WorldWideScience

Sample records for superplastic deformation behavior

  1. Superplastic Deformation of TC6 Alloy

    Directory of Open Access Journals (Sweden)

    DING Ling

    2016-12-01

    Full Text Available The superplastic tensile tests of TC6 alloy were conducted in the temperature range of 800-900℃ by using the maximum m value superplasticity deformation (Max m SPD method and the constant strain rate deformation method at the strain rate range of 0.0001-0.1 s-1. The stress-strain curve of the tensile tests was obtained and the microstructure near the fracture were analyzed by metallographic microscope. The result shows that the superplasticity of TC6 alloy is excellent, and the elongation increases first and then decreases with the increase of strain rate or temperature. When the temperature is 850℃ and strain rate is 0.001 s-1 at constant stain rate tensile tests, the elongation reaches up to 993%. However, the elongation using Max m SPD method at 850℃ is 1353%. It is shown that the material can achieve better superplasticity by using Max m SPD tensile compared to constant stain rate tensile under the same temperature. The superplastic deformation of TC6 alloy can enhance the dynamic recrystallization behavior significantly, the dynamic recrystallization behavior is promoted when strain rate and temperature are increased.

  2. The Neighbor Switching Mechanism of Superplastic Deformation

    Science.gov (United States)

    Sherwood, David John

    At one time the notion that crystal plasticity resulted from the simultaneous motion of lattice planes over one another was entertained. This idea was displaced by the concept that relative atomic motions occur sequentially when dislocations move through the crystal. Similarly, McLean suggested that grains switch neighbors sequentially in a polycrystalline material undergoing superplastic flow. Morral and Ashby observed that the neighbor switching reactions in a froth occurred at irregular cells, and that these irregularities were associated with dislocations in the cellular array. They introduced cellular dislocation glide as a model for superplastic flow, and suggested that if the concentration of these defects required to make the froth flow increased with the flow stress, then the froth would have a non-Newtonian viscosity, like many superplastic materials. Cahn and Padawer pointed out that cellular dislocation climb was used as a model for grain growth by Hillert; this process results in the elimination of cells from the froth. Sato, Kuribayashi and Horiuchi used cellular dislocation climb to model both grain motion and the deformation-enhanced grain growth which can accompany superplastic flow. Here, the neighbor switching mechanism of superplastic deformation is developed as a topic in dislocation theory. The compatibility theory of dislocations is developed at an introductory level with exterior calculus. "Compatibility" of a cellular array corresponds to statements, a la Rivier, about the distribution of edges amongst the cells. The theory of dislocation motion, or crystal plasticity, is also developed with exterior calculus. Morral and Ashby's constitutive relationship for superplastic flow is analyzed and two models for deformation-enhanced grain growth are developed. The constitutive relationship and grain growth kinetics for superplastic flow are illustrated by modelling the behavior exhibited by single phase (Sn-1% Bi) and quasi -single phase (7475 Al

  3. Cavity coalescence in superplastic deformation

    Energy Technology Data Exchange (ETDEWEB)

    Stowell, M.J.; Livesey, D.W.; Ridley, N.

    1984-01-01

    An analysis of the probability distribution function of particles randomly dispersed in a solid has been applied to cavitation during superplastic deformation and a method of predicting cavity coalescence developed. Cavity size distribution data were obtained from two microduplex nickel-silver alloys deformed superplastically to various extents at elevated temperature, and compared to theoretical predictions. Excellent agreement occurred for small void sizes but the model underestimated the number of voids in the largest size groups. It is argued that the discrepancy results from a combination of effects due to non-random cavity distributions and to enhanced growth rates and incomplete spheroidization of the largest cavities.

  4. Microstructure evolution and fracture behavior in superplastic deformation of hot-rolled AZ31 Mg alloy sheet

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    Yin, D.L.; Zhang, K.F.; Wang, G.F. [School of Material Science and Technology, Harbin Inst. of Tech. (China)

    2005-07-01

    Fine-grained AZ31 magnesium alloy sheets were prepared through hot rolling process. The superplastic properties of hot-rolled AZ31 Mg alloy was examined by uniaxial tensile tests at a temperature range 250{proportional_to}450 C and strain rate range 0.7 x 10{sup -3}{proportional_to}1.4 x 10{sup -1} s{sup -1}. Optical and scanning electronic microscope (SEM) were used to observe the microstructure evolution and fracture behavior in superplastic deformation of AZ31 Mg alloy and the values of deformation activation energy at various temperatures were calculated. It is demonstrated that, the hot-rolled AZ31 alloy begins to exhibit superplasticity from 300 C and a maximum elongation of 362.5% is obtained at 400 C and 0.7 x 10{sup -3} s{sup -1}. In the temperature range 300{proportional_to}400 C, the dominant superplastic deformation mechanism is grain boundary sliding (GBS) controlled by grain boundary diffusion and the influence of temperature on the fracture behavior of AZ31 Mg alloy is characterized by the change from dimple-aggregating type to intercrystalline one. (orig.)

  5. Superplastic Deformation Behavior of Hot-rolled AZ31 Magnesium Alloy Sheet at Elevated Temperatures

    Institute of Scientific and Technical Information of China (English)

    ZHANG Kaifeng; YIN Deliang; WANG Guofeng; HAN Wenbo

    2006-01-01

    Uniaxial tensile tests were carried out in the temperature range of 250-450 ℃ and the strain rate range of 0.7×10-3-1.4×10-1s-1 to evaluate the superplasticity of AZ31 Mg alloy. The threshold stress which characterizes the difficulty for grain boundary sliding was calculated at various temperatures. The surface relieves of superplastically deformed specimens were observed by using a scanning electronic microscope (SEM). Results show that, at the temperature of 400 ℃ and strain rate of 0.7×10-3 s-1, the strain rate sensitivity exponent, i e, m value reaches 0.47 and the maximum elongation of 362.5% is achieved. Grain boundary sliding (GBS) is the primary deformation mechanism and characterized by a pronounced improvement in the homogeneity with increasing temperatures. A large number of filaments were formed at the end of deformation and intergranular cavities were produced with the necking and fracture of filaments. Finally, the model for the formation of intergranular cavities was proposed.

  6. Microstructure Evolution and Mechanical Behavior of Ultrafine Ti-6Al-4V During Low Temperature Superplastic Deformation (Postprint)

    Science.gov (United States)

    2016-09-13

    alloys , Russ. J. Non- Ferrous Met. 56 (2016) 437e441. [40] B.B. Straumal, X. Sauvage, B. Baretzky, A.A. Mazilkin, R.Z. Valiev, Grain boundary films in...dynamic coarsening response and plastic-flow behavior of the alloy with a mean size of α (sub)grains and β particles of 0.1–0.4 μm were determined via a...Very limited cavitation was observed in the specimens after superplastic deformation under optimal conditions. 15. SUBJECT TERMS Titanium alloy ; Low

  7. Effect of grain boundary microstructure on superplastic deformation of Al-Li-Cu-Mg-Zr alloy

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    Kobayashi, S.; Yoshimura, T.; Tsurekawa, S.; Watanabe, T. [Tohoku Univ., Sendai (Japan). Dept. of Machine Intelligence and Syst. Eng.

    1999-07-01

    It is common knowledge that grain boundary sliding (GBS) is the most important deformation mechanism for superplastic deformation. In this investigation, Al-Li-Cu-Mg-Zr alloys having two distinct microstructures were produced to examine the effect of grain boundary (GB) microstructure on superplastic deformation. The effective GB microstructure to develop the superplastic deformation is discussed. Specimens with homogeneous and {l_brace}011{r_brace} textured grains, including high frequency of low-angle GBs showed superplastic behavior. The texture was weakened and most of low-angle GBs were changed into random GBs during deformation. Mean grain size increased slightly with deformation. On the other hand, specimens with heterogeneous and randomly oriented grains, with a high frequency of random GBs resulted in nonsuperplastic behavior. This microstructure was essentially unchanged by deformation. Extensive cavitation at GB triple junctions was also observed after superplastic deformation. In particular, cavities were most likely to form at the triple junctions composed of two or more random GBs. We will discuss the development of superplasticity through the optimization of GB microstructures in polycrystalline materials. (orig.)

  8. CONSTITUTE EQUATIONS OF 40Cr STEEL UNDER SUPERPLASTIC COMPRESSIVE DEFORMATION

    Institute of Scientific and Technical Information of China (English)

    K.K. Zhang; Y.L. Yang; S.Z. Liu; C.X. Han; D. Xu

    2003-01-01

    The microstructure of 40Cr steel sample and its surface is ultra-fined through saltbath cyclic quenching and high frequency hardening, then the superplasticity is studied under isothermal superplastic compressive deformation condition. The experimental results indicate that the stress-strain curves are shown to take place obvious superplastic flow characteristic at the temperature of 730-770℃ and at the initial strain rate of (1.7-5.0)× 10-4s-1. Its strain rate sensitivity is 0.30-0.38, the steady superplastic flow stress is 60-70MPa, the superplastic flow activation energy is 198-217kJ/mol,and it is close to α-Fe grain boundary self-diffusion activation energy. The superplastic compressive constitute equations of this steel are correspondingly set up. Due to the finer microstructure of high frequency hardening, it appears bigger strain rate sensitivity value, smaller the steady superplastic flow stress and the superplastic flow activation energy, so it has better superplastic deformation capability.

  9. Superplasticity

    Science.gov (United States)

    Rouxel, T.

    Permanent deformation of a material through flow, e.g., creep, viscosity, viscoplasticity, gets easier as the grain size in the material gets smaller. In the most spectacular cases, relative extensions greater than 100% (nominal strain > 1) can be obtained at relatively low temperatures compared with the temperatures usually required to observe creep in materials: this is the effect known as superplasticity. Typically, superplasticity only occurs in fine-grained dense materials (grains 0.5Tmelting, when such a temperature has any meaning (materials sometimes decomposing before melting). Even in ancient times, smiths made good use of this remarkable property to forge tough, hard steel blades. The steel used by the Persians at the time of the crusades, and by Saladin's armies, or Damascus steel, is one of the greatest achievements of metallurgy and the forge, where the choice of alloy at the outset (in this case a steel with a high carbon content, known as wootz, from India) and the masterly control of a judicious forging cycle (the thickness of the initial ingot was first reduced by a factor of about 10 by hammering) produced a material with ideal fine microstructure for making sharp cutting blades that could also resist mechanical shocks. Figure 9.1 illustrates the phenomenon of superplastic behaviour for a steel containing 1.6% carbon (ultrahigh carbon steel), with a fine microstructure, close to Damascus steel, which seems to have been produced first in India in the fourth century BC.

  10. Deformation of superplastic alloys at relatively low strain rates

    Energy Technology Data Exchange (ETDEWEB)

    Grivas, D.

    1978-02-01

    The superplastic and sub-superplastic creep properties of Pb-Sn eutectic and Al-Zn eutectoid alloys were studied. Various thermomechanical treatments we tested to check the possibilities of whether the subsuperplastic deformation mechanism is affected by these treatments. All thermomechanical histories were found to reveal the same stress exponent, which is believed to be indicative of the predominant mechanism. The mechanical data in the low stress region lead us to suggest that dislocation glide is the predominant mechanism in this region. At higher stresses extensive grain boundary sliding takes place and the dislocation movement is directed to relieve the stress concentration developed by the grain movement.

  11. Superplasticity and superplastic forming of ceramics

    Energy Technology Data Exchange (ETDEWEB)

    Nieh, T.G.; Wadsworth, J.

    1994-05-01

    Recent advances in the basic understanding of superplasticity and superplastic forming of ceramics are reviewed. Deformation mechanisms as well as microstructural requirements for superplastic ceramics are discussed. Microstructural effects, such as grain size, dynamic grain growth, and the presence of grain-boundary liquid phases, on the superplastic properties and deformation behavior of ceramics are addressed. Superplastic forming, and particularly biaxial gas-pressure forming, of several ceramics, including YTZP and Al{sub 2}O{sub 3}/YTZP, is also presented. The forming behavior of these ceramics is correlated with that obtained from conventional uniaxial tests. Examples of concurrent superplastic forming and diffusion bonding (SPF/DB) of metal-ceramic hybrids are given.

  12. Influence of superplastic deformation on the anisotropy of 03Kh26N6T steel

    Science.gov (United States)

    Fuad, M. F. Akhmed; Tsepin, M. A.; Lobach, A. A.

    1991-10-01

    The maximum difference in relative elongation parallel and transverse to the rolling direction at the optimum temperature of superplastic deformation does not completely characterize the anisotropy since it is caused by the increased sensitivity of superplastic deformation to transverse grain dimensions in these directions.

  13. Deformation and reconstruction mechanisms in coarse-grained superplastic Al-Mg alloys

    NARCIS (Netherlands)

    Soer, W. A.; Chezan, A. R.; De Hosson, J. Th. M.

    2006-01-01

    This paper concentrates on the superplastic response of fine-grained and coarse-grained Al-Mg alloys under uniaxial tension. To identify the main characteristics of superplastic deformation and to determine the optimum deformation parameters, the microstructure and dislocation substructure of the al

  14. Carburizing of Duplex Stainless Steel (DSS) Under Compression Superplastic Deformation

    Science.gov (United States)

    Ahamad, Nor Wahida; Jauhari, Iswadi

    2012-12-01

    A new surface carburizing technique which combines superplastic deformation with superplastic carburizing (SPC) is introduced. SPC was conducted on duplex stainless steel under compression mode at a fixed 0.5 height reduction strain rates ranging from 6.25 × 10-5 to 1 × 10-3 s-1 and temperature ranging from 1173 K to 1248 K (900 °C to 975 °C). The results are compared with those from conventional and non-superplastic carburizing. The results show that thick hard carburized layers are formed at a much faster rate compared with the other two processes. A more gradual hardness transition from the surface to the substrate is also obtained. The highest carburized layer thickness and surface hardness are attained under SPC process at 1248 K (975 °C) and 6.25 × 10-5 s-1 with a value of (218.3 ± 0.5) μm and (1581.0 ± 5.0) HV respectively. Other than that, SPC also has the highest scratch resistance.

  15. Effect of Post-Rolling after ECAP on Superplastic Behavior of Commercial Al-Mg Alloy

    Institute of Scientific and Technical Information of China (English)

    Dong Hyuk Shin; Byung Du Ahn; Hyun Soo; Woo Kyeom Kim; Kyung-Tae Park

    2004-01-01

    A commercial Al-Mg alloy was subjected to equal channel angular pressing of 4 passes with and without postrolling, and the effects of post-rolling on the deformation characteristics of the alloy at 723 K were examined. Post-rolling was found to influence the deformation behavior significantly. The deformation behavior of the alloy processed only by equal channel angular pressing was characterized by (a) localized deformation indicated by severe surface prominence and depression, (b) the strain rate sensitivity of 0.33, and (c) moderate high strain rate superplastic elongations. By contrast, that of the alloy processed by equal channel angular pressing and post-rolling (70 % thickness reduction) was manifested by (a) uniform deformation associated with grain boundary sliding throughout the sample, (b) a sigmoidal behavior showing the strain rate sensitivity of 0.45 at the intermediate strain rates in the logarithmic stress-strain rate curve, and (c) very large high strain rate superplastic elongations.

  16. Discontinuous Dynamic Recrystallization of Inconel 718 Superalloy During the Superplastic Deformation

    Science.gov (United States)

    Huang, Linjie; Qi, Feng; Hua, Peitao; Yu, Lianxu; Liu, Feng; Sun, Wenru; Hu, Zhuangqi

    2015-09-01

    The superplastic behavior of Inconel 718 superalloy with particular emphasis on the microstructural evolution has been systematically investigated through tensile tests at the strain rate of 10-3 s-1 and the temperatures ranging from 1223 K to 1253 K (950 °C to 980 °C). Its elongations exceeded 300 pct under all of the experimental conditions and peaked a maximum value of 520 pct at 1223 K (950 °C). Moreover, the stress reached the top value at the strain of 0.3, and then declined until the tensile failure. In addition, we have found that the grain size reduced after deformation while the δ phase precipitation increased. Microstructural evolution during the superplasticity was characterized via transmission electron microscope, and the randomly distributed dislocation, dislocation network, dislocation arrays, low-angled subgrains, and high-angled recrystallized new grains were observed in sequence. These new grains were found to nucleate at the triple junction, twin boundary, and near the δ phase. Based on these results, it is deemed that the discontinuous dynamic recrystallization occurred as the main mechanism for the superplastic deformation of Inconel 718 alloy.

  17. Effect of current pulses on fracture morphology in superplastic deformation of 2091 Al-Li alloy

    Institute of Scientific and Technical Information of China (English)

    1999-01-01

    The effect of current pulses on the fracture morphology in the superplastic deformation of 2091 AlLi alloy at two kinds of initial strain rate ((ε)1 = 3.33 × 10 -3 s-1;(ε)2= 3.33 × 10-2 s- 1 ) was investigated. Experimental results show that current pulse turns fracture of superplastic deformation at low strain rate from local interior fracture morphology to typical fracture by growth and interlinkage of cavities, and at high strain rate from rough grain boundary surface to smooth grain boundary surface. It is indicated that the characteristic, that current pulse promotes atomic diffusion, maintains an equiaxial grain microstructure at low strain rate, and accelerates the development of diffusional type of cavity and relaxes stress concentration at triple junction of grain boundaries at high strain rate, and makes the superplastic deformation at two kinds of strain rate show a normal superplastic fracture morphology.

  18. Superplastic deformation of commercial 00Cr22Ni5Mo3N0.17 duplex stainless steel

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    The superplastic behavior of a commercial duplex stainless steel has been studied by means of isothermal hot tensile testat temperatures of 850-1050℃ for the initial strain rates ranging from 3×l0-4 s-1 to 5X10-2 s-1. At 960℃, the best superplastic de-formation that caused the maximum elongation greater than 840% was obtained for an initial strain rate of 1.2×10-3 s-1. At 850℃, thebest elongation 500% was achieved for an initial strain rate of 2.5×10-3 s-1. During the deformation in higher temperature region,coarse γ grains formed during the prior treatments were broken into spherical particles, resulting in a homogeneous dispersion of γparticles within the δ-ferrite matrix. However, at lower temperatures between 800 and 950℃, the σ phase was formed through theeutectoid decomposition of δ→γ+σ, resulting finally in the stable equiaxed micro-duplex structures with δ/γ and γ/σ, respectively.The precipitation of the σ phase played an important role in improving the superplasticity at 850℃. The strain-rate sensitivity coeffi-cient, m-values, were also determined by the strain rate change tests. The microstructure studies show that the superplastic processoccurs mainly by the local work hardening and the subsequent dynamic recrystallization and a grain boundary sliding and grain switching mechanism.

  19. Micrograin Superplasticity: Characteristics and Utilization

    Directory of Open Access Journals (Sweden)

    Farghalli A. Mohamed

    2011-07-01

    Full Text Available Micrograin Superplasticity refers to the ability of fine-grained materials (1 µm < d < 10 μm, where d is the grain size to exhibit extensive neck-free elongations during deformation at elevated temperatures. Over the past three decades, good progress has been made in rationalizing this phenomenon. The present paper provides a brief review on this progress in several areas that have been related to: (a the mechanical characteristics of micrograin superplasticity and their origin; (b the effect of impurity content and type on deformation behavior, boundary sliding, and cavitation during superplastic deformation; (c the formation of cavity stringers; (d dislocation activities and role during superplastic flow; and (e the utilization of superplasticity.

  20. Phase boundary sliding model controlled by diffusion-solution zone in superplastic deformation

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    With scanning electron microscope (SEM), the surface morphology of phase boundary sliding (PBS) in superplastic deformation (SPD) of Zn-Al alloy and the diffusion behavior of Zn, Al interfaces in their powers' sintering have been investigated. The results show that Zn-Al eutectoid microstructure can be achieved through their powders' sintering, and the diffusion characteristic between Zn and Al is just a demonstration of Kirkendall effect, in which Zn can dissolve into Al whereas A1 can hardly dissolve into Zn. During sintering, a diffusion-solution zone ?′ has formed and subsequently transformed into a eutectoid microstructure in the cooling process. The superplastic deformation mechanism of Zn-Al eutectic alloy is phase boundary sliding which is controlled by the diffusion-solution zone ?′. If the diffusion-solution zone ?′ is unsaturated, it will have much more crystal defects and the combination between ?′ and phase ? is weak, thus the process of phase boundary sliding becomes easily; on the contrary, if the diffusion-solution zone ?′ becomes thick and saturated, the sliding will be difficult.

  1. Superplastic Deformation and Viscous Flow in an Zr-Based Metallic Glass at 410 Degrees C

    Energy Technology Data Exchange (ETDEWEB)

    Liu, C.T.; Mukai, T.; Nieh, T.G.; Wadsworth, J.; Wang, J.G.

    1998-12-01

    The thermal properties of an amorphous alloy (composition in at.%: Zr-l0Al-5Ti-l7.9Cu-14.6Ni), and particularly the glass transition and crystallization temperature as a function of heating rate, were characterized using Differential Scanning Calorimetry (DSC). X-ray diffraction analyses and Transmission Electron Microscopy were also conducted on samples heat-treated at different temperatures for comparison with the DSC results. Superplasticity in the alloy was studied at 410 degrees C, a temperature within the supercooled liquid region. Both single strain rate and strain rate cycling tests in tension were carried out to investigate the deformation behavior of the alloy in the supercooled liquid region. The experimental results indicated that the alloy did not behave like a Newtonian fluid.

  2. Effect of state of stress on the cavitation behavior of Al 5083 superplastic material

    Energy Technology Data Exchange (ETDEWEB)

    Chandra, Namas; Kalu, Peter [Dept. of Mech. Eng., Florida State Univ., Tallahassee, FL (United States); Khraisheh, Marwan K. [Dept. of MEch. Eng., Univ. of Kentucky, Lexington, KY (United States)

    2005-07-01

    In this paper we address the controversial issue of nucleation of cavities in Al 5083 alloys and their subsequent growth to coalescence and failure. We focus on the origin and growth of cavities not only during the primary processing of Al 5083 in sheet forms, but also during the manufacture of these sheets into SPF (superplastic forming) components. Experimental observations of pre-existing cavities in this alloy are made using optical and electron microscopy. The role of sheet rolling direction, and the state of stress during superplastic deformation on the cavity formation and coalescence are also discussed. The effect of the state of stress (uniaxial, plane strain, balanced biaxial, and tri-axial) on the growth characteristics of cavitation is also examined. It is found that the uniaxial model based cavitation cannot directly be extended to predict the behavior of more complex stress states, unless great care is taken to identify the right strain measure for the mapping process. (orig.)

  3. Influence of superplastic deformation on the anisotropy of 03Kh26N6T steel

    Energy Technology Data Exchange (ETDEWEB)

    Akhmed Faud, M.F.; Tsepin, M.A.; Lobach, A.A. [Tabbinskii Metallurgical Institute, Cario (Egypt)]|[Moscow Institute of Steel and Alloys (Russian Federation)] [and others

    1992-03-01

    The rules of change in anisotropy of 03Kh26N6T corrosion-resistant steel with a nonequiaxial fine-grained structure deformed under superplastic conditions were considered and an investigation was made of the change in anisotropy of the plastic properties in connection with the presence of original metallographic nonuniformity of the steel structure. 8 refs., 5 figs.

  4. Superplastic behavior of coarse-grained aluminum alloys

    NARCIS (Netherlands)

    Chezan, AR; De Hosson, JTM

    2005-01-01

    In this paper we concentrate on the superplastic behavior and the microstructural evolution of two coarse-grained Al alloys: Al-4.4w/oMg and Al-4.4w/oMg-0.4w/oCu. The values for the strain rate sensitivity index and activation energy suggest that solute drag on dislocation motion is an important phe

  5. Mechanical analysis of temperature impact on stability during superplastic tensile deformation

    Institute of Scientific and Technical Information of China (English)

    SONG; Yuquan; GUAN; Zhiping; WANG; Minghui; SONG; Jiawang

    2006-01-01

    Based on state equation that stress is the function of strain, strain-rate and temperature, the paper establishes the differential constitutive equation used for analyzing load-stability and the variational constitutive equation used for analyzing geometry-stability during superplastic tensile deformation, which contain strain hardening index, strain-rate sensitivity index, temperature sensitivity index introducted for the first time and temperature undulation index introducted for the first time in the paper. And then, based on the universal condition of plastic elementary theory, the paper analyzes load-stability and geometry-stability under continuously rising temperature and under the non-uniform temperature along the axes of specimen respectively. The results prove the impact of continuously rising speed and non-uniform value of temperature on deformation stability is that the faster temperature rises and the more non-uniform temperature is, the smaller the corresponding uniform strain of load-stability and geometry-stability are; strain hardening index is the necessary condition of stability during superplastic tensile deformation, and geometry-instability will not happen when load-instability occurs, but happen when uniform deformation has lasted after load-instability; in the superplastic temperature field, constant temperature is not necessary condition of superplasticitiy, but during the deformation, the slower temperature rises and the more uniform temperature is, the more stable deformation is.

  6. Superplastic behavior of hot extruded gamma TiAl (Mo, Si) alloys

    Energy Technology Data Exchange (ETDEWEB)

    Jimenez, J.A.; Carsi, M.; Ruano, O.A. [Dept. of Physical Metallurgy, Centro Nacional de Investigaciones Metalurgicas, C.S.I.C., Madrid (Spain); Frommeyer, G.; Knippscher, S. [Dept. of Materials Engineering, Max Planck Inst. fuer Eisenforschung, Duesseldorf (Germany); Wittig, J. [Dept. of Materials Science and Engineering, Vanderbilt Univ., Nashville (United States)

    2003-07-01

    Superplastic behavior of hot extruded intermetallic Ti-46Al-1.7(Mo,Si) (at%) alloys was studied by stress change tests in compression and tensile tests at temperatures ranging from 700 to 1050 C. The material produced by arc melting exhibited a structure of coarse lamellar grains in the as-cast condition that transforms to an equiaxic near {gamma} microstructure after processing by hot extrusion at 1250 C. This microstructure consists of zones of {gamma} grains finer than 1 {mu}m and band like regions with coarser grains, ranging from 5 to 20 {mu}m. In addition to {gamma} grains, a volume fraction of more than 20 vol% of {alpha}{sub 2}-Ti{sub 3}Al particles finely dispersed are also present in the fine-grained zones. Compression tests of the extruded material at stresses ranging from 4 to 825 MPa showed values of the strain-rate-sensitivity exponent near 0.5 at low stresses and/or high temperatures. The microstructure in the fine-grained areas remains essentially constant during deformation. TEM analysis of deformed samples in this regime leads to relate grain boundary sliding as the mechanism controlling the deformation process. High elongation to failure, characteristic of superplasticity, was achieved at 975 and 1050 C at an initial strain rate of 4.6 x 10{sup -4} and 4.6 x 10{sup -3} s{sup -1}. (orig.)

  7. Influence of fluoridation on the strength of superplastic Zn-21Al-2Cu alloy deformed in a saline medium

    Energy Technology Data Exchange (ETDEWEB)

    Elizalde-Torres, J.; Torres-Villasenor, G. [UNAM, Mexico Distrito Federal (Mexico); Sandoval-Jimenez, A. [Instituto Nacional de Investigaciones Nucleares, Mexico Distrito Federal (Mexico)

    1999-04-09

    The interest in Zi-Al-Cu alloys has intensified in recent years because they possess the highest known yield strengths among the entire series of Zn-Al superplastic alloys. The superplastic materials are generally fine-grained materials and the deformation is associated with the grain boundary processes. Because of this, the superplastic alloys are exposed to a potential danger of intergranular stress corrosion cracking under susceptible service conditions. Consequently, the study of enhancing the strength and increasing the corrosion resistance of the material at room temperature is an important research area. Fluorine passivation technology of metal surfaces (fluoridation) has been proved to be very effective in the protection of several metals such as austenitic stainless steel and aluminum. In the present investigation the superplastic Zn-Al-Cu alloy has been studied to evaluate the effects of fluoridation and the stress corrosion damage.

  8. Effect of electric current pulse on grain growth in superplastic deformation of 2091 Al-Li alloy

    Institute of Scientific and Technical Information of China (English)

    刘志义; 许晓嫦; 崔建忠

    2003-01-01

    The effect of electric current pulse on the grain growth in the superplastic deformation of 2091 Al-Li alloy was investigated. Optical metallographic microstructure observation and average linear intercept measuring results show that at same strain, the grain size in the superplastic deformation loaded with electric current pulse is smaller than that unemploying electric current pulse, and so does the grain growth rate. TEM observation shows that the dislocation density at grain boundary in the superplastic deformation applied with electric current pulse is lower than that unemploying electric current pulse.It indicates that electric current pulse increases the rate of dislocation slip and climb in grain boundary, which leads to a decrease of both the density of the dislocation slipping across grain boundary at same strain rate and the driving force for grain growth, therefore the rate of grain growth decreases.The established model for grain growth shows an exponential relation of grain size with strain.

  9. A technique to study the granular flow during superplastic deformation

    Energy Technology Data Exchange (ETDEWEB)

    Munoz-Andrade, J.D. [DCBI, Dept. de Materiales, Univ. Autonoma Metropolitana (Mexico); Universidad Central de Venezuela, Caracas. Facultad de Ingenieria; Mendoza-Allende, A.; Montemayor-Aldrete, J.A. [Universidad Autonoma de Puebla (Mexico). Dept. de Fisica; Torres-Villasenor, G. [Universidad Nacional Autonoma de Mexico, Mexico City (Mexico). Inst. de Investigaciones en Materiales

    1999-07-01

    A new technique for scanning electron microscopy (SEM), which provides a mesoscopic coordinate system inscribed on the surface of the center of a tension test specimen, and relates this system to another fixed at rest in laboratory it is developed. Such technique allows to establish in a repeatable way any angle relative to any axis of any coordinate system, or distances between grains, or to measure local or global true deformation in parallel or perpendicular direction relatives to the tension axis. This technique was applied to give some results on a Zn-20.2% Al-1.8% Cu Alloy tension test specimen with 412 {mu}m length. (orig.)

  10. Stored energy analysis of Zn-5Al eutectic alloy in superplastic deformation

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    The stored energy and the energy release during SPD (superplastic deformation) ofa Zn-5Al alloy were studied. The alloy after rolling process gains more stored energy, and the as-rolled specimen can obtain maximum elongation and minimum flow stress without hot holding treatment before SPD. Experimental results show that stored energy release process is along with SPD process and is also an impetus to SPD. The as-rolled Zn-5Al alloy has 48 J/mol stored energy which was measured with DSC (differential scanning calorimeter) and conforms well to the calculated value. The as-rolled Zn-5Al alloy after SPD with an elongation of 2 500% releases 112 J/mol stored energy. Analysis shows that the strain rate is in direct ratio to the rate of stored energy release.

  11. Superplastic behavior of silica nanowires obtained by direct patterning of silsesquioxane-based precursors

    Science.gov (United States)

    Yılmaz, Mustafa; Wollschläger, Nicole; Nasr Esfahani, Mohammad; Österle, Werner; Leblebici, Yusuf; Erdem Alaca, B.

    2017-03-01

    Silica nanowires spanning 10 μm-deep trenches are fabricated from different types of silsesquioxane-based precursors by direct e-beam patterning on silicon followed by release through deep reactive ion etching. Nanowire aspect ratios as large as 150 are achieved with a critical dimension of about 50 nm and nearly rectangular cross-sections. In situ bending tests are carried out inside a scanning electron microscope, where the etch depth of 10 μ {{m}} provides sufficient space for deformation. Silica NWs are indeed observed to exhibit superplastic behavior without fracture with deflections reaching the full etch depth, about two orders of magnitude larger than the nanowire thickness. A large-deformation elastic bending model is utilized for predicting the deviation from the elastic behavior. The results of forty different tests indicate a critical stress level of 0.1–0.4 GPa for the onset of plasticity. The study hints at the possibility of fabricating silica nanowires in a monolithic fashion through direct e-beam patterning of silsesquioxane-based resins. The fabrication technology is compatible with semiconductor manufacturing and provides silica nanowires with a very good structural integrity.

  12. Forming of superplastic ceramics

    Energy Technology Data Exchange (ETDEWEB)

    Lesuer, D.R.; Wadsworth, J.; Nieh, T.G.

    1994-05-01

    Superplasticity in ceramics has now advanced to the stage that technologically viable superplastic deformation processing can be performed. In this paper, examples of superplastic forming and diffusion bonding of ceramic components are given. Recent work in biaxial gas-pressure forming of several ceramics is provided. These include yttria-stabilized, tetragonal zirconia (YTZP), a 20% alumina/YTZP composite, and silicon. In addition, the concurrent superplastic forming and diffusion bonding of a hybrid ceramic-metal structure are presented. These forming processes offer technological advantages of greater dimensional control and increased variety and complexity of shapes than is possible with conventional ceramic shaping technology.

  13. Thinning Behavior Simulations in Superplastic Forming of Friction Stir Processed Titanium 6Al-4V

    Science.gov (United States)

    Edwards, Paul D.; Sanders, Daniel G.; Ramulu, M.; Grant, Glenn; Trapp, Tim; Comley, Peter

    2010-06-01

    A study was undertaken to simulate the thinning behavior of titanium 6Al-4V alloy sheet during Superplastic Forming and to evaluate the feasibility of controlling thinning in areas of interest with Friction Stir Processing (FSP) of the material. The commercially available Finite Element Analysis software ABAQUS was used to execute these simulations. Material properties of the parent sheet and the Friction Stir Processed regions input into the models were determined experimentally by elevated temperature tensile testing. The results of these simulations were compared to experimental test results via Superplastically Forming representative aerospace parts and analytical computations for validation. It was found that numerical simulations can be used to predict the thin-out characteristics of superplastically formed titanium parts and the thin-out can be controlled in desired areas by FSP, locally, prior to forming.

  14. Thermally assisted deformation of structural superplastics and nanostructured materials: A personal perspective

    Indian Academy of Sciences (India)

    K A Padmanabhan

    2003-02-01

    Optimal structural superplasticity and the deformation of nanostructured materials in the thermally activated region are regarded as being caused by the same physical process. In this analysis, grain/interphase boundary sliding controls the rate of deformation at the level of atomistics. Boundary sliding develops to a mesoscopic level by plane interface formation involving two or more boundaries and at this stage the rate controlling step is boundary migration. In other words, grain/interphase boundary sliding is viewed as a two-scale process. The non-zero, unbalanced shear stresses present at the grain/interphase boundaries ensure that near-random grain rotation is also a non-rate controlling concomitant of this mechanism. Expressions have been derived for the free energy of activation for the atomic scale rate controlling process, the threshold stress that should be crossed for the commencement of mesoscopic boundary sliding, the inverse Hall-Petch effect and the steady state rate equation connecting the strain rate to the independent variables of stress, temperature and grain size. Beyond the point of inflection in the log stress-log strain rate plot, climb controlled multiple dislocation motion within the grains becomes increasingly important and at sufficiently high stresses becomes rate controlling. The predictions have been validated experimentally.

  15. Effects of crystal boundary gliding and dislocation on superplastic deformation of SiCw/6061 Al composite

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    SiCw/6061Al composite was fabricated with squeeze casting method, hot extruded and superplastically tensile tested. At the temperature of 570  ℃and the strain rate of 2.0×10-3 s-1, an elongation of 280% was obtained. The change of grain shape, dislocation density and distribution was observed by TEM. The results show that during the superplastic deformation grain shape on the whole is unchanged, but the dislocation density and distribution vary quite a lot with the tensile action. Under the optimal straining conditions, dislocation mainly distributes along the grain boundary, which has an important effect on cooperative strain especially. When the strain magnitude is big enough, there appears stacking faults and twin crystals, which also has some effect on the cooperative strain.

  16. Rheology of Superplastic Ceramics

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Constitutive equation of rheglogy describing a phenomenological level of superplastic deformation as functional correlation between tensor components of stress and strain rate has been analyzed for the case of superplastic ceramic flow. Rheological properties of material are taken into account by means of scalar rheological coefficients of shear and volume viscosity, which are functions of temperature, effective stress (or strain rate) and density of material.

  17. Superplasticity in a lean Fe-Mn-Al steel.

    Science.gov (United States)

    Han, Jeongho; Kang, Seok-Hyeon; Lee, Seung-Joon; Kawasaki, Megumi; Lee, Han-Joo; Ponge, Dirk; Raabe, Dierk; Lee, Young-Kook

    2017-09-29

    Superplastic alloys exhibit extremely high ductility (>300%) without cracks when tensile-strained at temperatures above half of their melting point. Superplasticity, which resembles the flow behavior of honey, is caused by grain boundary sliding in metals. Although several non-ferrous and ferrous superplastic alloys are reported, their practical applications are limited due to high material cost, low strength after forming, high deformation temperature, and complicated fabrication process. Here we introduce a new compositionally lean (Fe-6.6Mn-2.3Al, wt.%) superplastic medium Mn steel that resolves these limitations. The medium Mn steel is characterized by ultrafine grains, low material costs, simple fabrication, i.e., conventional hot and cold rolling, low deformation temperature (ca. 650 °C) and superior ductility above 1300% at 850 °C. We suggest that this ultrafine-grained medium Mn steel may accelerate the commercialization of superplastic ferrous alloys.Research in new alloy compositions and treatments may allow the increased strength of mass-produced, intricately shaped parts. Here authors introduce a superplastic medium manganese steel which has an inexpensive lean chemical composition and which is suited for conventional manufacturing processes.

  18. Superplastic Deformation and Microstructural Evolution of Ti-6Al-4V Alloy%Ti-6Al-4V合金超塑性变形及微观组织演变

    Institute of Scientific and Technical Information of China (English)

    朱堂葵; 李淼泉

    2012-01-01

    通过高温拉伸试验研究了Ti-6Al-4V合金的高温变形力学行为和超塑性,并对试样断口附近的组织进行了观察.结果表明,随着变形温度的升高或初始应变速率的降低,Ti-6Al-4V合金的流动应力明显减小 ;Ti-6Al-4V合金的最佳超塑性变形工艺参数为880℃/0.001 s-1,最大延伸率为689%,峰值应力仅为30.03 MPa ;在超塑性拉伸过程中,试样变形区发生明显的动态再结晶,使片层状的α相晶粒破碎、细化和等轴化,促进超塑性的增加;随着变形温度的提高、变形量增大和变形时间的加长,再结晶α相发生了聚集长大,从而使显微组织明显粗化.对于双态组织的两相钛合金,最佳超塑性变形温度应低于或等于片层状α→β转变的终了温度.%The deformation behavior and superplasticity of Ti-6A1-4V alloy at elevated temperature have been investigated through tensile tests. The microstructures near the fracture of the specimen have been observed by optical microscopy. The results show that the flow stress of Ti-6AI-4V alloy decreases obviously with increasing of the temperature or decreasing of the initial strain rate. The temperature and the initial strain rate of optimal superplastic deformation are 880 ℃ and 0.001 s-1, respectively. Under this optimal condition, the maximum elongation is 689%; however, the peak stress is only 30.03 MPa. During the superplastic tensile deformation, the dynamic recrystallization occurs obviously in the deformation zone of the specimen and the lamellar α grain is broken, refined and spheroidized, so that the superplasticity can be improved. With increasing of the deformation temperature, the deformation amount and the deformation time, the recrystal α grain will merge and grow up, causing obvious coarsening of the microstructure. The temperature of optimal superplastic deformation should not exceed the ceasing temperature of lamellar α→β phase transformation for the α+β titanium alloy

  19. Modeling microstructural evolution and the mechanical response of superplastic materials

    Energy Technology Data Exchange (ETDEWEB)

    Lesuer, D.R.; Syn, C.K.; Cadwell, K.L.; Preuss, C.S.

    1993-01-11

    A model has been developed that accounts for grain growth during, superplastic flow and its subsequent influence on stress-strain-strain rate behavior. These studies are experimentally based and have involved two different types of superplastic materials -- a quasi-single phase metal (Coronze 638) and a microduplex metal (ultrahigh-carbon steel - UHCS). In both materials the kinetics of strain-enhanced grain growth have been studied as a function of strain, strain rate and temperature. An equation for the rate of grain growth has been developed that incorporates the influence of temperature. The evolution of the grain size distribution during superplastic deformation has also been investigated. Our model integrates grain growth laws derived from these studies with two mechanism based, rate dependent constitutive laws to predict the stress-strainstrain rate behavior of materials during superplastic deformation. The influence of crain size distribution and its evolution with strain and strain rate on the stress-strain-strain rate behavior has been represented through the use of distributed parameters. The model can capture the stress-strain-strain rate behavior over a wide range of strains and strain rates with a single set of parameters. Many subtle features of the mechanical response of these materials can be adequately predicted.

  20. Investigation on Superplasticity in SiCp/2024 Cold Rolling Sheet after Heat Treatment

    Institute of Scientific and Technical Information of China (English)

    Bol(u) XIAO; Zongyi MA; Jing BI

    2003-01-01

    High strain rate superplastic deformation behavior of powder metallurgy (PM) processed 17 vol. pct SiCp/2024 Al composite sheet after heat treatment was investigated over a range of temperature from 753 to 833 K. At 813 K,a maximum elongation of 259% was discovered at a strain rate of 10-1 s-1. The activation energy was closed to that for lattice diffusion of Al and increased at temperature upon incipient melting temperature. The mechanism of superplastic deformation for present composites was attributed to lattice diffusion controlled grain boundary sliding.

  1. Characterization of Grain Boundaries in Superplastically Deformed Y-TZP Ceramics

    NARCIS (Netherlands)

    Boutz, Michel M.R.; Chen, Chu Sheng; Winnubst, Louis; Burggraaf, Anthonie J.

    1994-01-01

    The effects of compressive deformation on the grain boundary characteristics of fine-grained Y-TZP have been investigated using surface spectroscopy, impedance analysis, and transmission electron microscopy. After sintering at low temperature (1150°C), the grain boundaries are covered by an ultrathi

  2. High-temperature tensile deformation behavior of aluminum oxide with and without an applied electric field

    Science.gov (United States)

    Campbell, James

    1998-12-01

    Ceramics are usually considered to be brittle, but under certain conditions some ceramics exhibit a large degree of ductility. They are fine-grained and exhibit superplastic behavior when deformed at high temperatures and low stresses. Whereas superplasticity gives enhanced ductility to metals, it may be the only method for imparting large plasticity to ceramics. Electric fields have been shown to increase ductility, reduce flow stress and reduce cavitation in the superplastic forming of 7475 Al and yttria-stabilized zirconia. Thus, the concurrent application of an electric field may give improved superplastic properties and increased plasticity to a marginally ductile ceramic such as aluminum oxide (alpha-alumina). Fine-grained alumina tensile specimens, formed by dry pressing and sintering a spray-dried powder, were tested in tension at high temperature with and without an electric field of 300 V/cm. Constant strain rate, strain rate cycling and stress relaxation tests were performed. The effects of an electric field on the ductility, flow stress, cavitation and parameters of the Weertman-Dorn deformation equation were measured. Without an electric field, the following deformation parameters were found: the stress exponent n = 2.2, the grain size exponent p = 1.9, the activation energy Q = 490 kJ/mol and the threshold stress sigmao ≈ 0 MPa, indicating structural superplasticity where grain boundary sliding is the predominant deformation mode and was likely accommodated by the motion of grain boundary dislocations. An electric field of 300 V/cm gave a Joule heating temperature increase of ˜30°C and caused the alumina to swell 5--25% (increasing with time), even while under no applied stress, thereby reducing its ductility and flow stress. After correcting for Joule heating and swelling there was still a significant flow stress reduction produced by the field and the following deformation parameters were found: n = 2.2, p = 1.9, Q = 950 kJ/mol and sigmao ≈ 0

  3. Early stages of superplasticity and positron lifetime spectroscopy in an Al-Mg-Cu alloy

    Energy Technology Data Exchange (ETDEWEB)

    Ayciriex, M.D.; Romero, R.; Somoza, A. [Universidad Nacional del Centro de la Provincia de Buenos Aires (Argentina). Instituto de Fisica de Materiales Tandil

    1996-07-01

    In the present paper, by using positron lifetime technique, a careful study is carried out to analyze the microstructural changes induced on samples of an Al-based commercial alloy (Al-Mg-Cu-Mn-Cr) by superplastic deformation in the early stages of superplastic behavior of the alloy (strain range from 0.2% to 100%). These results are compared with those obtained on specimens only heat treated at the same temperature and for a time equivalent to the elapsed time during each tensile test, in order to evaluate the thermal contribution to the microstructural changes induced during the superplastic deformation process. Moreover, the positron results were linked with the microstructural evolution of the samples followed by means of optical microscopy and Vickers microhardness technique.

  4. Deformation behavior and mechanisms of Ti- 1023 alloy

    Institute of Scientific and Technical Information of China (English)

    BAO Ru-qiang; HUANG Xu; CAO Chun-xiao

    2006-01-01

    The deformation behavior and mechanisms of Ti-1023 alloy were studied in the temperature range of 650-900 ℃ and strain rate range of 0.001-10 s-1 by compression and tensile tests. The results show that in a limited strain rate range of 0.001-0.1 s-1,the kinetic rate equation is obeyed and a linear fit is obtained at all the temperatures. The apparent activation energy is 322 kJ/mol in the α-β region and 160 kJ/mol in the β region, respectively. Power dissipation maps of this alloy developed by using Gleeble test data show three domains in the tested range. Superplasticity, marked by abnormal elongation at 700 ℃, occurs in the temperature range of 650-750 ℃ and at strain rates below about 0.03 s-1 Large grain superplasticity takes place in the temperature range of 750-850℃ and strain rates range of 0.001-0.03 s-1. Dynamic recrystallization occurs in the temperature range of 850-900 ℃ and at strain rates below about 1 s-1. The instability maps of this alloy were also developed.

  5. Effect of superplastic forming exposure on fatigue crack propagation behavior of Ti-6Al-4V alloy

    Science.gov (United States)

    Jeong, Daeho; Kwon, Yongnam; Goto, Masahiro; Kim, Sangshik

    2016-09-01

    The effect of superplastic forming (SPF) exposure on the ɛ (strain)-N (number of cycles to failure) fatigue and fatigue crack propagation (FCP) behaviors of Ti-6Al-4V (Ti64) alloy was examined at 298 and 473 K. To simulate the thermal exposure during superplastic forming process, the mill-annealed Ti64 alloy sheet was heated in the vacuum chamber with the pre-determined temperature profile. Notable microstructural change during the SPF exposure included the shape of transformed β phase from fine and round particles in the as-received specimen to coarse angular particles in the as-exposed specimen. The effective grain size tended to increase with the exposure, enhancing the slip reversibility and the resistance to FCP. However, the crack hindering effect by fine, particle-like β phase became weak with the exposure, offseting the beneficial effect associated with the increment of effective grain size. The effect of SPF exposure on ɛ-N fatigue and FCP behavior of mill-annealed Ti64 alloy was therefore marginal, excluding the effect of α-case (the oxygen-enriched phase) on the surface.

  6. Influence of carbon content on superplastic behavior in Ti- and B-added Cr-Mo steels

    Energy Technology Data Exchange (ETDEWEB)

    Aramaki, M.; Higashida, K.; Onodera, R. [Kyushu Univ., Fukuoka (Japan). Dept. of Materials Science and Engineering

    1999-05-01

    Superplasticity has been investigated in various ferrous alloys and steels. However, in these materials, especially in hypoeutectoid steels below the A{sub 1} temperature, the relationship between the content of carbon and elongation to failure is not obvious. In the present investigation, the influence of carbon content on superplastic behavior is studied using carbon steels based on Cr-Mo steel. In order to obtain the fine grain structure, a small amount of Ti and B were added and the content of carbon was controlled to be in the range from 0.24 to 0.83 pct. The largest value of elongation to failure was 644 pct, which was obtained for a specimen containing 0.58 pct carbon. The temperature and strain rate at which the maximum value was obtained were 710 C and 5 {times} 10{sup {minus}4} s{sup {minus}1}, respectively. Of all the specimens, this specimen had the minimum grain size. Moreover, the area fraction of carbide took the maximum value at the temperature where the largest elongation value was obtained. These results show that the addition of carbon has an effect on grain refinement by the formation of carbide, but excess amounts of carbon (>0.6 pct) bring about premature failure because of the resulting coarse microstructure and larger carbides.

  7. Superplasticity of Ti2448 Alloy with Nanostructured Grains

    Institute of Scientific and Technical Information of China (English)

    M.J. Xiao; Y.X. Tian; G.W. Mao; S.J. Li; Y.L. Hao; R. Yang

    2011-01-01

    Ti-24Nb-4Zr-8Sn, abbreviated as Ti2448 from its chemical composition in weight percent, is a multifunctional β type titanium alloy with body centered cubic (bcc) crystal structure, and its highly localized plastic deformation behavior contributes significantly to grain refinement during conventional cold processing. In the paper, the nanostructured (NS) alloy with grain size less than 50 nm produced by cold rolling has been used to investigate its superplastic deformation behavior by uniaxial tensile tests at initial strain rates of 1.5×10-2, 1.5×10-3 and 1.6×10-4 s-1 and temperatures of 600, 650 and 700℃. The results show that, in comparison with the coarse-grained alloy with size of 50 μm, the NS alloy has better superplasticity with elongation up to ~275% and ultimate strength of 50-100 Mpa. Strain rate sensitivity (m) of the NS alloy is 0.21, 0.30 and 0.29 for 600, 650 and 700℃, respectively. These results demonstrate that grain refinement is a valid way to enhance the superplasticity of Ti2448 alloy.

  8. Enhanced superplasticity in an extruded high strength Mg–Gd–Y–Zr alloy with Ag addition

    Energy Technology Data Exchange (ETDEWEB)

    Movahedi-Rad, A. [School of Metallurgical and Materials Engineering, College of Engineering, University of Tehran, Tehran (Iran, Islamic Republic of); Mahmudi, R., E-mail: mahmudi@ut.ac.ir [School of Metallurgical and Materials Engineering, College of Engineering, University of Tehran, Tehran (Iran, Islamic Republic of); Wu, G.H.; Jafari Nodooshan, H.R. [National Engineering Research Center of Light Alloy Net Forming, Shanghai Jiao Tong University, Shanghai 200240 (China)

    2015-03-25

    Highlights: • Addition of 2% Ag to the base alloy refined the microstructure and increased m-value. • Volume fractions of both high angle grain boundaries and particles increased after Ag addition. • Ag-containing alloy had an m-value of 0.51, typical of superplastic materials. • Grain boundary sliding accommodated by lattice diffusion was the dominant deformation mechanism. - Abstract: The effect of 2 wt% Ag addition on the superplastic behavior of an extruded Mg–8.5Gd–2.5Y–0.5Zr (wt%) alloy was investigated by impression testing in the temperature range of 523–598 K. The average sizes of the dynamically recrystallized grains of the Ag-free and Ag-containing alloys were about 8 and 3 μm, respectively. Analysis of electron backscattered diffraction (EBSD) data confirmed the higher fractions of high-angle grain boundaries (HAGBs) in the Ag-containing alloy. The deformation response of this alloy in proper temperature range conforms to regions I, II and III, typical of superplastic deformation behavior. The addition of Ag to the base alloys led to enhanced superplasticity in region II by increasing the strain rate sensitivity (SRS) indices (m-values) from 0.25 to 0.51 and 0.36 to 0.46 at 573 and 598 K, respectively. These high m-values together with the activation energy of 181 kJ/mol suggest that the major mechanism involved in superplastic deformation is grain boundary sliding (GBS) accommodated by lattice diffusion at temperatures above 573 K.

  9. Formability and cavitation behavior of superplastic AA5083 aluminum alloy under biaxial tension

    Institute of Scientific and Technical Information of China (English)

    LUO Ying-bing; LI Da-yong; PENG Ying-hong

    2006-01-01

    The superplastic forming potential of two fine-grained 5083 aluminum alloys were studied under biaxial tension using a pneumatic bulge test. Experiments were performed at temperatures ranging from 475 to 525 ℃ with three different strain paths ranging from equi-biaxial to approaching plane strain. The shape of the forming limited diagram(FLD) is found to be significantly different from FLDs commonly used in room temperature stamping. The effects of temperature on final thickness distribution, dome height and cavitation were investigated for the case of equi-biaxial stretching. Increasing temperature in free bulge forming can improve the thickness distribution of final parts but have no significant effect on dome height. The results indicate that determination of forming limits in SPF cannot be represented with a simple FLD and additional metrics such as external thinning and internal cavitation needed to determine the SPF potential of a material.

  10. Creep study of mechanisms involved in low-temperature superplasticity of UFG Ti-6Al-4V processed by SPD

    Energy Technology Data Exchange (ETDEWEB)

    Kral, Petr, E-mail: pkral@ipm.cz [Institute of Physics of Materials, ASCR, Zizkova 22, CZ -61662 Brno (Czech Republic); CEITEC – IPM ASCR, v.v.i., Zizkova 22, CZ-61662 Brno (Czech Republic); Dvorak, Jiri [Institute of Physics of Materials, ASCR, Zizkova 22, CZ -61662 Brno (Czech Republic); CEITEC – IPM ASCR, v.v.i., Zizkova 22, CZ-61662 Brno (Czech Republic); Blum, Wolfgang [Inst. f. Werkstoffwissenschaften, University of Erlangen-Nürnberg, D-91058 Erlangen (Germany); Kudryavtsev, Egor; Zherebtsov, Sergey; Salishchev, Gennady [Belgorod State University, Laboratory of Bulk Nanostructured Materials, Pobeda Str. 85, 308015 Belgorod (Russian Federation); Kvapilova, Marie; Sklenicka, Vaclav [Institute of Physics of Materials, ASCR, Zizkova 22, CZ -61662 Brno (Czech Republic); CEITEC – IPM ASCR, v.v.i., Zizkova 22, CZ-61662 Brno (Czech Republic)

    2016-06-15

    The deformation kinetics of ultrafine-grained Ti-6Al-4V with mean (sub)grain size about 150 nm (produced by isothermal multiaxial forging) and superplastic properties at the relatively low temperature of 873 K was investigated in compression and tension over a large range of strain rates from 10{sup −7} to 10{sup −2} s{sup −1}. Electron microscopic observations showed that the grains coarsen during deformation towards the quasi-stationary spacing w{sub qs} of strain induced boundaries. In spite of the grain coarsening the grains were generally smaller than w{sub qs} allowing high-angle boundaries to dominate the quasi-stationary strength. Texture measurements indicate that dislocation glide plays a large role in deformation. Glide in this alloy is significantly influenced by solid solution strengthening leading to a stress sensitivity of strain rate of n = 3. The present ultrafine-grained Ti alloy displays a stress sensitivity exponent n = 2 over an extended stress range where its superplastic behavior is optimal. While the deformation kinetics of present ultrafine-grained Ti alloy can be roughly explained by the traditional formula for superplastic flow, the significant discrepancy to the measured values suggests that solid solution strengthening must be taken into account to get a complete insight. - Highlights: • The UFG Ti-6Al-4V alloy behaves superplastically at low temperature of 873 K. • Grain coarsening at low stresses limits superplasticity of UFG Ti alloy. • Solute strengthening plays an important role in low-temperature superplasticity. • Acceleration of creep in UFG Ti alloy is caused by processes related to hab.

  11. A high-strain-rate superplastic ceramic.

    Science.gov (United States)

    Kim, B N; Hiraga, K; Morita, K; Sakka, Y

    2001-09-20

    High-strain-rate superplasticity describes the ability of a material to sustain large plastic deformation in tension at high strain rates of the order of 10-2 to 10-1 s-1 and is of great technological interest for the shape-forming of engineering materials. High-strain-rate superplasticity has been observed in aluminium-based and magnesium-based alloys. But for ceramic materials, superplastic deformation has been restricted to low strain rates of the order of 10-5 to 10-4 s-1 for most oxides and nitrides with the presence of intergranular cavities leading to premature failure. Here we show that a composite ceramic material consisting of tetragonal zirconium oxide, magnesium aluminate spinel and alpha-alumina phases exhibits superplasticity at strain rates up to 1 s-1. The composite also exhibits a large tensile elongation, exceeding 1,050 per cent for a strain rate of 0.4 s-1. The tensile flow behaviour and deformed microstructure of the material indicate that superplasticity is due to a combination of limited grain growth in the constitutive phases and the intervention of dislocation-induced plasticity in the zirconium oxide phase. We suggest that the present results hold promise for the application of shape-forming technologies to ceramic materials.

  12. Critical Strain Rate of Uniform Deformation in Cross Section at Diffusion Dominated Superplastic Tensile Test%扩散控制超塑性拉伸断面均匀收缩的临界应变速率

    Institute of Scientific and Technical Information of China (English)

    张诗昌; 罗敏; 杨倩; 陈伟

    2012-01-01

    A parameter named λ was put forward and an equation was deduced to characterize the uniform deformation of superplastic tensile test under the conditions of difiusion dominated deformation. By solving the equation at λ=0, a critical strain rate εcn of uniform deformation was got ten. The results show that εcn is direct proportion to strain and diffusion coefficient and inversely proportion to the cross section area of undeformed specimens. The results of the tested A of AZ31 alloy under superplastic tensile show that A is becoming significant small and the cross section of the specimen tends to be uniform deformation when strain rate is near εcn.%引入了一个衡量超塑性拉伸断面收缩均匀性的特征参数λ,在假设变形以扩散为主的条件下,导出了λ的表达式.令λ=0时,得到断面均匀收缩的临界应变速率(.εcn).(.εcn)与扩散系数和应变量成正比,与试样原始截面积成反比.对AZ31镁合金超塑性拉伸特征参数λ值的测定结果表明;当应变速率越接近于临界应变速率,λ越小,试样越接近均匀变形.

  13. Gas-pressure forming of superplastic ceramic sheet

    Energy Technology Data Exchange (ETDEWEB)

    Nieh, T.G.; Wadsworth, J.

    1993-06-24

    Superplasticity in ceramics has now advanced to the stage that technologically viable superplastic deformation processing can be performed. In this paper, examples of biaxial gas-pressure forming of several ceramics are given. These include yttria stabilized, tetragonal zirconia (YTZP) a 20% alumina/YTZP composite, and silicon. In addition, the concurrent superplastic forming and diffusion bonding of a hybrid YTZP/C103 (ceramic-metal) structure are presented. These forming processes offer technological advantages of greater dimensional control and increased variety and complexity of shapes than is possible with conventional ceramic shaping technology.

  14. Grain boundary dynamics in ceramics superplasticity

    Directory of Open Access Journals (Sweden)

    Wakai, E.

    2001-04-01

    Full Text Available Superplasticity refers to an ability of polycrystalline solids to exhibit exceptionally large elongation in tension. The application of superplasticity makes it possible to fabricate ceramic components by superplastic forming (SPF, concurrent with diffusion bonding, and superplastic sinter-forging just like superplastic metals. Furthermore the superplastic deformation plays an important role in stress-assisted densification processes such as hot isostatic pressing (HIP and hot pressing (HP. The ceramics superplasticity has been one of intensive research fields in the last decade. Although most of reports are still limited to those of zirconia[1], new developments have been achieved in superplasticity of Si3N4 and SiC in recent years. It is clearly demonstrated that the superplasticity is one of the common natures of fine-grained ceramics and nanocrystalline ceramics at elevated temperatures.

    La superplaticidad se refiere a la capacidad que posee un sólido policristalino de presentar alargamientos excepcionalmente elevados en tracción. La aplicación de la superplasticidad hace posible la fabricación de componentes cerámicos por conformado superplástico, soldadura por difusión y forja-sinterizado superplástica, igual que en metales superplásticos. Además, la deformación superplástica tiene un rol importante en los procesos de densificación asistidos por tensiones, tales como la compactación isostática en caliente y el prensado en caliente. Las cerámicas superplásticas han sido uno de los campos donde se ha realizado una investigación más intensa en la última década. Aunque, la mayoría de los informes se limitan a la circonia[1] se han alcanzado nuevos desarrollos en superplasticidad de Si3N4 y SiC. Está claramente demostrado que la superplasticidad es una propiedad intrínseca de las cerámicas de pequeño tamaño de grano y de las cer

  15. 粉末冶金法制备超细晶AZ31镁合金及超塑性变形研究%Powder Metallurgy Prepared Ultra-fine Grain AZ31 Alloy and Its Superplastic Deformation

    Institute of Scientific and Technical Information of China (English)

    林莺莺; 胡杰仁

    2013-01-01

    采用粉末冶金法制备超细晶AZ31镁合金材料,并对其微观组织形貌及相成分进行研究;利用单向拉伸试验研究了该材料在不同条件下超塑性变形.结果表明,采用球磨、冷压制坯和热挤压法可获得晶粒尺寸在1微米以下的超细晶组织,该材料在250℃,1×10-3s-1的应变速率条件下获得了最大伸长率,基本达到超塑性状态.%Ultra-fine grain AZ31 alloy bars were fabricated by power metallurgy process,and the microstructure and phase composition were also researched.The superplastic deformation was studied by simple tension test.According to the results,AZ31 alloy with the grain size under 1 μm was prepared by the process of high energy ball milling,cold compacting and hot extrusion.The superplastic deformation was achieved under the temperature of 250 ℃ and strain rate of 1 × 10-3 s-1.

  16. Superplastic flow lubricates carbonate faults during earthquake slip

    Science.gov (United States)

    De Paola, Nicola; Holdsworth, Robert; Viti, Cecilia; Collettini, Cristiano; Faoro, Igor; Bullock, Rachael

    2014-05-01

    Tectonic earthquakes are hosted in the shallower portion of crustal fault zones, where fracturing and cataclasis are thought to be the dominant processes during frictional sliding. Aseismic shear in lower crust and lithospheric mantle shear zones is accomplished by crystal plasticity, including superplastic flow acting at low strain rates on ultrafine-grained rocks. Superplasticity has also been observed at high strain rates for a range of nano-phase alloys and ceramics, and could potentially occur in fine-grained geological materials, if deformed at high strain rates and temperatures. We performed a set of displacement-controlled experiments to explore whether superplastic flow can effectively weaken faults, and facilitate earthquake propagation. The experiments were performed on fine-grained synthetic gouges (63 lubrication mechanisms. When T ≥ 800 °C are attained, micro-textures diagnostic of diffusion-dominated grain boundary sliding are widespread within the slip zone, and suggest bulk superplastic flow. Flow stresses predicted by superplasticity constitutive laws at the slip zone temperatures, grain sizes and strain rates attained during the experiments match those we measured in the laboratory (μ = 0.16). We propose therefore that the activation of diffusion creep at high temperatures (T ≥ 800 °C) leads to slip zone-localised superplastic flow and that this causes the dynamic weakening of carbonate faults at seismic slip rates. Note, however, that both cataclasis and dislocation creep operating at lower temperatures, during the earlier stages of slip, are critical, precursory processes needed to produce the nanoscale grain sizes required to activate grainsize sensitive mechanisms during superplastic flow. Finally, the re-strengthening observed during the decelerating phase of deformation can be explained by the falling temperature "switching off" slip zone-localized superplasticity, leading to a return to frictional sliding. These results indicate

  17. Quantitative determination of homogeneous strain value in superplastic tension

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    After load instability, a passage of homogeneous strain ε can be still continued in superplastic tensile deformation. But untill now, no one has given the precise value of ε corresponding to actual materials, neither in experimental measurements nor in theoretical calculations. Using the elaborate experimental measuring methods of m value and its function expressions, the note first gives the method to determine homogeneous ε, and the homogeneous ε value of typical superplastic alloy Zn-5% Al under 18℃ and 340℃ respectively.

  18. Superplasticity of metals: phenomenology based on rheological properties and structural dynamics

    Energy Technology Data Exchange (ETDEWEB)

    Smirnov, O.M. [Moscow State Steel and Alloys Inst. (Russian Federation). Lab. of Superplastic Mater. Deformation

    1997-12-31

    Fine structure superplasticity (FSSP), high strain rate superplasticity (HSRSP) and phase transformation superplasticity (PTSP) as well as superplastic-like behaviour of some natural and industrial materials evidently belong to the same type of rheological behaviour i.e. non-linear viscoplastic flow. Temperature map has been proposed as a base for rheological analysis of various types of superplastic and superplastic-like flow of metallic materials. A phenomenological model has been developed to describe deformation of polycrystalline materials at elevated temperatures in a wide range of strain rates with respect to structure evolution during deformation. Rheological analysis of FSSP, HSRSP and PTSP materials along with a slurry during rheocasting shows similarities and peculiarities of superplastic and superplastic-like behaviour. The value of apparent viscosity seems to be an informative index for estimation of rheological and physical state of grain boundaries as a viscous phase and of polycrystalline material as a whole. A new process of impulse bulk forming is presented to show unique possibility of joining in one process two stages of a regular superplastic technology, i.e. preparation of ultrafine grain structure followed by HSRSP deformation. (orig.) 37 refs.

  19. Superplasticity and cavitation in an aluminum-magnesium alloy

    Science.gov (United States)

    Bae, Donghyun

    2000-10-01

    Fundamental issues related to the forming performance of superplastic metals include the mechanisms of flow and cavitation occurring during the forming process. Cavitation beyond a critical amount is damaging to the mechanical behavior of fabricated parts. Therefore, the role of process parameters which influence cavitation must be precisely documented and understood. In this study, (1) the mechanism of deformation, (2) cavity formation and growth, and (3) the effect of forming parameters on cavitation are systematically investigated in a fine grain Al-4.7%Mg-0.8%Mn-0.4%Cu alloy. The mechanical flow response of the alloy is characterized by a new type of step strain-rate test which preserves the initial microstructure of the alloy. Under isostructural condition, sigmoidal log s vs. log 3˙ relationship is determined and then analyzed by using a grain-mantle based quantitative model1 for superplastic flow. The activation energies in both grain-mantle creep and core creep are analyzed, and the overall controlling mechanism is found to be dislocation glide and climb. Grain-mantle creep rate in the low strain-rate region is found to be enhanced many times due to a high concentration of vacancies near grain boundaries. Cavitation caused by superplastic straining under uniaxial tension is evaluated by the SEM (for frame associated with superplastic deformation. In the model, faster cavity growth is predicted for lower m and for smaller cavity density when cavity stress fields are not overlapping. Observed cavitation quantitatively agrees with the present model, but diffusional growth is found to be too slow, which cannot explain the observed nanoscale void growth behavior. Another parameter affecting the degree of cavitation is the imposed stress-state. Cavity growth rate as well as cavity nucleation rate increase with the level of mean hydrostatic tension. For a fixed cavitation volume fraction, V, the principal surface strains, 31 and 32 , for the various stress

  20. Enhanced foaming of cellular metals by internal stress superplasticity

    Energy Technology Data Exchange (ETDEWEB)

    Kitazono, K.; Sato, E.; Kuribayashi, K. [The Inst. of Space and Astronautical Science, Kanagawa (Japan)

    2004-07-01

    Effects of internal stress superplasticity on solid-state foaming process were examined using Al-8.69Si alloy and pure zinc compacts produced by the powder metallurgical (P/M) route. Isothermal and thermal cycling compression creep behaviors revealed that composite CTE (coefficient of thermal expansion)-mismatch superplasticity was induced in P/M Al-Si alloy, however, no difference was shown in the solid-state foaming. On the other hand, the foaming rate of P/M zinc was enhanced by anisotropic CTE-mismatch superplasticity. The cell morphology of the foamed zinc has anisotropy due to the original powder compact produced by hot-extrusion. (orig.)

  1. Deformation Behavior of Nanoporous Metals

    Energy Technology Data Exchange (ETDEWEB)

    Biener, J; Hodge, A M; Hamza, A V

    2007-11-28

    of free surfaces can no longer be neglected. As the material becomes more and more constraint by the presence of free surfaces, length scale effects on plasticity become more and more important and bulk properties can no longer be used to describe the material properties. Even the elastic properties may be affected as the reduced coordination of surface atoms and the concomitant redistribution of electrons may soften or stiffen the material. If, and to what extend, such length scale effects control the mechanical behavior of nanoporous materials depends strongly on the material and the characteristic length scale associated with its plastic deformation. For example, ductile materials such as metals which deform via dislocation-mediated processes can be expected to exhibit pronounced length scale effects in the sub-micron regime where free surfaces start to constrain efficient dislocation multiplication. In this chapter we will limit our discussion to our own area of expertise which is the mechanical behavior of nanoporous open-cell gold foams as a typical example of nanoporous metal foams. Throughout this chapter we will review our current understanding of the mechanical properties of nanoporous open-cell foams including both experimental and theoretical studies.

