modelling of gas transport to optimise such processes.

  4. Technique for measuring very high surface velocities

    International Nuclear Information System (INIS)

    Maron, Y.


    An interferometric technique for measuring displacements of surfaces moving at velocities in the range of a few millimeters per microsecond is presented. The Doppler shift of frequency of light scattered from such surfaces is too high to be detectable by known devices. The present technique is based upon monitoring the signal resulting from the interference between two beams reflected from the surface at different incidence angles. Measurement systems for specularly as well as diffusely reflecting surfaces are described. Light source with very modest temporal coherence delivering about 100 mw power is required. The accuracy of the technique is discussed. (author)

  5. Hot punching of high-aspect-ratio 3D polymeric microstructures for drug delivery

    DEFF Research Database (Denmark)

    Petersen, Ritika Singh; Keller, Stephan Sylvest; Boisen, Anja


    Hot punching: a highly versatile method of fabricating high-aspect-ratio 3D microstructures for drug delivery with good replication fidelity and yield.......Hot punching: a highly versatile method of fabricating high-aspect-ratio 3D microstructures for drug delivery with good replication fidelity and yield....

  6. Addressing Cultural Aspects of Organisations in High Risk Industries

    International Nuclear Information System (INIS)

    Gisquet, Elsa; Jeffroy, Francois; LEVY, Emmanuelle


    The concept of Safety Culture is a key element of many initiatives aimed at improving the safety of nuclear facilities. In particular, the IAEA has focused its development strategy on taking into account human and organisational factors. In this context, the IRSN has mainly devoted its evaluations and research to theoretical lines arising from ergonomics and the sociology of organisations. Although this orientation has helped to formulate documented assessments, it is necessary to better take into account cultural aspects, because some of these contribute to risk management. They can, for example, be an important part of provisions to promote cooperation between different professions (maintenance and operation, operation and decommissioning, operation and research, etc.), between project organisation and daily organisation (outage management, change implementation, dismantling work sites, etc.), between companies (relations between customers and service providers). The IRSN thus conducted a study aimed at defining guidelines for the use of the 'culture' and 'safety culture' concepts in safety assessments of nuclear facilities. First, the contributions and limitations of the safety culture concept are identified, leading as a second stage to a review of the main works on culture that have been conducted in anthropology, sociology, management science and ergonomics. These studies show that taking into account cultural aspects can give access to phenomena that are difficult to deal with using other organisation analytical frameworks. On this basis, four analysis plans were defined, which provide a breakdown of the overall 'culture' topic: organisational cultures, professional cultures, social cultures and relations, and national cultures. In the fourth part of the document, these analysis plans are used to revisit safety assessments performed in the past. In doing so, the relationship between cultural aspects and safety are specified and

  7. Gas-Assisted Heating Technology for High Aspect Ratio Microstructure Injection Molding

    Directory of Open Access Journals (Sweden)

    Shia-Chung Chen


    Full Text Available A hot gas is used for heating the cavity surface of a mold. Different mold gap sizes were designed. The mold surface temperature was heated to above the glass transition temperature of the plastic material, and the mold then closed for melt filling. The cavity surface can be heated to 130°C to assist the melt filling of the microfeatures. Results show that hot gas heating can improve the filling process and achieve 91% of the high aspect ratio microgrooves (about 640.38 μm of the maximum of 700 μm. The mold gap size strongly affects the heating speed and heating uniformity. Without surface preheating, the center rib is the highest. When the heating target temperature is 90°C or 100°C, the three microribs have a good uniformity of height. However, when the target temperature exceeds 100°C, the left side rib is higher than the other ribs.

  8. Dielectrophoretically structured piezoelectric composites with high aspect ratio piezoelectric particles inclusions

    NARCIS (Netherlands)

    Ende, D.A. van den; Kempen, S.E. van; Wu, X.; Groen, W.A.; Randall, C.A.; Zwaag, S. van der


    Piezoelectric composites were prepared by dielectrophoretic alignment of high aspect ratio piezoelectric particles in a thermosetting polymer matrix. A high level of alignment was achieved in the cured composite from a resin containing randomly oriented high aspect ratio particles. Upon application

  9. High-Energy Aspects of Solar Flares: Observations and Models

    Energy Technology Data Exchange (ETDEWEB)

    Liu, Wei [Lockheed Martin Solar and Astrophysics Laboratory; Guo, Fan [Los Alamos National Laboratory


    The paper begins by describing the structure of the Sun, with emphasis on the corona. The Sun is a unique plasma laboratory, which can be probed by Sun-grazing comets, and is the driver of space weather. Energization and particle acceleration mechanisms in solar flares is presented; magnetic reconnection is key is understanding stochastic acceleration mechanisms. Then coupling between kinetic and fluid aspects is taken up; the next step is feedback of atmospheric response to the acceleration process – rapid quenching of acceleration. Future challenges include applications of stochastic acceleration to solar energetic particles (SEPs), Fermi γ-rays observations, fast-mode magnetosonic wave trains in a funnel-shaped wave guide associated with flare pulsations, and the new SMEX mission IRIS (Interface Region Imaging Spectrograph),

  10. Aspects of data on the breakup of highly excited nuclei

    International Nuclear Information System (INIS)

    Warwick, A.I.; Wieman, H.H.; Gutbrod, H.H.; Ritter, H.G.; Stelzer, H.; Weik, F.; Kaufman, S.B.; Steinberg, E.P.; Wilkins, B.D.


    There is an awakening of theoretical interest in the mechanisms by which nuclear fragments (4 less than or equal to A less than or equal to 150) are produced in violent collisions of heavy ions. With this in mind we review some aspects of the available experimental data and point out some challenging features against which to test the models. The concept of evaporation is tremendously powerful when applied to pieces of nuclei of low excitation (1 or 2 MeV/u). Current interest focuses on higher excitations, at the point where the binding energy of the system vanishes. This is the transition from liquid nuclei to a gas of nucleons, and it may be that the critical phenomena that certainly exist in infinite nuclear matter will be manifest in finite nuclei under these conditions

  11. Some new aspects of super-high temperature superconductors

    Energy Technology Data Exchange (ETDEWEB)

    Huang, C.Y. (Research and Development Div., Lockheed Missiles and Space Co., Palto Alto, CA (US)); Rabinowitz, M. (Electric Power Research Inst., Palo Alto, CA (USA). Electrical Systems Div.)


    The authors review some salient features of the recently observed experimental evidence of ceramic super-high temperature superconductivity (T{sub c} {gt} 200 K). Two theoretical estimates which are capable of accounting for super-high T{sub c} are presented. For comparison, several reports on non-ceramic oxide super-high temperature superconductors are discussed.

  12. Metallization of high aspect ratio, out of plane structures

    DEFF Research Database (Denmark)

    Vazquez, Patricia; Dimaki, Maria; Svendsen, Winnie Edith


    This work is dedicated to developing a novel three dimensional structure for electrochemical measurements in neuronal studies. The final prototype will allow not only for the study and culture on chip of neuronal cells, but also of brain tissue. The use of out-of-plane electrodes instead of planar...... ones increases the sensitivity of the system and increases the signal-to-noise ratio in the recorded signals, due to the higher availability of surface area. The main bottleneck of the out-of-plane electrode fabrication lies in the metallization process for transforming them into active electrodes...

  13. Fabrication of 3D high aspect ratio PDMS microfluidic networks with a hybrid stamp. (United States)

    Kung, Yu-Chun; Huang, Kuo-Wei; Fan, Yu-Jui; Chiou, Pei-Yu


    We report a novel methodology for fabricating large-area, multilayer, thin-film, high aspect ratio, 3D microfluidic structures with through-layer vias and open channels that can be bonded between hard substrates. It is realized by utilizing a hybrid stamp with a thin plastic sheet embedded underneath a PDMS surface. This hybrid stamp solves an important edge protrusion issue during PDMS molding while maintaining necessary stamp elasticity to ensure the removal of PDMS residues at through-layer regions. Removing edge protrusion is a significant progress toward fabricating 3D structures since high aspect ratio PDMS structures with flat interfaces can be realized to facilitate multilayer stacking and bonding to hard substrates. Our method also allows for the fabrication of 3D deformable channels, which can lead to profound applications in electrokinetics, optofluidics, inertial microfluidics, and other fields where the shape of the channel cross section plays a key role in device physics. To demonstrate, as an example, we have fabricated a microfluidic channel by sandwiching two 20 μm wide, 80 μm tall PDMS membranes between two featureless ITO glass substrates. By applying electrical bias to the two ITO substrates and pressure to deform the thin membrane sidewalls, strong electric field enhancement can be generated in the center of a channel to enable 3D sheathless dielectrophoretic focusing of biological objects including mammalian cells and bacteria at a flow speed up to 14 cm s(-1).

  14. On some aspects of high voltage electron microscopy

    International Nuclear Information System (INIS)

    Jouffrey, B.; Trinquier, J.


    The present paper deals with high voltage electron microscopy (HVEM). It is an overview on this domain due to the pionneer work of G. Dupouy which has permitted to perform a new kind of electron microscopy. Since this time, HVEM has shown its interest in high resolution, irradiations, chemical analysis, in situ experiments

  15. Study of Ag induced bimetallic (Au-Ag) nanowires on silicon (5 5 12) surfaces: Experiment and theoretical aspects (United States)

    Bhukta, Anjan; Bagarti, Trilochan; Guha, Puspendu; Ravulapalli, Sathyavathi; Satpati, Biswarup; Rakshit, Bipul; Maiti, Paramita; Parlapalli, Venkata Satyam


    The reconstructed vicinal (high index) silicon surfaces, such as, Si (5 5 12) composes row-like structures that can be used as templates for growing aligned nanowires. By using a sub-monolayers of Ag, prior to Au deposition on reconstructed Si (5 512) surface, intermixing of Au and Ag, enhancement of aspect ratio of bimetallic Au-Ag nanowires with tunable morphology is reported. This is attributed to a combined effect of pre-grown Ag strips as nucleation centers for incoming Au ad-atoms and anisotropic Au-Ag intermixing. To achieve optimum conditions for the growth of larger aspect ratio Au-Ag nanostructures, the growth kinetics have been studied by varying growth and annealing temperatures. At ≈400 °C, the Ag diffused into silicon substrate and the inter-diffusion found to inhibit the formation of Au-Ag bimetallic nanostructures. Controlled experiments under ultra-high vacuum condition in a molecular beam epitaxy system and in-situ scanning tunneling microscopy measurements along with ex-situ scanning transmission and secondary electron microscopy measurements have been carried out to understand the bimetallic nanostructure growth. Kinetic Monte Carlo (KMC) simulations based on kinematics of ad-atoms on an anisotropic template with a solid on solid model in which the relative ratios of binding energies (that are obtained from the Density Functional Theory) have been used and the KMC simulations results agree with the experimental observations. Advantage of having bimetallic structures as effective substrates for Surface enhanced Raman spectroscopy application is demonstrated by detecting Rhodamine 6 G (R6G) molecule at the concentration of 10-7M.

  16. Basic aspects of high-Tc grain boundary devices

    International Nuclear Information System (INIS)

    Mannhart, J.; Moler, K.A.; Sigrist, M.


    Grain boundaries are extensively used as high-quality Josephson junctions in high-T c superconductors. Their superconducting characteristics can generally be well described by conventional models of strongly coupled Josephson junctions. Here, we report on highly anomalous critical current vs. magnetic field dependencies of grain boundaries in YBa 2 Cu 3 O 7-x . Direct imaging with scanning SQUID microscopy provides evidence of magnetic flux generated by single grain boundaries. Conventional Josephson junction models cannot explain these effects if a superconducting order parameter with a pure s-wave symmetry is assumed. The results have significant implications for our understanding of the properties of grain boundaries in high-T c superconductors and for their applications. (orig.)

  17. Some health aspects of high-energy society

    International Nuclear Information System (INIS)

    Cook, E.


    The intensive use of inanimate energy in industrialized or high-energy society has subsidized research, development, and higher education and has brought about changes in nutrition and life-style that have led to great advances in public health and medicine. The emergence of high-energy society, however, has brought with it a new set of health problems, within which the direct effects of measurable pollution may turn out to be more easily dealt with than some of the indirect and hard-to-calculate consequences of high energy use. High-energy society is critically dependent on energy-intensive transport systems, and these systems in turn are dependent upon a continual supply of petroleum products. In the short-term, the aorta of any industrialized nation is its petroleum-supply network. In the longer run, high-energy society faces the depletion and exhaustion of all the nonrenewable resources on which it has fed. Even if technology provides adequate substitute energy systems, high-energy society may deteriorate socially from inability to cope with affluence

  18. Corrosion aspects of high-level waste disposal in salt domes

    International Nuclear Information System (INIS)

    Roerbo, K.


    In the ELSAM/ELKRAT waste management project it is planned that the high-level waste is glassified, encapsuled in canisters and finally deposited in a deep hole drilled in a salt dome. In the present report corrosion aspects of the canisters after deposition are discussed. The chemical environment will probably be a limited amount of brine coming from brine inclusions in the surrounding salt and moving up against the temperature gradient, the temperature at the canister surface being in the range of 100-150degC. The possible types of corrosion and the expected corrosion rates for a number of potential canister materials (mild steel, austenitic and ferritic stainless steels, Ni-base alloys, copper, titanium and a few combinations of materials) are discussed. Mild steel (possibly combined with an inner layer of copper or titanium) might possibly be an appropriate choice of material for the canister. (author)

  19. Facile Route to Vertically Aligned High-Aspect Ratio Block Copolymer Films via Dynamic Zone Annealing (United States)

    Singh, Gurpreet; Kulkarni, Manish; Yager, Kevin; Smilgies, Detlef; Bucknall, David; Karim, Alamgir


    Directed assembly of block copolymers (BCP) can be used to fabricate a diversity of nanostructures useful for nanotech applications. The ability to vertically orient etchable high aspect ratio (˜30) ordered BCP domains on flexible substrates via continuous processing methods are particularly attractive for nanomanufacturing. We apply sharp dynamic cold zone annealing (CZA-S) to create etchable, and predominantly vertically oriented 30nm cylindrical domains in 1 μm thick poly(styrene-b-methylmethacrylate) films on low thermal conductivity rigid (quartz) and flexible (PDMS & Kapton) substrates. Under similar static conditions, temporally stable vertical cylinders form within a narrow zone above a critical temperature gradient. Primary ordering mechanism of CZA-S involves sweeping this vertically orienting zone created at maximum thermal gradient. An optimal speed is needed since the process competes with preferential surface wetting dynamics that favors parallel orientation. GISAXS of etched BCP films confirms internal morphology.

  20. High aspect ratio MEMS capacitor for high frequency impedance matching applications

    DEFF Research Database (Denmark)

    Yalcinkaya, Arda Deniz; Jensen, Søren; Hansen, Ole


    We present a microelectromechanical tunable capacitor with a low control voltage, a wide tuning range and adequate electrical quality factor. The device is fabricated in a single-crystalline silicon layer using deep reactive ion etching (DRIE) for obtaining high-aspect ratio (> 20) parallel comb......-drive structures with vertical sidewalls. The process sequence for fabrication of the devices uses only one lithographic masking step and can be completed in a short time. The fabricated device was characterized with respect to electrical quality factor, tuning range, self-resonance frequency and transient...... response and it was found that the device is a suitable passive component to be used in impedance matching applications, band-pass filtering or voltage controlled oscillators in the Very High Frequency (VHF) and Ultra High Frequency (UHF) bands....


    International Nuclear Information System (INIS)

    Pikin, A.


    Some applications of an Electron Beam Ion Source (EBIS) require intensities of highly charged ions significantly greater than those which have been achieved in present EBIS sources. For example, the ion source for the Relativistic Heavy Ion Collider (RHIC) at Brookhaven National Laboratory (BNL) must be capable of generating 3x10 9 ions of Au 35+ or 2 x 10 9 ions of U 45+ per pulse [1]. In this case, if the fraction of ions of interest is 20% of the total ion space charge, the total extracted charge is ∼∼ 5 x 10 11 . It is also desirable to extract these ions in a 10 ps pulse to allow single turn injection into the first synchrotron. Requirements for an EBIS which could meet the needs of the LHC at CERN are similar (∼ 1.5 x 10 9 ions of Pb 54+ in 5.5 micros). This charge yield is about an order of magnitude greater than that achieved in existing EBIS sources, and is what is meant here by ''high current''. This also implies, then, an EBIS with a high electron beam current. The scope of problems in a high current EBIS is broad, and includes generating a sufficient total charge of electrons in the volume of the ion trap, achieving a stable electron beam (without high frequency oscillations), preventing ions in the trap from acquiring too much energy (which can lead to a high rate of ion loss and increase in the emittance of the extracted ion beam), injection of metal ions into the ion trap, and achieving the appropriate vacuum in the ionization region. Development of the Electron Beam Test Stand (EBTS) at BNL addresses these problems, and is an attempt to develop the technologies relevant to a high current EBIS. The final goal of this development is to build an EBIS for RHIC. The general description of this project is published in [2]. In this chapter the discussion is limited to the handling of a high perveance electron beam and to vacuum issues

  2. Some Physical and Engineering Aspects of High Current EBIS

    International Nuclear Information System (INIS)

    Pikin, A; Prelec, K.


    Some applications of an Electron Beam Ion Source (EBIS) require intensities of highly charged ions significantly greater than those which have been achieved in present EBIS sources. For example, the ion source for the Relativistic Heavy Ion Collider (RHIC) at Brookhaven National Laboratory (BNL) must be capable of generating 3 x 10 9 ions of Au 35+ or 2 x 10 9 ions of U 45+ per pulse. In this case, if the fraction of ions of interest is 20% of the total ion space charge, the total extracted charge is approximately 5 x 10 11 . It is also desirable to extract these ions in a 10 micros pulse to allow single turn injection into the first synchrotrons. Requirements for an EBIS which could meet the needs of the LHC at CERN are similar (approximately 1.5 x 10 9 ions of Pb 54+ in 5.5 micros). This charge yield is about an order of magnitude greater than that achieved in existing EBIS sources, and is what is meant here by high current. This also implies, then, an EBIS with a high electron beam current

  3. Engineering and biotechnological aspects for the manufacturing of high quality fried potato products. (United States)

    Reimerdes, Ernst H; Franke, Knut


    Fried potato products have become very popular foods over the last decades. High quality standards have been established for these products by the food industry including uniform brown color and crispness. During frying, Maillard reactions takes place which contribute to color and taste development in these products. However, safety aspects are also influenced by these reactions, e.g., acrylamide formation. Maintaining high safety standards as well as the expected quality requires systematic research based on an integrated approach including all relevant variables, e.g., raw material properties, processing conditions and equipment concepts. Selected results of these investigations are presented and discussed, regarding influence of composition, e.g., precursor levels for Maillard reactions, treatment of raw materials and addition of reactants to frying fat. It has been demonstrated that a combined treatment of the potato sticks by coating of product surfaces and partial pre-drying can be successfully applied to produce well-browned French fries with lower acrylamide contents. Reductions up to 75% could be reached compared to samples without treatment. Furthermore, addition of a water/oil emulsion containing glutamine in the aqueous phase has been shown to influence Maillard reactions at the product surface, resulting in lower acrylamide contents at the same state of browning.

  4. Characterization of high surface area silicon oxynitrides

    International Nuclear Information System (INIS)

    Lednor, P.W.; DeRuiter, R.; Emeis, K.A.


    In heterogenous catalysis, liquid or gaseous feedstocks are converted over a solid catalyst into more desirable products. Such processes form an essential part of the oil and petrochemical industries. The solid catalyst usually consists of an inorganic phase, with or without metal particles on the surface. Examples include platinum particles on gamma alumina (a reforming catalyst used in oil processing), chromium particles on silica (an ethylene polymerization catalyst) and zeolites or amorphous silica-aluminas (used as solid acids).Oxides have been widely investigated in catalysis, and silica, alumina, and aluminosilicates find application commercially on a large scale. On the other hand, non-oxide materials such as nitrides, carbides and borides have been relatively little investigated. The main reason for this has been the lack of routes to the high surface area forms usually required in catalysis. However, this situation has changed significantly in recent years, due to the interest in high surface area non-oxides as precursors to fully dense ceramics; in this paper, the authors have reviewed synthetic routes to high surface area non-oxides

  5. High Surface Area Tunnels in Hexagonal WO₃. (United States)

    Sun, Wanmei; Yeung, Michael T; Lech, Andrew T; Lin, Cheng-Wei; Lee, Chain; Li, Tianqi; Duan, Xiangfeng; Zhou, Jun; Kaner, Richard B


    High surface area in h-WO3 has been verified from the intracrystalline tunnels. This bottom-up approach differs from conventional templating-type methods. The 3.67 Å diameter tunnels are characterized by low-pressure CO2 adsorption isotherms with nonlocal density functional theory fitting, transmission electron microscopy, and thermal gravimetric analysis. These open and rigid tunnels absorb H(+) and Li(+), but not Na(+) in aqueous electrolytes without inducing a phase transformation, accessing both internal and external active sites. Moreover, these tunnel structures demonstrate high specific pseudocapacitance and good stability in an H2SO4 aqueous electrolyte. Thus, the high surface area created from 3.67 Å diameter tunnels in h-WO3 shows potential applications in electrochemical energy storage, selective ion transfer, and selective gas adsorption.

  6. International aspects of high-temperature reactor development

    International Nuclear Information System (INIS)

    Balthesen, E.


    The development of high-temperature reactor technology is under way in the Federal Republic of Germany, the United States, the Soviet Union and Japan. Access of nuclear energy to the heat market is the common goal in the long run. HTR applications for oil recovery and refining are under investigation in the Republic of China. The German pebble-bed reactor concept is beginning to be accepted worldwide. Due to extensive development work, market maturity for the technology for electricity and process-steam production has been achieved in the Federal Republic. (orig.) [de

  7. Present status and future aspects of highly precise radiotherapy

    International Nuclear Information System (INIS)

    Oita, Masataka; Takegawa, Yoshihiro; Maezawa, Hiroshi; Ikushima, Hitoshi; Osaki, Kyosuke; Nishitani, Hiromu


    This review describes about therapeutic equipments, irradiation technology, actual practice of highly precise radiotherapy (RT) and its tasks in future. Development of radiation equipments has made the therapy highly precise. At present, there are reportedly 836 linacs and 23 microtrons in Japan (March, 2005), most of which are computerized, new generation equipments. Image-guided RT, CT-linac system, real-time tumor-tracking RT (RTRT), tomotherapy and cyberknife are introduced owing to development of concerned devices and equipments. In addition, there are 7 facilities with proton and/or heavy ion beams. In parallel with the machine development above, irradiation has become to that from 2D to 3D by multi-gate technique with use of multi-leaf collimator and intensity-modulated RT is introduced. RTRT is an example of 4D RT. Practically, stereotactic irradiation (STI) to brain tumor has resulted in 1-year cumulative survival rate of 58% in 16 cases (23 foci, median size 1.2 cm and volume 0.57 ml) with median dose of 21.0 Gy in authors' hospital. STI in the early stage lung cancers is also practically conducted without severe adverse effects. Future tasks involve the further development of irradiation techniques and RT planning, QA/QC system, and raising of experts in related fields, which is a national problem. (T.I.)

  8. Physical aspects of mercury-free high pressure discharge lamps

    International Nuclear Information System (INIS)

    Born, M.


    This paper gives a summary of recent results about the replacement of mercury in high pressure discharge lamps by metallic zinc. Actually, this topic is of high relevance for the lighting industry due to the need of more environmentally friendly products. The work presented here is supported by the German government under contract no. 13N8072. Pure zinc/argon discharges as well as lamps including zinc or mercury and metal halide additives are investigated. Experimental data are compared with model calculations of the energy balance involving the transport of heat and radiation. Since the excitation energies of relevant zinc transistions are lower than for mercury, axis temperatures of pure zinc lamps are about 300 K below the value of mercury arcs. In addition, the thermal conductivity of zinc including the contribution of radiation diffusion is larger than compared to mercury. From lamp voltage measurements it is found that the cross section for elastical electron scattering by zinc atoms is about the same as for mercury. When adding metal halides to a pure zinc discharge with argon as a starting gas, i.e. NaI, TlI, DyI3, axis temperatures decrease to about 5100 K due to strong radiation cooling. In order to obtain sufficiently large lamp voltages, wall temperatures of more than 1300 K are adjusted by means of polycrystalline aluminaoxide (Al2O3) as a wall material. Electrical field strenghts of 6.0 V/mm and 8.6 V/mm are measured for metal halide lamps containing zinc or mercury, respectively. The light technical data of the discharges are very close, since mercury and zinc do not contribute significantly to the radiation in the visible range. Efficacies of up to 93 lm/W and 100 lm/W are found in metal halide lamps with zinc and mercury, respectively. Consequently, zinc turns out to be an attractive replacer for mercury in this type of lamp not only from an environmental point of view

  9. High surface area electrode for high efficient microbial electrosynthesis (United States)

    Nie, Huarong; Cui, Mengmeng; Lu, Haiyun; Zhang, Tian; Russell, Thomas; Lovley, Derek


    Microbial electrosynthesis, a process in which microorganisms directly accept electrons from an electrode to convert carbon dioxide and water into multi carbon organic compounds, affords a novel route for the generation of valuable products from electricity or even wastewater. The surface area of the electrode is critical for high production. A biocompatible, highly conductive, three-dimensional cathode was fabricated from a carbon nanotube textile composite to support the microorganism to produce acetate from carbon dioxide. The high surface area and macroscale porous structure of the intertwined CNT coated textile ?bers provides easy microbe access. The production of acetate using this cathode is 5 fold larger than that using a planar graphite electrode with the same volume. Nickel-nanowire-modified carbon electrodes, fabricated by microwave welding, increased the surface area greatly, were able to absorb more bacteria and showed a 1.5 fold increase in performance

  10. Some aspects of ultra high energy gamma ray astronomy

    International Nuclear Information System (INIS)

    De Jager, O.C.


    A short review of ultra high energy (UHE) gamma ray astronomy (10 11 14 eV) as well as a description of a planned experiment to be erected at Potchefstroom is given in the introduction. This experiment will be the first and only one in the Southern Hemisphere and as such may play an important role in this new field of astronomy and astrophysics. In the first part the necessary infrastructure for astronomical observations of known celestial objects is developed. This embodies the special physical, mechanical and astronomical constraints in this type of astronomy, such as the definition of the various astronomical coordinate systems and transformations between them, the effect of precession and nutation on the source position etc. This leads to automatic observation schedules for the various applicable techniques of observation. In the second part the various effects which may influence the arrival time of a gamma ray at the telescope is investigated. It is found that dispersion and relativistic effects are negligible, given the special type of analysis used in this low counting rate system. The classic Doppler effect due to the motion of Earth as well as the configuration of the telescope does have a major effect and must be taken into consideration when analysing the data. A simple method, depending only on the movement of Earth around the sun, is developed to simplify the identification of pulsars at the planned observatory where computing facilities are limited

  11. Theoretical aspects of electronic structure of high Tc superconductors

    International Nuclear Information System (INIS)

    Gupta, R.P.


    Although the mechanism responsible for the high T c superconductivity is still unknown, it is nevertheless clear that superconductivity in hole doped materials depends sensitively on the number of holes, C h , per CuO 2 plane. A correlation between C h and T c has been established. In this paper we present several examples of the critical dependence of the charge transfer and thus the value of C h on the cristallographic characteristics. For example, our electronic structure investigations of YBa 2 Cu 3 O 6.5 using several configurations of the oxygen atoms on the chains show that the order-disorder phenomena of the oxygen atoms play a crucial role on the value of C h and T c . We have also studied the variation of the charge transfer and C h as a function of hydrostatic pressure for several cuprates: La 1.85 Sr 0.15 CuO 4 (ΔT c /Δp ∼ 0.3 - 0.4 K/kbar); YBa 2 Cu 4 O 8 (ΔT c /Δp ∼ 5.5 K/kbar). We show that the values of C h increase under pressure [fr

  12. Mechanistic Aspects in the Formation, Growth and Surface Functionalization of Metal Oxide Nanoparticles in Organic Solvents. (United States)

    Deshmukh, Rupali; Niederberger, Markus


    The synthesis of metal oxide nanoparticles in organic solvents, so-called nonaqueous (or nonhydrolytic) processes represent powerful alternatives to aqueous approaches and have become an independent research field. 10 Years ago, when we published our first review on organic reaction pathways in nonaqueous sol-gel approaches, the number of examples was relatively limited. Nowadays, it is almost impossible to provide an exhaustive overview. Here we review the development of the last few years, without neglecting pioneering examples, which help to follow the historical development. The importance of a profound understanding of mechanistic aspects of nanoparticle crystallization and formation mechanisms can't be overestimated, when it comes to the design of rational synthesis concepts under minimization of trial-and-error experiments. The main reason for the progress in mechanistic understanding lies in the availability of characterization tools that make it possible to monitor chemical reactions from the dissolution of the precursor to the nucleation and growth of the nanoparticles, by ex situ methods involving sampling after different reaction times, but more and more also by in situ studies. After a short introduction to experimental aspects of nonaqueous sol-gel routes to metal oxide nanoparticles, we provide an overview of the main and basic organic reaction pathways in these approaches. Afterwards, we summarize the main characterization methods to study formation mechanisms, and then we discuss in great depth the chemical formation mechanisms of many different types of metal oxide nanoparticles. The review concludes with a paragraph on selected crystallization mechanisms reported for nonaqueous systems and a few illustrative examples of nonaqueous sol-gel concepts applied to surface chemistry. © 2017 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

  13. The black silicon method VI: high aspect ratio trench etching for MEMS applications

    NARCIS (Netherlands)

    Jansen, Henricus V.; de Boer, Meint J.; Elwenspoek, Michael Curt


    Etching high aspect ratio trenches (HART's) in silicon is becoming increasingly important for MEMS applications. Currently, the most important technique is dry reactive ion etching (RIE). This paper presents solutions for the most notorious problems during etching HART's: tilting and the aspect


    Directory of Open Access Journals (Sweden)

    G. D. Liakhevich


    Full Text Available In Belarus concrete with strength up to 60 MPA is used for construction. At the same time high strength concrete with compressive strength above 60 MPA is widely used in all industrially developed countries. High- strength concrete is included in regulatory documents of the European Union and that fact has laid a solid foundation for its application. High strength concrete is produced using highly dispersed silica additives, such as micro-silica and plasticizers (super-plasticizers with a water/cement (w/c ratio not greater than 0.4.Theoretical aspects of high-strength concrete for bridge structures have been studied in the paper. The paper shows a positive impact of highly dispersed additives on structure and physico-mechanical properties of cement compositions, namely: reduction of total porosity of a cement stone in concrete while increasing volumetric concentration and dispersion of a filler; binding of calcium hydroxide with the help of amorphised micro-silica; increased activity of mineral additives during their thin shredding; acceleration of the initial stage of chemical hardening of cement compositions with highly dispersed particle additives that serve as centers of crystallization; “binder-additive” cluster formation due to high surface energy of highly dispersed additive particles; hardening of surface area between a cement stone and aggregates in concrete; high-strength concretes are gaining strength much faster than conventional concretes.Technology of preparation and composition of high-strength concrete using highly dispersed mineral additives and super-plasticizer has been developed in the paper. This concrete will ensure a higher density, wa- ter-and gas tightness, increased resistance to aggressive environment, reduced consumption of concrete and reinforcement, reduced transport and installation weight, increased initial strength, early easing of shutters and preliminary compression, increased length of bridge spans

  15. Localized mold heating with the aid of selective induction for injection molding of high aspect ratio micro-features

    International Nuclear Information System (INIS)

    Park, Keun; Lee, Sang-Ik


    High-frequency induction is an efficient, non-contact means of heating the surface of an injection mold through electromagnetic induction. Because the procedure allows for the rapid heating and cooling of mold surfaces, it has been recently applied to the injection molding of thin-walled parts or micro/nano-structures. The present study proposes a localized heating method involving the selective use of mold materials to enhance the heating efficiency of high-frequency induction heating. For localized induction heating, a composite injection mold of ferromagnetic material and paramagnetic material is used. The feasibility of the proposed heating method is investigated through numerical analyses in terms of its heating efficiency for localized mold surfaces and in terms of the structural safety of the composite mold. The moldability of high aspect ratio micro-features is then experimentally compared under a variety of induction heating conditions.

  16. Trends in Surface Temperature at High Latitudes (United States)

    Comiso, Josefino C.


    The earliest signal of a climate change is expected to be found in the polar regions where warming is expected to be amplified on account of ice-albedo feedbacks associated with the high reflectivity of snow and ice. Because of general inaccessibility, there is a general paucity of in situ data and hence the need to use satellite data to observe the large-scale variability and trends in surface temperature in the region. Among the most important sensors for monitoring surface temperature has been the Advanced Very High Resolution Radiometer (AVHRR) which was first launched in 1978 and has provided continuous thermal infrared data since 1981. The top of the atmosphere data are converted to surface temperature data through various schemes that accounts for the unique atmospheric and surface conditions in the polar regions. Among the highest source of error in the data is cloud masking which is made more difficult in the polar region because of similar Signatures of clouds and snow lice covered areas. The availability of many more channels in the Moderate Resolution Imaging Spectroradiometer (MODIS) launched on board Terra satellite in December 1999 and on board Aqua in May 2002 (e.g., 36 visible and infrared channels compared to 5 for AVHRR) made it possible to minimize the error. Further capabilities were introduced with the Advanced Microwave Scanning Radiometer (AMSR) which has the appropriate frequency channels for the retrieval of sea surface temperature (SST). The results of analysis of the data show an amplified warming in the Arctic region, compared with global warming. The spatial distribution of warming is, however, not uniform and during the last 3 decades, positive temperature anomalies have been most pronounced in North America, Greenland and the Arctic basin. Some regions of the Arctic such as Siberia and the Bering Sea surprisingly show moderate cooling but this may be because these regions were anomalously warm in the 1980s when the satellite record

  17. High surface area fibrous silica nanoparticles

    KAUST Repository

    Polshettiwar, Vivek


    Disclosed are high surface area nanoparticles that have a fibrous morphology. The nanoparticles have a plurality of fibers, wherein each fiber is in contact with one other fiber and each fiber has a length of between about 1 nm and about 5000 nm. Also disclosed are applications of the nanoparticles of the present invention, and methods of fabrication of the nanoparticles of the present invention.

  18. Aspect Ratio Scaling of Ideal No-wall Stability Limits in High Bootstrap Fraction Tokamak Plasmas

    International Nuclear Information System (INIS)

    Menard, J.E.; Bell, M.G.; Bell, R.E.; Gates, D.A.; Kaye, S.M.; LeBlanc, B.P.; Maingi, R.; Sabbagh, S.A.; Soukhanovskii, V.; Stutman, D.


    Recent experiments in the low aspect ratio National Spherical Torus Experiment (NSTX) [M. Ono et al., Nucl. Fusion 40 (2000) 557] have achieved normalized beta values twice the conventional tokamak limit at low internal inductance and with significant bootstrap current. These experimental results have motivated a computational re-examination of the plasma aspect ratio dependence of ideal no-wall magnetohydrodynamic stability limits. These calculations find that the profile-optimized no-wall stability limit in high bootstrap fraction regimes is well described by a nearly aspect ratio invariant normalized beta parameter utilizing the total magnetic field energy density inside the plasma. However, the scaling of normalized beta with internal inductance is found to be strongly aspect ratio dependent at sufficiently low aspect ratio. These calculations and detailed stability analyses of experimental equilibria indicate that the nonrotating plasma no-wall stability limit has been exceeded by as much as 30% in NSTX in a high bootstrap fraction regime

  19. Key Techniques on Preparing High Aspect Ratio Micro and Nano Structures

    DEFF Research Database (Denmark)

    Jian, Zhao; Lianhe, Dong; Xiaoli, Zhu


    effectively. The mechanism of action between NaCl and HSQ was analyzed. The collapse and adhesion of resist structure due to the effect of gas-liquid interfacial capillary surface tension were suppressed by the CO2 supercritical drying method. Large-area dense nano-structures with the aspect ratio of 12...

  20. Synthesis of high aspect ratio ZnO nanowires with an inexpensive handcrafted electrochemical setup

    Energy Technology Data Exchange (ETDEWEB)

    Taheri, Ali, E-mail:, E-mail: [Nuclear Science and Technology Institute (Iran, Islamic Republic of); Saramad, Shahyar; Setayeshi, Saeed [Amirkabir University of Technology, Faculty of Energy Engineering and Physics (Iran, Islamic Republic of)


    In this work, high aspect ratio zinc oxide nanowires are synthesized using templated one-step electrodeposition technique. Electrodeposition of the nanowires is done using a handcrafted electronic system. Nuclear track-etched polycarbonate membrane is used as a template to form the high aspect ratio nanowires. The result of X-ray diffraction and scanning electron microscopy shows that nanowires with a good crystallinity and an aspect ratio of more than 30 can be achieved in a suitable condition. The height of electrodeposited nanowires reaches to about 11 μm. Based on the obtained results, high aspect ratio ZnO nanowires can be formed using inexpensive electrodeposition setup with an acceptable quality.

  1. Atomic Layer Deposition for Coating of High Aspect Ratio TiO2 Nanotube Layers (United States)


    We present an optimized approach for the deposition of Al2O3 (as a model secondary material) coating into high aspect ratio (≈180) anodic TiO2 nanotube layers using the atomic layer deposition (ALD) process. In order to study the influence of the diffusion of the Al2O3 precursors on the resulting coating thickness, ALD processes with different exposure times (i.e., 0.5, 2, 5, and 10 s) of the trimethylaluminum (TMA) precursor were performed. Uniform coating of the nanotube interiors was achieved with longer exposure times (5 and 10 s), as verified by detailed scanning electron microscopy analysis. Quartz crystal microbalance measurements were used to monitor the deposition process and its particular features due to the tube diameter gradient. Finally, theoretical calculations were performed to calculate the minimum precursor exposure time to attain uniform coating. Theoretical values on the diffusion regime matched with the experimental results and helped to obtain valuable information for further optimization of ALD coating processes. The presented approach provides a straightforward solution toward the development of many novel devices, based on a high surface area interface between TiO2 nanotubes and a secondary material (such as Al2O3). PMID:27643411

  2. High-Speed Additive Manufacturing Through High-Aspect-Ratio Nozzles (United States)

    Shaw, Leon; Islam, Mashfiqul; Li, Jie; Li, Ling; Ayub, S. M. Imran


    The feasibility of layer-by-layer manufacturing through high-aspect-ratio (HAR) nozzles for microextrusion of paste to deposit planes has been investigated. Various conditions for paste extrusion, including nozzle moving speed, piston speed, extrusion rate, and distance between the nozzle tip and substrate, have been evaluated. By linking various microextrusion parameters together with the aid of a critical distance concept derived from microextrusion using circular nozzles and addressing the extrusion delay in response to the change of the piston speed and air pocket problems properly, we successfully microextruded single planes, multilayer objects, and larger planes made of multiple smaller planes side by side through HAR nozzles. It is further demonstrated that the X-Y dimensions of an extruded plane in the steady-state extrusion stage are determined by the nozzle travel distance and the length of the HAR nozzle opening if microextrusion is conducted with proper conditions. However, the height of the extruded plane is not only determined by the microextrusion conditions, but also affected by the drying shrinkage of the paste after microextrusion. This demonstration of the feasibility of using a HAR nozzle machine opens the door to manufacture of multimaterial, multilayer devices with high productivity in the near future.

  3. High-Speed Additive Manufacturing Through High-Aspect-Ratio Nozzles (United States)

    Shaw, Leon; Islam, Mashfiqul; Li, Jie; Li, Ling; Ayub, S. M. Imran


    The feasibility of layer-by-layer manufacturing through high-aspect-ratio (HAR) nozzles for microextrusion of paste to deposit planes has been investigated. Various conditions for paste extrusion, including nozzle moving speed, piston speed, extrusion rate, and distance between the nozzle tip and substrate, have been evaluated. By linking various microextrusion parameters together with the aid of a critical distance concept derived from microextrusion using circular nozzles and addressing the extrusion delay in response to the change of the piston speed and air pocket problems properly, we successfully microextruded single planes, multilayer objects, and larger planes made of multiple smaller planes side by side through HAR nozzles. It is further demonstrated that the X- Y dimensions of an extruded plane in the steady-state extrusion stage are determined by the nozzle travel distance and the length of the HAR nozzle opening if microextrusion is conducted with proper conditions. However, the height of the extruded plane is not only determined by the microextrusion conditions, but also affected by the drying shrinkage of the paste after microextrusion. This demonstration of the feasibility of using a HAR nozzle machine opens the door to manufacture of multimaterial, multilayer devices with high productivity in the near future.

  4. High-aspect ratio micro- and nanostructures enabled by photo-electrochemical etching for sensing and energy harvesting applications (United States)

    Alhalaili, Badriyah; Dryden, Daniel M.; Vidu, Ruxandra; Ghandiparsi, Soroush; Cansizoglu, Hilal; Gao, Yang; Saif Islam, M.


    Photo-electrochemical (PEC) etching can produce high-aspect ratio features, such as pillars and holes, with high anisotropy and selectivity, while avoiding the surface and sidewall damage caused by traditional deep reactive ion etching (DRIE) or inductively coupled plasma (ICP) RIE. Plasma-based techniques lead to the formation of dangling bonds, surface traps, carrier leakage paths, and recombination centers. In pursuit of effective PEC etching, we demonstrate an optical system using long wavelength (λ = 975 nm) infra-red (IR) illumination from a high-power laser (1-10 W) to control the PEC etching process in n-type silicon. The silicon wafer surface was patterned with notches through a lithography process and KOH etching. Then, PEC etching was introduced by illuminating the backside of the silicon wafer to enhance depth, resulting in high-aspect ratio structures. The effect of the PEC etching process was optimized by varying light intensities and electrolyte concentrations. This work was focused on determining and optimizing this PEC etching technique on silicon, with the goal of expanding the method to a variety of materials including GaN and SiC that are used in designing optoelectronic and electronic devices, sensors and energy harvesting devices.

  5. Large-area, high-aspect-ratio SU-8 molds for the fabrication of PDMS microfluidic devices

    International Nuclear Information System (INIS)

    Natarajan, S; Chang-Yen, D A; Gale, B K


    A relatively low-cost fabrication method using soft lithography and molding for large-area, high-aspect-ratio microfluidic devices, which have traditionally been difficult to fabricate, has been developed and is presented in this work. The fabrication process includes novel but simple modifications of conventional microfabrication steps and can be performed in any standard microfabrication facility. Specifically, the fabrication and testing of a microfluidic device for continuous flow deposition of bio-molecules in an array format are presented. The array layout requires high-aspect-ratio elastomeric channels that are 350 µm tall, extend more than 10 cm across the substrate and are separated by as little as 20 µm. The mold from which these channels were fabricated consisted of high-quality, 335 µm tall SU-8 structures with a high-negative aspect ratio of 17 on a 150 mm silicon wafer and was produced using spin coating and UV-lithography. Several unique processing steps are introduced into the lithographic patterning to eliminate many of the problems experienced when fabricating tall, high-aspect-ratio SU-8 structures. In particular, techniques are used to ensure uniform molds, both in height and quality, that are fully developed even in the deep negative-aspect-ratio areas, have no leftover films at the top of the structures caused by overexposure and no bowing or angled sidewalls from diffraction of the applied UV light. Successful microfluidic device creation was demonstrated using these molds by casting, curing and bonding a polydimethylsiloxane (PDMS) elastomer. A unique microfluidic device, requiring these stringent geometries, for continuous flow printing of a linear array of 16 protein and antibody spots has been demonstrated and validated by using surface plasmon resonance imaging of printed arrays

  6. Recycling of water of high pressure cleaning of pipes. Phase 1. Quality demands and economical aspects

    International Nuclear Information System (INIS)

    Van Weers, A.W.; Zwaard, J.


    According to the regulation 6.1 in the current licence Surface Water Pollution Law (WVO, abbreviated in Dutch) of October 10, 1997, ECN carried out the first phase of a study on the title subject with respect to pipes applied in oil and gas exploration. In the present situation water of the so-called pipe-cleaner is transported via a seapipe after precipitation and membrane filtration. Next to the quality demands and economical aspects attention is paid to a number of environmental aspects

  7. High aspect ratio silver grid transparent electrodes using UV embossing process (United States)

    Kim, Dong Jin; Lim, Mikyung; Lee, Seung S.; Kim, Jin-Ha


    This study presents a UV embossing process to fabricate high aspect ratio silver grid transparent electrodes on a polymer film. Transparent electrodes with a high optical transmittance (93 %) and low sheet resistance (4.6 Ω/sq) were fabricated without any high temperature or vacuum processes. The strong adhesion force between the UV resin and the silver ink enables the fabrication of silver microstructures with an aspect ratio higher than 3. The high aspect ratio results in a low sheet resistance while maintaining a high optical transmittance. Multi-layer transparent electrodes were fabricated by repeating the proposed UV process. Additionally, a large-area of 8-inch touch panel was fabricated with the proposed UV process. The proposed UV process is a relatively simple and low cost process making it suitable for large-area production as well as mass production.

  8. High aspect ratio silver grid transparent electrodes using UV embossing process

    Directory of Open Access Journals (Sweden)

    Dong Jin Kim


    Full Text Available This study presents a UV embossing process to fabricate high aspect ratio silver grid transparent electrodes on a polymer film. Transparent electrodes with a high optical transmittance (93 % and low sheet resistance (4.6 Ω/sq were fabricated without any high temperature or vacuum processes. The strong adhesion force between the UV resin and the silver ink enables the fabrication of silver microstructures with an aspect ratio higher than 3. The high aspect ratio results in a low sheet resistance while maintaining a high optical transmittance. Multi-layer transparent electrodes were fabricated by repeating the proposed UV process. Additionally, a large-area of 8-inch touch panel was fabricated with the proposed UV process. The proposed UV process is a relatively simple and low cost process making it suitable for large-area production as well as mass production.

  9. Leptothrix sp sheaths modified with iron oxide particles: Magnetically responsive, high aspect ratio functional material

    Czech Academy of Sciences Publication Activity Database

    Šafařík, Ivo; Angelova, R.; Baldíková, Eva; Pospišková, K.; Šafaříková, Miroslava


    Roč. 71, FEB (2017), s. 1342-1346 ISSN 0928-4931 R&D Projects: GA ČR(CZ) GA14-11516S; GA MŠk(CZ) LD14075 Institutional support: RVO:67179843 Keywords : removal * Leptothrix * Magnetic modification * Iron oxide * High aspect ratio material Subject RIV: EI - Biotechnology ; Bionics OBOR OECD: Environmental science s (social aspects to be 5.7) Impact factor: 4.164, year: 2016

  10. Fabrication of ultra-high aspect ratio (>160:1) silicon nanostructures by using Au metal assisted chemical etching (United States)

    Li, Hailiang; Ye, Tianchun; Shi, Lina; Xie, Changqing


    We present a facile and effective approach for fabricating high aspect ratio, dense and vertical silicon nanopillar arrays, using a combination of metal etching following electron-beam lithography and Au metal assisted chemical etching (MacEtch). Ti/Au nanostructures used as catalysts in MacEtch are formed by single layer resist-based electron-beam exposure followed by ion beam etching. The effects of MacEtch process parameters, including half period, etching time, the concentrations of H2O2 and HF, etching temperature and drying method are systematically investigated. Especially, we demonstrate an enhancement of etching quality by employing cold MacEtch process, and an enhancement in preventing the collapse of high aspect ratio nanostructures by employing low surface tension rinse liquid and natural evaporation in the drying stage. Using an optimized MacEtch process, vertical silicon nanopillar arrays with a period of 250 nm and aspect ratio up to 160:1 are realized. Our results should be instructive for exploring the achievable aspect ratio limit in silicon nanostructures and may find potential applications in photovoltaic devices, thermoelectric devices and x-ray diffractive optics.

  11. An overview of the reliability prediction related aspects of high power IGBTs in wind power applications

    DEFF Research Database (Denmark)

    Busca, Christian; Teodorescu, Remus; Blaabjerg, Frede


    Reliability is becoming more and more important as the size and number of installed Wind Turbines (WTs) increases. Very high reliability is especially important for offshore WTs because the maintenance and repair of such WTs in case of failures can be very expensive. WT manufacturers need...... to consider the reliability aspect when they design new power converters. By designing the power converter considering the reliability aspect the manufacturer can guarantee that the end product will ensure high availability. This paper represents an overview of the various aspects of reliability prediction...... of high power Insulated Gate Bipolar Transistors (IGBTs) in the context of wind power applications. At first the latest developments and future predictions about wind energy are briefly discussed. Next the dominant failure mechanisms of high power IGBTs are described and the most commonly used lifetime...

  12. Aspects of artificial neural networks - with applications in high energy physics

    International Nuclear Information System (INIS)

    Roegnvaldsson, T.S.


    Different aspects of artificial neural networks are studied and discussed. They are demonstrated to be powerful general purpose algorithms, applicable to many different problem areas like pattern recognition, function fitting and prediction. Multi-layer perceptron (MPL) models are shown to out perform previous standard approaches on both off-line and on-line analysis tasks in high energy physics, like quark flavour tagging and mass reconstruction, as well as being powerful tools for prediction tasks. It is also demonstrated how a self-organizing network can be employed to extract information from data, for instance to track down origins of unexpected model discrepancies. Furthermore, it is proved that the MPL is more efficient than the learning vector quantization technique on classification problems, by producing smoother discrimination surfaces, and that an MPL network should be trained with a noisy updating schedule if the Hessian is ill-conditioned - A result that is especially important for MPL network with more than just one hidden layer. 81 refs, 6 figs

  13. Formation of high aspect ratio polyamide-6 nanofibers via electrically induced double layer during electrospinning

    International Nuclear Information System (INIS)

    Nirmala, R.; Nam, Ki Taek; Park, Soo-Jin; Shin, Yu-Shik; Navamathavan, R.; Kim, Hak Yong


    In the present study, the formation of high aspect ratio nanofibers in polyamide-6 was investigated as a function of applied voltage ranging from 15 to 25 kV using electrospinning technique. All other experimental parameters were kept constant. The electrospun polyamide-6 nanofibers were characterized by field-emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and matrix-assisted laser desorption ionization time-of-flight (MALDI-TOF). FE-SEM images of polyamide-6 nanofibers showed that the diameter of the electrospun fiber was decreased with increasing applied voltage. At the critical applied voltage, the polymer solution was completely ionized to form the dense high aspect ratio nanofibers in between the main nanofibers. The diameter of the polyamide-6 nanofibers was observed to be in the range of 75-110 nm, whereas the high aspect ratio structures consisted of regularly distributed very fine nanofibers with diameters of about 9-28 nm. Trends in fiber diameter and diameter distribution were discussed for the high aspect ratio nanofibers. TEM results revealed that the formation of double layers in polyamide-6 nanofibers and then split-up into ultrafine fibers. The electrically induced double layer in combination with the polyelectrolytic nature of solution is proposed as the suitable mechanisms for the formation of high aspect ratio nanofibers in polyamide-6.

  14. Turbulent Flow past High Temperature Surfaces (United States)

    Mehmedagic, Igbal; Thangam, Siva; Carlucci, Pasquale; Buckley, Liam; Carlucci, Donald


    Flow over high-temperature surfaces subject to wall heating is analyzed with applications to projectile design. In this study, computations are performed using an anisotropic Reynolds-stress model to study flow past surfaces that are subject to radiative flux. The model utilizes a phenomenological treatment of the energy spectrum and diffusivities of momentum and heat to include the effects of wall heat transfer and radiative exchange. The radiative transport is modeled using Eddington approximation including the weighted effect of nongrayness of the fluid. The time-averaged equations of motion and energy are solved using the modeled form of transport equations for the turbulence kinetic energy and the scalar form of turbulence dissipation with an efficient finite-volume algorithm. The model is applied for available test cases to validate its predictive capabilities for capturing the effects of wall heat transfer. Computational results are compared with experimental data available in the literature. Applications involving the design of projectiles are summarized. Funded in part by U.S. Army, ARDEC.

  15. Water evaporation on highly viscoelastic polymer surfaces. (United States)

    Pu, Gang; Severtson, Steven J


    Results are reported for a study on the evaporation of water droplets from a highly viscoelastic acrylic polymer surface. These are contrasted with those collected for the same measurements carried out on polydimethylsiloxane (PDMS). For PDMS, the evaporation process involves the expected multistep process including constant drop area, constant contact angle, and finally a combination of these steps until the liquid is gone. In contrast, water evaporation from the acrylic polymer shows a constant drop area mode throughout. Furthermore, during the evaporation process, the drop area actually expands on the acrylic polymer. The single mode evaporation process is consistent with formation of wetting structures, which cannot be propagated by the capillary forces. Expansion of the drop area is attributed to the influence of the drop capillary pressure. Furthermore, the rate of drop area expansion is shown to be dependent on the thickness of the polymer film.

  16. High aspect ratio PDMS replication through proton beam fabricated Ni masters

    International Nuclear Information System (INIS)

    Kan, J.A. van; Wang, L.P.; Shao, P.G.; Bettiol, A.A.; Watt, F.


