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Sample records for surface analysis lsa

  1. Meteosat SEVIRI Fire Radiative Power (FRP) products from the Land Surface Analysis Satellite Applications Facility (LSA SAF) - Part 1: Algorithms, product contents and analysis

    Science.gov (United States)

    Wooster, M. J.; Roberts, G.; Freeborn, P. H.; Xu, W.; Govaerts, Y.; Beeby, R.; He, J.; Lattanzio, A.; Mullen, R.

    2015-06-01

    Characterising changes in landscape scale fire activity at very high temporal resolution is best achieved using thermal observations of actively burning fires made from geostationary Earth observation (EO) satellites. Over the last decade or more, a series of research and/or operational "active fire" products have been developed from these types of geostationary observations, often with the aim of supporting the generation of data related to biomass burning fuel consumption and trace gas and aerosol emission fields. The Fire Radiative Power (FRP) products generated by the Land Surface Analysis Satellite Applications Facility (LSA SAF) from data collected by the Meteosat Second Generation (MSG) Spinning Enhanced Visible and Infrared Imager (SEVIRI) are one such set of products, and are freely available in both near real-time and archived form. Every 15 min, the algorithms used to generate these products identify and map the location of new SEVIRI observations containing actively burning fires, and characterise their individual rates of radiative energy release (fire radiative power; FRP) that is believed proportional to rates of biomass consumption and smoke emission. The FRP-PIXEL product contains the highest spatial resolution FRP dataset, delivered for all of Europe, northern and southern Africa, and part of South America at a spatial resolution of 3 km (decreasing away from the west African sub-satellite point) at the full 15 min temporal resolution. The FRP-GRID product is an hourly summary of the FRP-PIXEL data, produced at a 5° grid cell size and including simple bias adjustments for meteorological cloud cover and for the regional underestimation of FRP caused, primarily, by the non-detection of low FRP fire pixels at SEVIRI's relatively coarse pixel size. Here we describe the enhanced geostationary Fire Thermal Anomaly (FTA) algorithm used to detect the SEVIRI active fire pixels, and detail methods used to deliver atmospherically corrected FRP information

  2. INTEGRASI PERINGKAS DOKUMEN OTOMATIS DENGAN ALGORITMA LATENT SEMANTIC ANALYSIS (LSA PADA PERINGKAS DOKUMEN OTOMATIS UNTUK PROSES CLUSTERING DOKUMEN

    Directory of Open Access Journals (Sweden)

    Ardytha Luthfiarta

    2014-08-01

    Full Text Available Teknologi pengklasteran dokumen memiliki peran yang signifkan dalam kemajuan teknologi informasi, diantaranya mempunyai peranan penting dalam pengembangan web  di bidang akurasi kategorisasi keyword otomatis pada search engine, kategorisasi berita untuk surat kabar elektronik,  peningkatan rating situs dengan teknologi Search Engine Optimization (SEO dan sangat memungkinkan untuk diimplementasikan dalam berbagai teknologi informasi lainnya, oleh karena  itu diperlukan penelitian untuk meningkatkan ketepatan akurasi dalam pengklasteran dokumen. Dalam penelitian ini Algoritma Latent Semantic Analysis (LSA dapat melakukan proses reduksi kalimat dengan lebih baik dibandingkan algoritma Feature Based sehingga mendapatkan hasil akurasi proses clustering dokumen yang lebih akurat. Beberapa tahapan clustering dalam penelitian ini, yaitu preprocessing, peringkas dokumen otomatis dengan metode fitur, peringkas dokumen otomatis dengan LSA, pembobotan kata, dan algoritma clustering. Hasil penelitian menunjukkan tingkat akurasi menggunakan peringkas dokumen otomatis dengan LSA dalam proses clustering dokumen mencapai 71,04 % yang diperoleh pada tingkat peringkas dokumen otomatis dengan LSA 40% dibandingkan dengan hasil clustering tanpa peringkas dokumen otomatis yang hanya mencapai tingkat akurasi 65,97 %. Kata kunci: Text Mining, Clustering, Peringkas Dokumen Otomatis, LSA.

  3. Preliminary Design of a LSA Aircraft Using Wind Tunnel Tests

    Directory of Open Access Journals (Sweden)

    Norbert ANGI

    2015-12-01

    Full Text Available This paper presents preliminary results concerning the design and aerodynamic calculations of a light sport aircraft (LSA. These were performed for a new lightweight, low cost, low fuel consumption and long-range aircraft. The design process was based on specific software tools as Advanced Aircraft Analysis (AAA, XFlr 5 aerodynamic and dynamic stability analysis, and Catia design, according to CS-LSA requirements. The calculations were accomplished by a series of tests performed in the wind tunnel in order to assess experimentally the aerodynamic characteristics of the airplane.

  4. Assessment of the EUMETSAT LSA-SAF evapotranspiration product for drought monitoring in Europe

    Science.gov (United States)

    Sepulcre-Canto, Guadalupe; Vogt, Jürgen; Arboleda, Alirio; Antofie, Tiberiu

    2014-08-01

    Evapotranspiration is a key parameter for water stress assessment as it is directly related to the moisture status of the soil-vegetation system and describes the moisture transfer from the surface to the atmosphere. With the launch of the Meteosat Second Generation geostationary satellites and the setup of the Satellite Application Facilities, it became possible to operationally produce evapotranspiration data with high spatial and temporal evolution over the entire continents of Europe and Africa. In the frame of this study we present an evaluation of the potential of the evapotranspiration (ET) product from the EUMETSAT Satellite Application Facility on Land Surface Analysis (LSA-SAF) for drought assessment and monitoring in Europe. To assess the potential of this product, the LSA-SAF ET was used as input for the ratio of ET to reference evapotranspiration (ET0), the latter estimated from the ECMWF interim reanalysis. In the analysis two case studies were considered corresponding to the drought episodes of spring/summer 2007 and 2011. For these case studies, the ratio ET/ET0 was compared with meteorological drought indices (SPI, SPEI and Sc-PDSI for 2007 and SPI for 2011) as well as with the anomalies of the fraction of absorbed photosynthetic active radiation (fAPAR) derived from remote sensing data. The meteorological and remote sensing indicators were taken from the European Drought Observatory (EDO) and the CARPATCLIM climatological atlas. Results show the potential of ET/ET0 to characterize soil moisture variability, and to give additional information to fAPAR and to precipitation distribution for drought assessment. The main limitations of the proposed ratio for drought characterization are discussed, including options to overcome them. These options include the use of filters to discriminate areas with a low percentage vegetation cover or areas that are not in their growing period and the use of evapotranspiration without water restriction (ETwwr

  5. Technology transfer - LSA project to industry

    Science.gov (United States)

    Gallagher, B. D.

    1981-01-01

    Program goals, procedural steps, and examples of different situations encountered in the Low-cost Solar Array (LSA) project managed at the Jet Propulsion Laboratory in conjunction with industrial contractors are outlined. The project is intended to result in the production-ready status of photovoltaic panels which produce power at $.70/peak W by 1986. The first phase of the program identified materials and processes which were promising for further development. Phase II served to correct steps and materials which did not work and were important to the array processing. The third phase will bring the processes to technical readiness by demonstration of successful fabrication of modules at a scale which can be increased to commercial production. An information exchange is ongoing between manufacturers and the JPL to alter specific steps which yield results which vary from those found in the laboratory when transferred to the factory.

  6. Nuclear regulatory review of licensee self-assessment (LSA)

    International Nuclear Information System (INIS)

    2003-01-01

    Licensee self-assessment (LSA) by nuclear power plant operators is described as all the activities that a licensee performs in order to identify opportunities for improvements. An LSA is part of an organisation's holistic management system, which must include other process elements. Particularly important elements are: a process for choosing which identified potential improvements should be implemented and a process of project management for implementing the improvements chosen. Nuclear regulators expect the licensee to run an effective LSA programme, which reflects the licensee's 'priority to safety'. Based on contributions from members of the NEA Committee on Nuclear Regulatory Activities (CNRA), this publication provides an overview of the current regulatory philosophy on and approaches to LSA as performed by licensees. The publication's intended audience is primarily nuclear safety regulators, but government authorities, nuclear power plant operators and the general public may also be interested. (author)

  7. Adaptive Self-Occlusion Behavior Recognition Based on pLSA

    Directory of Open Access Journals (Sweden)

    Hong-bin Tu

    2013-01-01

    Full Text Available Human action recognition is an important area of human action recognition research. Focusing on the problem of self-occlusion in the field of human action recognition, a new adaptive occlusion state behavior recognition approach was presented based on Markov random field and probabilistic Latent Semantic Analysis (pLSA. Firstly, the Markov random field was used to represent the occlusion relationship between human body parts in terms an occlusion state variable by phase space obtained. Then, we proposed a hierarchical area variety model. Finally, we use the topic model of pLSA to recognize the human behavior. Experiments were performed on the KTH, Weizmann, and Humaneva dataset to test and evaluate the proposed method. The compared experiment results showed that what the proposed method can achieve was more effective than the compared methods.

  8. LSA glass-ceramic tiles made by powder pressing

    International Nuclear Information System (INIS)

    Figueira, F.C.; Bertan, F.M.; Riella, H.G.; Uggioni, E.; Bernardin, A.M.

    2009-01-01

    A low cost alternative for the production of glass-ceramic materials is the pressing of the matrix glass powders and its consolidation simultaneously with crystallization in a single stage of sintering. The main objective of this work was to obtain LSA glass ceramics with low thermal expansion, processed by pressing and sintering a ceramic frit powder. The raw materials were homogenized and melted (1480 deg C, 80min), and the melt was poured in water. The glass was chemically (XRF and AAS) and thermally (DTA, 10 deg C/min, air) characterized, and then ground (60min and 120min). The ground powders were characterized (laser diffraction) and compressed (35MPa and 45MPa), thus forming four systems. The compacts were dried (150 deg C, 24h) and sintered (1175 deg C and 1185 deg C, 10 deg C/min). Finally, the glass-ceramics were characterized by microstructural analysis (SEM and XRD), mechanical behavior (σbending) and thermal analysis (α). The best results for thermal expansion were those for the glass-ceramics processed with smaller particle size and greater compaction pressure. (author)

  9. Pain Expression Recognition Based on pLSA Model

    Directory of Open Access Journals (Sweden)

    Shaoping Zhu

    2014-01-01

    Full Text Available We present a new approach to automatically recognize the pain expression from video sequences, which categorize pain as 4 levels: “no pain,” “slight pain,” “moderate pain,” and “ severe pain.” First of all, facial velocity information, which is used to characterize pain, is determined using optical flow technique. Then visual words based on facial velocity are used to represent pain expression using bag of words. Final pLSA model is used for pain expression recognition, in order to improve the recognition accuracy, the class label information was used for the learning of the pLSA model. Experiments were performed on a pain expression dataset built by ourselves to test and evaluate the proposed method, the experiment results show that the average recognition accuracy is over 92%, which validates its effectiveness.

  10. Correlation of serum biomarkers (TSA & LSA) and epithelial dysplasia in early diagnosis of oral precancer and oral cancer.

    Science.gov (United States)

    Sawhney, Hemant; Kumar, C Anand

    Oral cancer is currently the most frequent cause of cancer-related deaths, which is usually preceded by oral pre-cancerous lesions and conditions. Altered glycosylation of glycoconjugates, such as sialic acid, fucose, etc. are amongst the important molecular changes that accompany malignant transformation. The purpose of our study was to evaluate usefulness of serum Total Sialic Acid (TSA) and serum Lipid-Bound Sialic Acid (LSA) as markers of oral precancerous lesions and histopathologically correlating them with grades of epithelial dysplasia. Blood samples were collected from 50 patients with oral precancer (Leukoplakia & OSMF), 25 patients with untreated oral cancer and 25 healthy subjects. Serum sialic acid (total and lipid bound) levels were measured spectrophotometrically. Tissue samples from all the patients were evaluated for dysplasia. Serum levels of total and lipid bound sialic acid were significantly elevated in patients with oral precancer and cancer when compared with healthy subjects. Analysis of variance test documented that there is progressive rise in serum levels of sialic acid with the degree of dysplastic changes in oral precancer patients. We observed positive correlation between serum levels of the markers and the extent of malignant disease (TNM Clinical staging) as well as histopathological grades. The results suggested that serum levels of TSA and LSA progressively increases with grades of dysplasia in precancerous groups and cancer group, when compared with healthy controls. These glycoconjugates, especially LSA has the clinical utility in indicating a premalignant change.

  11. Uncertainties, confidence ellipsoids and security polytopes in LSA

    Science.gov (United States)

    Grabe, Michael

    1992-05-01

    For a given error model, the uncertainties of and the couplings between parameters estimated by a least-squares adjustment (LSA) are formalized. The error model is restricted to normally distributed random errors and to systematic errors that remain constant during measurement, but whose magnitudes and signs are unknown. An outline of the associated, new formalism for estimating measurement uncertainties is sketched as regards its function as a measure of the consistency between theory and experiment. The couplings due to random errors lead to ellipsoids stemming from singular linear mappings of Hotelling's ellipsoids. Those introduced by systematic errors create convex polytopes, so-called security polytopes, which are singular linear mappings of hyperblocks caused by a ldworst-case treatment” of systematic errors.

  12. From analysis to surface

    DEFF Research Database (Denmark)

    Bemman, Brian; Meredith, David

    In recent years, a significant body of research has focused on developing algorithms for computing analyses of mu- sical works automatically from encodings of these works' surfaces [3,4,7,10,11]. The quality of the output of such analysis algorithms is typically evaluated by comparing it with a “......In recent years, a significant body of research has focused on developing algorithms for computing analyses of mu- sical works automatically from encodings of these works' surfaces [3,4,7,10,11]. The quality of the output of such analysis algorithms is typically evaluated by comparing...... an effective (i.e., comput- able), correct and complete description of some aspect of the structure of the music. Generating the surface struc- ture of a piece from an analysis in this manner serves as a proof of the analysis' correctness, effectiveness and com- pleteness. We present a reductive analysis...

  13. Long Term Validation of Land Surface Temperature Retrieved from MSG/SEVIRI with Continuous in-Situ Measurements in Africa

    Directory of Open Access Journals (Sweden)

    Frank-M. Göttsche

    2016-05-01

    Full Text Available Since 2005, the Land Surface Analysis Satellite Application Facility (LSA SAF operationally retrieves Land Surface Temperature (LST for the Spinning Enhanced Visible and Infrared Imager (SEVIRI on board Meteosat Second Generation (MSG. The high temporal resolution of the Meteosat satellites and their long term availability since 1977 make their data highly valuable for climate studies. In order to ensure that the LSA SAF LST product continuously meets its target accuracy of 2 °C, it is validated with in-situ measurements from four dedicated LST validation stations. Three stations are located in highly homogenous areas in Africa (semiarid bush, desert, and Kalahari semi-desert and typically provide thousands of monthly match-ups with LSA SAF LST, which are used to perform seasonally resolved validations. An uncertainty analysis performed for desert station Gobabeb yielded an estimate of total in-situ LST uncertainty of 0.8 ± 0.12 °C. Ignoring rainy seasons, the results for the period 2009–2014 show that LSA SAF LST consistently meets its target accuracy: the highest mean root-mean-square error (RMSE for LSA SAF LST over the African stations was 1.6 °C while mean absolute bias was 0.1 °C. Nighttime and daytime biases were up to 0.7 °C but had opposite signs: when evaluated together, these partially compensated each other.

  14. LSA glass-ceramic tiles made by powder pressing; Obtencao de placas vitroceramicas do sistema LSA utilizando a prensagem de pos

    Energy Technology Data Exchange (ETDEWEB)

    Figueira, F.C.; Bertan, F.M. [Colorminas Colorificio e Mineracao, Icara, SC (Brazil); Riella, H.G. [Universidade Federal de Santa Catarina (UFSC), Florianopolis, SC (Brazil). Programa de Pos-Graduaco em Engenharia Quimica; Uggioni, E. [Universidade do Extremo Sul Catarinense (UFSC), Florianopolis, SC (Brazil). Curso de Engenharia de Materiais; Bernardin, A.M., E-mail: amb@unesc.ne [Servico Nacional de Aprendizagem Industrial (SENAI), Tijucas, SC (Brazil). Dept. de Tecnologia em Ceramica

    2009-07-01

    A low cost alternative for the production of glass-ceramic materials is the pressing of the matrix glass powders and its consolidation simultaneously with crystallization in a single stage of sintering. The main objective of this work was to obtain LSA glass ceramics with low thermal expansion, processed by pressing and sintering a ceramic frit powder. The raw materials were homogenized and melted (1480 deg C, 80min), and the melt was poured in water. The glass was chemically (XRF and AAS) and thermally (DTA, 10 deg C/min, air) characterized, and then ground (60min and 120min). The ground powders were characterized (laser diffraction) and compressed (35MPa and 45MPa), thus forming four systems. The compacts were dried (150 deg C, 24h) and sintered (1175 deg C and 1185 deg C, 10 deg C/min). Finally, the glass-ceramics were characterized by microstructural analysis (SEM and XRD), mechanical behavior ({sigma}bending) and thermal analysis ({alpha}). The best results for thermal expansion were those for the glass-ceramics processed with smaller particle size and greater compaction pressure. (author)

  15. Quantitative Hydrocarbon Surface Analysis

    Science.gov (United States)

    Douglas, Vonnie M.

    2000-01-01

    The elimination of ozone depleting substances, such as carbon tetrachloride, has resulted in the use of new analytical techniques for cleanliness verification and contamination sampling. The last remaining application at Rocketdyne which required a replacement technique was the quantitative analysis of hydrocarbons by infrared spectrometry. This application, which previously utilized carbon tetrachloride, was successfully modified using the SOC-400, a compact portable FTIR manufactured by Surface Optics Corporation. This instrument can quantitatively measure and identify hydrocarbons from solvent flush of hardware as well as directly analyze the surface of metallic components without the use of ozone depleting chemicals. Several sampling accessories are utilized to perform analysis for various applications.

  16. Development of an improved radiological basis and revised requirements for the transport of LSA/SCO materials

    International Nuclear Information System (INIS)

    Gray, I.L.S.; Lange, F.; Hoermann, E.; Carr, N.A.

    2004-01-01

    The IAEA Regulations for the Safe Transport of Radioactive Material specify a range of package requirements that are dependent upon the activity and properties of the radioactive material being transported. For example, Type A packages can be used for the transport of material with an activity of up to one A1 of special form material and one A2 of other material. The A1 and A2 values are determined for over 350 radionuclides using the Q system in the advisory material. This system models the following pathways in the event of a severe accident: External photon dose; External beta dose; Inhalation dose; Skin and ingestion dose due to contamination transfer; Submersion dose. Industrial packages can be used for the transport of low specific activity (LSA) material and surface contaminated objects (SCO) and the particular requirements for these types of materials are derived from a simplistic radiological model that is often referred to as the 10 mg inhalation model. This is because it is based on the assumption that, in a dusty environment, an individual would inhale no more than 10 mg in such a situation, although there is limited reliable information to justify this assumption. Furthermore, there are deficiencies in the specification of some of the material requirements for LSA/SCO material in the IAEA Transport Regulations. Consequently, this can cause some difficulties for operators in complying with the regulations and to competent authorities in their compliance assurance role. Particular areas of difficulty include: It can be difficult to distinguish between LSA-type material and SCO-type; It is difficult to distinguish surface contamination from activity within the object, and between fixed and nonfixed contamination; In order to demonstrate compliance with SCO requirements, measurements of both accessible and nonaccessible contamination are required, although it is not clear how compliance with the inaccessible contamination limit can be measured if it cannot

  17. First characterization of Plasmodium vivax liver stage antigen (PvLSA) using synthetic peptides.

    Science.gov (United States)

    Goo, Youn-Kyoung; Seo, Eun-Jeong; Choi, Yeon-Kyung; Shin, Hyun-Il; Sattabongkot, Jetsumon; Ji, So-Young; Chong, Chom-Kyu; Cho, Shin-Hyung; Lee, Won-Ja; Kim, Jung-Yeon

    2014-02-12

    Plasmodium vivax is the most widespread human malaria in tropical and subtropical countries, including the Republic of Korea. Vivax malaria is characterized by hypnozoite relapse and long latency infection by the retained liver stage of P. vivax, and somewhat surprisingly, little is known of the liver stage antigens of this parasite. Here, we report for the first time the characterization of a liver stage antigen of P. vivax (PvLSA). Five peptides located inside PvLSA were synthesized, and specific anti-sera to the respective peptides were used to localize PvLSA on P. vivax parasites in human liver cells by immunofluorescence. Western blotting and enzyme-linked immunosorbent assay were performed using the five peptides and sera collected from vivax malaria patients and from normal healthy controls. PvLSA was localized on P. vivax parasites in human liver cells. Vivax malaria-infected patients were detected using the five peptides by western blotting. Furthermore, the peptides reacted with the sera of vivax malaria patients. These results suggest that PvLSA may function during the liver stage of P. vivax.

  18. Results of the Valiant Mona LSA early feasibility study for descending thoracic aneurysms.

    Science.gov (United States)

    Roselli, Eric E; Arko, Frank R; Thompson, Matthew M

    2015-12-01

    Stent graft coverage of the left subclavian artery (LSA) may be required to achieve an adequate landing zone in up to 40% of descending thoracic aneurysms (DTAs). The Valiant Mona LSA Thoracic Stent Graft System (Medtronic, Santa Rosa, Calif) consists of a main stent graft and a branch stent graft designed to maintain LSA patency while diverting circulation through the encroaching aneurysm. Participating in the United States Food and Drug Administration's new Innovation Pathway, this first-in-human, early feasibility study evaluates early clinical experience of the Valiant Mona LSA Stent Graft System in patients with DTAs where the proximal landing zone necessitates LSA coverage. This premarket, nonrandomized, single-arm prospective study recruited nine patients (age 72.9 ± 7.6 years). Primary end points were aneurysm-related mortality, stroke, paraplegia, left arm/hand ischemia, and treatment success. Neurologic events were assessed by imaging and by independent neurologists. Inclusion criteria required patients with a DTA or penetrating aortic ulcer to have a distance of ≥10 mm between the left common carotid artery and the LSA. Mean aneurysm diameter was 53.7 ± 10.0 mm. The indication for repair was for saccular DTA in five patients or fusiform DTA in four. Seven patients were at American Society of Anesthesiologists Physical Status Classification III/IV. All nine patients received one main stent graft (diameter 28 to 42 mm) and one branch stent graft (diameter 10 to 14 mm). To extend device coverage distally, a commercial Valiant Captivia device was implanted in seven patients. No uncorrected endoleaks were observed at the end of the implant procedure. Four endoleaks developed before discharge in four of eight evaluable patients. Two were identified as type II and two were of undetermined type. No endoleak resulted in a secondary intervention. Technical success, defined by the clinical investigational plan, was achieved in all nine patients intraoperatively

  19. Use of Language Sample Analysis by School-Based SLPs: Results of a Nationwide Survey

    Science.gov (United States)

    Pavelko, Stacey L.; Owens, Robert E., Jr.; Ireland, Marie; Hahs-Vaughn, Debbie L.

    2016-01-01

    Purpose: This article examines use of language sample analysis (LSA) by school-based speech-language pathologists (SLPs), including characteristics of language samples, methods of transcription and analysis, barriers to LSA use, and factors affecting LSA use, such as American Speech-Language-Hearing Association certification, number of years'…

  20. Safety evaluation for packaging (Onsite) transport of LSA-II liquids in MC-312 cargo tanks

    International Nuclear Information System (INIS)

    Carlstrom, R.F.

    1996-01-01

    This safety evaluation for packaging authorizes the onsite transfer of bulk LSA-II radioactive liquids in the 222-S Laboratory Cargo Tank and Liquid Effluent Treatment Facility Cargo Tanks (which are U.S. Department of Transportation MC-312 specification cargo tanks) from their operating facilities to tank farm facilities

  1. Latente semantische analyse (LSA) en EVC's: wat kunnen we er mee?

    NARCIS (Netherlands)

    Van Bruggen, Jan; Rusman, Ellen; Giesbers, Bas

    2005-01-01

    Presentation (in Dutch) on the LSA results of a test corpus for positioning. The results clearly indicate that in small size corpora stopping high frequency terms improves performance. A number of metrics to decide on the optimum number of singular values are presented and evaluated

  2. Hybrid LSA-ANN Based Home Energy Management Scheduling Controller for Residential Demand Response Strategy

    Directory of Open Access Journals (Sweden)

    Maytham S. Ahmed

    2016-09-01

    Full Text Available Demand response (DR program can shift peak time load to off-peak time, thereby reducing greenhouse gas emissions and allowing energy conservation. In this study, the home energy management scheduling controller of the residential DR strategy is proposed using the hybrid lightning search algorithm (LSA-based artificial neural network (ANN to predict the optimal ON/OFF status for home appliances. Consequently, the scheduled operation of several appliances is improved in terms of cost savings. In the proposed approach, a set of the most common residential appliances are modeled, and their activation is controlled by the hybrid LSA-ANN based home energy management scheduling controller. Four appliances, namely, air conditioner, water heater, refrigerator, and washing machine (WM, are developed by Matlab/Simulink according to customer preferences and priority of appliances. The ANN controller has to be tuned properly using suitable learning rate value and number of nodes in the hidden layers to schedule the appliances optimally. Given that finding proper ANN tuning parameters is difficult, the LSA optimization is hybridized with ANN to improve the ANN performances by selecting the optimum values of neurons in each hidden layer and learning rate. Therefore, the ON/OFF estimation accuracy by ANN can be improved. Results of the hybrid LSA-ANN are compared with those of hybrid particle swarm optimization (PSO based ANN to validate the developed algorithm. Results show that the hybrid LSA-ANN outperforms the hybrid PSO based ANN. The proposed scheduling algorithm can significantly reduce the peak-hour energy consumption during the DR event by up to 9.7138% considering four appliances per 7-h period.

  3. Surface analysis the principal techniques

    CERN Document Server

    Vickerman, John C

    2009-01-01

    This completely updated and revised second edition of Surface Analysis: The Principal Techniques, deals with the characterisation and understanding of the outer layers of substrates, how they react, look and function which are all of interest to surface scientists. Within this comprehensive text, experts in each analysis area introduce the theory and practice of the principal techniques that have shown themselves to be effective in both basic research and in applied surface analysis. Examples of analysis are provided to facilitate the understanding of this topic and to show readers how they c

  4. Decreased surface albedo driven by denser vegetation on the Tibetan Plateau

    International Nuclear Information System (INIS)

    Tian, Li; Zhang, Yangjian; Zhu, Juntao

    2014-01-01

    The Tibetan Plateau (TP) has fundamental ecological and environmental significance to China and Asia through its influence on regional and continental climates. In recent years, climate warming has caused unprecedented changes to land surface processes on the TP, which would unavoidably undermine the ecological and environmental functions of the TP. Among the numerous land surface processes potentially impacted by climate warming, the effect of vegetation greenness on surface energy balance is one of the most critical, but has been long ignored. In this study, we investigated the spatial and temporal patterns of land surface albedo (LSA) on the TP and evaluated the vegetation greenness in relation to patterns of LSA. We found that LSA has been decreasing in most of the vegetated grasslands on the TP from 2000 to 2013, as compared to a flat trend for desert area. The regions where LSA has been decreasing were spatially correlated to areas of increased vegetation greenness. Along rising altitude, LSA decreasing rate exhibited an overall decreasing trend. Across the TP, elevated vegetation greenness in grasslands acted as a primary factor pulling down LSA. The driving effects of vegetation greenness on LSA vary with grassland types, as revealed by a more significant relationship between vegetation greenness and LSA for the sparsely vegetated zone (i.e. steppe) than the more densely vegetated zone (i.e. meadow). Furthermore, the driving effect of vegetation greenness on LSA exhibited an obvious dependence on altitude as effects with rising altitude were relatively strong up to 3000 m, then weakened from 3500 m to 5000 m, and then the effects again increased from 5000 to 6000 m. The growing season LSA trend revealed in this study emphasizes the need to give greater attention to the growing season LSA flux in future surface energy balance studies. (letter)

  5. Endovascular repair of an innominate artery pseudoaneurysm using the Valiant Mona LSA branched graft device

    Directory of Open Access Journals (Sweden)

    Josh A. Sibille, MD

    2017-03-01

    Full Text Available A 60-year-old woman involved in a motor vehicle collision presented with a traumatic pseudoaneurysm of the innominate artery origin in addition to multiple concomitant injuries. She was classified as a high-risk candidate for open repair. An experimental thoracic branched graft device was used for coverage of the injury with the addition of a right carotid-to-left carotid-to-left subclavian artery bypass. Follow-up imaging showed resolution of the pseudoaneurysm and patency of her bypass grafts. This is the first described use of the Mona LSA Branch Thoracic Stent Graft System (Medtronic, Minneapolis, Minn in the innominate artery.

  6. Assessment of the Suomi NPP VIIRS Land Surface Albedo Data Using Station Measurements and High-Resolution Albedo Maps

    Directory of Open Access Journals (Sweden)

    Yuan Zhou

    2016-02-01

    Full Text Available Land surface albedo (LSA, one of the Visible Infrared Imaging Radiometer Suite (VIIRS environmental data records (EDRs, is a fundamental component for linking the land surface and the climate system by regulating shortwave energy exchange between the land and the atmosphere. Currently, the improved bright pixel sub-algorithm (BPSA is a unique algorithm employed by VIIRS to routinely generate LSA EDR from VIIRS top-of-atmosphere (TOA observations. As a product validation procedure, LSA EDR reached validated (V1 stage maturity in December 2014. This study summarizes recent progress in algorithm refinement, and presents comprehensive validation and evaluation results of VIIRS LSA by using extensive field measurements, Moderate Resolution Imaging Spectroradiometer (MODIS albedo product, and Landsat-retrieved albedo maps. Results indicate that: (1 by testing the updated desert-specific look-up-table (LUT that uses a stricter standard to select the training data specific for desert aerosol type in our local environment, it is found that the VIIRS LSA retrieval accuracy is improved over a desert surface and the absolute root mean square error (RMSE is reduced from 0.036 to 0.023, suggesting the potential of the updated desert LUT to the improve the VIIRS LSA product accuracy; (2 LSA retrieval on snow-covered surfaces is more accurate if the newly developed snow-specific LUT (RMSE = 0.082 replaces the generic LUT (RMSE = 0.093 that is employed in the current operational LSA EDR production; (3 VIIRS LSA is also comparable to high-resolution Landsat albedo retrieval (RMSE < 0.04, although Landsat albedo has a slightly higher accuracy, probably owing to higher spatial resolution with less impacts of mixed pixel; (4 VIIRS LSA retrievals agree well with the MODIS albedo product over various land surface types, with overall RMSE of lower than 0.05 and the overall bias as low as 0.025, demonstrating the comparable data quality between VIIRS and the MODIS LSA

  7. Surface analysis and techniques in biology

    CERN Document Server

    Smentkowski, Vincent S

    2014-01-01

    This book highlights state-of-the-art surface analytical instrumentation, advanced data analysis tools, and the use of complimentary surface analytical instrumentation to perform a complete analysis of biological systems.

  8. Relationship between Mixed Pixel Spectral Value of Landsat 8 OLI Data and LAPAN Surveillance Aircraft (LSA Aerial Photo Data

    Directory of Open Access Journals (Sweden)

    Nurwita Mustika Sari

    2017-07-01

    Full Text Available Medium resolution satellite data such as Landsat is very potential for mixed pixel (mixel to occur. Indonesian land use diverse especially urban areas makes high potential mixel in the first Landsat pixel size of 30 meters x 30 meters on the actual condition. Aircraft multispectral aerial photo data LAPAN Surveillance Aircraft (LSA with a spatial resolution reached 58 cm can display objects in more detail in these sizes. The purpose of this research is to study mixel on Landsat data with multispectral data LSA as a complement Landsat data. The method proposed in this study is a visual interpretation with GEOBIA method for classification of land cover, and then test the validity of the sample to be used in research, and the use of such vegetation index NDVI to see the connection between vegetation index data of vegetation index LSA with Landsat data. The results showed that the regression equation obtained by regression between NDVI of Landsat data and NDVI of  LSA with a significance of less than 0.05 is y = 0.732x - 0102 with a value of R2 = 0.887. Through these results we can conclude that the NDVI values on both the data related to one another.

  9. A Comparative Study Of The Predisposing Factors And Natural History Of Lichen sclerosus ET Atrophicus (LSA In Children And Adults

    Directory of Open Access Journals (Sweden)

    Iraji Fariba

    2003-01-01

    Full Text Available Lichen sclerosus et atrophicus (LSA is a chronic inflammatory dermatosis that results in white plaques with epidermal atrophy usually affecting the genital area in both adults and children. The causes of LSA are not clear but possible predisponsing factors include trauma, infection (borrelia, human papilloma virus, autoimmune diseases and local irritation. This study is a retrospective case review of children and adults with LSA attending the department of Dermatology at the Royal Infirmary in Edinburgh, clinical notes for 22 patients were reviewed for age, sex, personal and familial history, symptoms associated diseases and clinical course and treatment. The mean ages at diagnosis of LSA in 9 children (8F: 1M and 13 adults (13 F were 7 and 57.5 years respectively. The mean duration of illness was 1.5 year in children and 5.5 year in adults. Itching was the most common symptom in both children and adults. Children also suffered with difficulties in defaecation and in micturation , dribbling, incontinence, constipation and bleeding. Atopy and hypothyroidism were common associated conditions in both the groups. Squamous cell carcinoma of the vulva was confirmed in two adult patients. This study showed the variable symptoms in children, which seemed more severe than in the adult population.

  10. Laser surface alloying (LSA) of aluminium (AA 1200) with TiB2 for hardness improvement

    CSIR Research Space (South Africa)

    Popoola, AP

    2010-10-01

    Full Text Available and D, from these profiles secondary phases were identified, phases present in the alloyed layer are: TiB2, AlTi, AlB2, Al, Ti, B. The Al and Ti belong to the same crystal system and the same space group, and as such their peaks are overlapping.... The same for TiB2 and AlB2 � they belong to the same space group and peaks are overlapping. However, the XRD result of sample D also showed the presence of Al3Ti, this is an intermetallic phase that exhibits high hardness, high melting and also very...

  11. A comparison of all-weather land surface temperature products

    Science.gov (United States)

    Martins, Joao; Trigo, Isabel F.; Ghilain, Nicolas; Goettche, Frank-M.; Ermida, Sofia; Olesen, Folke-S.; Gellens-Meulenberghs, Françoise; Arboleda, Alirio

    2017-04-01

    The Satellite Application Facility on Land Surface Analysis (LSA-SAF, http://landsaf.ipma.pt) has been providing land surface temperature (LST) estimates using SEVIRI/MSG on an operational basis since 2006. The LSA-SAF service has since been extended to provide a wide range of satellite-based quantities over land surfaces, such as emissivity, albedo, radiative fluxes, vegetation state, evapotranspiration, and fire-related variables. Being based on infra-red measurements, the SEVIRI/MSG LST product is limited to clear-sky pixels only. Several all-weather LST products have been proposed by the scientific community either based on microwave observations or using Soil-Vegetation-Atmosphere Transfer models to fill the gaps caused by clouds. The goal of this work is to provide a nearly gap-free operational all-weather LST product and compare these approaches. In order to estimate evapotranspiration and turbulent energy fluxes, the LSA-SAF solves the surface energy budget for each SEVIRI pixel, taking into account the physical and physiological processes occurring in vegetation canopies. This task is accomplished with an adapted SVAT model, which adopts some formulations and parameters of the Tiled ECMWF Scheme for Surface Exchanges over Land (TESSEL) model operated at the European Center for Medium-range Weather Forecasts (ECMWF), and using: 1) radiative inputs also derived by LSA-SAF, which includes surface albedo, down-welling fluxes and fire radiative power; 2) a land-surface characterization obtained by combining the ECOCLIMAP database with both LSA-SAF vegetation products and the H(ydrology)-SAF snow mask; 3) meteorological fields from ECMWF forecasts interpolated to SEVIRI pixels, and 4) soil moisture derived by the H-SAF and LST from LSA-SAF. A byproduct of the SVAT model is surface skin temperature, which is needed to close the surface energy balance. The model skin temperature corresponds to the radiative temperature of the interface between soil and atmosphere

  12. Global Analysis of Minimal Surfaces

    CERN Document Server

    Dierkes, Ulrich; Tromba, Anthony J

    2010-01-01

    Many properties of minimal surfaces are of a global nature, and this is already true for the results treated in the first two volumes of the treatise. Part I of the present book can be viewed as an extension of these results. For instance, the first two chapters deal with existence, regularity and uniqueness theorems for minimal surfaces with partially free boundaries. Here one of the main features is the possibility of 'edge-crawling' along free parts of the boundary. The third chapter deals with a priori estimates for minimal surfaces in higher dimensions and for minimizers of singular integ

  13. Gap Surface Plasmon Waveguide Analysis

    DEFF Research Database (Denmark)

    Nielsen, Michael Grøndahl; Bozhevolnyi, Sergey I.

    2014-01-01

    Plasmonic waveguides supporting gap surface plasmons (GSPs) localized in a dielectric spacer between metal films are investigated numerically and the waveguiding properties at telecommunication wavelengths are presented. Especially, we emphasize that the mode confinement can advantageously be con...

  14. Thin film surface reconstruction analysis

    International Nuclear Information System (INIS)

    Imperatori, P.

    1996-01-01

    The study of the atomic structure of surfaces and interfaces is a fundamental step in the knowledge and the development of new materials. Among the several surface-sensitive techniques employed to characterise the atomic arrangements, grazing incidence x-ray diffraction (GIXD) is one of the most powerful. With a simple data treatment, based on the kinematical theory, and using the classical methods of x-ray bulk structure determination, it gives the atomic positions of atoms at a surface or an interface and the atomic displacements of subsurface layers for a complete determination of the structure. In this paper the main features of the technique will be briefly reviewed and selected of application to semiconductor and metal surfaces will be discussed

  15. Thin film surface reconstruction analysis

    Energy Technology Data Exchange (ETDEWEB)

    Imperatori, P. [CNR, Monterotondo Stazione, Rome (Italy). Istituto di Chimica dei materiali

    1996-09-01

    The study of the atomic structure of surfaces and interfaces is a fundamental step in the knowledge and the development of new materials. Among the several surface-sensitive techniques employed to characterise the atomic arrangements, grazing incidence x-ray diffraction (GIXD) is one of the most powerful. With a simple data treatment, based on the kinematical theory, and using the classical methods of x-ray bulk structure determination, it gives the atomic positions of atoms at a surface or an interface and the atomic displacements of subsurface layers for a complete determination of the structure. In this paper the main features of the technique will be briefly reviewed and selected of application to semiconductor and metal surfaces will be discussed.

  16. Large-scale Bubble Structure of the Intersteller Medium (ISM) and Properties of the Local Spiral Arm (LSA)

    Science.gov (United States)

    Bochkarev, N. G.

    1984-01-01

    Bubbles which are very common structure units in the Galaxy and galaxies were examined. Collection of radio, optical, infrared and X-ray observations of the Cyg superbubble (CSB) region of the sky show that the CSB is not a single bubble object. Between 50 to 75 percent of its X-ray emission is ascribed to discrete sources. The other 25 to 50% X-ray emission, probably originates from bubbles around 8 OB associations of the region. All bubbles located within the spiral structure of Galaxy, M31 and M33 have diameter 300 pc. The large distance of stellar association from the galactic plane (GP) combined with picture of the gas distribution within the LSA shows that a Reyleigh-Taylor instability in the LSA can develop and give use to the formation of compact stellar clusters, such as the Cyg OB2 association. Development stages of the Reyleigh-Taylor instability, some peculiarities of the dust distribution and departures of the local structure from the galactic grand design suggest the absence of a spiral shockwave in the LSA.

  17. Surface computing and collaborative analysis work

    CERN Document Server

    Brown, Judith; Gossage, Stevenson; Hack, Chris

    2013-01-01

    Large surface computing devices (wall-mounted or tabletop) with touch interfaces and their application to collaborative data analysis, an increasingly important and prevalent activity, is the primary topic of this book. Our goals are to outline the fundamentals of surface computing (a still maturing technology), review relevant work on collaborative data analysis, describe frameworks for understanding collaborative processes, and provide a better understanding of the opportunities for research and development. We describe surfaces as display technologies with which people can interact directly, and emphasize how interaction design changes when designing for large surfaces. We review efforts to use large displays, surfaces or mixed display environments to enable collaborative analytic activity. Collaborative analysis is important in many domains, but to provide concrete examples and a specific focus, we frequently consider analysis work in the security domain, and in particular the challenges security personne...

  18. Improving evapotranspiration in a land surface model using biophysical variables derived from MSG/SEVIRI satellite

    Directory of Open Access Journals (Sweden)

    N. Ghilain

    2012-08-01

    Full Text Available Monitoring evapotranspiration over land is highly dependent on the surface state and vegetation dynamics. Data from spaceborn platforms are desirable to complement estimations from land surface models. The success of daily evapotranspiration monitoring at continental scale relies on the availability, quality and continuity of such data. The biophysical variables derived from SEVIRI on board the geostationary satellite Meteosat Second Generation (MSG and distributed by the Satellite Application Facility on Land surface Analysis (LSA-SAF are particularly interesting for such applications, as they aimed at providing continuous and consistent daily time series in near-real time over Africa, Europe and South America. In this paper, we compare them to monthly vegetation parameters from a database commonly used in numerical weather predictions (ECOCLIMAP-I, showing the benefits of the new daily products in detecting the spatial and temporal (seasonal and inter-annual variability of the vegetation, especially relevant over Africa. We propose a method to handle Leaf Area Index (LAI and Fractional Vegetation Cover (FVC products for evapotranspiration monitoring with a land surface model at 3–5 km spatial resolution. The method is conceived to be applicable for near-real time processes at continental scale and relies on the use of a land cover map. We assess the impact of using LSA-SAF biophysical variables compared to ECOCLIMAP-I on evapotranspiration estimated by the land surface model H-TESSEL. Comparison with in-situ observations in Europe and Africa shows an improved estimation of the evapotranspiration, especially in semi-arid climates. Finally, the impact on the land surface modelled evapotranspiration is compared over a north–south transect with a large gradient of vegetation and climate in Western Africa using LSA-SAF radiation forcing derived from remote sensing. Differences are highlighted. An evaluation against remote sensing derived land

  19. SURFACE ENERGY BALANCE OVER ORANGE ORCHARD USING SURFACE RENEWAL ANALYSIS

    Directory of Open Access Journals (Sweden)

    Salvatore Barbagallo

    2009-12-01

    Full Text Available Reliable estimation of surface sensible and latent heat flux is the most important process to appraise energy and mass exchange among atmosphere and biosphere. In this study the surface energy fluxes were measured over an irrigated orange orchard during 2005-2008 monitoring periods using a Surface Renewal- Energy Balance approach. The experimental area is located in a representative orchard growing area of eastern Sicily (Italy. The performance of Surface Renewal (SR analysis for estimating sensible heat flux (H was analysed and evaluated in terms of correlation with H fluxes from the eddy covariance (EC method. Study revealed that the mean available energy (RN- G and latent heat flux (LE were of about 300 W m-2 and 237 W m-2, respectively, during dry periods and unstable-case atmospheric conditions. The estimated crop coefficient Kc values for the orchard crop averaged close to 0.80, which is considerably higher than previous FAO studies that found the value to be 0.65 for citrus with 70% of ground cover. The intercepted photosynthetically active radiation (LI PAR by the crop was measured and relationships between LAI and crop coefficient (Kc were established.

  20. SECTION 6.2 SURFACE TOPOGRAPHY ANALYSIS

    DEFF Research Database (Denmark)

    Seah, M. P.; De Chiffre, Leonardo

    2005-01-01

    Surface physical analysis, i.e. topography characterisation, encompasses measurement, visualisation, and quantification. This is critical for both component form and for surface finish at macro-, micro- and nano-scales. The principal methods of surface topography measurement are stylus profilometry......, optical scanning techniques, and scanning probe microscopy (SPM). These methods, based on acquisition of topography data from point by point scans, give quantitative information of heights with respect to position. Based on a different approach, the so-called integral methods produce parameters...

  1. Surface analysis with low energy ion scattering

    International Nuclear Information System (INIS)

    Taglauer, E.; Heiland, W.

    1976-01-01

    Principles and applications of low energy ion scattering for surface analysis are presented. Basic features are the binary collision concept, the scattering cross-sections and the ion neutralization process. The potential and the limitations of the method are outlined. Some pertinent experimental aspects are considered. In a number of examples the performance of the technique is demonstrated for qualitative composition analysis and for studies of surface structures. Finally a few comparisons are made with other techniques, such as AES, LEED, or SIMS. (orig.) [de

  2. Repository surface design site layout analysis

    International Nuclear Information System (INIS)

    Montalvo, H.R.

    1998-01-01

    The purpose of this analysis is to establish the arrangement of the Yucca Mountain Repository surface facilities and features near the North Portal. The analysis updates and expands the North Portal area site layout concept presented in the ACD, including changes to reflect the resizing of the Waste Handling Building (WHB), Waste Treatment Building (WTB), Carrier Preparation Building (CPB), and site parking areas; the addition of the Carrier Washdown Buildings (CWBs); the elimination of the Cask Maintenance Facility (CMF); and the development of a concept for site grading and flood control. The analysis also establishes the layout of the surface features (e.g., roads and utilities) that connect all the repository surface areas (North Portal Operations Area, South Portal Development Operations Area, Emplacement Shaft Surface Operations Area, and Development Shaft Surface Operations Area) and locates an area for a potential lag storage facility. Details of South Portal and shaft layouts will be covered in separate design analyses. The objective of this analysis is to provide a suitable level of design for the Viability Assessment (VA). The analysis was revised to incorporate additional material developed since the issuance of Revision 01. This material includes safeguards and security input, utility system input (size and location of fire water tanks and pump houses, potable water and sanitary sewage rates, size of wastewater evaporation pond, size and location of the utility building, size of the bulk fuel storage tank, and size and location of other exterior process equipment), main electrical substation information, redundancy of water supply and storage for the fire support system, and additional information on the storm water retention pond

  3. Repository Surface Design Site Layout Analysis

    International Nuclear Information System (INIS)

    Montalvo, H.R.

    1998-01-01

    The purpose of this analysis is to establish the arrangement of the Repository surface facilities and features near the North Portal. The analysis updates and expands the North Portal area site layout concept presented in the ACD (Reference 5.5), including changes to reflect the resizing of the Waste Handling Building (WHB), Waste Treatment Building (WTB), Carrier Preparation Building (CPB), and site parking areas; the addition of the Carrier Washdown Buildings (CWBs); the elimination of the Cask Maintenance Facility (CMF); and the development of a concept for site grading and flood control. The analysis also establishes the layout of the surface features (e.g., roads and utilities) that connect all the repository surface areas (North Portal Operations Area, South Portal Development Operations Area, Emplacement Shaft Surface Operations Area, and Development Shaft Surface Operations Area) and locates an area for a potential lag storage facility. Details of South Portal and shaft layouts will be covered in separate design analyses. The objective of this analysis is to provide a suitable level of design for the Viability Assessment (VA). The analysis was revised to incorporate additional material developed since the issuance of Revision 01. This material includes safeguards and security input, utility system input (size and location of fire water tanks and pump houses, potable water and sanitary sewage rates, size of wastewater evaporation pond, size and location of the utility building, size of the bulk fuel storage tank, and size and location of other exterior process equipment), main electrical substation information, redundancy of water supply and storage for the fire support system, and additional information on the storm water retention pond

  4. SURFACE TEXTURE ANALYSIS FOR FUNCTIONALITY CONTROL

    DEFF Research Database (Denmark)

    De Chiffre, Leonardo; Andreasen, Jan Lasson; Tosello, Guido

    This document is used in connection with three exercises of 3 hours duration as a part of the course VISION ONLINE – One week course on Precision & Nanometrology. The exercises concern surface texture analysis for functionality control, in connection with three different case stories. This docume...... contains a short description of each case story, 3-D roughness parameters analysis and relation with the product’s functionality.......This document is used in connection with three exercises of 3 hours duration as a part of the course VISION ONLINE – One week course on Precision & Nanometrology. The exercises concern surface texture analysis for functionality control, in connection with three different case stories. This document...

  5. Gyral Folding Pattern Analysis via Surface Profiling

    Science.gov (United States)

    Li, Kaiming; Guo, Lei; Li, Gang; Nie, Jingxin; Faraco, Carlos; Cui, Guangbin; Zhao, Qun; Miller, L. Stephen; Liu, Tianming

    2010-01-01

    Folding is an essential shape characteristic of the human cerebral cortex. Descriptors of cortical folding patterns have been studied for decades. However, many previous studies are either based on local shape descriptors such as curvature, or based on global descriptors such as gyrification index or spherical wavelets. This paper proposes a gyrus-scale folding pattern analysis technique via cortical surface profiling. Firstly, we sample the cortical surface into 2D profiles and model them using a power function. This step provides both the flexibility of representing arbitrary shape by profiling and the compactness of representing shape by parametric modeling. Secondly, based on the estimated model parameters, we extract affine-invariant features on the cortical surface, and apply the affinity propagation clustering algorithm to parcellate the cortex into cortical regions with strict hierarchy and smooth transitions among them. Finally, a second-round surface profiling is performed on the parcellated cortical surface, and the number of hinges is detected to describe the gyral folding pattern. We have applied the surface profiling method to two normal brain datasets and a Schizophrenia patient dataset. The experimental results demonstrate that the proposed method can accurately classify human gyri into 2-hinge, 3-hinge and 4-hinge patterns. The distribution of these folding patterns on brain lobes and the relationship between fiber density and gyral folding patterns are further investigated. Results from the Schizophrenia dataset are consistent with commonly found abnormality in former studies by others, which demonstrates the potential clinical applications of the proposed technique. PMID:20472071

  6. Surface analysis with STM and AFM

    CERN Document Server

    Magonov, Sergi N

    1996-01-01

    Scanning tunneling microscopy (STM) and atomic force microscopy (AFM) are powerful tools for surface examination. In the past, many STM and AFM studies led to erroneous conclusions due to lack of proper theoretical considerations and of an understanding of how image patterns are affected by measurement conditions. For this book, two world experts, one on theoretical analysis and the other on experimental characterization, have joined forces to bring together essential components of STM and AFM studies: The practical aspects of STM, the image simulation by surface electron density plot calculat

  7. Surface analysis methods in materials science

    CERN Document Server

    Sexton, Brett; Smart, Roger

    1992-01-01

    The idea for this book stemmed from a remark by Philip Jennings of Murdoch University in a discussion session following a regular meeting of the Australian Surface Science group. He observed that a text on surface analysis and applica­ tions to materials suitable for final year undergraduate and postgraduate science students was not currently available. Furthermore, the members of the Australian Surface Science group had the research experience and range of coverage of sur­ face analytical techniques and applications to provide a text for this purpose. A of techniques and applications to be included was agreed at that meeting. The list intended readership of the book has been broadened since the early discussions, particularly to encompass industrial users, but there has been no significant alter­ ation in content. The editors, in consultation with the contributors, have agreed that the book should be prepared for four major groups of readers: - senior undergraduate students in chemistry, physics, metallur...

  8. Microchemical surface analysis of two Numidian coins

    International Nuclear Information System (INIS)

    Mousser, Henia; Amri, Redha; Madani, Abdelghani; Darchen, Andre; Mousser, Abdelhamid

    2011-01-01

    This work is a contribution to the microchemical surface analysis of two Numidian coins. Numidia was an ancient kingdom of northern Algeria during 2nd and 1st century BC. Investigations were performed with scanning electron microscopy (SEM) coupled with energy dispersive spectrometry (EDS), energy dispersive X-ray fluorescence spectrometry (EDXRF) and X-ray diffraction (XRD). The identification of the coins was done thanks to the name initials and effigy of King Massinissa. SEM observations of coins showed heterogeneous surfaces. SEM and EDXRF analyses showed an alloy structure with copper (65%), antimony (19%) and lead (16%). The XRD identified a metal structure and corrosion products which were on the coin surfaces: Litharge (PbO), Hydrocerussite (Pb 3 (CO 3 ) 2 (OH) 2 ), Bindheimite (Pb 2 Sb 2 O 7 ) and Bystromite (MgSb 2 O 6 ).

  9. Advanced wettability analysis of implant surfaces

    Directory of Open Access Journals (Sweden)

    Jennissen Herbert P.

    2016-09-01

    Full Text Available New methodologies are a major driving force of scientific progress. In this case the finding that contact angles can be expressed as complex numbers offers the possibility of a much refined analysis beyond zero degrees of rough ultra-/superhydrophilic, (now called hyperhydrophilic, metal surfaces, which play a distinct role in dental and orthopedic implantology. The approaches, a short theoretical introduction and examples from medical applications are given.

  10. Surface analysis of stone and bone tools

    Science.gov (United States)

    Stemp, W. James; Watson, Adam S.; Evans, Adrian A.

    2016-03-01

    Microwear (use-wear) analysis is a powerful method for identifying tool use that archaeologists and anthropologists employ to determine the activities undertaken by both humans and their hominin ancestors. Knowledge of tool use allows for more accurate and detailed reconstructions of past behavior, particularly in relation to subsistence practices, economic activities, conflict and ritual. It can also be used to document changes in these activities over time, in different locations, and by different members of society, in terms of gender and status, for example. Both stone and bone tools have been analyzed using a variety of techniques that focus on the observation, documentation and interpretation of wear traces. Traditionally, microwear analysis relied on the qualitative assessment of wear features using microscopes and often included comparisons between replicated tools used experimentally and the recovered artifacts, as well as functional analogies dependent upon modern implements and those used by indigenous peoples from various places around the world. Determination of tool use has also relied on the recovery and analysis of both organic and inorganic residues of past worked materials that survived in and on artifact surfaces. To determine tool use and better understand the mechanics of wear formation, particularly on stone and bone, archaeologists and anthropologists have increasingly turned to surface metrology and tribology to assist them in their research. This paper provides a history of the development of traditional microwear analysis in archaeology and anthropology and also explores the introduction and adoption of more modern methods and technologies for documenting and identifying wear on stone and bone tools, specifically those developed for the engineering sciences to study surface structures on micro- and nanoscales. The current state of microwear analysis is discussed as are the future directions in the study of microwear on stone and bone tools.

  11. Surface Properties of TNOs: Preliminary Statistical Analysis

    Science.gov (United States)

    Antonieta Barucci, Maria; Fornasier, S.; Alvarez-Cantal, A.; de Bergh, C.; Merlin, F.; DeMeo, F.; Dumas, C.

    2009-09-01

    An overview of the surface properties based on the last results obtained during the Large Program performed at ESO-VLT (2007-2008) will be presented. Simultaneous high quality visible and near-infrared spectroscopy and photometry have been carried out on 40 objects with various dynamical properties, using FORS1 (V), ISAAC (J) and SINFONI (H+K bands) mounted respectively at UT2, UT1 and UT4 VLT-ESO telescopes (Cerro Paranal, Chile). For spectroscopy we computed the spectral slope for each object and searched for possible rotational inhomogeneities. A few objects show features in their visible spectra such as Eris, whose spectral bands are displaced with respect to pure methane-ice. We identify new faint absorption features on 10199 Chariklo and 42355 Typhon, possibly due to the presence of aqueous altered materials. The H+K band spectroscopy was performed with the new instrument SINFONI which is a 3D integral field spectrometer. While some objects show no diagnostic spectral bands, others reveal surface deposits of ices of H2O, CH3OH, CH4, and N2. To investigate the surface properties of these bodies, a radiative transfer model has been applied to interpret the entire 0.4-2.4 micron spectral region. The diversity of the spectra suggests that these objects represent a substantial range of bulk compositions. These different surface compositions can be diagnostic of original compositional diversity, interior source and/or different evolution with different physical processes affecting the surfaces. A statistical analysis is in progress to investigate the correlation of the TNOs’ surface properties with size and dynamical properties.

  12. Analysis of cell surface antigens by Surface Plasmon Resonance imaging

    NARCIS (Netherlands)

    Stojanovic, Ivan; Schasfoort, Richardus B.M.; Terstappen, Leonardus Wendelinus Mathias Marie

    2013-01-01

    Surface Plasmon Resonance (SPR) is most commonly used to measure bio-molecular interactions. SPR is used significantly less frequent for measuring whole cell interactions. Here we introduce a method to measure whole cells label free using the specific binding of cell surface antigens expressed on

  13. Surface Preparation for Microdebonding Analysis of Composites

    International Nuclear Information System (INIS)

    Kahraman, Ramazan; Mandell, J. F.

    1999-01-01

    The bond strength between fibers and matrix is an essential property of all composite materials and it must be measured accurately to be able to correlate it with the composite behavior. There are several factors affecting its measurement. This paper discusses the polishing and load application aspects of the indentation test technique for fibre-matrix bond strength determination in polymer and ceramic matrix composites. Different polishing procedures are suggested for polymer and ceramic surfaces for obtaining a smooth surface which is a must for the test results to be reliable. The geometry of the fibers tested was also found to affect the analysis results. For best results, fibers with similar size and which are similarly surrounded by other fibers should be tested. Care should be taken during load application on a fiber for the loading probe not to approach the fiber circumference. The force should be applied in a small increments as possible, however starting from a high enough level to prevent fiber breakage due to surface damage from several loading steps. (Author)

  14. A radiation analysis of lunar surface habitats

    International Nuclear Information System (INIS)

    De Angelis, G.; Wilson, J.W.; Tripathi, R.K.; Clowdsley, M.S.; Nealy, J.E.

    2003-01-01

    An analysis is performed on the radiation environment found on the surface of the Moon, and applied to different possible lunar base mission scenarios. An optimization technique has been used to minimize the astronaut radiation exposure and at the same time control the effect of shielding, in terms of mass addition and material choice, as a mission cost driver. The optimization process performs minimization of mass along all phases of a mission scenario, considered in terms of time frame, equipment, location, crew characteristics and performance required, radiation exposure annual and career limit constraints (those proposed in NCRP 132), and implementation of the ALARA principle. In the lunar environment manned habitats are to host future crews involved in the construction and/or in the utilization of moon based infrastructure. Three different kinds of lunar missions are considered in the analysis, Moon Base Construction Phase, during which astronauts are on the surface just to build an outpost for future resident crews, Moon Base Outpost Phase, during which astronaut crews are resident but continuing exploration and installation activities, and Moon Base Routine Phase, with shifting resident crews. In each scenario various kinds of habitats, from very simple shelters to more complex bases, are considered in detail (e.g. shape, thickness, materials, etc) with considerations of various shielding strategies. The results for all scenarios clearly showed that the direct exposure to the space environment like in transfers and EVAs phases gives the most of the dose, with the proposed shielded habitats and shelters giving quite a good protection from radiation. Operational constraints on hardware and scenarios have all been considered by the optimization techniques. Within the limits of this preliminary analysis, the three Moon Base related mission scenarios are perfectly feasible from the astronaut radiation safety point of view with the currently adopted and proposed

  15. Probabilistic Latent Semantic Analyses (PLSA in Bibliometric Analysis for Technology Forecasting

    Directory of Open Access Journals (Sweden)

    Wang Zan

    2007-03-01

    Full Text Available Due to the availability of internet-based abstract services and patent databases, bibliometric analysis has become one of key technology forecasting approaches. Recently, latent semantic analysis (LSA has been applied to improve the accuracy in document clustering. In this paper, a new LSA method, probabilistic latent semantic analysis (PLSA which uses probabilistic methods and algebra to search latent space in the corpus is further applied in document clustering. The results show that PLSA is more accurate than LSA and the improved iteration method proposed by authors can simplify the computing process and improve the computing efficiency

  16. AMATCHMETHOD BASED ON LATENT SEMANTIC ANALYSIS FOR EARTHQUAKEHAZARD EMERGENCY PLAN

    Directory of Open Access Journals (Sweden)

    D. Sun

    2017-09-01

    Full Text Available The structure of the emergency plan on earthquake is complex, and it’s difficult for decision maker to make a decision in a short time. To solve the problem, this paper presents a match method based on Latent Semantic Analysis (LSA. After the word segmentation preprocessing of emergency plan, we carry out keywords extraction according to the part-of-speech and the frequency of words. Then through LSA, we map the documents and query information to the semantic space, and calculate the correlation of documents and queries by the relation between vectors. The experiments results indicate that the LSA can improve the accuracy of emergency plan retrieval efficiently.

  17. Surface renewal analysis for estimating turbulent surface fluxes

    International Nuclear Information System (INIS)

    Castellvi, F.

    2009-01-01

    A decade ago, the need for a long-term surface monitoring was recognized to better understand the soil-vegetation-atmosphere scalar exchange and interaction processes. the AmeriFlux concept emerged in the IGBP workshop (La Thuile, IT, 1995). Continuous acquisition of surface fluxes for different species such as temperature, water vapour, CO x , halocarbon, ozone, etc.,) and momentum allows determination of the influence of local (canopy) exchanges, fossil fuel emission, large-scale biotic exchange on ambient concentrations which are crucial to take decisions for protecting natural environments and water resources, to develop new perspective for modern agriculture and forest management and to better understand the global climate change. (Author)

  18. Surface and interface analysis an electrochemists toolbox

    CERN Document Server

    Holze, Rudolf

    2009-01-01

    A broad, almost encyclopedic overview of spectroscopic and other analytical techniques useful for investigations of phase boundaries in electrochemistry is presented. The analysis of electrochemical interfaces and interphases on a microscopic, even molecular level, is of central importance for an improved understanding of the structure and dynamics of these phase boundaries. The gained knowledge will be needed for improvements of methods and applications reaching from electrocatalysis, electrochemical energy conversion, biocompatibility of metals, corrosion protection to galvanic surface treatment and finishing. The book provides an overview as complete as possible and enables the reader to choose methods most suitable for tackling his particular task. It is nevertheless compact and does not flood the reader with the details of review papers.

  19. Surface Management System Departure Event Data Analysis

    Science.gov (United States)

    Monroe, Gilena A.

    2010-01-01

    This paper presents a data analysis of the Surface Management System (SMS) performance of departure events, including push-back and runway departure events.The paper focuses on the detection performance, or the ability to detect departure events, as well as the prediction performance of SMS. The results detail a modest overall detection performance of push-back events and a significantly high overall detection performance of runway departure events. The overall detection performance of SMS for push-back events is approximately 55%.The overall detection performance of SMS for runway departure events nears 100%. This paper also presents the overall SMS prediction performance for runway departure events as well as the timeliness of the Aircraft Situation Display for Industry data source for SMS predictions.

  20. Multidisciplinary design optimization using response surface analysis

    Science.gov (United States)

    Unal, Resit

    1992-01-01

    Aerospace conceptual vehicle design is a complex process which involves multidisciplinary studies of configuration and technology options considering many parameters at many values. NASA Langley's Vehicle Analysis Branch (VAB) has detailed computerized analysis capabilities in most of the key disciplines required by advanced vehicle design. Given a configuration, the capability exists to quickly determine its performance and lifecycle cost. The next step in vehicle design is to determine the best settings of design parameters that optimize the performance characteristics. Typical approach to design optimization is experience based, trial and error variation of many parameters one at a time where possible combinations usually number in the thousands. However, this approach can either lead to a very long and expensive design process or to a premature termination of the design process due to budget and/or schedule pressures. Furthermore, one variable at a time approach can not account for the interactions that occur among parts of systems and among disciplines. As a result, vehicle design may be far from optimal. Advanced multidisciplinary design optimization (MDO) methods are needed to direct the search in an efficient and intelligent manner in order to drastically reduce the number of candidate designs to be evaluated. The payoffs in terms of enhanced performance and reduced cost are significant. A literature review yields two such advanced MDO methods used in aerospace design optimization; Taguchi methods and response surface methods. Taguchi methods provide a systematic and efficient method for design optimization for performance and cost. However, response surface method (RSM) leads to a better, more accurate exploration of the parameter space and to estimated optimum conditions with a small expenditure on experimental data. These two methods are described.

  1. Assessing the Big Five Personality Traits with Latent Semantic Analysis

    Science.gov (United States)

    We tested whether the characteristics of a persons personality can be assessed by an automated analysis of the semantic content of a persons written...the Big Five personality traits. Participants essays were processed for content by Latent Semantic Analysis (LSA; T. Landauer and S. Dumais, 1997...a model of lexical semantics. We found that LSA could assess individuals on three of the Big Five traits, and we discuss ways to improve such techniques in future work.