  2. Cyclic Shearing Deformation Behavior of Saturated Clays

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    The apparatus for static and dynamic universal triaxial and torsional shear soil testing is employed to perform stress-controlled cyclic single-direction torsional shear tests and two-direction coupled shear tests under unconsolidated-undrained conditions. Through a series of tests on saturated clay, the effects of initial shear stress and stress reversal on the clay's strain-stress behavior are examined, and the behavior of pore water pressure is studied. The experimental results indicate that the patterns of stress-strain relations are distinctly influenced by the initial shear stress in the cyclic single-direction shear tests. When the initial shear stress is large and no stress reversal occurs, the predominant deformation behavior is characterized by an accumulative effect. When the initial shear stress is zero and symmetrical cyclic stress occurs, the predominant deformation behavior is characterized by a cyclic effect. The pore water pressure fluctuates around the confining pressure with the increase of cycle number. It seems that the fluctuating amplitude increases with the increase of the cyclic stress. But a buildup of pore water pressure does not occur. The deformations of clay samples under the complex initial and the cyclic coupled stress conditions include the normal deviatoric deformation and horizontal shear deformation, the average deformation and cyclic deformation. A general strain failure criterion taking into account these deformations is recommended and is proved more stable and suitable compared to the strain failure criteria currently used.

  3. Hot deformation behavior of FGH96 superalloys

    Institute of Scientific and Technical Information of China (English)

    Jiantao Liu; Guoquan Liu; Benfu Hu; Yuepeng Song; Ziran Qin; Yiwen Zhang

    2006-01-01

    The hot deformation behavior of FGH96 superalloys at 1070-1170℃ and 5×10-4-2×10-1 s-1 were investigated by means of the isothermal compression tests at a Gleeble-1500 thermal mechanical simulator. The results show that dynamic recovery acts as the main softening mechanism below 2×10-3 s-1, whereas dynamic recrystallization acts as the main softening mechanism above 2×10-3 s-1during deformation; the temperature increase caused by the deformation and the corresponding softening stress is negligible; the thermal-mechanical constitutive model to describe the hot deformation behavior is given, and the value of the apparent deformation activation energy (Qdef) is determined to be 354.93 kJ/mol.

  4. Materials issues in some advanced forming techniques, including superplasticity

    Energy Technology Data Exchange (ETDEWEB)

    Wadsworth, J.; Henshall, G.A.; Nieh, T.G. [and others

    1995-08-22

    From mechanics and macroscopic viewpoints, the sensitivity of the flow stress of a material to the strain rate, i.e. the strain rate sensitivity (m), governs the development of neck formation and therefore has a strong influence on the tensile ductility and hence formability of materials. Values of strain rate sensitivity range from unity, for the case of Newtonian viscous materials, to less than 0.1 for some dispersion strengthened alloys. Intermediate values of m = 0.5 are associated with classical superplastic materials which contain very fine grain sizes following specialized processing. An overview is given of the influence of strain rate sensitivity on tensile ductility and of the various materials groups that can exhibit high values of strain rate sensitivity. Recent examples of enhanced formability (or extended tensile ductility) in specific regimes between m = 1 and m = 0.3 are described, and potential areas for commercial exploitation are noted. These examples include: internal stress superplasticity, superplastic ceramics, superplastic intermetallics, superplastic laminated composites, superplastic behavior over six orders of magnitude of strain rate in a range of aluminum-based alloys and composites, and enhanced ductility in Al-Mg alloys that require no special processing for microstructural development.

  5. The relation between severe plastic deformation microstructure and corrosion behavior of AZ31 magnesium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Ben Hamu, G. [Department of Materials Engineering, Ben-Gurion University of the Negev, Beer-Sheva 84105 (Israel); Eliezer, D. [Department of Materials Engineering, Ben-Gurion University of the Negev, Beer-Sheva 84105 (Israel); Institute of Materials Science and Engineering, TU Clausthal (Germany)], E-mail: deliezer@bgu.ac.il; Wagner, L. [Institute of Materials Science and Engineering, TU Clausthal (Germany)

    2009-01-22

    The quest for ever, higher performance in structural applications has resulted in the outgoing development of new or improved materials with novel crystallographic textures, microstructures, and compositions. However, commercial applicability of such materials depends heavily on the development of economical and robust manufacturing methods. Due to the promise of excellent properties, such as superplasticity, high strength, good ductility, enhanced high cycle fatigue life, and good corrosion resistance, interest has grown in nanostructure bulk materials. Those materials are defined most often as materials exhibiting nanocrystalline grain structures and particle sizes below 100 nm in at least one dimension. In recent years, bulk nanostructure materials processed by methods of severe plastic deformation (SPD) such as equal channel angular extrusion (ECAE) have attracted the growing interest of specialists in materials science. The main object of this research is to compare the microstructural changing and corrosion behavior of magnesium alloy AZ31 after extrusion and severe plastic deformation by ECAE process. The ECAE process can produce intense and uniform deformation by simple shear and provides a convenient procedure for introducing an ultra fine grain size into a material. The samples were prepared by using hot extrusion methods. Hardness and AC and DC polarization tests were carried out on the extruded rods, and the microstructure was examined using optical, electron microscopy (SEM, TEM) and EDS. The results showed that the severe plastic deformation process affected both the microstructure and the corrosion behavior of AZ31 Mg alloy. These results can be explained by the effects of the process on microstructure of AZ31 Mg alloy such as grain size and dislocation density caused by the change in recrystallization behavior.

  6. Large deformation behavior of fat crystal networks

    NARCIS (Netherlands)

    Kloek, W.; Vliet, van T.; Walstra, P.

    2005-01-01

    Compression and wire-cutting experiments on dispersions of fully hydrogenated palm oil in sunflower oil with varying fraction solid fat were carried out to establish which parameters are important for the large deformation behavior of fat crystal networks. Compression experiments showed that the app

  7. Activation Energy for Superplastic Flow Above Critical Temperature of Die Steels

    Institute of Scientific and Technical Information of China (English)

    WEN Jiu-ba; ZHANG Ke-ke; CHEN Fu-xiao; YANG Yong-shun

    2006-01-01

    Some commercial cold working die steels GCr15 and CrWMn with ultra-fine grain size were chosen as tested materials to research the activation energy for superplastic flow at different temperatures and strain rates above critical temperature. Based on the Arrhenius equation, the activation energy for superplastic flow is evaluated. The activation energy at constant strain rate is estimated by the logσt vs 1/T relationship. The results show that the activation energy is usually small under the conditions of optimal flow. The characteristics of superplastic deformation of steels above the critical temperature were also analyzed.

  8. Superplasticity of a Ti-24Al-14Nb-3V-0.5Mo Intermetallic Alloy

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Superplastic properties and microstructural evolution of a Ti-24Al-14Nb-3V-0.5Mo (at. pct)intermetallic alloy were studied. Optimum superplastic properties were obtained for temperatures in the interval 960°C< T<980°C. The apparent activation energy in the superplastic regime was determined and the deformation mechanism was also discussed. Based on the studies, a curve panel with three sheets sandwich structure was fabricated successfully. The microstructures corresponding to different strain in the part were also studied.

  9. Sputter deposition of pure titanium onto complete denture base of Ti-6Al-4V deformed by superplastic forming. Chososei keiseishita Ti-6Al-4V gishi zenbusho eno sputter jochaku ni yoru jun Ti no hifuku

    Energy Technology Data Exchange (ETDEWEB)

    Kato, M.; Sonoda, T. (Government Industrial Research Institute, Nagoya, Nagoya (Japan))

    1991-07-01

    In order to improve the biocompatibility of TiNi shape memory alloy and Ti-6Al-4V alloy of functional Ti base alloys which are paid attention as the dental materials or implant materials, the sputter deposition coating using bio-inactive Ti metal was studied. DC source was superior to RF source in characteristics of sputtered film and the rate of deposition. The wiping with gauze impregnated by acetone followed by the ultrasonic cleaning was more effective for the precleaning of the substrate. The sputtered Ti film thickness was nearly proportional to electric power and showed the orientation which depended highly on the heating temperature of the substrate. The complete surface of denture base of Ti-6Al-4V deformed by superplastic forming was well coated with pure Ti and the prospect of biocompatibility of this Ti alloy could be obtained. But the film deposited by the heating condition showed the different characteristics of film compared with that formed under the cooling condition, and it is necessary that the effect of this on the biocompatibility must be investigated. 10 refs., 11 figs.

  10. Effect of equal channel angular extrusion on the microstructure and superplasticity of an Al-Li alloy

    Science.gov (United States)

    Salem, H. G.; Lyons, J. S.

    2002-08-01

    This research investigates the use of equal channel angular extrusion (ECAE) processing to produce a superplastic form of the aluminum alloy 2098. The starting material was a hot-rolled and precipitation-hardened plate with elongated grains of width 67-92 µm, and a composition in weight percent of 2.2% Li, 1.3% Cu, 0.73% Mg, 0.05% Zr, balance Al. Microstructural evolution was investigated with optical and transmission electron microscopy (TEM) and microhardness measurements after each step of a multipass ECAE process. ECAE produced a submicron grain structure with an average size of about 0.5 µm. The sub-grain microstructure size was a function of the magnitude of the input strain and the extrusion temperature. Misorientation angles of the developed submicron structure increase with increasing number of passes at warm working temperatures. Superplastic behavior of the ECAE-processed alloy was achieved. However, the low zirconium content of the 2098 alloy resulted in grain growth of the refined structure at the superplastic processing temperatures, placing a lower limit on the deformation rates that can be used.

  11. Hot Deformation Behavior of 2124 Al Alloy

    Institute of Scientific and Technical Information of China (English)

    S.Ramanathan; R.Karthikeyan; V.Deepak Kumar; G.Ganesan

    2006-01-01

    The mechanical behavior of 2124 Al alloy produced by powder metallurgy was investigated with compression test at different temperatures and strain rates. The tests were performed in the temperature range of 300℃~500℃ and at strain rates from 0.001 s-1 to 1.0 s-1. The compression flow curves exhibited an initial sharp increase with strain, followed by monotonous hardening. The maximum stress decreased with decreasing strain rate and increasing temperature. The hot deformation characteristics of the material were studied using processing maps. The domain of safety and unsafe regime were identified and validated through microstructural examination.

  12. A two-step superplastic forging forming of semi-continuously cast AZ70 magnesium alloy

    Directory of Open Access Journals (Sweden)

    Pan Wang

    2015-03-01

    Full Text Available A two-step technology combined forging with superplastic forming has been developed to enhance the forgeability of semi-continuously cast AZ70 magnesium alloy and realize the application of the as-cast magnesium alloy in large deformation bullet shell. In the first step, fine-grained microstructure preforms that are suitable for superplastic forming were obtained by reasonably designing the size of the initial blanks with the specific height-to-diameter ratio, upsetting the blanks and subsequent annealing. In the second step, the heat treated preforms were forged into the end products at the superplastic conditions. The end products exhibit high quality surface and satisfied microstructure. Consequently, this forming technology that not only avoids complicating the material preparation but also utilizes higher strain rate superplastic provides a near net-shaped novel method on magnesium forging forming technology using as-cast billet.

  13. Superplasticity in an Aluminum Alloy 6061/A12O3p Composite

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    The superplasticity of an Al2O3p/6061Al composite, fabricated by powder metallurgy techniques,has been investigated. Instead of any special thermomechanical processing or hot rolling, simple hot extrusion has been employed to obtain a fine grained structure before superplastic testing.Superplastic tensile tests were performed at strain rates ranging from 10-2 to 10-4 s-1 and at temperatures from 833 to 893 K. A maximum elongation of 200% was achieved at a temperature of 853 K and an initial strain rate of 1.67×10-3 s-1. The highest value obtained for the strain rate sensitivity index (m) was 0.32. Differential scanning calorimeter was used to ascertain the possibility of any partial melting in the vicinity of optimum superplastic temperature. These results suggested that no liquid phase existed where maximum elongation was achieved and deformation took place entirely in the solid state.

  14. Integrated Manufacturing of Aerospace Components by Superplastic Forming Technology

    Directory of Open Access Journals (Sweden)

    Ju Min Kyung

    2015-01-01

    Full Text Available Aerospace vehicle requires lightweight structures to obtain weight saving and fuel efficiency. It is known that superplastic characteristics of some materials provide significant opportunity for forming complicated, lightweight components of aerospace structure. One of the most important advantages of using superplastic forming process is its simplicity to form integral parts and economy in tooling[1]. For instance, it can be applied to blow-forming, in which a metal sheet is deformed due to the pressure difference of hydrostatic gas on both sides of the sheet. Since the loading medium is gas pressure difference, this forming is different from conventional sheet metal forming technique in that this is stress-controlled rather than strain and strain rate controlled. This method is especially advantageous when several sheet metals are formed into complex shapes. In this study, it is demonstrated that superplastic forming process with titanium and steel alloy can be applied to manufacturing lightweight integral structures of aerospace structural parts and rocket propulsion components. The result shows that the technology to design and develop the forming process of superplastic forming can be applied for near net shape forming of a complex contour of a thrust chamber and a toroidal fuel tank.

  15. Deformation, fatigue and fracture behavior of two cast anisotropic superalloys

    Science.gov (United States)

    Milligan, Walter W.; Huron, Eric S.; Antolovich, Stephen D.

    1987-01-01

    Tensile and low cycle fatigue (LCF) tests were conducted on two cast anisotropic superalloys. The effects of temperature, strain rate and stress range were investigated. Deformation behavior was extensively characterized and modeled. LCF and fracture behavior were studied and correlated with deformation behavior.

  16. Superplasticity and cooperative grain boundary sliding in nanocrystalline Ni{sub 3}Al

    Energy Technology Data Exchange (ETDEWEB)

    Mara, N.A. [Center for Integrated Nanotechnologies, Los Alamos National Laboratory, Los Alamos, NM 87545 (United States)], E-mail: namara@lanl.gov; Sergueeva, A.V.; Mara, T.D. [Materials Science Division, University of California, Davis, One Shields Avenue, Davis, CA 95616 (United States); McFadden, S.X. [Sandia Laboratories, Livermore, CA 94550 (United States); Mukherjee, A.K. [Materials Science Division, University of California, Davis, One Shields Avenue, Davis, CA 95616 (United States)

    2007-08-15

    Cooperative grain boundary sliding (CGBS) has been shown to account for the majority of macroscopic strain seen in microcrystalline metallic systems undergoing superplastic deformation. While CGBS has been observed on the surface of microcrystalline samples deforming superplastically through the shifting of diamond scribe lines, there have been few transmission electron microscopy results showing such occurrences in the bulk of the material, or the details behind the micromechanism of CGBS. In this work, nanocrystalline Ni{sub 3}Al produced via high-pressure torsion is deformed superplastically in the electron microscope. High-temperature ({approx}700 deg. C) in situ tensile testing shows the nature of CGBS at the nanoscale through direct observation of this phenomenon.

  17. Current assisted superplastic forming of titanium alloy

    Directory of Open Access Journals (Sweden)

    Wang Guofeng

    2015-01-01

    Full Text Available Current assisted superplastic forming combines electric heating technology and superplastic forming technology, and can overcome some shortcomings of traditional superplastic forming effectively, such as slow heating rate, large energy loss, low production efficiency, etc. Since formability of titanium alloy at room temperature is poor, current assisted superplastic forming is suitable for titanium alloy. This paper mainly introduces the application of current assisted superplastic forming in the field of titanium alloy, including forming technology of double-hemisphere structure and bellows.

  18. Superplasticity in ceramic and metal matrix composites and the role of grain size, segregation, interfaces, and second phase morphology

    Energy Technology Data Exchange (ETDEWEB)

    Wadsworth, J.; Nieh, T.G.

    1992-10-01

    Structural ceramics and ceramic composites have been shown to exhibit superplasticity in recent times and this discovery has attracted tremendous interest. Although the number of ceramics exhibits superplasticity is now quite large, there are gaps in understanding the requirements for superplasticity in ceramics. Also, superplastic behavior at very high strain rates (1 s{sup {minus}1}) in metallic-based materials is an area of increasing research. In this case, the phenomenon has been observed quite extensively in aluminum alloy-based metal matrix composites and mechanically alloyed aluminum- and nickel-based materials. Again, the details of the structural requirements of this phenomenon are not yet understood. In the present paper, experimental results on superplasticity in ceramic-based materials and on high strain rate behavior in metallic-based materials are presented. The roles of grain size, grain boundary and interface chemistry, and second phase morphology and compatibility with the matrix material will be emphasized.

  19. Strain-hardening and warm deformation behaviors of extruded Mg–Sn–Yb alloy sheet

    Directory of Open Access Journals (Sweden)

    Jing Jiang

    2014-06-01

    Full Text Available Strain-hardening and warm deformation behaviors of extruded Mg–2Sn–0.5Yb alloy (at.% sheet were investigated in uniaxial tensile test at temperatures of 25–250 °C and strain rates of 1 × 10−3 s−1–0.1 s−1. The data fit with the Kocks–Mecking type plots were used to show different stages of strain hardening. Besides III-stage and IV-stage, the absence of the II-stage strain hardening at room temperature should be related to the sufficient dynamic recrystallization during extrusion. The decrease of strain hardening ability of the alloy after yielding was attributed to the reduction of dislocation density with increasing testing temperature. Strain rate sensitivity (SRS was significantly enhanced with increasing temperature, and the corresponding m-value was calculated as 0.07–0.12, which indicated that the deformation mechanism was dominated by the climb-controlled dislocation creep at 200 °C. Furthermore, the grain boundary sliding (GBS was activated at 250 °C, which contributed to the higher SRS. The activation energy was calculated as 213.67 kJ mol−1, which was higher than that of lattice diffusion or grain boundary self-diffusion. In addition, the alloy exhibited a quasi superplasticity at 250 °C with a strain rate of 1 × 10−3 s−1, which was mainly related to the fine microstructure and the presence of the Mg2Sn and Mg2(Sn,Yb particles.

  20. Modeling and optimization of shape change in shell spatial cross-sections under superplastic moulding

    Science.gov (United States)

    Chumachenko, E. N.

    2008-08-01

    The necessity to develop and optimize new technological processes of gas moulding of shells under the superplasticity conditions, which ensure large elongation and complexity of the shape of end items, makes the specialists in the field of mathematical simulation to pose and solve problems of constant improvement of the imitation models. Because of a large number of "embedded" nonlinearities (the physical properties of the material, friction, and unknown boundaries), the solution of such problems requires large computer resources, high qualification of designers, and large amount of labor. In the present paper, we consider the problems of express analysis of pattern change of spatial shells on the basis of estimation of the behavior of their critical cross-sections. We solve problems of moulding of titan shells (made of VT6 alloy) in a matrix of complicated shape. We theoretically and experimentally justify the methods for predicting and constructing the optimal technological processes of shell deformation under conditions close to superplasticity by using the 2.5D designing procedures.

  1. An investigation of neutron irradiation test on superplastic zirconia-ceramic materials

    Energy Technology Data Exchange (ETDEWEB)

    Shibata, Taiju; Ishihara, Masahiro; Baba, Shinichi; Hayashi, Kimio [Japan Atomic Energy Research Inst., Oarai, Ibaraki (Japan). Oarai Research Establishment; Motohashi, Yoshinobu [Ibaraki Univ., Mito (Japan)

    2000-05-01

    A neutron irradiation test on superplastic ceramic materials at high temperature has been proposed as an innovative basic research on high-temperature engineering using the High Temperature Engineering Test Reactor (HTTR). For the effective execution of the test, we reviewed the superplastic deformation mechanism of ceramic materials and discussed neutron irradiation effects on the superplastic deformation process of stabilized Tetragonal Zirconia Polycrystal (TZP), which is a representative superplastic ceramic material. As a result, we pointed out that the decrease in the activation energy for superplastic deformation is expected by the radiation-enhanced diffusion. We selected a fast neutron fluence of 5x10{sup 20} n/cm{sup 2} and an irradiation temperature of about 600degC as test conditions for the first irradiation test on TZP and decided to perform a preliminary irradiation test by the Japan Materials Testing Reactor (JMTR). Moreover, we estimated the radioactivity of irradiated TZP and indicated that it is in the order of 10{sup 10} Bq/g (about 0.3 Ci/g) immediately after irradiation to a thermal neutron fluence of 3x10{sup 20} n/cm{sup 2} and that it decays to about 1/100 in a year. (author)

  2. Method of producing superplastic alloys and superplastic alloys produced by the method

    Science.gov (United States)

    Troeger, Lillianne P. (Inventor); Starke, Jr., Edgar A. (Inventor); Crooks, Roy (Inventor)

    2002-01-01

    A method for producing new superplastic alloys by inducing in an alloy the formation of precipitates having a sufficient size and homogeneous distribution that a sufficiently refined grain structure to produce superplasticity is obtained after subsequent PSN processing. An age-hardenable alloy having at least one dispersoid phase is selected for processing. The alloy is solution heat-treated and cooled to form a supersaturated solid solution. The alloy is plastically deformed sufficiently to form a high-energy defect structure useful for the subsequent heterogeneous nucleation of precipitates. The alloy is then aged, preferably by a multi-stage low and high temperature process, and precipitates are formed at the defect sites. The alloy then is subjected to a PSN process comprising plastically deforming the alloy to provide sufficient strain energy in the alloy to ensure recrystallization, and statically recrystallizing the alloy. A grain structure exhibiting new, fine, equiaxed and uniform grains is produced in the alloy. An exemplary 6xxx alloy of the type capable of being produced by the present invention, and which is useful for aerospace, automotive and other applications, is disclosed and claimed. The process is also suitable for processing any age-hardenable aluminum or other alloy.

  3. Metallurgical Characterization of Superplastic Forming

    Science.gov (United States)

    1980-09-01

    The trans - formation of constant-crosshead-speed stress-strain curves into constant-strain- rate curves is clearly not satisfactory because it is based...MILL-ANNEALED AND SUPERPLASTICALLY- FORMED CONDITIONS; FORMING TEMPERATURE - 949EPC (17400F). 01"tln Stoi rte yeld grasa Ultimate l to oret~lSri as...1975), p. 163. 7. G. Rai and N. J. Grant, "On the Measurermients of Superplasticity in an Al-Cu Alloy," Met. Trans . 6A, 385 (1975). 8. A. K, Mukherjee

  4. Grain size control and superplasticity in 6013-type aluminum alloys

    Science.gov (United States)

    Troeger, Lillianne Plaster Whitelock

    grain diameter of ˜10 mum. The refined microstructure exhibits superplasticity above 500°C, where the strain rate sensitivity reaches a maximum of 0.5 (at 540°C for strain rates between 2 x 10-4 s-1 and 5 x 10-4 s-1). The maximum uniaxial elongation (375%) occurred in the regime of the maximum strain rate sensitivity. The corresponding flow stress was 680 psi (4.7 Mpa). Biaxial cone tests were performed in order to better evaluate the high-temperature forming characteristics of the material. During tests with back pressure, cone height-to-radius ratios near 1.2 were obtained with maximum strain approaching 2.0 for strain rates near 1 x 10-3 s-1 . The effect of superplastic deformation on the microstructure is described in terms of the effect of strain on grain size and porosity for a cone sample. The ultimate goal of the project is to advance the fundamental understanding of the complex interrelationships between processing, microstructure, and superplastic performance.

  5. Achieving superplastic properties in a ZK10 magnesium alloy processed by equal-channel angular pressing

    Directory of Open Access Journals (Sweden)

    Roberto B. Figueiredo

    2017-04-01

    Full Text Available Equal-channel angular pressing provides an opportunity for refining the grain structure and introducing superplastic properties in magnesium alloys. This report describes the use of this processing technique with a ZK10 (Mg–1.0 wt.% Zn–0.26 wt.% Zr alloy. The grain structure was successfully refined from ∼12.9 to ∼5.2 μm after 4 passes and superplastic elongations were observed when testing at low strain rates at temperatures of 473 and 523 K. An analysis shows that the superplastic behavior is consistent with the conventional theoretical model for superplastic flow and at higher stresses and strain rates there is a transition to control by a viscous glide process.

  6. Superplastic forming gas pressure of titanium alloy bellows

    Institute of Scientific and Technical Information of China (English)

    王刚; 张凯锋; 陈军; 阮雪榆

    2004-01-01

    The complex superplastic forming (SPF) technology applying gas pressure and compressive axial load is an advanced forming method for titanium alloy bellows, whose forming process consists of the three main forming phases namely bulging, clamping and calibrating phase. The influence of forming gas pressure in various phases on the forming process was analyzed and the models of forming gas pressure for bellows were derived according to the thin shell theory and the plasticity deformation theory. Using the model values, taking a two-convolution DN250 Ti6Al-4V titanium alloy bellows as an example, a series of superplastic forming tests were performed to evaluate the influence of the variation of forming gas pressure on the forming process. According to the experimental results these models were corrected to make the forming gas pressures prediction more accurate.

  7. Superplasticity in Aeroengine Titanium Alloy VT-9 and its Modified Compositions

    Directory of Open Access Journals (Sweden)

    Abhijit Dutta

    1986-04-01

    Full Text Available The alloy (Ti-6.5AL-3.3 Mo-1.6Zr-O.3Si is a Soviet composition designated VT-9. Excellent superplastic characteristics found by us in this alloy prompted us to explore the possibility of use of Si-free VT-9 in sheet form for superplastic forming. An optimum thermomechanical processing produced a microstructure that resulted in an elongation of 1700 per cent at a fairly high deformation rate (2 X 10-3 set-1. Thus, the same aeroengine alloy (VT-9 can be used for superplastically formed airframe parts in the Si-free condition. The present study also shows that for making the forming process commercially viable, deformation temperature could be lowered by temporarily alloying with hydrogen in a particular concentration range (0.1 to 0.2 wt per cent.

  8. Dynamic reverse phase transformation induced high-strain-rate superplasticity in low carbon low alloy steels with commercial potential.

    Science.gov (United States)

    Cao, Wenquan; Huang, Chongxiang; Wang, Chang; Dong, Han; Weng, Yuqing

    2017-08-23

    Superplastic materials are capable of exhibiting large tensile elongation at elevated temperature, which is of great industrial significance because it forms the basis of a fabrication method to produce complex shapes. Superplasticity with elongation larger than 500% has been widely realized in many metals and alloys, but seldomly been succeeded in low carbon low alloy steel, even though it is commercially applied in the largest quantity. Here we report ultrahigh superplastic elongation of 900-1200% in the FeMnAl low carbon steels at high strain rate of 10(-2)-10(-3) s(-1). Such high-strain-rate superplasticity was attributed to dynamic austenite reverse phase transformation from a heavily cold rolled ferrite to fine-grained ferrite/austenite duplex microstructure and subsequent limited dynamic grain coarsening, under which a large fraction of high angle boundaries can be resulted for superplastic deformation. It is believed that this finding of the low carbon low alloy steel with ultrahigh superplasticity and relative low cost would remarkably promote the application of superplastic forming technique in automobile, aeronautical, astronautical and other fields.

  9. Deformation behavior and microstructure evolution of wrought magnesium alloys

    Science.gov (United States)

    Wang, Shouren; Song, Linghui; Kang, Sukbong; Cho, Jaehyung; Wang, Yingzi

    2013-05-01

    There are many researches on the deformation behavior of wrought magnesium alloys, such as AZ31, AZ80, AZ91, and ZK60 magnesium alloys at different temperatures and strain rates, but few of them focuses on the deformation behavior of AZ41M and ZK60M alloys, especially under the twin-roll casting (TRC) state. Meanwhile, the existing researches only focus on the grain refinement law of the magnesium alloys under deformation conditions, the deformation mechanism has not been revealed yet. The hot compression behavior of AZ41M and ZK60M magnesium alloys under the temperature and strain rate ranges of 250-400 °C and 0.001-1 s-1 are studied by thermal simulation methods using Gleeble 1500 machine and virtual simulation using finite element analysis software. Simulation results show that sine hyperbolic law is the most suitable flow stress model for wider deformation conditions. The most reasonable selected deformation conditions of ZK60M alloy is 350 °C/0.1 s-1 for TRC and 350 °C/1 s-1 for conventional casting (CC), while AZ41M alloy is 300 °C/0.01 s-1 for TRC and 350 °C/0.1 s-1 for CC. Deformation behavior and dynamic recrystallization (DRX) mechanism of them are analyzed at the same deformation conditions. The microstructures of AZ41M and ZK60M alloys are observed at different deformed conditions by optical microscopy (OM) and electron back scatter diffraction (EBSD) and it reveals the flow behavior and deformation mechanism of them. Working harden and work soften contribute to the activation of basal, non-basal slip systems which promote DRX. The proposed research reveals the deformation behavior and mechanism of the AZ41M and ZK 60M magnesium alloys and concludes their optimized deformation parameters and processes and provides a theory basis for their manufacturing and application.

  10. Maintaining the mechanical strength of La-, Y-co-substituted zirconia porous ceramics through the superplastically foaming method

    Energy Technology Data Exchange (ETDEWEB)

    Kishimoto, Akira, E-mail: kishim-a@cc.okayama-u.ac.jp; Okada, Masanori; Teranishi, Takashi; Hayashi, Hidetaka

    2013-10-01

    The superplastically foaming method was adopted to make closed-pore inclusive zirconia-based ceramics. Lanthanum oxide was added to monoclinic or tetragonal yttria-stabilised zirconia to reduce the thermal conductivity of the matrix. Sintering and superplastic deformation led to a solid solution and transformation to the cubic phase. The resulting superplastically foamed porous ceramics having a porosity of 45% had only 40% of the thermal conductivity of the fully densified ceramics having the same composition. This value was comparable to that of conventionally fabricated porous ceramics with the same composition and porosity. The superplastically foamed ceramics had 60%, while conventionally fabricated ceramics had only 20%, of the mechanical strength of the fully dense ceramics.

  11. Isothermal superplastic solid state bonding of 40Cr and Cr12MoV steels based on surface modification

    Institute of Scientific and Technical Information of China (English)

    Zhang Keke; Zhang Zhanling; Liu Shuai; Yue Yun; Ma Ning; Yang Yunlin

    2009-01-01

    Based on the feasibility of isothermal superplastic solid state bonding of 40Cr and Cr12MoV steels, the surfaces of both steels to be bonded were ultra-fined through high frequency hardening, then the superplastic solid state bonding were conducted, the microstructure and fracture surface of bonded joint were observed and analysed, and bonding mechanisms was researched. The experimental results show that with the sample surfaces of 40Cr and Cr12MoV steels after the high frequency hardening, under the prepressing stress of 56.6 MPa, initial strain rate of 1.5×10~(-2) min~(-1) and at the bonding temperature of 800-820℃, the superplastic solid state bonding can be carried out in about 3.5min, and the joint strength is up to that of 40Cr steel base metal and the radial expansion ratio of the joint does not exceed 6%. The superplastic solid state bonding parameter of both steels is within the ranges of the isothermal compressive superplastic deformation of Cr12MoV steel, and the deformation in Cr12MoV steel side near the interfacial zone of joint presents the characteristic of superplasticity. In bonding process, the atoms in two sides of joint interface have diffused each other.

  12. Superplastically foaming method to make closed pores inclusive porous ceramics

    Energy Technology Data Exchange (ETDEWEB)

    Kishimoto, Akira; Hayashi, Hidetaka, E-mail: kishim-a@cc.okayama-u.ac.jp [Division of Molecular and Material Science, Graduate School of Natural Science and Technology, Okayama University Okayama (Japan)

    2011-04-15

    Porous ceramics incorporates pores to improve several properties including thermal insulation maintaining inherenet ceramic properties such as corrosion resistance and large mechanical strength. Conventional porous ceramics is usually fabricated through an insufficient sintering. Since the sintering accompanies the exclusion of pores, it must be terminated at the early stage to maintain the high porosity, leading to degraded strength and durability. Contrary to this, we have innovated superplastically foaming method to make ceramic foams only in the solid state. In this method, the previously inserted foam agent evaporates after the full densification of matrix at around the sintering temperature. Closed pores expand utilizing the superplastic deformation driven by the evolved gas pressure. The typical features of this superplastically foaming method are listed as follows, 1. The pores are introduced after sintering the solid polycrystal. 2. Only closed pores are introduced, improving the insulation of gas and sound in addition to heat. 3. The pore walls are fully densified expecting a large mechanical strength. 4. Compared with the melt foaming method, this method is practical because the fabrication temperature is far below the melting point and it does not need molds. 5. The size and the location pores can be controlled by the amount and position of the foam agent.

  13. SUPERPLASTICITY OF A SiCw/2024 Al COMPOSITE MADE BY PRESSURE INFILTRATION

    Institute of Scientific and Technical Information of China (English)

    X.J. Xu; W. Wang; L. Cai

    2002-01-01

    The superplastic characteristics of the β-SiC whisker reinforced 2024 aluminum com-posite, fabricated by pressure infiltration and hot-rolling after extrusion, were inves-tigated. The composite has a fine grain size of about 1μm, and exhibits a maximumtensile elongation of 370% in the initial strain rate of 3.3× 10-3 s-1 at 788K. The su-perplastic deformation mechanism of the composite is thought to be grain boundary(interface) sliding accommodated by grain boundary diffusion of aluminum atom andan appropriate amount of liquid phase.

  14. Recrystallization and superplasticity at 300 C in an aluminum-magnesium alloy

    Science.gov (United States)

    Hales, S. J.; Mcnelley, T. R.; Mcqueen, H. J.

    1991-01-01

    Variations in thermomechanical processing (TMP) which regulate the microstructural characteristics and superplastic response of an Al-10Mg-0.1Zr alloy at 300 C were evaluated. Mechanical property data revealed that the superplastic ductility can be enhanced by simultaneously increasing the total rolling strain, the reduction per pass, and the duration of reheating intervals between passes during isothermal rolling. Texture and microscopy data were consistent with the development of a refined microstructure by recovery-dominated processes, i.e., continuous recrystallization, during the processing. The mechanisms by which a refined substructure can be progressively converted into a fine-grained structure during repeated cycles of deformation and annealing are addressed. A qualitative description of the complex sequence of developments leading to a microstructure better suited to support superplastic response is presented.

  15. Recrystallization and superplasticity at 300 °C in an aluminum-magnesium alloy

    Science.gov (United States)

    Hales, S. J.; McNelley, T. R.; McQueen, H. J.

    1991-05-01

    Variations in thermomechanical processing (TMP) which regulate the microstructural characteristics and superplastic response of an Al-lOMg-0.1Zr alloy at 300 °C were evaluated. Mechanical property data revealed that the superplastic ductility can be enhanced by simultaneously increasing the total rolling strain, the reduction per pass, and the duration of reheating intervals between passes during isothermal rolling. Texture and microscopy data were consistent with the development of a refined microstructure by recovery-dominated processes, i.e., continuous recrystallization, during the processing. The mechanisms by which a refined substructure can be progressively converted into a fine-grained structure during repeated cycles of deformation and annealing are addressed. A qualitative description of the complex sequence of developments leading to a microstructure better suited to support superplastic response is presented.

  16. Effect of partial melting on superplasticity ofAlNp/6061Al composite

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    AlN particulate reinforced 6061 aluminum alloy composite was fabricated by powder metallurgy method and hot-rolled after extrusion. Tensile strength and elongation at elevated temperature were measured by tensile test at initial strain rates between 10-2 s-1 and 100 s-1. The AlNp/6061Al composite exhibits an m-value of 0.42 and a maximum elongation of 450% at 863?K. Differential scanning calorimeter was used to ascertain the possibility of any partial melting in the vicinity of optimum superplastic temperature. Partial melting resulting from solute segregation at interfaces has much influence on superplasticity of the composite. It is postulated that AlNp/matrix interface sliding occurs along with grain boundary in superplastic deformation.

  17. Effect of Rare Earth on Superplasticity of Zn-5Al Eutectic Alloy

    Institute of Scientific and Technical Information of China (English)

    石志强; 叶以富; 李世春; 王焕荣; 滕新营

    2002-01-01

    The superplastic deformation curves of Zn-5Al eutectic alloy containing small amount of rare earth were measured, and the influence of rare earth on structure and superplasticity characteristics of the alloy was examined with optical microscope, XDF and TEM. The results show that the elongation of Zn-5Al eutectic alloy can be increased if less than 0.2 %(mass fraction) misch-metal was added. Rare earth which exists in the form of compounds Al2CeZn2 and CeZn3 can refrain the dissolution and diffusion of Zn to Al and postpone the saturation of the diffusion-dissolution zone(DDZ) above 350 ℃, and in such a way boost up α/β interface sliding which benefits the superplasticity.

  18. Deformation Behavior of Hot Isostatic Pressing FGH96 Superalloy

    Institute of Scientific and Technical Information of China (English)

    LIU Yuhong; LI Fuguo; YU Hongbo

    2006-01-01

    The deformation behavior of hot isostatic pressing (HIP) FGH96 superalloy was characterized in the temperature range of 1 000-1 100 ℃ and strain rate range of 0. 001-0.1 s-1 using hot compression testing. The flow curves of HIP FGH96 superalloy during hot deformation was analyzed systematically. The results show that deformation temperature, strain rate and strain are the main influence factors on flow stress of HIP FGH96 superalloy during hot deformation. The flow stress displays a peak at a critical strain and then decreases with further increase in strain. For a given strain, the flow stress decreases with the increase of deformation temperature, and increases with the increase of strain rate. A mathematical model of these flow curves was established through regression analysis and taking the strain as a modification factor. The calculated stress values agree well with the experimental values.

  19. The Cyclic Deformation Behavior of Severe Plastic Deformation (SPD Metals and the Influential Factors

    Directory of Open Access Journals (Sweden)

    Charles C. F. Kwan

    2012-02-01

    Full Text Available A deeper understanding of the mechanical behavior of ultra-fine (UF and nanocrystalline (NC grained metals is necessary with the growing interest in using UF and NC grained metals for structural applications. The cyclic deformation response and behavior of UF and NC grained metals is one aspect that has been gaining momentum as a major research topic for the past ten years. Severe Plastic Deformation (SPD materials are often in the spotlight for cyclic deformation studies as they are usually in the form of bulk work pieces and have UF and NC grains. Some well known techniques in the category of SPD processing are High Pressure Torsion (HPT, Equal Channel Angular Pressing (ECAP, and Accumulative Roll-Bonding (ARB. In this report, the literature on the cyclic deformation response and behavior of SPDed metals will be reviewed. The cyclic response of such materials is found to range from cyclic hardening to cyclic softening depending on various factors. Specifically, for SPDed UF grained metals, their behavior has often been associated with the observation of grain coarsening during cycling. Consequently, the many factors that affect the cyclic deformation response of SPDed metals can be summarized into three major aspects: (1 the microstructure stability; (2 the limitation of the cyclic lifespan; and lastly (3 the imposed plastic strain amplitude.

  20. Deformation behavior of curling strips on tearing tubes

    Energy Technology Data Exchange (ETDEWEB)

    Choi, Ji Won; Kwon, Tae Soo; Jung, Hyun Seung; Kim, Jin Sung [Dept. of Robotics and Virtual Engineering, Korea University of Science and Technology, Seoul (Korea, Republic of)

    2015-10-15

    This paper discusses the analysis of the curl deformation behavior when a dynamic force is applied to a tearing tube installed on a flat die to predict the energy absorption capacity and deformation behavior. The deformation of the tips of the curling strips was obtained when the curl tips and tube body are in contact with each other, and a formula describing the energy dissipation rate caused by the deformation of the curl tips is proposed. To improve this formula, we focused on the variation of the curl radius and the reduced thickness of the tube. A formula describing the mean curl radius is proposed and verified using the curl radius measurement data of collision test specimens. These improved formulas are added to the theoretical model previously proposed by Huang et al. and verified from the collision test results of a tearing tube.

  1. Deformation Behavior of Severely Deformed Al and Related Mechanisms Through Warm Tensile Test

    Science.gov (United States)

    Charkhesht, V.; Kazeminezhad, M.

    2017-01-01

    Flow stress and ductility behaviors of the annealed and severely deformed Al were investigated at warm deformation temperatures. Constrained groove pressing (CGP) method as a severe plastic deformation process was used. The tensile test was carried out at the temperature range of the 298-573 K and strain rate range of 0.001-0.1 s-1 to present the elevated temperature deformation behavior utilizing hyperbolic sine constitutive equation. The flow stress of the CGPed sample is increased with the number of CGP passes and decreased with temperature. Dynamic recovery and strain softening are found as main restoration mechanisms. Flow stress amounts are not remarkably affected by the strain rate. Values of the elongation are decreased with the number of CGP passes. Values of the calculated strain rate sensitivity are utilized to justify the elongation behavior. Shear bands created by CGP remarkably decrease the fracture elongation values. Temperature interval of 298-473 K cannot remarkably affect the flow stress and ductility. The interval of 473-573 K is chosen as critical temperature interval in which the values of flow stress and elongation are remarkably decreased and increased, respectively. Increasing the temperature up to 573 K causes recrystallization in shear bands. Scanning electron microscope was used to study fracture surface which can truly predict the elongation behavior. With increasing the temperature, the shear decohesion area is gradually replaced with fully dimpled structures. Finally, hot deformation activation energy for CGPed samples was calculated about 85 kJ/mol which is close to the grain boundary diffusion activation energy in pure Al.

  2. Deformation and fatigue behavior of SSME turbopump blade materials

    Science.gov (United States)

    Milligan, Walter W.; Antolovich, Stephen D.

    1987-01-01

    Directionally solidified and single crystal superalloys which are intended for use as turbopump blade materials are anisotropic both elastically and plastically. Therefore, isotropic constitutive models must be modified. Several models which are now being developed are based on metallurgical theories of deformation in these types of alloys. However, these theories have not been fully justified, and the temperature and strain regimes over which they may be valid are poorly defined. The objective of this work is to study the deformation behavior of the alloys, in order to determine the validity of these models and to thereby support the ongoing research efforts in solid mechanics.

  3. Deformation behavior of open-cell stainless steel foams

    Energy Technology Data Exchange (ETDEWEB)

    Kaya, A.C., E-mail: a.kaya@campus.tu-berlin.de; Fleck, C.

    2014-10-06

    This study presents the deformation and cell collapse behavior of open-cell stainless steel foams. 316L stainless-steel open-cell foams with two porosities (30 and 45 pores per inch, ppi) were produced with the pressureless powder metallurgical method, and tested in quasi-static compression. As a result of the manufacturing technique, 316L stainless steel open-cell foams have a high amount of microporosity. The deformation behavior was investigated on a macroscopic scale by digital image correlation (DIC) evaluation of light micrographs and on the microscopic scale by in situ loading of cells in the scanning electron microscope. The deformation behavior of the metal foams was highly affected by microstructural features, such as closed pores and their distribution throughout the foam specimen. Moreover, the closed pores made a contribution to the plateau stress of the foams through cell face stretching. Strut buckling and bending are the dominant mechanisms in cell collapse. Although there are edge defects on the struts, the struts have an enormous plastic deformation capability. The cell size of the steel foams had no significant effect on the mechanical properties. Due to the inhomogeneities in the microstructure, the measured plateau stresses of the foams showed about 20% scatter at the same relative density.

  4. SUPERPLASTICITY OF A WATER-QUENCHED AND TEMPERED 40Cr STEEL

    Institute of Scientific and Technical Information of China (English)

    X.J.Xu; G.L.Liu; L.J Shi; X.N.Cheng; L.Cai

    2004-01-01

    The superplastic deformation characteristics, of commercial 40Cr (i.e., 5140) steel that was water-quenched only 1 times and subsequent high-temperature tempered, were investigated.The results showed that the 40Cr steel has a fine grain of 10-15μm at room temperature,and exhibits a tensile elongation of 304%, a true flow stress of 89.3MPa and a strain rate sensitivity m-value of 0.227 at the initial strain rate of 1.0×10-3s-1and at the temperature of 750℃. The final fracture is caused by the development of neck. The experimental result of elongation is in good agreement with the theoretically predicated value according to the analytical expression ef = (1/f)mexp(nv+mε)-1(where ef, m, f, nv and e is respectively elongation, average strain rate sensitivity, initial geometric defect, average strain hardening sensitivity at constant deformation velocity and average true strain). The fracture surface is intergraular, and superplastic deformation induces an equiaxed and grown grain. Decreasing strain rate increases tensile elongation and strain rate sensitivity m-value. The primary superplastic deformation mechanism is thought to be atom-diffusion-controlled grain boundary sliding.

  5. Superplastic forming of Al-Li alloys for lightweight, low-cost structures

    Science.gov (United States)

    Hales, Stephen J.; Wagner, John A.

    1991-01-01

    Superplastic forming of advanced aluminum alloys is being evaluated as an approach for fabricating low-cost, light-weight, cryogenic propellant tanks. Built-up structure concepts (with inherent reduced scrap rate) are under investigation to offset the additional raw material expenses incurred by using aluminum lithium alloys. This approach to fabrication offers the potential for significant improvements in both structural efficiency and overall manufacturing costs. Superplasticity is the ability of specially processed material to sustain very large forming strains without failure at elevated temperatures under controlled deformation conditions. It was demonstrated that superplastic forming technology can be used to fabricate complex structural components in a single operation and increase structural efficiency by as much as 60 percent compared to conventional configurations in skin-stiffened structures. Details involved in the application of this technology to commercial grade superplastic aluminum lithium material are presented. Included are identification of optimum forming parameters, development of forming procedures, and assessment of final part quality in terms of cavitation volume and thickness variation.

  6. Investigation on hot deformation behavior of AZ31 madnesium alloy

    Institute of Scientific and Technical Information of China (English)

    汪凌云; HUANG; Guangsheng; 等

    2002-01-01

    The hot compressive deformation of extruded AZ31 magnesium alloy with the mass fractions of Al and Zn equal to 3%and 1% respectively is studied by a Gleeble-1500D thermal mechanical simulator over the temperature range from 200℃to 400℃ and the strain rate from 10-3 s-1 to 100s-1.The true stress-strain curves of the strain of 65% are tested.The deformation activation energy is obtained and the flow stress model is established by analyzng the effects of strain rate and temperature on the flow stress.Zener-Hollomon parameter is introduced to describe the softening behaviors of AZ31 magnesium alloy resulted from dynamic recrystallization during the hot compressive deformation,whose natural logarithm is linear with the critical strain of dynamic recrystallization.

  7. Hot deformation behavior of delta-processed superalloy 718

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Y., E-mail: wangyanhit@yahoo.cn [State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083 (China); School of Aeronautics and Astronautics, Central South University, Changsha 410083 (China); Shao, W.Z.; Zhen, L.; Zhang, B.Y. [School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001 (China)

    2011-03-25

    Research highlights: {yields} The peak stress for hot deformation can be described by the Z parameter. {yields} The grain size of DRX was inversely proportional to the Z parameter. {yields} The dissolution of {delta} phases was greatly accelerated under hot deformation. {yields}The {delta} phase stimulated nucleation can serve as the main DRX mechanism. - Abstract: Flow stress behavior and microstructures during hot compression of delta-processed superalloy 718 at temperatures from 950 to 1100 deg. C with strain rates of 10{sup -3} to 1 s{sup -1} were investigated by optical microscopy (OM), electron backscatter diffraction (EBSD) technique and transmission electron microscopy (TEM). The relationship between the peak stress and the deformation conditions can be expressed by a hyperbolic-sine type equation. The activation energy for the delta-processed superalloy 718 is determined to be 467 kJ/mol. The change of the dominant deformation mechanisms leads to the decrease of stress exponent and the increase of activation energy with increasing temperature. The dynamically recrystallized grain size is inversely proportional to the Zener-Hollomon (Z) parameter. It is found that the dissolution rate of {delta} phases under hot deformation conditions is much faster than that under static conditions. Dislocation, vacancy and curvature play important roles in the dissolution of {delta} phases. The main nucleation mechanisms of dynamic recrystallization (DRX) for the delta-processed superalloy 718 include the bulging of original grain boundaries and the {delta} phase stimulated DRX nucleation, which is closely related to the dissolution behavior of {delta} phases under certain deformation conditions.

  8. High-strain-rate superplasticity in oxide ceramics: a trial of microstructural design based on creep-cavitation mechanisms

    Institute of Scientific and Technical Information of China (English)

    Keijiro HIRAGA; Byung-Nam KIM; Koji MORITA; Hidehiro YOSHIDA; Yoshio SAKKA; Masaaki TABUCHI

    2011-01-01

    From existing knowledge about high-temperature cavitation mechanisms, necessary conditions were discussed for the suppression of cavitation failure during superplastic deformation in ceramic materials. The discussion, where special attention was placed on the relaxation of stress concentrations during grain-boundary sliding and cavity nucleation and growth, leaded to a conclusion that cavitation failure could be retarded by the simultaneous controlling of the initial grain size, the number of residual defects,diffusivity, dynamic grain growth and the homogeneity of microstructure. On the basis of this conclusion, high-strain-rate superplasticity (defined as superplasticity at a strain rate higher than 0.01 s-1) could be intentionally attained in some oxide ceramic materials. This was shown in tetragonal zirconia and composites consisting of zirconia, α-alumina and a spinel phase.

  9. Hot deformation behavior of EA4T steel

    Institute of Scientific and Technical Information of China (English)

    Gang XU; Lina WANG; Shiqi LI; Le WANG

    2012-01-01

    The compressive deformation behavior of EA4T steel was investigated at temperatures ranging from 950 to 1150℃ and strain rates from 0.1 to 20 s-1 on Gleeble-1500 thermo-simulation machine.The work hardening rate versus stress curves were used to determine the characteristic points of flow curves.The application of constitutive equations to determine the hot working constants of this material was discussed.Furthermore,the effect of Zener-Hollomon parameter (Z) on the characteristic points of flow curves was studied using the power law relation.The deformation activation energy of this steel was determined as 309.5 kJ/mol.Some behaviors were compared to other steels.

  10. Role of Steel Object Surface Condition on Behavior During Deformation

    Science.gov (United States)

    D'yachenko, S. S.; Ponomarenko, I. V.; Dub, S. N.

    2015-09-01

    Comparative analysis is provided for specimen mechanical properties of steels 18KhGT and 20Kh with tensile testing in relation to surface treatment: grinding, polishing, nitriding, carburizing, and ion-plasma treatment. It is shown that surface condition has a considerable effect on specimen behavior during deformation. It is established that the most favorable effect applies to ion bombardment with low-energy ions recommended as an effective method for improving component structural strength.

  11. Superplasticity of a fine-grained Mg–9Gd–4Y–0.4Zr alloy evaluated using shear punch testing

    Directory of Open Access Journals (Sweden)

    Reza Alizadeh

    2014-07-01

    Full Text Available The superplasticity of an extruded fine-grained Mg–9Gd–4Y–0.4Zr alloy was investigated by measuring the strain rate sensitivity using shear punch testing (SPT. Shear punch tests were conducted at shear strain rates in the range of 3 × 10−3–2 × 10−1 s−1 and at temperatures in the range of 573–773 K. The results indicate the strain rate sensitivity, m, increases from about 0.11 at 573 K to about 0.40 at 723 K and then decreases to 0.32 with a further increase in test temperature. A strain rate sensitivity of 0.40 and an activation energy of 140 kJ/mol are indicative of a superplastic deformation behavior dominated by grain boundary sliding accommodated by lattice diffusion at temperatures above 673 K.

  12. Size-dependent deformation behavior of nanocrystalline graphene sheets

    Energy Technology Data Exchange (ETDEWEB)

    Yang, Zhi [State Key Laboratory for Mechanical Behavior of Materials, Xi’an Jiaotong University, Xi’an 710049, Shaanxi (China); Huang, Yuhong [College of Physics and Information Technology, Shaanxi Normal University, Xi’an 710062, Shaanxi (China); Ma, Fei, E-mail: mafei@mail.xjtu.edu.cn [State Key Laboratory for Mechanical Behavior of Materials, Xi’an Jiaotong University, Xi’an 710049, Shaanxi (China); Department of Physics and Materials Science, City University of Hong Kong, Tat Chee Avenue, Kowloon, Hong Kong (China); Sun, Yunjin [Faculty of Food Science and Engineering, Beijing University of Agriculture, Beijing Key Laboratory of Agricultural Product Detection and Control of Spoilage Organisms and Pesticide Residue, Beijing Laboratory of Food Quality and Safety, Beijing 102206 (China); Xu, Kewei, E-mail: kwxu@mail.xjtu.edu.cn [State Key Laboratory for Mechanical Behavior of Materials, Xi’an Jiaotong University, Xi’an 710049, Shaanxi (China); Department of Physics and Opt-electronic Engineering, Xi’an University of Arts and Science, Xi’an 710065, Shaanxi (China); Chu, Paul K., E-mail: paul.chu@cityu.edu.hk [Department of Physics and Materials Science, City University of Hong Kong, Tat Chee Avenue, Kowloon, Hong Kong (China)

    2015-08-15

    Highlights: • MD simulation is conducted to study the deformation of nanocrystalline graphene. • Unexpectedly, the elastic modulus decreases with the grain size considerably. • But the fracture stress and strain are nearly insensitive to the grain size. • A composite model with grain domains and GBs as two components is suggested. - Abstract: Molecular dynamics (MD) simulation is conducted to study the deformation behavior of nanocrystalline graphene sheets. It is found that the graphene sheets have almost constant fracture stress and strain, but decreased elastic modulus with grain size. The results are different from the size-dependent strength observed in nanocrystalline metals. Structurally, the grain boundaries (GBs) become a principal component in two-dimensional materials with nano-grains and the bond length in GBs tends to be homogeneously distributed. This is almost the same for all the samples. Hence, the fracture stress and strain are almost size independent. As a low-elastic-modulus component, the GBs increase with reducing grain size and the elastic modulus decreases accordingly. A composite model is proposed to elucidate the deformation behavior.

  13. Analysis on the deformation and fracture behavior of carbon steel by in situ tensile test

    Institute of Scientific and Technical Information of China (English)

    Fan Li; Haibo Huang

    2006-01-01

    The deformation and fracture behaviors of low-carbon steel, medium-carbon steel, and high-carbon steel were studied on internal microstructure using the scanning electron microscopy in situ tensile test. The microstructure mechanism of their deformation and fracture behavior was analyzed. The results show that the deformation and fracture behavior of low-carbon steel depends on the grain size of ferrite, the deformation and fracture behavior of medium-carbon steel depends on the size of ferrite grain and pearlite lump,and the deformation and fracture behavior of high-carbon steel depends on the size of pearlite lump and the pearlitic interlamellar spacing.

  14. Deformation behavior of dispersion-strengthened copper at high temperature

    Institute of Scientific and Technical Information of China (English)

    WANG Mengjun; ZHANG Yingchun; LUO Yun; LIU Xinyu

    2006-01-01

    The deformation behavior of dispersion-strengthened copper with different compositions was investigated by hot compression simulation tests on a Gleeble-1500 thermal-mechanical simulator. The microstructure during deformation at high temperature was also studied. The result shows that at the beginning of hot compression simulation, the flowing stress of the dispersion-strengthened copper quickly attains a peak value and the stress shows a greater decrease when the temperature is higher and the strain rate is lower. The dispersion particles lead to an obvious increase in the recrystallization temperature. Under experimental conditions, dynamic recovery is the main softening method. The constitutive equation at high temperature of 1.2%Al2O3-0.4%WC/Cu is obtained.

  15. High strain rate superplastic aluminium alloys: the way forward?

    Energy Technology Data Exchange (ETDEWEB)

    Grimes, R.; Dashwood, R.J.; Flower, H.M. [Imperial Coll. of Science, Technology and Medicine, London (United Kingdom). Dept. of Materials

    2001-07-01

    The technical and commercial barriers to the development and successful exploitation of a high strain rate superplastically deformable aluminium alloy for use in the automotive industry are considered in this paper. Batch processing routes, such as mechanical alloying or equal channel angular extrusion, employed to deliver appropriate chemistry and structure, are inherently costly and unlikely to deliver either the quantity or the size of strip required commercially. There is evidence that there is still scope for development of conventional casting and rolling routes, but a particulate casting route combined with roll consolidation offers the prospect of a commercially viable Al-Mg-Zr product. The use of alloying additions, including zirconium, is also discussed and comparative costs are presented: on this basis the use of scandium appears economically prohibitive. (orig.)

  16. Deformation Behavior across the Zircon-Scheelite Phase Transition

    Science.gov (United States)

    Yue, Binbin; Hong, Fang; Merkel, Sébastien; Tan, Dayong; Yan, Jinyuan; Chen, Bin; Mao, Ho-Kwang

    2016-09-01

    The pressure effects on plastic deformation and phase transformation mechanisms of materials are of great importance to both Earth science and technological applications. Zircon-type materials are abundant in both nature and the industrial field; however, there is still no in situ study of their deformation behavior. Here, by employing radial x-ray diffraction in a diamond anvil cell, we investigate the dislocation-induced texture evolution of zircon-type gadolinium vanadate (GdVO4 ) in situ under pressure and across its phase transitions to its high-pressure polymorphs. Zircon-type GdVO4 develops a (001) compression texture associated with dominant slip along ⟨100 ⟩{001 } starting from 5 GPa. This (001) texture transforms into a (110) texture during the zircon-scheelite phase transition. Our observation demonstrates a martensitic mechanism for the zircon-scheelite transformation. This work will help us understand the local deformation history in the upper mantle and transition zone and provides fundamental guidance on material design and processing for zircon-type materials.

  17. Deformation Behavior across the Zircon-Scheelite Phase Transition.

    Science.gov (United States)

    Yue, Binbin; Hong, Fang; Merkel, Sébastien; Tan, Dayong; Yan, Jinyuan; Chen, Bin; Mao, Ho-Kwang

    2016-09-23

    The pressure effects on plastic deformation and phase transformation mechanisms of materials are of great importance to both Earth science and technological applications. Zircon-type materials are abundant in both nature and the industrial field; however, there is still no in situ study of their deformation behavior. Here, by employing radial x-ray diffraction in a diamond anvil cell, we investigate the dislocation-induced texture evolution of zircon-type gadolinium vanadate (GdVO_{4}) in situ under pressure and across its phase transitions to its high-pressure polymorphs. Zircon-type GdVO_{4} develops a (001) compression texture associated with dominant slip along ⟨100⟩{001} starting from 5 GPa. This (001) texture transforms into a (110) texture during the zircon-scheelite phase transition. Our observation demonstrates a martensitic mechanism for the zircon-scheelite transformation. This work will help us understand the local deformation history in the upper mantle and transition zone and provides fundamental guidance on material design and processing for zircon-type materials.

  18. Static Recrystallization Behavior of Hot Deformed Austenite for Micro-Alloyed Steel

    Institute of Scientific and Technical Information of China (English)

    Jie HUANG; Zhou XU; Xin XING

    2003-01-01

    Static recrystallization behavior of austenite for micro-alloyed steel during hot rolling was studied and the influence (τ-ε diagram) of holding time and deformation at different deformations and isothermal temperatures on microstructuralstate of austen

  19. Fatigue Behavior and Deformation Mechanisms in Inconel 718 Superalloy Investigated

    Science.gov (United States)

    2005-01-01

    The nickel-base superalloy Inconel 718 (IN 718) is used as a structural material for a variety of components in the space shuttle main engine (SSME) and accounts for more than half of the total weight of this engine. IN 718 is the bill-of-material for the pressure vessels of nickel-hydrogen batteries for the space station. In the case of the space shuttle main engine, structural components are typically subjected to startup and shutdown load transients and occasional overloads in addition to high-frequency vibratory loads from routine operation. The nickel-hydrogen battery cells are prooftested before service and are subjected to fluctuating pressure loads during operation. In both of these applications, the structural material is subjected to a monotonic load initially, which is subsequently followed by fatigue. To assess the life of these structural components, it is necessary to determine the influence of a prior monotonic load on the subsequent fatigue life of the superalloy. An insight into the underlying deformation and damage mechanisms is also required to properly account for the interaction between the prior monotonic load and the subsequent fatigue loading. An experimental investigation was conducted to establish the effect of prior monotonic straining on the subsequent fatigue behavior of wrought, double-aged, IN 718 at room temperature. First, monotonic strain tests and fully-reversed, strain-controlled fatigue tests were conducted on uniform-gage-section IN 718 specimens. Next, fully reversed fatigue tests were conducted under strain control on specimens that were monotonically strained in tension. Results from this investigation indicated that prior monotonic straining reduced the fatigue resistance of the superalloy particularly at the lowest strain range. Some of the tested specimens were sectioned and examined by transmission electron microscopy to reveal typical microstructures as well as the active deformation and damage mechanisms under each of

  20. Numerical simulation of industrial superplastic forming. Final report

    Energy Technology Data Exchange (ETDEWEB)

    Haberman, K.S.; Bennett, J.G.; Piltch, M.S.

    1996-11-01

    Superplastic forming (SPF) is a metal forming process that allows a variety of components with very complex geometries to be produced at a fraction of the cost of conventional machining. The industrial superplastic forming process can be optimized with the application of the finite element method to predict the optimal pressure schedules, overall forming time, and the final thickness distribution. This paper discusses the verification and applications of NIKE3D in 4 optimizing the industrial superplastic forming process.

  1. Deformation behavior of reduced activation ferritic steel during tensile test

    Energy Technology Data Exchange (ETDEWEB)

    Shiba, Kiyoyuki [Department of Material Science and Engineering, Japan Atomic Energy Research Institute, Tokai-mura, Naka-gun, Ibakaki 319-1195 (Japan)]. E-mail: shiba@realab01.tokai.jaeri.go.jp; Hirose, Takanori [Department of Fusion Engineering Research, Japan Atomic Energy Research Institute, 801-1 Mukouyama, Naka, Ibaraki 311-0193 (Japan)

    2006-02-15

    Deformation behavior of reduced activation martensitic steel F82H during tensile tests were studied. True stress-true strain diagrams were calculated with minimum diameter determined from the specimen profile obtained by laser micro-gauge scanning the diameter along the longitudinal direction during tensile test. Cylindrical specimens of F82H were used for the measurement and test temperatures were room temperature (RT), 300, 400, 500 and 600 deg. C. Tensile tests were carried out with 1 x 10{sup -4} s{sup -1} of strain rate. Other strain rates (1 x 10{sup -3} and 1 x 10{sup -5} s{sup -1}) were applied for the tests at RT. Although uniform elongation of F82H is relatively small at elevated temperature, true stress increases to fracture after necking starts. True stress decreases temporarily after yielding at 600 deg. C, but it increases again to fracture like the specimens tested at lower temperatures. Influence of strain rate to true stress-true strain relationship at room temperature was small, but unstable deformation occurred in narrower area at higher strain rate.

  2. Super-plasticity of Zr64.80Cu14.85Ni10.35Al10 bulk metallic glass at room temperature

    Institute of Scientific and Technical Information of China (English)

    TAO PingJun; YANG YuanZheng; BAI XiaoJun; XIE ZhiWei; CHEN XianCao; DONG ZhenJiang; Wen JianGuo

    2008-01-01

    Generally, bulk metallic glasses (BMGs) exhibit a very limited plastic deformation under a compression load at room temperature, often less than 2% before fracturing. In this letter, through an appropriate choice of BMGs' composition, an amorphous rod of Zr64.80Cu14.85Ni10.35Al10 with a diameter of 2 mm was prepared by using copper mold suction casting. X-ray diffraction and differential scanning calorimetry were utilized to determine its structure and thermal stability, and the uniaxial compression test was adopted to study its plastic deformation behavior at room temperature simultaneously. The results showed that the glass transition temperature and onset temperature of the exothermic reaction of the amorphous rod were 646 and 750 K, respectively, and its micro-hardness was 594.7 Hv. During com-pression, when the engineering strain and engineering stress arrived at 9.05% and 1732 MPa, respec-tively, i.e., the true strain and true stress reached 9.42% and 1560 MPa, respectively, the amorphous rod started to yield. After yielding, with the increase of load, the strain increased and the glass rod ulti-mately were compressed into flake-like form. Although the maximum engineering strain was larger than 70%, i.e., the maximum true strain exceeded by 120%, the amorphous specimen was not fractured, indicating that it has super-plasticity at room temperature. Through the appropriate choice of compo-sition and optimization of the technological process, flexible BMG with super-plasticity at room tem-perature could be produced.

  3. Viscoelastoplastic constitutive model for creep deformation behavior of asphalt sand

    Institute of Scientific and Technical Information of China (English)

    叶永; 杨新华; 陈传尧

    2008-01-01

    A uniaxial viscoelastoplastic model that can describe whole creep behaviors of asphalt sand at different temperatures was presented.The model was composed of three submodels in series,which describe elastoplastic,viscoelastic and viscoplastic characteristics respectively.The constitutive equation was established for uniaxial loading condition,and the creep representation was also obtained.The constitutive parameters were determined by uniaxial compression tests under controlled-stress of 0.1 MPa with five different test temperatures of 20,40,45,50 and 60 ℃.Expressions of the model parameters in terms of temperatures were also given.The model gave prediction at various temperatures consistent with the experimental results,and can reflect the total deformation characterization of asphalt sands.

  4. Type-IV Pilus Deformation Can Explain Retraction Behavior

    CERN Document Server

    Ghosh, Ranajay; Vaziri, Ashkan

    2014-01-01

    Polymeric filament like type IV Pilus (TFP) can transfer forces in excess of 100pN during their retraction before stalling, powering surface translocation(twitching). Single TFP level experiments have shown remarkable nonlinearity in the retraction behavior influenced by the external load as well as levels of PilT molecular motor protein. This includes reversal of motion near stall forces when the concentration of the PilT protein is lowered significantly. In order to explain this behavior, we analyze the coupling of TFP elasticity and interfacial behavior with PilT kinetics. We model retraction as reaction controlled and elongation as transport controlled process. The reaction rates vary with TFP deformation which is modeled as a compound elastic body consisting of multiple helical strands under axial load. Elongation is controlled by monomer transport which suffer entrapment due to excess PilT in the cell periplasm. Our analysis shows excellent agreement with a host of experimental observations and we prese...

  5. Deformation Behavior of Ultra-low Carbon Steel in Ferrite Region during Warm Processing

    Institute of Scientific and Technical Information of China (English)

    XU Guang; CHEN Zhenye; LIU Li; YU Shengfu

    2008-01-01

    The hot deformation experiments of ultra-low carbon steel in ferrite range were carried out ina hot simulator in order to research hot deformation behaviors of ultra-low carbon steel in ferrite range at low temperature.The results show that the influences of deformation parameters on flow stress are different to those in austenitic deformation.The deformation characteristic parameters were calculated for ultra-low carbon steel in ferrite region.The flow stress equation for ultra-low carbon steel in ferritic deformation at low temperature was obtained.

  6. Development of fine-grain size titanium 6Al–4V alloy sheet material for low temperature superplastic forming

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Tuoyang [State Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan (China); Liu, Yong, E-mail: yonliu@csu.edu.cn [State Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan (China); Sanders, Daniel G. [Boeing Research and Technology, Seattle, WA (United States); Liu, Bin; Zhang, Weidong; Zhou, Canxu [State Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan (China)

    2014-07-01

    Fine-grained titanium 6Al–4V alloy, which typically has a grain size of about 1–2 μm, can be made to superplastic form at around 800 °C with special processing. The normal temperature for superplastic forming (SPF) with conventional titanium 6Al–4V sheet material is 900 °C. The lower temperature performance is of interest to the Boeing Company because it can be exploited to achieve significant cost savings in processing by reducing the high-temperature oxidation of the SPF dies, improving the heater rod life for the hot presses, increasing operator safety and replacing the chemical milling operation to remove alpha case contamination with a less intensive nitric hydrofluoric acid etchant (pickle). In this report, room temperature tensile tests and elevated temperature constant strain rate tensile tests of fine-grained Ti–6Al–4V sheets provided by the Baoti Company of Xi'an, China, were conducted according to the test method standards of ASTM-E8 and ASTM-E2448. The relationships among the processing parameters, microstructure and superplastic behavior have been analyzed. The results show that two of the samples produced met the Boeing minimum requirements for low-temperature superplasticity. The successful material was heat-treated at 800 °C subsequent to hot rolling above the beta transus temperature, T{sub β}-(150–250 °C). It was found that the sheet metal microstructure has a significant influence on superplastic formability of the Ti–6Al–4V alloy. Specifically, fine grains, a narrow grain size distribution, low grain aspect ratio and moderate β phase volume fraction can contribute to higher superplastic elongations.