    In application areas where multiple samples are required (for example tissue engineering substrates), proton beam writing (PBW) is a suitable technique to fabricate high quality metal masters. These masters can then be used to replicate multiple copies in polymers, either through nanoimprinting or softlithography. Since poly(dimethyl siloxane) (PDMS) is a compatible material in tissue engineering we explore PDMS casting on Ni masters as an alternative way to replicate high aspect ratio micro structures. Ni masters with grooves spaced 2.5 μm apart, and 13 μm deep were successfully replicated in PDMS: These PDMS structures, which have aspect ratio of more than 5, are comparable to the best high aspect ratios reported in PDMS replication

  17. The Surface Chemical Properties of Novel High Surface Area Solids ...

    African Journals Online (AJOL)

    during zeolite synthesis.22 Because raw fly ash has large quanti- ties of a host of elements, many of these will act as nucleation sites, which results in many small crystals rather than a few large ones. Acid etching removed the needle-like structures on the particle surfaces, revealing a porous underlying structure. (Fig. 1c).

  18. Highly Manufacturable Deep (Sub-Millimeter) Etching Enabled High Aspect Ratio Complex Geometry Lego-Like Silicon Electronics

    KAUST Repository

    Ghoneim, Mohamed T.


    A highly manufacturable deep reactive ion etching based process involving a hybrid soft/hard mask process technology shows high aspect ratio complex geometry Lego-like silicon electronics formation enabling free-form (physically flexible, stretchable, and reconfigurable) electronic systems.

  19. Characterization and anti-settlement aspects of surface micro-structures from Cancer pagurus

    International Nuclear Information System (INIS)

    Sullivan, T; Regan, F; McGuinness, K; Connor, N E O’


    Tuning surface and material properties to inhibit or prevent settlement and attachment of microorganisms is of interest for applications such as antifouling technologies. Here, optimization of nano- and microscale structures on immersed surfaces can be utilized to improve cell removal while reducing adhesion strength and the likelihood of initial cellular attachment. Engineered surfaces capable of controlling cellular behaviour under natural conditions are challenging to design due to the diversity of attaching cell types in environments such as marine waters, where many variations in cell shape, size and adhesion strategy exist. Nevertheless, understanding interactions between a cell and a potential substrate for adhesion, including topographically driven settlement cues, offers a route to designing surfaces capable of controlling cell settlement. Biomimetic design of artificial surfaces, based upon microscale features from natural surfaces, can be utilized as model surfaces to understand cell–surface interactions. The microscale surface features of the carapace from the crustacean Cancer pagurus has been previously found to influence the rate of attachment of particular organisms when compared to smooth controls. However, the nature of microscale topographic features from C. pagurus have not been examined in sufficient detail to allow design of biomimetic surfaces. In this work, the spatial distribution, chemical composition, size and shape descriptors of microscale surface features from C. pagurus are characterized in detail for the first time. Additionally, the influence of topography from C. pagurus on the settlement of marine diatoms is examined under field conditions. (paper)

  20. Practical aspects of spherical near-field antenna measurements using a high-order probe

    DEFF Research Database (Denmark)

    Laitinen, Tommi; Pivnenko, Sergey; Nielsen, Jeppe Majlund


    Two practical aspects related to accurate antenna pattern characterization by probe-corrected spherical near-field antenna measurements with a high-order probe are examined. First, the requirements set by an arbitrary high-order probe on the scanning technique are pointed out. Secondly, a channel...... balance calibration procedure for a high-order dual-port probe with non-identical ports is presented, and the requirements set by this procedure for the probe are discussed....

  1. BisGMA/TEGDMA dental composite containing high aspect-ratio hydroxyapatite nanofibers (United States)

    Chen, Liang; Yu, Qingsong; Wang, Yong; Li, Hao


    Objectives The objectives of this study are to investigate the properties of high aspect-ratio hydroxyapatite (HAP) nanofibers and the reinforcing effect of such fibers on bisphenol A glycidyl methacrylate (BisGMA)/triethylene glycol dimethacrylate (TEGDMA) dental resins (without silica microparticle filler) and dental composites (with silica microparticle filler) with various mass fractions (loading rates). Methods HAP nanofibers were synthesized using a wet-chemical method and characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), and thermal gravimetric analysis (TGA). Biaxial flexural strength (BFS) of the HAP nanofibers reinforced dental resins without any microsized filler and dental composites with silica microparticle filler was tested and analysis of variance (ANOVA) was used for the statistically analysis of acquired data. The morphology of fracture surface of tested dental composite samples was examined by SEM. Results The HAP nanofibers with aspect-ratios of 600 to 800 can be successfully fabricated with a simple wet-chemical method in aqueous solution. Impregnation of small mass fractions of the HAP nanofibers (5 wt% or 10 wt%) into the BisGMA/TEGDMA dental resins or impregnation of small mass fractions of the HAP nanofibers (2 wt% or 3 wt%) into the dental composites can substantially improve the biaxial flexural strength of the resulting dental resins and composites. A percolation threshold of HAP nanofibers, beyond which more nanofibers will no longer further increase the mechanical properties of dental composites containing HAP nanofibers, was observed for the dental composites with or without silica microparticle filler. Our mechanical testing and fractographic analysis indicated that the relatively good dispersion of HAP nanofibers at low mass fraction is the key reason for the significantly improved biaxial flexural strength, while higher mass fraction of HAP nanofibers tends to lead to bundles that cannot effectively

  2. Aspects of nitrogen surface chemistry relevant to TiN chemical vapor deposition

    Energy Technology Data Exchange (ETDEWEB)

    Schulberg, M.T.; Allendorf, M.D.; Outka, D.A.


    NH{sub 3} is an important component of many chemical vapor deposition (CVD) processes for TiN films, which are used for diffusion barriers and other applications in microelectronic circuits. In this study, the interaction of NH{sub 3} with TiN surfaces is examined with temperature programmed desorption (TPD) and Auger electron spectroscopy. NH{sub 3} has two adsorption states on TiN: a chemisorbed state and a multilayer state. A new method for analyzing TPD spectra in systems with slow pumping speeds yields activation energies for desorption for the two states of 24 kcal/mol and 7.3 kcal/mol, respectively. The sticking probability into the chemisorption state is {approximately}0.06. These results are discussed in the context of TiN CVD. In addition, the high temperature stability of TiN is investigated. TiN decomposes to its elements only after heating to 1300 K, showing that decomposition is unlikely to occur under CVD conditions.

  3. Influence of aspect ratio and surface defect density on hydrothermally grown ZnO nanorods towards amperometric glucose biosensing applications (United States)

    Shukla, Mayoorika; Pramila; Dixit, Tejendra; Prakash, Rajiv; Palani, I. A.; Singh, Vipul


    In this work, hydrothermally grown ZnO Nanorods Array (ZNA) has been synthesized over Platinum (Pt) coated glass substrate, for biosensing applications. In-situ addition of strong oxidizing agent viz KMnO4 during hydrothermal growth was found to have profound effect on the physical properties of ZNA. Glucose oxidase (GOx) was later immobilized over ZNA by means of physical adsorption process. Further influence of varying aspect ratio, enzyme loading and surface defects on amperometric glucose biosensor has been analyzed. Significant variation in biosensor performance was observed by varying the amount of KMnO4 addition during the growth. Moreover, investigations revealed that the suppression of surface defects and aspect ratio variation of the ZNA played key role towards the observed improvement in the biosensor performance, thereby significantly affecting the sensitivity and response time of the fabricated biosensor. Among different biosensors fabricated having varied aspect ratio and surface defect density of ZNA, the best electrode resulted into sensitivity and response time to be 18.7 mA cm-2 M-1 and bio-sensing applications.

  4. Some aspects of the ion solid collision studies using highly charged and energetic heavy ion beams

    International Nuclear Information System (INIS)

    Tandon, P.N.


    Some aspects of the ion solid collision studies using highly charged and energetic heavy ions are presented. These relate to the polarization acquired by such ions when they travel through a polarized ferromagnetic material. The effects of the wake potential as investigated by the radiative electron capture are also presented. (author). 22 refs., 9 figs

  5. What Aspects of Principal Leadership Are Most Highly Correlated with School Outcomes in China? (United States)

    Zheng, Qiao; Li, Lingyan; Chen, Huijuan; Loeb, Susanna


    Purpose: The purpose of this study is to build a broader framework for Chinese principal leadership and to determine what aspects of principal leadership correlate most highly with school outcomes from the perspectives of both principals and teachers. Method: The data come from a 2013 national student achievement assessment in China comprising…

  6. Numerical Simulations of Noise Generated by High Aspect Ratio Supersonic Rectangular Jets - Validation (United States)

    Viswanath, Kamal; Johnson, Ryan; Kailasanath, Kailas; Malla, Bhupatindra; Gutmark, Ephraim


    The noise from high performance jet engines of both civilian and military aircraft is an area of active concern. Asymmetric exhaust nozzle configurations, in particular rectangular, potentially offer a passive way of modulating the farfield noise and are likely to become more important in the future. High aspect ratio nozzles offer the further benefit of easier airframe integration. In this study we validate the far field noise for ideally and over expanded supersonic jets issuing from a high aspect ratio rectangular nozzle geometry. Validation of the acoustic data is performed against experimentally recorded sound pressure level (SPL) spectra for a host of observer locations around the asymmetric nozzle. Data is presented for a slightly heated jet case for both nozzle pressure ratios. The contrast in the noise profile from low aspect ratio rectangular and circular nozzle jets are highlighted, especially the variation in the azimuthal direction that shows ``quiet'' and ``loud'' planes in the farfield in the peak noise direction. This variation is analyzed in the context of the effect of mixing at the sharp corners, the sense of the vortex pairs setup in the exit plane, and the evolution of the high aspect ratio exit cross-section as it propagates downstream including possible axis-switching. Supported by Office of Naval Research (ONR) through the Computational Physics Task Area under the NRL 6.1 Base Program.

  7. Leptothrix sp sheaths modified with iron oxide particles: Magnetically responsive, high aspect ratio functional material

    Czech Academy of Sciences Publication Activity Database

    Šafařík, Ivo; Angelova, R.; Baldíková, E.; Pospíšková, K.; Šafaříková, Miroslava


    Roč. 71, February (2017), s. 1342-1346 ISSN 0928-4931 Institutional support: RVO:60077344 Keywords : Leptothrix * magnetic modification * iron oxide * high aspect ratio material Subject RIV: BM - Solid Matter Physics ; Magnetism OBOR OECD: Material s engineering Impact factor: 4.164, year: 2016

  8. Artificial playing surfaces research: a review of medical, engineering and biomechanical aspects. (United States)

    Dixon, S J; Batt, M E; Collop, A C


    In this paper, current knowledge of artificial playing surfaces is reviewed. Research status in the fields of sports medicine, engineering and biomechanics is described. A multidisciplinary approach to the study of artificial sports surface properties is recommended. The development of modelling techniques to characterise fundamental material properties is described as the most appropriate method for the unique specification of material properties such as stiffness and damping characteristics. It is suggested that the systematic manipulation of fundamental surface material properties in biomechanics research will allow the identification of subject responses to clearly defined surface variation. It is suggested that subjects should be grouped according to characteristic behaviour on specific sports surfaces. It is speculated that future biomechanics research will identify subject criterion related to differing group responses. The literature evidence of interactions between sports shoes and sports surfaces leads to the suggestion that sports shoe and sports surface companies should work together in the development of ideal shoe - surface combinations for particular groups of subjects.

  9. Proton beam writing and electroplating for the fabrication of high aspect ratio Au microstructures

    International Nuclear Information System (INIS)

    Yue Weisheng; Ren Yaping; Kan, Jeroen Anton van; Chiam, S.-Y.; Jian, Linke; Moser, Herbert O.; Osipowicz, Thomas; Watt, Frank


    We present an approach to fabricate tall high aspect ratio Au microstructures by means of proton beam direct writing. Combining proton beam direct writing and electroplating, we successfully produced gold structures with sub-micrometer lateral dimensions, structure heights in excess of 11 μm, and aspect ratios over 28. Sidewall quality of the Au structures was improved by lowering the process temperature to 20 deg. C when developing PMMA patterns with GG developer. The application of such structures as X-ray masks for deep X-ray lithography with synchrotron radiation was demonstrated.

  10. Optimal Design of Airfoil with High Aspect Ratio in Unmanned Aerial Vehicles


    Kyoungwoo Park; Ji-Won Han; Hyo-Jae Lim; Byeong-Sam Kim; Juhee Lee


    Shape optimization of the airfoil with high aspect ratio of long endurance unmanned aerial vehicle (UAV) is performed by the multi-objective optimization technology coupled with computational fluid dynamics (CFD). For predicting the aerodynamic characteristics around the airfoil the high-fidelity Navier-Stokes solver is employed and SMOGA (Simple Multi-Objective Genetic Algorithm), which is developed by authors, is used for solving the multi-objective optimization problem...

  11. Corrosion resistance, chemistry, and mechanical aspects of Nitinol surfaces formed in hydrogen peroxide solutions

    Energy Technology Data Exchange (ETDEWEB)

    Shabalovskay, Svetlana A.; Anderegg, James W.; Undisz, Andreas; Rettenmayr, Markus; Rondelli, Gianni C.


    Ti oxides formed naturally on Nitinol surfaces are only a few nanometers thick. To increase their thickness, heat treatments are explored. The resulting surfaces exhibit poor resistance to pitting corrosion. As an alternative approach to accelerate surface oxidation and grow thicker oxides, the exposure of Nitinol to strong oxidizing H2O2 aqueous solutions (3 and 30%) for various periods of time was used. Using X-Ray Photoelectron Spectroscopy (XPS) and Auger spectroscopy, it was found that the surface layers with variable Ti (6–15 at %) and Ni (5–13 at %) contents and the thickness up to 100 nm without Ni-enriched interfaces could be formed. The response of the surface oxides to stress in superelastic regime of deformations depended on oxide thickness. In the corrosion studies performed in both strained and strain-free states using potentiodynamic and potentiostatic polarizations, the surfaces treated in H2O2 showed no pitting in corrosive solution that was assigned to higher chemical homogeneity of the surfaces free of secondary phases and inclusions that assist better biocompatibility of Nitinol medical devices. © 2012 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater 100B: 1490–1499, 2012

  12. High Temperature Surface Parameters for Solar Power

    National Research Council Canada - National Science Library

    Butler, C. F; Jenkins, R. J; Rudkin, R. L; Laughridge, F. I


    ... at a given distance from the sun. Thermal conversion efficiencies with a concentration ratio of 50 have been computed for each surface when exposed to solar radiation at the Earth's mean orbital radius...

  13. Some physical aspects of the surface waters around the little Andaman Island

    Digital Repository Service at National Institute of Oceanography (India)

    Murty, C.S.; Das, P.K.; Gouveia, A.D.

    Along with the thermal and haline characteristics of the waters during the peak northeast monsoon period (February),observations on stratifications, inversions, mixed layers, nature and depth of thermocline, wind-induced surface drifts, zones...

  14. Large-eddy simulation of the high-Reynolds-number flow through a high-aspect-ratio cooling duct

    NARCIS (Netherlands)

    Kaller, Thomas; Pasquariello, Vito; Hickel, S.; Adams, Nikolaus A.


    We present well-resolved large-eddy-simulations (LES) of a straight, high-aspect-ratio cooling duct (HARCD) at a bulk Reynolds number of Re = 110 • 103 and an average Nusselt number of Nu = 371. The geometry and boundary conditions have been defined together with Rochlitz et al.

  15. Candida albicans aspects of novel silane system-coated titanium and zirconia implant surfaces. (United States)

    Villard, Nicolas; Seneviratne, Chaminda; Tsoi, James Kit Hon; Heinonen, Markku; Matinlinna, Jukka


    The aim of the present study was to evaluate the effect of novel silane system coatings on zirconia and titanium implant surfaces and the attachment of the fungal pathogen Candida albicans. Titanium and zirconia specimens were silica-coated and silanized either with a commercial silane primer (RelyX Ceramic Primer™, 3M ESPE) or a novel silane system primer. The novel silane system primer was a blend of 1.0 vol% 3-acryloxypropyltrimethoxysilane and 0.3 vol% bis-1,2-(triethoxysilyl)ethane diluted in acidified ethanol-water solvent. The surface roughness (Ra ), the surface free energy and the chemical composition of substrate surfaces after treatments were evaluated. C. albcans biofilms were developed on silica-coated + silanized surfaces during 48 h of incubation time. Colony forming units (CFU) and real-time PCR (RT-PCR) quantified the cells on the material surfaces. Statistical analyses were carried out by 1-way ANOVA, Tukey post hoc and Games Howell post hoc test at 5% significance level (p). On zirconia and titanium surfaces, the Ra and the chemical composition of the specimens were equal (P silanization. CFU of C. albicans was significantly lower on zirconia coated with RelyX Ceramic Primer™, (P silanes (P = 0.002). RT-PCR revealed no differences between the mean quantities of C. albicans (P ≥ 0.067). Silica-coating and silanization had modified the titanium and zirconia surfaces significantly. Both the control and experimental silane primers might inhibit the biofilm formation of C. albicans. © 2014 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.

  16. A review on the wettability of dental implant surfaces II: Biological and clinical aspects. (United States)

    Gittens, Rolando A; Scheideler, Lutz; Rupp, Frank; Hyzy, Sharon L; Geis-Gerstorfer, Jürgen; Schwartz, Zvi; Boyan, Barbara D


    Dental and orthopedic implants have been under continuous advancement to improve their interactions with bone and ensure a successful outcome for patients. Surface characteristics such as surface topography and surface chemistry can serve as design tools to enhance the biological response around the implant, with in vitro, in vivo and clinical studies confirming their effects. However, the comprehensive design of implants to promote early and long-term osseointegration requires a better understanding of the role of surface wettability and the mechanisms by which it affects the surrounding biological environment. This review provides a general overview of the available information about the contact angle values of experimental and of marketed implant surfaces, some of the techniques used to modify surface wettability of implants, and results from in vitro and clinical studies. We aim to expand the current understanding on the role of wettability of metallic implants at their interface with blood and the biological milieu, as well as with bacteria, and hard and soft tissues. Copyright © 2014 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

  17. A Review on the Wettability of Dental Implant Surfaces II: Biological and Clinical Aspects (United States)

    Gittens, Rolando A.; Scheideler, Lutz; Rupp, Frank; Hyzy, Sharon L.; Geis-Gerstorfer, Jürgen; Schwartz, Zvi; Boyan, Barbara D.


    Dental and orthopaedic implants have been under continuous advancement to improve their interactions with bone and ensure a successful outcome for patients. Surface characteristics such as surface topography and surface chemistry can serve as design tools to enhance the biological response around the implant, with in vitro, in vivo and clinical studies confirming their effects. However, the comprehensive design of implants to promote early and long-term osseointegration requires a better understanding of the role of surface wettability and the mechanisms by which it affects the surrounding biological environment. This review provides a general overview of the available information about the contact angle values of experimental and of marketed implant surfaces, some of the techniques used to modify surface wettability of implants, and results from in vitro and clinical studies. We aim to expand the current understanding on the role of wettability of metallic implants at their interface with blood and the biological milieu, as well as with bacteria, and hard and soft tissues. PMID:24709541

  18. Electron capture by highly charged ions from surfaces and gases

    Energy Technology Data Exchange (ETDEWEB)

    Allen, F.


    In this study highly charged ions produced in Electron Beam Ion Traps are used to investigate electron capture from surfaces and gases. The experiments with gas targets focus on spectroscopic measurements of the K-shell x-rays emitted at the end of radiative cascades following electron capture into Rydberg states of Ar{sup 17+} and Ar{sup 18+} ions as a function of collision energy. The ions are extracted from an Electron Beam Ion Trap at an energy of 2 keVu{sup -1}, charge-selected and then decelerated down to 5 eVu{sup -1} for interaction with an argon gas target. For decreasing collision energies a shift to electron capture into low orbital angular momentum capture states is observed. Comparative measurements of the K-shell x-ray emission following electron capture by Ar{sup 17+} and Ar{sup 18+} ions from background gas in the trap are made and a discrepancy in the results compared with those from the extraction experiments is found. Possible explanations are discussed. For the investigation of electron capture from surfaces, highly charged ions are extracted from an Electron Beam Ion Trap at energies of 2 to 3 keVu{sup -1}, charge-selected and directed onto targets comprising arrays of nanoscale apertures in silicon nitride membranes. The highly charged ions implemented are Ar{sup 16+} and Xe{sup 44+} and the aperture targets are formed by focused ion beam drilling in combination with ion beam assisted thin film deposition, achieving hole diameters of 50 to 300 nm and aspect ratios of 1:5 to 3:2. After transport through the nanoscale apertures the ions pass through an electrostatic charge state analyzer and are detected. The percentage of electron capture from the aperture walls is found to be much lower than model predictions and the results are discussed in terms of a capillary guiding mechanism. (orig.)

  19. Surface degradation of high Tc superconductors

    International Nuclear Information System (INIS)

    Lu, Q.; Larkins, G.L. Jr.; Jones, W.K.; Kennedy, R.J.; Chern, G.


    This paper reports on surface degradation studies of the YBa 2 Cu 3 O 7-x (123) and Bi-Sr-Ca-Cu-O (2223) superconducting ceramics performed in N 2 , Ar 2 , O 2 , wet and dry air. By using a non-contact, room temperature technique the time dependence of the surface impedance of both 123 and Bi-Sr-Ca-Cu-O bulk ceramics are measured from 100 Hz to 20 kHz. In humid environments the rate of degradation is dependent on the humidity and appears to be unaffected by the carrier gas. The surface impedance change due to humidity follows a power law and does not appear to saturate at a final value

  20. Metrological Aspects of Surface Topographies Produced by Different Machining Operations Regarding Their Potential Functionality

    Directory of Open Access Journals (Sweden)

    Żak Krzysztof


    Full Text Available This paper presents a comprehensive methodology for measuring and characterizing the surface topographies on machined steel parts produced by precision machining operations. The performed case studies concern a wide spectrum of topographic features of surfaces with different geometrical structures but the same values of the arithmetic mean height Sa. The tested machining operations included hard turning operations performed with CBN tools, grinding operations with Al2O3 ceramic and CBN wheels and superfinish using ceramic stones. As a result, several characteristic surface textures with the Sa roughness parameter value of about 0.2 μm were thoroughly characterized and compared regarding their potential functional capabilities. Apart from the standard 2D and 3D roughness parameters, the fractal, motif and frequency parameters were taken in the consideration.

  1. Flight Loads Prediction of High Aspect Ratio Wing Aircraft Using Multibody Dynamics

    Directory of Open Access Journals (Sweden)

    Michele Castellani


    Full Text Available A framework based on multibody dynamics has been developed for the static and dynamic aeroelastic analyses of flexible high aspect ratio wing aircraft subject to structural geometric nonlinearities. Multibody dynamics allows kinematic nonlinearities and nonlinear relationships in the forces definition and is an efficient and promising methodology to model high aspect ratio wings, which are known to be prone to structural nonlinear effects because of the high deflections in flight. The multibody dynamics framework developed employs quasi-steady aerodynamics strip theory and discretizes the wing as a series of rigid bodies interconnected by beam elements, representative of the stiffness distribution, which can undergo arbitrarily large displacements and rotations. The method is applied to a flexible high aspect ratio wing commercial aircraft and both trim and gust response analyses are performed in order to calculate flight loads. These results are then compared to those obtained with the standard linear aeroelastic approach provided by the Finite Element Solver Nastran. Nonlinear effects come into play mainly because of the need of taking into account the large deflections of the wing for flight loads computation and of considering the aerodynamic forces as follower forces.

  2. High speed machined surface roughness measurement ...

    African Journals Online (AJOL)

    Surface roughness monitoring techniques using non-contact methods based on computer vision technology are becoming popular and cost effective. An evolvable hardware configuration using reconfigurable Xilinx Virtex FPGA xcv1000 architecture with capability to compensate for poor illumination environment is ...

  3. Fabrication of High Aspect Ratio SU-8 Structures for Integrated Spectrometers

    DEFF Research Database (Denmark)

    Anhøj, Thomas Aarøe


    This dissertation deals with the fabrication of integrated spectrometers for use in miniaturized chemical analysis systems, also called 'lab-on-a-chip'-systems. The spectrometers are based on concave re ection gratings, and are fabricated in the epoxy-based material SU-8 by means...... of photolithography. Successful fabrication of re ection gratings requires a high degree of precision in the photolithographic process. The fabrication process has thus been optimized by optimizing the photolithographic process for fabrication of high aspect ratio structures, i.e. structures with details...... of the photolithographic SU-8 fabrication process has caused the aspect ratio of the narrowest resolvable trench to rise from approximately 6 to 11.4. Simultaneously, the optimized process eliminates all problems regarding cracks in the fabricated structures. If the fabrication of the re ection grating is not perfect...

  4. Is judgement of biotechnological ethical aspects related to high school students' knowledge?


    Črne-Hladnik, Helena; Hladnik, Aleš; Javornik, Branka; Košmelj, Katarina; Peklaj, Cirila


    Abstract Quantitative and qualitative studies of various aspects of the perception of biotechnology were conducted among 469 Slovenian high school students of average age 17 years. Our research aimed to explore relationships among students' pre-knowledge of molecular- and human genetics, and their attitudes to four specific biotechnological applications. These applications ? Bt corn, genetically modified salmon, somatic- and germ line gene therapy ? were investigated from the viewp...

  5. Fabrication process for tall, sharp, hollow, high aspect ratio polymer microneedles on a platform

    International Nuclear Information System (INIS)

    Ceyssens, Frederik; Chaudhri, Buddhadev Paul; Van Hoof, Chris; Puers, Robert


    This paper reports on a new lithographic process for fabricating arrays of tall, high aspect ratio (defined as height/wall thickness), hollow, polymer microneedles on a platform. The microneedles feature a high sharpness (down to 3 µm tip radius) and aspect ratio (>65) which is a factor 2 and 4 better than the state of the art, respectively. The maximum achievable needle shaft length is over 1 mm. The improved performance was obtained by using an anisotropically patterned silicon substrate covered with an antireflective layer as mold for the needle tip and an optimized SU-8 lithographic process. Furthermore, a platform containing liquid feedthroughs holding an arbitrary number of needles out of plane can be manufactured with only one additional process step. The high aspect ratio microneedles undergo failure at the critical load of around 230 mN in the case of 1 mm long hollow needles with triangular cross section and a base of 175 µm. Penetration into human skin is demonstrated as well. (paper)

  6. Heavy metal transport processes in surface water and groundwater. Geochemical and isotopic aspects

    International Nuclear Information System (INIS)

    Tricca, A.


    This work deals with the transport mechanisms of trace elements in natural aquatic systems. The experimental field is situated in the Upper Rhine Rift Valley because of the density and variety of its hydrological net. This study focused on three aspects: the isotopic tracing with Sr, Nd and O allowed to characterize the hydro-system. The 87 Sr/ 86 Sr and 143 Nd/ 144 Nd ratios show that the system is controlled by two natural end members a carbonate and a silicate one and a third end member of anthropogenic origin. The isotopic data allowed also to investigate the exchange processes between the dissolved and the particulate phases of the water samples. Because of their use in the industry and their very low concentrations in natural media, the Rare Earth Elements (REE) are very good tracers of anthropogenic contamination. Furthermore, due to their similar chemical properties with the actinides,they constitute excellent analogues to investigate the behaviour of fission products in the nature. In this study we determined the distribution of the REE within a river between the dissolved, the colloidal and the particulate phases. Among the REE of the suspended load, we distinguished between the exchangeable and the residual REE by means OF IN HCl leading experiments. The third topic is the investigation of uranium series disequilibrium using α-Spectrometry. The determination of ratios 234 U/ 238 U as well as of the activities short-lived radionuclides like 222 Rn, 224 Ra, 226 Ra, 228 Ra, 210 Po and 210 Pb have been performed. Their activities are controlled by chemical and physical parameters and depend also on the lithology of the source area. The combination of the three aspects provided relevant informations about the exchanges between the different water masses, about the transport mechanisms of the REE. Furthermore, the uranium series disequilibrium provided informations about the geochemical processes at a micro-scale. (author)

  7. Surface processing by high power excimer laser

    International Nuclear Information System (INIS)

    Stehle, M.


    Surface processing with lasers is a promising field of research and applications because lasers bring substantial advantages : laser beams work at distance, laser treatments are clean in respect of environment consideration and they offer innovative capabilities for surface treatment which cannot be reached by other way. Excimer lasers are pulsed, gaseous lasers which emit in UV spectral range - the most common are XeCl (308 nm), KrF (248 nm), ArF (193 nm). From 1980 up to 1994, many of them have been used for research, medical and industrial applications such as spectroscopy, PRK (photo-refractive keratotomy) and micro-machining. In the last six years, from 1987 up to 1993, efforts have been done in order to jump from 100 W average power up to 1 kW for XeCl laser at λ = 308 nm. It was the aim of AMMTRA project in Japan as EU205 and EU213 Eureka projects in Europe. In this framework, SOPRA developed VEL (Very large Excimer Laser). In 1992, 1 kW (10 J x 100 Hz) millstone has been reached for the first time, this technology is based on X-Ray preionization and large laser medium (5 liters). Surface treatments based on this laser source are the main purpose of VEL Lasers. Some of them are given for instance : a) Turbine blades made with metallic substrate and ceramic coatings on the top, are glazed in order to increase corrosion resistance of ceramic and metal sandwich. b) Selective ablation of organic coatings deposited on fragile composite material is investigated in Aerospace industry. c) Chock hardening of bulk metallic materials or alloys are investigated for automotive industry in order to increase wear resistance. d) Ablation of thin surface oxides of polluted steels are under investigation in nuclear industry for decontamination. (J.P.N.)

  8. Technological Aspects of Corrosion-Resistant Steels Surfacing by Intense Relativistic Electron Beams (United States)

    Belozerov, V. V.; Donets, S. E.; Klepikov, V. F.; Kivshik, V. F.; Lytvynenko, V. V.; Lonin, Yu. F.; Ponomarev, A. G.; Uvarov, V. T.

    Intense tubular relativistic electron beams are a promising tool for a number of practical applications, such as obtaining nanodispersed powder materials, surface properties modification of products, remote surfacing, etc. In current technologies for obtaining of nanopowder materials, one of the leading techniques is one based on the materials handling concentrated flows of energy. Using the various technological equipment (pulse current generators, accelerators), energy is inputted into the material in the form of intense impulse current, the plasma flows of charged particle beams. Each of the specified types of impact is characterized by a certain decomposition mechanism of processed materials to micro- and nano-sized state. Thus, the action of intense pulsed currents based on the thermal evaporation of a melt conductor with its subsequent condensation in liquid, the use of plasma flows and charged particle beams also involves evaporation and condensation of a material in a vacuum or in a special atmosphere.

  9. Qualité géométrique & aspect des surfaces : approches locales et globales


    Le Goïc , Gaëtan


    Accounting for customers' perception of manufactured goods has become a major challenge for the industry. This process is to be established from early design to retail. Customers are nowadays more aware and detail oriented about perceived quality of products. This allows one to set not only an estimated price but also the expected quality of the product. Surface appearance analysis has therefore become a key industrial issue. Two approaches are proposed here to formalize the detection methodo...

  10. Some legal aspects on high level radioactive waste disposal in Japan

    International Nuclear Information System (INIS)

    Tanabe, Tomoyuki


    In Japan, it is considered to be an urgent problem to prepare the system for the research and execution of high level radioactive waste disposal. Under what regulation scheme the disposal should be done has not been sufficiently examined. In this research, the examination was carried out on the legal aspects of high level radioactive waste disposal as follows. First, the current legislation on the disposal in Japan was analyzed, and it was made clear that high level radioactive waste disposal has not been stipulated clearly. Next, on the legal choices which are conceivable on the way the legislation for high level radioactive waste disposal should be, from the aspects of applying the law on regulating nuclear reactors and others, applying the law on nuclear power damage reparation, and industrialization by changing the government ordinances, those were arranged in six choices, and the examination was carried out for each choice from the viewpoints of the relation with the base stipulation for waste-burying business, the speciality of high level radioactive waste disposal as compared with other actions of nuclear power business, the coordination with existing nuclear power of nuclear power business, the coordination with existing nuclear power law system and the formation of national consensus. In this research, it was shown that the execution of high level radioactive waste disposal as the business based on the separate legislation is the realistic choice. (K.I.)

  11. Theoretical aspects of heavy-flavour production at ultra-high cosmic ray energies

    Directory of Open Access Journals (Sweden)

    Gonçalves V. P.


    Full Text Available The main theoretical aspects of heavy-flavour production at ultra-high cosmic ray energies are reviewed, with particular emphasis in the new dynamical effects which are expected to be present in the kinematical range probed by the IceCube and Pierre Auger Observatories. The gluon saturation effects for heavy quark production and the contribution of double parton scattering processes are analysed. Finally, the intrinsic heavy quark hypothesis is presented and some of its phenomenological implications at high energies are discussed.

  12. Thermal, structural, and fabrication aspects of diamond windows for high power synchrotron x-ray beamlines

    International Nuclear Information System (INIS)

    Khounsary, A.M.; Phillips, W.


    Recent advances in chemical vapor deposition (CVD) technology have made it possible to produce thin free-standing diamond foils that can be used as the window material in high heat load, synchrotron beamlines. Numerical simulations suggest that these windows can offer an attractive and at times the only altemative to beryllium windows for use in third generation x-ray synchrotron radiation beamlines. Utilization, design, and fabrication aspects of diamond windows for high heat load x-ray beamlines are discussed, as are the microstructure characteristics bearing on diamond's performance in this role. Analytic and numerical results are also presented to provide a basis for the design and testing of such windows

  13. Front-surface fabrication of moderate aspect ratio micro-channels in fused silica by single picosecond Gaussian-Bessel laser pulse (United States)

    Liu, Xin; Sanner, Nicolas; Sentis, Marc; Stoian, Razvan; Zhao, Wei; Cheng, Guanghua; Utéza, Olivier


    Single-shot Gaussian-Bessel laser beams of 1 ps pulse duration and of 0.9 μm core size and 60 μm depth of focus are used for drilling micro-channels on front side of fused silica in ambient condition. Channels ablated at different pulse energies are fully characterized by AFM and post-processing polishing procedures. We identify experimental energy conditions (typically 1.5 µJ) suitable to fabricate non-tapered channels with mean diameter of 1.2 µm and length of 40 μm while maintaining an utmost quality of the front opening of the channels. In addition, by further applying accurate post-polishing procedure, channels with high surface quality and moderate aspect ratio down to a few units are accessible, which would find interest in the surface micro-structuring of materials, with perspective of further scalability to meta-material specifications.

  14. Hybrid UV Lithography for 3D High-Aspect-Ratio Microstructures

    International Nuclear Information System (INIS)

    Park, Sungmin; Nam, Gyungmok; Kim, Jonghun; Yoon, Sang-Hee


    Three-dimensional (3D) high-aspect-ratio (HAR) microstructures for biomedical applications (e.g., microneedle, microadhesive, etc.) are microfabricated using the hybrid ultraviolet (UV) lithography in which inclined, rotational, and reverse-side UV exposure processes are combined together. The inclined and rotational UV exposure processes are intended to fabricate tapered axisymmetric HAR microstructures; the reverse-side UV exposure process is designed to sharpen the end tip of the microstructures by suppressing the UV reflection on a bottom substrate which is inevitable in conventional UV lithography. Hybrid UV lithography involves fabricating 3D HAR microstructures with an epoxy-based negative photoresist, SU-8, using our customized UV exposure system. The effects of hybrid UV lithography parameters on the geometry of the 3D HAR microstructures (aspect ratio, radius of curvature of the end tip, etc.) are measured. The dependence of the end-tip shape on SU-8 soft-baking condition is also discussed

  15. Hybrid UV Lithography for 3D High-Aspect-Ratio Microstructures

    Energy Technology Data Exchange (ETDEWEB)

    Park, Sungmin; Nam, Gyungmok; Kim, Jonghun; Yoon, Sang-Hee [Inha Univ, Incheon (Korea, Republic of)


    Three-dimensional (3D) high-aspect-ratio (HAR) microstructures for biomedical applications (e.g., microneedle, microadhesive, etc.) are microfabricated using the hybrid ultraviolet (UV) lithography in which inclined, rotational, and reverse-side UV exposure processes are combined together. The inclined and rotational UV exposure processes are intended to fabricate tapered axisymmetric HAR microstructures; the reverse-side UV exposure process is designed to sharpen the end tip of the microstructures by suppressing the UV reflection on a bottom substrate which is inevitable in conventional UV lithography. Hybrid UV lithography involves fabricating 3D HAR microstructures with an epoxy-based negative photoresist, SU-8, using our customized UV exposure system. The effects of hybrid UV lithography parameters on the geometry of the 3D HAR microstructures (aspect ratio, radius of curvature of the end tip, etc.) are measured. The dependence of the end-tip shape on SU-8 soft-baking condition is also discussed.

  16. Highly stable superhydrophobic surfaces under flow conditions (United States)

    Lee, Moonchan; Yim, Changyong; Jeon, Sangmin


    We synthesized hydrophobic anodic aluminum oxide nanostructures with pore diameters of 35, 50, 65, and 80 nm directly on quartz crystal microresonators, and the stability of the resulting superhydrophobicity was investigated under flow conditions by measuring changes in the resonance frequency and dissipation factor. When the quartz substrates were immersed in water, their hydrophobic surfaces did not wet due to the presence of an air interlayer. The air interlayer was gradually replaced by water over time, which caused decreases in the resonance frequency (i.e., increases in mass) and increases in the dissipation factor (i.e., increases in viscous damping). Although the water contact angles of the nanostructures increased with increasing pore size, the stability of their superhydrophobicity increased with decreasing pore size under both static conditions (without flow) and dynamic conditions (with flow); this increase can be attributed to an increase in the solid surface area that interacts with the air layer above the nanopores as the pore size decreases. Further, the effects of increasing the flow rate on the stability of the superhydrophobicity were quantitatively determined.

  17. Temporal aspects of surface water quality variation using robust statistical tools. (United States)

    Mustapha, Adamu; Aris, Ahmad Zaharin; Ramli, Mohammad Firuz; Juahir, Hafizan


    Robust statistical tools were applied on the water quality datasets with the aim of determining the most significance parameters and their contribution towards temporal water quality variation. Surface water samples were collected from four different sampling points during dry and wet seasons and analyzed for their physicochemical constituents. Discriminant analysis (DA) provided better results with great discriminatory ability by using five parameters with (P < 0.05) for dry season affording more than 96% correct assignation and used five and six parameters for forward and backward stepwise in wet season data with P-value (P < 0.05) affording 68.20% and 82%, respectively. Partial correlation results revealed that there are strong (r(p) = 0.829) and moderate (r(p) = 0.614) relationships between five-day biochemical oxygen demand (BOD(5)) and chemical oxygen demand (COD), total solids (TS) and dissolved solids (DS) controlling for the linear effect of nitrogen in the form of ammonia (NH(3)) and conductivity for dry and wet seasons, respectively. Multiple linear regression identified the contribution of each variable with significant values r = 0.988, R(2) = 0.976 and r = 0.970, R(2) = 0.942 (P < 0.05) for dry and wet seasons, respectively. Repeated measure t-test confirmed that the surface water quality varies significantly between the seasons with significant value P < 0.05.

  18. Ag Nanorod Arrays for SERS: Aspects of Spectral Reproducibility, Surface Contamination, and Spectral Sensitivity

    Directory of Open Access Journals (Sweden)

    Martin Šubr


    Full Text Available Ag nanorod arrays prepared by oblique angle vapor deposition (OAD represent regular, large area substrates for surface-enhanced Raman scattering (SERS spectroscopy. We studied uniformity and spectral reproducibility of silver OAD-fabricated substrates (AgOADs by spectral mapping of methylene blue. The results demonstrate good reproducibility apart from occasional “hot-spot” sites where the intensity is higher. The number of “hot-spots” represents 2%–6% of SERS-active sites of mapping substrate area. We were able to obtain good SERS spectra of testing amino acid tryptophan at 1 × 10−5 M concentration and three different free-base porphyrins down to ∼10−7 M concentration. We found out that keeping the AgOADs in a vacuum chamber overnight prevents the surface from binding any contaminants from the ambient atmosphere, without significant reduction in the SERS enhancement. Such substrates provide stable SERS enhancement even when stored for 1 year after preparation.

  19. Temporal Aspects of Surface Water Quality Variation Using Robust Statistical Tools

    Directory of Open Access Journals (Sweden)

    Adamu Mustapha


    Full Text Available Robust statistical tools were applied on the water quality datasets with the aim of determining the most significance parameters and their contribution towards temporal water quality variation. Surface water samples were collected from four different sampling points during dry and wet seasons and analyzed for their physicochemical constituents. Discriminant analysis (DA provided better results with great discriminatory ability by using five parameters with (P<0.05 for dry season affording more than 96% correct assignation and used five and six parameters for forward and backward stepwise in wet season data with P-value (P<0.05 affording 68.20% and 82%, respectively. Partial correlation results revealed that there are strong (rp=0.829 and moderate (rp=0.614 relationships between five-day biochemical oxygen demand (BOD5 and chemical oxygen demand (COD, total solids (TS and dissolved solids (DS controlling for the linear effect of nitrogen in the form of ammonia (NH3 and conductivity for dry and wet seasons, respectively. Multiple linear regression identified the contribution of each variable with significant values r = 0.988, R2 = 0.976 and r = 0.970, R2 = 0.942 (P<0.05 for dry and wet seasons, respectively. Repeated measure t-test confirmed that the surface water quality varies significantly between the seasons with significant value P<0.05.

  20. Fundamental aspects on ion-beam surface modification: defect production and migration processes

    International Nuclear Information System (INIS)

    Rehn, L.E.; Averback, R.S.; Okamoto, P.R.


    Ion-beam modification of metals is generating increasing scientific interest not only because it has exciting technological potential, but also because it has raised fundamental questions concerning radiation-induced diffusion processes. In addition to the implanted species, several defect production and migration mechanisms contribute to changes in the near-surface composition of an alloy during ion bombardment, e.g., atoms exchange positions via displacements and replacement sequences; preferential sputtering effects arise; radiation-enhanced diffusion and radiation-induced segregation occur. The latter two defect migration mechanisms are of particular significance since they can alter the composition to depths which are much greater than the implanted ion range. By altering various parameters such as irradiation temperature, ion mass, energy, and current density, and initial alloying distributions, a rich variety of near-surface composition profiles can be created. We have utilized changes in ion mass and energy, and irradiation temperature to distinguish defect production from defect migration effects. Experimental results are presented which provide a guide to the relative efficiencies of different mechanisms under various irradiation conditions. 46 references

  1. Design Concepts for Low Aspect Ratio High Pressure Turbines for High Bypass Ratio Turbofans, Phase II (United States)

    National Aeronautics and Space Administration — The performance gains and weight reductions from using Ceramic Matrix Composite(CMC) turbine blades in both the High Pressure Turbine(HPT) and Low Pressure...

  2. A high-reflective surface measurement method based on conoscopic holography technology (United States)

    Cheng, Xu; Li, ZhongWei; Shi, YuSheng; Zhao, HengShuang; Zhan, Guomin


    Measuring high-reflective surfaces using optical method is always a big challenging problem. This paper presents a high-reflective surface measurement method based on conoscopic holography technology using a 4D motion platform equipped with a conoscopic holography optical probe. There are two key problems needed to solve before the automate scan of the complex shape surface: the coordinate calibration and the path planning. To improve the calibration efficiency and accuracy, the coordinate calibration is divided into two parts: the rough calibration and the accurate registration. The path planning consists of two aspects including: the path points generation and the path points verification. In addition, by scanning the objects having high-reflective surfaces, such as the metal blades, coins and other work-pieces, the efficiency of the measurement method has been verified.

  3. Results of design studies and wind tunnel tests of high-aspect-ratio supercritical wings for an energy efficient transport (United States)

    Steckel, D. K.; Dahlin, J. A.; Henne, P. A.


    These basic characteristics of critical wings included wing area, aspect ratio, average thickness, and sweep as well as practical constraints on the planform and thickness near the wing root to allow for the landing gear. Within these constraints, a large matrix of wing designs was studied with spanwise variations in the types of airfoils and distribution of lift as well as some small planform changes. The criteria by which the five candidate wings were chosen for testing were the cruise and buffet characteristics in the transonic regime and the compatibility of the design with low speed (high-lift) requirements. Five wing-wide-body configurations were tested in the NASA Ames 11-foot transonic wind tunnel. Nacelles and pylons, flap support fairings, tail surfaces, and an outboard aileron were also tested on selected configurations.

  4. Process optimization of high aspect ratio sub-32nm HSQ/AR3 bi-layer resist pillar (United States)

    Chen, Wei-Su; Tsai, Ming-Jinn


    RRAM is the candidate of next generation new non-volatile memory. The etched stacking film thickness of RRAM cell pillar is not easy to reduce below 50 nm during CD scaling down since part of RRAM cell pillar height is removed during CMP polishing of dielectric passivation to expose the pillar top surface for the following metallization process. Therefore resist pillar pattern with high aspect ratio (AR) is needed to act as etch mask for defining thick RRAM cell pillar structure. Bilayer resist (BLR) process is most suitable for forming high AR pattern. Dry develop process is the key step for generating sub-32 nm high AR BLR pillar pattern. In this study optimization of dry develop process is investigated for high AR pillar with hydrogen silsesquioxane (HSQ) as upper thin imaging layer for e-beam exposure and AR3-600 as the thick underlayer for etching resistant. Experimental results are summarized below. Highest AR of ~6 for HSQ/AR3 BLR semi-dense L/S=1/2 pillar with vertical profile is obtained under optimized dry develop condition with O2, N2, Ar flow rates, chamber pressure, top and bottom power of 8, 5, 0 sccm, 1 mTorr, 200 and 100 watts respectively. AR is lower for looser pattern density. CD variation between HSQ/AR3-600 BLR pillars with different pattern density is optimized to 5.6 nm. The pillar profile is vertical in vacuum for pattern of any density but distorts more severe for denser pattern during ventilation to atmosphere. The most critical process parameters for obtaining high aspect ratio BLR pillar are O2 flow rate and top power. Sidewall profile angle of pillar is mainly dependent on chamber pressure and bottom power.

  5. Kwik Bond Polymers(R) high friction surface treatment. (United States)


    High friction surface treatment (HFST) was applied to two on-ramps in the Seattle urban area to improve : friction resistance. The ramps were high accident locations. The system applied was polyester resin binder and : calcined bauxite aggregate. Tes...

  6. Evaluation of Tyregrip(R) high-friction surfacing. (United States)


    This report describes the installation of Tyregrip, a high friction surface, on a high accident location to reduce accident : rates. Tyregrip is a thin polymer overlay system that uses a two part epoxy binder and calcined bauxite aggregate. Postc...

  7. Spatial aspects of surface water quality in the Jakara Basin, Nigeria using chemometric analysis. (United States)

    Mustapha, Adamu; Aris, Ahmad Zaharin


    Multivariate statistical techniques such as hierarchical Agglomerated cluster analysis (HACA), discriminant analysis (DA), principal component analysis (PCA), and factor analysis (FA) were applied to identify the spatial variation and pollution sources of Jakara River, Kano, Nigeria. Thirty surface water samples were collected: 23 along Getsi River and 7 along the main channel of River Jakara. Twenty-three water quality parameters, namely pH, temperature, turbidity, electrical conductivity (EC), dissolved oxygen (DO), 5-day biochemical oxygen demand (BOD(5)), Faecal coliform, total solids (TS), nitrates (NO(3)(-)), phosphates (PO(4)(3-)), cobalt (Co), iron (Fe), nickel (Ni), manganese (Mn), copper (Cu), sodium (Na), potassium (K), mercury (Hg), chromium (Cr), cadmium (Cd), lead (Pb), magnesium (Mg), and calcium(Ca) were analysed. HACA grouped the sampling points into three clusters based on the similarities of river water quality characteristics: industrial, domestic, and agricultural water pollution sources. Forward and backward DA effectively discriminated 5 and 15 water quality variables, respectively, each assigned with 100% correctness from the original 23 variables. PCA and FA were used to investigate the origin of each water quality parameter due to various land use activities, 7 principal components were obtained with 77.5% total variance, and in addition PCA identified 3 latent pollution sources to support HACA. From this study, one can conclude that the application of multivariate techniques derives meaningful information from water quality data.

  8. Materials and surface aspects in the development of SRF Niobium cavities

    CERN Document Server

    Antoine, C


    Foreword from author; When I joined the CEA Saclay SRF group in 1989, my initial background was physical chemistry and surface science, which I completed later on with solid state physics and metallurgy. Most accelerator physicists at that time had training in RF, plasma physics, nuclear or particle physics. We were very few with a background in material science. Working with people with a different background than yours reveals to be both challenging and funny: you can impress them with things you consider basic while they simply do not believe you for other things you consider so well admitted that you do not even remember where it comes from. At the end it obliges you to reconsider your basics and re-question many results, which opens many new and sometimes unexpected paths. Like usual in science, answering one question rises many new ones, and trying to improve cavities performance led to fascinating physics problems. Exploring some of these problems often requires techniques and expertise that are far be...

  9. New Surface Aspects towards Photocatalytic Activity of Doped Supported Titanium Dioxide

    Directory of Open Access Journals (Sweden)

    Samia A. Kosa


    Full Text Available The present work aims to synthesize nanoscale well dispersed TiO2/SiO2 and TiO2/Al2O3 nanoparticle photocatalysts via an impregnation method for the removal of methyl orange, which was used as a model compound of organic pollutant in wastewater, from an aqueous medium. Also within this frame work, La and Ce metals were loaded onto the surfaces of TiO2/SiO2 and TiO2/Al2O3 by an impregnation method to enhance the photocatalytic activity of the nanoparticles; the activities and physicochemical properties of the photocatalysts were compared before and after loading of metallic La and Ce. The oxide system was characterized by different techniques, including XRD, UV-Vis spectroscopy, FT-IR spectroscopy, SEM, and EDX spectroscopy. Finally, the optimal conditions to complete the photocatalytic oxidation of methyl orange dye were studied. This work holds promise for the efficient photodegradation of pollutants by nanoparticle photocatalysts.

  10. High-aspect-ratio grooves fabricated in silicon by a single pass of femtosecond laser pulses

    International Nuclear Information System (INIS)

    Ma Yuncan; Shi Haitao; Si Jinhai; Ren Hai; Chen Tao; Chen Feng; Hou Xun


    High-aspect-ratio grooves have been fabricated in silicon by a single pass of femtosecond laser pulses in water and ambient air. Scanning electron microscopy and energy dispersive x-ray spectroscopy were employed to image for the morphology of the photoinduced grooves and analyze the chemical composition in the surrounding of the grooves. It was observed that the sidewall of the grooves fabricated in water was much smoother than that in ambient air, and there were homogeneous nano-scale protrusions on the sidewall of the grooves fabricated in water. Meanwhile, oxygen species, which was incorporated into the grooves fabricated in air, was not observed in those in water.

  11. Psychosocial aspects and management of evaluation in secondary high and low achievement

    Directory of Open Access Journals (Sweden)

    Alicia Rivera Morales


    Full Text Available This article describes a segment of a broader study of mixed cut occurs. In this space only part of the qualitative analysis is recovered around the psychosocial aspects that influence the management of the evaluation results from the application of semi-structured interviews and focus groups with 80 senior secondary schools with high and low achievement located in four states of Mexico: Sonora, Durango, Mexico City and Oaxaca. The findings are presented from categories they consider the meaning, beliefs and expectations about evaluation and how these aspects influence the actions of the directors of the schools studied. Polarized cases allow, in their contrasts, identify processes and factors that mark the differences or similarities between them. Thus it was found that school principals low achievement hope to change the attitude of teachers towards the assessment, expect supervisors to monitor teachers and external support (specialists that indicate how to evaluate them. Moreover, the idea that a school with high achievement is an organization that promotes the participation director, has high expectations of students and teachers, its management system and decision-making can achieve the objectives set, and reasserts Assessment proposes actions that seek continuous improvement.

  12. Controllable fabrication of periodic arrays of high-aspect-ratio micro-nano hierarchical structures and their superhydrophobicity (United States)

    Ma, Zhibo; Jiang, Chengyu; Li, Xiangming; Ye, Fang; Yuan, Weizheng


    This paper demonstrates a flexible and controllable fabrication of vertically aligned and high-aspect-ratio (HAR) micro-nano hierarchical structures using conventional micro-technologies. We first masked the nanopatterns on a photoresist mold by shifting the same photomask, which could be performed using conventional contact microlithography. Thereby replicating nanopatterns onto an aluminium mold and successfully fabricating silicon nanopillar arrays about 300 nm in diameter and 5 µm in height via the deep reactive etching (DRIE) process. We also fabricated micro-nano hierarchical structures with variable aspect ratios using the proposed nanopattern technology and DRIE process without using any special nanopatterning equipment or techniques. The proposed method not only simplified the fabrication process but also produced HAR (higher than 15) structures. We also investigate the replica molding steps from the fabricated silicon stamp to a UV-curable polymer replica using a PDMS mold and conventional nano-imprinting, where each nanopillar diameter was 320 nm with 95% fidelity. As a result, the hierarchical structure arrays show stable superhydrophobic surface properties with a contact angle of approximately 160°. Owing to the cost efficiency of mass production and the fidelity of the strategy, the methodology could provide a general approach for fabricating complex three-dimensional periodic hierarchical structures onto a single chip and can be applied to various fields of multifunctional applications.