  2. A Heterogeneous System Based on Latent Semantic Analysis Using GPU and Multi-CPU

    Directory of Open Access Journals (Sweden)

    Gabriel A. León-Paredes

    2017-01-01

    Full Text Available Latent Semantic Analysis (LSA is a method that allows us to automatically index and retrieve information from a set of objects by reducing the term-by-document matrix using the Singular Value Decomposition (SVD technique. However, LSA has a high computational cost for analyzing large amounts of information. The goals of this work are (i to improve the execution time of semantic space construction, dimensionality reduction, and information retrieval stages of LSA based on heterogeneous systems and (ii to evaluate the accuracy and recall of the information retrieval stage. We present a heterogeneous Latent Semantic Analysis (hLSA system, which has been developed using General-Purpose computing on Graphics Processing Units (GPGPUs architecture, which can solve large numeric problems faster through the thousands of concurrent threads on multiple CUDA cores of GPUs and multi-CPU architecture, which can solve large text problems faster through a multiprocessing environment. We execute the hLSA system with documents from the PubMed Central (PMC database. The results of the experiments show that the acceleration reached by the hLSA system for large matrices with one hundred and fifty thousand million values is around eight times faster than the standard LSA version with an accuracy of 88% and a recall of 100%.

  3. Analysis of Fluid Flow over a Surface

    Science.gov (United States)

    McCloud, Peter L. (Inventor)

    2013-01-01

    A method, apparatus, and computer program product for modeling heat radiated by a structure. The flow of a fluid over a surface of a model of the structure is simulated. The surface has a plurality of surface elements. Heat radiated by the plurality of surface elements in response to the fluid flowing over the surface of the model of the structure is identified. An effect of heat radiated by at least a portion of the plurality of surface elements on each other is identified. A model of the heat radiated by the structure is created using the heat radiated by the plurality of surface elements and the effect of the heat radiated by at least a portion of the plurality of surface elements on each other.

  4. Global Surface Warming Hiatus Analysis Data

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — These data were used to conduct the study of the global surface warming hiatus, an apparent decrease in the upward trend of global surface temperatures since 1998....

  5. Computer simulation, nuclear techniques and surface analysis

    Directory of Open Access Journals (Sweden)

    Reis, A. D.

    2010-02-01

    Full Text Available This article is about computer simulation and surface analysis by nuclear techniques, which are non-destructive. The “energy method of analysis” for nuclear reactions is used. Energy spectra are computer simulated and compared with experimental data, giving target composition and concentration profile information. Details of prediction stages are given for thick flat target yields. Predictions are made for non-flat targets having asymmetric triangular surface contours. The method is successfully applied to depth profiling of 12C and 18O nuclei in thick targets, by deuteron (d,p and proton (p,α induced reactions, respectively.

    Este artículo trata de simulación por ordenador y del análisis de superficies mediante técnicas nucleares, que son no destructivas. Se usa el “método de análisis en energía” para reacciones nucleares. Se simulan en ordenador espectros en energía que se comparan con datos experimentales, de lo que resulta la obtención de información sobre la composición y los perfiles de concentración de la muestra. Se dan detalles de las etapas de las predicciones de espectros para muestras espesas y planas. Se hacen predicciones para muestras no planas que tienen contornos superficiales triangulares asimétricos. Este método se aplica con éxito en el cálculo de perfiles en profundidad de núcleos de 12C y de 18O en muestras espesas a través de reacciones (d,p y (p,α inducidas por deuterones y protones, respectivamente.

  6. Surface analysis of selected hydrophobic materials

    Science.gov (United States)

    Wisniewska, Sylwia Katarzyna

    This dissertation contains a series of studies on hydrophobic surfaces by various surface sensitive techniques such as contact angle measurements, Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and atomic force microscopy (AFM). Hydrophobic surfaces have been classified as mineral surfaces, organic synthetic surfaces, or natural biological surfaces. As a model hydrophobic mineral surface, elemental sulfur has been selected. The sulfur surface has been characterized for selected allotropic forms of sulfur such as rhombic, monoclinic, plastic, and cyclohexasulfur. Additionally, dextrin adsorption at the sulfur surface was measured. The structure of a dextrin molecule showing hydrophobic sites has been presented to support the proposed hydrophobic bonding nature of dextrin adsorption at the sulfur surface. As a model organic hydrophobic surface, primary fatty amines such as dodecylamine, hexadecylamine, and octadecylamine were chosen. An increase of hydrophobicity, significant changes of infrared bands, and surface topographical changes with time were observed for each amine. Based on the results it was concluded that hydrocarbon chain rearrangement associated with recrystallization took place at the surface during contact with air. A barley straw surface was selected as a model of biological hydrophobic surfaces. The differences in the contact angles for various straw surfaces were explained by the presence of a wax layer. SEM images confirmed the heterogeneity and complexity of the wax crystal structure. AFM measurements provided additional structural details including a measure of surface roughness. Additionally, straw degradation as a result of conditioning in an aqueous environment was studied. Significant contact angle changes were observed as soon as one day after conditioning. FTIR studies showed a gradual wax layer removal due to straw surface decomposition. SEM and AFM images revealed topographical changes and biological

  7. Autonomous Aerobraking Using Thermal Response Surface Analysis

    Science.gov (United States)

    Prince, Jill L.; Dec, John A.; Tolson, Robert H.

    2007-01-01

    Aerobraking is a proven method of significantly increasing the science payload that can be placed into low Mars orbits when compared to an all propulsive capture. However, the aerobraking phase is long and has mission cost and risk implications. The main cost benefit is that aerobraking permits the use of a smaller and cheaper launch vehicle, but additional operational costs are incurred during the long aerobraking phase. Risk is increased due to the repeated thermal loading of spacecraft components and the multiple attitude and propulsive maneuvers required for successful aerobraking. Both the cost and risk burdens can be significantly reduced by automating the aerobraking operations phase. All of the previous Mars orbiter missions that have utilized aerobraking have increasingly relied on onboard calculations during aerobraking. Even though the temperature of spacecraft components has been the limiting factor, operational methods have relied on using a surrogate variable for mission control. This paper describes several methods, based directly on spacecraft component maximum temperature, for autonomously predicting the subsequent aerobraking orbits and prescribing apoapsis propulsive maneuvers to maintain the spacecraft within specified temperature limits. Specifically, this paper describes the use of thermal response surface analysis in predicting the temperature of the spacecraft components and the corresponding uncertainty in this temperature prediction.

  8. Microstructure, microhardness, composition, and corrosive properties of stainless steel 304. I. Laser surface alloying with silicon by beam-oscillating method

    International Nuclear Information System (INIS)

    Isshiki, Y.; Shi, J.; Hashimoto, M.; Nakai, H.

    2000-01-01

    Laser surface alloying (LSA) with silicon was conducted on austenitic stainless steel 304. Silicon slurry composed of silicon particle of 5 μm in average diameter was made and a uniform layer was supplied on the substrate stainless steel. The surface was melted with beam-oscillated carbon dioxide laser and then LSA layers of 0.4-1.2 mm in thickness were obtained. When an impinged energy density was adjusted to be equal to or lower than 100 W mm -2 , LSA layers retained rapidly solidified microstructure with dispersed cracks. In these samples, Fe 3 Si was detected and the concentration of Si in LSA layer was estimated to be 10.5 wt.% maximum. When the energy density was equal to or greater than 147 W mm -2 , cellular grained structure with no crack was formed. No iron silicate was observed and alpha iron content in LSA layers increased. Si concentration within LSA layers was estimated to be 5 to 9 wt.% on average. Crack-free as-deposited samples exhibited no distinct corrosion resistance. The segregation of Si was confirmed along the grain boundaries and inside the grains. The microstructure of these samples changed with solution-annealing and the corrosion resistance was fairly improved with the time period of solution-annealing. (orig.)

  9. Surface Operations Data Analysis and Adaptation Tool, Phase II

    Data.gov (United States)

    National Aeronautics and Space Administration — This effort undertook the creation of a Surface Operations Data Analysis and Adaptation (SODAA) tool to store data relevant to airport surface research and...

  10. Atomic force microscopy analysis of different surface treatments of Ti dental implant surfaces

    International Nuclear Information System (INIS)

    Bathomarco, R.V.; Solorzano, G.; Elias, C.N.; Prioli, R.

    2004-01-01

    The surface of commercial unalloyed titanium, used in dental implants, was analyzed by atomic force microscopy. The morphology, roughness, and surface area of the samples, submitted to mechanically-induced erosion, chemical etching and a combination of both, were compared. The results show that surface treatments strongly influence the dental implant physical and chemical properties. An analysis of the length dependence of the implant surface roughness shows that, for scan sizes larger than 50 μm, the average surface roughness is independent of the scanning length and that the surface treatments lead to average surface roughness in the range of 0.37 up to 0.48 μm. It is shown that the implant surface energy is sensitive to the titanium surface area. As the area increases there is a decrease in the surface contact angle

  11. Atomic force microscopy analysis of different surface treatments of Ti dental implant surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Bathomarco, R.V.; Solorzano, G.; Elias, C.N.; Prioli, R

    2004-06-30

    The surface of commercial unalloyed titanium, used in dental implants, was analyzed by atomic force microscopy. The morphology, roughness, and surface area of the samples, submitted to mechanically-induced erosion, chemical etching and a combination of both, were compared. The results show that surface treatments strongly influence the dental implant physical and chemical properties. An analysis of the length dependence of the implant surface roughness shows that, for scan sizes larger than 50 {mu}m, the average surface roughness is independent of the scanning length and that the surface treatments lead to average surface roughness in the range of 0.37 up to 0.48 {mu}m. It is shown that the implant surface energy is sensitive to the titanium surface area. As the area increases there is a decrease in the surface contact angle.

  12. Land Surface Albedo From EPS/AVHRR : Method For Retrieval and Validation

    Science.gov (United States)

    Jacob, G.

    2015-12-01

    The scope of Land Surface Analysis Satellite Applications Facility (LSA-SAF) is to increase benefit from EUMETSAT Satellites (MSG and EPS) data by providing added value products for the meteorological and environmental science communities with main applications in the fields of climate modelling, environmental management, natural hazards management, and climate change detection. The MSG/SEVIRI daily albedo product is disseminated operationally by the LSA-SAF processing centre based in Portugal since 2009. This product so-called MDAL covers Europe and Africa includes in the visible, near infrared and shortwave bands at a resolution of 3km at the equator. Recently, an albedo product at 1km so-called ETAL has been built from EPS/AVHRR observations in order to primarily MDAL product outside the MSG disk, while ensuring a global coverage. The methodology is common to MSG and EPS data and relies on the inversion of the BRDF (Bidirectional Reflectance Distribution Function) model of Roujean et al. On a given target, ETAL products exploits the variability of viewing angles whereas MDAL looks at the variations of solar illumination. The comparison of ETAL albedo product against MODIS and MSG/SEVIRI products over the year 2015 is instructive in many ways and shows in general a good agreement between them. The dispersion may be accounted by different factors that will be explained The additional information provided by EPS appears to be particularly beneficial for high latitudes during winter and for snow albedo.

  13. 2nd international conference on ion beam surface layer analysis

    International Nuclear Information System (INIS)

    1975-01-01

    The papers of this conference are concerned with the fundamental aspects and with the application of surface layer analysis. It is reported amongst others about backscattering analysis, Auger electron spectroscopy, channelling and microprobe. (HPOE) [de

  14. Inverse analysis of inner surface temperature history from outer surface temperature measurement of a pipe

    International Nuclear Information System (INIS)

    Kubo, S; Ioka, S; Onchi, S; Matsumoto, Y

    2010-01-01

    When slug flow runs through a pipe, nonuniform and time-varying thermal stresses develop and there is a possibility that thermal fatigue occurs. Therefore it is necessary to know the temperature distributions and the stress distributions in the pipe for the integrity assessment of the pipe. It is, however, difficult to measure the inner surface temperature directly. Therefore establishment of the estimation method of the temperature history on inner surface of pipe is needed. As a basic study on the estimation method of the temperature history on the inner surface of a pipe with slug flow, this paper presents an estimation method of the temperature on the inner surface of a plate from the temperature on the outer surface. The relationship between the temperature history on the outer surface and the inner surface is obtained analytically. Using the results of the mathematical analysis, the inverse analysis method of the inner surface temperature history estimation from the outer surface temperature history is proposed. It is found that the inner surface temperature history can be estimated from the outer surface temperature history by applying the inverse analysis method, even when it is expressed by the multiple frequency components.

  15. La participación de los trabajadores en el capital social mediante operaciones de asistencia financiera. Especial referencia al art. 81.2 LSA

    OpenAIRE

    Nieto Rojas, Patricia

    2007-01-01

    La integración de los trabajadores en el capital social puede ser instrumentada mediante diferentes vías: distribución gratuita de acciones, entrega de opciones sobre acciones o mediante la asistencia financiera para la adquisición de acciones; el objetivo del presente artículo es analizar las implicaciones laborales de este último mecanismo previsto en el artículo 81.2 LSA que exceptúa de la prohibición general de asistencia financiera a los negocios dirigidos a facilitar la adquisición de a...

  16. Analysis of Separated Flow over Blocked Surface

    Directory of Open Access Journals (Sweden)

    Onur YEMENİCİ

    2013-04-01

    Full Text Available In this study, the separated flow over flat and blocked surfaces was investigated experimentally. Velocity and turbulence intensity measurements were carried out by a constanttemperature hot wire anemometer and static pressure measurements by a micro-manometer. The flow separations and reattachments were occurred before the first block, on the first block, between blocks and after the last block, and the presence of the blocks significantly increased the turbulent intensity

  17. Analysis of surface contaminants on beryllium windows

    International Nuclear Information System (INIS)

    Gmur, N.F.

    1986-12-01

    It is known that various crystalline and liquid compounds form on the downstream surfaces of beryllium windows exposed to air. It is also known that the integrity of such windows may be compromised resulting in leaks through the window. The purpose of this report is to document the occurrences described as they pertain to the NSLS and to analyze, where possible, the various substances formed

  18. Surface noise analysis using a single-ion sensor

    Science.gov (United States)

    Daniilidis, N.; Gerber, S.; Bolloten, G.; Ramm, M.; Ransford, A.; Ulin-Avila, E.; Talukdar, I.; Häffner, H.

    2014-06-01

    We use a single-ion electric-field noise sensor in combination with in situ surface treatment and analysis tools, to investigate the relationship between electric-field noise from metal surfaces in vacuum and the composition of the surface. These experiments are performed in a setup that integrates ion trapping capabilities with surface analysis tools. We find that treatment of an aluminum-copper surface with energetic argon ions significantly reduces the level of room-temperature electric-field noise, but the surface does not need to be atomically clean to show noise levels comparable to those of the best cryogenic traps. The noise levels after treatment are low enough to allow fault-tolerant trapped-ion quantum information processing on a microfabricated surface trap at room temperature.

  19. Plasma diagnostics surface analysis and interactions

    CERN Document Server

    Auciello, Orlando

    2013-01-01

    Plasmas and their interaction with materials have become subjects of major interest because of their importance in modern forefront technologies such as microelectronics, fusion energy, and space. Plasmas are used in microelectronics to process semiconductors (etching of patterns for microcircuits, plasma-induced deposition of thin films, etc.); plasmas produce deleterious erosion effects on surfaces of materials used for fusion devices and spaceships exposed to the low earth environment.Diagnostics of plasmas and materials exposed to them are fundamental to the understanding of the physical a

  20. Analysis of surface with low energy ions

    International Nuclear Information System (INIS)

    Oliver, A.; Miranda, J.

    1989-01-01

    Nuclear techniques applied to element analysis presents different characteristics depending on projectile energy. It can seen observed than an energy (E ≅ 1 MeV) exists which separate two regions for which sensitivity, information analysis and resolution in detection are different. For this work, we describe for the energy region E ≤ 1 MeV, the advantage of the three most used techniques which are PIXE, RBS y RNR. (Author)

  1. In situ surface-enhanced raman spectroelectrochemical analysis system with a hemin modified nanostructured gold surface

    NARCIS (Netherlands)

    Yuan, Tao; Le Thi Ngoc, Loan; van Nieuwkasteele, Jan William; Odijk, Mathieu; van den Berg, Albert; Permentier, Hjalmar; Bischoff, Rainer; Carlen, Edwin

    2015-01-01

    An integrated surface-enhanced Raman scattering (SERS) spectroelectrochemical (SEC) analysis system is presented that combines a small volume microfluidic sample chamber (<100 mu L) with a compact three-electrode configuration for in situ surface-enhanced Raman spectroelectrochemistry. The SEC

  2. In situ surface-enhanced Raman spectroelectrochemical analysis system with a hemin modified nanostructured gold surface

    NARCIS (Netherlands)

    Yuan, Tao; Le Thi Ngoc, Loan; van Nieuwkasteele, Jan; Odijk, Mathieu; van den Berg, Albert; Permentier, Hjalmar; Bischoff, Rainer; Carlen, Edwin T

    2015-01-01

    An integrated surface-enhanced Raman scattering (SERS) spectroelectrochemical (SEC) analysis system is presented that combines a small volume microfluidic sample chamber (<100 μL) with a compact three-electrode configuration for in situ surface-enhanced Raman spectroelectrochemistry. The SEC system

  3. Statistical analysis of the Martian surface

    Science.gov (United States)

    Landais, F.; Schmidt, F.; Lovejoy, S.

    2015-10-01

    We investigate the scaling properties of the topography of Mars [10]. Planetary topographic fields are well known to exhibit (mono)fractal behavior. Indeed, fractal formalism is efficient to reproduce the variability observed in topography. Still, a single fractal dimension is not enough to explain the huge variability and intermittency. Previous study have shown that fractal dimensions might be different from a region to another, excluding a general description at the planetary scale. In this project, we are analyzing the Martian topographic data with a multifractal formalism to study the scaling intermittency. In the multifractal paradigm, the local variation of the fractal dimension is interpreted as a statistical property of multifractal fields. The results suggest a multifractal behaviour from planetary scale down to 10 km. From 10 km to 600 m, the topography seems to be simple monofractal. This transition indicates a significant in the geological processes governing the Red Planet's surface.

  4. The analysis of pigments on rock surfaces

    International Nuclear Information System (INIS)

    Fankhauser, B.; O'Connor, S.; Pittelkow, Y.

    1997-01-01

    A limestone slab of roof fall coated with a red pigment was recovered from a Rockshelter in the Napier Ranges of the Kimberley region, Western Australia. Next to the roof fall fragment in the same stratigraphic layer was a piece of ochre. Three questions were presented: (1) is the red substance an ochre? (2) is the piece of ochre identical to the red substance on the roof fall? and (3) are the layers of pigment on the top and bottom of the limestone slab the same? In addition, as an extension from these questions, a general method was developed for the in situ analysis of ochre pigments on substrates to determine likely compositions and ochre sources. The analysis of the red pigment presented an analytical problem because the substance was intimately associated with the rock slab and therefore the analysis had to be done in situ. Not only was the red layer thin, but on a micro level it was uneven. Energy dispersive x-ray analysis (EDXA) penetrated the red layer, simultaneously analysing this layer and the rock substrate to different degrees depending upon the thickness of the red layer. Determining if the substance was actually ochre involved a comparison of elemental analyses between the background (slab) and background with red coating. Coatings of other ochres with known elemental concentrations on the same limestone background gave a comparison of the effect of simultaneously analysing a thin layer and background with different compositions. Three graphical methods useful for insitu analysis are demeonstrated. The find dates (around 40,000 BP) add to a growing body of data in support of the widespread use of ochre accompanying the earliest documented use of widely separated and environmentally diverse regions of Australia by Aboriginal people

  5. Error analysis of aspheric surface with reference datum.

    Science.gov (United States)

    Peng, Yanglin; Dai, Yifan; Chen, Shanyong; Song, Ci; Shi, Feng

    2015-07-20

    Severe requirements of location tolerance provide new challenges for optical component measurement, evaluation, and manufacture. Form error, location error, and the relationship between form error and location error need to be analyzed together during error analysis of aspheric surface with reference datum. Based on the least-squares optimization method, we develop a least-squares local optimization method to evaluate form error of aspheric surface with reference datum, and then calculate the location error. According to the error analysis of a machined aspheric surface, the relationship between form error and location error is revealed, and the influence on the machining process is stated. In different radius and aperture of aspheric surface, the change laws are simulated by superimposing normally distributed random noise on an ideal surface. It establishes linkages between machining and error analysis, and provides an effective guideline for error correcting.

  6. Auto-correlation analysis of ocean surface wind vectors

    Indian Academy of Sciences (India)

    M. Senthilkumar (Newgen Imaging) 1461 1996 Oct 15 13:05:22

    In this work, an auto-correlation analysis of a time series data of surface winds measured in situ by a deep water buoy in the Indian Ocean has been carried out. Hourly time series data available for 240 hours in the month of May, 1999 were subjected to an auto-correlation analysis. The analysis indicates an exponential fall ...

  7. Indian Ocean surface winds from NCMRWF analysis as compared to ...

    Indian Academy of Sciences (India)

    The quality of the surface wind analysis at the National Centre for Medium Range Weather Forecasts (NCMRWF), New Delhi over the tropical Indian Ocean and its improvement in 2001 are examined by comparing it with in situ buoy measurements and satellite derived surface winds from NASA QuikSCAT satellite (QSCT) ...

  8. Auto-correlation analysis of ocean surface wind vectors

    Indian Academy of Sciences (India)

    The nature of the inherent temporal variability of surface winds is analyzed by comparison of winds obtained through different measurement methods. In this work, an auto-correlation analysis of a time series data of surface winds measured in situ by a deep water buoy in the Indian Ocean has been carried out. Hourly time ...

  9. Assessing ground compaction via time lapse surface wave analysis

    Czech Academy of Sciences Publication Activity Database

    Dal Moro, Giancarlo; Al-Arifi, N.; Moustafa, S.S.R.

    2016-01-01

    Roč. 13, č. 3 (2016), s. 249-256 ISSN 1214-9705 Institutional support: RVO:67985891 Keywords : Full velocity spectrum (FVS) analysis * ground compaction * ground compaction * phase velocities * Rayleigh waves * seismic data inversion * surface wave dispersion * surface waves Subject RIV: DC - Siesmology, Volcanology, Earth Structure Impact factor: 0.699, year: 2016

  10. Applications of surface analysis in the wire industry

    Science.gov (United States)

    Stout, David A.

    The quality of wire is judged not only by its physical properties such as tensile strength and fatigue resistance, but also by its surface finish. The surface roughness, oxide formation, cleanliness, and plating homogeneity and porosity are just a few of the surface properties than can influence the performance of a wire product. Coupled to this is the large amount of surface area generated in drawing wire. For example, a ten pound spool holds nine miles of 0.006″ diameter stainless steel wire. For these reasons surface analysis has become important both to the manufacturer and consumer of wire products. When surface analysis equipment such as AES, ESCA, and SIMS was first becoming commercially available in the late sixties and early seventies, the wire industry was beginning to enter a phase of technological development for many of its products. Wire manufacturers and users began using surface analysis to investigate such topics as adhesion of brass plated automobile tire cord to rubber and diffusion of layered deposits. Examples of surface analysis used for process control, problem solving, and project development include discoloration problems on stainless steel wire, welding problems with composite wires, diffusion formed brass coatings, and diffusion problems with solder coated and Cu plated steel wire.

  11. Synthesis, Structure and Hirshfeld surface analysis, vibrational and ...

    Indian Academy of Sciences (India)

    3

    lead to the formation of a three-dimensional architecture. Hirshfeld surface analysis for visually analyzing intermolecular interactions in crystal structures employing molecular surface contours and 2D fingerprint plots have been used to scrutinize molecular shapes. The vibration properties of this structure were studied by IR ...

  12. NOAA High-Resolution Sea Surface Temperature (SST) Analysis Products

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — This archive covers two high resolution sea surface temperature (SST) analysis products developed using an optimum interpolation (OI) technique. The analyses have a...

  13. Synthesis, structure and Hirshfeld surface analysis, vibrational and ...

    Indian Academy of Sciences (India)

    dimensional architecture. Hirshfeld surface analysis for visually analysing intermolecular interactions in crystal structures employing molecular sur- face contours and 2D fingerprint plots has been used to scrutinize molecular shapes. The vibration ...

  14. Microscopic Analysis and Modeling of Airport Surface Sequencing, Phase II

    Data.gov (United States)

    National Aeronautics and Space Administration — Although a number of airportal surface models exist and have been successfully used for analysis of airportal operations, only recently has it become possible to...

  15. Microscopic Analysis and Modeling of Airport Surface Sequencing, Phase I

    Data.gov (United States)

    National Aeronautics and Space Administration — The complexity and interdependence of operations on the airport surface motivate the need for a comprehensive and detailed, yet flexible and validated analysis and...

  16. Analysis of Terminal Metallic Armor Plate Free-Surface Bulging

    National Research Council Canada - National Science Library

    Rapacki, Jr, E. J

    2008-01-01

    An analysis of the bulge formed on the free-surface of the terminal metallic plate of an armor array is shown to lead to reasonable estimates of the armor array's remaining penetration/perforation resistance...

  17. Quantitation of Surface Coating on Nanoparticles Using Thermogravimetric Analysis.

    Science.gov (United States)

    Dongargaonkar, Alpana A; Clogston, Jeffrey D

    2018-01-01

    Nanoparticles are critical components in nanomedicine and nanotherapeutic applications. Some nanoparticles, such as metallic nanoparticles, consist of a surface coating or surface modification to aid in its dispersion and stability. This surface coating may affect the behavior of nanoparticles in a biological environment, thus it is important to measure. Thermogravimetric analysis (TGA) can be used to determine the amount of coating on the surface of the nanoparticle. TGA experiments run under inert atmosphere can also be used to determine residual metal content present in the sample. In this chapter, the TGA technique and experimental method are described.

  18. Aberration analysis for freeform surface terms overlay on general decentered and tilted optical surfaces.

    Science.gov (United States)

    Yang, Tong; Cheng, Dewen; Wang, Yongtian

    2018-03-19

    Aberration theory helps designers to better understand the nature of imaging systems. However, the existing aberration theory of freeform surfaces has many limitations. For example, it only works in the special case when the central area of the freeform surface is used. In addition, the light footprint is limited to a circle, which does not match the case of an elliptical footprint for general systems. In this paper, aberrations generated by freeform surface term overlay on general decentered and tilted optical surfaces are analyzed. For the case when the off-axis section of a freeform surface is used, the aberration equation for using stop and nonstop surfaces is discussed, and the aberrations generated by Zernike terms up to Z 17/18 are analyzed in detail. To solve the problem of the elliptical light footprint for tilted freeform surfaces, the scaled pupil vector is used in the aberration analysis. The mechanism of aberration transformation is discovered, and the aberrations generated by different Zernike terms in this case are calculated. Finally we proposed aberration equations for freeform terms on general decentered and tilted freeform surfaces. The research result given in this paper offers an important reference for optical designers and engineers, and it is of great importance in developing analytical methods for general freeform system design, tolerance analysis, and system assembly.

  19. Multiscale analysis of surface morphologies by curvelet and contourlet transforms

    International Nuclear Information System (INIS)

    Li, Linfu; Zhang, Xiangchao; Zhang, Hao; He, Xiaoying; Xu, Min

    2015-01-01

    The surface topographies of precision components are critical to their functionalities. However, it is challenging to characterize the topographies of complex surfaces, especially for structured surfaces. The wavelet families are promising for the multiscale geometry analysis of nonstochastic surfaces. The second-generation curvelet transform provides a sparse representation and good multiscale decomposition for curve singularities. However, the contourlet expansion, composed of bases oriented along various directions in multiple scales with smaller redundancy rates, has a remarkable capability of representing borderlines. In this paper they are both adopted for the characterization of surface topographies. Different components can be extracted according to their scales and morphological characteristics; as a result, the corresponding manufacturing processes and functionalities can be analyzed specifically. Numerical experiments are given to demonstrate the capabilities of these methods in sparse representation and effective extraction of geometry features of different nonstochastic surfaces. (paper)

  20. Ion induced optical emission for surface and depth profile analysis

    International Nuclear Information System (INIS)

    White, C.W.

    1977-01-01

    Low-energy ion bombardment of solid surfaces results in the emission of infrared, visible, and ultraviolet radiation produced by inelastic ion-solid collision processes. The emitted optical radiation provides important insight into low-energy particle-solid interactions and provides the basis for an analysis technique which can be used for surface and depth profile analysis with high sensitivity. The different kinds of collision induced optical radiation emitted as a result of low-energy particle-solid collisions are reviewed. Line radiation arising from excited states of sputtered atoms or molecules is shown to provide the basis for surface and depth profile analysis. The spectral characteristics of this type of radiation are discussed and applications of the ion induced optical emission technique are presented. These applications include measurements of ion implant profiles, detection sensitivities for submonolayer quantities of impurities on elemental surfaces, and the detection of elemental impurities on complex organic substrates

  1. Near surface stress analysis strategies for axisymmetric fretting

    Indian Academy of Sciences (India)

    In this paper, we develop design tools for Near Surface Analysis (NSA) for understanding axisymmetric fretting. Axisymmetric Fretting Analysis (AFA) becomes formidable owing to localised tractions that call for Fourier transform techniques. We develop two different NSA strategies based on two-dimensional plane strain ...

  2. Analysis of Anomaly in Land Surface Temperature Using MODIS Products

    Science.gov (United States)

    Yorozu, K.; Kodama, T.; Kim, S.; Tachikawa, Y.; Shiiba, M.

    2011-12-01

    Atmosphere-land surface interaction plays a dominant role on the hydrologic cycle. Atmospheric phenomena cause variation of land surface state and land surface state can affect on atmosphereic conditions. Widely-known article related in atmospheric-land interaction was published by Koster et al. in 2004. The context of this article is that seasonal anomaly in soil moisture or soil surface temperature can affect summer precipitation generation and other atmospheric processes especially in middle North America, Sahel and south Asia. From not only above example but other previous research works, it is assumed that anomaly of surface state has a key factor. To investigate atmospheric-land surface interaction, it is necessary to analyze anomaly field in land surface state. In this study, soil surface temperature should be focused because it can be globally and continuously observed by satellite launched sensor. To land surface temperature product, MOD11C1 and MYD11C1 products which are kinds of MODIS products are applied. Both of them have 0.05 degree spatial resolution and daily temporal resolution. The difference of them is launched satellite, MOD11C1 is Terra and MYD11C1 is Aqua. MOD11C1 covers the latter of 2000 to present and MYD11C1 covers the early 2002 to present. There are unrealistic values on provided products even if daily product was already calibrated or corrected. For pre-analyzing, daily data is aggregated into 8-days data to remove irregular values for stable analysis. It was found that there are spatial and temporal distribution of 10-years average and standard deviation for each 8-days term. In order to point out extreme anomaly in land surface temperature, standard score for each 8-days term is applied. From the analysis of standard score, it is found there are large anomaly in land surface temperature around north China plain in early April 2005 and around Bangladesh in early May 2009.

  3. Contribution of surface analysis spectroscopic methods to the lubrication field

    International Nuclear Information System (INIS)

    Blanc, C.

    1979-01-01

    The analytical surface technics such as ESCA, AES and SIMS are tested to be applied to a particular lubrication field. One deals with a 100 C 6 steel surface innumered in tricresylphosphate at 110 0 C for 15 days. The nature of the first layers is studied after relevant solvant cleaning. An iron oxide layer is produced on the bearing surface, namely αFe 2 -O 3 . ESCA, AES and SIMS studies show an overlayer of iron phosphate. The exact nature of iron phosphate is not clearly established but the formation of a ferrous phosphate coating can be assumed from ESCA analysis [fr

  4. Autonomous Aerobraking: Thermal Analysis and Response Surface Development

    Science.gov (United States)

    Dec, John A.; Thornblom, Mark N.

    2011-01-01

    A high-fidelity thermal model of the Mars Reconnaissance Orbiter was developed for use in an autonomous aerobraking simulation study. Response surface equations were derived from the high-fidelity thermal model and integrated into the autonomous aerobraking simulation software. The high-fidelity thermal model was developed using the Thermal Desktop software and used in all phases of the analysis. The use of Thermal Desktop exclusively, represented a change from previously developed aerobraking thermal analysis methodologies. Comparisons were made between the Thermal Desktop solutions and those developed for the previous aerobraking thermal analyses performed on the Mars Reconnaissance Orbiter during aerobraking operations. A variable sensitivity screening study was performed to reduce the number of variables carried in the response surface equations. Thermal analysis and response surface equation development were performed for autonomous aerobraking missions at Mars and Venus.

  5. Glass fibres reinforced polyester composites degradation monitoring by surface analysis

    Energy Technology Data Exchange (ETDEWEB)

    Croitoru, Catalin [“Transilvania” University of Brasov, Materials Engineering and Welding Department, Eroilor 29 Str., 500036 Brasov (Romania); Patachia, Silvia, E-mail: st.patachia@unitbv.ro [“Transilvania” University of Brasov, Product Design Environment and Mechatronics Department, Eroilor 29 Str., 500036 Brasov (Romania); Papancea, Adina [“Transilvania” University of Brasov, Product Design Environment and Mechatronics Department, Eroilor 29 Str., 500036 Brasov (Romania); Baltes, Liana; Tierean, Mircea [“Transilvania” University of Brasov, Materials Engineering and Welding Department, Eroilor 29 Str., 500036 Brasov (Romania)

    2015-12-15

    Highlights: • Glass fibre-reinforced polyester composites surface analysis by photographic method. • The composites are submitted to accelerated ageing by UV irradiation at 254 nm. • The UV irradiation promotes differences in the surface chemistry of the composites. • MB dye is differently adsorbed on surfaces with different degradation degrees. • Good correlation between the colouring degree and surface chemistry. - Abstract: The paper presents a novel method for quantification of the modifications that occur on the surface of different types of gel-coated glass fibre-reinforced polyester composites under artificial UV-ageing at 254 nm. The method implies the adsorption of an ionic dye, namely methylene blue, on the UV-aged composite, and computing the CIELab colour space parameters from the photographic image of the coloured composite's surface. The method significantly enhances the colour differences between the irradiated composites and the reference, in contrast with the non-coloured ones. The colour modifications that occur represent a good indicative of the surface degradation, alteration of surface hydrophily and roughness of the composite and are in good correlation with the ATR-FTIR spectroscopy and optical microscopy results. The proposed method is easier, faster and cheaper than the traditional ones.

  6. Ion beam analysis of metal ion implanted surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Evans, P.J.; Chu, J.W.; Johnson, E.P.; Noorman, J.T. [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia); Sood, D.K. [Royal Melbourne Inst. of Tech., VIC (Australia)

    1993-12-31

    Ion implantation is an established method for altering the surface properties of many materials. While a variety of analytical techniques are available for the characterisation of implanted surfaces, those based on particle accelerators such as Rutherford backscattering (RBS) and nuclear reaction analysis (NRA) provide some of the most useful and powerful for this purpose. Application of the latter techniques to metal ion implantation research at ANSTO will be described with particular reference to specific examples from recent studies. Where possible, the information obtained from ion beam analysis will be compared with that derived from other techniques such as Energy Dispersive X-ray (EDX) and Auger spectroscopies. 4 refs., 5 figs.

  7. Analysis of passive surface-wave noise in surface microseismic data and its implications

    Science.gov (United States)

    Forghani-Arani, F.; Willis, M.; Haines, S.; Batzle, M.; Davidson, M.

    2011-01-01

    Tight gas reservoirs are projected to be a major portion of future energy resources. Because of their low permeability, hydraulic fracturing of these reservoirs is required to improve the permeability and reservoir productivity. Passive seismic monitoring is one of the few tools that can be used to characterize the changes in the reservoir due to hydraulic fracturing. Although the majority of the studies monitoring hydraulic fracturing exploit down hole microseismic data, surface microseismic monitoring is receiving increased attention because it is potentially much less expensive to acquire. Due to a broader receiver aperture and spatial coverage, surface microseismic data may be more advantageous than down hole microseismic data. The effectiveness of this monitoring technique, however, is strongly dependent on the signal-to-noise ratio of the data. Cultural and ambient noise can mask parts of the waveform that carry information about the subsurface, thereby decreasing the effectiveness of surface microseismic analysis in identifying and locating the microseismic events. Hence, time and spatially varying suppression of the surface-wave noise ground roll is a critical step in surface microseismic monitoring. Here, we study a surface passive dataset that was acquired over a Barnett Shale Formation reservoir during two weeks of hydraulic fracturing, in order to characterize and suppress the surface noise in this data. We apply techniques to identify the characteristics of the passive ground roll. Exploiting those characteristics, we can apply effective noise suppression techniques to the passive data. ?? 2011 Society of Exploration Geophysicists.

  8. Generalized surface momentum balances for the analysis of surface dilatational data

    NARCIS (Netherlands)

    Sagis, L.M.C.

    2013-01-01

    Dilatational rheological properties of interfaces are often determined using drop tensiometers, in which the interface of the droplet is subjected to oscillatory area changes. A dynamic surface tension is determined either by image analysis of the droplet profile or by measuring the capillary

  9. Surface composition of biomedical components by ion beam analysis

    International Nuclear Information System (INIS)

    Kenny, M.J.; Wielunski, L.S.; Baxter, G.R.

    1991-01-01

    Materials used for replacement body parts must satisfy a number of requirements such as biocompatibility and mechanical ability to handle the task with regard to strength, wear and durability. When using a CVD coated carbon fibre reinforced carbon ball, the surface must be ion implanted with uniform dose of nitrogen ions in order to make it wear resistant. The mechanism by which the wear resistance is improved is one of radiation damage and the required dose of about 10 16 cm -2 can have a tolerance of about 20%. To implant a spherical surface requires manipulation of the sample within the beam and control system (either computer or manually operated) to enable uniform dose all the way from polar to equatorial regions on the surface. A manipulator has been designed and built for this purpose. In order to establish whether the dose is uniform, nuclear reaction analysis using the reaction 14 N(d,α) 12 C is an ideal method of profiling. By taking measurements at a number of points on the surface, the uniformity of nitrogen dose can be ascertained. It is concluded that both Rutherford Backscattering and Nuclear Reaction Analysis can be used for rapid analysis of surface composition of carbon based materials used for replacement body components. 2 refs., 2 figs

  10. Surface analysis of graphite fiber reinforced polyimide composites

    Science.gov (United States)

    Messick, D. L.; Progar, D. J.; Wightman, J. P.

    1983-01-01

    Several techniques have been used to establish the effect of different surface pretreatments on graphite-polyimide composites. Composites were prepared from Celion 6000 graphite fibers and the polyimide LARC-160. Pretreatments included mechanical abrasion, chemical etching and light irradiation. Scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS) were used in the analysis. Contact angle of five different liquids of varying surface tensions were measured on the composites. SEM results showed polymer-rich peaks and polymer-poor valleys conforming to the pattern of the release cloth used durng fabrication. Mechanically treated and light irradiated samples showed varying degrees of polymer peak removal, with some degradation down to the graphite fibers. Minimal changes in surface topography were observed on concentrations of surface fluorine even after pretreatment. The light irradiation pretreatment was most effective at reducing surface fluorine concentrations whereas chemical pretreatment was the least effective. Critical surface tensions correlated directly with the surface fluorine to carbon ratios as calculated from XPS.

  11. Analysis of surface degradation of high density polyethylene (HDPE ...

    Indian Academy of Sciences (India)

    Unknown

    Analysis of surface degradation of high density polyethylene (HDPE) insulation ... ammonium chloride as the contaminant, in high density polyethylene ..... liquid in the material. When diffusion is driven by the concentration gradient and if there is no chemical change between liquid and material, this would result in mass.

  12. Synthesis, structure and Hirshfeld surface analysis, vibrational and ...

    Indian Academy of Sciences (India)

    Hirshfeld surface analysis for visually analysing intermolecular interactions in crystal structures employing molecular surfacecontours and 2D fingerprint plots has been used to scrutinize molecular shapes. The vibration properties of this structure were studied by IR spectroscopy and Raman scattering. Vibration spectra ...

  13. Indian Ocean surface winds from NCMRWF analysis as compared to ...

    Indian Academy of Sciences (India)

    R. Narasimhan (Krishtel eMaging) 1461 1996 Oct 15 13:05:22

    Indian Ocean surface winds from NCMRWF analysis as compared to QuikSCAT and moored buoy winds. B N Goswami1 and E N Rajagopal2. 1Centre for Atmospheric and Oceanic Sciences, Indian Institute of Science, Bangalore 560 012, India. 2National Centre for Medium Range Weather Forecasting, Department of ...

  14. Difraction analysis of iron materials after surface machining

    Czech Academy of Sciences Publication Activity Database

    Čerňanský, Marian; Ganev, N.; Barcal, J.; Drahokoupil, Jan; Kolařík, K.

    2006-01-01

    Roč. 2006, suppl. 23 (2006), s. 369-374 ISSN 0044-2968 Institutional research plan: CEZ:AV0Z10100520 Keywords : iron materials * surface treatment * size-strain * residual stress * phase analysis Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.897, year: 2006

  15. Boundary surface and microstructure analysis of ceramic materials

    International Nuclear Information System (INIS)

    Woltersdorf, J.; Pippel, E.

    1992-01-01

    The article introduces the many possibilities of high voltage (HVEM) and high resolution electron microscopy (HREM) for boundary surface and microstructure analysis of ceramic materials. The investigations are limited to ceramic long fibre composites and a ceramic fibre/glass matrix system. (DG) [de

  16. Hirschfeld surface analysis of two new phosporothioic triamides structures

    Czech Academy of Sciences Publication Activity Database

    Alamdar, A.H.; Pourayoubi, M.; Saneei, A.; Dušek, Michal; Kučeráková, Monika; Henriques, Margarida Isabel Sousa

    2015-01-01

    Roč. 71, č. 9 (2015), s. 824-833 ISSN 2053-2296 R&D Projects: GA ČR(CZ) GA14-03276S Institutional support: RVO:68378271 Keywords : phosphorothioic triamide * Hirshfeld surface analysis * two-dimensional fingerprint plot * crystal structure * hydrogen-bonding pattern. Subject RIV: CC - Organic Chemistry Impact factor: 0.479, year: 2015

  17. Surface analysis of DLC coating on cam-tappet system

    OpenAIRE

    FOUVRY, Siegfried; PAGNOUX, Geoffrey; PEIGNEY, Michael; DELATTRE, Benoit; MERMAT-ROLLET, Guillaume

    2013-01-01

    Tribomechanical properties of diamond-like carbon (DLC) coatings make them particularly interesting for numerous applications, like automotive ones. But although DLC coatings show a generally high wear resistance, they sometimes can exhibit severe multiple wear. In this study, a surface analysis of worn coated tappets is performed, leading to a complete coupled wear scenario.

  18. Surface water quality assessment using factor analysis | Boyacioglu ...

    African Journals Online (AJOL)

    In this study, the factor analysis technique is applied to surface water quality data sets obtained from the Buyuk Menderes River Basin, Turkey, during two different hydrological periods. Results show that the indices which changed the quality of water in two seasons and locations differed. During low-flow conditions, water ...

  19. Corrected Debye-Hückel analysis of surface complexation. II. A theory of surface charging.

    Science.gov (United States)

    Gunnarsson, Magnus; Abbas, Zareen; Ahlberg, Elisabet; Gobom, Sylvia; Nordholm, Sture

    2002-05-01

    A theory of surface charging of colloidal particles suspended in an electrolyte solution is presented. The charging at the particle surface is assumed to originate from the adsorption and desorption of protons and is therefore strongly dependent on the acidity of the solution. The surface binding of protons occurs locally at sites of occupancy zero or one that are described by a binding energy u(0) and a three-dimensional vibration of frequency nu. The diffuse screening of ions at the surface is described by the corrected Debye-Hückel analysis assuming linear response. The model contains a capacitor layer close to the charged surface and the finite size of the electrolyte ions is taken into account. The theory has been applied to titrated surface charge data on goethite (alpha-FeOOH) at NaClO(4) background concentrations ranging from 0.01 to 1.0 M. The protonation mechanism used in the modeling of these data corresponds to the 1-pK approach. A very good description of the experimental data was obtained at the highest ionic strength. Close to the pH(pzc) the theory also gave a good description at lower ionic strengths. However, at low salt concentrations and pH values far away from the pH(pzc) the electrostatic potential outside the capacitor layer becomes so high that nonlinear electrostatic effects become important and the theory therefore underestimates the surface charge. These results were compared with model calculations obtained using existing surface complexation models.

  20. SURFACE ELECTROMYOGRAPHY IN BIOMECHANICS: APPLICATIONS AND SIGNAL ANALYSIS ASPECTS

    Directory of Open Access Journals (Sweden)

    DEAK GRAłIELA-FLAVIA

    2009-12-01

    Full Text Available Surface electromyography (SEMG is a technique for detecting and recording the electrical activity of the muscles using surface electrodes. The EMG signal is used in biomechanics mainly as an indicator of the initiation of muscle activation, as an indicator of the force produced by a contracting muscle, and as an index ofthe fatigue occurring within a muscle. EMG, used as a method of investigation, can tell us if the muscle is active or not, if the muscle is more or less active, when it is on or off, how much active is it, and finally, if it fatigues.The purpose of this article is to discuss some specific EMG signal analysis aspects with emphasis on comparison type analysis and frequency fatigue analysis.

  1. A Probabilistic Analysis of Surface Water Flood Risk in London.

    Science.gov (United States)

    Jenkins, Katie; Hall, Jim; Glenis, Vassilis; Kilsby, Chris

    2017-10-30

    Flooding in urban areas during heavy rainfall, often characterized by short duration and high-intensity events, is known as "surface water flooding." Analyzing surface water flood risk is complex as it requires understanding of biophysical and human factors, such as the localized scale and nature of heavy precipitation events, characteristics of the urban area affected (including detailed topography and drainage networks), and the spatial distribution of economic and social vulnerability. Climate change is recognized as having the potential to enhance the intensity and frequency of heavy rainfall events. This study develops a methodology to link high spatial resolution probabilistic projections of hourly precipitation with detailed surface water flood depth maps and characterization of urban vulnerability to estimate surface water flood risk. It incorporates probabilistic information on the range of uncertainties in future precipitation in a changing climate. The method is applied to a case study of Greater London and highlights that both the frequency and spatial extent of surface water flood events are set to increase under future climate change. The expected annual damage from surface water flooding is estimated to be to be £171 million, £343 million, and £390 million/year under the baseline, 2030 high, and 2050 high climate change scenarios, respectively. © 2017 Society for Risk Analysis.

  2. Data Analysis Techniques for a Lunar Surface Navigation System Testbed

    Science.gov (United States)

    Chelmins, David; Sands, O. Scott; Swank, Aaron

    2011-01-01

    NASA is interested in finding new methods of surface navigation to allow astronauts to navigate on the lunar surface. In support of the Vision for Space Exploration, the NASA Glenn Research Center developed the Lunar Extra-Vehicular Activity Crewmember Location Determination System and performed testing at the Desert Research and Technology Studies event in 2009. A significant amount of sensor data was recorded during nine tests performed with six test subjects. This paper provides the procedure, formulas, and techniques for data analysis, as well as commentary on applications.

  3. Analysis of leaf surfaces using scanning ion conductance microscopy.

    Science.gov (United States)

    Walker, Shaun C; Allen, Stephanie; Bell, Gordon; Roberts, Clive J

    2015-05-01

    Leaf surfaces are highly complex functional systems with well defined chemistry and structure dictating the barrier and transport properties of the leaf cuticle. It is a significant imaging challenge to analyse the very thin and often complex wax-like leaf cuticle morphology in their natural state. Scanning electron microscopy (SEM) and to a lesser extent Atomic force microscopy are techniques that have been used to study the leaf surface but their remains information that is difficult to obtain via these approaches. SEM is able to produce highly detailed and high-resolution images needed to study leaf structures at the submicron level. It typically operates in a vacuum or low pressure environment and as a consequence is generally unable to deal with the in situ analysis of dynamic surface events at submicron scales. Atomic force microscopy also possess the high-resolution imaging required and can follow dynamic events in ambient and liquid environments, but can over exaggerate small features and cannot image most leaf surfaces due to their inherent roughness at the micron scale. Scanning ion conductance microscopy (SICM), which operates in a liquid environment, provides a potential complementary analytical approach able to address these issues and which is yet to be explored for studying leaf surfaces. Here we illustrate the potential of SICM on various leaf surfaces and compare the data to SEM and atomic force microscopy images on the same samples. In achieving successful imaging we also show that SICM can be used to study the wetting of hydrophobic surfaces in situ. This has potentially wider implications than the study of leaves alone as surface wetting phenomena are important in a range of fundamental and applied studies. © 2015 The Authors Journal of Microscopy © 2015 Royal Microscopical Society.

  4. In situ surface-enhanced Raman spectroelectrochemical analysis system with a hemin modified nanostructured gold surface.

    Science.gov (United States)

    Yuan, Tao; Le Thi Ngoc, Loan; van Nieuwkasteele, Jan; Odijk, Mathieu; van den Berg, Albert; Permentier, Hjalmar; Bischoff, Rainer; Carlen, Edwin T

    2015-03-03

    An integrated surface-enhanced Raman scattering (SERS) spectroelectrochemical (SEC) analysis system is presented that combines a small volume microfluidic sample chamber (Raman spectroelectrochemistry. The SEC system includes a nanostructured Au surface that serves dual roles as the electrochemical working electrode (WE) and SERS substrate, a microfabricated Pt counter electrode (CE), and an external Ag/AgCl reference electrode (RE). The nanostructured Au WE enables highly sensitive in situ SERS spectroscopy through large and reproducible SERS enhancements, which eliminates the need for resonant wavelength matching of the laser excitation source with the electronic absorption of the target molecule. The new SEC analysis system has the merits of wide applicability to target molecules, small sample volume, and a low detection limit. We demonstrate in situ SERS spectroelectrochemistry measurements of the metalloporphyrin hemin showing shifts of the iron oxidation marker band ν4 with the nanostructured Au working electrode under precise potential control.

  5. A description of the BNL active surface analysis facility

    International Nuclear Information System (INIS)

    Tyler, J.W.

    1989-11-01

    Berkeley Nuclear Laboratories has a responsibility for the assessment of radioactive specimens arising both from post irradiation examination of power reactor components and structures and experimental programmes concerned with fission and activation product transport. Existing analytical facilities have been extended with the commissioning of an active surface analysis instrument (XSAM 800pci, Kratos Analytical). Surface analysis involves the characterisation of the outer few atomic layers of a solid surface/interface whose chemical composition and electronic structure will probably be different from the bulk. The new instrument consists three interconnected chambers positioned in series; comprising of a high vacuum sample introduction chamber, an ultra-high vacuum sample treatment/fracture chamber and an ultra-high vacuum sample analysis chamber. The sample analysis chamber contains the electron, X-ray and ion-guns and the electron and ion detectors necessary for performing X-ray photoelectron spectroscopy, scanning Auger microscopy and secondary-ion mass spectroscopy. The chamber also contains a high stability manipulator to enable sub-micron imaging of specimens to be achieved and provide sample heating and cooling between - 180 and 600 0 C. (author)

  6. Analysis of surface hardness of artificially aged resin composites

    Directory of Open Access Journals (Sweden)

    Denise Cremonezzi Tornavoi

    2012-02-01

    Full Text Available This study evaluated the effect of artificially accelerated aging (AAA on the surface hardness of eight composite resins: Filtek Z250, Filtek Supreme, 4 Seasons, Herculite, P60, Tetric Ceram, Charisma, and Filtek Z100. Sixteen specimens were made from the test piece of each material, using an 8.0 × 2.0 mm teflon matrix. After 24 hours, eight specimens from each material were submitted to three surface hardness readings using a Shimadzu Microhardness Tester for 5 seconds at a load of 50 gf. The other eight specimens remained in the artificially accelerated aging machine for 382 hours and were submitted to the same surface hardness analysis. The means of each test specimen were submitted to the Kolmogorov-Smirnov test (p > 0.05, ANOVA and Tukey test (p < 0.05. With regard to hardness (F = 86.74, p < 0.0001 the analysis showed significant differences among the resin composite brands. But aging did not influence the hardness of any of the resin composites (F = 0.39, p = 0.53. In this study, there was interaction between the resin composite brand and the aging factors (F = 4.51, p < 0.0002. It was concluded that notwithstanding the type of resin, AAA did not influence surface hardness. However, with regard to hardness there was a significant difference among the resin brands.

  7. Satellite Based Analysis of Surface Urban Heat Island Intensity

    Directory of Open Access Journals (Sweden)

    Gémes Orsolya

    2016-06-01

    Full Text Available The most obvious characteristics of urban climate are higher air and surface temperatures compared to rural areas and large spatial variation of meteorological parameters within the city. This research examines the long term and seasonal development of urban surface temperature using satellite data during a period of 30 years and within a year. The medium resolution Landsat data were (preprocessed using open source tools. Besides the analysis of the long term and seasonal changes in land surface temperature within a city, also its relationship with changes in the vegetation cover was investigated. Different urban districts and local climate zones showed varying strength of correlation. The temperature difference between urban surfaces and surroundings is defined as surface urban heat island (SUHI. Its development shows remarkable seasonal and spatial anomalies. The satellite images can be applied to visualize and analyze the SUHI, although they were not collected at midday and early afternoon, when the phenomenon is normally at its maximum. The applied methodology is based on free data and software and requires minimal user interaction. Using the results new urban developments (new built up and green areas can be planned, that help mitigate the negative effects of urban climate.

  8. In Vitro Analysis of Fibronectin-Modified Titanium Surfaces

    Science.gov (United States)

    Chang, Yu-Chi; Lee, Wei-Fang; Feng, Sheng-Wei; Huang, Haw-Ming; Lin, Che-Tong; Teng, Nai-Chia; Chang, Wei Jen

    2016-01-01

    Background Glow discharge plasma (GDP) procedure is an effective method for grafting various proteins, including albumin, type I collagen, and fibronectin, onto a titanium surface. However, the behavior and impact of titanium (Ti) surface modification is yet to be unraveled. Purpose The purpose of this study is to evaluate and analyze the biological properties of fibronectin-grafted Ti surfaces treated by GDP. Materials and Methods Grade II Ti discs were initially cleaned and autoclaved to obtain original specimens. Subsequently, the specimens were GDP treated and grafted with fibronectin to form Ar-GDP (Argon GDP treatment only) and GDP-fib (fibronectin coating following GDP treatment) groups. Blood coagulation test and MG-63 cell culture were performed to evaluate the biological effects on the specimen. Results There was no significant difference between Ar-GDP and GDP-fib groups in blood compatibility analysis. While in the MTT test, cellular proliferation was benefited from the presence of fibronectin coating. The numbers of cells on Ar-GDP and GDP-fib specimens were greater than those in the original specimens after 24 h of culturing. Conclusions GDP treatment combined with fibronectin grafting favored MG-63 cell adhesion, migration, and proliferation on titanium surfaces, which could be attributed to the improved surface properties. PMID:26731536

  9. Automated analysis of damages for radiation in plastics surfaces

    International Nuclear Information System (INIS)

    Andrade, C.; Camacho M, E.; Tavera, L.; Balcazar, M.

    1990-02-01

    Analysis of damages done by the radiation in a polymer characterized by optic properties of polished surfaces, of uniformity and chemical resistance that the acrylic; resistant until the 150 centigrade grades of temperature, and with an approximate weight of half of the glass. An objective of this work is the development of a method that analyze in automated form the superficial damages induced by radiation in plastic materials means an images analyst. (Author)

  10. Market basket analysis visualization on a spherical surface

    Science.gov (United States)

    Hao, Ming C.; Hsu, Meichun; Dayal, Umeshwar; Wei, Shu F.; Sprenger, Thomas; Holenstein, Thomas

    2001-05-01

    This paper discusses the visualization of the relationships in e-commerce transactions. To date, many practical research projects have shown the usefulness of a physics-based mass- spring technique to layout data items with close relationships on a graph. We describe a market basket analysis visualization system using this technique. This system is described as the following: (1) integrates a physics-based engine into a visual data mining platform; (2) use a 3D spherical surface to visualize the cluster of related data items; and (3) for large volumes of transactions, uses hidden structures to unclutter the display. Several examples of market basket analysis are also provided.

  11. Analysis of polymer surfaces and thin-film coatings with Raman and surface enhanced Raman scattering

    CERN Document Server

    McAnally, G D

    2001-01-01

    This thesis investigates the potential of surface-enhanced Raman scattering (SERS) for the analysis and characterisation of polymer surfaces. The Raman and SERS spectra from a PET film are presented. The SERS spectra from the related polyester PBT and from the monomer DMT are identical to PET, showing that only the aromatic signals are enhanced. Evidence from other compounds is presented to show that loss of the carbonyl stretch (1725 cm sup - sup 1) from the spectra is due to a chemical interaction between the silver and surface carbonyl groups. The interaction of other polymer functional groups with silver is discussed. A comparison of Raman and SERS spectra collected from three faces of a single crystal shows the SERS spectra are depolarised. AFM images of the silver films used to obtain SERS are presented. They consist of regular islands of silver, fused together to form a complete film. The stability and reproducibility and of these surfaces is assessed. Band assignments for the SERS spectrum of PET are ...

  12. Analysis of polymer surfaces and thin-film coatings with Raman and surface enhanced Raman scattering

    International Nuclear Information System (INIS)

    McAnally, Gerard David

    2001-01-01

    This thesis investigates the potential of surface-enhanced Raman scattering (SERS) for the analysis and characterisation of polymer surfaces. The Raman and SERS spectra from a PET film are presented. The SERS spectra from the related polyester PBT and from the monomer DMT are identical to PET, showing that only the aromatic signals are enhanced. Evidence from other compounds is presented to show that loss of the carbonyl stretch (1725 cm -1 ) from the spectra is due to a chemical interaction between the silver and surface carbonyl groups. The interaction of other polymer functional groups with silver is discussed. A comparison of Raman and SERS spectra collected from three faces of a single crystal shows the SERS spectra are depolarised. AFM images of the silver films used to obtain SERS are presented. They consist of regular islands of silver, fused together to form a complete film. The stability and reproducibility and of these surfaces is assessed. Band assignments for the SERS spectrum of PET are presented. A new band in the spectrum (1131 cm -1 ) is assigned to a complex vibration using a density functional calculation. Depth profiling through a polymer film on to the silver layer showed the SERS signals arise from the silver surface only. The profiles show the effects of refraction on the beam, and the adverse affect on the depth resolution. Silver films were used to obtain SERS spectra from a 40 nm thin-film coating on PET, without interference from the PET layer. The use of an azo dye probe as a marker to detect the coating is described. Finally, a novel method for the synthesis of a SERS-active vinyl-benzotriazole monomer is reported. The monomer was incorporated into a thin-film coating and the SERS spectrum obtained from the polymer. (author)

  13. Contribution of Microchemical Surface Analysis of Archaeological Artefacts

    Science.gov (United States)

    Mousser, H.; Madani, A.; Amri, R.; Mousser, A.; Darchen, A.

    2009-11-01

    Museum CIRTA of the town of Constantine has a collection of more than 35000 coins and statuettes going back to Numide, Roman, Republican, Vandal and Byzantine times and is struck in the name of the cities, of the kingdoms and the empires. Surface analysis of these coins gives information about the chemical composition and leads to recommendations for restoration and preservations. This work is a contribution of microchemical surface study of coin with the effigy of the Numide King Massinissa (Constantine between 3rd and 2nd century before Jesus Christ). The photographic and scanning electron microscopy coupled with energy dispersive spectrometry (SEM + EDS) and diffraction of X-ray (DRX) was used. The optic microscopy (OMP) and SEM pictures of coins showed heterogeneous surface. Scanning electron microscopy coupled with energy dispersive spectrometry identified three basic metals copper (46.06%), antimony (17.74%) and lead (12.06%), (Weight Percentage). The DRX identifies stages (copper and lead) and their crystalline oxides Bindheimite (Pb2Sb2O7) and Bystromite (MgSb2O6) on the coin's surface.

  14. Coastal surface water suitability analysis for irrigation in Bangladesh

    Science.gov (United States)

    Mahtab, Mohammad Hossain; Zahid, Anwar

    2018-03-01

    Water with adequate quality and quantity is very important for irrigation to ensure the crop yields. Salinity is common problem in the coastal waters in Bangladesh. The intensity of salinity in the coastal zone in Bangladesh is not same. It fluctuates over the year. Sodium is another hazard which may hamper permeability and ultimately affects the fertility. It can reduce the crop yields. Although surface water is available in the coastal zone of Bangladesh, but its quality for irrigation needs to be monitored over the year. This paper will investigate the overall quality of coastal surface waters. Thirty-three water samples from different rivers were collected both in wet period (October-December) and in dry period (February-April). Different physical and chemical parameters are considered for investigation of the adequacy of water with respect to international irrigation water quality standards and Bangladesh standards. A comparison between the dry and wet period coastal surface water quality in Bangladesh will also be drawn here. The analysis shows that coastal surface water in Bangladesh is overall suitable for irrigation during wet period, while it needs treatment (which will increase the irrigation cost) for using for irrigation during dry period. Adaptation to this situation can improve the scenario. An integrated plan should be taken to increase the water storing capacity in the coastal area to harvest water during wet period.

  15. Rate law analysis of water oxidation on a hematite surface.

    Science.gov (United States)

    Le Formal, Florian; Pastor, Ernest; Tilley, S David; Mesa, Camilo A; Pendlebury, Stephanie R; Grätzel, Michael; Durrant, James R

    2015-05-27

    Water oxidation is a key chemical reaction, central to both biological photosynthesis and artificial solar fuel synthesis strategies. Despite recent progress on the structure of the natural catalytic site, and on inorganic catalyst function, determining the mechanistic details of this multiredox reaction remains a significant challenge. We report herein a rate law analysis of the order of water oxidation as a function of surface hole density on a hematite photoanode employing photoinduced absorption spectroscopy. Our study reveals a transition from a slow, first order reaction at low accumulated hole density to a faster, third order mechanism once the surface hole density is sufficient to enable the oxidation of nearest neighbor metal atoms. This study thus provides direct evidence for the multihole catalysis of water oxidation by hematite, and demonstrates the hole accumulation level required to achieve this, leading to key insights both for reaction mechanism and strategies to enhance function.

  16. Statistical Analysis of Magnetic Abrasive Finishing (MAF) On Surface Roughness

    Science.gov (United States)

    Givi, Mehrdad; Tehrani, Alireza Fadaei; Mohammadi, Aminollah

    2010-06-01

    Magnetic assisted finishing is one of the nontraditional methods of polishing that recently has been attractive for the researchers. This paper investigates the effects of some parameters such as rotational speed of the permanent magnetic pole, work gap between the permanent pole and the work piece, number of the cycles and the weight of the abrasive particles on aluminum surface plate finishing. The three levels full factorial method was used as the DOE technique (design of experiments) for studying the selected factors. Analysis of Variance (ANOVA) has been used to determine significant factors and also to obtain an equation based on data regression. Experimental results indicate that for a change in surface roughness ΔRa, number of cycles and working gap are found to be the most significant parameters followed by rotational speed and then weight of powders.

  17. Storage fee analysis for a retrievable surface storage facility

    International Nuclear Information System (INIS)

    Field, B.B.; Rosnick, C.K.

    1973-12-01

    Conceptual design studies are in progress for a Water Basin Concept (WBC) and an alternative Sealed Storage Cask Concept (SSCC) of a Retrievable Surface Storage Facility (RSSF) intended as a Federal government facility for storing high-level radioactive wastes until a permanent disposal method is established. The RSSF will be a man-made facility with a design life of at least 100 y, and will have capacity to store all of the high-level waste from the reprocessing of nuclear power plant spent fuels generated by the industry through the year 2000. This report is a basic version of ARH-2746, ''Retrievable Surface Storage Facility, Water Basin Concept, User Charge Analysis.'' It is concerned with the issue of establishing a fee to cover the cost of storing nuclear wastes both in the RSSF and at the subsequent disposal facility. (U.S.)

  18. Bio-inspired nanotechnology from surface analysis to applications

    CERN Document Server

    Walsh, Tiffany

    2014-01-01

    This book focuses on the use of bio-inspired and biomimetic methods for the fabrication and activation of nanomaterials. This includes studies concerning the binding of the biomolecules to the surface of inorganic structures, structure/function relationships of the final materials, and extensive discussions on the final applications of such biomimetic materials in unique applications including energy harvesting/storage, biomedical diagnostics, and materials assembly. This book also: ·          Covers the sustainable features of bio-inspired nanotechnology ·          Includes studies on the unique applications of biomimetic materials, such as energy harvesting and biomedical diagnostics Bio-Inspired Nanotechnology: From Surface Analysis to Applications is an ideal book for researchers, students, nanomaterials engineers, bioengineers, chemists, biologists, physicists, and medical researchers.