  7. Ultrahigh carbon steels, Damascus steels, and superplasticity

    Energy Technology Data Exchange (ETDEWEB)

    Sherby, O.D. [Stanford Univ., CA (United States). Dept. of Materials Science and Engineering; Wadsworth, J. [Lawrence Livermore National Lab., CA (United States)

    1997-04-01

    The processing properties of ultrahigh carbon steels (UHCSs) have been studied at Stanford University over the past twenty years. These studies have shown that such steels (1 to 2.1% C) can be made superplastic at elevated temperature and can have remarkable mechanical properties at room temperature. It was the investigation of these UHCSs that eventually brought us to study the myths, magic, and metallurgy of ancient Damascus steels, which in fact, were also ultrahigh carbon steels. These steels were made in India as castings, known as wootz, possibly as far back as the time of Alexander the Great. The best swords are believed to have been forged in Persia from Indian wootz. This paper centers on recent work on superplastic UHCSs and on their relation to Damascus steels. 32 refs., 6 figs.

  8. Ultrafine-grained magnesium–lithium alloy processed by high-pressure torsion: Low-temperature superplasticity and potential for hydroforming

    Energy Technology Data Exchange (ETDEWEB)

    Matsunoshita, Hirotaka [Department of Materials Science and Engineering, Faculty of Engineering, Kyushu University, Fukuoka 819-0395 (Japan); Edalati, Kaveh, E-mail: kaveh.edalati@zaiko6.zaiko.kyushu-u.ac.jp [Department of Materials Science and Engineering, Faculty of Engineering, Kyushu University, Fukuoka 819-0395 (Japan); WPI, International Institute for Carbon-Neutral Energy Research (WPI-I2CNER), Kyushu University, Fukuoka 819-0395 (Japan); Furui, Mitsuaki [Graduate School of Science and Engineering for Research, University of Toyama, Toyama 930-8555 (Japan); Horita, Zenji [Department of Materials Science and Engineering, Faculty of Engineering, Kyushu University, Fukuoka 819-0395 (Japan); WPI, International Institute for Carbon-Neutral Energy Research (WPI-I2CNER), Kyushu University, Fukuoka 819-0395 (Japan)

    2015-07-29

    A Mg–Li alloy with 8 wt% Li was processed by severe plastic deformation (SPD) through the process of high-pressure torsion (HPT) to achieve ultrafine grains with an average grain size of ~500 nm. Tensile testing with an initial strain rate of 10{sup −3} s{sup −1} showed that the alloy exhibited superplasticity at a temperature of 323 K or higher. Tensile testing in boiling water confirmed that the specimens were elongated to 350–480% at 373 K under the initial strain rates of 10{sup −3} s{sup −1} to {sup 1}0{sup −2} s{sup −1} with a strain rate sensitivity of ~0.3. The current study suggests that not only superplastic forming but also superplastic hydroforming should be feasible after the grain refinement using the HPT method.

  9. Relation of deformation behavior with precipitation and groundwater of the Babaoshan fault in Beijing

    Institute of Scientific and Technical Information of China (English)

    HUANG Fu-qiong; CHEN Yong; BAI Chang-qing; ZHANG Jing; YAN Rui; YANG Ming-bo; LAN Cong-xin; ZHANG Xiao-dong; JIANG Zai-sen

    2005-01-01

    We discuss the influence of precipitation and groundwater on the deformation behavior of the Babaoshan fault of Beijing by using long-term observation data from Dahuichang station during 1970~2003. The results show that a)the pore pressure on fault zone as well as the fault deformation behavior exhibited periodically variation as precipitation changed steadily and periodically; b) the periodicity of the pore pressure of fault zones disappeared and the manner of fault deformation behavior changed when precipitation was small and/or was in aberrance. This implies that rainfall plays a key role in fault deformation behavior through changing the pore pressure of fault zones. Combining the existing results about the Babaoshan fault, it is concluded that precipitation and groundwater may adjust the stress/strain field by controlling the deformation behavior of the fault, which can provide direct observation evidence for the interaction of fluid and solid in shallow crust of the Earth.

  10. Hot Workability and Superplasticity of Low-Al and High-Nb Containing TiAl Alloys

    Science.gov (United States)

    Tang, Bin; Zhao, Fengtong; Chu, Yudong; Kou, Hongchao; Li, Jinshan

    2017-09-01

    The superplastic deformation mechanism of low-Al and high-Nb containing TiAl alloy was investigated in compression mode. The experimental results showed that intense dynamic recrystallization (DRX) breaks the balance and leads to a significant drop in flow stress after the peak when deforming below 950°C. Arrhenius kinetic analysis revealed that the activation energy for superplastic compression first increased then decreased with temperature, suggesting a change in the deformation mechanism. Microstructure observations showed that, when deformed at 850°C, the deformation mechanism was grain-boundary sliding accommodated by γ-DRX, γ-intragranular deformation, and β/B2-phase decomposition, while the mechanism was grain-boundary sliding accommodated by γ-DRX, β/B2-DRX, and γ → β/B2 + α 2 phase transformation when deformed at 1000°C. After compression, the microstructure tended to be uniform, which may yield important information for the development of new deformation techniques for TiAl alloys.

  11. Thermal deformation behavior and microstructure of nuclear austenitic stainless steel

    Institute of Scientific and Technical Information of China (English)

    2009-01-01

    Gleeble-1500D thermal simulation tester was employed in the hot-compression investigation of as-cast nuclear 304 austenitic stainless steel under conditions: deformation temperature 950―1200℃; deformations 30% and 50%; deformation rates 0.01 and 0.1 s?1. The results show that the flow stress decreases with temperature rise under the same strain rate and deformation, that the flow stress increases with deformation under the same temperature and strain rate, and that the flow stress increases with strain rate under the same temperature condition, i.e., work hardening becomes distinct. Materials exhibit better strength-toughness when the strain rate is 0.01 s-1, the deformation is 50%, and the temperature is 1050℃.

  12. Effects of hydrogenation on ambient deformation behaviors of Ti-45Al alloy

    Institute of Scientific and Technical Information of China (English)

    SU Yan-qing; LIU Xin-wang; ZHAO Long; WANG Liang; GUO Jing-jie; FU Heng-zhi

    2009-01-01

    Effects of hydrogenation on ambient deformation behaviors of Ti-45Al alloy were studied. The stress-strain curves demonstrate that the plastic deformation of the hydrogenated alloys becomes more remarkable than that of the unhydrogenated alloy.Meanwhile, the compression strength and maximum strain are reduced. Both the hydride and hydrogen atoms in the interstices affect the compression deformation behaviors. The reason of the hydrogen-induced embrittlement is that the hydride is easy to become the nucleus of the cracks. And the variation of plastic deformation process is attributed to hydrogen-promoted emission, multiplication and motion of dislocation.

  13. Deformation behavior of Fe-based bulk metallic glass during nanoindentation

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    Fe-based bulk metallic glasses (BMGs) normally exhibit super high strength but significant brittleness at ambient temperature. Therefore,it is difficult to investigate the plastic deformation behavior and mechanism in these alloys through conven-tional tensile and compressive tests due to lack of distinct macroscopic plastic strain. In this work,the deformation behavior of Fe52Cr15Mo9Er3C15B6 BMG was in-vestigated through instrumented nanoindentation and uniaxial compressive tests. The results show that serrated flow,the typical plastic deformation feature of BMGs,could not be found in as-cast and partially crystallized samples during nanoinden-tation. In addition,the deformation behavior and mechanical properties of the alloy are insensitive to the applied loading rate. The mechanism for the appearance of the peculiar deformation behavior in the Fe-based BMG is discussed in terms of the temporal and spatial characteristics of shear banding during nanoindentation.

  14. Deformation behavior of Fe-based bulk metallic glass during nanoindentation

    Institute of Scientific and Technical Information of China (English)

    LI Lei; LIU Yuan; ZHANG TaiHua; GU JianSheng; WEI BingChen

    2008-01-01

    Fe-based bulk metallic glasses (BMGs) normally exhibit super high strength but significant brittleness at ambient temperature. Therefore, it is difficult to investigate the plastic deformation behavior and mechanism in these alloys through conven-tional tensile and compressive tests due to lack of distinct macroscopic plastic strain. In this work, the deformation behavior of Fe52Cr15Mo9Er3C15B6 BMG was in-vestigated through instrumented nanoindentation and uniaxial compressive tests. The results show that serrated flow, the typical plastic deformation feature of BMGs, could not be found in as-cast and partially crystallized samples during nanoinden-tation. In addition, the deformation behavior and mechanical properties of the alloy are insensitive to the applied loading rate. The mechanism for the appearance of the peculiar deformation behavior in the Fe-based BMG is discussed in terms of the temporal and spatial characteristics of shear banding during nanoindentation.

  15. Experimental Investigation on Creep Deformation Behavior of Medium-strength Marble Rock

    OpenAIRE

    Li Yong; Zhu Weishen; Li Shucai

    2014-01-01

    The creep deformation behavior of rocks has significant effect on the stability of underground structures. This study presents the short-term and creep deformation behavior of medium-strength marble rock using a conventional uniaxial compression testing machine and a servo-controlled rheology testing machine. The uniaxial compressive strength is obtained by the uniaxial compression testing machine. During the creep behavior test, two types of rock specimens (dry and water-saturated) are speci...

  16. Constitution modeling and deformation behavior of yttrium bearing TiAl alloy

    Institute of Scientific and Technical Information of China (English)

    CHEN Yuyong; YANG Fei; KONG Fantao; XIAO Shulong

    2011-01-01

    The deformation flow behaviors of Ti-45Al-5.4V-3.6Nb-0.3Y alloy at different temperatures and strain rates were studied by isothermal compressing simulation test. The apparent activation energy of deformation was calculated to be 402.096 kJ/mol and constitutive equation was established to describe the flow behavior. Microstructure and flow softening observations exhibited that Ti-45Al-5.4V-3.6Nb-0.3Y alloy had bad hot workability at low temperature (lower than 1 100 ℃) and high strain rate (higher than 0.5 s-1) characterized by localization deformation and instability. With deformation temperature higher than 1 150 ℃ and strain rate lower than 0.01 s-1, the alloy owned good hot deformability, and plenty of dynamic recrystallized grains could be observed in the deformed microstructures.

  17. Deformation behavior during nanoindentation in Ce-based bulk metallic glasses

    Institute of Scientific and Technical Information of China (English)

    ZHANG Lingchen; XING Dongmei; ZHANG Taihua; WEI Bingchen; LI Weihuo; WANG Yuren

    2006-01-01

    The deformation behavior and the effect of the loading rate on the plastic deformation in Ce-based bulk metallic glasses (BMGs) were investigated through nanoindentation tests. The results showed that the loading rate dependence of plastic deformation during nanoindentation measurements in the Ce-based BMGs is quite unique in contrast to that of other BMG alloys. The load-displacement (P-h)curves of Ce60Al15Cu10Ni15 BMG exhibit a homogeneous plastic deformation at low loading rates, and a prominent serrated flow at high strain rates, whereas,the P-h curves of Ce65Al10Cu10Ni10Nb5 exhibit homogenous plastic deformation at all studied loading rates. The room temperature creep behavior could clearly be observed in these two alloys. The mechanism of the unique plastic deformation feature in the Ce-based BMGs was studied.

  18. Hot compression deformation behavior of the Mg-AI-Y-Zn magnesium alloy

    Institute of Scientific and Technical Information of China (English)

    FANG Xiya; YI Danqing; WANG Bin; WU Chunping; ZHANG Hong

    2008-01-01

    The hot deformation behavior of a Mg-Al-Y-Zn magnesium alloy was investigated by hot compressive testing on a Gleeble-1500 thermal simulator at the temperanging from 523 to 673 K with the swain rate varying from 0.001 to 1s-1.The relationships among flow stress,swain rate,and deformation temperature were analyzed,and the deformation activation energy and stress exponent were calculated.Microstructure evolution of the alloy under different conditions was examined.The results indicated that the maximum value of the flow stress increased with the decrease of deformation temperature or the increase of swain rate.Under the present deformation conditions,dynamic recrystallization (DRX) oeettrred in the alloy,which was the main softening mechanism during deformation at elevated temperature.The deformation temperature and strain had significant effects on the microstructure of the alloy.

  19. Deformation behavior of laser bending of circular sheet metal

    Institute of Scientific and Technical Information of China (English)

    Q. Nadeem; S. J. Na

    2011-01-01

    @@ The application of a thermal source in non-contact forming of sheet metal has long been used.However, the replacement of this thermal source with a laser beam promises much greater controllability of the process.This yields a process with strong potential for application in aerospace, shipbuilding, automobile, and manufacturing industries, as well as the rapid manufacturing of prototypes and adjustment of misaligned components.%The application of a thermal source in non-contact forming of sheet metal has long been used. However, the replacement of this thermal source with a laser beam promises much greater controllability of the process. This yields a process with strong potential for application in aerospace, shipbuilding, automobile, and manufacturing industries, as well as the rapid manufacturing of prototypes and adjustment of misaligned components. Forming is made possible through laser-induced non-uniform thermal stresses. In this letter, we use the geometrical transition from rectangular to circle-shaped specimen and ring-shaped specimen to observe the effect of geometry on deformation in laser forming. We conduct a series of experiments on a wide range of specimen geometries. The reasons for this behavior are also analyzed. Experimental results are compared with simulated values using the software ABAQUS. The utilization of line energy is found to be higher in the case of laser forming along linear irradiation than along curved ones. We also analyze the effect of strain hindrance. The findings of the study may be useful for the inverse problem, which involves acquiring the process parameters for a known target shape of a wide range of complex shape geometries.

  20. Research on the diffusion bonding of superplastic magnesium alloy

    Institute of Scientific and Technical Information of China (English)

    于彦东; 张凯锋; 蒋大鸣; 郑海荣; 王刚

    2002-01-01

    The elevated temperature tensile experiments have been carried out on the magnesium alloy and results indicate that the magnesium alloy has excellent superplastic property. Gleebe-1500 testing machine was used in the diffusion bonding experiment on the superplastic magnesium alloy. Then, the shear strength of the joints under different conditions is obtained through shear testing and the optimum processing parameters for the diffusion bonding are achieved. By metallurgical microscope and scanning electron microscope (SEM), it is revealed that the micromechanism of diffusion bonding is the slide of grain boundaries caused by the growth of grains and atom diffusion of the superplastic magnesium alloy.

  1. Free Bulging at Constant Pressure of Superplastic Sheet Metal

    Directory of Open Access Journals (Sweden)

    Costanzo Bellini

    2015-08-01

    Full Text Available This work intends to establish, by means of analytical modelling, a practical definition of the superplastic behaviour by using the results of the free bulging of sheet metal instead of the results of the traditional tensile test. In particular this paper analyses the superplastic flow of PbSn60 alloy and it focuses the attention on the value of H parameter corresponding to the maximum value of dt/dH, never considered in the literature. This parameter can represent a practical tool in industrial applications to establish the superplastic behaviour of a sheet metal.

  2. Superplastic Forming of Aluminum (Task C)

    Science.gov (United States)

    1989-03-01

    purchase order number 9-342779-01 was modified to incorporate integral hinge attachment features to drawing number 160K136160. The material used to form a...0.805 7. Trans. Drill 8 his. from 136153-3 & 136152-1 Hinges C/T Straps and 136161-11 & -13 Fittings .016 0.053 8. Disassemble 0.182 9. DBR 0.008 0.158 10...door utilizes a conventional aluminum alloy skin stiffened by a weld bonded monolithic superplastically formed element fabricated trom Supral 220

  3. Influence of thermally activated processes on the deformation behavior during low temperature ECAP

    Science.gov (United States)

    Fritsch, S.; Scholze, M.; F-X Wagner, M.

    2016-03-01

    High strength aluminum alloys are generally hard to deform. Therefore, the application of conventional severe plastic deformation methods to generate ultrafine-grained microstructures and to further increase strength is considerably limited. In this study, we consider low temperature deformation in a custom-built, cooled equal channel angular pressing (ECAP) tool (internal angle 90°) as an alternative approach to severely plastically deform a 7075 aluminum alloy. To document the maximum improvement of mechanical properties, these alloys are initially deformed from a solid solution heat-treated condition. We characterize the mechanical behavior and the microstructure of the coarse grained initial material at different low temperatures, and we analyze how a tendency for the PLC effect and the strain-hardening rate affect the formability during subsequent severe plastic deformation at low temperatures. We then discuss how the deformation temperature and velocity influence the occurrence of PLC effects and the homogeneity of the deformed ECAP billets. Besides the mechanical properties and these microstructural changes, we discuss technologically relevant processing parameters (such as pressing forces) and practical limitations, as well as changes in fracture behavior of the low temperature deformed materials as a function of deformation temperature.

  4. Characterizing volumetric deformation behavior of naturally occuring bituminous sand materials

    CSIR Research Space (South Africa)

    Anochie-Boateng, Joseph

    2009-05-01

    Full Text Available newly proposed hydrostatic compression test procedure. The test procedure applies field loading conditions of off-road construction and mining equipment to closely simulate the volumetric deformation and stiffness behaviour of oil sand materials. Based...

  5. Permanent deformation behavior of naturally occurring bituminous sands

    CSIR Research Space (South Africa)

    Anochie-Boateng, Joseph

    2008-01-01

    Full Text Available were compacted close to field densities and then tested for permanent deformation at two temperatures using a newly proposed test procedure. The procedure applied stress states and ratios determined from field-loading characteristics of haul trucks...

  6. Effects of friction stir processing on the microstructure and superplasticity of in situ nano-ZrB2/2024Al composite

    Institute of Scientific and Technical Information of China (English)

    Yutao Zhao; Xizhou Kai; Gang Chen; Weili Lin; Chunmei Wang

    2016-01-01

    In this study, in situ nano-ZrB2/2024Al composites fabricated from 2024Al–K2ZrF6–KBF4 system were processed by friction stir processing (FSP) to achieve superplasticity of the composites. And the effects of particle contents (1 wt%, 3 wt%, 5 wt%), matrix grain size (micron or sub-micron), strain rates (5 × 10¯3 s¯1, 1 × 10¯2 s¯1, 2 × 10¯2 s¯1) and deformation temperatures (400 K, 480 K, 600 K, 700 K, 750 K) on the superplasticity of the composites were investigated. After the friction stir processing, the coarse grains of the cast composites with matrix grain size of about 80–100 μm and nano-ZrB2 reinforcement size of 30–100 nm were crushed into small grains about 1 μm in size, and the uniformity of the nano-ZrB2 reinforcements was also improved. And under the same superplastic tensile testing condition at the temperature of 750 K and strain rate of 5 × 10¯3 s¯1, the FSP nano 3 wt%ZrB2/2024Al composite exhibited an superplastic elongation of 292.5%, while the elongation of the corresponding cast composite was only less than 100%. Meanwhile, the m values of the FSP composites were always higher than the cast composites, especially the FSP composites with 3 wt% particles has the m value of 0.5321 i.e., the FSP composites should had better superplastic properties than cast ones. Furthermore, the FSP composites had higher apparent deformation activation energy (Q) than that of the lattice diffusion of pure aluminium, indicating that the deformation mechanisms of the FSP composites should be grain boundary sliding mechanisms.

  7. STUDY ON THE HOT DEFORMATION BEHAVIORS OF Al-Zn-Mg-Cu-Cr ALUMINUM ALLOY

    Institute of Scientific and Technical Information of China (English)

    G.Y. Lin; Z.F. Zhang; H. Zhang; D.S. Peng; J. Zhou

    2008-01-01

    The hot deformation behaviors and mierostructures of Al-Zn-Mg-Cu-Cr aluminum alloy have been studied using thermal simulation test, optical microscopy and transmission electron microscopy. As a result, the true stress versus true strain curves and the microstructures under various deformation conditions are obtained. The microstructures gradually incline to dynamic-recrystallization with the deformation temperature rising and the recrystallization grains refine with the decrease of deformation temperature or with raising the strain rates. The quantitative relationship between the Zener-HoUomon parameter (Z) and average recrystallization grain size in the subsequent heat treatment is set up.

  8. Dental implant superstructures by superplastic forming

    Energy Technology Data Exchange (ETDEWEB)

    Curtis, R.V.; Garriga-Majo, D.; Soo, S.; Pagliaria, D. [Kings Coll., London (United Kingdom). Dept. of Dental Biomaterials Science; Juszczyk, A.S.; Walter, J.D. [Kings Coll., London (United Kingdom). Dept. of Prosthetic Dentistry

    2001-07-01

    A novel application of superplastic forming is described for the production of fixed-bridge dental implant superstructures. Finite element analysis (FEA) has shown that Ti-6Al-4V sheet would be a suitable candidate material for the design of a fixed-bridge dental implant superstructure. Traditionally superstructures are cast in gold alloy onto pre-machined gold alloy cylinders but castings are often quite bulky and 25% of castings do not fit accurately (1) which means that sectioning and soldering is required to obtain a fit that is clinically acceptable and will not prejudice the integrity of the commercially pure cp-titanium implants osseointegrated with the bone. Superplastic forming is shown to be a forming technique that would allow the production of strong, light-weight components of thin section with low residual stress that could be suitable for such applications. Considerable cost savings over traditional dental techniques can be achieved using a low-cost ceramic die material. The properties of these die materials are optimised so that suitable components can be produced. Satisfactory hot strength is demonstrated and thermal properties are matched to those of the titanium alloy for accurate fit of the prosthesis. (orig.)

  9. Elastic stability of superplastically formed/diffusion-bonded orthogonally corrugated core sandwich plates

    Science.gov (United States)

    Ko, W. L.

    1980-01-01

    The paper concerns the elastic buckling behavior of a newly developed superplastically formed/diffusion-bonded (SPF/DB) orthogonally corrugated core sandwich plate. Uniaxial buckling loads were calculated for this type of sandwich plate with simply supported edges by using orthotropic sandwich plate theory. The buckling behavior of this sandwich plate was then compared with that of an SPF/DB unidirectionally corrugated core sandwich plate under conditions of equal structural density. It was found that the buckling load for the former was considerably higher than that of the latter.

  10. New method for making super-plastic glasses

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    @@ It was a long-cherished dream for materials scientists to find a nearly ideal metallic alloy with high strength and super-plasticity concurrently as a super-material both extremely strong and exceptionally hard for human use.

  11. Hot deformation behavior of rare earth magnesium alloy without pre-homogenization treatment

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    The behavior and structure evolvement of as-cast Mg-Gd-Y-Nd-Zr magnesium alloy during the hot deformation process were discussed. The flow stress behavior of magnesium alloy over the strain rate range of 0.002-1 s-1 and the temperature range of 573-723 K was researched on Gleeble-1500D hot simulator under the maximum deformation degree of 60%. The experimental results show that the relationship between stress and strain is obviously affected by the strain rate and deformation temperature. The important softening mechanisms are eutectic melting and discontinuous dynamic recrystallization (DDRX) during deformation. The fragments of eutectie melting along the boundaries can turn round so as to take effect of the slippage between grains. The flow stress of Mg-7Gd-5Y-1.2Nd-Zr magnesium alloy during high temperature deformation can be represented by a Zener-Hollomon parameter in the hyperbolic Arrhenius-type equation. The strain coefficient n and deformation activation energy Q are evaluated by linear regression analysis. A, α and n in the analytical expressions of σ are fitted to be 2.401 93× 1015, 0.017 3 MPa-1 and 3.218 19,respectively. The hot deformation activation energy of alloy during hot deformation is 234.950 58 kJ/mol. The results also show that the structure of primitive microstructure has an effect on the plastic deformation.

  12. Influence of Mn Content and Hot Deformation on Transformation Behavior of C-Mn Steels

    Institute of Scientific and Technical Information of China (English)

    LI Long; DING Hua; DU Lin-xiu; WEN Jing-lin; SONG Hong-mei; ZHANG Pi-jun

    2008-01-01

    The hot deformation behaviors and the microstructural evolution of plain C-Mn steels with similar contents of C and Si but different contents of Mn have been investigated by compressive processing using Gleeble-1500 mechanical simulator. Influence of Mn and hot deformation on continuous cooling transformation of steels has been studied. The experimental results showed that deformation in austenite region accelerated transformation process, and the extent is dependent on the hot deformation and cooling conditions. The hot deformation would promote transformation process, but the increase of transformation temperature is dependent on Mn contents. The results have also shown that the effect of deformation on ferrite transformation becomes more obvious with the increase of Mn content at relatively low cooling rate.

  13. Work-hardening behavior of mild steel under cyclic deformation at finite strains

    Energy Technology Data Exchange (ETDEWEB)

    Hu, Z. (Univ. Paris-Nord, Villetaneuse (France))

    1994-10-01

    The work-hardening behavior of mild steel under monotonic deformation at large shears and cyclic deformation under a wide range of shear amplitudes (from 3 to 34%) has been experimentally investigated and modeled. The influence of shear amplitude, the effect of the amount of pre-shear and that of pre-cyclic deformation have been studied. Considering the evolution of both polarized persistent dislocation structures and no-polarized low-energy dislocation configurations, a physically-based phenomenological model with four internal variables has been proposed. The model explains the cyclic hardening behavior at large strains, the work-hardening stagnation followed by a resumption of work-hardening under Bauschinger deformation with large pre-strains and under cyclic deformation with moderate strain amplitudes. A good qualitative and quantitative agreement has been achieved between experimental results and model predictions.

  14. Superplastic forming and diffusion bonding: Progress and trends

    Directory of Open Access Journals (Sweden)

    Zhiqiang Li

    2015-01-01

    Full Text Available This paper summarized recent progress in metal superplasticity and the application of Superplastic Forming/Diffusion Bonding (SPF/DB or SPF/Welding in typical structures. Various aerospace components such as three dimensional lattice structures made by SPF/DB have been demonstrated. In addition, some newly developed technologies, such as melt droplet spreading/thermo-mechanical forming (MDS/TMF, were also included. Finally, the future potential of SPF/DB technology was predicted.

  15. Viscoelastic materials with anisotropic rigid particles: stress-deformation behavior

    NARCIS (Netherlands)

    Sagis, L.M.C.; Linden, van der E.

    2001-01-01

    In this paper we have derived constitutive equations for the stress tensor of a viscoelastic material with anisotropic rigid particles. We have assumed that the material has fading memory. The expressions are valid for slow and small deformations from equilibrium, and for systems that are nearly

  16. Effect of deformation temperature on the hot compressive behavior of metal matrix composites with misaligned whiskers

    Institute of Scientific and Technical Information of China (English)

    LI Aibin; MENG Qingyuan; GENG Lin; DENG Chunfeng; YAN Yiwu

    2007-01-01

    A multi-inclusion cell model is used to investigate the effect of deformation temperature and whisker rotation on the hot compressive behavior of metal matrix composites with misaligned whiskers. Numerical results show that deformation temperature influences the work-hardening behavior of the matrix and the rotation behavior of the whiskers. With increasing temperature, the work hardening rate of the matrix decreases, but the whisker rotation angle increases. Both whisker rotation and the increase of deformation temperature can induce reductions in the load supported by whisker and the load transferred from matrix to whisker. Additionally, it is found that during large strain deformation at higher temperatures, the enhancing of deformation temperature can reduce the effect of whisker rotation. Meanwhile, the stress-strain behavior of the composite is rather sensitive to deformation temperature. At a relatively lower temperature (150℃), the composite exhibits work hardening due to the matrix work hardening, but at relatively higher temperatures (300℃ and above),the composite shows strain softening due to whisker rotation. It is also found that during hot compression at higher temperatures, the softening rate of the composite decreases with increasing temperature. The predicted stress-strain behavior of the composite is approximately in agreement with the experimental results.

  17. Superplasticity of low carbon HSLA steel during bainite transformation. Teitanso teigokinko no beinaito hentai ni okeru chososei kyodo

    Energy Technology Data Exchange (ETDEWEB)

    Nakajima, H.; Yamamoto, S.; Miyaji, H.; Furubayashi, E. (National Research Inst. for Metals, Tsukuba, Ibaraki (Japan))

    1993-12-01

    Recently, the development of high strength low alloy steel (HSLA steel) of untempered type is advanced by using the comparatively high strength and excellent tenacity of the bainite or martensite of carbon remained being transformed. In the present researches, the superplasticity during the bainite transformation due to the continuous cooling and changes of the structure as well as the mechanical properties due to the superplastic deformation are examined with the samples of Mn-Cr-Mo system HSLA steel. The results obtained therefrom are shown as follows. The temperatre range of B[sub S] and bainite transformation is moving to the higher temperature side along with the increasing of the applied stress when it is over 60 MPa. The bainitic structure is composed of the mixture lath-like bainitic ferrite and granular bainitic ferrite in the use of having no applied stress, while the percentage of the latter increases simultaneously with the increasing of the applied stress. Transformation superplastic strain is increasing together with the increasing of the applied stress, and its increasing is over the linear function when the applied stress is above about 50 MPa. 22 refs., 9 figs., 2 tabs.

  18. Mechanisms of Superplastic Deformation of Nanocrystalline Silicon Carbide Ceramics

    Science.gov (United States)

    2012-08-01

    CAMPBELL MZ436 30 44 D DEBUSSCHER MZ436 20 29 J ERIDON MZ436 21 24 W HERMAN MZ435 01 24 S PENTESCU MZ436 21 24 38500 MOUND RD... HESS & EISENHARDT G ALLEN D MALONE T RUSSELL 9113 LE SAINT DR FAIRFIELD OH 45014 NO. OF NO. OF COPIES ORGANIZATION COPIES

  19. Superplastic behaviour of AZ91 magnesium alloy processed by high-pressure torsion

    Energy Technology Data Exchange (ETDEWEB)

    Al-Zubaydi, Ahmed S.J., E-mail: asaz1e11@soton.ac.uk [Materials Research Group, Faculty of Engineering and the Environment, University of Southampton, Southampton SO17 1BJ (United Kingdom); Branch of Materials Science, Department of Applied Sciences, University of Technology, Baghdad (Iraq); Zhilyaev, Alexander P. [Institute for Problems of Metals Superplasticity, Russian Academy of Sciences, Khalturina 39, Ufa 450001 (Russian Federation); Wang, Shun C.; Reed, Philippa A.S. [Materials Research Group, Faculty of Engineering and the Environment, University of Southampton, Southampton SO17 1BJ (United Kingdom)

    2015-06-18

    An investigation has been conducted on the tensile properties of a fine-grained AZ91 magnesium alloy processed at room temperature by high pressure torsion (HPT). Tensile testing was carried out at 423 K, 473 K and 573 K using strain rates from 1×10{sup −1} s{sup −1} to 1×10{sup −4} s{sup −1} for samples processed in HPT for N=1, 3, 5 and 10 turns. After testing was completed, the microstructures were investigated by scanning electron microscopy and energy dispersive spectroscopy. The alloy processed at room temperature in HPT exhibited excellent superplastic behaviour with elongations higher than elongations reported previously for fine-grained AZ91 alloy produced by other severe plastic deformation processes, e.g. HPT, ECAP and EX-ECAP. A maximum elongation of 1308% was achieved at a testing temperature of 573 K using a strain rate of 1×10{sup −4} s{sup −1}, which is the highest value of elongation reported to date in this alloy. Excellent high-strain rate superplasticity (HSRSP) was achieved with maximum elongations of 590% and 860% at temperatures of 473 K and 573 K, respectively, using a strain rate of 1×10{sup −2} s{sup −1}. The alloy exhibited low-temperature superplasticity (LTSP) with maximum elongations of 660% and 760% at a temperature of 423 K and using strain rates of 1×10{sup −3} s{sup −1} and 1×10{sup −4} s{sup −1}, respectively. Grain-boundary sliding (GBS) was identified as the deformation mechanism during HSRSP, and the glide-dislocation creep accommodated by GBS dominated during LTSP. Grain-boundary sliding accommodated with diffusion creep was the deformation mechanism at high test temperature and slow strain rates. An enhanced thermal stability of the microstructure consisting of fine equiaxed grains during deformation at elevated temperature was attributed to the extremely fine grains produced in HPT at room temperature, a high volume fraction of nano β-particles, and the formation of β-phase filaments.

  20. Deformation and fatigue behaviors of carburized automotive gear steel and predictions

    Directory of Open Access Journals (Sweden)

    Bonglae Jo

    2016-07-01

    Full Text Available The fatigue behavior of carburized components such as automotive transmission gears is very complex due to hardness and microstructure difference, residual stresses and multi-axial stress states developed between the case and the core. In addition, automotive gears in service, commonly used in helical type, are actually subjected to complex stress conditions such as bending, torsion, and contact stress states. This study presents experimental and analytical results on deformation behavior of carburized steels, widely used in automotive gears, under cyclic stress conditions including axial and torsion loadings. Axial fatigue tests and rotating bending fatigue tests are also included. Predictions of cyclic deformation and fatigue behaviors of the carburized steel with two-layer model are compared with experimental results. The carburized steel investigated in this study exhibited cyclic softening under both axial loading and torsional loading. Predicted results with simple two-layer model for the cyclic deformation and fatigue behaviors were comparatively similar to the experimental data.

  1. Experimental Investigation on Creep Deformation Behavior of Medium-strength Marble Rock

    Directory of Open Access Journals (Sweden)

    Li Yong

    2014-01-01

    Full Text Available The creep deformation behavior of rocks has significant effect on the stability of underground structures. This study presents the short-term and creep deformation behavior of medium-strength marble rock using a conventional uniaxial compression testing machine and a servo-controlled rheology testing machine. The uniaxial compressive strength is obtained by the uniaxial compression testing machine. During the creep behavior test, two types of rock specimens (dry and water-saturated are specified to be used to perform the uniaxial creep tests. Two rheological failure modes and the relationship curves between axial/circumferential strain and stress levels of marble specimens are also obtained from the creep test results. Eventually, the creep deformation behaviors are compared with those of typical soft rocks. These creep curves combined with a given creep constitutive model would provide accurate parameters for long-term stability analyses of actual projects.

  2. PLASTIC DEFORMATION BEHAVIOR OF ELECTROFORMED COPPER LINER OF SHAPED CHARGE AT DIFFERENT STRAIN RATES

    Institute of Scientific and Technical Information of China (English)

    H.Y. Gao; W.H. Tian; A.L. Fan; Q. Sun

    2003-01-01

    The paper deals with different plastic deformation behavior of electroformed copperliner of shaped charge, deformed at high strain rate (about 1×107 s-1) and normalstrain rate (4×10-4 s-1). The crystallographic orientation distribution of grains inrecovered slugs which had undergone high-strain-rate plastic deformation during ex-plosive detonation was investigated by electron backscattering Kikuchi pattern tech-nique. Cellular structures formed by tangled dislocations and sub-grain boundariesconsisting of dislocation arrays were detected in the recovered slugs. Some twins andslip dislocations were observed in specimen deformed at normal strain rate. It wasfound that dynamic recovery and recrystallization take place during high-strain-ratedeformation due to the temperature rising, whereas the conventional slip mechanismoperates during deformation at normal strain rate.

  3. PLASTIC DEFORMATION BEHAVIOR OF ELECTROFORMED COPPER LINER OF SHAPED CHARGE AT DIFFERENT STRAIN RATES

    Institute of Scientific and Technical Information of China (English)

    H.Y.Gao; Q.Sun

    2003-01-01

    The paper deals with different plastic deformation behavior of electroformed copper liner of shaped charge,depormed at high strain rate(about 1×107s-1) and normal strain rate (4×10-4s-1).The crystallographic orientation distribution of grains in recovered slugs which had undergone high-strain-rate plastic deformation during ex-plosive detonation was investigated by electron backscattering Kikuchi pattern tech-nique.Cellualar structures formed by tangled disocations and sub-grain boundaries consisting of dislocation arrays were detected in the recovered slugs.Some twins and slip dislocations were observed in specimen deformed at normal strain rate.It was found that dynamic recovery and recrystallization take place during high-strain-rate deformation due to the temperature rising,whereas the conventional slip mechanism operates during deformation at normal strain rate.

  4. Deformation behavior of duplex austenite and ε-martensite high-Mn steel

    Directory of Open Access Journals (Sweden)

    Ki Hyuk Kwon, Byeong-Chan Suh, Sung-Il Baik, Young-Woon Kim, Jong-Kyo Choi and Nack J Kim

    2013-01-01

    Full Text Available Deformation and work hardening behavior of Fe–17Mn–0.02C steel containing ε-martensite within the austenite matrix have been investigated by means of in situ microstructural observations and x-ray diffraction analysis. During deformation, the steel shows the deformation-induced transformation of austenite → ε-martensite → α'-martensite as well as the direct transformation of austenite → α'-martensite. Based on the calculation of changes in the fraction of each constituent phase, we found that the phase transformation of austenite → ε-martensite is more effective in work hardening than that of ε-martensite → α'-martensite. Moreover, reverse transformation of ε-martensite → austenite has also been observed during deformation. It originates from the formation of stacking faults within the deformed ε-martensite, resulting in the formation of 6H-long periodic ordered structure.

  5. Low Temperature Superplasticity of Ti-6Al-4V Processed by Warm Multidirectional Forging (Preprint)

    Science.gov (United States)

    2012-07-01

    using a JEOL JEM-2100FX transmission electron microscope (TEM) and a Quanta 600 field-emission-gun scanning-electron microscope (SEM). Results and...factor of three compared to the initial condition (Fig. 2b). A backscattered electron ( BSE ) image revealed the distribution of the  phase in the...a) BSE image of Ti-6Al-4V after annealing at Т=550С for 0.5 hour and (b) grain size as a function of soak time at 550C. Superplastic Behavior

  6. Effect of deformation temperature and strain rate on semi-solid deformation behavior of spray-formed Al-70 %Si alloys

    Institute of Scientific and Technical Information of China (English)

    ZHANG Di; YANG Bin; ZHANG Ji-shan; ZHANG Yong-an; XIONG Bai-qing

    2005-01-01

    Spray-formed Al-70%Si(mass fraction) alloys were deformed by compression in the semi-solid state.The effects of the deformation temperature, strain rate and the microstructure were studied. Two strain rates(1 s-1and 0.1 s-1) and six deformation temperatures (600 ℃, 720 ℃ , 780 ℃, 900 ℃, 1 000 ℃ and 1 100 ℃) were chosen. The stress-strain curve exhibits a peak at low strain and then decreases to a plateau before it starts to increase again as the strain increases. The stress required for deformation at lower strain rate and at higher deformation temperatures is less than those at higher strain rate and at lower deformation temperatures. Four mechanisms of semisolid deformation can be used to explain the different behaviors of the stress-strain curves under different conditions.

  7. Deformation behavior of Zr-based bulk metallic glass and composite in the supercooled liquid region

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    A Zr-based bulk metallic glass (BMG) with a composition of (Zr75Cu25)78.5Ta4Ni10Al7.5 and a bulk metallic glass matrix composite (BMGC) with a composition of (Zr75Cu25)74.5Ta8Ni10Al7.5 have been prepared by copper-mold casting. The compres-sive deformation behavior of the BMG and BMGC was investigated in the super-cooled region at different temperatures and various strain rates ranging from 8×10-4s-1 to 8×10-2s-1. It was found that both the strain rate and test temperature signifi-cantly affect the deformation behavior of the two alloys. The deformation follows Newtonian flow at low strain rates but non-Newtonian flow at high strain rates. The deformation mechanism for the two kinds of alloys was discussed in terms of the transition state theory.

  8. A Density Functional Theory Study on the Deformation Behaviors of Fe-Si-B Metallic Glasses

    Directory of Open Access Journals (Sweden)

    Guang-Ping Zheng

    2012-08-01

    Full Text Available Density functional theory has been employed to investigate the deformation behaviors of glassy Fe-Si-B model systems prepared by ab initio molecular dynamics. The atomistic deformation defects which are closely related to the local dilation volumes or excess volumes and unstable bonding have been systematically analyzed. It has been found that the icosahedral structures are relatively stable under shear deformation until fracture occurs. Plastic flow is indicated by interruption of percolating icosahedral structures, caused by unstable Fe-Si bonding of p-s hybridization in nature.

  9. Large N behavior of mass deformed ABJM theory

    Science.gov (United States)

    Nosaka, Tomoki; Shimizu, Kazuma; Terashima, Seiji

    2016-03-01

    In this paper, using the localization technique we analyze the large N limit of the mass deformed Aharony-Bergman-Jafferis-Maldacena (ABJM) theory on the three sphere with a finite mass parameter and finite Chern-Simons levels. We find two different solutions of the saddle point equations in the large N limit. With these solutions we compute the free energy limit and find that there is a first order phase transition. Our results may predict a phase transition in the dual gravity theory.

  10. Large N behavior of mass deformed ABJM theory

    CERN Document Server

    Nosaka, Tomoki; Terashima, Seiji

    2015-01-01

    In this paper, using the localization technique we analyze the large N limit of the mass deformed Aharony-Bergman-Jafferis-Maldacena (ABJM) theory on the three sphere with a finite mass parameter and finite Chern-Simons levels. We find two different solutions of the saddle point equations in the large N limit. With these solutions we compute the free energy and find that there is a first order phase transition. Our results may predict a phase transition in the dual gravity theory.

  11. Scaling up of High-Pressure Sliding (HPS) for Grain Refinement and Superplasticity

    Science.gov (United States)

    Takizawa, Yoichi; Masuda, Takahiro; Fujimitsu, Kazushige; Kajita, Takahiro; Watanabe, Kyohei; Yumoto, Manabu; Otagiri, Yoshiharu; Horita, Zenji

    2016-09-01

    The process of high-pressure sliding (HPS) is a method of severe plastic deformation developed recently for grain refinement of metallic materials under high pressure. The sample for HPS is used with a form of sheet or rod. In this study, an HPS facility with capacities of 500 tonnes for vertical pressing and of 500 and 300 tonnes for horizontal forward and backward pressings, respectively, was newly built and applied for grain refinement of a Mg alloy as AZ61, Al alloys such as Al-Mg-Sc, A2024 and A7075 alloys, a Ti alloy as ASTM-F1295, and a Ni-based superalloy as Inconel 718. Sheet samples with dimensions of 10 to 30 mm width, 100 mm length, and 1 mm thickness were processed at room temperature and ultrafine grains with sizes of ~200 to 300 nm were successfully produced in the alloys. Tensile testing at elevated temperatures confirmed the advent of superplasticity with total elongations of more than 400 pct in all the alloys. It is demonstrated that the HPS can make all the alloys superplastic through processing at room temperature with a form of rectangular sheets.

  12. Compression Deformation Behavior of AZ81 Magnesium Alloy at Elevated Temperatures

    Directory of Open Access Journals (Sweden)

    Xiaoping Luo

    2014-01-01

    Full Text Available The hot deformation behavior of an AZ81 magnesium alloy was investigated by hot compressive testing on a Gleeble-1500 thermal mechanical simulator in the temperature range from 200 to 400°C and in the strain rate range of 0.001–5 s−1. The relationships among flow stress, strain rate, and deformation temperature were analyzed, and the deformation activation energy and stress exponent were calculated. The microstructure evolution of the AZ81 magnesium alloy under high deformation was examined. The results indicated that the maximum value of the flow stress increased with the decrease of deformation temperature and the increase of strain rate. When the deformation temperature is constant, the flow stress of the AZ81 magnesium alloy increases with the increase of strain rate, which can be demonstrated by a Zener-Hollomon parameter in a hyperbolic-sine-type equation with a hot compression deformation activation energy of 176.01 KJ/mol and basic hot deformation material factors A, n, and a in the analytical expression of the AZ81 magnesium alloy flow stress of 3.21227×1014 s−1, 7.85, and 0.00866 MPa, respectively.

  13. Shear Deformation Behaviors of Sn3.5Ag Lead-free Solder Samples

    Institute of Scientific and Technical Information of China (English)

    Jing Han; Hongtao Chen; Mingyu Li; Chunqing Wang

    2013-01-01

    In this study,shear tests have been performed on the as-reflowed Sn3.5Ag solder bumps and joints to investigate the deformation behavior of Sn3.5Ag lead-free solder samples.Scanning electron microscopy (SEM) was employed to characterize the microstructures of the samples and orientation imaging microscopy (OIM) with electron backscattered diffraction (EBSD) in SEM was used to obtain crystallographic orientation of grains to provide a detailed characterization of the deformation behavior in Sn3.5Ag solder samples after shear tests.The deformation behavior in solder samples under shear stress was discussed.The experimental results suggest that the dynamic recrystallization could occur under shear stress at room temperature and recrystallized grains should evolve from subgrains by rotation.Compared with that of non-recrystallized and as-reflowed microstructures,the microhardness of the recrystallized microstructure decreased after shear tests.

  14. Use of multiscale zirconium alloy deformation models in nuclear fuel behavior analysis

    Energy Technology Data Exchange (ETDEWEB)

    Montgomery, Robert; Tomé, Carlos; Liu, Wenfeng; Alankar, Alankar; Subramanian, Gopinath; Stanek, Christopher

    2017-01-01

    Accurate prediction of cladding mechanical behavior is a key aspect of modeling nuclear fuel behavior, especially for conditions of pellet-cladding interaction (PCI), reactivity-initiated accidents (RIA), and loss of coolant accidents (LOCA). Current approaches to fuel performance modeling rely on empirical models for cladding creep, growth and plastic deformation, which are limited to the materials and conditions for which the models were developed. CASL has endeavored to improve upon this approach by incorporating a microstructurally-based, atomistically-informed, zirconium alloy mechanical deformation analysis capability into the BISON-CASL engineering scale fuel performance code. Specifically, the viscoplastic self-consistent (VPSC) polycrystal plasticity modeling approach, developed by Lebensohn and Tome´ [2], has been coupled with BISON-CASL to represent the mechanistic material processes controlling the deformation behavior of the cladding. A critical component of VPSC is the representation of the crystallographic orientation of the grains within the matrix material and the ability to account for the role of texture on deformation. The multiscale modeling of cladding deformation mechanisms allowed by VPSC far exceed the functionality of typical semi-empirical constitutive models employed in nuclear fuel behavior codes to model irradiation growth and creep, thermal creep, or plasticity. This paper describes the implementation of an interface between VPSC and BISON-CASL and provides initial results utilizing the coupled functionality.

  15. Compression deformation behaviors of sheet metals at various clearances and side forces

    Directory of Open Access Journals (Sweden)

    Zhan Mei

    2015-01-01

    Full Text Available Modeling sheet metal forming operations requires understanding of plastic behaviors of sheet metals along non-proportional strain paths. The plastic behavior under reversed uniaxial loading is of particular interest because of its simplicity of interpretation and its application to material elements drawn over a die radius and underwent repeated bending. However, the attainable strain is limited by failures, such as buckling and in-plane deformation, dependent on clearances and side forces. In this study, a finite element (FE model was established for the compression process of sheet specimens, to probe the deformation behavior. The results show that: With the decrease of the clearance from a very large value to a very small value, four defects modes, including plastic t-buckling, micro-bending, w-buckling, and in-plane compression deformation will occur. With the increase of the side force from a very small value to a very large value, plastic t-buckling, w-buckling, uniform deformation, and in-plane compression will occur. The difference in deformation behaviors under these two parameters indicates that the successful compression process without failures for sheet specimens only can be carried out under a reasonable side force.

  16. Dynamic recrystallization behavior of a γ′-hardened nickel-based superalloy during hot deformation

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Hongbin; Zhang, Kaifeng [School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001 (China); Jiang, Shaosong, E-mail: jiangshaosong@hit.edu.cn [School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001 (China); Zhou, Haiping [School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001 (China); Zhao, Changhong; Yang, Xiaoli [Fushun Special Steel Co. Ltd, Fushun 113000 (China)

    2015-02-25

    Highlights: • The relationship between the peak stress and stable DRX grain size has been expressed by a power law function. • The effect of CDRX characterized by progressive subgrain rotation became weaker with the increasing deformation temperature. • The effect of DDRX became stronger with the increasing strain for the alloy deformed at 1160 °C/0.1 s{sup −1}. • The fraction of twin boundaries is closely related to the deformation temperature and strain. - Abstract: The hot deformation behavior of a γ′-hardened nickel-based superalloy was investigated by means of isothermal compression tests in the temperature range of 1010–1210 °C with a strain rate of 0.1 s{sup −1}. The electron backscatter diffraction (EBSD) technique and transmission electron microscope (TEM) were employed to investigate the effect of deformation temperature and strain on the microstructure evolution and nucleation mechanisms of dynamic recrystallization (DRX). Microstructure observations revealed that the size and volume fraction of DRX grains increased with the increasing temperature. A power exponent relationship was obtained between the stable DRX grain size and the peak stress. Additionally, it was found that the effect of CDRX characterized by progressive subgrain rotation became weaker with the increasing deformation temperature, and DDRX was the operating nucleation mechanism of DRX at higher deformation temperature. On the other hand, the effect of DDRX became stronger with the increasing strain, and CDRX can only be considered as an assistant nucleation mechanism of DRX at the later stage of deformation for the alloy deformed at 1160 °C. Nucleation of DRX can also be activated by the twinning formation. Hence, particular attention was also paid to the evolution of twin boundaries during hot deformation.

  17. Deformation behavior of metallic glass composites reinforced with shape memory nanowires studied via molecular dynamics simulations

    Science.gov (United States)

    Şopu, D.; Stoica, M.; Eckert, J.

    2015-05-01

    Molecular dynamics simulations indicate that the deformation behavior and mechanism of Cu64Zr36 composite structures reinforced with B2 CuZr nanowires are strongly influenced by the martensitic phase transformation and distribution of these crystalline precipitates. When nanowires are distributed in the glassy matrix along the deformation direction, a two-steps stress-induced martensitic phase transformation is observed. Since the martensitic transformation is driven by the elastic energy release, the strain localization behavior in the glassy matrix is strongly affected. Therefore, the composite materials reinforced with a crystalline phase, which shows stress-induced martensitic transformation, represent a route for controlling the properties of glassy materials.

  18. The deformation behavior of soil mass in the subsidence region of Beijing, China

    Science.gov (United States)

    Tian, F.; Liu, J.-R.; Luo, Y.; Zhu, L.; Yang, Y.; Zhou, Y.

    2015-11-01

    Land subsidence induced by excessive groundwater withdrawal has been a major environmental and geological problem in the Beijing plain area. The monitoring network of land subsidence in Beijing has been established since 2002 and has covered the entire plain area by the end of 2008. Based on data from extensometers and groundwater observation wells, this paper establishes curves of variations over time for both soil mass deformation and water levels and the relationship between soil mass deformation and water level. In addition, an analysis of deformation behavior is carried out for soil mass with various lithologies at different depths depending on the corresponding water level. Finally, the deformation behavior of soil mass is generalized into five categories. The conclusions include: (i) the current rate of deformation of the shallow soil mass is slowing, and most of the mid-deep and deep soil mass continue to compress at a more rapid speed; (ii) the sand strata behaves elastically, while the clay soil mass at different depths is usually characterized by elastic-plastic and creep deformation, which can be considered as visco-elastoplastic.

  19. Thermal image analysis of plastic deformation and fracture behavior by a thermo-video measurement system

    Science.gov (United States)

    Ohbuchi, Yoshifumi; Sakamoto, Hidetoshi; Nagatomo, Nobuaki

    2016-12-01

    The visualization of the plastic region and the measurement of its size are necessary and indispensable to evaluate the deformation and fracture behavior of a material. In order to evaluate the plastic deformation and fracture behavior in a structural member with some flaws, the authors paid attention to the surface temperature which is generated by plastic strain energy. The visualization of the plastic deformation was developed by analyzing the relationship between the extension of the plastic deformation range and the surface temperature distribution, which was obtained by an infrared thermo-video system. Furthermore, FEM elasto-plastic analysis was carried out with the experiment, and the effectiveness of this non-contact measurement system of the plastic deformation and fracture process by a thermography system was discussed. The evaluation method using an infrared imaging device proposed in this research has a feature which does not exist in the current evaluation method, i.e. the heat distribution on the surface of the material has been measured widely by noncontact at 2D at high speed. The new measuring technique proposed here can measure the macroscopic plastic deformation distribution on the material surface widely and precisely as a 2D image, and at high speed, by calculation from the heat generation and the heat propagation distribution.

  20. Phase transformation and deformation behavior of NiTi-Nb eutectic joined NiTi wires.

    Science.gov (United States)

    Wang, Liqiang; Wang, Cong; Zhang, Lai-Chang; Chen, Liangyu; Lu, Weijie; Zhang, Di

    2016-04-06

    NiTi wires were brazed together via eutectic reaction between NiTi and Nb powder deposited at the wire contact region. Phase transformation and deformation behavior of the NiTi-Nb eutectic microstructure were investigated using transmission electron microscopy (TEM) and cyclic loading-unloading tests. Results show that R phase and B19' martensite transformation are induced by plastic deformation. R phase transformation, which significantly contributes to superelasticity, preferentially occurs at the interfaces between NiTi and eutectic region. Round-shaped Nb-rich phase with rod-like and lamellar-type eutectics are observed in eutectic regions. These phases appear to affect the deformation behavior of the brazed NiTi-Nb region via five distinct stages in stress-strain curves: (I) R phase reorientation, (II) R phase transformation from parent phase, (III) elastic deformation of reoriented martensite accompanied by the plastic deformation of Nb-rich phase and lamellar NiTi-Nb eutectic, (IV) B19' martensitic transformation, and (V) plastic deformation of the specimen.

  1. Geometrically nonlinear deformation and the emergent behavior of polarons in soft matter.

    Science.gov (United States)

    Li, Xiaobao; Liu, Liping; Sharma, Pradeep

    2015-11-07

    Mechanical strain can alter the electronic structure of both bulk semiconductors as well as nanostructures such as quantum dots. This fact has been extensively researched and exploited for tailoring electronic properties. The strain mediated interaction between the charge carriers and the lattice is interpreted through the so-called deformation potential. In the case of soft materials or nanostructures, such as DNA, the deformation potential leads to the formation of polarons which largely determine the electronic characteristics of DNA and similar polymer entities. In addition, polarons are also speculated to be responsible for the mechanism of quantum actuation in carbon nanotubes. The deformation potential is usually taken to be a linear function of the lattice deformation (U ∼ αε) where α is the deformation potential "constant" that determines the coupling strength and ε is the mechanical strain. In this letter, by carefully accounting for nonlinear geometric deformation that has been hitherto ignored so far in this context, we show that the deformation potential constant is renormalized in a non-trivial manner and is hardly a constant. It varies spatially within the material and with the size of the material. This effect, while negligible for hard materials, is found to be important for soft materials and critically impacts the interpretation of quantities such as polaron size, binding energy, and accordingly, electronic behavior.

  2. Scale-bridging analysis on deformation behavior of high-nitrogen austenitic steels.

    Science.gov (United States)

    Lee, Tae-Ho; Ha, Heon-Young; Hwang, Byoungchul; Kim, Sung-Joon; Shin, Eunjoo; Lee, Jong Wook

    2013-08-01

    Scale-bridging analysis on deformation behavior of high-nitrogen austenitic Fe-18Cr-10Mn-(0.39 and 0.69)N steels was performed by neutron diffraction, electron backscattered diffraction (EBSD), and transmission electron microscopy (TEM). Two important modes of deformation were identified depending on the nitrogen content: deformation twinning in the 0.69 N alloy and strain-induced martensitic transformation in the 0.39 N alloy. The phase fraction and deformation faulting probabilities were evaluated based on analyses of peak shift and asymmetry of neutron diffraction profiles. Semi in situ EBSD measurement was performed to investigate the orientation dependence of deformation microstructure and it showed that the variants of ε martensite as well as twin showed strong orientation dependence with respect to tensile axis. TEM observation showed that deformation twin with a {111} mathematical left angle bracket 112 mathematical right angle bracket crystallographic component was predominant in the 0.69 N alloy whereas two types of strain-induced martensites (ε and α' martensites) were observed in the 0.39 N alloy. It can be concluded that scale-bridging analysis using neutron diffraction, EBSD, and TEM can yield a comprehensive understanding of the deformation mechanism of nitrogen-alloyed austenitic steels.

  3. Study on Hot Deformation Behavior of 7085 Aluminum Alloy during Backward Extrusion Process

    Directory of Open Access Journals (Sweden)

    R. B. Mei

    2015-01-01

    Full Text Available Compression test was carried out and the true stress-strain curves were obtained from the hot compression of 7085 alloy. A numerical simulation on the deformation behavior of 7085 aluminum alloy during the backward extrusion was also performed by finite element method. The results show that dynamic recrystallization occurs in the hot compression of 7085 alloy and the peak stress reaches higher values as the strain rate increases and deformation temperature decreases. The backward extrusion processes include contact deformation, initial deformation, and steady deformation. Severe plastic deformation of shear and compression occurs when the metal flowed into the channel between fillet of punch and wall of die so that the grain size can be refined by backward extrusion. The deformation in the region of top of wall is too small to meet the mechanical properties of requirements and the metal usually needs to be trimmed. The experiments with the same parameters as simulation had been carried out and the experimental cup after extrusion has better quality.

  4. Superplastic Micro-forming Mechanism and Size Effects of Micro-array Made of Nanocrystalline Material%纳米材料微阵列超塑微成形机理与尺度效应

    Institute of Scientific and Technical Information of China (English)

    王国峰; 李优; 刘奇; 赵相禹

    2015-01-01

    微成形技术是未来批量制造高精密微小零件的关键技术,但是,微小尺度下材料的塑性变形行为不仅表现出明显的尺度效应,而且零件尺度已经接近常规材料的晶粒尺寸,每个晶粒的形状、取向、变形特征对整体变形产生复杂的影响,难以保证微成形的工艺稳定性。本项目采用纳米材料进行微成形,制造微阵列,零件内部包含大量的晶粒,可以排除晶粒复杂性的影响,而且纳米材料具有超塑性,在超塑状态下,变形抗力和摩擦力都明显降低,从而显著降低微成形工艺对模具性能的苛刻要求,提高工艺稳定性和成形精度。目前,纳米材料超塑性微成形技术方面的研究极少,变形时纳米材料的力学行为、变形机理、尺度效应、位错演化、力学模型等关键问题还有待研究。采用电沉积技术制备晶粒尺寸可控的纳米材料,将工艺实验研究、性能测试、组织分析、力学性能表征、数值模拟相结合,深入探究了纳米材料微阵列超塑性微成形机理和成形规律,以促进该技术的广泛应用。%ABSTRACT:Micro-forming is a key technique for fabricating high-precision micro-part in large volume. However, plastic deformation at small scale has obvious size effects. The shape, orientation and deformation behavior of each grain have complicated influence on the micro-forming, since the scale of the parts approaches to the size of grain in common materi-als. Consequently, it is very hard to ensure the processing stability of micro-forming. In the current project, nanocrystalline materials were used to form micro-array. The influence of grain complexity could be eliminated since there were a lot of grains in the micro-part. In addition, nanocrystalline materials usually have superplasticity. Under this condition, the de-formation force and friction decrease obviously, which decreases the requirement on the mechanical

  5. Alloy-dependent deformation behavior of highly ductile nanocrystalline AuCu thin films

    Energy Technology Data Exchange (ETDEWEB)

    Lohmiller, Jochen [Karlsruhe Institute of Technology, Institute for Applied Materials, P.O. Box 3640, 76021 Karlsruhe (Germany); Laboratory for Nanometallurgy, Department of Materials, ETH Zurich, Wolfgang-Pauli-Str. 10, 8093 Zurich (Switzerland); Spolenak, Ralph [Laboratory for Nanometallurgy, Department of Materials, ETH Zurich, Wolfgang-Pauli-Str. 10, 8093 Zurich (Switzerland); Gruber, Patric A., E-mail: patric.gruber@kit.edu [Karlsruhe Institute of Technology, Institute for Applied Materials, P.O. Box 3640, 76021 Karlsruhe (Germany)

    2014-02-10

    Nanocrystalline thin films on compliant substrates become increasingly important for the development of flexible electronic devices. In this study, nanocrystalline AuCu thin films on polyimide substrate were tested in tension while using a synchrotron-based in situ testing technique. Analysis of X-ray diffraction profiles allowed identifying the underlying deformation mechanisms. Initially, elastic and microplastic deformation is observed, followed by dislocation-mediated shear band formation, and eventually macroscopic crack formation. Particularly the influence of alloy composition, heat-treatment, and test temperature were investigated. Generally, a highly ductile behavior is observed. However, high Cu concentrations, annealing, and/or large plastic strains lead to localized deformation and hence reduced ductility. On the other hand, enhanced test temperature allows for a delocalized deformation and extended ductility.

  6. Inflation-predictable behavior and co-eruption deformation at Axial Seamount

    Science.gov (United States)

    Nooner, Scott L.; Chadwick, William W.

    2016-12-01

    Deformation of the ground surface at active volcanoes provides information about magma movements at depth. Improved seafloor deformation measurements between 2011 and 2015 documented a fourfold increase in magma supply and confirmed that Axial Seamount’s eruptive behavior is inflation-predictable, probably triggered by a critical level of magmatic pressure. A 2015 eruption was successfully forecast on the basis of this deformation pattern and marked the first time that deflation and tilt were captured in real time by a new seafloor cabled observatory, revealing the timing, location, and volume of eruption-related magma movements. Improved modeling of the deformation suggests a steeply dipping prolate-spheroid pressure source beneath the eastern caldera that is consistent with the location of the zone of highest melt within the subcaldera magma reservoir determined from multichannel seismic results.

  7. Deformation Behavior of Mg-8 wt%Li Alloy under High-speed Impact

    Institute of Scientific and Technical Information of China (English)

    SHA Gui-ying; LIU Chun-zhong; YU Tao; SHI Ji-hong

    2006-01-01

    Deformation behavior of the Mg-8 wt%Li alloy at high strain rate was studied by means of the Split Hopkinson Pressure Bar (with strain rate of 103 s-1). It is found that shear localization proves to be the main damage mode for the alloy during dynamic loading. Strain and strain rate are the two necessary parameters affecting the occurrence of deformation and shear bands. Deformation bands begin to form when the strain and strain rate reach 0.20 and 1 900 s-1 respectively and will develop gradually with the strain rate increasing. Besides, deformation bands will transform into shear bands when the strain and strain rate reach above 0.25 and 3 500 s-1 separately.

  8. Finite element simulations of deformation behavior in equal channel angular pressing using a rotated die

    Institute of Scientific and Technical Information of China (English)

    Yixuan TAN; Saiyi LI

    2012-01-01

    A new die design for equal channel angular pressing (ECAP) of square cross-section billet was proposed by a 45° rotation of the inlet and outlet channels around the channel axes.ECAP utilizing the rotated and conventional dies was simulated in three dimensions using the finite element method.Conditions with different material properties and friction coefficients were studied.The billet deformation behavior was evaluated in terms of the spatial distribution of equivalent plastic strain,plastic deformation zone and load history.The results show that the rotated die appears to produce billets with a smaller deformation inhomogeneity over the entire crosssection and a greater average of equivalent plastic strain at the cost of a slightly larger working load.The billet deformation enters into a steady state earlier in the case of the rotated die than the conventional die under the condition of a relatively large friction coefficient.

  9. Hot-deformation behaviors of AZ31 alloys with different initial states

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    The hot-deformation behaviors of three types of AZ31 samples, extruded sheet, hot rolled sheet and east rod were studied.These samples had different initial grain size and texture. Compression deformation of these samples was carried out using a Gleeble 1500D under a series of thermal deformation conditions. Mierostructure and texture of the initial and deformed samples were examined using electron backscatter diffraction (EBSD) techniques. The flow curves for all these three types of samples shifted upward with strain rate increasing. Significant grain refinement was noticed in the hot rolled sheet sample. The grain size was reduced to 3.7 μm after 50% (ε=0.69) compression. The DRX grains in both the extruded rod and hot rolled sheet samples presented the same basal plane texture, irrespective of the difference in the initial texture of the samples.

  10. Analysis of the deformation behavior of low Cu-Cr-Zr alloy

    Science.gov (United States)

    Morozova, A.; Belyakov, A.; Kaibyshev, R.

    2016-11-01

    Mechanical properties and the microstrustural evolution of low Cu-Cr-Zr alloy subjected to equal channel angular pressing (ECAP) at 400°C via route BC after the solution treatment were investigated. Plastic deformation resulted in the formation of a large number of low-angle subgrain boundaries in initial coarse grains. New fine grains formed due to a progressive increase in misorientations of strain-induced (sub)boundaries. The ultrafine grain formation during large plastic deformation was accompanied by significant strengthening. The variation of the strain hardening rate with the flow stress after the total strain ɛ ˜ 1-12 was studied. The deformation behavior was discussed in terms of the dislocation-density-related Voce equation. Large plastic deformation led to an increase in both the ɛC and ɛV parameters in the Voce equation. The relationship between strain hardening and microstructure is considered in detail using the Voce parameters.

  11. Recrystailization Behavior of Deformed Austenite in High Strength Microalloyed Pipeline Steel

    Institute of Scientific and Technical Information of China (English)

    YANG Jing-hong; LIU Qing-you; SUN Dong-bai; LI Xiang-yang

    2009-01-01

    Using methods of single-hit hot compression and stress relaxation after deformation on a Gleeble 1500D thermomechanical simulator,the curves of flow stress and stress relaxation,the microstructure and the recrystallization behavior of Nb-V-Ti high strength microalloyed low carbon pipeline steel were studied,and the influence of the thermomechanical treatment parameters on dynamic and static recrystallization of the steel was investigated.It was found that microalloying elements improved the deformation activation energy and produced a retardation of the recrystallization due to the solid solution and precipitation pinning.The deformation conditions such as deformation temperature,strain,and strain rate influenced the recrystallization kinetics and the microstructure respectively.Equations obtained can be used to valuate and predict the dynamic and static recrystallizations.

  12. Investigation on Deformation Behavior of Nickel Aluminum Bronze by Neutron Diffraction and Transmission Electron Microscopy

    Science.gov (United States)

    Xu, Xiaoyan; Wang, Hong; Lv, Yuting; Lu, Weijie; Sun, Guangai

    2016-05-01

    The deformation behavior, deformation microstructures, and generated inter-phase stresses of nickel aluminum bronze were investigated by in situ neutron diffraction instrument and transmission electron microscopy in this paper. Lattice strains calculated by both peak shifting and broadening by Gaussian fitting of α and κ phase neutron diffraction peak profiles at both holding stress conditions and unloaded stress conditions were compared. Twining and stacking faults in α matrix were observed after deformed by different tensile stresses. Compressive internal/residual stress in α matrix and tensile internal stress in κ phase in elasto-plastic region were calculated based on neutron diffraction analysis. The piled-up dislocations around hard κ phases increase with increasing the deformation degree, which raise the stress concentration near α/ κ interface and increase the internal stresses.

  13. Influence of deformation behavior, oxydation, and temperature on the long time cyclic stress behavior of high temperature steels

    Science.gov (United States)

    Maile, K.

    1982-01-01

    The influence of different parameters on the creep-fatigue behavior of several steel alloys was investigated. The higher the temperature the lower the crack initiation value. Pauses during the cycle reduce the damage. Oxidation reduces and protective gas increases the lifetime. Prior loading and prior deformation reduce the lifetime. Short annealing slightly affects the cycle stress behavior. The test results do not satisfactorily agree with methods of extrapolation and damage accumulation.

  14. Healing behavior of preexisting hydrogen micropores in aluminum alloys during plastic deformation

    Energy Technology Data Exchange (ETDEWEB)

    Toda, H., E-mail: toda@pse.tut.ac.jp [Department of Production Systems Engineering, Toyohashi University of Technology, Toyohashi, Aichi 441-8580 (Japan); Minami, K. [Department of Production Systems Engineering, Toyohashi University of Technology, Toyohashi, Aichi 441-8580 (Japan); Koyama, K.; Ichitani, K. [Furukawa-Sky Aluminum Corp., 1351, Uwanodai, Fukaya, Saitama 366-8511 (Japan); Kobayashi, M. [Department of Production Systems Engineering, Toyohashi University of Technology, Toyohashi, Aichi 441-8580 (Japan); Uesugi, K.; Suzuki, Y. [Japan Synchrotron Radiation Research Institute, Mikazuki-cho, Sayo-gun, Hyogo 679-5198 (Japan)

    2009-09-15

    Synchrotron X-ray microtomography was used to observe the shrinkage and annihilation behaviors of hydrogen micropores in three dimensions during hot and cold plastic deformation of an Al-Mg alloy. Whether complete healing of micropores is achieved after plastic deformation was examined by exposing the material to a high temperature after plastic deformation. Although micropores generally show a pattern of shrinking and closing, closer inspection of a single specimen revealed a variety of geometrically variable behaviors. It is noteworthy that some of the micropores are reinitiated in positions identical to those before their annihilation, even after an 8-22% macroscopic strain has been further applied after annihilation. We attribute local variations such as these to significant local strain variation, which we measured in a series of tomographic volumes by tracking the microstructural features.