  13. Simulation and optimization of a micromachined gyroscope using high-aspect-ratio micromachining fabrication process (United States)

    Ruan, Aiwu Y.; Tse, Man S.; Chong, Gang Y.


    Micromachined gyroscopes rely on tuned vibration mode frequencies to measure rotation rates and typically have complex modes of vibration for the mechanical microstructures. Although there are many reports on how to exactly tune the drive and sense modes of vibration to maximize sensitivity of micromachined gyroscope, there are only few reports on the detailed analysis of modes of vibration. Modes of vibration are strongly dependent on the design parameters of the mechanical structure of the gyroscope including the dimension of the proof mass, types and dimensions of the suspension, and residual mechanical stress of the high aspect-ratio polysilicon film used to form the microstructures of the micromachined gyroscope. In this paper, an electrostatic drive and capacitive sense in-plane decoupled gyroscope for measuring vertical angular velocity is proposed to study the effects of the geometrical variables on modes of vibration. Finite-element analysis (FEA) simulation was performed on simplifiedmodel of the in-plane decoupled micromachined gyroscope microstructure. For optimal result the drive-mode and sense-mode suspensions of the micromachined gyroscope should be fabricated from thick polysilicon microstructure to give large aspect ratio suspension systems for the in-plane decoupled micromachined gyroscope. Folded-beam suspension design is recommended for the drive-mode suspension in order to relieve the residual stress of the thick polysilicon film for high aspect-ratio micromachine dgyroscope. It is critical to control the process variations of the suspension beam dimension, especially the beam width variation in order to achieve the goal of accurately control resonant frequencies of micromachined gyrocope.

  14. Study on the change of aspect ratios of small surface cracks emanated from a toe of corner boxing; Mawashi yosetsudome tanbu kara hassei denpasuru bishi bisho hyomen kiretsu no aspect hi henka ni kansuru kenkyu

    Energy Technology Data Exchange (ETDEWEB)

    Toyosada, M.; Yamaguchi, K.; Takeda, K.; Watanabe, Y. [Kyushu University, Fukuoka (Japan). Faculty of Engineering


    The fatigue test of specimens with a stiffener was carried out to examine the change in aspect ratio (crack depth/length) of fatigue cracks in a stress concentration field and residual stress field. The aspect ratio of surface cracks just after generation can be represented with the single virtual surface crack with the same value as K value at the deepest point considering an interference effect from near cracks. No discontinuous change in K value is found at the deepest point even during growth and combination of cracks on a surface. The change in K value at the deepest point is thus the criterion to represent growth and combination of surface cracks considering the interference effect. The change in aspect ratio of the typical single virtual surface crack linearly decreases with an increase in crack depth. The shape of surface cracks generating and growing in a residual stress field is more flat than that in no residual stress field. In addition, in a residual stress field, surface cracks are longer at the same crack depth, and fatigue lives are shorter. 7 refs., 12 figs.

  15. Droplet Depinning on Inclined Surfaces at High Reynolds Numbers (United States)

    White, Edward; Singh, Natasha; Lee, Sungyon


    Contact angle hysteresis enables a sessile liquid drop to adhere to a solid surface when the surface is inclined, the drop is exposed to gas-phase flow, or the drop is exposed to both forcing modalities. Previous work by Schmucker and White (2012.DFD.M4.6) identified critical depinning Weber numbers for water drops subject to gravity- and wind-dominated forcing. This work extends the Schmucker and White data and finds the critical depinning Weber number obeys a two-slope linear model. Under pure wind forcing at Reynolds numbers above 1500 and with zero surface inclination, Wecrit = 8.0 . For non-zero inclinations, α, Wecrit decreases proportionally to A Bo sinα where A is the drop aspect ratio and Bo is its Bond number. The same relationship holds for α behavior. Supported by the National Science Foundation through Grant CBET-1605947.

  16. Mechanical Design of High Lift Systems for High Aspect Ratio Swept Wings (United States)

    Rudolph, Peter K. C.


    The NASA Ames Research Center is working to develop a methodology for the optimization and design of the high lift system for future subsonic airliners with the involvement of two partners. Aerodynamic analysis methods for two dimensional and three dimensional wing performance with flaps and slats deployed are being developed through a grant with the aeronautical department of the University of California Davis, and a flap and slat mechanism design procedure is being developed through a contract with PKCR, Inc., of Seattle, WA. This report documents the work that has been completed in the contract with PKCR on mechanism design. Flap mechanism designs have been completed for seven (7) different mechanisms with a total of twelve (12) different layouts all for a common single slotted flap configuration. The seven mechanisms are as follows: Simple Hinge, Upside Down/Upright Four Bar Linkage (two layouts), Upside Down Four Bar Linkages (three versions), Airbus A330/340 Link/Track Mechanism, Airbus A320 Link/Track Mechanism (two layouts), Boeing Link/Track Mechanism (two layouts), and Boeing 767 Hinged Beam Four Bar Linkage. In addition, a single layout has been made to investigate the growth potential from a single slotted flap to a vane/main double slotted flap using the Boeing Link/Track Mechanism. All layouts show Fowler motion and gap progression of the flap from stowed to a fully deployed position, and evaluations based on spanwise continuity, fairing size and number, complexity, reliability and maintainability and weight as well as Fowler motion and gap progression are presented. For slat design, the options have been limited to mechanisms for a shallow leading edge slat. Three (3) different layouts are presented for maximum slat angles of 20 deg, 15 deg and 1O deg all mechanized with a rack and pinion drive similar to that on the Boeing 757 airplane. Based on the work of Ljungstroem in Sweden, this type of slat design appears to shift the lift curve so that

  17. Maintenance oriented tokamak reactor with low activation material and high aspect ratio configuration

    International Nuclear Information System (INIS)

    Nishio, S.; Ueda, S.; Aoki, I.


    Some of the difficulties of maintenance of a tokamak system are due to the radioactivity of its materials and the complexity of its configuration. To mitigate the difficulties, very low activation SiC/SiC composite material and a torus configuration with a high aspect ratio of eight are introduced. The torus system is divided radially into equal sectors, each of which forms an assembling unit. All piping and feeder systems are shifted to the spacious central torus region. The new concept is called DREAM tokamak reactor, which is an acronym for DRastically EAsy Maintenance. The maximum toroidal field strength of 20 T and the plasma major and minor radii of 16 m and 2 m lead to a high fusion power of 5.5 GW, under moderate physics constraints such as an MHD safety factor of three, a Troyon factor of three for the beta limit and an energy confinement time enhancement factor of two. (author)

  18. Electrochemical CO2reduction on Au surfaces: mechanistic aspects regarding the formation of major and minor products. (United States)

    Cave, Etosha R; Montoya, Joseph H; Kuhl, Kendra P; Abram, David N; Hatsukade, Toru; Shi, Chuan; Hahn, Christopher; Nørskov, Jens K; Jaramillo, Thomas F


    In the future, industrial CO 2 electroreduction using renewable energy sources could be a sustainable means to convert CO 2 and water into commodity chemicals at room temperature and atmospheric pressure. This study focuses on the electrocatalytic reduction of CO 2 on polycrystalline Au surfaces, which have high activity and selectivity for CO evolution. We explore the catalytic behavior of polycrystalline Au surfaces by coupling potentiostatic CO 2 electrolysis experiments in an aqueous bicarbonate solution with high sensitivity product detection methods. We observed the production of methanol, in addition to detecting the known products of CO 2 electroreduction on Au: CO, H 2 and formate. We suggest a mechanism that explains Au's evolution of methanol. Specifically, the Au surface does not favor C-O scission, and thus is more selective towards methanol than methane. These insights could aid in the design of electrocatalysts that are selective for CO 2 electroreduction to oxygenates over hydrocarbons.

  19. Etching of Silicon in HBr Plasmas for High Aspect Ratio Features (United States)

    Hwang, Helen H.; Meyyappan, M.; Mathad, G. S.; Ranade, R.


    Etching in semiconductor processing typically involves using halides because of the relatively fast rates. Bromine containing plasmas can generate high aspect ratio trenches, desirable for DRAM and MEMS applications, with relatively straight sidewalk We present scanning electron microscope images for silicon-etched trenches in a HBr plasma. Using a feature profile simulation, we show that the removal yield parameter, or number of neutrals removed per incident ion due to all processes (sputtering, spontaneous desorption, etc.), dictates the profile shape. We find that the profile becomes pinched off when the removal yield is a constant, with a maximum aspect ratio (AR) of about 5 to 1 (depth to height). When the removal yield decreases with increasing ion angle, the etch rate increases at the comers and the trench bottom broadens. The profiles have ARs of over 9:1 for yields that vary with ion angle. To match the experimentally observed etched time of 250 s for an AR of 9:1 with a trench width of 0.135 microns, we find that the neutral flux must be 3.336 x 10(exp 17)sq cm/s.

  20. Manufacture of high aspect ratio micro-pillar wall shear stress sensor arrays (United States)

    Gnanamanickam, Ebenezer P.; Sullivan, John P.


    In the field of experimental fluid mechanics the measurement of unsteady, distributed wall shear stress has proved historically challenging. Recently, sensors based on an array of flexible micro-pillars have shown promise in carrying out such measurements. Similar sensors find use in other applications such as cellular mechanics. This work presents a manufacturing technique that can manufacture micro-pillar arrays of high aspect ratio. An electric discharge machine (EDM) is used to manufacture a micro-drilling tool. This micro-drilling tool is used to form holes in a wax sheet which acts as the mold for the micro-pillar array. Silicone rubber is cast in these molds to yield a micro-pillar array. Using this technique, micro-pillar arrays with a maximum aspect ratio of about 10 have been manufactured. Manufacturing issues encountered, steps to alleviate them and the potential of the process to manufacture similar micro-pillar arrays in a time-efficient manner are also discussed.

  1. A high-aspect-ratio design for the International Thermonuclear Engineering Reactor

    International Nuclear Information System (INIS)

    Wesley, J.C.


    Design features and performance parameters for HARD - the high-aspect-ratio (A = 4) International Thermonuclear Engineering Reactor (ITER) design variant developed by the U. S. ITER Team - are presented. The HARD design makes it possible for ITER to achieve both the ignition/extended-burn and the steady-state/technology-testing performance goals set forth in the ITER Terms of Reference. These performance capabilities are obtained in a device that is otherwise similar in concept, size and cost to the low-aspect-ratio (A = 2.8) ITER design defined during the ITER Conceptual Design Activity (CDA). HARD is based on the same physics and engineering guidelines as the CDA design and achieves the same ignition performance (ignition margin evaluated against ITER-89P confinement scaling) with inductively-driven plasmas as ITER CDA, but with much greater margin for inductive sustainment of the pulse duration. With non-inductive current drive, HARD operates at lower plasma current and higher plasma density and bootstrap current fraction than ITER CDA, is less constrained by beta limit and divertor considerations, and has increased peaking of the neutron wall load at the test module location. These factors give HARD a much better potential than ITER CDA to achieve the steady-state operation and 1 MWa/m 2 technology-testing fluence goals of the ITER objectives

  2. Surface modification of lignocellulosic fibers using high-frequency ultrasound (United States)

    Jayant B. Gadhe; Ram B. Gupta; Thomas Elder


    Enzymatic and chemical oxidation of fiber surfaces has been reported in the literature as a method for producing medium density fiberboards without using synthetic adhesives. This work focuses on modifying the surface properties of wood fibers by the generation of free radicals using high-frequency ultrasound. A sonochemical reactor operating at 610 kHz is used to...

  3. Highly smooth Nb surfaces fabricated by buffered electropolishing

    International Nuclear Information System (INIS)

    Wu, Andy T; John Mammossor; Phillips, H.; Jean Delayen; Charles Reece; Amy Wilkerson; David Smith; Robert Ike


    It is demonstrated that highly smooth Nb surfaces can be obtained through Buffered ElectroPolishing (BEP) employing an electrolyte consisting of lactic, sulfuric, and hydrofluoric acids. Parameters that control the polishing process are optimized to achieve the smoothest surface finish with the help of surface observations using a scanning electron microscope and a Metallographic Optical Microscope (MOM). The polishing rate of BEP is determined to be 0.646 (micro)m/min that is much higher than 0.381 (micro)m/min achieved by the conventional ElectroPolishing (EP) process widely used in the Superconducting Radio Frequency (SRF) community. A high precision and large scan area 3-D profilometer is used to view morphology of the treated Nb surfaces. Statistical data, such as, rms, total indicator runout, and arithmetic mean deviation of the Nb surfaces are extracted from the profilometer images. It is found that Nb surfaces treated by BEP are an order of magnitude smoother than those treated by the optimized EP process. The chemical composition of the Nb surfaces after BEP is analyzed by static and dynamic Secondary Ion Mass Spectrometer (SIMS) systems. Cracking patterns of the Nb surfaces under different primary ion sources of Ga + , Au + , and Ar + are reported. The depth profile of the surface niobium oxides is studied through continuously monitoring niobium and its relevant oxides' peaks as a function of time. Dynamic SIMS results imply that the surface oxide structure of Nb may be more complicated than what usually believed and can be inhomogeneous. Preliminary results of BEP on Nb SRF single cell cavities and half-cells are reported. It is shown that smooth and bright surfaces can be obtained in 30 minutes when the electric field inside a SRF cavity is uniform during a BEP process. This study reveals that BEP is a highly promising technique for surface treatment on Nb SRF cavities to be used in particle accelerators

  4. NOAA High-Resolution Sea Surface Temperature (SST) Analysis Products (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — This archive covers two high resolution sea surface temperature (SST) analysis products developed using an optimum interpolation (OI) technique. The analyses have a...

  5. Alternative aggregates and materials for high friction surface treatments. (United States)


    The State of Florida has used high friction surface treatments (HFSTs) since 2006 to reduce wet weather crashes on : tight curves and intersections and to maintain bridge decks; however, the Florida Department of Transportation : (FDOT) has reported ...

  6. Evaluation of high friction surface locations in Kansas. (United States)


    In 2009, the Kansas Department of Transportation entered into an agreement with the Federal Highway : Administration to fulfill the requirements of the High Friction Surface Materials Enhancing Safety at Horizontal : Curves on the National Highway Sy...

  7. Public satisfaction survey of high friction surface treatment. (United States)


    Missouri adults in Callaway County were surveyed to capture their satisfaction with a local high friction surface treatment on : westbound US 54. This treatment was implemented in Project J5P3012. The results are weighted proportionally to the county...

  8. Surface charge compensation for a highly charged ion emission microscope

    International Nuclear Information System (INIS)

    McDonald, J.W.; Hamza, A.V.; Newman, M.W.; Holder, J.P.; Schneider, D.H.G.; Schenkel, T.


    A surface charge compensation electron flood gun has been added to the Lawrence Livermore National Laboratory (LLNL) highly charged ion (HCI) emission microscope. HCI surface interaction results in a significant charge residue being left on the surface of insulators and semiconductors. This residual charge causes undesirable aberrations in the microscope images and a reduction of the Time-Of-Flight (TOF) mass resolution when studying the surfaces of insulators and semiconductors. The benefits and problems associated with HCI microscopy and recent results of the electron flood gun enhanced HCI microscope are discussed

  9. Partial compensation interferometry for measurement of surface parameter error of high-order aspheric surfaces (United States)

    Hao, Qun; Li, Tengfei; Hu, Yao


    Surface parameters are the properties to describe the shape characters of aspheric surface, which mainly include vertex radius of curvature (VROC) and conic constant (CC). The VROC affects the basic properties, such as focal length of an aspheric surface, while the CC is the basis of classification for aspheric surface. The deviations of the two parameters are defined as surface parameter error (SPE). Precisely measuring SPE is critical for manufacturing and aligning aspheric surface. Generally, SPE of aspheric surface is measured directly by curvature fitting on the absolute profile measurement data from contact or non-contact testing. And most interferometry-based methods adopt null compensators or null computer-generated holograms to measure SPE. To our knowledge, there is no effective way to measure SPE of highorder aspheric surface with non-null interferometry. In this paper, based on the theory of slope asphericity and the best compensation distance (BCD) established in our previous work, we propose a SPE measurement method for high-order aspheric surface in partial compensation interferometry (PCI) system. In the procedure, firstly, we establish the system of two element equations by utilizing the SPE-caused BCD change and surface shape change. Then, we can simultaneously obtain the VROC error and CC error in PCI system by solving the equations. Simulations are made to verify the method, and the results show a high relative accuracy.

  10. Microwave dynamics of high aspect ratio superconducting nanowires studied using self-resonance (United States)

    Santavicca, Daniel F.; Adams, Jesse K.; Grant, Lierd E.; McCaughan, Adam N.; Berggren, Karl K.


    We study the microwave impedance of extremely high aspect ratio (length/width ≈ 5000) superconducting niobium nitride nanowires. The nanowires are fabricated in a compact meander geometry that is in series with the center conductor of a 50 Ω coplanar waveguide transmission line. The transmission coefficient of the sample is measured up to 20 GHz. At high frequency, a peak in the transmission coefficient is seen. Numerical simulations show that this is a half-wave resonance along the length of the nanowire, where the nanowire acts as a high impedance, slow wave transmission line. This resonance sets the upper frequency limit for these nanowires as inductive elements. Fitting simulations to the measured resonance enables a precise determination of the nanowire's complex sheet impedance at the resonance frequency. The real part is a measure of dissipation, while the imaginary part is dominated by kinetic inductance. We characterize the dependence of the sheet resistance and sheet inductance on both temperature and current and compare the results to recent theoretical predictions for disordered superconductors. These results can aid in the understanding of high frequency devices based on superconducting nanowires. They may also lead to the development of novel superconducting devices such as ultra-compact resonators and slow-wave structures.

  11. Safety aspects of preoperative high-dose glucocorticoid in primary total knee replacement

    DEFF Research Database (Denmark)

    Jørgensen, C C; Pitter, F T; Kehlet, H


    Background: Preoperative single high-dose glucocorticoid may have early outcome benefits in total hip arthroplasty (THA) and knee arthroplasty (TKA), but long-term safety aspects have not been evaluated. Methods: From October 2013, the departments reporting to the prospective Lundbeck Foundation...... Database for Fast-track Hip and Knee Replacement introduced preoperative methylprednisolone (MP) 125 mg as part of a multimodal analgesic protocol in TKA. We analysed the risk of length of hospital stay (LOS) >4 days, 30 and 90 day readmissions in patients with MP vs patients having TKA before the use...... of MP and adjusted for comorbidity and place of surgery. An unadjusted comparison was specifically done to evaluate deep prosthetic infections. Results: Of a total of 3927 TKA procedures, 1442 received MP. Median LOS was 2 days in both groups, but the fraction with LOS >4 days was 6.0% vs 11.5% (P

  12. Measurement and simulation of jet mass caused by a high-aspect ratio pertubation

    Energy Technology Data Exchange (ETDEWEB)

    Keiter, Paul A [Los Alamos National Laboratory; Cooley, James [Los Alamos National Laboratory; Kyrala, George [Los Alamos National Laboratory; Wilson, Doug [Los Alamos National Laboratory; Blue, Brent [LLNL/GA; Elliott, Jim [LLNL; Edwards, John [LLNL; Robey, Harry [LLNL; Spears, Brian [LLNL


    Inertial confinement fusion (ICF) capsule performance can be negatively impacted by the presence of hydrodynamic instabilities. To perform a gas fill on an ICF capsule current plans involve drilling a small hole and inserting a fill tube to inject the gas mixture into the capsule. This introduces a perturbation on the capsule, which can seed hydrodynamic instabilities. The small hole can cause jetting of the shell material into the gas, which might adversely affect the capsule performance. We have performed simulations and experiments to study the hydrodynamic evolution of jets from high-aspect ratio holes, such as the fill tube hole. Although simulations using cold materials over predict the amount of mass in the jet, when a reasonable amount of preheat (< 1 eV) is introduced, the simulations are in better agreement with the experiment.

  13. Scaling model for high-aspect-ratio microballoon direct-drive implosions at short laser wavelengths

    International Nuclear Information System (INIS)

    Schirmann, D.; Juraszek, D.; Lane, S.M.; Campbell, E.M.


    A scaling model for hot spherical ablative implosions in direct-drive mode is presented. The model results have been compared with experiments from LLE, ILE, and LLNL. Reduction of the neutron yield due to illumination nonuniformities is taken into account by the assumption that the neutron emission is cut off when the gas shock wave reflected off the center meets the incoming pusher, i.e., at a time when the probability of shell breakup is greatly enhanced. The main advantage of this semiempirical scaling model is that it elucidates the principal features of these simple implosions and permits one to estimate very quickly the performance of a high-aspect-ratio direct-drive target illuminated by short-wavelength laser light. (Author)

  14. Extensive Air Showers High Energy Phenomena and Astrophysical Aspects - A Tutorial, Reference Manual and Data Book

    CERN Document Server

    Grieder, Peter K.F


    Extensive air showers are a very unique phenomenon. In the more than six decades since their discovery by Auger et al. we have learned a great deal about these extremely energetic events and gained deep insights into high-energy phenomena, particle physics and astrophysics. In this Tutorial, Reference Manual and Data Book Peter K. F. Grieder provides the reader with a comprehensive view of the phenomenology and facts of the various types of interactions and cascades, theoretical background, experimental methods, data evaluation and interpretation, and air shower simulation. He discusses astrophysical aspects of the primary radiation and addresses the questions that continue to puzzle researchers. The book is divided into two parts, each in its own separate volume: Part I in Volume I deals mainly with the basic theoretical framework of the processes that determine an air shower and ends with a summary of ways to extract information on the primary radiation from air shower observations. It also presents a compi...

  15. Pilot Study of Inhaled Aerosols Targeted via Magnetic Alignment of High Aspect Ratio Particles in Rabbits

    Directory of Open Access Journals (Sweden)

    Gillian E. S. Redman


    Full Text Available Recently, inhaled pharmaceutical aerosols have seen increased investigation in the treatment of lung cancer, where the inability to deliver adequate therapeutic drug concentrations to tumour sites may be overcome with improved targeted delivery to the site of the tumour. In this study, the feasibility of magnetically targeted delivery of high aspect ratio particles loaded with iron oxide nanoparticles was studied in 19 New Zealand White rabbits. Half of the exposed rabbits had a magnetic field placed externally over their right lung. Iron sensitive magnetic resonance images of the lungs were acquired to determine the iron concentrations in the right and left lung of each animal. The right/left ratio increased in the middle and basal regions of the lung where, due to the morphology of the rabbit lung, this method of targeting is most effective. With further optimization, this technique could be an effective method for increasing the dose of drug delivered to a specific site within the lung.

  16. Gust response analysis and wind tunnel test for a high-aspect ratio wing

    Directory of Open Access Journals (Sweden)

    Liu Yi


    Full Text Available A theoretical nonlinear aeroelastic response analysis for a flexible high-aspect ratio wing excited by harmonic gust load is presented along with a companion wind tunnel test. A multidisciplinary coupled numerical calculation is developed to simulate the flexible model wing undergoing gust load in the time domain via discrete nonlinear finite element structural dynamic analysis and nonplanar unsteady vortex lattice aerodynamic computation. A dynamic perturbation analysis about a nonlinear static equilibrium is also used to determine the small perturbation flutter boundary. A novel noncontact 3-D camera measurement analysis system is firstly used in the wind tunnel test to obtain the spatial large deformation and responses. The responses of the flexible wing under different static equilibrium states and frequency gust loads are discussed. The fair to good quantitative agreements between the theoretical and experimental results demonstrate that the presented analysis method is an acceptable way to predict the geometrically nonlinear gust response for flexible wings.

  17. A hypothetical model for predicting the toxicity of high aspect ratio nanoparticles (HARN) (United States)

    Tran, C. L.; Tantra, R.; Donaldson, K.; Stone, V.; Hankin, S. M.; Ross, B.; Aitken, R. J.; Jones, A. D.


    The ability to predict nanoparticle (dimensional structures which are less than 100 nm in size) toxicity through the use of a suitable model is an important goal if nanoparticles are to be regulated in terms of exposures and toxicological effects. Recently, a model to predict toxicity of nanoparticles with high aspect ratio has been put forward by a consortium of scientists. The High aspect ratio nanoparticles (HARN) model is a platform that relates the physical dimensions of HARN (specifically length and diameter ratio) and biopersistence to their toxicity in biological environments. Potentially, this model is of great public health and economic importance, as it can be used as a tool to not only predict toxicological activity but can be used to classify the toxicity of various fibrous nanoparticles, without the need to carry out time-consuming and expensive toxicology studies. However, this model of toxicity is currently hypothetical in nature and is based solely on drawing similarities in its dimensional geometry with that of asbestos and synthetic vitreous fibres. The aim of this review is two-fold: (a) to present findings from past literature, on the physicochemical property and pathogenicity bioassay testing of HARN (b) to identify some of the challenges and future research steps crucial before the HARN model can be accepted as a predictive model. By presenting what has been done, we are able to identify scientific challenges and research directions that are needed for the HARN model to gain public acceptance. Our recommendations for future research includes the need to: (a) accurately link physicochemical data with corresponding pathogenicity assay data, through the use of suitable reference standards and standardised protocols, (b) develop better tools/techniques for physicochemical characterisation, (c) to develop better ways of monitoring HARN in the workplace, (d) to reliably measure dose exposure levels, in order to support future epidemiological

  18. Is Judgement of Biotechnological Ethical Aspects Related to High School Students' Knowledge? (United States)

    Črne-Hladnik, Helena; Hladnik, Aleš; Javornik, Branka; Košmelj, Katarina; Peklaj, Cirila


    Quantitative and qualitative studies of various aspects of the perception of biotechnology were conducted among 469 Slovenian high school students of average age 17 years. Our research aimed to explore relationships among students' pre-knowledge of molecular and human genetics, and their attitudes to four specific biotechnological applications. These applications-Bt corn, genetically modified (GM) salmon, somatic and germ line gene therapy (GT)-were investigated from the viewpoints of usefulness, moral acceptance and risk perception. In addition, patterns and quality of moral reasoning related to the biotechnological applications from the aspect of moral acceptability were examined. Clear gender differences were found regarding the relationship between our students' pre-knowledge of genetics and their attitudes to biotechnological applications. While females with a better genetics background expressed a higher risk perception in the case of GM salmon, their similarly well-educated male colleagues emphasized the risk associated with the use of germ line GT. With all four biotechnological applications, patterns of both rationalistic-deontological and teleological-and intuitive moral reasoning were identified. Students with poorer genetics pre-knowledge applied an intuitive pattern of moral reasoning more frequently than their peers with better pre-knowledge. A pattern of emotive reasoning was detected only in the case of GM salmon. A relatively low quality of students' moral reasoning, as demonstrated by their brief and small number of supporting justifications (explanations), show that there is a strong need for practising skills of argumentation about socio-scientific issues in Slovenian high schools on a much larger scale. The implications for future research and classroom applications are discussed.

  19. Fabrication of high-aspect-ratio nano structures using a nano x-ray shadow mask

    International Nuclear Information System (INIS)

    Kim, Yong Chul; Lee, Seung S


    This paper describes a novel method for the fabrication of high-aspect-ratio nano structures (HAR-nano structures) using a nano x-ray shadow mask and deep x-ray lithography (DXRL). The nano x-ray shadow mask is fabricated by depositing an x-ray absorber layer (Au, 3 µm) onto the back side of a nano shadow mask. The nano shadow mask is produced with nano-sized apertures whose dimensions are reduced to several tens of nanometers by the accumulation of low-stress silicon nitride (Si x N y ) using the LPCVD process on the shadow mask. A shadow mask containing apertures with a size of 1 µm is fabricated on a bulk micromachined Si x N y membrane. The thickness of an absorber layer must be in the range of several tens of micrometers in order to obtain a contrast of more than 100 for the conventional DXRL process at the Pohang Light Source (PLS). However, a 3 µm thick absorber layer can provide a sufficient contrast if the modified DXRL of the central beam-stop method is used, which blocks high-energy x-rays. A nano shadow mask with 30 nm sized apertures is fabricated and a nano x-ray shadow mask with 250 nm sized apertures is fabricated by depositing a 3 µm thick absorber layer on a nano shadow mask with 500 nm sized apertures. HAR-nano structures (circles with a diameter of 420 nm and lines with a width of 274 nm) with aspect ratios of over 10:1 on a 3.2 µm SU-8 are successfully fabricated by using the nano x-ray shadow mask and the central beam-stop method

  20. Dewetting of liquids on ceramic surfaces at high temperatures. (United States)

    Ravishankar, N; Gilliss, Shelley R; Carter, C Barry


    The influence of surface structure and chemistry on high-temperature dewetting of silicate liquids on ceramic surfaces has been investigated. Model systems based on well-defined crystallography and known chemistry have been used to illustrate the effect of surface roughness and chemistry on the dewetting process. Reconstructed ceramic surfaces provide ideal substrates to study effects of surface roughness. It has been shown that the morphology of dewet droplets depend on the length scale and the crystallography of the facets on the surface. Complex pattern formation due to solute redistribution during dewetting is illustrated in the case of SiO2 dewetting on (001) rutile substrates. The role of kinetics on the dewetting process has also been clarified.

  1. Field emission from the surface of highly ordered pyrolytic graphite

    Energy Technology Data Exchange (ETDEWEB)

    Knápek, Alexandr, E-mail: [Institute of Scientific Instruments of the ASCR, v.v.i., Královopolská 147, Brno (Czech Republic); Sobola, Dinara; Tománek, Pavel [Department of Physics, FEEC, Brno University of Technology, Technická 8, Brno (Czech Republic); Pokorná, Zuzana; Urbánek, Michal [Institute of Scientific Instruments of the ASCR, v.v.i., Královopolská 147, Brno (Czech Republic)


    Highlights: • HOPG shreds were created and analyzed in the UHV conditions. • Current-voltage measurements have been done to confirm electron tunneling, based on the Fowler-Nordheim theory. • Surface was characterized by other surface evaluation methods, in particular by: SNOM, SEM and AFM. - Abstract: This paper deals with the electrical characterization of highly ordered pyrolytic graphite (HOPG) surface based on field emission of electrons. The effect of field emission occurs only at disrupted surface, i.e. surface containing ripped and warped shreds of the uppermost layers of graphite. These deformations provide the necessary field gradients which are required for measuring tunneling current caused by field electron emission. Results of the field emission measurements are correlated with other surface characterization methods such as scanning near-field optical microscopy (SNOM) or atomic force microscopy.

  2. High contact angle hysteresis of superhydrophobic surfaces: Hydrophobic defects (United States)

    Chang, Feng-Ming; Hong, Siang-Jie; Sheng, Yu-Jane; Tsao, Heng-Kwong


    A typical superhydrophobic surface is essentially nonadhesive and exhibits very low water contact angle (CA) hysteresis, so-called Lotus effect. However, leaves of some plants such as scallion and garlic with an advancing angle exceeding 150° show very serious CA hysteresis. Although surface roughness and epicuticular wax can explain the very high advancing CA, our analysis indicates that the unusual hydrophobic defect, diallyl disulfide, is the key element responsible for contact line pinning on allium leaves. After smearing diallyl disulfide on an extended polytetrafluoroethylene (PTFE) film, which is originally absent of CA hysteresis, the surface remains superhydrophobic but becomes highly adhesive.

  3. Comprehensive surface treatment of high-speed steel tool (United States)

    Fedorov, Sergey V.; Aleshin, Sergey V.; Swe, Min Htet; Abdirova, Raushan D.; Kapitanov, Alexey V.; Egorov, Sergey B.


    One of the promising directions of hardening of high-speed steel tool is the creation on their surface of the layered structures with the gradient of physic-chemical properties between the wear-resistant coatings to the base material. Among the methods of such surface modification, a special process takes place based on the use of pulsed high-intensity charged particle beams. The high speed of heating and cooling allows structural-phase transformations in the surface layer, which cannot be realized in a stationary mode. The treatment was conducted in a RITM-SP unit, which constitutes a combination of a source of low-energy high-current electron beams "RITM" and two magnetron spraying systems on a single vacuum chamber. The unit enables deposition of films on the surface of the desired product and subsequent liquid-phase mixing of materials of the film and the substrate by an intense pulse electron beam. The article discusses features of the structure of the subsurface layer of high-speed steel M2, modified by surface alloying of a low-energy high-current electron beam, and its effect on the wear resistance of the tool when dry cutting hard to machine Nickel alloy. A significant decrease of intensity of wear of high-speed steel with combined treatment happens due to the displacement of the zone of wear and decrease the radius of rounding of the cutting edge because of changes in conditions of interaction with the material being treated.

  4. Surfaces for high heat dissipation with no Leidenfrost limit (United States)

    Sajadi, Seyed Mohammad; Irajizad, Peyman; Kashyap, Varun; Farokhnia, Nazanin; Ghasemi, Hadi


    Heat dissipation from hot surfaces through cooling droplets is limited by the Leidenfrost point (LFP), in which an insulating vapor film prevents direct contact between the cooling droplet and the hot surface. A range of approaches have been developed to raise this limit to higher temperatures, but the limit still exists. Recently, a surface architecture, decoupled hierarchical structure, was developed that allows the suppression of LFP completely. However, heat dissipation by the structure in the low superheat region was inferior to other surfaces and the structure required an extensive micro/nano fabrication procedure. Here, we present a metallic surface structure with no LFP and high heat dissipation capacity in all temperature ranges. The surface features the nucleate boiling phenomenon independent of the temperature with an approximate heat transfer coefficient of 20 kW m-2 K-1. This surface is developed in a one-step process with no micro/nano fabrication. We envision that this metallic surface provides a unique platform for high heat dissipation in power generation, photonics/electronics, and aviation systems.

  5. Two dimensional simulation of high power laser-surface interaction

    International Nuclear Information System (INIS)

    Goldman, S.R.; Wilke, M.D.; Green, R.E.L.; Johnson, R.P.; Busch, G.E.


    For laser intensities in the range of 10 8 --10 9 W/cm 2 , and pulse lengths of order 10 microsec or longer, the authors have modified the inertial confinement fusion code Lasnex to simulate gaseous and some dense material aspects of the laser-matter interaction. The unique aspect of their treatment consists of an ablation model which defines a dense material-vapor interface and then calculates the mass flow across this interface. The model treats the dense material as a rigid two-dimensional mass and heat reservoir suppressing all hydrodynamic motion in the dense material. The computer simulations and additional post-processors provide predictions for measurements including impulse given to the target, pressures at the target interface, electron temperatures and densities in the vapor-plasma plume region, and emission of radiation from the target. The authors will present an analysis of some relatively well diagnosed experiments which have been useful in developing their modeling. The simulations match experimentally obtained target impulses, pressures at the target surface inside the laser spot, and radiation emission from the target to within about 20%. Hence their simulational technique appears to form a useful basis for further investigation of laser-surface interaction in this intensity, pulse-width range. This work is useful in many technical areas such as materials processing

  6. Large-Eddy Simulation of Flow and Pollutant Dispersion in High-Aspect-Ratio Urban Street Canyons with Wall Model (United States)

    Li, Xian-Xiang; Liu, Chun-Ho; Leung, Dennis Y. C.


    A large-eddy simulation (LES) with a one-equation subgrid-scale (SGS) model was developed to investigate the flow field and pollutant dispersion inside street canyons of high aspect ratio (AR). A 1/7th power-law wall model was implemented near rigid walls to mitigate the demanding near-wall resolution requirements in LES. This LES model had been extensively validated against experimental results for street canyons of AR = 1 and 2 before it was applied to the cases of AR = 3 and 5. A ground-level passive pollutant line source, located in the middle of the street, was used to simulate vehicular emissions. Three and five vertically aligned primary recirculations were developed in the street canyons of AR 3 and 5, respectively. The ground-level mean wind speed was less than 0.5% of the free stream value, which makes it difficult for the pollutant to be transported upward for removal. High pollutant concentration and variance were found near the buildings where the air flow is upwards. It was found that the velocity fluctuation, pollutant concentration and variance were all closely related to the interactions between the primary recirculations and/or the free surface layer. Several quantities, which are non-linear functions of AR, were introduced to quantify the air quality in street canyons of different configurations.

  7. Laboratory Activity Worksheet to Train High Order Thinking Skill of Student on Surface Chemistry Lecture (United States)

    Yonata, B.; Nasrudin, H.


    A worksheet has to be a set with activity which is help students to arrange their own experiments. For this reason, this research is focused on how to train students’ higher order thinking skills in laboratory activity by developing laboratory activity worksheet on surface chemistry lecture. To ensure that the laboratory activity worksheet already contains aspects of the higher order thinking skill, it requires theoretical and empirical validation. From the data analysis results, it shows that the developed worksheet worth to use. The worksheet is worthy of theoretical and empirical feasibility. This conclusion is based on the findings: 1) Assessment from the validators about the theoretical feasibility aspects in the category is very feasible with an assessment range of 95.24% to 97.92%. 2) students’ higher thinking skill from N Gain values ranges from 0.50 (enough) to 1.00 (high) so it can be concluded that the laboratory activity worksheet on surface chemistry lecture is empirical in terms of worth. The empirical feasibility is supported by the responses of the students in very reasonable categories. It is expected that the laboratory activity worksheet on surface chemistry lecture can train students’ high order thinking skills for students who program surface chemistry lecture.

  8. The high-temperature vaporization/decomposition of actinide materials: fundamental and technological aspects

    International Nuclear Information System (INIS)

    Haire, R.G.


    The unique and variable chemistry exhibited across the actinide series offers a scientifically challenging group of elements. Investigations of their high-temperature materials science and thermodynamics can provide important insights into fundamental actinide science and generate critical information for technological applications. The wide variations in the physicochemical properties and the availability of the various actinide elements necessitates special experimental techniques be employed, even when investigating a single property (e.g., the enthalpy of vaporization). Experimental approaches range can from classical to novel methods to permit studies of the rarer and the more intensely radioactive members. We have developed special equipment and techniques to investigate the high-temperature, physicochemical properties of several actinides through Md, as well as the precursor elements, radium and actinium. These experimental approaches employed both alloys and solid solutions of compounds, in addition to the pure elements themselves. The vaporization/decomposition of compounds and the sublimation of the elements, together with the associated thermodynamics, are the main issues. Results for several of the actinide elements, some of the techniques employed and systematic comparisons of the thermochemical aspects of bonding are discussed to give a fuller understanding of the series as a whole. (orig.)

  9. Progress in the fabrication of high aspect ratio zone plates by soft x-ray lithography

    International Nuclear Information System (INIS)

    Divan, R.; Mancini, D. C.; Moldovan, N. A.; Lai, B.; Assoufid, L.; Leondard, Q.; Cerrina, F.


    Fabrication of Fresnel zone plates for the hard x-ray spectral region combines the challenge of high lateral resolution (∼100 nm) with a large thickness requirement for the phase-shifting material (0.5-3 (micro)m). For achieving a high resolution, the initial mask was fabricated by e-beam lithography and gold electroforming. To prevent the collapse of the structures between the developing and electroforming processes, drying was completely eliminated. Fabrication errors, such as nonuniform gold electroplating and collapse of structures, were systematically analyzed and largely eliminated. We optimized the exposure and developing processes for 950k and 2200k polymethylmethacrylate of different thicknesses and various adhesion promoters. We discuss the effects of these fabrication steps on the zone plate's resolution and aspect ratio. Fresnel zone plates with 110 nm outermost zone width, 150 (micro)m diameter, and 1.3 (micro)m gold thickness were fabricated. Preliminary evaluation of the FZPs was done by scanning electron microscopy and atomic force microscopy. The FZP focusing performance was characterized at the Advanced Photon Source at Argonne National Laboratory

  10. Aeroelastic Optimization Design for High-Aspect-Ratio Wings with Large Deformation

    Directory of Open Access Journals (Sweden)

    Changchuan Xie


    Full Text Available This paper presents a framework of aeroelastic optimization design for high-aspect-ratio wing with large deformation. A highly flexible wing model for wind tunnel test is optimized subjected to multiple aeroelastic constraints. Static aeroelastic analysis is carried out for the beamlike wing model, using a geometrically nonlinear beam formulation coupled with the nonplanar vortex lattice method. The flutter solutions are obtained using the P-K method based on the static equilibrium configuration. The corresponding unsteady aerodynamic forces are calculated by nonplanar doublet-lattice method. This paper obtains linear and nonlinear aeroelastic optimum results, respectively, by the ISIGHT optimization platform. In this optimization problem, parameters of beam cross section are chosen as the design variables to satisfy the displacement, flutter, and strength requirements, while minimizing wing weight. The results indicate that it is necessary to consider geometrical nonlinearity in aeroelastic optimization design. In addition, optimization strategies are explored to simplify the complex optimization process and reduce the computing time. Different criterion values are selected and studied for judging the effects of the simplified method on the computing time and the accuracy of results. In this way, the computing time is reduced by more than 30% on the premise of ensuring the accuracy.

  11. Aspects of Teacher Education that Affect Student Success in Arizona Public High Schools

    Directory of Open Access Journals (Sweden)

    Faith Elizabeth Andreasen


    Full Text Available This study was designed to investigate what aspects of teacher education (if any affect student success. Questionnaires were mailed to a random sample of high- and low-performing urban and rural public high schools across Arizona. Quantitative variables that were researched include the level of degree a teacher attains, the route a teacher chooses to achieve certification, teachers’ attendance at core-subject related workshops, teacher mentoring, and teacher collaboration using data based information to drive decision-making. Qualitative research enabled teachers to state a valuable skill learned in college that promotes student success and to reveal what they felt their current school does to promote student success. A mixed methodology approach was used to analyze the data; quantitatively through regression analysis and qualitatively through coded themes.A detailed explanation was presented with accompanying data to support the statements. The results of this research support teacher mentoring and attendance at core subject related workshops as vehicles to promote student success. This dissertation provides information for policy makers, administrators, and teachers who are invested in promoting student success.

  12. Analysis of surface degradation of high density polyethylene (HDPE ...

    Indian Academy of Sciences (India)


    Analysis of surface degradation of high density polyethylene (HDPE) insulation ... ammonium chloride as the contaminant, in high density polyethylene ..... liquid in the material. When diffusion is driven by the concentration gradient and if there is no chemical change between liquid and material, this would result in mass.

  13. Plasma–Surface Interactions Under High Heat and Particle Fluxes

    Directory of Open Access Journals (Sweden)

    Gregory De Temmerman


    Full Text Available The plasma-surface interactions expected in the divertor of a future fusion reactor are characterized by extreme heat and particle fluxes interacting with the plasma-facing surfaces. Powerful linear plasma generators are used to reproduce the expected plasma conditions and allow plasma-surface interactions studies under those very harsh conditions. While the ion energies on the divertor surfaces of a fusion device are comparable to those used in various plasma-assited deposition and etching techniques, the ion (and energy fluxes are up to four orders of magnitude higher. This large upscale in particle flux maintains the surface under highly non-equilibrium conditions and bring new effects to light, some of which will be described in this paper.

  14. The evaluation of vacuum venting and variotherm process for improving the replication by injection molding of high aspect ratio micro features for biomedical application (United States)

    Sorgato, Marco; Lucchetta, Giovanni


    The aspect ratio achievable in replicating micro features is one of the most important process characteristics and it is a major manufacturing constraint in applying injection molding in a range of micro engineering applications. Vacuum venting has been reported to be an effective technique in replicating micro features by microinjection molding. High surface-to-volume ratio and reduced dimensions of micro parts promote the instantaneous drop of melt temperature and consequently lead to incomplete filling. This study aims to investigate the effects of variotherm process, cavity evacuation and their interaction on the production of a micro fluidic filter for biomedical applications. A low-viscosity polystyrene and a cyclic olefin copolymer were molded applying a combination of mold evacuation and a rapid mold temperature variation that keeps the cavity temperature above the glass transition temperature during the injection phase. The research revealed the importance of these molding technologies in enhancing part filling and the replication quality for high aspect ratio micro features.

  15. Interferometric method for measuring high velocities of diffuse surfaces

    International Nuclear Information System (INIS)

    Maron, Y.


    An interferometric method for measuring the displacement of diffuse surfaces moving with velocities of a few microsecond is presented. The method utilizes the interference between two light beams reflected from a constant area of the moving surface at two different angles. It enables the detection of high rate velocity variations. Light source of a fairly low temporal coherence and power around 100mW is needed. (author)

  16. Surface interactions involved in flashover with high density electronegative gases.

    Energy Technology Data Exchange (ETDEWEB)

    Hodge, Keith Conquest; Warne, Larry Kevin; Jorgenson, Roy Eberhardt; Wallace, Zachariah Red; Lehr, Jane Marie


    This report examines the interactions involved with flashover along a surface in high density electronegative gases. The focus is on fast ionization processes rather than the later time ionic drift or thermalization of the discharge. A kinetic simulation of the gas and surface is used to examine electron multiplication and includes gas collision, excitation and ionization, and attachment processes, gas photoionization and surface photoemission processes, as well as surface attachment. These rates are then used in a 1.5D fluid ionization wave (streamer) model to study streamer propagation with and without the surface in air and in SF6. The 1.5D model therefore includes rates for all these processes. To get a better estimate for the behavior of the radius we have studied radial expansion of the streamer in air and in SF6. The focus of the modeling is on voltage and field level changes (with and without a surface) rather than secondary effects, such as, velocities or changes in discharge path. An experiment has been set up to carry out measurements of threshold voltages, streamer velocities, and other discharge characteristics. This setup includes both electrical and photographic diagnostics (streak and framing cameras). We have observed little change in critical field levels (where avalanche multiplication sets in) in the gas alone versus with the surface. Comparisons between model calculations and experimental measurements are in agreement with this. We have examined streamer sustaining fields (field which maintains ionization wave propagation) in the gas and on the surface. Agreement of the gas levels with available literature is good and agreement between experiment and calculation is good also. Model calculations do not indicate much difference between the gas alone versus the surface levels. Experiments have identified differences in velocity between streamers on the surface and in the gas alone (the surface values being larger).

  17. High-Density Infrared Surface Treatments of Refractories

    Energy Technology Data Exchange (ETDEWEB)

    Tiegs, T.N.


    Refractory materials play a crucial role in all energy-intensive industries and are truly a crosscutting technology for the Industries of the Future (IOF). One of the major mechanisms for the degradation of refractories and a general decrease in their performance has been the penetration and corrosion by molten metals or glass. Methods and materials that would reduce the penetration, wetting, and corrosive chemistry would significantly improve refractory performance and also maintain the quality of the processed liquid, be it metal or glass. This report presents the results of an R&D project aimed at investigating the use of high-density infrared (HDI) heating to surface treat refractories to improve their performance. The project was a joint effort between Oak Ridge National Laboratory (ORNL) and the University of Missouri-Rolla (UMR). HDI is capable of heating the near-surface region of materials to very high temperatures where sintering, diffusion, and melting can occur. The intended benefits of HDI processing of refractories were to (1) reduce surface porosity (by essentially sealing the surface to prevent liquid penetration), (2) allow surface chemistry changes to be performed by bonding an adherent coating onto the underlying refractory (in order to inhibit wetting and/or improve corrosion resistance), and (3) produce noncontact refractories with high-emissivity surface coatings.

  18. Cellulosic fibers with high aspect ratio from cornhusks via controlled swelling and alkaline penetration. (United States)

    Ma, Zhuanzhuan; Pan, Gangwei; Xu, Helan; Huang, Yiling; Yang, Yiqi


    Cellulosic fibers with high aspect ratio have been firstly obtained from cornhusks via controlled swelling in organic solvent and simultaneous tetramethylammonium hydroxide (TMAOH) post treatment within restricted depth. Cornhusks, with around 42% cellulose content, are a copious and inexpensive source for natural fibers. However, cornhusk fibers at 20tex obtained via small-molecule alkaline extraction were too coarse for textile applications. Continuous NaOH treatment would result in fine fibers but with length of about 0.5-1.5mm, too short for textile use. In this research, post treatment using TMAOH and under controlled swelling significantly reduced fineness of cornhusk fibers from 21.3±2.88 to 5.72±0.21tex. Fiber length was reduced from 105.47±10.03 to47.2±27.4mm. The cornhusk fibers had more oriented microstructures and cellulose content increased to 84.47%. Besides, cornhusk fibers had similar tenacity, longer elongation, and lower modulus compared to cotton and linen, which endowed them with durability and flexibility. Copyright © 2015 Elsevier Ltd. All rights reserved.

  19. Finite element analysis of high aspect ratio wind tunnel wing model: A parametric study (United States)

    Rosly, N. A.; Harmin, M. Y.


    Procedure for designing the wind tunnel model of a high aspect ratio (HAR) wing containing geometric nonlinearities is described in this paper. The design process begins with identification of basic features of the HAR wing as well as its design constraints. This enables the design space to be narrowed down and consequently, brings ease of convergence towards the design solution. Parametric studies in terms of the spar thickness, the span length and the store diameter are performed using finite element analysis for both undeformed and deformed cases, which respectively demonstrate the linear and nonlinear conditions. Two main criteria are accounted for in the selection of the wing design: the static deflections due to gravitational loading should be within the allowable margin of the size of the wind tunnel test section and the flutter speed of the wing should be much below the maximum speed of the wind tunnel. The findings show that the wing experiences a stiffness hardening effect under the nonlinear static solution and the presence of the store enables significant reduction in linear flutter speed.

  20. Aspects of the SO(5) symmetry and the problem of high temperature superconductivity (United States)

    Demler, Eugene A.

    This dissertation reviews several aspects of the SO(5) theory, that unifies superconductivity and antiferromagnetism and that has recently been suggested in connection with the problem of high temperature superconductivity. Microscopic analysis of the pi operators (generators of the SO(5) symmetry) is given for the t-J and Hubbard models and it is argued that pseudo-Goldstone bosons that correspond to these operators produce resonant peaks observed in neutron scattering experiments on YBCO. Microscopic models with exact SO(5) symmetry are considered and the nature of the AF/SC transition in these systems is discussed. Analysis of a non-Abelian SU(2) holonomy of the SO (5) spinor states is presented, the SO(5) Berry's phase is shown to be related to the second Hopf map and described by a Yang monopole at the degeneracy point. These results are used to show that fermionic excitations in models with exact SO(5) symmetry may be described as four component Dirac fermions coupled to SU(2) gauge fields in 2 + 1 dimensions. Finally some experimental tests of the SO(5) model are suggested.

  1. Bosch-like method for creating high aspect ratio poly(methyl methacrylate) (PMMA) structures

    KAUST Repository

    Haiducu, Marius


    This paper presents a method for etching millimetre-deep trenches in commercial grade PMMA using deep-UV at 254 nm. The method is based on consecutive cycles of irradiation and development of the exposed areas, respectively. The exposure segment is performed using an inexpensive, in-house built irradiation box while the development part is accomplished using an isopropyl alcohol (IPA):H2O developer. The method was tested and characterized by etching various dimension square test structures in commercial grade, mirrored acrylic. The undercut of the sidewalls due to the uncollimated nature of the irradiation light was dramatically alleviated by using a honeycomb metallic grid in between the irradiation source and the acrylic substrate and by rotating the latter using a direct current (DC) motor-driven stage. By using an extremely affordable set-up and non-toxic, environmentally friendly materials and substances, this process represents an excellent alternative to microfabricating microfluidic devices in particular and high aspect ratio structures in general using PMMA as substrate. © 2012 SPIE.

  2. Special aspects on nuclear targets for high-energy heavy-ion accelerator experiments

    International Nuclear Information System (INIS)

    Folger, H.; Hartmann, W.; Klemm, J.; Thalheimer, W.


    Important facts about the GSI UNILAC accelerator are reviewed under the special aspects of target and stripper foil applications including general range considerations as seen after the upgrading of the machine to an energy of 20 MeV/u for all ions up to uranium. It is also reported about current works and recent developments in target preparations at GSI divided into four main groups of preparation procedures with sufficient overlap: cold rollings, carbon sublimation-condensations, focussed heavy-ion sputter deposition, and the wide field of high-vacuum evaporation-condensations. Among others, a Ca reduction-distillation procedure is described, a new assembly is shown for sublimation-condensations of uniform C layers of 0.1 to 0.76 mg/cm 2 area densities. A selection of only a few applications of targets at the UNILAC can be given. Improved actinide targets are discussed, in-beam measurements of properties of targets on rotating wheels are explained, and a large-area target wheel with a circumference of nearly one meter is shown. SEM micrographs of damaged targets are given and explained. (orig.)