  19. Analysis and design of functional micro/nano structured surfaces

    Science.gov (United States)

    Xu, Zhenzhen; Kong, Lingbao; Xu, Min

    2016-03-01

    In recent years, more and more attention has been paid to the bionic structure and functional materials. The theoretical research and fabricating ways of the Super-hydrophobic surface have sound achievements. However, the existing methods largely depend on the precision of the equipment and complex chemical substances, and it is hard to ensure the consistence of the material surface. Therefore, construction of microstructure on the surface of the material by using the method of mechanical processing to make the scale of the Super-hydrophobic surface to promote the popularization and application of Super-hydrophobic surface is of great significance. In order to put forward the innovative microstructure and to provide theoretical basis for the subsequent mechanical processing, based on the analysis of the classical theory of Super-hydrophobic, the super-hydrophobic film was by sol gel method. To explore the effects of different ratio of materials on the hydrophobicity, a micro/nano-structured super-hydrophobic coating was obtained by coating a film improved by hexamethyldisilazane (HMDS) after a film improved by polyethylene glycol (PEG) was coated. The microstructure of bilayer films is analyzed, and the double-layer film structure is simplified to design two kinds of microstructure models. For the design of the two models based on the Wenzel and Cassie equations, a roughness factor is adopted to establish the quantitative relationship between the contact angle and the microstructure parameters, and the microstructure parameters is also analyzed by using MATLAB software, and hence the optimized microstructure parameters is obtained.

  20. Morphological characteristics of primary enamel surfaces versus permanent enamel surfaces: SEM digital analysis.

    Science.gov (United States)

    Lucchese, A; Storti, E

    2011-09-01

    The morphology of permanent and primary enamel surface merits further analysis. The objective of this study was to illustrate a method of SEM digital image processing able to quantify and discriminate between the morphological characteristics of primary and permanent tooth enamel. Sixteen extracted teeth, 8 primary teeth and 8 permanent teeth, kept in saline solution, were analysed. The teeth were observed under SEM. The SEM images were analysed by means of digitally processed algorithms. The two algorithms used were: Local standard deviation to measure surface roughness with the roughness index (RI); Hough's theorem to identify linear structures with the linear structure index (LSI). The SEM images of primary teeth enamel show smooth enamel with little areas of irregularity. No linear structures are apparent. The SEM images of permanent enamel show a not perfectly smooth surface; there are furrows and irregularities of variable depth and width. In the clinical practice a number of different situations require the removal of a thin layer of enamel. Only a good morphological knowledge of both permanent and primary tooth enamel gives the opportunity to identify and exploit the effects of rotary tools on enamel, thus allowing for a correct finishing technique.

  1. Multi-channel Analysis of Passive Surface Waves (MAPS)

    Science.gov (United States)

    Xia, J.; Cheng, F. Mr; Xu, Z.; Wang, L.; Shen, C.; Liu, R.; Pan, Y.; Mi, B.; Hu, Y.

    2017-12-01

    Urbanization is an inevitable trend in modernization of human society. In the end of 2013 the Chinese Central Government launched a national urbanization plan—"Three 100 Million People", which aggressively and steadily pushes forward urbanization. Based on the plan, by 2020, approximately 100 million people from rural areas will permanently settle in towns, dwelling conditions of about 100 million people in towns and villages will be improved, and about 100 million people in the central and western China will permanently settle in towns. China's urbanization process will run at the highest speed in the urbanization history of China. Environmentally friendly, non-destructive and non-invasive geophysical assessment method has played an important role in the urbanization process in China. Because human noise and electromagnetic field due to industrial life, geophysical methods already used in urban environments (gravity, magnetics, electricity, seismic) face great challenges. But humanity activity provides an effective source of passive seismic methods. Claerbout pointed out that wavefileds that are received at one point with excitation at the other point can be reconstructed by calculating the cross-correlation of noise records at two surface points. Based on this idea (cross-correlation of two noise records) and the virtual source method, we proposed Multi-channel Analysis of Passive Surface Waves (MAPS). MAPS mainly uses traffic noise recorded with a linear receiver array. Because Multi-channel Analysis of Surface Waves can produces a shear (S) wave velocity model with high resolution in shallow part of the model, MPAS combines acquisition and processing of active source and passive source data in a same flow, which does not require to distinguish them. MAPS is also of ability of real-time quality control of noise recording that is important for near-surface applications in urban environment. The numerical and real-world examples demonstrated that MAPS can be

  2. Adlayers of dimannoside thiols on gold: surface chemical analysis.

    Science.gov (United States)

    Dietrich, Paul M; Horlacher, Tim; Girard-Lauriault, Pierre-Luc; Gross, Thomas; Lippitz, Andreas; Min, Hyegeun; Wirth, Thomas; Castelli, Riccardo; Seeberger, Peter H; Unger, Wolfgang E S

    2011-04-19

    Carbohydrate films on gold based on dimannoside thiols (DMT) were prepared, and a complementary surface chemical analysis was performed in detail by X-ray photoelectron spectroscopy (XPS), time-of-flight secondary ion mass spectrometry (ToF-SIMS), near-edge X-ray absorption fine structure (NEXAFS), FT-IR, and contact angle measurements in order to verify formation of ω-carbohydrate-functionalized alkylthiol films. XPS (C 1s, O 1s, and S 2p) reveals information on carbohydrate specific alkoxy (C-O) and acetal moieties (O-C-O) as well as thiolate species attached to gold. Angle-resolved synchrotron XPS was used for chemical speciation at ultimate surface sensitivity. Angle-resolved XPS analysis suggests the presence of an excess top layer composed of unbound sulfur components combined with alkyl moieties. Further support for DMT attachment on Au is given by ToF-SIMS and FT-IR analysis. Carbon and oxygen K-edge NEXAFS spectra were interpreted by applying the building block model supported by comparison to data of 1-undecanethiol, poly(vinyl alcohol), and polyoxymethylene. No linear dichroism effect was observed in the angle-resolved C K-edge NEXAFS. © 2011 American Chemical Society

  3. An intelligent hybrid system for surface coal mine safety analysis

    Energy Technology Data Exchange (ETDEWEB)

    Lilic, N.; Obradovic, I.; Cvjetic, A. [University of Belgrade, Belgrade (Serbia)

    2010-06-15

    Analysis of safety in surface coal mines represents a very complex process. Published studies on mine safety analysis are usually based on research related to accidents statistics and hazard identification with risk assessment within the mining industry. Discussion in this paper is focused on the application of AI methods in the analysis of safety in mining environment. Complexity of the subject matter requires a high level of expert knowledge and great experience. The solution was found in the creation of a hybrid system PROTECTOR, whose knowledge base represents a formalization of the expert knowledge in the mine safety field. The main goal of the system is the estimation of mining environment as one of the significant components of general safety state in a mine. This global goal is subdivided into a hierarchical structure of subgoals where each subgoal can be viewed as the estimation of a set of parameters (gas, dust, climate, noise, vibration, illumination, geotechnical hazard) which determine the general mine safety state and category of hazard in mining environment. Both the hybrid nature of the system and the possibilities it offers are illustrated through a case study using field data related to an existing Serbian surface coal mine.

  4. Surface proteome analysis and characterization of surface cell antigen (Sca or autotransporter family of Rickettsia typhi.

    Directory of Open Access Journals (Sweden)

    Khandra T Sears

    Full Text Available Surface proteins of the obligate intracellular bacterium Rickettsia typhi, the agent of murine or endemic typhus fever, comprise an important interface for host-pathogen interactions including adherence, invasion and survival in the host cytoplasm. In this report, we present analyses of the surface exposed proteins of R. typhi based on a suite of predictive algorithms complemented by experimental surface-labeling with thiol-cleavable sulfo-NHS-SS-biotin and identification of labeled peptides by LC MS/MS. Further, we focus on proteins belonging to the surface cell antigen (Sca autotransporter (AT family which are known to be involved in rickettsial infection of mammalian cells. Each species of Rickettsia has a different complement of sca genes in various states; R. typhi, has genes sca1 thru sca5. In silico analyses indicate divergence of the Sca paralogs across the four Rickettsia groups and concur with previous evidence of positive selection. Transcripts for each sca were detected during infection of L929 cells and four of the five Sca proteins were detected in the surface proteome analysis. We observed that each R. typhi Sca protein is expressed during in vitro infections and selected Sca proteins were expressed during in vivo infections. Using biotin-affinity pull down assays, negative staining electron microscopy, and flow cytometry, we demonstrate that the Sca proteins in R. typhi are localized to the surface of the bacteria. All Scas were detected during infection of L929 cells by immunogold electron microscopy. Immunofluorescence assays demonstrate that Scas 1-3 and 5 are expressed in the spleens of infected Sprague-Dawley rats and Scas 3, 4 and 5 are expressed in cat fleas (Ctenocephalides felis. Sca proteins may be crucial in the recognition and invasion of different host cell types. In short, continuous expression of all Scas may ensure that rickettsiae are primed i to infect mammalian cells should the flea bite a host, ii to remain

  5. Moessbauer backscattering spectrometer for mineralogical analysis of the Mars surface

    International Nuclear Information System (INIS)

    Klingelhoefer, G.; Foh, J.; Held, P.; Jaeger, H.; Kankeleit, E.; Teucher, R.

    1992-01-01

    A Moessbauer spectrometer for the mineralogical analysis of the Mars surface is under development. This instrument will be installed on a Mars-Rover, included in the Soviet Union Mars-94/96 Mars mission. Due to power and mass restrictions the electromechanical drive and the electronic components have been extremely miniaturized in comparison to standard systems. Solid state detectors (PIN-diodes) are used for γ- and x-ray detection. The whole spectrometer is controlled by a microprocessor (transputer). An additional application as X-ray fluorescence spectrometer is proposed. (orig.)

  6. Surface recombination analysis in silicon-heterojunction solar cells

    Energy Technology Data Exchange (ETDEWEB)

    Barrio, R.; Gandia, J.J.; Carabe, J.; Gonzalez, N.; Torres, I. [CIEMAT, Madrid (Spain); Munoz, D.; Voz, C. [Universitat Politecnica de Catalunya, Barcelona (Spain)

    2010-02-15

    The origin of this work is the understanding of the correlation observed between efficiency and emitter-deposition temperature in single silicon-heterojunction solar cells prepared by depositing an n-doped hydrogenated-amorphous-silicon thin film onto a p-type crystalline-silicon wafer. In order to interpret these results, surface-recombination velocities have been determined by two methods, i.e. by fitting the current-voltage characteristics to a theoretical model and by means of the Quasi-Steady-State Photoconductance Technique (QSSPC). In addition, effective diffusion lengths have been estimated from internal quantum efficiencies. The analysis of these data has led to conclude that the performance of the cells studied is limited by back-surface recombination rather than by front-heterojunction quality. A 12%-efficient cell has been prepared by combining optimum emitter-deposition conditions with back-surface-field (BSF) formation by vacuum annealing of the back aluminium contact. This result has been achieved without using any transparent conductive oxide. (author)

  7. Thermal Desorption Analysis of Effective Specific Soil Surface Area

    Science.gov (United States)

    Smagin, A. V.; Bashina, A. S.; Klyueva, V. V.; Kubareva, A. V.

    2017-12-01

    A new method of assessing the effective specific surface area based on the successive thermal desorption of water vapor at different temperature stages of sample drying is analyzed in comparison with the conventional static adsorption method using a representative set of soil samples of different genesis and degree of dispersion. The theory of the method uses the fundamental relationship between the thermodynamic water potential (Ψ) and the absolute temperature of drying ( T): Ψ = Q - aT, where Q is the specific heat of vaporization, and a is the physically based parameter related to the initial temperature and relative humidity of the air in the external thermodynamic reservoir (laboratory). From gravimetric data on the mass fraction of water ( W) and the Ψ value, Polyanyi potential curves ( W(Ψ)) for the studied samples are plotted. Water sorption isotherms are then calculated, from which the capacity of monolayer and the target effective specific surface area are determined using the BET theory. Comparative analysis shows that the new method well agrees with the conventional estimation of the degree of dispersion by the BET and Kutilek methods in a wide range of specific surface area values between 10 and 250 m2/g.

  8. Static stability analysis of embedded flexoelectric nanoplates considering surface effects

    Science.gov (United States)

    Ebrahimi, Farzad; Barati, Mohammad Reza

    2017-10-01

    In this paper, electromechanical buckling behavior of size-dependent flexoelectric nanoplates is investigated based on nonlocal and surface elasticity theories. Flexoelectricity represents the coupling between strain gradients and electrical polarizations. Flexoelectric nanoplates can tolerate higher buckling loads compared with conventional piezoelectric nanoplates, especially at lower thicknesses. The flexoelectric nanoplate is in contact with a two-parameter elastic foundation, which consists of infinite linear springs and a shear layer. Nonlocal elasticity theory of Eringen is applied in the analysis of flexoelectric nanoplates for the first time. The residual surface stresses which are usually neglected in the modeling of flexoelectric nanoplates are incorporated into nonlocal elasticity to provide better understanding of the physics of the problem. Applying an analytical solution which satisfies various boundary conditions, the governing equations obtained from Hamilton's principle are solved. The reliability of the present approach is verified by comparing the obtained results with those provided in literature. Finally, the influences of nonlocal parameter, surface effect, plate geometrical parameters, elastic foundation and boundary conditions on the buckling characteristics of flexoelectric nanoplates are explored.

  9. Improving knowledge management systems with latent semantic analysis

    International Nuclear Information System (INIS)

    Sebok, A.; Plott, C.; LaVoie, N.

    2006-01-01

    Latent Semantic Analysis (LSA) offers a technique for improving lessons learned and knowledge management systems. These systems are expected to become more widely used in the nuclear industry, as experienced personnel leave and are replaced by younger, less-experienced workers. LSA is a machine learning technology that allows searching of text based on meaning rather than predefined keywords or categories. Users can enter and retrieve data using their own words, rather than relying on constrained language lists or navigating an artificially structured database. LSA-based tools can greatly enhance the usability and usefulness of knowledge management systems and thus provide a valuable tool to assist nuclear industry personnel in gathering and transferring worker expertise. (authors)

  10. Paired Expression Analysis of Tumor Cell Surface Antigens

    Directory of Open Access Journals (Sweden)

    Rimas J. Orentas

    2017-08-01

    Full Text Available Adoptive immunotherapy with antibody-based therapy or with T cells transduced to express chimeric antigen receptors (CARs is useful to the extent that the cell surface membrane protein being targeted is not expressed on normal tissues. The most successful CAR-based (anti-CD19 or antibody-based therapy (anti-CD20 in hematologic malignancies has the side effect of eliminating the normal B cell compartment. Targeting solid tumors may not provide a similar expendable marker. Beyond antibody to Her2/NEU and EGFR, very few antibody-based and no CAR-based therapies have seen broad clinical application for solid tumors. To expand the way in which the surfaceome of solid tumors can be analyzed, we created an algorithm that defines the pairwise relative overexpression of surface antigens. This enables the development of specific immunotherapies that require the expression of two discrete antigens on the surface of the tumor target. This dyad analysis was facilitated by employing the Hotelling’s T-squared test (Hotelling–Lawley multivariate analysis of variance for two independent variables in comparison to a third constant entity (i.e., gene expression levels in normal tissues. We also present a unique consensus scoring mechanism for identifying transcripts that encode cell surface proteins. The unique application of our bioinformatics processing pipeline and statistical tools allowed us to compare the expression of two membrane protein targets as a pair, and to propose a new strategy based on implementing immunotherapies that require both antigens to be expressed on the tumor cell surface to trigger therapeutic effector mechanisms. Specifically, we found that, for MYCN amplified neuroblastoma, pairwise expression of ACVR2B or anaplastic lymphoma kinase (ALK with GFRA3, GFRA2, Cadherin 24, or with one another provided the strongest hits. For MYCN, non-amplified stage 4 neuroblastoma, neurotrophic tyrosine kinase 1, or ALK paired with GFRA2, GFRA3, SSK

  11. Surface analysis in steel nitrides by using Moessbauer spectroscopy

    International Nuclear Information System (INIS)

    Figueiredo, R.S. de.

    1991-07-01

    The formation of iron nitride layer at low temperatures, 600-700 K, by Moessbauer spectroscopy is studied. These layers were obtained basically through two different processes: ion nitriding and ammonia gas nitriding. A preliminary study about post-discharge nitriding was made using discharge in hollow cathode as well as microwave excitation. The assembly of these chambers is also described. The analysis of the nitrided samples was done by CEMS and CXMS, aided by optical microscopy, and the CEMS and CXMS detectors were constructed by ourselves. We also made a brief study about these detectors, testing as acetone as the mixture 80% He+10% C H 4 as detection gases for the use of CEMS. The surface analysis of the samples showed that in the ammonia gas process nitriding the nitrided layer starts by the superficial formation of an iron nitride rich nitrogen. By thermal evolution this nitride promotes the diffusion of nitrogen and the formation of other more stable nitrides. (author)

  12. Response surface analysis to improve dispersed crude oil biodegradation

    Energy Technology Data Exchange (ETDEWEB)

    Zahed, Mohammad A.; Aziz, Hamidi A.; Mohajeri, Leila [School of Civil Engineering, Universiti Sains Malaysia, Nibong Tebal, Penang (Malaysia); Isa, Mohamed H. [Civil Engineering Department, Universiti Teknologi PETRONAS, Tronoh, Perak (Malaysia)

    2012-03-15

    In this research, the bioremediation of dispersed crude oil, based on the amount of nitrogen and phosphorus supplementation in the closed system, was optimized by the application of response surface methodology and central composite design. Correlation analysis of the mathematical-regression model demonstrated that a quadratic polynomial model could be used to optimize the hydrocarbon bioremediation (R{sup 2} = 0.9256). Statistical significance was checked by analysis of variance and residual analysis. Natural attenuation was removed by 22.1% of crude oil in 28 days. The highest removal on un-optimized condition of 68.1% were observed by using nitrogen of 20.00 mg/L and phosphorus of 2.00 mg/L in 28 days while optimization process exhibited a crude oil removal of 69.5% via nitrogen of 16.05 mg/L and phosphorus 1.34 mg/L in 27 days therefore optimization can improve biodegradation in shorter time with less nutrient consumption. (Copyright copyright 2012 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  13. XPS analysis of nanostructured materials and biological surfaces

    International Nuclear Information System (INIS)

    Baer, D.R.; Engelhard, M.H.

    2010-01-01

    This paper examines the types of information that XPS can provide about a variety of nanostructured materials. Although it is sometimes not considered a 'nanoscale analysis method,' XPS can provide a great deal of information about elemental distributions, layer or coating structure and thicknesses, surface functionality, and even particles sizes on the 1-20 nm scale for sample types that may not be readily analyzed by other methods. This information is important for both synthetic nanostructured or nanosized materials and a variety of natural materials with nanostructure. Although the links between nanostructure materials and biological systems may not at first be obvious, many biological molecules and some organisms are the sizes of nanoparticles. The nanostructure of cells and microbes plays a significant role in how they interact with their environment. The interaction of biomolecules with nanoparticles is important for medical and toxicity studies. The interaction of biomolecules is important for sensor function and many nanomaterials are now the active elements in sensors. This paper first discusses how nanostructures influences XPS data as a part of understanding how simple models of sample structure and data analysis can be used to extract information about the physical and chemical structures of the materials being analyzed. Equally important, aspects of sample and analysis limitations and challenges associated with understanding nanostructured materials are indicated. Examples of the application of XPS to nanostructured and biological systems and materials are provided.

  14. SEM Analysis of Surface Impact on Biofilm Antibiotic Treatment.

    Science.gov (United States)

    Gomes, Luciana Calheiros; Mergulhão, Filipe José

    2017-01-01

    The aim of this work was to use scanning electron microscopy (SEM) to investigate the effect of ampicillin treatment on Escherichia coli biofilms formed on two surface materials with different properties, silicone (SIL) and glass (GLA). Epifluorescence microscopy (EM) was initially used to assess biofilm formation and killing efficiency on both surfaces. This technique showed that higher bacterial colonization was obtained in the hydrophobic SIL than in the hydrophilic GLA. It has also shown that higher biofilm inactivation was attained for GLA after the antibiotic treatment (7-log reduction versus 1-log reduction for SIL). Due to its high resolution and magnification, SEM enabled a more detailed analysis of the antibiotic effect on biofilm cells, complementing the killing efficiency information obtained by EM. SEM micrographs revealed that ampicillin-treated cells have an elongated form when compared to untreated cells. Additionally, it has shown that different materials induced different levels of elongation on cells exposed to antibiotic. Biofilms formed on GLA showed a 37% higher elongation than those formed on SIL. Importantly, cell elongation was related to viability since ampicillin had a higher bactericidal effect on GLA-formed biofilms. These findings raise the possibility of using SEM for understanding the efficacy of antimicrobial treatments by observation of biofilm morphology.

  15. Proteomic analysis of the shistosome tegument and its surface membranes

    Directory of Open Access Journals (Sweden)

    Simon Braschi

    2006-10-01

    Full Text Available The tegument surface of the adult schistosome, bounded by a normal plasma membrane overlain by a secreted membranocalyx, holds the key to understanding how schistosomes evade host immune responses. Recent advances in mass spectrometry (MS, and the sequencing of the Schistosoma mansoni transcriptome/genome, have facilitated schistosome proteomics. We detached the tegument from the worm body and enriched its surface membranes by differential extraction, before subjecting the preparation to liquid chromatography-based proteomics to identify its constituents. The most exposed proteins on live worms were labelled with impearmeant biotinylation reagents, and we also developed methods to isolate the membranocalyx for analysis. We identified transporters for sugars, amino acids, inorganic ions and water, which confirm the importance of the tegument plasma membrane in nutrient acquisition and solute balance. Enzymes, including phosphohydrolases, esterases and carbonic anhydrase were located with their catalytic domains external to the plasma membrane, while five tetraspanins, annexin and dysferlin were implicated in membrane architecture. In contrast, few parasite proteins could be assigned to the membranocalyx but mouse immune response proteins, including three immunoglobulins and two complement factors, were detected, plus host membrane proteins such as CD44, integrin and a complement regulatory protein, testifying to the acquisitive properties of the secreted bilayer.

  16. Hygrothermal analysis of surface layers of historical masonry

    Science.gov (United States)

    Kočí, Václav; Maděra, Jiří; Keppert, Martin; Černý, Robert

    2017-11-01

    The paper deals with the hygrothermal analysis of surface layers of historical masonry. Solid brick provided with a traditional and two modified lime-based plasters is studied. The heat and moisture transport in the envelope is induced by an exposure of the wall from the exterior side to dynamic climatic conditions of Olomouc, Czech Republic. The transport processes are described using diffusion type of mathematical model based on experimentally determined material properties. The computational results indicate that hygric transport and accumulation properties of exterior plasters affect the hygrothermal performance of the underlying solid brick in a very significant way, being able to regulate the amount of transported moisture. The modified lime plasters are not found generally superior to the traditional lime plasters in that respect. Therefore, their suitability for historical masonry should be assessed case by case, with a particular attention to the climatic conditions and to the properties of the load bearing structure.

  17. Analysis of MAGSAT and surface data of the Indian region

    Science.gov (United States)

    Agarwal, G. C. (Principal Investigator)

    1983-01-01

    Techniques and significant results of an analysis of MAGSAT and surface data of the Indian region are described. Specific investigative tasks included: (1) use of the multilevel data at different altitudes to develop a model for variation of magnetic anomaly with altitude; (2) development of the regional model for the description of main geomagnetic field for the Indian sub-continent using MAGSAT and observatory data; (3) development of regional mathematical model of secular variations over the Indian sub-continent; and (4) downward continuation of the anomaly field obtained from MAGSAT and its combination with the existing observatory data to produce a regional anomaly map for elucidating tectonic features of the Indian sub-continent.

  18. Evaluation of flyash surface phenomena and the application of surface analysis technology. Summary report: Phase I. [44 elements; 86 references

    Energy Technology Data Exchange (ETDEWEB)

    Smith, R.D.

    1981-06-01

    The factors governing the formation of flyash surfaces during and following coal combustion are reviewed. The competing chemical and physical processes during the evolution of inorganic material in coal during combustion into flyash are described with respect to various surface segregation processes. Two mechanisms leading to surface enrichment are volatilization-condensation processes and diffusion processes within individual flyash particles. The experimental evidence for each of these processes is reviewed. It is shown that the volatilization-condensation process is the major factor leading to trace element enrichment in smaller flyash particles. Evidence also exists from surface analyses of flyash and representative mineral matter that diffusion processes may lead to surface enrichment of elements not volatilized or cause transport of surface-condensed elements into the flyash matrix. The semiquantitative determination of the relative importance of these two processes can be determined by comparison of concentration versus particle size profiles with surface-depth profiles obtained using surface analysis techniques. A brief description of organic transformations on flyash surfaces is also presented. The various surface analytical techniques are reviewed and the relatively new technique of Static-Secondary Ion Mass Spectroscopy is suggested as having significant advantages in studies of surfaces and diffusion processes in model systems. Several recommendations are made for research relevant to flyash formation and processes occurring on flyash surfaces.

  19. Surface-Source Downhole Seismic Analysis in R

    Science.gov (United States)

    Thompson, Eric M.

    2007-01-01

    This report discusses a method for interpreting a layered slowness or velocity model from surface-source downhole seismic data originally presented by Boore (2003). I have implemented this method in the statistical computing language R (R Development Core Team, 2007), so that it is freely and easily available to researchers and practitioners that may find it useful. I originally applied an early version of these routines to seismic cone penetration test data (SCPT) to analyze the horizontal variability of shear-wave velocity within the sediments in the San Francisco Bay area (Thompson et al., 2006). A more recent version of these codes was used to analyze the influence of interface-selection and model assumptions on velocity/slowness estimates and the resulting differences in site amplification (Boore and Thompson, 2007). The R environment has many benefits for scientific and statistical computation; I have chosen R to disseminate these routines because it is versatile enough to program specialized routines, is highly interactive which aids in the analysis of data, and is freely and conveniently available to install on a wide variety of computer platforms. These scripts are useful for the interpretation of layered velocity models from surface-source downhole seismic data such as deep boreholes and SCPT data. The inputs are the travel-time data and the offset of the source at the surface. The travel-time arrivals for the P- and S-waves must already be picked from the original data. An option in the inversion is to include estimates of the standard deviation of the travel-time picks for a weighted inversion of the velocity profile. The standard deviation of each travel-time pick is defined relative to the standard deviation of the best pick in a profile and is based on the accuracy with which the travel-time measurement could be determined from the seismogram. The analysis of the travel-time data consists of two parts: the identification of layer-interfaces, and the

  20. Surface topography analysis for dimensional quality control of replication at the micrometre scale

    DEFF Research Database (Denmark)

    Balcon, M.; Marinello, F.; Tosello, Guido

    2011-01-01

    and replica surfaces must be quantitatively analysed and compared. In the present work, reference simulated surfaces were considered and studied in order to evaluate the effectiveness and traceability of different analysis tools for replication quality control. Topographies were analysed simulating different...... surface mapping techniques, such as optical profilometry, scanning probe microscopy and scanning electron microscopy. Different strategies for surface analysis and comparison are proposed and discussed taking into account the instrument, the measuring range and the functionality of the surface....

  1. Surface return direction-of-arrival analysis for radar ice sounding surface clutter suppression

    DEFF Research Database (Denmark)

    Nielsen, Ulrik; Dall, Jørgen

    2015-01-01

    Airborne radar ice sounding is challenged by surface clutter masking the depth signal of interest. Surface clutter may even be prohibitive for potential space-based ice sounding radars. To some extent the radar antenna suppresses the surface clutter, and a multi-phase-center antenna in combination...

  2. Ambient Surface Analysis of Organic Monolayers using Direct Analysis in Real Time Orbitrap Mass Spectrometry

    NARCIS (Netherlands)

    Manova, R.K.; Joshi, S.; Debrassi, A.; Bhairamadgi, N.S.; Roeven, E.; Gagnon, J.; Tahir, M.N.; Claassen, F.W.; Scheres, L.M.W.; Wennekes, T.; Schroën, C.G.P.H.; Beek, van T.A.; Zuilhof, H.; Nielen, M.W.F.

    2014-01-01

    A better characterization of nanometer-thick organic layers (monolayers) as used for engineering surface properties, biosensing, nanomedicine, and smart materials will widen their application. The aim of this study was to develop direct analysis in real time high-resolution mass spectrometry

  3. Gis-Based Surface Analysis of Archaeological Finds

    Science.gov (United States)

    Kovács, K.; Hanke, K.; Moser, M.

    2011-09-01

    The international research project HiMAT (History of Mining Activities in the Tyrol and adjacent areas) is dedicated to the study of mining history in the Eastern Alps by various scientific disciplines. The aim of this program is the analysis of the mining activities' impacts on environment and human societies. Unfortunately, there is only a limited number of specific regions (e.g. Mitterberg) to offer possibilities to investigate the former mining expansions. Within this multidisciplinary project, the archaeological sites and finds are analyzed by the Surveying and Geoinformation Unit at the University of Innsbruck. This paper shows data fusion of different surveying and post-processing methods to achieve a photo-realistic digital 3D model of one of these most important finds, the Bronze Age sluice box from the Mitterberg. The applied workflow consists of four steps: 1. Point cloud processing, 2. Meshing of the point clouds and editing of the models, 3. Image orientation, bundle and image adjustment, 4. Model texturing. In addition, a short range laser scanning survey was organized before the conservation process of this wooden find. More accurate research opportunities were offered after this detailed documentation of the sluice box, for example the reconstruction of the broken parts and the surface analysis of this archaeological object were implemented using these high-resolution datasets. In conclusion, various unperceived patterns of the wooden boards were visualized by the GIS-based tool marks investigation.

  4. GIS-BASED SURFACE ANALYSIS OF ARCHAEOLOGICAL FINDS

    Directory of Open Access Journals (Sweden)

    K. Kovács

    2012-09-01

    Full Text Available The international research project HiMAT (History of Mining Activities in the Tyrol and adjacent areas is dedicated to the study of mining history in the Eastern Alps by various scientific disciplines. The aim of this program is the analysis of the mining activities’ impacts on environment and human societies. Unfortunately, there is only a limited number of specific regions (e.g. Mitterberg to offer possibilities to investigate the former mining expansions. Within this multidisciplinary project, the archaeological sites and finds are analyzed by the Surveying and Geoinformation Unit at the University of Innsbruck. This paper shows data fusion of different surveying and post-processing methods to achieve a photo-realistic digital 3D model of one of these most important finds, the Bronze Age sluice box from the Mitterberg. The applied workflow consists of four steps: 1. Point cloud processing, 2. Meshing of the point clouds and editing of the models, 3. Image orientation, bundle and image adjustment, 4. Model texturing. In addition, a short range laser scanning survey was organized before the conservation process of this wooden find. More accurate research opportunities were offered after this detailed documentation of the sluice box, for example the reconstruction of the broken parts and the surface analysis of this archaeological object were implemented using these high-resolution datasets. In conclusion, various unperceived patterns of the wooden boards were visualized by the GIS-based tool marks investigation.

  5. Numerical analysis of surface subsidence in asymmetric parallel highway tunnels

    Directory of Open Access Journals (Sweden)

    Ratan Das

    2017-02-01

    Full Text Available Tunnelling related hazards are very common in the Himalayan terrain and a number of such instances have been reported. Several twin tunnels are being planned for transportation purposes which will require good understanding for prediction of tunnel deformation and surface settlement during the engineering life of the structure. The deformational behaviour, design of sequential excavation and support of any jointed rock mass are challenging during underground construction. We have raised several commonly assumed issues while performing stability analysis of underground opening at shallow depth. For this purpose, Kainchi-mod Nerchowck twin tunnels (Himachal Pradesh, India are taken for in-depth analysis of the stability of two asymmetric tunnels to address the influence of topography, twin tunnel dimension and geometry. The host rock encountered during excavation is composed mainly of moderately to highly jointed grey sandstone, maroon sandstone and siltstones. In contrast to equidimensional tunnels where the maximum subsidence is observed vertically above the centreline of the tunnel, the result from the present study shows shifting of the maximum subsidence away from the tunnel centreline. The maximum subsidence of 0.99 mm is observed at 4.54 m left to the escape tunnel centreline whereas the maximum subsidence of 3.14 mm is observed at 8.89 m right to the main tunnel centreline. This shifting clearly indicates the influence of undulating topography and in-equidimensional noncircular tunnel.

  6. Analysis of variability of tropical Pacific sea surface temperatures

    Science.gov (United States)

    Davies, Georgina; Cressie, Noel

    2016-11-01

    Sea surface temperature (SST) in the Pacific Ocean is a key component of many global climate models and the El Niño-Southern Oscillation (ENSO) phenomenon. We shall analyse SST for the period November 1981-December 2014. To study the temporal variability of the ENSO phenomenon, we have selected a subregion of the tropical Pacific Ocean, namely the Niño 3.4 region, as it is thought to be the area where SST anomalies indicate most clearly ENSO's influence on the global atmosphere. SST anomalies, obtained by subtracting the appropriate monthly averages from the data, are the focus of the majority of previous analyses of the Pacific and other oceans' SSTs. Preliminary data analysis showed that not only Niño 3.4 spatial means but also Niño 3.4 spatial variances varied with month of the year. In this article, we conduct an analysis of the raw SST data and introduce diagnostic plots (here, plots of variability vs. central tendency). These plots show strong negative dependence between the spatial standard deviation and the spatial mean. Outliers are present, so we consider robust regression to obtain intercept and slope estimates for the 12 individual months and for all-months-combined. Based on this mean-standard deviation relationship, we define a variance-stabilizing transformation. On the transformed scale, we describe the Niño 3.4 SST time series with a statistical model that is linear, heteroskedastic, and dynamical.

  7. Experimental analysis of surface finish in normal conducting cavities

    Science.gov (United States)

    Zarrebini-Esfahani, A.; Aslaninejad, M.; Ristic, M.; Long, K.

    2017-10-01

    A normal conducting 805 MHz test cavity with an in built button shaped sample is used to conduct a series of surface treatment experiments. The button enhances the local fields and influences the likelihood of an RF breakdown event. Because of their smaller sizes, compared to the whole cavity surface, they allow practical investigations of the effects of cavity surface preparation in relation to RF breakdown. Manufacturing techniques and steps for preparing the buttons to improve the surface quality are described in detail. It was observed that even after the final stage of the surface treatment, defects on the surface of the cavities still could be found.

  8. The Planet Mercury Surface Spectroscopy and Analysis from the Kuiper Airborne Observatory and Analysis and Modeling to Determine Surface Composition

    Science.gov (United States)

    Sprague, Ann

    1997-01-01

    We had two successful flights to observe Mercury from the Kuiper Airborne Observatory (KAO) using High-efficiency Infrared Faint-Object Grating Spectrograph (HIFOGS). Flights were May 8, 1995 (eastern elongation) and July 6, 1995 (western elongation) For the observations one half of the primary mirror was covered to prevent sunlight from entering the telescope. All equipment and the airplane and its crew performed well. These flights were historical firsts for the KAO and for spectroscopy of Mercury in that it was the first time any spectroscopic observations of Mercury from above the Earth's atmosphere had been made. It was the first time the KAO had been used to @bserve an object less than 30 degrees from the Sun. Upon completion of the basic data reduction it became obvious that extensive modeling and analysis would be required to understand the data. It took three years of a graduate student's time and part time the PI to do the thermal modeling and the spectroscopic analysis. This resulted in a lengthy publication. A copy of this publication is attached and has all the data obtained in both KAO flights and the results clearly presented. Notable results are: (1) The observations found an as yet unexplained 5 micron emission enhancement that we think may be a real characteristic of Mercury's surface but could have an instrumental cause; (2) Ground-based measurements or an emission maximum at 7.7 microns were corroborated. The chemical composition of Mercury's surface must be feldspathic in order to explain spectra features found in the data obtained during the KAO flights.

  9. Concepts in Navel Aesthetic: A Comprehensive Surface Anatomy Analysis.

    Science.gov (United States)

    Visconti, Giuseppe; Visconti, Emiliano; Bonomo, Lorenzo; Salgarello, Marzia

    2015-02-01

    The navel contributes to abdominal surface identity and beauty. In Western societies, the display of the navel in women's fashion has grown and, nowadays, women are much more concerned about its shape and position. Despite this, few studies are available on navel surface anatomy and there is no standardization regarding its proper placement in cosmetic abdominoplasty. In this observational study, we analyzed navel shape and position on 81 high quality pictures, having been chosen as top 2013 bikini models by editors of mass media. An on-line survey on navel shape and position has been made via facebook.com, involving 1,682 people. The analysis revealed that navel position is quite variable based on the proportions analyzed with an acceptable narrow data spread of the xiphoid-umbilicus:umbilicus-abdominal mean crease ratio of 1.62 ± 0.16. The data dispersion for the other three ratios was wider, making them less reliable as references. The most appreciated navel shape was the vertical oval with superior hooding (82 %), and the less appreciated ones were the horizontal oval (29 %) and the protruding shape (47 %). When comparing navel position on the same body, the majority of participants choose the one with the navel relocated according to the golden ratio (i.e., 1.618) CONCLUSION: The most attractive navel position is located at the xiphoid-umbilicus:umbilicus-abdominal crease golden ratio. Bony landmarks seem to be not reliable as references for proper navel positioning. The use of the Fibonacci (golden mean) caliper intraoperatively might aid in proper positioning of the navel in abdominoplasty.

  10. Surface analysis of transition metal oxalates: Damage aspects

    Energy Technology Data Exchange (ETDEWEB)

    Chenakin, S.P., E-mail: chenakin@imp.kiev.ua [Université Libre de Bruxelles (ULB), Chimie-Physique des Matériaux, B-1050 Bruxelles (Belgium); Institute of Metal Physics, Nat. Acad. Sci. of Ukraine, Akad. Vernadsky Blvd. 36, 03680 Kiev (Ukraine); Szukiewicz, R. [Université Libre de Bruxelles (ULB), Chimie-Physique des Matériaux, B-1050 Bruxelles (Belgium); Barbosa, R.; Kruse, N. [Université Libre de Bruxelles (ULB), Chimie-Physique des Matériaux, B-1050 Bruxelles (Belgium); Voiland School of Chemical Engineering and Bioengineering, Washington State University, 155 Wegner Hall, Pullman, WA 99164-6515 (United States)

    2016-05-15

    Highlights: • Gas evolution from the Mn, Co, Ni and Cu oxalate hydrates in vacuum, during exposure to X-rays and after termination of X-ray irradiation is studied. • A comparative study of the damage caused by X-rays in NiC{sub 2}O{sub 4} and CuC{sub 2}O{sub 4} is carried out. • Effect of Ar{sup +} bombardment on the structure and composition of CoC{sub 2}O{sub 4} is studied. - Abstract: The behavior of transition metal oxalates in vacuum, under X-ray irradiation and low-energy Ar{sup +} ion bombardment was studied. A comparative mass-spectrometric analysis was carried out of gas evolution from the surface of Mn, Co, Ni and Cu oxalate hydrates in vacuum, during exposure to X-rays and after termination of X-ray irradiation. The rates of H{sub 2}O and CO{sub 2} liberation from the oxalates were found to be in an inverse correlation with the temperatures of dehydration and decomposition, respectively. X-ray photoelectron spectroscopy (XPS) was employed to study the X-ray induced damage in NiC{sub 2}O{sub 4} and CuC{sub 2}O{sub 4} by measuring the various XP spectral characteristics and surface composition of the oxalates as a function of time of exposure to X-rays. It was shown that Cu oxalate underwent a significantly faster degradation than Ni oxalate and demonstrated a high degree of X-ray induced reduction from the Cu{sup 2+} to the Cu{sup 1+} chemical state. 500 eV Ar{sup +} sputter cleaning of CoC{sub 2}O{sub 4} for 10 min was found to cause a strong transformation of the oxalate structure which manifested itself in an appreciable alteration of the XP core-level and valence band spectra. The analysis of changes in stoichiometry and comparison of XP spectra of bombarded oxalate with respective spectra of a reference carbonate CoCO{sub 3} implied that the bombardment-induced decomposition of CoC{sub 2}O{sub 4} gave rise to the formation of CoO-like and disordered CoCO{sub 3}-like phases.

  11. Oral methotrexate/6-mercaptopurine may be superior to a multidrug LSA2L2 Maintenance therapy for higher risk childhood acute lymphoblastic leukemia: results from the NOPHO ALL-92 study

    DEFF Research Database (Denmark)

    Schmiegelow, Kjeld; Heyman, Mats; Kristinsson, Jon

    2009-01-01

    The importance of maintenance therapy for higher risk childhood acute lymphoblastic leukemia (ALL) is uncertain. Between 1992 and 2001 the Nordic Society for Pediatric Haematology/Oncology compared in a nonrandomized study conventional oral methotrexate (MTX)/6-mercaptopurine (6MP) maintenance...... therapy with a multidrug cyclic LSA2L2 regimen. 135 children with B-lineage ALL and a white blood count > or =50 x 10/L and 98 children with T-lineage ALL were included. Of the 234 patients, the 135 patients who received MTX/6MP maintenance therapy had a lower relapse risk than the 98 patients who...

  12. Preparation of polymeric superhydrophobic surfaces and analysis of their wettability

    Science.gov (United States)

    Zhuang, Jian; Huang, Manling; Zhang, Yajun; Wu, Daming; Kuang, Tairong; Xu, Hong; Zhang, Xiaoxu

    2015-10-01

    In this paper, we presented three simple, facile and low-cost manufacturing methods—template method, nanoparticle filling method and extrusion stamping forming method—to fabricate the polymeric superhydrophobic surfaces. The stainless steel wire mesh as the template and glass beads was investigated in this study for the first time and low-cost hollow glass beads were rarely used as particles for fabricating the superhydrophobic surface. The water contact angle measurement of polymeric surfaces was used to investigate the effect of mesh count, glass beads and PTFE on fabricating polymeric superhydrophobic surface. It was found that the mesh count significantly affected the hydrophobicity of polymer surface in template method. The addition of glass beads improved the hydrophobicity by nanoparticle filling method. The addition of PTFE was of importance to fabricate the superhydrophobic surface by extrusion stamping forming method. The surface microstructure was also observed by scanning electron microscope.

  13. Pressure relieving support surfaces (PRESSURE) trial: cost effectiveness analysis.

    Science.gov (United States)

    Iglesias, Cynthia; Nixon, Jane; Cranny, Gillian; Nelson, E Andrea; Hawkins, Kim; Phillips, Angela; Torgerson, David; Mason, Su; Cullum, Nicky

    2006-06-17

    To assess the cost effectiveness of alternating pressure mattresses compared with alternating pressure overlays for the prevention of pressure ulcers in patients admitted to hospital. Cost effectiveness analysis carried out alongside the pressure relieving support surfaces (PRESSURE) trial; a multicentre UK based pragmatic randomised controlled trial. 11 hospitals in six UK NHS trusts. Intention to treat population comprising 1971 participants. Kaplan Meier estimates of restricted mean time to development of pressure ulcers and total costs for treatment in hospital. Alternating pressure mattresses were associated with lower overall costs (283.6 pounds sterling per patient on average, 95% confidence interval--377.59 pounds sterling to 976.79 pounds sterling) mainly due to reduced length of stay in hospital, and greater benefits (a delay in time to ulceration of 10.64 days on average,--24.40 to 3.09). The differences in health benefits and total costs for hospital stay between alternating pressure mattresses and alternating pressure overlays were not statistically significant; however, a cost effectiveness acceptability curve indicated that on average alternating pressure mattresses compared with alternating pressure overlays were associated with an 80% probability of being cost saving. Alternating pressure mattresses for the prevention of pressure ulcers are more likely to be cost effective and are more acceptable to patients than alternating pressure overlays.

  14. Crystal structure and Hirshfeld surface analysis of pulcherrin J

    Directory of Open Access Journals (Sweden)

    K. Osahon Ogbeide

    2017-10-01

    Full Text Available The title compound, C29H36O4 [systematic name (4aR,5R,6aS,7R,11aS,11bR-4a-hydroxy-4,4,7,11b-tetramethyl-1,2,3,4,4a,5,6,6a,7,11,11a,11b-dodecahydrophenanthro[3,2-b]furan-5-yl cinnamate], a natural diterpene known as pulcherrin J, was isolated from stem barks of medicinally important Caesalpinia pulcherrima (L.. The crystal structure of pulcherrin J shows it to be composed of a central core of three trans-fused cyclohexane rings and a near planar five-membered furan ring, along with an axially oriented cinnamate moiety and an hydroxy substituent attached at positions 4a and 5 of the steroid ring system, respectively. The absolute structure was established with the use of Cu Kα radiation. In the crystal, molecules are linked by O—H...O hydrogen bonds to generate [100] C(8 chains. Hirshfeld surface analysis indicates that the most significant contacts in packing are H...H (67.5%, followed by C...H (19.6% and H...O (12.9%.

  15. Introduction to global analysis minimal surfaces in riemannian manifolds

    CERN Document Server

    Moore, John Douglas

    2017-01-01

    During the last century, global analysis was one of the main sources of interaction between geometry and topology. One might argue that the core of this subject is Morse theory, according to which the critical points of a generic smooth proper function on a manifold M determine the homology of the manifold. Morse envisioned applying this idea to the calculus of variations, including the theory of periodic motion in classical mechanics, by approximating the space of loops on M by a finite-dimensional manifold of high dimension. Palais and Smale reformulated Morse's calculus of variations in terms of infinite-dimensional manifolds, and these infinite-dimensional manifolds were found useful for studying a wide variety of nonlinear PDEs. This book applies infinite-dimensional manifold theory to the Morse theory of closed geodesics in a Riemannian manifold. It then describes the problems encountered when extending this theory to maps from surfaces instead of curves. It treats critical point theory for closed param...

  16. Response Predicting LTCC Firing Shrinkage: A Response Surface Analysis Study

    Energy Technology Data Exchange (ETDEWEB)

    Girardi, Michael; Barner, Gregg; Lopez, Cristie; Duncan, Brent; Zawicki, Larry

    2009-02-25

    The Low Temperature Cofired Ceramic (LTCC) technology is used in a variety of applications including military/space electronics, wireless communication, MEMS, medical and automotive electronics. The use of LTCC is growing due to the low cost of investment, short development time, good electrical and mechanical properties, high reliability, and flexibility in design integration (3 dimensional (3D) microstructures with cavities are possible)). The dimensional accuracy of the resulting x/y shrinkage of LTCC substrates is responsible for component assembly problems with the tolerance effect that increases in relation to the substrate size. Response Surface Analysis was used to predict product shrinkage based on specific process inputs (metal loading, layer count, lamination pressure, and tape thickness) with the ultimate goal to optimize manufacturing outputs (NC files, stencils, and screens) in achieving the final product design the first time. Three (3) regression models were developed for the DuPont 951 tape system with DuPont 5734 gold metallization based on green tape thickness.

  17. Introduction to global analysis minimal surfaces in Riemannian manifolds

    CERN Document Server

    Moore, John Douglas

    2017-01-01

    During the last century, global analysis was one of the main sources of interaction between geometry and topology. One might argue that the core of this subject is Morse theory, according to which the critical points of a generic smooth proper function on a manifold M determine the homology of the manifold. Morse envisioned applying this idea to the calculus of variations, including the theory of periodic motion in classical mechanics, by approximating the space of loops on M by a finite-dimensional manifold of high dimension. Palais and Smale reformulated Morse's calculus of variations in terms of infinite-dimensional manifolds, and these infinite-dimensional manifolds were found useful for studying a wide variety of nonlinear PDEs. This book applies infinite-dimensional manifold theory to the Morse theory of closed geodesics in a Riemannian manifold. It then describes the problems encountered when extending this theory to maps from surfaces instead of curves. It treats critical point theory for closed param...

  18. GHRSST Level 4 ODYSSEA Mediterranean Sea Regional Foundation Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at Ifremer/CERSAT...

  19. GHRSST Level 4 G1SST Global Foundation Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis by the JPL OurOcean...

  20. GHRSST Level 4 RAMSSA Australian Regional Foundation Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the Australian Bureau...

  1. GHRSST Level 4 GAMSSA Global Foundation Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the Australian Bureau...

  2. GHRSST Level 4 AVHRR_AMSR_OI Global Blended Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) global Level 4 sea surface temperature analysis produced daily on a 0.25 degree grid at the NOAA...

  3. GHRSST Level 4 EUR Mediterranean Sea Regional Foundation Sea Surface Temperature Analysis (GDS version 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily by Ifremer/CERSAT (France) using optimal...

  4. GHRSST Level 4 OSPO Global Nighttime Foundation Sea Surface Temperature Analysis (GDS version 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the Office of...

  5. GHRSST Level 4 MUR North America Regional Foundation Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced as a retrospective dataset at the JPL Physical...

  6. GHRSST Level 4 ODYSSEA Global Foundation Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at Ifremer/CERSAT...

  7. GHRSST Level 4 K10_SST Global 1 meter Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the Naval...

  8. GHRSST Level 4 OSTIA Global Foundation Sea Surface Temperature Analysis (GDS versions 1 and 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the UK Met Office...

  9. GHRSST Level 4 OSPO Global Foundation Sea Surface Temperature Analysis (GDS version 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the Office of...

  10. GHRSST Level 4 DMI_OI Global Foundation Sea Surface Temperature Analysis (GDS version 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis by the Danish...

  11. GHRSST Level 4 ODYSSEA Eastern Central Pacific Regional Foundation Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at Ifremer/CERSAT...

  12. GHRSST Level 4 MW_OI Global Foundation Sea Surface Temperature analysis (GDS version 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) global Level 4 sea surface temperature analysis produced daily on a 0.25 degree grid at Remote Sensing...

  13. Analysis of surface contaminants on beryllium and aluminum windows

    International Nuclear Information System (INIS)

    Gmur, N.F.

    1987-06-01

    An effort has been made to document the types of contamination which form on beryllium window surfaces due to interaction with a synchrotron radiation beam. Beryllium windows contaminated in a variety of ways (exposure to water and air) exhibited surface powders, gels, crystals and liquid droplets. These contaminants were analyzed by electron diffraction, electron energy loss spectroscopy, energy dispersive x-ray spectroscopy and wet chemical methods. Materials found on window surfaces include beryllium oxide, amorphous carbon, cuprous oxide, metallic copper and nitric acid. Aluminum window surface contaminants were also examined

  14. Quantitative spatial analysis of the mouse brain lipidome by pressurized liquid extraction surface analysis

    DEFF Research Database (Denmark)

    Almeida, Reinaldo; Berzina, Zane; Christensen, Eva Arnspang

    2015-01-01

    Here we describe a novel surface sampling technique termed pressurized liquid extraction surface analysis (PLESA), which in combination with a dedicated high-resolution shotgun lipidomics routine enables both quantification and in-depth structural characterization of molecular lipid species...... extracted directly from tissue sections. PLESA uses a sealed and pressurized sampling probe that enables the use of chloroform-containing extraction solvents for efficient in situ lipid microextraction with a spatial resolution of 400 μm. Quantification of lipid species is achieved by the inclusion...... of internal lipid standards in the extraction solvent. The analysis of lipid microextracts by nanoelectrospray ionization provides long-lasting ion spray which in conjunction with a hybrid ion trap-orbitrap mass spectrometer enables identification and quantification of molecular lipid species using a method...

  15. Analysis of surface bond lengths reported for chemisorption on metal surfaces

    Science.gov (United States)

    Mitchell, K. A. R.

    1985-01-01

    A review is given of bond length information available from the techniques of surface crystallography (particularly with LEED, SEXAFS and photoelectron diffraction) for chemisorption on well-defined surfaces of metals (M). For adsorbed main-group atoms (X), measured X-M interatomic distances for 38 combinations of X and M have been assessed with a bond order-bond length relation in combination with the Schomaker-Stevenson approach for determining single-bond lengths. When the surface bond orders are fixed primarily by the valency of X, this approach appears to provide a simple framework for predicing X-M surface bond lengths. Further, in cases where agreement has been reached from different surface crystallographic techniques, this framework has the potential for assessing refinements to the surface bonding model (e.g. in determining the roles of the effective surface valency of M, and of coordinate bonding and supplementary π bonding between X and M). Preliminary comparisons of structural data are also given for molecular adsorption (CO and ethylidyne) and for the chemisorption of other metal atoms.

  16. Analysis and research on curved surface's prototyping error based on FDM process

    Science.gov (United States)

    Gong, Y. D.; Zhang, Y. C.; Yang, T. B.; Wang, W. S.

    2008-12-01

    Analysis and research methods on curved surface's prototyping error with FDM (Fused Deposition Modeling) process are introduced in this paper, then the experiment result of curved surface's prototyping error is analyzed, and the integrity of point cloud information and the fitting method of curved surface prototyping are discussed as well as the influence on curved surface's prototyping error with different software. Finally, the qualitative and quantitative conclusions on curved surface's prototyping error are acquired in this paper.

  17. Expanding the boundaries of local similarity analysis.

    Science.gov (United States)

    Durno, W Evan; Hanson, Niels W; Konwar, Kishori M; Hallam, Steven J

    2013-01-01

    Pairwise comparison of time series data for both local and time-lagged relationships is a computationally challenging problem relevant to many fields of inquiry. The Local Similarity Analysis (LSA) statistic identifies the existence of local and lagged relationships, but determining significance through a p-value has been algorithmically cumbersome due to an intensive permutation test, shuffling rows and columns and repeatedly calculating the statistic. Furthermore, this p-value is calculated with the assumption of normality -- a statistical luxury dissociated from most real world datasets. To improve the performance of LSA on big datasets, an asymptotic upper bound on the p-value calculation was derived without the assumption of normality. This change in the bound calculation markedly improved computational speed from O(pm²n) to O(m²n), where p is the number of permutations in a permutation test, m is the number of time series, and n is the length of each time series. The bounding process is implemented as a computationally efficient software package, FASTLSA, written in C and optimized for threading on multi-core computers, improving its practical computation time. We computationally compare our approach to previous implementations of LSA, demonstrate broad applicability by analyzing time series data from public health, microbial ecology, and social media, and visualize resulting networks using the Cytoscape software. The FASTLSA software package expands the boundaries of LSA allowing analysis on datasets with millions of co-varying time series. Mapping metadata onto force-directed graphs derived from FASTLSA allows investigators to view correlated cliques and explore previously unrecognized network relationships. The software is freely available for download at: http://www.cmde.science.ubc.ca/hallam/fastLSA/.

  18. Expanding the boundaries of local similarity analysis

    Directory of Open Access Journals (Sweden)

    Durno W Evan

    2013-01-01

    Full Text Available Abstract Background Pairwise comparison of time series data for both local and time-lagged relationships is a computationally challenging problem relevant to many fields of inquiry. The Local Similarity Analysis (LSA statistic identifies the existence of local and lagged relationships, but determining significance through a p-value has been algorithmically cumbersome due to an intensive permutation test, shuffling rows and columns and repeatedly calculating the statistic. Furthermore, this p-value is calculated with the assumption of normality -- a statistical luxury dissociated from most real world datasets. Results To improve the performance of LSA on big datasets, an asymptotic upper bound on the p-value calculation was derived without the assumption of normality. This change in the bound calculation markedly improved computational speed from O(pm2n to O(m2n, where p is the number of permutations in a permutation test, m is the number of time series, and n is the length of each time series. The bounding process is implemented as a computationally efficient software package, FASTLSA, written in C and optimized for threading on multi-core computers, improving its practical computation time. We computationally compare our approach to previous implementations of LSA, demonstrate broad applicability by analyzing time series data from public health, microbial ecology, and social media, and visualize resulting networks using the Cytoscape software. Conclusions The FASTLSA software package expands the boundaries of LSA allowing analysis on datasets with millions of co-varying time series. Mapping metadata onto force-directed graphs derived from FASTLSA allows investigators to view correlated cliques and explore previously unrecognized network relationships. The software is freely available for download at: http://www.cmde.science.ubc.ca/hallam/fastLSA/.

  19. 'The surface management system' (SuMS) database: a surface-based database to aid cortical surface reconstruction, visualization and analysis

    Science.gov (United States)

    Dickson, J.; Drury, H.; Van Essen, D. C.

    2001-01-01

    Surface reconstructions of the cerebral cortex are increasingly widely used in the analysis and visualization of cortical structure, function and connectivity. From a neuroinformatics perspective, dealing with surface-related data poses a number of challenges. These include the multiplicity of configurations in which surfaces are routinely viewed (e.g. inflated maps, spheres and flat maps), plus the diversity of experimental data that can be represented on any given surface. To address these challenges, we have developed a surface management system (SuMS) that allows automated storage and retrieval of complex surface-related datasets. SuMS provides a systematic framework for the classification, storage and retrieval of many types of surface-related data and associated volume data. Within this classification framework, it serves as a version-control system capable of handling large numbers of surface and volume datasets. With built-in database management system support, SuMS provides rapid search and retrieval capabilities across all the datasets, while also incorporating multiple security levels to regulate access. SuMS is implemented in Java and can be accessed via a Web interface (WebSuMS) or using downloaded client software. Thus, SuMS is well positioned to act as a multiplatform, multi-user 'surface request broker' for the neuroscience community.

  20. Isolation of residuals using trend surface analysis to magnetic data ...

    African Journals Online (AJOL)

    Polynomial surfaces of various degrees are fitted to a magnetic data of Awo area, southwestern Nigeria with the aim of isolating the residuals of the area associated with mineralogy. The fourth degree surface correlates better with the magnetic map of the study area. The residualized data were obtained by subtracting the ...

  1. Land Surface Microwave Emissivity Dynamics: Observations, Analysis and Modeling

    Science.gov (United States)

    Tian, Yudong; Peters-Lidard, Christa D.; Harrison, Kenneth W.; Kumar, Sujay; Ringerud, Sarah

    2014-01-01

    Land surface microwave emissivity affects remote sensing of both the atmosphere and the land surface. The dynamical behavior of microwave emissivity over a very diverse sample of land surface types is studied. With seven years of satellite measurements from AMSR-E, we identified various dynamical regimes of the land surface emission. In addition, we used two radiative transfer models (RTMs), the Community Radiative Transfer Model (CRTM) and the Community Microwave Emission Modeling Platform (CMEM), to simulate land surface emissivity dynamics. With both CRTM and CMEM coupled to NASA's Land Information System, global-scale land surface microwave emissivities were simulated for five years, and evaluated against AMSR-E observations. It is found that both models have successes and failures over various types of land surfaces. Among them, the desert shows the most consistent underestimates (by approx. 70-80%), due to limitations of the physical models used, and requires a revision in both systems. Other snow-free surface types exhibit various degrees of success and it is expected that parameter tuning can improve their performances.

  2. Multi-component joint analysis of surface waves

    Czech Academy of Sciences Publication Activity Database

    Dal Moro, Giancarlo; Moura, R.M.M.; Moustafa, S.S.R.

    2015-01-01

    Roč. 119, AUG (2015), s. 128-138 ISSN 0926-9851 Institutional support: RVO:67985891 Keywords : surface waves * surface wave dispersion * seismic data acquisition * seismic data inversion * velocity spectrum Subject RIV: DB - Geology ; Mineralogy Impact factor: 1.355, year: 2015

  3. Lung sound analysis helps localize airway inflammation in patients with bronchial asthma

    Directory of Open Access Journals (Sweden)

    Shimoda T

    2017-03-01

    Full Text Available Terufumi Shimoda,1 Yasushi Obase,2 Yukio Nagasaka,3 Hiroshi Nakano,1 Akiko Ishimatsu,1 Reiko Kishikawa,1 Tomoaki Iwanaga1 1Clinical Research Center, Fukuoka National Hospital, Fukuoka, 2Second Department of Internal Medicine, School of Medicine, Nagasaki University, Nagasaki, 3Kyoto Respiratory Center, Otowa Hospital, Kyoto, Japan Purpose: Airway inflammation can be detected by lung sound analysis (LSA at a single point in the posterior lower lung field. We performed LSA at 7 points to examine whether the technique could identify the location of airway inflammation in patients with asthma. Patients and methods: Breath sounds were recorded at 7 points on the body surface of 22 asthmatic subjects. Inspiration sound pressure level (ISPL, expiration sound pressure level (ESPL, and the expiration-to-inspiration sound pressure ratio (E/I were calculated in 6 frequency bands. The data were analyzed for potential correlation with spirometry, airway hyperresponsiveness (PC20, and fractional exhaled nitric oxide (FeNO. Results: The E/I data in the frequency range of 100–400 Hz (E/I low frequency [LF], E/I mid frequency [MF] were better correlated with the spirometry, PC20, and FeNO values than were the ISPL or ESPL data. The left anterior chest and left posterior lower recording positions were associated with the best correlations (forced expiratory volume in 1 second/forced vital capacity: r=–0.55 and r=–0.58; logPC20: r=–0.46 and r=–0.45; and FeNO: r=0.42 and r=0.46, respectively. The majority of asthmatic subjects with FeNO ≥70 ppb exhibited high E/I MF levels in all lung fields (excluding the trachea and V50%pred <80%, suggesting inflammation throughout the airway. Asthmatic subjects with FeNO <70 ppb showed high or low E/I MF levels depending on the recording position, indicating uneven airway inflammation. Conclusion: E/I LF and E/I MF are more useful LSA parameters for evaluating airway inflammation in bronchial asthma; 7-point lung

  4. A far-ultraviolet photometer for planetary surface analysis

    International Nuclear Information System (INIS)

    Henry, R.C.; Fastie, W.G.; Lucke, R.L.; Hapke, B.W.

    1976-01-01

    The measurement of local variations in the far-ultraviolet albedo is explored as a means of detecting changes in the refractive index of rocks and dust on the surface of atmosphereless planets and satellites. Far-ultraviolet spectrophotometric measurements of the lunar surface which were obtained on the Apollo 17 orbital mission are presented to demonstrate that significant albedo variations occur in the spectral range 120 to 170 nm. These data also confirm the hypothesis that the albedo variations represent refractive index differences in the surface materials. A three-band photometer is described which, when put in orbit around a solar system object, is capable of providing refractive index maps with a sensitivity of 1 part in the second decimal place and with kilometer resolution. Comparative surface composition and surface history analyses based on such maps are discussed

  5. Performance analysis of PV panel under varying surface temperature

    Directory of Open Access Journals (Sweden)

    Kumar Tripathi Abhishek

    2018-01-01

    Full Text Available The surface temperature of PV panel has an adverse impact on its performance. The several electrical parameters of PV panel, such as open circuit voltage, short circuit current, power output and fill factor depends on the surface temperature of PV panel. In the present study, an experimental work was carried out to investigate the influence of PV panel surface temperature on its electrical parameters. The results obtained from this experimental study show a significant reduction in the performance of PV panel with an increase in panel surface temperature. A 5W PV panel experienced a 0.4% decrease in open circuit voltage for every 1°C increase in panel surface temperature. Similarly, there was 0.6% and 0.32% decrease in maximum power output and in fill factor, respectively, for every 1°C increase in panel surface temperature. On the other hand, the short circuit current increases with the increase in surface temperature at the rate of 0.09%/°C.

  6. Roughness analysis of graphite surfaces of casting elements

    Directory of Open Access Journals (Sweden)

    M. Wieczorowski

    2010-01-01

    Full Text Available In the paper profilometric measurements of graphite casting elements were described. Basic topics necessary to assess roughness of their surfaces and influence of asperities on various properties related to manufacturing and use were discussed. Stylus profilometer technique of surface irregularities measurements including its limits resulting from pickup geometry and its contact with measured object were ana-lyzed. Working principle of tactile profilometer and phenomena taking place during movement of a probe on a measured surface were shown. One of the important aspects is a flight phenomenon, which means movement of a pickup without contact with a surface during inspection resulting from too high scanning speed. results of comparison research for graphite elements of new and used mould and pin composing a set were presented. Using some surface roughness, waviness and primary profile parameters (arithmetical mean of roughness profile heights Ra, biggest roughness profile height Rz, maximum primary profile height Pt as well as maximum waviness profile height Wt a possibility of using surface asperities parameters as a measure of wear of chill graphite elements was proved. The most often applied parameter is Ra, but with a help of parameters from W and P family it was shown, that big changes occur not only for roughness but also for other components of surface irregularities.