  15. Stored energy and annealing behavior of heavily deformed aluminium

    DEFF Research Database (Denmark)

    Kamikawa, Naoya; Huang, Xiaoxu; Kondo, Yuka

    2012-01-01

    followed by 0.5 h annealing at 200-600°C, where the former treatment leads to discontinuous recrystallization and the latter to uniform structural coarsening. This behavior has been analyzed in terms of the relative change during annealing of energy stored as elastic energy in the dislocation structure...... and as boundary energy in the high-angle boundaries. © (2012) Trans Tech Publications, Switzerland....

  16. Superplasticity and joining of zirconia-based ceramics

    Energy Technology Data Exchange (ETDEWEB)

    Dominguez-Rodriguez, A.; Gutierrez-Mora, F.; Jimenez-Melendo, M.; Chaim, R.; Routbort, J. L.

    1999-12-10

    Steady-state creep and joining of alumina/zirconia composites containing alumina volume fractions of 20, 60, and 85% have been investigated between 1,250 and 1,350 C. Superplasticity of these compounds is controlled by grain-boundary sliding and the creep rate is a function of alumina volume fraction, not grain size. Using the principles of superplasticity, pieces of the composite have been joined by applying the stress required to achieve 5 to 10% strain to form a strong interface at temperatures as low as 1,200 C.

  17. Superplastic Forming and Diffusion Bonding of Titanium Alloys

    Directory of Open Access Journals (Sweden)

    A. K. Ghosh

    1986-04-01

    Full Text Available New and advanced fabrication methods for titanium components are emerging today to replace age-old fabrication processes and reduce component cost. Superplastic forming and diffusion bonding are two such advanced fabrication technologies which when applied individually or in combination can provide significant cost and weight benefits and a rather broad manufacturing technology base. This paper briefly reviews the state of understanding of the science and technology of super plastic forming of titanium alloys, and their diffusion bonding capability. Emphasis has been placed on the metallurgy of superplastic flow in two phase titanium alloys, the microstructural and external factors which influence this behaviour.

  18. Nanometric Gouge in High-Speed Shearing Experiments: Superplasticity?

    Science.gov (United States)

    Green, H. W.; Lockner, D. A.; Bozhilov, K. N.; Maddon, A.; Beeler, N. M.; Reches, Z.

    2010-12-01

    High-speed shearing experiments on solid rock samples typically generate a gouge with sub-micron grain size that appears to control the frictional resistance at velocities approaching 1 m/s (Reches & Lockner, Nature, in press). We conducted experiments on Kasota dolomite samples and observed profound weakening (friction drops from ~0.8 to ~ 0.2) under earthquake conditions (up to slip-velocity ~ 0.95 m/s and normal stress 28.4 MPa). During these runs the experimental fault had T ≥ 800°C and developed a shining, dark surface. We report here analysis of such a surface with scanning electron microscopy (SEM) and atomic force microscopy (AFM). SEM analysis shows a slickensided gouge made up of particles all ≤ 50nm with a large fraction ≤ 20nm. The spacing of the slickenside striations is less than 1 µm. Over large areas of the slickensided surface the nanometric gouge has been replaced by an undeformed, interlocking crystalline pavement of 100-300 nm grain size. Qualitative chemical analysis of this pavement surface by energy-dispersive X-ray spectroscopy reveals only a weak carbon peak, suggesting that the dolomite has been decarbonated. The development of a “pavement” of grain size ~200 nm in our experiments is remarkably similar to the observations of Han et al. (JGR, 2010, Fig. 14(d)). However, their experiments either did not develop such a nanometric gouge or it was completely replaced by the coarser pavement. These present observations of nanometric gouge that recrystallizes during the short time interval of elevated temperature following termination of deformation are reminiscent of the nanometric “gouge” produced in very high-pressure experiments (1-14 GPa) that have failed by transformation-induced faulting during the olivine-spinel transformation (Green and Burnley, Nature, 1989; Green et al., Nature, 1990). In the high-pressure experiments, the gouge consists of a nanocrystalline aggregate of the spinel phase that flowed at very high strain

  19. Constitutive Modeling for Flow Behaviors of Superaustenitic Stainless Steel S32654 during Hot Deformation

    Institute of Scientific and Technical Information of China (English)

    En-xiang PU; Han FENG; Min LIU; Wen-jie ZHENG; Han DONG; Zhi-gang SONG

    2016-01-01

    Hot deformation behavior of superaustenitic stainless steel S32654 was investigated with hot compression tests at temperatures of 950-1 250 ℃ and strain rates of 0�001-10 s-1 .Above 1 150 ℃,with strain rate lower than 0�1 s-1 ,the flow curves exhibit nearly steady-state behavior,while at higher strain rate,continuous flow softening occurs.To provide a precise prediction of flow behavior for the alloy,the constitutive modeling considering effect of strain was derived on the basis of the obtained experimental data and constitutive relationship which incorporated Ar-rhenius term and hyperbolic-sine type equation.The material constantsα,n,Q and lnA are found to be functions of the strain and can be fitted employing eighth-order polynomial.The developed constitutive model can be employed to describe the deformation behavior of superaustenitic stainless steel S32654.

  20. RHEOLOGICAL DEFORMATION BEHAVIOR MODEL OF SUGAR DOUGH IN THE CONDITIONS OF MONOAXIAL COMPRESSION

    Directory of Open Access Journals (Sweden)

    G. O. Magomedov

    2014-01-01

    Full Text Available Summary. The knowledge of regularities of deformation behavior of the processed confectionery masses with certain rheological properties allows to calculate parameters of shaping process and to select processing equipment for its carrying out. The article studies the obtaining of the rheological equation of deformation behavior of sugar dough in the conditions of monoaxial compression which is realized in sugar cookies dough pieces formation processes. The results of the pilot studies confirming adequacy of the offered rheological equation are presented. The behavior of an elastic-, viscous- and plastic body in the conditions of quasistatic test for creeping during which the set size is tension, and the measured one is relative deformation is considered. The main rheological properties of sugar dough received experimentally are given. Values of rheological constants are received and it is revealed that at 95% confidential probability, the rheological equation for the general deformation of an elastic-, viscous- and plastic body adequately describes experimental data. The maximum fault thus makes 2,3%. It is established that dough pieces shaping processes from the sugar dough possessing visco- and plastic properties should be realized at an external tension (power impact from the forming body which exceeds a limit of fluidity of the dough formed. The level of external tension, as well as the duration of its influence (that is formation duration should be chosen taking into account the residual deformations in the processed mass which guarantee giving of a certain geometrical form and drawing on a surface of dough pieces. The rheological model of sugar dough allows to predict its deformation behavior in the formation conditions, and to calculate the parameters of sugar dough formation process.

  1. Cooperative grain boundary sliding at room temperature of a Zn-20.2%Al-1.8%Cu superplastic alloy

    Energy Technology Data Exchange (ETDEWEB)

    Munoz-Andrade, J.D. [Dept. de Materiales, Univ. Autonoma Metropolitana Unidad Azcapotzalco (Mexico); Mendoza-Allende, A.; Montemayor-Aldrete, J.A. [Inst. de Fisica, Univ. Nacional Autonoma de Mexico (Mexico); Torres-Villasenor, G. [Inst. de Investigacion en Materiales, Univ. Nacional Autonoma de Mexico (Mexico)

    2001-07-01

    By applying a new technique [1-2] which provides a mesoscopic coordinate system inscribed on the surface of a tensile specimen, with 371 {mu}m gage length for a Zn-20.2%Al-1.8%Cu superplastic alloy deformed at room temperature it is possible to show that: Deformation of the sample it is homogeneous at macroscopic level, but inhomogeneous at mesoscopical level. The inhomogeneity is ascribed to the sliding of grain blocks. For 28.5% of deformation the distribution function for the block sizes is described by: N(x) = 1.37 x{sup 3}exp(-3x/12.2 {mu}m), where, N(x) is the number of blocks of size x, inside an area of about 172 x 244 ({mu}m){sup 2}. (orig.)

  2. Hot deformation behavior of KFC copper alloy during compression at elevated temperatures

    Institute of Scientific and Technical Information of China (English)

    ZHANG Hui; ZHANG Hong-gang; PENG Da-shu

    2006-01-01

    The hot deformation behavior of a KFC copper alloy was studied by compression deformation tests on Gleeble 1500 machine at strain rates ranging between 0.01-10 s-1 and deformation temperature of 650-850 ℃, and associated structural changes were studied by observations of metallography and TEM. The results show that the true stress-true strain curves for a KFC copper alloy are characterized by multiple peaks or a single peak flow, and tend to a steady state at high strains. The peak stress can be represented by a Zener-Hollomon parameter in the hyperbolic-sine-type equation with the hot deformation activation energy Q of 289 kJ/mol. The dynamic recrystallization(DRX) occurs by bulging out of part serrated grain-boundary, and the dynamic recrystallization grain size is dependent sensitively on deformation temperature T and strain rate ε, also a function of Z. The dynamic spherical Fe-rich precipitates and successive dynamic particles coarsening has been assumed to be responsible for flow softening at high strains, and this is more effective when samples deformed at low temperatures and higher strain rates.

  3. Effects of Compression Parameters on Deformation Behaviors of Semi-Solid ZA27 Alloys

    Institute of Scientific and Technical Information of China (English)

    CHEN Ti-jun; HAO Yuan; SUN Jun

    2003-01-01

    An investigation was performed on the effects of semi-solid compression parameters,such as strain rate,compression temperature and heating time at these temperatures on deformation behaviors of two kinds of ZA27 alloys,one was modified by Zr and the other was unmodified.The results indicate that with the increasing of the strain,the stress of the modified composite first sharply increases to a peak value,then dramatically decreases to a plateau value,and again increases till the end of deformation.But for the unmodified,after being up to a peak value,the stress only decreases slowly.As the compression temperature or the heating time decreases,or the strain rate increases,the stress level and the cracking degree of these two kinds of alloys increase.Under the same deformation conditions,the stress level and the cracking degree of the unmodified alloy are higher than those of the modified one.But there is an exception that the stress level of the unmodified alloy is minimum and smaller than that of the modified one when deformed at the low temperature of 450℃.These phenomena were mainly discussed through analyzing the microstructures under different conditions and the deformation mechanisms at different deformation stages.

  4. Use of multiscale zirconium alloy deformation models in nuclear fuel behavior analysis

    Science.gov (United States)

    Montgomery, Robert; Tomé, Carlos; Liu, Wenfeng; Alankar, Alankar; Subramanian, Gopinath; Stanek, Christopher

    2017-01-01

    Accurate prediction of cladding mechanical behavior is a key aspect of modeling nuclear fuel behavior, especially for conditions of pellet-cladding interaction (PCI), reactivity-initiated accidents (RIA), and loss of coolant accidents (LOCA). Current approaches to fuel performance modeling rely on empirical constitutive models for cladding creep, growth and plastic deformation, which are limited to the materials and conditions for which the models were developed. To improve upon this approach, a microstructurally-based zirconium alloy mechanical deformation analysis capability is being developed within the United States Department of Energy Consortium for Advanced Simulation of Light Water Reactors (CASL). Specifically, the viscoplastic self-consistent (VPSC) polycrystal plasticity modeling approach, developed by Lebensohn and Tomé [1], has been coupled with the BISON engineering scale fuel performance code to represent the mechanistic material processes controlling the deformation behavior of light water reactor (LWR) cladding. A critical component of VPSC is the representation of the crystallographic nature (defect and dislocation movement) and orientation of the grains within the matrix material and the ability to account for the role of texture on deformation. A future goal is for VPSC to obtain information on reaction rate kinetics from atomistic calculations to inform the defect and dislocation behavior models described in VPSC. The multiscale modeling of cladding deformation mechanisms allowed by VPSC far exceed the functionality of typical semi-empirical constitutive models employed in nuclear fuel behavior codes to model irradiation growth and creep, thermal creep, or plasticity. This paper describes the implementation of an interface between VPSC and BISON and provides initial results utilizing the coupled functionality.

  5. Modeling the deformation behavior of nanocrystalline alloy with hierarchical microstructures

    Energy Technology Data Exchange (ETDEWEB)

    Liu, Hongxi; Zhou, Jianqiu, E-mail: zhouj@njtech.edu.cn [Nanjing Tech University, Department of Mechanical Engineering (China); Zhao, Yonghao, E-mail: yhzhao@njust.edu.cn [Nanjing University of Science and Technology, Nanostructural Materials Research Center, School of Materials Science and Engineering (China)

    2016-02-15

    A mechanism-based plasticity model based on dislocation theory is developed to describe the mechanical behavior of the hierarchical nanocrystalline alloys. The stress–strain relationship is derived by invoking the impeding effect of the intra-granular solute clusters and the inter-granular nanostructures on the dislocation movements along the sliding path. We found that the interaction between dislocations and the hierarchical microstructures contributes to the strain hardening property and greatly influence the ductility of nanocrystalline metals. The analysis indicates that the proposed model can successfully describe the enhanced strength of the nanocrystalline hierarchical alloy. Moreover, the strain hardening rate is sensitive to the volume fraction of the hierarchical microstructures. The present model provides a new perspective to design the microstructures for optimizing the mechanical properties in nanostructural metals.

  6. Mechanical problems of superplastic fill-forming bulge solved by one-dimensional tensile and two-dimensional free bulging constitutive equations

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Because of the strong structural sensitivity of superplasticity, the deformation rule must be affected by stress-state. It is necessary to prove whether one-dimensional tensile constitutive equation can be directly generalized to deal with the two-dimensional mechanical problems or not. In this paper, theoretical results of fill-forming bulge have been derived from both one-dimensional tensile and two-dimensional bulging constitutive equation with variable m value. By comparing theoretical analysis and experimental results made on typical superplastic alloy Zn-wt22%Al, it is shown that one-dimensional tensile constitutive equation cannot be directly generalized to deal with two-dimensional mechanical questions. A method to correct deviation between theoretical and experimental results is also proposed.

  7. Investigation on the viscoelastic behaviors of a circular dielectric elastomer membrane undergoing large deformation

    Directory of Open Access Journals (Sweden)

    Bing Wang

    2016-12-01

    Full Text Available To explore the time-dependent dissipative behaviors of a circular dielectric elastomer membrane subject to force and voltage, a viscoelastic model is formulated based on the nonlinear theory for dissipative dielectrics. The circular membrane is attached centrally to a light rigid disk and then connected to a fixed rigid ring. When subject to force and voltage, the membrane deforms into an out-of plane shape, undergoing large deformation. The governing equations to describe the large deformation are derived by using energy variational principle while the viscoelasticity of the membrane is describe by a two-unit spring-dashpot model. The evolutions of the considered variables and the deformed shape are illustrated graphically. In calculation, the effects of the voltage and the pre-stretch on the electromechanical behaviors of the membrane are examined and the results show that they significantly influence the electromechanical behaviors of the membrane. It is expected that the present model may provide some guidelines in the design and application of such dielectric elastomer transducers.

  8. Deformation behavior of a high strength multiphase steel at macro- and micro-scales

    Energy Technology Data Exchange (ETDEWEB)

    Diego-Calderón, I. de, E-mail: irenedediego.calderon@imdea.org [IMDEA Materials Institute, Calle Eric Kandel 2, Getafe 28906, Madrid (Spain); Santofimia, M.J. [Department of Materials Science and Engineering, Delft University of Technology, 2628 CD Delft (Netherlands); Molina-Aldareguia, J.M.; Monclús, M.A.; Sabirov, I. [IMDEA Materials Institute, Calle Eric Kandel 2, Getafe 28906, Madrid (Spain)

    2014-08-12

    Advanced high strength steels via quenching and partitioning (Q and P) process are a mainstream trend in modern steel research. This work contributes to a better understanding of their local mechanical properties and local deformation behavior at the micro-scale in relation to their local microstructure. A low alloyed steel was subjected to Q and P heat treatments leading to the formation of complex multiphase microstructures. Nanoindentation tests were performed to measure nanohardness of individual phases and to generate 2D maps showing nanohardness distribution on the surface of the material. To study local in-plane plastic strain distribution during deformation, in situ tensile tests were carried out using the digital image correlation technique. Significant partitioning of plastic strain between phase microconstituents during tensile deformation is shown. The effect of the microstructure on the mechanical behavior of the Q and P processed steel is analyzed. The local plastic deformation behavior of individual phases is discussed with respect to their strength and their spatial orientation.

  9. Investigation on the viscoelastic behaviors of a circular dielectric elastomer membrane undergoing large deformation

    Science.gov (United States)

    Wang, Bing; Wang, Zhengang; He, Tianhu

    2016-12-01

    To explore the time-dependent dissipative behaviors of a circular dielectric elastomer membrane subject to force and voltage, a viscoelastic model is formulated based on the nonlinear theory for dissipative dielectrics. The circular membrane is attached centrally to a light rigid disk and then connected to a fixed rigid ring. When subject to force and voltage, the membrane deforms into an out-of plane shape, undergoing large deformation. The governing equations to describe the large deformation are derived by using energy variational principle while the viscoelasticity of the membrane is describe by a two-unit spring-dashpot model. The evolutions of the considered variables and the deformed shape are illustrated graphically. In calculation, the effects of the voltage and the pre-stretch on the electromechanical behaviors of the membrane are examined and the results show that they significantly influence the electromechanical behaviors of the membrane. It is expected that the present model may provide some guidelines in the design and application of such dielectric elastomer transducers.

  10. Deformation Behavior of Recycled Concrete Aggregate during Cyclic and Dynamic Loading Laboratory Tests

    Directory of Open Access Journals (Sweden)

    Wojciech Sas

    2016-09-01

    Full Text Available Recycled concrete aggregate (RCA is a relatively new construction material, whose applications can replace natural aggregates. To do so, extensive studies on its mechanical behavior and deformation characteristics are still necessary. RCA is currently used as a subbase material in the construction of roads, which are subject to high settlements due to traffic loading. The deformation characteristics of RCA must, therefore, be established to find the possible fatigue and damage behavior for this new material. In this article, a series of triaxial cyclic loading and resonant column tests is used to characterize fatigue in RCA as a function of applied deviator stress after long-term cyclic loading. A description of the shakedown phenomenon occurring in the RCA and calculations of its resilient modulus (Mr as a function of fatigue are also presented. Test result analysis with the stress-life method on the Wohler S-N diagram shows the RCA behavior in accordance with the Basquin law.

  11. Low Cycle Fatigue Behavior of 316LN Stainless Steel Alloyed with Varying Nitrogen Content. Part I: Cyclic Deformation Behavior

    Science.gov (United States)

    Prasad Reddy, G. V.; Sandhya, R.; Sankaran, S.; Mathew, M. D.

    2014-10-01

    In this study, the influence of cyclic strain amplitude on the evolution of cyclic stress-strain response and the associated cyclic deformation mechanisms in 316LN stainless steel with varying nitrogen content (0.07 to 0.22 wt pct) is reported in the temperature range 773 K to 873 K (500 °C to 600 °C). Two mechanisms, namely dynamic strain aging and secondary cyclic hardening, are found to strongly influence the cyclic stress response. Deformation substructures associated with both the mechanisms showed planar mode of deformation. These mechanisms are observed to be operative over certain combinations of temperature and strain amplitude. For strain amplitudes >0.6 pct, wavy or mixed mode of deformation is noticed to suppress both the mechanisms. Cyclic stress-strain curves revealed both single and dual-slope behavior depending on the test temperature. Increase in nitrogen content is found to increase the tendency toward planar mode of deformation, while increase in strain amplitude leads to transition from planar slip bands to dislocation cell/wall structure formation, irrespective of the nitrogen content in 316LN stainless steel.

  12. Tensile behavior of Sn-0.7Cu with Zn addition at various deformation temperatures

    Institute of Scientific and Technical Information of China (English)

    Zhongbing LUO; Jie ZHAO; Junshan ZHANG; Lai WANG

    2011-01-01

    The tensile behavior of Sn-0.7Cu and Sn-0.7Cu-lZn was compared at various deformation temperatures. Refined microstructure and γ-CuZn particles were discovered with Zn addition. The strengths of Zn-containing solder were higher than that of Sn-0.7Cu at room and subzero temperatures. With the elevation of deformation temperature, they both decreased and they were nearly the same at 80 ℃. The works of fracture exhibited the similar evolution law. For Sn-0.7Cu solder, the elongation after fracture was smaller and the reduction of area was bigger than those of Sn-0.7Cu-1Zn. This shows that Zn addition improved the deformation stability, which is attributed to the modification of the microstructure. Dimples in fracture surface became smaller and shallower with the decreasing temperature. Ductile fracture was discovered in all the samples.

  13. Altering strength and plastic deformation behavior via alloying and laminated structure in nanocrystalline metals

    Energy Technology Data Exchange (ETDEWEB)

    Gu, C. [State Key Laboratory for Mechanical Behavior of Material, Xi' an Jiaotong University, Xi' an 710049 (China); Wang, F., E-mail: wangfei@mail.xjtu.edu.cn [State Key Laboratory for Strength and Vibration of Mechanical Structures, Xi' an Jiaotong University, Xi' an 710049 (China); Huang, P., E-mail: huangping@mail.xjtu.edu.cn [State Key Laboratory for Mechanical Behavior of Material, Xi' an Jiaotong University, Xi' an 710049 (China); Lu, T.J. [State Key Laboratory for Strength and Vibration of Mechanical Structures, Xi' an Jiaotong University, Xi' an 710049 (China); MOE Key Laboratory for Multifunctional Materials and Structures, Xi' an Jiaotong University, Xi' an 710049 (China); Xu, K.W. [State Key Laboratory for Mechanical Behavior of Material, Xi' an Jiaotong University, Xi' an 710049 (China)

    2015-07-29

    Nanoindentation and electron microscope techniques have been performed on sputtering deposited monolayered nanocrystalline CuNb and multilayered CuNb/Cu thin films. Microstructural features, hardness and surface morphologies of residual indentation have been evaluated to identify the effects of alloying and laminated structure on strength and plastic deformation behavior of nanocrystalline metals. By altering the content of Nb in CuNb alloy and adding crystalline Cu layers into CuNb alloy, the volume fraction of amorphous phase in CuNb alloy and interface structures changed dramatically, resulting in various trends that are related to hardness, indentation induced pileup and shear banding deformation. Based on the experimental results, the dominant deformation mechanisms of the CuNb and CuNb/Cu thin films with various Nb contents were proposed and extended to be discussed.

  14. Hot Deformation Behavior and Dynamic Recrystallization of Medium Carbon LZ50 Steel

    Science.gov (United States)

    Du, Shiwen; Chen, Shuangmei; Song, Jianjun; Li, Yongtang

    2017-01-01

    Hot deformation and dynamic recrystallization behaviors of a medium carbon steel LZ50 were systematically investigated in the temperature range from 1143 K to 1443 K (870 °C to 1170 °C) at strain rates from 0.05 to 3s-1 using a Gleeble-3500 thermo-simulation machine. The flow stress constitutive equation for hot deformation of this steel was developed with the two-stage Laasraoui equation. The activation energy of the tested steel was 304.27 KJ/mol, which was in reasonable agreement with those reported previously. The flow stress of this steel in hot deformation was mainly controlled by dislocation climb during their intragranular motion. The effect of Zener-Hollomon parameter on the characteristic points of the flow curves was studied, and the dependence of critical strain on peak strain obeyed a linear equation. Dynamic recrystallization was the most important softening mechanism for the tested steel during hot deformation. Kinetic equation of this steel was also established based on the flow stress. The austenite grain size of complete dynamic recrystallization was a power law function of Zener-Hollomon parameter with an exponent of -0.2956. Moreover, the microstructures induced under different deformation conditions were analyzed.

  15. Hot Deformation Behavior and Dynamic Recrystallization of Medium Carbon LZ50 Steel

    Science.gov (United States)

    Du, Shiwen; Chen, Shuangmei; Song, Jianjun; Li, Yongtang

    2017-03-01

    Hot deformation and dynamic recrystallization behaviors of a medium carbon steel LZ50 were systematically investigated in the temperature range from 1143 K to 1443 K (870 °C to 1170 °C) at strain rates from 0.05 to 3s-1 using a Gleeble-3500 thermo-simulation machine. The flow stress constitutive equation for hot deformation of this steel was developed with the two-stage Laasraoui equation. The activation energy of the tested steel was 304.27 KJ/mol, which was in reasonable agreement with those reported previously. The flow stress of this steel in hot deformation was mainly controlled by dislocation climb during their intragranular motion. The effect of Zener-Hollomon parameter on the characteristic points of the flow curves was studied, and the dependence of critical strain on peak strain obeyed a linear equation. Dynamic recrystallization was the most important softening mechanism for the tested steel during hot deformation. Kinetic equation of this steel was also established based on the flow stress. The austenite grain size of complete dynamic recrystallization was a power law function of Zener-Hollomon parameter with an exponent of -0.2956. Moreover, the microstructures induced under different deformation conditions were analyzed.

  16. Deformation behavior of metallic glasses with shear band like atomic structure: a molecular dynamics study.

    Science.gov (United States)

    Zhong, C; Zhang, H; Cao, Q P; Wang, X D; Zhang, D X; Ramamurty, U; Jiang, J Z

    2016-08-02

    Molecular dynamics simulations were employed to investigate the plastic deformation within the shear bands in three different metallic glasses (MGs). To mimic shear bands, MG specimens were first deformed until flow localization occurs, and then the volume of the material within the localized regions was extracted and replicated. Homogeneous deformation that is independent of the size of the specimen was observed in specimens with shear band like structure, even at a temperature that is far below the glass transition temperature. Structural relaxation and rapid cooling were employed to examine the effect of free volume content on the deformation behavior. This was followed by detailed atomic structure analyses, employing the concepts of Voronoi polyhedra and "liquid-like" regions that contain high fraction of sub-atomic size open volumes. Results suggest that the total fraction of atoms in liquid-like regions is a key parameter that controls the plastic deformation in MGs. These are discussed in the context of reported experimental results and possible strategies for synthesizing monolithic amorphous materials that can accommodate large tensile plasticity are suggested.

  17. Closed Die Deformation Behavior of Cylindrical Iron-Alumina Metal Matrix Composites During Cold Sinter Forging

    Science.gov (United States)

    Prasanna Kumar, Undeti Jacob; Gupta, Pallav; Jha, Arun Kant; Kumar, Devendra

    2016-10-01

    The present paper aims to study the closed die deformation behavior of cylindrical Fe-Al2O3 metal matrix composites (MMCs). Closed die was manufactured by machining the high carbon steel block followed by oil quenching and then finishing. Samples sintered at a temperature of 1100 °C for 1 h were characterized with X-ray diffraction and scanning electron microscopy, which showed the formation of Fe, Al2O3 and nano size FeAl2O4 phases respectively. Density and hardness of the composite samples were determined after sintering. Closed die deformation studies of the prepared composite samples were carried under three different interfacial frictional conditions i.e. dry, solid lubricating and liquid lubricating. Hardness, density and metallographic characterizations were also done for the deformed samples. On comparing the micrographs of the samples before and after deformation it was revealed that in deformed specimens recrystallization has taken place due to the difference in the energy between the strained iron matrix and unstrained alumina reinforcement during closed die forging process. Experimental density of the samples was also verified with the theoretical density using the standard equations. It is expected that the results of the present investigations will be helpful in developing quality MMC components for wide industrial applications.

  18. Effect of Cu concentration on the semi-solid deformation behavior and microstructure of Ti–Cu alloy

    Directory of Open Access Journals (Sweden)

    Yong-Nan Chen

    2015-05-01

    Full Text Available The semi-solid compressive deformation behavior of Ti–Cu alloys was investigated by Gleeble-3500 hot simulator at the deformation temperatures ranging from 1273 to 1473 K with strain rates ranging from 5×10−3 to 5×10−1 s−1. The relationship between Cu concentration and flow stress was analyzed, and the deformation apparent activation energy was also calculated. The results show that Cu concentration has significant influence on the flows’ behavior of Ti–Cu alloys, especially at high semi-solid deformation temperatures. The Ti–14Cu exhibits the highest flow stress at 1273 and 1373 K, Ti–2.5Cu alloy exhibits the highest flow stress at 1473 K, and Ti–7Cu alloy shows the lowest flow stress at all tested temperatures, which corresponds to liquid fraction caused by varied Cu concentration and the deformation temperature. The difference in microstructure suggests that the shape and distribution of Ti2Cu precipitates are significantly affected by Cu concentration. The increase in Cu concentration leads to the growth and precipitation of acicular Ti2Cu along grain boundaries at high semi-solid deformation temperatures. The deformation apparent activation energy of Ti–14Cu alloy significantly decreases from solid deformation to semi-solid deformation owing to the change in main deformation mechanism from plastic deformation of solid particles to solid particles’ slippage and rotation of grain boundaries.

  19. Effect of Nb content on deformation behavior and shape memory properties of Ti–Nb alloys

    Energy Technology Data Exchange (ETDEWEB)

    Tobe, H. [Division of Materials Science, University of Tsukuba, Tsukuba, Ibaraki 305-8573 (Japan); Kim, H.Y., E-mail: heeykim@ims.tsukuba.ac.jp [Division of Materials Science, University of Tsukuba, Tsukuba, Ibaraki 305-8573 (Japan); Inamura, T.; Hosoda, H. [Precision and Intelligence Laboratory, Tokyo Institute of Technology, Yokohama 226-8503 (Japan); Nam, T.H. [School of Materials Science and Engineering and ERI, Gyeongsang National University, 900 Gazwadong, Jinju, Gyeongnam 660-701 (Korea, Republic of); Miyazaki, S., E-mail: miyazaki@ims.tsukuba.ac.jp [Division of Materials Science, University of Tsukuba, Tsukuba, Ibaraki 305-8573 (Japan); School of Materials Science and Engineering and ERI, Gyeongsang National University, 900 Gazwadong, Jinju, Gyeongnam 660-701 (Korea, Republic of); Center of Excellence for Advanced Materials Research, King Abdulaziz University, P.O. Box 80203, Jeddah 21589 (Saudi Arabia)

    2013-11-15

    Highlights: ► Reorientation of martensite variants occurred by the deformation of the {1 1 1} type I and 〈2 1 1〉 type II twins. ► Magnitude of twinning shear in Ti–20Nb is larger than that in Ti–23Nb. ► Ti–20Nb exhibited a higher stress for the reorientation of martensite variants when compared with Ti–23Nb. -- Abstract: Deformation behavior and shape memory properties of Ti–(20, 23) at.% Nb alloys in a single α″ martensite state were investigated. The Ti–20Nb alloy exhibited a higher stress for the reorientation of martensite variants when compared with the Ti–23Nb alloy. The recovery strain due to the shape memory effect in the Ti–20Nb alloy was smaller than that in the Ti–23Nb alloy. Transmission electron microscope (TEM) observation revealed that the reorientation of martensite variants occurred by the deformation of {1 1 1} type I and 〈2 1 1〉 type II twins. The Nb content dependence of the deformation behavior and shape memory properties was discussed considering the magnitude of twinning shear of the twins.

  20. Effect of Deformation Mode on the Wear Behavior of NiTi Shape Memory Alloys

    Science.gov (United States)

    Yan, Lina; Liu, Yong

    2016-06-01

    Owing to good biocompatibility, good fatigue resistance, and excellent superelasticity, various types of bio-medical devices based on NiTi shape memory alloy (SMA) have been developed. Due to the complexity in deformation mode in service, for example NiTi implants, accurate assessment/prediction of the surface wear process is difficult. This study aims at providing a further insight into the effect of deformation mode on the wear behavior of NiTi SMA. In the present study, two types of wear testing modes were used, namely sliding wear mode and reciprocating wear mode, to investigate the effect of deformation mode on the wear behavior of NiTi SMA in both martensitic and austenitic states. It was found that, when in martensitic state and under high applied loads, sliding wear mode resulted in more surface damage as compared to that under reciprocating wear mode. When in austenitic state, although similar trends in the coefficient of friction were observed, the coefficient of friction and surface damage in general is less under reciprocating mode than under sliding mode. These observations were further discussed in terms of different deformation mechanisms involved in the wear tests, in particular, the reversibility of martensite variant reorientation and stress-induced phase transformation, respectively.

  1. Friction role in deformation behaviors of high-strength TA18 tubes in numerical control bending

    Science.gov (United States)

    Fang, Jun; Liang, Chuang; Lu, Shiqiang; Wang, Kelu; Zheng, Deliang

    2017-09-01

    In order to reveal the friction role in deformation behaviors of high-strength TA18 tubes in numerical control (NC) bending, a three dimensional (3D) elastic-plastic finite element (FE) model of high-strength TA18 tubes for whole process in NC bending was established based on ABAQUS code, and its reliability was validated by the experimental results in literature. Then, the bending deformation behaviors under different friction coefficients between tube and various dies were studied with respect to multiple defects such as wall thinning, wall thickening and cross section deformation. The results show that the wall thinning ratio and cross section deformation ratio increase with the increase of the friction coefficient between mandrel and tube f m or decrease of the friction coefficient between pressure die and tube f p, while the friction coefficient between bending die and tube f b has no obvious effect on these. The wall thickening ratio decreases with the increase of f b, f m or decrease of f p.

  2. Hot Deformation Behavior of SiCP/A1-Cu Composite

    Directory of Open Access Journals (Sweden)

    CHENG Ming-yang

    2017-02-01

    Full Text Available Using the Gleeble-1500D simulator, the high temperature plastic deformation behavior of SiCp/Al-Cu composite were investigated at 350-500℃ with the strain rate of 0.01-10s-1. The true stress-strain curves were obtained in the tests. Constitutive equation and processing map were established. The results show that the softening mechanism of dynamic recrystallization is a feature of high-temperature flow stress-strain curves of SiCp/A1-Cu composite, and the peak stress increases with the decrease of deformation temperature or the increase of strain rate.The flow stress behavior of the composite during hot compression deformation can be represented by a Zener-Hollomon parameter in the hyperbolic sine form. Its activation energy for hot deformation Q is 320.79kJ/mol. The stable regions and the instability regions in the processing map were identified and the microstructures in different regions of processing map were studied.There are particle breakage and void in the instability regions.

  3. Low temperature deformation behavior of an electromagnetically bulged 5052 aluminum alloy

    Science.gov (United States)

    Li, Zu; Li, Ning; Wang, Duzhen; Ouyang, Di; Liu, Lin

    2016-07-01

    The fundamental understanding of the deformation behavior of electromagnetically formed metallic components under extreme conditions is important. Here, the effect of low temperature on the deformation behavior of an electromagnetically-bulged 5052 aluminum alloy was investigated through uniaxial tension. We found that the Portevin-Le Chatelier Effect, designated by the serrated characteristic in stress-strain curves, continuously decays until completely disappears with decreasing temperature. The physical origin of the phenomenon is rationalized on the basis of the theoretical analysis and the Monte Carlo simulation, which reveal an increasing resistance to dislocation motion imposed by lowering temperature. The dislocations are captured completely by solute atoms at ‑50 °C, which results in the extinction of Portevin-Le Chatelier. The detailed mechanism responsible for this process is further examined through Monte Carlo simulation.

  4. Deformation behavior of release agent coated glass fibre / epoxy composite using carbon nanotubes as strain sensors

    Directory of Open Access Journals (Sweden)

    Paweena Sureeyatanapas

    2013-02-01

    Full Text Available The deformation behavior of model glass fiber in epoxy composites has been studied using Raman spectroscopyproperties. Single walled carbon nanotubes (SWNTs were introduced at the glass fiber/epoxy interface as strain sensors,which can be detected by Raman Spectroscopy, to sense the strain profile of the fiber under deformation. The release agentwas applied on the fiber surface before composite fabrication. It was found that at high strain level, the behavior of a singlefiber in a composite did not follow a classical shear-lag model as shown in the fragmentation study. This is due to the interfacial failure caused by the release agent. The strain mapping result can be compared to that without release agent coating.The finding confirmed the application of SWNTs as strain sensors at the fiber/composite interface.

  5. Corrosion behavior of HPT-deformed TiNi alloys in cell culture medium

    Science.gov (United States)

    Shri, D. N. Awang; Tsuchiya, K.; Yamamoto, A.

    2017-09-01

    In recent years there are growing interest in fabrication of bulk nanostructured metals and alloys by using severe plastic deformation (SPD) techniques as new alternative in producing bulk nanocrystalline materials. These techniques allows for processing of bulk, fully dense workpiece with ultrafine grains. Metal undergoes SPD processing in certain techniques such as high pressure torsion (HPT), equal-channel angular pressing (ECAP) or multi-directional forging (MDF) are subjected to extensive hydrostatic pressure that may be used to impart a very high strain to the bulk solid without the introduction of any significant change in overall dimension of the sample. The change in the structure (small grain size and high-volume fraction of grain boundaries) of the material may result in the corrosion behavior different from that of the coarse-grained material. Electrochemical measurements were done to understand the corrosion behavior of TiNi alloys before and after HPT deformation. The experiment was carried out using standard three electrode setup (a sample as working electrode; a platinum wire as a counter electrode and a saturated calomel electrode in saturated KCl as a reference electrode) with the surface area of 26.42 mm2 exposed to the EMEM+10% FBS cell culture medium. The measurements were performed in an incubator with controlled environment at 37 °C and 5% CO2, simulating the cell culture condition. The potential of the specimen was monitored over 1 hour, and the stabilized potential was used as the open-circuit potential (EOCP). Potentiodynamic curves were scanned in the potential range from -0.5 V to 1.5 V relative to the EOCP, at a rate of 0.5 mV/s. The result of OCP-time measurement done in the cell culture medium shows that the OCP of HPT-deformed samples shifts towards to the more positive rather than that of BHPT samples. The OCP of deformed samples were ennobled to more than +70 mV for Ti-50mol%. The shift of OCP towards the nobler direction

  6. Effects of friction stir processing on the microstructure and superplasticity of in situ nano-ZrB2/2024Al composite

    Directory of Open Access Journals (Sweden)

    Yutao Zhao

    2016-02-01

    Full Text Available In this study, in situ nano-ZrB2/2024Al composites fabricated from 2024Al–K2ZrF6–KBF4 system were processed by friction stir processing (FSP to achieve superplasticity of the composites. And the effects of particle contents (1 wt%, 3 wt%, 5 wt%, matrix grain size (micron or sub-micron, strain rates (5×10−3 s−1, 1×10−2 s−1, 2×10−2 s−1 and deformation temperatures (400 K, 480 K, 600 K, 700 K, 750 K on the superplasticity of the composites were investigated. After the friction stir processing, the coarse grains of the cast composites with matrix grain size of about 80–100 μm and nano-ZrB2 reinforcement size of 30–100 nm were crushed into small grains about 1 μm in size, and the uniformity of the nano-ZrB2 reinforcements was also improved. And under the same superplastic tensile testing condition at the temperature of 750 K and strain rate of 5×10−3 s−1, the FSP nano 3 wt%ZrB2/2024Al composite exhibited an superplastic elongation of 292.5%, while the elongation of the corresponding cast composite was only less than 100%. Meanwhile, the m values of the FSP composites were always higher than the cast composites, especially the FSP composites with 3 wt% particles has the m value of 0.5321 i.e., the FSP composites should had better superplastic properties than cast ones. Furthermore, the FSP composites had higher apparent deformation activation energy (Q than that of the lattice diffusion of pure aluminium, indicating that the deformation mechanisms of the FSP composites should be grain boundary sliding mechanisms.

  7. Specimen- and grain-size dependence of compression deformation behavior in nanocrystalline copper

    OpenAIRE

    Okamoto, Norihiko L.; Kashioka, Daisuke; Hirato, Tetsuji; Inui, Haruyuki

    2014-01-01

    The compression deformation behavior of electrodeposited nanocrystalline copper pillars with average grain sizes (d) of 360, 100, and 34 nm has been investigated as a function of specimen size (D). The yield stress for nanocrystalline pillars with d = 360 and 100 nm does not depend on specimen size, exhibiting essentially the bulk yield stress until the specimen size is reduced down to the critical values ((D/d)∗ = 35 and 85), below which the yield stress decreases with the decrease in specim...

  8. BASIC STUDY ON TENSION SOFTENING AND CYCLIC DEFORMATION BEHAVIOR OF SOLIDIFIED BODY FOR THE COHESIVE SOIL

    Science.gov (United States)

    Urano, Kazuhiko; Adachi, Yuji; Mihara, Masaya; Yamada, Atsuo; Kawamura, Makoto

    So far, authors have proposed a method to improve earthquake resistance of pile foundations by partially solidifying an underground part of the pile foundations, and the effect of reinforcement has been confirmed by shaking table tests and the lateral loading tests of a full scale model. Though the solidified body is usually designed as an elastic body, it is possible to design the body considering the damage by the tensile stress when a seismic ground motion is assumed to be level 2. Therefore, material tests of the solidified body for the cohesive soil were executed, and the characteristics of the tension softening and the cyclic deformation behavior of the solidified bod y were clarified. Moreover, loading tests that used wall models of the solidified body were executed, and the effects of the shape on the tension softening and the cyclic deformation behavior of the solidified body were clarified. In addition, a numerical simulation by elastoplastic FEM analysis that considers the damage of the solidified body was executed, and the tension softening and the cyclic deformation behavior of the solidified body were reproduced.

  9. Hot Deformation Behavior and Processing Maps of 2099 Al-Li Alloy

    Science.gov (United States)

    Chen, Bin; Tian, Xiao-lin; Li, Xiao-ling; Lu, Chen

    2014-06-01

    Hot deformation behavior and processing maps of the 2099 Al-Li alloy are investigated by tensile test at the temperature range from 250 to 450 °C and the strain rate range from 0.001 to 5.0 s-1. The typical true stress-true strain curves show that the flow stress increases with increasing the strain rate and decreasing the deforming temperature. All curves exhibit rapid work hardening at an initial stage of strain followed by remarkable dynamic softening. Based on the flow stress behavior, the processing maps are calculated and analyzed according to the dynamic materials model (DMM). The processing maps exhibit an instability domain in the temperature and strain rate ranges: T = 250-260 °C and = 0.1-0.5 s-1. The maps also exhibit an optimum hot working condition in the stability domain that occurs in the temperature of 400 °C for a strain rate of 0.001 s-1 and having a maximum efficiency of 60%. The microstructural examinations exhibit the occurrence of dynamic recovery (DRV) during hot deformation of the 2099 alloy which is the dominant softening mechanism in the alloy. The fracture behavior changes from a brittle fracture to a ductile fracture as strain rate decreases and temperature increases.

  10. Hot deformation behavior of an aluminum-matrix hybrid nanocomposite fabricated by friction stir processing

    Energy Technology Data Exchange (ETDEWEB)

    Khodabakhshi, F. [Department of Materials Science and Engineering, Sharif University of Technology, P.O. Box 11365-9466, Azadi Avenue, 14588 Tehran (Iran, Islamic Republic of); Department of Mechanical and Mechatronics Engineering, University of Waterloo, Waterloo, ON (Canada); Gerlich, A.P. [Department of Mechanical and Mechatronics Engineering, University of Waterloo, Waterloo, ON (Canada); Simchi, A., E-mail: simchi@sharif.edu [Department of Materials Science and Engineering, Sharif University of Technology, P.O. Box 11365-9466, Azadi Avenue, 14588 Tehran (Iran, Islamic Republic of); Institute for Nanoscience and Nanotechnology, Sharif University of Technology, P.O. Box 11365-9466, Azadi Avenue, 14588 Tehran (Iran, Islamic Republic of); Kokabi, A.H. [Department of Materials Science and Engineering, Sharif University of Technology, P.O. Box 11365-9466, Azadi Avenue, 14588 Tehran (Iran, Islamic Republic of)

    2015-02-25

    A fine-grained aluminum-matrix hybrid nanocomposite reinforced with TiO{sub 2}, MgO and Al{sub 3}Ti nanoparticles was prepared via reactive friction stir processing (FSP) of an Al–Mg sheet with pre-placed TiO{sub 2} particles (50 nm; 3.1 vol%). The microstructure of the hybrid nanocomposite comprises high-angle grain boundaries (~90%) with an average size of 2 µm and hard inclusions with sizes in the range of 30–50 nm. Evaluation of the hot deformation behavior of the nanocomposite by uniaxial tensile testing at different temperatures (300–450 °C) and strain rates (0.001–0.1 s{sup −1}) shows that the deformation apparent activation energy of the nanocomposite is 137 kJ mol{sup −1} at ≤300 °C. The values of the activation energy for the Al–Mg alloy before and after FSP at this temperature range are about 105 and 135 kJ mol{sup −1}, respectively. This observation highlights the role of ultrafine hard particles and the structural changes induced by FSP on the deformation process. At the higher temperatures, the deformation activation energy for the aluminum alloy without and with the reinforcing particles is 303 and 456 kJ mol{sup −1}, respectively. Detailed microstructural analysis by electron back scattered diffraction and transmission electron microscopy suggests that dynamic recrystallization is responsible for the deformation behavior at the elevated temperatures. Meanwhile, the presence of the hard nanoparticles operates as a grain growth inhibitor improving the thermal stability of the fine-grained aluminum alloy.

  11. Influence of adhesive shear deformation on laminate structural behavior with application to parabolic trough solar collectors

    Science.gov (United States)

    Clauss, D. B.; Reuter, R. C., Jr.

    1983-02-01

    A simplified theory for the bending behavior of a thin flat bilamina panel was developed which includes the effects of shear deformation in the central adhesive layer. Static equilibrium equations for elastic thermomechanical cylindrical bending of a thin plate are used. A solution form is proposed which greatly facilitates application of this theory to structural panels with numerous discrete property changes in the variable direction. The influence of adhesive shear stiffness parameters upon overall laminate behavior is characterized through numerical examples typifying various thermal and mechanical loading conditions.

  12. Deformation Behavior of Sub-micron and Micron Sized Alumina Particles in Compression.

    Energy Technology Data Exchange (ETDEWEB)

    Sarobol, Pylin; Chandross, Michael E.; Carroll, Jay; Mook, William; Boyce, Brad; Kotula, Paul Gabriel; McKenzie, Bonnie Beth; Bufford, Daniel Charles; Hall, Aaron Christopher.

    2014-09-01

    The ability to integrate ceramics with other materials has been limited due to high temperature (>800degC) ceramic processing. Recently, researchers demonstrated a novel process , aerosol deposition (AD), to fabricate ceramic films at room temperature (RT). In this process, sub - micro n sized ceramic particles are accelerated by pressurized gas, impacted on the substrate, plastically deformed, and form a dense film under vacuum. This AD process eliminates high temperature processing thereby enabling new coatings and device integration, in which ceramics can be deposited on metals, plastics, and glass. However, k nowledge in fundamental mechanisms for ceramic particle s to deform and form a dense ceramic film is still needed and is essential in advancing this novel RT technology. In this wo rk, a combination of experimentation and atomistic simulation was used to determine the deformation behavior of sub - micron sized ceramic particle s ; this is the first fundamental step needed to explain coating formation in the AD process . High purity, singl e crystal, alpha alumina particles with nominal size s of 0.3 um and 3.0 um were examined. Particle characterization, using transmission electron microscopy (TEM ), showed that the 0.3 u m particles were relatively defect - free single crystals whereas 3.0 u m p articles were highly defective single crystals or particles contained low angle grain boundaries. Sub - micron sized Al 2 O 3 particles exhibited ductile failure in compression. In situ compression experiments showed 0.3um particles deformed plastically, fractured, and became polycrystalline. Moreover, dislocation activit y was observed within the se particles during compression . These sub - micron sized Al 2 O 3 particles exhibited large accum ulated strain (2 - 3 times those of micron - sized particles) before first fracture. I n agreement with the findings from experimentation , a tomistic simulation s of nano - Al 2 O 3 particles showed dislocation slip and

  13. Assessment of Tungsten Content on Tertiary Creep Deformation Behavior of Reduced Activation Ferritic-Martensitic Steel

    Science.gov (United States)

    Vanaja, J.; Laha, Kinkar

    2015-10-01

    Tertiary creep deformation behavior of reduced activation ferritic-martensitic (RAFM) steels having different tungsten contents has been assessed. Creep tests were carried out at 823 K (550 °C) over a stress range of 180 to 260 MPa on three heats of the RAFM steel (9Cr-W-0.06Ta-0.22V) with tungsten content of 1, 1.4, and 2.0 wt pct. With creep exposure, the steels exhibited minimum in creep rate followed by progressive increase in creep rate until fracture. The minimum creep rate decreased, rupture life increased, and the onset of tertiary stage of creep deformation delayed with the increase in tungsten content. The tertiary creep behavior has been assessed based on the relationship, , considering minimum creep rate () instead of steady-state creep rate. The increase in tungsten content was found to decrease the rate of acceleration of tertiary parameter ` p.' The relationships between (1) tertiary parameter `p' with minimum creep rate and time spent in tertiary creep deformation and (2) the final creep rate with minimum creep rate revealed that the same first-order reaction rate theory prevailed in the minimum creep rate as well as throughout the tertiary creep deformation behavior of the steel. A master tertiary creep curve of the steels has been developed. Scanning electron microscopic investigation revealed enhanced coarsening resistance of carbides in the steel on creep exposure with increase in tungsten content. The decrease in tertiary parameter ` p' with tungsten content with the consequent decrease in minimum creep rate and increase in rupture life has been attributed to the enhanced microstructural stability of the steel.

  14. Hot deformation and dynamic recrystallization behaviors of Mg–Gd–Y–Zr alloy

    Energy Technology Data Exchange (ETDEWEB)

    Xiao, H.C. [School of Materials Science and Engineering, Central South University, Changsha 410083 (China); Jiang, S.N., E-mail: shnjiang@csu.edu.cn [School of Materials Science and Engineering, Central South University, Changsha 410083 (China); School of Civil Engineering, Central South University, Changsha 410083 (China); Tang, B.; Hao, W.H.; Gao, Y.H.; Chen, Z.Y.; Liu, C.M. [School of Materials Science and Engineering, Central South University, Changsha 410083 (China)

    2015-03-25

    Hot deformation and dynamic recrystallization (DRX) behaviors of Mg–8.3Gd–2.6Y–0.4Zr alloy were investigated by uniaxial compression tests conducted at temperatures ranging from 300 °C to 500 °C and strain rates varying from 0.001 s{sup −1} to 1 s{sup −1}. The results reveal that the alloy exhibits a high deformability due to the DRX softening when the temperature is >400 °C. Apart from the premature failure at relative low temperatures, the stress–strain curves exhibit typical features of DRX that the flow stress presents a peak and then gradually declines to a steady-state. Optical microscopy examinations exhibit that DRX takes place dominantly either at twin boundaries or initial grain boundaries depending on the deformation conditions. With increasing temperature or decreasing strain rate, the DRX sites would transfer from the twin boundaries to initial grain boundaries gradually. The analysis of transmission electron microscopy (TEM) images indicates that the deformation is controlled by basal slip and twinning in the temperature range of 300–350 °C, continuous DRX associated with the operation of multiple slips plays a dominant role when temperature is >400 °C.

  15. Elastodynamic shape modeler: a tool for defining the deformation behavior of virtual tissues.

    Science.gov (United States)

    Radetzky, A; Nürnberger, A; Pretschner, D P

    2000-01-01

    A main goal of surgical simulators is the creation of virtual training environments for prospective surgeons. Thus, students can rehearse the various steps of surgical procedures on a computer system without any risk to the patient. One main condition for realistic training is the simulated interaction with virtual medical devices, such as endoscopic instruments. In particular, the virtual deformation and transection of tissues are important. For this application, a neuro-fuzzy model has been developed, which allows the description of the visual and haptic deformation behavior of the simulated tissue by means of expert knowledge in the form of medical terms. Pathologic conditions affecting the visual and haptic tissue response can be easily changed by a medical specialist without mathematical knowledge. By using the personal computer-based program Elastodynamic Shape Modeler, these conditions can be adjusted via a graphical user interface. With a force feedback device, which is similar to a real laparoscopic instrument, virtual deformations can be performed and the resulting haptic feedback can be felt. Thus, use of neuro-fuzzy technologies for the definition and calculation of virtual deformations seems applicable to the simulation of surgical interventions in virtual environments.

  16. High temperature deformation behavior and processing map for a nickel-titanium shape memory alloy

    Science.gov (United States)

    Yin, Xiang-Qian; Lee, Sang-Won; Li, Yan-Feng; Park, Chan-Hee; Mi, Xu-Jun; Yeom, Jong-Taek

    2017-09-01

    The hot deformation behavior of 49.2Ti-50.8Ni shape memory alloy was studied using hot compressive deformation testing in the temperature range of 1023-1323 K and at strain rates of 0.01-10 s-1. The work-hardening rate was induced to analyze the stress-strain curves, and the critical stress σc and the dynamic recovery saturation stress σsat were measured which can be specified approximately by the expressions: σsat-1.12σp and σc-0.86σp. An Arrhenius model was calculated to describe the relationship between peak stress and the Z parameter. The relationship between deformation activation energy, the deformation conditions and the effect of Ni component in a binary TiNi alloy on the activation energy were discussed in this work. With the help of electron backscattering diffraction, a connected mode dynamic recrystallization microstructure was confirmed in peak efficiency regimes (850 °C & 0.01 s-1 and 1050 °C & 10 s-1) of the processing map.

  17. Effects of Initial Microstructure Characteristics on Hot Deformation Behaviors of 2E12 Aluminum Alloy

    Directory of Open Access Journals (Sweden)

    PAN Su-ping

    2016-11-01

    Full Text Available Three alloys with different microstructure characteristics were prepared, which microstructures were characterized as enriched with eutectics, supersaturated solid solution and coarse precipitates. Combined isothermal hot compression test and microstructure observation, the hot deformation behaviors of three alloys were studied in the temperature range of 340-490℃ and strain rate range of 0.001-10s-1. The results show initial microstructure characteristics have significant influences on the hot deformation of alloys. Among three alloys, the alloy enriched with coarse precipitates has the largest peak stress value while the alloy enriched with eutectics has the smallest one. The flow behaviors of three alloys were described by the hyperbolic sine constitutive equations. The deformation activation energy for three alloys calculated to be 178.6, 222.1, 154.9kJ/mol, respectively. The processing maps were calculated and analyzed according to the dynamic materials model. Among three alloys, the alloy enriched with coarse precipitates has the widest processing range while the alloy enriched with eutectics has the narrowest one.

  18. Hot-Deformation Behavior and Hot-Processing Maps of AISI 410 Martensitic Stainless Steel

    Science.gov (United States)

    Qi, Rong-Sheng; Jin, Miao; Guo, Bao-Feng; Liu, Xin-Gang; Chen, Lei

    2016-10-01

    The compressive deformation behaviors of 410 martensitic stainless steel were investigated on a Gleeble-1500 thermomechanical simulator, and the experimental stress-strain data were obtained. The measured flow stress was corrected for friction and temperature. A constitutive equation that accounts for the influence of strain was established, and the hot-processing maps at different strain were plotted. The microstructure evolution of the hot-deformation process was studied on the basis of microstructural observations at high temperatures. Phase-transformation experiments on 410 steel were conducted at high temperatures to elucidate the effects of temperature on the delta-ferrite content. The initial forging temperature and optimum process parameters were obtained on the basis of the processing map and the changes in the delta-ferrite content at high temperatures.

  19. Modelling the viscoplastic behavior and the heterogeneous intracrystalline deformation of columnar ice polycrystals

    Energy Technology Data Exchange (ETDEWEB)

    Lebensohn, Ricardo A [Los Alamos National Laboratory; Montagnat, Maurine [LGGE (FRANCE); Mansuy, Philippe [MICHELIN (FRANCE); Duval, Paul [LGGE (FRANCE); Philip, A [LGGE (FRANCE)

    2008-01-01

    A full-field formulation based on Fast Fourier Transforms (FFT) has been adapted and used to predict the micromechanical fields that develop in columnar Ih ice polycrystals deforming in compression by dislocation creep. The predicted intragranular mechanical fields are in qualitative good agreement with experimental observations, in particular those involving the formation of shear and kink bands. These localization bands are associated with the large internal stresses that develop during creep in such anisotropic material, and their location, intensity, morphology and extension are found to depend strongly on the crystallographic orientation of the grains and on their interaction with neighbor crystals. The predictions of the model are also discussed in relation with the deformation of columnar sea and lake ice, and with the mechanical behavior of granular ice of glaciers and polar ice sheets, as well.

  20. Quasi-static Torsional Deformation Behavior of Porous Ti6Al4V alloy.

    Science.gov (United States)

    Balla, Vamsi Krishna; Martinez, Shantel; Rogoza, Ben Tunberg; Livingston, Chase; Venkateswaran, Deepak; Bose, Susmita; Bandyopadhyay, Amit

    2011-07-20

    Laser processed Ti6Al4V alloy samples with total porosities of 0%, 10% and 20% have been subjected to torsional loading to determine mechanical properties and to understand the deformation behavior. The torsional yield strength and modulus of porous Ti alloy samples was found to be in the range of 185-332 MPa and 5.7-11 GPa, respectively. With an increase in the porosity both the strength and the modulus decreased, and at 20% porosity the torsional modulus of Ti6Al4V alloy was found to be very close to that of human cortical bone. Further, the experiments revealed clear strain hardening and ductile deformation in all the samples, which suggests that the inherent brittleness associated solid-state sintered porous materials can be completely eliminated via laser processing for load bearing metal implant applications.

  1. Hot Deformation Behavior of SA508Gr.4N Steel for Reactor Pressure Vessels

    Directory of Open Access Journals (Sweden)

    YANG Zhi-qiang

    2017-08-01

    Full Text Available The high-temperature plastic deformation and dynamic recrystallization behavior of SA508Gr.4N steel were investigated through hot deformation tests in a Gleeble1500D thermal mechanical simulator. The compression tests were performed in the temperature range of 1050-1250℃ and the strain rate range of 0.001-0.1s-1 with true strain of 0.16. The results show that from the high-temperature true stress-strain curves of the SA508Gr.4N steel, the main feature is dynamic recrystallization,and the peak stress increases with the decrease of deformation temperature or the increase of strain rate, indicating the experimental steel is temperature and strain rate sensitive material. The constitutive equation for SA508Gr.4N steel is established on the basis of the true stress-strain curves, and exhibits the characteristics of the high-temperature flow behavior quite well, while the activation energy of the steel is determined to be 383.862kJ/mol. Furthermore, an inflection point is found in the θ-σ curve, while the -dθ/dσ-σ curve shows a minimum value. The critical strain increases with increasing strain rate and decreasing deformation temperature. A linear relationship between critical strain (εc and peak strain (εp is found and could be expressed as εc/εp=0.517. The predicted model of critical strain could be described as εc=8.57×10-4Z0.148.

  2. Boronization and Carburization of Superplastic Stainless Steel and Titanium-Based Alloys

    Directory of Open Access Journals (Sweden)

    Masafumi Matsushita

    2011-07-01

    Full Text Available Bronization and carburization of fine-grain superplastic stainless steel is reviewed, and new experimental results for fine grain Ti88.5Al4.5V3Fe2Mo2 are reported. In superplastic duplex stainless steel, the diffusion of carbon and boron is faster than in non-superplastic duplex stainless steel. Further, diffusion is activated by uniaxial compressive stress. Moreover, non-superplastic duplex stainless steel shows typical grain boundary diffusion; however, inner grain diffusion is confirmed in superplastic stainless steel. The presence of Fe and Cr carbides or borides is confirmed by X-ray diffraction, which indicates that the diffused carbon and boron react with the Fe and Cr in superplastic stainless steel. The Vickers hardness of the carburized and boronized layers is similar to that achieved with other surface treatments such as electro-deposition. Diffusion of boron into the superplastic Ti88.5Al4.5V3Fe2Mo2 alloy was investigated. The hardness of the surface exposed to boron powder can be increased by annealing above the superplastic temperature. However, the Vickers hardness is lower than that of Ti boride.

  3. Modeling of stress relaxation of a semi-crystalline multiblock copolymer and its deformation behavior.

    Science.gov (United States)

    Yan, Wan; Fang, Liang; Heuchel, Matthias; Kratz, Karl; Lendlein, Andreas

    2015-01-01

    Stress relaxation can strongly influence the shape-memory capability of polymers. Recently a modified Maxwell-Wiechert model comprising two Maxwell units and a single spring unit in parallel has been introduced to successfully describe the shape recovery characteristics of amorphous polyether urethanes. In this work we explored whether such a modified Maxwell-Wiechert model is capable to describe the stress relaxation behavior of a semi-crystalline multiblock copolymer named PCL-PIBMD, which consists of crystallizable poly(ɛ-caprolactone) (PCL) segments and crystallizable poly(3S-isobutylmorpholine-2,5-dione) (PIBMD) segments. The stress relaxation behavior of PCL-PIBMD was explored after uniaxial deformation to different strains ranging from 50 to 900% with various strain rates of 1 or 10 or 50 mm·min -1. The modeling results indicated that under the assumption that in PCL-PIBMD both PCL and PIBMD blocks have narrow molecular weight distributions and are arranged in sequence, the two relaxation processes can be related to the amorphous PCL and PIBMD domains and the spring element can be associated to the PIBMD crystalline domains. The first Maxwell unit representing the faster relaxation process characterized by the modulus E1 and the relaxation time τ1 is related to the amorphous PCL domains (which are in the rubbery state), while the second Maxwell unit (E2 ; τ2) represents the behavior of the amorphous PIBMD domains, which are in the glassy state at 50 °C. Increasing strain rates resulted in an increase of E1 and a significant reduction in τ1, whereas the elastic modulus as well as the relaxation time related to the amorphous PIBMD domains remained almost constant. When a higher deformation was applied (ɛ ≥ 200% ) lower values for the elastic moduli of the three model elements were obtained. In general the applied model was also capable to describe the relaxation behavior of PCL-PIBMD at a deformation temperature of 20 °C, where additional crystalline

  4. Time-dependent deformation behavior of polyvinylidene fluoride binder: Implications on the mechanics of composite electrodes

    Science.gov (United States)

    Santimetaneedol, Arnuparp; Tripuraneni, Rajasekhar; Chester, Shawn A.; Nadimpalli, Siva P. V.

    2016-11-01

    The majority of existing battery models that simulate composite electrode behavior assume the binder as a linear elastic material due to lack of a thorough understanding of time-dependent mechanical behavior of binders. Here, thin films of polyvinylidene fluoride binder, prepared according to commercial battery manufacturing method, are subjected to standard monotonic, load-unload, and relaxation tests to characterize the time-dependent mechanical behavior. The strain in the binder samples is measured with the digital image correlation technique to eliminate experimental errors. The experimental data showed that for (charging/discharging) time scales of practical importance, polyvinylidene fluoride behaves more like an elastic-viscoplastic material as opposed to a visco-elastic material; based on this observation, a simple elastic-viscoplastic model, calibrated against the data is adopted to represent the deformation behavior of binder in a Si-based composite electrode; the lithiation/delithiation process of this composite was simulated at different C rates and the stress/strain behavior was monitored. It is observed that the linear elastic assumption of the binder leads to inaccurate results and the time-dependent constitutive behavior of the binder not only leads to accurate prediction of the mechanics but is an essential step towards developing advanced multi-physics models for simulating the degradation behavior of batteries.

  5. Finite Element Simulation in Superplastic forming of Friction Stir Welded Aluminium Alloy 6061-T6

    Directory of Open Access Journals (Sweden)

    P Ganesh

    2011-09-01

    Full Text Available Superplasticity in materials is the ability of materials to achieve large elongation only under specific conditions of temperature and strain rate. Superplastic Forming (SPF is an important industrial process that has found application in sheet metal forming in the aerospace and automotive industries. Friction Stir Welding (FSW is a solid state joining process that can alter the grain structure of the parent material. FSW process is an effective tool to refine the grain structure of the sheet metal and enhance their Superplasticity. Friction Stir Welding was used to join Superplastic AA 6061-T6 sheets. The Finite Element Simulation was performed for the Superplastic Forming of the Friction Stir Welded joints to evaluate the thinning and formability of AA 6061-T6 for hemispherical shape. The commercially available Finite Element Software ABAQUS was used to execute these simulations.

  6. Understanding compressive deformation behavior of porous Ti using finite element analysis

    Energy Technology Data Exchange (ETDEWEB)

    Roy, Sandipan; Khutia, Niloy [Department of Aerospace Engineering and Applied Mechanics, Indian Institute of Engineering Science and Technology, Shibpur (India); Das, Debdulal [Department of Metallurgy and Materials Engineering, Indian Institute of Engineering Science and Technology, Shibpur (India); Das, Mitun, E-mail: mitun@cgcri.res.in [Bioceramics and Coating Division, CSIR-Central Glass and Ceramic Research Institute, Kolkata (India); Balla, Vamsi Krishna [Bioceramics and Coating Division, CSIR-Central Glass and Ceramic Research Institute, Kolkata (India); Bandyopadhyay, Amit [W. M. Keck Biomedical Materials Research Laboratory, School of Mechanical and Materials Engineering, Washington State University, Pullman, WA 99164 (United States); Chowdhury, Amit Roy, E-mail: arcbesu@gmail.com [Department of Aerospace Engineering and Applied Mechanics, Indian Institute of Engineering Science and Technology, Shibpur (India)

    2016-07-01

    In the present study, porous commercially pure (CP) Ti samples with different volume fraction of porosities were fabricated using a commercial additive manufacturing technique namely laser engineered net shaping (LENS™). Mechanical behavior of solid and porous samples was evaluated at room temperature under quasi-static compressive loading. Fracture surfaces of the failed samples were analyzed to determine the failure modes. Finite Element (FE) analysis using representative volume element (RVE) model and micro-computed tomography (CT) based model have been performed to understand the deformation behavior of laser deposited solid and porous CP-Ti samples. In vitro cell culture on laser processed porous CP-Ti surfaces showed normal cell proliferation with time, and confirmed non-toxic nature of these samples. - Highlights: • Porous CP-Ti samples fabricated using additive manufacturing technique • Compressive deformation behavior of porous samples closely matches with micro-CT and RVE based analysis • In vitro studies showed better cell proliferation with time on porous CP-Ti surfaces.

  7. Deformation Behavior and TExture Evolution of Steel Alloys under Axial-Torsional Loading

    Energy Technology Data Exchange (ETDEWEB)

    Siriruk, A.; Kant, M.; Penumadu, D.; Garlea, E.; Vogel, S.

    2011-06-01

    Using hollow cylinder samples with suitable geometry obtained from round bar stock, the deformation behavior of bcc Fe based 12L14 steel alloy is evaluated under multi-axial conditions. A stacked strain gage rosette and extensometer mounted on the cylindrical surface at the mid height of the specimen provided strain tensor as a function of applied stress for pure tensile and torsion tests prior to yielding. This study examines elastic and yield behavior and effects of these with respect to texture evolution. Hollow cylinder specimen geometry (tubes) with small wall thickness and relatively (to its thickness) large inner diameter is used. The variation of observed yield surface in deviatoric plane and the effect on mode of deformation (tension versus torsion versus its combination) on stress-strain behavior is discussed. Bulk texture was studied using neutron time-of-flight diffractometer at High-Pressure-Preferred Orientation (HIPPO) - Los Alamos Neutron Science Center (LANSCE) instrument and the evolution of texture and related anisotropy for pure tension versus torsion are also included.

  8. An Explicit Approach Toward Modeling Thermo-Coupled Deformation Behaviors of SMPs

    Directory of Open Access Journals (Sweden)

    Hao Li

    2017-03-01

    Full Text Available A new elastoplastic J 2 -flow models with thermal effects is proposed toward simulating thermo-coupled finite deformation behaviors of shape memory polymers. In this new model, an elastic potential evolving with development of plastic flow is incorporated to characterize the stress-softening effect at unloading and, moreover, thermo-induced plastic flow is introduced to represent the strain recovery effect at heating. It is shown that any given test data for both effects may be accurately simulated by means of direct and explicit procedures. Numerical examples for model predictions compare well with test data in literature.

  9. Precipitation behavior in a nitride-strengthened martensitic heat resistant steel during hot deformation

    Directory of Open Access Journals (Sweden)

    Wenfeng Zhang

    2015-09-01

    Full Text Available The stress relaxation curves for three different hot deformation processes in the temperature range of 750–1000 °C were studied to develop an understanding of the precipitation behavior in a nitride-strengthened martensitic heat resistant steel (Zhang et al., Mater. Sci. Eng. A, 2015 [1]. This data article provides supporting data and detailed information on how to accurately analysis the stress relaxation data. The statistical analysis of the stress peak curves, including the number of peaks, the intensity of the peaks and the integral value of the pumps, was carried out. Meanwhile, the XRD energy spectrum data was also calculated in terms of lattice distortion.