  3. Optimization of laser energy deposition for single-shot high aspect-ratio microstructuring of thick BK7 glass

    Energy Technology Data Exchange (ETDEWEB)

    Garzillo, Valerio; Grigutis, Robertas [Dipartimento di Scienza e Alta Tecnologia, University of Insubria, Via Valleggio 11, I-22100 Como (Italy); Jukna, Vytautas [Centre de Physique Theorique, CNRS, Ecole Polytechnique, Université Paris-Saclay, F-91128 Palaiseau (France); LOA, ENSTA-ParisTech, CNRS, Ecole Polytechnique, Université Paris Saclay, F-91762 Palaiseau (France); Couairon, Arnaud [Centre de Physique Theorique, CNRS, Ecole Polytechnique, Université Paris-Saclay, F-91128 Palaiseau (France); Di Trapani, Paolo [Dipartimento di Scienza e Alta Tecnologia, University of Insubria and CNISM UdR Como, Via Valleggio 11, I-22100 Como (Italy); Jedrkiewicz, Ottavia, E-mail: [Istituto di Fotonica e Nanotecnologie, CNR and CNISM UdR Como, Via Valleggio 11, I-22100 Como (Italy)


    We investigate the generation of high aspect ratio microstructures across 0.7 mm thick glass by means of single shot Bessel beam laser direct writing. We study the effect on the photoinscription of the cone angle, as well as of the energy and duration of the ultrashort laser pulse. The aim of the study is to optimize the parameters for the writing of a regular microstructure due to index modification along the whole sample thickness. By using a spectrally resolved single pulse transmission diagnostics at the output surface of the glass, we correlate the single shot material modification with observations of the absorption in different portions of the retrieved spectra, and with the absence or presence of spectral modulation. Numerical simulations of the evolution of the Bessel pulse intensity and of the energy deposition inside the sample help us interpret the experimental results that suggest to use picosecond pulses for an efficient and more regular energy deposition. Picosecond pulses take advantage of nonlinear plasma absorption and avoid temporal dynamics effects which can compromise the stationarity of the Bessel beam propagation.

  4. Variable deflection response of sensitive CNT-on-fiber artificial hair sensors from CNT synthesis in high aspect ratio microcavities (United States)

    Slinker, Keith; Maschmann, Matthew R.; Kondash, Corey; Severin, Benjamin; Phillips, David; Dickinson, Benjamin T.; Reich, Gregory; Baur, Jeff


    Crickets, locusts, bats, and many other animals detect changes in their environment with distributed arrays of flow-sensitive hairs. Here we discuss the fabrication and characterization of a relatively new class of pore-based, artificial hair sensors that take advantage of the mechanical properties of structural microfibers and the electromechanical properties of self-aligned carbon nanotube arrays to rapidly transduce changes in low speed air flow. The radially aligned nanotubes are able to be synthesized along the length of the fibers inside the high aspect ratio cavity between the fiber surface and the wall of a microcapillary pore. The growth self-positions the fibers within the capillary and forms a conductive path between detection electrodes. As the hair is deflected, nanotubes are compressed to produce a typical resistance change of 1-5% per m/s of air speed which we believe are the highest sensitivities reported for air velocities less than 10 m/s. The quasi-static response of the sensors to point loads is compared to that from the distributed loads of air flow. A plane wave tube is used to measure their dynamic response when perturbed at acoustic frequencies. Correlation of the nanotube height profile inside the capillary to a diffusion transport model suggests that the nanotube arrays can be controllably tapered along the fiber. Like their biological counterparts, many applications can be envisioned for artificial hair sensors by tailoring their individual response and incorporating them into arrays for detecting spatio-temporal flow patterns over rigid surfaces such as aircraft.

  5. New technique of machining high precision mirror surface press roller (United States)

    Hongsen, Deng


    High precision mirror surface press roller machining technique of corrosion and grinding proof is one of the key techniques that the production enterprises as well as the machining and manufacturing of the following industries sought to resolve for a long time: plastics, papermaking, rubber, film, and chip production. In Oct. 1984, a new comprehensive machining technique of metal brush coating, grinding with abrasive belt, as well as buffing was used to conduct nearly 20 experiments. In Jan. 1985, a pair of middle convex high precision mirror surface press rollers was successfully machined. The technical process is described.

  6. The flow field in a high aspect ratio cooling duct with and without one heated wall (United States)

    Rochlitz, Henrik; Scholz, Peter; Fuchs, Thomas


    The flow in a high aspect ratio generic cooling duct is described for different Reynolds numbers and for adiabatic as well as non-adiabatic conditions. The Reynolds number is varied in a range from 39,000 to 111,000. The generic cooling duct facility allows for applying a constant temperature on the duct's lower wall, and it ensures having well-defined boundary conditions. The high-quality, optical noninvasive measurement methods, namely Particle Image Velocimetry (2C2D-PIV, i.e., two velocity components in a plane), Stereo Particle Image Velocimetry (3C2D-PIV, i.e., three velocity components in a plane) and Volumetric Particle Tracking Velocimetry (3C3D-PTV, i.e., three velocity components in a volume), are used to characterize the flow in detail. Pressure transducers are installed for measuring the pressure losses. The repeatability and the validity of the data are discussed in detail. For that purpose, modifications in the test facility and in the experimental setup as well as comparisons between the different measurement methods are given. A focus lies on the average velocity distribution and on the turbulent statistics. The longitudinal velocity profile is analyzed in detail for Reynolds number variations. Secondary flows are identified with velocities of two orders of magnitude smaller than the longitudinal velocity. Reynolds stress distributions are given for several different cases. The Reynolds number dependency of overline{u'^2} and overline{v'^2} is shown, and a comparison between the adiabatic and the heated case is given. overline{u'^2} changes significantly when the lower wall heat flux is applied, whereas overline{v'^2} and overline{u'v'} almost stay constant.

  7. Geometrical Nonlinear Aeroelastic Stability Analysis of a Composite High-Aspect-Ratio Wing

    Directory of Open Access Journals (Sweden)

    Chang Chuan Xie


    Full Text Available A composite high-aspect-ratio wing of a high-altitude long-endurance (HALE aircraft was modeled with FEM by MSC/NASTRAN, and the nonlinear static equilibrium state is calculated under design load with follower force effect, but without load redistribution. Assuming the little vibration amplitude of the wing around the static equilibrium state, the system is linearized and the natural frequencies and mode shapes of the deformed structure are obtained. Planar doublet lattice method is used to calculate unsteady aerodynamics in frequency domain ignoring the bending effect of the deflected wing. And then, the aeroelastic stability analysis of the system under a given load condition is successively carried out. Comparing with the linear results, the nonlinear displacement of the wing tip is higher. The results indicate that the critical nonlinear flutter is of the flap/chordwise bending type because of the chordwise bending having quite a large torsion component, with low critical speed and slowly growing damping, which dose not appear in the linear analysis. Furthermore, it is shown that the variation of the nonlinear flutter speed depends on the scale of the load and on the chordwise bending frequency. The research work indicates that, for the very flexible HALE aircraft, the nonlinear aeroelastic stability is very important, and should be considered in the design progress. Using present FEM software as the structure solver (e.g. MSC/NASTRAN, and the unsteady aerodynamic code, the nonlinear aeroelastic stability margin of a complex system other than a simple beam model can be determined.

  8. Technology and engineering aspects of high power pulsed single longitudinal mode dye lasers (United States)

    Rawat, V. S.; Mukherjee, Jaya; Gantayet, L. M.


    Tunable single mode pulsed dye lasers are capable of generating optical radiations in the visible range having very small bandwidths (transform limited), high average power (a few kW) at a high pulse repetition rate (a few tens of kHz), small beam divergence and relatively higher efficiencies. These dye lasers are generally utilized laser dyes dissolved in solvents such as water, heavy water, ethanol, methanol, etc. to provide a rapidly flowing gain medium. The dye laser is a versatile tool, which can lase either in the continuous wave (CW) or in the pulsed mode with pulse duration as small as a few tens of femtoseconds. In this review, we have examined the several cavity designs, various types of gain mediums and numerous types of dye cell geometries for obtaining the single longitudinal mode pulsed dye laser. Different types of cavity configuration, such as very short cavity, short cavity with frequency selective element and relatively longer cavity with multiple frequency selective elements were reviewed. These single mode lasers have been pumped by all kinds of pumping sources such as flash lamps, Excimer, Nitrogen, Ruby, Nd:YAG, Copper Bromide and Copper Vapor Lasers. The single mode dye lasers are either pumped transversely or longitudinally to the resonator axis. The pulse repletion rate of these pump lasers were ranging from a few Hz to a few tens of kHz. Physics technology and engineering aspects of tuning mechanism, mode hop free scanning and dye cell designs are also presented in this review. Tuning of a single mode dye laser with a resolution of a few MHz per step is a technologically challenging task, which is discussed here.

  9. Vacuum surface flashover and high pressure gas streamers

    International Nuclear Information System (INIS)

    Elizondo, J.M.; Krogh, M.L.; Smith, D.; Stolz, D.; Wright, S.N.


    Pre-breakdown current traces obtained during high pressure gas breakdown and vacuum surface flashover show similar signatures. The initial pre-breakdown current spike, a flat constant current phase, and the breakdown phase with voltage collapse and current surge differ mostly in magnitude. Given these similarities, a model, consisting of the initial current spike corresponding to a fast precursor streamer (ionization wave led by a photoionizing front), the flat current stage as the heating or glow phase, and the terminal avalanche and gap closure, is applied to vacuum surface flashover. A simple analytical approximation based on the resistivity changes induced in the vacuum and dielectric surface is presented. The approximation yields an excellent fit to pre-breakdown time delay vs applied field for previously published experimental data. A detailed kinetics model that includes surface and gas contributions is being developed based in the initial approximation

  10. Analyzing surface coatings in situ: High-temperature surface film analyzer developed

    International Nuclear Information System (INIS)



    Scientists at Argonne National Laboratory (ANL) have devised a new instrument that can analyze surface coatings under operating conditions. The High-Temperature Surface Film Analyzer is the first such instrument to analyze the molecular composition and structure of surface coatings on metals and solids under conditions of high temperature and pressure in liquid environments. Corrosion layers, oxide coatings, polymers or paint films, or adsorbed molecules are examples of conditions that can be analyzed using this instrument. Film thicknesses may vary from a few molecular layers to several microns or thicker. The instrument was originally developed to study metal corrosion in aqueous solutions similar to the cooling water systems of light-water nuclear reactors. The instrument may have use for the nuclear power industry where coolant pipes degrade due to stress corrosion cracking, which often leads to plant shutdown. Key determinants in the occurrence of stress corrosion cracking are the properties and composition of corrosion scales that form inside pipes. The High-Temperature Surface Analyzer can analyze these coatings under laboratory conditions that simulate the same hostile environment of high temperature, pressure, and solution that exist during plant operations. The ability to analyze these scales in hostile liquid environments is unique to the instrument. Other applications include analyzing paint composition, corrosion of materials in geothermal power systems, integrity of canisters for radioactive waste storage, corrosion inhibitor films on piping and drilling systems, and surface scales on condenser tubes in industrial hot water heat exchangers. The device is not patented

  11. High Efficiency, High Temperature Foam Core Heat Exchanger for Fission Surface Power Systems, Phase II Project (United States)

    National Aeronautics and Space Administration — Fission-based power systems with power levels of 30 to ≥100 kWe will be needed for planetary surface bases. Development of high temperature, high efficiency...

  12. High Efficiency, High Temperature Foam Core Heat Exchanger for Fission Surface Power Systems, Phase II (United States)

    National Aeronautics and Space Administration — Fission-based power systems with power levels of 30 to ≥100 kWe will be needed for planetary surface bases. Development of high temperature, high efficiency heat...

  13. Topographic forcing and related uncertainties on glacier surface energy balance in High Mountain Asia (United States)

    Olson, M.; Rupper, S.; Shean, D. E.


    Topography directly influences the amount of global radiation, as well as other key energy flux terms, arriving on a glacier surface. This is particularly important in regions of variable and complex topography such as High Mountain Asia (HMA). In this region surface energy and mass balance estimates often rely heavily on modeling, and thus require accurate accounting of topography through available remote sensing platforms. Our previous work shows that topographic shading from surrounding terrain can alter the mean daily potential direct shortwave radiation by upwards of 20% for some valley glaciers. In this work, we find in regions of high topographic relief that shading frequently dominates in the ablation zone rather than the accumulation zone, contrary to the findings of some previous studies. This however, is largely dependent on the valley aspect and relative relief of nearby terrain. In addition, we examine the impact of topography, primarily topographic shading, on components of surface energy balance for a large sample of glaciers across different regions in HMA. Our results show that while the impact of topographic shading is highly variable throughout HMA, the magnitude of influence can often be predicted based on simple characteristics such as latitude, valley aspect, and orientation of the immediate surrounding topography. We also explore the uncertainty in topographic shading and in calculated surface energy due to the spatial resolution and accuracy of DEMs. In particular, we compare the shading and energy balance results utilizing a suite of DEMs, including 2 m, 8 m, and 30 m World View DEMs, 30 m ASTER GDEM, 30 m SRTM DEM, and 30 m ALOS DEM. These results will help us improve glacier energy and mass balance modeling accuracy, and demonstrate limitations and uncertainties when modeling changes in surface energy fluxes due to surrounding topography for mountain glaciers.

  14. Design methodology to enhance high impedance surfaces performances

    Directory of Open Access Journals (Sweden)

    M. Grelier


    Full Text Available A methodology is introduced for designing wideband, compact and ultra-thin high impedance surfaces (HIS. A parametric study is carried out to examine the effect of the periodicity on the electromagnetic properties of an HIS. This approach allows designers to reach the best trade-off for HIS performances.

  15. Linked Min.B configuration inside high shear magnetic surface

    International Nuclear Information System (INIS)

    Ohasa, K.; Ikuta, K.


    Arrangement of the l = m baseball coils to form the toroidally linked Min.B configuration with large rotational transform is studied analytically and numerically. By an optimization the closed magnetic isobars are obtained inside the last closed magnetic surface having practical volume and high shear if l = 3 baseball coils are arranged. (auth.)

  16. Highly antibacterial UHMWPE surfaces by implantation of titanium ions

    Energy Technology Data Exchange (ETDEWEB)

    Delle Side, D., E-mail: [LEAS, Dipartimento di Matematica e Fisica “Ennio de Giorgi”, Università del Salento, Lecce (Italy); Istituto Nazionale di Fisica Nucleare – Sezione di Lecce, Lecce (Italy); Nassisi, V.; Giuffreda, E.; Velardi, L. [LEAS, Dipartimento di Matematica e Fisica “Ennio de Giorgi”, Università del Salento, Lecce (Italy); Istituto Nazionale di Fisica Nucleare – Sezione di Lecce, Lecce (Italy); Alifano, P.; Talà, A.; Tredici, S.M. [Dipartimento di Scienze e Tecnologie Biologiche ed Ambientali, Università del Salento, Lecce (Italy)


    The spreading of pathogens represents a serious threat for human beings. Consequently, efficient antimicrobial surfaces are needed in order to reduce risks of contracting severe diseases. In this work we present the first evidences of a new technique to obtain a highly antibacterial Ultra High Molecular Weight Polyethylene (UHMWPE) based on a non-stoichiometric titanium oxide coating, visible-light responsive, obtained through ion implantation.

  17. Highly antibacterial UHMWPE surfaces by implantation of titanium ions (United States)

    Delle Side, D.; Nassisi, V.; Giuffreda, E.; Velardi, L.; Alifano, P.; Talà, A.; Tredici, S. M.


    The spreading of pathogens represents a serious threat for human beings. Consequently, efficient antimicrobial surfaces are needed in order to reduce risks of contracting severe diseases. In this work we present the first evidences of a new technique to obtain a highly antibacterial Ultra High Molecular Weight Polyethylene (UHMWPE) based on a non-stoichiometric titanium oxide coating, visible-light responsive, obtained through ion implantation.

  18. High aspect ratio silicon nanowires control fibroblast adhesion and cytoskeleton organization (United States)

    Andolfi, Laura; Murello, Anna; Cassese, Damiano; Ban, Jelena; Dal Zilio, Simone; Lazzarino, Marco


    Cell-cell and cell-matrix interactions are essential to the survival and proliferation of most cells, and are responsible for triggering a wide range of biochemical pathways. More recently, the biomechanical role of those interactions was highlighted, showing, for instance, that adhesion forces are essential for cytoskeleton organization. Silicon nanowires (Si NWs) with their small size, high aspect ratio and anisotropic mechanical response represent a useful model to investigate the forces involved in the adhesion processes and their role in cellular development. In this work we explored and quantified, by single cell force spectroscopy (SCFS), the interaction of mouse embryonic fibroblasts with a flexible forest of Si NWs. We observed that the cell adhesion forces are comparable to those found on collagen and bare glass coverslip, analogously the membrane tether extraction forces are similar to that on collagen but stronger than that on bare flat glass. Cell survival did not depend significantly on the substrate, although a reduced proliferation after 36 h was observed. On the contrary both cell morphology and cytoskeleton organization revealed striking differences. The cell morphology on Si-NW was characterized by a large number of filopodia and a significant decrease of the cell mobility. The cytoskeleton organization was characterized by the absence of actin fibers, which were instead dominant on collagen and flat glass support. Such findings suggest that the mechanical properties of disordered Si NWs, and in particular their strong asymmetry, play a major role in the adhesion, morphology and cytoskeleton organization processes. Indeed, while adhesion measurements by SCFS provide out-of-plane forces values consistent with those measured on conventional substrates, weaker in-plane forces hinder proper cytoskeleton organization and migration processes.

  19. Alignment method combining interference lithography with anisotropic wet etch technique for fabrication of high aspect ratio silicon gratings. (United States)

    Zheng, Yanchang; Qiu, Keqiang; Chen, Huoyao; Chen, Yong; Liu, Zhengkun; Liu, Ying; Xu, Xiangdong; Hong, Yilin


    A method was developed for aligning interference fringes generated in interference lithography to the vertical {111} planes of oriented silicon wafers. The alignment error is 0.036°. This high precision method makes it possible to combine interference lithography with anisotropic wet etch technique for the fabrication of high aspect ratio silicon gratings with extremely smooth sidewalls over a large sample area. With this alignment method, 320 nm and 2 μm period silicon gratings have been successfully fabricated. The highest aspect ratio is up to 100. The sample area is about 50 mm × 60 mm. The roughness (root mean square) of the sidewall is about 0.267 nm.

  20. Low-temperature plasma etching of high aspect-ratio densely packed 15 to sub-10 nm silicon features derived from PS-PDMS block copolymer patterns

    International Nuclear Information System (INIS)

    Liu, Zuwei; Sassolini, Simone; Olynick, Deirdre L; Gu, Xiaodan; Hwu, Justin


    The combination of block copolymer (BCP) lithography and plasma etching offers a gateway to densely packed sub-10 nm features for advanced nanotechnology. Despite the advances in BCP lithography, plasma pattern transfer remains a major challenge. We use controlled and low substrate temperatures during plasma etching of a chromium hard mask and then the underlying substrate as a route to high aspect ratio sub-10 nm silicon features derived from BCP lithography. Siloxane masks were fabricated using poly(styrene-b-siloxane) (PS-PDMS) BCP to create either line-type masks or, with the addition of low molecular weight PS-OH homopolymer, dot-type masks. Temperature control was essential for preventing mask migration and controlling the etched feature’s shape. Vertical silicon wire features (15 nm with feature-to-feature spacing of 26 nm) were etched with aspect ratios up to 17 : 1; higher aspect ratios were limited by the collapse of nanoscale silicon structures. Sub-10 nm fin structures were etched with aspect ratios greater than 10 : 1. Transmission electron microscopy images of the wires reveal a crystalline silicon core with an amorphous surface layer, just slightly thicker than a native oxide. (paper)

  1. Instability and associated roll structure of Marangoni convection in high Prandtl number liquid bridge with large aspect ratio (United States)

    Yano, T.; Nishino, K.; Kawamura, H.; Ueno, I.; Matsumoto, S.


    This paper reports the experimental results on the instability and associated roll structures (RSs) of Marangoni convection in liquid bridges formed under the microgravity environment on the International Space Station. The geometry of interest is high aspect ratio (AR = height/diameter ≥ 1.0) liquid bridges of high Prandtl number fluids (Pr = 67 and 207) suspended between coaxial disks heated differentially. The unsteady flow field and associated RSs were revealed with the three-dimensional particle tracking velocimetry. It is found that the flow field after the onset of instability exhibits oscillations with azimuthal mode number m = 1 and associated RSs traveling in the axial direction. The RSs travel in the same direction as the surface flow (co-flow direction) for 1.00 ≤ AR ≤ 1.25 while they travel in the opposite direction (counter-flow direction) for AR ≥ 1.50, thus showing the change of traveling directions with AR. This traveling direction for AR ≥ 1.50 is reversed to the co-flow direction when the temperature difference between the disks is increased to the condition far beyond the critical one. This change of traveling directions is accompanied by the increase of the oscillation frequency. The characteristics of the RSs for AR ≥ 1.50, such as the azimuthal mode of oscillation, the dimensionless oscillation frequency, and the traveling direction, are in reasonable agreement with those of the previous sounding rocket experiment for AR = 2.50 and those of the linear stability analysis of an infinite liquid bridge.

  2. High surface area carbon and process for its production

    Energy Technology Data Exchange (ETDEWEB)

    Romanos, Jimmy; Burress, Jacob; Pfeifer, Peter; Rash, Tyler; Shah, Parag; Suppes, Galen


    Activated carbon materials and methods of producing and using activated carbon materials are provided. In particular, biomass-derived activated carbon materials and processes of producing the activated carbon materials with prespecified surface areas and pore size distributions are provided. Activated carbon materials with preselected high specific surface areas, porosities, sub-nm (<1 nm) pore volumes, and supra-nm (1-5 nm) pore volumes may be achieved by controlling the degree of carbon consumption and metallic potassium intercalation into the carbon lattice during the activation process.

  3. Surface intermediates on metal electrodes at high temperatures

    DEFF Research Database (Denmark)

    Zachau-Christiansen, Birgit; Jacobsen, Torben; Bay, Lasse


    The mechanisms widely conceived for the O(2)-reduction or H(2)-oxidation reactions in SOFC's involve intermediate O/H species adsorbed on the electrode surface. The presence of these intermediates is investigated by linear sweep voltammetry. In air at moderate temperatures (500 degrees C) Pt...... in contact with YSZ is covered with adsorbed oxygen which vanishes at high temperature (1000 degrees C). On Ni (YSZ) a specific layer of NiO is observed above the equilibrium potential while no surface species involving hydrogen can be identified at SOFC anode conditions. (C) 1998 Published by Elsevier...... Science B.V. All rights reserved....

  4. Surface passivation of high purity granular metals: zinc, cadmium, lead

    Directory of Open Access Journals (Sweden)

    Pirozhenko L. A.


    Full Text Available For the high purity metals (99.9999%, such as zinc, cadmium, and lead, which are widely used as initial components in growing semiconductor and scintillation crystals (CdTe, CdZnTe, ZnSe, (Cd, Zn, Pb WO4, (Cd, Zn, Pb MoO4 et al., it is very important to ensure reliable protection of the surface from oxidation and adsorption of impurities from the atmosphere. The specific features of surface passivation of high purity cadmium, lead and zinc are not sufficiently studied and require specific methodologies for further studies. The use of organic solutions in the schemes of chemical passivation of the investigated metals avoids hydrolysis of the obtained protective films. The use of organic solvents with pure cation and anion composition as the washing liquid prevents chemisorption of ions present in the conventionally used distilled water. This keeps the original purity of the granular metals. Novel compositions of etchants and etching scheme providing simultaneous polishing and passivation of high purity granular Zn, Cd and Pb are developed. Chemical passivation allows storing metals in the normal atmospheric conditions for more than half a year for Zn and Cd and up to 30 days for Pb without changing the state of the surface. The use of the glycerol-DMF solution in the processes for obtaining Pb granules provides self-passivation of metal surfaces and eliminates the additional chemical processing while maintaining the quality of corrosion protection.

  5. Cell surface topology creates high Ca2+ signalling microdomains

    DEFF Research Database (Denmark)

    Brasen, Jens Christian; Olsen, Lars Folke; Hallett, Maurice B


    20 microM Ca2+ to be activated. In this paper, we have resolved this apparent paradox by showing that the surface topology of cells represents an important and hitherto unrecognized feature for generating microdomains of high Ca2+ in cells. We show that whereas the standard modeling assumption...... of a smooth cell surface predicts only moderate localized effects, the more realistic "wrinkled" surface topology predicts that Ca2+ concentrations up to 80 microM can persist within the folds of membranes for significant times. This intra-wrinkle location may account for 5% of the total cell volume. Using......-wrinkle location is also a strategic location at which Ca2+ acts as a regulator of the cortical cytoskeleton and plasma membrane expansion....

  6. High intensity surface plasma waves, theory and PIC simulations (United States)

    Raynaud, M.; Héron, A.; Adam, J.-C.


    With the development of intense (>1019 W cm‑2) short pulses (≤25 fs) laser with very high contrast, surface plasma wave (SPW) can be explored in the relativistic regime. As the SPW propagates with a phase velocity close to the speed of light it may results in a strong acceleration of electron bunches along the surface permitting them to reach relativistic energies. This may be important e.g. for applications in the field of plasma-based accelerators. We investigate in this work the excitation of SPWs on grating preformed over-dense plasmas for laser intensities ranging from 1019 up to 1021 W cm‑2. We discuss the nature of the interaction with respect to the solid case in which surface plasmon can be resonantly excited with weak laser intensity. In particular, we show the importance of the pulse duration and focalization of the laser beam on the amplitude of the SPW.

  7. Technical aspects of osteoid osteoma ablation in children using MR-guided high intensity focussed ultrasound. (United States)

    Yarmolenko, Pavel S; Eranki, Avinash; Partanen, Ari; Celik, Haydar; Kim, AeRang; Oetgen, Matthew; Beskin, Viktoriya; Santos, Domiciano; Patel, Janish; Kim, Peter C W; Sharma, Karun


    Osteoid osteoma (OO) is a painful bone tumour occurring in children and young adults. Magnetic resonance imaging-guided high intensity focussed ultrasound (MR-HIFU) allows non-invasive treatment without ionising radiation exposure, in contrast to the current standard of care treatment with radiofrequency ablation (RFA). This report describes technical aspects of MR-HIFU ablation in the first 8 paediatric OO patients treated in a safety and feasibility clinical trial (total enrolment of up to 12 patients). OO lesions and adjacent periosteum were treated with MR-HIFU ablation in 5-20 sonications (sonication duration = 16-48 s, frequency = 1.2 MHz, acoustic power = 20-160 W). Detailed treatment workflow, patient positioning and coupling strategies, as well as temperature and tissue perfusion changes were summarised and correlated. MR-HIFU ablation was feasible in all eight cases. Ultrasound standoff pads were shaped to conform to extremity contours providing acoustic coupling and aided patient positioning. The energy delivered was 10 ± 7 kJ per treatment, raising maximum temperature to 83 ± 3 °C. Post ablation contrast-enhanced MRI showed ablated volumes ranging 0.46-19.4 cm 3 extending further into bone (7 ± 4 mm) than into soft tissue (4 ± 6 mm, p = 0.01, Mann-Whitney). Treatment time ranged 30-86 min for sonication and 160 ± 40 min for anaesthesia. No serious treatment-related adverse events were observed. Complete pain relief with no medication occurred in 7/8 patients within 28 days following treatment. MR-HIFU ablation of painful OO appears technically feasible in children and it may become a non-invasive and radiation-free alternative for painful OO. Therapy success, efficiency, and applicability may be improved through specialised equipment designed more specifically for extremity bone ablation.

  8. Aspects of possible magmatic disruption of a high-level radioactive waste repository in southern Nevada

    International Nuclear Information System (INIS)

    Crowe, B.; Amos, R.; Perry, F.; Self, S.; Vaniman, D.


    The Nevada Test Site (NTS) region is located within the central section of a north-northeast-trending basaltic volcanic belt of late Cenozoic age, a part of the Quaternary volcanic province of the Great Basin. Future volcanism within the belt represents a potential hazard to storage of high-level radioactive waste within a buried repository located in the southwestern NTS. The hazards of future volcanism in the region are being characterized through a combination of volcanic hazards studies, probability determinations, and consequence analyses. Basaltic activity within the NTS regions is divided into two age groups consisting of relatively large-volume silicic cycle basalts (8 to 10 Myr) and rift basalts (< 8 to 0.3 Myr). This paper describes the processes of basaltic magmatism ranging from derivation of basalt melts at depth, through ascent through the upper mantle and crust, to surface eruption. Each stage in the evolution and dispersal of basaltic magma is described, and the disruption and potential dispersal of stored radioactive waste is evaluated. These data document areas of knowns and unknowns in the processes of basaltic volcanisms and provide background data necessary to assist calculations of radiation release levels due to disruption of a repository. 9 figures, 11 tables

  9. SIP Shear Walls: Cyclic Performance of High-Aspect-Ratio Segments and Perforated Walls (United States)

    Vladimir Kochkin; Douglas R. Rammer; Kevin Kauffman; Thomas Wiliamson; Robert J. Ross


    Increasing stringency of energy codes and the growing market demand for more energy efficient buildings gives structural insulated panel (SIP) construction an opportunity to increase its use in commercial and residential buildings. However, shear wall aspect ratio limitations and lack of knowledge on how to design SIPs with window and door openings are barriers to the...

  10. Ultra-high aspect ratio replaceable AFM tips using deformation-suppressed focused ion beam milling

    DEFF Research Database (Denmark)

    Savenko, Alexey; Yildiz, Izzet; Petersen, Dirch Hjorth


    in terms of defining the shape and size of the tip. Due to beam-induced deformation, it has so far not been possible to define HAR structures using lateral FIB milling. In this work we obtain aspect ratios of up to 45, with tip diameters down to 9 nm, by a deformation-suppressing writing strategy. Several...

  11. Large-scale high aspect ratio Al-doped ZnO nanopillars arrays as anisotropic metamaterials

    DEFF Research Database (Denmark)

    Shkondin, Evgeniy; Takayama, Osamu; Panah, Mohammad Esmail Aryaee


    High aspect ratio free-standing Al-doped ZnO (AZO) nanopillars and nanotubes were fabricated using a combination of advanced reactive ion etching and atomic layer deposition (ALD) techniques. Prior to the pillar and tube fabrication, AZO layers were grown on flat silicon and glass substrates with...

  12. Resent developments in high-frequency surface-wave techniques (United States)

    Xia, J.; Pan, Y.; Zeng, C.


    High-frequency Rayleigh-wave methods, such as Multi-channel Analysis of Surface Waves (MASW), are getting increasingly attention in the near-surface geophysics and geotechnique community in the last 20 years because of their non-invasive, non-destructive, efficient, and low-cost advantages and their success in environmental and engineering applications. They are viewed by near-surface geophysics community as the one of most promise techniques in the future. However, they face unique problems related to extremely irregular velocity variations in near-surface geology or man-made constructions, for example, highway, foundation, dam, levee, jetty, etc., which are not solvable by techniques or algorithms widely used in earthquake seismology or oil/gas seismic exploration. We present solutions to the problems associated with near-surface materials that possess velocity inverse and high Poisson's ratio. Calculation of dispersion curves by existing algorithms may fail for some special velocity models due to velocity inverse (a high-velocity layer on the top of a low-velocity layer). Two velocity models are most common in near-surface applications. One is a low-velocity half space model and the other a high-velocity topmost layer. The former model results in a complex matrix that no roots can be found in the real number domain, which implies that no phase velocities can be calculated in certain frequency ranges based on current exist algorithms. A solution is to use the real part of the root of the complex number. It is well-known that phase velocities approach about 91% of the shear (S)-wave velocity of the topmost layer when wavelengths are much shorter than the thickness of the topmost layer. The later model, however, results in that phase velocities in a high-frequency range calculated using the current algorithms approach a velocity associated with the S-wave velocity of the second layer NOT the topmost layer. A solution to this problem is to use a two-layer model to

  13. Interaction of slow highly charged ions with surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Aumayr, F. [Technische Universitaet Wien (Austria)


    A review will be presented on recent investigations concerning the interaction of slow ({le} 10{sup 6} m/s) ions in high charge states approaching a clean metal surface. Detailed information on the generation and decay of transiently formed multiply excited {open_quotes}hollow atoms{close_quotes} can be gained from the measurement of total yields and energy distributions of emitted electrons and, in particular, from the electron emission statistics. By comparing measured results with model calculations based on a recently extended classical over-barrier approach, different sources for the observed electron emission can be identified: autoionisation of the multiply excited hollow atoms on their way toward the surface; promotion above the vacuum barrier of electrons previously captured by the projectile, due to their self- and image-charge screening near the surface; `peeling-off` of electrons still bound in highly excited projectile states at the moment of surface impact, and finally; electron emission due to final subsurface de-excitation.

  14. Frequency selective surfaces based high performance microstrip antenna

    CERN Document Server

    Narayan, Shiv; Jha, Rakesh Mohan


    This book focuses on performance enhancement of printed antennas using frequency selective surfaces (FSS) technology. The growing demand of stealth technology in strategic areas requires high-performance low-RCS (radar cross section) antennas. Such requirements may be accomplished by incorporating FSS into the antenna structure either in its ground plane or as the superstrate, due to the filter characteristics of FSS structure. In view of this, a novel approach based on FSS technology is presented in this book to enhance the performance of printed antennas including out-of-band structural RCS reduction. In this endeavor, the EM design of microstrip patch antennas (MPA) loaded with FSS-based (i) high impedance surface (HIS) ground plane, and (ii) the superstrates are discussed in detail. The EM analysis of proposed FSS-based antenna structures have been carried out using transmission line analogy, in combination with the reciprocity theorem. Further, various types of novel FSS structures are considered in desi...

  15. Spectrophotometry of four galaxies of high surface brightness

    International Nuclear Information System (INIS)

    Arakelyan, M.A.; Magtesyap, A.P.


    Spectrophotometry of emission lines for the nuclei of galaxies of high surface brightness Nos 428, 449, 454 and 532 from the Arakelyan (1975) list is carried out. Clouds of ionized gas are detected at the distances of approximately 2 kpc from the nuclei of the two former galaxies. Besides there seems to be a cloud moving along the line of sight with velocity approximately 1500 km/s in the galaxy No. 449

  16. The field emission properties of high aspect ratio diamond nanocone arrays fabricated by focused ion beam milling

    Directory of Open Access Journals (Sweden)

    Z.L. Wang, Q. Wang, H.J. Li, J.J. Li, P. Xu, Q. Luo, A.Z. Jin, H.F. Yang and C.Z. Gu


    Full Text Available High aspect ratio diamond nanocone arrays are formed on freestanding diamond film by means of focused ion beam (FIB milling technology and hot-filament chemical vapor deposition (HFCVD method. The structure and phase purity of an individual diamond nanocone are characterized by scanning electron microscopy (SEM and micro-Raman spectroscopy. The result indicates that the diamond cones with high aspect ratio and small tip apex radius can be obtained by optimizing the parameters of FIB milling and diamond growth. The diamond nanocone arrays were also used to study the electron field emission properties and electric field shielding effect, finding high emission current density, low threshold and weak shielding effect, all attributable to the high field enhancement factor and suitable cone density of the diamond nanocone emitter

  17. High aspect ratio micro tool manufacturing for polymer replication using mu EDM of silicon, selective etching and electroforming

    DEFF Research Database (Denmark)

    Tosello, Guido; Bissacco, Giuliano; Tang, Peter Torben


    Mass fabrication of polymer micro components with high aspect ratio micro-structures requires high performance micro tools allowing the use of low cost replication processes such as micro injection moulding. In this regard an innovative process chain, based on a combination of micro electrical di...... discharge machining (mu EDM) of a silicon substrate, electroforming and selective etching was used for the manufacturing of a micro tool. The micro tool was employed for polymer replication by means of the injection moulding process....

  18. Microbiology of the surface water samples in the high background radiation areas of Ramsar, Iran

    International Nuclear Information System (INIS)

    Motamedifar, Mohammad; Zamani, Khosrow; Sedigh, Hadi; Mortazavi, Seyed Mohammad Javad; Taeb, Shahram; Haghani, M.; Mortazavi, Seyed Ali Reza; Soofi, Amir


    Residents of high background radiation areas of Ramsar have lived in these areas for many generations and received radiation doses much higher than the dose limit recommended by ICRP for radiation workers. The radioactivity of the high background radiation areas of Ramsar is reported to be due to 226 Ra and its decay products, which have been brought to the surface by the waters of hot springs. Over the past years the department has focused on different aspects of the health effects of the elevated levels of natural radiation in Ramsar. This study was aimed to perform a preliminary investigation on the bioeffects of exposure to elevated levels of natural radiation on the microbiology of surface water samples. Water samples were collected from surface water streams in Talesh Mahalleh district, Ramsar as well as a nearby area with normal levels of background radiation. Only two strains of bacteria, that is, Providencia stuartii and Shimwellia blattae, could be isolated from the water samples collected from high background radiation areas, while seven strains (Escherichia coli, Enterobacter asburiae, Klebsiella pneumoniae, Shigella dysenteriae, Buttiauxella agerstis, Tatumella punctuata and Raoultella ornithinolytica) were isolated from the water samples collected from normal background radiation areas. All the bacteria isolated from water samples of high and normal background radiation areas were sensitive to ultraviolet radiation, heat, betadine, alcohol, and deconex. Although other investigators have reported that bacteria isolated from hot springs show radioresistance, the results reported here do not reveal any adaptive response. (author)

  19. High Efficiency, High Temperature Foam Core Heat Exchanger for Fission Surface Power Systems, Phase I (United States)

    National Aeronautics and Space Administration — Fission-based power systems are anticipated for various planetary surface human base applications with power levels of 30-100+ kWe. The development of high...

  20. Materials surface damage and modification under high power plasma exposures (United States)

    Garkusha, I.; Makhlaj, V.; Byrka, O.; Taran, V.; Voitsenya, V.; Malykhin, S.; Herashchenko, S.; Surovitskiy, S.; Nowakowska-Langier, K.; Sadowski, M. J.; Skladnik-Sadowska, E.; Terentyev, D.


    Influence of powerful plasma impacts on several materials used for the construction of energy systems, i.e. different grades of steels as well as tungsten coatings, has been discussed. Irradiations of these materials with hydrogen and helium plasma streams have been performed in several high-current-pulse and quasi-stationary plasma accelerators which provided the variation of a power load upon the exposed surface as well as changes of the particle flux in wide ranges: the energy flux density in the range of 1-25 MJ/m2, particle flux - up to 1026-1029 ion/m2s, the plasma stream velocity - up to about 500 km/s, and the pulse duration in the range of 1-250 μs. A response of the investigated materials to extreme plasma loads, which are relevant to transient events in fusion reactors, is briefly discussed. It is demonstrated that a broad combination of mechanisms of powerful plasma interactions with various materials includes not only a surface damage caused by different erosion mechanisms, but under certain conditions it may also result in a significant improvement of material properties in the near-surface surface layer of several tens-μm in thickness. Some improvement of the structure and substructure of such a layer may be caused by the high-speed quenching, the shock wave formation and material alloying with plasma- and coating-species. The creation of unique surface structures and a considerable improvement of physical and mechanical properties of different materials can be achieved by the pulsed plasma alloying, i.e. pre-deposited coating modifications and mixing caused by the impacting plasma streams.

  1. Fundamentals of figure control and fracture-'free' finishing for high aspect ratio laser optics

    Energy Technology Data Exchange (ETDEWEB)

    Suratwala, Tayyab [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)


    The high level objectives of the this work were to: 1) scientifically understand critical phenomena affecting the surface figure during full aperture finishing; 2) utilize these fundamentals to more deterministically control the surface figure during finishing; 3) successfully polish under rogue particle-‘free’ environments during polishing by understanding/preventing key sources of rogue particles.

  2. Real-time High-fidelity Surface Flow Simulation. (United States)

    Ren, Bo; Yuan, Tailing; Li, Chenfeng; Xu, Kun; Hu, Shi-Min


    Surface flow phenomena, such as rain water flowing down a tree trunk and progressive water front in a shower room, are common in real life. However, compared with the 3D spatial fluid flow, these surface flow problems have been much less studied in the graphics community. To tackle this research gap, we present an efficient, robust and high-fidelity simulation approach based on the shallow-water equations. Specifically, the standard shallow-water flow model is extended to general triangle meshes with a feature-based bottom friction model, and a series of coherent mathematical formulations are derived to represent the full range of physical effects that are important for real-world surface flow phenomena. In addition, by achieving compatibility with existing 3D fluid simulators and by supporting physically realistic interactions with multiple fluids and solid surfaces, the new model is flexible and readily extensible for coupled phenomena. A wide range of simulation examples are presented to demonstrate the performance of the new approach.

  3. High-frequency EPR of surface impurities on nanodiamond (United States)

    Peng, Zaili; Stepanov, Viktor; Takahashi, Susumu

    Diamond is a fascinating material, hosting nitrogen-vacancy (NV) defect centers with unique magnetic and optical properties. There have been many reports that suggest the existence of paramagnetic impurities near surface of various kinds of diamonds. Electron paramagnetic resonance (EPR) investigation of mechanically crushed nanodiamonds (NDs) as well as detonation NDs revealed g 2 like signals that are attributed to structural defects and dangling bonds near the diamond surface. In this presentation, we investigate paramagnetic impurities in various sizes of NDs using high-frequency (HF) continuous wave (cw) and pulsed EPR spectroscopy. Strong size dependence on the linewidth of HF cw EPR spectra reveals the existence of paramagnetic impurities in the vicinity of the diamond surface. We also study the size dependence of the spin-lattice and spin-spin relaxation times (T1 and T2) of single substitutional nitrogen defects in NDs Significant deviations from the temperature dependence of the phonon-assisted T1 process were observed in the ND samples, and were attributed to the contribution from the surface impurities. This work was supported by the Searle Scholars Program and the National Science Foundation (DMR-1508661 and CHE-1611134).

  4. High aspect ratio nano-fabrication of photonic crystal structures on glass wafers using chrome as hard mask. (United States)

    Hossain, Md Nazmul; Justice, John; Lovera, Pierre; McCarthy, Brendan; O'Riordan, Alan; Corbett, Brian


    Wafer-scale nano-fabrication of silicon nitride (Si x N y ) photonic crystal (PhC) structures on glass (quartz) substrates is demonstrated using a thin (30 nm) chromium (Cr) layer as the hard mask for transferring the electron beam lithography (EBL) defined resist patterns. The use of the thin Cr layer not only solves the charging effect during the EBL on the insulating substrate, but also facilitates high aspect ratio PhCs by acting as a hard mask while deep etching into the Si x N y . A very high aspect ratio of 10:1 on a 60 nm wide grating structure has been achieved while preserving the quality of the flat top of the narrow lines. The presented nano-fabrication method provides PhC structures necessary for a high quality optical response. Finally, we fabricated a refractive index based PhC sensor which shows a sensitivity of 185 nm per RIU.

  5. Evaluation of a Candidate Trace Contaminant Control Subsystem Architecture: The High Velocity, Low Aspect Ratio (HVLA) Adsorption Process (United States)

    Kayatin, Matthew J.; Perry, Jay L.


    Traditional gas-phase trace contaminant control adsorption process flow is constrained as required to maintain high contaminant single-pass adsorption efficiency. Specifically, the bed superficial velocity is controlled to limit the adsorption mass-transfer zone length relative to the physical adsorption bed; this is aided by traditional high-aspect ratio bed design. Through operation in this manner, most contaminants, including those with relatively high potential energy are readily adsorbed. A consequence of this operational approach, however, is a limited available operational flow margin. By considering a paradigm shift in adsorption architecture design and operations, in which flows of high superficial velocity are treated by low-aspect ratio sorbent beds, the range of well-adsorbed contaminants becomes limited, but the process flow is increased such that contaminant leaks or emerging contaminants of interest may be effectively controlled. To this end, the high velocity, low aspect ratio (HVLA) adsorption process architecture was demonstrated against a trace contaminant load representative of the International Space Station atmosphere. Two HVLA concept packaging designs (linear flow and radial flow) were tested. The performance of each design was evaluated and compared against computer simulation. Utilizing the HVLA process, long and sustained control of heavy organic contaminants was demonstrated.

  6. A nanoscale conical polymethyl methacrylate (PMMA) sub-wavelength structure with a high aspect ratio realized by a stamping method. (United States)

    Kim, Dae-Seon; Kim, Dong-Hyun; Jang, Jae-Hyung


    A high aspect ratio conical sub-wavelength structure (SWS) was designed by using rigorous coupled-wave analysis (RCWA) method and was realized on polymethyl methacrylate (PMMA) film using a stamping technique. The silicon template containing a hexagonal array of conical holes with a period of 350 nm and an aspect ratio of 2.8 was fabricated by electron-beam (e-beam) lithography followed by a two-step etching process. The SWS with a high aspect ratio was easily transferred from the fabricated silicon template to PMMA film using the stamping method. The replicated PMMA SWS has an array of cones with nanoscale tips and an aspect ratio higher than 2.8. The average reflectance and transmittance of the PMMA film with the conical SWS in the wavelength ranging from 500 and 1500 nm was improved from 7.1 and 91.1% to 4.3 and 94.2%, respectively, as compared to flat PMMA film.

  7. Fabrication of wear-resistant silicon microprobe tips for high-speed surface roughness scanning devices (United States)

    Wasisto, Hutomo Suryo; Yu, Feng; Doering, Lutz; Völlmeke, Stefan; Brand, Uwe; Bakin, Andrey; Waag, Andreas; Peiner, Erwin


    Silicon microprobe tips are fabricated and integrated with piezoresistive cantilever sensors for high-speed surface roughness scanning systems. The fabrication steps of the high-aspect-ratio silicon microprobe tips were started with photolithography and wet etching of potassium hydroxide (KOH) resulting in crystal-dependent micropyramids. Subsequently, thin conformal wear-resistant layer coating of aluminum oxide (Al2O3) was demonstrated on the backside of the piezoresistive cantilever free end using atomic layer deposition (ALD) method in a binary reaction sequence with a low thermal process and precursors of trimethyl aluminum and water. The deposited Al2O3 layer had a thickness of 14 nm. The captured atomic force microscopy (AFM) image exhibits a root mean square deviation of 0.65 nm confirming the deposited Al2O3 surface quality. Furthermore, vacuum-evaporated 30-nm/200-nm-thick Au/Cr layers were patterned by lift-off and served as an etch mask for Al2O3 wet etching and in ICP cryogenic dry etching. By using SF6/O2 plasma during inductively coupled plasma (ICP) cryogenic dry etching, micropillar tips were obtained. From the preliminary friction and wear data, the developed silicon cantilever sensor has been successfully used in 100 fast measurements of 5- mm-long standard artifact surface with a speed of 15 mm/s and forces of 60-100 μN. Moreover, the results yielded by the fabricated silicon cantilever sensor are in very good agreement with those of calibrated profilometer. These tactile sensors are targeted for use in high-aspect-ratio microform metrology.

  8. Local community opinions regarding the socio-environmental aspects of lignite surface mining: Experiences from central Poland

    International Nuclear Information System (INIS)

    Badera, Jarosław; Kocoń, Paweł


    Surface lignite mining covers large areas and usually generates social conflicts which pose one of several energy security threats to certain states. Therefore, defining the social conditions determines the success of a mining project. Two communes were chosen for a public opinion study: Kleszczów, where the Bełchatów mine is located, and Złoczew, where a lignite deposit will soon be developed. The analysis shows, as opposed to other areas in Poland that have been projected for development, that both local communities are characterised by a high level of acceptance for lignite mining. In both cases, awareness about the profits was stronger than anxiety about the investment's negative effects. However, most inhabitants could not assess the mining company's diligence concerning its responsibility for mining damages as well as the diligence of external experts assessing the environmental impacts of excavation. Most respondents also could not assess if the legal regulations of public participation in the decision process were sufficient, but the negative opinions outweighed the positive ones. From the perspective of the energy policy, dialogue-type social communication is needed for every case of a new energy-mining project. Research on local public opinion should be the first step to opening up a social debate. - Highlights: • Lignite mining can generate social conflicts, which may threaten energy security. • Examined communes are characterised by a high level of acceptance for lignite mining. • Inhabitants cannot assess if the legal regulations of mining activity are sufficient. • From the perspective of the energy policy, broader social communication is needed. • Research on the public opinion should be the first step to open up a social debate

  9. Radiation control aspects of the civil construction for a high power free electron laser (FEL) facility

    International Nuclear Information System (INIS)

    Dunn, T.; Neil, G.; Stapleton, G.


    The paper discusses some of the assumptions and methods employed for the control of ionizing radiation in the specifications for the civil construction of a planned free electron laser facility based on a 200 MeV, 5 mA superconducting recirculation electron accelerator. Consideration is given firstly to the way in which the underlying building configuration and siting aspects were optimized on the basis of the early assumptions of beam loss and radiation goals. The various design requirements for radiation protection are then considered, and how they were folded into an aesthetically pleasing and functional building


    Directory of Open Access Journals (Sweden)

    P. M. Glamazdin


    Full Text Available Boilers of KVGM and PTVM series are characterized by high values of NOx and CO content in the combustion products. Reduction of NOx and CO content can be achieved by two ways: by installing the condensing heat recovery unit at the boiler outlet and by improving the heat and mass transfer processes in boiler furnaces. Application of the condensing heat recovery units causes pollution of resulting condensate by low-concentration acids. The authors conducted a study in order to determine the effectiveness of the previously applied methods of suppressing the emission of nitrogen oxides in the boilers of these types. Equalization of the temperature field and, consequently, enhancement of heat transfer in the furnace by substitution the used burners by the more advanced ones, the design of which facilitates reduction the emission of nitrogen oxides, were applied to all the upgraded facilities. The studies fulfilled demonstrate that a reduction of NOx emissions in water-heating high power boilers is fairly possible by means of modernization of the latter. The authors have developed the project of the PTVM-30 boiler modernization, which was implemented at a large boiler plant in the city of Vinnitsa (Ukraine. The project included a number of technical solutions. Six burners were replaced by the two ones that were located in the hearth; also the hearth screen was dismantled. At the same time, reducing the total surface area of the heating caused by the exclusion of hearth screen was compensated by filling the locations of the six embrasures of staff burners on the side screens with straightened furnace tubes. Installing the burners separate from the screen made it possible to eliminate the transfer of vibration to the furnace tubes, and – via them – to the boilers setting. Automation provided “associated regulations”. Draught machines were equipped with frequency regulators. During commissioning of the boiler the studies were carried out that

  11. A metamaterial electromagnetic energy rectifying surface with high harvesting efficiency (United States)

    Duan, Xin; Chen, Xing; Zhou, Lin


    A novel metamaterial rectifying surface (MRS) for electromagnetic energy capture and rectification with high harvesting efficiency is presented. It is fabricated on a three-layer printed circuit board, which comprises an array of periodic metamaterial particles in the shape of mirrored split rings, a metal ground, and integrated rectifiers employing Schottky diodes. Perfect impedance matching is engineered at two interfaces, i.e. one between free space and the surface, and the other between the metamaterial particles and the rectifiers, which are connected through optimally positioned vias. Therefore, the incident electromagnetic power is captured with almost no reflection by the metamaterial particles, then channeled maximally to the rectifiers, and finally converted to direct current efficiently. Moreover, the rectifiers are behind the metal ground, avoiding the disturbance of high power incident electromagnetic waves. Such a MRS working at 2.45 GHz is designed, manufactured and measured, achieving a harvesting efficiency up to 66.9% under an incident power density of 5 mW/cm2, compared with a simulated efficiency of 72.9%. This high harvesting efficiency makes the proposed MRS an effective receiving device in practical microwave power transmission applications.

  12. Characterization of the aspects of osteoprogenitor cell interactions with physical tetracalcium phosphate anchorage on titanium implant surfaces

    International Nuclear Information System (INIS)

    Ko, Chia-Ling; Chang, Ya-Yuan; Liou, Cian-Hua; Chen, Wen-Cheng


    Well-designed implants are used not only to modify the geometry of the implant but also to change the chemical properties of its surfaces. The present study aims to assess the biofunctional effects of tetracalcium phosphate (TTCP) particles as a physical anchor on the implant surface derived through sandblasting. The characteristics of the surface, cell viability, and alkaline phosphatase (ALP) activity toward osteoprogenitor cells (D1) were obtained. D1 cells were cultured on a plain surface that underwent sandblasting and acid etching (SLA) (control SLA group) and on different SLA surfaces with different anchoring TTCP rates (new test groups, M and H). The mean anchoring rates were 57% (M) and 74% (H), and the anchored thickness was estimated to range from 12.6 μm to 18.3 μm. Compared with the control SLA surface on Ti substrate, the new test groups with different TTCP anchoring rates (M and H) failed to improve cell proliferation significantly but had a well-differentiated D1 cell phenotype that enhanced ALP expression in the early stage of cell cultures, specifically, at day 7. Results suggest that the SLA surface with anchored TTCP can accelerate progenitor bone cell mineralization. This study shows the potential clinical application of the constructed geometry in TTCP anchorage on Ti for dental implant surface modification. - Highlights: • TTCP (tetracalcium phosphate) as a physical anchorage on implant is characterized. • Theoretical values of anchored thickness and capping areas were estimated. • TTCP anchored by sandblasting can accelerate progenitor bone cell mineralization. • TTCP anchored on SLA (sandblasting and acid etching) surface is a promising method

  13. Characterization of the aspects of osteoprogenitor cell interactions with physical tetracalcium phosphate anchorage on titanium implant surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Ko, Chia-Ling [Advanced Medical Devices and Composites Laboratory, Department of Fiber and Composite Materials, Feng Chia University, Taichung 40724, Taiwan (China); Dental Medical Devices and Materials Research Center, College of Dental Medicine, Kaohsiung Medical University, Kaohsiung 807, Taiwan (China); Chang, Ya-Yuan; Liou, Cian-Hua [Alliance Global Technology Co., Ltd., Kaohsiung Medical Device Special Zone in Southern Taiwan Science Park, Kaohsiung 82151, Taiwan (China); Chen, Wen-Cheng, E-mail: [Advanced Medical Devices and Composites Laboratory, Department of Fiber and Composite Materials, Feng Chia University, Taichung 40724, Taiwan (China)


    Well-designed implants are used not only to modify the geometry of the implant but also to change the chemical properties of its surfaces. The present study aims to assess the biofunctional effects of tetracalcium phosphate (TTCP) particles as a physical anchor on the implant surface derived through sandblasting. The characteristics of the surface, cell viability, and alkaline phosphatase (ALP) activity toward osteoprogenitor cells (D1) were obtained. D1 cells were cultured on a plain surface that underwent sandblasting and acid etching (SLA) (control SLA group) and on different SLA surfaces with different anchoring TTCP rates (new test groups, M and H). The mean anchoring rates were 57% (M) and 74% (H), and the anchored thickness was estimated to range from 12.6 μm to 18.3 μm. Compared with the control SLA surface on Ti substrate, the new test groups with different TTCP anchoring rates (M and H) failed to improve cell proliferation significantly but had a well-differentiated D1 cell phenotype that enhanced ALP expression in the early stage of cell cultures, specifically, at day 7. Results suggest that the SLA surface with anchored TTCP can accelerate progenitor bone cell mineralization. This study shows the potential clinical application of the constructed geometry in TTCP anchorage on Ti for dental implant surface modification. - Highlights: • TTCP (tetracalcium phosphate) as a physical anchorage on implant is characterized. • Theoretical values of anchored thickness and capping areas were estimated. • TTCP anchored by sandblasting can accelerate progenitor bone cell mineralization. • TTCP anchored on SLA (sandblasting and acid etching) surface is a promising method.