  7. A model of the ground surface temperature for micrometeorological analysis

    Science.gov (United States)

    Leaf, Julian S.; Erell, Evyatar

    2017-07-01

    Micrometeorological models at various scales require ground surface temperature, which may not always be measured in sufficient spatial or temporal detail. There is thus a need for a model that can calculate the surface temperature using only widely available weather data, thermal properties of the ground, and surface properties. The vegetated/permeable surface energy balance (VP-SEB) model introduced here requires no a priori knowledge of soil temperature or moisture at any depth. It combines a two-layer characterization of the soil column following the heat conservation law with a sinusoidal function to estimate deep soil temperature, and a simplified procedure for calculating moisture content. A physically based solution is used for each of the energy balance components allowing VP-SEB to be highly portable. VP-SEB was tested using field data measuring bare loess desert soil in dry weather and following rain events. Modeled hourly surface temperature correlated well with the measured data (r 2 = 0.95 for a whole year), with a root-mean-square error of 2.77 K. The model was used to generate input for a pedestrian thermal comfort study using the Index of Thermal Stress (ITS). The simulation shows that the thermal stress on a pedestrian standing in the sun on a fully paved surface, which may be over 500 W on a warm summer day, may be as much as 100 W lower on a grass surface exposed to the same meteorological conditions.

  8. Profilometric analysis of root surfaces after using various polishing agents

    Directory of Open Access Journals (Sweden)

    Anjan Jana

    2016-01-01

    Full Text Available Background: Polishing is an important step in oral prophylaxis procedure which retards further accumulation of plaque on the root surfaces. Though polishing was done with various abrasive particles with different sizes over a long period of time, it was never been highlighted to evaluate the ideal polishing material and the particle size that would produce the ideal surface smoothness (Ra 5 μm are not able to produce the surface smoothness <0.2 μm. Only, submicron sized particles are able to produce the desired smoothness.

  9. SIMS imaging in the analysis of chemically altered coal surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Martin, R.R. (Western Ontario Univ., London, ON (Canada)); Maephee, J.A. (Canmet Energy Research Lab., 555 Booth St., Ottawa, Ontario (CA))

    1989-01-01

    Secondary ion mass spectrometry (SIMS) has been used to study the low temperature oxidation of coal. Specifically, SIMS imaging has been used to study the surface distribution of /sup 16/O/sup -/ and /sup 18/O/sup -/ after mild oxidation in /sup 18/O/sub 2/ and to correlate the results with the organic and inorganic regions on the coal. In addition, coal surfaces have been treated with Tollens' reagent and the resulting silver deposition has been used as a probe for specific reactive oxygen functional groups. The results suggest the presence of surface peroxides, as well as an intimate association of reactive oxygen with the mineral apatite.

  10. Isotope analysis of U using surface ionization mass spectrometry

    International Nuclear Information System (INIS)

    Cesario, Jean

    Surface ionization mass spectrometry is a good technique for the determination of U isotope concentrations. The principles of the method are described: ionization, optical systems, measuring systems. The sensitivity and accuracy of the method are presented [fr

  11. Surface Ship Shock Modeling and Simulation: Two-Dimensional Analysis

    Directory of Open Access Journals (Sweden)

    Young S. Shin

    1998-01-01

    Full Text Available The modeling and simulation of the response of a surface ship system to underwater explosion requires an understanding of many different subject areas. These include the process of underwater explosion events, shock wave propagation, explosion gas bubble behavior and bubble-pulse loading, bulk and local cavitation, free surface effect, fluid-structure interaction, and structural dynamics. This paper investigates the effects of fluid-structure interaction and cavitation on the response of a surface ship using USA-NASTRAN-CFA code. First, the one-dimensional Bleich-Sandler model is used to validate the approach, and second, the underwater shock response of a two-dimensional mid-section model of a surface ship is predicted with a surrounding fluid model using a constitutive equation of a bilinear fluid which does not allow transmission of negative pressures.

  12. Surface Operations Data Analysis and Adaptation Tool, Phase I

    Data.gov (United States)

    National Aeronautics and Space Administration — The Surface Management System (SMS), developed by NASA Ames Research Center in cooperation with the FAA, has received wide and significant acceptance by the air...

  13. Surface free energy analysis of adsorbents used for radioiodine adsorption

    Energy Technology Data Exchange (ETDEWEB)

    González-García, C.M. [Departamento de Física Aplicada, Universidad de Extremadura, Avda. Elvas s/n, 06006 Badajoz (Spain); Román, S., E-mail: sroman@unex.es [Departamento de Física Aplicada, Universidad de Extremadura, Avda. Elvas s/n, 06006 Badajoz (Spain); González, J.F.; Sabio, E. [Departamento de Física Aplicada, Universidad de Extremadura, Avda. Elvas s/n, 06006 Badajoz (Spain); Ledesma, B. [Departamento de Ingeniería Mecánica, Energética y de los Materiales, Universidad de Extremadura, Avda. Elvas s/n, 06006 Badajoz (Spain)

    2013-10-01

    In this work, the surface free energy of biomass-based activated carbons, both fresh and impregnated with triethylenediamine, has been evaluated. The contribution of Lifshitz van der Waals components was determined by the model proposed by van Oss et al. The results obtained allowed predicting the most probable configurations of the impregnant onto the carbon surface and its influence on the subsequent adsorption of radioactive methyl iodide.

  14. Power Spectral Density Specification and Analysis of Large Optical Surfaces

    Science.gov (United States)

    Sidick, Erkin

    2009-01-01

    The 2-dimensional Power Spectral Density (PSD) can be used to characterize the mid- and the high-spatial frequency components of the surface height errors of an optical surface. We found it necessary to have a complete, easy-to-use approach for specifying and evaluating the PSD characteristics of large optical surfaces, an approach that allows one to specify the surface quality of a large optical surface based on simulated results using a PSD function and to evaluate the measured surface profile data of the same optic in comparison with those predicted by the simulations during the specification-derivation process. This paper provides a complete mathematical description of PSD error, and proposes a new approach in which a 2-dimentional (2D) PSD is converted into a 1-dimentional (1D) one by azimuthally averaging the 2D-PSD. The 1D-PSD calculated this way has the same unit and the same profile as the original PSD function, thus allows one to compare the two with each other directly.

  15. Apollo remote analysis system applied to surface and underwater in-situ elemental analysis

    International Nuclear Information System (INIS)

    Evans, L.G.; Bielefeld, M.J.; Eller, E.L.; Schmadebeck, R.L.; Trombka, J.I.; Mustafa, M.G.; Senftle, F.E.; Heath, R.L.; Stehling, K.; Vadus, J.

    1976-01-01

    The surveying of the elemental composition of bulk samples over extended areas in near real-time would be an invaluable tool for surface and underwater environmental analysis. However, few techniques provide such a capability. Based on the experience from the orbital gamma-ray spectrometer experiments on Apollo 15 and 16 in which elemental composition of large portions of the moon were determined, an analysis system has been developed for terrestrial applications, which can fulfill these requirements. A portable, compact pulsed neutron generator and NaI(Tl) detector system coupled to associated electronics under mini-computer control can provide the timing and spectral characteristics necessary to determine elemental composition for many applications. Field trials of the system for underwater elemental analysis are planned during the next year

  16. Surface analysis of thin film coatings on container glass

    International Nuclear Information System (INIS)

    Bhargava, A.; Wood, B.

    1999-01-01

    Full text: Container glass is generally coated with a tin oxide layer followed by a coating of polymer. These coatings are believed to improve the mechanical properties of container glass as well as aid in the application of advertising labels to glass. The tin oxide layer on commercial beer bottles has a total thickness of about 15-20nm which consists of an interfacial layer comprising 70-85% of the total thickness. The polymer coating is about 2-5nm thick and also possesses an interfacial layer with tin oxide. A PHI Model 560 XPS/ SAM/ SIMS multi-technique system Is used to estimate concentration profiles of Sn, O, C, Si, Ca, Na and O. A combination of XPS, AES and SIMS is necessary to describe the coatings. Instrumental conditions and sample preparation methods are developed to optimize the analysis of thin films on glass. The coating comprises of three areas, namely (A) where polymer and tin co-exist (B) a pure tin oxide layer and (C) where tin co-exists with glass. By varying the chemical source of tin, it is possible to systematically vary the thickness of the interface and the concentration profile of Sn. Using XRD, crystalline phase(s) could be detected in tin oxide films as thin as 15nm. While the principle phase is cassiterite, a second phase is also detected which is believed to originate from the interface. Using a UMIS 2000 nanoindentor system, instrumental parameters are optimized for measurement of elastic modulus of films at varying depths, i.e. from surface of coating to the bulk of the glass. A sharp rise is observed at depth corresponding to the interface which is indicative of the significance of the interfacial layer. Samples are prepared by systematic ion-milling which are representative of various regions of the coating, namely (A), (B) and (C). These samples are analyzed by XRD and TEM. Based on these studies, a structural model of tin oxide layer and interface is presented to explain increase in elastic modulus at the interface. Copyright

  17. NOAA Optimum Interpolation 1/4 Degree Daily Sea Surface Temperature (OISST) Analysis, Version 2

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — This high-resolution sea surface temperature (SST) analysis product was developed using an optimum interpolation (OI) technique. The SST analysis has a spatial grid...

  18. Chemical analysis of surface oxygenated moieties of fluorescent carbon nanoparticles

    Science.gov (United States)

    Huang, Jie; Deming, Christopher P.; Song, Yang; Kang, Xiongwu; Zhou, Zhi-You; Chen, Shaowei

    2012-01-01

    Water-soluble carbon nanoparticles were prepared by refluxing natural gas soot in concentrated nitric acid. The surface of the resulting nanoparticles was found to be decorated with a variety of oxygenated species, as suggested by spectroscopic measurements. Back potentiometric titration of the nanoparticles was employed to quantify the coverage of carboxylic, lactonic, and phenolic moieties on the particle surface by taking advantage of their vast difference of acidity (pKa). The results were largely consistent with those reported in previous studies with other carbonaceous (nano)materials. Additionally, the presence of ortho- and para-quinone moieties on the nanoparticle surface was confirmed by selective labelling with o-phenylenediamine, as manifested in X-ray photoelectron spectroscopy, photoluminescence, and electrochemical measurements. The results further supported the arguments that the surface functional moieties that were analogous to 9,10-phenanthrenequinone were responsible for the unique photoluminescence of the nanoparticles and the emission might be regulated by surface charge state, as facilitated by the conjugated graphitic core matrix.

  19. Chemical analysis of surface oxygenated moieties of fluorescent carbon nanoparticles.

    Science.gov (United States)

    Huang, Jie; Deming, Christopher P; Song, Yang; Kang, Xiongwu; Zhou, Zhi-You; Chen, Shaowei

    2012-02-07

    Water-soluble carbon nanoparticles were prepared by refluxing natural gas soot in concentrated nitric acid. The surface of the resulting nanoparticles was found to be decorated with a variety of oxygenated species, as suggested by spectroscopic measurements. Back potentiometric titration of the nanoparticles was employed to quantify the coverage of carboxylic, lactonic, and phenolic moieties on the particle surface by taking advantage of their vast difference of acidity (pK(a)). The results were largely consistent with those reported in previous studies with other carbonaceous (nano)materials. Additionally, the presence of ortho- and para-quinone moieties on the nanoparticle surface was confirmed by selective labelling with o-phenylenediamine, as manifested in X-ray photoelectron spectroscopy, photoluminescence, and electrochemical measurements. The results further supported the arguments that the surface functional moieties that were analogous to 9,10-phenanthrenequinone were responsible for the unique photoluminescence of the nanoparticles and the emission might be regulated by surface charge state, as facilitated by the conjugated graphitic core matrix. This journal is © The Royal Society of Chemistry 2012

  20. Experimental Analysis of Grease Friction Properties on Sliding Textured Surfaces

    Directory of Open Access Journals (Sweden)

    Xijun Hua

    2017-10-01

    Full Text Available There is comprehensive work on the tribological properties and lubrication mechanisms of oil lubricant used on textured surfaces, however the use of grease lubrication on textured surfaces is rather new. This research article presents an experimental study of the frictional behaviours of grease lubricated sliding contact under mixed lubrication conditions. The influences of surface texture parameters on the frictional properties were investigated using a disc-on-ring tribometer. The results showed that the friction coefficient is largely dependent on texture parameters, with higher and lower texture density resulting in a higher friction coefficient at a fixed texture depth. The sample with texture density of 15% and texture depth of 19 μm exhibited the best friction properties in all experimental conditions because it can store more grease and trap wear debris. The reduction of friction is mainly attributable to the formation of a stable grease lubrication film composed of oil film, transfer film and deposited film, and the hydrodynamic pressure effect of the surface texture, which increases the mating gap and reduces the probability of asperity contact. This result will help in understanding the tribological behaviour of grease on a textured surface and in predicting the lubrication conditions of sliding bearings for better operation in any machinery.

  1. Analysis of flame surface density measurements in turbulent premixed combustion

    Energy Technology Data Exchange (ETDEWEB)

    Halter, Fabien [Institut PRISME, Universite d' Orleans, 45072 Orleans (France); Chauveau, Christian; Goekalp, Iskender [Institut de Combustion, Aerothermique, Reactivite et Environnement, Centre National de la Recherche Scientifique, 45071 Orleans (France); Veynante, Denis [Laboratoire E.M2.C, Centre National de la Recherche Scientifique, Ecole Centrale Paris, 92295 Chatenay-Malabry (France)

    2009-03-15

    In premixed turbulent combustion, reaction rates can be estimated from the flame surface density. This parameter, which measures the mean flame surface area available per unit volume, may be obtained from algebraic expressions or by solving a transport equation. In this study, detailed measurements were performed on a Bunsen-type burner fed with methane/air mixtures in order to determine the local flame surface density experimentally. This burner, located in a high-pressure combustion chamber, allows investigation of turbulent premixed flames under various flow, mixture, and pressure conditions. In the present work, equivalence ratio was varied from 0.6 to 0.8 and pressure from 0.1 to 0.9 MPa. Flame front visualizations by Mie scattering laser tomography are used to obtain experimental data on the instantaneous flame front dynamics. The exact equation given by Pope is used to obtain flame surface density maps for different flame conditions. Some assumptions are made in order to access three-dimensional information from our two-dimensional experiments. Two different methodologies are proposed and tested in term of global mass balance (what enters compared to what is burned). The detailed experimental flame surface data provided for the first time in this work should progressively allow improvement of turbulent premixed flame modeling approaches. (author)

  2. Surface integrity analysis when milling ultrafine-grained steels

    Directory of Open Access Journals (Sweden)

    Alessandro Roger Rodrigues

    2012-02-01

    Full Text Available This paper quantifies the effects of milling conditions on surface integrity of ultrafine-grained steels. Cutting speed, feed rate and depth of cut were related to microhardness and microstructure of the workpiece beneath machined surface. Low-carbon alloyed steel with 10.8 µm (as-received and 1.7 µm (ultrafine grain sizes were end milled using the down-milling and dry condition in a CNC machining center. The results show ultrafine-grained workpiece preserves its surface integrity against cutting parameters more than the as-received material. Cutting speed increases the microhardness while depth of cut deepens the hardened layer of the as-received material. Also, deformations of microstructure following feed rate direction were observed in workpiece subsurface.

  3. Infrared Analysis Of Enzymes Adsorbed Onto Model Surfaces

    Science.gov (United States)

    Story, Gloria M.; Rauch, Deborah S.; Brode, Philip F.; Marcott, Curtis A.

    1989-12-01

    The adsorption of the enzymes, subtilisin BPN' and lysozyme, onto model surfaces was examined using attenuated total reflectance (ATR) infrared (IR) spectroscopy. Using a cylindrical internal reflection (CIRcle) cell with a Germanium (Ge) internal reflection element (IRE), model hydrophilic surfaces were made by plasma cleaning the IRE and model hydrophobic surfaces were made by precoating the IRE with a thin film of polystyrene. Gas chromatography (GC)-IR data collection software was used to monitor adsorption kinetics during the first five minutes after injection of the enzyme into the CIRcle cell. It was found that for both lysozyme and BPN', most of the enzyme that was going to adsorb onto the model surface did so within ten seconds after injection. Nearly an order-of-magnitude more BPN' adsorbed on the hydrophobic Ge surface than the hydrophilic one, while lysozyme adsorbed somewhat more strongly to the hydrophilic Ge surface. Overnight, the lysozyme layer continued to increase in thickness, while BPN' maintained its initial coverage. The appearance of carboxylate bands in some of the adsorbed BPN' spectra suggests the occurrence of peptide bond hydrolysis. A Au/Pd coating on the CIRcle cell o-rings had a significant effect on the adsorption of BPN'. (This coating was applied in an attempt to eliminate interfering Teflon absorption bands.) An apparent electrochemical reaction occurred, involving BPN', Ge, Au/Pd, and the salt solution used to stabilize BPN'. The result of this reaction was enhanced adsorption of the enzyme around the coated o-rings, etching of the Ge IRE at the o-ring site, and some autolysis of the enzyme. No such reaction was observed with lysozyme.

  4. Preliminary surface analysis of etched, bleached, and normal bovine enamel

    International Nuclear Information System (INIS)

    Ruse, N.D.; Smith, D.C.; Torneck, C.D.; Titley, K.C.

    1990-01-01

    X-ray photoelectron spectroscopic (XPS) and secondary ion-mass spectroscopic (SIMS) analyses were performed on unground un-pumiced, unground pumiced, and ground labial enamel surfaces of young bovine incisors exposed to four different treatments: (1) immersion in 35% H2O2 for 60 min; (2) immersion in 37% H3PO4 for 60 s; (3) immersion in 35% H2O2 for 60 min, in distilled water for two min, and in 37% H3PO4 for 60 s; (4) immersion in 37% H3PO4 for 60 s, in distilled water for two min, and in 35% H2O2 for 60 min. Untreated unground un-pumiced, unground pumiced, and ground enamel surfaces, as well as synthetic hydroxyapatite surfaces, served as controls for intra-tooth evaluations of the effects of different treatments. The analyses indicated that exposure to 35% H2O2 alone, besides increasing the nitrogen content, produced no other significant change in the elemental composition of any of the enamel surfaces investigated. Exposure to 37% H3PO4, however, produced a marked decrease in calcium (Ca) and phosphorus (P) concentrations and an increase in carbon (C) and nitrogen (N) concentrations in unground un-pumiced specimens only, and a decrease in C concentration in ground specimens. These results suggest that the reported decrease in the adhesive bond strength of resin to 35% H2O2-treated enamel is not caused by a change in the elemental composition of treated enamel surfaces. They also suggest that an organic-rich layer, unaffected by acid-etching, may be present on the unground un-pumiced surface of young bovine incisors. This layer can be removed by thorough pumicing or by grinding. An awareness of its presence is important when young bovine teeth are used in a model system for evaluation of resin adhesiveness

  5. Eddy current analysis by BEM utilizing loop electric and surface magnetic currents as unknowns

    International Nuclear Information System (INIS)

    Ishibashi, Kazuhisa

    2002-01-01

    The surface integral equations whose unknowns are the surface electric and magnetic currents are widely used in eddy current analysis. However, when the skin depth is thick, computational error is increased especially in obtaining electromagnetic fields near the edge of the conductor. In order to obtain the electromagnetic field accurately, we propose an approach to solve surface integral equations utilizing loop electric and surface magnetic currents as unknowns. (Author)

  6. Strain-stress analysis of surface prosthesis of hip joint

    Czech Academy of Sciences Publication Activity Database

    Návrat, Tomáš; Fuis, Vladimír; Florian, Z.; Hlavoň, Pavel

    2007-01-01

    Roč. 40, č. 2 (2007), S559-S559 ISSN 0021-9290. [ISB 2007. Taipei, 01.07.2007-05.07.2007] R&D Projects: GA ČR GA101/05/0136 Institutional research plan: CEZ:AV0Z20760514 Keywords : surface prosthesis * hip joint * FEM Subject RIV: BO - Biophysics Impact factor: 2.897, year: 2007

  7. Climate Prediction Center (CPC) Global Land Surface Air Temperature Analysis

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A station observation-based global land monthly mean surface air temperature dataset at 0.5 0.5 latitude-longitude resolution for the period from 1948 to the present...

  8. Modeling and analysis for surface roughness and material removal ...

    African Journals Online (AJOL)

    user

    terms of cutting parameters is also developed using regression modeling. The results indicate that the developed model is suitable for prediction of surface roughness and material removal rate in machining of unidirectional glass fiber reinforced plastics (UD-GFRP) composites. The predicted values and measured values ...

  9. Surface reactivity and layer analysis of chemisorbed reaction films in ...

    Indian Academy of Sciences (India)

    Administrator

    Abstract. Studies on surface reactivity of substrate iron (Fe-particles) were made in the tribo-chemical environment of alkyl octadecenoates. Two alkyl octadecenoates namely ethyl octadecenoate and methyl. 12-hydroxy octadecenoate, slightly different in their chemical nature, were taken for preparing the chemisorbed ...

  10. poincare surface analysis of two coupled quintic oscillators in a ...

    African Journals Online (AJOL)

    DJFLEX

    Simonovic, N. S. J., 1997. Classical chaos in the hydrogen atom near a metal Surface, J. Phys. B: At. Mol. Opt. Phys. 30, L613-L618. Wang, S. and Yu, P., 2005. Bifurcation of limit cycles in a quintic Hamiltonian system under a sixth-order perturbation, Chaos, Solitons and Fractals. 26 pp. 1317-1335. POINCARE SURFACE ...

  11. Surface plasmon resonance spectroscopy for analysis of influenza vaccines

    Science.gov (United States)

    The hemagglutinin (HA) compounds are surface glycoproteins of a virus that can initiate an immune response from a host organism. Hemagglutinin and the related neuraminidase (NA) compounds are the basis for virus strain classification and have become part of the accepted HN taxonomy. These compounds ...

  12. Climate Prediction Center (CPC) Global Land Surface Air Temperature Analysis

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A station observation-based global land monthly mean surface air temperature dataset at 0.5 x 0.5 latitude-longitude resolution for the period from 1948 to the...

  13. Monitoring and analysis of surface changes from undermining

    Czech Academy of Sciences Publication Activity Database

    Kajzar, Vlastimil; Doležalová, Hana

    2013-01-01

    Roč. 59, č. 4 (2013), s. 1-10 ISSN 1802-5420 R&D Projects: GA MŠk ED2.1.00/03.0082 Institutional support: RVO:68145535 Keywords : undermining * surface changes * surveying methods Subject RIV: DH - Mining, incl. Coal Mining http://gse.vsb.cz/2013/LIX-2013-4-1-10.pdf

  14. Hirshfeld surface analysis of new organotin(IV)-phosphoramide complexes

    Czech Academy of Sciences Publication Activity Database

    Pourayoubi, M.; Bayraq, S.S.; Tarahhomi, A.; Nečas, M.; Fejfarová, Karla; Dušek, Michal

    2014-01-01

    Roč. 751, SI (2014), s. 508-518 ISSN 0022-328X R&D Projects: GA ČR(CZ) GAP204/11/0809 Institutional support: RVO:68378271 Keywords : organotin(IV)-phosphoramide complexes * Hirshfeld surfaces * two-dimensional fingerprint plots * crystal packing Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 2.173, year: 2014

  15. Groundnut-Corn Starch Blend- A Response Surface Analysis

    African Journals Online (AJOL)

    Cookie bars were produced from mixtures of cassava and groundnut flours with cornstarch as binder. Box-Behnken response surface design for k=3 was used to study the effects of experimental variables for cassava flour (25-75%), groundnut flour (25-75%) and corn starch (5-15%). Effects of the experimental variables on ...

  16. Surface analysis of polydimethylsiloxane fouled with bovine serum albumin

    CSIR Research Space (South Africa)

    Windvoel, T

    2010-01-01

    Full Text Available are not well understood. The effects of BSA combined with surfactants (surface active molecules) have been studied but not the effects of BSA independently, even though some proteins can act as surfactants. It is important to know whether a protein is a...

  17. Surface reactivity and layer analysis of chemisorbed reaction films in ...

    Indian Academy of Sciences (India)

    Administrator

    Studies on surface reactivity of substrate iron (Fe-particles) were made in the tribo-chemical environment of alkyl octadecenoates. Two alkyl octadecenoates namely ethyl octadecenoate and methyl. 12-hydroxy octadecenoate, slightly different in their chemical nature, were taken for preparing the chemisorbed reaction films ...

  18. Modelling surface run-off and trends analysis over India

    Indian Academy of Sciences (India)

    responsible for run-off generation plays a major role in run-off modelling at region scales. Remote sensing, GIS and advancement of the computer technology based evaluation of land surface prop- erties at spatial and temporal scales are very useful input data for hydrological models. Using remote sensing data is not only ...

  19. Near surface stress analysis strategies for axisymmetric fretting

    Indian Academy of Sciences (India)

    through integration. In order to compare the near surface stresses from cylinder, strip and half-plane models, the applied traction profile is assumed to be ... the method of Fourier sine or cosine integral transform can be employed. ..... into two parts since the direct calculation of the integrals becomes difficult for some cases.

  20. Modeling and analysis for surface roughness and material removal ...

    African Journals Online (AJOL)

    International Journal of Engineering, Science and Technology ... A multiple objective utility model has been studied to optimize both the dependent parameters. ... Keywords: UD-GFRP composites, ANOVA, multi response optimization, utility concept, regression modeling, surface roughness, material removal rate, ...

  1. Enhancing multilingual latent semantic analysis with term alignment information.

    Energy Technology Data Exchange (ETDEWEB)

    Chew, Peter A.; Bader, Brett William

    2008-08-01

    Latent Semantic Analysis (LSA) is based on the Singular Value Decomposition (SVD) of a term-by-document matrix for identifying relationships among terms and documents from co-occurrence patterns. Among the multiple ways of computing the SVD of a rectangular matrix X, one approach is to compute the eigenvalue decomposition (EVD) of a square 2 x 2 composite matrix consisting of four blocks with X and XT in the off-diagonal blocks and zero matrices in the diagonal blocks. We point out that significant value can be added to LSA by filling in some of the values in the diagonal blocks (corresponding to explicit term-to-term or document-to-document associations) and computing a term-by-concept matrix from the EVD. For the case of multilingual LSA, we incorporate information on cross-language term alignments of the same sort used in Statistical Machine Translation (SMT). Since all elements of the proposed EVD-based approach can rely entirely on lexical statistics, hardly any price is paid for the improved empirical results. In particular, the approach, like LSA or SMT, can still be generalized to virtually any language(s); computation of the EVD takes similar resources to that of the SVD since all the blocks are sparse; and the results of EVD are just as economical as those of SVD.

  2. Multivariate analysis of attachment of biofouling organisms in response to material surface characteristics.

    Science.gov (United States)

    Gatley-Montross, Caitlyn M; Finlay, John A; Aldred, Nick; Cassady, Harrison; Destino, Joel F; Orihuela, Beatriz; Hickner, Michael A; Clare, Anthony S; Rittschof, Daniel; Holm, Eric R; Detty, Michael R

    2017-12-29

    Multivariate analyses were used to investigate the influence of selected surface properties (Owens-Wendt surface energy and its dispersive and polar components, static water contact angle, conceptual sign of the surface charge, zeta potentials) on the attachment patterns of five biofouling organisms (Amphibalanus amphitrite, Amphibalanus improvisus, Bugula neritina, Ulva linza, and Navicula incerta) to better understand what surface properties drive attachment across multiple fouling organisms. A library of ten xerogel coatings and a glass standard provided a range of values for the selected surface properties to compare to biofouling attachment patterns. Results from the surface characterization and biological assays were analyzed separately and in combination using multivariate statistical methods. Principal coordinate analysis of the surface property characterization and the biological assays resulted in different groupings of the xerogel coatings. In particular, the biofouling organisms were able to distinguish four coatings that were not distinguishable by the surface properties of this study. The authors used canonical analysis of principal coordinates (CAP) to identify surface properties governing attachment across all five biofouling species. The CAP pointed to surface energy and surface charge as important drivers of patterns in biological attachment, but also suggested that differentiation of the surfaces was influenced to a comparable or greater extent by the dispersive component of surface energy.

  3. Surface integrity analysis of abrasive water jet-cut surfaces of friction stir welded joints

    Czech Academy of Sciences Publication Activity Database

    Kumar, R.; Chattopadhyaya, S.; Dixit, A. R.; Bora, B.; Zeleňák, Michal; Foldyna, Josef; Hloch, Sergej; Hlaváček, Petr; Ščučka, Jiří; Klich, Jiří; Sitek, Libor; Vilaca, P.

    2017-01-01

    Roč. 88, č. 5 (2017), s. 1687-1701 ISSN 0268-3768 R&D Projects: GA MŠk(CZ) LO1406; GA MŠk ED2.1.00/03.0082 Institutional support: RVO:68145535 Keywords : friction stir welding (FSW) * abrasive water jet (AWJ) * optical profilometer * topography * surface roughness Subject RIV: JQ - Machines ; Tools OBOR OECD: Mechanical engineering Impact factor: 2.209, year: 2016 http://link.springer.com/article/10.1007/s00170-016-8776-0

  4. Computer analysis of transient heat transfer from coated surfaces

    International Nuclear Information System (INIS)

    Menard, A.; Holmes, D.

    1983-01-01

    The transient thermal response of internally heated, coated surfaces in contact with liquid helium was investigated with a previously developed computer model. The coatings were found to affect the time required to initiate film boiling or to quench a superconductor in the substrate. The energy which can be absorbed without an unacceptably large temperature rise depends most strongly upon the coating thermal property group (kpC /SUB p/ ) /SUP 1/2/ and on the peak nucleate boiling heat flux. Dielectric materials for electrical insulation usually have low thermal property group values, but a new class of ceramic materials shows great promise for application with superconducting devices as electrical insulations with good thermal properties. Coating materials with thermal property group values greater than that of OFHC copper at liquid helium temperatures provide the same thermal stability as a bare copper surface exposed to the helium bath. Possible applications of the new materials to potted windings are also discussed

  5. Thermal analysis of protruding surfaces in the JET divertor

    Czech Academy of Sciences Publication Activity Database

    Corre, Y.; Bunting, P.; Coenen, J.W.; Gaspar, J.; Iglesias, D.; Matthews, G.F.; Balboa, I.; Coffey, I.; Dejarnac, Renaud; Firdaouss, M.; Gauthier, E.; Jachmich, S.; Krieger, K.; Pitts, R.A.; Rack, M.; Silburn, S.A.

    2017-01-01

    Roč. 57, č. 6 (2017), č. článku 066009. ISSN 0029-5515 EU Projects: European Commission(XE) 633053 - EUROfusion Institutional support: RVO:61389021 Keywords : IR thermography * heat flux * tungsten melting Subject RIV: BL - Plasma and Gas Discharge Physics OBOR OECD: Fluids and plasma physics (including surface physics) Impact factor: 3.307, year: 2016 http://iopscience.iop.org/article/10.1088/1741-4326/aa687e/meta

  6. Assessment of Response Surface Models using Independent Confirmation Point Analysis

    Science.gov (United States)

    DeLoach, Richard

    2010-01-01

    This paper highlights various advantages that confirmation-point residuals have over conventional model design-point residuals in assessing the adequacy of a response surface model fitted by regression techniques to a sample of experimental data. Particular advantages are highlighted for the case of design matrices that may be ill-conditioned for a given sample of data. The impact of both aleatory and epistemological uncertainty in response model adequacy assessments is considered.

  7. Correction of systematic behaviour in topographical surface analysis

    DEFF Research Database (Denmark)

    Quagliotti, Danilo; Baruffi, Federico; Tosello, Guido

    2016-01-01

    Four specimens in the sub-micrometre range and with different polishing were topographically investigated in fiveareas over their respective surfaces. Uncertainties were evaluated with and without correction for systematicbehaviour and successively analysed by a design of experiment (DOE). Result...... showed that the correction forsystematic behaviour allowed for a lower value of the estimated uncertainty when the correction was adequate tocompletely recognise the systematic effects. If not, the correction can produce an overestimation of the uncertainty....

  8. Analysis of shape correctness of surfaces of diamond burnished components

    Directory of Open Access Journals (Sweden)

    Varga Gyula

    2017-01-01

    Full Text Available In these days, diamond burnishing is frequently used for final finishing manufacturing operations of components. Diamond burnishing belongs to cold plastic manufacturing procedures. When using this technique, the following advantages can be obtained: micro-hardness of near surface layer is increasing; surface roughness is improving and the shape correctness is also improving. This paper deals with how the different technological parameters of burnishing, such as the feed rate, the burnishing speed and the burnishing force effect on the cylindricity of the burnished workpiece. The experiment was done on some specimen having outer cylindrical surfaces. The experiments were executed by the Taguchi type Full Factorial Experiment Design method with which empirical formulas can be efficiently created. The measurements of the cylindricity of specimens were done with a circular and position error measuring. From the measured data, special improvement ratios were calculated in order to define the appropriate range of technological parameters which results high improvements. Further aim was to compare the measured values of different cylindricity parameters.

  9. Quantitative Analysis and Efficient Surface Modification of Silica Nanoparticles

    Directory of Open Access Journals (Sweden)

    Hak-Sung Jung

    2012-01-01

    Full Text Available Aminofunctional trialkoxysilanes such as aminopropyltrimethoxysilane (APTMS and (3-trimethoxysilylpropyldiethylenetriamine (DETAS were employed as a surface modification molecule for generating monolayer modification on the surface of silica (SiO2 nanoparticles. We were able to quantitatively analyze the number of amine functional groups on the modified SiO2 nanoparticles by acid-base back titration method and determine the effective number of amine functional groups for the successive chemical reaction by absorption measurements after treating with fluorescent rhodamine B isothiocyanate (RITC molecules. The numbers of amine sites measured by back titration were 2.7 and 7.7 ea/nm2 for SiO2-APTMS and SiO2-DETAS, respectively, while the numbers of effective amine sites measured by absorption calibration were about one fifth of the total amine sites, namely, 0.44 and 1.3 ea/nm2 for SiO2-APTMS(RITC and SiO2-DETAS(RITC, respectively. Furthermore, it was confirmed that the reactivity of amino groups on the surface-modified silica nanoparticles could be maintained in ethanol for more than 1.5 months without showing any significant differences in the reactivity.

  10. Analysis of water microdroplet condensation on silicon surfaces

    Science.gov (United States)

    Honda, Takuya; Fujimoto, Kenya; Yoshimoto, Yuta; Mogi, Katsuo; Kinefuchi, Ikuya; Sugii, Yasuhiko; Takagi, Shu; Univ. of Tokyo Team; Tokyo Inst. of Tech. Team

    2016-11-01

    We observed the condensation process of water microdroplets on flat silicon (100) surfaces by means of the sequential visualization of the droplets using an environmental scanning electron microscope. As previously reported for nanostructured surfaces, the condensation process of water microdroplets on the flat silicon surfaces also exhibits two modes: the constant base (CB) area mode and the constant contact angle (CCA) mode. In the CB mode, the contact angle increases with time while the base diameter is constant. Subsequently, in the CCA mode, the base diameter increases with time while the contact angle remains constant. The dropwise condensation model regulated by subcooling temperature does not reproduce the experimental results. Because the subcooling temperature is not constant in the case of a slow condensation rate, this model is not applicable to the condensation of the long time scale ( several tens of minutes). The contact angle of water microdroplets ( several μm) tended to be smaller than the macro contact angle. Two hypotheses are proposed as the cause of small contact angles: electrowetting and the coalescence of sub- μm water droplets.

  11. Californium-252 plasma desorption mass analysis of proteins adsorbed on polymer and modified-polymer surfaces

    International Nuclear Information System (INIS)

    Hill, J.C.

    1987-01-01

    A new Cf-252 plasma desorption mass spectrometer has been built specifically for the analysis of large biomolecules. This mass spectrometer was used to investigate the interactions between proteins adsorbed onto polymer surfaces and how the chemical nature of the polymer surface influences the production of stable, gas-phase molecule ions. Chemical modification of the polymer surfaces was achieved by means of ultra-violet irradiation, resulting in the production of a more hydrophilic surface. Analysis of a series of model compounds adsorbed onto modified and non-modified polymer surfaces indicates that the wettability of the surface is an important influence in the production of stable molecular ions. This information was then utilized to aid in the analysis of lysozyme, myoglobin, and porcine trypsin

  12. Statistical analysis of planktic foraminifera of the surface Continental ...

    African Journals Online (AJOL)

    Planktic foraminiferal assemblage recorded from selected samples obtained from shallow continental shelf sediments off southwestern Nigeria were subjected to statistical analysis. The Principal Component Analysis (PCA) was used to determine variants of planktic parameters. Values obtained for these parameters were ...

  13. Fractal analysis of AFM images of the surface of Bowman's membrane of the human cornea.

    Science.gov (United States)

    Ţălu, Ştefan; Stach, Sebastian; Sueiras, Vivian; Ziebarth, Noël Marysa

    2015-04-01

    The objective of this study is to further investigate the ultrastructural details of the surface of Bowman's membrane of the human cornea, using atomic force microscopy (AFM) images. One representative image acquired of Bowman's membrane of a human cornea was investigated. The three-dimensional (3-D) surface of the sample was imaged using AFM in contact mode, while the sample was completely submerged in optisol solution. Height and deflection images were acquired at multiple scan lengths using the MFP-3D AFM system software (Asylum Research, Santa Barbara, CA), based in IGOR Pro (WaveMetrics, Lake Oswego, OR). A novel approach, based on computational algorithms for fractal analysis of surfaces applied for AFM data, was utilized to analyze the surface structure. The surfaces revealed a fractal structure at the nanometer scale. The fractal dimension, D, provided quantitative values that characterize the scale properties of surface geometry. Detailed characterization of the surface topography was obtained using statistical parameters, in accordance with ISO 25178-2: 2012. Results obtained by fractal analysis confirm the relationship between the value of the fractal dimension and the statistical surface roughness parameters. The surface structure of Bowman's membrane of the human cornea is complex. The analyzed AFM images confirm a fractal nature of the surface, which is not taken into account by classical surface statistical parameters. Surface fractal dimension could be useful in ophthalmology to quantify corneal architectural changes associated with different disease states to further our understanding of disease evolution.

  14. Fuzzy surfaces in GIS and geographical analysis theory, analytical methods, algorithms and applications

    CERN Document Server

    Lodwick, Weldon

    2007-01-01

    Surfaces are a central to geographical analysis. Their generation and manipulation are a key component of geographical information systems (GISs). However, geographical surface data is often not precise. When surfaces are used to model geographical entities, the data inherently contains uncertainty in terms of both position and attribute. Fuzzy Surface in GIS and Geographical Analysis sets out a process to identify the uncertainty in geographic entities. It describes how to successfully obtain, model, analyze, and display data, as well as interpret results within the context of GIS. Focusing on uncertainty that arises from transitional boundaries, the book limits its study to three types of uncertainties: intervals, fuzzy sets, and possibility distributions. The book explains that uncertainty in geographical data typically stems from these three and it is only natural to incorporate them into the analysis and display of surface data. The book defines the mathematics associated with each method for analysis,...

  15. Parametric analysis of change in wave number of surface waves

    Directory of Open Access Journals (Sweden)

    Tadić Ljiljana

    2015-01-01

    Full Text Available The paper analyzes the dependence of the change wave number of materials soil constants, ie the frequency of the waves. The starting point in this analysis cosists of wave equation and dynamic stiffness matrix of soil.

  16. QAPP for Hydraulic Fracturing (HF) Surface Spills Data Analysis

    Science.gov (United States)

    This QAPP provides information concerning the analysis of spills associated with hydraulic fracturing. This project is relevant to both the chemical mixing and flowback and produced water stages of the HF water cycle as found in the HF Study Plan.

  17. Surface enhanced Raman scattering (SERS) fabrics for trace analysis

    Energy Technology Data Exchange (ETDEWEB)

    Liu, Jun [National Engineering Laboratory for Advanced Yarn and Fabric Formation and Clean Production, Wuhan Textile University, Wuhan 430073 (China); Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials & Key Laboratory for the Synthesis and Application of Organic Functional Molecules, Ministry of Education & College of Chemistry & Chemical Engineering, Hubei University, Wuhan 430062 (China); Zhou, Ji [Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials & Key Laboratory for the Synthesis and Application of Organic Functional Molecules, Ministry of Education & College of Chemistry & Chemical Engineering, Hubei University, Wuhan 430062 (China); Tang, Bin, E-mail: bin.tang@deakin.edu.au [National Engineering Laboratory for Advanced Yarn and Fabric Formation and Clean Production, Wuhan Textile University, Wuhan 430073 (China); Institute for Frontier Materials, Deakin University, Geelong, Victoria 3216 (Australia); Zeng, Tian; Li, Yaling [Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials & Key Laboratory for the Synthesis and Application of Organic Functional Molecules, Ministry of Education & College of Chemistry & Chemical Engineering, Hubei University, Wuhan 430062 (China); Li, Jingliang [Institute for Frontier Materials, Deakin University, Geelong, Victoria 3216 (Australia); Ye, Yong, E-mail: yeyong@hubu.edu.cn [Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials & Key Laboratory for the Synthesis and Application of Organic Functional Molecules, Ministry of Education & College of Chemistry & Chemical Engineering, Hubei University, Wuhan 430062 (China); Wang, Xungai [National Engineering Laboratory for Advanced Yarn and Fabric Formation and Clean Production, Wuhan Textile University, Wuhan 430073 (China); Institute for Frontier Materials, Deakin University, Geelong, Victoria 3216 (Australia)

    2016-11-15

    Highlights: • Gold nanoparticles are in-situ synthesized on silk fabrics by heating. • Flexible silk fabrics with gold nanoparticles are used for surface-enhanced Raman scattering (SERS). • SERS activities of silk fabrics with different gold contents are investigated. - Abstract: Flexible SERS active substrates were prepared by modification of silk fabrics with gold nanoparticles. Gold nanoparticles were in-situ synthesized after heating the silk fabrics immersed in gold ion solution. Localized surface plasmon resonance (LSPR) properties of the treated silk fabrics varied as the concentration of gold ions changed, in relation to the morphologies of gold nanoparticles on silk. In addition, X-ray diffraction (XRD) was used to observe the structure of the gold nanoparticle treated silk fabrics. The SERS enhancement effect of the silk fabrics treated with gold nanoparticles was evaluated by collecting Raman signals of different concentrations of p-aminothiophenol (PATP), 4-mercaptopyridine (4-MPy) and crystal violet (CV) solutions. The results demonstrate that the silk fabrics corresponding to 0.3 and 0.4 mM of gold ions possess high SERS activity compared to the other treated fabrics. It is suggested that both the gold content and morphologies of gold nanoparticles dominate the SERS effect of the treated silk fabrics.

  18. Organic analysis of lunar samples and the Martian surface.

    Science.gov (United States)

    Oro, J.; Flory, D.

    1973-01-01

    In addition to the organogenic elements (H, C, N, O, S, P) which are necessary for the synthesis of organic molecules, the lunar samples from Apollo 11, 12, 14, and 15 contain substantial amounts of CO, N2, and CO2 which are released at relatively high temperatures and smaller amounts of more complex organic compounds (e.g., benzene). The lunar surface provides one of the less favorable solar system models for the synthesis of organic compounds; yet small amounts of these compounds have been detected in the returned samples. It is reasonable to assume that the different physical and developmental features of the planet Mars (increased gravitational field, presence of an atmosphere with CO2, CO, and H2O, recent volcanic and tectonic activity, etc.) would favor an increased organic content of the surface of this planet relative to the moon. Therefore the organic molecules present in the Martian soil should be measurable by miniaturized mass spectrometers after fractional distillation or gas chromatographic separation of the volatiles released by moderate heating.

  19. Predicting Biological Age from a Skin Surface Capacitive Analysis

    Science.gov (United States)

    Bevilacqua, Alessandro; Gherardi, Alessandro; Ferri, Massimo

    The skin is the largest (and the most exposed) organ of the body both in terms of surface area and weight. Its care is of great importance for both aesthetics and health issues. Often, the skin appearance gives us information about the skin health status as well as hints at the biological age. Therefore, the skin surface characterization is of great significance for dermatologists as well as for cosmetic scientists in order to evaluate the effectiveness of medical or cosmetic treatments. So far, no in vivo measurements regarding skin topography characterization could be achieved routinely to evaluate skin aging. This work describes how a portable capacitive device, normally used for fingerprint acquisition, can be utilized to achieve measures of skin aging routinely. The capacitive images give a high resolution (50 μm) representation of skin topography, in terms of wrinkles and cells. In this work, we have addressed the latter: through image segmentation techniques, cells have been localized and identified and a feature related to their area distribution has been generated. Accurate experiments accomplished in vivo show how the feature we conceived is linearly related to skin aging. Besides, since this finding has been achieved using a low cost portable device, this could boost research in this field as well as open doors to an application based on an embedded system.

  20. Surface topographical and structural analysis of Ag+-implanted polymethylmethacrylate

    International Nuclear Information System (INIS)

    Arif, Shafaq; Rafique, M. Shahid; Saleemi, Farhat; Naab, Fabian; Toader, Ovidiu; Sagheer, Riffat; Bashir, Shazia; Zia, Rehana; Siraj, Khurram; Iqbal, Saman

    2016-01-01

    Specimens of polymethylmethacrylate (PMMA) were implanted with 400-keV Ag + ions at different ion fluences ranging from 1 × 10 14 to 5 × 10 15 ions/cm 2 using a 400-kV NEC ion implanter. The surface topographical features of the implanted PMMA were investigated by a confocal microscope. Modifications in the structural properties of the implanted specimens were analyzed in comparison with pristine PMMA by X-ray diffraction (XRD) and Raman spectroscopy. UV–Visible spectroscopy was applied to determine the effects of ion implantation on optical transmittance of the implanted PMMA. The confocal microscopic images revealed the formation of hillock-like microstructures along the ion track on the implanted PMMA surface. The increase in ion fluence led to more nucleation of hillocks. The XRD pattern confirmed the amorphous nature of pristine and implanted PMMA, while the Raman studies justified the transformation of Ag + -implanted PMMA into amorphous carbon at the ion fluence of ⩾5 × 10 14 ions/cm 2 . Moreover, the decrease in optical transmittance of PMMA is associated with the formation of hillocks and ion-induced structural modifications after implantation.

  1. Thermodynamic analysis of shark skin texture surfaces for microchannel flow

    Science.gov (United States)

    Yu, Hai-Yan; Zhang, Hao-Chun; Guo, Yang-Yu; Tan, He-Ping; Li, Yao; Xie, Gong-Nan

    2016-09-01

    The studies of shark skin textured surfaces in flow drag reduction provide inspiration to researchers overcoming technical challenges from actual production application. In this paper, three kinds of infinite parallel plate flow models with microstructure inspired by shark skin were established, namely blade model, wedge model and the smooth model, according to cross-sectional shape of microstructure. Simulation was carried out by using FLUENT, which simplified the computation process associated with direct numeric simulations. To get the best performance from simulation results, shear-stress transport k-omega turbulence model was chosen during the simulation. Since drag reduction mechanism is generally discussed from kinetics point of view, which cannot interpret the cause of these losses directly, a drag reduction rate was established based on the second law of thermodynamics. Considering abrasion and fabrication precision in practical applications, three kinds of abraded geometry models were constructed and tested, and the ideal microstructure was found to achieve best performance suited to manufacturing production on the basis of drag reduction rate. It was also believed that bionic shark skin surfaces with mechanical abrasion may draw more attention from industrial designers and gain wide applications with drag-reducing characteristics.

  2. [Surface-enhanced Raman spectroscopy analysis of thiabendazole pesticide].

    Science.gov (United States)

    Lin, Lei; Wu, Rui-mei; Liu, Mu-hua; Wang, Xiao-bin; Yan, Lin-yuan

    2015-02-01

    Surface-enhanced Raman spectroscopy (SERS) technique was used to analyze the Raman peaks of thiabendazole pesticides in the present paper. Surface enhanced substrates of silver nanoparticle were made based on microwave technology. Raman signals of thiabendazole were collected by laser Micro-Raman spectrometer with 514. 5 and 785 nm excitation wavelengths, respectively. The Raman peaks at different excitation wavelengths were analyzed and compared. The Raman peaks 782 and 1 012 at 785 nm excitation wavelength were stronger, which were C--H out-of-plane vibrations. While 1284, 1450 and 1592 cm(-1) at 514.5 nm excitation wavelength were stronger, which were vng and C==N stretching. The study results showed that the intensity of Raman peak and Raman shift at different excitation wavelengths were different And strong Raman signals were observed at 782, 1012, 1284, 1450 and 1592 cm(-1) at 514.5 and 785 nm excitation wavelengths. These characteristic vibrational modes are characteristic Raman peaks of carbendazim pesticide. The results can provide basis for the rapid screening of pesticide residue in agricultural products and food based on Raman spectrum.

  3. Surface enhanced Raman scattering (SERS) fabrics for trace analysis

    International Nuclear Information System (INIS)

    Liu, Jun; Zhou, Ji; Tang, Bin; Zeng, Tian; Li, Yaling; Li, Jingliang; Ye, Yong; Wang, Xungai

    2016-01-01

    Highlights: • Gold nanoparticles are in-situ synthesized on silk fabrics by heating. • Flexible silk fabrics with gold nanoparticles are used for surface-enhanced Raman scattering (SERS). • SERS activities of silk fabrics with different gold contents are investigated. - Abstract: Flexible SERS active substrates were prepared by modification of silk fabrics with gold nanoparticles. Gold nanoparticles were in-situ synthesized after heating the silk fabrics immersed in gold ion solution. Localized surface plasmon resonance (LSPR) properties of the treated silk fabrics varied as the concentration of gold ions changed, in relation to the morphologies of gold nanoparticles on silk. In addition, X-ray diffraction (XRD) was used to observe the structure of the gold nanoparticle treated silk fabrics. The SERS enhancement effect of the silk fabrics treated with gold nanoparticles was evaluated by collecting Raman signals of different concentrations of p-aminothiophenol (PATP), 4-mercaptopyridine (4-MPy) and crystal violet (CV) solutions. The results demonstrate that the silk fabrics corresponding to 0.3 and 0.4 mM of gold ions possess high SERS activity compared to the other treated fabrics. It is suggested that both the gold content and morphologies of gold nanoparticles dominate the SERS effect of the treated silk fabrics.

  4. In-situ analysis of planetary surfaces by Moessbauer spectroscopy

    International Nuclear Information System (INIS)

    Klingelhoefer, G.

    1998-01-01

    Iron is one of the key elements in the evolution of the solar system and is highly abundant in terrestrial planets. Its oxidation state reflects the history of the oxidation-reduction reactions on planetary surfaces. The identification of iron mineralogies and the relative abundance of iron oxidation states (2+ and 3+) will contribute to a much deeper understanding of the evolution of planetary bodies and their surfaces. Miniaturized Moessbauer spectrometers are under development primarily for missions to the planet Mars and the Moon, but there is also an interest on using such an instrument for space missions to the planet Venus, comets and asteroids. The instrument MIMOS II developed at TU Darmstadt meets the requirements for space application as low mass (about 500 g), small volume, and low power consumption (about 1 W). The instrument has been tested extensively in the laboratory but also recently in the field mounted on the robotic arm of a prototype Martian Rover under development at JPL/NASA, United States

  5. Assessment of surface water quality using hierarchical cluster analysis

    Directory of Open Access Journals (Sweden)

    Dheeraj Kumar Dabgerwal

    2016-02-01

    Full Text Available This study was carried out to assess the physicochemical quality river Varuna inVaranasi,India. Water samples were collected from 10 sites during January-June 2015. Pearson correlation analysis was used to assess the direction and strength of relationship between physicochemical parameters. Hierarchical Cluster analysis was also performed to determine the sources of pollution in the river Varuna. The result showed quite high value of DO, Nitrate, BOD, COD and Total Alkalinity, above the BIS permissible limit. The results of correlation analysis identified key water parameters as pH, electrical conductivity, total alkalinity and nitrate, which influence the concentration of other water parameters. Cluster analysis identified three major clusters of sampling sites out of total 10 sites, according to the similarity in water quality. This study illustrated the usefulness of correlation and cluster analysis for getting better information about the river water quality.International Journal of Environment Vol. 5 (1 2016,  pp: 32-44

  6. Individual IOL Surface Topography Analysis by the WaveMaster Reflex UV

    Directory of Open Access Journals (Sweden)

    Marc Kannengießer

    2013-01-01

    Full Text Available Purpose. In order to establish inspection routines for individual intraocular lenses (IOLs, their surfaces have to be measured separately. Currently available measurement devices lack this functionality. The purpose of this study is to evaluate a new topography measurement device based on wavefront analysis for measuring individual regular and freeform IOL surfaces, the “WaveMaster Reflex UV” (Trioptics, Wedel, Germany. Methods. Measurements were performed on IOLs with increasingly complex surface geometries: spherical surfaces, surfaces modelled by higher-order Zernike terms, and freeform surfaces from biometrical patient data. Two independent parameters were measured: the sample’s radius of curvature (ROC and its residual (difference of sample topography and its best-fit sphere. We used a quantitative analysis method by calculating the residuals’ root-mean-square (RMS and peak-to-Valley (P2V values. Results. The sample’s best-fit ROC differences increased with the sample’s complexity. The sample’s differences of RMS values were 80 nm for spherical surfaces, 97 nm for higher-order samples, and 21 nm for freeform surfaces. Graphical representations of both measurement and design topographies were recorded and compared. Conclusion. The measurements of spherical surfaces expectedly resulted in better values than those of freeform surfaces. Overall, the wavefront analysing method proves to be an effective method for evaluating individual IOL surfaces.

  7. Quantitative surface analysis using deuteron-induced nuclear reactions

    International Nuclear Information System (INIS)

    Afarideh, Hossein

    1991-01-01

    The nuclear reaction analysis (NRA) technique consists of looking at the energies of the reaction products which uniquely define the particular elements present in the sample and it analysis the yield/energy distribution to reveal depth profiles. A summary of the basic features of the nuclear reaction analysis technique is given, in particular emphasis is placed on quantitative light element determination using (d,p) and (d,alpha) reactions. The experimental apparatus is also described. Finally a set of (d,p) spectra for the elements Z=3 to Z=17 using 2 MeV incident deutrons is included together with example of more applications of the (d,alpha) spectra. (author)

  8. Multispectral UV imaging for surface analysis of MUPS tablets with special focus on the pellet distribution

    DEFF Research Database (Denmark)

    Novikova, Anna; Carstensen, Jens Michael; Rades, Thomas

    2016-01-01

    In the present study the applicability of multispectral UV imaging in combination with multivariate image analysis for surface evaluation of MUPS tablets was investigated with respect to the differentiation of the API pellets from the excipients matrix, estimation of the drug content as well...... on the tablet surface allowed an estimation of the true drug content in the respective MUPS tablet. In addition, the pellet distribution in the MUPS formulations could be estimated by UV image analysis of the tablet surface. In conclusion, this study revealed that UV imaging in combination with multivariate...... image analysis is a promising approach for the automatic quality control of MUPS tablets during the manufacturing process....

  9. Methods of remote surface chemical analysis for asteroid missions

    International Nuclear Information System (INIS)

    Sagdeev, R.Z.; Managadze, G.G.; Shutyaev, I.Yu.; Timofeev, P.P.; Szegoe, K.

    1984-06-01

    Different remote sensing methods are discussed which can be applied to investigate the chemical composition of minor bodies of the Solar System. The secondary-ion method, remote laser mass-analysis and electron beam induced X-ray emission analysis are treated in detail. Relative advantages of these techniques are analyzed. The physical limitation of the methods: effects of solar magnetic field and solar wind on the secondary-ion and laser methods and the effect of electrostatic potential of the space apparatus on the ion and electron beam methods are described. First laboratory results of remote laser method are given. (D.Gy.)

  10. Analysis of Surface Wave Attenuation in Mangrove Forests

    Directory of Open Access Journals (Sweden)

    Safwan Hadi

    2003-11-01

    Full Text Available This paper presents an analytical study on surface wave attenuation in mangrove forest using analytical model developed by Massel et.al. (1999. The energy dissipation in the frequency domain is determined by treating the mangrove forest as a random media with certain characteristics using the geometry of mangrove trunks and their locations. Initial nonlinear governing equations are linearized using the concept of minimalization in the stochastic sense and interactions between mangrove trunks and roots have been introduced through the modification of the drag coefficients. To see the effectiveness of the mangrove forest in attenuating wave energy the analytical model was applied to two types of mangrove forest i.e. Rhizophora and Ceriops forests. The resulting rate of wave energy attenuation depends strongly on the density of the mangrove forest, and on diameter of mangrove roots and trunks. More effective wave energy attenuation is shown by Rhizophora.

  11. Aerodynamic configuration design using response surface methodology analysis

    Science.gov (United States)

    Engelund, Walter C.; Stanley, Douglas O.; Lepsch, Roger A.; Mcmillin, Mark M.; Unal, Resit

    1993-01-01

    An investigation has been conducted to determine a set of optimal design parameters for a single-stage-to-orbit reentry vehicle. Several configuration geometry parameters which had a large impact on the entry vehicle flying characteristics were selected as design variables: the fuselage fineness ratio, the nose to body length ratio, the nose camber value, the wing planform area scale factor, and the wing location. The optimal geometry parameter values were chosen using a response surface methodology (RSM) technique which allowed for a minimum dry weight configuration design that met a set of aerodynamic performance constraints on the landing speed, and on the subsonic, supersonic, and hypersonic trim and stability levels. The RSM technique utilized, specifically the central composite design method, is presented, along with the general vehicle conceptual design process. Results are presented for an optimized configuration along with several design trade cases.

  12. Stability analysis of rough surfaces in adhesive normal contact

    Science.gov (United States)

    Rey, Valentine; Bleyer, Jeremy

    2018-03-01

    This paper deals with adhesive frictionless normal contact between one elastic flat solid and one stiff solid with rough surface. After computation of the equilibrium solution of the energy minimization principle and respecting the contact constraints, we aim at studying the stability of this equilibrium solution. This study of stability implies solving an eigenvalue problem with inequality constraints. To achieve this goal, we propose a proximal algorithm which enables qualifying the solution as stable or unstable and that gives the instability modes. This method has a low computational cost since no linear system inversion is required and is also suitable for parallel implementation. Illustrations are given for the Hertzian contact and for rough contact.

  13. Analysis III analytic and differential functions, manifolds and Riemann surfaces

    CERN Document Server

    Godement, Roger

    2015-01-01

    Volume III sets out classical Cauchy theory. It is much more geared towards its innumerable applications than towards a more or less complete theory of analytic functions. Cauchy-type curvilinear integrals are then shown to generalize to any number of real variables (differential forms, Stokes-type formulas). The fundamentals of the theory of manifolds are then presented, mainly to provide the reader with a "canonical'' language and with some important theorems (change of variables in integration, differential equations). A final chapter shows how these theorems can be used to construct the compact Riemann surface of an algebraic function, a subject that is rarely addressed in the general literature though it only requires elementary techniques. Besides the Lebesgue integral, Volume IV will set out a piece of specialized mathematics towards which the entire content of the previous volumes will converge: Jacobi, Riemann, Dedekind series and infinite products, elliptic functions, classical theory of modular fun...

  14. Cell behavior related to implant surfaces with different microstructure and chemical composition: an in vitro analysis.

    Science.gov (United States)

    Conserva, Enrico; Lanuti, Anna; Menini, Maria

    2010-01-01

    This paper reports on an in vitro comparison of osteoblast and mesenchymal stem cell (MSC) adhesion, proliferation, and differentiation related to two different surface treatments applied to the same implant design to determine whether the interaction between cells and implants is influenced by surface structure and chemical composition of the implants. Thirty-nine implants with a sandblasted (SB) surface and 39 implants with a grit-blasted and high-temperature acid-etched (GBAE) surface were used. The implant macrostructures and microstructures were analyzed by high- and low-voltage scanning electron microscopy (SEM) and by stereo-SEM. The surface chemical composition was investigated by energy dispersive analysis and x-ray photoemission spectroscopy. SaOS-2 osteoblasts and human MSCs were used for the evaluation of cell proliferation and alkaline phosphatase enzymatic activity in contact with the two surfaces. The GBAE surface showed fewer contaminants and a very high percentage of titanium (19.7%) compared to the SB surface (14.2%). The two surfaces showed similar mean roughness (Ra), but the depth (Rz) and density (RSm) of the porosity were significantly increased in the GBAE surface. The GBAE surface presented more osteoblast and MSC proliferation than the SB surface. No statistically significant differences in alkaline phosphatase activity were found between surfaces for either cellular line. The GBAE surface showed less surface contaminants and a higher percentage of titanium (19.7%) than the SB surface. The macro/micropore structured design and chemical composition of the GBAE surface allowed greater cell adhesion and proliferation and an earlier cell spreading but did not play an obvious role in in vitro cellular differentiation.

  15. Indian Ocean surface winds from NCMRWF analysis as compared to ...

    Indian Academy of Sciences (India)

    R. Narasimhan (Krishtel eMaging) 1461 1996 Oct 15 13:05:22

    Other modification of the forecast model introduced in 2001 include introduction of a non-local PBL scheme and use of daily NCEP SST analysis instead of SST climatol- ogy. These changes seem to have overcome some of the initial spin-up related deficiency of the forecast model and resulted in a better definition of the ini-.

  16. Multi-scale Analysis of Topographic Surface Roughness in the Midland Valley, Scotland

    OpenAIRE

    Grohmann, Carlos

    2017-01-01

    Surface roughness is an important geomorphological variable which has been used in the earth and planetary sciences to infer material properties, current/past processes and the time elapsed since formation. No single definition exists, however within the context of geomorphometry we use surface roughness as a expression of the variability of a topographic surface at a given scale, where the scale of analysis is determined by the size of the landforms or geomorphic features of interest. Six te...

  17. Support surfaces for pressure ulcer prevention: A network meta-analysis.

    Science.gov (United States)

    Shi, Chunhu; Dumville, Jo C; Cullum, Nicky

    2018-01-01

    Pressure ulcers are a prevalent and global issue and support surfaces are widely used for preventing ulceration. However, the diversity of available support surfaces and the lack of direct comparisons in RCTs make decision-making difficult. To determine, using network meta-analysis, the relative effects of different support surfaces in reducing pressure ulcer incidence and comfort and to rank these support surfaces in order of their effectiveness. We conducted a systematic review, using a literature search up to November 2016, to identify randomised trials comparing support surfaces for pressure ulcer prevention. Two reviewers independently performed study selection, risk of bias assessment and data extraction. We grouped the support surfaces according to their characteristics and formed evidence networks using these groups. We used network meta-analysis to estimate the relative effects and effectiveness ranking of the groups for the outcomes of pressure ulcer incidence and participant comfort. GRADE was used to assess the certainty of evidence. We included 65 studies in the review. The network for assessing pressure ulcer incidence comprised evidence of low or very low certainty for most network contrasts. There was moderate-certainty evidence that powered active air surfaces and powered hybrid air surfaces probably reduce pressure ulcer incidence compared with standard hospital surfaces (risk ratios (RR) 0.42, 95% confidence intervals (CI) 0.29 to 0.63; 0.22, 0.07 to 0.66, respectively). The network for comfort suggested that powered active air-surfaces are probably slightly less comfortable than standard hospital mattresses (RR 0.80, 95% CI 0.69 to 0.94; moderate-certainty evidence). This is the first network meta-analysis of the effects of support surfaces for pressure ulcer prevention. Powered active air-surfaces probably reduce pressure ulcer incidence, but are probably less comfortable than standard hospital surfaces. Most prevention evidence was of low or

  18. Relationships between surface energy analysis and functional characteristics of dairy powders.

    Science.gov (United States)

    Kondor, Anett; Hogan, Sean A

    2017-12-15

    Surface energetics of demineralised whey (DMW), skimmed milk (SMP), phosphocasein (PCN) and infant milk formula (IMF) powders were determined by inverse gas chromatography (IGC). All four milk powders were amphoteric in nature with the dispersive (apolar) component of surface energy dominating the specific (polar) contribution. PCN and IMF had the highest and lowest extent of surface heterogeneity, respectively. PCN also demonstrated the poorest functional properties of the powders examined. In contrast, IMF had excellent flow and rehydration properties. Thermodynamic work of cohesion was highest in PCN and may have contributed to inadequate rehydration behaviour. Glass transition temperature of IMF powder, determined by IGC, suggested a surface dominated by lactose. Surface heterogeneity provided a better indicator of functional behaviour than total surface energy. IGC is a useful complementary technique for chemical and structural analysis of milk powders and allows improved insight into the contribution of surface and bulk factors to functionality. Copyright © 2017 Elsevier Ltd. All rights reserved.