  10. A molecular mechanics approach for analyzing tensile nonlinear deformation behavior of single-walled carbon nanotubes

    Institute of Scientific and Technical Information of China (English)

    Yu Wang; Daining Fang; Ai Kah Soh; Bin Liu

    2007-01-01

    In this paper, by capturing the atomic informa-tion and reflecting the behaviour governed by the nonlin-ear potential function, an analytical molecular mechanics approach is proposed. A constitutive relation for single-walled carbon nanotubes (SWCNT's) is established to describe the nonlinear stress-strain curve of SWCNT's and to predict both the elastic properties and breaking strain of SWCNT's during tensile deformation. An analysis based on the virtual internal bond (VIB) model proposed by P. Zhang et al. is also presented for comparison. The results indicate that the proposed molecular mechanics approach is indeed an acceptable analytical method for analyzing the mechanical behavior of SWCNT's.

  11. Laser deposition and deformation behavior of Ti-Nb-Zr-Ta alloys for orthopedic implants.

    Science.gov (United States)

    Nag, S; Banerjee, R

    2012-12-01

    Microstructure and mechanical properties of laser deposited complex quaternary Ti-34Nb-7Zr-7Ta (all wt%), an orthopedic load-bearing implant alloy, has been investigated in detail in both as-deposited as well as heat-treated (β-solutionized and quenched) conditions. The difference in stress-strain behavior of this alloy in the above conditions has been characterized using scanning electron microscopy (SEM), orientation imaging microscopy (OIM™) and transmission electron microscopy (TEM). Compared to the sample in heat-treated condition, the as-deposited sample showed evidence of strong growth related texture. Again in the as-deposited post tensile-tested condition formation of a high density of shear bands, possibly arising from slip localization due to shearing of ω precipitates in the β matrix is observed. TEM investigations also show the presence of lenticular shaped deformation induced ω phase within the shear bands. In contrast, in case of the β-solutionized sample, twinning and the formation of stress-induced plates appears to be the primary mode of deformation. The change in deformation mechanism and thus the tensile property of this alloy could be attributed to the crystallographic texture along the growth direction as well as diffusion mediated isothermal ω precipitates, that cause an enrichment of Nb and Ta in the β matrix, during the laser-deposition process. This is no longer present after the solutionizing treatment. Copyright © 2012 Elsevier Ltd. All rights reserved.

  12. Bonding Behavior of Deformed Steel Rebars in Sustainable Concrete Containing both Fine and Coarse Recycled Aggregates.

    Science.gov (United States)

    Kim, Sun-Woo; Park, Wan-Shin; Jang, Young-Il; Jang, Seok-Joon; Yun, Hyun-Do

    2017-09-14

    In order to assess the bond behavior of deformed steel rebars in recycled-aggregate concrete (RAC) incorporating both fine and coarse recycled aggregate, pull-out tests were carried out in this study on 16-mm diameter deformed steel rebars embedded concentrically in RAC. The concrete was designed using equivalently mixed proportions of both recycled coarse aggregate and recycled fine aggregate. The tests employed five types of recycled aggregate replacement combinations and three types of rebar placement orientation (i.e., vertical bars and two-tiered and three-tiered horizontal bars). Based on the pull-out test results, the maximum bond strength tended to decrease and the slip at the maximum bond strength increased as the average water absorption of the aggregate increased, irrespective of the rebar orientation or placement location within the concrete member. The pull-out test results for the horizontal steel rebars embedded in RAC indicate that the casting position effect could be determined from the mid-depth of the concrete member, irrespective of the member's height. The normalized bond versus slip relationship between the deformed rebar and the RAC could be predicted using an empirical model based on regression analysis of the experimental data.

  13. Hot Deformation Behavior of 1Cr12Ni3Mo2VN Martensitic Stainless Steel

    Science.gov (United States)

    He, Xiaomao; Jiang, Peng; Zhou, Leyu; Chen, Chao; Deng, Xiaochun

    2017-08-01

    1Cr12Ni3Mo2VN is a new type of martensitic stainless steel for the last-stage blades of large-capacity nuclear and thermal power turbines. The deformation behavior of this steel was studied by thermal compression experiments that performed on a Gleeble-3500 thermal simulator at a temperature range of 850°C to 1200°C and a strain rate of 0.01s-1 to 20s-1. When the deformation was performed at high temperature and low strain rate, a necklace type of microstructures was observed, the plastic deformation mechanism is grain boundary slip and migration, when at low temperature and lower strain rate, the slip bands were observed, the mechanism is intracrystalline slips, and when at strain rate of 20s-1, twins were observed, the mechanism are slips and twins. The Arrhenius equation was applied to describe the constitutive equation of the flow stress. The accuracy of the equation was verified by using the experimental data and the correlation coefficient R2 = 0.9786, and the equation can provide reasonable data for the design and numerical simulation of the forging process.

  14. The deformation behavior of solid polymers and modeling with the viscoplasticity theory based on overstress

    Science.gov (United States)

    Khan, Fazeel Jilani

    The inelastic deformation of six engineering polymers has been investigated with the desideratum being a thorough mapping of the mechanical response characteristics and the subsequent application of a state-variable based constitutive material model to the data. Materials included in the investigation were polycarbonate (PC), Nylon 66, high-density polyethylene (HDPE), polyethylene-terephthalate (PET), polyethersulfone (PES) and polyphenylene oxide (PPO). Cylindrical specimens were machined from as-received rod stock. The use of a servo-hydraulic test frame with control mode switching capability has permitted data collection under strain and load controlled test configurations. In the region of homogeneous deformation with strain typically less than 10%, during loading all materials have been found to exhibit, (i) positive non-linear rate sensitivity in loading, (ii) the magnitude of the response in creep, relaxation and recovery tests varies non-linearly with changes in the prior loading rate, and (iii) in the inelastic flow region the stress drop in relaxation has been found to be independent of the test strain value. In addition to these findings, perhaps the most singular deformation response has been in the instance of relaxation (creep) during unloading when the rate of change of stress (strain) may undergo a change in sign. This phenomenon has been labeled 'rate reversal' and has surfaced in tensile and compression load conditions. The preponderance of data, therefore, suggests that the amorphous versus crystalline distinction does not largely manifest itself in the qualitative nature of the deformation behavior. This finding endorses the competence of macro-based models to undertake the task of polymer deformation modeling. Common response characteristics such as positive strain rate sensitivity, monotonic decreases in the stress magnitude in a relaxation test (strain hold), and response during creep have been modeled well with the existing viscoplasticity

  15. Hot Ductility and Compression Deformation Behavior of TRIP980 at Elevated Temperatures

    Science.gov (United States)

    Zhang, Mei; Li, Haiyang; Gan, Bin; Zhao, Xue; Yao, Yi; Wang, Li

    2017-04-01

    The hot ductility tests of a kind of 980 MPa class Fe-0.31C (wt pct) TRIP steel (TRIP980) with the addition of Ti/V/Nb were conducted on a Gleeble-3500 thermomechanical simulator in the temperatures ranging from 873 K to 1573 K (600 °C to 1300 °C) at a constant strain rate of 0.001 s-1. It is found that the hot ductility trough ranges from 873 K to 1123 K (600 °C to 850 °C). The recommended straightening temperatures are from 1173 K to 1523 K (900 °C to 1250 °C). The isothermal hot compression deformation behavior was also studied by means of Gleeble-3500 in the temperatures ranging from 1173 K to 1373 K (900 °C to 1100 °C) at strain rates ranging from 0.01 s-1 to 10 s-1. The results show that the peak stress decreases with the increasing temperature and the decreasing strain rate. The deformation activation energy of the test steel is 436.7 kJ/mol. The hot deformation equation of the steel has been established, and the processing maps have been developed on the basis of experimental data and the principle of dynamic materials model (DMM). By analyzing the processing maps of strains of 0.5, 0.7, and 0.9, it is found that dynamic recrystallization occurs in the peak power dissipation efficiency domain, which is the optimal area of hot working. Finally, the factors influencing hot ductility and thermal activation energy of the test steel were investigated by means of microscopic analysis. It indicates that the additional microalloying elements play important roles both in the loss of hot ductility and in the enormous increase of deformation activation energy for the TRIP980 steel.

  16. Ghost spins and quantum critical behavior in a spin chain with local bond deformation

    Science.gov (United States)

    Dai, Jianhui; Wang, Yupeng; Eckern, U.

    1999-09-01

    We study the impurity-induced critical behavior in an integrable SU(2)-invariant model consisting of an open spin chain of arbitrary spin S (Takhatajian-Babujian model) interacting with an impurity of spin S-->' located at one of the boundaries. For S=1/2 or S'=1/2, the impurity interaction takes a very simple form JS-->1.S-->' that describes the deformed boundary bond between the impurity S-->' and the first bulk spin S-->1 with an arbitrary coupling strength J. For a weak coupling 0S, and S'=J0/[(S+S')2-1/4], the impurity spin is split into two ghost spins. Their cooperative effect leads to a variety of new critical behaviors with different values of \\|S'-S\\|.

  17. Hot deformation behavior of a spray-deposited AZ31 magnesium alloy

    Institute of Scientific and Technical Information of China (English)

    LI Yongbing; CHEN Yunbo; CUI Hua; DING Jie; ZUO Lingli; ZHANG Jishan

    2009-01-01

    The flow stress behavior of an as-spray-deposited AZ31 magnesium alloy with fine grains was investigated by means of compression tests with a Gleeble 1500 thermal mechanical simulator at isothermal constant strain rates of 0.01, 0.1, 1.0, and 10 s-1; the testing temperatures ranged from 623 to 723 K. It is demonstrated that a linear equation can be fitted between the Zemer-Hollomon parameter Z and stress in a double-log scale. The effect of deformation parameters on the behavior of recrystallization was analyzed. Dynamic recrystallization (DRX) generally occurs at a higher temperature and at a lower strain rate. The constitutive equation of the spray-deposited AZ31 magnesium alloy is elevated temperatures due to the fine grain, which provides a large amount of nucleation sites and a high-diffnsivity path for the atom.

  18. Effective-stress-law behavior of Austin chalk rocks for deformation and fracture conductivity

    Energy Technology Data Exchange (ETDEWEB)

    Warpinski, N.R.; Teufel, L.W.

    1994-08-01

    Austin chalk core has been tested to determine the effective law for deformation of the matrix material and the stress-sensitive conductivity of the natural fractures. For deformation behavior, two samples provided data on the variations of the poroelastic parameter, {alpha}, for Austin chalk, giving values around 0.4. The effective-stress-law behavior of a Saratoga limestone sample was also measured for the purpose of obtaining a comparison with a somewhat more porous carbonate rock. {alpha} for this rock was found to be near 0.9. The low {alpha} for the Austin chalk suggests that stresses in the reservoir, or around the wellbore, will not change much with changes in pore pressure, as the contribution of the fluid pressure is small. Three natural fractures from the Austin chalk were tested, but two of the fractures were very tight and probably do not contribute much to production. The third sample was highly conductive and showed some stress sensitivity with a factor of three reduction in conductivity over a net stress increase of 3000 psi. Natural fractures also showed a propensity for permanent damage when net stressed exceeded about 3000 psi. This damage was irreversible and significantly affected conductivity. {alpha} was difficult to determine and most tests were inconclusive, although the results from one sample suggested that {alpha} was near unity.

  19. Modeling of high homologous temperature deformation behavior for stress and life-time analyses

    Energy Technology Data Exchange (ETDEWEB)

    Krempl, E. [Rensselaer Polytechnic Institute, Troy, NY (United States)

    1997-12-31

    Stress and lifetime analyses need realistic and accurate constitutive models for the inelastic deformation behavior of engineering alloys at low and high temperatures. Conventional creep and plasticity models have fundamental difficulties in reproducing high homologous temperature behavior. To improve the modeling capabilities {open_quotes}unified{close_quotes} state variable theories were conceived. They consider all inelastic deformation rate-dependent and do not have separate repositories for creep and plasticity. The viscoplasticity theory based on overstress (VBO), one of the unified theories, is introduced and its properties are delineated. At high homologous temperature where secondary and tertiary creep are observed modeling is primarily accomplished by a static recovery term and a softening isotropic stress. At low temperatures creep is merely a manifestation of rate dependence. The primary creep modeled at low homologous temperature is due to the rate dependence of the flow law. The model is unaltered in the transition from low to high temperature except that the softening of the isotropic stress and the influence of the static recovery term increase with an increase of the temperature.

  20. Evaluation of Dynamic Deformation Behaviors in Metallic Materials under High Strain-Rates Using Taylor Bar Impact Test

    Energy Technology Data Exchange (ETDEWEB)

    Bae, Kyung Oh; Shin, Hyung Seop [Andong National Univ., Andong (Korea, Republic of)

    2016-09-15

    To ensure the reliability and safety of various mechanical systems in accordance with their high-speed usage, it is necessary to evaluate the dynamic deformation behavior of structural materials under impact load. However, it is not easy to understand the dynamic deformation behavior of the structural materials using experimental methods in the high strain-rate range exceeding 10{sup 4} s{sup -1}. In this study, the Taylor bar impact test was conducted to investigate the dynamic deformation behavior of metallic materials in the high strain-rate region, using a high-speed photography system. Numerical analysis of the Taylor bar impact test was performed using AUTODYN S/W. The results of the analysis were compared with the experimental results, and the material behavior in the high strain-rate region was discussed.

  1. Deformation behavior of metastable β-type Ti-25Nb-2Mo-4Sn alloy for biomedical applications.

    Science.gov (United States)

    Guo, S; Meng, Q K; Cheng, X N; Zhao, X Q

    2014-10-01

    The deformation behavior of metastable β-type Ti-25Nb-2Mo-4Sn (wt%) alloy subjected to different thermo-mechanical treatments was discussed by the combining results from transmission electron microscope, tensile test and in-situ synchrotron X-ray diffraction. Visible "double yielding" behavior, which is characterized by the presence of stress-plateau, was observed in the solution treated specimen. Upon a cold rolling treatment, the Ti-25Nb-2Mo-4Sn alloy performs nonlinear deformation because of the combined effects of elastic deformation and stress-induced α″ martensitic transformation. After the subsequent annealing, the β phase is completely stabilized and no stress-induced martensitic transformation takes place on loading due to the inhibitory effect of grain boundaries and dislocations on martensitic transformation. As a result, the annealed specimen exhibits linear elastic deformation.

  2. Microscale Mechanical Deformation Behaviors and Mechanisms in Bulk Metallic Glasses Investigated with Micropillar Compression Experiments

    Science.gov (United States)

    Ye, Jianchao

    2011-12-01

    Over the past years of my PhD study, the focused-ion-beam (FIB) based microcompression experiment has been thoroughly investigated with respect to the small-scale deformation in metallic glasses. It was then utilized to explore the elastic and plastic deformation mechanisms in metallic glasses. To this end, micropillars with varying sample sizes and aspect ratios were fabricated by the FIB technique and subsequently compressed on a modified nanoindentation system. An improved formula for the measurement of the Young's modulus was derived by adding a geometrical prefactor to the Sneddon's solution. Through the formula, geometry-independent Young's moduli were extracted from microcompression experiments, which are consistent with nanoindentation results. Furthermore, cyclic microcompression was developed, which revealed reversible inelastic deformation in the apparent elastic regime through high-frequency cyclic loading. The reversible inelastic deformation manifests as hysteric loops in cyclic microcompression and can be captured by the Kelvin-type viscoelastic model. The experimental results indicate that the free-volume zones behave essentially like supercooled liquids with an effective viscosity on the order of 1 x 108 Pas. The microscopic yield strengths were first extracted with a formula derived based on the Mohr-Coulomb law to account for the geometrical effects from the tapered micropillar and the results showed a weak size effect on the yield strengths of a variety of metallic-glass alloys, which can be attributed to Weibull statistics. The nature of the yielding phenomenon was explored with the cyclic micro-compression approach. Through cyclic microcompression of a Zr-based metallic glass, it can be demonstrated that its yielding stress increases at higher applied stress rate but its yielding strain is kept at a constant of ~ 2%. The room-temperature post-yielding deformation behavior of metallic glasses is characterized by flow serrations, which were

  3. A Computational Investigation on Bending Deformation Behavior at Various Deflection Rates for Enhancement of Absorbable Energy in TRIP Steel

    Science.gov (United States)

    Pham, Hang Thi; Iwamoto, Takeshi

    2016-08-01

    Transformation-induced plasticity (TRIP) steel might have a high energy-absorption characteristic because it could possibly consume impact energy by not only plastic deformation but also strain-induced martensitic transformation (SIMT) during deformation. Therefore, TRIP steel is considered to be suitable for automotive structures from the viewpoint of safety. Bending deformation due to buckling is one of the major collapse modes of automotive structures. Thus, an investigation on the bending deformation behavior and energy-absorption characteristic in TRIP steel at high deformation rate is indispensable to clarify the mechanism of better performance. Some past studies have focused on the improvement of mechanical properties by means of SIMT; however, the mechanism through which the energy-absorption characteristic in steel can be improved is still unclear. In this study, the three-point bending deformation behavior of a beam specimen made of type-304 austenitic stainless steel, a kind of TRIP steel, is investigated at various deflection rates by experiments and finite-element simulations based on a constitutive model proposed by one of the authors. After confirming the validity of the computation, the rate-sensitivity of energy absorption from the viewpoint of hardening behavior is examined and the improvement of the energy-absorption characteristic in TRIP steel including its mechanism is discussed.

  4. A Composite Modeling Analysis of the Deformation Behavior of Medium Manganese Steels

    Energy Technology Data Exchange (ETDEWEB)

    Rana, Radhakanta [CSM/ASPPRC; Gibbs, Paul J [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); De Moor, Emmanuel [CSM/ASPPRC; Speer, John G [CSM/ASPPRC; Matlock, David K [CSM/ASPPRC

    2014-09-01

    The deformation behavior of medium manganese steels was evaluated with uniaxial tensile testing and the results were correlated with predictions of a composite model shown previously to provide design insight into the development of multi-phase steels with third-generation advanced high strength steel (3GAHSS) properties. An equilibrium thermodynamic-based methodology to design microstructures containing systematic amounts of metastable austenite with controlled stability against transformation is presented. The analysis is based on Mn enrichment of austenite during intercritical annealing of medium Mn (7 and 10 wt pct.) low carbon (0.1 and 0.15 wt pct) steels. The steels were produced as laboratory heats that were hot and cold rolled prior to annealing. After annealing the microstructures consisted primarily of either a matrix of fine grained ferrite with austenite contents between 32.6 and 45.2 wt pct (7Mn, 0.1C steels) or a matrix of martensite with various amounts of austenite in the higher Mn steel. The different intercritical annealing conditions produced steels with wide variations in austenite contents and austenite compositions (Mn and C contents) resulting in steels with significant variations in austenite stability. Predictions based on the composite analysis with different assumed flow behaviors for the individual constituents and stability functions for the meta-stable austenite are presented and shown to accurately predict strength-ductility combinations over a range of austenite volume fractions for the 7Mn steel. Applicability of the composite analysis is extended to consider the deformation behavior of the 10Mn steel and evaluate other possible microstructural combinations leading to 3GAHSS properties.

  5. Deformation behavior and microstructural evolution of 7075-T6 aluminum alloy at cryogenic temperatures

    Science.gov (United States)

    Lee, Woei-Shyan; Lin, Ching-Rong

    2016-10-01

    The impact deformation behavior and associated microstructural evolution of 7075-T6 aluminum alloy at cryogenic temperatures are investigated using a compressive split-Hopkinson pressure bar (SHPB) system. Cylindrical specimens are deformed at strain rates of 1 × 103 s-1, 2 × 103 s-1, 3 × 103 s-1 and 5 × 103 s-1 and temperatures of 0 °C, -100 °C and -196 °C. It is shown that the flow stress is strongly dependent on the strain rate and temperature. For a given temperature, the flow stress varies with the strain rate in accordance with a power law relation with an average exponent of 0.157 and an activation energy of 0.7 kJ/mol. Moreover, the coupled effects of the strain rate and temperature on the flow stress are adequately described by the Zener-Hollomon parameter (Z). For all test temperatures, catastrophic failure occurs only under the highest strain rate of 5 × 103 s-1, and is the result of adiabatic shear. An increasing strain rate or reducing temperature leads to a greater dislocation density and a smaller grain size. Finally, the dependence of the flow stress on the microstructural properties of the impacted 7075-T6 specimens is well described by a specific Hall-Petch constitutive model with constants of K = 108.3 MPa μm1/2 and K‧ = 16.1 MPa μm, respectively. Overall, the results presented in this study provide a useful insight into the combined effects of strain rate and temperature on the flow resistance and deformability of 7075-T6 alloy and confirm that 7075-T6 is well suited to the fabrication of fuel tanks and related structural components in the aerospace field.

  6. High Temperature Creep and Superplasticity in a Mg-Zn-Zr Alloy

    Institute of Scientific and Technical Information of China (English)

    S. Spigarelli; M. El Mehtedi; M. Regev; E. Gariboldi; N. Lecis

    2012-01-01

    Creep and superplasticity were investigated by testing a fine-grained extruded Mg–Zn–Zr magnesium alloy under a wide range of applied stress in the temperature range between 100 and 300 ℃. Grain boundary sliding became the dominating mechanism at 200 ℃, leading to a true superplastic behaviour at 300 ℃, where superplasticity was attained even under relatively high strain rates (5×10-3 s-1 ). By contrast, for lower temperatures, the straining process was controlled by dislocation climb. A comprehensive model, taking into account the simultaneous operation of the different mechanisms, was developed to describe the strain rate dependence on applied stress.

  7. Elastic constants for superplastically formed/diffusion-bonded sandwich structures

    Science.gov (United States)

    Ko, W. L.

    1979-01-01

    Formulae and the associated graphs are presented for contrasting the effective elastic constants for a superplastically formed/diffusion-bonded (SPF/DB) corrugated sandwich core and a honeycomb sandwich core. The results used in the comparison of the structural properties of the two types of sandwich cores are under conditions of equal sandwich density. It was found that the stiffness in the thickness direction of the optimum SPF/DB corrugated core (i.e., triangular truss core) was lower than that of the honeycomb core, and that the former had higher transverse shear stiffness than the latter.

  8. Thermomechanical Processing and Superplasticity of AZ91 Magnesium Alloy

    Institute of Scientific and Technical Information of China (English)

    Rongshi CHEN; J.J. Blandin; M.Suéry; Qudong WANG; Enhou HAN

    2004-01-01

    The effect of extrusion on grain refinement has been studied in the AZ91 cast ingots. It is found that grain size smaller than 10 μm can be obtained by the extrusion processing. Vickers hardness measurements were also carried out to evaluate the effect of these processes on the room temperature mechanical properties. The experimental results of high temperature tensile tests revealed that the stress was inversely proportional to the square of the grain size and that the activation energy for superplastic flow was higher than that for grain boundary diffusion.

  9. Effects of contents of Nb and C on hot deformation behaviors of high Nb X80 pipeline steels

    Institute of Scientific and Technical Information of China (English)

    QIAO Gui-ying; XIAO Fu-ren; ZHANG Xiao-bing; CAO Ya-bin; LIAO Bo

    2009-01-01

    The behavior of the flow deformation and the effects of contents of Nb and C on deformation behaviors of high Nb X80 pipeline steels during hot compression deformation were studied by thermal simulation test.The content of solid solution Nb was quantificationally studied during the reheating and hot deformation process,and the effects of change of solid solution Nb in steels on hot deformation behaviors were discussed.The results show that the contents of Nb and C have great effects on the flow stress behaviors of high Nb X80 pipeline steels.When the C content in steels is constant,the recrystallization activation energy increases from 387 to 481 kJ/mol with increasing the Nb from 0.082% to 0.13% (mass fraction).However,the effect of Nb is correlative to the C content,I.e.w(Nb)/w(C).When w(Nb)/w(C) decreases from 3.61 to 2.18,the recrystallization activation energy decreases from 481 to 434 kJ/mol.

  10. Flow Behavior and Evolution of Microstructure during Hot Deformation for a High Mo Stainless Steel

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    The mechanical behaviors of high Mo austenitic stainless steel 00Cr20Ni18Mo6Cu[N] have been investigated using the methods of hot compression simulation test on the Thermecmaster-Z simulator. The dynamic recrystallization kinetic equation was established, Avrami coefficient n lies in between 0.9~2 depending on deformation parameters. A perfect flow stress model considering dynamic recrystallization was also established. Dynamic recrystallization tends to complete at 1050℃ and high strain rate, but at temperature below 950℃, it is hard to occur. Double-stage interrupt compression tests were carried out. Activation energy for static and metadynamic recrystallization have been obtained respectively (QSRX=483.7, QMDRX=253.5 k J/mol). Avrami coefficient of MDRX is about 0.5, and t0.5-kinetics equations of SRX and MDRX have also been constructed. The evolution of microstructures during interrupt compression deformation was investigated. Static and metadynamic recrystallizationis essential to improve plasticity, at temperature above 1000℃ increasing interpass time has advantage for static and metadynamic recrystallization.

  11. Hot deformation behavior of medium carbon V-N microalloyed steel

    Institute of Scientific and Technical Information of China (English)

    XU Lei; WANG Cheng-yang; LIU Guo-quan; BAI Bing-zhe

    2009-01-01

    Processing maps for a medium carbon V-N microalloyed steel(designated as VN steel) and a medium carbon V-N bared steel(designated as Non-VN steel) were developed to study the hot deformation behavior and the influence of vanadium and nitrogen,in the temperature range of 750-1 100 ℃ and strain rate range of 0.005-30 s~(-1).Experimental results show that the processing map for the VN steel exhibits two dynamic recrystallization and three instability domains,while that for the Non-VN steel has one dynamic recrystallization and three instability domains.The instability domains of VN steel are larger than those of the Non-VN steel,and the VN steel is easier to be unstable when being hot deformed at high temperature and high stain rate.The addition and precipitation of vanadium and nitrogen can hinder the dynamic recrystallization.Compared with the Non-VN steel,the VN steel has higher dynamic recrystallization critical strain and the corresponding stress.

  12. Hot tensile deformation behavior of twin roll casted 7075 aluminum alloy

    Science.gov (United States)

    Wang, Lei; Yu, Huashun; Lee, Yunsoo; Kim, Hyoung-Wook

    2015-09-01

    High temperature deformation behavior of the 7075 aluminum alloy sheets fabricated by twin roll casting and rolling was investigated by hot tensile tests at different temperatures from 350 to 500 °C and various initial strain rates from 1×10-3 to 1×10-2 s-1. The results show that flow stress increased with increasing initial strain rate and decreasing deformation temperature. A large elongation of 200% was obtained at relatively high strain rate of 5×10-3 s-1 at 450 °C. It is closely related with the grain boundary sliding at elevated temperature attributed to the recrystallized fine grains and the large volume fraction of high-angle grain boundaries. The fracture transformation mechanism changes from ductile transgranular fracture to ductile intergranular fracture due to the recrystallized fine grains at high temperature. High density and uniform cavities observed in large elongation samples at high temperature reveals the contribution of grain boundary sliding. Necking-controlled failure mode was characterized by rare cavities with low elongation.

  13. Investigation of Hot Deformation Behavior of Duplex Stainless Steel Grade 2507

    Science.gov (United States)

    Kingklang, Saranya; Uthaisangsuk, Vitoon

    2016-10-01

    Recently, duplex stainless steels (DSSs) are being increasingly employed in chemical, petro-chemical, nuclear, and energy industries due to the excellent combination of high strength and corrosion resistance. Better understanding of deformation behavior and microstructure evolution of the material under hot working process is significant for achieving desired mechanical properties. In this work, plastic flow curves and microstructure development of the DSS grade 2507 were investigated. Cylindrical specimens were subjected to hot compression tests for different elevated temperatures and strain rates by a deformation dilatometer. It was found that stress-strain responses of the examined steel strongly depended on the forming rate and temperature. The flow stresses increased with higher strain rates and lower temperatures. Subsequently, predictions of the obtained stress-strain curves were done according to the Zener-Hollomon equation. Determination of material parameters for the constitutive model was presented. It was shown that the calculated flow curves agreed well with the experimental results. Additionally, metallographic examinations of hot compressed samples were performed by optical microscope using color tint etching. Area based phase fractions of the existing phases were determined for each forming condition. Hardness of the specimens was measured and discussed with the resulted microstructures. The proposed flow stress model can be used to design and optimize manufacturing process at elevated temperatures for the DSS.

  14. Tensile deformation and fracture behavior of CuZn5 brass alloy at high temperature

    Energy Technology Data Exchange (ETDEWEB)

    Sharififar, M., E-mail: m.sharififar@ut.ac.ir; Akbari Mousavi, S.A.A., E-mail: akbarimusavi@ut.ac.ir

    2014-01-31

    Alpha brass alloys are widely used for production of rectangular waveguides because of their low bulk resistivity. In this paper, the microstructure, tensile deformation and fracture behavior of CuZn5 brass alloy were investigated. The strain rate sensitivity and its relation to post-uniform deformation in tensile test and correlation between strain hardening exponent (n) and temperature were examined. The results show that strain hardening exponent decreases from 0.5 to 0.4 with increase in test temperature from 250 to 450 °C. Tensile fracture mechanisms of as-extruded CuZn5 brass alloy were studied over a range of temperatures from 300 to 450 °C and range of strain rates from 0.01 to 0.4 1/s by means of scanning electron microscope (SEM) and Atomic Force Microscope (AFM). The results show that different fracture mechanisms operate in different temperature and strain rate ranges. While transgranular dimple fracture is dominant at 300 °C and 0.4 1/s, the dominant fracture mechanism at 450 °C and 0.01 1/s is cleavage facets. Precipitations and grain boundary sliding at high temperature may be the mechanism of ductility drop. Dynamic strain ageing (DSA) did not occur since none of the manifestations of DSA are observed.

  15. Investigation of Hot Deformation Behavior of Duplex Stainless Steel Grade 2507

    Science.gov (United States)

    Kingklang, Saranya; Uthaisangsuk, Vitoon

    2017-01-01

    Recently, duplex stainless steels (DSSs) are being increasingly employed in chemical, petro-chemical, nuclear, and energy industries due to the excellent combination of high strength and corrosion resistance. Better understanding of deformation behavior and microstructure evolution of the material under hot working process is significant for achieving desired mechanical properties. In this work, plastic flow curves and microstructure development of the DSS grade 2507 were investigated. Cylindrical specimens were subjected to hot compression tests for different elevated temperatures and strain rates by a deformation dilatometer. It was found that stress-strain responses of the examined steel strongly depended on the forming rate and temperature. The flow stresses increased with higher strain rates and lower temperatures. Subsequently, predictions of the obtained stress-strain curves were done according to the Zener-Hollomon equation. Determination of material parameters for the constitutive model was presented. It was shown that the calculated flow curves agreed well with the experimental results. Additionally, metallographic examinations of hot compressed samples were performed by optical microscope using color tint etching. Area based phase fractions of the existing phases were determined for each forming condition. Hardness of the specimens was measured and discussed with the resulted microstructures. The proposed flow stress model can be used to design and optimize manufacturing process at elevated temperatures for the DSS.

  16. A simple higher order shear deformation theory for mechanical behavior of laminated composite plates

    Science.gov (United States)

    Adim, Belkacem; Daouadji, Tahar Hassaine; Rabahi, Aberezak

    2016-06-01

    In the present study, the static, buckling, and free vibration of laminated composite plates is examined using a refined shear deformation theory and developed for a bending analysis of orthotropic laminated composite plates. These models take into account the parabolic distribution of transverse shear stresses and satisfy the condition of zero shear stresses on the top and bottom surfaces of the plates. The most interesting feature of this theory is that it allows for parabolic distributions of transverse shear stresses across the plate thickness and satisfies the conditions of zero shear stresses at the top and bottom surfaces of the plate without using shear correction factors. The number of independent unknowns in the present theory is four, as against five in other shear deformation theories. In the analysis, the equation of motion for simply supported thick laminated rectangular plates is obtained through the use of Hamilton's principle. The accuracy of the analysis presented is demonstrated by comparing the results with solutions derived from other higher order models and with data found in the literature. It can be concluded that the proposed theory is accurate and simple in solving the static, the buckling, and free vibration behaviors of laminated composite plates.

  17. Deformation behavior of two continuously cooled vanadium microalloyed steels at liquid nitrogen temperature

    Directory of Open Access Journals (Sweden)

    Glišić Dragomir M.

    2013-01-01

    Full Text Available The aim of this work was to establish deformation behaviour of two vanadium microalloyed medium carbon steels with different contents of carbon and titanium by tensile testing at 77 K. Samples were reheated at 1250°C/30 min and continuously cooled at still air. Beside acicular ferrite as dominant morphology in both microstructures, the steel with lower content of carbon and negligible amount of titanium contains considerable fraction of grain boundary ferrite and pearlite. It was found that Ti-free steel exhibits higher strain hardening rate and significantly lower elongation at 77 K than the fully acicular ferrite steel. The difference in tensile behavior at 77 K of the two steels has been associated with the influence of the pearlite, together with higher dislocation density of acicular ferrite. [Projekat Ministarstva nauke Republike Srbije, br. OI174004

  18. Temperature dependence of the deformation behavior of 316 stainless steel after low temperature neutron irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Pawel-Robertson, J.E.; Rowcliffe, A.F.; Grossbeck, M.L. [Oak Ridge National Lab., TN (United States)] [and others

    1996-10-01

    The effects of low temperature neutron irradiation on the tensile behavior of 316 stainless steel have been investigated. A single heat of solution annealed 316 was irradiated to 7 and 18 dpa at 60, 200, 330, and 400{degrees}C. The tensile properties as a function of dose and as a function of temperature were examined. Large changes in yield strength, deformation mode, strain to necking, and strain hardening capacity were seen in this irradiation experiment. The magnitudes of the changes are dependent on both irradiation temperature and neutron dose. Irradiation can more than triple the yield strength over the unirradiated value and decrease the strain to necking (STN) to less than 0.5% under certain conditions. A maximum increase in yield strength and a minimum in the STN occur after irradiation at 330{degrees}C but the failure mode remains ductile.

  19. Effects of twin and stacking faults on the deformation behaviors of Al nanowires under tension loading

    Institute of Scientific and Technical Information of China (English)

    An Min-Rong; Song Hai-Yang; Su Jin-Fang

    2012-01-01

    The effects of twin spacing and temperature on the deformation behavior of nanotwinned A1 under tensile loading are investigated using a molecular dynamic (MD) simulation method. The result shows that the yield strength of nanotwinned A1 decreases with the increase of twin spacing,which is related to the repulsive force between twin boundary and the dislocation. The result also shows that there is no strain-hardening at the yield point. On the contrary,the stress is raised by strain hardening in the plastic stage.In addition,we also investigate the effects of stacking fault thickness and temperature on the yield strength of the Al nanowire.The simulation results indicate that the stacking fault may strengthen the A1 nanowire when the thickness of the stacking fault is below a critical value.

  20. Hot deformation behavior and flow stress model of F40MnV steel

    Institute of Scientific and Technical Information of China (English)

    WANG Jin; CHEN Jun; ZHAO Zhen; RUAN Xue-yu

    2007-01-01

    Single hit compression tests were performed at 1 223-1 473 K and strain rate of 0.1-10 s-1 to study hot deformation behavior and flow stress model of F40MnV steel. The dependence of the peak stress, initial stress, saturation stress, steady state stress and peak stain on Zener-Hollomon parameter were obtained. The mathematical models of dynamic recrystallization fraction and grain size were also obtained. Based on the tested data.the flow stress model of F40MnV steel was established in dynamic recovery region and dynamic recrystallization region, respectively. The results show that the activation energy for dynamic recrystallization is 278.6 kJ/mol by regression analysis. The flow stress model of F40MnV steel is proved to approximate the tested data and suitable for numerical simulation of hot forging.

  1. Study on the Deformation Behavior of Mg-3.6%Er Magnesium Alloy

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    The deformation behaviour of a casting Mg-3.6%Er magnesium alloy after T6 treatment was studied in tensile tests from room temperature to 450 ℃ under different strain rates ranging from 1.0×10-4 to 6.0×10-3 s-1.Obtained local plateau in the temperature dependence of the ultimate strength (σ b) and yield strength (σ 0.2) under constant strain rate indicated the presence of dynamic strain ageing (DSA).Serrated flow was observed at the temperature of 200, 250, and 300 ℃.The observed negative strain rate sensitivity suggested that the serrated flow behavior arose from DSA.The temperature and strain rate dependence of the critical strain for the onset of serrated flow was analyzed using a phenomenological DSA equation, and the apparent activation energy Q for the serrated flow was obtained by calculation.

  2. HOT DEFORMATION AND MARTENSITIC TRANSFORMATION BEHAVIORS OF Fe-32%Ni ALLOY

    Institute of Scientific and Technical Information of China (English)

    J. Huang; Z.Xu

    2006-01-01

    The Hot deformation and martensitic transformation behaviors of Fe-32% Ni alloy was investigated by measurements of electrical resistance and X-ray diffraction. With the increase in strain,the austenite goes through from the work-hardened to the partial dynamically re-crystallized and then to the completed dynamically re-crystallized. The martensitic transformation characteristics depend on the austenite states. The work-hardening in small strain is helpful to martensitic transformation due to the low dislocation density and little lattice distortion, while the high dislocation density and severe lattice distortion by the increase in strain will hinder the martensitic nucleation.Once dynamic re-crystallization (DRX) takes place, the martensitic transformation will be enhanced again, which is related to the heterogeneous dynamic substructures. The growing DRX grain can enhance the martensitic nucleation due to the low dislocation density near its grain boundary.

  3. Hot deformation behaviors and flow stress model of GCr15 bearing steel

    Institute of Scientific and Technical Information of China (English)

    LIAO Shu-lun; ZHANG Li-wen; YUE Chong-xiang; PEI Ji-bin; GAO Hui-ju

    2008-01-01

    The hot deformation behaviors of GCr15 bearing steel were investigated by isothermal compression tests, performed on a Gleeble-3800 thermal-mechanical simulator at temperatures between 950℃ and 1 150 ℃ and strain rates between 0.1 and 10s-1.The peak stress and peak strain as functions of processing parameters were obtained. The dependence of peak stress on strain rate and temperature obeys a hyperbolic sine equation with a Zener-Hollomon parameter. By regression analysis, in the temperature range of 950-1150℃ and strain rate range of 0.1-10 s-1, the mean activation energy and the stress exponent were determined to be 351kJ/mol and 4.728, respectively. Meanwhile, models of flow stress and dynamic recrystallization (DRX) grain size were also established. The model predictions show good agreement with experimental results.

  4. Deformation behavior and microstructural evolution of nanocrystalline aluminum alloys and composites

    Science.gov (United States)

    Ahn, Byungmin

    routes. Strain rate sensitivity in room temperature deformation was examined as a function of grain size using nanoindentation. Negative strain rate sensitivity was observed in nanocrystalline and ultrafine-grained materials, while a conventional alloy was strain rate insensitive. For multi-scale materials, local displacements in bimodal materials during tensile deformation were measured by digital image correlation. Inhomogeneous strain behavior was observed between nanocrystalline and coarse-grained regions and attributed to differences in dislocation plasticity. In the Al matrix nanocomposite with hybrid microstructures, microstructural evolution of the composite powder with boron-carbide reinforcements was investigated as a function of milling time.

  5. Constitutive Analysis and Hot Deformation Behavior of Fine-Grained Mg-Gd-Y-Zr Alloys

    Science.gov (United States)

    Alizadeh, R.; Mahmudi, R.; Ruano, O. A.; Ngan, A. H. W.

    2017-09-01

    Mg-Gd-Y-Zr alloys are among the newly developed magnesium alloys with superior strength properties at elevated temperatures. Accordingly, the hot shear deformation behavior of fine-grained extruded Mg-9Gd-4Y-0.4Zr (GWK940), Mg-5Gd-4Y-0.4Zr (GWK540), and Mg-5Gd-0.4Zr (GK50) alloys was investigated using the localized shear punch testing (SPT) method. Shear punch tests were performed at 573 K, 623 K, 673 K, 723 K, and 773 K (300 °C, 350 °C, 400 °C, 450 °C, and 500 °C) under shear strain rates in the range of 6.7 × 10-3 to 6.7 × 10-2 s-1. The new fitting method of Rieiro, Carsi, and Ruano was used for direct calculation of the Garofalo constants. It was concluded that the Garofalo equation can be used satisfactorily for describing the deformation behavior of the alloys in the entire studied ranges of strain rates and temperatures. In addition, stability maps were obtained by calculations based on the Lyapunov criteria using the Garofalo constants. The predicted stability ranges of temperature and strain rate were similar for the studied alloys. At an intermediate strain rate of 0.05 s-1, the optimal temperature at which a stable region is expected was found to be 648 K to 673 K (375 °C to 400 °C) for all three materials. The most pronounced effect of the Gd and Y elements was to enhance the high-temperature strength of the alloys.

  6. Biomechanical behaviors of dragonfly wing:relationship between configuration and deformation

    Institute of Scientific and Technical Information of China (English)

    Ren Huai-Hui; Wang Xi-Shu; Chen Ying-Long; Li Xu-Dong

    2012-01-01

    In this paper,the natural structures of a dragonfly wing,including the corrugation of the chordwise cross-section,the sandwich microstructure veins,and the junctions between the vein and the membrane,have been investigated with experimental observations,and the morphological parameters of these structural features are measured. The experimental result indicates that the corrugated angle among the longitudinal veins ranges from 80° to 150°,and the sandwiched microstructure vein mainly consists of chitin and protein layers.Meanwhile,different finite element models,which include models I and I* for the planar forewings,models Ⅱ and Ⅱ* for the corrugated forewings,and a submodel with solid veins and membranes,are created to investigate the effects of these structural features on the natural frequency/modal,the dynamical behaviors of the flapping flight,and the deformation mechanism of the forewings.The numerical results indicate that the corrugated forewing has a more reasonable natural frequency/modal,and the first order up-down flapping frequency of the corrugated wing is closer to the experimental result (about 27.00 Hz),which is significantly larger than that of the planar forewing (10.94 Hz).For the dynamical responses,the corrugated forewing has a larger torsional angle than the planar forewing,but a lower flapping angle.In addition,the sandwich microstructure veins can induce larger amplitudes of torsion deformation,because of the decreasing stiffness of the whole forewing.For the submodel of the forewing,the average stress of the chitin layer is much larger than that of the protein layer in the longitudinal veins.These simulative methods assist us to explain the flapping flight mechanism of the dragonfly and to design a micro aerial vehicle by automatically adjusting the corrugated behavior of the wing.

  7. Three-Dimensional Crystal Plasticity Finite Element Simulation of Hot Compressive Deformation Behaviors of 7075 Al Alloy

    Science.gov (United States)

    Li, Lei-Ting; Lin, Y. C.; Li, Ling; Shen, Lu-Ming; Wen, Dong-Xu

    2015-03-01

    Three-dimensional crystal plasticity finite element (CPFE) method is used to investigate the hot compressive deformation behaviors of 7075 aluminum alloy. Based on the grain morphology and crystallographic texture of 7075 aluminum alloy, the microstructure-based representative volume element (RVE) model was established by the pole figure inversion approach. In order to study the macroscopic stress-strain response and microstructural evolution, the CPFE simulations are performed on the established microstructure-based RVE model. It is found that the simulated stress-strain curves and deformation texture well agree with the measured results of 7075 aluminum alloy. With the increasing deformation degree, the remained initial weak Goss texture component tends to be strong and stable, which may result in the steady flow stress. The grain orientation and grain misorientation have significant effects on the deformation heterogeneity during hot compressive deformation. In the rolling-normal plane, the continuity of strain and misorientation can maintain across the low-angle grain boundaries, while the discontinuity of strain and misorientation is observed at the high-angle grain boundaries. The simulated results demonstrate that the developed CPFE model can well describe the hot compressive deformation behaviors of 7075 aluminum alloy under elevated temperatures.

  8. Age hardening characteristics and mechanical behavior of Al-Cu-Li-Zr-In alloys

    Science.gov (United States)

    Wagner, John A.

    1989-01-01

    An investigation was conducted to determine the age-hardening response and cryogenic mechanical properties of superplastic Al-Cu-Li-Zr-In alloys. Two alloys with compositions Al-2.65Cu-2.17Li-O.13Zr (baseline) and Al-2.60Cu-2.34Li-0.16Zr-0.17In were scaled-up from 30 lb permanent mold ingots to 350 lb DC (direct chill) ingots and thermomechanically processed to 3.2 mm thick sheet. The microstructure of material which contained the indium addition was partially recrystallized compared to the baseline suggesting that indium may influence recrystallization behavior. The indium-modified alloy exhibited superior hardness and strength compared to the baseline alloy when solution-heat-treated at 555 C and aged at 160 C or 190 C. For each alloy, strength increased and toughness was unchanged or decreased when tested at - 185 C compared to ambient temperature. By using optimized heat treatments, the indium-modified alloy exhibited strength levels approaching those of the baseline alloy without deformation prior to aging. The increase in strength of these alloys in the T6 condition make them particularly attractive for superplastic forming applications where post-SPF parts cannot be cold deformed to increase strength.

  9. The effect of elevated temperature on the inelastic deformation behavior of PMR-15 solid polymer

    Science.gov (United States)

    Ryther, Chad E. C.

    The inelastic deformation behavior of PMR-15 neat resin, a high-temperature thermoset polymer, was investigated at temperatures in the 274--316 °C range. The experimental program was developed to explore the influence of temperature on strain-controlled tensile loading, relaxation and creep behaviors. The experimental results clearly demonstrate that the mechanical behavior of PMR-15 polymer exhibits a strong dependence on temperature. During strain-controlled tensile loading, the slope of the stress-strain curve in the quasi-elastic region decreases and the slope of the stress-strain curve in the flow stress region increases with increasing temperature. At a given strain rate, the flow stress level decreases with increasing temperature. Furthermore, the transition from quasi-elastic behavior to inelastic flow becomes less pronounced with increasing temperature. During relaxation, the amount of the stress drop for a given prior strain rate decreases with increasing temperature. At a given prior strain rate and creep stress level, increasing temperature results in increased creep strain accumulation. Based on the experimental results the Viscoplasticity Based on Overstress for Polymers (VBOP) theory was augmented to account for the effects of elevated temperature. Several model parameters were determined to depend on temperature. Those parameters were developed into functions of temperature. The augmented VBOP was then employed to predict the response of the PMR-15 polymer under various test histories at temperatures in the 274--316 °C range. An enhanced procedure for determining VBOP model parameters that utilizes a McLean type dip test to assess the equilibrium stress was developed. Model predictions were considerably improved by employing an enhanced model characterization procedure. Additionally, the effects of prior isothermal aging at various temperatures in the 260--316 °C range on the inelastic deformation behavior of PMR-15 at 288 °C were evaluated. For

  10. Effect of thermal processing practices on the properties of superplastic Al-Li alloys

    Science.gov (United States)

    Hales, Stephen J.; Lippard, Henry E.

    1993-01-01

    The effect of thermal processing on the mechanical properties of superplastically formed structural components fabricated from three aluminum-lithium alloys was evaluated. The starting materials consisted of 8090, 2090, and X2095 (Weldalite(TM) 049), in the form of commercial-grade superplastic sheet. The experimental test matrix was designed to assess the impact on mechanical properties of eliminating solution heat treatment and/or cold water quenching from post-forming thermal processing. The extensive hardness and tensile property data compiled are presented as a function of aging temperature, superplastic strain and temper/quench rate for each alloy. The tensile properties of the materials following superplastic forming in two T5-type tempers are compared with the baseline T6 temper. The implications for simplifying thermal processing without degradation in properties are discussed on the basis of the results.

  11. Deformation behavior in reactor pressure vessel steels as a clue to understanding irradiation hardening.

    Energy Technology Data Exchange (ETDEWEB)

    DiMelfi, R. J.; Alexander, D. E.; Rehn, L. E.

    1999-10-25

    post-yield hardening rate is clearly greater than that of the unirradiated material, and the flow curves cannot be made to superimpose. The binary iron-base model alloys studied here show a less pronounced difference in flow behavior for neutrons and electrons than exhibited by the steels, implicating the effect of alloy chemistry. Our results are analyzed in the context of classical theories dealing with the interaction between the deformation microstructure, i.e. glide dislocations, and irradiation-produced defects. Our findings provide clues about the way different alloy constituents interact with the different kinds of irradiation damage to strengthen the material differently.

  12. A Study of Hardening Behavior Based on a Finite-Deformation Gradient Crystal-Plasticity Model

    CERN Document Server

    Pouriayevali, Habib

    2016-01-01

    A systematic study on the different roles of the governing components of a well-defined finite-deformation gradient crystal-plasticity model proposed by (Gurtin, 2008b) is carried out, in order to visualize the capability of the model in the prediction of a wide range of hardening behaviors as well as rate-dependent, scale-variation and Bauschinger-like responses in a single crystal. A function of accumulation rates of dislocations is employed and viewed as a measure of formation of short-range interactions which impede dislocation movements within a crystal. The model is first represented in the reference configuration for the purpose of numerical implementation, and then implemented in the FEM software ABAQUS via a user-defined subroutine (UEL). Our simulation results reveal that the dissipative gradient-strengthening is also identified as a source of isotropic-hardening behavior, which represents the effect of cold work introduced by (Gurtin and Ohno, 2011). Moreover, plastic flows in predefined slip syste...

  13. Cyclic Deformation Behavior of a Rare-Earth Containing Extruded Magnesium Alloy: Effect of Heat Treatment

    Science.gov (United States)

    Mirza, F. A.; Chen, D. L.; Li, D. J.; Zeng, X. Q.

    2015-03-01

    The present study was aimed at evaluating strain-controlled cyclic deformation behavior of a rare-earth (RE) element containing Mg-10Gd-3Y-0.5Zr (GW103K) alloy in different states (as-extruded, peak-aged (T5), and solution-treated and peak-aged (T6)). The addition of RE elements led to an effective grain refinement and weak texture in the as-extruded alloy. While heat treatment resulted in a grain growth modestly in the T5 state and significantly in the T6 state, a high density of nano-sized and bamboo-leaf/plate-shaped β' (Mg7(Gd,Y)) precipitates was observed to distribute uniformly in the α-Mg matrix. The yield strength and ultimate tensile strength, as well as the maximum and minimum peak stresses during cyclic deformation in the T5 and T6 states were significantly higher than those in the as-extruded state. Unlike RE-free extruded Mg alloys, symmetrical hysteresis loops in tension and compression and cyclic stabilization were present in the GW103K alloy in different states. The fatigue life of this alloy in the three conditions, which could be well described by the Coffin-Manson law and Basquin's equation, was equivalent within the experimental scatter and was longer than that of RE-free extruded Mg alloys. This was predominantly attributed to the presence of the relatively weak texture and the suppression of twinning activities stemming from the fine grain sizes and especially RE-containing β' precipitates. Fatigue crack was observed to initiate from the specimen surface in all the three alloy states and the initiation site contained some cleavage-like facets after T6 heat treatment. Crack propagation was characterized mainly by the characteristic fatigue striations.

  14. Tensile Deformation Behavior of Fe-Mn-Al-C Low Density Steels

    Institute of Scientific and Technical Information of China (English)

    Xiao-feng ZHANG; Hao YANG; De-ping LENG; Long ZHANG; Zhen-yi HUANG; Guang CHEN

    2016-01-01

    Room temperature tensile tests of Fe-Mn-Al-C low density steels with four different chemical compositions were conducted to clarify the dominant deformation mechanisms.Parameters like product of strength and elongation, as well as specific strength and curves of stress-strain relations were calculated.The microstructures and tensile frac-ture morphologies were observed by optical microscope,scanning electron microscope and transmission electron mi-croscope.The tensile behavior of low density steel was correlated to the microstructural evolution during plastic de-formation,and the effects of elements,cooling process and heat treatment temperature on the mechanical properties of the steels were analyzed.The results show that the tensile strength of steels with different cooling modes is more than 1 000 MPa.The highest tensile strength of 28Mn-12Al alloy reached 1 230 MPa,with corresponding specific strength of 189.16 MPa.cm3 .g-1 ,while the specific strength of 28Mn-10Al alloy was 178.98 MPa.cm3 .g-1 , and the excellent product of strength and elongation of 28Mn-8Al alloy was over 69.2 GPa.%.A large number of ferrite reduced the ductility and strain hardening rate of the alloy,while the existence ofκcarbides may improve the strength but weaken the plasticity.Some fineκcarbides appeared in the water-quenched specimen,while coarseκcarbides were observed in the air-cooled specimen.High temperature heat treatment improved the decomposition ki-netics ofγphase and the diffusion rate of carbon,thus speeded up the precipitation of fineκcarbides.The dominant deformation mechanism of low density steel was planar glide,including shear-band-induced plasticity and microband-induced plasticity.

  15. In situ characterization of the deformation and failure behavior of non-stochastic porous structures processed by selective laser melting

    Energy Technology Data Exchange (ETDEWEB)

    Gorny, B.; Niendorf, T.; Lackmann, J. [Lehrstuhl fuer Werkstoffkunde (Materials Science), University of Paderborn, Pohlweg 47-49, 33098 Paderborn (Germany); Thoene, M.; Troester, T. [Lehrstuhl fuer Leichtbau im Automobil (Automotive Lightweight Construction), University of Paderborn, Pohlweg 47-49, 33098 Paderborn (Germany); Direct Manufacturing Research Center (DMRC), Mersinweg 3, 33098 Paderborn (Germany); Maier, H.J., E-mail: hmaier@mail.upb.de [Lehrstuhl fuer Werkstoffkunde (Materials Science), University of Paderborn, Pohlweg 47-49, 33098 Paderborn (Germany)

    2011-10-15

    Highlights: {yields} The present study focused on deformation behavior and failure mechanisms in lattice structure produced by selective laser melting (SLM). {yields} It is demonstrated that heat treatments can be used to increase the energy absorption of an SLM-processed structure. {yields} An in situ testing procedure was introduced, where local strains were calculated by digital image correlation {yields} Shear failure could be predicted by localization using Tresca strains. {yields} The approach employed provides a means to understand the microstructure-mechanical property-local deformation relationship. - Abstract: Cellular materials are promising candidates for load adapted light-weight structures. Direct manufacturing (DM) tools are effective methods to produce non-stochastic structures. Many DM studies currently focus on optimization of the geometric nature of the structures obtained. The literature available so far reports on the mechanical properties but local deformation mechanisms are not taken into account. In order to fill this gap, the current study addresses the deformation behavior of a lattice structure produced by selective laser melting (SLM) on the local scale by means of a comprehensive experimental in situ approach, including electron backscatter diffraction, scanning electron microscopy and digital image correlation. SLM-processed as well as heat treated lattice structures made from TiAl6V4 alloy were employed for mechanical testing. It is demonstrated that the current approach provides means to understand the microstructure-mechanical property-local deformation relationship to allow for optimization of load adapted lattice structures.

  16. Multi-axial load application and DIC measurement of advanced composite beam deformation behavior

    Directory of Open Access Journals (Sweden)

    Berggreen C.

    2010-06-01

    Full Text Available For the validation of a new beam element formulation, a wide set of experimental data consisting of deformation patterns obtained for a number of specially designed composite beam elements, have been obtained. The composite materials applied in the beams consist of glass-fiber reinforced plastic with specially designed layup configurations promoting advanced coupling behavior. Furthermore, the beams are designed with different cross-section shapes. The data obtained from the experiments are also used in order to improve the general understanding related to practical implementation of mechanisms of elastic couplings due to anisotropic properties of composite materials. The knowledge gained from these experiments is therefore essential in order to facilitate an implementation of passive control in future large wind turbine blades. A test setup based on a four-column MTS servo-hydraulic testing machine with a maximum capacity of 100 kN was developed, see Figure 1. The setup allows installing and testing beams of different cross-sections applying load cases such as axial extension, shear force bending, pure bending in two principal directions as well as pure torsion, see Figure 2. In order to apply multi-axial loading, a load application system consisting of three hydraulic actuators were mounted in two planes using multi-axial servo-hydraulic control. The actuator setup consists of the main actuator on the servo-hydraulic test machine working in the vertical axis (depicted on Figure 1 placed at the testing machine crosshead and used for application of vertical forces to the specimens. Two extra actuators are placed in a horizontal plane on the T-slot table of the test machine in different positions in order to apply loading at the tip of the specimen in various configurations. In order to precisely characterize the global as well as surface deformations of the beam specimens tested, a combination of different measurement systems were used during

  17. Deformation behaviour and microstructure development of magnesium AZ 31 alloy during hot and semi-hot deformation

    Energy Technology Data Exchange (ETDEWEB)

    Kawalla, R.; Stolnikov, A. [Institut fuer Metallformung, TU Bergakademie Freiberg, Bernhard-von-Cotta-Str. 4, 09596 Freiberg (Germany)

    2004-07-01

    Deformation properties and microstructure development between 20 and 450 C were investigated for Magnesium AZ31 alloy. It was found that this alloy softens preferably by dynamic recrystallisation. This process starts at suitable deformation conditions above 150 C. However, the temperature region above 250 C is more interesting for the production process the semi-finished products. The recrystallised grain size depends heavily on the deformation temperature. A grain size with a mean diameter smaller than 10 {mu}m can be created below 300 C. For further processing of Magnesium sheets, temperatures above 100 C are suitable, but temperatures above 300 C are responsible for superplasticity. (Abstract Copyright [2004], Wiley Periodicals, Inc.)

  18. Quasi-static tensile deformation and fracture behavior of a highly particle-filled composite using digital image correlation method

    Institute of Scientific and Technical Information of China (English)

    2011-01-01

    Polymer bonded explosives (PBXs) are highly particle-filled composite materials.This paper experimentally studies the tensile deformation and fracture behavior of a PBX simulation by using the semi-circular bending (SCB) test.The deformation and fracture process of a pre-notched SCB sample with a random speckle pattern is recorded by a charge coupled device camera.The displacement and strain fields on the observed surface during the loading process are obtained by using the digital image correlation method....

  19. Finite deformation analysis of continuum structures with time dependent anisotropic elastic plastic material behavior (LWBR/AWBA Development Program)

    Energy Technology Data Exchange (ETDEWEB)

    Hutula, D.N.

    1980-03-01

    A finite element procedure is presented for finite deformation analysis of continuum structures with time-dependent anisotropic elastic-plastic material behavior. An updated Lagrangian formulation is used to describe the kinematics of deformation. Anisotropic constitutive relations are referred, at each material point, to a set of three mutually orthogonal axes which rotate as a unit with an angular velocity equal to the spin at the point. The time-history of the solution is generated by using a linear incremental procedure with residual force correction, along with an automatic time step control algorithm which chooses time step sizes to control the accuracy and numerical stability of the solution.

  20. Crl2MoV钢焊接区表面高频淬火后的超塑性焊接%Superplastic Welding of Crl2MoV Steel after High Frequency Surface Quenching

    Institute of Scientific and Technical Information of China (English)

    王冰莹; 袁霄梅; 刘帅

    2012-01-01

    Superplastic welding of Cr12MoV steel was carried out after high frequency surface quenching. Process parameters chosen were: heating temperature was 800 ℃, welding time was 5 min, pre-stress was 56.6 MPa, and joint microstructure was observed and analyzed. The results show that local welding zone after high frequency quenching for Cr12MoV steel is in its superplastic deformation temperature and strain rate range, the joint tensile strength can reach values of base metal after short period of superplastic welding.%对Crl2MoV钢进行表面高频淬火后超塑性焊接,选用的工艺参数为:加热温度为800℃,焊接时间t=5min,预压应力σ0=56.6MPa,初始应变速率ε0=2.5×10^-4s^-1。对接头组织进行了观察和分析。试验结果表明,焊接区局部高频淬火后的Crl2MoV钢在其超塑变形温度及应变速率范围内,经短时间超塑焊接,其接头抗拉伸强度可以达到母材值。

  1. Effect of zinc crystals size on galvanized steel deformation and electrochemical behavior

    Directory of Open Access Journals (Sweden)

    José Daniel Culcasi

    2009-09-01

    Full Text Available Hot-dip galvanized steel sheets with different spangle sizes were deformed by means of rolling and tension. The change of preferential crystallographic orientation and of superficial characteristics due to the deformation was analyzed by means of both X-rays diffraction and optical and scanning electronic microscopy. A correlation between such changes and the involving deformation modes was intended to be done and the spangle size influence on these modes was studied. Coating reactivity change due to the deformation was investigated by means of quasi-steady DC electrochemical tests. The results allow to infer that, in great spangle samples, the main deformation mechanism is twinning whereas in small spangle ones, pyramidal slip systems happen as well. The increase of the reactivity with the deformation is greater in tension than in rolling and it is more important in small than in great spangle samples.

  2. Deformation behavior of SiC particle reinforced Al matrix composites based on EMA model

    Institute of Scientific and Technical Information of China (English)

    CHENG Nan-pu; ZENG Su-min; YU Wen-bin; LIU Zhi-yi; CHEN Zhi-qian

    2007-01-01

    Effects of the matrix properties, particle size distribution and interfacial matrix failure on the elastoplastic deformation behavior in Al matrix composites reinforced by SiC particles with an average size of 5 μm and volume fraction of 12% were quantitatively calculated by using the expanded effective assumption(EMA) model. The particle size distribution naturally brings about the variation of matrix properties and the interfacial matrix failure due to the presence of SiC particles. The theoretical results coincide well with those of the experiment. The current research indicates that the load transfer between matrix and reinforcements, grain refinement in matrix, and enhanced dislocation density originated from the thermal mismatch between SiC particles and Al matrix increase the flow stress of the composites, but the interfacial matrix failure is opposite. It also proves that the load transfer, grain refinement and dislocation strengthening are the main strengthening mechanisms, and the interfacial matrix failure and ductile fracture of matrix are the dominating fracture modes in the composites. The mechanical properties of the composites strongly depend on the metal matrix.

  3. Plastic deformation behavior of Fe–Co–B–Si–Nb–Cr bulk metallic glasses under nanoindentation

    Energy Technology Data Exchange (ETDEWEB)

    Kim, J.T.; Hong, S.H.; Lee, C.H. [HMC, Faculty of Nanotechnology and Advanced Materials Engineering, Sejong University, 98 Gunja-dong, Gwangjin-gu, Seoul 143-747 (Korea, Republic of); Park, J.M., E-mail: jinman_park@hotmail.com [Materials Research Center, Samsung Advanced Institute of Technology (SAIT), San 14-1, Nongseo-dong, Giheung-gu, Yongin-si, Gyeonggi-do 446-712 (Korea, Republic of); Kim, T.W.; Lee, W.H. [HMC, Faculty of Nanotechnology and Advanced Materials Engineering, Sejong University, 98 Gunja-dong, Gwangjin-gu, Seoul 143-747 (Korea, Republic of); Yim, H.I. [Department of Physics, Sookmyung Women’s University, Hyochangwongil 52, Yongsan-ku, Seoul 140-742 (Korea, Republic of); Kim, K.B., E-mail: kbkim@sejong.ac.kr [HMC, Faculty of Nanotechnology and Advanced Materials Engineering, Sejong University, 98 Gunja-dong, Gwangjin-gu, Seoul 143-747 (Korea, Republic of)

    2014-02-25

    Highlights: • Additional Cr modulation of atomic structure of Fe-Co-B-Si-Nb BMGs. • An amount of free volume characterized by a combination of nanoindentation and AFM. • Free volume determined by height measurement of AFM after nanoindentation. -- Abstract: In this work, we investigate the effect of Cr addition on thermal properties and indentation behavior of Fe{sub 52}Co{sub 20−x}B{sub 20}Si{sub 4}Nb{sub 4}Cr{sub x} alloys with x = 0, 1, 3 and 5 at.%, respectively. Among all studied alloys, the Fe{sub 52}Co{sub 17}B{sub 20}Si{sub 4}Nb{sub 4}Cr{sub 3} bulk metallic glass (BMG) exhibits the highest thermal stability with large supercooled liquid region of 40 K and the pronounced plastic deformation features which is serrated flow (pop-in event) and significant pile-up of materials around indents. This demonstrates that the appropriate addition of Cr in Fe-based BMG can induce the internal atomic structure modulation and promote the mechanical softening, which are discussed in terms of free volume concept.

  4. OBSERVATIONS ON DEFORMATION BEHAVIOR OF HIGH PERFORMANCE FIBERS BY POLARIZING OPTICAL MICROSCOPY

    Institute of Scientific and Technical Information of China (English)

    Chang-fa Xiao; Yu-feng Zhang

    2000-01-01

    By means of polarizing optical microscopy (POM), deformation behavior of four kinds of fibers, i.e. ultra high molecular weight polyethylene (UHMW-PE) fiber, polyvinyl alcohol (PVA) fiber, polyethylene terephthalate (PET) fiber,and wholly aromatic (p-hydroxybenzoic acid/2-hydroxy-6-naphthoic acid) copolyester [P(HBA/HNA)]/PET (ACPET blend) fiber, in axial compression, axial impacting, and bending was observed. In compression, kink bands formed at an angle of 55~60° to the fiber axis in 10-times-drawn UHMW-PE fiber, 75~80° in 40-times-drawn sample, 80° in PVA fiber, and 90°in the ACPET blend fiber. In impacting and bending, band angles of UHMW-PE, PVA and PET fibers are nearly the same as those formed in compression, indicating that slip systems do not change. For any of the four kinds of fiber, band spacing exhibits great differences in compression, in impacting, and in bending, which may be attributed to the differences in the degrees of strain or stress concentration.

  5. Cyclic Deformation of Advanced High-Strength Steels: Mechanical Behavior and Microstructural Analysis

    Science.gov (United States)

    Hilditch, Timothy B.; Timokhina, Ilana B.; Robertson, Leigh T.; Pereloma, Elena V.; Hodgson, Peter D.

    2009-02-01

    The fatigue properties of multiphase steels are an important consideration in the automotive industry. The different microstructural phases present in these steels can influence the strain life and cyclic stabilized strength of the material due to the way in which these phases accommodate the applied cyclic strain. Fully reversed strain-controlled low-cycle fatigue tests have been used to determine the mechanical fatigue performance of a dual-phase (DP) 590 and transformation-induced plasticity (TRIP) 780 steel, with transmission electron microscopy (TEM) used to examine the deformed microstructures. It is shown that the higher strain life and cyclic stabilized strength of the TRIP steel can be attributed to an increased yield strength. Despite the presence of significant levels of retained austenite in the TRIP steel, both steels exhibited similar cyclic softening behavior at a range of strain amplitudes due to comparable ferrite volume fractions and yielding characteristics. Both steels formed low-energy dislocation structures in the ferrite during cyclic straining.

  6. Deformation Behavior at High Temperature of Feeder Pipe Material in CANDU

    Energy Technology Data Exchange (ETDEWEB)

    Kim, SungSoo; Lee, Yoon Sang; Kim, Young Suk [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2016-10-15

    The specification of these nuclear materials is called as a SA106 in pipe shape. The chemical composition of SA106 is same as mild steel. The deformation behavior at high temperature in mild steel is rarely understood yet, although mild steel is a major structural material in commercial nuclear reactors. Thus, the high temperature tensile tests were carried out up to 500℃. The results are properly interpreted in the aspects of the short range order reaction. This paper is concluded as follows. 1. The FC mild steel shows a yield point. at below 400℃, whereas the WQ does not show the yield point. The reason why the yield point appears is due to the destruction of SRO formed during furnace cooling process 2. The serration appears at 50-150℃, at which the exothermic reaction takes place. The origin of the exothermic reaction is a formation of SRO between Fe and C. 3. The shape of serration changes significantly at above 121℃ and becomes downward generally, this is mainly due to both destruction of SRO by the disordering and by the shearing.

  7. Viscoelasticity behavior for finite deformations, using a consistent hypoelastic model based on Rivlin materials

    Science.gov (United States)

    Altmeyer, Guillaume; Panicaud, Benoit; Rouhaud, Emmanuelle; Wang, Mingchuan; Roos, Arjen; Kerner, Richard

    2016-11-01

    When constructing viscoelastic models, rate-form relations appear naturally to relate strain and stress tensors. One has to ensure that these tensors and their rates are indifferent with respect to the change of observers and to the superposition with rigid body motions. Objective transports are commonly accepted to ensure this invariance. However, the large number of transport operators developed makes the choice often difficult for the user and may lead to physically inconsistent formulation of hypoelasticity. In this paper, a methodology based on the use of the Lie derivative is proposed to model consistent hypoelasticity as an equivalent incremental formulation of hyperelasticity. Both models are shown to be reversible and completely equivalent. Extension to viscoelasticity is then proposed from this consistent model by associating consistent hypoelastic models with viscous behavior. As an illustration, Mooney-Rivlin nonlinear elasticity is coupled with Newton viscosity and a Maxwell-like material is investigated. Numerical solutions are then presented to illustrate a viscoelastic material subjected to finite deformations for a large range of strain rates.