  14. Silicon surface evolution at high temperature in UHV. (United States)

    Ignatescu, Valerian; Blakely, Jack


    The step distribution, associated with the miscut of a Si wafer can be modified by controlled step flow. There are many studies of step-flow dynamics during sublimation or deposition at high temperature. In our group, atomically flat, step-free surfaces were previously obtained over areas of up to 50 by 50 microns by annealing Si samples in UHV. The surface of a normal crystal wafer does not usually show a step-terrace structure. Instead, a Czochralski Si wafer, mirror polished by chemical-mechanical polishing, has an rms roughness of 1-2 nm. A sizable thermal budget has to be used to remove this initial roughness or that induced by reactive ion etching. We report here results of the evolution of step distributions over a range of temperatures. By inducing a temperature gradient on our Si samples we were able to study the stages that occur as the surface transforms towards an atomically flat one. The samples were later reannealed to see the morphological changes that occurred on previously examined regions. We have also investigated the processes of trench formation near the walls of etched craters and of ridge development around the edges of mesas structures.

  15. Drag reduction using wrinkled surfaces in high Reynolds number laminar boundary layer flows (United States)

    Raayai-Ardakani, Shabnam; McKinley, Gareth H.


    Inspired by the design of the ribbed structure of shark skin, passive drag reduction methods using stream-wise riblet surfaces have previously been developed and tested over a wide range of flow conditions. Such textures aligned in the flow direction have been shown to be able to reduce skin friction drag by 4%-8%. Here, we explore the effects of periodic sinusoidal riblet surfaces aligned in the flow direction (also known as a "wrinkled" texture) on the evolution of a laminar boundary layer flow. Using numerical analysis with the open source Computational Fluid Dynamics solver OpenFOAM, boundary layer flow over sinusoidal wrinkled plates with a range of wavelength to plate length ratios ( λ / L ), aspect ratios ( 2 A / λ ), and inlet velocities are examined. It is shown that in the laminar boundary layer regime, the riblets are able to retard the viscous flow inside the grooves creating a cushion of stagnant fluid that the high-speed fluid above can partially slide over, thus reducing the shear stress inside the grooves and the total integrated viscous drag force on the plate. Additionally, we explore how the boundary layer thickness, local average shear stress distribution, and total drag force on the wrinkled plate vary with the aspect ratio of the riblets as well as the length of the plate. We show that riblets with an aspect ratio of close to unity lead to the highest reduction in the total drag, and that because of the interplay between the local stress distribution on the plate and stream-wise evolution of the boundary layer the plate has to exceed a critical length to give a net decrease in the total drag force.

  16. High Efficiency Acetylcholinesterase Immobilization on DNA Aptamer Modified Surfaces

    Directory of Open Access Journals (Sweden)

    Orada Chumphukam


    Full Text Available We report here the in vitro selection of DNA aptamers for electric eel acetylcholinesterase (AChE. One selected aptamer sequence (R15/19 has a high affinity towards the enzyme (Kd = 157 ± 42 pM. Characterization of the aptamer showed its binding is not affected by low ionic strength (~20 mM, however significant reduction in affinity occurred at high ionic strength (~1.2 M. In addition, this aptamer does not inhibit the catalytic activity of AChE that we exploit through immobilization of the DNA on a streptavidin-coated surface. Subsequent immobilization of AChE by the aptamer results in a 4-fold higher catalytic activity when compared to adsorption directly on to plastic.

  17. Designing high-temperature steels via surface science and thermodynamics (United States)

    Gross, Cameron T.; Jiang, Zilin; Mathai, Allan; Chung, Yip-Wah


    Electricity in many countries such as the US and China is produced by burning fossil fuels in steam-turbine-driven power plants. The efficiency of these power plants can be improved by increasing the operating temperature of the steam generator. In this work, we adopted a combined surface science and computational thermodynamics approach to the design of high-temperature, corrosion-resistant steels for this application. The result is a low-carbon ferritic steel with nanosized transition metal monocarbide precipitates that are thermally stable, as verified by atom probe tomography. High-temperature Vickers hardness measurements demonstrated that these steels maintain their strength for extended periods at 700 °C. We hypothesize that the improved strength of these steels is derived from the semi-coherent interfaces of these thermally stable, nanosized precipitates exerting drag forces on impinging dislocations, thus maintaining strength at elevated temperatures.

  18. Highly variable Pliocene sea surface conditions in the Norwegian Sea (United States)

    Bachem, Paul E.; Risebrobakken, Bjørg; De Schepper, Stijn; McClymont, Erin L.


    The Pliocene was a time of global warmth with small sporadic glaciations, which transitioned towards the larger-scale Pleistocene glacial-interglacial variability. Here, we present high-resolution records of sea surface temperature (SST) and ice-rafted debris (IRD) in the Norwegian Sea from 5.32 to 3.14 Ma, providing evidence that the Pliocene surface conditions of the Norwegian Sea underwent a series of transitions in response to orbital forcing and gateway changes. Average SSTs are 2 °C above the regional Holocene mean, with notable variability on millennial to orbital timescales. Both gradual changes and threshold effects are proposed for the progression of regional climate towards the Late Pliocene intensification of Northern Hemisphere glaciation. Cooling from 4.5 to 4.3 Ma may be linked to the onset of poleward flow through the Bering Strait. This cooling was further intensified by a period of cool summers due to weak obliquity forcing. A 7 °C warming of the Norwegian Sea at 4.0 Ma suggests a major increase in northward heat transport from the North Atlantic, leading to an enhanced zonal SST gradient in the Nordic Seas, which may be linked to the expansion of sea ice in the Arctic and Nordic Seas. A warm Norwegian Sea and enhanced zonal temperature gradient between 4.0 and 3.6 Ma may have been a priming factor for increased glaciation around the Nordic Seas due to enhanced evaporation and precipitation at high northern latitudes.

  19. Submonolayer Quantum Dots for High Speed Surface Emitting Lasers

    Directory of Open Access Journals (Sweden)

    Zakharov ND


    Full Text Available AbstractWe report on progress in growth and applications of submonolayer (SML quantum dots (QDs in high-speed vertical-cavity surface-emitting lasers (VCSELs. SML deposition enables controlled formation of high density QD arrays with good size and shape uniformity. Further increase in excitonic absorption and gain is possible with vertical stacking of SML QDs using ultrathin spacer layers. Vertically correlated, tilted or anticorrelated arrangements of the SML islands are realized and allow QD strain and wavefunction engineering. Respectively, both TE and TM polarizations of the luminescence can be achieved in the edge-emission using the same constituting materials. SML QDs provide ultrahigh modal gain, reduced temperature depletion and gain saturation effects when used in active media in laser diodes. Temperature robustness up to 100 °C for 0.98 μm range vertical-cavity surface-emitting lasers (VCSELs is realized in the continuous wave regime. An open eye 20 Gb/s operation with bit error rates better than 10−12has been achieved in a temperature range 25–85 °Cwithout current adjustment. Relaxation oscillations up to ∼30 GHz have been realized indicating feasibility of 40 Gb/s signal transmission.

  20. The Social Organization of the High School: School-Specific Aspects of School Crime (United States)

    Ianni, Francis A. J.


    Describes a study of three New York high schools (rural, suburban, and urban) that developed a model of high school social organization in order to provide a school-specific focus for examining school violence and crime. (JG)

  1. Microfluidic active mixers employing ultra-high aspect-ratio rare-earth magnetic nano-composite polymer artificial cilia

    International Nuclear Information System (INIS)

    Rahbar, Mona; Gray, Bonnie L; Shannon, Lesley


    We present a new micromixer based on highly magnetic, flexible, high aspect-ratio, artificial cilia that are fabricated as individual micromixer elements or in arrays for improved mixing performance. These new cilia enable high efficiency, fast mixing in a microchamber, and are controlled by small electromagnetic fields. The artificial cilia are fabricated using a new micromolding process for nano-composite polymers. Cilia fibers with aspect-ratios as high as 8:0.13 demonstrate the fabrication technique's capability in creating ultra-high aspect-ratio microstructures. Cilia, which are realized in polydimethylsiloxane doped with rare-earth magnetic powder, are magnetized to produce permanent magnetic structures with bidirectional deflection capabilities, making them highly suitable as mixers controlled by electromagnetic fields. Due to the high magnetization level of the polarized nano-composite polymer, we are able to use miniature electromagnets providing relatively small magnetic fields of 1.1 to 7 mT to actuate the cilia microstructures over a very wide motion range. Mixing performances of a single cilium, as well as different arrays of multiple cilia ranging from 2 to 8 per reaction chamber, are characterized and compared with passive diffusion mixing performance. The mixer cilia are actuated at different amplitudes and frequencies to optimize mixing performance. We demonstrate that more than 85% of the total volume of the reaction chamber is fully mixed after 3.5 min using a single cilium mixer at 7 mT compared with only 20% of the total volume mixed with passive diffusion. The time to achieve over 85% mixing is further reduced to 70 s using an array of eight cilia microstructures. The novel microfabrication technique and use of rare-earth permanently-magnetizable nano-composite polymers in mixer applications has not been reported elsewhere by other researchers. We further demonstrate improved mixing over other cilia micromixers as enabled by the high

  2. An in situ vapour phase hydrothermal surface doping approach for fabrication of high performance Co3O4 electrocatalysts with an exceptionally high S-doped active surface. (United States)

    Tan, Zhijin; Liu, Porun; Zhang, Haimin; Wang, Yun; Al-Mamun, Mohammad; Yang, Hua Gui; Wang, Dan; Tang, Zhiyong; Zhao, Huijun


    A facile in situ vapour phase hydrothermal (VPH) surface doping approach has been developed for fabrication of high performance S-doped Co3O4 electrocatalysts with an unprecedentedly high surface S content (>47%). The demonstrated VPH doping approach could be useful for enrichment of surface active sites for other metal oxide electrocatalysts.

  3. Effects of aspect ratio and specimen size on uniaxial failure stress of iron green bodies at high strain rates

    Directory of Open Access Journals (Sweden)

    Kuroyanagi Yuki


    Full Text Available Powder metallurgy is used for the production of a number of mechanical parts and is an essential production method. These are great advantages such as product cost effectiveness and product uniqueness. In general, however parts created by powder metallurgy have low strength because of low density. In order to increase strength as well as density, new techniques such as high-velocity-compaction (HVC was developed and further investigation has been conducted on improvement of techniques and optimum condition using computer simulation. In this study, the effects of aspect ratio and specimen size of iron green bodies on failure strength of uniaxial compression and failure behavior were examined using a split Hopkinson pressure Bar. The diameters of specimens were 12.5 mm and 25 mm the aspect ratios (thickness/diameter were 0.8 and 1.2.

  4. High aspect ratio iridescent three-dimensional metal–insulator–metal capacitors using atomic layer deposition

    Energy Technology Data Exchange (ETDEWEB)

    Burke, Micheal, E-mail:; Blake, Alan; Djara, Vladimir; O' Connell, Dan; Povey, Ian M.; Cherkaoui, Karim; Monaghan, Scott; Scully, Jim; Murphy, Richard; Hurley, Paul K.; Pemble, Martyn E.; Quinn, Aidan J., E-mail: [Tyndall National Institute, University College Cork, Cork (Ireland)


    The authors report on the structural and electrical properties of TiN/Al{sub 2}O{sub 3}/TiN metal–insulator–metal (MIM) capacitor structures in submicron three-dimensional (3D) trench geometries with an aspect ratio of ∼30. A simplified process route was employed where the three layers for the MIM stack were deposited using atomic layer deposition (ALD) in a single run at a process temperature of 250 °C. The TiN top and bottom electrodes were deposited via plasma-enhanced ALD using a tetrakis(dimethylamino)titanium precursor. 3D trench devices yielded capacitance densities of 36 fF/μm{sup 2} and quality factors >65 at low frequency (200 Hz), with low leakage current densities (<3 nA/cm{sup 2} at 1 V). These devices also show strong optical iridescence which, when combined with the covert embedded capacitance, show potential for system in package (SiP) anticounterfeiting applications.

  5. Evaluation of engineering aspects of backfill placement for high level nuclear waste (HLW) deep geologic repositories

    International Nuclear Information System (INIS)

    Roberds, W.; Kleppe, J.; Gonano, L.


    This report includes the identification and subjective evaluation of alternative schemes for backfilling around waste packages and within emplacement rooms. The aspects of backfilling specifically considered in this study include construction and testing; costs have not been considered. However, because construction and testing are simply implementation and verification of design, a design basis for backfill is required. A generic basis has been developed for this study by first identifying qualitative performance objectives for backfill and then weighting each with respect to its potential influence on achieving the repository system performance objectives. Alternative backfill materials and additives have been identified and evaluated with respect to the perceived extent to which each combination can be expected to achieve the backfill design basis. Several distinctly different combinations of materials and additives which are perceived to have the highest potential for achieving the backfill design basis have been selected for further study. These combinations include zeolite/clinoptilolite, bentonite, muck, and muck mixed with bentonite. Feasible alternative construction and testing procedures for each selected combination have been discussed. Recommendations have been made regarding appropriate backfill schemes for hard rock (i.e., basalt at Hanford, Washington, tuff at Nevada Test Site, and generic granite) and salt (i.e., domal salt on the Gulf Coast and generic bedded salt). 27 references, 8 figures, 31 tables


    Directory of Open Access Journals (Sweden)

    Andrei Radu IOVA


    Full Text Available The pupil-teacher communication and the teacher communication skills seem to be key concepts to reach the objectives of the educational act. Recent studies highlight the link between the teacher communication skills, their efficiency, and the fact that these skills could play a more important role for the education that the teaching staff training, his intelligence level and teaching methods. The research goal was the investigation of the aspects specific to the educational communication, that constitute facilitator factors and barriers in the learning process and in the relation teacher-pupil. The quantitative analysis was based on a questionnaire for pupils and teachers, that aimed the investigation of the respondents perception on what it is a good teacher in order to identify those skills that make the difference, from the pupils point of view, and also from the teachers point of view, between a competent teacher and an ineffective one. The research used a double approach, quantitative and qualitative one. The quantitative study allowed the inclusion of a number of 151 subjects and the survey of some dimensions of teacherpupil communication. The qualitative research used a number of 47 subjects, but it allowed the consolidation of the approached topics. The results obtained were interpreted based on the differences that appear in the pupils and teaching staff opinions, but also through the investigation of those dimensions that make the difference, in the case of a model teaching staff, between the pupils and teachers perceptions.

  7. High resolution remote sensing of water surface patterns (United States)

    Woodget, A.; Visser, F.; Maddock, I.; Carbonneau, P.


    The assessment of in-stream habitat availability within fluvial environments in the UK traditionally includes the mapping of patterns which appear on the surface of the water, known as 'surface flow types' (SFTs). The UK's River Habitat Survey identifies ten key SFTs, including categories such as rippled flow, upwelling, broken standing waves and smooth flow. SFTs result from the interaction between the underlying channel morphology, water depth and velocity and reflect the local flow hydraulics. It has been shown that SFTs can be both biologically and hydraulically distinct. SFT mapping is usually conducted from the river banks where estimates of spatial coverage are made by eye. This approach is affected by user subjectivity and inaccuracies in the spatial extent of mapped units. Remote sensing and specifically the recent developments in unmanned aerial systems (UAS) may now offer an alternative approach for SFT mapping, with the capability for rapid and repeatable collection of very high resolution imagery from low altitudes, under bespoke flight conditions. This PhD research is aimed at investigating the mapping of SFTs using high resolution optical imagery (less than 10cm) collected from a helicopter-based UAS flown at low altitudes (less than 100m). This paper presents the initial findings from a series of structured experiments on the River Arrow, a small lowland river in Warwickshire, UK. These experiments investigate the potential for mapping SFTs from still and video imagery of different spatial resolutions collected at different flying altitudes and from different viewing angles (i.e. vertical and oblique). Imagery is processed using 3D mosaicking software to create orthophotos and digital elevation models (DEM). The types of image analysis which are tested include a simple, manual visual assessment undertaken in a GIS environment, based on the high resolution optical imagery. In addition, an object-based image analysis approach which makes use of the

  8. Elaboration of high-temperature friction polymer material and study of its wear aspects

    International Nuclear Information System (INIS)

    Gventsadze, L.


    High-temperature friction composite material is elaborated and its physical, mechanical and tribologic features are studied. It is shown, that addition to the friction material composition of filling material having nanopores -diatomite-and its modification with polyethilensilan leads to friction materials friction coefficient stability and wear resistance increase at high temperatures (400-600 ℃). (author)

  9. Surface aspects of discolouration in Bisphenol A Polycarbonate (BPA-PC), used as lens in LED-based products (United States)

    Yazdan Mehr, M.; van Driel, W. D.; Udono, H.; Zhang, G. Q.


    The surface-related reactions during discolouration of Bisphenol A Polycarbonate (BPA-PC), used as LED lens plates, under thermal stress are studied. X-ray photoelectron spectroscopy (XPS) has been used to monitor the changes in the surface chemistry of BPA-PC plates over a temperature range of 100-140 °C for a period up to 3000 h. Increasing time under thermal stress is associated with the discolouration, and increase in the yellowing index (YI) of PC plastic lens. The XPS results show that discolouration is associated with oxidation at the surface, finding a significant increase in the signal ratio O1s/C1s in the XPS spectra of degraded specimens. During thermal ageing, the Csbnd H concentration decreases and new oxide features Cdbnd O and Osbnd Cdbnd O form, with the latter being a support for oxidation at the surface being a major reaction during discolouration. Results also show that irradiation with blue light during thermal ageing accelerates the kinetics of discolouration and the increased O1s/C1s ratio in XPS spectra.

  10. Exotic high activity surface patterns in PtAu nanoclusters

    KAUST Repository

    Mokkath, Junais Habeeb


    The structure and chemical ordering of PtAu nanoclusters of 79, 135, and 201 atoms are studied via a combination of a basin hopping atom-exchange technique (to locate the lowest energy homotops at fixed composition), a symmetry orbit technique (to find the high symmetry isomers), and density functional theory local reoptimization (for determining the most stable homotop). The interatomic interactions between Pt and Au are derived from the empirical Gupta potential. The lowest energy structures show a marked tendency toward PtcoreAushell chemical ordering by enrichment of the more cohesive Pt in the core region and of Au in the shell region. We observe a preferential segregation of Pt atoms to (111) facets and Au atoms to (100) facets of the truncated octahedron cluster motif. Exotic surface patterns are obtained particularly for Pt-rich compositions, where Pt atoms are being surrounded by Au atoms. These surface arrangements boost the catalytic activity by creating a large number of active sites. © 2013 American Chemical Society.

  11. Core surface flow modelling from high-resolution secular variation

    DEFF Research Database (Denmark)

    Holme, R.; Olsen, Nils


    -flux hypothesis, but the spectrum of the SV implies that a conclusive test of frozen-flux is not possible. We parametrize the effects of diffusion as an expected misfit in the flow prediction due to departure from the frozen-flux hypothesis; at low spherical harmonic degrees, this contribution dominates...... the expected departure of the SV predictions from flow to the observed SV, while at high degrees the SV model uncertainty is dominant. We construct fine-scale core surface flows to model the SV. Flow non-uniqueness is a serious problem because the flows are sufficiently small scale to allow flow around non......-series of magnetic data and better parametrization of the external magnetic field....

  12. Surface sputtering in high-dose Fe ion implanted Si

    International Nuclear Information System (INIS)

    Ishimaru, Manabu


    Microstructures and elemental distributions in high-dose Fe ion implanted Si were characterized by means of transmission electron microscopy and Rutherford backscattering spectroscopy. Single crystalline Si(0 0 1) substrates were implanted at 350 deg. C with 120 keV Fe ions to fluences ranging from 0.1 x 10 17 to 4.0 x 10 17 /cm 2 . Extensive damage induced by ion implantation was observed inside the substrate below 1.0 x 10 17 /cm 2 , while a continuous iron silicide layer was formed at 4.0 x 10 17 /cm 2 . It was found that the spatial distribution of Fe projectiles drastically changes at the fluence between 1.0 x 10 17 and 4.0 x 10 17 /cm 2 due to surface sputtering during implantation

  13. Rapid mold temperature variation for assisting the micro injection of high aspect ratio micro-feature parts using induction heating technology (United States)

    Chen, Shia-Chung; Jong, Wen-Ren; Chang, Yaw-Jen; Chang, Jen-An; Cin, Jin-Chuan


    Hot embossing and injection molding are popular methods to duplicate micro features formed during polymer micro-fabrication of MEMS devices. However, both methods face challenges in filling the polymer melt completely into a micro-featured geometry of a high aspect ratio. In this study, electromagnetic induction heating combined with water cooling is used to achieve rapid mold surface temperature control during the micro-feature injection molding process. A CAE simulation was also developed through integration of both thermal and electromagnetic analysis modules of ANSYS, and its capability and accuracy were verified experimentally. Efficiency evaluations of induction heating and the uniformity of mold temperature control were conducted on a micro-featured mold. This mold was designed with a micro channel array of 30-50 µm in width and 120 and 600 µm in depth, corresponding to aspect ratios ranging from about 2.4 to 12. The accuracies of the micro channels in molded PMMA parts can be used to evaluate the effect of mold temperature on replication accuracy. It was found that rapid mold surface heating with temperature rising from 60 °C to between 100 °C and 140 °C by induction heating requires 2-3.5 s, while the mold temperature returns to 60 °C in about 70-110 s. The simulated mold surface temperature results are consistent with measured results. Achieving the same temperature variation by switching circulation coolants of different temperatures requires at least 7 min. The simulation also reveals that the electromagnetic wave can penetrate into the bottom of the micro channel and results in only about a 2 °C difference in temperature uniformity. For mold temperatures of 100 °C, 120 °C and 140 °C, the molded channel depths were 94.9 µm, 105.4 µm and 116.0 µm, respectively, when the ideal channel depth was 120 µm. When the channel depth is 600 µm, the mold temperature must exceed 120 °C, so that reasonable accuracy in micro-feature replication can be

  14. Predicting the Wear of High Friction Surfacing Aggregate

    Directory of Open Access Journals (Sweden)

    David Woodward


    Full Text Available High friction surfacing (HFS is a specialist type of road coating with very high skid resistance. It is used in the UK at locations where there is significant risk of serious or fatal accidents. This paper considers the aggregate used in HFS. Calcined bauxite is the only aggregate that provides the highest levels of skid resistance over the longest period. No naturally occurring aggregate has been found to give a comparable level of in-service performance. This paper reviews the historical development of HFS in the UK relating to aggregate. In-service performance is predicted in the laboratory using the Wear test which subjects test specimens to an estimated 5–8 years simulated trafficking. Examples are given of Wear test data. They illustrate why calcined bauxite performs better than natural aggregate. They show how the amount of calcined bauxite can be reduced by blending with high skid resistant natural aggregates. Data from the Wear test can be related to every HFS laboratory experiment and road trial carried out in the UK for over the last 50 years. Anyone considering the prediction of HFS performance needs to carefully consider the data given in this paper with any other test method currently being considered or used to investigate HFS.

  15. Climatologies at high resolution for the earth's land surface areas (United States)

    Karger, Dirk Nikolaus; Conrad, Olaf; Böhner, Jürgen; Kawohl, Tobias; Kreft, Holger; Soria-Auza, Rodrigo Wilber; Zimmermann, Niklaus E.; Linder, H. Peter; Kessler, Michael


    High-resolution information on climatic conditions is essential to many applications in environmental and ecological sciences. Here we present the CHELSA (Climatologies at high resolution for the earth's land surface areas) data of downscaled model output temperature and precipitation estimates of the ERA-Interim climatic reanalysis to a high resolution of 30 arc sec. The temperature algorithm is based on statistical downscaling of atmospheric temperatures. The precipitation algorithm incorporates orographic predictors including wind fields, valley exposition, and boundary layer height, with a subsequent bias correction. The resulting data consist of a monthly temperature and precipitation climatology for the years 1979-2013. We compare the data derived from the CHELSA algorithm with other standard gridded products and station data from the Global Historical Climate Network. We compare the performance of the new climatologies in species distribution modelling and show that we can increase the accuracy of species range predictions. We further show that CHELSA climatological data has a similar accuracy as other products for temperature, but that its predictions of precipitation patterns are better.

  16. High Quality Acquisition of Surface Electromyography - Conditioning Circuit Design (United States)

    Shobaki, Mohammed M.; Malik, Noreha Abdul; Khan, Sheroz; Nurashikin, Anis; Haider, Samnan; Larbani, Sofiane; Arshad, Atika; Tasnim, Rumana


    The acquisition of Surface Electromyography (SEMG) signals is used for many applications including the diagnosis of neuromuscular diseases, and prosthesis control. The diagnostic quality of the SEMG signal is highly dependent on the conditioning circuit of the SEMG acquisition system. This paper presents the design of an SEMG conditioning circuit that can guarantee to collect high quality signal with high SNR such that it is immune to environmental noise. The conditioning circuit consists of four stages; consisting of an instrumentation amplifier that is used with a gain of around 250; 4th order band pass filter in the 20-500Hz frequency range as the two initial stages. The third stage is an amplifier with adjustable gain using a variable resistance; the gain could be changed from 1000 to 50000. In the final stage the signal is translated to meet the input requirements of data acquisition device or the ADC. Acquisition of accurate signals allows it to be analyzed for extracting the required characteristic features for medical and clinical applications. According to the experimental results, the value of SNR for collected signal is 52.4 dB which is higher than the commercial system, the power spectrum density (PSD) graph is also presented and it shows that the filter has eliminated the noise below 20 Hz.

  17. Highly variable Pliocene sea surface conditions in the Norwegian Sea

    Directory of Open Access Journals (Sweden)

    P. E. Bachem


    Full Text Available The Pliocene was a time of global warmth with small sporadic glaciations, which transitioned towards the larger-scale Pleistocene glacial–interglacial variability. Here, we present high-resolution records of sea surface temperature (SST and ice-rafted debris (IRD in the Norwegian Sea from 5.32 to 3.14 Ma, providing evidence that the Pliocene surface conditions of the Norwegian Sea underwent a series of transitions in response to orbital forcing and gateway changes. Average SSTs are 2 °C above the regional Holocene mean, with notable variability on millennial to orbital timescales. Both gradual changes and threshold effects are proposed for the progression of regional climate towards the Late Pliocene intensification of Northern Hemisphere glaciation. Cooling from 4.5 to 4.3 Ma may be linked to the onset of poleward flow through the Bering Strait. This cooling was further intensified by a period of cool summers due to weak obliquity forcing. A 7 °C warming of the Norwegian Sea at 4.0 Ma suggests a major increase in northward heat transport from the North Atlantic, leading to an enhanced zonal SST gradient in the Nordic Seas, which may be linked to the expansion of sea ice in the Arctic and Nordic Seas. A warm Norwegian Sea and enhanced zonal temperature gradient between 4.0 and 3.6 Ma may have been a priming factor for increased glaciation around the Nordic Seas due to enhanced evaporation and precipitation at high northern latitudes.

  18. Some design aspects of high-speed vertical-axis wind turbines

    National Research Council Canada - National Science Library

    Templin, R. J; South, P


    ... (rotor height to diameter ratio, solidity, number of blades, etc.) for high-speed vertical-axis wind turbines from kilowatt to megawatt sizes and shows that very large turbines are theoretically feasible...

  19. Structural aspects of high-Tc superconductors from neutron profile refinement studies

    International Nuclear Information System (INIS)

    Sequeira, A.


    The new high-temperature (high-Tc) superconductors have evoked worldwide interest in detecting and characterising their structure and properties. Among the variety of techniques used to characterise these materials, neutron profile refinement using polycrystalline samples has provided the most definitive information regarding their bulk crystal structures. At Trombay the structures of a variety of high-Tc superconductors in the Y-Ba-Cu-O, Tl-Ba-Ca-Cu-O and Bi-Sr-Ca-Cu-O systems have been investigated by neutron diffraction at the high-flux DHRUVA reactor. The results of these investigations are reviewed within the context of the current structural models of these materials and some of the novel structural features observed are highlighted. (orig.)

  20. Key Techniques on Preparing High Aspect Ratio Micro and Nano Structures

    DEFF Research Database (Denmark)

    Jian, Zhao; Lianhe, Dong; Xiaoli, Zhu


    The HSQ has the advantages of high resolution, high contrast and low edge roughness. Through a lot of process experiments, the optimization conditions of the electron beam exposure dose, the proportion of the developer, the developing time and the developing temperature were explored. The relatio......The HSQ has the advantages of high resolution, high contrast and low edge roughness. Through a lot of process experiments, the optimization conditions of the electron beam exposure dose, the proportion of the developer, the developing time and the developing temperature were explored....... The relationship between electron beam exposure dose and line width was explored. The electron beam proximity effect in exposure generated by scattered electrons and backscattered electrons was effectively eliminated. Through adding appropriate NaCl in the conventional developer, the graphic contrast was improved...

  1. Research trends in biomimetic medical materials for tissue engineering: 3D bioprinting, surface modification, nano/micro-technology and clinical aspects in tissue engineering of cartilage and bone. (United States)

    Chen, Cen; Bang, Sumi; Cho, Younghak; Lee, Sahnghoon; Lee, Inseop; Zhang, ShengMin; Noh, Insup


    This review discusses about biomimetic medical materials for tissue engineering of bone and cartilage, after previous scientific commentary of the invitation-based, Korea-China joint symposium on biomimetic medical materials, which was held in Seoul, Korea, from October 22 to 26, 2015. The contents of this review were evolved from the presentations of that symposium. Four topics of biomimetic medical materials were discussed from different research groups here: 1) 3D bioprinting medical materials, 2) nano/micro-technology, 3) surface modification of biomaterials for their interactions with cells and 4) clinical aspects of biomaterials for cartilage focusing on cells, scaffolds and cytokines.

  2. The flow over a 'high' aspect ratio gothic wing at supersonic speeds (United States)

    Narayan, K. Y.


    Results are presented of an experimental investigation on a nonconical wing which supports an attached shock wave over a region of the leading edge near the vertex and a detached shock elsewhere. The shock detachment point is determined from planform schlieren photographs of the flow field and discrepancies are shown to exist between this and the one calculated by applying the oblique shock equations normal to the leading edge. On a physical basis, it is argued that the shock detachment has to obey the two-dimensional law normal to the leading edges. From this, and from other measurements on conical wings, it is thought that the planform schlieren technique may not be particularly satisfactory for detecting shock detachment. Surface pressure distributions are presented and are explained in terms of the flow over related delta wings which are identified as a vertex delta wing and a local delta wing.

  3. Injection molding micro patterns with high aspect ratio using a polymeric flexible stamper

    Directory of Open Access Journals (Sweden)


    Full Text Available Poor filling occurs during the injection molding process of micro- or nano- scale patterns mainly because the hot polymer melt rapidly cools and its skin quickly solidifies upon contact with the mold surface. In this study, it is proposed to use Polyethylene terephthalate (PET film coated with patterned polyurethane acrylate (PUA as an effective thermal barrier. It can significantly hinder heat transfer into the mold during the molding process and thus may keep the melt viscosity low for longer duration. As a result, the replication would be improved not only during the filling phase but also during the packing phase. In order to verify the validity of the use of polymeric stamper, the melt-film interface temperature was evaluated by numerical simulation. Experimental results indicated that patterns possessing widths within the range of one to tens of micrometers and a height of approximately 10 µm were successfully filled and demolded.

  4. Thermal and structural design aspects of high-temperature blankets for fusion synfuel production

    International Nuclear Information System (INIS)

    Powell, J.R.; Fillo, J.A.; Reich, M.


    The most promising process, high temperature electrolysis (HTE) of steam at temperatures of greater than or equal to 1000 0 C is examined. In HTE, a large fraction (up to approx. 50%) of the energy input to split water to hydrogen and oxygen comes from thermal energy. For the projected operating conditions achieved by high temperature fusion blankets, overall efficiencies for hydrogen production should be on the order of 60%. The design, thermal-hydraulics, and materials for such blankets are discussed

  5. Novel silicon fabrication process for high-aspect-ratio micromachined parts

    Energy Technology Data Exchange (ETDEWEB)

    Fleming, J.G.; Barron, C.C.


    Bulk micromachining generally refers to processes involving wet chemical etching of structures formed out of the silicon substrate and so is limited to fairly large, crude structures. Surface micromachining allows intricate patterning of thin films of polysilicon and other materials to form essentially two-dimensional layered parts (since the thickness of the parts is limited by the thickness of the deposited films). There is a third type of micromachining in which the part is formed by filling a mold which was defined by photolithographic means. Historically micromachining molds have been formed in some sort of photopolymer, be it with x-ray lithography (``LIGA``) or more conventional UV lithography, with the aim of producing piece parts. Recently, however, several groups including ours at Sandia have independently come up with the idea of forming the mold for mechanical parts by etching into the silicon substrate itself. In Sandia`s mold process, the mold is recessed into the substrate using a deep silicon trench etch, lined with a sacrificial or etch-stop layer, and then filled with any of a number of mechanical materials. The completed structures are not ejected from the mold to be used as piece parts rather, the mold is dissolved from around selected movable segments of the parts, leaving the parts anchored to the substrate. Since the mold is recessed into the substrate, the whole micromechanical structure can be formed, planarized, and integrated with standard silicon microelectronic circuits before the release etch. In addition, unlike surface-micromachined parts, the thickness of the molded parts is limited by the depth of the trench etch (typically 10--50 {mu}m) rather than the thickness of deposited polysilicon (typically 2 {mu}m). The capability of fabricating thicker (and therefore much stiffer and more massive) parts is critical for motion-sensing structures involving large gimballed platforms, proof masses, etc.

  6. XPS and contact angle study of cotton surface oxidation by catalytic bleaching, Colloids and Surfaces A: Physicochemical and Engineering Aspects, 296

    NARCIS (Netherlands)

    Topalovic, T.; Nierstrasz, Vincent; Bautista, J.; Bautista, Lorenzo; Jocic, Dragan; Jocic, D.; Navarro, Antonio; Warmoeskerken, Marinus


    Surface chemistry and wetting properties of cotton fibres as affected by catalytic bleaching have been investigated. Two types of cotton fabric have been analysed: the regular and a model cotton fabric. In the regular – double scoured cotton fabric, cellulose was contaminated with both non-removable

  7. Nano-patterned superconducting surface for high quantum efficiency cathode

    Energy Technology Data Exchange (ETDEWEB)

    Hannon, Fay; Musumeci, Pietro


    A method for providing a superconducting surface on a laser-driven niobium cathode in order to increase the effective quantum efficiency. The enhanced surface increases the effective quantum efficiency by improving the laser absorption of the surface and enhancing the local electric field. The surface preparation method makes feasible the construction of superconducting radio frequency injectors with niobium as the photocathode. An array of nano-structures are provided on a flat surface of niobium. The nano-structures are dimensionally tailored to interact with a laser of specific wavelength to thereby increase the electron yield of the surface.

  8. Drug-lactose binding aspects in adhesive mixtures: controlling performance in dry powder inhaler formulations by altering lactose carrier surfaces. (United States)

    Zhou, Qi Tony; Morton, David A V


    For dry powder inhaler formulations, micronized drug powders are commonly mixed with coarse lactose carriers to facilitate powder handling during the manufacturing and powder aerosol delivery during patient use. The performance of such dry powder inhaler formulations strongly depends on the balance of cohesive and adhesive forces experienced by the drug particles under stresses induced in the flow environment during aerosolization. Surface modification with appropriate additives has been proposed as a practical and efficient way to alter the inter-particulate forces, thus potentially controlling the formulation performance, and this strategy has been employed in a number of different ways with varying degrees of success. This paper reviews the main strategies and methodologies published on surface coating of lactose carriers, and considers their effectiveness and impact on the performance of dry powder inhaler formulations. Copyright © 2011 Elsevier B.V. All rights reserved.

  9. Improved energy storage, magnetic and electrical properties of aligned, mesoporous and high aspect ratio nanofibers of spinel-NiMn2O4 (United States)

    Bhagwan, Jai; Rani, Stuti; Sivasankaran, V.; Yadav, K. L.; Sharma, Yogesh


    Spinel-NiMn2O4 (NMO) nanofibers of high aspect ratio, high surface area (50 m2 g-1) and homogeneous pore size distribution are fabricated by electrospinning process and characterized by XRD, FTIR, XPS, BET, FESEM, TEM techniques. Further, multifunctional properties (energy storage properties, magnetic and electrical properties) of NMO nanofibers are also examined. High specific capacitance (Cs) of 410 (±5) F g-1 at 1 A g-1, good rate capability and high cycling stability (up to 5000 cycles) are demonstrated by NMO nanofibers. Furthermore, NMO-based solid-state symmetric supercapacitor (SSSC) shows a high Cs of 170 (±5) F g-1 at 0.5 A g-1 in potential range of 0.0V-2.0 V and exhibits excellent energy density of ∼95 W h kg-1 and power density of 1030 W Kg-1. The above storage properties i.e. high energy density and output voltage of 2.0 V are further supplemented by lighting up a red colored LED (1.8 V @ current 20 mA) at least for 5 min. The ionic diffusion coefficient of NMO based electrode is found to be ∼4.84 × 10-11 cm2 s-1. Magnetic and dielectric properties of NMO nanofibers are also examined and results are discussed.

  10. Microstructural and aqueous corrosion aspects of laser-surface-melted type 304 SS plasma-coated mild steel (United States)

    Pujar, M. G.; Dayal, R. K.; Singh Raman, R. K.


    Plasma spray deposition of metals, ceramics, or plastics onto base metals to produce wear- and corrosion-resistant surfaces is a promising technique whereby base metal performance can be considerably im-proved. Because these coatings invariably contain pores, voids, and cracks, laser surface melting may be employed to improve their homogeneity. This study focuses on the corrosion performance of laser- sur-face- melted type 304 SS plasma- coated mild steel specimens. Mild steel strips were plasma coated with an approximately 100 to 200 μm thick layer of type 304 by transferred plasma jet. These specimens were sub-sequently laser irradiated using a 3 kW continuous- wave CO2 gas laser. Eight different sets of specimens were selected based on different laser beam travel speeds. Scanning electron microscopic studies of the plasma- coated specimens revealed both pancake and flowery types of deposited particles. Optical micro-scopic studies followed by anodic polarization experiments were carried out on these specimens in IN H2SO4 medium. It was observed that specimens with laser beam interaction times ranging from 30 to 120 ms showed relatively better general corrosion performance than specimens with interaction times of from 15 to 24 ms.

  11. High power density systems used in advanced metallurgical applications and safety aspects

    International Nuclear Information System (INIS)

    Mirji, K.V.; Ramesh, N.


    This topic concerns about the operation and development of electron beam (EB) machines utilized in metallurgical applications such as EB melting and EB welding. They are popular in purification of refractory metals and welding of their alloy components. In this equipment, EB generation, acceleration, harnessing and energy dissipation need to be performed under high vacuum conditions. The high voltage required for acceleration is generated by using 3 phase 415 Volts, 50 Hz ac power supply. The transformers used have to be specially designed to withstand frequent, high short circuit currents which result from discharges during processing. The high voltage rectifiers are similarly designed to cater to such duties, apart from generating high voltage with low ripple contents. Apart from trans-rectifiers, the cables need to be designed with proper termination at the gun to ensure safety of operating personnel, while ensuring ease of connection. Practical problems of electric discharges due to sudden evolution of gaseous and metallic impurities, proper dissipation of residual charge on cathode assembly and the EB gun need to be handled carefully. (author)

  12. Multiple aspects of high school students' strategic processing on reading outcomes: The role of quantity, quality, and conjunctive strategy use. (United States)

    Parkinson, Meghan M; Dinsmore, Daniel L


    While the literature on strategy use is relatively mature, measures of strategy use overwhelmingly measure only one aspect of that use, frequency, when relating that strategy use to performance outcomes. While this might be one important attribute of strategy use, there is increasing evidence that quality and conditional use of cognitive and metacognitive strategies may also be important. This study examines how multiple aspects of strategy use, namely frequency, quality, and conjunctive use of strategies, influence task performance on both well- and ill-structured task outcomes in addition to other concomitant variables that may interact with strategic processing during reading. The sample consisted of 21 high school students enrolled in an upper-level biology class in a suburban school in the north-eastern United States. These participants completed measures of prior knowledge and interest, then read either an expository or persuasive text while thinking aloud. They then completed a passage recall and open-ended response following passage completion. In general, quantity was not positively related to the study outcomes and was negatively related to one of them. Quality of strategy use, on the other hand, was consistently related to positive reading outcomes. The influence of knowledge and interest in terms of strategies is also discussed as well as six cases which illustrate the relation of aspects of strategy use and the other concomitant variables. Evaluating strategy use by solely examining the frequency of strategy use did not explain differences in task performance as well as evaluating the quality and conjunctive use of strategies. Further, important relations between prior knowledge, interest, and the task outcomes appeared to be mediated and moderated by the aspects of strategy use investigated. © 2017 The British Psychological Society.

  13. Electrochemical growth of high-aspect ratio nanostructured silver chloride on silver and its application to miniaturized reference electrodes

    Energy Technology Data Exchange (ETDEWEB)

    Safari, S; Selvaganapathy, P R [Department of Mechanical Engineering, McMaster University, Hamilton, ON, L8S 4L7 (Canada); Derardja, A [Faculty of Science and Engineering, University of Batna (Algeria); Deen, M J, E-mail:, E-mail: [Electrical and Computer Engineering, McMaster University, Hamilton, ON, L8S 4L8 (Canada)


    The sensitivity of many biological and chemical sensors is critically dependent on the stability of the potential of the reference electrode being used. The stability of a reference electrode's potential is highly influenced by the properties of its surface. In this paper, for the first time, the formation of nanosheets of silver chloride on silver wire is observed and controlled using high anodic constant potential (>0.5 V) and pulsed electrodeposition. The resulting nanostructured morphology substantially improves the electrode's potential stability in comparison with the conventional globular surface structure. The increased stability is attributed to the increase in the surface area of the silver chloride produced by the nanosheet formation.

  14. Aspects of the selection, design and use of high lysine cereals

    International Nuclear Information System (INIS)

    Munck, L.


    A discussion of the need for and the considerations involved in the breeding of high lysine cereals is presented. Progress in the discovery and exploitation of genotypes with high lysine characters in maize and barley are briefly reviewed. The role and some of the characteristics of the dye-binding capacity (DBC) methods are evaluated along with the ways in which DBC results should be used in combination with other information. Lastly, the changes in attitudes and procedures associated with the acceptance of a product of a new technology such as nutritionally improved cereals is discussed. (author)

  15. Some aspects of the applications of wire chambers in high energy physics experiments at large accelerators

    International Nuclear Information System (INIS)

    Turala, M.


    An application of proportional and drift chambers in four large spectrometers at the accelerators of IHEP Serpukhov and CERN Geneva is described. An operation of wire chambers at high intensities and high multiplicities of particles is discussed. The results of investigations of their efficiencies, spatial resolution (for one and two-dimensional readout) and long term stability are presented. Problems of preselection of a given class of events are discussed. The systems for preselection of defined multiplicities or a scattering angle of particles, in which proportional chambers have been used, are described and the results of their application in the real experiments are presented. (author)

  16. Aspects of High-Q Tunable Antennas and Their Deployment for 4G Mobile Communications

    DEFF Research Database (Denmark)

    Bahramzy, Pevand; Jagielski, Ole; Svendsen, Simon


    Tunable antennas are very promising for future generations of mobile communications, where broad frequency coverage will be required increasingly. This work describes the design of small high-Quality factor (Q) tunable antennas based on Micro-Electro-Mechanical Systems (MEMS), which are capable o...

  17. High-Aspect-Ratio CMOS add-on modules for RF passive components

    NARCIS (Netherlands)

    Sagkol, H.


    Commercial wireless communication technologies stemmed mostly from the research done through and after the Second World War as outlined in Chapter 1. Earlier systems were intended for military applications, hence had very high performance and were very expensive and bulky. Later, with the dawn of


    Directory of Open Access Journals (Sweden)

    Sergey F. Rodionov


    Full Text Available The approach is offered to development of the informational and educational environment of high technical school,based on deep integration of electronic educational content with methods and tools for the engineering problemssolving. The application program interface (API is used asthe main integration instrument, which modern Its have.

  19. Plasma-surface interactions under high heat and particle fluxes

    NARCIS (Netherlands)

    De Temmerman, G.; Bystrov, K.; Liu, F.; Liu, W.; Morgan, T.; Tanyeli, I.; van den Berg, M.; Xu, H.; Zielinski, J.


    The plasma-surface interactions expected in the divertor of a future fusion reactor are characterized by extreme heat and particle fluxes interacting with the plasma-facing surfaces. Powerful linear plasma generators are used to reproduce the expected plasma conditions and allow plasma-surface

  20. High-surface-area silica nanospheres (KCC-1) with a fibrous morphology

    KAUST Repository

    Polshettiwar, Vivek


    Fibrous nanosilica: A new family of high-surface-area silica nanospheres (KCC-1) have been prepared (see picture). KCC-1 features excellent physical properties, including high surface area, unprecedented fibrous surface morphology, high thermal (up to 950 °C) and hydrothermal stabilities, and high mechanical stability. Copyright © 2010 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  1. Certification and safety aspects relating to the transport of passengers on high altitude balloons in Europe (United States)

    Schoenmaker, Annelie


    High-altitude balloons typically fly between 25 and 50 km in altitude, which, while below the Karman line of 100 km, is yet far above the altitudes typically flown by aircraft. For example, the highest-flying commercial aircraft - the Concorde - had a maximum cruising altitude of only 18 km. zero2infinity, a Spanish company, is currently developing a pressurized pod named “bloon” which will be capable of lifting six people, including two pilot crew members and four paying passengers, to an altitude of 36 km through the use of high-altitude balloons. The boundary between Airspace and Outer Space has never been legally defined, mostly because of the lack of activities taking place between the altitude where airplanes fly and the lowest orbiting spacecraft. High-altitude balloons do fly at these in-between altitudes and the prospect of commercializing access to these parts of the stratosphere poses some questions in a new light. Given the relatively low altitude at which they fly, it may well be that these types of balloons would be considered to operate exclusively within air space. However, given the technology involved in crewed high altitude balloon flights, which is more similar to spacecraft engineering than to traditional hot-air or gas ballooning, it is necessary to evaluate the various legal regimes, codes, and regulations that would apply to such flights, especially regarding licenses and liabilities. For high altitude balloon flights commencing in Europe, the European Aviation Safety Agency (EASA) would very likely be the competent certification or licensing agency for these flights, although there would likely be input from various national aviation authorities as well. However, because the European Commission (EC) has not yet issued regulations regarding commercial spaceflight, particularly the use of high altitude balloons, new rules and regulations governing such flights may still need to be drafted and promulgated. With the development of

  2. Nano-scaled graphene platelets with a high length-to-width aspect ratio (United States)

    Zhamu, Aruna; Guo, Jiusheng; Jang, Bor Z.


    This invention provides a nano-scaled graphene platelet (NGP) having a thickness no greater than 100 nm and a length-to-width ratio no less than 3 (preferably greater than 10). The NGP with a high length-to-width ratio can be prepared by using a method comprising (a) intercalating a carbon fiber or graphite fiber with an intercalate to form an intercalated fiber; (b) exfoliating the intercalated fiber to obtain an exfoliated fiber comprising graphene sheets or flakes; and (c) separating the graphene sheets or flakes to obtain nano-scaled graphene platelets. The invention also provides a nanocomposite material comprising an NGP with a high length-to-width ratio. Such a nanocomposite can become electrically conductive with a small weight fraction of NGPs. Conductive composites are particularly useful for shielding of sensitive electronic equipment against electromagnetic interference (EMI) or radio frequency interference (RFI), and for electrostatic charge dissipation.

  3. Geological aspects of the high level waste and spent fuel disposal programme in Slovakia

    Energy Technology Data Exchange (ETDEWEB)

    Matej, Gedeon; Milos, Kovacik; Jozef, Hok [Geological Survey of Slovak Republic, Bratislava (Slovakia)


    An autonomous programme for development of a deep geological high level waste and spent fuel disposal began in 1996. One of the most important parts in the programme is siting of the future deep seated disposal. Geological conditions in Slovakia are complex due to the Alpine type tectonics that formed the geological environment during Tertiary. Prospective areas include both crystalline complexes (tonalites, granites, granodiorites) and Neogene (Miocene) argillaceous complexes. (author)

  4. Numerical aspects of the modelling of the local effects of a high level waste repository

    International Nuclear Information System (INIS)

    Ferreri, J.C.; Ventura, M.A.


    The numerical approximations adapted for the development of the computational models for the prediction of the effects of the emplacement of a high level waste repository are reviewed. The problems considered include: the thermal history of the rocky mass constituting the burial media, the flow of underground water and the associated migration of radionuclides in the same media. Results associated with verification of the implemented codes are presented. Their limitations and advantages are discussed. (Author) [es

  5. Nuclear design aspect of the Korean high intensity proton accelerator project

    Energy Technology Data Exchange (ETDEWEB)

    Chang, Jonghwa; Song, Tae-Yung [Korea Atomic Energy Research Inst., Yusong, Taejon (Korea, Republic of)


    A plan to construct a high current proton accelerator has been proposed by KAERI. We are presenting the required nuclear design to support the project as well as a brief overview of the proposed proton accelerator. The target and core design is highlighted to show feasibility of incineration of minor actinides from the spent fuel of light water reactors. Radiation shielding and activation analyses are also important for the design and the license of the accelerator. (author)

  6. Coal upgrading based on the high temperature reactor - engineering and economic aspects

    International Nuclear Information System (INIS)

    Barnert, H.; Neis, H.


    The development of the high temperature reactor in the FRG was opened with the aim of economically producing electricity which might be achieved with the next project works. Moreover, the HTR supplies process heat of very high temperature which may be used with metallic heat exchangers in the range up to 1000 0 C. From these reasons and regarding the world power prospects and the special power situation in our own country, the FRG began to develop methods of upgrading fossil primary energy sources using high-temperature heat from the HTR about 15 years ago. Meanwhile great progress has been achieved in research, development and test works; the modules are developed to a great extent. Economical service is expected for future utilization of selected processes. Problems to be still accomplished are first of all related to system testing as well as further exhaustion of the HTR's temperature potential. The proposed extension of the AVR to some process heat facility offers the possibility of testing the system in a low-cost and accelerated manner. (author)

  7. Assessment of the radiological protection aspects of disposal of high level waste on the ocean floor

    International Nuclear Information System (INIS)

    Grimwood, P.D.; Webb, G.A.M.


    This study is a preliminary assessment of the potential radiological consequences of disposal of solidified high-level radioactive waste on the floor of the deep ocean. As an input to the modelling used in the assessment, an arbitrary choice is made to consider the total high-level waste which would be generated by a postulated world nuclear power programme to the year 2000. It is assumed that all this waste, in solidified form, is disposed of on to the floor of the North Atlantic. The body of this report is the modelling of the subsequent release of activity into the water, its dispersion in the ocean and eventual uptake in marine organisms and sediments. The consequent radiation exposure of man is assessed in terms of both individual and collective doses. It is intended that only broad conclusions should be drawn from this study. The objective of the assessment is to highlight those subject areas where more study of information is required before a decision can be reached regarding this method of disposal. No overriding reason connected with the radiological protection considerations has been identified which would preclude the disposal of suitably conditioned high-level waste on the ocean floor. Further evaluation of this disposal option is therefore justified. (author)


    Directory of Open Access Journals (Sweden)

    Otstavnov Stanislav Sergeevich


    Full Text Available The article presents the data obtained from comprehensive study of russian hi-tech medical equipment market. The size and the structure of Russian medical equipment market in 2005-2011 were investigated and market size forecast for 2012-2015 was given. Priority segments of Russian high-tech medical equipment market were identified (products with a high degree of visualization, anesthetic and ventilation equipment, patient monitors based on the analysis of literature sources and morbidity structure. Key players in key segments of the market were identified and their financial performance such as number of employees, revenue, net profit, researches and development expenses were compared (according to actual annual reports. Research allowed to draw the following conclusion: today in the key segments of Russian high-tech medical equipment market the leadership of foreign companies (Hitachi, Philips, Siemens, Toshiba, General Electric, Dräger is indisputable, objective preconditions for the fundamental change of the situation are absent. Import substitution requires the consolidation of domestic producers, adequate funding and human resource. The results can be used in practice by medical industry companies and State authorities on purpose to upgrade the medical industry.