  19. Dispersion analysis of passive surface-wave noise generated during hydraulic-fracturing operations

    Science.gov (United States)

    Forghani-Arani, Farnoush; Willis, Mark; Snieder, Roel; Haines, Seth S.; Behura, Jyoti; Batzle, Mike; Davidson, Michael

    2014-01-01

    Surface-wave dispersion analysis is useful for estimating near-surface shear-wave velocity models, designing receiver arrays, and suppressing surface waves. Here, we analyze whether passive seismic noise generated during hydraulic-fracturing operations can be used to extract surface-wave dispersion characteristics. Applying seismic interferometry to noise measurements, we extract surface waves by cross-correlating several minutes of passive records; this approach is distinct from previous studies that used hours or days of passive records for cross-correlation. For comparison, we also perform dispersion analysis for an active-source array that has some receivers in common with the passive array. The active and passive data show good agreement in the dispersive character of the fundamental-mode surface-waves. For the higher mode surface waves, however, active and passive data resolve the dispersive properties at different frequency ranges. To demonstrate an application of dispersion analysis, we invert the observed surface-wave dispersion characteristics to determine the near-surface, one-dimensional shear-wave velocity.

  20. Hyperspectral Surface Analysis for Ripeness Estimation and Quick UV-C Surface Treatments for Preservation of Bananas

    Science.gov (United States)

    Zhao, W.; Yang, Zh.; Chen, Zh.; Liu, J.; Wang, W. Ch.; Zheng, W. Yu.

    2016-05-01

    This study aimed to determine the ripeness of bananas using hyperspectral surface analysis and how a rapid UV-C (ultraviolet-C light) surface treatment could reduce decay. The surface of the banana fruit and its stages of maturity were studied using a hyperspectral imaging technique in the visible and near infrared (370-1000 nm) regions. The vselected color ratios from these spectral images were used for classifying the whole banana into immature, ripe, half-ripe and overripe stages. By using a BP neural network, models based on the wavelengths were developed to predict quality attributes. The mean discrimination rate was 98.17%. The surface of the fresh bananas was treated with UV-C at dosages from 15-55 μW/cm2. The visual qualities with or without UV-C treatment were compared using the image, the chromatic aberration test, the firmness test and the area of black spot on the banana skin. The results showed that high dosages of UV-C damaged the banana skin, while low dosages were more efficient at delaying changes in the relative brightness of the skin. The maximum UV-C treatment dose for satisfactory banana preservation was between 21 and 24 μW/cm2. These results could help to improve the visual quality of bananas and to classify their ripeness more easily.

  1. Chemical analysis of outgassing contaminants on spacecraft surfaces

    Science.gov (United States)

    Mcnutt, R. C.

    1973-01-01

    Methods for analyzing and characterizing outgassing contaminants from such materials as RTV 501 potting compound and S 13 G paint are presented. Fractional distillation of a gross distillate from RTV 501 rubber was carried out and the distilled fractions examined as to their ultraviolet and infrared spectra by gas liquid chromatography. A sensitive technique for structural analysis and molecular identification was found to consist of a gas chromatography-mass spectroscopy system, which was determined to be economically unfeasible at present.

  2. Synthesis, structure and Hirshfeld surface analysis, vibrational and ...

    Indian Academy of Sciences (India)

    2.2 Crystal data and structure determination. For the structural study we chose a crystal with the dimen- sions of 0.31 × 0.28 × 0.19 mm3. The single crystal was fixed on a Bruker APEXII CCD four-circle diffractometer;. MoKα radiation (λ = 0.71073 Ε) was used in order to study its structural analysis. The crystal structure has ...

  3. Surface topography analysis for dimensional quality control of replication at the micrometre scale

    DEFF Research Database (Denmark)

    Balcon, M.; Marinello, F.; Tosello, Guido

    2011-01-01

    and replica surfaces must be quantitatively analysed and compared. In the present work, reference simulated surfaces were considered and studied in order to evaluate the effectiveness and traceability of different analysis tools for replication quality control. Topographies were analysed simulating different...

  4. Analysis of bacterial detachment from substratum surfaces by the passage of air-liquid interfaces

    NARCIS (Netherlands)

    Gomez-Suarez, C; Busscher, HJ; van der Mei, HC

    A theoretical analysis of the detachment of bacteria adhering to substratum surfaces upon the passage of an air-liquid interface is given, together with experimental results for bacterial detachment in the absence and presence of a conditioning film on different substratum surfaces. Bacteria

  5. Analysis of leaf surface sesquiterpenes in potato varieties.

    Science.gov (United States)

    Szafranek, Beata; Chrapkowska, Karolina; Pawińska, Maria; Szafranek, Janusz

    2005-04-20

    A comparative study of potato leaf sesquiterpenes was carried out. GC, GC-MS, and NMR analyses were used to identify and quantify the sesquiterpenes in the leaf surfaces of 10 potato (Solanum tuberosum) varieties. Two sesquiterpene alcohols and 17 sesquiterpene hydrocarbons were identified and quantitatively determined. The distribution of the sesquiterpenes was found to be variety-specific. The sesquiterpene contents of the different potato varieties were subjected to cluster and principal component analyses. The eight potato varieties of the main chemotype cluster were dominated by beta-caryophyllene (9-148 ng/cm2), germacrene D (2-46 ng/cm2), germacrene D-4-ol (0.4-31 ng/cm2), beta-sesquiphellandrene (1-34 ng/cm2), and an unknown sesquiterpene alcohol III (0.2-37 ng/cm2). Chemometric classification distinguished two varieties, Mila and Vistula, from a major cluster. The Vistula variety was distinguished from the others by its high contents of beta-caryophyllene, alpha-humulene, germacrene D, and germacrene D-4-ol and the Mila variety by beta-elemene, trans-alpha-bergamotene, (Z)-beta-farnesene, (E)-beta-farnesene, trans-beta-bergamotene, beta-sesquiphellandrene, and unknown sesquiterpene alcohols I, II, III.

  6. Extended Reconstructed Sea Surface Temperature (ERSST) Monthly Analysis, Version 3b

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — Version 3b (v3b) of the Extended Reconstructed Sea Surface Temperature (ERSST) dataset is a monthly SST analysis on a 2-degree global grid based on the International...

  7. Spatially-resolved protein surface microsampling from tissue sections using liquid extraction surface analysis.

    Science.gov (United States)

    Wisztorski, Maxence; Desmons, Annie; Quanico, Jusal; Fatou, Benoit; Gimeno, Jean-Pascal; Franck, Julien; Salzet, Michel; Fournier, Isabelle

    2016-06-01

    Tissue microenvironment characterization presents a challenge for a better understanding of the full complexity of a pathology. Unfortunately, making a precise "picture" of the disease needs an efficient microsampling method coupled to an accurate localization for performing region-dependent proteomics. Here, we present a method that enables rapid and reproducible extraction of proteins from a tissue section to analyze a specific region at a millimeter scale. The method used a liquid-microjunction extraction with conventional detergent solution for proteomics analysis. We successfully performed immunoblotting experiments and showed the possibility to retrieve and identify more than 1400 proteins from a 1-mm diameter spot size on tissue sections with a high degree of reproducibility both qualitatively and quantitatively. Moreover, the small size of the extracted region achieved by this sampling method allows the possibility to perform multiple extractions on different tissue section points. Ten points on a sagittal rat brain tissue section were analyzed and the measured proteins clearly distinguished the different parts of the brain, thus permitting precise functional mapping. We thus demonstrate that with this technology, it is possible to map the tissue microenvironment and gain an understanding of the molecular mechanisms at millimeter resolution. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  8. A Human Lectin Microarray for Sperm Surface Glycosylation Analysis *

    Science.gov (United States)

    Sun, Yangyang; Cheng, Li; Gu, Yihua; Xin, Aijie; Wu, Bin; Zhou, Shumin; Guo, Shujuan; Liu, Yin; Diao, Hua; Shi, Huijuan; Wang, Guangyu; Tao, Sheng-ce

    2016-01-01

    Glycosylation is one of the most abundant and functionally important protein post-translational modifications. As such, technology for efficient glycosylation analysis is in high demand. Lectin microarrays are a powerful tool for such investigations and have been successfully applied for a variety of glycobiological studies. However, most of the current lectin microarrays are primarily constructed from plant lectins, which are not well suited for studies of human glycosylation because of the extreme complexity of human glycans. Herein, we constructed a human lectin microarray with 60 human lectin and lectin-like proteins. All of the lectins and lectin-like proteins were purified from yeast, and most showed binding to human glycans. To demonstrate the applicability of the human lectin microarray, human sperm were probed on the microarray and strong bindings were observed for several lectins, including galectin-1, 7, 8, GalNAc-T6, and ERGIC-53 (LMAN1). These bindings were validated by flow cytometry and fluorescence immunostaining. Further, mass spectrometry analysis showed that galectin-1 binds several membrane-associated proteins including heat shock protein 90. Finally, functional assays showed that binding of galectin-8 could significantly enhance the acrosome reaction within human sperms. To our knowledge, this is the first construction of a human lectin microarray, and we anticipate it will find wide use for a range of human or mammalian studies, alone or in combination with plant lectin microarrays. PMID:27364157

  9. Surface chemical composition analysis of heat-treated bamboo

    International Nuclear Information System (INIS)

    Meng, Fan-dan; Yu, Yang-lun; Zhang, Ya-mei; Yu, Wen-ji; Gao, Jian-min

    2016-01-01

    Highlights: • Investigate the detailed chemical components contents change of bamboo due to heating. • Chemical analysis of bamboo main components during heating. • Identify the connection between the oxygen to carbon atomic ratio changes and chemical degradation. - Abstract: In this study, the effect of heat treatment on the chemical composition of bamboo slivers was studied. The chemical properties of the samples were examined by chemical analysis. Results showed a decrease in the contents of holocellulose and α-cellulose, as well as an increase in the contents of lignin and extractives. Changes in the chemical structure of bamboo components were analyzed by Fourier transform infrared spectroscopy (FTIR) and X-ray photoelectron spectroscopy (XPS). FTIR spectroscopy results indicated that hemicellulose contents decrease, whereas lignin contents increase after heat treatment. Ester formation linked to lignin decreased the hygroscopicity of the bamboo samples and consequently improved their dimensional stability and durability. XPS spectroscopy results showed that hemicelluloses and celluloses are relatively more sensitive to the heating process than lignin. As a consequence, hemicellulose and cellulose contents decreased, whereas lignin contents increased during heat treatment. The results obtained in this study provide useful information for the future utilization of heat-treated bamboo.

  10. Surface analysis of dental amalgams by X-ray photoelectron spectroscopy and X-ray diffraction.

    Science.gov (United States)

    Uo, Motohiro; Berglund, Anders; Cardenas, Juan; Pohl, Lars; Watari, Fumio; Bergman, Maud; Sjöberg, Staffan

    2003-11-01

    It is important to characterize the surface of dental amalgam in order to understand the process of mercury release from amalgam restorations in the oral cavity. The mercury evaporation occurs not only from the newly made restoration but also from the set material. The surfaces of four different types of amalgams, which had been well set, were analyzed with X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD) and the relationship between surface compositions and mercury release was studied. Fresh amalgam surfaces as well as aged surfaces, which were stored for 30 days in air, were investigated using XPS and the chemical states of amalgam components and oxygen were studied. The aged surfaces were also characterized with XRD and grazing angle XRD. With increased oxidation, the surface contents of tin and oxygen were increased in all amalgams. In contrast, the surface contents of copper and mercury were decreased. An increase of zinc or indium content were observed in zinc or indium containing amalgams, respectively. A surface layer enriched with indium and oxygen was clearly detected by XPS but not with grazing angle XRD. The thickness of the enriched surface layer is estimated to be in the order of few nanometer, which is approximately equal to the analysis depth of XPS. In addition, the presence of metallic elements, like tin and zinc, that readily form a stable oxide layer at the surface suppress the release of mercury.

  11. Surface analysis of PEGylated nano-shields on nanoparticles installed by hydrophobic anchors

    DEFF Research Database (Denmark)

    Ebbesen, M F; Whitehead, Bradley Joseph; Gonzalez, Borja Ballarin

    2013-01-01

    Purpose: This work describes a method for functionalisation of nanoparticle surfaces with hydrophilic "nano-shields" and the application of advanced surface characterisation to determine PEG amount and accumulation at the outmost 10 nm surface that is the predominant factor in determining protein....... Surface and bulk analysis was performed including X-ray photoelectron spectroscopy (XPS), nuclear magnetic resonance spectroscopy (NMR) and zeta potential. Cellular uptake was investigated in RAW 264.7 macrophages by flow cytometry. Results: Sub-micron nanoparticles were formed and the combination of (NMR...

  12. A new response surface approach for structural reliability analysis

    Science.gov (United States)

    Thacker, B. H.; Wu, X.-T.

    1992-01-01

    This paper describes a new approach for computing structural reliability by post-processing previously computed probabilistic results for stress and strength. The objective is to provide an accurate method whereby independent probabilistic analyses for stress and strength functions can be performed independently and combined at a later time to compute probability of failure. The method provides a capability for testing different strength measures without the need for re-computing the probabilistic stress response. The proposed approach takes full account of the basic random variables effecting both stress and strength, and the failure region in the variable space identified during separate stress/strength probabilistic analyses. A simple closed-form example and a more complex analysis of a turbine blade subject to creep rupture is used to illustrate the method.

  13. Albumin adsorption onto surfaces of urine collection and analysis containers.

    Science.gov (United States)

    Robinson, Mary K; Caudill, Samuel P; Koch, David D; Ritchie, James; Hortin, Glen; Eckfeldt, John H; Sandberg, Sverre; Williams, Desmond; Myers, Gary; Miller, W Greg

    2014-04-20

    Adsorption of albumin onto urine collection and analysis containers may cause falsely low concentrations. We added (125)I-labeled human serum albumin to urine and to phosphate buffered solutions, incubated them with 22 plastic container materials and measured adsorption by liquid scintillation counting. Adsorption of urine albumin (UA) at 5-6 mg/l was containers, and to instrument sample cups and showed <1% change in concentration at 5 mg/l and <0.5% change at 20 mg/l or higher concentrations. Adsorption of albumin from phosphate buffered solutions (2-28%) was larger than that from urine. Albumin adsorption differed among urine samples and plastic materials, but the total influence of adsorption was <1% for all materials and urine samples tested. Adsorption of albumin from phosphate buffered solutions was larger than that from urine and could be a limitation for preparations used as calibrators. Copyright © 2014 Elsevier B.V. All rights reserved.

  14. The quantitative analysis of silicon carbide surface smoothing by Ar and Xe cluster ions

    Science.gov (United States)

    Ieshkin, A. E.; Kireev, D. S.; Ermakov, Yu. A.; Trifonov, A. S.; Presnov, D. E.; Garshev, A. V.; Anufriev, Yu. V.; Prokhorova, I. G.; Krupenin, V. A.; Chernysh, V. S.

    2018-04-01

    The gas cluster ion beam technique was used for the silicon carbide crystal surface smoothing. The effect of processing by two inert cluster ions, argon and xenon, was quantitatively compared. While argon is a standard element for GCIB, results for xenon clusters were not reported yet. Scanning probe microscopy and high resolution transmission electron microscopy techniques were used for the analysis of the surface roughness and surface crystal layer quality. The gas cluster ion beam processing results in surface relief smoothing down to average roughness about 1 nm for both elements. It was shown that xenon as the working gas is more effective: sputtering rate for xenon clusters is 2.5 times higher than for argon at the same beam energy. High resolution transmission electron microscopy analysis of the surface defect layer gives values of 7 ± 2 nm and 8 ± 2 nm for treatment with argon and xenon clusters.

  15. Surface analysis of 316 stainless steel treated with cold atmospheric plasma

    Science.gov (United States)

    Williams, David F.; Kellar, Ewen J. C.; Jesson, David A.; Watts, John F.

    2017-05-01

    The surface of 316 stainless steel has been modified using cold atmospheric plasma (CAP) to increase the surface free energy (by cleaning the and chemically activating the surface)IN preparation for subsequent processes such as painting, coating or adhesive bonding. The analyses carried out, on CAP treated 316 stainless steel surfaces, includes X-ray photoelectron spectroscopy (XPS), imaging XPS (iXPS), and surface free energy (SFE) analysis using contact angle measurements. The CAP treatment is shown to increase the SFE of as-received 316 stainless steel from ∼39 mJ m-1 to >72 mJ m-1 after a short exposure to the plasma torch. This was found to correlate to a reduction in adventitious carbon, as determined by XPS analysis of the surface. The reduction from ∼90 at% to ∼30% and ∼39 at%, after being plasma treated for 5 min and 15 s respectively, shows that the process is relatively quick at changing the surface. It is suggested that the mechanism that causes the increase in surface free energy is chain scission of the hydrocarbon contamination triggered by free electrons in the plasma plume followed by chemical functionalisation of the metal oxide surface and some of the remaining carbon contamination layer.

  16. AFM stochastic analysis of surface twisted nanograin chains of iron oxide: a kinetic study

    International Nuclear Information System (INIS)

    Akhavan, O; Azimirad, R

    2009-01-01

    We have studied the stochastic parameters of surface iron oxide nanograin chains, 97 nm in diameter and 2.4 μm in length, prepared at different annealing temperatures, using atomic force microscopy (AFM) spectral analysis. In this regard, the roughness of the thin films including self-assembled twisted nanograin chains has been analysed and characterized using the height-height correlation function, the roughness exponent as well as the power spectrum density of the AFM profiles and their gradient, for the different annealing temperatures. The tip convolution effect on the stochastic parameters under study has also been investigated. The kinetics of the formation of nanograins on the film surface has been obtained using the AFM spectral analysis of the profiles and their gradient. The activation energy needed for the formation of surface nanograin chains was found to be 0.55 eV. It has been shown that the tip-surface interaction affects mainly the diffusion parameters obtained by using the surface roughness analysis of the profiles, while use of the surface roughness analysis of the gradient of the profiles results in a nearly independent tip convolution effect on the diffusion parameters. Hence, this work also provides a method for calculating the required activation energy for the formation of self-assembled nanostructures affecting the roughness of a surface.

  17. Imaging Analysis of Carbohydrate-Modified Surfaces Using ToF-SIMS and SPRi

    Directory of Open Access Journals (Sweden)

    Manish Dubey

    2010-07-01

    Full Text Available Covalent modification of surfaces with carbohydrates (glycans is a prerequisite for a variety of glycomics-based biomedical applications, including functional biomaterials, glycoarrays, and glycan-based biosensors. The chemistry of glycan immobilization plays an essential role in the bioavailability and function of the surface bound carbohydrate moiety. However, the scarcity of analytical methods to characterize carbohydrate-modified surfaces complicates efforts to optimize glycan surface chemistries for specific applications. Time-of-Flight Secondary Ion Mass Spectrometry (ToF-SIMS is a surface sensitive technique suited for probing molecular composition at the biomaterial interface. Expanding ToF-SIMS analysis to interrogate carbohydrate-modified materials would increase our understanding of glycan surface chemistries and advance novel tools in the nascent field of glycomics. In this study, a printed glycan microarray surface was fabricated and subsequently characterized by ToF-SIMS imaging analysis. A multivariate technique based on principal component analysis (PCA was used to analyze the ToF-SIMS dataset and reconstruct ToF-SIMS images of functionalized surfaces. These images reveal chemical species related to the immobilized glycan, underlying glycan-reactive chemistries, gold substrates, and outside contaminants. Printed glycoarray elements (spots were also interrogated to resolve the spatial distribution and spot homogeneity of immobilized glycan. The bioavailability of the surface-bound glycan was validated using a specific carbohydrate-binding protein (lectin as characterized by Surface Plasmon Resonance Imaging (SPRi. Our results demonstrate that ToF-SIMS is capable of characterizing chemical features of carbohydrate-modified surfaces and, when complemented with SPRi, can play an enabling role in optimizing glycan microarray fabrication and performance.

  18. Imaging Analysis of Carbohydrate-Modified Surfaces Using ToF-SIMS and SPRi.

    Science.gov (United States)

    Bolles, Kathryn M; Cheng, Fang; Burk-Rafel, Jesse; Dubey, Manish; Ratner, Daniel M

    2010-07-07

    Covalent modification of surfaces with carbohydrates (glycans) is a prerequisite for a variety of glycomics-based biomedical applications, including functional biomaterials, glycoarrays, and glycan-based biosensors. The chemistry of glycan immobilization plays an essential role in the bioavailability and function of the surface bound carbohydrate moiety. However, the scarcity of analytical methods to characterize carbohydrate-modified surfaces complicates efforts to optimize glycan surface chemistries for specific applications. Time-of-Flight Secondary Ion Mass Spectrometry (ToF-SIMS) is a surface sensitive technique suited for probing molecular composition at the biomaterial interface. Expanding ToF-SIMS analysis to interrogate carbohydrate-modified materials would increase our understanding of glycan surface chemistries and advance novel tools in the nascent field of glycomics. In this study, a printed glycan microarray surface was fabricated and subsequently characterized by ToF-SIMS imaging analysis. A multivariate technique based on principal component analysis (PCA) was used to analyze the ToF-SIMS dataset and reconstruct ToF-SIMS images of functionalized surfaces. These images reveal chemical species related to the immobilized glycan, underlying glycan-reactive chemistries, gold substrates, and outside contaminants. Printed glycoarray elements (spots) were also interrogated to resolve the spatial distribution and spot homogeneity of immobilized glycan. The bioavailability of the surface-bound glycan was validated using a specific carbohydrate-binding protein (lectin) as characterized by Surface Plasmon Resonance Imaging (SPRi). Our results demonstrate that ToF-SIMS is capable of characterizing chemical features of carbohydrate-modified surfaces and, when complemented with SPRi, can play an enabling role in optimizing glycan microarray fabrication and performance.

  19. Surface Fire Hazards Analysis Technical Report-Constructor Facilities

    International Nuclear Information System (INIS)

    Flye, R.E.

    2000-01-01

    The purpose of this Fire Hazards Analysis Technical Report (hereinafter referred to as Technical Report) is to assess the risk from fire within individual fire areas to ascertain whether the U.S. Department of Energy (DOE) fire safety objectives are met. The objectives identified in DOE Order 420.1, Change 2, Facility Safety, Section 4.2, establish requirements for a comprehensive fire and related hazards protection program for facilities sufficient to minimize the potential for: The occurrence of a fire or related event; A fire that causes an unacceptable on-site or off-site release of hazardous or radiological material that will threaten the health and safety of employees, the public, or the environment; Vital DOE programs suffering unacceptable interruptions as a result of fire and related hazards; Property losses from a fire and related events exceeding defined limits established by DOE; and Critical process controls and safety class systems being damaged as a result of a fire and related events

  20. Molecular Analysis of Bacterial Microbiota on Brazilian Currency Note Surfaces

    Directory of Open Access Journals (Sweden)

    Tairacan Augusto Pereira da Fonseca

    2015-10-01

    Full Text Available Currency notes have been implicated as a vehicle for transmitting community-acquired bacterial infections. However, the overall diversity of the bacterial population residing on banknotes is still unknown in Brazil. In this study, we aimed to investigate the overall bacterial population from 150 different Brazilian Rial (R$ notes in circulation using a culture-independent Illumina massively parallel sequencing approach of the 16S rRNA genes. Samples were randomly collected from three different street markets or “feiras” in the metropolitan region of São Paulo. Taxonomical composition revealed the abundance of Proteobacteria phyla, followed by Firmicutes and Streptophyta, with a total of 1193 bacterial families and 3310 bacterial genera. Most of these bacterial genera are of human, animal, and environmental origins. Also, our analysis revealed the presence of some potential pathogenic bacterial genera including Salmonella, Staphylococcus, and Klebsiella. The results demonstrate that there is a tremendous diversity of bacterial contamination on currency notes, including organisms known to be opportunistic pathogens. One of the factors that may contribute to the richness of bacterial diversity in currency notes is personal hygiene. Thus, our results underscore the need to increase public awareness of the importance of personal hygiene of money handlers who also handle food.

  1. Molecular Analysis of Bacterial Microbiota on Brazilian Currency Note Surfaces.

    Science.gov (United States)

    Pereira da Fonseca, Tairacan Augusto; Pessôa, Rodrigo; Sanabani, Sabri Saeed

    2015-10-22

    Currency notes have been implicated as a vehicle for transmitting community-acquired bacterial infections. However, the overall diversity of the bacterial population residing on banknotes is still unknown in Brazil. In this study, we aimed to investigate the overall bacterial population from 150 different Brazilian Rial (R$) notes in circulation using a culture-independent Illumina massively parallel sequencing approach of the 16S rRNA genes. Samples were randomly collected from three different street markets or "feiras" in the metropolitan region of São Paulo. Taxonomical composition revealed the abundance of Proteobacteria phyla, followed by Firmicutes and Streptophyta, with a total of 1193 bacterial families and 3310 bacterial genera. Most of these bacterial genera are of human, animal, and environmental origins. Also, our analysis revealed the presence of some potential pathogenic bacterial genera including Salmonella, Staphylococcus, and Klebsiella. The results demonstrate that there is a tremendous diversity of bacterial contamination on currency notes, including organisms known to be opportunistic pathogens. One of the factors that may contribute to the richness of bacterial diversity in currency notes is personal hygiene. Thus, our results underscore the need to increase public awareness of the importance of personal hygiene of money handlers who also handle food.

  2. ANALYSIS OF SURFACE DEFECTS OF ALUMINUM AND ITS ALLOYS WITH A SCANNING KELVIN PROBE

    Directory of Open Access Journals (Sweden)

    A. K. Tyavlovsky

    2017-01-01

    Full Text Available Currently, the use of probe electrometry in non-destructive testing is constrained by the complexity of measurement results interpretation. An output signal of electrometric probe depends on a number of physical and chemical parameters of surface including chemical composition variations, stresses, dislocations, crystallographic orientation of a surface, etc. The study aims to the use of probe electrometry methods for nondestructive testing and analysis of precision metal surfaces’ defects after different treatment or processing.Control of surface defects of aluminum and its alloys was performed with a scanning Kelvin probe technique. The results of scanning were plotted in a form of contact potential difference (CPD distribution map. Additionally, a histogram of CPD values distribution and statistical characteristics including the expectation of CPD mean value and histogram half-width were calculated either for the whole distribution or for each individual mode in a case of multimodal distribution.The spatial CPD distribution of A99 aluminum and AMG-2 alloy surfaces after electrochemical polishing and diamond finishing was studied. An additional study was held for AMG-2 surface after the formation of 30 microns thick specific nanostructured alumina oxide surface layer. Higher quality surfaces have characterized as more homogeneous distribution of the physical properties (at half-width distribution histogram. Surfaces with higher mechanical strength and overall better mechanical properties found to have lower CPD values that correspond to higher electron work function and surface energy. The presence of the second mode in the CPD distribution histogram indicates the significant proportion of defect areas on the sample surface.Analysis of visualized CPD distribution maps using defined criteria allows detecting and characterizing such defects as residual stress areas, areas with reduced microhardness, surface contamination spots, corrosion

  3. Analysis of coatings appearance and durability testing induced surface defects using image capture/processing/analysis

    Directory of Open Access Journals (Sweden)

    Lee, F.

    2003-12-01

    Full Text Available There are no established and accepted techniques available for accurate characterization appearance changes brought about by scratch and mar damage. Scratch and mar resistance is related to the ability of a coating in resisting deformation. The appearance change is brought about by surface roughening which in turn leads to a reduction in gloss and reflectivity. This paper focuses on the measurement of the appearance of coating by image analysis and gloss measurement.

    No hay técnicas establecidas o aceptadas para una caracterización precisa de los cambios de apariencia dados por los rayones profundos y daños superficiales en los recubrimientos. La resistencia a estos eventos está relacionada con la habilidad del recubrimiento a resistir la deformación. El cambio de apariencia se presenta en la superficie como una aspereza que va llevando a la reducción del brillo y de la reflectancia. Este trabajo se centra en las mediciones de apariencia de un recubrimiento por análisis de imágenes y medición de brillo.

  4. Fabrication and quantitative roughness analysis of hierarchical multiscale polymer surface structures

    Science.gov (United States)

    Huovinen, Eero; Takkunen, Laura; Suvanto, Mika; Pakkanen, Tapani A.

    2014-05-01

    Nature's functional surfaces are typically hierarchical multiscale structures. There are several techniques for producing such artificial structures on polymers but their mass production is not straightforward. We present here a simple and versatile method for manufacturing hierarchical multiscale polymer surface patterns. The microroughening technique permits the single-step production of multilevel three-dimensional surface architectures in a mechanically durable nickel mold. The molding technique is suitable for area-controlled fabrication of structures with various geometrical shapes on smooth and curved surfaces. The mold structures were transferred to polypropylene surfaces by means of injection molding. The fabricated surface structures were characterized by using a filtered power spectral density method which facilitated a quantitative study of the roughness distributions at different length scales of structure periodicities. Analysis showed that the microroughening technique is an appropriate tool for controlled production of surface roughness at a micro-nanometer scale. Roughness distribution values can be used for predicting surface structure-related properties such as wetting, and the distributions can also be simulated without an experimental preparation process. The work presents a suitable approach for mass production of hierarchical polymer surfaces at different length scales and provides a new route for designing surface structures with tunable wetting properties.

  5. The interpretation of dream meaning: Resolving ambiguity using Latent Semantic Analysis in a small corpus of text.

    Science.gov (United States)

    Altszyler, Edgar; Ribeiro, Sidarta; Sigman, Mariano; Fernández Slezak, Diego

    2017-11-01

    Computer-based dreams content analysis relies on word frequencies within predefined categories in order to identify different elements in text. As a complementary approach, we explored the capabilities and limitations of word-embedding techniques to identify word usage patterns among dream reports. These tools allow us to quantify words associations in text and to identify the meaning of target words. Word-embeddings have been extensively studied in large datasets, but only a few studies analyze semantic representations in small corpora. To fill this gap, we compared Skip-gram and Latent Semantic Analysis (LSA) capabilities to extract semantic associations from dream reports. LSA showed better performance than Skip-gram in small size corpora in two tests. Furthermore, LSA captured relevant word associations in dream collection, even in cases with low-frequency words or small numbers of dreams. Word associations in dreams reports can thus be quantified by LSA, which opens new avenues for dream interpretation and decoding. Copyright © 2017 Elsevier Inc. All rights reserved.

  6. Comparative study of binding constants from Love wave surface acoustic wave and surface plasmon resonance biosensors using kinetic analysis.

    Science.gov (United States)

    Lee, Sangdae; Kim, Yong-Il; Kim, Ki-Bok

    2013-11-01

    Biosensors are used in a variety of fields for early diagnosis of diseases, measurement of toxic contaminants, quick detection of pathogens, and separation of specific proteins or DNA. In this study, we fabricated and evaluated the capability of a high sensitivity Love wave surface acoustic wave (SAW) biosensor. The experimental setup was composed of the fabricated 155-MHz Love wave SAW biosensor, a signal measurement system, a liquid flow system, and a temperature-control system. Subsequently, we measured the lower limit of detection (LOD) of the 155-MHz Love wave SAW biosensor, and calculated the association and dissociation constants between protein G and anti-mouse IgG using kinetic analysis. We compared these results with those obtained using a commercial surface plasmon resonance (SPR) biosensor. We found that the LOD of the SAW biosensor for anti-mouse IgG and mouse IgG was 0.5 and 1 microg/ml, respectively, and the resultant equilibrium association and dissociation constants were similar to the corresponding values obtaining using the commercial SPR biosensor. Thus, we conclude that the fabricated 155-MHz Love wave SAW biosensor exhibited the high sensitivity of the commercial SPR biosensor and was able to analyze the binding properties of the ligand and receptor by kinetic analysis similarly to the commercial SPR biosensor.

  7. Software design for analysis of multichannel intracardial and body surface electrocardiograms

    NARCIS (Netherlands)

    Potse, Mark; Linnenbank, André C.; Grimbergen, Cornelis A.

    2002-01-01

    Analysis of multichannel ECG recordings (body surface maps (BSMs) and intracardial maps) requires special software. We created a software package and a user interface on top of a commercial data analysis package (MATLAB) by a combination of high-level and low-level programming. Our software was

  8. Surface Acoustic Wave Monitor for Deposition and Analysis of Ultra-Thin Films

    Science.gov (United States)

    Hines, Jacqueline H. (Inventor)

    2015-01-01

    A surface acoustic wave (SAW) based thin film deposition monitor device and system for monitoring the deposition of ultra-thin films and nanomaterials and the analysis thereof is characterized by acoustic wave device embodiments that include differential delay line device designs, and which can optionally have integral reference devices fabricated on the same substrate as the sensing device, or on a separate device in thermal contact with the film monitoring/analysis device, in order to provide inherently temperature compensated measurements. These deposition monitor and analysis devices can include inherent temperature compensation, higher sensitivity to surface interactions than quartz crystal microbalance (QCM) devices, and the ability to operate at extreme temperatures.

  9. Numerical Inversion of SRNF Maps for Elastic Shape Analysis of Genus-Zero Surfaces.

    Science.gov (United States)

    Laga, Hamid; Xie, Qian; Jermyn, Ian H; Srivastava, Anuj

    2017-12-01

    Recent developments in elastic shape analysis (ESA) are motivated by the fact that it provides a comprehensive framework for simultaneous registration, deformation, and comparison of shapes. These methods achieve computational efficiency using certain square-root representations that transform invariant elastic metrics into euclidean metrics, allowing for the application of standard algorithms and statistical tools. For analyzing shapes of embeddings of in , Jermyn et al. [1] introduced square-root normal fields (SRNFs), which transform an elastic metric, with desirable invariant properties, into the metric. These SRNFs are essentially surface normals scaled by square-roots of infinitesimal area elements. A critical need in shape analysis is a method for inverting solutions (deformations, averages, modes of variations, etc.) computed in SRNF space, back to the original surface space for visualizations and inferences. Due to the lack of theory for understanding SRNF maps and their inverses, we take a numerical approach, and derive an efficient multiresolution algorithm, based on solving an optimization problem in the surface space, that estimates surfaces corresponding to given SRNFs. This solution is found to be effective even for complex shapes that undergo significant deformations including bending and stretching, e.g., human bodies and animals. We use this inversion for computing elastic shape deformations, transferring deformations, summarizing shapes, and for finding modes of variability in a given collection, while simultaneously registering the surfaces. We demonstrate the proposed algorithms using a statistical analysis of human body shapes, classification of generic surfaces, and analysis of brain structures.

  10. Multichannel biomedical time series clustering via hierarchical probabilistic latent semantic analysis.

    Science.gov (United States)

    Wang, Jin; Sun, Xiangping; Nahavandi, Saeid; Kouzani, Abbas; Wu, Yuchuan; She, Mary

    2014-11-01

    Biomedical time series clustering that automatically groups a collection of time series according to their internal similarity is of importance for medical record management and inspection such as bio-signals archiving and retrieval. In this paper, a novel framework that automatically groups a set of unlabelled multichannel biomedical time series according to their internal structural similarity is proposed. Specifically, we treat a multichannel biomedical time series as a document and extract local segments from the time series as words. We extend a topic model, i.e., the Hierarchical probabilistic Latent Semantic Analysis (H-pLSA), which was originally developed for visual motion analysis to cluster a set of unlabelled multichannel time series. The H-pLSA models each channel of the multichannel time series using a local pLSA in the first layer. The topics learned in the local pLSA are then fed to a global pLSA in the second layer to discover the categories of multichannel time series. Experiments on a dataset extracted from multichannel Electrocardiography (ECG) signals demonstrate that the proposed method performs better than previous state-of-the-art approaches and is relatively robust to the variations of parameters including length of local segments and dictionary size. Although the experimental evaluation used the multichannel ECG signals in a biometric scenario, the proposed algorithm is a universal framework for multichannel biomedical time series clustering according to their structural similarity, which has many applications in biomedical time series management. Copyright © 2014 Elsevier Ireland Ltd. All rights reserved.

  11. Treatment by gliding arc of epoxy resin: preliminary analysis of surface modifications

    Science.gov (United States)

    Faubert, F.; Wartel, M.; Pellerin, N.; Pellerin, S.; Cochet, V.; Regnier, E.; Hnatiuc, B.

    2016-12-01

    Treatments with atmospheric pressure non-thermal plasma are easy to implement and inexpensive. Among them gliding arc (GlidArc) remains rarely used in surface treatment of polymers. However, it offers economic and flexible way to treat quickly large areas. In addition the choice of carrier gas makes it possible to bring the active species and other radicals allowing different types of grafting and functionalization of the treated surfaces, for example in order to apply for anti-biofouling prevention. This preliminary work includes analysis of the surface of epoxy resins by infrared spectroscopy: the different affected chemical bonds were studied depending on the duration of treatment. The degree of oxidation (the C/O ratio) is obtained by X-ray microanalysis and contact angle analysis have been performed to determinate the wettability properties of the treated surface. A spectroscopic study of the plasma allows to determine the possible active species in the different zones of the discharge.

  12. Trend-surface analysis of morphometric parameters: A case study in southeastern Brazil

    Science.gov (United States)

    Grohmann, Carlos Henrique

    2005-10-01

    Trend-surface analysis was carried out on data from morphometric parameters isobase and hydraulic gradient. The study area, located in the eastern border of Quadrilátero Ferrífero, southeastern Brazil, presents four main geomorphological units, one characterized by fluvial dissection, two of mountainous relief, with a scarp of hundreds of meters of fall between them, and a flat plateau in the central portion of the fluvially dissected terrains. Morphometric maps were evaluated in GRASS-GIS and statistics were made on R statistical language, using the spatial package. Analysis of variance (ANOVA) was made to test the significance of each surface and the significance of increasing polynomial degree. The best results were achieved with sixth-order surface for isobase and second-order surface for hydraulic gradient. Shape and orientation of residual maps contours for selected trends were compared with structures inferred from several morphometric maps, and a good correlation is present.

  13. Grasping Claws of Bionic Climbing Robot for Rough Wall Surface: Modeling and Analysis

    Directory of Open Access Journals (Sweden)

    Quansheng Jiang

    2017-12-01

    Full Text Available Aiming at the inspection of rough stone and concrete wall surfaces, a grasping module of cross-arranged claw is designed. It can attach onto rough wall surfaces by hooking or grasping walls. First, based on the interaction mechanism of hooks and rough wall surfaces, the hook structures in claw tips are developed. Then, the size of the hook tip is calculated and the failure mode is analyzed. The effectiveness and reliability of the mechanism are verified through simulation and finite element analysis. Afterwards, the prototype of the grasping module of claw is established to carry out grasping experiment on vibrating walls. Finally, the experimental results demonstrate that the proposed cross-arranged claw is able to stably grasp static wall surfaces and perform well in grasping vibrating walls, with certain anti-rollover capability. This research lays a foundation for future researches on wall climbing robots with vibrating rough wall surfaces.

  14. Investigation of ozone zero phenomenon using new electrode and surface analysis technique

    Science.gov (United States)

    Taguchi, M.; Ochiai, Y.; Kawagoe, R.; Kato, Y.; Teranishi, K.; Suzuki, S.; Itoh, H.

    2011-07-01

    Results of our experimental investigation on the ozone zero phenomenon suggested us the importance of the electrode surface condition. This means that the main cause of the phenomenon, that is, temporal decrease of ozone concentration at the outlet of DBD type ozone generator and the recovery characteristics from the phenomenon are considered as the surface reaction process, which are influenced strongly by the surface condition. The surface condition is never constant during the ozone generation and varies gradually or remarkably with time depending on the experimental conditions. Therefore we have been continued to make clear the cause of the phenomenon, for example, the reproducibility of the phenomenon, using new electrodes and together with the surface analysis technique etc. In this paper, we describe on the above results and discussion.

  15. Analysis of WEDM Process Parameters on Surface Roughness and Kerf using Taguchi Method

    Directory of Open Access Journals (Sweden)

    Asfana Banu

    2017-12-01

    Full Text Available In obtaining the best quality of engineering parts, the quality of machined surface plays an essential role. The fatigue strength, wear resistance, and corrosion of workpiece are some of the aspects of the qualities that can be improved. This paper investigates the effect of wire electrical discharge machining (WEDM process parameters on surface roughness and kerf on stainless steel using distilled water as dielectric fluid and brass wire as tool electrode. The selected process parameters are voltage open, wire speed, wire tension, voltage gap, and off time. Empirical models using Taguchi method were developed for the estimation of surface roughness and kerf. The analysis revealed that off time has major influence on surface roughness and kerf. The optimum machining parameters for minimum surface roughness and kerf were found to be 10 V open voltage, 2.84 µs off time, 12 m/min wire speed, 6.3 N wire tension, and 54.91 V voltage gap.

  16. The multilevel analysis of surface acting and mental health: A moderation of positive group affective tone

    Science.gov (United States)

    Lee, Meng-Shiu; Huang, Jui-Chan; Wu, Tzu-Jung

    2017-06-01

    The purpose of this study is to investigate the relationship among surface acting, mental health, and positive group affective tone. According to the prior theory, this study attempts to establish a comprehensive research framework among these variables, and furthermore tests the moderating effect of positive group affective tone. Data were collected from 435 employees in 52 service industrial companies by questionnaire, and this study conducted multilevel analysis. The results showed that surface acting will negatively affect the mental health. In addition, the positive group affective tone have significant moderating effect on the relationship among surface acting and mental health. Finally, this study discusses managerial implications and highlights future research suggestions.

  17. Multi-Parameter Analysis of Surface Finish in Electro-Discharge Machining of Tool Steels

    Directory of Open Access Journals (Sweden)

    Cornelia Victoria Anghel

    2006-10-01

    Full Text Available The paper presents a multi- parameter analysis of surface finish imparted to tool-steel plates by electro-discharge machining (EDM is presented. The interrelationship between surface texture parameters and process parameters is emphasized. An increased number of parameters is studied including amplitude, spacing, hybrid and fractal parameters,, as well. The correlation of these parameters with the machining conditions is investigated. Observed characteristics become more pronounced, when intensifying machining conditions. Close correlation exists between certain surface finish parameters and EDM input variables and single and multiple statistical regression models are developed.

  18. Evaluation of abrasive waterjet produced titan surfaces topography by spectral analysis techniques

    Directory of Open Access Journals (Sweden)

    D. Kozak

    2012-01-01

    Full Text Available Experimental study of a titan grade 2 surface topography prepared by abrasive waterjet cutting is performed using methods of the spectral analysis. Topographic data are acquired by means of the optical profilometr MicroProf®FRT. Estimation of the areal power spectral density of the studied surface is carried out using the periodogram method combined with the Welch´s method. Attention is paid to a structure of the areal power spectral density, which is characterized by means of the angular power spectral density. This structure of the areal spectral density is linked to the fine texture of the surface studied.

  19. Estimation of small surface displacements in the Upper Rhine Graben area from a combined analysis of PS-InSAR, levelling and GNSS data

    Science.gov (United States)

    Fuhrmann, T.; Caro Cuenca, M.; Knöpfler, A.; van Leijen, F. J.; Mayer, M.; Westerhaus, M.; Hanssen, R. F.; Heck, B.

    2015-10-01

    The intra-plate deformation of the Upper Rhine Graben (URG) located in Central Europe is investigated using geodetic measurement techniques. We present a new approach to calculate a combined velocity field from InSAR, levelling and GNSS measurements. As the expected tectonic movements in the URG area are small (less than 1 mm a-1), the best possible solutions for linear velocity rates from single-technique analyses are estimated in a first step. Second, we combine the velocity rates obtained from InSAR (line of sight velocity rates in ascending and descending image geometries), levelling (vertical velocity rates) and GNSS (horizontal velocity rates) using least-squares adjustment (LSA). Focusing on the Northern URG area, we analyse SAR data on four different image stacks (ERS ascending, ERS descending, Envisat ascending, Envisat descending) using the Persistent Scatterer (PS) approach. The linear velocity rates in ascending and descending image geometries, respectively, are estimated in an LSA from joint time-series analysis of ERS and Envisat data. Vertical velocity rates from levelling are obtained from a consistent adjustment of more than 40 000 measured height differences using a kinematic displacement model. Horizontal velocity rates in east and north direction are calculated from a time-series analysis of daily coordinate estimates at 76 permanently operating GNSS sites in the URG region. As the locations, at which the measurement data of PS-InSAR, levelling and GNSS reside, do not coincide, spatial interpolation is needed during several steps of the rigorous processing. We use Ordinary Kriging to interpolate from a given set of data points to the locations of interest with a special focus on the modeling and propagation of errors. The final 3-D velocity field is calculated at a 200 m grid, which carries values only close to the location of PS points, resulting in a mean horizontal and vertical precision of 0.30 and 0.13 mm a-1, respectively. The vertical

  20. Support surfaces for pressure ulcer prevention: A network meta-analysis.

    Directory of Open Access Journals (Sweden)

    Chunhu Shi

    Full Text Available Pressure ulcers are a prevalent and global issue and support surfaces are widely used for preventing ulceration. However, the diversity of available support surfaces and the lack of direct comparisons in RCTs make decision-making difficult.To determine, using network meta-analysis, the relative effects of different support surfaces in reducing pressure ulcer incidence and comfort and to rank these support surfaces in order of their effectiveness.We conducted a systematic review, using a literature search up to November 2016, to identify randomised trials comparing support surfaces for pressure ulcer prevention. Two reviewers independently performed study selection, risk of bias assessment and data extraction. We grouped the support surfaces according to their characteristics and formed evidence networks using these groups. We used network meta-analysis to estimate the relative effects and effectiveness ranking of the groups for the outcomes of pressure ulcer incidence and participant comfort. GRADE was used to assess the certainty of evidence.We included 65 studies in the review. The network for assessing pressure ulcer incidence comprised evidence of low or very low certainty for most network contrasts. There was moderate-certainty evidence that powered active air surfaces and powered hybrid air surfaces probably reduce pressure ulcer incidence compared with standard hospital surfaces (risk ratios (RR 0.42, 95% confidence intervals (CI 0.29 to 0.63; 0.22, 0.07 to 0.66, respectively. The network for comfort suggested that powered active air-surfaces are probably slightly less comfortable than standard hospital mattresses (RR 0.80, 95% CI 0.69 to 0.94; moderate-certainty evidence.This is the first network meta-analysis of the effects of support surfaces for pressure ulcer prevention. Powered active air-surfaces probably reduce pressure ulcer incidence, but are probably less comfortable than standard hospital surfaces. Most prevention evidence was

  1. Analysis of Shift and Deformation of Planar Surfaces Using the Least Squares Plane

    Directory of Open Access Journals (Sweden)

    Hrvoje Matijević

    2006-12-01

    Full Text Available Modern methods of measurement developed on the basis of advanced reflectorless distance measurement have paved the way for easier detection and analysis of shift and deformation. A large quantity of collected data points will often require a mathematical model of the surface that fits best into these. Although this can be a complex task, in the case of planar surfaces it is easily done, enabling further processing and analysis of measurement results. The paper describes the fitting of a plane to a set of collected points using the least squares distance, with previously excluded outliers via the RANSAC algorithm. Based on that, a method for analysis of the deformation and shift of planar surfaces is also described.

  2. Data-Driven Surface Traversability Analysis for Mars 2020 Landing Site Selection

    Science.gov (United States)

    Ono, Masahiro; Rothrock, Brandon; Almeida, Eduardo; Ansar, Adnan; Otero, Richard; Huertas, Andres; Heverly, Matthew

    2015-01-01

    The objective of this paper is three-fold: 1) to describe the engineering challenges in the surface mobility of the Mars 2020 Rover mission that are considered in the landing site selection processs, 2) to introduce new automated traversability analysis capabilities, and 3) to present the preliminary analysis results for top candidate landing sites. The analysis capabilities presented in this paper include automated terrain classification, automated rock detection, digital elevation model (DEM) generation, and multi-ROI (region of interest) route planning. These analysis capabilities enable to fully utilize the vast volume of high-resolution orbiter imagery, quantitatively evaluate surface mobility requirements for each candidate site, and reject subjectivity in the comparison between sites in terms of engineering considerations. The analysis results supported the discussion in the Second Landing Site Workshop held in August 2015, which resulted in selecting eight candidate sites that will be considered in the third workshop.

  3. Reference-free total reflection X-ray fluorescence analysis of semiconductor surfaces with synchrotron radiation.

    Science.gov (United States)

    Beckhoff, Burkhard; Fliegauf, Rolf; Kolbe, Michael; Müller, Matthias; Weser, Jan; Ulm, Gerhard

    2007-10-15

    Total reflection X-ray fluorescence (TXRF) analysis is a well-established method to monitor lowest level contamination on semiconductor surfaces. Even light elements on a wafer surface can be excited effectively when using high-flux synchrotron radiation in the soft X-ray range. To meet current industrial requirements in nondestructive semiconductor analysis, the Physikalisch-Technische Bundesanstalt (PTB) operates dedicated instrumentation for analyzing light element contamination on wafer pieces as well as on 200- and 300-mm silicon wafer surfaces. This instrumentation is also suited for grazing incidence X-ray fluorescence analysis and conventional energy-dispersive X-ray fluorescence analysis of buried and surface nanolayered structures, respectively. The most prominent features are a high-vacuum load-lock combined with an equipment front end module and a UHV irradiation chamber with an electrostatic chuck mounted on an eight-axis manipulator. Here, the entire surface of a 200- or a 300-mm wafer can be scanned by monochromatized radiation provided by the plane grating monochromator beamline for undulator radiation in the PTB laboratory at the electron storage ring BESSY II. This beamline provides high spectral purity and high photon flux in the range of 0.078-1.86 keV. In addition, absolutely calibrated photodiodes and Si(Li) detectors are used to monitor the exciting radiant power respectively the fluorescence radiation. Furthermore, the footprint of the excitation radiation at the wafer surface is well-known due to beam profile recordings by a CCD during special operation conditions at BESSY II that allow for drastically reduced electron beam currents. Thus, all the requirements of completely reference-free quantitation of TXRF analysis are fulfilled and are to be presented in the present work. The perspectives to arrange for reference-free quantitation using X-ray tube-based, table-top TXRF analysis are also addressed.

  4. Surface enhanced Raman optical activity as an ultra sensitive tool for ligand binding analysis

    DEFF Research Database (Denmark)

    Johannessen, Christian; Abdali, Salim

    2007-01-01

    The Surface Enhanced Resonance Raman Scattering (SERRS) and Surface Enhanced Resonance Raman Optical Activity (SERROA) spectra of myoglobin and the myoglobin-azide complex were measured on very dilute samples (100 nM protein) in order to analyze the sensitivity of SERROA spectroscopy when inducing...... upon azide complexation. Application of this method allows for rapid analysis of ligand binding in metalloproteins in dilute aqueous solution and could in the future, when combined with theoretical studies, increase the obtainable structural resolution of proteins beyond that of X-ray analysis....

  5. The structural and compositional analysis of single crystal surfaces using low energy ion scattering

    International Nuclear Information System (INIS)

    Armour, D.G.; Van der Berg, J.A.; Verheij, IL.K.

    1979-01-01

    The use of ion scattering for surface composition and structure analysis has been reviewed. The extreme surface specificity of this technique has been widely used to obtain quitative information in a straightforward way, but the/aolc/currence of charge exchange processes, thermal lattice vibrations and multiple scattering have precluded quantitative analysis of experimental data. Examples are quoted to illustrate the progress that has been made in understanding these fundamental processes and in applying this knowledge to the development of the analytical capabilities of the technique. (author)

  6. Surface analysis of 316 stainless steel treated with cold atmospheric plasma

    Energy Technology Data Exchange (ETDEWEB)

    Williams, David F., E-mail: david.williams@surrey.ac.uk [Department of Mechanical Engineering Sciences, University Of Surrey, Guildford, Surrey GU2 7XH (United Kingdom); TWI Ltd Granta Park Great Abington, Cambridge CB21 6AL (United Kingdom); Kellar, Ewen J.C. [TWI Ltd Granta Park Great Abington, Cambridge CB21 6AL (United Kingdom); Jesson, David A.; Watts, John F. [Department of Mechanical Engineering Sciences, University Of Surrey, Guildford, Surrey GU2 7XH (United Kingdom)

    2017-05-01

    Highlights: • Reduction in carbon contamination from ∼80 at.% to 40 at.% after 15 s treatment. • Associated carbon thickness reduction from 4.5 nm to 0.5 nm. • Area treated by torch has a diameter of 11 mm measured using imaging XPS. - Abstract: The surface of 316 stainless steel has been modified using cold atmospheric plasma (CAP) to increase the surface free energy (by cleaning the and chemically activating the surface)IN preparation for subsequent processes such as painting, coating or adhesive bonding. The analyses carried out, on CAP treated 316 stainless steel surfaces, includes X-ray photoelectron spectroscopy (XPS), imaging XPS (iXPS), and surface free energy (SFE) analysis using contact angle measurements. The CAP treatment is shown to increase the SFE of as-received 316 stainless steel from ∼39 mJ m{sup −1} to >72 mJ m{sup −1} after a short exposure to the plasma torch. This was found to correlate to a reduction in adventitious carbon, as determined by XPS analysis of the surface. The reduction from ∼90 at% to ∼30% and ∼39 at%, after being plasma treated for 5 min and 15 s respectively, shows that the process is relatively quick at changing the surface. It is suggested that the mechanism that causes the increase in surface free energy is chain scission of the hydrocarbon contamination triggered by free electrons in the plasma plume followed by chemical functionalisation of the metal oxide surface and some of the remaining carbon contamination layer.

  7. Analysis of surfaces for characterization of fungal burden - Does it matter?

    Science.gov (United States)

    Viegas, Carla; Faria, Tiago; Meneses, Márcia; Carolino, Elisabete; Viegas, Susana; Gomes, Anita Quintal; Sabino, Raquel

    2016-01-01

    Mycological contamination of occupational environments can be a result of fungal spores' dispersion in the air and on surfaces. Therefore, it is very important to assess it in both types of the samples. In the present study we assessed fungal contamination in the air and in the surface samples to show relevance of surfaces sampling in complementing the results obtained in the air samples. In total, 42 settings were assessed by the analysis of air and surfaces samples. The settings were divided into settings with a high fungal load (7 poultry farms and 7 pig farms, 3 cork industries, 3 waste management plants, 2 wastewater treatment plants and 1 horse stable) and a low fungal load (10 hospital canteens, 8 college canteens and 1 maternity hospital). In addition to culture-based methods, molecular tools were also applied to detect fungal burden in the settings with a higher fungal load. From the 218 sampling sites, 140 (64.2%) presented different species in the examined surfaces when compared with the species identified in the air. A positive association in the high fungal load settings was found between the presence of different species in the air and surfaces. Wastewater treatment plants constituted the setting with the highest number of different species between the air and surface. We observed that surfaces sampling and application of molecular tools showed the same efficacy of species detection in high fungal load settings, corroborating the fact that surface sampling is crucial for a correct and complete analysis of occupational scenarios. This work is available in Open Access model and licensed under a CC BY-NC 3.0 PL license.

  8. Analysis of surfaces for characterization of fungal burden – Does it matter?

    Directory of Open Access Journals (Sweden)

    Carla Viegas

    2016-08-01

    Full Text Available Objectives: Mycological contamination of occupational environments can be a result of fungal spores’ dispersion in the air and on surfaces. Therefore, it is very important to assess it in both types of the samples. In the present study we assessed fungal contamination in the air and in the surface samples to show relevance of surfaces sampling in complementing the results obtained in the air samples. Material and Methods: In total, 42 settings were assessed by the analysis of air and surfaces samples. The settings were divided into settings with a high fungal load (7 poultry farms and 7 pig farms, 3 cork industries, 3 waste management plants, 2 wastewater treatment plants and 1 horse stable and a low fungal load (10 hospital canteens, 8 college canteens and 1 maternity hospital. In addition to culture-based methods, molecular tools were also applied to detect fungal burden in the settings with a higher fungal load. Results: From the 218 sampling sites, 140 (64.2% presented different species in the examined surfaces when compared with the species identified in the air. A positive association in the high fungal load settings was found between the presence of different species in the air and surfaces. Wastewater treatment plants constituted the setting with the highest number of different species between the air and surface. Conclusions: We observed that surfaces sampling and application of molecular tools showed the same efficacy of species detection in high fungal load settings, corroborating the fact that surface sampling is crucial for a correct and complete analysis of occupational scenarios.

  9. GHRSST Level 4 RTO Terra MODIS-AMSRE Night North America Regional Blended Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the JPL Physical...

  10. GHRSST Level 4 ODYSSEA North-Western Europe Regional Foundation Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at Ifremer/CERSAT...

  11. Determination of the appropriate use of pavement surface history in the KDOT life-cycle analysis process.

    Science.gov (United States)

    2008-09-01

    The primary objective of this study was to evaluate KDOTs pavement surfacing history and recommend : whether or not the departments life-cycle cost analysis (LCCA) procedure should include a surfacing history : component, and, if so, how the LC...

  12. GHRSST Level 4 MUR Global Foundation Sea Surface Temperature Analysis (v4.1) (GDS versions 1 and 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced as a retrospective dataset (four day latency) and...

  13. GHRSST Level 4 REMO_OI_SST_5km Regional Foundation Sea Surface Temperature Analysis (GDS version 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature (SST) analysis produced daily on an operational basis by the...

  14. GHRSST Level 4 CMC0.2deg Global Foundation Sea Surface Temperature Analysis (GDS version 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature (SST) analysis produced daily on an operational basis at the Canadian...

  15. GHRSST Level 4 DMI_OI North Sea and Baltic Sea Regional Foundation Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis by the Danish...

  16. GHRSST Level 4 RTO Aqua MODIS-AMSRE Night North America Regional Blended Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the JPL Physical...

  17. GHRSST Level 4 RTO Terra MODIS-AMSRE Day North America Regional Blended Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the JPL Physical...

  18. GHRSST Level 4 CMC0.1deg Global Foundation Sea Surface Temperature Analysis (GDS version 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature (SST) analysis produced daily on an operational basis at the Canadian...

  19. GHRSST Level 4 MW_IR_OI Global Foundation Sea Surface Temperature analysis (GDS versions 1 and 2)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) global Level 4 sea surface temperature analysis produced daily on a 0.81 degree grid at Remote Sensing...

  20. GHRSST Level 4 RTO Aqua MODIS-AMSRE Day North America Regional Blended Sea Surface Temperature Analysis (GDS version 1)

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A Group for High Resolution Sea Surface Temperature (GHRSST) Level 4 sea surface temperature analysis produced daily on an operational basis at the JPL Physical...

  1. Adhesion and friction in polymer films on solid substrates: conformal sites analysis and corresponding surface measurements.

    Science.gov (United States)

    An, Rong; Huang, Liangliang; Mineart, Kenneth P; Dong, Yihui; Spontak, Richard J; Gubbins, Keith E

    2017-05-21

    In this work, we present a statistical mechanical analysis to elucidate the molecular-level factors responsible for the static and dynamic properties of polymer films. This analysis, which we term conformal sites theory, establishes that three dimensionless parameters play important roles in determining differences from bulk behavior for thin polymer films near to surfaces: a microscopic wetting parameter, α wx , defined as the ratio of polymer-substrate interaction to polymer-polymer interaction; a dimensionless film thickness, H*; and dimensionless temperature, T*. The parameter α wx introduced here provides a more fundamental measure of wetting than previous metrics, since it is defined in terms of intermolecular forces and the atomic structure of the substrate, and so is valid at the nanoscale for gas, liquid or solid films. To test this theoretical analysis, we also report atomic force microscopy measurements of the friction coefficient (μ), adhesion force (F A ) and glass transition temperature (T g ) for thin films of two polymers, poly(methyl methacrylate) (PMMA) and polystyrene (PS), on two planar substrates, graphite and silica. Both the friction coefficient and the glass transition temperature are found to increase as the film thickness decreases, and this increase is more pronounced for the graphite than for the silica surface. The adhesion force is also greater for the graphite surface. The larger effects encountered for the graphite surface are attributed to the fact that the microscopic wetting parameter, α wx , is larger for graphite than for silica, indicating stronger attraction of polymer chains to the graphite surface.

  2. System architecture and operational analysis of medium displacement unmanned surface vehicle sea hunter as a surface warfare component of distributed lethality

    Science.gov (United States)

    2017-06-01

    NAVAL POSTGRADUATE SCHOOL MONTEREY, CALIFORNIA THESIS Approved for public release. Distribution is unlimited. SYSTEM ARCHITECTURE ...TITLE AND SUBTITLE SYSTEM ARCHITECTURE AND OPERATIONAL ANALYSIS OF MEDIUM DISPLACEMENT UNMANNED SURFACE VEHICLE SEA HUNTER AS A SURFACE WARFARE...traceability, requirements and capabilities while determining the architecture framework in accordance with the Department of Defense Architectural

  3. On the contraction of the W(001)-(1x1) surface using LEED intensity analysis

    International Nuclear Information System (INIS)

    Read, M.N.; Russell, G.J.

    1979-01-01

    Three recent independent attempts at reducing the W(001)-(1x1) surface structure by LEED beam intensity analysis have yielded contractions of the topmost layer spacing of 6+-6%, 11+-2%, 4.4+-3% normal to the surface plane. The authors investigate possible reasons for the discrepancies by comparing published experimental and theoretical profiles of these workers as well as their own. Their main conclusions are that the direct comparison of experimental data of different investigators shows deviations which are comparable to the changes in the calculated profiles for various surface contractions. Also the deviations between calculated intensity profiles using different (but still realistic) assumed scattering potentials are comparable to the changes in the calculated profiles for various surface contractions. (Auth.)

  4. Quantitative strain analysis of surfaces and interfaces using extremely asymmetric x-ray diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Akimoto, Koichi [Graduate School of Engineering, Nagoya University, Nagoya, 464-8603 (Japan); Emoto, Takashi, E-mail: akimoto@nagoya-u.j [Toyota National College of Technology, Toyota, Aichi 471-8525 (Japan)

    2010-12-01

    Strain can reduce carrier mobility and the reliability of electronic devices and affect the growth mode of thin films and the stability of nanometer-scale crystals. To control lattice strain, a technique for measuring the minute lattice strain at surfaces and interfaces is needed. Recently, an extremely asymmetric x-ray diffraction method has been developed for this purpose. By employing Darwin's dynamical x-ray diffraction theory, quantitative evaluation of strain at surfaces and interfaces becomes possible. In this paper, we review our quantitative strain analysis studies on native SiO{sub 2}/Si interfaces, reconstructed Si surfaces, Ni/Si(111)-H interfaces, sputtered III-V compound semiconductor surfaces, high-k/Si interfaces, and Au ion-implanted Si. (topical review)

  5. Global surface temperature change analysis based on MODIS data in recent twelve years

    Science.gov (United States)

    Mao, K. B.; Ma, Y.; Tan, X. L.; Shen, X. Y.; Liu, G.; Li, Z. L.; Chen, J. M.; Xia, L.

    2017-01-01

    Global surface temperature change is one of the most important aspects in global climate change research. In this study, in order to overcome shortcomings of traditional observation methods in meteorology, a new method is proposed to calculate global mean surface temperature based on remote sensing data. We found that (1) the global mean surface temperature was close to 14.35 °C from 2001 to 2012, and the warmest and coldest surface temperatures of the global in the recent twelve years occurred in 2005 and 2008, respectively; (2) the warmest and coldest surface temperatures on the global land surface occurred in 2005 and 2001, respectively, and on the global ocean surface in 2010 and 2008, respectively; and (3) in recent twelve years, although most regions (especially the Southern Hemisphere) are warming, global warming is yet controversial because it is cooling in the central and eastern regions of Pacific Ocean, northern regions of the Atlantic Ocean, northern regions of China, Mongolia, southern regions of Russia, western regions of Canada and America, the eastern and northern regions of Australia, and the southern tip of Africa. The analysis of daily and seasonal temperature change indicates that the temperature change is mainly caused by the variation of orbit of celestial body. A big data model based on orbit position and gravitational-magmatic change of celestial body with the solar or the galactic system should be built and taken into account for climate and ecosystems change at a large spatial-temporal scale.

  6. Exploring Surface Analysis Techniques for the Detection of Molecular Contaminants on Spacecraft

    Science.gov (United States)

    Rutherford, Gugu N.; Seasly, Elaine; Thornblom, Mark; Baughman, James

    2016-01-01

    Molecular contamination is a known area of concern for spacecraft. To mitigate this risk, projects involving space flight hardware set requirements in a contamination control plan that establishes an allocation budget for the exposure of non-volatile residues (NVR) onto critical surfaces. The purpose of this work will focus on non-contact surface analysis and in situ monitoring to mitigate molecular contamination on space flight hardware. By using Scanning Electron Microscopy and Energy Dispersive Spectroscopy (SEM-EDS) with Raman Spectroscopy, an unlikely contaminant was identified on space flight hardware. Using traditional and surface analysis methods provided the broader view of the contamination sources allowing for best fit solutions to prevent any future exposure.