  8. The Difference of Structural State and Deformation Behavior between Teenage and Mature Human Dentin.

    Science.gov (United States)

    Panfilov, Peter; Zaytsev, Dmitry; Antonova, Olga V; Alpatova, Victoria; Kiselnikova, Larissa P

    2016-01-01

    Objective. The cause of considerable elasticity and plasticity of human dentin is discussed in the relationship with its microstructure. Methods. Structural state of teenage and mature human dentin is examined by using XRD and TEM techniques, and their deformation behavior under compression is studied as well. Result. XRD study has shown that crystallographic type of calcium hydroxyapatite in human dentin (calcium hydrogen phosphate hydroxide Ca9HPO4(PO4)5OH; Space Group P63/m (176); a = 9,441 A; c = 6,881 A; c/a = 0,729; Crystallite (Scherrer) 200 A) is the same for these age groups. In both cases, dentin matrix is X-ray amorphous. According to TEM examination, there are amorphous and ultrafine grain phases in teenage and mature dentin. Mature dentin is stronger on about 20% than teenage dentin, while teenage dentin is more elastic on about 20% but is less plastic on about 15% than mature dentin. Conclusion. The amorphous phase is dominant in teenage dentin, whereas the ultrafine grain phase becomes dominant in mature dentin. Mechanical properties of human dentin under compression depend on its structural state, too.

  9. The Difference of Structural State and Deformation Behavior between Teenage and Mature Human Dentin

    Directory of Open Access Journals (Sweden)

    Peter Panfilov

    2016-01-01

    Full Text Available Objective. The cause of considerable elasticity and plasticity of human dentin is discussed in the relationship with its microstructure. Methods. Structural state of teenage and mature human dentin is examined by using XRD and TEM techniques, and their deformation behavior under compression is studied as well. Result. XRD study has shown that crystallographic type of calcium hydroxyapatite in human dentin (calcium hydrogen phosphate hydroxide Ca9HPO4(PO45OH; Space Group P63/m (176; a = 9,441 A; c = 6,881 A; c/a = 0,729; Crystallite (Scherrer 200 A is the same for these age groups. In both cases, dentin matrix is X-ray amorphous. According to TEM examination, there are amorphous and ultrafine grain phases in teenage and mature dentin. Mature dentin is stronger on about 20% than teenage dentin, while teenage dentin is more elastic on about 20% but is less plastic on about 15% than mature dentin. Conclusion. The amorphous phase is dominant in teenage dentin, whereas the ultrafine grain phase becomes dominant in mature dentin. Mechanical properties of human dentin under compression depend on its structural state, too.

  10. SUPERPLASTICITY AND DIFFUSION BONDING OF IN718 SUPERALLOY

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    The superplasticity and diffusion bonding of IN718 superalloy were studied in this article. The strain rate sensitivity index m was obtained at different temperatures and various initial strain rates using the tensile speed mutation method; m reached its maximum value 0.53 at an initial strain rate of 1 ×10-4s-1 at 1253K. The diffusion bonding parameters, including the bonding temperature T,pressure p, and time t, affected the mechanism of joints. When the bonded specimen with 25μm thick nickel foil interlayer was tensile at room temperature, the shear fracture of the joints with nickel foil interlayer took place at the IN718 part. Microstructure study was carried out with the bonded samples. The microstructure shows an excellent bonding at the interfaces. The optimum parameters for the diffusion bonding are: T= 1273-1323K, p = 20-30MPa, t = 45-60min.

  11. Coping behavior of women with breast cancer with visible postsurgery deformity

    Directory of Open Access Journals (Sweden)

    Sirota N. A.

    2013-01-01

    Full Text Available Research was carried out to explore coping strategies in cancer patients. In all, 70 women with breast cancer were studied: 35 of them had visible postsurgery deformity, and 35 did not have visible postsurgery deformity. The purpose of the research was to uncover their preferences for using various strategies and resources to cope with their illness. The results showed that both groups of women had a special set of strategies for coping with stress. The women with visible postsurgery deformity made significantly less use of resources for coping with their illness than did the subgroup of women without visible postsurgery deformity.

  12. Stress-induced deformation at Ap~Mp and thermal cycling behavior of Cu-Al-Ni single crystals

    Institute of Scientific and Technical Information of China (English)

    陈庆福; 蔡伟; 赵连城

    2001-01-01

    Stress-induced deformation in Ap~Mp and concomitant shape recovery behavior of Cu-13.4Al-4.0Ni single crystals were studied. Abnormal high stress-induced deformation exists in Ap~Mp under the conditions of either heating with load or cooling with load. The recovered deformation is successively composed of four parts, the recoveries from superelasticity, normal reverse transformation, thermally activated reverse transformation of partially stabilized martensite and reverse transformation of stabilized martensite by over-heating. With increasing cycling number, the recovery part from normal reverse transformation decreases, while that from reverse transformation of stabilized martensite by over-heating increases, which shows a typical stabilization of martensite.

  13. Hot Superplastic Powder Forging for Transparent nanocrystalline Ceramics

    Energy Technology Data Exchange (ETDEWEB)

    Cannon, W. Roger

    2006-05-22

    The program explored a completely new, economical method of manufacturing nanocrystalline ceramics, Hot Superplastic Powder Forging (HSPF). The goal of the work was the development of nanocrystalline/low porosity optically transparent zirconia/alumina. The high optical transparency should result from lack of grain boundary scattering since grains will be smaller than one tenth the wavelength of light and from elimination of porosity. An important technological potential for this process is manufacturing of envelopes for high-pressure sodium vapor lamps. The technique for fabricating monolithic nanocrystalline material does not begin with powder whose particle diameter is <100 nm as is commonly done. Instead it begins with powder whose particle diameter is on the order of 10-100 microns but contains nanocrystalline crystallites <<100 nm. Spherical particles are quenched from a melt and heat treated to achieve the desired microstructure. Under a moderate pressure within a die or a mold at temperatures of 1100C to 1300C densification is by plastic flow of superplastic particles. A nanocrystalline microstructure results, though some features are greater than 100nm. It was found, for instance, that in the fully dense Al2O3-ZrO2 eutectic specimens that a bicontinuous microstructure exists containing <100 nm ZrO2 particles in a matrix of Al2O3 grains extending over 1-2 microns. Crystallization, growth, phase development and creep during hot pressing and forging were studied for several compositions and so provided some details on development of polycrystalline microstructure from heating quenched ceramics.

  14. Experimental Study on Anisotropic Strength and Deformation Behavior of a Coal Measure Shale under Room Dried and Water Saturated Conditions

    Directory of Open Access Journals (Sweden)

    Jingyi Cheng

    2015-01-01

    Full Text Available This paper presents an experimental investigation of anisotropic strength and deformation behavior of coal measure shale. The effect of two factors (i.e., anisotropy and water content on shale strength and deformation behavior was studied. A series of uniaxial and triaxial compression tests were conducted on both room dried and water saturated samples for different lamination angles. The test results indicate that (1 the compressive strength, cohesion, internal friction angle, tangent Young’s modulus, and axial strain corresponding to the peak and residual strengths of room dried specimens exhibit anisotropic behavior that strongly depends on the orientation angle (β; (2 in comparison to the room dried samples, the compressive strength and Young’s modulus as well as the anisotropy are all reduced for water saturated specimens; and (3 the failure mechanism of the samples can be summarized into two categories: sliding along lamination and shearing of rock material, with the type occurring in a particular situation depending strongly on the lamination orientation angles with respect to the major principal stress. According to the findings, it is strongly recommended that the effect of anisotropy and water content on the strength and deformation behavior of the rock must be considered in ground control designs.

  15. Deformation behavior of Cu-12wt%AI alloy wires with continuous columnar crystals in dieless drawing process

    Institute of Scientific and Technical Information of China (English)

    LIU XueFeng; WU YuHui; XIE JianXin

    2009-01-01

    The microstructure and mechanical properties of Cu-12wt%AI alloy wires which are composed of continuous columnar crystals after dieless drawing forming at drawing speed of 1.0-1.4 mm/s and deformation temperature of 600-900℃ were analyzed,and deformation behavior of the alloy during dieless drawing forming was experimentally investigated.The results showed that in the above-mentioned conditions,recrystallization phenomenon was not found during dieless drawing forming.When a drawing speed of 1.0 mm/s was used,the grain boundaries were out of straight gradually with increasing deformation temperature from 600℃ to 900℃,and tensile strength of the dieless drawn Cu-12wt%AI alloy wires increased while elongations decreased with increasing deformation temperature.At drawing speed of 1.1-1.2 mm/s and deformation temperature of 600℃,the effect of dieless drawing forming process on the microstructure of the alloy was inconspicuous,and when drawing speed was up to 1.3-1.4 mm/s,the grain boundaries of continuous columnar crystals became zigzag while there was little effect of drawing speed of 1.1-1.4 mm/s on the elongation and tensile strength of the alloy wires.

  16. Deformation behavior of Cu-12wt%Al alloy wires with continuous columnar crystals in dieless drawing process

    Institute of Scientific and Technical Information of China (English)

    2009-01-01

    The microstructure and mechanical properties of Cu-12wt%Al alloy wires which are composed of continuous columnar crystals after dieless drawing forming at drawing speed of 1.0―1.4 mm/s and deformation temperature of 600―900℃ were analyzed, and deformation behavior of the alloy during dieless drawing forming was experimentally investigated. The results showed that in the abovemen-tioned conditions, recrystallization phenomenon was not found during dieless drawing forming. When a drawing speed of 1.0 mm/s was used, the grain boundaries were out of straight gradually with increasing deformation temperature from 600℃ to 900℃, and tensile strength of the dieless drawn Cu-12wt%Al alloy wires increased while elongations decreased with increasing deformation temperature. At drawing speed of 1.1―1.2 mm/s and deformation temperature of 600℃, the effect of dieless drawing forming process on the microstructure of the alloy was inconspicuous, and when drawing speed was up to 1.3―1.4 mm/s, the grain boundaries of continuous columnar crystals became zigzag while there was little effect of drawing speed of 1.1―1.4 mm/s on the elongation and tensile strength of the alloy wires.

  17. In-situ tube burst testing and high-temperature deformation behavior of candidate materials for accident tolerant fuel cladding

    Science.gov (United States)

    Gussev, M. N.; Byun, T. S.; Yamamoto, Y.; Maloy, S. A.; Terrani, K. A.

    2015-11-01

    One of the most essential properties of accident tolerant fuel (ATF) for maintaining structural integrity during a loss-of-coolant accident (LOCA) is high resistance of the cladding to plastic deformation and burst failure, since the deformation and burst behavior governs the cooling efficiency of flow channels and the process of fission product release. To simulate and evaluate the deformation and burst process of thin-walled cladding, an in-situ testing and evaluation method has been developed on the basis of visual imaging and image analysis techniques. The method uses a specialized optics system consisting of a high-resolution video camera, a light filtering unit, and monochromatic light sources. The in-situ testing is performed using a 50 mm long pressurized thin-walled tubular specimen set in a programmable furnace. As the first application, ten (10) candidate cladding materials for ATF, i.e., five FeCrAl alloys and five nanostructured steels, were tested using the newly developed method, and the time-dependent images were analyzed to produce detailed deformation and burst data such as true hoop stress, strain (creep) rate, and failure stress. Relatively soft FeCrAl alloys deformed and burst below 800 °C, while negligible strain rates were measured for higher strength alloys.

  18. Microstructure and Deformation Behavior of Ti-10V-2Fe-3Al Alloy during Hot Forming Process

    Institute of Scientific and Technical Information of China (English)

    GUAN Renguo; ZHAO Zhanyong; Choi KS; Lee CS

    2015-01-01

    The microstructure evolution and formability of Ti-10V-2Fe-3Al alloy related to the initial microstructures and processing variables were investigated during hot forming process. The experimental results show that theα-phase growth is controlled by solute diffusion during the heat treatment processes. Four different microstructures were established by combinations of several heat treatments, and Ti-10V-2Fe-3Al alloy shows excellent formability both above and below theβ transus temperature. The alloy possesses low deformation resistance and active restoration mechanism during the deformation. A constitutive equation describing the hot deformation behavior of Ti-10V-2Fe-3Al alloy was obtained. Higher lfow stress was observed for the acicular morphology ofαphase in microstructures with large aspect ratios as compared with that of small aspect ratios. Due to the dynamic recovery in softβphase, and the dynamic recrystallization and breakage of acicularα-phase, lfow softening occurred signiifcantly during deformation. Dynamic recrystallization also occurred especially in the severely deformed regions of forged parts.

  19. A study on hot deformation behavior of Ni-42.5Ti-7.5Cu alloy

    Energy Technology Data Exchange (ETDEWEB)

    Etaati, Amir, E-mail: amir.etaati@gmail.com [Faculty of Engineering and Surveying, University of Southern Queensland (Australia); Dehghani, Kamran [Department of Mining and Metallurgy, AmirKabir University of Technology, Tehran (Iran, Islamic Republic of)

    2013-06-15

    To investigate the hot deformation behavior of the Ni-42.5Ti-7.5Cu (wt%) alloy, hot compression tests were carried out at the temperatures from 800 °C to 1000 °C and at the strain rates of 0.001 s{sup −1} to 1 s{sup −1}. The results show that the occurrence of dynamic recrystallization (DRX) is the dominate restoration mechanism during the hot deformation of this alloy. There is an increase in peak and steady state stresses with decreasing the deformation temperature and increasing the strain rate. The experimental results were then used to determine the constants of developed constitutive equations. There is a good agreement between the measured and predicted results indicating a high accuracy of developed model. Zener–Hollomon (Z) parameter, calculated based on the developed model, indicates that DRX was postponed when the logarithm of the Zener–Hollomon parameter fell around 33 at strain rate of 0.001 s{sup −1} and temperature of 900 °C. This phenomenon can be regarded as the interactions between solute atoms and mobile dislocations. The established constitutive equations can be used to predict and analyze the hot deformation behavior of Ni-42.5Ti-7.5Cu alloy. - Highlights: • Flow stress behavior of Ni-42.5Ti-7.5Cu studied and modeled for the first time. • The model considered the compensation of both strain and strain rate. • DRX was postponed when logarithm of Z parameter was around 33 at strain rate of 0.001 s{sup −1} and 900 °C. • Ti(NiCu){sub 2} Precipitates, formed via SIP during deformation, postponed DRX.

  20. Evaluating the effects of hydroxyapatite coating on the corrosion behavior of severely deformed 316Ti SS for surgical implants

    Energy Technology Data Exchange (ETDEWEB)

    Mhaede, Mansour, E-mail: mansour.mhaede@yahoo.com [Institute of Materials Science and Engineering, Clausthal University of Engineering, Agicolastr.6, 38678 Clausthal-Zellerfeld (Germany); Faculty of Engineering, Zagazig University, 44519 Zagazig (Egypt); Ahmed, Aymen; Wollmann, Manfred; Wagner, Lothar [Institute of Materials Science and Engineering, Clausthal University of Engineering, Agicolastr.6, 38678 Clausthal-Zellerfeld (Germany)

    2015-05-01

    The present work investigates the effects of severe plastic deformation by cold rolling on the microstructure, the mechanical properties and the corrosion behavior of austenitic stainless steel (SS) 316Ti. Hydroxyapatite coating (HA) was applied on the deformed material to improve their corrosion resistance. The martensitic transformation due to cold rolling was recorded by X-ray diffraction spectra. The effects of cold rolling on the corrosion behavior were studied using potentiodynamic polarization. The electrochemical tests were carried out in Ringer's solution at 37 ± 1 °C. Cold rolling markedly enhanced the mechanical properties while the electrochemical tests referred to a lower corrosion resistance of the deformed material. The best combination of both high strength and good corrosion resistance was achieved after applying hydroxyapatite coating. - Highlights: • Cold rolling markedly increases the hardness of SS 316Ti from 125 to 460 HV10. • Higher deformation degrees lead to lower corrosion resistance. • Application of HA-coating leads to significant improvement of the corrosion resistance.

  1. Deformation Behavior of Nanostructured Ceramic Coatings Deposited by Thermal Plasma Spray

    Institute of Scientific and Technical Information of China (English)

    Xianliang JIANG; Eric Jordan; Leon Shaw; Maurice Gell

    2004-01-01

    Al2O3-13 wt pct TiO2 coating deposited by direct current plasma spray consists of nanostructured region and microlamellae. Bend test shows that the ceramic coating can sustain some deformation without sudden failure. The deformation is achieved through the movement of nano-particles in the nanostructured region under tensile stress.

  2. Effect of Strain Rate on Deformation Behavior of AlCoCrFeNi High-Entropy Alloy by Nanoindentation

    Science.gov (United States)

    Tian, L.; Jiao, Z. M.; Yuan, G. Z.; Ma, S. G.; Wang, Z. H.; Yang, H. J.; Zhang, Y.; Qiao, J. W.

    2016-06-01

    In this study, nanoindentation tests with continuous stiffness measurement technique were measured to investigate the deformation behavior of a high-entropy alloy AlCoCrFeNi under different indentation strain rates at room temperature. Results suggest that the creep behavior exhibits remarkable strain rate dependence. In-situ scanning images showed a conspicuous pileup around the indents, indicating that an extremely localized plastic deformation occurred during the nanoindentation. Under different strain rates, elastic modulus basically remains unchanged, while the hardness decreases with increasing indentation depth due to the indentation size effect. Furthermore, the modulus and hardness of AlCoCrFeNi HEAs are greater than that of the Al x CoCrFeNi ( x = 0.3,0.5) at the strain rate of 0.2 s-1 due to its higher negative enthalpy of mixing related to the atomic binding force, and the solid solution strengthening induced by the lattice distortion, respectively.

  3. Actuation Mechanism of Two-step Reverse Transformation Behavior in TiNi Alloys Deformed at Parent Phase

    Institute of Scientific and Technical Information of China (English)

    HUAILi-min; CUILi-shan; ZHANGLai-bin; ZHENGYan-jun

    2004-01-01

    The actuation mechanism of TiNi shape memory alloy wires, which were deformed at parentphase followed by a cooling process under constant strain constraint, was investigated. The experimental resuhsshow that the two-step reverse martensitic transformation behavior occurs during the heating process, and the tem-perature range of reverse transformation was olwiously widened with the increasing of prestrain,The recovery strainvs temperature curves exhibits an actuation eharaeteristic of linear output recovery strain in a wide temperaturerange.

  4. Deformation behavior after stress-induced martensite transformation in a Ti-50.8 at.% Ni alloy

    Directory of Open Access Journals (Sweden)

    Wang Xiebin

    2015-01-01

    Full Text Available In this study, the deformation behavior of a Ti-50.8 at.% Ni thin wire, which was subjected to different heat treatments, was investigated by means of uniaxial tensile tests. Considerable ductility (tensile elongation >50% and a large variation of the stress-strain relations are observed after different heat treatments, especially in the stage after the stress-induced martensite transformation plateau. A possible explanation for the observed phenomenon is discussed in this work.

  5. Modeling and simulation of deformation and fracture behavior of components made of fully lamellar {gamma}TiAl alloy

    Energy Technology Data Exchange (ETDEWEB)

    Kabir, Mohammad Rizviul [GKSS-Forschungszentrum Geesthacht GmbH (Germany). Inst. fuer Materialforschung

    2008-07-01

    The present work deals with the modeling and simulation of deformation and fracture behavior of fully lamellar {gamma}TiAl alloy; focusing on understanding the variability of local material properties and their influences on translamellar fracture. Afracture model has been presented that takes the inhomogeneity of the local deformation behavior of the lamellar colonies as well as the variability in fracture strength and toughness into consideration. To obtain the necessary model parameters, a hybrid methodology of experiments and simulations has been adopted. The experiments were performed at room temperature that demonstrates quasi-brittle response of the TiAl polycrystal. Aremarkable variation in stress-strain curves has been found in the tensile tests. Additional fracture tests showed significant variations in crack initiation and propagation during translamellar fracture. Analyzing the fracture surfaces, the micromechanical causes of these macroscopic scatter have been explained. The investigation shows that the global scatter in deformation and fracture response is highly influenced by the colony orientation and tilting angle with respect to the loading axis. The deformation and fracture behavior have been simulated by a finite element model including the material decohesion process described by a cohesive model. In order to capture the scatter of the macroscopic behavior, a stochastic approach is chosen. The local variability of stressstrain in the polycrystal and the variability of fracture parameters of the colonies are implemented in the stochastic approach of the cohesive model. It has been shown that the proposed approach is able to predict the stochastic nature of crack initiation and propagation as observed from the experiments. The global specimen failure with stable or unstable crack propagation can be explained in terms of the local variation of material properties. (orig.)

  6. Study on the Thermal Fatigue Behavior of Hot Deformed Wear Resistance Cast Iron and Effect of Carbide

    Institute of Scientific and Technical Information of China (English)

    Dong Litao; Liu Rongchang; Li Xingyuan; Chen Xiuhong

    2007-01-01

    The thermal fatigue behavior of wear resistance cast iron with different quantity of deformation has been investigated. The results show that eutectic carbide is the main location and passage for initiation and extension of thermal fatigue cracks, approving that the more serious, the carbide breaks. The higher thermal fatigue resistance of wear resistance cast iron will be and thermal fatigue fracture belongs mainly to brittleness.

  7. Study of the influence of degenerative intervertebral disc changes on the deformation behavior of the cervical spine segment in flexion

    Science.gov (United States)

    Kolmakova, Tatyana V.

    2016-11-01

    The paper describes the model of the cervical spine segment (C3-C4) and the calculation results of the deformation behavior of the segment under degenerative changes of the intervertebral disc. The segment model was built based on the experimental literature data taking into account the presence of the cortical and cancellous bone tissue of vertebral bodies. The calculation results show that degenerative changes of the intervertebral disc cause the immobility of the C3 vertebra at flexion.

  8. Structural properties, deformation behavior and thermal stability of martensitic Ti-Nb alloys

    Energy Technology Data Exchange (ETDEWEB)

    Boenisch, Matthias

    2016-06-10

    Ti-Nb alloys are characterized by a diverse metallurgy which allows obtaining a wide palette of microstructural configurations and physical properties via careful selection of chemical composition, heat treatment and mechanical processing routes. The present work aims to expand the current state of knowledge about martensite forming Ti-Nb alloys by studying 15 binary Ti-c{sub Nb}Nb (9 wt.% ≤ c{sub Nb} ≤ 44.5 wt.%) alloy formulations in terms of their structural and mechanical properties, as well as their thermal stability. The crystal structures of the martensitic phases, α{sup '} and α'', and the influence of the Nb content on the lattice (Bain) strain and on the volume change related to the β → α{sup '}/α'' martensitic transformations are analyzed on the basis of Rietveld-refinements. The magnitude of the shuffle component of the β → α{sup '}/α'' martensitic transformations is quantified in relation to the chemical composition. The largest transformation lattice strains are operative in Nb-lean alloys. Depending on the composition, both a volume dilatation and contraction are encountered and the volume change may influence whether hexagonal martensite α{sup '} or orthorhombic martensite α'' forms from β upon quenching. The mechanical properties and the deformation behavior of martensitic Ti-Nb alloys are studied by complementary methods including monotonic and cyclic uniaxial compression, nanoindentation, microhardness and impulse excitation technique. The results show that the Nb content strongly influences the mechanical properties of martensitic Ti-Nb alloys. The elastic moduli, hardness and strength are minimal in the vicinity of the limiting compositions bounding the interval in which orthorhombic martensite α'' forms by quenching. Uniaxial cyclic compressive testing demonstrates that the elastic properties of strained samples are different than those of unstrained ones

  9. On the deformation mechanisms and electrical behavior of highly stretchable metallic interconnects on elastomer substrates

    Science.gov (United States)

    Arafat, Yeasir; Dutta, Indranath; Panat, Rahul

    2016-09-01

    Flexible metallic interconnects are highly important in the emerging field of deformable/wearable electronics. In our previous work [Arafat et al., Appl. Phys. Lett. 107, 081906 (2015)], interconnect films of Indium metal, periodically bonded to an elastomer substrate using a thin discontinuous/cracked adhesion interlayer of Cr, were shown to sustain a linear strain of 80%-100% without failure during repeated cycling. In this paper, we investigate the mechanisms that allow such films to be stretched to a large strain without rupture along with strategies to prevent a deterioration in their electrical performance under high linear strain. Scanning Electron Microscopy and Digital Image Correlation are used to map the strain field of the Cr adhesion interlayer and the In interconnect film when the elastomer substrate is stretched. It is shown that the Cr interlayer morphology, consisting of islands separated by bi-axial cracks, accommodates the strain primarily by widening of the cracks between the islands along the tensile direction. This behavior is shown to cause the strain in the In interconnect film to be discontinuous and concentrated in bands perpendicular to the loading direction. This localization of strain at numerous periodically spaced locations preempts strain-localization at one location and makes the In film highly stretchable by delaying rupture. Finally, the elastic-plastic mismatch-driven wrinkling of the In interconnect upon release from first loading cycle is utilized to delay the onset of plasticity and allow the interconnect to be stretched repeatedly up to 25% linear strain in subsequent cycles without a deterioration of its electrical performance.

  10. Microstructural evolution and deformation behavior of twinning-induced plasticity (TWIP) steel during wire drawing

    Energy Technology Data Exchange (ETDEWEB)

    Hwang, Joong-Ki [Graduate Institute of Ferrous Technology, POSTECH, Pohang 790-784 (Korea, Republic of); Steel Products Research Group, Technical Research Laboratories, POSCO, Pohang 790-785 (Korea, Republic of); Yi, Il-Cheol [Graduate Institute of Ferrous Technology, POSTECH, Pohang 790-784 (Korea, Republic of); Son, Il-Heon; Yoo, Jang-Yong [Steel Products Research Group, Technical Research Laboratories, POSCO, Pohang 790-785 (Korea, Republic of); Kim, Byoungkoo [Materials Technology Development Team, DHIC, Changwon 642-792 (Korea, Republic of); Zargaran, A. [Graduate Institute of Ferrous Technology, POSTECH, Pohang 790-784 (Korea, Republic of); Kim, Nack J., E-mail: njkim@postech.ac.kr [Graduate Institute of Ferrous Technology, POSTECH, Pohang 790-784 (Korea, Republic of)

    2015-09-17

    The effect of wire drawing on the microstructural evolution and deformation behavior of Fe–Mn–Al–C twinning-induced plasticity (TWIP) steel has been investigated. The inhomogeneities of the stress state, texture, microstructure, and mechanical properties were clarified over the cross section of drawn wire with the aid of numerical simulation, Schmid factor analysis, and electron backscatter diffraction (EBSD) techniques. The analysis of texture in drawn wire shows that a mixture of <111> and <100> fiber texture was developed with strain; however, the distribution of <111> and <100> fibers was inhomogeneous along the radial direction of wire due to uneven strain distribution and different stress state along the radial direction. It has also been shown that the morphology, volume fraction, and variant system of twins as well as twinning rate were dependent on the imposed stress state. The surface area was subjected to larger strain and more complex stress state involving compression, shear, and tension than the center area, resulting in a larger twin volume fraction and more twin variants in the former than in the latter at all the strain levels. While the surface area was saturated with twins at an early stage of drawing, the center area was not saturated with twins even at fracture, implying that the fracture of wire were initiated at the surface area because of the exhaustion of ductility due to twinning. Based on these results, it is suggested that imposing a uniform strain distribution along the radial direction of wire by the control of processing conditions such as die angle and amount of reduction per pass is necessary to increase the drawing limit of TWIP steel.

  11. Deformation behavior of lead zirconate titanate ceramics under uniaxial compression measured by the digital image correlation method

    Science.gov (United States)

    Chen, Di; Carter, Emma; Kamlah, Marc

    2016-09-01

    The deformation behavior of lead zirconate titanate bulk ceramic specimen under uniaxial compression was monitored by the digital image correlation method and the homogeneity of the deformation was discussed. Combined with using a Sawyer-Tower circuit, the depolarization curve was also obtained. Because of the friction at both the top and bottom surfaces of the lead zirconate titanate ceramic specimen, the distribution of deformation under large uniaxial compressive stresses usually shows a barrel shape. By focusing on correspondingly selected regions of interest and calculating the values of strain components there, the barreling behavior was proved. This barreling behavior is due to elastic strains, in the first place, while the remnant strains are less affected by this phenomenon. All these findings are the experimental justifications for the selection of an aspect ratio of 3:1 for our specimens, where only the central cubic region of a specimen represents the desired purely uniaxial stress state. Only from this region, true uniaxial stress-strain results can be obtained to develop constitutive models.

  12. How Deformation Behavior Controls Product Performance After Twin Screw Granulation With High Drug Loads and Crospovidone as Disintegrant.

    Science.gov (United States)

    Meier, Robin; Moll, Klaus-Peter; Krumme, Markus; Kleinebudde, Peter

    2017-01-01

    This study addresses the quantitative influence of 12 different materials (active pharmaceutical ingredients and excipients as surrogate active pharmaceutical ingredients) on the critical quality attributes of twin screw granulated products and subsequently produced tablets. Prestudies demonstrated the significant influence of the chosen model materials (in combination with crospovidone) on the disintegration behavior of the resulting tablets, despite comparable tablet porosities. This study elucidates possible reasons for the varying disintegration behavior by investigating raw material, granule, and tablet properties. An answer could be found in the mechanical properties of the raw materials and the produced granules. Through compressibility studies, the materials could be classified into materials with high compressibility, which deform rather plastically under compression stress, and low compressibility, which display breakages under compression stress. In general, and apart from (pseudo)-polymorphic transformations, brittle materials featured excellent disintegration performance, even at low resulting tablet porosities <8%, whereas plastically deformable materials mostly did not reveal any disintegration. These findings must be considered in the development of simplified formulations with high drug loads, in which the active pharmaceutical ingredient predominantly defines the deformation behavior of the granule.

  13. Effects of strain rate on the hot deformation behavior and dynamic recrystallization in China low activation martensitic steel

    Energy Technology Data Exchange (ETDEWEB)

    Fang, Yuanyuan [School of Material Science and Engineering, Jiangsu University, Zhenjiang 212013 (China); Chen, Xizhang, E-mail: kernel.chen@gmail.com [School of Mechanical and Electrical Engineering, Wenzhou University, Wenzhou 325035 (China); Madigan, Bruce [Montana Tech, Butte, MT (United States); Cao, Hongyan [School of Material Science and Engineering, Jiangsu University, Zhenjiang 212013 (China); Konovalov, Sergey [Center for Collective Use Material Science, Siberian State Industrial University, Novokuznetsk (Russian Federation)

    2016-02-15

    Graphical abstract: - Highlights: • Average grain sizes of 1.8 μm are observed at strain rate of 10 s{sup −1}. • Peak stress value increased, but strain decreased with increasing of strain rate. • A catenuliform recrystallized occurred at a strain rate of 5 s{sup −1}. • DRX effect improved with increasing of deformation amounts. - Abstract: To investigate the effects of strain rate on dynamic recrystallization (DRX) behavior on China low activation martensitic steel, hot uniaxial compression tests with strain rates ranging from 0.1 s{sup −1} to 10 s{sup −1} and deformations amounts of 40% and 70% where conducted. The true stress–true strain curves were analyzed for the occurrence of DRX under the different strain rates and compressive deformation amounts. The steel microstructures were examined and linked to the observed stress-strain diagrams to study DRX. Results show that DRX was responsible for refining the grain structure over a wide range of strain rates under 70% deformation. However, significant DRX occurred only at the relatively low strain rate of 0.1 s{sup −1} under 40% deformation. The original elongated microstructure of the rolled plate from which the specimens were taken was replaced by dynamic recrystallization grains. At 70% deformation, the average grain size was 4.2 μm at a strain rate of 0.1 s{sup −1}, 2.5 μm at a strain rate of 5 s{sup −1}, 1.8 μm at a strain rate of 10 s{sup −1}. In conclusion, with increasing strain rate, the recrystallized grain size decreased and the peak stress increased.

  14. Deformation behaviors of 21-6-9 stainless steel tube numerical control bending under different friction conditions

    Institute of Scientific and Technical Information of China (English)

    方军; 鲁世强; 王克鲁; 姚正军

    2015-01-01

    For contact dominated numerical control (NC) bending process of tube, the effect of friction on bending deformation behaviors should be focused on to achieve precision bending forming. A three dimensional (3D) elastic-plastic finite element (FE) model of NC bending process was established under ABAQUS/Explicit platform, and its reliability was validated by the experiment. Then, numerical study on bending deformation behaviors under different frictions between tube and various dies was explored from multiple aspects such as wrinkling, wall thickness change and cross section deformation. The results show that the large friction of wiper die−tube reduces the wrinkling wave ratioη and cross section deformation degreeΔD and increases the wall thinning degreeΔt. The large friction of mandrel−tube causes largeη,Δt andΔD, and the onset of wrinkling near clamp die. The large friction of pressure die−tube reducesΔt andΔD, and the friction on this interface has little effect onη. The large friction of bending die−tube reducesη andΔD, and the friction on this interface has little effect onΔt. The reasonable friction coefficients on wiper die−tube, mandrel−tube, pressure die−tube and bending die−tube of 21-6-9 (0Cr21Ni6Mn9N) stainless steel tube in NC bending are 0.05−0.15, 0.05−0.15, 0.25−0.35 and 0.25−0.35, respectively. The results can provide a guideline for applying the friction conditions to establish the robust bending environment for stable and precise bending deformation of tube bending.

  15. Warm deformation behavior of hot-rolled AZ31 Mg alloy

    Energy Technology Data Exchange (ETDEWEB)

    Yin, D.L. [Key Laboratory of Precision Hot Processing of Metals, Harbin Institute of Technology, Harbin 150001 (China)]. E-mail: d_l_yin2000@hit.edu.cn; Zhang, K.F. [Key Laboratory of Precision Hot Processing of Metals, Harbin Institute of Technology, Harbin 150001 (China); Wang, G.F. [Key Laboratory of Precision Hot Processing of Metals, Harbin Institute of Technology, Harbin 150001 (China); Han, W.B. [Key Laboratory of Precision Hot Processing of Metals, Harbin Institute of Technology, Harbin 150001 (China)

    2005-02-15

    Uniaxial tensile test was employed to evaluate the warm deformation properties of hot-rolled AZ31 Mg alloy at a temperature range of 50-200 deg. C and a strain rate range of 1.4 x 10{sup -3} s{sup -1}-1.4 x 10{sup -1} s{sup -1}. The dynamic recrystallization (DRX) and twinning during the warm deformation were observed by optical microscopy (OM) and transmission electronic microscopy (TEM). It is shown that twinning characterized by a compound mode with differently oriented twins intersecting each other is the dominant deformation mechanism at low temperatures and initial deformation stage. The distortion energy accumulated by twinning is the reason for the occurrence of DRX.

  16. Episodic behavior of Gondwanide deformation in eastern Australia: Insights from the Gympie Terrane

    Science.gov (United States)

    Hoy, Derek; Rosenbaum, Gideon

    2017-08-01

    The mechanisms that drove Permian-Triassic orogenesis in Australia and throughout the Cordilleran-type Gondwanan margin is a subject of debate. Here we present field-based results on the structural evolution of the Gympie Terrane (eastern Australia), with the aim of evaluating its possible role in triggering widespread orogenesis. We document several deformation events (D1-D3) in the Gympie Terrane and show that the earliest deformation, D1, occurred only during the final pulse of orogenesis (235-230 Ma) within the broader Gondwanide Orogeny. In addition, we found no evidence for a crustal suture, suggesting that terrane accretion was not the main mechanism behind deformation. Rather, the similar spatiotemporal evolution of Permian-Triassic orogenic belts in Australia, Antarctica, South Africa, and South America suggest that the Gondwanide Orogeny was more likely linked to large-scale tectonic processes such as plate reorganization. In the context of previous work, our results highlight a number of spatial and temporal variations in pulses of deformation in eastern Australia, suggesting that shorter cycles of deformation occurred at a regional scale within the broader episode of the Gondwanide Orogeny. Similarly to the Cenozoic evolution of the central and southern Andes, we suggest that plate coupling and orogenic cycles in the Late Paleozoic to Early Mesozoic Gondwanide Orogeny have resulted from the superposition of mechanisms acting at a range of scales, perhaps contributing to the observed variations in the intensity, timing, and duration of deformation phases within the orogenic belt.

  17. INVESTIGATION INTO HOT DEFORMATION BEHAVIOR OF SPRAY FORMED SUPERALLOY GH742

    Institute of Scientific and Technical Information of China (English)

    Z.Li; G.Q.Zhang; Z.H.Zhang; S.F.Tian

    2004-01-01

    In order to evaluate the deformation characteristics of spray formed superalloy GH742 and determine the appropriate forging procedure of the alloy on this basis,the influence of deformation temperature and strain rate on the ductility of spray formed GH742 was investigated by using the Gleeble-3500 thermal-mechanical testing machine.It is shown that the forgeability of spray formed GH742 is better than conventional GH742 by ingot metallurgy because of refined grain structure and enhanced chemical homogeneity of spray formed GH742.In the temperature range of 1020 to 1100℃,the ductility of spray formed GH742 is dependent on the deformation temperature and is increased linearly in proportion to the increment of deformation temperature,which is more than 40% at 1020℃ and more than 60% at the temperature between 1100 and 1140℃.Furthermore,the results indicate the flow stress is affected considerably by the deformation temperature and strain rate.In the temperature range of 1020 to 1140℃,the maximum flow stress of spray formed GH742 increases with the increment of strain rate and decreases with the increment of the deformation temperature.

  18. Severe plastic deformation using friction stir processing, and the characterization of microstructure and mechanical behavior using neutron diffraction

    Science.gov (United States)

    Woo, Wanchuck

    Friction-stir welding (FSW) is a solid-state joining process, which utilizes a cylindrical rotating tool consisting of a concentric threaded tool pin and tool shoulder. The strong metallurgical bonding during the FSW is accomplished through: (1) the severe plastic deformation caused by the rotation of the tool pin that plunges into the material and travels along the joining line; and (2) the frictional heat generated mainly from the pressing tool shoulder. Recently, a number of variations of the FSW have been applied to modify the microstructure, for example, grain refinements and homogenization of precipitate particles, namely friction-stir processing (FSP). Applications of the FSP/FSW are widespread for the transportation industries. The microstructure and mechanical behavior of light-weight materials subjected to the FSW/FSP are being studied extensively. However, separating the effect of the frictional heat and severe plastic deformation on the residual stress and texture has been a standing problem for the fundamental understanding of FSW/FSP. The fundamental issues are: (i) the heat- and plastic-deformation-induced internal stresses that may be detrimental to the integrity and performance of components; (ii) the frictional heating that causes a microstructural softening due to the dissolution or growth of the precipitates in precipitation-hardenable Al alloys during the process; and (iii) the crystallographic texture can be significantly altered from the original texture, which could affect the physical and mechanical properties. The understanding of the influences of the de-convoluted sources (e.g. frictional heat, severe plastic deformation, or their combination) on the residual stress, microstructural softening, and texture variations during FSW can be used for a physicsvi based optimization of the processing parameters and new tool designs. Furthermore, the analyses and characterization of the natural aging behavior and the aging kinetics can be

  19. VISCOELASTIC BEHAVIOR OF THE NON-HOOKE DEFORMATION BEFORE YIELDING IN UNIAXIAL DRAWING OF AMORPHOUS POLY(ETHYLENE TEREPHTHALATE)

    Institute of Scientific and Technical Information of China (English)

    Zhen-hua Yuan; De-yan Shen; Ren-yuan Qian

    2001-01-01

    Viscoelastic behavior of the non-Hooke deformation of amorphous PET film before yield was investigated in the temperature region 74-80.5 ℃ around the glass transition temperature. The film specimen was drawn to yield point followed by unloading to zero stress, then the residual deformation was held constant, while the subsequent evolution of the stress was recorded. An induction period was found in the course of stress evolution followed by a stress step-increase. The induction period decreases with increasing drawing temperature with an activation energy of 1.10 MJ/mol @ K, which is attributed to the time needed for the relaxation of rubbery deformation through cooperative internal rotations. At temperatures lower than 74℃, there is no stress increase or the induction period becomes too long to be observed. Thus the nature of anelasticity in the non-Hooke region before yielding is attributed to stress induced rubbery deformation. The experimental results are interpreted in terms of Perez' rheological model of a series connected Hooke spring and a Voigt element consisting of a parallel connected elastic spring and a dashpot.``

  20. Ultrasonic Nondestructive Testing of Superplastic Solid-State Welding Joint for Different Steels

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Based on quantitative microscopic examinations of welds and welding rate for different steels (40Cr and T10A) joint, which possess the ultra-fine microstructure after high frequency hardening (HFH) and salt-bath cyclic quenching (SCQ), the suitable defect grey scale threshold value was determined, and the welding rate of superplastic solid-state welding of different steels (40Cr and T10A steel) was systematically inspected and analyzed by means of self-made ultrasonic imaging inspection system. The experimental results showed that the superplastic solid-state weld of different steels can be inspected more accurately, reliably and quickly by this system, and the results were in good accordance with that of metallographic observation. The welding rate of superplastic welding is in linear relation with tensile strength of joint.

  1. Ultrasonic C-scanning imaging inspection of superplastic solid-state welded joint quality

    Institute of Scientific and Technical Information of China (English)

    张柯柯; 陈怀东; 杨蕴林; 薛锦

    2002-01-01

    Based on a large amount of dissection at welded interface and quantitative microscopic examination of welded rate, the suitable limit grey scale value was determined, and the welded rate of superplastic solid-state welding interface of heterogeneous steel was systematically studied by means of self-made ultrasonic C-scanning imaging inspection system. The experimental results show: the welded state of superplastic solid-state welding interface of heterogeneous steel can be conducted to be more accurately, reliably and quickly inspected by means of this system, and the ultrasonic testing results are good consistent with actual examination results of the interface defective distribution. Within the extent of the suitble welded rate,the welded rate in 40Cr/T10A superplastic welding process tested by this system is linear with its tensile strength of joint.

  2. Superplasticity of the aluminum alloys containing the Al{sub 3}Ni eutectic particles

    Energy Technology Data Exchange (ETDEWEB)

    Portnoy, V.K. [Department of Physical Metallurgy Non-Ferrous Metals, National University of Science and Technology ' ' MISIS' ' , Moscow (Russian Federation); Mikhaylovskaya, A.V.

    2012-09-15

    The structures and parameters of superplasticity of aluminum alloys containing fine and coarse eutectic Al{sub 3}Ni particles were investigated. Traditional hot and cold rolling were used for sheet producing. The research alloys have low- or high - alloying solid solution. Superplasticity characterization of the alloy with high-alloying solid solution is much better beside alloys with low-alloying solid solution. Alloying by zirconium improves superplasticity in some investigated alloys. Some alloys with partially recrystallized structure show d = 500-700% at T = 0.95 Tm with the constant strain rates to the range of (1.10{sup -3}-1.10{sup -2}) s{sup -1}. (Copyright copyright 2012 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  3. Microstructure and Properties of Superplastic Welding between 4OCr and CrWMn Steels

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Superplastic welding of tool steel and structural steel was investigated. The welding between 40Cr and CrWMn steels was carried out under the conditions of temperature 750~780°C, strain rate 2×10-4 s-1, compressive stress 50~90 MPa for 3~5 min. The joints show similar strength to that of 40Cr steel and the good metallurgical joining is formed. The structural change occurring during superplastic welding was analyzed by metallography and distribution of carbon content in the vicinity of the welding joint was also determined. The mechanism of superplastic welding for steels is proposed to be the disappearance of original bond interfaces caused by atomic diffusion and the grain sliding.

  4. Influences of silicon on the work hardening behavior and hot deformation behavior of Fe–25 wt%Mn–(Si, Al) TWIP steel

    Energy Technology Data Exchange (ETDEWEB)

    Li, Dejun, E-mail: lidejun352@163.com [CNPC Tubular Goods Research Institute, Xi’an 710077 (China); The Key Lab for Petroleum Tubular Goods Engineering, CNPC, Xi’an 710077 (China); Feng, Yaorong; Song, Shengyin; Liu, Qiang; Bai, Qiang [CNPC Tubular Goods Research Institute, Xi’an 710077 (China); The Key Lab for Petroleum Tubular Goods Engineering, CNPC, Xi’an 710077 (China); Ren, Fengzhang [School of Material Science and Engineering, Henan University of Science and Technology, Luoyang 471023 (China); Shangguan, Fengshou [CNPC Tubular Goods Research Institute, Xi’an 710077 (China); The Key Lab for Petroleum Tubular Goods Engineering, CNPC, Xi’an 710077 (China)

    2015-01-05

    Highlights: • Influence of Si on work hardening behavior of Fe–25 wt%Mn TWIP steel was investigated. • Influence of Si on hot deformation behavior of Fe–25 wt%Mn TWIP steel was studied. • Si blocks dislocation glide and favors mechanical twinning in Fe–25 wt%Mn TWIP steel. • The addition of Si increases the hot deformation activation energy of Fe–25 wt%Mn TWIP steel. • The addition of Si retards the nucleation and growth of DRX grains of Fe–25 wt%Mn TWIP steel. - Abstract: The influence of silicon on mechanical properties and hot deformation behavior of austenitic Fe–25 wt%Mn TWIP steel was investigated by means of the comparison research between 25Mn3Al and 25Mn3Si3Al steel. The results show that the 25Mn3Si3Al steel has higher yield strength and higher hardness than that of 25Mn3Al steel because of the solution strengthening caused by Si atoms and possesses higher uniform deformation ability and tensile strength than that of 25Mn3Al steel due to the higher work hardening ability of 25Mn3Si3Al steel. 25Mn3Si3Al steel presents a clear four-stage curve of work hardening rate in course of cold compression. Quite the opposite, the 25Mn3Al steel presents a monotonic decline curve of work hardening rate. The difference of the work hardening behavior between 25Mn3Al and 25Mn3Si3Al steel can be attributed to the decline of stacking fault energy (SFE) caused by the addition of 3 wt% Si. The dislocation glide plays an important role in the plastic deformation of 25Mn3Al steel even though the mechanical twinning is still one of the main deformation mechanisms. The 3 wt% Si added into the 25Mn3Al steel blocks the dislocation glide and promotes the mechanical twinning, and then the dislocation glide characteristics cannot be observed in cold deformed microstructure of 25Mn3Si3Al steel. The hot compression tests reveal that the hot deformation resistance of the 25Mn3Si3Al steel is significantly higher than that of the 25Mn3Al steel due to the solid

  5. Constitutive Cyclic Deformation Behavior in Single-crystal and Directionally Solidified SSME High-pressure Fuel Turbopump Airfoil Materials

    Science.gov (United States)

    Milligan, W. W.; Huron, E. S.; Antolovich, S. D.

    1985-01-01

    The major goal of the project is to correlate mechanical properties with microstructural deformation behavior and to develop models for constitutive response under a variety of monotonic and cyclic loading cycles, temperatures, strain levels, strain rates, and environments. Two alloys are being studied as candidate SSME turbine blade materials. The first is PWA 1480, which is a single-crystal alloy whose nominal composition is reported. The second alloy being studied is D.S. Mar-M 246 + Hf. This is a directionally solidified material, and its nominal composition is also reported. The major areas of interest for the two materials will be slightly different. The single-crystal alloy lends itself well to fundamental deformation studies, since resolved shear stresses on slip planes are all known and only one grain is present. The D.S. material presents an excellent opportunity to study the effects of slightly misaligned grains on deformation behavior. The two materials will be studied by using approximately the same test matrix, so a good degree of direct comparison will also be possible.

  6. EFFECTS OF HIGH-DENSITY CURRENT PULSES ON WORKHARDENING BEHAVIORS OF AUSTENITE STAINLESS STEELIN WIRE-DRAWING DEFORMATION

    Institute of Scientific and Technical Information of China (English)

    K.F. Yao; P. Yu; J. Wang; W. Fang; M.X. Zheng

    2001-01-01

    The influence of high-density palsing current on the work-hardening behavior of H0Cr17Ni6Mn3 and 1Cr18Ni9 stainless steels in wire-drawing deformation processes has been studied. It was found that the drawing stress and the work-hardening rate of wires were significantly reduced by applying current pulses in drawing process. The work-hardening behavior of the multi-courses drawing deformation can be well described by Hollomon formula σ = kεn. With the application of current pulses in drawing deformation, the work-hardening exponents of H0Cr17Ni6Mn3 steel wires and 1Cr18Ni9 stainless steel wires were reduced by 33% and 45%, respectively, and their work-hardening coefficients were reduced by 41% and 47%, respectively. It was also found that the work-hardening coefficient of wires was reduced with the increment of the frequency of current pulses, while the work-hardening exponents of both steels were insensitive to the pulsing frequency.``

  7. Continuous recrystallization during thermomechanical processing of a superplastic Al-10Mg-0.1Zr alloy

    Science.gov (United States)

    Hales, S. J.; Mcnelley, T. R.; Crooks, R.

    1990-01-01

    Microstructural evolution via static continuous recrystallization during thermomechanical processing of an Al-Mg-Zr alloy is addressed. Mechanical property data demonstrated that as-rolled material was capable of superplastic response without further treatment. Further, superplastic ductility at 300 C was enhanced by a factor of five by increasing the reheating time between rolling passes during processing also at 300 C. This enhanced ductility was associated with a Cu-texture and a microstructure consisting of predominantly high-angle boundaries. Processing to minimize recovery resulted in a strong Brass-texture component, a predominantly low-angle boundary microstructure and poorer ductility.

  8. Investigation on the factors influencing the thickness distribution of superplastic-formed components

    Institute of Scientific and Technical Information of China (English)

    GAO Chong-yang; FANG You-tong

    2005-01-01

    In the superplastic sheet forming process, the uniformity of the sheet's final thickness distribution is vital for ensuring the good mechanical quality of the formed components. The influences of the component shape and the contact friction on the final thickness distribution were investigated in this work by using finite element method on a series of axisymmetric models. It was concluded that shape optimization and friction elimination are required to get uniform thickness distribution, and eventually to improve the mechanical quality of the formed components. The constitutive equation of the Ti-6A1-4V superplastic material was also determined on the basis of experimental data.

  9. Continuous recrystallization during thermomechanical processing of a superplastic Al-10Mg-0.1Zr alloy

    Science.gov (United States)

    Hales, S. J.; Mcnelley, T. R.; Crooks, R.

    1990-01-01

    Microstructural evolution via static continuous recrystallization during thermomechanical processing of an Al-Mg-Zr alloy is addressed. Mechanical property data demonstrated that as-rolled material was capable of superplastic response without further treatment. Further, superplastic ductility at 300 C was enhanced by a factor of five by increasing the reheating time between rolling passes during processing also at 300 C. This enhanced ductility was associated with a Cu-texture and a microstructure consisting of predominantly high-angle boundaries. Processing to minimize recovery resulted in a strong Brass-texture component, a predominantly low-angle boundary microstructure and poorer ductility.

  10. Experimental and FE simulation validation of sheet thickness optimization in superplastic forming of Al alloy

    Energy Technology Data Exchange (ETDEWEB)

    Kumaresan, G.; Jothilingam, A. [Anna University, Chennai (India)

    2016-07-15

    Superplasticity is the ability of a polycrystalline materials to exhibit very large elongations without necking prior to failure. In this paper, the superplastic forming potential of fine grained 7075 aluminium alloy was studied. The process parameters like pressure, forming time and initial sheet thickness were selected, using the design of experiments technique. The same condition of formation process was attempted in the finite element simulation using ABAQUS software. The deviation of the thickness distribution between the simulation and experiment was made and the variation lies within 8%.

  11. HIGH STRAIN RATE SUPERPLASTICITY OF A AIN PARTICULATE REINFORCED 6061Al COMPOSITE

    Institute of Scientific and Technical Information of China (English)

    L.H. Han; J.T. Niu; D.M. Jiang; T. Imai

    2001-01-01

    The superplasticity of AlNp/6061Al composite, fabricated by powder metallurgy method and hot-rolled after extrusion, was investigated. The AlNp/6061Al composite exhibits an m-value of 0.49 and a maximum elongation of 438% in the strain rates ranging from 10-2-10°s-1 and at temperatures from 823K to 893K. Differential scanning calorimeter was used to ascertain the possibility of any partial melting in the vicinity of optimum superplastic temperature. These results suggested that liquid phase existed where maximum elongation was obtained.

  12. Numerical simulation and experimental study on cavity growth in uniaxial tension of superplastic magnesium alloy

    Institute of Scientific and Technical Information of China (English)

    于彦东; 张凯锋; 郑海荣; 蒋大鸣

    2003-01-01

    The cavity growth was studied in uniaxial tension of superplastic magnesium alloy. An exponentially increasing cavity growth model was introduced into the numerical simulation effectively. A three-dimensional rigid visco-plastic finite element method (FEM) program was developed to predict the variation of radius and volume fraction of cavity. Experimental radius and volume fraction of cavity were determined based on the optical microscope observation and analyses. The values obtained by numerical simulation are perfectly in agreement with experimental results. The results are potentially helpful to designing the optimal processing parameters for superplastic forming of materials and to enhance their subsequent mechanical properties.

  13. Hot Deformation Behavior of a Differential Pressure Casting Mg-8Gd-4Y-Nd-Zr Alloy

    Science.gov (United States)

    Tang, Changping; Liu, Wenhui; Chen, Yuqiang; Liu, Xiao; Deng, Yunlai

    2016-11-01

    To fabricate components with high performance, the compression behavior and microstructure evolution of a differential pressure casting Mg-8Gd-4Y-Nd-Zr alloy were investigated. The cylindrical samples were compressed at temperatures ranging from 350 °C to 525 °C and strain rates ranging from 0.001 s-1 to 2 s-1. For the compression at 350 °C, dynamic precipitation occurs and consumes much of the solutes in the matrix, which should be avoided. The recrystallized grain size (d) decreases when the proposed deformation parameter (Z) increases, and the resulting Z-d relationship is established. Finally, a superior deformation process of 500 °C/0.01 s-1 is determined based on the experimental results. Moreover, a plate with an ultimate tensile strength of 413 MPa was fabricated.

  14. Hot Deformation Behavior of a Differential Pressure Casting Mg-8Gd-4Y-Nd-Zr Alloy

    Science.gov (United States)

    Tang, Changping; Liu, Wenhui; Chen, Yuqiang; Liu, Xiao; Deng, Yunlai

    2017-01-01

    To fabricate components with high performance, the compression behavior and microstructure evolution of a differential pressure casting Mg-8Gd-4Y-Nd-Zr alloy were investigated. The cylindrical samples were compressed at temperatures ranging from 350 °C to 525 °C and strain rates ranging from 0.001 s-1 to 2 s-1. For the compression at 350 °C, dynamic precipitation occurs and consumes much of the solutes in the matrix, which should be avoided. The recrystallized grain size (d) decreases when the proposed deformation parameter (Z) increases, and the resulting Z-d relationship is established. Finally, a superior deformation process of 500 °C/0.01 s-1 is determined based on the experimental results. Moreover, a plate with an ultimate tensile strength of 413 MPa was fabricated.

  15. Effect of Temperature on the Deformation Behavior of B2 Austenite in a Polycrystalline Ni49.9Ti50.1 (at.Percent) Shape Memory Alloy

    Science.gov (United States)

    Garg, A.; Benafan, O.; Noebe, R. D.; Padula, S. A., II; Clausen, B.; Vogel, S.; Vaidyanathan, R.

    2013-01-01

    Superelasticity in austenitic B2-NiTi is of great technical interest and has been studied in the past by several researchers [1]. However, investigation of temperature dependent deformation in B2-NiTi is equally important since competing mechanisms of stress-induced martensite (SIM), retained martensite, plastic and deformation twinning can lead to unusual mechanical behaviors. Identification of the role of various mechanisms contributing to the overall deformation response of B2-NiTi is imperative to understanding and maturing SMA-enabled technologies. Thus, the objective of this work was to study the deformation of polycrystalline Ni49.9Ti50.1 (at. %) above A(sub f) (105 C) in the B2 state at temperatures between 165-440 C, and generate a B2 deformation map showing active deformation mechanisms in different temperature-stress regimes.

  16. Yielding and deformation behavior of the single crystal superalloy PWA 1480

    Science.gov (United States)

    Milligan, Walter W.; Antolovich, Stephen D.

    1987-01-01

    Interrupted tensile tests were conducted to fixed plastic strain levels in 100 ordered single crystals of the nickel based superalloy PWA 1480. Testing was done in the range of 20 to 1093 C, at strain rate of 0.5 and 50 percent/min. The yield strength was constant from 20 to 760 C, above which the strength dropped rapidly and became a strong function of strain rate. The high temperature data were represented very well by an Arrhenius type equation, which resulted in three distinct temperature regimes. The deformation substructures were grouped in the same three regimes, indicating that there was a fundamental relationship between the deformation mechanisms and activation energies. Models of the yielding process were considered, and it was found that no currently available model was fully applicable to this alloy. It was also demonstrated that the initial deformation mechanism (during yielding) was frequently different from that which would be inferred by examining specimens which were tested to failure.

  17. Influence of static tensile testing on the deformation behavior of Al-4% Cu alloy containing micro- and nanoparticles

    Science.gov (United States)

    Khrustalyov, Anton; Vorozhtov, Sergey; Kulkov, Sergey

    2016-11-01

    At present, aluminum alloys reinforced with nonmetallic particles are of great interest in various fields of science and technology due to their high specific strength, hardness, wear resistance, and other properties. At the same time there is a great interest in the study of processes occurring during plastic deformation of such materials under static tensile loading. Plastic flow of metals occurs through the creation and movement of linear defects (dislocations), in which there is a phenomenon of discontinuous yielding. An introduction of particles into aluminum alloy promotes a considerable increase of stiffness and specific strength of alloys, and the study of the deformation behavior of such alloys is of great interest. The objective of this research is to analyze mechanical properties and the deformation behavior of aluminum alloy with the identification of mechanisms of plastic deformation when introducing solid nonmetallic micro- and nanoparticles into the soft aluminum matrix. An analysis of the microstructure of the obtained alloys shows that the introduction of particles (Al2O3, TiB2, TiC) leads to a reduction of the alloy grain size from 350 to 170 µm while residual porosity does not exceed 2%. Tensile tests performed show that the change in the type and quantity of particles also changes characteristics of discontinuous yielding, thus resulting in an increase of yield strength (from 18 to 40 MPa), reduction of ductility (from 15 to 2%), and moreover a significant increase of tensile strength (from 77 to 130 MPa), as compared to the initial Al-4 wt % Cu alloy.

  18. Statistical model for the mechanical behavior of the tissue engineering non-woven fibrous matrices under large deformation.

    Science.gov (United States)

    Rizvi, Mohd Suhail; Pal, Anupam

    2014-09-01

    The fibrous matrices are widely used as scaffolds for the regeneration of load-bearing tissues due to their structural and mechanical similarities with the fibrous components of the extracellular matrix. These scaffolds not only provide the appropriate microenvironment for the residing cells but also act as medium for the transmission of the mechanical stimuli, essential for the tissue regeneration, from macroscopic scale of the scaffolds to the microscopic scale of cells. The requirement of the mechanical loading for the tissue regeneration requires the fibrous scaffolds to be able to sustain the complex three-dimensional mechanical loading conditions. In order to gain insight into the mechanical behavior of the fibrous matrices under large amount of elongation as well as shear, a statistical model has been formulated to study the macroscopic mechanical behavior of the electrospun fibrous matrix and the transmission of the mechanical stimuli from scaffolds to the cells via the constituting fibers. The study establishes the load-deformation relationships for the fibrous matrices for different structural parameters. It also quantifies the changes in the fiber arrangement and tension generated in the fibers with the deformation of the matrix. The model reveals that the tension generated in the fibers on matrix deformation is not homogeneous and hence the cells located in different regions of the fibrous scaffold might experience different mechanical stimuli. The mechanical response of fibrous matrices was also found to be dependent on the aspect ratio of the matrix. Therefore, the model establishes a structure-mechanics interdependence of the fibrous matrices under large deformation, which can be utilized in identifying the appropriate structure and external mechanical loading conditions for the regeneration of load-bearing tissues.

  19. Thermal behavior of Nickel deformed to ultra-high strain by high pressure torsion

    DEFF Research Database (Denmark)

    Zhang, Hongwang; Huang, Xiaoxu; Pippan, Richard

    2012-01-01

    Polycrystalline Ni (99.5 %) has been deformed to an ultra-high strain of εvM=100 (εvM, von Mises strain) by high pressure torsion (HPT) at room temperature. The deformed sample is nanostructured with an average boundary spacing of 90 nm, a high density of dislocations of >1015m-2 and a large....... The isochronal annealing leads to a hardness drop in three stages: a relatively small decrease at low temperatures (recovery) followed by a rapid decrease at intermediate temperatures (discontinuous recrystallization) and a slow decrease at high temperatures (grain growth). Due to the presence of a small amount...

  20. Effect of Incomplete Thermal Cycle on Transformation Behavior of Deformed TiNi Thin Film

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Compared with the undeformed TiNi film, the martensite-austenite transformation (M-A) of the deformed one is elevated to a higher temperature on the first heating, but it nearly returns back to the original temperature on the second heating. An incomplete M-A transformation of the deformed TiNi film on the first heating divides the total martensite population into the self-accommodating martensite M2 and the oriented martensite M1. Thus, two transformations corresponding to M1-A and M2-A transition occur on the second heating. However, the forward transformation is not affected by the incomplete thermal cycle.

  1. Effect of Initial Backfill Temperature on the Deformation Behavior of Early Age Cemented Paste Backfill That Contains Sodium Silicate

    Directory of Open Access Journals (Sweden)

    Aixiang Wu

    2016-01-01

    Full Text Available Enhancing the knowledge on the deformation behavior of cemented paste backfill (CPB in terms of stress-strain relations and modulus of elasticity is significant for economic and safety reasons. In this paper, the effect of the initial backfill temperature on the CPB’s stress-strain behavior and modulus of elasticity is investigated. Results show that the stress-strain relationship and the modulus of elasticity behavior of CPB are significantly affected by the curing time and initial temperature of CPB. Additionally, the relationship between the modulus of elasticity and unconfined compressive strength (UCS and the degree of hydration was evaluated and discussed. The increase of UCS and hydration degree leads to an increase in the modulus of elasticity, which is not significantly affected by the initial temperature.

  2. Macroscopic inhomogeneous deformation behavior arising in single crystal Ni-Mn-Ga foils under tensile loading

    Science.gov (United States)

    Murasawa, Go; Yeduru, Srinivasa R.; Kohl, Manfred

    2016-12-01

    This study investigated macroscopic inhomogeneous deformation occurring in single-crystal Ni-Mn-Ga foils under uniaxial tensile loading. Two types of single-crystal Ni-Mn-Ga foil samples were examined as-received and after thermo-mechanical training. Local strain and the strain field were measured under tensile loading using laser speckle and digital image correlation. The as-received sample showed a strongly inhomogeneous strain field with intermittence under progressive deformation, but the trained sample result showed strain field homogeneity throughout the specimen surface. The as-received sample is a mainly polycrystalline-like state composed of the domain structure. The sample contains many domain boundaries and large domain structures in the body. Its structure would cause large local strain band nucleation with intermittence. However, the trained one is an ideal single-crystalline state with a transformation preferential orientation of variants after almost all domain boundary and large domain structures vanish during thermo-mechanical training. As a result, macroscopic homogeneous deformation occurs on the trained sample surface during deformation.

  3. Hydrostatic and shear behavior of frictionless granular assemblies under different deformation conditions

    NARCIS (Netherlands)

    Imole, Olukayode Isaiah; Kumar, Nishant; Magnanimo, Vanessa; Luding, Stefan

    2013-01-01

    Stress- and structure-anisotropy (bulk) responses to various deformation modes are studied for dense packings of linearly elastic, frictionless, polydisperse spheres in the (periodic) triaxial box element test configuration. The major goal is to formulate a guideline for the procedure of how to cali

  4. Influence of thermo hydrogen treatment on hot deformation behavior of Ti600 alloy

    Institute of Scientific and Technical Information of China (English)

    ZHAO Jing-wei; DING Hua; WANG Yao-qi; HOU Hong-liang

    2009-01-01

    Hot compressive deformation of Ti600 alloy after thermo hydrogen treatment (THT) was carried out within hydrogen content range of 0-0.5%, temperature range of 760-920 ℃ and strain rate range of 0.01-10 s-1. The flow stress of Ti600 alloy after THT was obtained under hot deformation condition, and the influence of hydrogen on work-hardening rate (S*), strain energy density (U*), and deformation activation energy (Q) was analysed. The results show that the flow stress of Ti600 alloy decreases remarkably with the increase of hydrogen when the hydrogen content is less than 0.3%. Both S* and U* decrease with the increase of hydrogen when the hydrogen content is less than 0.3%, and when the hydrogen content is more than 0.3%, S* and U* increase with hydrogen addition. The value of Q decreases with the increase of strain at the same hydrogen content. The addition of small quantity of hydrogen leads to an increase of Q at small strain values, and when the strain reaches 0.6, the value of Q decreases gradually with the increase of hydrogen. When the hydrogen content is within the range of 0.1%-0.3%, the flow stress of Ti600 alloy is decreased when being deformed at the temperature range of 760-920 ℃.

  5. Hydrostatic and shear behavior of frictionless granular assemblies under different deformation conditions

    NARCIS (Netherlands)

    Imole, O.I.; Kumar, N.; Magnanimo, V.; Luding, S.

    2013-01-01

    Stress- and structure-anisotropy (bulk) responses to various deformation modes are studied for dense packings of linearly elastic, frictionless, polydisperse spheres in the (periodic) triaxial box element test configuration. The major goal is to formulate a guideline for the procedure of how to cali

  6. Mechanical Properties and Fracture Behavior of Cu-Co-Be Alloy after Plastic Deformation and Heat Treatment

    Institute of Scientific and Technical Information of China (English)

    Yan-jun ZHOU; Ke-xing SONG; Jian-dong XING; Zhou LI; Xiu-hua GUO

    2016-01-01

    Mechanical properties and fracture behavior of Cu-0.84Co-0.23Be alloy after plastic deformation and heat treatment were comparatively investigated.Severe plastic deformation by hot extrusion and cold drawing was adopted to induce large plastic strain of Cu-0.84Co-0.23Be alloy.The tensile strength and elongation are up to 476.6 MPa and 1 8%,respectively.The fractured surface consists of deep dimples and micro-voids.Due to the formation of su-persaturated solid solution on the Cu matrix by solution treatment at 950 ℃ for 1 h,the tensile strength decreased to 271.9 MPa,while the elongation increased to 42%.The fracture morphology is parabolic dimple.Furthermore,the tensile strength increased significantly to 580.2 MPa after aging at 480 ℃ for 4 h.During the aging process,a large number of precipitates formed and distributed on the Cu matrix.The fracture feature of aged specimens with low elongation (4.6%)exhibits an obvious brittle intergranular fracture.It is confirmed that the mechanical properties and fracture behavior are dominated by the microstructure characteristics of Cu-0.84Co-0.23Be alloy after plastic de-formation and heat treatment.In addition,the fracture behavior at 450 ℃ of aged Cu-0.84Co-0.23Be alloy was also studied.The tensile strength and elongation are 383.6 MPa and 11.2%,respectively.The fractured morphologies are mainly candy-shaped with partial parabolic dimples and equiaxed dimples.The fracture mode is multi-mixed mechanism that brittle intergranular fracture plays a dominant role and ductile fracture is secondary.

  7. Effect of r-value and texture on plastic deformation and necking behavior in interstitial-free steel sheets

    Science.gov (United States)

    Oh, Gyu-Jin; Lee, Kye-Man; Huh, Moo-Young; Park, Jin Eon; Park, Soo Ho; Engler, Olaf

    2017-01-01

    Three initial tensile specimens having different textures and, in consequence, different r-values were cut from a sheet of an interstitial-free steel. Using these specimens, the effect of r-value and texture on plastic deformation and the necking behavior were studied by tackling the strain state and texture during tensile tests. A reduced decrease in work hardening rate of tensile specimens with higher r-values led to a slower onset of diffuse necking which offers an increased uniform elongation. A slower reduction in thickness of specimens with a higher r-value provided a favorable resistance against onset of failure by localized necking.