    Directory of Open Access Journals (Sweden)

    Станислав Сергеевич Отставнов


    Full Text Available The article presents the data obtained from comprehensive study of russian hi-tech medical equipment market. The size and the structure of Russian medical equipment market in 2005-2011 were investigated and market size forecast for 2012-2015 was given. Priority segments of Russian high-tech medical equipment market were identified (products with a high degree of visualization, anesthetic and ventilation equipment, patient monitors  based on the analysis of literature sources and morbidity structure. Key players in key segments of the market were identified and their financial performance such as number of employees, revenue, net profit, researches and development expenses were compared (according to actual annual reports.Research allowed to draw the following conclusion: today in the key segments of Russian high-tech medical equipment market the leadership of foreign companies  (Hitachi, Philips, Siemens, Toshiba, General Electric, Dräger is indisputable, objective preconditions for the fundamental change of the situation are absent. Import substitution requires the consolidation of domestic producers, adequate funding and human resource.The results can be used in practice by medical industry companies and State authorities on purpose to upgrade the medical industry.DOI:

  10. Some Aspects of High $E_T$ Jets in p-p Collisions at LHC

    CERN Document Server

    AUTHOR|(CDS)2070208; Kohli, J M


    The Higgs boson is a hypothetical massive scalar elementary particle predicted to exist by the Standard Model of particle physics. It is the only Standard Model particle not yet observed. It plays a key role in explaining the origin of the mass of other elementary particles, in particular the difference between the massless photon and the very heavy W and Z bosons. Low mass Standard Model Higgs decay predominantly into bbbar mode. The relatively high number of signal events at low Higgs masses is nonetheless much smaller compared to the number of background events especially QCD, which makes a search delicate in this channel. One way to reduce an enormous background is to study Weak Boson Fusion produced Higgs boson which is characterized by two high ET back to back jets in opposite rapidity region. The two high ET jets at opposite rapidity can be used to tag the events where Higgs is produced. Since at LHC, the real data will emerge only after year 2007, the simulated data is the need for the physics analysi...

  11. A PIV Study of Baseline and Controlled Flow over the Highly Deflected Flap of a Generic Low Aspect Ratio Trapezoidal Wing (United States)

    Tewes, Philipp; Genschow, Konstantin; Little, Jesse; Wygnanski, Israel


    A detailed flow survey using PIV was conducted over a highly-deflected flap (55°) of a low-aspect ratio trapezoidal wing. The wing section is a NACA 0012 with 45° sweep at both the leading and trailing edges, an aspect ratio of 1.5 and a taper ratio of 0.27. The main element is equipped with 7 equally spaced fluidic oscillators, covering the inner 60 % of the span, located near the flap hinge. Experiments were carried out at 0° and 8° incidence at a Reynolds number of 1.7 .106 for both baseline and active flow control (AFC) cases. Velocity ISO-surfaces, x-vorticity and streamlines are analyzed / discussed. A flap leading edge vortex governs the baseline flow field for 0°. This vortical structure interacts with the jets emitted by the actuators (Cμ = 1 %). Its development is hampered and the vortex is redirected toward the trailing edge resulting in a CL increase. At 8°, the dominant flap leading edge vortex could not be detected and is believed to have already merged with the tip vortex. AFC attached the flow over the flap and enhanced the lift by up to 20 % while maintaining longitudinal stability. The dominant flow features in the AFC cases are actuator-generated streamwise vortices which appear stronger at 8°. This work was supported by the Office of Naval Research under ONR Grant No. N00014-14-1-0387.

  12. Echo planar perfusion imaging with high spatial and temporal resolution: methodology and clinical aspects

    International Nuclear Information System (INIS)

    Bitzer, M.; Klose, U.; Naegele, T.; Friese, S.; Kuntz, R.; Voigt, K.; Fetter, M.; Opitz, H.


    The purpose of the present study was to analyse specific advantages of calculated parameter images and their limitations using an optimized echo-planar imaging (EPI) technique with high spatial and temporal resolution. Dynamic susceptibility contrast magnetic resonance imaging (DSC-MRI) was performed in 12 patients with cerebrovascular disease and in 13 patients with brain tumours. For MR imaging of cerebral perfusion an EPI sequence was developed which provides a temporal resolution of 0.68 s for three slices with a 128 x 128 image matrix. To evaluate DSC-MRI, the following parameter images were calculated pixelwise: (1) Maximum signal reduction (MSR); (2) maximum signal difference (ΔSR); (3) time-to-peak (T p ); and (4) integral of signal-intensity-time curve until T p (S Int ). The MSR maps were superior in the detection of acute infarctions and ΔSR maps in the delineation of vasogenic brain oedema. The time-to-peak (T p ) maps seemed to be highly sensitive in the detection of poststenotic malperfused brain areas (sensitivity 90 %). Hyperperfused areas of brain tumours were detectable down to a diameter of 1 cm with high sensitivity (> 90 %). Distinct clinical and neuroradiological conditions revealed different suitabilities for the parameter images. The time-to-peak (T p ) maps may be an important advantage in the detection of poststenotic ''areas at risk'', due to an improved temporal resolution using an EPI technique. With regard to spatial resolution, a matrix size of 128 x 128 is sufficient for all clinical conditions. According to our results, a further increase in matrix size would not improve the spatial resolution in DSC-MRI, since the degree of the vascularization of lesions and the susceptibility effect itself seem to be the limiting factors. (orig.)

  13. Technological aspects of lift-slab method in high-rise-building construction. (United States)

    Gaidukov, Pavel V.; Pugach, Evgeny M.


    The utilization efficiency of slab lifting technology for high-rise-building construction is regarded in the present article. The main problem of the article is organizing technology abilities indication, which proves the method application possibility. There is the comparing of lifting technologies and sequential concrete-frame extension, as follows: the first one: the parameters are defined, and the second one: the organizational model is executed. This model defines borders of the usage methods, as well. There is the mathematic model creating, which describes boundary conditions of the present technologies usage. This model allows to predict construction efficiency for different stored-number buildings.

  14. Aspects of flexural behavior of high strength concrete elements with or without steel fibers

    Directory of Open Access Journals (Sweden)

    Gheorghe-Alexandru Bărbos


    Full Text Available Steel fiber reinforced high strength concrete (SFRHSC is concrete made of hydraulic cements containing fine or fine and coarse aggregate and discontinuous discrete steel fibers. In tension, SFRHSC fails only after the steel fiber breaks or is pulled out of the cement matrix. A more general and current approach to the mechanics of fiber reinforcing assumes a crack arrest mechanism based on fracture mechanics. In this model, the energy to extend a crack and debond the fibers in the matrix relates to the properties of the composite. The designers may best view SFRHSC as a concrete with increased strain capacity, impact resistance, energy absorption, fatigue endurance and tensile strength.

  15. The anomalous high temperatures of November 2010 over Greece: meteorological and climatological aspects

    Directory of Open Access Journals (Sweden)

    K. Tolika


    Full Text Available This paper presents an analysis of the exceptionally high maximum (Tmax and minimum (Tmin temperatures which occurred during November 2010 and affected the entire Greek region. This severe "warm cold-season spell" was unusual because of its prolonged duration and intensity for the entire month and particularly the maximum temperature anomalies, which in comparison with the 1958–2000 climatological average, exceeded 5 °C at several stations. Comparing the observed record with future projections from three regional climate models revealed that Tmax and Tmin, on several days in November 2010, exceeded the 90th percentile of the simulated data. An examination of the atmospheric – synoptic conditions during this period showed that the anomalous high temperatures could probably be related to the negative phase of the Eastern Mediterranean Pattern (EMP, with an intense pole of negative anomalies located over the British Isles, and to the east, a second pole of positive anomalies, centred over the Caspian Sea. Finally, an attempt is made to further investigate the mechanisms responsible for this phenomenon, for example, the thermal forcing in the tropics (Niño 3 or Niño 3.4.

  16. The anomalous high temperatures of November 2010 over Greece: meteorological and climatological aspects (United States)

    Tolika, K.; Pytharoulis, I.; Maheras, P.


    This paper presents an analysis of the exceptionally high maximum (Tmax) and minimum (Tmin) temperatures which occurred during November 2010 and affected the entire Greek region. This severe "warm cold-season spell" was unusual because of its prolonged duration and intensity for the entire month and particularly the maximum temperature anomalies, which in comparison with the 1958-2000 climatological average, exceeded 5 °C at several stations. Comparing the observed record with future projections from three regional climate models revealed that Tmax and Tmin, on several days in November 2010, exceeded the 90th percentile of the simulated data. An examination of the atmospheric - synoptic conditions during this period showed that the anomalous high temperatures could probably be related to the negative phase of the Eastern Mediterranean Pattern (EMP), with an intense pole of negative anomalies located over the British Isles, and to the east, a second pole of positive anomalies, centred over the Caspian Sea. Finally, an attempt is made to further investigate the mechanisms responsible for this phenomenon, for example, the thermal forcing in the tropics (Niño 3 or Niño 3.4).

  17. Important aspects for consideration in minimizing plant outage times. Swiss experience in achieving high availability

    International Nuclear Information System (INIS)

    Malcotsis, G.


    Operation of Swiss nuclear power plants has not been entirely free of trouble. They have experienced defective fuel elements, steam generator tube damage, excessive vibration of the core components, leakages in the recirculation pump seals and excessive corrosion and erosion in the steam-feedwater plant. Despite these technical problems in the early life of the plants, on overall balance the plants can be considered to have performed exceedingly well. The safety records from more than 40 reactor-years of operation are excellent and, individually and collectively, the capacity factors obtained are among the highest in the world. The problems mentioned have been solved and the plants continue operation with high availabilities. This success can be attributed to the good practices of the utilities with regard to the choice of special design criteria, plant organization, plant operation and plant maintenance, and also to the pragmatic approach of the licensing authorities and their consultants to quality assurance and quality control. The early technical problems encountered, the corresponding solutions adopted and the factors that contributed towards achieving high availabilities in Swiss nuclear power plants are briefly described. (author)

  18. Mechanisms involved in the hydrothermal growth of ultra-thin and high aspect ratio ZnO nanowires

    Energy Technology Data Exchange (ETDEWEB)

    Demes, Thomas [Univ. Grenoble Alpes, CNRS, Grenoble-INP, LMGP, F-38000 Grenoble (France); Ternon, Céline, E-mail: [Univ. Grenoble Alpes, CNRS, Grenoble-INP, LMGP, F-38000 Grenoble (France); Univ. Grenoble Alpes, CNRS, LTM, F-38000 Grenoble (France); Morisot, Fanny [Univ. Grenoble Alpes, CNRS, Grenoble-INP, LMGP, F-38000 Grenoble (France); Univ. Grenoble Alpes, CNRS, Grenoble-INP" 2, IMEP-LaHC, F-38000 Grenoble (France); Riassetto, David [Univ. Grenoble Alpes, CNRS, Grenoble-INP, LMGP, F-38000 Grenoble (France); Legallais, Maxime [Univ. Grenoble Alpes, CNRS, Grenoble-INP, LMGP, F-38000 Grenoble (France); Univ. Grenoble Alpes, CNRS, Grenoble-INP" 2, IMEP-LaHC, F-38000 Grenoble (France); Roussel, Hervé; Langlet, Michel [Univ. Grenoble Alpes, CNRS, Grenoble-INP, LMGP, F-38000 Grenoble (France)


    Highlights: • ZnO nanowires are grown on sol-gel ZnO seed layers by hydrothermal synthesis. • Ultra-thin and high aspect ratio nanowires are obtained without using additives. • Nanowire diameter is 20–25 nm regardless of growth time and seed morphology. • A nanowire growth model is developed on the basis of thermodynamic considerations. • The nanowires are intended for integration into electrically conductive nanonets. - Abstract: Hydrothermal synthesis of ZnO nanowires (NWs) with tailored dimensions, notably high aspect ratios (AR) and small diameters, is a major concern for a wide range of applications and still represents a challenging and recurring issue. In this work, an additive-free and reproducible hydrothermal procedure has been developed to grow ultra-thin and high AR ZnO NWs on sol-gel deposited ZnO seed layers. Controlling the substrate temperature and using a low reagent concentration (1 mM) has been found to be essential for obtaining such NWs. We show that the NW diameter remains constant at about 20–25 nm with growth time contrary to the NW length that can be selectively increased leading to NWs with ARs up to 400. On the basis of investigated experimental conditions along with thermodynamic and kinetic considerations, a ZnO NW growth mechanism has been developed which involves the formation and growth of nuclei followed by NW growth when the nuclei reach a critical size of about 20–25 nm. The low reagent concentration inhibits NW lateral growth leading to ultra-thin and high AR NWs. These NWs have been assembled into electrically conductive ZnO nanowire networks, which opens attractive perspectives toward the development of highly sensitive low-cost gas- or bio-sensors.

  19. Length-dependent charge generation from vertical arrays of high-aspect-ratio ZnO nanowires. (United States)

    Rivera, Vivian Farías; Auras, Florian; Motto, Paolo; Stassi, Stefano; Canavese, Giancarlo; Celasco, Edvige; Bein, Thomas; Onida, Barbara; Cauda, Valentina


    Aqueous chemical growth of zinc oxide nanowires is a flexible and effective approach to obtain dense arrays of vertically oriented nanostructures with high aspect ratio. Herein we present a systematic study of the different synthesis parameters that influence the ZnO seed layer and thus the resulting morphological features of the free-standing vertically oriented ZnO nanowires. We obtained a homogeneous coverage of transparent conductive substrates with high-aspect-ratio nanowire arrays (length/diameter ratio of up to 52). Such nanostructured vertical arrays were examined to assess their electric and piezoelectric properties, and showed an electric charge generation upon mechanical compressive stress. The principle of energy harvesting with these nanostructured ZnO arrays was demonstrated by connecting them to an electronic charge amplifier and storing the generated charge in a series of capacitors. We found that the generated charge and the electrical behavior of the ZnO nanowires are strictly dependent on the nanowire length. We have shown the importance of controlling the morphological properties of such ZnO nanostructures for optimizing a nanogenerator device. Copyright © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  20. Nonlinear Large Deflection Theory with Modified Aeroelastic Lifting Line Aerodynamics for a High Aspect Ratio Flexible Wing (United States)

    Nguyen, Nhan; Ting, Eric; Chaparro, Daniel


    This paper investigates the effect of nonlinear large deflection bending on the aerodynamic performance of a high aspect ratio flexible wing. A set of nonlinear static aeroelastic equations are derived for the large bending deflection of a high aspect ratio wing structure. An analysis is conducted to compare the nonlinear bending theory with the linear bending theory. The results show that the nonlinear bending theory is length-preserving whereas the linear bending theory causes a non-physical effect of lengthening the wing structure under the no axial load condition. A modified lifting line theory is developed to compute the lift and drag coefficients of a wing structure undergoing a large bending deflection. The lift and drag coefficients are more accurately estimated by the nonlinear bending theory due to its length-preserving property. The nonlinear bending theory yields lower lift and span efficiency than the linear bending theory. A coupled aerodynamic-nonlinear finite element model is developed to implement the nonlinear bending theory for a Common Research Model (CRM) flexible wing wind tunnel model to be tested in the University of Washington Aeronautical Laboratory (UWAL). The structural stiffness of the model is designed to give about 10% wing tip deflection which is large enough that could cause the nonlinear deflection effect to become significant. The computational results show that the nonlinear bending theory yields slightly less lift than the linear bending theory for this wind tunnel model. As a result, the linear bending theory is deemed adequate for the CRM wind tunnel model.

  1. Safety aspects of forced flow cooldown transients in modular high temperature gas-cooled reactors

    International Nuclear Information System (INIS)

    Kroeger, P.G.


    During some of the design basis accidents in Modular High Temperature Gas Cooled Reactors (MHTGRs) the main Heat Transport System (HTS) and the Shutdown Cooling System (SCS), are assumed to have failed. Decay heat is then removed by the passive Reactor Cavity Cooling System (RCCS) only. If either forced flow cooling system becomes available during such a transient, its restart could significantly reduce the down-time. This paper uses the THATCH code to examine whether such restart, during a period of elevated core temperatures, can be accomplished within safe limits for fuel and metal component temperatures. If the reactor is scrammed, either system can apparently be restarted at any time, without exceeding any safe limits. However, under unscrammed conditions a restart of forced cooling can lead to recriticality, with fuel and metal temperatures significantly exceeding the safety limits

  2. Some aspects of the metal purity in high strength Al-alloys

    International Nuclear Information System (INIS)

    Banizs, K.; Csernay-Balint, J.; Voeroes, G.


    The effect of Fe and Si on the properties of some high strength age-hardenable Al-alloys was investigated. It was found that a certain quantity (> 0.15 %) of Fe is advantageous to the formation of the cell-structure in the cast ingot both in the AlCuMg and AlZnMgCu alloys. An increased Fe-content causes a finer cell-structure. A higher Fe:Si ratio results in more homogeneous cell size distribution. Higher Si-content in the alloy decreases the favourable cast parameter range and increases the inclination to cracking of large diameter (> 270 mm) ingots. The reason of the correlation found between metal purity and mechanical properties is discussed

  3. Theoretical aspects of some collective instabilities in high-energy particle storage rings

    International Nuclear Information System (INIS)

    Ruggiero, F.


    After an introduction to single-particle dynamics, based on a unified Hamiltonian treatment of betatron and synchrotron oscillations, we consider two examples of collective instabilities which can limit the performances of high-energy storage rings: the transverse mode coupling instability, due to wake fields, and the incoherent beam-beam instability. Special emphasis is placed on the localization of the interactions between particles and surrounding structures, such as the accelerating RF cavities. We derive an exact invariant for the linearized synchrotron motion and, starting from the Vlasov equation, we discuss the coherent synchro-betatron resonances caused by localized impedance. Under suitable assumptions, we show that the effect of the beam-beam kicks in electron-positron machines can be described by new diffusive terms in a ''renormalized'' Fokker-Planck equation and is therefore equivalent to an additional source of noise for the betatron oscillations. (orig.)

  4. Aspects of passive magnetic levitation based on high-T(sub c) superconducting YBCO thin films (United States)

    Schoenhuber, P.; Moon, F. C.


    Passive magnetic levitation systems reported in the past were mostly confined to bulk superconducting materials. Here we present fundamental studies on magnetic levitation employing cylindrical permanent magnets floating above high-T(sub c) superconducting YBCO thin films (thickness about 0.3 mu m). Experiments included free floating rotating magnets as well as well-established flexible beam methods. By means of the latter, we investigated levitation and drag force hysteresis as well as magnetic stiffness properties of the superconductor-magnet arrangement. In the case of vertical motion of the magnet, characteristic high symmetry of repulsive (approaching) and attractive (withdrawing) branches of the pronounced force-displacement hysteresis could be detected. Achievable force levels were low as expected but sufficient for levitation of permanent magnets. With regard to magnetic stiffness, thin films proved to show stiffness-force ratios about one order of magnitude higher than bulk materials. Phenomenological models support the measurements. Regarding the magnetic hysteresis of the superconductor, the Irie-Yamafuji model was used for solving the equation of force balance in cylindrical coordinates allowing for a macroscopic description of the superconductor magnetization. This procedure provided good agreement with experimental levitation force and stiffness data during vertical motion. For the case of (lateral) drag force basic qualitative characteristics could be recovered, too. It is shown that models, based on simple asymmetric magnetization of the superconductor, describe well asymptotic transition of drag forces after the change of the magnet motion direction. Virgin curves (starting from equilibrium, i.e. symmetric magnetization) are approximated by a linear approach already reported in literature only. This paper shows that basic properties of superconducting thin films allow for their application to magnetic levitation or - without need of levitation

  5. How high are the personnel costs for OSCE? A financial report on management aspects. (United States)

    Rau, Thea; Fegert, Jörg; Liebhardt, Hubert


    The OSCE (objective structured clinical examination) was put to the test in order to assess the clinical practical skills of students in medical studies in the medical faculties. For the implementation of an OSCE, a large number of personnel is necessary. In particular for subjects with limited resources, therefore, efficient cost planning is required. In the winter semester 09/10, the Department of Neurology at the Medical Faculty of the University of Ulm introduced the OSCE as a pilot project. A financial report retrospectively shows the personnel expenses. The report is intended as an example for an insight into the resources needed for the OSCE with simulated patients. Included in the calculation of the financial costs of the OSCE were: employment, status of staff involved in the OSCE, subject-matter and temporal dimension of the task. After the exam, acceptance of the examination format was reviewed by a focus group interview with the teachers and students. The total expenses for the personnel involved in the OSCE amounted to 12,468 €. The costing of the clinic's share was calculated at 9,576 €. Tuition fees from the students have been used to the amount of 2.892 €. For conversion of total expenditure to the number of examines the sum of 86 € per student was calculated. Both students and teachers confirmed the validity of the OSCE and recognised the added value in the learning effects. The high acceptance of the OSCE in neurology by both students and teachers favours maintaining the test format. Against the background of the high financial and logistical costs, however, in individual cases it should be assessed how in the long-term efficient examination procedure will be possible.

  6. Some aspects of using Be as high heat flux protective armour material

    International Nuclear Information System (INIS)

    Gervash, A.; Mazul, I.; Yablokov, N.; Linke, J.


    The beryllium as plasma facing armour material must protect the actively cooled copper alloy heat sink of the First Wall and Divertor components from sputtering erosion, disruption and VDE transients and withstand the number of cycles under expected heat and neutron fluxes. The presented paper discusses some topical questions and presents recent results obtained in Russia in the frame of such consideration. In real operation beryllium as plasma facing component will be subjected to sequence of normal (cyclic heat fluxes) and off-normal (disruption, VDE) heat loads. Aiming to investigate the results of mentioned events the experiments with the number of Russian Be grades (DShG-200, TGP-56, TShG-56, TR-30, Condensed Be) as well as S-65C (ITER reference grade) at simulated disruption loads (∝5 MJ/m 2 ) and subsequent thermal cycling (∝5 MW/m 2 , 1000 cycles) were carried out. Experiments have revealed no macroscopic damage of the tested grades, although significant differences in crack formation and propagation were observed. The main statistics of performed experiments is presented and discussed. One of the main requirements to use Be as a candidate for plasma facing component is providing a reliable joint between Be and Cu-alloy heat sink structure. The unique Russian fast brazing process of joining beryllium to Cu-alloy that allows to survive high heat fluxes ≥10 MW/m 2 during thousand heating/cooling cycles without serious damaging in the armour material and its joint was described in previous works. The main goal of experiments presented in this paper was to study the high heat flux durability limit for joints as function of the pulse duration (i.e. investigation of creep/fatigue interaction). Authors present a description of the testing procedure and discuss the first results of mentioned experiments. (orig.)

  7. Potential safety features and safety analysis aspects for high performance light water reactor (HPLWR)

    International Nuclear Information System (INIS)

    Aksan, N.; Schulenberg, T.; Squarer, D.


    Research Activities are ongoing worldwide to develop advanced nuclear power plants with high thermal efficiency for the purpose to improve their economical competitiveness. Within the 5th Framework Programme of the European Commission, a project has been launched with the main objective to assess the technical and economical feasibility of a high efficiency LWR operating at super critical pressure conditions. Several European research institutions, industrial partners and the University of Tokyo participated and worked in this common research project. Within the aims of the development of the HPLWR is to use both passive and active safety systems for performing safety related functions in the event of transients or accidents. Consequently substantial effort has been invested in order to define the safety features of the plant in a European environment, as well as to incorporate passive safety features into the design. Throughout this process, the European Utility Requirements (EUR) and requirements known from Generation IV initiative were considered as a guideline in general terms in order to include further advanced ideas. The HPLWR general features were compared to both requirements, indicating a potential to meet these. Since, the supercritical HPLWR represents a challenge for best-estimate safety codes like RELAP5, CATHARE and TRAB due to the fact that these codes were developed for two-phase or single-phase coolant at pressures far below critical point, work on the preliminary assessment of the appropriateness of these codes have been performed for selected relevant phenomena, and application of the codes to the selected transients on the basis of defined 'reference design'. An overview on their successful upgrade to supercritical pressures and application to some plant safety analysis are provided in the paper. Further elaborations in relation to future needs are also discussed. (author)

  8. High Speed Surface Thermocouples Interface to Wireless Transmitters (United States)


    0.0055 - Oxy Acetylene Platinum Surface TC - Diesel Piston Platinum Surface TC - Oxy Acetylene Platinum Surface TC Pt Photo Pickup --Cr Photo ...Astrophysicists and astronomers On asteroids, meteors, moons , planets, or in the coronas of stars Plans to Transition this SBIR Technology to the Customer...analysis, and research and development work. Images Depicting the Developed Technology See Figure 2 for a photo containing both a MesoScribe sample

  9. High-aspect-ratio HfC nanobelts accompanied by HfC nanowires: Synthesis, characterization and field emission properties

    Energy Technology Data Exchange (ETDEWEB)

    Tian, Song, E-mail: [State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072 (China); School of Materials Science and Engineering, Chongqing Jiaotong University, Chongqing 400074 (China); Zhang, Yulei; Ren, Jincui; Qiang, Xinfa; Zhang, Shouyang [State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072 (China); Li, Hejun, E-mail: [State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072 (China)


    Highlights: • HfC naobelts accompanied by HfC nanowires were synthesized by a catalytic CVD method. • HfC nanobelts as a novel structure of HfC ceramic are reported for the first time. • HfC nanobelts have 100–200 μm in lengths and reach up to 10 μm in widths. • The synthesized product is promising field nanoemitters. - Abstract: As a key refractory carbide, hafnium carbide (HfC) is commonly used as structural materials while the field emission (FE) application of HfC in the field of vacuum microelectronics is almost the only one for functional material purposes. Based on its outstanding physical and chemical characteristics, HfC is identified as a potential candidate with satisfactory mechanical properties and long-term and/or high-temperature FE stability for future applications in high-performance field emitters. However, the development of HfC in various FE applications is hindered because it is not facile to fabricate large-scale low-dimensional HfC field nanoemitters. Herein, High-aspect-ratio HfC nanobelts accompanied by HfC nanowires were synthesized on a large scale by a traditional and simple catalytic chemical vapor deposition (CVD) method. Classical vapor–liquid–solid (VLS) theory was employed to explain the growth of the HfC nanowires and nanobelts along axial direction. The thin HfO{sub 2} shell and thin C layer surrounding the nanostructures might give rise to the diameter fluctuation of HfC nanowires and the width increase of HfC nanobelts in lateral direction. Field emission results show that the high-aspect-ratio HfC nanobelts accompanied by the nanowires are promising field nanoemitters, which exhibit excellent field emission properties with a fairly low turn-on field of ∼1.5 V μm{sup −1} and a low current fluctuation less than ∼10%. This suggests that HfC ceramics with high-aspect-ratio nanostructures are ideal cathode material for various field emission applications.

  10. Improve oxidation resistance at high temperature by nanocrystalline surface layer


    Xia, Z. X.; Zhang, C.; Huang, X. F.; Liu, W. B.; Yang, Z. G.


    An interesting change of scale sequence occurred during oxidation of nanocrystalline surface layer by means of a surface mechanical attrition treatment. The three-layer oxide structure from the surface towards the matrix is Fe3O4, spinel FeCr2O4 and corundum (Fe,Cr)2O3, which is different from the typical two-layer scale consisted of an Fe3O4 outer layer and an FeCr2O4 inner layer in conventional P91 steel. The diffusivity of Cr, Fe and O is enhanced concurrently in the nanocrystalline surfac...

  11. Surface Characterization for High Purity Fe-Cr Alloys


    Iwai, H.; Oiwa, R.; Takaki, S.; Abiko, K.


    Fe-50mass%Cr was prepared in a cold crucible furnace with induction heating, then refined by floating-zone melting (FZM). The chemistries on the surface before and after FZM were compared by XPS measurement. C and O were observed on top surfaces both before and after as a hydrocarbon, carbonyl group and carboxyl group which are adsorbed chemical components. The other impurities were observed on the surface in both cases ; however, the number and level of impurities on the surface after FZM we...

  12. Computational local stiffness analysis of biological cell: High aspect ratio single wall carbon nanotube tip

    Energy Technology Data Exchange (ETDEWEB)

    TermehYousefi, Amin, E-mail: [Department of Human Intelligence Systems, Graduate School of Life Science and Systems Engineering, Kyushu Institute of Technology (Kyutech) (Japan); Bagheri, Samira; Shahnazar, Sheida [Nanotechnology & Catalysis Research Centre (NANOCAT), IPS Building, University Malaya, 50603 Kuala Lumpur (Malaysia); Rahman, Md. Habibur [Department of Computer Science and Engineering, University of Asia Pacific, Green Road, Dhaka-1215 (Bangladesh); Kadri, Nahrizul Adib [Department of Biomedical Engineering, Faculty of Engineering, University Malaya, 50603 Kuala Lumpur (Malaysia)


    Carbon nanotubes (CNTs) are potentially ideal tips for atomic force microscopy (AFM) due to the robust mechanical properties, nanoscale diameter and also their ability to be functionalized by chemical and biological components at the tip ends. This contribution develops the idea of using CNTs as an AFM tip in computational analysis of the biological cells. The proposed software was ABAQUS 6.13 CAE/CEL provided by Dassault Systems, which is a powerful finite element (FE) tool to perform the numerical analysis and visualize the interactions between proposed tip and membrane of the cell. Finite element analysis employed for each section and displacement of the nodes located in the contact area was monitored by using an output database (ODB). Mooney–Rivlin hyperelastic model of the cell allows the simulation to obtain a new method for estimating the stiffness and spring constant of the cell. Stress and strain curve indicates the yield stress point which defines as a vertical stress and plan stress. Spring constant of the cell and the local stiffness was measured as well as the applied force of CNT-AFM tip on the contact area of the cell. This reliable integration of CNT-AFM tip process provides a new class of high performance nanoprobes for single biological cell analysis. - Graphical abstract: This contribution develops the idea of using CNTs as an AFM tip in computational analysis of the biological cells. The proposed software was ABAQUS 6.13 CAE/CEL provided by Dassault Systems. Finite element analysis employed for each section and displacement of the nodes located in the contact area was monitored by using an output database (ODB). Mooney–Rivlin hyperelastic model of the cell allows the simulation to obtain a new method for estimating the stiffness and spring constant of the cell. Stress and strain curve indicates the yield stress point which defines as a vertical stress and plan stress. Spring constant of the cell and the local stiffness was measured as well

  13. High quality broadband spatial reflections of slow Rayleigh surface acoustic waves modulated by a graded grooved surface

    KAUST Repository

    Xu, Yanlong


    We report high quality broadband spatial reflections of Rayleigh surface acoustic waves (SAWs) through a graded grooved surface. High quality means that no wave is allowed to transmit and the incident wave is nearly all reflected to the input side. The graded grooved surface is structured by drilling one dimensional array of graded grooves with increased depths on a flat surface. We investigate SAW dispersion relations, wave field distribution at several typical SAW wavelengths, and time evolution of a Gaussian pulse through the graded grooved surface. Results show that the input broadband Rayleigh SAWs can be slowed, spatially enhanced and stopped, and finally reflected to the input side. The study suggests that engraving the flat surface can be used as an efficient and economical way to manipulate Rayleigh SAWs, which has potential application in novel SAW devices such as filters, reflectors, sensors, energy harvesters, and diodes.


    International Nuclear Information System (INIS)

    Duignan, M; Charles Nash, C; Timothy Punch, T


    A principal role of the DOE Savannah River Site is to safely dispose of a large volume of liquid nuclear waste held in many storage tanks. An in-tank ion exchange unit is being considered for cesium removal to accelerate waste processing. This unit is planned to have a relatively high bed height to diameter ratio (10:1). Complicating the design is the need to cool the ion exchange media; therefore, the ion exchange column will have a central cooling core making the flow path annular. To separate cesium from waste the media being considered is made of resorcinol formaldehyde resin deposited on spherical plastic beads and is a substitute for a previously tested resin made of crystalline silicotitanate. This spherical media not only has an advantage of being mechanically robust, but, unlike its predecessor, it is also reusable, that is, loaded cesium can be removed through elution and regeneration. Resin regeneration leads to more efficient operation and less spent resin waste, but its hydraulic performance in the planned ion exchange column was unknown. Moreover, the recycling process of this spherical resorcinol formaldehyde causes its volume to significantly shrink and swell. To determine the spherical media's hydraulic demand a linearly scaled column was designed and tested. The waste simulant used was prototypic of the wastes' viscosity and density. This paper discusses the hydraulic performance of the media that will be used to assist in the design of a full-scale unit

  15. Container material for the disposal of highly radioactive wastes: corrosion chemistry aspects

    International Nuclear Information System (INIS)

    Grauer, R.


    Prior to disposal in crystalline formations it is planned to enclose vitrified highly radioactive waste from nuclear power plants in metallic containers ensuring their isolation from the groundwater for at least 1,000 years. Appropriate metals can be either thermodynamically stable in the repository environment (such as copper), passive materials with very low corrosion rates (titanium, nickel alloys), or metals such as cast iron or unalloyed cast steels which, although they corrode, can be used in sections thick enough to allow for this corrosion. The first part of the report presents the essentials of corrosion science in order to enable even a non-specialist to follow the considerations and arguments necessary to choose the material and design the container against corrosion. Following this, the principles of the long-term extrapolation of corrosion behaviour are discussed. The second part summarizes and comments upon the literature search carried out to identify published results relevant to corrosion in a repository environment. Results of archeaological studies are included wherever possible. Not only the general corrosion behaviour but also localized corrosion and stress corrosion cracking are considered, and the influence of hydrogen on the material behaviour is discussed. Taking the corrosion behaviour as criterion, the author suggests the use either of copper or of cast iron or steel as an appropriate container material. The report concludes with proposals for further studies. (Auth.)

  16. Fabrication and electrical characterization of high aspect ratio poly-silicon filled through-silicon vias

    International Nuclear Information System (INIS)

    Dixit, Pradeep; Vehmas, Tapani; Vähänen, Sami; Monnoyer, Philippe; Henttinen, Kimmo


    This paper presents the fabrication and the electrical characterization of poly-Si filled through-silicon vias, which were etched in a 180 µm thin silicon device wafer, bonded to a handle wafer by plasma activated oxide-to-silicon bonding. Heavily doped poly-Si was used as interconnection material, which was deposited by low-pressure chemical vapor deposition. Two different via geometries, i.e. stadium shaped, and circular shaped, were tried. Sputtered aluminum metallization layers as double-side redistribution lines and contact pads, were used. Both Kelvin structures and daisy chains were fabricated and their electrical resistances were measured. The electrical resistance of a single stadium-shaped via was measured to be about 24 Ω. The electrical resistance was varying from 60 Ω to 90 Ω for two-vias daisy chains. Measured results indicate that this via-first technology can be used for varying range of sensor applications like microphone, oscillator, resonator, etc where CMOS compatibility and high temperature processing are the prime requirements. (paper)

  17. Aspects of the use of saturated fluorocarbon fluids in high energy physics

    Energy Technology Data Exchange (ETDEWEB)

    Hallewell, G., E-mail: Gregory.Hallewell@cern.c [Centre de Physique des Particules de Marseille, 163 Avenue de Luminy, Case 907, 13288 Marseille Cedex 09 (France)


    The excellent dielectric properties of saturated fluorocarbons have allowed their use in direct immersion liquid cooling of electronics, including supercomputers and as heat transfer media in vapour phase soldering and burn-in testing of electronics. Their high density, UV transparency, non-flammability, non-toxicity and radiation tolerance have led to their use as liquid and gas radiator media for RICH detectors in numerous particle physics experiments. Systems to circulate and purify saturated fluorocarbon Cherenkov radiator vapours often rely on thermodynamic evaporation-condensation cycles similar to those used in refrigeration. Their use as evaporative refrigerants was pioneered for the ATLAS silicon tracker, and they are now also used as evaporative coolants in ALICE and TOTEM and as liquid coolants in ATLAS and CMS. Ultrasonic techniques for vapour phase analysis of fluorocarbon mixtures-developed for the SLAC SLD barrel CRID radiator during the 1980s as an alternative to UV refractometry are again under development for the ATLAS tracker evaporative cooling system. Examples of fluorocarbon circulation systems, together with purification and analysis techniques for these versatile fluids are mentioned.

  18. Some Aspects of Crystal Centering During X-ray High-throughput Protein Crystallography Experiment (United States)

    Gaponov, Yu. A.; Matsugaki, N.; Sasajima, K.; Igarashi, N.; Wakatsuki, S.

    A set of algorithms and procedures of a crystal loop centering during X-ray high-throughput protein crystallography experiment has been designed and developed. A simple algorithm of the crystal loop detection and preliminary recognition has been designed and developed. The crystal loop detection algorithm is based on finding out the crystal loop ending point (opposite to the crystal loop pin) using image cross section (digital image column) profile analysis. The crystal loop preliminary recognition procedure is based on finding out the crystal loop sizes and position using image cross section profile analysis. The crystal loop fine recognition procedure based on Hooke-Jeeves pattern search method with an ellipse as a fitting pattern has been designed and developed. The procedure of restoring missing coordinate of the crystal loop is described. Based on developed algorithms and procedures the optimal auto-centering procedure has been designed and developed. A procedure of optimal manual crystal centering (Two Clicks Procedure) has been designed and developed. Developed procedures have been integrated into control software system PCCS installed at crystallography beamlines Photon Factory BL5A and PF-AR NW12, KEK.

  19. Reliable high-power diode lasers: thermo-mechanical fatigue aspects (United States)

    Klumel, Genady; Gridish, Yaakov; Szafranek, Igor; Karni, Yoram


    High power water-cooled diode lasers are finding increasing demand in biomedical, cosmetic and industrial applications, where repetitive cw (continuous wave) and pulsed cw operation modes are required. When operating in such modes, the lasers experience numerous complete thermal cycles between "cold" heat sink temperature and the "hot" temperature typical of thermally equilibrated cw operation. It is clearly demonstrated that the main failure mechanism directly linked to repetitive cw operation is thermo-mechanical fatigue of the solder joints adjacent to the laser bars, especially when "soft" solders are used. Analyses of the bonding interfaces were carried out using scanning electron microscopy. It was observed that intermetallic compounds, formed already during the bonding process, lead to the solders fatigue both on the p- and n-side of the laser bar. Fatigue failure of solder joints in repetitive cw operation reduces useful lifetime of the stacks to hundreds hours, in comparison with more than 10,000 hours lifetime typically demonstrated in commonly adopted non-stop cw reliability testing programs. It is shown, that proper selection of package materials and solders, careful design of fatigue sensitive parts and burn-in screening in the hard pulse operation mode allow considerable increase of lifetime and reliability, without compromising the device efficiency, optical power density and compactness.

  20. Aspects of operation of the Fermilab Booster RF System at very high intensity

    International Nuclear Information System (INIS)

    Griffin, J.E.


    The purpose of this note is to examine the likelihood and problems associated with operation of the Fermilab Booster rf systems as it presently exists, or with only minor modifications, at beam intensity approaching 5x10 13 protons per pulse. Beam loading of the rf system at such an intensity will be one order of magnitude larger than at the present operation level. It is assumed that the injection energy will be raised to 1 GeV with no major increase in the injected energy spread (longitudinal emittance). The beam will be bunched by adiabatic capture as is presently done although it may be necessary to remove one or two bunches prior to acceleration to allow clean extraction at 8 GeV. At very high intensity the charge in each bunch will interact with the vacuum chamber impedance (and with itself) in such a way as to reduce in some cases the bucket area generated by the rf voltage. Because this decrement must be made up by changes in the rf ring voltage if the required bucket area is to be maintained, these effects must be taken into consideration in any analysis of the capability of the rf system to accelerate very large intensity

  1. A topological screening heuristic for low-energy, high-index surfaces (United States)

    Sun, Wenhao; Ceder, Gerbrand


    Robust ab initio investigations of nanoparticle surface properties require a method to identify candidate low-energy surface facets a priori. By assuming that low-energy surfaces are planes with high atomic density, we devise an efficient algorithm to screen for low-energy surface orientations, even if they have high (hkl) miller indices. We successfully predict the observed low-energy, high-index { 10 12 bar } and { 10 1 bar 4 } surfaces of hematite α-Fe2O3, the {311} surfaces of cuprite Cu2O, and the {112} surfaces of anatase TiO2. We further tabulate candidate low-energy surface orientations for nine of the most common binary oxide structures. Screened surfaces are found to be generally applicable across isostructural compounds with varying chemistries, although relative surface energies between facets may vary based on the preferred coordination of the surface atoms.

  2. Surface finish effects on the high-cycle fatigue of Alloy 718

    International Nuclear Information System (INIS)

    Korth, G.E.


    Load control high-cycle fatigue tests at 427 and 649 0 C were conducted on Alloy 718 specimens given various surface finishes. The standard surface preparation for fatigue specimens involves a low-stress grind to minimize the residual surface stresses. A low-stress grind surface was used for generating baseline data; various other surfaces that could be considered feasible for large components fabricated in commercial shops were produced on test specimens, and the high-cycle fatigue strength of each was compared. Surface finishes produced by belt sanding, grit blasting, fine machining, and electropolishing were examined. Surface roughness measurements were taken on typical specimens with each surface finish, and residual stress profiles were measured on three of the surface types. Results show little or no difference in fatigue life for the various surfaces and indicate that residual stress profile and grain size are more important factors than surface roughness in determining high-cycle fatigue strength. 12 figures, 5 tables

  3. Aspects of nuclear process heat application of very high temperature reactors (VHTR)

    International Nuclear Information System (INIS)

    Jansing, W.T.; Kugeler, K.


    The different processes of high temperature process application require new concepts for heat exchangers to carry out key process like steam reforming of light hydrocarbons, gasification of coal or biomass, or thermo-chemical cycles for hydrogen production. These components have been tested in the German projects for high temperature development. The intention was always to test at original conditions of temperatures, pressures and gas atmospheres. Furthermore the time of testing should be long as possible, to be able to carry out extrapolations to the real lifetime of components. Partly test times of around 20 000 hours have been reached. Key components, which are discussed in this paper, are: Intermediate heat exchangers to separate the primary reactor side and the secondary process side. Here two components with a power of 10 MW have been tested with the result, that all requirements of a nuclear component with larger power (125 MW) can be fulfilled. The max. primary helium temperature was 950°C, the maximal secondary temperature was 900°C. These were components with helical wounded tubes and U-tubes. In the test facility KVK, which had been built to carry out many special tests on components for helium cycles, furthermore hot gas ducts (with large dimensions), hot gas valves (with large dimensions), steam generators (10 MW), helium circulators, the helium gas purification and special measurements installations for helium cycle have been tested. All these tests delivered a broad know how for the urther development of technologies using helium as working fluid. The total test time of KVK was longer than 20 000 h. In a large test facility for steam reforming (EVAⅡ10 MW, T He =950°C, p He =40 bar, T Reform =800°C) all technical details of the conversion process have been investigated and today the technical feasibility of this process is valuated as given. Two reformer bundles, one with baffles and one with separate guiding tubes for each reformer tube have

  4. Radiological protection aspects of geological disposal of high-level radioactive waste

    International Nuclear Information System (INIS)

    Matsuzuru, Hideo; Kimura, Hideo


    A high-level radioactive waste, generated at a nuclear fuel reprocessing plant, will be disposed of deep, i.e., several hundred meters, within geological formations, to isolate it from the human environment. Since the waste contains significant amounts of long-lived radionuclides, such as Tc-99, I-129, Cs-135 and transuranic elements, the safety of its disposal, particularly as regards the requirement for the radiological protection of human and his environment even in the far future, is one of the essential subjects of all countries engaged in nuclear power production. The radiological protection system has long been established and applied to regulate radiation exposures to the public associated with a relatively short-term release of radioactive materials, during normal and accidental conditions, from nuclear installations such as a power plant and reprocessing plant. Radioactive waste disposal, which potentially offers a long-term radiological consequence on the public, inevitably produces a specific requirement, from the standpoint of radiological protection, that individuals and populations in the future should be accorded at least a current level of the protection. This requirement has caused a serious debate, among the community of radiological protection, on how to establish radiological protection standards and criteria, and how to establish safety assessment methodologies to demonstrate compliance with them. We have discussed in this paper on specific items such as numerical guides to indicate radiological consequences, time frames over which calculations of the consequences are to be carried out, uncertainties to be involved in the calculations, and safety assessment methodologies. (author)

  5. Safety and radiation protection aspects of the management of radioactive wastes of high level activity

    International Nuclear Information System (INIS)

    Candes, P.; Pradel, J.


    Appropriate consideration is given in France to safety and protection problems to be solved from the production up to the final disposal of radioactive wastes of high level activity. The first stage of the work consisted in emphasizing the various technical options. Different strategies appear to be possible, taking into account technical, political, and psychological difficulties. This results in evaluating the safety problems to be solved in the framework of those strategies. In this field, the main safety and protection principles do not differ from those which apply to other nuclear facilities. Nevertheless, duration is in most cases a quite different factor (thousands or millions of years). The question is then raised of evaluating the importance to be given to very remote consequences, both at philosophical and scientific levels. As a first result of those considerations, the application of the ''barrier'' concept is recommended. This concept is familiar to safety specialists. Different barriers for which particular problems are listed and evaluated, are defined. Another results with regard to radiation protection principles is to consider that if safety provisions should lead to a containment of radioactive products as efficient as possible, it would not be realistic to consider such a containment as absolute, in particular for disposal durations arising to thousands of years. It is therefore assumed that a limited radioactivity transfer should be taken into account, and its consequences for environment and man be calculated. This is especially true in the study of an appropriate site for final storage, and the study should necessarily include a detailed investigation of the retention characteristics of soil layers, and the implementation of appropriate models giving a sufficiently accurate evaluation of the consequences of transfers, including those related to the effect of various elements after their arrival into the biosphere. The authors review the

  6. Safety and protection aspects of the management of high-level radioactive wastes

    International Nuclear Information System (INIS)

    Candes, P.; Pradel, J.


    Appropriate consideration is given in France to safety and protection problems to be solved from production up to the final disposal of high-level radioactive wastes. The first stage of this work consisted in emphasizing the various technical options. Different strategies appear to be possible, taking into account the technical, political and psychological difficulties. This results in evaluating the safety problems to be solved in the framework of those strategies. In this field the main safety and protection principles do not differ from those applying to other nuclear facilities. Nevertheless, the factor of time is in most cases quite different (thousands or millions of years). The question is then raised of evaluating the importance to be given to very remote consequences, both at philosophical and at scientific levels. As a first result of these considerations, the application of the barrier concept is recommended. This concept is familiar to safety specialists. Different barriers, for which particular problems are listed and evaluated, are defined. Another result with regard to radiation protection principles is to consider that if safety provisions should lead to as efficient a containment of radioactive products as possible, it would not be realistic to consider such a containment as absolute, in particular for disposal lasting anything up to thousands of years. It is therefore assumed that a limited radioactivity transfer should be taken into account, and its consequences for the environment and man calculated. This is especially true in the study of an appropriate site for final storage, and the study should necessarily include a detailed investigation of the retention characteristics of soil layers, and the implementation of appropriate models giving a sufficiently accurate evaluation of the consequences of transfers, including those related to the effect of various elements after their arrival into the biosphere. The authors review the different

  7. High-Yield Synthesis of Uniform Ag Nanowires with High Aspect Ratios by Introducing the Long-Chain PVP in an Improved Polyol Process

    Directory of Open Access Journals (Sweden)

    Jie-Jun Zhu


    Full Text Available Polyvinyl pyrrolidone (PVP with different molecular weights was used as capping agent to synthesize silver nanowires through a polyol process. The results indicated that the yields and aspect ratios of silver nanowires were controlled by the chain length of PVP and increased with increasing the molecular weight (MW of PVP. When the long-chain PVP-K90 (MW = 800,000 was used, the product was uniform in size and was dominated by nanowires with high aspect ratios. The growth mechanism of the nanowires was studied. It is proposed that the chemical adsorption of Ag+ on the PVP chains at the initial stage promotes the growth of Ag nanowires.

  8. Financial aspects of a seismic base isolation system for a steel high-rack structure

    Directory of Open Access Journals (Sweden)

    Kilar, V.


    Full Text Available The paper deals with the effects and costs of implementing a base isolation system for the mitigation of the seismic risk of an existing steel rack structure. Different realistic distributions of the payload mass and occupancy levels, which form different plan asymmetric variants, have been analysed. The results obtained by the pushover analysis (N2 method are presented as top floor envelopes and as plastic hinge damage patterns. In the presented cost study, the cost of the implementation of the proposed base isolation system is compared with the estimated costs of structural repairs to the damaged structural members of the superstructure, as well as with estimated expenses of the downtime period. The results have shown that base isolation is, in general, not economically feasible for lower ground motion intensities, whereas it could be of great benefit in the case of moderate and high intensities, especially if the downtime period is taken into account.El presente artículo trata sobre los efectos y costes de implementación de un sistema de aislamiento en cimentación para la mitigación del riesgo sísmico de la estructura de un bastidor de acero en altura prexistente. Se han analizado diferentes distribuciones realistas de la masa contribuyente y de los niveles de ocupación, conformando diferentes variantes asimétricas en planta. Se presentan los resultados obtenidos mediante el método N2 (análisis estático incremental no lineal como envolventes de las plantas superiores y como patrones de deterioro en estado plástico. En el estudio de costos presentado, el coste de implementación del sistema de aislamiento propuesto se compara con los costes estimados de reparación de los elementos superestructurales y los costes derivados del período de desocupación. Los resultados muestran que, en general, el aislamiento en la base no resulta viable económicamente para movimientos de baja intensidad, pero puede ser muy beneficioso en el caso de

  9. Synergetic aspects of gas-discharge: lateral patterns in dc systems with a high ohmic barrier (United States)

    Purwins, H.-G.; Stollenwerk, L.