  7. Numerical analysis of free surface instabilities in the IFMIF lithium target

    Energy Technology Data Exchange (ETDEWEB)

    Gordeev, S.; Heinzel, V. [Research Centre of Karlsruhe (Germany). Inst. for Reactor Safety; Moeslang, A. [Research Centre of Karlsruhe (Germany). Inst. for Material Research I

    2007-07-01

    The International Fusion Materials Facility (IFMIF) facility uses a high speed (10-20 m/s) Lithium (Li) jet flow as a target for two 40 MeV/125 mA deuteron beams. The major function of the Li target is to provide a stable Li jet for the production of an intense neutron flux. For the understanding the lithium jet behaviour and elimination of the free-surface flow instabilities a detailed analysis of the Li jet flow is necessary. Different kinds of instability mechanisms in the liquid jet flow have been evaluated and classified based on analytical and experimental data. Numerical investigations of the target free surface flow have been performed. Previous numerical investigations have shown in principle the suitability of CFD code Star- CD for the simulation of the Li-target flow. The main objective of this study is detailed numerical analysis of instabilities in the Li-jet flow caused by boundary layer relaxation near the nozzle exit, transition to the turbulence flow and back wall curvature. A number of CFD models are developed to investigate the formation of instabilities on the target surface. Turbulence models are validated on the experimental data. Experimental observations have shown that the change of the nozzle geometry at the outlet such as a slight divergence of the nozzle surfaces or nozzle edge defects causes the flow separation and occurrence of longitudinal periodic structures on the free surface with an amplitude up to 5 mm. Target surface fluctuations of this magnitude can lead to the penetration of the deuteron beam in the target structure and cause the local overheating of the back plat. Analysis of large instabilities in the Li-target flow combined with the heat distribution in lithium depending on the free surface shape is performed in this study. (orig.)

  8. Heterogeneous structure and surface tension effects on mechanical response in pulmonary acinus: A finite element analysis.

    Science.gov (United States)

    Koshiyama, Kenichiro; Nishimoto, Keisuke; Ii, Satoshi; Sera, Toshihiro; Wada, Shigeo

    2018-01-20

    The pulmonary acinus is a dead-end microstructure that consists of ducts and alveoli. High-resolution micro-CT imaging has recently provided detailed anatomical information of a complete in vivo acinus, but relating its mechanical response with its detailed acinar structure remains challenging. This study aimed to investigate the mechanical response of acinar tissue in a whole acinus for static inflation using computational approaches. We performed finite element analysis of a whole acinus for static inflation. The acinar structure model was generated based on micro-CT images of an intact acinus. A continuum mechanics model of the lung parenchyma was used for acinar tissue material model, and surface tension effects were explicitly included. An anisotropic mechanical field analysis based on a stretch tensor was combined with a curvature-based local structure analysis. The airspace of the acinus exhibited nonspherical deformation as a result of the anisotropic deformation of acinar tissue. A strain hotspot occurred at the ridge-shaped region caused by a rod-like deformation of acinar tissue on the ridge. The local structure becomes bowl-shaped for inflation and, without surface tension effects, the surface of the bowl-shaped region primarily experiences isotropic deformation. Surface tension effects suppressed the increase in airspace volume and inner surface area, while facilitating anisotropic deformation on the alveolar surface. In the lungs, the heterogeneous acinar structure and surface tension induce anisotropic deformation at the acinar and alveolar scales. Further research is needed on structural variation of acini, inter-acini connectivity, or dynamic behavior to understand multiscale lung mechanics. Copyright © 2018 Elsevier Ltd. All rights reserved.

  9. Numerical analysis of free surface instabilities in the IFMIF lithium target

    International Nuclear Information System (INIS)

    Gordeev, S.; Heinzel, V.; Moeslang, A.

    2007-01-01

    The International Fusion Materials Facility (IFMIF) facility uses a high speed (10-20 m/s) Lithium (Li) jet flow as a target for two 40 MeV/125 mA deuteron beams. The major function of the Li target is to provide a stable Li jet for the production of an intense neutron flux. For the understanding the lithium jet behaviour and elimination of the free-surface flow instabilities a detailed analysis of the Li jet flow is necessary. Different kinds of instability mechanisms in the liquid jet flow have been evaluated and classified based on analytical and experimental data. Numerical investigations of the target free surface flow have been performed. Previous numerical investigations have shown in principle the suitability of CFD code Star- CD for the simulation of the Li-target flow. The main objective of this study is detailed numerical analysis of instabilities in the Li-jet flow caused by boundary layer relaxation near the nozzle exit, transition to the turbulence flow and back wall curvature. A number of CFD models are developed to investigate the formation of instabilities on the target surface. Turbulence models are validated on the experimental data. Experimental observations have shown that the change of the nozzle geometry at the outlet such as a slight divergence of the nozzle surfaces or nozzle edge defects causes the flow separation and occurrence of longitudinal periodic structures on the free surface with an amplitude up to 5 mm. Target surface fluctuations of this magnitude can lead to the penetration of the deuteron beam in the target structure and cause the local overheating of the back plat. Analysis of large instabilities in the Li-target flow combined with the heat distribution in lithium depending on the free surface shape is performed in this study. (orig.)

  10. Human fetal osteoblast behavior on zirconia dental implants and zirconia disks with microstructured surfaces. An experimental in vitro study.

    Science.gov (United States)

    Delgado-Ruíz, Rafael Arcesio; Gomez Moreno, Gerardo; Aguilar-Salvatierra, Antonio; Markovic, Aleksa; Mate-Sánchez, Jose Eduardo; Calvo-Guirado, José Luis

    2016-11-01

    To measure the lateral surface area of microgrooved zirconia implants, to evaluate the cell geometry and cell density of human fetal osteoblasts seeded on zirconia microgrooved implants, to describe the surface roughness and chemistry, and to evaluate the activity of human fetal osteoblasts seeded on zirconia microgrooved disks. This experimental in vitro study used 62 zirconia implants and 130 zirconia disks. Two experimental groups were created for the implants: 31 non-microgrooved implants (Control) and 31 microgrooved implants (Test); two experimental groups were created for the disks: 65 non-microgrooved disks (Control) and 65 microgrooved disks (Test). The following evaluations of the implants were made: lateral surface area (LSA), cell morphology, and density of human fetal osteoblasts seeded on implant surfaces. On the disks, surface parameters (roughness and chemistry) and cell activity (alkaline phosphatase - ALP and alizarin red - ALZ) were evaluated at 7 and 15 days. LSA was lower for control implants (62.8 mm) compared with test implants (128.74 mm) (P zirconia implants with microgrooves. (ii) The LSA of microgrooved zirconia implants is greater and provides more available surface compared with implants of the same dimensions without microgrooves. (iii) Microgrooves on zirconia implants modify the morphology and guide the size and alignment of human fetal osteoblasts. (iv) Zirconia surfaces with microgrooves of 30 μm width and 70 μm separation between grooves enhance ALP and ALZ expression by human fetal osteoblasts. © 2015 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.

  11. Historic Surface Rupture Informing Probabilistic Fault Displacement Analysis: New Zealand Case Studies

    Science.gov (United States)

    Villamor, P.; Litchfield, N. J.; Van Dissen, R. J.; Langridge, R.; Berryman, K. R.; Baize, S.

    2016-12-01

    Surface rupture associated with the 2010 Mw7.1 Darfield Earthquake (South Island, New Zealand) was extremely well documented, thanks to an immediate field mapping response and the acquisition of LiDAR data within days of the event. With respect to informing Probabilistic Fault Displacement Analysis (PFDHA) the main insights and outcomes from this rupture through Quaternary gravel are: 1) significant distributed deformation either side of the main trace (30 to 300 m wide deformation zone) and how the deformation is distributed away from the main trace; 2) a thorough analysis of uncertainty of the displacement measures obtained using the LIDAR data and repeated measurements from several scientists; and 3) the short surface rupture length for the reported magnitude, resulting from complex fault rupture with 5-6 reverse and strike-slip strands, most of which had no surface rupture. While the 2010 event is extremely well documented and will be an excellent case to add to the Surface Rupture during Earthquakes database (SURE), other NZ historical earthquakes that are not so well documented, but can provide important information for PFDHA. New Zealand has experienced about 10 historical surface fault ruptures since 1848, comprising ruptures on strike-slip, reverse and normal faults. Mw associated with these ruptures ranges between 6.3 and 8.1. From these ruptures we observed that the surface expression of deformation can be influenced by: fault maturity; the type of Quaternary sedimentary cover; fault history (e.g., influence of inversion tectonics, flexural slip); fault complexity; and primary versus secondary rupture. Other recent >Mw 6.6 earthquakes post-2010 that did not rupture the ground surface have been documented with InSAR and can inform Mw thresholds for surface fault rupture. It will be important to capture all this information and that of similar events worldwide to inform the SURE database and ultimately PFDHA.

  12. The use of artificial intelligence methods for visual analysis of properties of surface layers

    Directory of Open Access Journals (Sweden)

    Tomasz Wójcicki

    2014-12-01

    Full Text Available [b]Abstract[/b]. The article presents a selected area of research on the possibility of automatic prediction of material properties based on the analysis of digital images. Original, holistic model of forecasting properties of surface layers based on a multi-step process that includes the selected methods of processing and analysis of images, inference with the use of a priori knowledge bases and multi-valued fuzzy logic, and simulation with the use of finite element methods is presented. Surface layers characteristics and core technologies of their production processes such as mechanical, thermal, thermo-mechanical, thermo-chemical, electrochemical, physical are discussed. Developed methods used in the model for the classification of images of the surface layers are shown. The objectives of the use of selected methods of processing and analysis of digital images, including techniques for improving the quality of images, segmentation, morphological transformation, pattern recognition and simulation of physical phenomena in the structures of materials are described.[b]Keywords[/b]: image analysis, surface layer, artificial intelligence, fuzzy logic

  13. Neutron activation analysis to the profile surface sediments from several sites on the Havana Bay

    International Nuclear Information System (INIS)

    Diaz Riso, O.; Gelen, A.; Lopez, N.; Gonzalez, H.; Manso, M.V.; Graciano, A.M.; Nogueira, C.A.; Beltran, J.; Soto, J.

    2003-01-01

    Instrumental neutron activation analysis (INAA) technique was employed to analyze the surface sediments from several sites on the Havana Bay, Cuba. Measurements of heavy and trace elements in the sediments are reported. The results show that the concentration of the elements is site dependent. The data suggest that an anthropogenic input into the bay from domestic sewage and industries occurred

  14. Unconventional optimized surface wave acquisition and analysis: Comparative tests in a perilagoon area

    Czech Academy of Sciences Publication Activity Database

    Dal Moro, Giancarlo; Ponta, R.; Mauro, R.

    2015-01-01

    Roč. 114, MAR (2015), s. 158-167 ISSN 0926-9851 Institutional support: RVO:67985891 Keywords : surface waves * Rayleigh waves * phase velocity * group velocity * dispersion * full velocity spectrum /FVS/ analysis Subject RIV: DB - Geology ; Mineralogy Impact factor: 1.355, year: 2015

  15. A comparison of surface marker analysis and FAB classification in acute myeloid leukemia

    NARCIS (Netherlands)

    van der Reijden, H. J.; van Rhenen, D. J.; Lansdorp, P. M.; van't Veer, M. B.; Langenhuijsen, M. M.; Engelfriet, C. P.; von dem Borne, A. E.

    1983-01-01

    Surface marker analysis with rosette tests and a large panel of xenoantisera and monoclonal antibodies was done on the malignant cells of 55 patients with acute myeloid leukemia (AML). The diagnosis was made on morphological and cytochemical grounds, and the leukemias were classified according to

  16. Optimization of dextran syntesis and acidic hydrolisis by surface response analysis

    Directory of Open Access Journals (Sweden)

    GUIMARÃES D.P.

    1999-01-01

    Full Text Available The influence of some variables in the in vitro synthesis of dextran by dextransucrase from Leusconostoc mesenteroides NRRL B512F, as well as in the acidic hydrolysis of the dextran produced, were studied in order to maximize the production of clinical dextran (dextran 70 and dextran 40. The experiments were conducted using a factorial design and surface response analysis.

  17. Detection analysis of surface hydroxyl active sites and simulation calculation of the surface dissociation constants of aqueous diatomite suspensions

    Science.gov (United States)

    Ma, Shu-Cui; Wang, Zhi-Gang; Zhang, Ji-Lin; Sun, De-Hui; Liu, Gui-Xia

    2015-02-01

    The surface properties of the diatomite were investigated using nitrogen adsorption/deadsorption isotherms, TG-DSC, FTIR, and XPS, and surface protonation-deprotonation behavior was determined by continuous acid-base potentiometric titration technique. The diatomite sample with porous honeycomb structure has a BET specific surface area of 10.21 m2/g and large numbers of surface hydroxyl functional groups (i.e. tbnd Si-OH, tbnd Fe-OH, and tbnd Al-OH). These surface hydroxyls can be protonated or deprotonated depending on the pH of the suspension. The experimental potentiometric data in two different ionic strength solutions (0.1 and 0.05 mol/L NaCl) were fitted using ProtoFit GUI V2.1 program by applying diffuse double layer model (DLM) with three amphoteric sites and minimizing the sum of squares between a dataset derivative function and a model derivative function. The optimized surface parameters (i.e. surface dissociation constants (log K1, log K2) and surface site concentrations (log C)) of the sample were obtained. Based on the optimized surface parameters, the surface species distribution was calculated using Program-free PHREEQC 3.1.2. Thus, this work reveals considerable new information about surface protonation-deprotonation processes and surface adsorptive behaviors of the diatomite, which helps us to effectively use the cheap and cheerful diatomite clay adsorbent.

  18. The transient response for different types of erodable surface thermocouples using finite element analysis

    Directory of Open Access Journals (Sweden)

    Mohammed Hussein

    2007-01-01

    Full Text Available The transient response of erodable surface thermocouples has been numerically assessed by using a two dimensional finite element analysis. Four types of base metal erodable surface thermocouples have been examined in this study, included type-K (alumel-chromel, type-E (chromel-constantan, type-T (copper-constantan, and type-J (iron-constantan with 50 mm thick- ness for each. The practical importance of these types of thermocouples is to be used in internal combustion engine studies and aerodynamics experiments. The step heat flux was applied at the surface of the thermocouple model. The heat flux from the measurements of the surface temperature can be commonly identified by assuming that the heat transfer within these devices is one-dimensional. The surface temperature histories at different positions along the thermocouple are presented. The normalized surface temperature histories at the center of the thermocouple for different types at different response time are also depicted. The thermocouple response to different heat flux variations were considered by using a square heat flux with 2 ms width, a sinusoidal surface heat flux variation width 10 ms period and repeated heat flux variation with 2 ms width. The present results demonstrate that the two dimensional transient heat conduction effects have a significant influence on the surface temperature history measurements made with these devices. It was observed that the surface temperature history and the transient response for thermocouple type-E are higher than that for other types due to the thermal properties of this thermocouple. It was concluded that the thermal properties of the surrounding material do have an impact, but the properties of the thermocouple and the insulation materials also make an important contribution to the net response.

  19. Analysis of concentric and eccentric contractions in biceps brachii muscles using surface electromyography signals and multifractal analysis.

    Science.gov (United States)

    Marri, Kiran; Swaminathan, Ramakrishnan

    2016-06-23

    Muscle contractions can be categorized into isometric, isotonic (concentric and eccentric) and isokinetic contractions. The eccentric contractions are very effective for promoting muscle hypertrophy and produce larger forces when compared to the concentric or isometric contractions. Surface electromyography signals are widely used for analyzing muscle activities. These signals are nonstationary, nonlinear and exhibit self-similar multifractal behavior. The research on surface electromyography signals using multifractal analysis is not well established for concentric and eccentric contractions. In this study, an attempt has been made to analyze the concentric and eccentric contractions associated with biceps brachii muscles using surface electromyography signals and multifractal detrended moving average algorithm. Surface electromyography signals were recorded from 20 healthy individuals while performing a single curl exercise. The preprocessed signals were divided into concentric and eccentric cycles and in turn divided into phases based on range of motion: lower (0°-90°) and upper (>90°). The segments of surface electromyography signal were subjected to multifractal detrended moving average algorithm, and multifractal features such as strength of multifractality, peak exponent value, maximum exponent and exponent index were extracted in addition to conventional linear features such as root mean square and median frequency. The results show that surface electromyography signals exhibit multifractal behavior in both concentric and eccentric cycles. The mean strength of multifractality increased by 15% in eccentric contraction compared to concentric contraction. The lowest and highest exponent index values are observed in the upper concentric and lower eccentric contractions, respectively. The multifractal features are observed to be helpful in differentiating surface electromyography signals along the range of motion as compared to root mean square and median

  20. Detection analysis of surface hydroxyl active sites and simulation calculation of the surface dissociation constants of aqueous diatomite suspensions

    Energy Technology Data Exchange (ETDEWEB)

    Ma, Shu-Cui [State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022 (China); Key Laboratory of Applied Chemistry and Nanotechnology at Universities of Jilin Province, Changchun University of Science and Technology, Changchun 130022 (China); Wang, Zhi-Gang [State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022 (China); Zhang, Ji-Lin, E-mail: zjl@ciac.ac.cn [State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022 (China); Sun, De-Hui [Changchun Institute Technology, Changchun 130012 (China); Liu, Gui-Xia, E-mail: liuguixia22@163.com [Key Laboratory of Applied Chemistry and Nanotechnology at Universities of Jilin Province, Changchun University of Science and Technology, Changchun 130022 (China)

    2015-02-01

    Highlights: • To examine surface hydroxyl functional groups of the calcined diatomite by TGA-DSC, FTIR, and XPS. • To calculate the optimized log K{sub 1}, log K{sub 2} and log C values and the surface species distribution of each surface reactive site using ProtoFit and PHREEQC, respectively. - Abstract: The surface properties of the diatomite were investigated using nitrogen adsorption/deadsorption isotherms, TG-DSC, FTIR, and XPS, and surface protonation–deprotonation behavior was determined by continuous acid–base potentiometric titration technique. The diatomite sample with porous honeycomb structure has a BET specific surface area of 10.21 m{sup 2}/g and large numbers of surface hydroxyl functional groups (i.e. ≡Si-OH, ≡Fe-OH, and ≡Al-OH). These surface hydroxyls can be protonated or deprotonated depending on the pH of the suspension. The experimental potentiometric data in two different ionic strength solutions (0.1 and 0.05 mol/L NaCl) were fitted using ProtoFit GUI V2.1 program by applying diffuse double layer model (DLM) with three amphoteric sites and minimizing the sum of squares between a dataset derivative function and a model derivative function. The optimized surface parameters (i.e. surface dissociation constants (log K{sub 1}, log K{sub 2}) and surface site concentrations (log C)) of the sample were obtained. Based on the optimized surface parameters, the surface species distribution was calculated using Program-free PHREEQC 3.1.2. Thus, this work reveals considerable new information about surface protonation–deprotonation processes and surface adsorptive behaviors of the diatomite, which helps us to effectively use the cheap and cheerful diatomite clay adsorbent.

  1. Texture Analysis of Hydrophobic Polycarbonate and Polydimethylsiloxane Surfaces via Persistent Homology

    Directory of Open Access Journals (Sweden)

    Ali Nabi Duman

    2017-09-01

    Full Text Available Due to recent climate change-triggered, regular dust storms in the Middle East, dust mitigation has become the critical issue for solar energy harvesting devices. One of the methods to minimize and prevent dust adhesion and create self-cleaning abilities is to generate hydrophobic characteristics on surfaces. The purpose of this study is to explore the topological features of hydrophobic surfaces. We use non-standard techniques from topological data analysis to extract morphological features from the AFM images. Our method recovers most of the previous qualitative observations in a robust and quantitative way. Persistence diagrams, which is a summary of topological structures, witness quantitatively that the crystallized polycarbonate (PC surface possesses spherulites, voids, and fibrils, and the texture height and spherulite concentration increases with the increased immersion period. The approach also shows that the polydimethylsiloxane (PDMS exactly copied the structures at the PC surface but 80 to 90 percent of the nanofibrils were not copied at PDMS surface. We next extract a feature vector from each persistence diagram to show which experiments hold features with similar variance using principal component analysis (PCA. The K-means clustering algorithm is applied to the matrix of feature vectors to support the PCA result, grouping experiments with similar features.

  2. Implementation of Bounding Surface Model into ABAQUS and Its Application to Wellbore Stability Analysis

    Science.gov (United States)

    Chen, S.; Al-Muntasheri, G.; Abousleiman, Y. N.

    2014-12-01

    The critical state concept based bounding surface model is one of the most widely used elastoplastic constitutive models for geomaterials, attributed mainly to its essential feature of allowing plastic deformation to occur for stress points within the bounding surface and thus the capability to represent the realistic non-recoverable behaviour of soils and rocks observed under the cyclic loading. This paper develops an implicit integration algorithm for the bounding surface model, using the standard return mapping approach (elastic predictor-plastic corrector), to obtain the updated stresses for the given strain increments. The formulation of the constitutive integration requires the derivation of a supplementary differential equation to describe the evolution of a key variable, i.e., the ratio between the image stress and the current stress quantities. It is essentially an extension of the integration scheme presented in an earlier work used for the simple bounding surface version of modified Cam Clay associated with a substantially simplified hardening rule. The integration algorithm for the bounding surface model is implemented into the finite element analysis commercial program, ABAQUS, through the material interface of UMAT (user defined material subroutine), and then used for the analysis of wellbore stability problem. The predictions from the ABAQUS simulations are generally in excellent agreement with the available analytical solutions, thus demonstrating the accuracy and robustness of the proposed integration scheme.

  3. Determination of elastic mechanical characteristics of surface coatings from analysis of signals obtained by impulse excitation

    Science.gov (United States)

    Nyaguly, E.; Craştiu, I.; Deac, S.; Gozman-Pop, C.; Drăgănescu, G.; Bereteu, L.

    2018-01-01

    Most of the surface coatings are based on the synthetic polymers, which are substances composed from very large molecules that form tough, flexible, adhesive films when applied to surfaces. The other components of surface coverings materials are pigments that provide colour, opacity, gloss and other properties. Surface coatings are two-phase composite materials: constitute a polymer matrix on the one side, and on the other side of the pigments and additives dispersed in the matrix. Their role is not only aesthetically but also to ensure anticorrosive protection or even improve some mechanical properties of coated surfaces. In this paper it will follow, starting from the mechanical properties of the substrate, the metallic sheet in general, to determine the new properties of the assembly of substrate and the two coating layers, also the determination of mechanical properties of the layers. From the analysis of vibroacoustic signals obtained by the impulse excitation of the sample, one can determine the elasticity modulus. These results come to validate the results based on finite element analysis (FEA) of the same samples.

  4. Development of Response Surface Models for Rapid Analysis & Multidisciplinary Optimization of Launch Vehicle Design Concepts

    Science.gov (United States)

    Unal, Resit

    1999-01-01

    Multdisciplinary design optimization (MDO) is an important step in the design and evaluation of launch vehicles, since it has a significant impact on performance and lifecycle cost. The objective in MDO is to search the design space to determine the values of design parameters that optimize the performance characteristics subject to system constraints. Vehicle Analysis Branch (VAB) at NASA Langley Research Center has computerized analysis tools in many of the disciplines required for the design and analysis of launch vehicles. Vehicle performance characteristics can be determined by the use of these computerized analysis tools. The next step is to optimize the system performance characteristics subject to multidisciplinary constraints. However, most of the complex sizing and performance evaluation codes used for launch vehicle design are stand-alone tools, operated by disciplinary experts. They are, in general, difficult to integrate and use directly for MDO. An alternative has been to utilize response surface methodology (RSM) to obtain polynomial models that approximate the functional relationships between performance characteristics and design variables. These approximation models, called response surface models, are then used to integrate the disciplines using mathematical programming methods for efficient system level design analysis, MDO and fast sensitivity simulations. A second-order response surface model of the form given has been commonly used in RSM since in many cases it can provide an adequate approximation especially if the region of interest is sufficiently limited.

  5. Determination of Substances Content of Soil Surface Using Fast Neutron Activation Analysis

    International Nuclear Information System (INIS)

    Elin Nuraini; Elisabeth; Sunardi

    2002-01-01

    Determination of substances content of soil surface using neutron activation analysis has been performed. The aim of this research is to determine whether there are any dangerous, hazardous and toxic substances that released from The Research and Development Center for Advanced Technology (RDCAT) as a government institution has possibility in releasing that substances to the environment by surface water, sewage or rain water that give any dangerous the environmental. The fast neutron activation analysis was used to analyze the type and concentration of substances qualitative and quantitatively. The quantitative analysis was performed using relative method. Samples were counted using NaI(TI) detector. The result showed that there are several substances such as Mn-55, Fe-56, P-31, Al-27. Zn,65 and Mg-24. And there are found any hazardous, dangerous and toxic substances in the samples that causing any danger to human and environment. (author)

  6. Theory and application of shapelets to the analysis of surface self-assembly imaging.

    Science.gov (United States)

    Suderman, Robert; Lizotte, Daniel J; Abukhdeir, Nasser Mohieddin

    2015-03-01

    A method for quantitative analysis of local pattern strength and defects in surface self-assembly imaging is presented and applied to images of stripe and hexagonal ordered domains. The presented method uses "shapelet" functions which were originally developed for quantitative analysis of images of galaxies (∝10(20)m). In this work, they are used instead to quantify the presence of translational order in surface self-assembled films (∝10(-9)m) through reformulation into "steerable" filters. The resulting method is computationally efficient (with respect to the number of filter evaluations), robust to variation in pattern feature shape, and, unlike previous approaches, is applicable to a wide variety of pattern types. An application of the method is presented which uses a nearest-neighbor analysis to distinguish between uniform (defect-free) and nonuniform (strained, defect-containing) regions within imaged self-assembled domains, both with striped and hexagonal patterns.

  7. Risk analysis of breakwater caisson under wave attack using load surface approximation

    Science.gov (United States)

    Kim, Dong Hyawn

    2014-12-01

    A new load surface based approach to the reliability analysis of caisson-type breakwater is proposed. Uncertainties of the horizontal and vertical wave loads acting on breakwater are considered by using the so-called load surfaces, which can be estimated as functions of wave height, water level, and so on. Then, the first-order reliability method (FORM) can be applied to determine the probability of failure under the wave action. In this way, the reliability analysis of breakwaters with uncertainties both in wave height and in water level is possible. Moreover, the uncertainty in wave breaking can be taken into account by considering a random variable for wave height ratio which relates the significant wave height to the maximum wave height. The proposed approach is applied numerically to the reliability analysis of caisson breakwater under wave attack that may undergo partial or full wave breaking.

  8. Surface science analysis of GaAs photocathodes following sustained electron beam delivery

    Directory of Open Access Journals (Sweden)

    V. Shutthanandan

    2012-06-01

    Full Text Available Degradation of the photocathode materials employed in photoinjectors represents a challenge for sustained operation of nuclear physics accelerators and high power free electron lasers (FEL. Photocathode quantum efficiency degradation is due to residual gases in the electron source vacuum system being ionized and accelerated back to the photocathode. These investigations are a first attempt to characterize the nature of the photocathode degradation, and employ multiple surface and bulk analysis techniques to investigate damage mechanisms including sputtering of the Cs-oxidant surface monolayer, other surface chemistry effects, and ion implantation. Surface and bulk analysis studies were conducted on two GaAs photocathodes, which were removed from the JLab FEL DC photoemission gun after delivering electron beam, and two control samples. The analysis techniques include helium ion microscopy, Rutherford backscattering spectrometry (RBS, atomic force microscopy, and secondary ion mass spectrometry (SIMS. In addition, two high-polarization strained superlattice GaAs photocathode samples, one removed from the continuous electron beam accelerator facility (CEBAF photoinjector and one unused, were also analyzed using transmission electron microscopy (TEM and SIMS. It was found that heat cleaning the FEL GaAs wafer introduces surface roughness, which seems to be reduced by prolonged use. The bulk GaAs samples retained a fairly well organized crystalline structure after delivering beam but show evidence of Cs depletion on the surface. Within the precision of the SIMS and RBS measurements, the data showed no indication of hydrogen implantation or lattice damage from ion back bombardment in the bulk GaAs wafers. In contrast, SIMS and TEM measurements of the strained superlattice photocathode show clear crystal damage in the wafer from ion back bombardment.

  9. Surface science analysis of GaAs photocathodes following sustained electron beam delivery

    Energy Technology Data Exchange (ETDEWEB)

    Carlos Hernandez-Garcia, Fay Hannon, Marcy Stutzman, V. Shutthanandan, Z. Zhu, M. Nandasri, S. V. Kuchibhatla, S. Thevuthasan, W. P. Hess

    2012-06-01

    Degradation of the photocathode materials employed in photoinjectors represents a challenge for sustained operation of nuclear physics accelerators and high power Free Electron Lasers (FEL). Photocathode quantum efficiency (QE) degradation is due to residual gasses in the electron source vacuum system being ionized and accelerated back to the photocathode. These investigations are a first attempt to characterize the nature of the photocathode degradation, and employ multiple surface and bulk analysis techniques to investigate damage mechanisms including sputtering of the Cs-oxidant surface monolayer, other surface chemistry effects, and ion implantation. Surface and bulk analysis studies were conducted on two GaAs photocathodes, which were removed from the JLab FEL DC photoemission gun after delivering electron beam, and two control samples. The analysis techniques include Helium Ion Microscopy (HIM), Rutherford Backscattering Spectrometry (RBS), Atomic Force Microscopy (AFM) and Secondary Ion Mass Spectrometry (SIMS). In addition, two high-polarization strained superlattice GaAs photocathode samples, one removed from the Continuous Electron Beam Accelerator Facility (CEBAF) photoinjector and one unused, were also analyzed using Transmission Electron Microscopy (TEM) and SIMS. It was found that heat cleaning the FEL GaAs wafer introduces surface roughness, which seems to be reduced by prolonged use. The bulk GaAs samples retained a fairly well organized crystalline structure after delivering beam but shows evidence of Cs depletion on the surface. Within the precision of the SIMS and RBS measurements the data showed no indication of hydrogen implantation or lattice damage from ion back bombardment in the bulk GaAs wafers. In contrast, SIMS and TEM measurements of the strained superlattice photocathode show clear crystal damage in the wafer from ion back bombardment.

  10. Finite element based contact analysis of radio frequency MEMs switch membrane surfaces

    Science.gov (United States)

    Liu, Jin-Ya; Chalivendra, Vijaya; Huang, Wenzhen

    2017-10-01

    Finite element simulations were performed to determine the contact behavior of radio frequency (RF) micro-electro-mechanical (MEM) switch contact surfaces under monotonic and cyclic loading conditions. Atomic force microscopy (AFM) was used to capture the topography of RF-MEM switch membranes and later they were analyzed for multi-scale regular as well as fractal structures. Frictionless, non-adhesive contact 3D finite element analysis was carried out at different length scales to investigate the contact behavior of the regular-fractal surface using an elasto-plastic material model. Dominant micro-scale regular patterns were found to significantly change the contact behavior. Contact areas mainly cluster around the regular pattern. The contribution from the fractal structure is not significant. Under cyclic loading conditions, plastic deformation in the 1st loading/unloading cycle smooth the surface. The subsequent repetitive loading/unloading cycles undergo elastic contact without changing the morphology of the contacting surfaces. The work is expected to shed light on the quality of the switch surface contact as well as the optimum design of RF MEM switch surfaces.

  11. Reconstruction Accuracy Assessment of Surface and Underwater 3D Motion Analysis: A New Approach

    Directory of Open Access Journals (Sweden)

    Kelly de Jesus

    2015-01-01

    Full Text Available This study assessed accuracy of surface and underwater 3D reconstruction of a calibration volume with and without homography. A calibration volume (6000 × 2000 × 2500 mm with 236 markers (64 above and 88 underwater control points—with 8 common points at water surface—and 92 validation points was positioned on a 25 m swimming pool and recorded with two surface and four underwater cameras. Planar homography estimation for each calibration plane was computed to perform image rectification. Direct linear transformation algorithm for 3D reconstruction was applied, using 1600000 different combinations of 32 and 44 points out of the 64 and 88 control points for surface and underwater markers (resp.. Root Mean Square (RMS error with homography of control and validations points was lower than without it for surface and underwater cameras (P≤0.03. With homography, RMS errors of control and validation points were similar between surface and underwater cameras (P≥0.47. Without homography, RMS error of control points was greater for underwater than surface cameras (P≤0.04 and the opposite was observed for validation points (P≤0.04. It is recommended that future studies using 3D reconstruction should include homography to improve swimming movement analysis accuracy.

  12. Surface and Thin Film Analysis A Compendium of Principles, Instrumentation, and Applications

    CERN Document Server

    Friedbacher, Gernot

    2011-01-01

    Surveying and comparing all techniques relevant for practical applications in surface and thin film analysis, this second edition of a bestseller is a vital guide to this hot topic in nano- and surface technology. This new book has been revised and updated and is divided into four parts - electron, ion, and photon detection, as well as scanning probe microscopy. New chapters have been added to cover such techniques as SNOM, FIM, atom probe (AP),and sum frequency generation (SFG). Appendices with a summary and comparison of techniques and a list of equipment suppliers make this book a rapid ref

  13. Comparative analysis of surface soil moisture retrieval using VSWI and TVDI in karst areas

    Science.gov (United States)

    Yan, Hongbo; Zhou, Guoqing; Lu, Xianjian

    2015-12-01

    Vegetation Supply Water Index (VSWI) and Temperature Vegetation dryness Index (TVDI) are two most commonly used methods for surface soil moisture (SSM) retrieval using electromagnetic spectrum of visible, near infrared and thermal infrared band. Both of them take into account the effect of vegetation index (VI) and surface temperature (Ts) on SSM. A comparative analysis of the ability and effect of the two methods for SSM retrieval in karst areas was carried out, using the remote sensing data of Landsat 8 OLI_TIRS. The study area is located in Guilin, which is a typical karst area. The experimental results show that TVDI is more suitable for SSM retrieval in karst areas.

  14. Analysis of the Forming Process of Conical-Like Helical Surfaces with Roller Tools

    Directory of Open Access Journals (Sweden)

    Kacalak W.

    2017-02-01

    Full Text Available The article presents a methodology of an analysis and modeling of technological systems and the grinding process of conical-like helical surfaces with the use of modern CAD/CAE systems and calculations in the Matlab system. The methodology developed allows one to carry out simulation tests for the accuracy of the grinding process of helical surfaces taking into consideration the deviations of the location and shape of the system’s elements, axial and radial striking the spindle of the workpiece machined and the grinding wheel as well as the tool’s geometrical features.

  15. Energy and angle resolved ion scattering spectroscopy: new possibilities for surface analysis

    International Nuclear Information System (INIS)

    Hellings, G.J.A.

    1986-01-01

    In this thesis the design and development of a novel, very sensitive and high-resolving spectrometer for surface analysis is described. This spectrometer is designed for Energy and Angle Resolved Ion Scattering Spectroscopy (EARISS). There are only a few techniques that are sensitive enough to study the outermost atomic layer of surfaces. One of these techniques, Low-Energy Ion Scattering (LEIS), is discussed in chapter 2. Since LEIS is destructive, it is important to make a very efficient use of the scattered ions. This makes it attractive to simultaneously carry out energy and angle dependent measurements (EARISS). (Auth.)

  16. ATSR sea surface temperature data in a global analysis with TOPEX/POSEIDON altimetry

    DEFF Research Database (Denmark)

    Knudsen, Per; Andersen, Ole Baltazar; Knudsen, Thomas

    1996-01-01

    Along Track Scanning Radiometer (ATSR) data from the ERS 1 satellite mission are used in a global analysis of the surface temperature of the oceans. The data are the low resolution 0.5 degrees by 0.5 degrees average temperatures and cover about 24 months. At global scales a significant seasonal...... variability is found. On each of the hemispheres the surface temperatures reach their maximum after summer heating. The seasonal sea level variability, as observed from TOPEX/POSEIDON, reaches its maximum 1.1-1.4 months later....

  17. Stability analysis on the free surface phenomena of a magnetic fluid for general use

    International Nuclear Information System (INIS)

    Mizuta, Yo

    2011-01-01

    This paper presents an analysis for elucidating a variety of physical processes on the interface (free surface) of magnetic fluid. The present analysis is composed of the magnetic and the fluid analysis, both of which have no limitations concerning the interface elevation or its profile. The magnetic analysis provides rigorous interface magnetic field under arbitrary distributions of applied magnetic field. For the fluid analysis, the equation for interface motion includes all nonlinear effects. Physical quantities such as the interface magnetic field or the interface stresses, obtained first as the wavenumber components, facilitate confirming the relations with those by the conventional theoretical analyses. The nonlinear effect is formulated as the nonlinear mode coupling between the interface profile and the applied magnetic field. The stability of the horizontal interface profile is investigated by the dispersion relation, and summarized as the branch line. Furthermore, the balance among the spectral components of the interface stresses are shown, within the sufficient range of the wavenumber space. - Research Highlights: → General, rigorous but compact analysis for free surface phenomena is shown. → Analysis is applied without limitations on the interface elevation or its profile. → Nonlinear effects are formulated as the nonlinear mode coupling. → Bifurcation of stability is summarized as the branch line. → Balance among the interface stresses are shown in the wavenumber space.

  18. Preliminary analysis of surface mining options for Naval Oil Shale Reserve 1

    Energy Technology Data Exchange (ETDEWEB)

    1981-07-20

    The study was undertaken to determine the economic viability of surface mining to exploit the reserves. It is based on resource information already developed for NOSR 1 and conceptual designs of mining systems compatible with this resource. Environmental considerations as they relate to surface mining have been addressed qualitatively. The conclusions on economic viability were based primarily on mining costs projected from other industries using surface mining. An analysis of surface mining for the NOSR 1 resource was performed based on its particular overburden thickness, oil shale thickness, oil shale grade, and topography. This evaluation considered reclamation of the surface as part of its design and cost estimate. The capital costs for mining 25 GPT and 30 GPT shale and the operating costs for mining 25 GPT, 30 GPT, and 35 GPT shale are presented. The relationship between operating cost and stripping ratio, and the break-even stripping ratio (BESR) for surface mining to be competitive with room-and-pillar mining, are shown. Identification of potential environmental impacts shows that environmental control procedures for surface mining are more difficult to implement than those for underground mining. The following three areas are of prime concern: maintenance of air quality standards by disruption, movement, and placement of large quantities of overburden; disruption or cutting of aquifers during the mining process which affect area water supplies; and potential mineral leaching from spent shales into the aquifers. Although it is an operational benefit to place spent shale in the open pit, leaching of the spent shales and contamination of the water is detrimental. It is therefore concluded that surface mining on NOSR 1 currently is neither economically desirable nor environmentally safe. Stringent mitigation measures would have to be implemented to overcome some of the potential environmental hazards.

  19. In situ analysis of aqueous structure and adsorption at fluorocarbon, hydrocarbon and mineral surfaces

    Science.gov (United States)

    Hopkins, Adam Justin

    Altering and controlling the properties of solid surfaces in aqueous or other liquid phase environments has been a sought after objective for decades. With the discovery of chemisorbed self-assembled monolayers, this dream has become a reality. Oxide and metal surfaces can now be readily coated with an array of commercially available products to produce a desired fnctionality. The presence of these coatings on solid surfaces affects properties of the interfacial region by altering interfacial electrostatic fields, changing the structure of interfacial water molecules and altering the interactions of adsorbed species. This dissertation reports on in situ studies of adsorption at several solid/aqueous interfaces using vibrational sum-frequency spectroscopy, a surface specific technique. These studies are augmented by the use of atomic force microscopy and contact angle goniometry to characterize the prepared surfaces and their interactions with adsorbates. The studies investigate how changes in the surface structure and chemistry, as well as the bulk aqueous phase, affect interfacial structure. The studies within are primarily focused on the interactions of water with bare and functionalized fused silica and the relationship between the aqueous phase composition and the structure of fluorocarbon and hydrocarbon self-assembled monolayers. The variations in aqueous structure are then examined in detail using ionic strength controlled experiments to understand the direct interactions of water hydrophobically coated silica. This analysis is followed by an investigation of the competitive adsorption of methanol and water at fluorocarbon and hydrocarbon monolayers which show spectroscopic signatures of the interaction strength between fluorocarbons and hydrocarbons. Further studies are performed using butylammonium chloride to verify these spectroscopic signatures and reveal different molecular structures of adsorbed species at chemically different hydrophobic surfaces

  20. Surface topography analysis and performance on post-CMP images (Conference Presentation)

    Science.gov (United States)

    Lee, Jusang; Bello, Abner F.; Kakita, Shinichiro; Pieniazek, Nicholas; Johnson, Timothy A.

    2017-03-01

    again be calculated and used as yet another quantifiable parameter for SPC. In this work we measured the post Cu CMP of a die designed for 14nm technology. A region of interest (ROI) known to be indicative of the CMP processing is chosen for the topography analysis. The ROI, of size 1800 x 2500 pixels where each pixel represents 2um, was repeatably measured. We show the sensitivity based on measurements and the comparison between center and edge die measurements. The topography measurements and surface patch analysis were applied to hundreds of images representing the periodic process qualification runs required to control and verify CMP performance and tool matching. The analysis is shown to be sensitive to process conditions that vary in polishing time, type of slurry, CMP tool manufacturer, and CMP pad lifetime. Keywords: Keywords: CMP, Topography, Image Processing, Metrology, Interference microscopy, surface processing [1] De Lega, Xavier Colonna, and Peter De Groot. "Optical topography measurement of patterned wafers." Characterization and Metrology for ULSI Technology 2005 788 (2005): 432-436. [2] de Groot, Peter. "Coherence scanning interferometry." Optical Measurement of Surface Topography. Springer Berlin Heidelberg, 2011. 187-208. [3] Watson, Layne T., Thomas J. Laffey, and Robert M. Haralick. "Topographic classification of digital image intensity surfaces using generalized splines and the discrete cosine transformation." Computer Vision, Graphics, and Image Processing 29.2 (1985): 143-167. [4] Wang, Jun, et al. "3D facial expression recognition based on primitive surface feature distribution." Computer Vision and Pattern Recognition, 2006 IEEE Computer Society Conference on. Vol. 2. IEEE, 2006.

  1. Automated analysis of art object surfaces using time-averaged digital speckle pattern interferometry

    Science.gov (United States)

    Lukomski, Michal; Krzemien, Leszek

    2013-05-01

    Technical development and practical evaluation of a laboratory built, out-of-plane digital speckle pattern interferometer (DSPI) are reported. The instrument was used for non-invasive, non-contact detection and characterization of early-stage damage, like fracturing and layer separation, of painted objects of art. A fully automated algorithm was developed for recording and analysis of vibrating objects utilizing continuous-wave laser light. The algorithm uses direct, numerical fitting or Hilbert transformation for an independent, quantitative evaluation of the Bessel function at every point of the investigated surface. The procedure does not require phase modulation and thus can be implemented within any, even the simplest, DSPI apparatus. The proposed deformation analysis is fast and computationally inexpensive. Diagnosis of physical state of the surface of a panel painting attributed to Nicolaus Haberschrack (a late-mediaeval painter active in Krakow) from the collection of the National Museum in Krakow is presented as an example of an in situ application of the developed methodology. It has allowed the effectiveness of the deformation analysis to be evaluated for the surface of a real painting (heterogeneous colour and texture) in a conservation studio where vibration level was considerably higher than in the laboratory. It has been established that the methodology, which offers automatic analysis of the interferometric fringe patterns, has a considerable potential to facilitate and render more precise the condition surveys of works of art.

  2. Surface analysis of gold nanoparticles functionalized with thiol-modified glucose SAMs for biosensor applications.

    Directory of Open Access Journals (Sweden)

    Valentina eSpampinato

    2016-02-01

    Full Text Available In this work, Time of Flight Secondary Ion Mass Spectrometry (ToF-SIMS, Principal Component Analysis (PCA and X-ray Photoelectron Spectroscopy (XPS have been used to characterize the surface chemistry of gold substrates before and after functionalization with thiol-modified glucose self-assembled monolayers and subsequent biochemical specific recognition of maltose binding protein (MBP.The results indicate that the surface functionalization is achieved both on flat and nanoparticles gold substrates thus showing the potential of the developed system as biodetection platform. Moreover, the method presented here has been found to be a sound and valid approach to characterize the surface chemistry of nanoparticles functionalized with large molecules.Both techniques were proved to be very useful tools for monitoring all the functionalization steps, including the investigation of the biological behaviour of the glucose-modified particles in presence of the maltose binding protein.

  3. Surface analysis of gold nanoparticles functionalized with thiol-modified glucose SAMs for biosensor applications.

    Science.gov (United States)

    Spampinato, Valentina; Parracino, Mariaantonietta; La Spina, Rita; Rossi, Francois; Ceccone, Giacomo

    2016-02-01

    In this work, Time of Flight Secondary Ion Mass Spectrometry (ToF-SIMS), Principal Component Analysis (PCA) and X-ray Photoelectron Spectroscopy (XPS) have been used to characterize the surface chemistry of gold substrates before and after functionalization with thiol-modified glucose self-assembled monolayers and subsequent biochemical specific recognition of maltose binding protein (MBP). The results indicate that the surface functionalization is achieved both on flat and nanoparticles gold substrates thus showing the potential of the developed system as biodetection platform. Moreover, the method presented here has been found to be a sound and valid approach to characterize the surface chemistry of nanoparticles functionalized with large molecules. Both techniques were proved to be very useful tools for monitoring all the functionalization steps, including the investigation of the biological behaviour of the glucose-modified particles in presence of the maltose binding protein.

  4. Preliminary study on the effect of heated surfaces upon bloodstain pattern analysis.

    Science.gov (United States)

    Larkin, Bethany A J; Banks, Craig E

    2013-09-01

    Bloodstain pattern analysis (BPA) involves the interpretation of distinct blood patterns found at crime scenes following a violent act. In this paper, we explored for the first time the effects of surface temperatures upon blood impacting a horizontal surface (steel) with its implications in BPA explored. Specific surface temperatures were explored over the range 24-250°C which relate to the four major boiling regimes of liquid media; natural convection, nucleate boiling, transition boiling, and film boiling, where a series of blood drops tests were performed at varying impact velocities. Blood was found to separate into its components at temperatures of 50°C+, displayed as temperature induced blood rings, where a single secondary and a series of further inner rings are exhibited. This consequently led to the development of a new constant Cd heated expressing the decrease in spread factor (D(s)/D(o)) at the secondary ring. © 2013 American Academy of Forensic Sciences.

  5. Dynamics of Plasma-Surface Interactions using In-situ Ion Beam Analysis

    International Nuclear Information System (INIS)

    Whyte, D.G.

    2009-01-01

    The overall goal of this proposal was to develop an innovative experimental facility that would allow for the measurement of real-time response of a material surface to plasma bombardment by employing in-situ high-energy ion beam analysis. This facility was successfully developed and deployed at U. Wisconsin-Madison and was named DIONISOS (Dynamics of IONic Implantation and Sputtering on Surfaces). There were several major highlights to the DIONISOS research which we will briefly highlight below. The full technical details of the DIONISOS development, deployment and research results are contained in the Appendices which contain several peer-reviewed publications and a PhD thesis devoted to DIONISOS. The DIONISOS results on deuterium retention in molybdenum were chosen as an invited talk at the 2008 International Conference on Plasma-Surface Interactions in Toledo, Spain.

  6. SEM Analysis of Residual Dentin Surface in Primary Teeth Using Different Chemomechanical Caries Removal Agents.

    Science.gov (United States)

    Thakur, Rachna; Patil, Sandya Devi S; Kush, Anil; Madhu, K

    The purpose of this in vitro study was to analyze the residual dentinal surfaces following caries removal using two chemomechanical methods (Papacarie Duo and Carie Care), by scanning electron microscopy (SEM). Twenty extracted primary molars with active occlusal carious lesions were randomly assigned two groups depending on the CMCR agent used for the caries excavation - Group 1 - with Papacarie Duo and Group - 2 with Carie Care. After the caries excavation, the specimens were subjected to SEM analysis. Though both the agents showed the minimal smear layer with the patent dentinal tubules, Carie care showed patent dentinal tubules with a clearly exposed peritubular and intertubular collagen network. Carie Care treated surface exhibited better surface morphology of residual dentin.

  7. Intercomparison and Spatiotemporal Analysis of Four Gridded Surface Air Temperature Datasets

    Science.gov (United States)

    Rao, Y.

    2016-12-01

    As one of the essential climate variables, surface air temperature (SAT) has been wildly used as the most important indicator for the global climate change. Currently, there are four widely used global SAT datasets, i.e., Berkley Earth Surface Temperature (BEST), NASA Goddard Institute of Space Sciences surface temperature (GISS), surface temperature developed by Climate Research Unit (CRU4), and NOAA Global Temperature dataset (NOAA). These four datasets are developed using similar source data (station measured air temperature for land and buoys/ships measured sea surface temperature). Previous studies suggested that global and hemispheric average SAT anomalies of these datasets have shown consistent surface warming trends. However, it is not clear how these four datasets compare with each other at grid scale (e.g., 5 degree) and what impacts are for the spatial patterns of estimated surface warming trends. In this study, a direct comparison for temperature anomalies at grid box scale shows that NOAA are consistently cooler than other three datasets across most grids over the land while GISS and BEST tend to be warmer than others over northern mid to high latitude land regions, Australia, southern Africa and South America. The differences are most notable over regions with sparse measurements such as Amazon region, north and central Africa, central Asia, Greenland, central Australia and Antarctic. Moreover, trend analysis (both linear and nonlinear) has been carried out using these four gridded datasets (1950-2015) separately. The result show a similar spatial pattern with previous comparison--notable differences for regions with sparse observations. Additionally, three leading modes from EOF analysis have also been compared to examine how they could capture the climate variability. The comparison results suggested that these datasets show notable differences in both spatial pattern and temporal trend in the leading modes. This inconsistency may lead to large

  8. "Jag känner inte för att bli en ... kille" Om heteronormativitet i ämnet idrott och hälsa

    Directory of Open Access Journals (Sweden)

    Håkan Larsson

    2007-01-01

    Full Text Available ”I don’t feel like being a ... boy.” On heteronormativity in physicaleducation. This article concerns gender, sexuality and heteronormativity inphysical education (PE. The aim is to elucidate girls’ and boys’ conditionsin relation to the heteronormative culture of the school subject. 24 pupilsin grade 8 and 9 were interviewed about their view on PE and on girls andboys in PE. A discourse analysis of the interviews was conducted, aiming atpinpointing the discursive rules as to how girls and boys can act as ‘normal’in PE teaching. The analysis shows how different kinds of activities, notablydance and ball games, subjectify girls and boys in different ways. In order to actas ‘normal’, girls and boys seem to have to conform to a heterosexual matrix.This means that boys might be viewed as queer should they be skilled dancers,and conversely that girls might be viewed as queer should they be skilled ballplayers. Every attempt to challenge the gender order in PE, must also be anattempt to challenge the heteronormative culture of the school subject.

  9. Analytical Round Robin for Elastic-Plastic Analysis of Surface Cracked Plates: Phase I Results

    Science.gov (United States)

    Wells, D. N.; Allen, P. A.

    2012-01-01

    An analytical round robin for the elastic-plastic analysis of surface cracks in flat plates was conducted with 15 participants. Experimental results from a surface crack tension test in 2219-T8 aluminum plate provided the basis for the inter-laboratory study (ILS). The study proceeded in a blind fashion given that the analysis methodology was not specified to the participants, and key experimental results were withheld. This approach allowed the ILS to serve as a current measure of the state of the art for elastic-plastic fracture mechanics analysis. The analytical results and the associated methodologies were collected for comparison, and sources of variability were studied and isolated. The results of the study revealed that the J-integral analysis methodology using the domain integral method is robust, providing reliable J-integral values without being overly sensitive to modeling details. General modeling choices such as analysis code, model size (mesh density), crack tip meshing, or boundary conditions, were not found to be sources of significant variability. For analyses controlled only by far-field boundary conditions, the greatest source of variability in the J-integral assessment is introduced through the constitutive model. This variability can be substantially reduced by using crack mouth opening displacements to anchor the assessment. Conclusions provide recommendations for analysis standardization.

  10. THE TIBIAL APERTURE SURFACE ANALYSIS IN ANTERIOR CRUCIATE LIGAMENT RECONSTRUCTION PROCESS.

    Science.gov (United States)

    Milojević, Zoran; Tabaković, Slobodan; Vićević, Marija; Obradović, Mirko; Vranjes, Miodrag; Milankov, Miroslav Z

    2016-01-01

    The tibial tunnel aperture in the anterior cruciate ligament reconstruction is usually analyzed as an ellipse, generated as an intersection between a tibial plateau and a tibial bone tunnel. The aim of this study is to show that the tibial tunnel aperture, which utilizes 3D tibial surface bone model, differs significantly from common computations which present the tibial tunnel anterior cruciate ligament aperture surface as an ellipse. An interactive program system was developed for the tibial tunnel aperture analysis which included the real tibia 3D surface bone model generated from a series of computed tomography images of ten male patients, their mean age being 25 years. In aperture calculation, the transverse drill angle of 10 degrees was used, whereas sagittal drill angles of 40 degrees, 50 degrees and 60 degrees were used with the drill-bit diameter set to 10 mm. The real 3D and 2D tibial tunnel aperture surface projection was calculated and compared with an ellipse. According to the calculations, generated 3D aperture surfaces were different for every patient even though the same drill parameters were used. For the sagittal drill angles of 40 degrees, 50 degrees and 60 degrees, the mean difference between the projected 3D and 2D area on the tibial plateau was 19.6 +/- 5.4%, 21.1 +/- 8.0% and 21.3 +/- 9.6%, respectively. The difference between the projected 3D area on the tibial plateau and ellipse surface was 54.8 +/- 16.3%, 39.6 +/- 10.4% and 25.0 +/- 8.0% for sagittal drill angles of 40 degrees, 50 degrees and 60 degrees, respectively. The tibial tunnel aperture surface area differs significantly from the ellipse surface area, which is commonly used in the anterior cruciate ligament reconstruction analysis. Inclusion of the 3D shape of the tibial attachment site in the preoperative anterior cruciate ligament reconstruction planning process can lead to a more precise individual anatomic anterior cruciate ligament reconstruction on the tibial bone. Both

  11. Analysis of cutting force signals by wavelet packet transform for surface roughness monitoring in CNC turning

    Science.gov (United States)

    García Plaza, E.; Núñez López, P. J.

    2018-01-01

    On-line monitoring of surface finish in machining processes has proven to be a substantial advancement over traditional post-process quality control techniques by reducing inspection times and costs and by avoiding the manufacture of defective products. This study applied techniques for processing cutting force signals based on the wavelet packet transform (WPT) method for the monitoring of surface finish in computer numerical control (CNC) turning operations. The behaviour of 40 mother wavelets was analysed using three techniques: global packet analysis (G-WPT), and the application of two packet reduction criteria: maximum energy (E-WPT) and maximum entropy (SE-WPT). The optimum signal decomposition level (Lj) was determined to eliminate noise and to obtain information correlated to surface finish. The results obtained with the G-WPT method provided an in-depth analysis of cutting force signals, and frequency ranges and signal characteristics were correlated to surface finish with excellent results in the accuracy and reliability of the predictive models. The radial and tangential cutting force components at low frequency provided most of the information for the monitoring of surface finish. The E-WPT and SE-WPT packet reduction criteria substantially reduced signal processing time, but at the expense of discarding packets with relevant information, which impoverished the results. The G-WPT method was observed to be an ideal procedure for processing cutting force signals applied to the real-time monitoring of surface finish, and was estimated to be highly accurate and reliable at a low analytical-computational cost.

  12. An Integrated Transcriptome-Wide Analysis of Cave and Surface Dwelling Astyanax mexicanus

    Science.gov (United States)

    Gross, Joshua B.; Furterer, Allison; Carlson, Brian M.; Stahl, Bethany A.

    2013-01-01

    Numerous organisms around the globe have successfully adapted to subterranean environments. A powerful system in which to study cave adaptation is the freshwater characin fish, Astyanax mexicanus. Prior studies in this system have established a genetic basis for the evolution of numerous regressive traits, most notably vision and pigmentation reduction. However, identification of the precise genetic alterations that underlie these morphological changes has been delayed by limited genetic and genomic resources. To address this, we performed a transcriptome analysis of cave and surface dwelling Astyanax morphs using Roche/454 pyrosequencing technology. Through this approach, we obtained 576,197 Pachón cavefish-specific reads and 438,978 surface fish-specific reads. Using this dataset, we assembled transcriptomes of cave and surface fish separately, as well as an integrated transcriptome that combined 1,499,568 reads from both morphotypes. The integrated assembly was the most successful approach, yielding 22,596 high quality contiguous sequences comprising a total transcriptome length of 21,363,556 bp. Sequence identities were obtained through exhaustive blast searches, revealing an adult transcriptome represented by highly diverse Gene Ontology (GO) terms. Our dataset facilitated rapid identification of sequence polymorphisms between morphotypes. These data, along with positional information collected from the Danio rerio genome, revealed several syntenic regions between Astyanax and Danio. We demonstrated the utility of this positional information through a QTL analysis of albinism in a surface x Pachón cave F2 pedigree, using 65 polymorphic markers identified from our integrated assembly. We also adapted our dataset for an RNA-seq study, revealing many genes responsible for visual system maintenance in surface fish, whose expression was not detected in adult Pachón cavefish. Conversely, several metabolism-related genes expressed in cavefish were not detected in

  13. Numerical analysis of high-speed liquid lithium free-surface flow

    Energy Technology Data Exchange (ETDEWEB)

    Gordeev, Sergej, E-mail: sergej.gordeev@kit.edu [Institute for Neutron Physics and Reactor Technology, Karlsruhe Institute for Technology-Campus North, Post box 3640, Hermann v. Helmholtz Platz 1, D76344 Eggenstein (Germany); Heinzel, Volker; Stieglitz, Robert [Institute for Neutron Physics and Reactor Technology, Karlsruhe Institute for Technology-Campus North, Post box 3640, Hermann v. Helmholtz Platz 1, D76344 Eggenstein (Germany)

    2012-08-15

    Highlights: Black-Right-Pointing-Pointer The free surface behavior of a high speed lithium jet is investigated by means of a CFD LES analysis. Black-Right-Pointing-Pointer The study is aiming to validate adequate LES technique. Black-Right-Pointing-Pointer The Osaka University experiments with liquid lithium jet have been simulated. Black-Right-Pointing-Pointer Four cases with jet flow velocities of 4, 9, 13 and 15 m/s are analyzed. Black-Right-Pointing-Pointer Calculation results show a good qualitative and a quantitative agreement with the experimental data. - Abstract: The free-surface stability of the target of the International Fusion Material Irradiation Facility (IFMIF) is one of the crucial issues, since the spatio-temporal behavior of the free-surface determines the neutron flux to be generated. This article investigates the relation between the evolution of a wall boundary layer in a convergent nozzle and the free surface shape of a high speed lithium jet by means of a CFD LES analysis using the Osaka University experiments. The study is aiming to validate adequate LES technique to analyze the individual flow phenomena observed. Four cases with jet flow velocities of 4, 9, 13 and 15 m/s are analyzed. First analyses of calculation results show that the simulation exhibits a good qualitative and a quantitative agreement with the experimental data, which allows in the future a more realistic prediction of the IFMIF target behavior.

  14. A semi-analytical decomposition analysis of surface plasmon generation and the optimal nanoledge plasmonic device.

    Science.gov (United States)

    Zeng, Zheng; Mendis, Madu N; Waldeck, David H; Wei, Jianjun

    Surface plasmon resonance (SPR) of nanostructured thin metal films (so-called nanoplasmonics) has attracted intense attention due to its versatility for optical sensing and chip-based device integration. Understanding the underlying physics and developing applications of nanoplasmonic devices with desirable optical properties, e.g. intensity of light scattering and high refractive index (RI) sensitivity at the perforated metal film, is crucial for practical uses in physics, biomedical detection, and environmental monitoring. This work presents a semi-analytical model that enables decomposition and quantitative analysis of surface plasmon generation at a new complex nanoledge aperture structure under plane-wave illumination, thus providing insight on how to optimize plasmonic devices for optimal plasmonic generation efficiencies and RI sensitivity. A factor analysis of parameters (geometric, dielectric-RI, and incident wavelength) relevant to surface plasmon generation is quantitatively investigated to predict the surface plasmon polariton (SPP) generation efficiency. In concert with the analytical treatment, a finite-difference time-domain (FDTD) simulation is used to model the optical transmission spectra and RI sensitivity as a function of the nanoledge device's geometric parameters, and it shows good agreement with the analytical model. Further validation of the analytical approach is provided by fabricating subwavelength nanoledge devices and testing their optical transmission and RI sensitivity.

  15. Automatic analysis of image of surface structure of cell wall-deficient EVC.

    Science.gov (United States)

    Li, S; Hu, K; Cai, N; Su, W; Xiong, H; Lou, Z; Lin, T; Hu, Y

    2001-01-01

    Some computer applications for cell characterization in medicine and biology, such as analysis of surface structure of cell wall-deficient EVC (El Tor Vibrio of Cholera), operate with cell samples taken from very small areas of interest. In order to perform texture characterization in such an application, only a few texture operators can be employed: the operators should be insensitive to noise and image distortion and be reliable in order to estimate texture quality from images. Therefore, we introduce wavelet theory and mathematical morphology to analyse the cellular surface micro-area image obtained by SEM (Scanning Electron Microscope). In order to describe the quality of surface structure of cell wall-deficient EVC, we propose a fully automatic computerized method. The image analysis process is carried out in two steps. In the first, we decompose the given image by dyadic wavelet transform and form an image approximation with higher resolution, by doing so, we perform edge detection of given images efficiently. In the second, we introduce many operations of mathematical morphology to obtain morphological quantitative parameters of surface structure of cell wall-deficient EVC. The obtained results prove that the method can eliminate noise, detect the edge and extract the feature parameters validly. In this work, we have built automatic analytic software named "EVC.CELL".

  16. Numerical analysis of high-speed liquid lithium free-surface flow

    International Nuclear Information System (INIS)

    Gordeev, Sergej; Heinzel, Volker; Stieglitz, Robert

    2012-01-01

    Highlights: ► The free surface behavior of a high speed lithium jet is investigated by means of a CFD LES analysis. ► The study is aiming to validate adequate LES technique. ► The Osaka University experiments with liquid lithium jet have been simulated. ► Four cases with jet flow velocities of 4, 9, 13 and 15 m/s are analyzed. ► Calculation results show a good qualitative and a quantitative agreement with the experimental data. - Abstract: The free-surface stability of the target of the International Fusion Material Irradiation Facility (IFMIF) is one of the crucial issues, since the spatio-temporal behavior of the free-surface determines the neutron flux to be generated. This article investigates the relation between the evolution of a wall boundary layer in a convergent nozzle and the free surface shape of a high speed lithium jet by means of a CFD LES analysis using the Osaka University experiments. The study is aiming to validate adequate LES technique to analyze the individual flow phenomena observed. Four cases with jet flow velocities of 4, 9, 13 and 15 m/s are analyzed. First analyses of calculation results show that the simulation exhibits a good qualitative and a quantitative agreement with the experimental data, which allows in the future a more realistic prediction of the IFMIF target behavior.