  8. Computational analysis of linear friction welding process and micromechanical modeling of deformation behavior for medium carbon steel

    Institute of Scientific and Technical Information of China (English)

    杨夏炜; 李文亚; 马铁军

    2015-01-01

    Finite element simulation of linear friction welding (LFW) medium carbon steel was carried out using the ABAQUS software. A two-dimensional (2D) coupled thermo-mechanical model was established. First, the temperature fields of medium carbon steel during LFW process were investigated. And then, the Mises stress and the 1st, 2nd and 3rd principal stresses fields’ evolution of the steel during LFW process were studied. The deformation behavior of LFW carbon steel was analyzed by using micromechanics model based on ABAQUS with Python code. The Lode parameter was expressed using the Mohr stress circle and it was investigated in detail.

  9. Indentation-Induced Mechanical Deformation Behaviors of AlN Thin Films Deposited on c-Plane Sapphire

    Directory of Open Access Journals (Sweden)

    Sheng-Rui Jian

    2012-01-01

    Full Text Available The mechanical properties and deformation behaviors of AlN thin films deposited on c-plane sapphire substrates by helicon sputtering method were determined using the Berkovich nanoindentation and cross-sectional transmission electron microscopy (XTEM. The load-displacement curves show the “pop-ins” phenomena during nanoindentation loading, indicative of the formation of slip bands caused by the propagation of dislocations. No evidence of nanoindentation-induced phase transformation or cracking patterns was observed up to the maximum load of 80 mN, from either XTEM or atomic force microscopy (AFM of the mechanically deformed regions. Instead, XTEM revealed that the primary deformation mechanism in AlN thin films is via propagation of dislocations on both basal and pyramidal planes. Furthermore, the hardness and Young’s modulus of AlN thin films estimated using the continuous contact stiffness measurements (CSMs mode provided with the nanoindenter are 16.2 GPa and 243.5 GPa, respectively.

  10. On the intergranular fracture behavior of high-temperature plastic deformation of 1420 Al-Li alloy

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    The tensile deformation hot simulation test of as-cast 1420 Al-Li alloy was performed on Gleeble-1500 Thermal Simulator in the deformation temperature range from 350 to 450 ℃, and the strain rate range from 0.01 to 10.0 s-1.The tensile fracture behavior of the 1420 Al-Li alloy at high temperature was studied experimently. The results show that the tensile fracture mode of the 1420 Al-Li alloy at high temperature is changed from typical transgranular ductile fracture to intergranular brittle fracture with the increase of the deformation temperature and the strain rate. It is made out that the precipitation of LiH is the fundamental reason for the intergranular brittle fracture of the 1420 Al-Li alloy at high temperature. The mechanism of hydrogen embrittlement of the 1420 Al-Li alloy at high temperature was discussed, and it was proposed that the hydrogen embrittlement at high temperature is an integrated function of the dynamic and the static force, which enrichs the theories of hydrogen embrittlement.

  11. Critical Deposition Condition of CoNiCrAlY Cold Spray Based on Particle Deformation Behavior

    Science.gov (United States)

    Ichikawa, Yuji; Ogawa, Kazuhiro

    2017-02-01

    Previous research has demonstrated deposition of MCrAlY coating via the cold spray process; however, the deposition mechanism of cold spraying has not been clearly explained—only empirically described by impact velocity. The purpose of this study was to elucidate the critical deposit condition. Microscale experimental measurements of individual particle deposit dimensions were incorporated with numerical simulation to investigate particle deformation behavior. Dimensional parameters were determined from scanning electron microscopy analysis of focused ion beam-fabricated cross sections of deposited particles to describe the deposition threshold. From Johnson-Cook finite element method simulation results, there is a direct correlation between the dimensional parameters and the impact velocity. Therefore, the critical velocity can describe the deposition threshold. Moreover, the maximum equivalent plastic strain is also strongly dependent on the impact velocity. Thus, the threshold condition required for particle deposition can instead be represented by the equivalent plastic strain of the particle and substrate. For particle-substrate combinations of similar materials, the substrate is more difficult to deform. Thus, this study establishes that the dominant factor of particle deposition in the cold spray process is the maximum equivalent plastic strain of the substrate, which occurs during impact and deformation.

  12. Flow Behavior and Microstructural Evolution of 7A85 High-Strength Aluminum Alloy During Hot Deformation

    Science.gov (United States)

    Liu, Xingang; Han, Shuang; Chen, Lei; Yang, Shuai; Jin, Miao; Guo, Baofeng; Mao, Tianhong

    2017-02-01

    Hot deformation behavior of 7A85 high-strength aluminum alloy was investigated at 593 K to 713 K (320 °C to 440 °C) and 0.01-10 s-1. The manifestation of flow curves was related to the strain rate. Typical single-peak curves were shown below 10 s-1, while two stress peaks appeared in the case of 10 s-1 and the second peak strain was almost three times larger than the first one. A constitutive equation considering the effect of strain was developed. Flow stress values predicted by the constitutive model demonstrated a good agreement with the experimental results over the entire range of strain rates and temperatures. Microstructure characterization revealed that dynamic recovery (DRV) and continuous dynamic recrystallization (CDRX) which depended on the Zener-Hollomon parameter (Z) closely, co-occurred at large strain (ɛ = 0.7). With decreasing Z-value, the dominant dynamic restoration mechanism gradually transformed from DRV to CDRX. The average subgrain size (d sub) showed a power-law relationship with Z. Recrystallization was sensitively dependent on the strain rate at above 683 K (410 °C). The fine equiaxed grains appeared at original grain boundaries and in deformed grains interior owing to CDRX. The high-curvature subgrain boundaries can also cause the nucleation of recrystallization within deformed grains.

  13. Low temperature superplasticity through grain refinement in Ti-6Al-4V by a novel route of quench-roll-recrystallise

    Directory of Open Access Journals (Sweden)

    Jalumedi Babu

    2015-07-01

    Full Text Available A ‘quench + roll + recrystallise’ method was simulated through compression testing of initially ‘water quenched’ Ti-6Al-4V alloy at a temperature of 973 K and rolling strain-rate 100 s−1 in order to achieve superplasticity at lower temperature through grain refinement, with a view to increase die life. Subsequent annealing of wire-cut specimens of a rolled sheet at temperatures 1023, 1073, 1123, and 1173 K revealed that, the structures became finer and equi-axial in the range of 1–2 μm, when annealed at 1073 and 1123 K. In compliance to this behavior, a tensile sample from industrially ‘quenched + rolled’ sheet at 973 K could produce an elongation of 740% at a temperature of 1073 K under a strain-rate of 10−3 s−1. Significant elongation of 652% was obtained at further lower temperature of 1023 K under a strain-rate of 10−3 s−1. Quench-roll-recrystallise technique pushes down superplastic forming temperature to 1023 K.

  14. Deformation and annealing behavior of heavily drawn oxygen-free high-conductivity (OFHC) copper

    Science.gov (United States)

    Waryoba, Daudi Rigenda

    Conductor wires used in pulsed high-field magnets require metallic materials with a beneficial combination of high mechanical strength to resist the Lorentz forces and high electrical conductivity to limit temperature excursions due to Joule heating. To achieve the required strength, most conductors are fabricated from microcomposite materials using the work hardening effect after heavy cold deformation such as wire drawing. Since the microstructure and texture of these microcomposites are complex, a detailed systematic study of these materials requires a separate study of the individual phases. This work presents a comprehensive study of the microstructure and microtexture evolution during deformation, and subsequent annealing of heavily deformed OFHC copper wires. Analytical tools used for investigation include optical microscopy, scanning electron microscopy (SEM), orientation-imaging microscopy (OIM) in SEM, and transmission electron microscopy (TEM). Mechanical properties were evaluated by tensile and microhardness testing. Some of the key features of the as-drawn wire are elongated grain size and shear bands. The intensity of the shear bands increased with strain. The ultimate tensile strength (UTS) and the microhardness of the heavily cold-drawn copper wires increased with strain, reached a saturation point and dropped at higher deformation strain. Deformation did not significantly alter the electrical conductivity of the wires. Deformed and recovered microstructures were characterized by a strong+weak duplex fiber texture. Nucleation of recrystallized grains occurred at shear bands and resulted in randomization of texture. On the other hand, recrystallization produced a strong+weak, which later changed to a fiber texture during abnormal grain growth. A detailed analysis showed that recrystallization was a growth-controlled mechanism, and proceeds from the outer surface to the core. Interestingly, secondary recrystallization was observed to proceed from the

  15. The influence of silicon and aluminum on austenite deformation behavior during fatigue and tensile loading

    Science.gov (United States)

    Lehnhoff, Gregory R.

    Advanced high strength steels (AHSS) for automobile light-weighting utilize Si and Al alloying to retain austenite in the microstructure during thermal partitioning treatments. This research project utilized fully austenitic steels with varied Si and Al compositions to understand the effect of these elements on austenite deformation response, including deformation induced martensite formation and deformation twinning. Specific focus was directed at understanding austenite deformation response during fatigue loading. Independent alloying additions of 2.5 wt pct Si and Al were made to a base steel composition of 15 Ni - 11 Cr - 1 Mn - 0.03 C (wt pct). Weak beam dark field transmission electron microscopy (TEM) imaging of dissociated dislocations was implemented to experimentally determine the influences of Si and Al on austenite stacking fault energy (SFE). The 2.5 wt pct Si alloying addition decreased the SFE by 6.4 mJ/m2, while the 2.5 wt pct Al alloying increased the SFE by 12 mJ/m2. Fully reversed, total strain controlled, low cycle fatigue (LCF) tests indicated that all four alloys underwent primary cyclic hardening and stabilization. Secondary cyclic strain hardening was correlated to BCC martensite formation using Feritscope magnetic fraction measurements of LCF specimens; the formation of 1 pct martensite led to 7 MPa of secondary hardening. TEM showed that martensite predominantly formed as parallel, irregular bands through strain induced nucleation on austenite shear bands. The austenite shear bands consisted of austenite {111} planes with concentrated dislocations, stacking faults, and/or HCP epsilon-martensite. Aluminum alloying promoted martensite formation during LCF, while Si suppressed martensite. Therefore, the strain induced nucleation process was not suppressed by the increased SFE associated with Al alloying. Tensile testing indicated that Si alloying promoted deformation twinning by lowering the SFE. Similarly to LCF loading, Al promoted

  16. The effect of composition on the mechanism of continuous recrystallization and superplastic response of aluminum-scandium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Bradley, E.L. III

    1993-05-01

    The continuous recrystallization (CRX) appears to be fundamental in Al-Sc because it occurs irrespective of solute composition. It appears to be due to a combination of subgrain coalescence at low strains and incorporation of additional dislocations generated during grain boundary sliding at higher strains when the misorientation has increased sufficiently. Alloying additives such as Mg, Li are more important with respect to deformation after CRX is completed. Mg, and to a lesser extent Li, affect the max m-values (strain-rate sensitivities) in Al-Sc by changing the melting points (mp). Max m- values correlate inversely with mp so that the alloy with the greatest Mg had the highest m-values and lowest mp; the stress is raised at which power-law creep and breakdown occurs. The power-law breakdonw at much lower stresses in Al-0.5Sc and Al-1.2Li-0.5Sc causes the m-value to decrease more rapidly with strain rate. Al alloys for commercial superplastic applications should contain elements that raise the power-law strength so that the m-values are maximized while preserving the post-formed mechanical properties. Refs, figs, tabs.

  17. Effect of Cyclic Pre-deformation on Uniaxial Tensile Behavior of Cu-16 at. pct Al Alloy with Low Stacking Fault Energy

    Science.gov (United States)

    Yan, Y.; Qi, C. J.; Han, D.; Ji, H. M.; Zhang, M. Q.; Li, X. W.

    2017-02-01

    To explore the effect of cyclic pre-deformation on static mechanical behavior of materials with different stacking fault energies (SFEs), polycrystalline Cu-16 at. pct Al alloy with a low SFE is selected as the target material in the present work, and the strengthening micro-mechanisms induced by cyclic pre-deformation are compared with the previous studies on pure Al with a high SFE and Cu with an intermediate SFE. The results show that the movement of dislocations exhibits a high slip planarity during cyclic pre-deformation at different total strain amplitudes Δ ɛ t/2, and some nano-sized deformation twins are formed after subsequent tension. The cyclic pre-deformation at an appropriate Δ ɛ t/2 of 1.0 × 10-3 promotes a significant increase in ultimate tensile strength σ UTS nearly without loss of tensile ductility, which primarily stems from the introduction of many mobile planar slip dislocations by cyclic pre-deformation as well as the formation of nano-sized deformation twins during subsequent tension. Based on the comparison of the strengthening micro-mechanisms induced by cyclic pre-deformation in Al, Cu, and Cu-16 at. pct Al alloy, it is deduced that a low-cycle cyclic pre-deformation at an appropriate condition is expected to cause a better strengthening effect on the static tensile properties of low SFE metals.

  18. Recent Achievements in Developing Low Temperature and High Strain Rate Superplastic Materials

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    This paper is to briefly outline our recent activities in developing low temperature or high strain rate superplastic materials, including aircraft-used and general-purpose Al- and Mg-base alloys or composites, as well as Ti3Al base intermetallic alloys. The processing routes applied included the thermomechanical treatment, equal channel angular pressing and other extrusion or forging methods.

  19. Surface properties and activation energy of superplastically carburized duplex stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Ahamad, Nor Wahida, E-mail: wahida_um@yahoo.com [Department of Mechanical and Materials Engineering, Faculty of Engineering, University Malaya, Lembah Pantai, 50603 Kuala Lumpur (Malaysia); Jauhari, Iswadi, E-mail: iswadi@um.edu.my [Department of Mechanical and Materials Engineering, Faculty of Engineering, University Malaya, Lembah Pantai, 50603 Kuala Lumpur (Malaysia); Azis, Sharidah Azuar Abdul, E-mail: sharidah_azuar@yahoo.com [Department of Mechanical and Materials Engineering, Faculty of Engineering, University Malaya, Lembah Pantai, 50603 Kuala Lumpur (Malaysia); Aziz, Nur Hafizah Abd, E-mail: phiza_aziz@yahoo.com [Department of Mechanical and Materials Engineering, Faculty of Engineering, University Malaya, Lembah Pantai, 50603 Kuala Lumpur (Malaysia)

    2010-08-01

    A new surface carburizing technique which combines superplastic phenomenon and carburizing process called superplastic carburizing (SPC) was introduced and compared with conventional carburizing (CC) process. Thermomechanically treated duplex stainless steel (DSS) with a fine grain microstructure that exhibits superplasticity was used as the superplastic material. SPC was carried out at temperatures of 1198-1248 K and a compression rate of 1 x 10{sup -4} s{sup -1} for various durations. Metallographic studies revealed that a carbon layer with a uniform, dense and smooth morphology formed on all carburized specimens. The case depth of the carbon layer was between 50.8 and 159.1 {mu}m. A remarkable increase in surface hardness was observed in the range 389.9-1129.0 HV. Activation energy for SPC was determined as 183.4 kJ mol{sup -1}, which is lower compare to CC process. The results indicate that SPC accelerates the diffusion of carbon atoms into the surface of DSS, thus increasing the thickness of the carburized layer and the surface hardness, at lower activation energy.

  20. Hot Deformation Behavior and Microstructural Evolution of a Medium Carbon Vanadium Microalloyed Steel

    Science.gov (United States)

    Cutrim, Rialberth M.; Rodrigues, Samuel F.; Reis, Gedeon S.; Silva, Eden S.; Aranas, Clodualdo; Balancin, Oscar

    2016-11-01

    Hot forging of steel requires application of large strains, under which conditions, dynamic recrystallization (DRX) is expected to take place. In this study, torsion tests were carried out on a medium carbon vanadium microalloyed steel (38MnSiVS5) to simulate hot forging. Deformations were applied isothermally in the temperature range 900-1200 °C at strain rates of 0.1-10 s-1 in order to observe for the occurrence of DRX and to investigate for the microstructural evolution during straining. The shape of the flow curves indicated that the recrystallization takes place during deformation. This was supported by optical microscopy performed on the quenched samples which displayed considerable amounts of recrystallized grains. It was shown that the grain size depends on straining conditions such as strain rate and temperature. Finally, it was revealed that these process parameters can considerably affect the evolution of microstructure of industrial grade steels by means of DRX.

  1. Experimental and Numerical Investigations on Strength and Deformation Behavior of Cataclastic Sandstone

    Science.gov (United States)

    Zhang, Y.; Shao, J. F.; Xu, W. Y.; Zhao, H. B.; Wang, W.

    2015-05-01

    This work is devoted to characterization of the deformation and strength properties of cataclastic sandstones. Before conducting mechanical tests, the physical properties were first examined. These sandstones are characterized by a loose damaged microstructure and poorly cemented contacts. Then, a series of mechanical tests including hydrostatic, uniaxial, and triaxial compression tests were performed to study the mechanical strength and deformation of the sandstones. The results obtained show nonlinear stress-strain responses. The initial microcracks are closed at hydrostatic stress of 2.6 MPa, and the uniaxial compressive strength is about 0.98 MPa. Under triaxial compression, there is a clear transition from volumetric compressibility to dilatancy and a strong dependency on confining pressure. Based on the experimental evidence, an elastoplastic model is proposed using a linear yield function and a nonassociated plastic potential. There is good agreement between numerical results and experimental data.

  2. Repeated Load Permanent Deformation Behavior of Mixes With and Wihtout Modified Bituments

    Directory of Open Access Journals (Sweden)

    Imran Hafeez

    2011-01-01

    Full Text Available Premature rutting in flexible pavement structure is being observed on most of the road network of Pakistan. It initiates primarily due to uncontrolled axle loading and high ambient temperatures. NHA (National Highway Authority, Pakistan has continuously been modifying aggregate gradations and penetration grade of bitumen, without any prior investigation of the mix behaviour under the prevailing axle load and environmental conditions of the country. A comprehensive laboratory investigation was carried out on six mixes ranging from finer to coarser. Specimens were subjected to cyclic loading on UTM-5P (Universal Testing Machine to study the resistance against permanent deformation of the mixes at 25, 40 and 550C. At low temperatures and stress levels, both coarse and fine graded mixes showed less accumulated strain, whereas at higher temperatures and stress levels, coarse graded mix with PMB (Polymer Modified Bitumen showed good resistance to permanent deformation.

  3. Inelastic deformation behavior of thermal barrier coatings exposed at a high-temperature environment

    Directory of Open Access Journals (Sweden)

    Arai M.

    2010-06-01

    Full Text Available Thermal barrier coatings (TBCs are usually deposited onto the surface of the high-temperature component such as gas turbine, in order to protect it from a hightemperature environment. Coating stress generated by such a high-temperature brings serious damages in TBCs in service. For predicting numerically it, it is necessary to develop the constitutive equation suite to plasam-sprayed TBCs. Previous studies have made clear that the freestanding ceramic coat peeled from TBC coated substrate deforms nonlinearly with a mechanical loading, however the results there have been restricted to the test done using as-sprayed sample. In this study, effect of deposition parameter and high-temperature exposure condition on stress-strain curve of the freestanding ceramic coating sample was examined. The associated deformation process was discussed with the microstructure changes observed after performing a bending test for the exposed sample.

  4. Deformation of Semi-Solid Metals - Refining, Strengthening, and Rheological Behavior.

    Science.gov (United States)

    1982-07-15

    described. This work extends earlier studies on " Rheocasting " and has broad, practical implications. The original Rheocast work, sponsored by ARO, led to... Rheocasting has now finally become a commercial reality. The broad area of forming and otherwise processing of metals in the semi-solid state is one that...than Rheocasting , for forming metals in their semi-solid state. And we wondered as well if we might find some way, through deformation in the semi-solid

  5. The role of deformation twinning in the fracture behavior and mechanism of basal textured magnesium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Ando, D., E-mail: dando@material.tohoku.ac.jp; Koike, J.; Sutou, Y.

    2014-04-01

    AZ31 magnesium alloys were deformed to 10% and to failure strain by tensile loading at room temperature. Scribed grids were drawn by a focused ion beam system (FIB) to visualize the local deformation in each grain. This showed that the magnitude of the strain was distributed non-uniformly in each grain. It was found that the low-strain grains accompanied {10–12} twins, while the severely strained grains accompanied {10–11}–{10–12} double twins. Cracks nucleated at the double twins and tended to propagate along {10–12} twin interfaces as well as within grains. Furthermore, fractography revealed three types of microstructural features: dimples, elliptic facets and sheared dimples. Most abundant were the dimples formed by ductile failure. The elliptic facets appeared to be due to crack propagation along the {10–12} twin interfaces. The sheared dimples were frequently observed in connection with localized shear deformation within the double twins. These results led us to conclude that premature and catastrophic failure of Mg alloys is mainly associated with double twins. Prevention of double twinning is essential to improve the ductility of Mg alloys.

  6. [The deformation behavior of human lumbar intervertebral discs subjected to long term axial dynamic compressive forces (author's transl)].

    Science.gov (United States)

    Köller, W; Funke, F; Hartmann, F

    1981-04-01

    49 specimens were studied in 67 axial compression tests; the duration test varied between 2 and 6 hours. All discs showed marked creep; after a big decrease in the first minutes the rate of creep decreases still slightly. Additional the results reveal a decreasing axial deformability with time. In the beginning of a test quickly the viscoelastic behavior alters to such a steady state that the disc behaves more like an elastic body. Loss of mass normally observed after compression tests is due to loss of liquid, but liquid absorption during mechanical load is possible too. The long term biochmechanical behavior is reproducible very well; a second experiment done with the same disc yields nearly the same results.

  7. On the effect of x-ray irradiation on the deformation and fracture behavior of human cortical bone

    Energy Technology Data Exchange (ETDEWEB)

    Barth, Holly D.; Launey, Maximilien E.; McDowell, Alastair A.; Ager III, Joel W.; Ritchie, Robert O.

    2010-01-10

    In situ mechanical testing coupled with imaging using high-energy synchrotron x-ray diffraction or tomography imaging is gaining in popularity as a technique to investigate micrometer and even sub-micrometer deformation and fracture mechanisms in mineralized tissues, such as bone and teeth. However, the role of the irradiation in affecting the nature and properties of the tissue is not always taken into account. Accordingly, we examine here the effect of x-ray synchrotron-source irradiation on the mechanistic aspects of deformation and fracture in human cortical bone. Specifically, the strength, ductility and fracture resistance (both work-of-fracture and resistance-curve fracture toughness) of human femoral bone in the transverse (breaking) orientation were evaluated following exposures to 0.05, 70, 210 and 630 kGy irradiation. Our results show that the radiation typically used in tomography imaging can have a major and deleterious impact on the strength, post-yield behavior and fracture toughness of cortical bone, with the severity of the effect progressively increasing with higher doses of radiation. Plasticity was essentially suppressed after as little as 70 kGy of radiation; the fracture toughness was decreased by a factor of five after 210 kGy of radiation. Mechanistically, the irradiation was found to alter the salient toughening mechanisms, manifest by the progressive elimination of the bone's capacity for plastic deformation which restricts the intrinsic toughening from the formation 'plastic zones' around crack-like defects. Deep-ultraviolet Raman spectroscopy indicated that this behavior could be related to degradation in the collagen integrity.

  8. The influence of martensite shape, concentration, and phase transformation strain on the deformation behavior of stable dual-phase steels

    Science.gov (United States)

    Bhattacharyya, A.; Sakaki, T.; Weng, G. J.

    1993-02-01

    A continuum model is developed to examine the influence of martensite shape, volume fraction, phase transformation strain, and thermal mismatch on the initial plastic state of the ferrite matrix following phase transformation and on the subsequent stress-strain behavior of the dual-phase steels upon loading. The theory is developed based on a relaxed constraint in the ductile matrix and an energy criterion to define its effective stress. In addition, it also assumes the martensite islands to possess a spheroidal shape and to be randomly oriented and homogenously dispersed in the ferrite matrix. It is found that for a typical water-quenched process from an intercritical temperature of 760 °C, the critical martensite volume fraction needed to induce plastic deformation in the ferrite matrix is very low, typically below 1 pct, regardless of the martensite shape. Thus, when the two-phase system is subjected to an external load, plastic deformation commences immediately, resulting in the widely observed “continuous yielding” behavior in dual-phase steels. The subsequent deformation of the dual-phase system is shown to be rather sensitive to the martensite shape, with the disc-shaped morphology giving rise to a superior overall response (over the spherical type). The stress-strain relations are also dependent upon the magnitude of the prior phase transformation strain. The strength coefficient h and the work-hardening exponent n of the smooth, parabolic-type stress-strain curves of the dual-phase system also increase with increasing martensite content for each selected inclusion shape. Comparison with an exact solution and with one set of experimental data indicates that the theory is generally within a reasonable range of accuracy.

  9. Effects of carbon and nitrogen on the tensile deformation behavior of SUS304 and 316 stainless steels at cryogenic temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Miura, Ritsu; Ohnishi, Keizo; Nakajima, Hideo; Shimamoto, Susumu

    1987-04-01

    Effects of C and N contents on the tensile properties and deformation behaviors at low temperatures have been investigated to obtain an alloy design basis on SUS 304 and 316 austenitic stainless steels for cryogenic application. Increase in C and N contents led to the increase in temperature dependency of 0.2% yield strength for both SUS 304 and 316 steels. However, SUS 316 steel showed larger temperature dependency than SUS 304 at the same level of (C + N) content, probably due to the solution strengthening effect of Mo. The results of multiple regression analyses on the effects of C and N contents on the 0.2% yield strength at each temperature indicated that the contributions of both C and N increase with decreasing temperature and that the contribution of N is larger than that of C at low temperatures. The deformation behavior of metastable austenitic steels could be comprehensively explained in relation to austenite stability. Increase in austenite stability resulted in increase in onset strain at which strain-induced martensitic transformation occurred. And increase in austenite stability also led to the decrease in transformation rate which in turn gave rise to lowering strain-hardening exponent. It has been also found that tensile elongation shows maximum at around M/sub d30/ temperature.

  10. The effect of various deformation processes on the corrosion behavior of casing and tubing carbon steels in sweet environment

    Science.gov (United States)

    Elramady, Alyaa Gamal

    The aim of this research project is to correlate the plastic deformation and mechanical instability of casing steel materials with corrosion behavior and surface change, in order to identify a tolerable degree of deformation for casing steel materials. While the corrosion of pipeline and casing steels has been investigated extensively, corrosion of these steels in sweet environments with respect to plastic deformation due to bending, rolling, autofrettage, or handling needs more investigation. Downhole tubular expansion of pipes (casings) is becoming standard practice in the petroleum industry to repair damaged casings, shutdown perforations, and ultimately achieve mono-diameter wells. Tubular expansion is a cold-drawing metal forming process, which consists of running conical mandrels through casings either mechanically using a piston or hydraulically by applying a back pressure. This mechanism subjects the pipes to large radial plastic deformations of up to 30 pct. of the inner diameter. It is known that cold-working is a way of strengthening materials such as low carbon steel, but given that this material will be subjected to corrosive environments, susceptibility to stress corrosion cracking (SCC) should be investigated. This research studies the effect of cold-work, in the form of cold-rolling and cold-expansion, on the surface behavior of API 5CT steels when it is exposed to a CO2-containing environment. Cold-work has a pronounced influence on the corrosion behavior of both API 5CT K55 and P110 grade steels. The lowest strength grade steel, API 5CT K55, performed poorly in a corrosive environment in the slow strain rate test. The ductile material exhibited the highest loss in strength and highest susceptibility to stress corrosion cracking in a CO 2-containing environment. The loss in strength declined with cold-rolling, which can be ascribed to the surface compressive stresses induced by cold-work. On the other hand, API 5CT P110 grade steels showed higher

  11. Mechanical behavior of materials engineering methods for deformation, fracture, and fatigue

    CERN Document Server

    Dowling, Norman E

    2012-01-01

    For upper-level undergraduate engineering courses in Mechanical Behavior of Materials. Mechanical Behavior of Materials, 4/e introduces the spectrum of mechanical behavior of materials, emphasizing practical engineering methods for testing structural materials to obtain their properties, and predicting their strength and life when used for machines, vehicles, and structures. With its logical treatment and ready-to-use format, it is ideal for upper-level undergraduate students who have completed elementary mechanics of materials courses.

  12. Deformation behavior and dynamic recrystallization of Mg-Y-Nd-Gd-Zr alloy

    Institute of Scientific and Technical Information of China (English)

    ZHAO Xin; ZHANG Kui; LI Xinggang; LI Yongjun; HE Qingbiao; SUN Jianfeng

    2008-01-01

    The characteristics of dynamic reerystallization (DRX) in Mg-Y-Nd-Gd-Zr-RE magnesium alloy were investigated by compres-sion tests at temperatures between 523 and 723 K and at strain rates ranging from 0.002 to 1 s-1 with maximum strain of 0.693. The strain-hardening rate can be obtained from true stress-true strain curves, plots of θ-σ,-(θ/ σ)-σ and lnθ-σ in different compression conditions were obtained by further study. The critical condition of the onset of DRX process was determined as ((/ σ)(-θ/ σ))=0. In the range of the above deformation temperature and strain rate, the ratio of critical stress (σc) to peak stress (am) and critical strain (εc) to the peak strain (εm) stood at σc/σm=0.62-0.89 and εc/εm=0.11-0.37, respectively. DRX could be observed during hot deformation process, microstructure evolution of the magnesium alloy at different temperatures and strain rates were studied with the aid of optical microscope(OM), and the average recrystal-lized grain size was measured by means of intercepts on photomicrographs. It was shown that the average dynamically recrystallized grain size (drec) changed with different deformation parameters, the natural logarithm of the average recrystallized grain size varied linearly with the natural logarithm of Zener-Hollomon parameter; the peak stress changed with the average recrystallized grain size, and the natural loga-rithm of the average recrystallized grain size varied linearly with the natural logarithm of the peak stress.

  13. Achieving large macroscopic compressive plastic deformation and work-hardening-like behavior in a monolithic bulk metallic glass by tailoring stress distribution

    Science.gov (United States)

    Chen, L. Y.; Ge, Q.; Qu, S.; Jiang, Q. K.; Nie, X. P.; Jiang, J. Z.

    2008-05-01

    The limited plastic deformation and lack of work hardening seriously restrict the applications of bulk metallic glasses (BMGs). Here, large macroscopic compressive plastic deformation (over 15%) and work-hardening-like behavior were achieved in a monolithic BMG through tailoring loading stress distribution experimentally. Numerical analysis was also carried out to investigate the stress distribution under the same mechanical condition. It is shown that loading induced stress gradient is responsible for the achievement mentioned above.

  14. Evaluation of the thermal-hydraulic response and fuel rod thermal and mechanical deformation behavior during the power burst facility test LOC-3. [PWR

    Energy Technology Data Exchange (ETDEWEB)

    Yackle, T.R.; MacDonald, P.E.; Broughton, J.M.

    1980-01-01

    An evaluation of the results from the LOC-3 nuclear blowdown test conducted in the Power Burst Facility is presented. The test objective was to examine fuel and cladding behavior during a postulated cold leg break accident in a pressurized water reactor (PWR). Separate effects of rod internal pressure and the degree of irradiation were investigated in the four-rod test. Extensive cladding deformation (ballooning) and failure occurred during blowdown. The deformation of the low and high pressure rods was similar; however, the previously irradiated test rod deformed to a greater extent than a similar fresh rod exposed to identical system conditions.

  15. Modeling Transverse Behavior of Kevlar® KM2 Single Fibers with Deformation-induced Damage

    OpenAIRE

    Cheng, Ming; Chen, Weinong

    2006-01-01

    Abstract A phenomenological continuum model is adapted to describe the transverse mechanical behavior of Kevlar? KM2 single fibers in compression. This model could be used for numerical simulations of the mechanical behaviors of fabrics made of Kevlar? KM2 fibers. An equivalent fiber model is used to form the phenomenological model in terms of nominal stress and nominal stretch ratio. Thi...

  16. A numerical and experimental study of temperature effects on deformation behavior of carbon steels at high strain rates

    Science.gov (United States)

    Pouya, M.; Winter, S.; Fritsch, S.; F-X Wagner, M.

    2017-03-01

    Both in research and in the light of industrial applications, there is a growing interest in methods to characterize the mechanical behavior of materials at high strain rates. This is particularly true for steels (the most important structural materials), where often the strain rate-dependent material behavior also needs to be characterized in a wide temperature range. In this study, we use the Finite Element Method (FEM), first, to model the compressive deformation behavior of carbon steels under quasi-static loading conditions. The results are then compared to experimental data (for a simple C75 steel) at room temperature, and up to testing temperatures of 1000 °C. Second, an explicit FEM model that captures wave propagation phenomena during dynamic loading is developed to closely reflect the complex loading conditions in a Split-Hopkinson Pressure Bar (SHPB) – an experimental setup that allows loading of compression samples with strain rates up to 104 s-1 The dynamic simulations provide a useful basis for an accurate analysis of dynamically measured experimental data, which considers reflected elastic waves. By combining numerical and experimental investigations, we derive material parameters that capture the strain rate- and temperature-dependent behavior of the C75 steel from room temperature to 1000 °C, and from quasi-static to dynamic loading.

  17. Deformation behaviors of magnesium alloy AZ31 sheet in cold deep drawing

    Institute of Scientific and Technical Information of China (English)

    YANG Lian-fa; MORI Ken-ichiro; TSUJI Hirokazu

    2008-01-01

    To investigate how the popular magnesium alloy AZ31 sheet (aluminum 3%, zinc 1%) behaves in cold working, deep drawing experiments at room temperature, along with finite element(FE) simulation,were performed on the cold forming sheet of the AZ31 alloy after being annealed under various conditions. The activities were focused on the fracture pattern, limit drawing ratio(LDR), deformation load, thickness distribution, anisotropic effect, as well as the influences of the annealing conditions and tool configuration on them. The results display that punch shoulder radius instead of die clearance, has much influence on the thickness distribution. The anisotropy is remarkable in cold working, which adversely impacts the LDR. The fracture often happens on the side wall at an angle to axis of the deformed specimen. The results also imply that the LDR for the material under present experimental conditions is 1.72, and annealing the material at 450 ℃ for 1 h may be preferable for the cold deep drawing.

  18. A novel unified dislocation density-based model for hot deformation behavior of a nickel-based superalloy under dynamic recrystallization conditions

    Science.gov (United States)

    Lin, Y. C.; Wen, Dong-Xu; Chen, Ming-Song; Chen, Xiao-Min

    2016-09-01

    In this study, a novel unified dislocation density-based model is presented for characterizing hot deformation behaviors in a nickel-based superalloy under dynamic recrystallization (DRX) conditions. In the Kocks-Mecking model, a new softening item is proposed to represent the impacts of DRX behavior on dislocation density evolution. The grain size evolution and DRX kinetics are incorporated into the developed model. Material parameters of the developed model are calibrated by a derivative-free method of MATLAB software. Comparisons between experimental and predicted results confirm that the developed unified dislocation density-based model can nicely reproduce hot deformation behavior, DRX kinetics, and grain size evolution in wide scope of initial grain size, strain rate, and deformation temperature. Moreover, the developed unified dislocation density-based model is well employed to analyze the time-variant forming processes of the studied superalloy.

  19. A coupled analysis of fluid flow, heat transfer and deformation behavior of solidifying shell in continuously cast beam blank

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Jung Eui; Yeo, Tae Jung; Oh, Kyu Hwan; Yoon, Jong Kyu [School of Materials Science and Engineering, Seoul Nat`l Univ., Seoul (Korea, Republic of); Han, Heung Nam [Oxford Center for Advanced Materials and Composites, Department of Materials, Univ. of Oxford (United Kingdom)

    1997-12-31

    A mathematical model for a coupled analysis of fluid flow, heat transfer and deformation behavior in the continuously cast beam blank has been developed. The fluid flow, heat transfer and solidification in the mold region were analyzed with 3-dimensional finite difference method (FDM) based on control volume method. A body fitted coordinate system was introduced for the complex geometry of the beam blank. The effects of turbulence and natural convection of molten steel were taken into account in determining the fluid flow in the strand. The thermo-elasto-plastic deformation behavior in the cast strand and the formation of air gap between the solidifying shell and the mold were analyzed by the finite element method (FEM) using the 2-dimensional slice temperature profile calculated by the FDM. The heat flow between the strand and the mold was evaluated by the coupled analysis between the fluid flow-heat transfer analysis and the thermo-elasto-plastic stress analysis. In order to determine the solid fraction in the mushy zone, the microsegregation of solute element was assessed. The effects of fluid flow on the heat transfer, the solidification of steel and the distribution of shell thickness during the casting of the beam blank were simulated. The deformation behavior of the solidifying shell and the possibility of cracking of the strand were also investigated. The recirculating flows were developed in the regions of the web and the flange tip. The impinging of the inlet flow from the nozzle retarded the growing of solidifying shell in the regions of the fillet and the flange. The air gap between the strand and the mold was formed near the region of the corner of the flange tip. At the initial stage of casting, the probability of the surface cracking was high in the regions of the fillet and the flange tip. After the middle stage of casting, the internal cracking was predicted in the regions of the flange tip, and between the fillet and the flange tip. (author) 38

  20. Effects of low temperature neutron irradiation on deformation behavior of austenitic stainless steels

    Energy Technology Data Exchange (ETDEWEB)

    Pawel, J.E.; Rowcliffe, A.F.; Alexander, D.J.; Grossbeck, M.L. [Oak Ridge National Laboratory, TN (United States); Shiba, K.

    1996-04-01

    An austenitic stainless steel, designated 316LN-IG, has been chosen for the first wall/shield (FW/S) structure for the International Thermonuclear Experimental Reactor (ITER). The proposed operational temperature range for the structure (100 to 250{degree}C) is below the temperature regimes for void swelling (400-600{degree}C) and for helium embrittlement (500-700{degree}C). However, the proposed neutron dose is such that large changes in yield strength, deformation mode, and strain hardening capacity could be encountered which could significantly affect fracture properties. Definition of the irradiation regimes in which this phenomenon occurs is essential to the establishment of design rules to protect against various modes of failure.

  1. Behavior of highly deformable relaxor-ferroelectric-based ceramics in an electric field

    Science.gov (United States)

    Talanov, M. V.; Reznichenko, L. A.

    2013-10-01

    The deformation characteristics of multicomponent barium-doped piezoelectric ceramics mPbMg1/3Nb2/3O3- n PbNi1/3Nb2/3O3- y PbZn1/3Nb2/3O3- x PbTiO3 are studied in electric fields E = 0-12 kV/cm. Anomalies are detected in the dependences of elastic strain ξ3 and piezoelectric modulus d {33/eff} on the external dc electric field. The history of the materials is shown to affect the change of piezoelectric modulus d {33/eff} in an electric field. The revealed dependences are used to propose a method to increase the efficiency of operation of piezoelectric actuators.

  2. Dynamic behavior of a rotating delaminated composite beam including rotary inertia and shear deformation effects

    Directory of Open Access Journals (Sweden)

    Ramazan-Ali Jafari-Talookolaei

    2015-09-01

    Full Text Available A finite element (FE model is developed to study the free vibration of a rotating laminated composite beam with a single delamination. The rotary inertia and shear deformation effects, as well as the bending–extension, bending–twist and extension–twist coupling terms are taken into account in the FE model. Comparison between the numerical results of the present model and the results published in the literature verifies the validity of the present model. Furthermore, the effects of various parameters, such as delamination size and location, fiber orientation, hub radius, material anisotropy and rotating speed, on the vibration of the beam are studied in detail. These results provide useful information in the study of the free vibration of rotating delaminated composite beams.

  3. Large-deformation and long-time behavior of entangled melts in complex geometries

    Science.gov (United States)

    Zhu, Xiangyang; Wang, Shi-Qing

    2012-02-01

    Recent particle-tracking velocimetric (PTV) observations have revealed strain localization either during startup shear beyond the stress overshoot or after a large step shear of entangled polymers [e.g., Macromolecules, 42, 6261 (2009)]. The physical pictures leading to these decohesion events have been put forward [J. Chem. Phys. 127, 064903(2007); J. Rheol. 53, 1389 (2009)]. In this presentation we apply the particle-tracking velocimetric method [Macromol. Mater. Engr. 292, 15 (2007)] to study similar strain localization phenomena originating from yielding of the entanglement network in other forms of deformation including uniaxial extension, ``squeeze flow'' and extrusion of polymers from a wide open space into a narrow opening. The striking discontinuities in the velocity profile can all be understood in terms of a shear yielding criterion. The research is funded, in part, by a grant from the National Science Foundation (CMMI-0926522)

  4. Cyclic Deformation Behavior and Fatigue Crack Propagation of Low Carbon Steel Prestrained in Tension

    Directory of Open Access Journals (Sweden)

    J. G. Wang

    2009-01-01

    Full Text Available The tests were performed on low carbon steel plate. In the tension fatigue tests, two angle values (ϕ=0° and ϕ=45°, ϕ is the angle between the loading and the rolling direction have been chosen. The influence of strain path change on the subsequent initial work softening rate and the saturation stress has been investigated. Dislocation microstructure was observed by transmission electron microscopy. It was found that the strain amount of preloading in tension has obviously affected the cyclic softening phenomenon and the initial cyclic softening rate. It was observed that the reloading axial stress for ϕ=45° case increased more than that of ϕ=0° case, due to the anisotropism of Q235. In the fatigue crack propagation tests, the experimental results show that with increasing the pretension deformation degree, the fatigue crack growth rate increases, especially at the near threshold section.

  5. Characterization of Hot Deformation Behavior of a Fe-Cr-Ni-Mo-N Superaustenitic Stainless Steel Using Dynamic Materials Modeling

    Science.gov (United States)

    Pu, Enxiang; Zheng, Wenjie; Song, Zhigang; Feng, Han; Zhu, Yuliang

    2017-02-01

    Hot deformation behavior of a Fe-24Cr-22Ni-7Mo-0.5N superaustenitic stainless steel was investigated by hot compression tests in a wide temperature range of 950-1250 °C and strain rate range of 0.001-10 s-1. The flow curves show that the flow stress decreases as the deformation temperature increases or the strain rate decreases. The processing maps developed on the basis of the dynamic materials model and flow stress data were adopted to optimize the parameters of hot working. It was found that the strain higher than 0.2 has no significant effect on the processing maps. The optimum processing conditions were in the temperature range of 1125-1220 °C and strain rate range of 0.1-3 s-1. Comparing to other stable domains, microstructural observations in this domain revealed the complete dynamic recrystallization (DRX) with finer and more uniform grain size. Flow instability occurred in the domain of temperature lower than 1100 °C and strain rate higher than 0.1 s-1.

  6. Late Quaternary surface deformation and rupture behavior of strong earthquake on the segment north of Mianning of the Anninghe fault

    Institute of Scientific and Technical Information of China (English)

    RAN YongKang; CHEN LiChun; CHENG JianWu; GONG HuiLing

    2008-01-01

    The Anninghe fault is an important active fault along the eastern boundary of Sichuan-Yunnan active tectonic block, and the study of its surface deformation and rupture behavior during strong earthquake in the late Quaternary is of fundamental importance for understanding the future seismic risk of the fault zone or even the entire western Sichuan region.Using the methods of detailed geomorphic and geological survey, digital image analysis, total station instrument survey, excavation of combined trench and dating, we analyze the geomorphologic sequences of the offset strata at several sites where the late Quaternary deformation remnants are fairly well preserved and obtain some new results as follows: Strong earthquake events with left-lateral displacements of about 3 m occurred at the two sites of Zimakua and Yejitong at 1634-1811,1030-1050 and 280-550 a BP, respectively, and the recurrence interval is 520-660 a; The youngest event in the area of Dahaizi-Ganhaizi should be the earthquake of 1536, other events are at 1768-1826, 2755-4108 and 4108-6593 a BP, respectively, with a recurrence interval of 1300-1900 a.The strong earthquake activity shows a clustering character.The possibility of occurrence of a strong earthquake exists on the north segment of the Anninghe fault sometime in the future.

  7. Late Quaternary surface deformation and rupture behavior of strong earthquake on the segment north of Mianning of the Anninghe fault

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    The Anninghe fault is an important active fault along the eastern boundary of Sichuan-Yunnan active tectonic block, and the study of its surface deformation and rupture behavior during strong earthquake in the late Quaternary is of fundamental importance for understanding the future seismic risk of the fault zone or even the entire western Sichuan region. Using the methods of detailed geomorphic and geological survey, digital image analysis, total station instrument survey, excavation of combined trench and dating, we analyze the geomorphologic sequences of the offset strata at several sites where the late Quaternary deformation remnants are fairly well preserved and obtain some new results as follows: Strong earthquake events with left-lateral displacements of about 3 m occurred at the two sites of Zimakua and Yejitong at 1634-1811, 1030-1050 and 280-550 a BP, respectively, and the recurrence interval is 520-660 a; The youngest event in the area of Dahaizi-Ganhaizi should be the earthquake of 1536, other events are at 1768-1826, 2755-4108 and 4108-6593 a BP, respectively, with a recurrence interval of 1300-1900 a. The strong earthquake activity shows a clustering character. The possibility of occurrence of a strong earthquake exists on the north segment of the Anninghe fault sometime in the future.

  8. Microstructure and hot deformation behavior of A356/Al2O3 composite fabricated by infiltration method

    Science.gov (United States)

    Yu, Seung-Baek; Jeon, Kyung-Soo; Kim, Mok-Soon; Lee, Jeung-Keun; Ryu, Kwan-Ho

    2017-07-01

    The hot deformation behavior of an A356/Al2O3 composite fabricated by the infiltration method was characterized in the temperature range of 300-500 °C and strain rate range of 0.001-1/s using compressive tests. The composite consists of an Al-Si based matrix and nano-sized Al2O3 particulates. A constitutive model was established based on the hyperbolic sine Arrhenius type equation and its hot workability was evaluated by means of processing maps based on Dynamic Material Modeling. The activation energy for hot deformation was calculated to be 223 kJ/mol, which is higher than the activation energy for self-diffusion of pure aluminum (142 kJ/mol). The optimum processing condition for the hot working of the composite was found to exist at 500 °C with a strain rate of 1/s, where a dynamic recrystallized microstructure was observed and the maximum efficiency was exhibited in the processing map. Voids were frequently detected at 500 °C with lower strain rates, deteriorating the workability of the composite.

  9. Response of the electron work function to deformation and yielding behavior of copper under different stress states

    Energy Technology Data Exchange (ETDEWEB)

    Li Wen [Dept. of Mechanical Engineering, Changchun University (China); Dept. of Chemical and Materials Engineering, University of Alberta, Edmonton, Alberta (Canada); Wang, Y.; Li, D.Y. [Dept. of Chemical and Materials Engineering, University of Alberta, Edmonton, Alberta (Canada)

    2004-07-01

    The high sensitivity of the electron work function (EWF) to surface condition has attracted increasing interests from materials scientists and engineers. In this study, using a scanning Kelvin probe changes in the EWF of copper under various loading condition and stress states were investigated. Experimental results showed that the tensile strain decreased the EWF in the elastic deformation range, while compressive strain increased the EWF. However, the EWF in the plastic deformation range always decreased with plastic strain no matter it was tensile or compressive. As shown by the simultaneous measurements of the EWF under conditions of plane stress states, yielding point can be related to the critical stress for the transition of the EWF from smooth variation to steep variation, which strongly depended on stress states. It was therefore demonstrated that Kelvin probing technique could be used for determining the onset of yielding since the EWF was a parameter sensitive to yielding process. The Kelvin probing has appeared to be a very promising method for characterizing the yielding behaviors under complex stress states for both homogeneous and inhomogeneous materials. (copyright 2004 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  10. Effect of electropulsing on deformation behavior, texture and microstructure of 5A02 aluminum alloy during uniaxial tension

    Energy Technology Data Exchange (ETDEWEB)

    Yan, Cong; Li, Ning, E-mail: hslining@mail.hust.edu.cn; Jiang, Huawen; Wang, Duzhen; Liu, Lin

    2015-06-25

    The effect of electropulsing on the deformation behavior, texture and microstructure of 5A02 aluminum alloy was investigated through uniaxial tension, electron backscattered diffraction (EBSD) and transmission electron microscope (TEM). The Portevin-Le Chatelier (PLC) effect reflected as the serrated characteristic in stress–strain curves, became conspicuous firstly but then disappeared with further increase of electropulsing intensity. The texture analysis exhibited that the electropulsing causes an increase of Cube texture, accompanied with a reduction of S texture. Microstructure characterization revealed a transition of slipping mode from planar slip to wave slip with increasing electropulsing intensity. The temperature rise induced by electropulsing, together with the influence of solute atoms, was proposed to rationalize the present phenomena in detail.

  11. Effect of strain rates on deformation behaviors of an in situ Ti-based metallic glass matrix composite

    Science.gov (United States)

    Jiao, Z. M.; Wang, Z. H.; Chu, M. Y.; Wang, Y. S.; Yang, H. J.; Qiao, J. W.

    2016-06-01

    Quasi-static and dynamic deformation behaviors of an in situ dendrite-reinforced metallic glass matrix composite: Ti56Zr18V10Cu4Be12 were investigated. Upon quasi-static compression, the composite exhibits distinguished work hardening, accompanied by the ultimate strength of 1290 MPa and the plasticity of 20 %. The improved plasticity is attributed to the multiplication of shear bands within the glass matrix and pileups of dislocations within the dendrites. Upon dynamic compression, the stable plastic flow prevails and the yielding stress increases with the strain rate. The macroscopic plasticity decreases considerably, since the shear bands cannot be effectively hindered by dendrites with deteriorated toughness. The dendrite-dominated mechanism results in the positive strain-rate sensitivity, and the Cowper-Symonds model is employed to depict the strain-rate dependency of yielding strength.

  12. Effects of Severe Plastic Deformation and Heat Treatment on Transformation Behavior of Explosively Welded Duplex TiNi-TiNi

    Institute of Scientific and Technical Information of China (English)

    Li Juntao; Zheng Yanjun; Cui Lishan

    2007-01-01

    The effects of severe plastic deformation and heat treatment on the transformation behavior of explosively welded duplex TiNi-TiNi shape memory alloys (SMAs) were investigated by differential scanning calorimeter (DSC) measurements. The explosively welded duplex TiNi-TiNi plate of 0.7 mm thickness was cold-rolled at room temperature to a 60% reduction in thickness and then annealed at different temperatures for different durations. The results showed that low temperature (623-723K) heat-treatment led to the crystallization of the amorphous region, and re-crystallization occurred in the specimens annealed at higher temperatures (over 873 K). Research indicated that the change of martensitic transformation temperature is due to the change of internal stresses with increasing heat treatment temperature. The change of annealing time also led to a change in martensitic transformation temperature, which was associated with the precipitation and decomposition of Ti3Ni4 in TiNi-1.

  13. Microstructure, elastic deformation behavior and mechanical properties of biomedical β-type titanium alloy thin-tube used for stents.

    Science.gov (United States)

    Tian, Yuxing; Yu, Zhentao; Ong, Chun Yee Aaron; Kent, Damon; Wang, Gui

    2015-05-01

    Cold-deformability and mechanical compatibility of the biomedical β-type titanium alloy are the foremost considerations for their application in stents, because the lower ductility restricts the cold-forming of thin-tube and unsatisfactory mechanical performance causes a failed tissue repair. In this paper, β-type titanium alloy (Ti-25Nb-3Zr-3Mo-2Sn, wt%) thin-tube fabricated by routine cold rolling is reported for the first time, and its elastic behavior and mechanical properties are discussed for the various microstructures. The as cold-rolled tube exhibits nonlinear elastic behavior with large recoverable strain of 2.3%. After annealing and aging, a nonlinear elasticity, considered as the intermediate stage between "double yielding" and normal linear elasticity, is attributable to a moderate precipitation of α phase. Quantitive relationships are established between volume fraction of α phase (Vα) and elastic modulus, strength as well as maximal recoverable strain (εmax-R), where the εmax-R of above 2.0% corresponds to the Vα range of 3-10%. It is considered that the "mechanical" stabilization of the (α+β) microstructure is a possible elastic mechanism for explaining the nonlinear elastic behavior.

  14. Mechanical Deformation Behavior of Sn-Ag-Cu Solders with Minor Addition of 0.05 wt.% Ni

    Science.gov (United States)

    Hammad, A. E.; El-Taher, A. M.

    2014-11-01

    The aim of the present work is to develop a comparative evaluation of the microstructural and mechanical deformation behavior of Sn-Ag-Cu (SAC) solders with the minor addition of 0.05 wt.% Ni. Test results showed that, by adding 0.05Ni element into SAC solders, generated mainly small rod-shaped (Cu,Ni)6Sn5 intermetallic compounds (IMCs) inside the β-Sn phase. Moreover, increasing the Ag content and adding Ni could result in the change of the shape and size of the IMC precipitate. Hence, a significant improvement is observed in the mechanical properties of SAC solders with increasing Ag content and Ni addition. On the other hand, the tensile results of Ni-doped SAC solders showed that both the yield stress and ultimate tensile strengths decrease with increasing temperature and with decreasing strain rate. This behavior was attributed to the competing effects of work hardening and dynamic recovery processes. The Sn-2.0Ag-0.5Cu-0.05Ni solder displayed the highest mechanical properties due to the formation of hard (Cu,Ni)6Sn5 IMCs. Based on the obtained stress exponents and activation energies, it is suggested that the dominant deformation mechanism in SAC (205)-, SAC (0505)- and SAC (0505)-0.05Ni solders is pipe diffusion, and lattice self-diffusion in SAC (205)-0.05Ni solder. In view of these results, the Sn-2.0Ag-0.5Cu-0.05Ni alloy is a more reliable solder alloy with improved properties compared with other solder alloys tested in the present work.

  15. Effect of heat treatment on tensile and fatigue deformation behavior of extruded Al-12 wt%Si alloy

    Science.gov (United States)

    Ham, Gi-Su; Baek, Min-Seok; Kim, Jong-Ho; Lee, Si-Woo; Lee, Kee-Ahn

    2017-01-01

    This study investigated the effect of heat treatment on tensile and high-cycle fatigue deformation behavior of extruded Al-12 wt%Si alloy. The material used in this study was extruded at a ratio of 17.7: 1 through extrusion process. To identify the effects of heat treatment, T6 heat treatment (515 °C/1 h, water quenching, and then 175 °C/10 h) was performed. Microstructural observation identified Si phases aligned in the extrusion direction in both extruded alloy (F) and heat treated alloy (T6). The average grain size of F alloy was 8.15 °C, and that of T6 alloy was 8.22 °C. Both alloys were composed of Al matrix, Si, Al2Cu, Al3Ni and AlFeSi phases. As T6 heat treatment was applied, Al2Cu phases became more finely and evenly distributed. Tensile results confirmed that yield strength increased from 119.0 MPa to 329.0 MPa, ultimate tensile strength increased from 226.8 MPa to 391.4 MPa, and the elongation decreased from 16.1% to 5.0% as T6 heat treatment was applied. High-cycle fatigue results represented F alloy's fatigue limit as 185 MPa and T6 alloy's fatigue limit as 275 MPa, indicating that high-cycle fatigue properties increased significantly as heat treatment was conducted. Through tensile and fatigue fracture surface analysis, this study considered the deformation behaviors of extruded and heat treated Al-Si alloys in relation to their microstructures.

  16. High-Temperature Deformation Behavior of a Ti-6Al-7Nb Alloy in Dual-Phase (α + β) and Single-Phase (β) Regions

    Science.gov (United States)

    Pilehva, F.; Zarei-Hanzaki, A.; Moemeni, S.; Khalesian, A. R.

    2016-01-01

    The present study aimed to characterizing the microstructure evolution of a Ti-6Al-7Nb biomedical type titanium alloy during hot working through hot compression tests. The hot deformation cycles were conducted under the strain rate of 0.0025, 0.025, and 0.25 s-1 in the temperature range of 850-1150 °C where both dual-phase (α + β) and single-phase (β) regions could be accessible. The flow stress behavior of the material for the entire deformation regime was interpreted via microstructural observations. The results indicated that in the single-phase β region (1050-1150 °C), the dynamically recrystallized (DRX) grains were formed at the deformed and elongated beta grain boundaries as a necklace-like structure. The variations in the dynamically recrystallized grain size were determined to follow the Zener-Hollomon relationship where DRX grain size was decreased by reducing the temperature and increasing the strain rate. The alloy deformation characteristics in α + β region were somewhat different. During deformation in the upper α + β temperature range (e.g., 1000 °C), the β phase would accommodate most of the deformation, while α regions remained undeformed. In the lower α + β temperature range (e.g., 850-950 °C), the kinking/bending of α lamellae as well as the subsequent globularization of α layers were postulated to be responsible for the observed flow softening behavior.

  17. A Study on the Hot Deformation Behavior of 47Zr-45Ti-5Al-3V Alloy with Initial Lamellar α Structure

    Science.gov (United States)

    Tan, Yuanbiao; Ji, Liyuan; Duan, Jingli; Liu, Wenchang; Zhang, Jingwu; Liu, Riping

    2016-09-01

    The hot deformation behavior of the 47Zr-45Ti-5Al-3V (wt pct) alloy with initial lamellar α structure was investigated by compression tests in the temperature range of 823 K to 1073 K (550 °C to 800 °C) and strain rate range of 10-3 to 100 s-1. In the α + β phase field, the flow curves exhibited a continuous flow softening. The extent of flow softening first decreased with increasing strain rate from 10-3 to 10-1 s-1, and then increased with further increasing strain rate to 100 s-1. In the single β phase field, the flow curves exhibited a pronounced stress drop at the very beginning of deformation at low temperatures and high strain rates. The magnitude of the stress drop increased with decreasing deformation temperature and increasing strain rate. At higher temperatures and lower strain rates, the flow curves exhibited typical characteristics of dynamic recrystallization. A hyperbolic-sine Arrhenius-type equation was used to characterize the dependence of the flow stress on deformation temperature and strain rate. The activation energy for deformation at different strains was calculated. In the α + β phase field, the activation energy for deformation increased from 333 to 355 kJ/mol with increasing strain, and then decreased to 312 kJ/mol. In the single β phase, the activation energy for deformation decreased from 169 to 136 kJ/mol with increasing strain.

  18. A Study on the Hot Deformation Behavior of 47Zr-45Ti-5Al-3V Alloy with Initial Lamellar α Structure

    Science.gov (United States)

    Tan, Yuanbiao; Ji, Liyuan; Duan, Jingli; Liu, Wenchang; Zhang, Jingwu; Liu, Riping

    2016-12-01

    The hot deformation behavior of the 47Zr-45Ti-5Al-3V (wt pct) alloy with initial lamellar α structure was investigated by compression tests in the temperature range of 823 K to 1073 K (550 °C to 800 °C) and strain rate range of 10-3 to 100 s-1. In the α + β phase field, the flow curves exhibited a continuous flow softening. The extent of flow softening first decreased with increasing strain rate from 10-3 to 10-1 s-1, and then increased with further increasing strain rate to 100 s-1. In the single β phase field, the flow curves exhibited a pronounced stress drop at the very beginning of deformation at low temperatures and high strain rates. The magnitude of the stress drop increased with decreasing deformation temperature and increasing strain rate. At higher temperatures and lower strain rates, the flow curves exhibited typical characteristics of dynamic recrystallization. A hyperbolic-sine Arrhenius-type equation was used to characterize the dependence of the flow stress on deformation temperature and strain rate. The activation energy for deformation at different strains was calculated. In the α + β phase field, the activation energy for deformation increased from 333 to 355 kJ/mol with increasing strain, and then decreased to 312 kJ/mol. In the single β phase, the activation energy for deformation decreased from 169 to 136 kJ/mol with increasing strain.

  19. Hot deformation behavior of 51.1Zr–40.2Ti–4.5Al–4.2V alloy in the single β phase field

    Directory of Open Access Journals (Sweden)

    Jingli Duan

    2015-02-01

    Full Text Available The hot deformation behavior of a newly developed 51.1Zr–40.2Ti–4.5Al–4.2 V alloy was investigated by compression tests in the deformation temperature range from 800 to 1050 °C and strain rate range from 10−3 to 100 s−1. At low temperatures and high strain rates, the flow curves exhibited a pronounced stress drop at the very beginning of deformation, followed by a slow decrease in flow stress with increasing strain. The magnitude of the stress drop increased with decreasing deformation temperature and increasing strain rate. At high temperatures and low strain rates, the flow curves exhibited typical characteristics of dynamic recrystallization. A hyperbolic-sine Arrhenius-type equation was used to characterize the dependences of the flow stress on deformation temperature and strain rate. The activation energy for hot deformation decreased slightly with increasing strain and then tended to be a constant value. A microstructural mechanism map was presented to help visualize the microstructure of this alloy under different deformation conditions.

  20. Strain rate dependent deformation and failure behavior of laser welded DP780 steel joint under dynamic tensile loading

    Energy Technology Data Exchange (ETDEWEB)

    Liu, Yang, E-mail: liuyang@mail.neu.edu.cn [Key Laboratory for Anisotropy and Texture of Materials, Ministry of Education, Northeastern University, Shenyang 110819 (China); Dong, Danyang, E-mail: dongdanyang@mail.neu.edu.cn [College of Science, Northeastern University, Shenyang 110819 (China); Wang, Lei, E-mail: wanglei@mail.neu.edu.cn [Key Laboratory for Anisotropy and Texture of Materials, Ministry of Education, Northeastern University, Shenyang 110819 (China); Chu, Xi, E-mail: chuxi.ok@163.com [College of Science, Northeastern University, Shenyang 110819 (China); Wang, Pengfei, E-mail: wpf1963871400@163.com [College of Science, Northeastern University, Shenyang 110819 (China); Jin, Mengmeng, E-mail: 24401878@163.com [College of Science, Northeastern University, Shenyang 110819 (China)

    2015-03-11

    Laser welded DP steel joints are used widely in the automotive industry for weight reduction. Understanding the deformation and fracture behavior of the base metal (BM) and its welded joint (WJ), especially at high strain rates, is critical for the design of vehicle structures. This paper is concerned with the effects of strain rate on the tensile properties, deformation and fracture behavior of the laser welded DP780 steel joint. Quasi-static and dynamic tensile tests were performed on the WJ and BM of the DP780 steel using an electromechanical universal testing machine and a high-speed tensile testing machine over a wide range of strain rate (0.0001–1142 s{sup −1}). The microstructure change and microhardness distribution of the DP780 steel after laser welding were examined. Digital image correlation (DIC) and high-speed photography were employed for the strain measurement of the DP780 WJ during dynamic tensile tests. The DP780 WJ is a heterogeneous structure with hardening in fusion zone (FZ) and inner heat-affected zone (HAZ), and softening in outer HAZ. The DP780 BM and WJ exhibit positive strain rate dependence on the YS and UTS, which is smaller at lower strain rates and becomes larger with increasing strain rate, while ductility in terms of total elongation (TE) tends to increase under dynamic loading. Laser welding leads to an overall reduction in the ductility of the DP780 steel. However, the WJ exhibits a similar changing trend of the ductility to that of the BM with respect to the strain rate over the whole strain rate range. As for the DP780 WJ, the distance of tensile failure location from the weld centerline decreases with increasing strain rate. The typical ductile failure characteristics of the DP780 BM and WJ do not change with increasing strain rate. DIC measurements reveal that the strain localization starts even before the maximum load is attained in the DP780 WJ and gradual transition from uniform strains to severely localized strains

  1. High temperature deformation behavior, thermal stability and irradiation performance in Grade 92 steel

    Science.gov (United States)

    Alsagabi, Sultan

    The 9Cr-2W ferritic-martensitic steel (i.e. Grade 92 steel) possesses excellent mechanical and thermophysical properties; therefore, it has been considered to suit more challenging applications where high temperature strength and creep-rupture properties are required. The high temperature deformation mechanism was investigated through a set of tensile testing at elevated temperatures. Hence, the threshold stress concept was applied to elucidate the operating high temperature deformation mechanism. It was identified as the high temperature climb of edge dislocations due to the particle-dislocation interactions and the appropriate constitutive equation was developed. In addition, the microstructural evolution at room and elevated temperatures was investigated. For instance, the microstructural evolution under loading was more pronounced and carbide precipitation showed more coarsening tendency. The growth of these carbide precipitates, by removing W and Mo from matrix, significantly deteriorates the solid solution strengthening. The MX type carbonitrides exhibited better coarsening resistance. To better understand the thermal microstructural stability, long tempering schedules up to 1000 hours was conducted at 560, 660 and 760°C after normalizing the steel. Still, the coarsening rate of M23C 6 carbides was higher than the MX-type particles. Moreover, the Laves phase particles were detected after tempering the steel for long periods before they dissolve back into the matrix at high temperature (i.e. 720°C). The influence of the tempering temperature and time was studied for Grade 92 steel via Hollomon-Jaffe parameter. Finally, the irradiation performance of Grade 92 steel was evaluated to examine the feasibility of its eventual reactor use. To that end, Grade 92 steel was irradiated with iron (Fe2+) ions to 10, 50 and 100 dpa at 30 and 500°C. Overall, the irradiated samples showed some irradiation-induced hardening which was more noticeable at 30°C. Additionally

  2. Deformation Behaviors of HIPped Foil Compared with Those of Sheet Titanium Alloys

    Science.gov (United States)

    Castelli, Michael G.

    1999-01-01

    Micromechanics-based modeling of composite material behaviors requires an accurate assessment of the constituent properties and behaviors. For the specific case of continuous-fiber-reinforced metal matrix composites (MMC's) manufactured from a foil/fiber/foil process, much emphasis has been placed on characterizing foil-based matrix materials that have been fabricated in the same way as the composite. Such materials are believed to yield mechanical properties and behaviors that are representative of the matrix constituent within the composite (in situ matrix). Therefore, these materials are desired for micromechanics modeling input. Unfortunately, such foils are extremely expensive to fabricate and procure because of the labor-intensive rolling process needed to produce them. As a potential solution to this problem that would maintain appropriately representative in situ properties, the matrix constituent could be characterized with sheet-based materials, which are considerably less expensive to manufacture than foils, are more readily procured, and result in fewer plies to obtain a desired panel thickness. The critical question is, however, does the consolidated sheet material exhibit the same properties and behaviors as do the consolidated foils? Researchers at NASA Lewis Research Center's Life Prediction Branch completed a detailed experimental investigation to answer this question for three titanium alloys commonly used in metal matrix composite form.

  3. Hot Deformation Behavior of GH738 for A-USC Turbine Blades

    Institute of Scientific and Technical Information of China (English)

    Li WANG; Gang YANG; Ting LEI; Shu-biao YIN; Lu WANG

    2015-01-01

    The hot deformation characteristics of GH738 superalloy over the temperature range of 1 000 °C to 1 200 °C and strain range of 0.01 s−1to 10.0 s−1under a strain of 1.0 s−1 were investigated through hot compression tests with a Gleeble-1500 simulation machine. The lfow stress reached peak value before lfow softening occurred. The average apparent activation energy (Q) of GH738 was calculated to be 430 kJ/mol, and the stress index (n) is approximately 4.08. The processing map was developed based on lfow stress data and dynamic materials model (DMM). The map shows a dynamic recrystallization (DRX) domain in 1 050 °C to 1 150 °C and 0.01 s−1 to 1.0 s−1 strain rate range with a peak efifciency of 45%, which is considered to be the optimum region for hot working. Moreover, the materials undergo lfow instability in the temperature range of 1 000 °C to 1 050 °C and strain range of 1.0 s−1to 10.0 s−1, and adiabatic shear bands can be observed in this domain.

  4. Deformation behavior of FRP-metal composites locally reinforced with carbon fibers

    Science.gov (United States)

    Scholze, M.; Kolonko, A.; Lindner, T.; Lampke, T.; Helbig, F.

    2016-03-01

    This study investigates variations of hybrid laminates, consisting of one aluminum sheet and a unidirectional glass fiber (GF) reinforced polyamide 6 (PA6) basic structure with partial carbon fiber (CF) reinforcement. To create these heterogeneous FRP laminates, it is necessary to design and produce semi-finished textile-based products. Moreover, a warp knitting machine in conjunction with a warp thread offset unit was used to generate bionic inspired compounds. By the variation of stacking prior to the consolidation process of the hybrid laminate, an oriented CF reinforcement at the top and middle layer of the FRP is realized. In both cases the GFRP layer prevents contact between the aluminum and carbon fibers. In so doing, the high strength of carbon fibers can be transferred to the hybrid laminate in load directions with an active prevention of contact corrosion. The interface strength between thermoplastic and metal component was improved by a thermal spray coating on the aluminum sheet. Because of the high surface roughness and porosity, mechanical interlock was used to provide high interface strength without bonding agents between both components. The resulting mechanical properties of the hybrid laminates are evaluated by three point bending tests in different load directions. The effect of local fiber orientation and layer positioning on failure and deformation mechanism is additionally investigated by digital image correlation (DIC).