    The understanding of self-organized patterns in spatially extended nonlinear dissipative systems is one of the most challenging subjects in modern natural sciences. Such patterns are also referred to as dissipative structures. We review this phenomenon in planar low temperature dc gas-discharge devices with a high ohmic barrier. It is demonstrated that for these systems a deep qualitative understanding of dissipative structures can be obtained from the point of view of synergetics. At the same time, a major contribution can be made to the general understanding of dissipative structures. The discharge spaces of the experimentally investigated systems, to good approximation, have translational and rotational symmetry by contraction. Nevertheless, a given system may exhibit stable current density distributions and related patterns that break these symmetries. Among the experimentally observed fundamental patterns one finds homogeneous isotropic states, fronts, periodic patterns, labyrinth structures, rotating spirals, target patterns and localized filaments. In addition, structures are observed that have the former as elementary building blocks. Finally, defect structures as well as irregular patterns are common phenomena. Such structures have been detected in numerous other driven nonlinear dissipative systems, as there are ac gas-discharge devices, semiconductors, chemical solutions, electrical networks and biological systems. Therefore, from the experimental observations it is concluded that the patterns in planar low temperature dc gas-discharge devices exhibit universal behavior. From the theoretical point of view, dissipative structures of the aforementioned kind are also referred to as attractors. The possible sets of attractors are an important characteristic of the system. The number and/or qualitative nature of attractors may change when changing parameters. The related bifurcation behavior is a central issue of the synergetic approach chosen in the present

  10. Synergetic aspects of gas-discharge: lateral patterns in dc systems with a high ohmic barrier

    International Nuclear Information System (INIS)

    Purwins, H-G; Stollenwerk, L


    The understanding of self-organized patterns in spatially extended nonlinear dissipative systems is one of the most challenging subjects in modern natural sciences. Such patterns are also referred to as dissipative structures. We review this phenomenon in planar low temperature dc gas-discharge devices with a high ohmic barrier. It is demonstrated that for these systems a deep qualitative understanding of dissipative structures can be obtained from the point of view of synergetics. At the same time, a major contribution can be made to the general understanding of dissipative structures. The discharge spaces of the experimentally investigated systems, to good approximation, have translational and rotational symmetry by contraction. Nevertheless, a given system may exhibit stable current density distributions and related patterns that break these symmetries. Among the experimentally observed fundamental patterns one finds homogeneous isotropic states, fronts, periodic patterns, labyrinth structures, rotating spirals, target patterns and localized filaments. In addition, structures are observed that have the former as elementary building blocks. Finally, defect structures as well as irregular patterns are common phenomena. Such structures have been detected in numerous other driven nonlinear dissipative systems, as there are ac gas-discharge devices, semiconductors, chemical solutions, electrical networks and biological systems. Therefore, from the experimental observations it is concluded that the patterns in planar low temperature dc gas-discharge devices exhibit universal behavior. From the theoretical point of view, dissipative structures of the aforementioned kind are also referred to as attractors. The possible sets of attractors are an important characteristic of the system. The number and/or qualitative nature of attractors may change when changing parameters. The related bifurcation behavior is a central issue of the synergetic approach chosen in the present

  11. High-resolution biosensor based on localized surface plasmons

    Czech Academy of Sciences Publication Activity Database

    Piliarik, Marek; Šípová, Hana; Kvasnička, Pavel; Galler, N.; Krenn, J. R.; Homola, Jiří


    Roč. 20, č. 1 (2012), s. 672-680 ISSN 1094-4087 R&D Projects: GA AV ČR KAN200670701; GA MŠk OC09058 Institutional research plan: CEZ:AV0Z20670512 Keywords : optical biosenzor * surface plasmon resonance * localized surface plasmon Subject RIV: JA - Electronics ; Optoelectronics, Electrical Engineering Impact factor: 3.546, year: 2012

  12. Facet-Mediated Growth of High-Quality Monolayer Graphene on Arbitrarily Rough Copper Surfaces. (United States)

    Lee, Hyo Chan; Jo, Sae Byeok; Lee, Eunho; Yoo, Min Seok; Kim, Hyun Ho; Lee, Seong Kyu; Lee, Wi Hyoung; Cho, Kilwon


    A synthetic approach for high-quality graphene on rough Cu surfaces via chemical vapor deposition is proposed. High-quality graphene is synthesized on rough Cu surfaces by inducing surface faceting of Cu surfaces prior to graphene growth. The electron mobility of synthesized graphene on the rough Cu surfaces is enhanced to 10 335 cm(2) V(-1) s(-1). © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  13. Hydrophobic and Metallophobic Surfaces: Highly Stable Non-wetting Inorganic Surfaces Based on Lanthanum Phosphate Nanorods. (United States)

    Sankar, Sasidharan; Nair, Balagopal N; Suzuki, Takehiro; Anilkumar, Gopinathan M; Padmanabhan, Moothetty; Hareesh, Unnikrishnan Nair S; Warrier, Krishna G


    Metal oxides, in general, are known to exhibit significant wettability towards water molecules because of the high feasibility of synergetic hydrogen-bonding interactions possible at the solid-water interface. Here we show that the nano sized phosphates of rare earth materials (Rare Earth Phosphates, REPs), LaPO4 in particular, exhibit without any chemical modification, unique combination of intrinsic properties including remarkable hydrophobicity that could be retained even after exposure to extreme temperatures and harsh hydrothermal conditions. Transparent nanocoatings of LaPO4 as well as mixture of other REPs on glass surfaces are shown to display notable hydrophobicity with water contact angle (WCA) value of 120° while sintered and polished monoliths manifested WCA greater than 105°. Significantly, these materials in the form of coatings and monoliths also exhibit complete non-wettability and inertness towards molten metals like Ag, Zn, and Al well above their melting points. These properties, coupled with their excellent chemical and thermal stability, ease of processing, machinability and their versatile photo-physical and emission properties, render LaPO4 and other REP ceramics utility in diverse applications.

  14. Boron Nitride Nanoporous Membranes with High Surface Charge by Atomic Layer Deposition. (United States)

    Weber, Matthieu; Koonkaew, Boonprakrong; Balme, Sebastien; Utke, Ivo; Picaud, Fabien; Iatsunskyi, Igor; Coy, Emerson; Miele, Philippe; Bechelany, Mikhael


    In this work, we report the design and the fine-tuning of boron nitride single nanopore and nanoporous membranes by atomic layer deposition (ALD). First, we developed an ALD process based on the use of BBr 3 and NH 3 as precursors in order to synthesize BN thin films. The deposited films were characterized in terms of thickness, composition, and microstructure. Next, we used the newly developed process to grow BN films on anodic aluminum oxide nanoporous templates, demonstrating the conformality benefit of BN prepared by ALD, and its scalability for the manufacturing of membranes. For the first time, the ALD process was then used to tune the diameter of fabricated single transmembrane nanopores by adjusting the BN thickness and to enable studies of the fundamental aspects of ionic transport on a single nanopore. At pH = 7, we estimated a surface charge density of 0.16 C·m -2 without slip and 0.07 C·m -2 considering a reasonable slip length of 3 nm. Molecular dynamics simulations performed with experimental conditions confirmed the conductivities and the sign of surface charges measured. The high ion transport results obtained and the ability to fine-tune nanoporous membranes by such a scalable method pave the way toward applications such as ionic separation, energy harvesting, and ultrafiltration devices.

  15. Rotor-dynamic design aspects for a variable frequency drive based high speed cryogenic centrifugal pump in fusion devices

    International Nuclear Information System (INIS)

    Das, Jotirmoy; Vaghela, Hitensinh; Bhattacharya, Ritendra; Patel, Pratik; Shukla, Vinit; Shah, Nitin; Sarkar, Biswanath


    Superconducting magnets of large size are inevitable for fusion devices due to high magnetic field requirements. Forced flow cooling of the superconducting magnets with high mass flowrate of the order ∼3 kg/s is required to keep superconducting magnets within its safe operational boundaries during various plasma scenarios. This important requirement can be efficiently fulfilled by employing high capacity and high efficiency cryogenic centrifugal pumps. The efficiency > 70% will ensure overall lower heat load to the cryoplant. Thermo-hydraulic design of cryogenic centrifugal pump revealed that to achieve the operational regime with high efficiency, the speed should be ∼ 10,000 revolutions per minute. In this regard, the rotor-dynamic design aspect is quite critical from the operational stability point of view. The rotor shaft design of the cryogenic pump is primarily an outcome of optimization between thermal heat-in leak at cryogenic temperature level from ambient, cryogenic fluid impedance and designed rotation speed of the impeller wheel. The paper describes the basic design related to critical speed of the rotor shaft, rotor whirl and system instability prediction to explore the ideal operational range of the pump from the system stability point of view. In the rotor-dynamic analysis, the paper also describes the Campbell plots to ensure that the pump is not disturbed by any of the critical speeds, especially while operating near the nominal and enhanced operating modes. (author)

  16. Multifunctional ultra-high vacuum apparatus for studies of the interactions of chemical warfare agents on complex surfaces. (United States)

    Wilmsmeyer, Amanda R; Gordon, Wesley O; Davis, Erin Durke; Mantooth, Brent A; Lalain, Teri A; Morris, John R


    A fundamental understanding of the surface chemistry of chemical warfare agents is needed to fully predict the interaction of these toxic molecules with militarily relevant materials, catalysts, and environmental surfaces. For example, rules for predicting the surface chemistry of agents can be applied to the creation of next generation decontaminants, reactive coatings, and protective materials for the warfighter. Here, we describe a multifunctional ultra-high vacuum instrument for conducting comprehensive studies of the adsorption, desorption, and surface chemistry of chemical warfare agents on model and militarily relevant surfaces. The system applies reflection-absorption infrared spectroscopy, x-ray photoelectron spectroscopy, and mass spectrometry to study adsorption and surface reactions of chemical warfare agents. Several novel components have been developed to address the unique safety and sample exposure challenges that accompany the research of these toxic, often very low vapor pressure, compounds. While results of vacuum-based surface science techniques may not necessarily translate directly to environmental processes, learning about the fundamental chemistry will begin to inform scientists about the critical aspects that impact real-world applications.

  17. Global High Resolution Sea Surface Flux Parameters From Multiple Satellites (United States)

    Zhang, H.; Reynolds, R. W.; Shi, L.; Bates, J. J.


    Advances in understanding the coupled air-sea system and modeling of the ocean and atmosphere demand increasingly higher resolution data, such as air-sea fluxes of up to 3 hourly and every 50 km. These observational requirements can only be met by utilizing multiple satellite observations. Generation of such high resolution products from multiple-satellite and in-situ observations on an operational basis has been started at the U.S. National Oceanic and Atmospheric Administration (NOAA) National Climatic Data Center. Here we describe a few products that are directly related to the computation of turbulent air-sea fluxes. Sea surface wind speed has been observed from in-situ instruments and multiple satellites, with long-term observations ranging from one satellite in the mid 1987 to six or more satellites since mid 2002. A blended product with a global 0.25° grid and four snapshots per day has been produced for July 1987 to present, using a near Gaussian 3-D (x, y, t) interpolation to minimize aliases. Wind direction has been observed from fewer satellites, thus for the blended high resolution vector winds and wind stresses, the directions are taken from the NCEP Re-analysis 2 (operationally run near real time) for climate consistency. The widely used Reynolds Optimum Interpolation SST analysis has been improved with higher resolutions (daily and 0.25°). The improvements use both infrared and microwave satellite data that are bias-corrected by in- situ observations for the period 1985 to present. The new versions provide very significant improvements in terms of resolving ocean features such as the meandering of the Gulf Stream, the Aghulas Current, the equatorial jets and other fronts. The Ta and Qa retrievals are based on measurements from the AMSU sounder onboard the NOAA satellites. Ta retrieval uses AMSU-A data, while Qa retrieval uses both AMSU-A and AMSU-B observations. The retrieval algorithms are developed using the neural network approach. Training

  18. Cooling high heat flux micro-electronic systems using refrigerants in high aspect ratio multi-microchannel evaporators

    International Nuclear Information System (INIS)

    Costa-Patry, E.


    Improving the energy efficiency of cooling systems can contribute to reduce the emission of greenhouse gases. Currently, most microelectronic applications are air-cooled. Switching to two-phase cooling systems would decrease power consumption and allow for the reuse of the extracted heat. For this type of application, multi-microchannel evaporators are thought to be well adapted. However, such devices have not been tested for a wide range of operating conditions, such that their thermal response to the high non-uniform power map typically generated by microelectronics has not been studied. This research project aims at clarifying these gray areas by investigating the behavior of the two-phase flow of different refrigerants in silicon and copper multi-microchannel evaporators under uniform, non-uniform and transient heat fluxes operating conditions. The test elements use as a heat source a pseudo-chip able to mimic the behavior of a CPU. It is formed by 35 independent sub-heaters, each having its own temperature sensor, such that 35 temperature and 35 heat flux measurements can be made simultaneously. Careful measurements of each pressure drop component (inlet, microchannels and outlet) found in the micro-evaporators showed the importance of the inlet and outlet restriction pressure losses. The overall pressure drop levels found in the copper test section were low enough to possibly be driven by a thermosyphon system. The heat transfer coefficients measured for uniform heat flux conditions were very high and typically followed a V-shape curve. The first branch was associated to the slug flow regime and the second to the annular flow regime. By tracking the minimum level of heat transfer, a transition criteria between the regimes was established, which included the effect of heat flux on the transition. Then for each branch, a different prediction method was used to form the first flow pattern-based prediction method for two-phase heat transfer in microchannels. A

  19. Robust Prediction of High Lift Using Surface Vorticity, Phase II (United States)

    National Aeronautics and Space Administration — FlightStream has been developed a fast, accurate, aerodynamic prediction code based on vorticity computations on the surface of an aircraft. The code, though still a...

  20. Design of bituminous surface mixes with high skid resistance. (United States)


    The Virginia Highway Research Council has proposed a study of the skid resistance of bituminous surfaces incorporating relatively hard and expensive aggregates. The hardness of the aggregates to be used aluminum oxide (Exolon) and calcined kaolin -- ...

  1. A simple microfluidic gradient generator with a soft-lithographically prototyped, high-aspect-ratio, ~2 µm wide microchannel. (United States)

    Ogawa, Tomohisa; Matsunaga, Nirai; Inomata, Saori; Tanaka, Masato; Futai, Nobuyuki


    We have developed a cast microfluidic chip that contains a thin (~2 µm wide) microchannel that is smoothly connected to thick microfluidics. The thin line features having high aspect ratio for a low-cost photolithography in which an emulsion photomask was used (1:1 ~ 1:3) were fabricated by exposing SU-8 photoresist to diffused 185 nm UV light emitted by a low-cost ozone lamp from the backside of the substrate to ensure sufficient crosslinking of small regions of the SU-8 photoresist. An H-shaped microfluidic configuration was used, in which the thin channel maintained constant diffusion fronts beyond purely static diffusion. We also demonstrated the long-term effects of a gradient of nerve growth factor on axon elongation by primary neurons cultured in the micro channel.

  2. Electrolytic Manganese Dioxide Coatings on High Aspect Ratio Micro-Pillar Arrays for 3D Thin Film Lithium Ion Batteries

    Directory of Open Access Journals (Sweden)

    Yafa Zargouni


    Full Text Available In this work, we present the electrochemical deposition of manganese dioxide (MnO2 thin films on carbon-coated TiN/Si micro-pillars. The carbon buffer layer, grown by plasma enhanced chemical vapor deposition (PECVD, is used as a protective coating for the underlying TiN current collector from oxidation, during the film deposition, while improving the electrical conductivity of the stack. A conformal electrolytic MnO2 (EMD coating is successfully achieved on high aspect ratio C/TiN/Si pillar arrays by tailoring the deposition process. Lithiation/Delithiation cycling tests have been performed. Reversible insertion and extraction of Li+ through EMD structure are observed. The fabricated stack is thus considered as a good candidate not only for 3D micorbatteries but also for other energy storage applications.

  3. pH-Dependent Toxicity of High Aspect Ratio ZnO Nanowires in Macrophages Due to Intracellular Dissolution

    KAUST Repository

    H. Müller, Karin


    High-aspect ratio ZnO nanowires have become one of the most promising products in the nanosciences within the past few years with a multitude of applications at the interface of optics and electronics. The interaction of zinc with cells and organisms is complex, with both deficiency and excess causing severe effects. The emerging significance of zinc for many cellular processes makes it imperative to investigate the biological safety of ZnO nanowires in order to guarantee their safe economic exploitation. In this study, ZnO nanowires were found to be toxic to human monocyte macrophages (HMMs) at similar concentrations as ZnCl2. Confocal microscopy on live cells confirmed a rise in intracellular Zn2+ concentrations prior to cell death. In vitro, ZnO nanowires dissolved very rapidly in a simulated body fluid of lysosomal pH, whereas they were comparatively stable at extracellular pH. Bright-field transmission electron microscopy (TEM) showed a rapid macrophage uptake of ZnO nanowire aggregates by phagocytosis. Nanowire dissolution occurred within membrane-bound compartments, triggered by the acidic pH of the lysosomes. ZnO nanowire dissolution was confirmed by scanning electron microscopy/energy-dispersive X-ray spectrometry. Deposition of electron-dense material throughout the ZnO nanowire structures observed by TEM could indicate adsorption of cellular components onto the wires or localized zinc-induced protein precipitation. Our study demonstrates that ZnO nanowire toxicity in HMMs is due to pH-triggered, intracellular release of ionic Zn2+ rather than the high-aspect nature of the wires. Cell death had features of necrosis as well as apoptosis, with mitochondria displaying severe structural changes. The implications of these findings for the application of ZnO nanowires are discussed. © 2010 American Chemical Society.

  4. Sequence stratigraphy and high-frequency cycles: New aspects for a quantitative evaluation of the Gulf of Suez basin, Egypt

    Energy Technology Data Exchange (ETDEWEB)

    Nio, S.D.; Yang, C.S. (International Geoservices, Leiderdorp (Netherlands)); Tewfik, N.; Darwish, M. (Earth Resource Exploration, Cairo (Egypt)); Jonkman, H. (International Geoservices, Leiderdorp (Netherlands))


    A new development in the application of sequence stratigraphic concepts in marine as well as continental basins is the recognition of high-frequency cyclic patterns in rock successions in the subsurface. Studies of six wells from the northern, central, and southern parts of the Gulf of Suez show the presence of well-preserved, high-frequency cycles with periodicities similar to the orbitally forced Malankovitch parameters. Subsurface rock successions, third-order sequences, and high-frequency cycles were compared with outcrops. After establishing the biostratigraphic framework for the above-mentioned wells, a sequence analysis was performed. Sequence boundaries and maximum flooding positions in each well were calibrated with the occurrences and evaluation of the high-frequency cycles. It became obvious that there is an intimate relationship between these high-frequency Milankovitch cycles and sequence organization. In addition, a close relationship can be observed in the subsurface as well as in outcrops between high-frequency climatic changes (connected to the Milankovitch cycles) and (litho)facies variability. Quantitative evaluations of each sequence and/or systems tract can be computed with the International Geoservices' cyclicity analysis tool (MILABAR). The results are summarized in a well composite chart, rate (NAR), and ratio of preserved time. In correlations between the wells, an accuracy of 500-100 Ka can be obtained. The quantitative evaluation of the sequence and high-frequency cycle analysis gave some new aspects concerning the (litho)facies and geodynamic development during the pre- as well as the synrift stages of the Gulf of Suez Basin.

  5. Effects of surface inactivation, high temperature drying and preservative treatment on surface roughness and colour of alder and beech wood (United States)

    Aydin, Ismail; Colakoglu, Gursel


    Although extensive research has been conducted in wood surface quality analysis, a unified approach to surface quality characterisation does not exist. Measurements of the variation in surface roughness and surface colour are used widely for the evaluation of wood surface quality. Colour is a basic visual feature for wood and wood-based products. Colour measurement is one of the quality control tests that should be carried out because the colour deviations are spotted easily by the consumers. On the other hand, a common problem faced by plywood manufacturers is panel delamination, for which a major cause is poor quality glue-bonds resulting from rough veneer. Rotary cut veneers with dimensions of 500 mm × 500 mm × 2 mm manufactured from alder ( Alnus glutinosa subsp. barbata) and beech ( Fagus orientalis Lipsky) logs were used as materials in this study. Veneer sheets were oven-dried in a veneer dryer at 110 °C (normal drying temperature) and 180 °C (high drying temperature) after peeling process. The surfaces of some veneers were then exposed at indoor laboratory conditions to obtain inactive wood surfaces for glue bonds, and some veneers were treated with borax, boric acid and ammonium acetate solutions. After these treatments, surface roughness and colour measurements were made on veneer surfaces. High temperature drying process caused a darkening on the surfaces of alder and beech veneers. Total colour change value (Δ E*) increased linear with increasing exposure time. Among the treatment solutions, ammonium acetate caused the biggest colour change while treatment with borax caused the lowest changes in Δ E* values. Considerable changes in surface roughness after preservative treatment did not occur on veneer surfaces. Generally, no clear changes were obtained or the values mean roughness profile ( Ra) decreased slightly in Ra values after the natural inactivation process.

  6. On the wettability diversity of C/SiC surface: Comparison of the ground C/SiC surface and ablated C/SiC surface from three aspects (United States)

    Wu, M. L.; Ren, C. Z.; Xu, H. Z.


    The coefficient of thermal conductivity was influenced by the wetting state of material. The wetting state usually depends on the surface wettability. C/SiC is a promising ceramic composites with multi-components. The wettability of C/SiC composites is hard to resort to the classical wetting theory directly. So far, few investigations focused on C/SiC surface wettability diversity after different material removal processes. In this investigation, comparative studies of surface wettability of ground C/SiC surface and laser-ablated C/SiC surface were carried out through apparent contact angle (APCA) measurements. The results showed that water droplets easily reached stable state on ground C/SiC surface; while the water droplets rappidly penetrated into the laser-ablated C/SiC surface. In order to find out the reason for wettability distinctions between the ground C/SiC surface and the laser-ablated C/SiC surface, comparative studies on the surface micro-structure, surface C-O-Si distribution, and surface C-O-Si weight percentage were carried out. The results showed that (1) A large number of micro cracks in the fuzzy pattern layer over laser-ablated C/SiC surfaces easily destoried the surface tension of water droplets, while only a few cracks existed over the ground C/SiC surfaces. (2) Chemical components (C, O, Si) were non-uniformly distributed on ground C/SiC surfaces, while the chemical components (C, O, Si) were uniformly distributed on laser-ablated C/SiC surfaces. (3) The carbon weight percentage on ground C/SiC surfaces were higher than that on laser-ablated C/SiC surfaces. All these made an essential contribution to the surface wettability diversity of C/SiC surface. Although more investigations about the quantitative influence of surface topography and surface chemical composition on composites wettability are still needed, the conslusion can be used in application: the wettability of C/SiC surface can be controlled by different material removal process

  7. Method for the preparation of high surface area high permeability carbons (United States)

    Lagasse, R.R.; Schroeder, J.L.


    A method for preparing carbon materials having high surface area and high macropore volume to provide high permeability. These carbon materials are prepared by dissolving a carbonizable polymer precursor, in a solvent. The solution is cooled to form a gel. The solvent is extracted from the gel by employing a non-solvent for the polymer. The non-solvent is removed by critical point drying in CO{sub 2} at an elevated pressure and temperature or evaporation in a vacuum oven. The dried product is heated in an inert atmosphere in a first heating step to a first temperature and maintained there for a time sufficient to substantially cross-link the polymer material. The cross-linked polymer material is then carbonized in an inert atmosphere. 3 figs.

  8. High-Resolution Seismic Imaging of Near-Surface Voids (United States)

    Gritto, R.; Korneev, V. A.; Elobaid, E. A.; Mohamed, F.; Sadooni, F.


    A major hazard in Qatar is the presence of karst, which is ubiquitous throughout the country including depressions, sinkholes, and caves. Causes for the development of karst include faulting and fracturing where fluids find pathways through limestone and dissolve the host rock to form caverns. Of particular concern in rapidly growing metropolitan areas that expand in heretofore unexplored regions are the collapse of such caverns. Because Qatar has seen a recent boom in construction, including the planning and development of complete new sub-sections of metropolitan areas, the development areas need to be investigated for the presence of karst to determine their suitability for the planned project. We present a suite of seismic techniques applied to a controlled experiment to detect, locate and estimate the size of a karst analog in form of a man-made water shaft on the campus of Qatar University, Doha, Qatar. Seismic waves are well suited for karst detection and characterization. Voids represent high-contrast seismic objects that exhibit strong responses due to incident seismic waves. However, the complex geometry of karst, including shape and size, makes their imaging nontrivial. While karst detection can be reduced to the simple problem of detecting an anomaly, karst characterization can be complicated by the 3D nature of the problem of unknown scale, where irregular surfaces can generate diffracted waves of different kind. In our presentation, we employ a variety of seismic techniques to demonstrate the detection and characterization of a vertical water collection shaft analyzing the phase, amplitude and spectral information of seismic waves that have been scattered by the object. We use the reduction in seismic wave amplitudes and the delay in phase arrival times in the geometrical shadow of the vertical shaft to independently detect and locate the object in space. Additionally, we use narrow band-pass filtered data combining two orthogonal transmission surveys

  9. Preparation of high surface area and high conductivity polyaniline nanoparticles using chemical oxidation polymerization technique (United States)

    Budi, S.; Yusmaniar; Juliana, A.; Cahyana, U.; Purwanto, A.; Imaduddin, A.; Handoko, E.


    In this work, polyaniline nanoparticles were synthesized using a chemical oxidation polymerization technique. The ammonium peroxydisulfate (APS)/aniline ratio, APS dropping time, and polymerization temperature were optimized to increase the surface area and conductivity of the polyaniline.The Fourier-transform infrared (FTIR) spectrum confirmed the formation of emeraldine salt polyaniline. X-ray diffraction (XRD) patterns indicated that amorphous and crystalline phases of the polyaniline were formed with crystallinity less than 40%. Scanning electron microscope (SEM) micrographs showed that the finest nanoparticles with uniform size distribution were obtained at the polymerization temperature of 0°C. A surface area analyzer (SAA) showed that the highest Brunauer-Emmett-Teller surface area (SBET ) of 42.14 m2/gwas obtained from an APS/aniline ratio of 0.75 with a dropping time of 0 s at a polymerization temperature of 0°C. A four-point probe measurement conducted at 75–300K indicated relatively high conductivity of the semiconductor characteristic of the polyaniline.

  10. Surface modifications of polypropylene by high energy carbon ions

    International Nuclear Information System (INIS)

    Saha, A.; Chakraborty, V.; Dutta, R.K.; Chintalapudi, S.N.


    Polypropylene was irradiated with 12 C ions of 3.6 and 5.4 MeV energies using 3 MV tandem accelerator. The surface modification was investigated by Scanning Electron Microscopy (SEM). Optical changes were monitored by UV-VIS and FTIR spectroscopy. At the lowest ion fluence, only blister formation of various sizes (1-6 μm) was observed. Polymer when irradiated at a fluence of 1x10 14 ions/cm 2 exhibited a network structure. A comparative study on dose dependence of surface and bulk modification has been described. (author)

  11. Strong uniaxial magnetic anisotropy in Co films on highly ordered grating-like nanopatterned Ge surfaces (United States)

    Alam Mollick, Safiul; Singh, Ranveer; Kumar, Mohit; Bhattacharyya, Satyaranjan; Som, Tapobrata


    We present a systematic investigation on uniaxial magnetic anisotropy (UMA) in Co thin films induced by high aspect ratio nanopatterned anisotropic substrates. Self-organized long grating-like nanostructures, with extreme regularities, are fabricated on Ge surfaces using Au-ion implantation at room temperature. Subsequently deposition of Co films are carried out on the same at two different angles. Magneto-optical Kerr effect measurements show strong UMA in Co films grown on ion-patterned Ge substrates, fabricated under different ion fluences, along and perpendicular to the direction of the patterns (long grating-like nanostructures). Magnetic force microscopy measurements under different externally applied magnetic fields reveal an easy domain wall motion when the field is applied along the grating-like nanostructures. On the other hand, high amplitude grating-like nanostructures hinder the spin rotation when the field is applied along the hard axis. The present study will be useful for magnetic recording media and ultra-small magnetic field sensors.

  12. Experimental investigation on the effects of cooling system on surface quality in high speed milling of an aluminium alloy (United States)

    Chirita, B.; Tampu, N. C.; Brabie, G.; Radu, M. C.


    Surface quality is often an important feature of industrial products, not only from the impact it has on the aesthetic aspect but also for the functional role of the parts. High quality surface increases corrosion resistance, assures a longer life cycle for the product and lowers the wear. For a machined part, surface quality is influenced by a series of factors such as the material of the part, the process type, tool geometry, cutting parameters or the cooling system. The choice of the cooling system is especially important, taking into account that the proper conditions will not only assure a superior surface quality, but will also lower the costs and reduce the environmental impact and health risks. The present study aims to investigate the performance of the cooling system and the effect of the cutting parameters on the characteristics of the surfaces resulted from high speed face milling of some parts made of Al 7050-T7451 aluminium alloy. Dry cutting conditions and minimum quantity lubrication (MQL) where used. The results were analysed using analysis of variance (ANOVA).

  13. Impact of high resolution land surface initialization in Indian summer ...

    Indian Academy of Sciences (India)

    transpiration coupling. Most of the previous land surface ..... break spell during the 2009 monsoon season (EXP1: red line, EXP2: blue line) and observation: black line). (figure 4a). However, the rainfall over northeast region is less compared to the break ...

  14. Facile preparation of superhydrophobic surface with high adhesive ...

    Indian Academy of Sciences (India)

    Glass substrates modified by carbon/silica composites are fabricated through a two-step process for the preparation of a superhydrophobic surface (water contact angle ≥ 150°). Carbon nanoparticles were first prepared through a deposition process on glass using a hydrothermal synthesis route, then the glass was ...

  15. Surface Intermediates on Metal Electrodes at High Temperature

    DEFF Research Database (Denmark)

    Zachau-Christiansen, Birgit; Jacobsen, Torben; Bay, Lasse


    The mechanisms widely suggested for the O2-reduc-tion or H2-oxidation SOFC reactions involve inter-mediate O/H species adsorbed on the electrode surface. The presence of these intermediates is investigated by linear sweep voltammetry. In airat moderate temperatures (500øC) Pt in contact with YSZ...

  16. Surface Plasmons on Highly Doped InP

    DEFF Research Database (Denmark)

    Panah, Mohammad Esmail Aryaee; Ottaviano, Luisa; Semenova, Elizaveta


    . The derived dielectric function is used to simulate the excitation of surface plasmons by a diffraction grating made of the grown material. The grating structure is fabricated using standard nanofabrication techniques. Spectral features from the grating agree well with the simulations and show spp coupling...

  17. High-resolution observations of combustion in heterogeneous surface fuels (United States)

    E. Louise Loudermilk; Gary L. Achtemeier; Joseph J. O' Brien; J. Kevin Hiers; Benjamin S. Hornsby


    In ecosystems with frequent surface fires, fire and fuel heterogeneity at relevant scales have been largely ignored. This could be because complete burns give an impression of homogeneity, or due to the difficulty in capturing fine-scale variation in fuel characteristics and fire behaviour. Fire movement between patches of fuel can have implications for modelling fire...

  18. Facile preparation of superhydrophobic surface with high adhesive ...

    Indian Academy of Sciences (India)

    a nearly perfect spherical shape on lotus leaves, which can be rolled off easily, is one of the most beautiful wonders of nature. This natural phenomenon is known as lotus .... by treatment with fluorosilicone, its WCA is 152. ◦. (inset of figure 3(b)), which indicates that the surface of the glass has superhydrophobic property.

  19. Preparation and Characterization of Highly Spherical Silica-titania Aerogel Beads with High Surface Area

    Directory of Open Access Journals (Sweden)

    YU Yu-xi


    Full Text Available The silica-titania aerogel beads were synthesized through sol-gel reaction followed by supercritical drying, in which TEOS and TBT as co-precursors, EtOH as solvents, HAC and NH3·H2O as catalysts. The as-prepared aerogel beads were characterized by SEM,TEM,XRD,FT-IR,TG-DTA and nitrogen adsorption-desorption. The results indicate that the diameter distribution of beads are between 1-8mm, the average diameter of beads is 3.5mm. The aerogel beads have nanoporous network structure with high specific surface area of 914.5m2/g, and the TiO2 particles are distributed in the aerogel uniformly, which keep the anatase crystal under high temperature.

  20. Theoretical aspects of surface reactions (United States)

    Nørskov, J. K.; Stoltze, P.


    A short review is given of our present understanding of the trends in the chemisorption energies and activation energies for dissociation of simple gas molecules on the transition metals. The effect of adsorbed alkali atoms on the activation energy for dissociation is also discussed. This is then used to explain the trends in activity along the transition metal rows and the promoting effect of K for the ammonia synthesis reaction. The basis for the description is the development of a kinetic model for the ammonia synthesis which can describe quantitatively the macroscopic kinetics of a commercial catalyst under industrial conditions. The model relates the reaction rate directly to the properties of the chemisorbed reactants, intermediates and product as measured for model single crystal systems under ultrahigh vacuum conditions.

  1. Microfabrication of high-aspect-ratio Bi-Te alloy microposts and applications in microsized cooling probes (United States)

    Huang, Lei; Wang, Wanjun; Murphy, Michael C.


    High aspect-ratio microposts of bismuth-telluride alloy with a height of up to 750 micrometer and a diameter of 150 micrometer have been fabricated with the LIGA technique. This work is the part of an on-going research effort to develop a microprobe based on Peltier effect for highly localized temperature manipulation on the microscale. Bismuth-telluride alloys were electrodeposited galvanostatically on a titanium substrate using an acidic solution containing Bi3+ and HTeO2- ions in 1 mol dm-3 nitric acid (pH equals 0). The Bi-Te alloy microposts were found to be monophasic, exhibit a polycrystalline structure, demonstrate excellent adhesion on the substrate and with good mechanical strength. The chemical composition of the microposts was dependent on the electrolyte composition of deposition bath and the current density used in the electroplating; by controlling these two factors either p- or n-type Bi-Te alloy microposts may be produced. This research demonstrates that the microfabrication of Peltier effect probes is feasible.

  2. Fermi surface of underdoped high-Tc superconducting cuprates

    International Nuclear Information System (INIS)

    Dai, X.; Su, Z.; Yu, L.


    The coexistence of a π-flux state and a d-wave resonant-valance-bond (RVB) state is considered in this paper within the slave-boson approach. A critical value of doping concentration δ c is found, below which the coexisting π-flux and d-wave RVB state is favored in energy. The pseudo-Fermi surface of spinons and the physical electron spectral function are calculated. A clear Fermi-level crossing is found along the (0,0) to (π, π) direction, but no such crossing is detected along the (π, 0) to (π, π) direction. Also, an energy gap of d-wave symmetry appears at the Fermi level in our calculation. The above results are in agreement with the angle-resolved photoemission experiments which indicate at a d-wave pseudogap and a half-pocket-like Fermi surface in underdoped cuprates. copyright 1997 The American Physical Society

  3. 3-D Numerical Simulation and Analysis of Complex Fiber Geometry RaFC Materials with High Volume Fraction and High Aspect Ratio based on ABAQUS PYTHON (United States)

    Jin, BoCheng


    Organic and inorganic fiber reinforced composites with innumerable fiber orientation distributions and fiber geometries are abundantly available in several natural and synthetic structures. Inorganic glass fiber composites have been introduced to numerous applications due to their economical fabrication and tailored structural properties. Numerical characterization of such composite material systems is necessitated due to their intrinsic statistical nature, which renders extensive experimentation prohibitively time consuming and costly. To predict various mechanical behavior and characterizations of Uni-Directional Fiber Composites (UDFC) and Random Fiber Composites (RaFC), we numerically developed Representative Volume Elements (RVE) with high accuracy and efficiency and with complex fiber geometric representations encountered in uni-directional and random fiber networks. In this thesis, the numerical simulations of unidirectional RaFC fiber strand RVE models (VF>70%) are first presented by programming in ABAQUS PYTHON. Secondly, when the cross sectional aspect ratios (AR) of the second phase fiber inclusions are not necessarily one, various types of RVE models with different cross sectional shape fibers are simulated and discussed. A modified random sequential absorption algorithm is applied to enhance the volume fraction number (VF) of the RVE, which the mechanical properties represents the composite material. Thirdly, based on a Spatial Segment Shortest Distance (SSSD) algorithm, a 3-Dimentional RaFC material RVE model is simulated in ABAQUS PYTHON with randomly oriented and distributed straight fibers of high fiber aspect ratio (AR=100:1) and volume fraction (VF=31.8%). Fourthly, the piecewise multi-segments fiber geometry is obtained in MATLAB environment by a modified SSSD algorithm. Finally, numerical methods including the polynomial curve fitting and piecewise quadratic and cubic B-spline interpolation are applied to optimize the RaFC fiber geometries

  4. A quantitative method to estimate high gloss polished tool steel surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Rebeggiani, S; Rosen, B-G [Halmstad University, The Functional Surfaces Research Group, Box 823, SE-301 18 HALMSTAD (Sweden); Sandberg, A, E-mail: [Uddeholms AB, SE-683 85 Hagfors (Sweden)


    Visual estimations are today the most common way to assess the surface quality of moulds and dies; a method that are both subjective and, with today's high demands on surfaces, hardly usable to distinguish between the finest surface qualities. Instead a method based on non-contact 3D-surface texture analysis is suggested. Several types of tool steel samples, manually as well as machine polished, were analysed to study different types of surface defects such as pitting, orange peel and outwardly features. The classification of the defect structures serves as a catalogue where known defects are described. Suggestions of different levels of 'high surface quality' defined in numerical values adapted to high gloss polished tool steel surfaces are presented. The final goal is to develop a new manual that can work as a 'standard' for estimations of tool steel surfaces for steel producers, mould makers, polishers etc.

  5. High Throughput Spectroscopic Catalyst Screening via Surface Plasmon Spectroscopy (United States)


    elements in a quasi-solid-state ion-gel capacitor. We show that in such a device that the localised surface plasmon resonance (LSPR) of a single Au NR...particles and the dielectric function of the supporting medium have on LSPR changes. Buso et al. and Della Gaspera et al. concluded that particle spectra to H2 induced dielectric function changes of nearby Pt NPs separated by a SiO2 support 23. More recent studies showed that

  6. [Socio-cultural aspects regarding the perception of quality of life amongst people engaging in extreme (high-risk) sports]. (United States)

    Pimentel, Giuliano Gomes de Assis


    Considering the search for adventure activities as a form of improving life quality, the present paper aimed at analyzing the perception of some dimensions of that category among hang-gliding apprentices. A questionnaire was applied to 30 brasilians hang-gliding and paragliding apprentices in order to identify aspects such as, physical activity, preventive behavior, nutrition, stress control and social relationships. Comparing results with the ones found in other adventure sports, it was observed that flyers adopt a competitive and risky behavior, not showing good results in relation to affectionate relationships and physical exercises. On the other hand, all of them are considered as wealthy and more used to dealing with stress. Even not possessing good physical conditioning, individuals practice flight just due to their technical knowledge and the dominium of technology Thus, apprentices use those sport tensions as a form of training the stress control in risky situations. Regarding mental health, activities of active leisure are highly recommended as an escape valve to stress. The group studied showed that besides increasing the tolerance to stress, generated by risky situations, individuals went beyond, once it was observed that the risks of such sport have turned the individuals into more and more insensitive to the professional life pressure.

  7. High aspect ratio silicon nanomoulds for UV embossing fabricated by directional thermal oxidation using an oxidation mask

    International Nuclear Information System (INIS)

    Chen, L Q; Chan-Park, Mary B; Yan, Y H; Zhang Qing; Li, C M; Zhang Jun


    Nanomoulding is simple and economical but moulds with nanoscale features are usually prohibitively expensive to fabricate because nanolithographic techniques are mostly serial and time-consuming for large-area patterning. This paper describes a novel, simple and inexpensive parallel technique for fabricating nanoscale pattern moulds by silicon etching followed by thermal oxidation. The mask pattern can be made by direct photolithography or photolithography followed by metal overetching for submicron- and nanoscale features, respectively. To successfully make nanoscale channels having a post-oxidation cross-sectional shape similar to that of the original channel, an oxidation mask to promote unidirectional (specifically horizontal) oxide growth is found to be essential. A silicon nitride or metal mask layer prevents vertical oxidation of the Si directly beneath it. Without this mask, rectangular channels become smaller but are V-shaped after oxidation. By controlling the silicon etch depth and oxidation time, moulds with high aspect ratio channels having widths ranging from 500 to 50 nm and smaller can be obtained. The nanomould, when passivated with a Teflon-like layer, can be used for first-generation replication using ultraviolet (UV) nanoembossing and second-generation replication in other materials, such as polydimethylsiloxane (PDMS). The PDMS stamp, which was subsequently coated with Au, was used for transfer printing of Au electrodes with a 600 nm gap which will find applications in plastics nanoelectronics

  8. Fractionation and Characterization of High Aspect Ratio Gold Nanorods Using Asymmetric-Flow Field Flow Fractionation and Single Particle Inductively Coupled Plasma Mass Spectrometry

    Directory of Open Access Journals (Sweden)

    Thao M. Nguyen


    Full Text Available Gold nanorods (GNRs are of particular interest for biomedical applications due to their unique size-dependent longitudinal surface plasmon resonance band in the visible to near-infrared. Purified GNRs are essential for the advancement of technologies based on these materials. Used in concert, asymmetric-flow field flow fractionation (A4F and single particle inductively coupled mass spectrometry (spICP-MS provide unique advantages for fractionating and analyzing the typically complex mixtures produced by common synthetic procedures. A4F fractions collected at specific elution times were analyzed off-line by spICP-MS. The individual particle masses were obtained by conversion of the ICP-MS pulse intensity for each detected particle event, using a defined calibration procedure. Size distributions were then derived by transforming particle mass to length assuming a fixed diameter. The resulting particle lengths correlated closely with ex situ transmission electron microscopy. In contrast to our previously reported observations on the fractionation of low-aspect ratio (AR GNRs (AR < 4, under optimal A4F separation conditions the results for high-AR GNRs of fixed diameter (≈20 nm suggest normal, rather than steric, mode elution (i.e., shorter rods with lower AR generally elute first. The relatively narrow populations in late eluting fractions suggest the method can be used to collect and analyze specific length fractions; it is feasible that A4F could be appropriately modified for industrial scale purification of GNRs.

  9. Catalytic Synthesis of Substrate-Free, Aligned and Tailored High Aspect Ratio Multiwall Carbon Nanotubes in an Ultrasonic Atomization Head CVD Reactor

    Directory of Open Access Journals (Sweden)

    Fahad Ali Rabbani


    Full Text Available Chemical vapor deposition (CVD method has proven its benchmark, over other methods, for the production of different types of carbon nanotubes (CNT on commercial and lab scale. In this study, an injection vertical CVD reactor fitted with an ultrasonic atomization head was used in a pilot-plant scale (height 274 cm, radius 25 cm for semicontinuous production of multiwall carbon nanotubes (MWCNTs. p-Xylene was used as a hydrocarbon precursor in which ferrocene was dissolved and provided the cracking catalyst. Atomization of the feed solution resulted in full and even dispersion of the catalytic solution. This dispersion led to the production of high aspect ratio MWCNTs (ranging from 8,000 to 12,000 at 850°C. Different experimental parameters affecting the quality and quantity of the produced CNTs were investigated. These included temperature, reaction time, and flow rate of the reaction and carrier gases. Different properties of the produced CNTs were characterized using SEM and TEM, while TGA was used to evaluate their purity. Specific surface area of selected samples was calculated by BET.

  10. Integrability of Liouville system on high genus Riemann surface: Pt. 1

    International Nuclear Information System (INIS)

    Chen Yixin; Gao Hongbo


    By using the theory of uniformization of Riemann-surfaces, we study properties of the Liouville equation and its general solution on a Riemann surface of genus g>1. After obtaining Hamiltonian formalism in terms of free fields and calculating classical exchange matrices, we prove the classical integrability of Liouville system on high genus Riemann surface

  11. Microstructural and hardness gradients in Cu processed by high pressure surface rolling

    DEFF Research Database (Denmark)

    He, Q. Y.; Zhu, X.-M.; Mei, Q. S.


    The surface of an annealed Cu plate was processed by a high pressure surface rolling (HPSR) process. It is found that the deformed surface layer in the Cu plate after HPSR can be as thick as 2 mm and is characterized by a gradient microstructure, with grain sizes varying from the nanoscale...

  12. Inundation Mapping Tidal Surface - Mean Higher High Water (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — These data are a derived product of the NOAA VDatum tool and they extend the tool's Mean Higher High Water (MHHW) tidal datum conversion inland beyond its original...

  13. Long-range surface plasmons for high-resolution surface plasmon resonance sensors

    Czech Academy of Sciences Publication Activity Database

    Nenninger, G. G.; Tobiška, Petr; Homola, Jiří; Yee, S. S.

    B74, 1/3 (2001), s. 145-151 ISSN 0925-4005. [European Conference on Optical Chemical Sensors and Biosensors EUROPT(R)ODE /5./. Lyon-Villeurbanne, 16.04.2000-19.04.2000] R&D Projects: GA ČR GA102/99/0549; GA ČR GA102/00/1536 Grant - others:Department of Defense(US) DAAD13-99-C-0032 Institutional research plan: CEZ:AV0Z2067918 Keywords : sensors * surface plasmons * biosensors Subject RIV: JB - Sensors, Measurment, Regulation Impact factor: 1.440, year: 2001

  14. Ultra high phase sensitive surface plasmon resonance biosensor (United States)

    Li, Ying-Chang; Chou, Chien


    This study demonstrates a novel phase-sensitive surface plasman resonance biosensor (PS-SPRB) which is able to convert the phase modulation into amplitude modulation analytically via a differential amplifier. PS-SPRB is able to measure biomolecule interactions at ultra-low concentration relying on the properties of phase sensitive detection at shot-noise detection in a real-time. The common-phase noise-rejection mode is provided in PS-SPRB to be able to immune the background phase noise efficiently. The experimental results confirm the detection sensitivity of 0.00001 wt % concentration of sucrose solution and 10 fg/ml mouse IgG interaction with anti IgG in real time.

  15. Method for producing high surface area chromia materials for catalysis (United States)

    Gash, Alexander E [Brentwood, CA; Satcher, Joe [Patterson, CA; Tillotson, Thomas [Tracy, CA; Hrubesh, Lawrence [Pleasanton, CA; Simpson, Randall [Livermore, CA


    Nanostructured chromium(III)-oxide-based materials using sol-gel processing and a synthetic route for producing such materials are disclosed herein. Monolithic aerogels and xerogels having surface areas between 150 m.sup.2/g and 520 m.sup.2/g have been produced. The synthetic method employs the use of stable and inexpensive hydrated-chromium(III) inorganic salts and common solvents such as water, ethanol, methanol, 1-propanol, t-butanol, 2-ethoxy ethanol, and ethylene glycol, DMSO, and dimethyl formamide. The synthesis involves the dissolution of the metal salt in a solvent followed by an addition of a proton scavenger, such as an epoxide, which induces gel formation in a timely manner. Both critical point (supercritical extraction) and atmospheric (low temperature evaporation) drying may be employed to produce monolithic aerogels and xerogels, respectively.

  16. Highly sensitive BTX detection using surface functionalized QCM sensor

    Energy Technology Data Exchange (ETDEWEB)

    Bozkurt, Asuman Aşıkoğlu; Özdemir, Okan; Altındal, Ahmet, E-mail: [Department of Physics, Yildiz Technical University, Davutpasa, 34210 Istanbul (Turkey)


    A novel organic compound was designed and successfully synthesized for the fabrication of QCM based sensors to detect the low concentrations of BTX gases in indoor air. The effect of the long-range electron orbital delocalization on the BTX vapour sensing properties of azo-bridged Pcs based chemiresistor-type sensors have also been investigated in this work. The sensing behaviour of the film for the online detection of volatile organic solvent vapors was investigated by utilizing an AT-cut quartz crystal resonator. It was observed that the adsorption of the target molecules on the coating surface cause a reversible negative frequency shift of the resonator. Thus, a variety of solvent vapors can be detected by using the phthalocyanine film as sensitive coating, with sensitivity in the ppm range and response times in the order of several seconds depending on the molecular structure of the organic solvent.

  17. Assimilation and High Resolution Forecasts of Surface and Near Surface Conditions for the 2010 Vancouver Winter Olympic and Paralympic Games (United States)

    Bernier, Natacha B.; Bélair, Stéphane; Bilodeau, Bernard; Tong, Linying


    A dynamical model was experimentally implemented to provide high resolution forecasts at points of interests in the 2010 Vancouver Olympics and Paralympics Region. In a first experiment, GEM-Surf, the near surface and land surface modeling system, is driven by operational atmospheric forecasts and used to refine the surface forecasts according to local surface conditions such as elevation and vegetation type. In this simple form, temperature and snow depth forecasts are improved mainly as a result of the better representation of real elevation. In a second experiment, screen level observations and operational atmospheric forecasts are blended to drive a continuous cycle of near surface and land surface hindcasts. Hindcasts of the previous day conditions are then regarded as today's optimized initial conditions. Hence, in this experiment, given observations are available, observation driven hindcasts continuously ensure that daily forecasts are issued from improved initial conditions. GEM-Surf forecasts obtained from improved short-range hindcasts produced using these better conditions result in improved snow depth forecasts. In a third experiment, assimilation of snow depth data is applied to further optimize GEM-Surf's initial conditions, in addition to the use of blended observations and forecasts for forcing. Results show that snow depth and summer temperature forecasts are further improved by the addition of snow depth data assimilation.

  18. Methods to estimate aspects of physical activity and sedentary behavior from high-frequency wrist accelerometer measurements. (United States)

    Staudenmayer, John; He, Shai; Hickey, Amanda; Sasaki, Jeffer; Freedson, Patty


    This investigation developed models to estimate aspects of physical activity and sedentary behavior from three-axis high-frequency wrist-worn accelerometer data. The models were developed and tested on 20 participants (n = 10 males, n = 10 females, mean age = 24.1, mean body mass index = 23.9), who wore an ActiGraph GT3X+ accelerometer on their dominant wrist and an ActiGraph GT3X on the hip while performing a variety of scripted activities. Energy expenditure was concurrently measured by a portable indirect calorimetry system. Those calibration data were then used to develop and assess both machine-learning and simpler models with fewer unknown parameters (linear regression and decision trees) to estimate metabolic equivalent scores (METs) and to classify activity intensity, sedentary time, and locomotion time. The wrist models, applied to 15-s windows, estimated METs [random forest: root mean squared error (rSME) = 1.21 METs, hip: rMSE = 1.67 METs] and activity intensity (random forest: 75% correct, hip: 60% correct) better than a previously developed model that used counts per minute measured at the hip. In a separate set of comparisons, the simpler decision trees classified activity intensity (random forest: 75% correct, tree: 74% correct), sedentary time (random forest: 96% correct, decision tree: 97% correct), and locomotion time (random forest: 99% correct, decision tree: 96% correct) nearly as well or better than the machine-learning approaches. Preliminary investigation of the models' performance on two free-living people suggests that they may work well outside of controlled conditions. Copyright © 2015 the American Physiological Society.

  19. Strategic and tactical aspect of the relations between the participants of ICP in high-rise construction (United States)

    Fedorov, Maksim; Matys, Elena; Kopytova, Anna


    Outlined the main trends in the development of the construction sector in the Russian Federation at the present stage of its development are identified problems and shortcomings of current investment in the construction industry. It is proved that to consider the investment and construction process should be in terms of the strategic and tactical aspects. It was established that, on the basis of the spirit and the participants of investment and construction process, the strategic aspect it should be focused primarily on the formation of financial resources (through various mechanisms) and to attract investors. A tactical aspect of the investment and construction process is focused on the choice of organizational form of the project and the rational use of resources generated by the investment in construction.

  20. High-speed 3D surface measurement with mechanical projector (United States)

    Hyun, Jae-Sang; Zhang, Song


    This paper presents a method to overcome the light spectral range limitation of using digital-light-processing (DLP) projector for 3D shape measurement by developing a mechanical projector. The mechanical projector enables much broader spectral range of light than that the DLP projector allows. The rapidly spinning disk with binary structures can generate desired sinusoidal patterns at a frequency of 10 kHz or higher with a single DC motor. By precisely synchronizing the camera with the projector, phase-shifted fringe patterns can be accurately captured for high-accuracy 3D shape measurement. We further employed a computational framework that could enable absolute phase and thus absolute 3D shape measurement. We developed such prototype system that experimentally demonstrated the success of the proposed method.

  1. Potential sputtering from a Si surface by very highly charged ion impact

    International Nuclear Information System (INIS)

    Tona, Masahide; Watanabe, Hirofumi; Takahashi, Satoshi; Nakamura, Nobuyuki; Yoshiyasu, Nobuo; Sakurai, Makoto; Yamada, Chikashi; Ohtani, Shunsuke


    We have observed radiation effect in collision of slow highly charged ions with the following target materials; a SiO 2 thin film, a Si(1 1 1)-(7 x 7) surface and a hydrogen terminated Si(1 1 1)-(1 x 1) surface. Secondary ion mass spectrometry and scanning tunneling microscopy revealed some features due to 'potential sputtering'; (a) strong dependence of secondary particle emission on the surface condition, (b) high yield of positive ion emission including cluster fragments and (c) creation of nanometer sized surface structure. The mechanism for the potential sputtering is briefly discussed, based on the 'Coulomb explosion' model

  2. Nano-scale surface modification of materials with slow, highly charged ion beams

    International Nuclear Information System (INIS)

    Sakurai, M.; Tona, M.; Takahashi, S.; Watanabe, H.; Nakamura, N.; Yoshiyasu, N.; Yamada, C.; Ohtani, S.; Sakaue, H.A.; Kawase, Y.; Mitsumori, K.; Terui, T.; Mashiko, S.


    Some results on surface modification of Si and graphite with highly charged ions (HCIs) are presented. Modified surfaces were observed using scanning tunneling microscopy. Crater-like structure with a diameter in nm region is formed on a Si(1 1 1)-(7 x 7) surface by the incidence of a single HCI. The protrusion structure is formed on a highly oriented pyrolytic graphite surface on the other hand, and the structure becomes an active site for molecular adsorption. A new, intense HCI source and an experimental apparatus are under development in order to process and observe aligned nanostructures created by the impact of collimated HCI beam

  3. Heat transfer tests under forced convection conditions with high wettable heater surface

    Energy Technology Data Exchange (ETDEWEB)

    Mitsutake, Toru; Morooka, Shin-ichi; Miura, Shigeru; Akiba, Miyuki; Sato, Hisaki; Shirakawa, Ken-etsu; Oosato, Tetsuo; Yamamoto, Seiji [Toshiba Co., Kanagawa (Japan)


    Under forced convection and atmospheric pressure conditions, heat transfer tests were performed using the annulus channel of a heater rod with highly wettable surface. Improvement of boiling heat transfer requires that the cooling liquid can contact the heating surface, or a high-wettability heating surface, even if a vapor bubble layer is generated on the surface. >From this point of view, high-wettable heating surface was studied. As oxide semiconductor-coated materials are highly-wettable, we made a TiO{sub 2} coated heater rod. TiO{sub 2} coated surface has a high-wettability, in terms of contact angle and Leidenfrost temperature. The boiling curve was measured with and without TiO coated surface. The results showed difference between with and without TiO{sub 2} coating. TiO{sub 2} coating rod showed lower boiling onset heat flux, wider nucleate boiling region and higher critical heat flux than without coating. In summary, high wettablity heater surface produced higher boiling heat transfer characteristics under forced convection conditions. (author)

  4. Study of surfaces and surface layers on high temperature materials after short-time thermal loads

    International Nuclear Information System (INIS)

    Bolt, H.; Hoven, H.; Koizlik, K.; Linke, J.; Nickel, H.; Wallura, E.