  17. Surface characterization and cytotoxicity analysis of plasma sprayed coatings on titanium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Rahman, Zia ur; Shabib, Ishraq [School of Engineering and Technology, Central Michigan University, Mount Pleasant, MI 48859 (United States); Science of Advanced Materials, Central Michigan University, Mount Pleasant, MI 48859 (United States); Haider, Waseem, E-mail: haide1w@cmich.edu [School of Engineering and Technology, Central Michigan University, Mount Pleasant, MI 48859 (United States); Science of Advanced Materials, Central Michigan University, Mount Pleasant, MI 48859 (United States)

    2016-10-01

    In the realm of biomaterials, metallic materials are widely used for load bearing joints due to their superior mechanical properties. Despite the necessity for long term metallic implants, there are limitations to their prolonged use. Naturally, oxides of titanium have low solubilities and form passive oxide film spontaneously. However, some inclusion and discontinuity spots in oxide film make implant to adopt the decisive nature. These defects heighten the dissolution of metal ions from the implant surface, which results in diminishing bio-integration of titanium implant. To increase the long-term metallic implant stability, surface modifications of titanium alloys are being carried out. In the present study, biomimetic coatings of plasma sprayed hydroxyapatite and titanium were applied to the surface of commercially pure titanium and Ti6Al4V. Surface morphology and surface chemistry were studied using scanning electron microscopy and X-ray photoelectron spectroscopy, respectively. Cyclic potentiodynamic polarization and electrochemical impedance spectroscopy were carried out in order to study their electrochemical behavior. Moreover, cytotoxicity analysis was conducted for osteoblast cells by performing MTS assay. It is concluded that both hydroxyapatite and titanium coatings enhance corrosion resistance and improve cytocompatibility. - Highlights: • Surface morphology and surface chemistry were studied using scanning electron microscopy and X-ray photoelectron spectroscopy. • The cyclic polarization tests revealed noticeable improvement towards the positive potentials for both Tip coatings. • CpTi-Hap and Ti6Al4V-Hap both demonstrate similar corrosion rate. • High cytotoxicity was observed for Mp when compared with Tip and Hap after 21 days of immersion. • Both Tip and Hap coatings promoted the osteoblast cell adhesion and exhibited stellar morphology.

  18. AFM Surface Roughness and Topography Analysis of Lithium Disilicate Glass Ceramic

    Directory of Open Access Journals (Sweden)

    M. Pantić

    2015-12-01

    Full Text Available The aim of this study is presenting AFM analysis of surface roughness of Lithium disilicate glass ceramic (IPS e.max CAD under different finishing procedure (techniques: polishing, glazing and grinding. Lithium disilicate glass ceramics is all-ceramic dental system which is characterized by high aesthetic quality and it can be freely said that properties of material provide all prosthetic requirements: function, biocompatibility and aesthetic. Experimental tests of surface roughness were investigated on 4 samples with dimensions: 18 mm length, 14 mm width and 12 mm height. Contact surfaces of three samples were treated with different finishing procedure (polishing, glazing and grinding, and the contact surface of the raw material is investigated as a fourth sample. Experimental measurements were done using the Atomic Force Microscopy (AFM of NT-MDT manufacturers, in the contact mode. All obtained results of different prepared samples are presented in the form of specific roughness parameters (Rа, Rz, Rmax, Rq and 3D surface topography.

  19. Mitigating the surface urban heat island: Mechanism study and sensitivity analysis

    Science.gov (United States)

    Meng, Chunlei

    2017-08-01

    In a surface urban heat island (SUHI), the urban land surface temperature (LST) is usually higher than the temperature of the surrounding rural areas due to human activities and surface characteristics. Because a SUHI has many adverse impacts on urban environment and human health, SUHI mitigation strategies are very important. This paper investigates the mechanism of a SUHI based on the basic physical laws that control the formation of a SUHI; five mitigation strategies are proposed, namely: sprinkling and watering; paving a pervious surface; reducing the anthropogenic heat (AH) release; using a "white roof"; increasing the fractional vegetation cover or leaf area index (LAI). To quantify the effect of these mitigation strategies, 26 sets of experiments are designed and implemented by running the integrated urban land model (IUM). The results of the sensitivity analysis indicate that sprinkling and watering is an effective measure for mitigating a SUHI for an entire day. Decreasing the AH release is also useful for both night- and daytime SUHI mitigation; however, the cooling extent is proportional to the diurnal cycle of AH. Increasing the albedo can reduce the LST in the daytime, especially when the solar radiation is significant; the cooling extent is approximately proportional to the diurnal cycle of the net radiation. Increasing the pervious surface percentage can mitigate the SUHI especially in the daytime. Increasing the fractional vegetation cover can mitigate the SUHI in the daytime but may aggravate the SUHI at night.

  20. Objective analysis of surface wind regimes over Israel using self-organizing maps

    Science.gov (United States)

    Berkovic, Sigalit

    2017-04-01

    The surface wind across Israel is studied using the method of Self Organizing maps (SOMs). Emphasis is made on identifying the characteristic diurnal patterns at the synoptic hours during the winter months. The investigation is made by analyzing surface wind measurements from 53 Israel Meteorological Service (IMS) stations during 2006-2012. The relation between surface wind patterns and synoptic variables (temperature, specific humidity, geopotential height and synoptic wind) is obtained from calculation of averages of these variables according to the surface wind SOMs classification. The synoptic data is derived from ECMWF ERA40 data. Under winter lows the flow over Israel is westerly with high steadiness (>0.8) and intensity (4-10 m/s). Under winter highs the flow over northern Israel is easterly with high steadiness (>0.8) and intensity. Wind intensity is proportional to the pressure gradient. Under transitional pressure gradients, the flow is determined by the local topography and the diurnal heating, its steadiness is relatively low and its intensity weakens. The wind regimes are in agreement with previous subjective and semi-objective classification studies of surface flow under the frequent synoptic classes. The ability to reconstruct subjective knowledge by an objective algorithm is crucial for future statistical climatological analysis and applications over Israel.

  1. XPS analysis of the carbon fibers surface modified via HMDSO to carbon nanotube growth

    Energy Technology Data Exchange (ETDEWEB)

    Cardoso, L.D.R.; Gomes, M.C.B.; Trava-Airoldi, V.J.; Corat, E.J.; Lugo, D.C. [Instituto Nacional de Pesquisas Espaciais (INPE), Sao Jose dos Campos, SP (Brazil)

    2016-07-01

    Full text: Carbon fibers (CF) have been widely used to reinforce structural composites. Due to their strength-to-weight properties, CF composites are finding increased structural uses in areas such as aerospace, aeronautical, automobile and others. The strength of the fiber-resin interface bond has been found to be the limiting factor to the mechanical properties of CF-epoxy materials, due to their non-polar nature that limit the affinity of CF to bind chemically to any matrix. The growth of carbon nanotubes (CNTs) on the surface of CF is a promising approach for improving mechanical, electrical and thermal properties of structural composites. However growing CNTs on CF presents some obstacles, such as diffusion of metal catalyst particles on CF, uneven CNT growth and loss of mechanical properties of CF. To avoid the diffusion of catalyst particles we modified the CF surface with hexamethyldisiloxane (HMDSO) at low temperature (400 °C), also preventing the loss of mechanical properties and allowing uniform CNTs growth. We deposited CNTs via floating catalyst method, with ferrocene providing the catalyst particle and the oxidative dehydrogenation reaction of acetylene providing the carbon. The CF surface modification was analyzed via X-ray photoelectron spectroscopy (XPS) and CNTs growth via scanning electron microscopy with field emission gun. The XPS analysis showed that HMDSO promotes the binding of oxygen to carbon and silicon present on CF surface, the chemical modification of the surface of the CF enables the uniform growth of carbon nanotubes. (author)

  2. XPS analysis of the carbon fibers surface modified via HMDSO to carbon nanotube growth

    International Nuclear Information System (INIS)

    Cardoso, L.D.R.; Gomes, M.C.B.; Trava-Airoldi, V.J.; Corat, E.J.; Lugo, D.C.

    2016-01-01

    Full text: Carbon fibers (CF) have been widely used to reinforce structural composites. Due to their strength-to-weight properties, CF composites are finding increased structural uses in areas such as aerospace, aeronautical, automobile and others. The strength of the fiber-resin interface bond has been found to be the limiting factor to the mechanical properties of CF-epoxy materials, due to their non-polar nature that limit the affinity of CF to bind chemically to any matrix. The growth of carbon nanotubes (CNTs) on the surface of CF is a promising approach for improving mechanical, electrical and thermal properties of structural composites. However growing CNTs on CF presents some obstacles, such as diffusion of metal catalyst particles on CF, uneven CNT growth and loss of mechanical properties of CF. To avoid the diffusion of catalyst particles we modified the CF surface with hexamethyldisiloxane (HMDSO) at low temperature (400 °C), also preventing the loss of mechanical properties and allowing uniform CNTs growth. We deposited CNTs via floating catalyst method, with ferrocene providing the catalyst particle and the oxidative dehydrogenation reaction of acetylene providing the carbon. The CF surface modification was analyzed via X-ray photoelectron spectroscopy (XPS) and CNTs growth via scanning electron microscopy with field emission gun. The XPS analysis showed that HMDSO promotes the binding of oxygen to carbon and silicon present on CF surface, the chemical modification of the surface of the CF enables the uniform growth of carbon nanotubes. (author)

  3. Mini-implants for Orthodontic Anchorage: Surface Analysis after Redrilling and Sterilization - An in vitro Study.

    Science.gov (United States)

    Gross, J M; Nascimento, G G; Araújo, V C; Bönecker, Mjs; Furuse, C

    2016-04-01

    This study aimed to investigate, in vitro, possible alterations on mini-implants surface after retrieval and if the cleaning process and sterilization can predispose damages. Two commercial mini-implants were tested for deformations after drilling and removing in artificial bone four times. Samples were analyzed by scanning electron microscopy, and surface alterations verified through thread and pitches deformation. To alterations caused by insertion/removal and the cleaning process and sterilization were verified in different procedures: Insertions and sterilization, only insertions, and only sterilization. Photomicrographs were analyzed in order to compare the surface characteristics. Head deformation was verified qualitatively. For a quantitative analysis, distances between threads were measured across the active part of the mini-implants. No deformation was observed in both groups. The cleaning and sterilization processes did not provoke alteration in both groups. Nevertheless, the presence of synthetic bone was noted in some samples. The mean distances between implant threads were similar after all steps in all regions in both groups. The results suggest that the tested mini-implants can be retrieved without damage of its surface after four cycles of insertion, removal, and sterilization. Orthodontic mini-implant, Redrilling, Sterilization. Mini-implants can be retrieved without damage to its surface after four cycles of insertion, removal, and sterilization in the same patient without representing a biological concern.

  4. Identification of soil erosion land surfaces by Landsat data analysis and processing

    International Nuclear Information System (INIS)

    Lo Curzio, S.

    2009-01-01

    In this paper, we outline the typical relationship between the spectral reflectance of aileron's on newly-formed land surfaces and the geo morphological features of the land surfaces at issue. These latter represent the products of superficial erosional processes due to the action of the gravity and/or water; thus, such land surfaces are highly representative of the strong soil degradation occurring in a wide area located on the boundary between Molise and Puglia regions (Southern Italy). The results of this study have been reported on thematic maps; on such maps, the detected erosional land surfaces have been mapped on the basis of their typical spectral signature. The study has been performed using Landsat satellite imagery data which have been then validated by means of field survey data. The satellite data have been processed using remote sensing techniques, such as: false colour composite, contrast stretching, principal component analysis and decorrelation stretching. The study has permitted to produce, in a relatively short time and at low expense, a map of the eroded land surfaces. Such a result represents a first and fundamental step in evaluating and monitoring the erosional processes in the study area [it

  5. Acute and subchronic toxicity analysis of surface modified paclitaxel attached hydroxyapatite and titanium dioxide nanoparticles.

    Science.gov (United States)

    Venkatasubbu, Gopinath Devanand; Ramasamy, S; Gaddam, Pramod Reddy; Kumar, J

    2015-01-01

    Nanoparticles are widely used for targeted drug delivery applications. Surface modification with appropriate polymer and ligands is carried out to target the drug to the affected area. Toxicity analysis is carried out to evaluate the safety of the surface modified nanoparticles. In this study, paclitaxel attached, folic acid functionalized, polyethylene glycol modified hydroxyapatite and titanium dioxide nanoparticles were used for targeted drug delivery system. The toxicological behavior of the system was studied in vivo in rats and mice. Acute and subchronic studies were carried out. Biochemical, hematological, and histopathological analysis was also done. There were no significant alterations in the biochemical parameters at a low dosage. There was a small change in alkaline phosphatase (ALP) level at a high dosage. The results indicate a safe toxicological profile.

  6. Support surface interface pressure, microenvironment, and the prevalence of pressure ulcers: an analysis of the literature.

    Science.gov (United States)

    Reger, Steven I; Ranganathan, Vinoth K; Sahgal, Vinod

    2007-10-01

    External pressure is the most frequently considered stress factor in the formation of ulcers. A review and analysis of existing literature addressing the relationship between pressure ulcer prevalence and interface pressures at various anatomic sites was conducted. Results suggest a nearly non-existent or slightly negative correlation between interface pressure and ulcer prevalence in general and spinal cord injured populations, respectively. Despite limitations of the analysis methods used, the observed lack of a direct relationship confirms the results of other studies and suggests that ulcer formation also may involve factors secondary to pressure and mechanical factors (eg, temperature, moisture, duration of the applied load, atrophy, and posture). Based on currently available information, clinicians should include these considerations when selecting a support surface. Studies directly relating primary stress factors and tissue viability with prevalence and incidence of pressure ulcers are needed to better understand the benefits of pressure-relieving support surfaces and to improve the effectiveness of prevention and treatment.

  7. Acute and subchronic toxicity analysis of surface modified paclitaxel attached hydroxyapatite and titanium dioxide nanoparticles

    Science.gov (United States)

    Venkatasubbu, Gopinath Devanand; Ramasamy, S; Gaddam, Pramod Reddy; Kumar, J

    2015-01-01

    Nanoparticles are widely used for targeted drug delivery applications. Surface modification with appropriate polymer and ligands is carried out to target the drug to the affected area. Toxicity analysis is carried out to evaluate the safety of the surface modified nanoparticles. In this study, paclitaxel attached, folic acid functionalized, polyethylene glycol modified hydroxyapatite and titanium dioxide nanoparticles were used for targeted drug delivery system. The toxicological behavior of the system was studied in vivo in rats and mice. Acute and subchronic studies were carried out. Biochemical, hematological, and histopathological analysis was also done. There were no significant alterations in the biochemical parameters at a low dosage. There was a small change in alkaline phosphatase (ALP) level at a high dosage. The results indicate a safe toxicological profile. PMID:26491315

  8. Low-energy ion-beam deposition apparatus equipped with surface analysis system

    International Nuclear Information System (INIS)

    Ohno, Hideki; Aoki, Yasushi; Nagai, Siro.

    1994-10-01

    A sophisticated apparatus for low energy ion beam deposition (IBD) was installed at Takasaki Radiation Chemistry Research Establishment of JAERI in March 1991. The apparatus is composed of an IBD system and a real time/in-situ surface analysis system for diagnosing deposited thin films. The IBD system provides various kinds of low energy ion down to 10 eV with current density of 10 μA/cm 2 and irradiation area of 15x15 mm 2 . The surface analysis system consists of RHEED, AES, ISS and SIMS. This report describes the characteristics and the operation procedure of the apparatus together with some experimental results on depositing thin carbon films. (author)

  9. An in situ-satellite blended analysis of global sea surface salinity

    Science.gov (United States)

    Xie, P.; Boyer, T.; Bayler, E.; Xue, Y.; Byrne, D.; Reagan, J.; Locarnini, R.; Sun, F.; Joyce, R.; Kumar, A.

    2014-09-01

    The blended monthly sea surface salinity (SSS) analysis, called the NOAA "Blended Analysis of Surface Salinity" (BASS), is constructed for the 4 year period from 2010 to 2013. Three data sets are employed as inputs to the blended analysis: in situ SSS measurements aggregated and quality controlled by NOAA/NODC, and passive microwave (PMW) retrievals from both the National Aeronautics and Space Administration's (NASA) Aquarius/SAC-D and the European Space Agency's (ESA) Soil Moisture-Ocean Salinity (SMOS) satellites. The blended analysis comprises two steps. First, the biases in the satellite retrievals are removed through probability distribution function (PDF) matching against temporally spatially colocated in situ measurements. The blended analysis is then achieved through optimal interpolation (OI), where the analysis for the previous time step is used as the first guess while the in situ measurements and bias-corrected satellite retrievals are employed as the observations to update the first guess. Cross validations illustrate improved quality of the blended analysis, with reduction in bias and random errors over most of the global oceans as compared to the individual inputs. Large uncertainty, however, remains in high-latitude oceans and coastal regions where the in situ networks are sparse and current-generation satellite retrievals have limitations. Our blended SSS analysis shows good agreements with the NODC in situ-based analysis over most of the tropical and subtropical oceans, but large differences are observed for high-latitude oceans and along coasts. In the tropical oceans, the BASS is shown to have coherent variability with precipitation and evaporation associated with the evolution of the El Niño-Southern Oscillation (ENSO).

  10. A cost and operational effectiveness analysis of alternative anti-surface warfare platforms

    OpenAIRE

    Skinner, Walter Mark.

    1993-01-01

    Approved for public release; distribution is unlimited. A Cost and Operational Effectiveness Analysis (COEA) is performed for three alternative anti-surface warfare (ASUW) platforms that will conduct operations in multi-service regional scenarios. Estimated program costs, historical cost variances, and measures of operational effectiveness are determined for each COEA alternative, and service life extension effects are examined. The data is merged in a mixed-integer optimization model, MPA...

  11. Ambient mass spectrometry: From the planar to the non-planar surface analysis

    Czech Academy of Sciences Publication Activity Database

    Rejšek, Jan; Vrkoslav, Vladimír; Cvačka, Josef

    2017-01-01

    Roč. 15, č. 1 (2017), s. 31 ISSN 2336-7202. [Mezioborové setkání mladých biologů, biochemiků a chemiků /17./. 30.05.2017-01.06.2017, Milovy] Institutional support: RVO:61388963 Keywords : ambient mass spectrometry * thin layer chromatography * non-planar surface analysis Subject RIV: CB - Analytical Chemistry, Separation

  12. Active tectonics revealed by isobase surfaces analysis from South Rifian Ridges, Northern Morocco

    OpenAIRE

    Amine, Afaf; El Ouardi, Hmidou

    2017-01-01

    The analysis of isobase maps, as one of surface dynamic parameters , helps understanding the tectonic geomorphology of South Rifian Ridges, Northern Morocco . The automatic generation of morphostructural map of 2nd and 3rd order channels is based on 30-grid Digital Elevation Modelin to Geographic Information System environment presents good results, supporting previous studies. Comparing to the western ridges, the eastern ones, specially Moulay Idriss massif, evidence neotectonic activity tri...

  13. Sensitivity analysis of the surface water- groundwater interaction for the sandy area of the Netherlands

    OpenAIRE

    Gomez del Campo, E.; Jousma, G.; Massop, H.T.L.

    1993-01-01

    The "Sensitivity Analysis of the Surface Water- Groundwater Interaction for the Sandy Area of the Netherlands" was carried out in the framework of a bilateral research project in support of the implementation of a nationwide geohydrological information system (REGIS) in the Netherlands. This project, conducted in cooperation between the TNO Institute for Applied Scientific Research (IGG-TNO) and !he Winand Staring Centre for Integrated Land, Soil and Water Research (SC-DLO), is aimed at defin...

  14. Accuracy Analysis of a Robotic Radionuclide Inspection and Mapping System for Surface Contamination

    International Nuclear Information System (INIS)

    Mauer, Georg F.; Kawa, Chris

    2008-01-01

    The mapping of localized regions of radionuclide contamination in a building can be a time consuming and costly task. Humans moving hand-held radiation detectors over the target areas are subject to fatigue. A contamination map based on manual surveys can contain significant operator-induced inaccuracies. A Fanuc M16i light industrial robot has been configured for installation on a mobile aerial work platform, such as a tall forklift. When positioned in front of a wall or floor surface, the robot can map the radiation levels over a surface area of up to 3 m by 3 m. The robot's end effector is a commercial alpha-beta radiation sensor, augmented with range and collision avoidance sensors to ensure operational safety as well as to maintain a constant gap between surface and radiation sensors. The accuracy and repeatability of the robotically conducted contamination surveys is directly influenced by the sensors and other hardware employed. This paper presents an in-depth analysis of various non-contact sensors for gap measurement, and the means to compensate for predicted systematic errors that arise during the area survey scans. The range sensor should maintain a constant gap between the radiation counter and the surface being inspected. The inspection robot scans the wall surface horizontally, moving down at predefined vertical intervals after each scan in a meandering pattern. A number of non-contact range sensors can be employed for the measurement of the gap between the robot end effector and the wall. The nominal gap width was specified as 10 mm, with variations during a single scan not to exceed ± 2 mm. Unfinished masonry or concrete walls typically exhibit irregularities, such as holes, gaps, or indentations in mortar joints. These irregularities can be sufficiently large to indicate a change of the wall contour. The responses of different sensor types to the wall irregularities vary, depending on their underlying principles of operation. We explored

  15. Fatigue crack growth and fracture mechanics analysis of a working roll surface layer material

    Directory of Open Access Journals (Sweden)

    M. Drobne

    2014-10-01

    Full Text Available Fatigue crack growth and fracture mechanics analysis of a working roll surface layer material is presented in this paper. The research is done on a hot strip mill working roll where High Chromium Steel is used for roll’s shell material. To obtain corresponding parameters, a rectangular single edge notched bend specimens – SENB, according to standard BS 7448, were used. The fatigue crack growth analysis was done on a resonant testing machine with use of special crack gauges, while for fracture mechanics parameters the electro–mechanical testing machine was used.

  16. In situ surface enhanced resonance Raman scattering analysis of a reactive dye covalently bound to cotton.

    Science.gov (United States)

    White, P C; Munro, C H; Smith, W E

    1996-06-01

    An in situ surface enhanced resonance Raman scattering (SERRS) procedure is described for the analysis of a reactive dye covalently bound to a single strand of a cotton fibre. This procedure can be completed in 5 h, whereas an alternative enzyme digestion method takes approximately 21 h. These two fibre preparation methods give similar spectra from picogram quantities of dye present on a 2-5 mm length of fibre. The in situ nature of the analysis and the small sample size make this method particularly suitable for forensic applications.

  17. Surface analysis of Al alloys with X-ray photoelectron and Auger electron spectroscopies

    International Nuclear Information System (INIS)

    Sakairi, Masatoshi; Suzuki, Keita; Sasaki, Ryo

    2015-01-01

    In this paper, X-ray photoelectron spectroscopy (XPS) and Auger electron spectroscopy (AES) were applied to investigate passive films formed on aluminum alloy in 0.5 kmol m -3 H 3 BO 3 /0.05 kmol m -3 Na 2 B 4 O 7 with different metal cations. The metal cation is classified by metal cation hardness, X, which are calculated based on the concept of hard and soft acids and bases (HSAB) of the acid and base in Lewis's rule. From XPS analysis, the metal cations with X > 4 were incorporated in passive films. The area-selected surface analysis of AES was also introduced. (author)

  18. Multispectral UV imaging for surface analysis of MUPS tablets with special focus on the pellet distribution.

    Science.gov (United States)

    Novikova, Anna; Carstensen, Jens M; Rades, Thomas; Leopold, Prof Dr Claudia S

    2016-12-30

    In the present study the applicability of multispectral UV imaging in combination with multivariate image analysis for surface evaluation of MUPS tablets was investigated with respect to the differentiation of the API pellets from the excipients matrix, estimation of the drug content as well as pellet distribution, and influence of the coating material and tablet thickness on the predictive model. Different formulations consisting of coated drug pellets with two coating polymers (Aquacoat ® ECD and Eudragit ® NE 30 D) at three coating levels each were compressed to MUPS tablets with various amounts of coated pellets and different tablet thicknesses. The coated drug pellets were clearly distinguishable from the excipients matrix using a partial least squares approach regardless of the coating layer thickness and coating material used. Furthermore, the number of the detected drug pellets on the tablet surface allowed an estimation of the true drug content in the respective MUPS tablet. In addition, the pellet distribution in the MUPS formulations could be estimated by UV image analysis of the tablet surface. In conclusion, this study revealed that UV imaging in combination with multivariate image analysis is a promising approach for the automatic quality control of MUPS tablets during the manufacturing process. Copyright © 2016 Elsevier B.V. All rights reserved.

  19. Analysis of naturally etched surface of brass sheathing from a nineteenth-century shipwreck

    Directory of Open Access Journals (Sweden)

    Ashkenazi D.

    2018-01-01

    Full Text Available The Akko Tower Wreck is ently the remains of a 25-m-long merchant brig, dated to the first half of the nineteenth century. During the 2015 underwater excavation, a piece of brass sheet was retrieved from the shipwreck and its surface and bulk were examined by metallurgical analyses. The examinations revealed a unique example of almost two hundred years’ natural etching, which took place in the sea underwater environment. The surface of the sheet was covered with different copper and zinc oxides, which were identified by XRD analysis. Observation of the naturally etched surface with multi-focal light microscopy and SEM-EDS analysis indicated a microstructure of annealed α-brass, similar to that of its bulk. S-OES chemical analysis of the bulk revealed a composition of 65.0 wt% Cu, 34.4 wt% Zn and 0.6 wt% Pb. Based on the thickness of the sheet and its good state of preservation, it is suggested that it was used as sheathing to protect the hull against marine organisms, and to improve the sailing qualities of the ship. The results provide further information about the Akko Tower shipwreck; and expand our knowledge regarding the corrosion processes and preservation of brass during a long burial period in marine environments.

  20. Developments in the analysis of footwall slopes in surface coal mining

    Energy Technology Data Exchange (ETDEWEB)

    Stead, D.; Eberhardt, E. [University of Saskatchewan, Saskatoon, SK (Canada). Dept. of Geological Sciences

    1997-03-01

    Surface mining of coal, particularly in areas of mountainous topography, often involves the formation of extensive footwall slopes parallel to the strata dip. Due to structural deformation steep dips on the limbs of folds may be encountered in association with thrust faults, jointing and residual shear strength conditions. Such an environment necessitates a rigorous assessment of footwall stability in order to ensure safe and economic exploitation of the coal. This paper provides a detailed review of the factors influencing footwall slope instability in surface coal mining and the major instability mechanisms. The analysis of footwalls in the design stage and the back analysis of footwall slope failures has in general been undertaken using predominantly two-dimensional limit equilibrium techniques often incorporating a simplistic elastic column analysis. The application of numerical modelling techniques to surface coal mine footwalls has received little attention. Here the authors illustrate the potential for investigating footwall failure mechanisms and stability using the distinct element method and other modelling techniques. 44 refs., 21 figs., 2 tabs.

  1. Analysis of corrosion layers in ancient Roman silver coins with high resolution surface spectroscopic techniques

    International Nuclear Information System (INIS)

    Keturakis, Christopher J.; Notis, Ben; Blenheim, Alex; Miller, Alfred C.; Pafchek, Rob; Notis, Michael R.; Wachs, Israel E.

    2016-01-01

    Highlights: • Five ancient silver alloy coins (225 BCE–244 CE) were analyzed using surface characterization techniques. • Both destructive and non-destructive surface characterization methods were developed. • Alloying with copper, even in small amounts, leads to the formation of an outer Cu 2 O corrosion layer. - Abstract: Determination of the microchemistry of surface corrosion layers on ancient silver alloy coins is important both in terms of understanding the nature of archaeological environmental conditions to which these ancient coins were exposed and also to help in their conservation. In this present study, five ancient silver alloy coins (225 BCE–244 CE) were used as test vehicles to measure their immediate surface microchemistry and evaluate the appropriateness and limitations of High Sensitivity-Low Energy Ion Scattering Spectroscopy (HS-LEIS, 0.3 nm depth analysis), High Resolution-X-ray Photoelectron Spectroscopy (HR-XPS, 1–3 nm depth analysis) and High Resolution-Raman Spectroscopy (HR-Raman, ∼1000 nm depth analysis). Additional information about the deeper corrosion layers, up to ∼300–1000 nm, was provided by dynamic HS-LEIS and HR-Raman spectroscopy. While not archeologically significant, the use of these coins of small commercial value provides data that is more representative of the weaker signals typically obtained from ancient corroded objects, which can be in stark contrast to pristine data often obtained from carefully prepared alloys of known composition. The oldest coins, from 225 to 214 BCE, possessed an outermost surface layer containing Cu 2 O, Na, Al, Pb, and adsorbed hydrocarbons, while the more recent coins, from 98 to 244 CE, contained Cu 2 O, Ag, N, F, Na, Al, S, Cl, and adsorbed hydrocarbons in similar corresponding surface layers. It thus appears that alloying with copper, even in small amounts, leads to the formation of an outer Cu 2 O layer. Depth profiling revealed the presence of K, Na, Cl, and S as key

  2. Gold nanorods for surface Plasmon resonance detection of mercury (II) in flow injection analysis.

    Science.gov (United States)

    Trieu, Khang; Heider, Emily C; Brooks, Scott C; Barbosa, Fernando; Campiglia, Andres D

    2014-10-01

    This article investigates the flow injection analysis of mercury (II) ions in tap water samples via surface Plasmon resonance detection. Quantitative analysis of mercury (II) is based on the chemical interaction of metallic mercury with gold nanorods immobilized on a glass substrate. A new flow cell design is presented with the ability to accommodate the detecting substrate in the sample compartment of commercial spectrometers. Two alternatives are here considered for mercury (II) detection, namely stop-flow and continuous flow injection analysis modes. The best limit of detection (2.4 ng mL(-1)) was obtained with the continuous flow injection analysis approach. The accurate determination of mercury (II) ions in samples of unknown composition is demonstrated with a fortified tap water sample. Copyright © 2014 Elsevier B.V. All rights reserved.

  3. GREY RELATIONAL ANALYSIS AND ITS APPLICATION ON SURFACE PROPERTIES DURING EDM AND POWDER MIXED EDM

    Directory of Open Access Journals (Sweden)

    S. TRIPATHY

    2017-09-01

    Full Text Available Electrical discharge machining is an extensively used non-conventional process for material removal in die manufacturing and aerospace industries. The mechanism of powder mixed electric discharge machining is very different from that of electrical discharge machining process. It was found that considerable research has been done on different aspects during electric discharge machining of various steels, but sufficient data is not available on the surface properties and optimum process parameters for machining of H-11 die steel. The present work investigates the effect of process parameters like powder oncentration, peak current, pulse-on-time, duty cycle and gap voltage on material removal rate, surface roughness, recast layer thickness and microhardness simultaneously during electrical discharge machining and powder mixed electrical discharge machining of H-11 hot work tool steel. Multiobjective optimization using grey relational analysis was used to determine the optimal setting of process parameters for maximum material removal rate, minimum surface roughness, minimum recast layer thickness and maximum micro-hardness simultaneously. The work material has been selected due to its brilliant mechanical properties and diverse industrial applications. Taguchi’s L27 orthogonal array was used to carry out the experiments. Analysis of variance was performed to determine the significant parameters at a 95% confidence interval. Conductive powder mixed to the dielectric fluid was graphite of size less than 53µm obtained from the sieve analysis. Electrolytic copper was used as the tool electrode. Investigation of micro-structures was done using scanning electron microscope to examine alterations and defects on the machined surface. Grey relational analysis exhibits an improvement of 0.2025 in the grey relational grade. The tendency of deviation of the response curves suggest that powder concentration of 0g/l, peak current of 3A, pulse-ontime of 150µs

  4. A fundamental approach to adhesion: Synthesis, surface analysis, thermodynamics and mechanics. [acid-base properties of titanium 6-4 surfaces

    Science.gov (United States)

    Siriwardane, R.; Wightman, J. P.

    1980-01-01

    The acid-base properties of titanium 6-4 plates (low surface area) were investigated after three different pretreatments, namely Turco, phosphate-fluoride and Pasa-Jell. A series of indicators was used and color changes were detected using diffuse reflectance visible spectroscopy. Electron spectroscopy for chemical analysis was used to examine the indicator on the Ti 6-4 surface. Specular reflectance infra-red spectroscopy was used to study the adsorption of stearic acid from cyclohexane solutions on the Ti 6-4 surface.

  5. Enamel surface topography analysis for diet discrimination. A methodology to enhance and select discriminative parameters

    Science.gov (United States)

    Francisco, Arthur; Blondel, Cécile; Brunetière, Noël; Ramdarshan, Anusha; Merceron, Gildas

    2018-03-01

    Tooth wear and, more specifically, dental microwear texture is a dietary proxy that has been used for years in vertebrate paleoecology and ecology. DMTA, dental microwear texture analysis, relies on a few parameters related to the surface complexity, anisotropy and heterogeneity of the enamel facets at the micrometric scale. Working with few but physically meaningful parameters helps in comparing published results and in defining levels for classification purposes. Other dental microwear approaches are based on ISO parameters and coupled with statistical tests to find the more relevant ones. The present study roughly utilizes most of the aforementioned parameters in their more or less modified form. But more than parameters, we here propose a new approach: instead of a single parameter characterizing the whole surface, we sample the surface and thus generate 9 derived parameters in order to broaden the parameter set. The identification of the most discriminative parameters is performed with an automated procedure which is an extended and refined version of the workflows encountered in some studies. The procedure in its initial form includes the most common tools, like the ANOVA and the correlation analysis, along with the required mathematical tests. The discrimination results show that a simplified form of the procedure is able to more efficiently identify the desired number of discriminative parameters. Also highlighted are some trends like the relevance of working with both height and spatial parameters, as well as the potential benefits of dimensionless surfaces. On a set of 45 surfaces issued from 45 specimens of three modern ruminants with differences in feeding preferences (grazing, leaf-browsing and fruit-eating), it is clearly shown that the level of wear discrimination is improved with the new methodology compared to the other ones.

  6. Microscopic droplet formation and energy transport analysis of condensation on scalable superhydrophobic nanostructured copper oxide surfaces.

    Science.gov (United States)

    Li, GuanQiu; Alhosani, Mohamed H; Yuan, ShaoJun; Liu, HaoRan; Ghaferi, Amal Al; Zhang, TieJun

    2014-12-09

    Utilization of nanotechnologies in condensation has been recognized as one opportunity to improve the efficiency of large-scale thermal power and desalination systems. High-performance and stable dropwise condensation in widely-used copper heat exchangers is appealing for energy and water industries. In this work, a scalable and low-cost nanofabrication approach was developed to fabricate superhydrophobic copper oxide (CuO) nanoneedle surfaces to promote dropwise condensation and even jumping-droplet condensation. By conducting systematic surface characterization and in situ environmental scanning electron microscope (ESEM) condensation experiments, we were able to probe the microscopic formation physics of droplets on irregular nanostructured surfaces. At the early stages of condensation process, the interfacial surface tensions at the edge of CuO nanoneedles were found to influence both the local energy barriers for microdroplet growth and the advancing contact angles when droplets undergo depinning. Local surface roughness also has a significant impact on the volume of the condensate within the nanostructures and overall heat transfer from the vapor to substrate. Both our theoretical analysis and in situ ESEM experiments have revealed that the liquid condensate within the nanostructures determines the amount of the work of adhesion and kinetic energy associated with droplet coalescence and jumping. Local and global droplet growth models were also proposed to predict how the microdroplet morphology within nanostructures affects the heat transfer performance of early-stage condensation. Our quantitative analysis of microdroplet formation and growth within irregular nanostructures provides the insight to guide the anodization-based nanofabrication for enhancing dropwise and jumping-droplet condensation performance.

  7. Surface Water Quality Assessment and Prioritize the Factors Pollute This Water Using Topsis Fuzzy Hierarchical Analysis

    Directory of Open Access Journals (Sweden)

    Mehdi Komasi

    2017-03-01

    Full Text Available Background & Objective: Nowadays, according to growth of industry and increasing population, water resources are seriousely shortened. This lack of water resources will require special management to be considered in industry and agriculture. Among the various sources of water, surface waters are more susceptible to infection. The most important of these sources of pollution are industrial pollution, detergent, pesticides, radioactive materials, heat and salt concentration.  Materials & methods: In this article, at first the importance of each pollutant will be evaluated base on the effects and its results and then quality evaluation of surface water will be studied. In order to assess the relative importance of these pollutants primarily using TOPSIS software, prioritize these factors as one of the hierarchical analysis and then is modeled with decision tree method using Weka software, the importance of each factor is evaluated and if it does not meet the minimal importance of the decision tree will be removed. Results: The results obtained from the Topsis fuzzy analysis indicate that surface water and groundwater are exposed to pollution about 74% and 26% respectively among the six pollutants examined in this study. In addition, results obtaned from the hierarchical tree in software Weka has shown that the heat factor, soluble salts and industrial pollutants give impac factor or purity about 0.1338, 0.0523 and 1.2694 respectively. Conclusion: Surface water is at greater risk of being polluted compared with groundwater. The heat factor and low concentration of dissolved salts have the low impact and industrial pollutants are considered as the most influential factors in surface water pollution.

  8. Interaction of energetic particles with polymer surfaces: surface morphology development and sputtered polymer-fragment ion analysis

    International Nuclear Information System (INIS)

    Michael, R.S.

    1987-01-01

    The core of this thesis is based on a series of papers that have been published or will soon be published in which the various processes taking place in the energetic particle-polymer surface interaction scene is investigated. Results presented show different developments on polymer surfaces when compared to the vast experimental data on energetic particle-metal surface interactions. The surface morphology development depends on the physical characteristics of the polymer. Sputtering yields of fluoropolymers were several orders higher than the sputtering yields of aliphatic and aromatic polymers. Depending on the chemical nature of the polymer, the surface morphology development was dependent upon the extent of radiation-damage accumulation. Fast Atom Bombardment Mass Spectrometry at low and high resolution was applied to the characterization of sputtered polymer fragment ions. Fragment ions and their intensities were used to identify polymer samples, observe radiation damage accumulation and probe polymer-polymer interface of a polymer-polymer sandwich structure. A model was proposed which attempts to explain the nature of processes involved in the energetic particle-polymer surface interaction region

  9. Sensitivity analysis and development of calibration methodology for near-surface hydrogeology model of Laxemar

    International Nuclear Information System (INIS)

    Aneljung, Maria; Sassner, Mona; Gustafsson, Lars-Goeran

    2007-11-01

    between measured and calculated surface water discharges, but the model generally underestimates the total runoff from the area. The model also overestimates the groundwater levels, and the modelled groundwater level amplitudes are too small in many boreholes. A number of likely or potential reasons for these deviations can be identified: The surface stream network description in the model is incomplete. This implies that too little overland water is drained from the area by the streams, which creates ponded areas in the model that do not exist in reality. These areas are characterized by large evaporation and infiltration, contributing to groundwater recharge and reducing transpiration from the groundwater table, in turn creating high and relatively stable groundwater levels compared to those measured at the site. In order to improve the agreement between measured and modelled surface water discharges, the evapotranspiration was reduced in the model; in effect, this implied a reduction of the potential evapotranspiration. This probably caused a larger groundwater recharge and less transpiration during summer, thereby reducing the variations in the modelled groundwater levels. If the MIKE 11 stream network is updated, the potential evapotranspiration could be increased again, such that the modelling of groundwater dynamics is improved. The bottom boundary condition and the hydraulic conductivity of the bedrock may have a large effect on model-calculated near-surface/surface water flows in Laxemar. A sensitivity analysis shows that lowering the hydraulic head at the bottom boundary (located at 150 metres below sea level) lowers the groundwater levels in the Quaternary deposits, but also implies smaller surface water discharges. Lowering the hydraulic conductivity of the bedrock would increase groundwater flows to Quaternary deposits in groundwater discharge areas, which raises groundwater levels and reduces fluctuation amplitudes. An alternative model approach, using a

  10. Utility of Gram stain for the microbiological analysis of burn wound surfaces.

    Science.gov (United States)

    Elsayed, Sameer; Gregson, Daniel B; Lloyd, Tracie; Crichton, Marilyn; Church, Deirdre L

    2003-11-01

    Surface swab cultures have attracted attention as a potential alternative to biopsy histology or quantitative culture methods for microbiological burn wound monitoring. To our knowledge, the utility of adding a Gram-stained slide in this context has not been evaluated previously. To determine the degree of correlation of Gram stain with culture for the microbiological analysis of burn wound surfaces. Prospective laboratory analysis. Urban health region/centralized diagnostic microbiology laboratory. Burn patients hospitalized in any Calgary Health Region burn center from November 2000 to September 2001. Gram stain plus culture of burn wound surface swab specimens obtained during routine dressing changes or based on clinical signs of infection. Degree of correlation (complete, high, partial, none), including weighted kappa statistic (kappa(w)), of Gram stain with culture based on quantitative microscopy and degree of culture growth. A total of 375 specimens from 50 burn patients were evaluated. Of these, 239 were negative by culture and Gram stain, 7 were positive by Gram stain only, 89 were positive by culture only, and 40 were positive by both methods. The degree of complete, high, partial, and no correlation of Gram stain with culture was 70.9% (266/375), 1.1% (4/375), 2.4% (9/375), and 25.6% (96/375), respectively. The degree of correlation for all 375 specimens, as expressed by the weighted kappa statistic, was found to be fair (kappa(w) = 0.32).Conclusion.-The Gram stain is not suitable for the microbiological analysis of burn wound surfaces.

  11. Morphological analysis of the left ventricular endocardial surface using a bag-of-features descriptor.

    Science.gov (United States)

    Mukhopadhyay, Anirban; Qian, Zhen; Bhandarkar, Suchendra M; Liu, Tianming; Voros, Szilard; Rinehart, Sarah

    2015-07-01

    The limitations of conventional imaging techniques have hitherto precluded a thorough and formal investigation of the complex morphology of the left ventricular (LV) endocardial surface and its relation to the severity of coronary artery disease (CAD). However, recent developments in high-resolution multirow-detector computed tomography (MDCT) scanner technology have enabled the imaging of the complex LV endocardial surface morphology in a single heartbeat. Analysis of high-resolution computed tomography images from a 320-MDCT scanner allows for the noninvasive study of the relationship between the percent diameter stenosis (DS) values of the major coronary arteries and localization of the cardiac segments affected by coronary arterial stenosis. In this paper, a novel approach for the analysis of the nonrigid LV endocardial surface from MDCT images, using a combination of rigid body transformation-invariant shape descriptors and a more generalized isometry-invariant Bag-of-Features descriptor, is proposed and implemented. The proposed approach is shown to be successful in identifying, localizing, and quantifying the incidence and extent of CAD and, thus, is seen to have a potentially significant clinical impact. Specifically, the association between the incidence and extent of CAD, determined via the percent DS measurements of the major coronary arteries, and the alterations in the endocardial surface morphology is formally quantified. The results of the proposed approach on 16 normal datasets and 16 abnormal datasets exhibiting CAD with varying levels of severity are presented. A multivariable regression test is employed to test the effectiveness of the proposed morphological analysis approach. Experiments performed on a strictly leave-one-out basis are shown to exhibit a distinct and interesting pattern in terms of the correlation coefficient values within the cardiac segments, where the incidence of coronary arterial stenosis is localized.

  12. Bacteria hold their breath upon surface contact as shown in a strain of Escherichia coli, using dispersed surfaces and flow cytometry analysis.

    Directory of Open Access Journals (Sweden)

    Jing Geng

    Full Text Available Bacteria are ubiquitously distributed throughout our planet, mainly in the form of adherent communities in which cells exhibit specific traits. The mechanisms underpinning the physiological shift in surface-attached bacteria are complex, multifactorial and still partially unclear. Here we address the question of the existence of early surface sensing through implementation of a functional response to initial surface contact. For this purpose, we developed a new experimental approach enabling simultaneous monitoring of free-floating, aggregated and adherent cells via the use of dispersed surfaces as adhesive substrates and flow cytometry analysis. With this system, we analyzed, in parallel, the constitutively expressed GFP content of the cells and production of a respiration probe--a fluorescent reduced tetrazolium ion. In an Escherichia coli strain constitutively expressing curli, a major E. coli adhesin, we found that single cell surface contact induced a decrease in the cell respiration level compared to free-floating single cells present in the same sample. Moreover, we show here that cell surface contact with an artificial surface and with another cell caused reduction in respiration. We confirm the existence of a bacterial cell "sense of touch" ensuring early signalling of surface contact formation through respiration down modulation.

  13. Uncertainty analysis of the Operational Simplified Surface Energy Balance (SSEBop) model at multiple flux tower sites

    Science.gov (United States)

    Chen, Mingshi; Senay, Gabriel B.; Singh, Ramesh K.; Verdin, James P.

    2016-01-01

    Evapotranspiration (ET) is an important component of the water cycle – ET from the land surface returns approximately 60% of the global precipitation back to the atmosphere. ET also plays an important role in energy transport among the biosphere, atmosphere, and hydrosphere. Current regional to global and daily to annual ET estimation relies mainly on surface energy balance (SEB) ET models or statistical and empirical methods driven by remote sensing data and various climatological databases. These models have uncertainties due to inevitable input errors, poorly defined parameters, and inadequate model structures. The eddy covariance measurements on water, energy, and carbon fluxes at the AmeriFlux tower sites provide an opportunity to assess the ET modeling uncertainties. In this study, we focused on uncertainty analysis of the Operational Simplified Surface Energy Balance (SSEBop) model for ET estimation at multiple AmeriFlux tower sites with diverse land cover characteristics and climatic conditions. The 8-day composite 1-km MODerate resolution Imaging Spectroradiometer (MODIS) land surface temperature (LST) was used as input land surface temperature for the SSEBop algorithms. The other input data were taken from the AmeriFlux database. Results of statistical analysis indicated that the SSEBop model performed well in estimating ET with an R2 of 0.86 between estimated ET and eddy covariance measurements at 42 AmeriFlux tower sites during 2001–2007. It was encouraging to see that the best performance was observed for croplands, where R2 was 0.92 with a root mean square error of 13 mm/month. The uncertainties or random errors from input variables and parameters of the SSEBop model led to monthly ET estimates with relative errors less than 20% across multiple flux tower sites distributed across different biomes. This uncertainty of the SSEBop model lies within the error range of other SEB models, suggesting systematic error or bias of the SSEBop model is within

  14. Contact studies of weak adhesive interactions in water with membrane enhanced surface acoustic wave analysis

    Science.gov (United States)

    Brass, David Alan

    The measurement of weak adhesive energies has previously been difficult to obtain. To measure these energies, I designed a technique that uses the combined sensitivities of both a quartz crystal resonator and the inflation of an elastomeric polymer membrane. The surfaces of the quartz crystal and/or the membrane are modified with water swollen polymer brushes, which are used to eliminate nonspecific adhesion. These brushes are then end-modified with adhesive functional groups. An analysis is developed for the frequency response of a quartz crystal resonator as the membrane layer is placed in contact with the surface of these swollen brushes. The shear wave generated at the resonator surface couples into the membrane layer with an efficiency that is strongly dependent on the thickness of the swollen brush layer. The calculated shift decreases substantially for increases in the brush thickness of ten to twenty nanometers, giving a net frequency response that is extremely sensitive to the degree of swelling of the brush. An optimum capping layer thickness is determined by balancing the resonant frequency shift against dissipative effects that weaken the crystal resonance. Detailed calculations are presented for the specific case of poly(ethylene glycol) (PEG) brushes swollen by water and capped by a poly(styrene-ethylene/butene-styrene) (SEBS) elastomeric, water-permeable membrane. These calculations show that the method is sensitive to the properties of the brush layer. This surface acoustic wave technique was coupled with an inflation method that enabled quantification of the adhesion between the membrane and the brush coated surface. This adhesive interaction is obtained from the contact angle made between the quartz and membrane surfaces and the tension on the membrane. An analysis of the membrane profile based on the numerical solution of the axisymmetric Laplace equation is developed and used to investigate both adhesive and non-adhesive situations with both an

  15. Aircraft High-Lift Aerodynamic Analysis Using a Surface-Vorticity Solver

    Science.gov (United States)

    Olson, Erik D.; Albertson, Cindy W.

    2016-01-01

    This study extends an existing semi-empirical approach to high-lift analysis by examining its effectiveness for use with a three-dimensional aerodynamic analysis method. The aircraft high-lift geometry is modeled in Vehicle Sketch Pad (OpenVSP) using a newly-developed set of techniques for building a three-dimensional model of the high-lift geometry, and for controlling flap deflections using scripted parameter linking. Analysis of the low-speed aerodynamics is performed in FlightStream, a novel surface-vorticity solver that is expected to be substantially more robust and stable compared to pressure-based potential-flow solvers and less sensitive to surface perturbations. The calculated lift curve and drag polar are modified by an empirical lift-effectiveness factor that takes into account the effects of viscosity that are not captured in the potential-flow solution. Analysis results are validated against wind-tunnel data for The Energy-Efficient Transport AR12 low-speed wind-tunnel model, a 12-foot, full-span aircraft configuration with a supercritical wing, full-span slats, and part-span double-slotted flaps.

  16. Quantitative and Qualitative Analysis of Surface Modified Cellulose Utilizing TGA-MS

    Directory of Open Access Journals (Sweden)

    Daniel Loof

    2016-05-01

    Full Text Available With the aim to enhance interfacial adhesion of a hydrophobic polymer matrix and cellulosic fibers and fillers, chemical surface modifications with silane coupling agents are performed. Thermogravimetric analysis (TGA could be used to determine the degree of surface functionalization. However, similar thermal properties of treated and untreated cellulose hamper a precise determination of silane loading. This contribution deals with quantitative determination of silane loading combining both TGA and elemental analysis. Firstly, silane modified celluloses were studied by FT-IR, Raman, solid state NMR spectroscopy, and polarized light microscopy in order to determine functional groups and to study the impact of chemical treatment on cellulose morphology. Secondly, thermal stability and pyrolysis processes were studied by TG-MS analysis. In order to determine the exact silane loading, the mass percentages of the appropriate elements were quantified by elemental analysis and correlated with the charred residues determined by TGA yielding a linear dependency. With that correlation, it was possible to determine silane loadings for additional samples utilizing simple TGA measurements. The main advantage of that approach is that only one calibration is necessary for routine analyses of further samples and TGA-MS coupling gives additional information on thermal stability and pyrolysis routes, simultaneously.

  17. Morphologic and Hemodynamic Analysis in the Patients with Multiple Intracranial Aneurysms: Ruptured versus Unruptured.

    Directory of Open Access Journals (Sweden)

    Linkai Jing

    Full Text Available The authors evaluated the impact of morphologic and hemodynamic factors on multiple intracranial aneurysms and aimed to identify which parameters can be reliable indexes as one aneurysm ruptured, and the others did not.Between June 2011 and May 2014, 69 patients harboring multiple intracranial aneurysms (69 ruptured and 86 unruptured were analyzed from 3D-digital subtraction angiography (DSA images and computational fluid dynamics (CFD. Morphologic and hemodynamic parameters were evaluated for significance with respect to rupture. Receiver operating characteristic (ROC analysis identified area under the curve (AUC and optimal thresholds separating ruptured from unruptured intracranial aneurysms for each parameter. Significant parameters were examined by binary logistic regression analysis to identify independent discriminators.Nine morphologic (size, neck width, surface area, volume, diameter of parent arteries, aspect ratio, size ratio, lateral/bifurcation type and regular/irregular type and 6 hemodynamic (WSSmean, WSSmin, OSI, LSA, flow stability and flow complexity parameters achieved statistical significance (p0.7. By binary logistic regression analysis, large aspect ratio and low WSSmean were the independently significant rupture factors (AUC, 0.924; 95% CI, 0.883-0.965.Large aspect ratio and low WSSmean were independently associated with the rupture status of multiple intracranial aneurysms.

  18. Morphologic and Hemodynamic Analysis in the Patients with Multiple Intracranial Aneurysms: Ruptured versus Unruptured.

    Science.gov (United States)

    Jing, Linkai; Fan, Jixing; Wang, Yang; Li, Haiyun; Wang, Shengzhang; Yang, Xinjian; Zhang, Ying

    2015-01-01

    The authors evaluated the impact of morphologic and hemodynamic factors on multiple intracranial aneurysms and aimed to identify which parameters can be reliable indexes as one aneurysm ruptured, and the others did not. Between June 2011 and May 2014, 69 patients harboring multiple intracranial aneurysms (69 ruptured and 86 unruptured) were analyzed from 3D-digital subtraction angiography (DSA) images and computational fluid dynamics (CFD). Morphologic and hemodynamic parameters were evaluated for significance with respect to rupture. Receiver operating characteristic (ROC) analysis identified area under the curve (AUC) and optimal thresholds separating ruptured from unruptured intracranial aneurysms for each parameter. Significant parameters were examined by binary logistic regression analysis to identify independent discriminators. Nine morphologic (size, neck width, surface area, volume, diameter of parent arteries, aspect ratio, size ratio, lateral/bifurcation type and regular/irregular type) and 6 hemodynamic (WSSmean, WSSmin, OSI, LSA, flow stability and flow complexity) parameters achieved statistical significance (p0.7). By binary logistic regression analysis, large aspect ratio and low WSSmean were the independently significant rupture factors (AUC, 0.924; 95% CI, 0.883-0.965). Large aspect ratio and low WSSmean were independently associated with the rupture status of multiple intracranial aneurysms.

  19. Uniformity analysis of dielectric barrier discharge (DBD) processed polyethylene terephthalate (PET) surface

    Science.gov (United States)

    Liu, Chaozong; Brown, Norman M. D.; Meenan, Brian J.

    2006-01-01

    A dielectric barrier discharge (DBD) plasma, operating in air at atmospheric pressure, has been used to induce changes in the surface properties of polyethylene terephthalate (PET) films. The effects that the key DBD operating parameters: discharge power, processing speed, processing duration, and electrode configurations, have on producing wettability changes in the PET surface region have been investigated. The approach taken involves the application of an Taguchi experimental design and robust analysis methodology. The various data sets obtained from these analyses have been used to studies the effect of the operating parameters on the surface uniformity and efficiency of the said treatment. In general, the results obtained indicate that DBD plasma processing is an effective method for the controlled surface modification of PET. Relatively short exposures to the atmospheric pressure discharge produces significant wettability changes at the polymer film surface, as indicted by pronounced reductions in the water contact angle measured. It was observed that the wettability of the resultant surface shows no significant differences in respect to orientation parallel (L-direction) or perpendicular (T-direction) to the electrode long axis. However, there was significant differences between the data obtained from these two orientations. Analysis of the role of each of the operating parameters concerned shows that they have a selective effectiveness with respect to resultant surface modification in terms of uniformity of modification and wettability. The number of treatment cycles and the electrode configuration used were found to have the most significant effects on the homogeneity of the resultant PET surface changes in L- and T-orientation, respectively. On the other hand, the applied power showed no significant role in this regard. The number of treatment cycles was found to be the dominant factor (at significance level of 0.05) in respect of water contact angle

  20. Nonlinear response surface in the study of interaction analysis of three combination drugs.

    Science.gov (United States)

    Wan, Wen; Pei, Xin-Yan; Grant, Steven; Birch, Jeffrey B; Felthousen, Jessica; Dai, Yun; Fang, Hong-Bin; Tan, Ming; Sun, Shumei

    2017-01-01

    Few articles have been written on analyzing three-way interactions between drugs. It may seem to be quite straightforward to extend a statistical method from two-drugs to three-drugs. However, there may exist more complex nonlinear response surface of the interaction index (II) with more complex local synergy and/or local antagonism interspersed in different regions of drug combinations in a three-drug study, compared in a two-drug study. In addition, it is not possible to obtain a four-dimensional (4D) response surface plot for a three-drug study. We propose an analysis procedure to construct the dose combination regions of interest (say, the synergistic areas with II≤0.9). First, use the model robust regression method (MRR), a semiparametric method, to fit the entire response surface of the II, which allows to fit a complex response surface with local synergy/antagonism. Second, we run a modified genetic algorithm (MGA), a stochastic optimization method, many times with different random seeds, to allow to collect as many feasible points as possible that satisfy the estimated values of II≤0.9. Last, all these feasible points are used to construct the approximate dose regions of interest in a 3D. A case study with three anti-cancer drugs in an in vitro experiment is employed to illustrate how to find the dose regions of interest. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  1. Analysis of Nb3Sn surface layers for superconducting radio frequency cavity applications

    International Nuclear Information System (INIS)

    Becker, Chaoyue; Posen, Sam; Hall, Daniel Leslie; Groll, Nickolas; Proslier, Thomas; Cook, Russell; Schlepütz, Christian M.; Liepe, Matthias; Pellin, Michael; Zasadzinski, John

    2015-01-01

    We present an analysis of Nb 3 Sn surface layers grown on a bulk Niobium (Nb) coupon prepared at the same time and by the same vapor diffusion process used to make Nb 3 Sn coatings on 1.3 GHz Nb cavities. Tunneling spectroscopy reveals a well-developed, homogeneous superconducting density of states at the surface with a gap value distribution centered around 2.7 ± 0.4 meV and superconducting critical temperatures (T c ) up to 16.3 K. Scanning transmission electron microscopy performed on cross sections of the sample's surface region shows an ∼2 μm thick Nb 3 Sn surface layer. The elemental composition map exhibits a Nb:Sn ratio of 3:1 and reveals the presence of buried sub-stoichiometric regions that have a ratio of 5:1. Synchrotron x-ray diffraction experiments indicate a polycrystalline Nb 3 Sn film and confirm the presence of Nb rich regions that occupy about a third of the coating volume. These low T c regions could play an important role in the dissipation mechanisms occurring during RF tests of Nb 3 Sn-coated Nb cavities and open the way for further improving a very promising alternative to pure Nb cavities for particle accelerators

  2. Microarray analysis of genes associated with cell surface NIS protein levels in breast cancer.

    Science.gov (United States)

    Beyer, Sasha J; Zhang, Xiaoli; Jimenez, Rafael E; Lee, Mei-Ling T; Richardson, Andrea L; Huang, Kun; Jhiang, Sissy M

    2011-10-11

    Na+/I- symporter (NIS)-mediated iodide uptake allows radioiodine therapy for thyroid cancer. NIS is also expressed in breast tumors, raising potential for radionuclide therapy of breast cancer. However, NIS expression in most breast cancers is low and may not be sufficient for radionuclide therapy. We aimed to identify biomarkers associated with NIS expression such that mechanisms underlying NIS modulation in human breast tumors may be elucidated. Published oligonucleotide microarray data within the National Center for Biotechnology Information Gene Expression Omnibus database were analyzed to identify gene expression tightly correlated with NIS mRNA level among human breast tumors. NIS immunostaining was performed in a tissue microarray composed of 28 human breast tumors which had corresponding oligonucleotide microarray data available for each tumor such that gene expression associated with cell surface NIS protein level could be identified. NIS mRNA levels do not vary among breast tumors or when compared to normal breast tissues when detected by Affymetrix oligonucleotide microarray platforms. Cell surface NIS protein levels are much more variable than their corresponding NIS mRNA levels. Despite a limited number of breast tumors examined, our analysis identified cysteinyl-tRNA synthetase as a biomarker that is highly associated with cell surface NIS protein levels in the ER-positive breast cancer subtype. Further investigation on genes associated with cell surface NIS protein levels within each breast cancer molecular subtype may lead to novel targets for selectively increasing NIS expression/function in a subset of breast cancers patients.

  3. XPS analysis of 440C steel surfaces lubricated with perfluoropolyethers under sliding conditions in high vacuum

    Science.gov (United States)

    Herrera-Fierro, Pilar; Masuko, Masabumi; Jones, William R., Jr.; Pepper, Stephen V.

    1994-01-01

    This work presents the results of the X-Ray Photoelectron Spectroscopy (XPS) analysis of AISI 440C ball surfaces lubricated with perfluoropolyether (PFPE) oils after friction experiments under sliding conditions at high load in air and vacuum environments. The PFPE lubricants tested were Demnum S100, Fomblin Z-25, and Krytox 143AB. It was found that all the PFPE lubricants were degraded by sliding contact causing the formation of inorganic fluorides on the metallic surfaces and a layer of organic decomposition products. KRYTOX 143AB was the least reactive of the three lubricants tested. It was also found that metal fluoride formed at off-scar areas. This suggests the formation of reactive species, such as COF2 or R(sub f)COF, during sliding experiments, which can diffuse through the lubricant film and react with the metallic surfaces away from the contact region. Comparison of reference specimens before sliding with those that had undergone the sliding tests showed that the amount of non-degraded PFPE remaining on the surface of the balls after the sliding experiments was greater than that of the balls without sliding.

  4. An analysis of critical heat flux on the external surface of the reactor vessel lower head

    International Nuclear Information System (INIS)

    Yang, Soo Hyung; Baek, Won Pil; Chang, Soon Heung

    1999-01-01

    CHF (Critical heat flux) on the external surface of the reactor vessel lower head is major key in the evaluation on the feasibility of IVR-EVC (In-Vessel Retention through External Vessel Cooling) concept. To identify the CHF on the external surface, considerable works have been performed. Through the review on the previous works related to the CHF on the external surface, liquid subcooling, induced flow along the external surface, ICI (In-Core Instrument) nozzle and minimum gap are identified as major parameters. According to the present analysis, the effects of the ICI nozzle and minimum gap on CHF are pronounced at the upstream of test vessel: on the other hand, the induced flow considerably affects the CHF at downstream of test vessel. In addition, the subcooling effect is shown at all of test vessel, and decreases with the increase in the elevation of test vessel. In the real application of the IVR-EVC concept, vertical position is known as a limiting position, at which thermal margin is the minimum. So, it is very important to precisely predict the CHF at vertical position in a viewpoint of gaining more thermal margins. However, the effects of the liquid subcooling and induced flow do not seem to be adequately included in the CHF correlations suggested by previous works, especially at the downstream positions

  5. Edge Trimming Analysis for Surface Quality of Hybrid Composite - CFRP/Al2024

    Science.gov (United States)

    Ismail, J.; Mohamed, S. B.; Mohamad, M.; Mohamad, W. N. F.; Mohamed, A. S.; Mohd, A.

    2017-10-01

    The application of hybrid composite materials has increased due to their strength and light weight ratio. Edge trimming of these materials was extremely difficult due to the anisotropic and non-homogeneous structures of CFRP and ductile nature of aluminium. This research was focused on edge trimming process via down milling operation. Three cutting parameters were examined namely spindle speed, feed rate and depth of cut. The extension of two level full factorial design, Centre Composite Design (CCD) was used to plan systematic experimental methodology. The analysis of the influence and the interaction factors associated to surface quality was studied. The objective was to obtain machined surface quality of CFRP/Al2024 between 0.4 µm to 0.6 µm. The depth of cut was the most significant factor for Al2014 and meanwhile the spindle speed and feed rate were significant factors of CFRP. The validation experiment was conducted at optimum level of recommendation control factors setting to compare the deviation of predicted value from actual/measured value. Surface roughness of CFRP was found to be at 0.594 micron at the setting of spindle speed, 11750 rpm, feed rate, 750 mm/min and depth of cut, 0.255 mm. For Al2024, the surface roughness was found to be at 0.32 micron.

  6. Stochastic analysis of 1D and 2D surface topography of x-ray mirrors

    Science.gov (United States)

    Tyurina, Anastasia Y.; Tyurin, Yury N.; Yashchuk, Valeriy V.

    2017-08-01

    The design and evaluation of the expected performance of new optical systems requires sophisticated and reliable information about the surface topography for planned optical elements before they are fabricated. The problem is especially complex in the case of x-ray optics, particularly for the X-ray Surveyor under development and other missions. Modern x-ray source facilities are reliant upon the availability of optics with unprecedented quality (surface slope accuracy quality optics. The uniqueness of the optics and limited number of proficient vendors makes the fabrication extremely time consuming and expensive, mostly due to the limitations in accuracy and measurement rate of metrology used in fabrication. We discuss improvements in metrology efficiency via comprehensive statistical analysis of a compact volume of metrology data. The data is considered stochastic and a new statistical model called Invertible Time Invariant Linear Filter (InTILF) is developed now for 2D surface profiles to provide compact description of the 2D data additionally to 1D data treated so far. The model captures faint patterns in the data and serves as a quality metric and feedback to polishing processes, avoiding high resolution metrology measurements over the entire optical surface. The modeling, implemented in our Beatmark software, allows simulating metrology data for optics made by the same vendor and technology. The forecast data is vital for reliable specification for optical fabrication, to be exactly adequate for the required system performance.

  7. An assessment of surface emissivity variation effects on plasma uniformity analysis using IR cameras

    Science.gov (United States)

    Greenhalgh, Abigail; Showers, Melissa; Biewer, Theodore

    2017-10-01

    The Prototype-Material Plasma Exposure eXperiment (Proto-MPEX) is a linear plasma device operating at Oak Ridge National Laboratory (ORNL). Its purpose is to test plasma source and heating concepts for the planned Material Plasma Exposure eXperiment (MPEX), which has the mission to test the plasma-material interactions under fusion reactor conditions. In this device material targets will be exposed to high heat fluxes (>10 MW/m2). To characterize the heat fluxes to the target a IR thermography system is used taking up to 432 frames per second videos. The data is analyzed to determine the surface temperature on the target in specific regions of interest. The IR analysis has indicated a low level of plasma uniformity; the plasma often deposits more heat to the edge of the plate than the center. An essential parameter for IR temperature calculation is the surface emissivity of the plate (stainless steel). A study has been performed to characterize the variation in the surface emissivity of the plate as its temperature changes and its surface finish is modified by plasma exposure.