    Being part of the plasma-wall interaction during TOKAMAK operation, erosion- and redeposition processes of First Wall materials substantially influence plasma parameters as well as the properties of the First Wall. An important redeposition process of eroded material is the formation of thin films by atomic condensation. Examinations of First Wall components after TOKAMAK operation lead to the assumption that these thin metallic films tend to agglomerate to small particles under subsequent heat load. In laboratory experiments it is shown that thin metallic films on various substrates can agglomerate under short time high heat fluxes and also under longer lasting lower thermal loads, thus verifying the ''agglomeration hypothesis''. (orig.) [de

  5. Distribution and Characteristics of Boulder Halos at High Latitudes on Mars: Ground Ice and Surface Processes Drive Surface Reworking (United States)

    Levy, J. S.; Fassett, C. I.; Rader, L. X.; King, I. R.; Chaffey, P. M.; Wagoner, C. M.; Hanlon, A. E.; Watters, J. L.; Kreslavsky, M. A.; Holt, J. W.; Russell, A. T.; Dyar, M. D.


    Boulder halos are circular arrangements of clasts present at Martian middle to high latitudes. Boulder halos are thought to result from impacts into a boulder-poor surficial unit that is rich in ground ice and/or sediments and that is underlain by a competent substrate. In this model, boulders are excavated by impacts and remain at the surface as the crater degrades. To determine the distribution of boulder halos and to evaluate mechanisms for their formation, we searched for boulder halos over 4,188 High Resolution Imaging Science Experiment images located between 50-80° north and 50-80° south latitude. We evaluate geological and climatological parameters at halo sites. Boulder halos are about three times more common in the northern hemisphere than in the southern hemisphere (19% versus 6% of images) and have size-frequency distributions suggesting recent Amazonian formation (tens to hundreds of millions of years). In the north, boulder halo sites are characterized by abundant shallow subsurface ice and high thermal inertia. Spatial patterns of halo distribution indicate that excavation of boulders from beneath nonboulder-bearing substrates is necessary for the formation of boulder halos, but that alone is not sufficient. Rather, surface processes either promote boulder halo preservation in the north or destroy boulder halos in the south. Notably, boulder halos predate the most recent period of near-surface ice emplacement on Mars and persist at the surface atop mobile regolith. The lifetime of observed boulders at the Martian surface is greater than the lifetime of the craters that excavated them. Finally, larger minimum boulder halo sizes in the north indicate thicker icy soil layers on average throughout climate variations driven by spin/orbit changes during the last tens to hundreds of millions of years.

  6. Effect of near-surface topography on high-frequency Rayleigh-wave propagation (United States)

    Wang, Limin; Xu, Yixian; Xia, Jianghai; Luo, Yinhe


    Rayleigh waves, which are formed due to interference of P- and Sv-waves near the free surface, propagate along the free surface and vanish exponentially in the vertical direction. Their propagation is strongly influenced by surface topography. Due to the high resolution and precision requirements of near-surface investigations, the high-frequency Rayleigh waves are usually used for near-surface structural detecting. Although there are some numerical studies on high-frequency Rayleigh-wave propagation on topographic free surface, detailed analysis of characters of high-frequency Rayleigh-wave propagation on topographic free surface remains untouched. Hence, research of propagation of Rayleigh waves on complex topographic surface becomes critical for Rayleigh-wave methods in near-surface applications. To study the propagation of high-frequency Rayleigh waves on topographic free surface, two main topographic models are designed in this study. One of the models contains a depressed topographic surface, and another contains an uplifted topographic surface. We numerically simulate the propagation of high-frequency Rayleigh waves on these two topographic surfaces by finite-difference method. Soon afterwards, we analyze the propagation character of high-frequency Rayleigh waves on such topographic models, and compare the variations on its energy and frequency before and after passing the topographic region. At last, we discuss the relationship between the variations and topographical steepness of each model. Our numerical results indicate that influence of depressed topography for high-frequency Rayleigh waves is more distinct than influence of uplifted topography. Rayleigh waves produce new scattering body waves during passing the depressed topography with reduction of amplitude and loss of high-frequency components. Moreover, the steeper the depressed topography is, the more energy of Rayleigh waves is lost. The uplifted topography with gentle slope produces similar

  7. Experimental aspects of buoyancy correction in measuring reliable high-pressure excess adsorption isotherms using the gravimetric method (United States)

    Nguyen, Huong Giang T.; Horn, Jarod C.; Thommes, Matthias; van Zee, Roger D.; Espinal, Laura


    Addressing reproducibility issues in adsorption measurements is critical to accelerating the path to discovery of new industrial adsorbents and to understanding adsorption processes. A National Institute of Standards and Technology Reference Material, RM 8852 (ammonium ZSM-5 zeolite), and two gravimetric instruments with asymmetric two-beam balances were used to measure high-pressure adsorption isotherms. This work demonstrates how common approaches to buoyancy correction, a key factor in obtaining the mass change due to surface excess gas uptake from the apparent mass change, can impact the adsorption isotherm data. Three different approaches to buoyancy correction were investigated and applied to the subcritical CO2 and supercritical N2 adsorption isotherms at 293 K. It was observed that measuring a collective volume for all balance components for the buoyancy correction (helium method) introduces an inherent bias in temperature partition when there is a temperature gradient (i.e. analysis temperature is not equal to instrument air bath temperature). We demonstrate that a blank subtraction is effective in mitigating the biases associated with temperature partitioning, instrument calibration, and the determined volumes of the balance components. In general, the manual and subtraction methods allow for better treatment of the temperature gradient during buoyancy correction. From the study, best practices specific to asymmetric two-beam balances and more general recommendations for measuring isotherms far from critical temperatures using gravimetric instruments are offered.

  8. Atomic layer deposition for coating of high aspect ratio TiO.sub.2./sub. nanotube layers

    Czech Academy of Sciences Publication Activity Database

    Zazpe, R.; Knaut, M.; Sopha, H.; Hromádko, L.; Albert, M.; Přikryl, J.; Gärtnerová, Viera; Bartha, J.W.; Macák, J. M.


    Roč. 32, č. 41 (2016), s. 10551-10558 ISSN 0743-7463 Institutional support: RVO:68378271 Keywords : aluminum * aluminum coatings * aspect ratio * coatings * nanotubes Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 3.833, year: 2016

  9. Narrow conductive structures with high aspect ratios through single-pass inkjet printing and evaporation-induced dewetting

    NARCIS (Netherlands)

    Abbel, R.; Teunissen, P.; Michels, J.; Groen, W.A.


    Inkjet printed silver lines contract to widths below 20-μm during drying on an organic planarization coating. Aspect ratios previously unprecedented with single pass inkjet printing on isotropic homogeneous substrates are obtained. This effect is caused by the subsequent evaporation of solvents from

  10. Functional Aspects of the Solution Structure and Dynamics of PAF, a Highly Stable Antifungal Protein from Penicillium chrysogenum (United States)

    Batta, Gyula; Barna, Teréz; Gáspári, Zoltán; Sándor, Szabolcs; Kövér, Katalin E.; Binder, Ulrike; Sarg, Bettina; Kaiserer, Lydia; Chhillar, Anil Kumar; Eigentler, Andrea; Leiter, Éva; Hegedüs, Nikoletta; Pócsi, István; Lindner, Herbert; Marx, Florentine


    Summary PAF is a promising antimycotic without toxic effects on mammalian cells and therefore may be a drug candidate against the often lethal Aspergillus infections in human. The pathogenesis of PAF on sensitive fungi involves G-protein coupled signaling followed by apoptosis. Here, the solution structure of this small, cationic, antifungal protein from Penicillium chrysogenum is determined by solution NMR. We proved that PAF belongs to the SCOP fold class of its closest homologue AFP from Aspergillus giganteus. PAF comprises five β—strands forming two orthogonally packed β—sheets sharing a common interface. The ambiguity in the assignment of two disulfide bonds of three was investigated by NMR dynamics combined with restrained molecular dynamics calculations. The clue could not be resolved: two ensembles with different disulfide patterns and the one with no S-S bond exhibit essentially the same fold. 15N relaxation dispersion and interference experiments did not reveal disulfide bond rearrangements via slow exchange. The measured order parameters and the 3.0 ns correlation time is appropriate for a compact monomeric protein of this size. We demonstrated by site-directed mutagenesis that the highly conserved and positively charged lysine-rich domain region on the surface enhances the toxicity of PAF. However, the efficacy of the OB fold is reduced in PAF compared to AFP, due to less solvent exposed aromatic regions explaining the absence of chitobiose binding. The present work lends further support to the understanding of the documented substantial differences between the mode of action of two highly homologous antifungal proteins. PMID:19459942

  11. High-rate production of micro- and nanostructured surfaces: Injection molding and novel process for metal tooling manufacturing (United States)

    De Jesus Vega, Marisely

    rapidly processed via liquid injection molding. LSR with its excellent mechanical properties, transparency, non-toxicity and rapid molding capabilities can bring the production of micro and nanostructured surfaces from laboratory research facilities to high-rate manufacturing. However, previous research on microstructured surfaces made off LSR does not focus on the processing aspect of this material. Therefore, there is a lack of understanding of how different processing conditions affect the replication of microstructures. Additionally, there are no reports molding nanostructures of LSR. Features between 115 microm and 0.250 microm were molded in this work and the effect of different processing conditions and features sizes were studied. For the last part of this work, a novel metal additive manufacturing technique was used for the production of microstructured surfaces to be used as tooling for injection molding. The printing method consists of metal pastes printed through a tip onto a steel substrate. Prior work has shown spreading and swelling of features when metal pastes extrude out of the printing tip. PDMS was studied as a binder material to minimize spreading and swelling of the features by curing right after printing. In addition, prior work has shown durability of this metal printed tool up to 5000 injection molding cycles. This work compares this durability to durability of commercially available selective laser sintering metal tools. Furthermore, surface roughness was studied as this is one of the most important things to consider when molding microchannels for certain applications.

  12. Nanofabrication on a Si surface by slow highly charged ion impact

    International Nuclear Information System (INIS)

    Tona, Masahide; Watanabe, Hirofumi; Takahashi, Satoshi; Nakamura, Nobuyuki; Yoshiyasu, Nobuo; Sakurai, Makoto; Terui, Toshifumi; Mashiko, Shinro; Yamada, Chikashi; Ohtani, Shunsuke


    We have observed surface chemical reactions which occur at the impact sites on a Si(1 1 1)-(7 x 7) surface and a highly oriented pyrolytic graphite (HOPG) surface bombarded by highly charged ions (HCIs) by using a scanning tunneling microscope (STM). Crater structures are formed on the Si(1 1 1)-(7 x 7) surface by single I 50+ -impacts. STM-observation for the early step of oxidation on the surface suggests that the impact site is so active that dangling bonds created by HCI impacts are immediately quenched by reaction with residual gas molecules. We show also the selective adsorption of organic molecules at a HCI-induced impact site on the HOPG surface

  13. Surface free energy of ultra-high molecular weight polyethylene modified by electron and gamma irradiation

    International Nuclear Information System (INIS)

    Abdul-Kader, A.M.; Turos, A.; Radwan, R.M.; Kelany, A.M.


    Surface free energy of biocompatible polymers is important factor which affects the surface properties such as wetting, adhesion and biocompatibility. In the present work, the change in the surface free energy of ultra-high molecular weight polyethylene (UHMWPE) samples, which is produced by electron beam and gamma ray irradiation were, investigated. Mechanism of the changes in surface free energy induced by irradiations of doses ranging from 25 to 500 kGy was studied. FTIR technique was applied for sample analysis. Contact angle measurements showed that wettability and surface free energy of samples have increased with increasing the irradiation dose, where the values of droplet contact angle of the samples decrease gradually with increasing the radiation dose. The increase in the wettability and surface free energy of the irradiated samples are attributed to formation of hydrophilic groups on the polymer surface by the oxidation, which apparently occurs by exposure of irradiated samples to the air.

  14. Electrodeposition of Gold to Conformally Fill High Aspect Ratio Nanometric Silicon Grating Trenches: A Comparison of Pulsed and Direct Current Protocols (United States)

    Znati, Sami A.; Chedid, Nicholas; Miao, Houxun; Chen, Lei; Bennett, Eric E.; Wen, Han


    Filling high-aspect-ratio trenches with gold is a frequent requirement in the fabrication of x-ray optics as well as micro-electronic components and other fabrication processes. Conformal electrodeposition of gold in sub-micron-width silicon trenches with an aspect ratio greater than 35 over a grating area of several square centimeters is challenging and has not been described in the literature previously. A comparison of pulsed plating and constant current plating led to a gold electroplating protocol that reliably filled trenches for such structures. PMID:27042384

  15. Structure and energetics of high index Fe, Al, Cu and Ni surfaces using equivalent crystal theory (United States)

    Rodriguez, Agustin M.; Bozzolo, Guillermo; Ferrante, John


    Equivalent crystal theory (ECT) is applied to the study of multilayer relaxations and surface energies of high-index faces of Fe, Al, Ni, and Cu. Changes in interplanar spacing as well as registry of planes close to the surface and the ensuing surface energies changes are discussed in reference to available experimental data and other theoretical calculations. Since ECT is a semiempirical method, the dependence of the results on the variation of the input used was investigated.

  16. Devices comprised of discrete high-temperature superconductor chips disposed on a surface

    Energy Technology Data Exchange (ETDEWEB)

    Van Duzer, T.


    A structure exposed to electromagnetic radiation is described, comprising: a metal surface and a plurality of discrete elements, each element including an insulating substrate and a high-temperature superconducting material substantially covering a face of said substrate, a portion of said metal surface being substantially covered with said elements with said superconducting material thereof adjacent to and in electrical contact with said metal surface, thereby reducing ohmic losses on exposure of said structure to said electromagnetic radiation.

  17. Reduced-volume antennas with integrated high-impedance electromagnetic surfaces.

    Energy Technology Data Exchange (ETDEWEB)

    Forman, Michael A.


    Several antennas with integrated high-impedance surfaces are presented. The high-impedance surface is implemented as a composite right/left-handed (CRLH) metamaterial fabricated from a periodic structure characterized by a substrate, filled with an array of vertical vias and capped by capacitive patches. Omnidirectional antennas placed in close proximity to the high-impedance surface radiate hemispherically with an increase in boresight far-field pattern gain of up to 10 dB and a front-to-back ratio as high as 13 dB at 2.45 GHz. Several TEM rectangular horn antennas are realized by replacing conductor walls with high-impedance surfaces. The TEM horn antennas are capable of operating below the TE{sub 1,0} cutoff frequency of a standard all-metal horn antenna, enabling a reduction in antenna volume. Above the cutoff frequency the TEM horn antennas function similarly to standard rectangular horn antennas.

  18. Test data on electrical contacts at high surface velocities and high current densities for homopolar generators

    International Nuclear Information System (INIS)

    Brennan, M.; Tolk, K.M.; Weldon, W.F.; Rylander, H.G.; Woodson, H.H.


    Test data is presented for one grade of copper graphite brush material, Morganite CMlS, over a wide range of surface velocities, atmospheres, and current densities that are expected for fast discharge (<100 ms) homopolar generators. The brushes were run on a copper coated 7075-T6 aluminum disk at surface speeds up to 277 m/sec. One electroplated copper and three flame sprayed copper coatings were used during the tests. Significant differences in contact voltage drops and surface mechanical properties of the copper coatings were observed

  19. High-resolution TOF-SIMS study of varying chain length self-assembled monolayer surfaces. (United States)

    Wolf, Kurt V; Cole, David A; Bernasek, Steven L


    A high-resolution time-of-flight secondary ionization mass spectrometer (TOF-SIMS) has been used to investigate chain length effects in hydrocarbon seff-assembled monolayer (SAM) surfaces on gold substrates. A wide range of n-alkanethiols was used to make homogeneous SAM surfaces, which included both odd and even hydrocarbon chain length thiols. Variations in coverage, extent of oxidation, and high-mass cluster formation as a function of hydrocarbon chain length of the alkanethiol SAM surfaces were investigated. Long-short chain length effects were observed for the relative coverage of the SAM surfaces, which directly influences the extent of oxidation for the thin films. The formation of gold-sulfur and gold-adsorbate cluster ions was also observed, since the mass range of the TOF-SIMS made it possible to monitor all of the cluster ions that were formed following the high-energy ion/surface interactions.

  20. Effect of High-Speed Milling Parameters on Surface Metamorphic Layer of TC17 Titanium Alloy

    Directory of Open Access Journals (Sweden)

    TAN Liang


    Full Text Available In order to provide the relatively accurate experimental basis for optimizing parameters and controlling surface metamorphic layer, ball end high-speed milling experiments of TC17 titanium alloy were carried out utilizing one of experimental design techniques based on the response surface methodology. The surface roughness prediction model was built, variance analyses were applied to check the significances of surface roughness model and input parameters, the effect of parameters on surface roughness was analyzed. Meanwhile, the residual stress, microhardness and microstructure under the condition of high, medium and low level of parameters were investigated. Results indicate that the model can predict the surface roughness effectively and feed per tooth and radial depth of cut have an obvious effect on surface roughness. Compressive residual stresses are detected on all milled surfaces and surface residual stresses are increased with the increase of the level of the milling parameters. The compressive residual stress layer is approximately 20 μm regardless of milling parameters level used. The process of thermal softening, then work hardening, and finally tending to stabilize are observed in the microhardness profiles. Grains of the surface layer are broken and bent, the thickness of plastic deformation layer is approximately 10 μm.

  1. Experimental Investigation of a High-Speed Hydrofoil with Parabolic Thickness Distribution and an Aspect Ratio of 3 (United States)

    Christopher, Kenneth W.


    An experimental investigation has been made to determine the hydro-dynamic characteristics of a 10-percent-thick hydrofoil with an aspect ratio of 3 designed to operate with acceptable efficiency at speeds in the neighborhood of 100 knots (169 fps). A cambered hydrofoil model with parabolic thickness distribution was investigated at a depth of chord over a range of angles of attack from -0.5 deg to 4.0 deg and at speeds from 120 to 210 fps. substantially wider range of operation at acceptable lift-drag ratios as well as higher maximum lift-drag-ratio values than did a hydrofoil of similar design with an aspect ratio of 1.

  2. Effect of process parameters on flow length and flash formation in injection moulding of high aspect ratio polymeric micro features

    DEFF Research Database (Denmark)

    Eladl, Abdelkhalik; Mostafa, Rania; Islam, Aminul


    part with four micro fingers with different aspect ratios (from 21 up to 150) and was carried out according to the Design of Experiments (DOE) statistical technique. The results show that holding pressure and injection velocity are the most influential parameters on part mass with a direct effect......This paper reports an investigation of the effects of process parameters on the quality characteristics of polymeric parts produced by micro injection moulding (µIM) with two different materials. Four injection moulding process parameters (injection velocity, holding pressure, melt temperature...... for both materials. Both parameters have a similar effect on flow length for both PP and ABS at all aspect ratios and have higher effects as the feature thickness decreased below 300 µm. The study shows that for the investigated materials the injection speed and packing pressure were the most influential...

  3. Surface-initiated phase transition in solid hydrogen under the high-pressure compression (United States)

    Lei, Haile; Lin, Wei; Wang, Kai; Li, Xibo


    The large-scale molecular dynamics simulations have been performed to understand the microscopic mechanism governing the phase transition of solid hydrogen under the high-pressure compression. These results demonstrate that the face-centered-cubic-to-hexagonal close-packed phase transition is initiated first at the surfaces at a much lower pressure than in the volume and then extends gradually from the surface to volume in the solid hydrogen. The infrared spectra from the surface are revealed to exhibit a different pressure-dependent feature from those of the volume during the high-pressure compression. It is thus deduced that the weakening intramolecular H-H bonds are always accompanied by hardening surface phonons through strengthening the intermolecular H2-H2 coupling at the surfaces with respect to the counterparts in the volume at high pressures. This is just opposite to the conventional atomic crystals, in which the surface phonons are softening. The high-pressure compression has further been predicted to force the atoms or molecules to spray out of surface to degrade the pressure. These results provide a glimpse of structural properties of solid hydrogen at the early stage during the high-pressure compression.

  4. High-speed surface transportation corridor : a conceptual framework, final report. (United States)


    Efficient transportation is indispensable for economic growth and prosperity. In this study we propose the development of a high-speed surface corridor and compatible vehicles. We present a conceptual framework for this corridor and vehicle. This pro...

  5. High Sensitivity Semiconductor Sensor Skins for Multi-Axis Surface Pressure Characterization, Phase II (United States)

    National Aeronautics and Space Administration — This NASA Phase II SBIR program would fabricate high sensitivity semiconductor nanomembrane 'sensor skins' capable of multi-axis surface pressure characterization on...

  6. High Sensitivity Semiconductor Sensor Skins for Multi-Axis Surface Pressure Characterization, Phase I (United States)

    National Aeronautics and Space Administration — This NASA Phase I SBIR program would fabricate high sensitivity semiconductor nanomembrane 'sensor skins' capable of multi-axis surface pressure characterization on...

  7. Surface disorder production during plasma immersion implantation and high energy ion implantation

    NARCIS (Netherlands)

    El-sherbiny, M.A.; Khanh, N.Q.; Wormeester, Herbert; Fried, M.; Fried, M.; Lohner, T.; Lohner, T.; Pinter, I.; Gyulai, J.


    High-depth-resolution Rutherford Backscattering Spectrometry (RBS) combined with channeling technique was used to analyze the surface layer formed during plasma immersion ion implantation (PIII) of single crystal silicon substrates. Single wavelength multiple angle of incidence ellipsometry (MAIE)

  8. Calibration and Validation of High Frequency Radar for Ocean Surface Current Mapping

    National Research Council Canada - National Science Library

    Kim, Kyung


    High Frequency (HF) radar backscatter instruments are being developed and tested in the marine science and defense science communities for their abilities to sense surface parameters remotely in the coastal ocean over large areas...

  9. An Investigation of Surface Current Patterns Related to Upwelling in Monterey Bay, Using High Frequency Radar

    National Research Council Canada - National Science Library

    Enriquez, Andres


    High Frequency (HF) radar backscatter instruments are under development and testing in the marine science and defense science communities for their abilities to remotely sense surface parameters in the coastal ocean over large areas...

  10. Surface chemistry of metals and their oxides in high temperature water

    International Nuclear Information System (INIS)

    Tomlinson, M.


    Examination of oxide and metal surfaces in water at high temperature by a broad spectrum of techniques is bringing understanding of corrosion product movement and alleviation of activity transport in CANDU-type reactor primary coolant circuits. (Author)

  11. Technology of surface wastewater purification, including high-rise construction areas (United States)

    Tsyba, Anna; Skolubovich, Yury


    Despite on the improvements in the quality of high-rise construction areas and industrial wastewater treatment, the pollution of water bodies continues to increase. This is due to the organized and unorganized surface untreated sewage entry into the reservoirs. The qualitative analysis of some cities' surface sewage composition is carried out in the work. Based on the published literature review, the characteristic contamination present in surface wastewater was identified. The paper proposes a new technology for the treatment of surface sewage and presents the results of preliminary studies.

  12. Graphene as a high impedance surface for ultra-wideband electromagnetic waves

    Energy Technology Data Exchange (ETDEWEB)

    Aldrigo, Martino; Costanzo, Alessandra [Department of Electrical, Electronic, and Information Engineering “Guglielmo Marconi” – DEI, University of Bologna, Viale del Risorgimento, 2, 40132 Bologna (Italy); Dragoman, Mircea [National Institute for Research and Development in Microtechnology (IMT), P.O. Box 38-160, 023573 Bucharest (Romania); Dragoman, Daniela [Department of Physics, University of Bucharest, P.O. Box MG-11, 077125 Bucharest (Romania)


    The metals are regularly used as reflectors of electromagnetic fields emitted by antennas ranging from microwaves up to THz. To enhance the reflection and thus the gain of the antenna, metallic high impedance surfaces (HIS) are used. HIS is a planar array of continuous metallic periodic cell surfaces able to suppress surface waves, which cause multipath interference and backward radiation in a narrow bandwidth near the cell resonance. Also, the image currents are reduced, and therefore the antenna can be placed near the HIS. We demonstrate that graphene is acting as a HIS surface in a very large bandwidth, from microwave to THz, suppressing the radiation leakages better than a metal.

  13. Target surface area effects on hot electron dynamics from high intensity laser-plasma interactions (United States)

    Zulick, C.; Raymond, A.; McKelvey, A.; Chvykov, V.; Maksimchuk, A.; Thomas, A. G. R.; Willingale, L.; Yanovsky, V.; Krushelnick, K.


    Reduced surface area targets were studied using an ultra-high intensity femtosecond laser in order to determine the effect of electron sheath field confinement on electron dynamics. X-ray emission due to energetic electrons was imaged using a {K}α imaging crystal. Electrons were observed to travel along the surface of wire targets, and were slowed mainly by the induced fields. Targets with reduced surface areas were correlated with increased hot electron densities and proton energies. Hybrid Vlasov-Fokker-Planck simulations demonstrated increased electric sheath field strength in reduced surface area targets.

  14. Single-Step Fabrication of High-Density Microdroplet Arrays of Low-Surface-Tension Liquids. (United States)

    Feng, Wenqian; Li, Linxian; Du, Xin; Welle, Alexander; Levkin, Pavel A


    A facile approach for surface patterning that enables single-step fabrication of high-density arrays of low-surface-tension organic-liquid microdroplets is described. This approach enables miniaturized and parallel high-throughput screenings in organic solvents, formation of homogeneous arrays of hydrophobic nanoparticles, polymer micropads of specific shapes, and polymer microlens arrays. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  15. How surface composition of high milk proteins powders is influenced by spray-drying temperature. (United States)

    Gaiani, C; Morand, M; Sanchez, C; Tehrany, E Arab; Jacquot, M; Schuck, P; Jeantet, R; Scher, J


    High milk proteins powders are common ingredients in many food products. The surface composition of these powders is expected to play an essential role during their storage, handling and/or final application. Therefore, an eventual control of the surface composition by modifying the spray-drying temperature could be very useful in the improvement of powder quality and the development of new applications. For this purpose, the influence of five spray-drying temperatures upon the surface composition of the powders was investigated by X-ray photoelectron spectroscopy. The major milk proteins were studied: native micellar casein and native whey, both more or less enriched in lactose. The results show a surface enrichment in lipids for all the powders and in proteins for many powders. Whatever the drying temperature, lipids and proteins are preferentially located near the surface whereas lactose is found in the core. This surface enrichment is also highly affected by the spray-drying temperature. More lipids, more proteins and less lactose are systematically observed at the surface of powders spray-dried at lower outlet air temperatures. The nature of proteins is also found essential; surface enrichment in lipids being much stronger for whey proteins containing powders than for casein containing powders. Additionally, we found a direct correlation between the lipids surface concentration and the wetting ability for the 25 powders studied.

  16. Controlled synthesis and photocatalytic properties of rhombic dodecahedral Ag3PO4 with high surface energy

    International Nuclear Information System (INIS)

    Xie, Yao; Huang, Zhaohui; Zhang, Zhijie; Zhang, Xiaoguang; Wen, Ruilong; Liu, Yangai; Fang, Minghao; Wu, Xiaowen


    Graphical abstract: The high amount of rhombic dodecahedral Ag 3 PO 4 particles with a high exposure of the {110} facets and high surface energy (the surface energy of the {110} facets was 1.31 J/m 2 , greater than that of the {100} facet (1.12 J/m 2 ).) exhibited excellent photocatalytic activity. - Highlights: • High contents of rhombic dodecahedral Ag 3 PO 4 photocatalysts are prepared. • Excessive EG can destroy the morphology of Ag 3 PO 4 in synthesis process. • The rhombic dodecahedral Ag 3 PO 4 exhibits high surface energy. • High surface energy implies high photocatalytic activity. - Abstract: In this study, a series of Ag 3 PO 4 photocatalysts with different contents of rhombic dodecahedral particles were prepared in one pot by a facile, novel hydrothermal method using ethylene glycol (EG), which served as both a morphology modifier and reducing agent. The effects of EG content on the morphologies of Ag 3 PO 4 photocatalysts were discussed. The photocatalytic activity of the Ag 3 PO 4 photocatalysts was evaluated by the degradation of methylene blue trihydrate under visible-light irradiation. With the use of 0.8% EG in the reaction solvent, the sample exhibited excellent photocatalytic activity, attributed to the high amount of rhombic dodecahedral Ag 3 PO 4 particles with a high exposure of the {110} facets and high surface energy. The surface energy of the {110} facets was 1.31 J/m 2 , greater than that of the {100} facet (1.12 J/m 2 ). However, with 1% EG in the reaction solvent, although the Ag 3 PO 4 photocatalysts were composed of a majority of rhombic dodecahedral Ag 3 PO 4 particles, tiny Ag particles formed from Ag + under the action of EG attached on the surface of the sample decreased the absorption of visible light, resulting in low photocatalytic activity.

  17. High Voltage Surface Degradation on Carbon Blacks in Lithium Ion Batteries

    DEFF Research Database (Denmark)

    Younesi, Reza

    In order to increase the power density of Li-ion batteries, much research is focused on developing cathode materials that can operate at high voltages above 4.5 V with a high capacity, high cycling stability, and rate capability. However, at high voltages all the components of positive electrodes...... including carbon black (CB) additives have a potential risk of degradation. Though the weight percentage of CB in commercial batteries is generally very small, the volumetric amount and thus the surface area of CB compose a rather large part of a cathode due to its small particle size (≈ 50 nm) and high...... surface area. In this work, the performance of Super P in Li-ion cells at high voltages up to 4.9 V is studied using electrochemical measurements as well as surface characterizations....

  18. Role of high resolution optical coherence tomography in diagnosing ocular surface squamous neoplasia with coexisting ocular surface diseases. (United States)

    Atallah, Marwan; Joag, Madhura; Galor, Anat; Amescua, Guillermo; Nanji, Afshan; Wang, Jianhua; Perez, Victor L; Dubovy, Sander; Karp, Carol L


    Coexistence of an ocular surface disease can mask the typical features of ocular surface squamous neoplasia (OSSN). The purpose of this study was to evaluate high resolution optical coherence tomography (HR-OCT) as an adjunct in the detection and differentiation of OSSN within coexisting ocular surface pathologies. Retrospective study of 16 patients with ocular surface disease and lesions suspicious for OSSN that were evaluated with HR-OCT. HR-OCT images of the lesions were taken to look for evidence of OSSN. Biopsies were performed in all cases, and the HR-OCT findings were compared to the histological results. Of the 16 patients with OSSN and a coexisting ocular surface disease, 12 were found to have OSSN by HR-OCT and all were subsequently confirmed by biopsy. Two patients had OSSN with rosacea, one with pingueculum, two within pterygia, one with Salzmann' nodular degeneration, six with limbal stem cell deficiency (LSCD)/scarring. In all 12 cases HR-OCT images revealed classical findings of hyper-reflective, thickened epithelium and an abrupt transition from normal to abnormal epithelium. OSSN was ruled out by HR-OCT in four cases (2 Salzmann's, 1 mucous membrane pemphigoid, and 1 LSCD). Negative findings were confirmed by biopsy. HR-OCT was used to follow resolution of the OSSN in positive cases, and it detected recurrence in 1 case. While histopathology is the gold standard in the diagnosis of OSSN, HR-OCT can be used to noninvasively detect the presence of OSSN in patients with coexisting ocular conditions. Copyright © 2017 Elsevier Inc. All rights reserved.

  19. Unique lift-off of droplet impact on high temperature nanotube surfaces (United States)

    Tong, Wei; Qiu, Lu; Jin, Jian; Sun, Lidong; Duan, Fei


    A unique liquid film lift-off during a falling water droplet impacting on a heated titanium oxide nanotube surface has been experimentally revealed through a high speed visualization system. It is suggested that the Leidenfrost point on the nanotube surface has been significantly delayed, as compared to that on the bare titanium surface. Such delay is inferred to be a result of the increase in the surface wettability and the capillary effect by the nanoscale tube structure. By measuring the liquid lift-off distance from the substrate surface, a droplet lift-off is typically divided into four stages, namely, first contact, first lift-off, second contact, and second lift-off. The residence time at each stage is quantitatively evaluated. As the surface temperature increases, the duration time is significantly reduced for both the first contact and the first lift-off stages.

  20. Near-surface modifications for improved crack tolerant behavior of high strength alloys: trends and prospects

    International Nuclear Information System (INIS)

    Hettche, L.R.; Rath, B.B.


    The purpose of this chapter is to examine the potential of surface modifications in improving the crack tolerant behavior of high strength alloys. Provides a critique of two of the most promising and versatile techniques: ion implantation and laser beam surface processing. Discusses crack tolerant properties; engineering characterization; publication trends and Department of Defense interests; and emergent surface modification techniques. Finds that the efficiency with which high strength alloys can be incorporated into a structure or component is dependent on the following crack tolerant properties: fracture toughness, fatigue resistance, sustained loading cracking resistance, fretting fatigue resistance, and hydrogen embrittlement resistance. Concludes that ion implantation and laser surface processing coupled with other advanced metallurgical procedures and fracture mechanic analyses provide the means to optimize both the bulk and surface controlled crack tolerant properties

  1. X-ray emission in slow highly charged ion-surface collisions

    International Nuclear Information System (INIS)

    Watanabe, H; Abe, T; Fujita, Y; Sun, J; Takahashi, S; Tona, M; Yoshiyasu, N; Nakamura, N; Sakurai, M; Yamada, C; Ohtani, S


    X-rays emitted in the collisions of highly charged ions with a surface have been measured to investigate dissipation schemes of their potential energies. While 8.1% of the potential energy was dissipated in the collisions of He-like I ions with a W surface, 29.1% has been dissipated in the case of He-like Bi ions. The x-ray emissions play significant roles in the dissipation of the potential energies in the interaction of highly charged heavy ions with the surface

  2. Experimental study on surface properties of the PMMA used in high power spark gaps (United States)

    Han, Ruoyu; Wu, Jiawei; Ding, Weidong; Liu, Yunfei; Gou, Yang


    This paper studies the surface properties of the Polymethylmethacrylate (PMMA) insulator samples used in high power spark gaps. Experiments on surface morphology, surface profile, surface chemical composition and surface leakage current were performed. Metal particles ejected in tangent direction of discharge spots were researched on the sample surface. Three kinds of distinct bands were found on the surface after 1500 shots: colorless and transparent sinking band, black band, and grey powdered coating band. The thickness of the coating band was tens of microns and the maximum radial erosion rate was about 10 μm/C. Surface content analysis indicated that the powdered coating was a mixture of decomposed insulator material and electrode material oxides. In addition, leakage current significantly depended on water content in the chamber and presented an U-shape curve distribution along the insulator surface, in keeping with the amount of powdered coating due to shock waves. Possible reasons of the surface property changes were discussed. Electroconductive oxides of low valence states of Cu and W produced by the reactions between electrode materials and arc plasmas were considered to be the cause of dielectric performance degradation.

  3. The assessment of elastic follow-up in high temperature piping systems - overall survey and theoretical aspects

    International Nuclear Information System (INIS)

    Boyle, J.T.; Nakamura, K.


    A review in some detail is presented, of simple and approximate methods for the assessment of elastic follow-up, to suggest possible modifications to the available methods to make them more appropriate for design purposes and to present a possible route for design based on simplified methods. An overall survey is given and the theoretical aspects of the various methods described in detail. In the second part of this paper these methods are compared to more exact solutions obtained by finite element analysis for a number of simple piping configurations subject to creep. (author)

  4. Highly Sensitive Local Surface Plasmon Resonance in Anisotropic Au Nanoparticles Deposited on Nanofibers

    Directory of Open Access Journals (Sweden)

    Masanari Saigusa


    Full Text Available This paper reports the facile and high-throughput fabrication method of anisotropic Au nanoparticles with a highly sensitive local surface plasmon resonance (LPR using cylindrical nanofibers as substrates. The substrates consisting of nanofibers were prepared by the electrospinning of poly(vinylidene fluoride (PVDF. The Au nanoparticles were deposited on the surface of electrospun nanofibers by vacuum evaporation. Scanning electron microscopy revealed the formation of a curved Au island structure on the surface of cylindrical nanofibers. Polarized UV-visible extinction spectroscopy showed anisotropy in their LPR arising from the high surface curvature of the nanofiber. The LPR of the Au nanoparticles on the thinnest nanofiber with a diameter of ~100 nm showed maximum refractive index (RI sensitivity over 500 nm/RI unit (RIU. The close correlation between the fiber diameter dependence of the RI sensitivity and polarization dependence of the LPR suggests that anisotropic Au nanoparticles improve RI sensitivity.

  5. Effect of Process Parameters on Flow Length and Flash Formation in Injection Moulding of High Aspect Ratio Polymeric Micro Features

    Directory of Open Access Journals (Sweden)

    Abdelkhalik Eladl


    Full Text Available This paper reports an investigation of the effects of process parameters on the quality characteristics of polymeric parts produced by micro injection moulding (μIM with two different materials. Four injection moulding process parameters (injection velocity, holding pressure, melt temperature and mould temperature were investigated using Polypropylene (PP and Acrylonitrile Butadiene Styrene (ABS. Three key characteristics of the mouldings were evaluated with respect to process settings and the material employed: part mass, flow length and flash formation. The experimentation employs a test part with four micro fingers with different aspect ratios (from 21 up to 150 and was carried out according to the Design of Experiments (DOE statistical technique. The results show that holding pressure and injection velocity are the most influential parameters on part mass with a direct effect for both materials. Both parameters have a similar effect on flow length for both PP and ABS at all aspect ratios and have higher effects as the feature thickness decreased below 300 μm. The study shows that for the investigated materials the injection speed and packing pressure were the most influential parameters for increasing the amount of flash formation, with relative effects consistent for both materials. Higher melt and mould temperatures settings were less influential parameters for increasing the flash amount when moulding with both materials. Of the two investigated materials, PP was the one exhibiting more flash formation as compared with ABS, when corresponding injection moulding parameters settings for both materials were considered.

  6. Experimental High-Resolution Land Surface Prediction System for the Vancouver 2010 Winter Olympic Games (United States)

    Belair, S.; Bernier, N.; Tong, L.; Mailhot, J.


    The 2010 Winter Olympic and Paralympic Games will take place in Vancouver, Canada, from 12 to 28 February 2010 and from 12 to 21 March 2010, respectively. In order to provide the best possible guidance achievable with current state-of-the-art science and technology, Environment Canada is currently setting up an experimental numerical prediction system for these special events. This system consists of a 1-km limited-area atmospheric model that will be integrated for 16h, twice a day, with improved microphysics compared with the system currently operational at the Canadian Meteorological Centre. In addition, several new and original tools will be used to adapt and refine predictions near and at the surface. Very high-resolution two-dimensional surface systems, with 100-m and 20-m grid size, will cover the Vancouver Olympic area. Using adaptation methods to improve the forcing from the lower-resolution atmospheric models, these 2D surface models better represent surface processes, and thus lead to better predictions of snow conditions and near-surface air temperature. Based on a similar strategy, a single-point model will be implemented to better predict surface characteristics at each station of an observing network especially installed for the 2010 events. The main advantage of this single-point system is that surface observations are used as forcing for the land surface models, and can even be assimilated (although this is not expected in the first version of this new tool) to improve initial conditions of surface variables such as snow depth and surface temperatures. Another adaptation tool, based on 2D stationnary solutions of a simple dynamical system, will be used to produce near-surface winds on the 100-m grid, coherent with the high- resolution orography. The configuration of the experimental numerical prediction system will be presented at the conference, together with preliminary results for winter 2007-2008.

  7. Single ion induced surface nanostructures: a comparison between slow highly charged and swift heavy ions. (United States)

    Aumayr, Friedrich; Facsko, Stefan; El-Said, Ayman S; Trautmann, Christina; Schleberger, Marika


    This topical review focuses on recent advances in the understanding of the formation of surface nanostructures, an intriguing phenomenon in ion-surface interaction due to the impact of individual ions. In many solid targets, swift heavy ions produce narrow cylindrical tracks accompanied by the formation of a surface nanostructure. More recently, a similar nanometric surface effect has been revealed for the impact of individual, very slow but highly charged ions. While swift ions transfer their large kinetic energy to the target via ionization and electronic excitation processes (electronic stopping), slow highly charged ions produce surface structures due to potential energy deposited at the top surface layers. Despite the differences in primary excitation, the similarity between the nanostructures is striking and strongly points to a common mechanism related to the energy transfer from the electronic to the lattice system of the target. A comparison of surface structures induced by swift heavy ions and slow highly charged ions provides a valuable insight to better understand the formation mechanisms. © 2011 IOP Publishing Ltd

  8. High-resolution hot-film measurement of surface heat flux to an impinging jet (United States)

    O'Donovan, T. S.; Persoons, T.; Murray, D. B.


    To investigate the complex coupling between surface heat transfer and local fluid velocity in convective heat transfer, advanced techniques are required to measure the surface heat flux at high spatial and temporal resolution. Several established flow velocity techniques such as laser Doppler anemometry, particle image velocimetry and hot wire anemometry can measure fluid velocities at high spatial resolution (µm) and have a high-frequency response (up to 100 kHz) characteristic. Equivalent advanced surface heat transfer measurement techniques, however, are not available; even the latest advances in high speed thermal imaging do not offer equivalent data capture rates. The current research presents a method of measuring point surface heat flux with a hot film that is flush mounted on a heated flat surface. The film works in conjunction with a constant temperature anemometer which has a bandwidth of 100 kHz. The bandwidth of this technique therefore is likely to be in excess of more established surface heat flux measurement techniques. Although the frequency response of the sensor is not reported here, it is expected to be significantly less than 100 kHz due to its physical size and capacitance. To demonstrate the efficacy of the technique, a cooling impinging air jet is directed at the heated surface, and the power required to maintain the hot-film temperature is related to the local heat flux to the fluid air flow. The technique is validated experimentally using a more established surface heat flux measurement technique. The thermal performance of the sensor is also investigated numerically. It has been shown that, with some limitations, the measurement technique accurately measures the surface heat transfer to an impinging air jet with improved spatial resolution for a wide range of experimental parameters.

  9. Physics-aspects of dose accuracy in high dose rate (HDR) brachytherapy: Source dosimetry, treatment planning, equipment performance and in vivo verification techniques


    Palmer, A; Bradley, D; Nisbet, A


    This study provides a review of recent publications on the physics-aspects of dosimetric accuracy in high dose rate (HDR) brachytherapy. The discussion of accuracy is primarily concerned with uncertainties, but methods to improve dose conformation to the prescribed intended dose distribution are also noted. The main aim of the paper is to review current practical techniques and methods employed for HDR brachytherapy dosimetry. This includes work on the determination of dose rate fields around...

  10. Synthetic microfluidic paper: high surface area and high porosity polymer micropillar arrays. (United States)

    Hansson, Jonas; Yasuga, Hiroki; Haraldsson, Tommy; van der Wijngaart, Wouter


    We introduce Synthetic Microfluidic Paper, a novel porous material for microfluidic applications that consists of an OSTE polymer that is photostructured in a well-controlled geometry of slanted and interlocked micropillars. We demonstrate the distinct benefits of Synthetic Microfluidic Paper over other porous microfluidic materials, such as nitrocellulose, traditional paper and straight micropillar arrays: in contrast to straight micropillar arrays, the geometry of Synthetic Microfluidic Paper was miniaturized without suffering capillary collapse during manufacturing and fluidic operation, resulting in a six-fold increased internal surface area and a three-fold increased porous fraction. Compared to commercial nitrocellulose materials for capillary assays, Synthetic Microfluidic Paper shows a wider range of capillary pumping speed and four times lower device-to-device variation. Compared to the surfaces of the other porous microfluidic materials that are modified by adsorption, Synthetic Microfluidic Paper contains free thiol groups and has been shown to be suitable for covalent surface chemistry, demonstrated here for increasing the material hydrophilicity. These results illustrate the potential of Synthetic Microfluidic Paper as a porous microfluidic material with improved performance characteristics, especially for bioassay applications such as diagnostic tests.

  11. Various categories of defects after surface alloying induced by high current pulsed electron beam irradiation

    International Nuclear Information System (INIS)

    Luo, Dian; Tang, Guangze; Ma, Xinxin; Gu, Le; Sun, Mingren; Wang, Liqin


    Highlights: • Four kinds of defects are found during surface alloying by high current electron beam. • Exploring the mechanism how these defects appear after irradiation. • Increasing pulsing cycles will help to get good surface quality. • Choosing proper energy density will increase surface quality. - Abstract: High current pulsed electron beam (HCPEB) is an attractive advanced materials processing method which could highly increase the mechanical properties and corrosion resistance. However, how to eliminate different kinds of defects during irradiation by HCPEB especially in condition of adding new elements is a challenging task. In the present research, the titanium and TaNb-TiW composite films was deposited on the carburizing steel (SAE9310 steel) by DC magnetron sputtering before irradiation. The process of surface alloying was induced by HCPEB with pulse duration of 2.5 μs and energy density ranging from 3 to 9 J/cm 2 . Investigation of the microstructure indicated that there were several forms of defects after irradiation, such as surface unwetting, surface eruption, micro-cracks and layering. How the defects formed was explained by the results of electron microscopy and energy dispersive spectroscopy. The results also revealed that proper energy density (∼6 J/cm 2 ) and multi-number of irradiation (≥50 times) contributed to high quality of alloyed layers after irradiation

  12. [Morphology of cracks in enamel surface produced experimentally using high and low temperature]. (United States)

    Suárez Quintanilla, J; Segade, L A; González Bahillo, J


    A scanning electron microscope study was made to study the morphological changes in the human enamel surface produced by low and high temperatures. Cracked dental enamel was observed when the teeth were exposed at low and high temperatures. When the time of exposition was increased, there are more enamel cracks which may be considered as enamel fractures.

  13. Zooplankton incidence in abnormally high sea surface temperature in the Eastern Arabian Sea

    Digital Repository Service at National Institute of Oceanography (India)

    Goswami, S.C.

    and internal waves may cause zooplankton abundance. Average biomass values in high sea surface temperature areas were higher (0.30 ml.m/3) than at the other stations (0.07 ml.m/3). Crustacean eggs, fish eggs and mysids clustered in pockets of abnormally high...

  14. Study on the surface constitute properties of high-speed end milling aluminum alloy (United States)

    Huang, Xiaoming; Li, Hongwei; Yumeng, Ma


    The physical and mechanical properties of the metal surface will change after the metal cutting processing. The comprehensive study of the influence of machining parameters on surface constitute properties are necessary. A high-speed milling experiment by means of orthogonal method with four factors was conducted for aluminum alloy7050-T7451. The surface constitutive properties of the Al-Alloy surface were measured using SSM-B4000TM stress-strain microprobe system. Based on all the load-depth curves obtained, the characteristics parameters such as strain hardening exponent n and yield strength σy of the milling surface are calculated. The effect of cutting speed, feed rate, and width and depth of cut on n and σy was investigated using the ANOVA techniques. The affecting degree of milling parameters on n and σy was v>fz> ap < ae. The influence of milling parameters on n and σ y was described and discussed.

  15. Lubricant-infused micro/nano-structured surfaces with tunable dynamic omniphobicity at high temperatures (United States)

    Daniel, Daniel; Mankin, Max N.; Belisle, Rebecca A.; Wong, Tak-Sing; Aizenberg, Joanna


    Omniphobic surfaces that can repel fluids at temperatures higher than 100 °C are rare. Most state-of-the-art liquid-repellent materials are based on the lotus effect, where a thin air layer is maintained throughout micro/nanotextures leading to high mobility of liquids. However, such behavior eventually fails at elevated temperatures when the surface tension of test liquids decreases significantly. Here, we demonstrate a class of lubricant-infused structured surfaces that can maintain a robust omniphobic state even for low-surface-tension liquids at temperatures up to at least 200 °C. We also demonstrate how liquid mobility on such surfaces can be tuned by a factor of 1000.

  16. Lubricant-infused micro/nano-structured surfaces with tunable dynamic omniphobicity at high temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Daniel, D; Mankin, MN; Belisle, RA; Wong, TS; Aizenberg, J


    Omniphobic surfaces that can repel fluids at temperatures higher than 100 degrees C are rare. Most state-of-the-art liquid-repellent materials are based on the lotus effect, where a thin air layer is maintained throughout micro/nanotextures leading to high mobility of liquids. However, such behavior eventually fails at elevated temperatures when the surface tension of test liquids decreases significantly. Here, we demonstrate a class of lubricant-infused structured surfaces that can maintain a robust omniphobic state even for low-surface-tension liquids at temperatures up to at least 200 degrees C. We also demonstrate how liquid mobility on such surfaces can be tuned by a factor of 1000. (C) 2013 Author(s).

  17. A Pulse Power Modulator System for Commercial High Power Ion Beam Surface Treatment Applications

    International Nuclear Information System (INIS)

    Barrett, D.M.; Cockreham, B.D.; Dragt, A.J.; Ives, H.C.; Neau, E.L.; Reed, K.W.; White, F.E.


    The Ion Beam Surface Treatment (lBESTrM) process utilizes high energy pulsed ion beams to deposit energy onto the surface of a material allowing near instantaneous melting of the surface layer. The melted layer typically re-solidifies at a very rapid rate which forms a homogeneous, fine- grained structure on the surface of the material resulting in significantly improved surface characteristics. In order to commercialize the IBESTTM process, a reliable and easy-to-operate modulator system has been developed. The QM-I modulator is a thyratron-switched five-stage magnetic pulse compression network which drives a two-stage linear induction adder. The adder provides 400 kV, 150 ns FWHM pulses at a maximum repetition rate of 10 pps for the acceleration of the ion beam. Special emphasis has been placed upon developing the modulator system to be consistent with long-life commercial service

  18. Field emission and high voltage cleaning of particulate contaminants on extended metallic surfaces

    International Nuclear Information System (INIS)

    Tan, J.; Bonin, B.; Safa, H.


    The vacuum insulation properties of extended metallic surfaces depends strongly on their cleanliness. The usual technique to reduce electronic field emission from such surfaces consists in exposing them to very high electric fields during limited periods of time. This kind of processing also reduces the occurrence of vacuum breakdown. The processing of the surface is generally believed to be due to a thermomechanical destruction of the emitting sites, initiated by the emission itself. Comparison of the electric forces vs adherence forces which act on dust particles lying on the surface shows that the processing could also be due simply to the mechanical removal of the dust particles, with a subsequent reduction of field emission from the contaminated surface. (author)

  19. High-Performance Stretchable Conductive Composite Fibers from Surface-Modified Silver Nanowires and Thermoplastic Polyurethane by Wet Spinning. (United States)

    Lu, Ying; Jiang, Jianwei; Yoon, Sungho; Kim, Kyung-Shik; Kim, Jae-Hyun; Park, Sanghyuk; Kim, Sang-Ho; Piao, Longhai


    Highly stretchable and conductive fibers have attracted great interest as a fundamental building block for the next generation of textile-based electronics. Because of its high conductivity and high aspect ratio, the Ag nanowire (AgNW) has been considered one of the most promising conducting materials for the percolation network-based conductive films and composites. However, the poor dispersibility of AgNWs in hydrophobic polymers has hindered their application to stretchable conductive composite fibers. In this paper, we present a highly stretchable and conductive composite fiber from the co-spinning of surface-modified AgNWs and thermoplastic polyurethane (PU). The surface modification of AgNWs with a polyethylene glycol derivative improved the compatibility of PU and AgNWs, which allowed the NWs to disperse homogeneously in the elastomeric matrix, forming effective percolation networks and causing the composite fiber to show enhanced electrical and mechanical performance. The maximum AgNW mass fraction in the composite fiber was 75.9 wt %, and its initial electrical conductivity was as high as 14 205 S/cm. The composite fibers also exhibited superior stretchability: the maximum rupture strain of the composite fiber with 14.6 wt % AgNW was 786%, and the composite fiber was also conductive even when it was stretched up to 200%. In addition, 2-dimensional (2-D) Ag nanoplates were added to the AgNW/PU composite fibers to increase the stability of the conductive network under repeated stretching and releasing. The Ag nanoplates acted as a bridge to effectively prevent the AgNWs from slippage and greatly improved the stability of the conductive network.

  20. Automated calculation of surface energy fluxes with high-frequency lake buoy data (United States)

    Woolway, R. Iestyn; Jones, Ian D; Hamilton, David P.; Maberly, Stephen C; Muroaka, Kohji; Read, Jordan S.; Smyth, Robyn L; Winslow, Luke A.


    Lake Heat Flux Analyzer is a program used for calculating the surface energy fluxes in lakes according to established literature methodologies. The program was developed in MATLAB for the rapid analysis of high-frequency data from instrumented lake buoys in support of the emerging field of aquatic sensor network science. To calculate the surface energy fluxes, the program requires a number of input variables, such as air and water temperature, relative humidity, wind speed, and short-wave radiation. Available outputs for Lake Heat Flux Analyzer include the surface fluxes of momentum, sensible heat and latent heat and their corresponding transfer coefficients, incoming and outgoing long-wave radiation. Lake Heat Flux Analyzer is open source and can be used to process data from multiple lakes rapidly. It provides a means of calculating the surface fluxes using a consistent method, thereby facilitating global comparisons of high-frequency data from lake buoys.