  8. [Anatomical names of skeletal surfaces: analysis and classification of Latin names, and comparison with corresponding Japanese names].

    Science.gov (United States)

    Shikano, Shun-ichi; Yamashita, Yasuo; Sato, Tatsuo

    2007-12-01

    For better understanding of the structures comprising the human body and in view of possible need for future revision, Latin anatomical names (Terminologia Anatomica) of the skeletal surfaces were analyzed and classified, and compared with the corresponding Japanese anatomical names. The words following Facies indicated: 1) morphological resemblance of the surface; 2) the structure that articulates with the surface; 3) the structure attached to the surface; 4) the structure in contact with the surface; 5) the way of connection between the surface and the structure that faces it; 6) the structure of which the surface is a component; 7) the structure that the surface faces; 8) the site that the surface faces; 9) the relative position of the surface; 10) the non-relative position of the surface; 11) an articulation of the surface; or 12) both the structure with which the surface articulates and the structure of which the surface is a component. Analysis of Latin names and comparison with Japanese names clarified some characteristics of both names and revealed some problems in them.

  9. Surface Roughness Analysis in the Hard Milling of JIS SKD61 Alloy Steel

    Directory of Open Access Journals (Sweden)

    Huu-That Nguyen

    2016-06-01

    Full Text Available Hard machining is an efficient solution that can be used to replace the grinding operation in the mold and die manufacturing industry. In this study, an attempt is made to analyze the effect of process parameters on workpiece surface roughness (Ra in the hard milling of JIS (Japanese Industrial Standard SKD61 steel, based on a combination of the Taguchi method and response surface methodology (RSM. The cutting parameters are selected based on the structural dynamic analysis of the machine tool. A set of experiments is designed according to the Taguchi technique. The average Ra is measured by a Mitutoyo Surftest SJ-400, and then analysis of variance (ANOVA is performed to determine the influences of cutting parameters on the given Ra. Quadratic mathematical modeling is introduced for prediction of the Ra during the hard milling process. The predicted values are in reasonable agreement with the observation of experiments. In an effort to obtain the minimizing Ra, a single objective optimization is employed based on the desirability function. The result shows that the percentage error between measured and predicted values of Ra is 3.2%, which is found to be insignificant. Eventually, the milled surface roughness under the optimized machining conditions is 0.122 µm. This finding shows that grinding may be replaced by finish hard milling in the mold and die manufacturing field.

  10. Do skeletal cephalometric characteristics correlate with condylar volume, surface and shape? A 3D analysis

    Directory of Open Access Journals (Sweden)

    Saccucci Matteo

    2012-05-01

    Full Text Available Abstract Objective The purpose of this study was to determine the condylar volume in subjects with different mandibular divergence and skeletal class using cone-beam computed tomography (CBCT and analysis software. Materials and methods For 94 patients (46 females and 48 males; mean age 24.3 ± 6.5 years, resultant rendering reconstructions of the left and right temporal mandibular joints (TMJs were obtained. Subjects were then classified on the base of ANB angle the GoGn-SN angle in three classes (I, II, III . The data of the different classes were compared. Results No significant difference was observed in the whole sample between the right and the left sides in condylar volume. The analysis of mean volume among low, normal and high mandibular plane angles revealed a significantly higher volume and surface in low angle subjects (p  Class III subjects also tended to show a higher condylar volume and surface than class I and class II subjects, although the difference was not significant. Conclusions Higher condylar volume was a common characteristic of low angle subjects compared to normal and high mandibular plane angle subjects. Skeletal class also appears to be associated to condylar volume and surface.

  11. Analysis of the silicone polymer surface aging profile with laser-induced breakdown spectroscopy

    Science.gov (United States)

    Wang, Xilin; Hong, Xiao; Wang, Han; Chen, Can; Zhao, Chenlong; Jia, Zhidong; Wang, Liming; Zou, Lin

    2017-10-01

    Silicone rubber composite materials have been widely used in high voltage transmission lines for anti-pollution flashover. The aging surface of silicone rubber materials decreases service properties, causing loss of the anti-pollution ability. In this paper, as an analysis method requiring no sample preparation that is able to be conducted on site and suitable for nearly all types of materials, laser-induced breakdown spectroscopy (LIBS) was used for the analysis of newly prepared and aging (out of service) silicone rubber composites. With scanning electron microscopy (SEM) and hydrophobicity test, LIBS was proven to be nearly non-destructive for silicone rubber. Under the same LIBS testing parameters, a linear relationship was observed between ablation depth and laser pulses number. With the emission spectra, all types of elements and their distribution in samples along the depth direction from the surface to the inner part were acquired and verified with EDS results. This research showed that LIBS was suitable to detect the aging layer depth and element distribution of the silicone rubber surface.

  12. Three-dimensional analysis of surface crack-Hertzian stress field interaction

    Science.gov (United States)

    Ballarini, R.; Hsu, Y.

    1989-01-01

    The results are presented of a stress intensity factor analysis of semicircular surface cracks in the inner raceway of an engine bearing. The loading consists of a moving spherical Hertzian contact load and an axial stress due to rotation and shrink fit. A 3-D linear elastic Boundary Element Method code was developed to perform the stress analysis. The element library includes linear and quadratic isoparametric surface elements. Singular quarter point elements were employed to capture the square root displacement variation and the inverse square root stress singularity along the crack front. The program also possesses the capability to separate the whole domain into two subregions. This procedure enables one to solve nonsymmetric fracture mechanics problems without having to separate the crack surfaces a priori. A wide range of configuration parameters was investigated. The ratio of crack depth to bearing thickness was varied from one-sixtieth to one-fifth for several different locations of the Hertzian load. The stress intensity factors for several crack inclinations were also investigated. The results demonstrate the efficiency and accuracy of the Boundary Element Method. Moreover, the results can provide the basis for crack growth calculations and fatigue life prediction.

  13. Influence of surface treatment on osseointegration of dental implants: histological, histomorphometric and radiological analysis in vivo.

    Science.gov (United States)

    Calvo-Guirado, José Luis; Satorres-Nieto, Marta; Aguilar-Salvatierra, Antonio; Delgado-Ruiz, Rafael Arcesio; Maté-Sánchez de Val, José Eduardo; Gargallo-Albiol, Jordi; Gómez-Moreno, Gerardo; Romanos, Georgios E

    2015-03-01

    The aim of this article is to compare the influence of surface treatment on the integration (at 2, 4 and 8 weeks) of 120 dental implants inserted in 60 tibiae of rabbits. Four different surfaces were double-blind tested: blasted, acid-etched and discrete crystal deposition (DCD) (group A); blasted (group B); acid-etched (group C) and blasted and acid-etched (group D). Bone-to-implant contact plus reverse torque and bone level were measured at the time of implant insertion and at 14, 28 and 56 days of healing. Group A showed the highest early and late bone-to-implant contact (BIC) values: 40.8 ± 2.3 % at 14 days decreasing to 27.7 ± 1.1 % after 28 days and 39.4 ± 1.4 % at 56 days. For group B, the average BIC values at 14, 28 and 56 days were 23.34 ± 2.1, 23.77 ± 1.9 and 29.47 ± 1.7 %, respectively. Group C showed a value of 25.72 ± 2.3 % after 14 days of integration, 34.92 ± 2.2 % at 28 days and 32.91 ± 1.6 % at 56 days. Group D showed a BIC value of 32 ± 2.5 % at 14 days, 32.85 ± 1.4 % at 28 days and 34.04 ± 2.3 % at 56 days. In the scanning electron microscopy (SEM) analysis, no statistically significant differences were found. The Ca/P ratio values were 1.762 for surface A, 1.625 for surface B, 1.663 for surface C and finally 1.722 for surface D. Therefore, we conclude that even if there seems to be a tendency to obtain better BIC results with surface A (blasted-etched and covered with hydroxyapatite (HA)), no statistical differences were obtained in this study. The study shows the influence of different implant surfaces in increasing osseointegation for immediate loading implants.

  14. Global spectral graph wavelet signature for surface analysis of carpal bones

    Science.gov (United States)

    Masoumi, Majid; Rezaei, Mahsa; Ben Hamza, A.

    2018-02-01

    Quantitative shape comparison is a fundamental problem in computer vision, geometry processing and medical imaging. In this paper, we present a spectral graph wavelet approach for shape analysis of carpal bones of the human wrist. We employ spectral graph wavelets to represent the cortical surface of a carpal bone via the spectral geometric analysis of the Laplace-Beltrami operator in the discrete domain. We propose global spectral graph wavelet (GSGW) descriptor that is isometric invariant, efficient to compute, and combines the advantages of both low-pass and band-pass filters. We perform experiments on shapes of the carpal bones of ten women and ten men from a publicly-available database of wrist bones. Using one-way multivariate analysis of variance (MANOVA) and permutation testing, we show through extensive experiments that the proposed GSGW framework gives a much better performance compared to the global point signature embedding approach for comparing shapes of the carpal bones across populations.

  15. Analysis of Bacterial Cell Surface Chemical Composition Using Cryogenic X-Ray Photoelectron Spectroscopy.

    Science.gov (United States)

    Ramstedt, Madeleine; Shchukarev, Andrey

    2016-01-01

    This chapter describes a method for measuring the average surface chemical composition with respect to lipids, polysaccharides, and peptides (protein + peptidoglycan) for the outer part of the bacterial cell wall. Bacterial cultures grown over night are washed with a buffer or saline at controlled pH. The analysis is done on fast-frozen bacterial cell pellets obtained after centrifugation, and the analysis requires access to X-ray photoelectron spectroscopy instrumentation that can perform analyses at cryogenic temperatures (for example using liquid nitrogen). The method can be used to monitor changes in the cell wall composition following environmental stimuli or genetic mutations. The data obtained originate from the outermost part of the cell wall. Thus, it is expected that for gram-negative bacteria only the outer membrane and part of the periplasmic peptidoglycan layer is probed during analysis, and for gram-positive bacteria only the top nanometers of the peptidoglycan layer of the cell wall is monitored.

  16. In-situ soil composition and moisture measurement by surface neutron activation analysis

    Science.gov (United States)

    Waring, C.; Smith, C.; Marks, A.

    2009-04-01

    Neutron activation analysis is widely known as a laboratory technique dependent upon a nuclear reactor to provide the neutron flux and capable of precise elemental analysis. Less well known in-situ geochemical analysis is possible with isotopic (252Cf & 241Am) or compact accelerator (D-T, D-D fusion reaction) neutron sources. Prompt gamma neutron activation analysis (PGNAA) geophysical borehole logging has been applied to mining issues for >15 years (CSIRO) using isotopic neutron sources and more recently to environmental and hydro-geological applications by ANSTO. Similarly, sophisticated geophysical borehole logging equipment based on inelastic neutron scattering (INS) has been applied in the oil and gas industry by large oilfield services companies to measure oil saturation indices (carbon/oxygen) using accelerator neutron sources. Recent advances in scintillation detector spectral performance has enabled improved precision and detection limits for elements likely to be present in soil profiles (H, Si, Al, Fe, Cl) and possible detection of many minor to trace elements if sufficiently abundant (Na, K, Mg, Ca, S, N, + ). To measure carbon an accelerator neutron source is required to provide fast neutrons above 4.8 MeV. CSIRO and ANSTO propose building a soil geochemical analysis system based on experience gained from building and applying PGNA borehole logging equipment. A soil geochemical analysis system could effectively map the 2D geochemical composition of the top 50cm of soil by dragging the 1D logging equipment across the ground surface. Substituting an isotopic neutron source for a D-T accelerator neutron source would enable the additional measurement of elemental carbon. Many potential ambiguities with other geophysical proxies for soil moisture may be resolved by direct geochemical measurement of H. Many other applications may be possible including time series in-situ measurements of soil moisture for differential drainage, hydrology, land surface

  17. Practical using of TXRF spectrometers with slitless collimators for the trace analysis of targets surfaces

    International Nuclear Information System (INIS)

    Egorov, V.K.; Zuev, A.P.; Kondratiev, O.S.; Egorov, E.V.

    2000-01-01

    TXRF spectrometer with the slitless collimator used for a formation of the x-ray excitating beam (TXRF-SC spectrometer) is a new variety of an instrument been destined for the trace analysis of surfaces by x-ray fluorescence method at the total reflection of the x-ray incident beam. Some theoretical concepts are introduced for a characterization of the x-ray optics been unique to the TXRF-SC spectrometer. The principle design of the TXRF-SC spectrometer used for the trace quantitative analysis of a surface are discussed. Spectra of a secondary x-ray radiation yield for typical targets been collected by using of the TXRF-SC spectrometer and calculation of surface trace elements concentrations are presented. The analytical and operating parameters of the TXRF-SC spectrometer and one characterized by standard optical scheme are compared. The slitless collimator of the x-ray radiation is formed by two quartz polished plates mated together. Lengths of the plates are not equal. The target is placed on the surface of the long quartz plate and produces the continuation of the initial slitless collimator. Target orientation problem vanishes but problem of the surface contact effect appears. The secondary x-ray radiation excitated in a surface of the target is led out across the hole in the long quartz plate. The radiation is registered by a standard Si (Li) semiconductor detector and is collected by a multi-channel analyzer. The fundamental difference of the x-ray optical scheme been unique to TXRF-SC spectrometer from the standard one is the excitation of a studied surface by a flared x-ray beam with angle ΔΘ = 2Θ c , where Θ c is the critical angle of the total reflection. The vital peculiarity of a x-ray slitless collimation is the absence of a radiation monochromatism in output of the collimator. The sensible divergence of the x-ray excitating beam and the availability in it of monochromatic and white radiation alike allow to get in the surface layer of target the

  18. Finite element analysis of transient viscous flow with free surface using filling pattern technique

    International Nuclear Information System (INIS)

    Kim, Ki Don; Yang, Dong Yol; Jeong, Jun Ho

    2001-01-01

    The filling pattern technique based on the finite element method and Eulerian mesh advancement approach has been developed to analyze incompressible transient viscous flow with free surfaces. The governing equation for flow analysis is Navier-Stokes equation including inertia and gravity effects. The penalty and predictor-corrector methods are used effectively for finite element formulation. The flow front surface and the volume inflow rate are calculated using the filling pattern technique to select an adequate pattern among four filling patterns at each triangular control volume. Using the proposed numerical technique, the collapse of a dam has been analyzed to predict flow phenomenon of fluid and the predicted front positions versus time have been compared with the reported experimental result

  19. Quantitative analysis of rat Ig (sub)classes binding to cell surface antigens

    International Nuclear Information System (INIS)

    Nilsson, R.; Brodin, T.; Sjoegren, H.-O.

    1982-01-01

    An indirect 125 I-labeled protein A assay for detection of cell surface-bound rat immunoglobulins is presented. The assay is quantitative and rapid and detects as little as 1 ng of cell surface-bound Ig. It discriminates between antibodies belonging to different IgG subclasses, IgM and IgA. The authors describe the production and specificity control of the reagents used and show that the test can be used for quantitative analysis. A large number of sera from untreated rats are tested to evaluate the frequency of falsely positive responses and variation due to age, sex and strain of rat. With this test it is relatively easy to quantitate the binding of classes and subclasses of rat immunoglobulins in a small volume (6 μl) of untreated serum. (Auth.)

  20. Glass Formation, Chemical Properties and Surface Analysis of Cu-Based Bulk Metallic Glasses

    Directory of Open Access Journals (Sweden)

    Akihisa Inoue

    2011-04-01

    Full Text Available This paper reviews the influence of alloying elements Mo, Nb, Ta and Ni on glass formation and corrosion resistance of Cu-based bulk metallic glasses (BMGs. In order to obtain basic knowledge for application to the industry, corrosion resistance of the Cu–Hf–Ti–(Mo, Nb, Ta, Ni and Cu–Zr–Ag–Al–(Nb bulk glassy alloy systems in various solutions are reported in this work. Moreover, X-ray photoelectron spectroscopy (XPS analysis is performed to clarify the surface-related chemical characteristics of the alloy before and after immersion in the solutions; this has lead to a better understanding of the correlation between the surface composition and the corrosion resistance.

  1. Longwave surface radiation over the globe from satellite data - An error analysis

    Science.gov (United States)

    Gupta, S. K.; Wilber, A. C.; Darnell, W. L.; Suttles, J. T.

    1993-01-01

    Errors have been analyzed for monthly-average downward and net longwave surface fluxes derived on a 5-deg equal-area grid over the globe, using a satellite technique. Meteorological data used in this technique are available from the TIROS Operational Vertical Sounder (TOVS) system flown aboard NOAA's operational sun-synchronous satellites. The data used are for February 1982 from NOAA-6 and NOAA-7 satellites. The errors in the parametrized equations were estimated by comparing their results with those from a detailed radiative transfer model. The errors in the TOVS-derived surface temperature, water vapor burden, and cloud cover were estimated by comparing these meteorological parameters with independent measurements obtained from other satellite sources. Analysis of the overall errors shows that the present technique could lead to underestimation of downward fluxes by 5 to 15 W/sq m and net fluxes by 4 to 12 W/sq m.

  2. Trim cut machining and surface integrity analysis of Nimonic 80A alloy using wire cut EDM

    Directory of Open Access Journals (Sweden)

    Amitesh Goswami

    2017-02-01

    Full Text Available This present work deals with the features of trim cut wire EDM machining of Nimonic 80A in terms of machining parameters, to predict material removal rate (MRR, surface roughness (Ra, wire wear ratio (WWR and microstructure analysis. Trim cut is performed after rough cut to remove the rough layer deposited after machining due to melting and re-solidification of the eroded metal from workpiece as well as from wire electrode. Taguchi’s design of experiments methodology has been used for planning and designing the experiments. The relative significance of various factors has also been evaluated and analyzed using ANOVA. The results clearly indicate trim cut potential for high surface finish compared to rough cut machining.

  3. GC/MS Analysis of Pesticides in the Ferrara Area (Italy) Surface Water: A Chemometric Study

    International Nuclear Information System (INIS)

    Pasti, L.; Dondi, F.; Nava, E.; Morelli, M.; Bignami, S.

    2007-01-01

    The development of a network to monitor surface waters is a critical element in the assessment, restoration and protection of water quality. In this study, concentrations of 42 pesticides - determined by GC-MS on samples from 11 points along the Ferrara area rivers - have been analyzed by chemometric tools. The data were collected over a three-year period (2002-2004). Principal component analysis of the detected pesticides was carried out in order to define the best spatial locations for the sampling points. The results obtained have been interpreted in view of agricultural land use. Time series data regarding pesticide contents in surface waters has been analyzed using the Autocorrelation function. This chemometric tool allows for seasonal trends and makes it possible to optimize sampling frequency in order to detect the effective maximum pesticide content

  4. Source-model technique analysis of electromagnetic scattering by surface grooves and slits.

    Science.gov (United States)

    Trotskovsky, Konstantin; Leviatan, Yehuda

    2011-04-01

    A computational tool, based on the source-model technique (SMT), for analysis of electromagnetic wave scattering by surface grooves and slits is presented. The idea is to use a superposition of the solution of the unperturbed problem and local corrections in the groove/slit region (the grooves and slits are treated as perturbations). In this manner, the solution is obtained in a much faster way than solving the original problem. The proposed solution is applied to problems of grooves and slits in otherwise planar or periodic surfaces. Grooves and slits of various shapes, both smooth ones as well as ones with edges, empty or filled with dielectric material, are considered. The obtained results are verified against previously published data. © 2011 Optical Society of America

  5. Analysis of homogeneity of mixed oxide (MOX) fuel surface by laser induced break down spectroscopy (LIBS)

    International Nuclear Information System (INIS)

    Detalle, V.; Lacour, J.L.; Mauchien, P.; Wagner, J.F.

    2000-01-01

    In the nuclear fuel cycle, plutonium is recycled to produce MOX fuel for use in PWR reactors. Surface inspections of mixed PuO 2 /UO 2 pellets is very important in the process. The performance of Laser Induced Breakdown Spectroscopy (LIBS) or Laser Ablation Optical Emission Spectroscopy (LA-OES) was therefore assessed for surface analysis of simulated MOX pellets containing a mixture of UO 2 and CeO 2 , and compared with results obtained with the standard Castaing microprobe analyzer technique. In LIBS, a material is ablated by focussing a laser beam, and the emission from neutral and ionized atoms can be used to determine the composition. An original experimental set up was developed to obtain a LIBS microprobe system for microanalysis of the sample surface. The instrument has three main components : a laser (quadrupled Nd YAG), an ablation head (using a microscope lens) and a detection unit (spectrometer combined with an ICCD Intensified Charge Coupled Device camera). The LIBS technique has well-known advantages particularly for nuclear applications: (1) it requires no sample preparation ; (2) only a small amount of material (craters 7 or 3 μm wide and 1 to 3 μm deep) is needed for the analysis; (3) analysis can be performed remotely via optical fiber, allowing measurements in a hostile environment and at atmospheric pressure. The experimental set-up developed demonstrated that the LIBS microprobe system can be used for surface analysis of UO 2 /CeO 2 pellets. Figure 1 shows the calibration curve obtained, with the Ce/U ratio versus Ce/U concentration. Good linearity was found and a relative standard deviation of 5 % was determined for 100 single shots. A qualitative comparison of the LIBS microanalysis set up and the Castaing microprobe analyzer is shown in Figure 2, which reveals the same features. Thus, both analytical techniques can identify the surface non-homogeneity of the pellet. While LIBS is destructive, it requires no sample preparation, is faster (2

  6. Analysis of the Impact of Wildfire on Surface Ozone Record in the Colorado Front Range

    Science.gov (United States)

    McClure-Begley, A.; Petropavlovskikh, I. V.; Oltmans, S. J.; Pierce, R. B.; Sullivan, J. T.; Reddy, P. J.

    2015-12-01

    Ozone plays an important role on the oxidation capacity of the atmosphere, and at ground-level has negative impacts on human health and ecosystem processes. In order to understand the dynamics and variability of surface ozone, it is imperative to analyze individual sources, interactions between sources, transport, and chemical processes of ozone production and accumulation. Biomass burning and wildfires have been known to emit a suite of particulate matter and gaseous compounds into the atmosphere. These compounds, such as, volatile organic compounds, carbon monoxide, and nitrogen oxides are precursor species which aid in the photochemical production and destruction of ozone. The Colorado Front Range (CFR) is a region of complex interactions between pollutant sources and meteorological conditions which result in the accumulation of ozone. High ozone events in the CFR associated with fires are analyzed for 2003-2014 to develop understanding of the large scale influence and variability of ozone and wildfire relationships. This study provides analysis of the frequency of enhanced ozone episodes that can be confirmed to be transported within and affected by the fires and smoke plumes. Long-term records of surface ozone data from the CFR provide information on the impact of wildfire pollutants on seasonal and diurnal ozone behavior. Years with increased local fire activity, as well as years with increased long-range transport of smoke plumes, are evaluated for the effect on the long-term record and high ozone frequency of each location. Meteorological data, MODIS Fire detection images, NOAA HYSPLIT Back Trajectory analysis, NOAA Smoke verification model, Fire Tracer Data (K+), RAQMS Model, Carbon Monoxide data, and Aerosol optical depth retrievals are used with NOAA Global Monitoring Division surface ozone data from three sites in Colorado. This allows for investigation of the interactions between pollutants and meteorology which result in high surface ozone levels.

  7. HYDROLOGIC AND FEATURE-BASED SURFACE ANALYSIS FOR TOOL MARK INVESTIGATION ON ARCHAEOLOGICAL FINDS

    Directory of Open Access Journals (Sweden)

    K. Kovács

    2012-07-01

    Full Text Available The improvement of detailed surface documentation methods provides unique tool mark-study opportunities in the field of archaeological researches. One of these data collection techniques is short-range laser scanning, which creates a digital copy of the object’s morphological characteristics from high-resolution datasets. The aim of our work was the accurate documentation of a Bronze Age sluice box from Mitterberg, Austria with a spatial resolution of 0.2 mm. Furthermore, the investigation of the entirely preserved tool marks on the surface of this archaeological find was also accomplished by these datasets. The methodology of this tool mark-study can be summarized in the following way: At first, a local hydrologic analysis has been applied to separate the various patterns of tools on the finds’ surface. As a result, the XYZ coordinates of the special points, which represent the edge lines of the sliding tool marks, were calculated by buffer operations in a GIS environment. During the second part of the workflow, these edge points were utilized to manually clip the triangle meshes of these patterns in reverse engineering software. Finally, circle features were generated and analysed to determine the different sections along these sliding tool marks. In conclusion, the movement of the hand tool could be reproduced by the spatial analysis of the created features, since the horizontal and vertical position of the defined circle centre points indicated the various phases of the movements. This research shows an exact workflow to determine the fine morphological structures on the surface of the archaeological find.

  8. Modelling and analysis of tool wear and surface roughness in hard turning of AISI D2 steel using response surface methodology

    Directory of Open Access Journals (Sweden)

    M. Junaid Mir

    2018-01-01

    Full Text Available The present work deals with some machinability studies on tool wear and surface roughness, in finish hard turning of AISI D2 steel using PCBN, Mixed ceramic and coated carbide inserts. The machining experiments are conducted based on the response surface methodology (RSM. Combined effects of three cutting parameters viz., cutting speed, cutting time and tool hardness on the two performance outputs (i.e. VB and Ra, are explored employing the analysis of variance (ANOVA.The relationship(s between input variables and the response parameters are determined using a quadratic regression model. The results show that the tool wear was influenced principally by the cutting time and in the second level by the cutting tool hardness. On the other hand, cutting time was the dominant factor affecting workpiece surface roughness followed by cutting speed. Finally, the multiple response optimizations of tool wear and surface roughness were carried out using the desirability function approach (DFA.

  9. A surface-based analysis of language lateralization and cortical asymmetry.

    Science.gov (United States)

    Greve, Douglas N; Van der Haegen, Lise; Cai, Qing; Stufflebeam, Steven; Sabuncu, Mert R; Fischl, Bruce; Brysbaert, Marc

    2013-09-01

    Among brain functions, language is one of the most lateralized. Cortical language areas are also some of the most asymmetrical in the brain. An open question is whether the asymmetry in function is linked to the asymmetry in anatomy. To address this question, we measured anatomical asymmetry in 34 participants shown with fMRI to have language dominance of the left hemisphere (LLD) and 21 participants shown to have atypical right hemisphere dominance (RLD). All participants were healthy and left-handed, and most (80%) were female. Gray matter (GM) volume asymmetry was measured using an automated surface-based technique in both ROIs and exploratory analyses. In the ROI analysis, a significant difference between LLD and RLD was found in the insula. No differences were found in planum temporale (PT), pars opercularis (POp), pars triangularis (PTr), or Heschl's gyrus (HG). The PT, POp, insula, and HG were all significantly left lateralized in both LLD and RLD participants. Both the positive and negative ROI findings replicate a previous study using manually labeled ROIs in a different cohort [Keller, S. S., Roberts, N., Garcia-Finana, M., Mohammadi, S., Ringelstein, E. B., Knecht, S., et al. Can the language-dominant hemisphere be predicted by brain anatomy? Journal of Cognitive Neuroscience, 23, 2013-2029, 2011]. The exploratory analysis was accomplished using a new surface-based registration that aligns cortical folding patterns across both subject and hemisphere. A small but significant cluster was found in the superior temporal gyrus that overlapped with the PT. A cluster was also found in the ventral occipitotemporal cortex corresponding to the visual word recognition area. The surface-based analysis also makes it possible to disentangle the effects of GM volume, thickness, and surface area while removing the effects of curvature. For both the ROI and exploratory analyses, the difference between LLD and RLD volume laterality was most strongly driven by differences

  10. A Surface-based Analysis of Language Lateralization and Cortical Asymmetry

    Science.gov (United States)

    Greve, Douglas N.; Van der Haegen, Lise; Cai, Qing; Stufflebeam, Steven; Sabuncu, Mert R.; Fischl, Bruce; Bysbaert, Marc

    2013-01-01

    Among brain functions, language is one of the most lateralized. Cortical language areas are also some of the most asymmetrical in the brain. An open question is whether the asymmetry in function is linked to the asymmetry in anatomy. To address this question, we measured anatomical asymmetry in 34 participants shown with fMRI to have language dominance of the left hemisphere (LLD) and 21 participants shown to have atypical right hemisphere dominance (RLD). All participants were healthy and left-handed, and most (80%) were female. Gray matter (GM) volume asymmetry was measured using an automated surface-based technique in both ROIs and exploratory analyses. In the ROI analysis, a significant difference between LLD and RLD was found in the insula. No differences were found in planum temporale (PT), pars opercularis (POp), pars triangularis (PTr), or Heschl’s gyrus (HG). The PT, POp, insula, and HG were all significantly left lateralized in both LLD and RLD participants. Both the positive and negative ROI findings replicate a previous study using manually labeled ROIs in a different cohort [Keller, S. S., Roberts, N., Garcia-Finana, M., Mohammadi, S., Ringelstein, E. B., Knecht, S., et al. Can the language-dominant hemisphere be predicted by brain anatomy? Journal of Cognitive Neuroscience, 23, 2013–2029, 2011]. The exploratory analysis was accomplished using a new surface-based registration that aligns cortical folding patterns across both subject and hemisphere. A small but significant cluster was found in the superior temporal gyrus that overlapped with the PT. A cluster was also found in the ventral occipitotemporal cortex corresponding to the visual word recognition area. The surface-based analysis also makes it possible to disentangle the effects of GM volume, thickness, and surface area while removing the effects of curvature. For both the ROI and exploratory analyses, the difference between LLD and RLD volume laterality was most strongly driven by

  11. Rapid thyroid dysfunction screening based on serum surface-enhanced Raman scattering and multivariate statistical analysis

    Science.gov (United States)

    Tian, Dayong; Lü, Guodong; Zhai, Zhengang; Du, Guoli; Mo, Jiaqing; Lü, Xiaoyi

    2018-01-01

    In this paper, serum surface-enhanced Raman scattering and multivariate statistical analysis are used to investigate a rapid screening technique for thyroid function diseases. At present, the detection of thyroid function has become increasingly important, and it is urgently necessary to develop a rapid and portable method for the detection of thyroid function. Our experimental results show that, by using the Silmeco-based enhanced Raman signal, the signal strength greatly increases and the characteristic peak appears obviously. It is also observed that the Raman spectra of normal and anomalous thyroid function human serum are significantly different. Principal component analysis (PCA) combined with linear discriminant analysis (LDA) was used to diagnose thyroid dysfunction, and the diagnostic accuracy was 87.4%. The use of serum surface-enhanced Raman scattering technology combined with PCA-LDA shows good diagnostic performance for the rapid detection of thyroid function. By means of Raman technology, it is expected that a portable device for the rapid detection of thyroid function will be developed.

  12. Analysis of personal care products on model skin surfaces using DESI and PADI ambient mass spectrometry.

    Science.gov (United States)

    Salter, Tara L; Green, Felicia M; Faruqui, Nilofar; Gilmore, Ian S

    2011-08-21

    Two ambient ionisation techniques, desorption electrospray ionisation (DESI) and plasma assisted desorption ionisation (PADI), have been used to analyse personal care products (PCPs) on fixed fibroblast cell surfaces. The similarities and differences between the two techniques for this type of analysis have been explored in various ways. Here, we show the results of DESI and PADI analysis of individual PCP ingredients as well as the analysis of these as complex creams on model skin surfaces, with minimal sample preparation. Typically, organosiloxanes and small molecules were detected from the creams. A study of the morphological damage of the fibroblast cells by the two ionisation techniques showed that for a less than 10% reduction in cell number, acquisition times should be limited to 5 s for PADI, which gives good signal levels; with DESI, the morphological damage was negligible. The operating parameters for the plasma source were optimised, and it was also found that the parameters could be modified to vary the relative intensity of different ions in the mass spectrum.

  13. Quantitative studies of rhubarb using quantitative analysis of multicomponents by single marker and response surface methodology.

    Science.gov (United States)

    Sun, Jiachen; Wu, Yueting; Dong, Shengjie; Li, Xia; Gao, Wenyuan

    2017-10-01

    In this work, we developed a novel approach to evaluate the contents of bioactive components in rhubarb. The present method was based on the quantitative analysis of multicomponents by a single-marker and response surface methodology approaches. The quantitative analysis of multicomponents by a single-marker method based on high-performance liquid chromatography coupled with photodiode array detection was developed and applied to determine the contents of 12 bioactive components in rhubarb. No significant differences were found in the results from the quantitative analysis of multicomponents by a single-marker and the external standard method. In order to maximize the extraction of 12 bioactive compounds in rhubarb, the ultrasonic-assisted extraction conditions were obtained by the response surface methodology coupled with Box-Behnken design. According to the obtained results, we showed that the optimal conditions would be as follows: proportion of ethanol/water 74.39%, solvent-to-solid ratio 24.07:1 v/w, extraction time 51.13 min, and extraction temperature 63.61°C. The analytical scheme established in this research should be a reliable, convenient, and appropriate method for quantitative determination of bioactive compounds in rhubarb. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  14. VASP: a volumetric analysis of surface properties yields insights into protein-ligand binding specificity.

    Directory of Open Access Journals (Sweden)

    Brian Y Chen

    2010-08-01

    Full Text Available Many algorithms that compare protein structures can reveal similarities that suggest related biological functions, even at great evolutionary distances. Proteins with related function often exhibit differences in binding specificity, but few algorithms identify structural variations that effect specificity. To address this problem, we describe the Volumetric Analysis of Surface Properties (VASP, a novel volumetric analysis tool for the comparison of binding sites in aligned protein structures. VASP uses solid volumes to represent protein shape and the shape of surface cavities, clefts and tunnels that are defined with other methods. Our approach, inspired by techniques from constructive solid geometry, enables the isolation of volumetrically conserved and variable regions within three dimensionally superposed volumes. We applied VASP to compute a comparative volumetric analysis of the ligand binding sites formed by members of the steroidogenic acute regulatory protein (StAR-related lipid transfer (START domains and the serine proteases. Within both families, VASP isolated individual amino acids that create structural differences between ligand binding cavities that are known to influence differences in binding specificity. Also, VASP isolated cavity subregions that differ between ligand binding cavities which are essential for differences in binding specificity. As such, VASP should prove a valuable tool in the study of protein-ligand binding specificity.

  15. Inverse modelling of Köhler theory – Part 1: A response surface analysis of CCN spectra with respect to surface-active organic species

    Directory of Open Access Journals (Sweden)

    S. Lowe

    2016-09-01

    Full Text Available In this study a novel framework for inverse modelling of cloud condensation nuclei (CCN spectra is developed using Köhler theory. The framework is established by using model-generated synthetic measurements as calibration data for a parametric sensitivity analysis. Assessment of the relative importance of aerosol physicochemical parameters, while accounting for bulk–surface partitioning of surface-active organic species, is carried out over a range of atmospherically relevant supersaturations. By introducing an objective function that provides a scalar metric for diagnosing the deviation of modelled CCN concentrations from synthetic observations, objective function response surfaces are presented as a function of model input parameters. Crucially, for the chosen calibration data, aerosol–CCN spectrum closure is confirmed as a well-posed inverse modelling exercise for a subset of the parameters explored herein. The response surface analysis indicates that the appointment of appropriate calibration data is particularly important. To perform an inverse aerosol–CCN closure analysis and constrain parametric uncertainties, it is shown that a high-resolution CCN spectrum definition of the calibration data is required where single-valued definitions may be expected to fail. Using Köhler theory to model CCN concentrations requires knowledge of many physicochemical parameters, some of which are difficult to measure in situ on the scale of interest and introduce a considerable amount of parametric uncertainty to model predictions. For all partitioning schemes and environments modelled, model output showed significant sensitivity to perturbations in aerosol log-normal parameters describing the accumulation mode, surface tension, organic : inorganic mass ratio, insoluble fraction, and solution ideality. Many response surfaces pertaining to these parameters contain well-defined minima and are therefore good candidates for calibration using a Monte

  16. Statistical analysis of surface roughness in turning based on cutting parameters and tool vibrations with response surface methodology (RSM)

    Science.gov (United States)

    Touati, Soufiane; Mekhilef, Slimane

    2018-03-01

    In this paper, we present an experimental study to determine the effect of the cutting conditions and tool vibration on the surface roughness in finish turning of 32CrMoV12-28 steel, using carbide cutting tool YT15. For these purposes, a linear quadratic model in interaction of connecting surface roughness (Ra, Rz) with different combinations of cutting parameters such as cutting speed, feed rate, depth of cut and tool vibration, in radial and in tangential cutting force directions (Vy) and (Vz) is elaborated. In order to express the degree of interaction of cutting parameters and tool vibration, a multiple linear regression and response surface methodology are adopted. The application of this statistical technique for predicting the surface roughness shows that the feed rate is the most dominant factor followed by the cutting speed. However, the depth of the cut and tool vibrations have secondary effect. The presented models have some interest since they are used in the cutting process optimization.

  17. An improved method for Multipath Hemispherical Map (MHM) based on Trend Surface Analysis

    Science.gov (United States)

    Wang, Zhiren; Chen, Wen; Dong, Danan; Yu, Chao

    2017-04-01

    Among various approaches developed for detecting the multipath effect in high-accuracy GNSS positioning, Only MHM (Multipath Hemispherical Map) and SF (Sidereal Filtering) can be implemented to real-time GNSS data processing. SF is based on the time repeatability of satellites which just suitable for static environment, while the spatiotemporal repeatability-based MHM is applicable not only for static environment but also for dynamic carriers with static multipath environment such as ships and airplanes, and utilizes much smaller number of parameters than ASF. However, the MHM method also has certain defects. Since the MHM take the mean of residuals from the grid as the filter value, it is more suitable when the multipath regime is medium to low frequency. Now existing research data indicate that the newly advanced Sidereal Filtering (ASF) method perform better with high frequency multipath reduction than MHM by contrast. To solve the above problem and improve MHM's performance on high frequency multipath, we combined binary trend surface analysis method with original MHM model to effectively analyze particular spatial distribution and variation trends of multipath effect. We computed trend surfaces of the residuals within a grid by least-square procedures, and chose the best results through the moderate successive test. The enhanced MHM grid was constructed from a set of coefficients of the fitted equation instead of mean value. According to the analysis of the actual observation, the improved MHM model shows positive effect on high frequency multipath reduction, and significantly reduced the root mean square (RMS) value of the carrier residuals. Keywords: Trend Surface Analysis; Multipath Hemispherical Map; high frequency multipath effect

  18. Analysis and 3D inspection system of drill holes in aeronautical surfaces

    Science.gov (United States)

    Rubio, R.; Granero, L.; Sanz, M.; García, J.; Micó, V.

    2017-06-01

    In aerospace industry, the structure of the aircraft is assembled using small parts or a combination of them that are made with different materials, such as for instance aluminium, titanium, composites or even 3D printed parts. The union between these small parts is a critical point for the integrity of the aircraft. The quality of this union will decide the fatigue of adjacent components and therefore the useful life of them. For the union process the most extended method is the rivets, mainly because their low cost and easy manufacturing. For this purpose it is necessary to made drill holes in the aeronautical surface to insert the rivets. In this contribution, we present the preliminary results of a 3D inspection system [1] for drill holes analysis in aeronautical surfaces. The system, based in optical triangulation, was developed by the Group of Optoelectronic Image Processing from the University of Valencia in the framework of the Airbus Defence and Space (AD&S), MINERVA project (Manufacturing industrial - means emerging from validated automation). The capabilities of the system permits to generate a point cloud with 3D information and GD&T (geometrical dimensions and tolerances) characteristics of the drill hole. For the inner surface defects detection, the system can generate an inner image of the drill hole with a scaled axis to obtain the defect position. In addition, we present the analysis performed for the drills in the wing station of the A-400 M. In this analysis the system was tested for diameters in the range of [10 - 15.96] mm, and for Carbon Fibre.

  19. Acid Aging Effects on Surfaces of PTFE Gaskets Investigated by Thermal Analysis

    Directory of Open Access Journals (Sweden)

    C. Fragassa

    2016-12-01

    Full Text Available This paper investigates the effect of a prolonged acid attack on the surface of PTFE by Thermogravimetric Analysis (TGA and Differential Scanning Calorimetry (DSC. PTFE is very non-reactive, partly because of the strength of carbon–fluorine bonds and for its high crystallinity, and, as a consequence, it is often used in containers and pipework with reactive and corrosive chemicals. The PTFE under analysis is commercialized by two alternative producers in form of Teflon tapes. These tapes are adopted, as gaskets, in process plants where tires moulds are cleaned by acid solutions inside a multistage ultrasonic process. In this case, PTFE shows, in a relatively short operation time, inexplicably phenomena of surface degradation, which could be related, in general terms, to an acid attack. But, even considering the combined effect of ultrasonic waves, temperature, humidity and acid attack, the PTFE properties of resistance nominally exclude the risk of the extreme erosion phenomena as observed. The present experimental research aim at investigating this contradiction. A possible explanation could be related to the presence in the cleaning solution of unexpected fluorides, able to produce fluorinating agents and, thus, degrade carbon-fluorine bonds. Considering more the 300 chemical elements a tire compound consists in, it is really complex to preserve the original chemical composition of the cleaning solution. In this research PTFE samples have been treated with different mixtures of acids with the aim at investigating the different aging effects. The thermal analysis has permitted the experimental characterization of PTFE surface properties after acid attack, providing evidence of the degradation phenomena. In particular, the different acid treatments adopted for accelerating the aging of gaskets have highlighted the different behaviour of the PTFE matrix, but also differences between manufacturers.

  20. Applications of Response Surface-Based Methods to Noise Analysis in the Conceptual Design of Revolutionary Aircraft

    Science.gov (United States)

    Hill, Geoffrey A.; Olson, Erik D.

    2004-01-01

    Due to the growing problem of noise in today's air transportation system, there have arisen needs to incorporate noise considerations in the conceptual design of revolutionary aircraft. Through the use of response surfaces, complex noise models may be converted into polynomial equations for rapid and simplified evaluation. This conversion allows many of the commonly used response surface-based trade space exploration methods to be applied to noise analysis. This methodology is demonstrated using a noise model of a notional 300 passenger Blended-Wing-Body (BWB) transport. Response surfaces are created relating source noise levels of the BWB vehicle to its corresponding FAR-36 certification noise levels and the resulting trade space is explored. Methods demonstrated include: single point analysis, parametric study, an optimization technique for inverse analysis, sensitivity studies, and probabilistic analysis. Extended applications of response surface-based methods in noise analysis are also discussed.

  1. Statistical Analysis of Nitrogen in the Soil of Constructed Wetland with Horizontal Sub-Surface Flow

    Directory of Open Access Journals (Sweden)

    Jakubaszek Anita

    2014-06-01

    Full Text Available The removal of nitrogen compounds in constructed wetlands depends on various physical, chemical and biomechanical factors as well as on conditions of the environment. The paper presents the results of a statistical analysis of the depositing of nitrogen at HSSF (horizontal subsurface flow construcred wetland. The results of the substrate showed that the highest contents of nitrogen existed in the surface soil layer up to 20 cm of the depth. Nitrogen accumulation decreased in the deposit with depth, and in the direction of the wastewater flow.

  2. Theory and applications of surface analysis to semiconductor research and development: a a tutorial

    International Nuclear Information System (INIS)

    Kazmerski, L.L.

    1986-01-01

    The fundamental principles of three of the more common surface analytical spectroscopies - Auger electron spectroscopy (AES), x-ray photoelectron spectroscopy (XPS) and secondary ion mass spectrometry (SIMS) - are discussed in terms of their physics, strengths and limitations. The focus of the discussions is on the application of these characterization tools to semiconductor electronics, specially for failure analysis and preventive measurements. An application, illustrating the complementary nature of the outputs of the three methods, examines the Au-GaAs Schotty barrier, specially the nature of the interfacial reaction. (Author) [pt

  3. Principal component analysis of bacteria using surface-enhanced Raman spectroscopy

    Science.gov (United States)

    Guicheteau, Jason; Christesen, Steven D.

    2006-05-01

    Surface-enhanced Raman scattering (SERS) provides rapid fingerprinting of biomaterial in a non-destructive manner. The problem of tissue fluorescence, which can overwhelm a normal Raman signal from biological samples, is largely overcome by treatment of biomaterials with colloidal silver. This work presents a study into the applicability of qualitative SER spectroscopy with principal component analysis (PCA) for the discrimination of four biological threat simulants; Bacillus globigii, Pantoea agglomerans, Brucella noetomae, and Yersinia rohdei. We also demonstrate differentiation of gram-negative and gram-positive species and as well as spores and vegetative cells of Bacillus globigii.

  4. Installation and Preliminary Test of the Ion Accelerator for the Surface Analysis at KOMAC

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Dae Il; Ahn, Tae Sung; Seo, Dong Hyuk; Kwon, Hyeok Jung; Kim, Cho Rong; Park, Jun Kue; Cho, Yong Sub [KAERI, Daejeon (Korea, Republic of)

    2016-05-15

    An electrostatic tandem accelerator, which had been operating over 25 years at KIGAM (Korea Institute of Geoscience and Mineral Resources), is moved to KOMAC (Korea Multi-purpose Accelerator Complex) last year. For the purpose of supplying the qualified and quantified data from the irradiated species as part of the user service of KOMAC. The accelerator is a pelletron with tandem type. The ion accelerator for surface analysis was moved at KOMAC last year. The installation with alignment was done. The conditioning of high voltage was operated up to 1.7 MV. The beam transmission to PIXE beam line was achieved as 51%.

  5. Surface thermal analysis of North Brabant cities and neighbourhoods during heat waves

    Directory of Open Access Journals (Sweden)

    Leyre Echevarria Icaza

    2016-03-01

    Full Text Available The urban heat island effect is often associated with large metropolises. However, in the Netherlands even small cities will be affected by the phenomenon in the future (Hove et al., 2011, due to the dispersed or mosaic urbanisation patterns in particularly the southern part of the country: the province of North Brabant. This study analyses the average night time land surface temperature (LST of 21 North-Brabant urban areas through 22 satellite images retrieved by Modis 11A1 during the 2006 heat wave and uses Landsat 5 Thematic Mapper to map albedo and normalized difference temperature index (NDVI values. Albedo, NDVI and imperviousness are found to play the most relevant role in the increase of night-time LST. The surface cover cluster analysis of these three parameters reveals that the 12 “urban living environment” categories used in the region of North Brabant can actually be reduced to 7 categories, which simplifies the design guidelines to improve the surface thermal behaviour of the different neighbourhoods thus reducing the Urban Heat Island (UHI effect in existing medium size cities and future developments adjacent to those cities.

  6. Advanced growth and surface analysis system for in situ studies of interface formation. Annual technical report

    International Nuclear Information System (INIS)

    Sayers, D.E.; Nemanich, R.J.; Wang, Z.

    1994-01-01

    This is the first annual report for developing an advanced integrated in situ UHV growth/analysis system for synchrotron radiation studies of interface and surface reactions which lead to epitaxial structures on Si, Ge, and Si 1-x Ge x alloys. This equipment will allow one to use techniques based on synchrotron radiation, such as photoemission, x-ray standing wave (XSW), and surface x-ray absorption spectroscopy (SXAFS) to determining the electronic states and atomic configurations of surfaces in metal-silicon, metal-germanium and metal-silicon-germanium alloys. Since the award of the contract the authors have completed a detailed design of the overall system, identified commercially available equipment which fits the requirements and have purchased or ordered all of this equipment. They have also custom designed a considerable amount of equipment which is not available commercially because of the special requirements. This includes both of the UHV chambers, sample manipulators, and a mobile support stand. In this report, they will describe the design and purchase status of the system. An overview of the equipment purchase status is given in Appendix 1. The details of their custom designed growth and analytical chambers are given in Appendix 2

  7. Recognition and prediction of individual and combined muscular activation modes via surface EMG analysis

    Directory of Open Access Journals (Sweden)

    Daniel Graupe

    2010-09-01

    Full Text Available The paper discusses how recognition of individual and combined muscular activation modes (functions and the prediction of intended such modes can be accomplished by identifying parameters of noninvasive surface EMG signals. It outlines the mathematical analysis of surface EMG signal to facilitate such recognition and related prediction, including recognition of intention (in terms of attempts to activate motor functions from the EMG, without accessing the CNS itself, in cases where a patient, say, a high-level amputee does not have the final-activation muscles and joints. The EMG activity thus allows to interpret and recognize CNS commands from minute variations in the parameters of surface EMG signals that record changes in the firing of motor neurons triggering contractions in related muscle fibers. We note that although in popular media this is sometimes referred to as detection of “thoughts”, no thoughts are detected, but only motor-outcomes of thoughts as found in the EMG signal. Examples of concrete cases where such recognition or prediction were accomplished in the author’s lab and in devices that came out of that lab, are given as are references to these in the literature over the last 35 years.

  8. Lateral Trunk Surface as a new parameter to estimate live body weight by Visual Image Analysis

    Directory of Open Access Journals (Sweden)

    S. Terramoccia

    2010-02-01

    Full Text Available Live weight of 74 milking Mediterranean buffaloes (Bubalus bubalis L. have been estimated by Visual Image Analysis. The total surface of lateral profile, tested in previous researches with viable result, was substituted by the measurement of the Lateral Trunk Surface (LTrS. The measurements were recorded by a camera equipped by a laser distance recorder and data were elaborated by a specific software. This parameter, eliminating the surface of neck, head and legs, that are less easily measurable, simplified and accelerated the procedure. Correlation between LTrS and live weight was r = 0.90 (P < 0.01. A significant equation (P < 0.01 was obtained from the recorded data of a random sample of 38 buffaloes. When the validation of the equation was tested on the other 36 subjects, the estimated live weight had a mean of 691.74 kg ± 68.55. This was corresponding to a 1.08% overestimation of the real weight.

  9. Disilicate Dental Ceramic Surface Preparation by 1070 nm Fiber Laser: Thermal and Ultrastructural Analysis.

    Science.gov (United States)

    Fornaini, Carlo; Poli, Federica; Merigo, Elisabetta; Brulat-Bouchard, Nathalie; El Gamal, Ahmed; Rocca, Jean-Paul; Selleri, Stefano; Cucinotta, Annamaria

    2018-01-31

    Lithium disilicate dental ceramic bonding, realized by using different resins, is strictly dependent on micro-mechanical retention and chemical adhesion. The aim of this in vitro study was to investigate the capability of a 1070 nm fiber laser for their surface treatment. Samples were irradiated by a pulsed fiber laser at 1070 nm with different parameters (peak power of 5, 7.5 and 10 kW, repetition rate (RR) 20 kHz, speed of 10 and 50 mm/s, and total energy density from 1.3 to 27 kW/cm²) and the thermal elevation during the experiment was recorded by a fiber Bragg grating (FBG) temperature sensor. Subsequently, the surface modifications were analyzed by optical microscope, scanning electron microscope (SEM), and energy dispersive X-ray spectroscopy (EDS). With a peak power of 5 kW, RR of 20 kHz, and speed of 50 mm/s, the microscopic observation of the irradiated surface showed increased roughness with small areas of melting and carbonization. EDS analysis revealed that, with these parameters, there are no evident differences between laser-processed samples and controls. Thermal elevation during laser irradiation ranged between 5 °C and 9 °C. A 1070 nm fiber laser can be considered as a good device to increase the adhesion of lithium disilicate ceramics when optimum parameters are considered.

  10. Surface free energy analysis of oil palm empty fruit bunches fiber reinforced biocomposites

    Science.gov (United States)

    Suryadi, G. S.; Nikmatin, S.; Sudaryanto; Irmansyah; Sukaryo, S. G.

    2017-05-01

    Study of the size effect of natural fiber from oil palm empty fruit bunches (OPEFB) as filler, onto the contact angle and surface free energy of fiber reinforced biocomposites has been done. The OPEFB fibers were prepared by mechanical milling and sieving to obtain various sizes of fiber (long-fiber, medium-fiber, short-fiber, and microparticle). The biocomposites has been produced by extrusion using single-screw extruder with EFB fiber as filler, recycled Acrylonitrile Butadiene Styrene (ABS) polymer as matrix, and primary antioxidant, acid scavanger, and coupling agent as additives. The obtained biocomposites in form of granular, were made into test piece by injection molding method. Contact angles of water, methanol, and hexane on the surface of biocomposites at room temperature were measured using Phoenix 300 Contact Angle Analyzer. The surface free energy (SFE) and their components were calculated using three previous known methods (Girifalco-Good-Fowkes-Young (GGFY), Owens-Wendt, and van Oss-Chaudhury-Good (vOCG)). The results showed that total SFE of Recycled ABS as control was about 24.38 mJ/m2, and SFE of biocomposites was lower than control, decreased with decreasing of EFB fiber size as biocomposites filler. The statistical analysis proved that there are no statistically significant differences in the value of the SFE calculated with the three different methods.

  11. Analysis of bulk and surface contributions in the neutron skin of nuclei

    International Nuclear Information System (INIS)

    Warda, M.; Vinas, X.; Roca-Maza, X.; Centelles, M.

    2010-01-01

    The neutron skin thickness of nuclei is a sensitive probe of the nuclear symmetry energy and has multiple implications for nuclear and astrophysical studies. However, precision measurements of this observable are difficult to obtain. The analysis of the experimental data may imply some assumptions about the bulk or surface nature of the formation of the neutron skin. Here we study the bulk or surface character of neutron skins of nuclei following from calculations with Gogny, Skyrme, and covariant nuclear mean-field interactions. These interactions are successful in describing nuclear charge radii and binding energies but predict different values for neutron skins. We perform the study by fitting two-parameter Fermi distributions to the calculated self-consistent neutron and proton densities. We note that the equivalent sharp radius is a more suitable reference quantity than the half-density radius parameter of the Fermi distributions to discern between the bulk and surface contributions in neutron skins. We present calculations for nuclei in the stability valley and for the isotopic chains of Sn and Pb.

  12. Comparison of two intraoral scanners based on three-dimensional surface analysis.

    Science.gov (United States)

    Lee, Kyung-Min

    2018-02-12

    This in vivo study evaluated the difference of two well-known intraoral scanners used in dentistry, namely iTero (Align Technology) and TRIOS (3Shape). Thirty-two participants underwent intraoral scans with TRIOS and iTero scanners, as well as conventional alginate impressions. The scans obtained with the two intraoral scanners were compared with each other and were also compared with the corresponding model scans by means of three-dimensional surface analysis. The average differences between the two intraoral scans on the surfaces were evaluated by color-mapping. The average differences in the three-dimensional direction between each intraoral scans and its corresponding model scan were calculated at all points on the surfaces. The average differences between the two intraoral scanners were 0.057 mm at the maxilla and 0.069 mm at the mandible. Color histograms showed that local deviations between the two scanners occurred in the posterior area. As for difference in the three-dimensional direction, there was no statistically significant difference between two scanners. Although there were some deviations in visible inspection, there was no statistical significance between the two intraoral scanners.

  13. Comparison of two intraoral scanners based on three-dimensional surface analysis

    Directory of Open Access Journals (Sweden)

    Kyung-Min Lee

    2018-02-01

    Full Text Available Abstract Background This in vivo study evaluated the difference of two well-known intraoral scanners used in dentistry, namely iTero (Align Technology and TRIOS (3Shape. Methods Thirty-two participants underwent intraoral scans with TRIOS and iTero scanners, as well as conventional alginate impressions. The scans obtained with the two intraoral scanners were compared with each other and were also compared with the corresponding model scans by means of three-dimensional surface analysis. The average differences between the two intraoral scans on the surfaces were evaluated by color-mapping. The average differences in the three-dimensional direction between each intraoral scans and its corresponding model scan were calculated at all points on the surfaces. Results The average differences between the two intraoral scanners were 0.057 mm at the maxilla and 0.069 mm at the mandible. Color histograms showed that local deviations between the two scanners occurred in the posterior area. As for difference in the three-dimensional direction, there was no statistically significant difference between two scanners. Conclusions Although there were some deviations in visible inspection, there was no statistical significance between the two intraoral scanners.

  14. Infrared surface analysis using a newly developed thin-sample preparation system.

    Science.gov (United States)

    Nagai, Naoto; Nishiyama, Itsuo; Kishima, Yoshio; Iida, Katsuhiko; Mori, Koichi

    2009-01-01

    We developed a new sampling system, the Nano Catcher, for measuring the surface chemical structure of polymers or industrial products and we evaluated the performance of the system. The system can directly pick up surface species whose depth is on the order of approximately 100 nm and can easily provide a sample for a Fourier transform infrared (FT-IR) system without the necessity of passing it over to a measurement plate. The FT-IR reflection data obtained from the Nano Catcher were compared with those obtained using the attenuated total reflection (ATR) method and sampling by hand. Chemical structural analysis of a depth region from a few tens of nanometers to a few hundred nanometers can be directly performed using this system. Such depths are beyond the scope of conventional X-ray photoelectron spectroscopy (XPS) and ATR methods. We can expect the use of the Nano Catcher system to lead to a great improvement in the detection of signals of surface species in these depth regions.

  15. Inference of sea surface temperature, near surface wind, and atmospheric water by Fourier analysis of Scanning Multichannel Microwave Radiometer data

    Science.gov (United States)

    Rosenkranz, P. W.

    1981-01-01

    The Scanning Multichannel Microwave Radiometer measures thermal microwave emission from the earth in both polarizations at wavelengths of 0.8, 1.4, 1.7, 2.8 and 4.6 cm. Similar instruments were launched on Nimbus 7 and Seasat. Both spatial resolution on the earth and relative sensitivity to different geophysical parameters change with wavelength. Therefore, spatial Fourier components of geophysical parameters are inferred from the corresponding Fourier components of the radiometer measurements, taking into account the different dependence of signal-to-noise ratio on spatial frequency for each radiometer wavelength. The geophysical parameters are sea surface temperature, near-surface wind speed, integrated water vapor mass, integrated liquid water mass, and the product of rainfall rate with height of the rain layer. The capabilities and limitations of the inversion method are illustrated by means of data from the North Atlantic and from tropical storms.

  16. MD simulation: determination of the physical properties and surface vaporization analysis of beryllium armours

    International Nuclear Information System (INIS)

    Prinzio, M. Di; Aquaro, D.

    2006-01-01

    The erosion of the divertor and of the first wall determined on the base of the anticipated operating conditions, is a critical issue that could affect the performance and the operating schedule of the nuclear fusion reactor ITER. This paper deals with the analysis of beryllium thermal properties by means of MD simulations, in order to better predict thermal behaviour of beryllium armoured PFCs in fusion devices. The importance of this analysis is clearly connected to thermal response evaluation of PFCs to high heat flux exposure, during off-normal events and Edge Localized Modes. The ensuing strong over-heating, in fact, produces material ablation through vaporization of surface material layers and possible loss of melting material. The overall PFCs erosion has bearings on plasma contamination, due to eroded material transport, and components lifetime, due to armour thickness reduction. An important feature of beryllium is its high vapour pressure. During thermal transients the strong vaporization keeps surface temperature relatively low but eroded thickness results high as well. Small changes in beryllium vapour pressure produce not negligible differences in thermal analyses results. On the basis of available force fields, classical Molecular Dynamics simulations have been carried out in order to better understand surface vaporization in tokamak conditions and to evaluate the effect of beryllium oxides formation. This effect has been successfully modelled by MD simulation, carried out with Moldy code. Morse stretching and bending potential for Be-O bond simulation have been used, and partial charges method, accounting for molecular polarity, has been employed. Since during short thermal transients, such as ELMs, only a few microns of Be armour will be overheated and reach melting threshold, the effective thermal conductivity is very important in determining the temperature evolution of surface layers and the ensuing erosion. Thermal conductivity can be evaluated

  17. Laser-based mass spectrometry for in situ chemical composition analysis of planetary surfaces

    Science.gov (United States)

    Frey, Samira; Neuland, Maike B.; Grimaudo, Valentine; Moreno-García, Pavel; Riedo, Andreas; Tulej, Marek; Broekmann, Peter; Wurz, Peter

    2016-04-01

    Mass spectrometry is an important analytical technique in space research. The chemical composition of planetary surface material is a key scientific question on every space mission to a planet, moon or asteroid. Chemical composition measurements of rocky material on the surface are of great importance to understand the origin and evolution of the planetary body.[1] A miniature laser ablation/ionisation reflectron- type time-of-flight mass spectrometer (instrument name LMS) was designed and built at the University of Bern for planetary research.[2] Despite its small size and light weight, the LMS instrument still maintains the same capabilities as large laboratory systems, which makes it suitable for its application on planetary space missions.[3-5] The high dynamic range of about eight orders of magnitude, high lateral (μm-level) and vertical (sub-nm level) resolution and high detection sensitivity for almost all elements (10 ppb, atomic fraction) make LMS a versatile instrument for various applications. LMS is a suitable instrument for in situ measurements of elemental and isotope composition with high precision and accuracy. Measurements of Pb- isotope abundances can be used for dating of planetary material. Measurements of bio-relevant elements allow searching for past or present life on a planetary surface. The high spatial resolution, both in lateral and vertical direction, is of considerable interest, e.g. for analysis of inhomogeneous, extraterrestrial samples as well as weathering processes of planetary material. References [1] P. Wurz, D. Abplanalp, M. Tulej, M. Iakovleva, V.A. Fernandes, A. Chumikov, and G. Managadze, "Mass Spectrometric Analysis in Planetary Science: Investigation of the Surface and the Atmosphere", Sol. Sys. Res., 2012, 46, 408. [2] U. Rohner, J.A. Whitby, P. Wurz, "A miniature laser ablation time of flight mass spectrometer for in situ planetary exploration" Meas. Sci. Tch., 2003, 14, 2159. [3] M. Tulej, A. Riedo, M.B. Neuland, S

  18. Design of the optimum insulator gate bipolar transistor using response surface method with cluster analysis

    CERN Document Server

    Wang, Chi Ling; Huang Sy Ruen; Yeh Chao Yu

    2004-01-01

    In this paper, a statistical methodology that can be used for the optimization of the Insulator Gate Bipolar Transistor (IGBT) devices is proposed. This is achieved by integrating the response surface method (RSM) with cluster analysis, weighted composite method and genetic algorithm (GA). The device characteristic of IGBT was simulated based upon the fabrication simulator, ATHENA, and the device simulator, ATLAS. This methodology, yielded another way to investigate the IGBT device and to make a decision in the tradeoff between the breakdown voltage and the on-resistance. In this methodology, we also show how to use cluster analysis to determine the dominant factors that are not visible in the screening of all experiments. 20 Refs.

  19. Failure Analysis and Thermochemical Surface Engineering of Bearings in the Wind Turbine Drivetrain

    DEFF Research Database (Denmark)

    West, Ole H.E.; Dahl, Kristian Vinter; Christiansen, Thomas Lundin

    backscatter diffraction (EBSD) and ion channelling contrast imaging (ICCI) were used. The gap between RLM and SEM (providing a good overview over the crack morphology) and TEM (providing very detailed information but from a very limited part of the sample) could be covered by the use of EBSD and ICCI...... charged rollers to reproduce WEC formation. The influence of different hoop stress levels was studied. The fracture surfaces as well as formed WECs were investigated. A detrimental effect of higher hoop stress levels on roller lifetime was found and based on the analysis of the formed WECs an incremental...... increase of WEA formation with each cycle was suggested. By X-ray diffraction stress analysis the nonuniform build-up of compressive stresses under testing was identified. Deep nitriding is considered as a potential remedy against WEC failure. Therefore nitriding experiments were conducted to study...

  20. Chemical imaging and solid state analysis at compact surfaces using UV imaging

    DEFF Research Database (Denmark)

    Wu, Jian X.; Rehder, Sönke; van den Berg, Frans

    2014-01-01

    , and microcrystalline cellulose together with magnesium stearate as excipients were used as model materials in the compacts. The UV imaging based drug and excipient distribution was in good agreement with hyperspectral NIR imaging. The UV wavelength region can be utilized in distinguishing between glibenclamide......Fast non-destructive multi-wavelength UV imaging together with multivariate image analysis was utilized to visualize distribution of chemical components and their solid state form at compact surfaces. Amorphous and crystalline solid forms of the antidiabetic compound glibenclamide...... and excipients in a non-invasive way, as well as mapping the glibenclamide solid state form. An exploratory data analysis supported the critical evaluation of the mapping results and the selection of model parameters for the chemical mapping. The present study demonstrated that the multi-wavelength UV imaging...