  5. On The Creep Behavior and Deformation Mechanisms Found in an Advanced Polycrystalline Nickel-Base Superalloy at High Temperatures

    Science.gov (United States)

    Deutchman, Hallee Zox

    Polycrystalline Ni-base superalloys are used as turbine disks in the hot section in jet engines, placing them in a high temperature and stress environment. As operating temperatures increase in search of better fuel efficiency, it becomes important to understand how these higher temperatures are affecting mechanical behavior and active deformation mechanisms in the substructure. Not only are operating temperatures increasing, but there is a drive to design next generation alloys in shorter time periods using predictive modeling capabilities. This dissertation focuses on mechanical behavior and active deformation mechanisms found in two different advanced polycrystalline alloy systems, information which will then be used to build advanced predictive models to design the next generation of alloys. The first part of this dissertation discusses the creep behavior and identifying active deformation mechanisms in an advanced polycrystalline Ni-based superalloy (ME3) that is currently in operation, but at higher temperatures and stresses than are experienced in current engines. Monotonic creep tests were run at 700°C and between 655-793MPa at 34MPa increments, on two microstructures (called M1 and M2) produced by different heat treatments. All tests were crept to 0.5% plastic strain. Transient temperature and transient stress tests were used determine activation energy and stress exponents of the M1 microstructure. Constant strain rate tests (at 10-4s-1) were performed on both microstructures as well. Following creep testing, both M1 and M2 microstructures were fully characterized using Scanning Electron Microscopy (SEM) for basic microstructure information, and Scanning Transmission Electron Microscopy (STEM) to determine active deformation mechanism. It was found that in the M1 microstructure, reorder mediated activity (such as discontinuous faulting and microtwinning) is dominant at low stresses (655-724 MPa). Dislocations in the gamma matrix, and overall planar

  6. Effect of two-stage aging on superplasticity of Al-Li alloy

    Institute of Scientific and Technical Information of China (English)

    LUO Zhi-hui; ZHANG Xin-ming; DU Yu-xuan; YE Ling-ying

    2006-01-01

    The effect of two-stage aging on the microstructures and superplasticity of 01420 Al-Li alloy was investigated by means of OM, TEM analysis and stretching experiment. The results demonstrate that the second phase particles distributed more uniformly with a larger volume fraction can be observed after the two-stage aging (120 ℃, 12 h+300 ℃, 36 h) compared with the single-aging(300 ℃, 48 h). After rolling and recrystallization annealing, fine grains with size of 8-10 μm are obtained, and the superplastic elongation of the specimens reaches 560% at strain rate of 8×10-4 s-1 and 480 ℃. Uniformly distributed fine particles precipitate both on grain boundaries and in grains at lower temperature. When the sheet is aged at high temperature, the particles become coarser with a large volume fraction.

  7. Superplastic Forming and Diffusion Bonding for Sandwich Structure of Ti-6Al-4V Alloy

    Institute of Scientific and Technical Information of China (English)

    Wenbo HAN; Kaifeng ZHANG; Guofeng WANG; Xiaojun ZHANG

    2005-01-01

    Superplastic forming and diffusion bonding (SPF/DB) is a well-established process for the manufacture of components almost exclusively from Ti-6Al-4V sheet material. The sandwich structure of Ti-6Al-4V alloy is investigated. The effects of the microstructure on the SPF/DB process were discussed. The microstructure at the interfaces and the distribution of thickness were researched.

  8. Cracking and load-deformation behavior of fiber reinforced concrete: Influence of testing method

    DEFF Research Database (Denmark)

    Paegle, Ieva; Minelli, Fausto; Fischer, Gregor

    2016-01-01

    on the definition of measured and derived parameters, including toughness, elastic properties and strength. This paper discusses a number of test procedures for selected material properties including tension and flexure. A comparative experimental study was carried out using two distinct fiber reinforced...... cementitious composites with strain hardening and strain softening behavior. Digital Image Correlation was utilized in the experimental program to detect and quantify the formation of cracks. Results show that the different test methodologies valuate specific aspects of material performance. The outcome...

  9. Monotonic and Cyclic Bond Behavior of Deformed CFRP Bars in High Strength Concrete

    OpenAIRE

    2016-01-01

    Composite reinforcing bars (rebars) that are used in concrete members with high performance (strength and durability) properties could have beneficial effects on the behavior of these members. This is especially vital when a building is constructed in an aggressive environment, for instance a corrosive environment. Although tension capacity/weight (or volume) ratios in composite rebars (carbon fiber reinforced polymer (CFRP), glass fiber reinforced polymer (GFRP), etc.) are very high when com...

  10. Development of Cutting Tool Through Superplastic Boronizing of Duplex Stainless Steel

    Science.gov (United States)

    Jauhari, Iswadi; Harun, Sunita; Jamlus, Siti Aida; Sabri, Mohd Faizul Mohd

    2017-03-01

    In this study, a cutting tool is developed from duplex stainless steel (DSS) using the superplastic boronizing technique. The feasibility of the development process is studied, and the cutting performances of the cutting tool are evaluated and compared with commercially available carbide and high-speed steel (HSS) tools. The superplastically boronized (SPB) cutting tool yielded a dense boronized layer of 50.5 µm with a surface hardness of 3956 HV. A coefficient of friction value of 0.62 is obtained, which is lower than 1.02 and 0.8 of the carbide and HSS tools. When tested on an aluminum 6061 surface under dry condition, the SPB cutting tool is also able to produce turning finishing below 0.4 µm, beyond the travel distance of 3000 m, which is comparable to the carbide tool, but produces much better results than HSS tool. Through superplastic boronizing of DSS, it is possible to produce a high-quality metal-based cutting tool that is comparable to the conventional carbide tool.

  11. Development of Cutting Tool Through Superplastic Boronizing of Duplex Stainless Steel

    Science.gov (United States)

    Jauhari, Iswadi; Harun, Sunita; Jamlus, Siti Aida; Sabri, Mohd Faizul Mohd

    2017-01-01

    In this study, a cutting tool is developed from duplex stainless steel (DSS) using the superplastic boronizing technique. The feasibility of the development process is studied, and the cutting performances of the cutting tool are evaluated and compared with commercially available carbide and high-speed steel (HSS) tools. The superplastically boronized (SPB) cutting tool yielded a dense boronized layer of 50.5 µm with a surface hardness of 3956 HV. A coefficient of friction value of 0.62 is obtained, which is lower than 1.02 and 0.8 of the carbide and HSS tools. When tested on an aluminum 6061 surface under dry condition, the SPB cutting tool is also able to produce turning finishing below 0.4 µm, beyond the travel distance of 3000 m, which is comparable to the carbide tool, but produces much better results than HSS tool. Through superplastic boronizing of DSS, it is possible to produce a high-quality metal-based cutting tool that is comparable to the conventional carbide tool.

  12. Numerical Simulation and Superplastic Forming of Ti-6Al-4V Alloy for a Dental Prosthesis

    Science.gov (United States)

    Li, Xiaomei; Soo, Steven

    2011-04-01

    This article investigates superplastic forming (SPF) technique in conjunction with finite element (FE) simulation applied to dental repair. The superplasticity of Ti-6Al-4V alloys has been studied using a uniquely designed five-hole test with the aim of obtaining the modeled grain size and the flow stress parameters. The data from the five-hole test are subsequently put into the FE program for the simulation of a partial upper denture dental prosthesis (PUD4). The FE simulation of the PUD4 is carried out to set up appropriate input parameters for pressing due to the SPF process being fully automatic controlled. A variety of strain rates ranging from 2.4 × 10-5 to 1 × 10-3 s-1 are selected for the characterization of superplastic properties of the alloy. The Superflag FE program is used to generate an appropriate pressure-time profile and provide information on thickness, grain size, and grain growth rate distribution. Both membrane elements and solid elements have been adopted in the simulation and the results from both types of elements are compared. An evaluation of predicted parameters for the SPF of the prosthesis is presented.

  13. Effects of Prior Aging at 316 deg C in Argon on Inelastic Deformation Behavior of PMR-15 Polymer at 316 deg C : Experiment and Modeling

    Science.gov (United States)

    2009-03-01

    after their original formation and decompose thermally at high temperatures [28,30]. Unsaturated polyesters , epoxies, vinylesters, and polyimides are...the VBOP is 48 selected as a suitable choice of constitutive model to represent the inelastic behavior of the PMR-15 neat resin at 316 ◦C. 7.2 Review ...Schoeppner (Member) date AFIT/GSS/ENY/09-M06 Abstract The inelastic deformation behavior of PMR-15 neat resin , a high-temperature polymer, was investigated at

  14. Influence of inclined twin boundaries on the deformation behavior of Cu micropillars

    Energy Technology Data Exchange (ETDEWEB)

    Imrich, P.J., E-mail: peter.imrich@stud.unileoben.ac.at [Erich Schmid Institute of Materials Science, Austrian Academy of Sciences, Jahnstraße 12, 8700 Leoben (Austria); Kirchlechner, C., E-mail: c.kirchlechner@mpie.de [Max-Planck-Institut für Eisenforschung, Max-Planck-Straße 1, 40237 Düsseldorf (Germany); Department of Materials Physics, Montanuniversität, Jahnstraße 12, 8700 Leoben (Austria); Dehm, G., E-mail: dehm@mpie.de [Max-Planck-Institut für Eisenforschung, Max-Planck-Straße 1, 40237 Düsseldorf (Germany)

    2015-08-26

    In situ micromechanical compression tests on Cu pillars were performed to evaluate the influence of twin boundaries on the mechanical behavior. The 1 µm sized Cu samples on a Si substrate prepared by focused ion beam milling were either single crystalline or contained 2–5 twin boundaries that were inclined to the compression direction. The strengths of the pillars vary, depending on the crystal orientation, associated twin boundary inclination and orientation of slip systems. Results show, that multiple slip systems are activated in each pillar. However, slip parallel to the twin boundaries prevails due to the long mean free path for dislocation movement.

  15. Comparison of the microstructure, deformation and crack initiation behavior of austenitic stainless steel irradiated in-reactor or with protons

    Energy Technology Data Exchange (ETDEWEB)

    Stephenson, Kale J., E-mail: kalejs@umich.edu; Was, Gary S.

    2015-01-15

    Highlights: • Dislocation loops were the prominent defect, but neutron irradiation caused higher loop density. • Grain boundaries had similar amounts of radiation-induced segregation. • The increment in hardness and yield stress due to irradiation were very similar. • Relative IASCC susceptibility was nearly identical. • The effect of dislocation channel step height on IASCC was similar. - Abstract: The objective of this study was to compare the microstructures, microchemistry, hardening, susceptibility to IASCC initiation, and deformation behavior resulting from proton or reactor irradiation. Two commercial purity and six high purity austenitic stainless steels with various solute element additions were compared. Samples of each alloy were irradiated in the BOR-60 fast reactor at 320 °C to doses between approximately 4 and 12 dpa or by a 3.2 MeV proton beam at 360 °C to a dose of 5.5 dpa. Irradiated microstructures consisted mainly of dislocation loops, which were similar in size but lower in density after proton irradiation. Both irradiation types resulted in the formation of Ni–Si rich precipitates in a high purity alloy with added Si, but several other high purity neutron irradiated alloys showed precipitation that was not observed after proton irradiation, likely due to their higher irradiation dose. Low densities of small voids were observed in several high purity proton irradiated alloys, and even lower densities in neutron irradiated alloys, implying void nucleation was in process. Elemental segregation at grain boundaries was very similar after each irradiation type. Constant extension rate tensile experiments on the alloys in simulated light water reactor environments showed excellent agreement in terms of the relative amounts of intergranular cracking, and an analysis of localized deformation after straining showed a similar response of cracking to surface step height after both irradiation types. Overall, excellent agreement was observed

  16. Effect of non-isothermal deformation of austenite on ferrite transformation behavior studied by in-situ neutron diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Shi, Zengmin, E-mail: shzm@ctgu.edu.cn [College of Materials and Chemical Engineering, China Three Gorges University, Yichang 443002 (China); Tomota, Yo [Graduate School of Science and Engineering, Ibaraki University, 4-12-1 Nakanarusawa, Hitachi, Ibaraki 316-8511 (Japan); Harjo, Stefanus; Su, Yuhua [J-PARC Center, Japan Atomic Energy Agency, 2-4 Shirane Shirakata, Tokai, Ibaraki 319-1195 (Japan); Chi, Bo; Pu, Jian [School of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan 430074 (China); Jian, Li, E-mail: lijian@hust.edu.cn [School of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan 430074 (China)

    2015-04-17

    The microstructure evolution and phase transformation of high strength 22SiMn2TiB steel during non-isothermal deformation were investigated by using in situ time-of-flight (TOF) neutron diffraction technique. The results indicate that the deformation of austenite promotes pearlite and ferrite transformation while suppresses bainite transformation. Deformation texture forms in austenite and then it influences the evolution of transformation texture. Deformation of austenite brings the changes in lattice parameters of austenite caused by carbon partitioning and elastic strains during the transformation. Volume fraction of the retained austenite decreases with a decreased carbon content as deformation amount increases.

  17. Deformation Behavior in Medium Mn Steel of Nanometer-Sized α' + γ Lamellar Structure

    Science.gov (United States)

    Heo, Yoon-Uk; Kim, Dong Hwi; Heo, Nam Hoe; Hong, Chang Wan; Kim, Sung-Joon

    2016-12-01

    Yielding and work-hardening phenomena in an Fe-10.62Mn-2.84Al-0.17C-0.5Mo steel, which is composed of nanometer-sized lamellae of α' and γ, are described on the basis of the Hall-Petch relations. Unlike the general expectation, yielding in the steel, which consists of lamellae of α' and mechanically stable γ, occurs through the propagation of pileup dislocations from α' to γ. However, when γ is mechanically unstable, yielding occurs through the stress-assisted martensitic transformation (SAMT) within the unstable γ region, resulting in a low YS of about 500 MPa. The overall prominent work-hardening behavior of this steel after yielding is due to the active SAMT, which does not accompany the increase in mobile dislocation density and so causes the high elastic strain rate. The carbon partitioning treatment increases the SAMT starting strength to about 980 MPa, which is caused by the mechanical stabilization of γ. The overall low work-hardening behavior of this case is mainly attributed to the active propagation of pile-up dislocation from α' to γ which causes the high plastic strain rate through the abrupt increase of mobile dislocation density.

  18. Hot Deformation Behavior of Ti-3.5Al-5Mo-6V-3Cr-2Sn-0.5Fe Alloy in α + β Field

    Directory of Open Access Journals (Sweden)

    Zhaoxin Du

    2015-02-01

    Full Text Available The deformation behavior of Ti-3.5Al-5Mo-6V-3Cr-2Sn-0.5Fe high strength β titanium alloy is systematically investigated by isothermal compression in α + β field with the deformation temperatures ranging from 1003 K to 1078 K, the strain rates ranging from 0.001 s−1 to 1 s−1 and the height reduction is around 50%. Essentially, the flow stress-strain curve of isothermal compression in α + β field exhibits a flow softening feature when the strain rate is higher than 0.1 s−1 as while it exhibits a steady-state feature as the strain rate is lower than 0.1 s−1. The peak stress increases with a decrease in deformation temperature and the increase of strain rate. The activation energy for deformation in α + β field was calculated and the average activation energy of 271.1 kJ/mol. The microstructure observation reveals that the isothermal deformation in the α + β field of the alloy is mainly controlled by the dynamic recovery mechanism accompanied with the secondary dynamic recrystallizitation of β phase. The α phase shows an obvious pinning effect for the movement of dislocations. During deformation, the α phase was elongated and fragmented.

  19. Study of microstructural evolution, microstructure-mechanical properties correlation and collaborative deformation-transformation behavior of quenching and partitioning (Q and P) steel

    Energy Technology Data Exchange (ETDEWEB)

    Sun, Jing; Yu, Hao, E-mail: yhzhmr@126.com; Wang, Shaoyang; Fan, Yongfei

    2014-02-24

    This paper presents a detailed characterization of the microstructural evolution of quenching and partitioning (Q and P) steel by dilatometer, X-ray diffraction and scanning electron microscopy. Influence of partitioning time on mechanical properties was investigated and the relationship between microstructures and mechanical properties was established. The results indicate that bainite transformation occurs at the preliminary stage of partitioning and the amount is proportional to quenching temperature. Martensite softening, bainite transformation kinetics, amount and stability of retained austenite collaboratively have effects on mechanical properties. The purpose of the EBSD investigation is to study the changes in the microstructure of the Q and P steel during deformation and obtain a better understanding of collaborative deformation-transformation behavior. During deformation, plastic deformation preferentially occurred in the vicinity of ferrite–martensite interfaces and spread to the interior of ferrite grain with strain increasing. Plastic deformation started to occur in martensite after large strain. Furthermore, grain rotation occurred in some austenite grains or divided into subgrains during deformation.

  20. In situ synchrotron high-energy X-ray diffraction study of microscopic deformation behavior of a hard-soft dual phase composite containing phase transforming matrix

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Junsong; Hao, Shijie; Jiang, Daqiang; Huan, Yong; Cui, Lishan; Liu, Yinong; Yang, Hong; Ren, Yang

    2017-05-01

    This study explored a novel intermetallic composite design concept based on the principle of lattice strain matching enabled by the collective atomic load transfer. It investigated the hard-soft microscopic deformation behavior of a Ti3Sn/TiNi eutectic hard-soft dual phase composite by means of in situ synchrotron high-energy X-ray diffraction (HE-XRD) during compression. The composite provides a unique micromechanical system with distinctive deformation behaviors and mechanisms from the two components, with the soft TiNi matrix deforming in full compliance via martensite variant reorientation and the hard Ti3Sn lamellae deforming predominantly by rigid body rotation, producing a crystallographic texture for the TiNi matrix and a preferred alignment for the Ti3Sn lamellae. HE-XRD reveals continued martensite variant reorientation during plastic deformation well beyond the stress plateau of TiNi. The hard and brittle Ti3Sn is also found to produce an exceptionally large elastic strain of 1.95% in the composite. This is attributed to the effect of lattice strain matching between the transformation lattice distortion of the TiNi matrix and the elastic strain of Ti3Sn lamellae. With such unique micromechanic characteristics, the composite exhibits high strength and large ductility.

  1. Abnormal Deformation Behavior of Oxygen-Modified β-Type Ti-29Nb-13Ta-4.6Zr Alloys for Biomedical Applications

    Science.gov (United States)

    Liu, Huihong; Niinomi, Mitsuo; Nakai, Masaaki; Cong, Xin; Cho, Ken; Boehlert, Carl J.; Khademi, Vahid

    2017-01-01

    Oxygen was added to the biomedical β-type Ti-29Nb-13Ta-4.6Zr alloy (TNTZ, mass pct) in order to improve its strength, while keeping its Young's modulus low. Conventionally, with an increase in the oxygen content, an alloy's tensile strength increases, while its tensile elongation-to-failure decreases. However, an abnormal deformation behavior has been reported in the case of oxygen-modified TNTZ alloys in that their strength increases monotonically while their elongation-to-failure initially decreases and then increases with the increase in the oxygen content. In this study, this abnormal tensile deformation behavior of oxygen-modified TNTZ alloys was investigated systematically. A series of TNTZ-(0.1, 0.3, and 0.7 mass pct)O alloy samples was prepared, treated thermomechanically, and finally solution treated; these samples are denoted as 0.1ST, 0.3ST, and 0.7ST, respectively. The main tensile deformation mechanisms in 0.1ST are a deformation-induced α″-martensitic transformation and {332} mechanical twinning. The large elongation-to-failure of 0.1ST is attributable to multiple deformation mechanisms, including the deformation-induced martensitic transformation and mechanical twinning as well as dislocation glide. In both 0.3ST and 0.7ST, dislocation glide is the predominant deformation mode. 0.7ST shows more homogeneous and extensive dislocation glide along with multiple slip systems and a higher frequency of cross slip. As a result, it exhibits a higher work-hardening rate and greater resistance to local stress concentration, both of which contribute to its elongation-to-failure being greater than that of 0.3ST.

  2. Evaluation of microscopic deformation behaviors of metal matrix composite by means of SFC test and acoustic emission (Part I :Effect of loading direction)

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Joon Hyun; Kang, Moon Phil [Pusan National University, Pusan (Korea, Republic of)

    1998-11-15

    Metal matrix composites(MMCs) offer significant increase in elastic modulus and strength as well as improve resistance to fatigue initiation, creep and wear. For the successful application of MMC to structure, it is very important to understand micro-failure mechanism of material. However, due to complex deformation behavior intrinsically of bulk composite panel, single fiber composite(SFC) has been successfully used to understand a fundamental mechanism of deformation in MMC. The substantial failure mechanisms of MMC were affected by many factors such as the loading direction, the heat treatment condition, matrix properties and volume fraction. In this study, the microscopic deformation behavior of MMC is investigated for single SiC fiber reinforced aluminium alloy under the different loading direction, that is, longitudinal and transverse loading. Acoustic emission(AE) technique has been also used to detect the signals corresponding to each microscopic deformation behavior under the loading. Special attention is given to AE characteristics associated with interfacial debonding between fiber and matrix under the different leading direction.

  3. Modeling the Hot Deformation Behaviors of As-Extruded 7075 Aluminum Alloy by an Artificial Neural Network with Back-Propagation Algorithm

    Science.gov (United States)

    Quan, Guo-zheng; Zou, Zhen-yu; Wang, Tong; Liu, Bo; Li, Jun-chao

    2017-01-01

    In order to investigate the hot deformation behaviors of as-extruded 7075 aluminum alloy, the isothermal compressive tests were conducted at the temperatures of 573, 623, 673 and 723 K and the strain rates of 0.01, 0.1, 1 and 10 s-1 on a Gleeble 1500 thermo-mechanical simulator. The flow behaviors showing complex characteristics are sensitive to strain, strain rate and temperature. The effects of strain, temperature and strain rate on flow stress were analyzed and dynamic recrystallization (DRX)-type softening characteristics of the flow behaviors with single peak were identified. An artificial neural network (ANN) with back-propagation (BP) algorithm was developed to deal with the complex deformation behavior characteristics based on the experimental data. The performance of ANN model has been evaluated in terms of correlation coefficient (R) and average absolute relative error (AARE). A comparative study on Arrhenius-type constitutive equation and ANN model for as-extruded 7075 aluminum alloy was conducted. Finally, the ANN model was successfully applied to the development of processing map and implanted into finite element simulation. The results have sufficiently articulated that the well-trained ANN model with BP algorithm has excellent capability to deal with the complex flow behaviors of as-extruded 7075 aluminum alloy and has great application potentiality in hot deformation processes.

  4. Monotonic and Cyclic Bond Behavior of Deformed CFRP Bars in High Strength Concrete

    Directory of Open Access Journals (Sweden)

    T. Tibet Akbas

    2016-05-01

    Full Text Available Composite reinforcing bars (rebars that are used in concrete members with high performance (strength and durability properties could have beneficial effects on the behavior of these members. This is especially vital when a building is constructed in an aggressive environment, for instance a corrosive environment. Although tension capacity/weight (or volume ratios in composite rebars (carbon fiber reinforced polymer (CFRP, glass fiber reinforced polymer (GFRP, etc. are very high when compared to steel rebars, major weaknesses in concrete members reinforced with these composite rebars may be the potential consequences of relatively poor bonding capacity. This may even be more crucial when the member is subjected to cyclic loading. Although monotonic bond tests are available in the literature, only limited experimental studies exist on bond characteristics under cyclic loading conditions. In order to fill this gap and propose preliminary design recommendations, 10 specimens of 10-mm-diameter ribbed CFRP rebars embedded in specially designed high strength concrete (f’c = 70 MPa blocks were subjected to monotonic and cyclic pullout tests. The experimental results showed that cyclically loaded CFRP rebars had less bond strength than those companion specimens loaded monotonically.

  5. Deformation behavior of NiAl-based alloys containing iron, cobalt, and hafnium

    Science.gov (United States)

    Pank, D. R.; Koss, D. A.; Nathal, M. V.

    1989-01-01

    The effects of alloying additions on the mechanical properties of the B2 intermetallic NiAl have been investigated in both the melt-spun ribbon and consolidated, bulk form. The study is based on a matrix of NiAl-based alloys with up to 20 at. pct Co and Fe additions and with reduced Al levels in the range of 30-40 at. pct. Characterization of the melt-spun ribbon by optical and scanning electron microscopy indicates a range of microstructures, including single-phase beta, gamma-prime necklace phase surrounding either martensitic or beta grains, and a mixture of equiaxed martensitic and gamma-prime grains. Bend ductility is present in melt-spun and annealed ribbons exhibiting the gamma-prime necklace structure and in a single-phase beta material containing 20 at. pct Fe. The analysis of compressive flow behavior on consolidated, bulk specimens indicates that the single-phase beta alloys exhibit a continuous decrease in yield stress with increasing temperature and profuse microcracking at grain boundaries. In contrast, multiphase (gamma-prime + either martensite or beta) alloys tend to display a peak in flow stress between 600 and 800 K, with little or no signs of microcracking. In general, heat treatments which convert the martensitic grains to beta + gamma-prime result in improved strength at temperatures above 600 K and better resistance to crack initiation.

  6. Influence of dynamic strain aging on tensile deformation behavior of alloy 617

    Energy Technology Data Exchange (ETDEWEB)

    Ekaputra, I. M. W. [Pukyong National University, Busan (Korea, Republic of); Kim, Woo Gon; Park, Jae Young; Kim, Seon Jin; Kim, Eung Seon [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2016-12-15

    To investigate the dynamic strain aging (DSA) behavior of Alloy 617, high-temperature tensile tests were carried out with strain rates variations of 10{sup -}3{sup /}s, 10{sup -4}/s, and 10{sup -5}/s from 24°C to 950°C. Five flow relationships, Hollomon, Ludwik, Swift, Ludwigson, and Voce, were applied to describe the tensile true stress–strain curves, and the DSA region was defined. In describing the tensile curves, Ludwigson's equation was superior to the other equations, and the DSA region was adequately defined by this equation as plateaus at intermediate temperatures from 200°C to 700°C. It was identified that Alloy 617 is dominated by three types of serrations, known as Types D, A+B, and C. The activation energy values for each serration type were obtained by the Arrhenius equation. By using the obtained activation energy values, the serrated yielding map and the DSA mechanism were drawn and manifested. In addition, the relationship between the tensile strength and strain rate at higher temperatures above 700°C was found to be closely related to the amounts of slip lines. In the scanning electron microscope (SEM) fractographs, there was a significant difference at the low, intermediate, and high temperatures, but almost the same to the three strain rates.

  7. Global and local deformation behavior and mechanical properties of individual phases in a quenched and partitioned steel

    Energy Technology Data Exchange (ETDEWEB)

    Diego-Calderón, I. de, E-mail: irenedediego.calderon@imdea.org [IMDEA Materials Institute, Calle Eric Kandel 2, Getafe 28906, Madrid (Spain); De Knijf, D. [Department of Materials Science and Engineering, Ghent University, Technologiepark 903, B-9052 Zwijnaarde (Ghent) (Belgium); Monclús, M.A.; Molina-Aldareguia, J.M.; Sabirov, I. [IMDEA Materials Institute, Calle Eric Kandel 2, Getafe 28906, Madrid (Spain); Föjer, C. [ArcelorMittal Global R& D Gent, Pres. J. F. Kennedylaan 3, B-9060 Zelzate (Belgium); Petrov, R.H. [Department of Materials Science and Engineering, Ghent University, Technologiepark 903, B-9052 Zwijnaarde (Ghent) (Belgium); Department of Materials Science and Engineering, Delft University of Technology, 2628 CD Delft (Netherlands)

    2015-04-10

    Third generation advanced high strength steels produced via quenching and partitioning (Q&P) treatment are receiving increased attention. A 0.25C–3Mn–1.5Si–0.023 Al steel was subjected to Q&P processing (with varying partitioning temperature and time) resulting in the formation of complex multi-phase microstructures. The effect of Q&P parameters on the microstructure and morphology of microconstituents was analyzed. Mechanical properties of the material and of its individual microconstituents were studied via tensile testing and nanoindentation on individual microconstituents, which were identified a priori by electron back-scattered diffraction analysis. Special attention is paid to the effect of the morphology of retained austenite on its transformation stability. In situ tensile tests and digital image correlation analysis were performed to study deformation behavior of the Q&P processed steel at the micro-scale with respect to the local microstructure. The effect of local microstructure and properties of individual phases on the degree of strain partitioning is discussed.

  8. Deformation and Recrystallization Behavior of the Cast Structure in Large Size, High Strength Steel Ingots: Experimentation and Modeling

    Science.gov (United States)

    Chadha, K.; Shahriari, D.; Tremblay, R.; Bhattacharjee, P. P.; Jahazi, M.

    2017-07-01

    Constitutive modeling of the ingot breakdown process of large size ingots of high strength steel was carried out through comprehensive thermomechanical processing using Gleeble 3800® thermomechanical simulator, finite element modeling (FEM), optical and electron back scatter diffraction (EBSD). For this purpose, hot compression tests in the range of 1473 K to 1323 K (1200 °C to 1050 °C) and strain rates of 0.25 to 2 s-1 were carried out. The stress-strain curves describing the deformation behavior of the dendritic microstructure of the cast ingot were analyzed in terms of the Arrhenius and Hansel-Spittel models which were implemented in Forge NxT 1.0® FEM software. The results indicated that the Arrhenius model was more reliable in predicting microstructure evolution of the as-cast structure during ingot breakdown, particularly the occurrence of dynamic recrystallization (DRX) process which was a vital parameter in estimating the optimum loads for forming of large size components. The accuracy and reliability of both models were compared in terms of correlation coefficient (R) and the average absolute relative error (ARRE).

  9. Deformation and Recrystallization Behavior of the Cast Structure in Large Size, High Strength Steel Ingots: Experimentation and Modeling

    Science.gov (United States)

    Chadha, K.; Shahriari, D.; Tremblay, R.; Bhattacharjee, P. P.; Jahazi, M.

    2017-09-01

    Constitutive modeling of the ingot breakdown process of large size ingots of high strength steel was carried out through comprehensive thermomechanical processing using Gleeble 3800® thermomechanical simulator, finite element modeling (FEM), optical and electron back scatter diffraction (EBSD). For this purpose, hot compression tests in the range of 1473 K to 1323 K (1200 °C to 1050 °C) and strain rates of 0.25 to 2 s-1 were carried out. The stress-strain curves describing the deformation behavior of the dendritic microstructure of the cast ingot were analyzed in terms of the Arrhenius and Hansel-Spittel models which were implemented in Forge NxT 1.0® FEM software. The results indicated that the Arrhenius model was more reliable in predicting microstructure evolution of the as-cast structure during ingot breakdown, particularly the occurrence of dynamic recrystallization (DRX) process which was a vital parameter in estimating the optimum loads for forming of large size components. The accuracy and reliability of both models were compared in terms of correlation coefficient (R) and the average absolute relative error (ARRE).

  10. Prediction of the Hot Compressive Deformation Behavior for Superalloy Nimonic 80A by BP-ANN Model

    Directory of Open Access Journals (Sweden)

    Guo-zheng Quan

    2016-02-01

    Full Text Available In order to predict hot deformation behavior of superalloy nimonic 80A, a back-propagational artificial neural network (BP-ANN and strain-dependent Arrhenius-type model were established based on the experimental data from isothermal compression tests on a Gleeble-3500 thermo-mechanical simulator at temperatures ranging of 1050–1250 °C, strain rates ranging of 0.01–10.0 s−1. A comparison on a BP-ANN model and modified Arrhenius-type constitutive equation has been implemented in terms of statistical parameters, involving mean value of relative (μ, standard deviation (w, correlation coefficient (R and average absolute relative error (AARE. The μ -value and w -value of the improved Arrhenius-type model are 3.0012% and 2.0533%, respectively, while their values of the BP-ANN model are 0.0714% and 0.2564%, respectively. Meanwhile, the R-value and ARRE-value for the improved Arrhenius-type model are 0.9899 and 3.06%, while their values for the BP-ANN model are 0.9998 and 1.20%. The results indicate that the BP-ANN model can accurately track the experimental data and show a good generalization capability to predict complex flow behavior. Then, a 3D continuous interaction space for temperature, strain rate, strain and stress was constructed based on the expanded data predicted by a well-trained BP-ANN model. The developed 3D continuous space for hot working parameters articulates the intrinsic relationships of superalloy nimonic 80A.

  11. Continuous Severe Plastic Deformation Processing of Aluminum Alloys

    Energy Technology Data Exchange (ETDEWEB)

    Raghavan Srinivasan (PI); Prabir K. Chaudhury; Balakrishna Cherukuri; Qingyou Han; David Swenson; Percy Gros

    2006-06-30

    Metals with grain sizes smaller than 1-micrometer have received much attention in the past decade. These materials have been classified as ultra fine grain (UFG) materials (grain sizes in the range of 100 to 1000-nm) and nano-materials (grain size <100-nm) depending on the grain size. This report addresses the production of bulk UFG metals through the use of severe plastic deformation processing, and their subsequent use as stock material for further thermomechanical processing, such as forging. A number of severe plastic deformation (SPD) methods for producing bulk UFG metals have been developed since the early 1990s. The most promising of these processes for producing large size stock that is suitable for forging is the equal channel angular extrusion or pressing (ECAE/P) process. This process involves introducing large shear strain in the work-piece by pushing it through a die that consists of two channels with the same cross-sectional shape that meet at an angle to each other. Since the cross-sections of the two channels are the same, the extruded product can be re-inserted into the entrance channel and pushed again through the die. Repeated extrusion through the ECAE/P die accumulates sufficient strain to breakdown the microstructure and produce ultra fine grain size. It is well known that metals with very fine grain sizes (< 10-micrometer) have higher strain rate sensitivity and greater elongation to failure at elevated temperature, exhibiting superplastic behavior. However, this superplastic behavior is usually manifest at high temperature (> half the melting temperature on the absolute scale) and very low strain rates (< 0.0001/s). UFG metals have been shown to exhibit superplastic characteristics at lower temperature and higher strain rates, making this phenomenon more practical for manufacturing. This enables part unitization and forging more complex and net shape parts. Laboratory studies have shown that this is particularly true for UFG metals produced

  12. Continuous Severe Plastic Deformation Processing of Aluminum Alloys

    Energy Technology Data Exchange (ETDEWEB)

    Raghavan Srinivasan (PI); Prabir K. Chaudhury; Balakrishna Cherukuri; Qingyou Han; David Swenson; Percy Gros

    2006-06-30

    Metals with grain sizes smaller than 1-micrometer have received much attention in the past decade. These materials have been classified as ultra fine grain (UFG) materials (grain sizes in the range of 100 to 1000-nm) and nano-materials (grain size <100-nm) depending on the grain size. This report addresses the production of bulk UFG metals through the use of severe plastic deformation processing, and their subsequent use as stock material for further thermomechanical processing, such as forging. A number of severe plastic deformation (SPD) methods for producing bulk UFG metals have been developed since the early 1990s. The most promising of these processes for producing large size stock that is suitable for forging is the equal channel angular extrusion or pressing (ECAE/P) process. This process involves introducing large shear strain in the work-piece by pushing it through a die that consists of two channels with the same cross-sectional shape that meet at an angle to each other. Since the cross-sections of the two channels are the same, the extruded product can be re-inserted into the entrance channel and pushed again through the die. Repeated extrusion through the ECAE/P die accumulates sufficient strain to breakdown the microstructure and produce ultra fine grain size. It is well known that metals with very fine grain sizes (< 10-micrometer) have higher strain rate sensitivity and greater elongation to failure at elevated temperature, exhibiting superplastic behavior. However, this superplastic behavior is usually manifest at high temperature (> half the melting temperature on the absolute scale) and very low strain rates (< 0.0001/s). UFG metals have been shown to exhibit superplastic characteristics at lower temperature and higher strain rates, making this phenomenon more practical for manufacturing. This enables part unitization and forging more complex and net shape parts. Laboratory studies have shown that this is particularly true for UFG metals produced

  13. Modeling the Effects of Cu Content and Deformation Variables on the High-Temperature Flow Behavior of Dilute Al-Fe-Si Alloys Using an Artificial Neural Network.

    Science.gov (United States)

    Shakiba, Mohammad; Parson, Nick; Chen, X-Grant

    2016-06-30

    The hot deformation behavior of Al-0.12Fe-0.1Si alloys with varied amounts of Cu (0.002-0.31 wt %) was investigated by uniaxial compression tests conducted at different temperatures (400 °C-550 °C) and strain rates (0.01-10 s(-1)). The results demonstrated that flow stress decreased with increasing deformation temperature and decreasing strain rate, while flow stress increased with increasing Cu content for all deformation conditions studied due to the solute drag effect. Based on the experimental data, an artificial neural network (ANN) model was developed to study the relationship between chemical composition, deformation variables and high-temperature flow behavior. A three-layer feed-forward back-propagation artificial neural network with 20 neurons in a hidden layer was established in this study. The input parameters were Cu content, temperature, strain rate and strain, while the flow stress was the output. The performance of the proposed model was evaluated using the K-fold cross-validation method. The results showed excellent generalization capability of the developed model. Sensitivity analysis indicated that the strain rate is the most important parameter, while the Cu content exhibited a modest but significant influence on the flow stress.

  14. Modeling the Effects of Cu Content and Deformation Variables on the High-Temperature Flow Behavior of Dilute Al-Fe-Si Alloys Using an Artificial Neural Network

    Directory of Open Access Journals (Sweden)

    Mohammad Shakiba

    2016-06-01

    Full Text Available The hot deformation behavior of Al-0.12Fe-0.1Si alloys with varied amounts of Cu (0.002–0.31 wt % was investigated by uniaxial compression tests conducted at different temperatures (400 °C–550 °C and strain rates (0.01–10 s−1. The results demonstrated that flow stress decreased with increasing deformation temperature and decreasing strain rate, while flow stress increased with increasing Cu content for all deformation conditions studied due to the solute drag effect. Based on the experimental data, an artificial neural network (ANN model was developed to study the relationship between chemical composition, deformation variables and high-temperature flow behavior. A three-layer feed-forward back-propagation artificial neural network with 20 neurons in a hidden layer was established in this study. The input parameters were Cu content, temperature, strain rate and strain, while the flow stress was the output. The performance of the proposed model was evaluated using the K-fold cross-validation method. The results showed excellent generalization capability of the developed model. Sensitivity analysis indicated that the strain rate is the most important parameter, while the Cu content exhibited a modest but significant influence on the flow stress.

  15. Role of B19' martensite deformation in stabilizing two-way shape memory behavior in NiTi

    Science.gov (United States)

    Benafan, O.; Padula, S. A.; Noebe, R. D.; Sisneros, T. A.; Vaidyanathan, R.

    2012-11-01

    Deformation of a B19' martensitic, polycrystalline Ni49.9Ti50.1 (at. %) shape memory alloy and its influence on the magnitude and stability of the ensuing two-way shape memory effect (TWSME) was investigated by combined ex situ mechanical experimentation and in situ neutron diffraction measurements at stress and temperature. The microstructural changes (texture, lattice strains, and phase fractions) during room-temperature deformation and subsequent thermal cycling were captured and compared to the bulk macroscopic response of the alloy. With increasing uniaxial strain, it was observed that B19' martensite deformed by reorientation and detwinning with preferred selection of the (1¯50)M and (010)M variants, (201¯)B19' deformation twinning, and dislocation activity. These mechanisms were indicated by changes in bulk texture from the neutron diffraction measurements. Partial reversibility of the reoriented variants and deformation twins was also captured upon load removal and thermal cycling, which after isothermal deformation to strains between 6% and 22% resulted in a strong TWSME. Consequently, TWSME functional parameters including TWSME strain, strain reduction, and transformation temperatures were characterized and it was found that prior martensite deformation to 14% strain provided the optimum condition for the TWSME, resulting in a stable two-way shape memory strain of 2.2%. Thus, isothermal deformation of martensite was found to be a quick and efficient method for creating a strong and stable TWSME in Ni49.9Ti50.1.

  16. THE MODEL OF PREVENTION OF VANDAL BEHAVIOR PROVIDED BY THE DEFORMATIONS AND DESTRUCTIONS OF VALUABLE SPHERE OF YOUTH

    Directory of Open Access Journals (Sweden)

    Irina V. Vorobyeva

    2015-01-01

    Full Text Available The aim of the present article is to discuss current opportunities for prevention of vandal behavior of young people, taking into account the structural features of valuable sphere of teenagers and young men. Methods. Methods involve psychognostic techniques such as an axiological questionnaire by S.Schwarz, a questionnaire «Motives of vandal behaviour» by I. V. Vorobyeva, O. V. Kruzhkova, S. A. Ostrikova; method of theoretical modelling. Results. Vandalism is described as a fairly common phenomenon among young people, which may be the result not only of deviant orientation of the individual, but also the result of a mismatch of individual values of teenager or young man and imposed by society requirements for his value orientations. 832 teenagers took part in the complex psychological studies. The following four different groups of respondents have been identified and studied: – with an agreed system of prosocial value orientations; – respondents with a mismatched (deformed system of values; – respondents with a destructive (antagonistic system of value orientations; – respondents with agreed antisocial system of value orientations. The model of prevention of vandalism among young people is developed on the basis of the psychological characteristics of these groups and the description of the genesis and causes of vandal behavior with following applying the method of theoretical modeling. This model is based on the principles of accounting axiological aspects of regulation of activity, consideration of personal values as a dynamic system, taking into account the degree of stability of the system of individual value orientations, differentiation and depth of the psychological impact of variation in the choice of forms and methods of psychological influence. The recommendations are proposed; the most appropriate psychological work aspects with each of the groups of respondents are described. Scientific novelty. The proposed authors

  17. Dynamic behavior and microstructural evolution during moderate to high strain rate hot deformation of a Fe-Ni-Cr alloy (alloy 800H)

    Science.gov (United States)

    Cao, Yu; Di, Hongshuang; Zhang, Jiecen; Yang, Yaohua

    2015-01-01

    The objective of the study is to fundamentally understand the dynamic behavior of alloy 800H at moderate to high strain rate using hot compression tests and propose nucleation mechanism associated with dynamic crystallization (DRX). We firstly investigated the dynamic behavior of alloy 800H with industrial scale strain rates using hot compression tests and adiabatic correction was performed to correct as-measured flow curves. Secondly, a Johnson-Cook model was established by using the corrected data and could give a precise prediction of elevated temperature flow stress for the studied alloy. Finally, the nucleation mechanism of DRX grains at high strain rates was studied. The results showed that the predominant nucleation mechanism for DRX is the formation of "bulge" at parent grain boundary. Additionally, the fragmentation of original grain at low deformation temperatures and the twinning near the bulged regions at high deformation temperatures also accelerate the DRX process.

  18. Macro-scale deformation behavior and characterization of deformation mechanisms below µm-scale in experimentally deformed Boom Clay by using the combination of triaxial compression, X-ray µ-CT imaging, DIC, BIB cross sectioning, and SEM

    Science.gov (United States)

    Oelker, Anne; Desbois, Guillaume; Urai, Janos L.; Bésuelle, Pierre; Viggiani, Gioacchino; Levasseur, Séverine

    2017-04-01

    Boom Clay is one formation being studied in Belgium as a potential host rock for deep geological disposal of radioactive waste. This poorly indurated clay presents in its natural state favorable properties against the migration of radionuclides: low permeability, low solute diffusion rates, good retention and sorption capacity for many radionuclides and good self-sealing capacity. During construction of disposal galleries, stress redistribution will lead to perturbation of the clay and the formation around galleries of the so-called "Excavation disturbed Zone" (EdZ). The study of deformation mechanisms and evolution of Boom Clay properties at macro but also micro scale allows to assess in a more mechanistic way the evolution of Boom Clay properties in this EdZ. In this work, we show microstructural investigations of Boom Clay deformed in undrained triaxial compression by linking conventional stress/strain curves with Digital Image Correlation (DIC) and scanning electron microscopy (SEM) imaging of broad-ion-beam (BIB) milled cross-sections to deduce deformation mechanisms based on microstructures at sub-micron resolution. Two specimens, collected in Mol (Belgium) at the European Underground Laboratories (URL) on HADES level, were analyzed: The major principal stress σ1 was applied parallel as well as perpendicular to the bedding direction with an initial mean normal effective stress of 4.5 MPa and an initial pore water pressure of 2.3 MPa, which are equal to the in-situ values. Linking the resulting DIC-derived maps of incremental strains with the corresponding stress/strain curve give not only information about the moment of the shear band development, but also on the way strain evolves within the specimen throughout the rest. Incremental DIC analysis of X-ray tomographic scans performed during loading tests give a time evolution of the strain field, and subsequently allow to detect strain localization which appears close to the stress peak. Regions with a

  19. The measurement of friction for superplastic forming of Ti-6Al-4V

    Energy Technology Data Exchange (ETDEWEB)

    Kelly, R.B.; Leen, S.B.; Pashby, I.R.; Kennedy, A.R. [School of M3EM, Univ. of Nottingham (United Kingdom)

    2004-07-01

    An experimental test for measuring the friction between Ti-6Al-4V sheet material and S310 stainless steel tool material at 900 C is presented. The test is intended for application to Ti-6Al-4V superplastic forming for the manufacture of aeroengine components. The work is motivated by the need for accurate, representative data for process modelling, where accurate simulation is critical to formed component dimensions. The results show a time dependency of friction. The effects of boron nitride density, applied normal load and die surface roughness are investigated. (orig.)

  20. Elastic constants for superplastically formed/diffusion-bonded corrugated sandwich core

    Science.gov (United States)

    Ko, W. L.

    1980-01-01

    Formulas and associated graphs for evaluating the effective elastic constants for a superplastically formed/diffusion bonded (SPF/DB) corrugated sandwich core, are presented. A comparison of structural stiffnesses of the sandwich core and a honeycomb core under conditions of equal sandwich core density was made. The stiffness in the thickness direction of the optimum SPF/DB corrugated core (that is, triangular truss core) is lower than that of the honeycomb core, and that the former has higher transverse shear stiffness than the latter.

  1. Microstructure and annealing behavior of a modified 9Cr-1Mo steel after dynamic plastic deformation to different strains

    DEFF Research Database (Denmark)

    Zhang, Zhenbo; Mishin, Oleg; Tao, N.R.;

    2015-01-01

    The microstructure, hardness and tensile properties of a modified 9Cr-1Mo steel processed by dynamic plastic deformation (DPD) to different strains (0.5 and 2.3) have been investigated in the as-deformed and annealed conditions. It is found that significant structural refinement and a high level...... of strength can be achieved by DPD to a strain of 2.3, and that the microstructure at this strain contains a large fraction of high angle boundaries. The ductility of the DPD processed steel is however low. Considerable structural coarsening of the deformed microstructure without pronounced recrystallization...

  2. Hot Deformation Behavior of As-Cast 2101 Grade Lean Duplex Stainless Steel and the Associated Changes in Microstructure and Crystallographic Texture

    Science.gov (United States)

    Patra, Sudipta; Ghosh, Abhijit; Singhal, Lokesh Kumar; Podder, Arijit Saha; Sood, Jagmohan; Kumar, Vinod; Chakrabarti, Debalay

    2016-11-01

    The hot deformation behavior of 2101 grade lean duplex stainless steel (DSS, containing 5 wt pct Mn, 0.2 wt pct N, and 1.4 wt pct Ni) and associated microstructural changes within δ-ferrite and austenite (γ) phases were investigated by hot-compression testing in a GLEEBLE 3500 simulator over a range of deformation temperatures, T def [1073 K to 1373 K (800 °C to 1100 °C)], and applied strains, ɛ (0.25 to 0.80), at a constant true strain rate of 1/s. The microstructural softening inside γ was dictated by discontinuous dynamic recrystallization (DDRX) at a higher T def [1273 K to 1373 K (1000 °C to 1100 °C)], while the same was dictated by continuous dynamic recrystallization (CDRX) at a lower T def (1173 K (900 °C)]. Dynamic recovery (DRV) and CDRX dominated the softening inside δ-ferrite at T def ≥ 1173 K (900 °C). The dynamic recrystallization (DRX) inside δ and γ could not take place upon deformation at 1073 K (800 °C). The average flow stress level increased 2 to 3 times as the T def dropped from 1273 to 1173 K (1000 °C to 900 °C) and finally to 1073 K (800 °C). The average microhardness values taken from δ-ferrite and γ regions of the deformed samples showed a different trend. At T def of 1373 K (1100 °C), microhardness decreased with the increase in strain, while at T def of 1173 K (900 °C), microhardness increased with the increase in strain. The microstructural changes and hardness variation within individual phases of hot-deformed samples are explained in view of the chemical composition of the steel and deformation parameters (T def and ɛ).

  3. Hot Deformation Behavior of As-Cast 2101 Grade Lean Duplex Stainless Steel and the Associated Changes in Microstructure and Crystallographic Texture

    Science.gov (United States)

    Patra, Sudipta; Ghosh, Abhijit; Singhal, Lokesh Kumar; Podder, Arijit Saha; Sood, Jagmohan; Kumar, Vinod; Chakrabarti, Debalay

    2017-01-01

    The hot deformation behavior of 2101 grade lean duplex stainless steel (DSS, containing 5 wt pct Mn, 0.2 wt pct N, and 1.4 wt pct Ni) and associated microstructural changes within δ-ferrite and austenite ( γ) phases were investigated by hot-compression testing in a GLEEBLE 3500 simulator over a range of deformation temperatures, T def [1073 K to 1373 K (800 °C to 1100 °C)], and applied strains, ɛ (0.25 to 0.80), at a constant true strain rate of 1/s. The microstructural softening inside γ was dictated by discontinuous dynamic recrystallization (DDRX) at a higher T def [1273 K to 1373 K (1000 °C to 1100 °C)], while the same was dictated by continuous dynamic recrystallization (CDRX) at a lower T def (1173 K (900 °C)]. Dynamic recovery (DRV) and CDRX dominated the softening inside δ-ferrite at T def ≥ 1173 K (900 °C). The dynamic recrystallization (DRX) inside δ and γ could not take place upon deformation at 1073 K (800 °C). The average flow stress level increased 2 to 3 times as the T def dropped from 1273 to 1173 K (1000 °C to 900 °C) and finally to 1073 K (800 °C). The average microhardness values taken from δ-ferrite and γ regions of the deformed samples showed a different trend. At T def of 1373 K (1100 °C), microhardness decreased with the increase in strain, while at T def of 1173 K (900 °C), microhardness increased with the increase in strain. The microstructural changes and hardness variation within individual phases of hot-deformed samples are explained in view of the chemical composition of the steel and deformation parameters ( T def and ɛ).

  4. Characterization of Deformation Behavior of Individual Grains in Polycrystalline Cu-Al-Mn Superelastic Alloy Using White X-ray Microbeam Diffraction

    Directory of Open Access Journals (Sweden)

    Eui Pyo Kwon

    2015-10-01

    Full Text Available White X-ray microbeam diffraction was applied to investigate the microscopic deformation behavior of individual grains in a Cu-Al-Mn superelastic alloy. Strain/stresses were measured in situ at different positions in several grains having different orientations during a tensile test. The results indicated inhomogeneous stress distribution, both at the granular and intragranular scale. Strain/stress evolution showed reversible phenomena during the superelastic behavior of the tensile sample, probably because of the reversible martensitic transformation. However, strain recovery of the sample was incomplete due to the residual martensite, which results in the formation of local compressive residual stresses at grain boundary regions.

  5. Bending springback behavior related to deformation-induced phase transformations in Ti-12Cr and Ti-29Nb-13Ta-4.6Zr alloys for spinal fixation applications.

    Science.gov (United States)

    Liu, Huihong; Niinomi, Mitsuo; Nakai, Masaaki; Hieda, Junko; Cho, Ken

    2014-06-01

    The springback behavior of Ti-12Cr and Ti-29Nb-13Ta-4.6Zr (TNTZ) during deformation by bending was investigated; and the microstructures of the non-deformed and deformed parts of both alloys were systematically examined to clarify the relationship between microstructure and springback behavior. For the deformed Ti-12Cr alloy, deformation-induced ω-phase transformation occurs in both the areas of compression and tension within the deformed part, which increases the Young׳s modulus. With the deformed TNTZ alloy, deformation-induced ω-phase transformation is observed in the area of compression within the deformed part; while a deformation-induced α″ martensite transformation occurs in the area under tension, which is likely to be associated with the pseudoelasticity of TNTZ. Among these two alloys, Ti-12Cr exhibits a smaller springback and a much greater bending strength when compared with TNTZ; making Ti-12Cr the more advantageous for spinal fixation applications.

  6. Effect of microalloying (Ca, Sr, and Ce) on elevated temperature tensile behavior of AZ31 magnesium sheet alloy

    Energy Technology Data Exchange (ETDEWEB)

    Shang, L., E-mail: lihong.shang@mail.mcgill.ca [McGill University, Dept. of Materials Eng., Montreal, QC H3A 2B2 (Canada); Yue, S. [McGill University, Dept. of Materials Eng., Montreal, QC H3A 2B2 (Canada); Verma, R.; Krajewski, P. [General Motors Research and Development Center, Warren, MI 48090 (United States); Galvani, C.; Essadiqi, E. [Natural Resources Canada-CANMET, Ottawa, ON K1A 0G1 (Canada)

    2011-04-25

    Research highlights: {yields} Hot tensile behavior of AZ31 sheet microalloyed with Ca, Sr and Ce was investigated. {yields} Under superplastic conditions the formability is notably improved by microalloying. {yields} Second phase particles resist grain coarsening and retard cavitations' development. {yields} Under the high Z conditions the deformation is controlled by the dislocation creep. {yields} Under the low Z conditions the deformation is controlled by grain boundary sliding. - Abstract: The effect of microalloying with calcium, strontium, and cerium on the microstructure and the elevated temperature deformation behavior of magnesium sheet alloy AZ31 was investigated. Base composition and microalloyed AZ31 materials were cast and rolled into wrought sheet by an identical thermo-mechanical process. A series of hot tensile tests (temperatures of 300 deg. C, 400 deg. C, and 450 deg. C; constant true strain rates of 0.1 s{sup -1}, 0.01 s{sup -1}, 0.001 s{sup -1}, and 0.0003 s{sup -1}) were performed to characterize the deformation behavior of the sheet alloys. Interrupted tensile tests were used to study microstructural evolution with strain. A well-dispersed and thermally stable second phase produced by microalloying refines, stabilizes the grain structure, and significantly enhances hot formability of AZ31 sheet. The enhancement is most pronounced under deformation conditions of 450 deg. C and; 0.0003 s{sup -1} strain rate, with tensile elongation increasing from 347% for the base alloy, to 406% with Ca only, 437% with Ca and Ce, and 552% with Ca, Sr and Ce for microalloyed AZ31 alloys. The second phase particles resist grain coarsening, promote grain boundary sliding, retard strain localization or necking, and postpone cavitation to higher strain levels to achieve this improvement in formability.

  7. Strength variation and deformational behavior in anisotropic granitic mylonites under high-temperature and -pressure conditions - An experimental study

    Science.gov (United States)

    Liu, Gui; Zhou, Yongsheng; Shi, Yaolin; Miao, Sheqiang; He, Changrong

    2017-03-01

    We performed deformation experiments on foliated granitic mylonites under high-temperature and -pressure conditions. To investigate the effects of pre-existing fabric properties on the rheology of the rocks, these experiments were carried out at different compression directions 30°, 45°, and 60° relative to the foliation, at temperatures of 600-850 °C, under confining pressures of 800-1200 MPa, within a strain rate range of 1 × 10-4/S - 2.5 × 10-6/S. The results of the experiments show that the deformation of three group samples is in the semi-brittle region at temperatures between 600 and 700 °C, and that the deformation of the samples transforms to plastic deformation by power-law creep with the stress exponent n = 3 ± 0.3 at temperatures between 800 and 850 °C. In the semi-brittle region, the mechanical data show that strength reaches its minimum value at an angle of 30° between the compression direction and the original foliation. In the plastic deformation regime, strength reaches its minimum value at an angle of 45° between the foliation and the orientation of the maximum principal stress. The strength with angles between 30° and 60° is lower than that of the compression direction perpendicular to foliation and the compression direction parallel to foliation. Microstructure analysis based on optical and electron microscopy of the deformation microstructures showed plastic deformation of aggregates of biotite and quartz at 800-850 °C. This deformation was extensive and formed new foliation. Quartz c-axis fabrics analysis by EBSD show that at temperatures of 600-700 °C, the c-axis fabric patterns could have been formed by the dominant activity of basal slip, similar with the starting granitic mylonite samples, but the dominant slip systems have been changed and transformed from basal slip to rhomb slip and prism slip at temperature of 800 °C and 850 °C. Microfractures were developed in hornblende and feldspar grains with local plastic

  8. The hot deformation behavior and microstructure evolution of HA/Mg-3Zn-0.8Zr composites for biomedical application.

    Science.gov (United States)

    Liu, Debao; Liu, Yichi; Zhao, Yue; Huang, Y; Chen, Minfang

    2017-08-01

    The hot deformation behavior of nano-sized hydroxylapatite (HA) reinforced Mg-3Zn-0.8Zr composites were performed by means of Gleeble-1500D thermal simulation machine in a temperature range of 523-673K and a strain rate range of 0.001-1s(-1), and the microstructure evolution during hot compression deformation were also investigated. The results show that the flow stress increases increasing strain rates at a constant temperature, and decreases with increasing deforming temperatures at a constant strain rate. Under the same processing conditions, the flow stresses of the 1HA/Mg-3Zn-0.8Zr specimens are higher than those of the Mg-3Zn-0.8Zr alloy specimens, and the difference is getting closer with increasing deformation temperature. The hot deformation behaviors of Mg-3Zn-0.8Zr and 1HA/Mg-3Zn-0.8Zr can be described by constitutive equation of hyperbolic sine function with the hot deformation activation energy being 124.6kJ/mol and 125.3kJ/mol, respectively. Comparing with Mg-3Zn-0.8Zr alloy, the instability region in the process map of 1HA/Mg-3Zn-0.8Zr expanded to a bigger extent at the same conditions. The optimum process conditions of 1HA/Mg-3Zn-0.8Zr composite is concluded as between the temperature window of 573-623K with a strain rate range of 0.001-0.1s(-1). A higher volume fraction and smaller grain size of dynamic recrystallization (DRX) grains was observed in 1HA/Mg-3Zn-0.8Zr specimens after the hot compression deformation compared with Mg-3Zn-0.8Zr alloy, which was ascribed to the presence of the HA particles that play an important role in particle-stimulated nucleation (PSN) mechanism and can effectively hinder the migration of interfaces. Copyright © 2017 Elsevier B.V. All rights reserved.

  9. Microstructure and High Temperature Plastic Deformation Behavior of Al-12Si Based Alloy Fabricated by an Electromagnetic Casting and Stirring Process

    Energy Technology Data Exchange (ETDEWEB)

    Jeon, Kyung-Soo; Roh, Heung-Ryeol; Kim, Mok-Soon [Inha University, Incheon (Korea, Republic of); Kim, Jong-Ho; Park, Joon-Pyo [Research Institute of Industrial Science and Technology, Pohang (Korea, Republic of)

    2017-06-15

    An as-received EMC/S (electromagnetic casting and stirring)-processed Al-12Si based alloy billet was homogenized to examine its microstructure and high temperature plastic deformation behavior, using compressive tests over the temperature range from 623 to 743 K and a strain rate range from 1.0×10{sup -3} to 1.0×10{sup 0}s{sup -1}. The results were compared with samples processed by the direct chill casting (DC) method. The fraction of equiaxed structure for the as-received EMC/S billet(41%) was much higher than that of the as-received DC billet(6 %). All true stress – true strain curves acquired from the compressive tests exhibited a peak stress at the initial stage of plastic deformation. Flow stress showed a steady state region after the appearance of peak stress with increasing strain. The peak stress decreased with increasing temperature at a given strain rate and a decreasing strain rate at a given temperature. A constitutive equation was made for each alloy, which could be used to predict the peak stress. A recrystallized grain structure was observed in all the deformed specimens, indicating that dynamic recrystallization is the predominant mechanism during high temperature plastic deformation of both the homogenized EMC/S and DC-processed Al-12Si based alloys.

  10. Influence of alloying and testing conditions on mechanical properties and deformation behavior of 〈100〉 tungsten-based single crystals

    Energy Technology Data Exchange (ETDEWEB)

    Skotnicova, Katerina, E-mail: Katerina.Skotnicova@vsb.cz [VSB – Technical University of Ostrava, Faculty of Metallurgy and Materials Engineering, Department of Regional Materials Science and Technology Centre, Avenue 17 Listopadu 15, 70833 Ostrava-Poruba (Czech Republic); Kirillova, Valentina M.; Ermishkin, Vjacheslav A. [Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Leninski Prospect 49, 119991 Moscow (Russian Federation); Cegan, Tomas; Jurica, Jan; Kraus, Martin [VSB – Technical University of Ostrava, Faculty of Metallurgy and Materials Engineering, Department of Regional Materials Science and Technology Centre, Avenue 17 Listopadu 15, 70833 Ostrava-Poruba (Czech Republic); Burkhanov, Gennadij S. [Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Leninski Prospect 49, 119991 Moscow (Russian Federation)

    2015-06-11

    The results of the pressure testing of mechanical properties of single crystals of pure tungsten and low-alloyed alloys W–2Re and W–1Re–1Mo (wt%) with a crystallographic orientation 〈100〉 which were prepared by plasma-arc melting are summarized. The effect of alloying and the deformation rate on these properties have also been investigated and the fracture surfaces of the individual single crystals have been evaluated with the aid of the photometric method. The differences in the deformation behavior of pure tungsten and W–Re and W–1Mo–Re alloys were observed, which relate to the particularities of rhenium and molybdenum action in the tungsten solid solution. It can be seen from the observed results that tungsten alloying with low rhenium and molybdenum contents decreased all mechanical properties when applying the deformation rate of 0.2 mm/min. The biggest decrease was observed for the offset yield strength value. When testing with the deformation rate of 2 mm/min, the strength limit of the W–2Re alloy increased to 2013 MPa, while R{sub pt0.2} decreased by 33% in comparison with the pure tungsten single crystal. However, the ε{sub r} value remained at the same level ∼30%. In the W–1Re–1Mo single crystal, the R{sub pt0.2} and R{sub mt} values decreased, while ε{sub r} increased slightly.

  11. Cyclic Deformation Behavior of Fe-18Cr-18Mn-0.63N Nickel-Free High-Nitrogen Austenitic Stainless Steel

    Science.gov (United States)

    Shao, C. W.; Shi, F.; Li, X. W.

    2015-04-01

    Cyclic deformation and damage behavior of a Ni-free high-nitrogen austenitic stainless steel with a composition of Fe-18Cr-18Mn-0.63N (weight pct) were studied, and the internal stress and effective stress were estimated by partitioning the hysteresis loop during cyclic straining at total strain amplitudes ranging from 3.0 × 10-3 to 1.0 × 10-2. It is found that immediate cyclic softening takes place at all strain amplitudes and subsequently a saturation or quasi-saturation state develops and occupies the main part of the whole fatigue life. The internal stress increases with increasing strain amplitude, while the variation of effective stress with strain amplitude is somewhat complicated. Such a phenomenon is discussed in terms of dislocation structures and the short-range ordering caused by the interaction between nitrogen atoms and substitutional atoms. The relationship of fatigue life vs plastic strain amplitude ( N f-Δ ɛ pl/2) follows a bilinear Coffin-Manson rule, resulting from the variation in slip deformation mode with the applied strain amplitude. At the low strain amplitude, cracks initiate along slip bands, and planar slip dislocation configurations dominate the major characteristic of internal microstructures. At high strain amplitudes, intergranular (mostly along grain boundaries and few along twin boundaries) cracks are generally found, and the deformation microstructures are mainly composed of dislocation cells, stacking faults and a small amount of deformation twins, in addition to planar slip dislocation structures.

  12. T23钢的热变形行为%Thermal deformation behavior of T23 steel

    Institute of Scientific and Technical Information of China (English)

    李红英; 巫荣海; 魏冬冬; 李阳华; 龙功名; 王晓峰

    2013-01-01

    The hot deformation behavior and corresponding microstructure of T23 steel were investigated at strain rates ranging from 0. 01 to 5 s-1 and at 1000 - 1250℃ by hot compression test on a Gleeble 1500 thermal-mechanical simulator. True stress-true strain curves were obtained. Processing map was established based on the dynamic material model and flow stress equation was derivated. The results show that both dynamic recovery and dynamic recrystallization occur during hot compression test. The higher the temperature is and the smaller the strain rate is, the more easily the dynamic recrystallization occurs. The processing maps with strain of 0. 5 and 0. 6 present four similar unstable areas, and the distribution of power dissipation factor is similar too. The peak area is 1175 - 1240℃ and 0.03 -0.25 s-1 , corresponding to the peak efficiency of 47. 3% (0.5) and 46. 3% (0.6). In flow stress equation, structure factor A is 5. 23 × 1012 s-1 , stress level parameters a is 0. 01155 Mpa , stress index n is 4.46869, respectively. Deformation activation energy is 368. 65 kJ/mol.%利用Gleeble-1500热模拟机进行热压缩实验,对T23钢在变形速率为0.01 ~5 s-1,变形温度为1000~1250 ℃的热变形行为和组织进行研究.根据实验获得的真应力-真应变曲线,基于动态材料模型建立了热加工图,并推导出流变应力方程.结果表明:T23钢在热压缩过程中存在动态回复和动态再结晶两种软化机制,变形温度越高或变形速率越小,越容易发生动态再结晶.真应变量为0.5和0.6的加工图具有4个类似的失稳区,功率耗散效率因子的分布规律大致相同,峰值区在1175 ~1240℃和0.03~0.25 s-1范围,对应的峰值效率分别为47.3%(0.5)和46.3%(0.6).流变应力方程中,结构因子A、应力水平参数α、应力指数n分别为5.23×1012 s-1、0.01155 MPa-1和4.46869,热变形激活能为368.65 kJ/mol.

  13. Structural mechanisms as revealed by real time mechano optical behavior of polylactic acid films in uni and biaxial deformation and heat setting processes

    Science.gov (United States)

    Ou, Xuesong

    In this study, structural development during PLA film processing was investigated with a new instrumented biaxial stretcher capable of real time monitoring of true stress, true strain and in-plane as well as out-of-plane birefringence under fast deformation rates. The effects of stretching rate and mode on mechano-optical behaviors and correspondent morphology development were investigated. At low deformation levels, a linear regime I associated with orientation of amorphous chains was observed in all modes of deformation. Following regime I, a steeper regime II associated with stress induced crystallization was observed during uniaxial constrained width (UCW) stretching under low rates before birefringence begins to level off in regime III due to finite extensibility of chains. During UCW stretching under high rate, regime I transformed directly into regime III, and this is associated with the formation of a very stable nematic mesophase. Direct transformation from regime I to regime III is observed during simultaneous biaxial (SIM) stretching under all rates. The kinetics of structural changes during heat setting from a pre-oriented state was investigated by rapid tracking of in and out-of-plane birefringence of pre-oriented films with a new instrumented annealing chamber capable of fast sample insertion and removal. Development of birefringence, which reflects overall chain orientation, and associated structural evolution during constrained annealing of extended PLA films were clarified. Structural evolution is determined by the competition between chain relaxation and registration of segments into well oriented nuclei that grow during annealing, leading to formation of a long range network of chains that arrests the chains in their oriented state. At low deformation the temporal evolution of birefringence first involves relaxation followed by a rapid increase associated with crystallization. The initial relaxation disappears with increase in deformation in the

  14. Reliability Assessment of Impact Tensile Testing Apparatus using a Drop-bar Striker for Intermediate Strain-rate Range and Evaluation of Dynamic Deformation Behaviors for a Carbon Steel

    Energy Technology Data Exchange (ETDEWEB)

    Bae, Kyung Oh; Kim, Dae Woong; Shin, Hyung Seop [Andong National Univ., Andong (Korea, Republic of); Park, Lee Ju; Kim, Hyung Won [Agency for Defense Development, Daejeon (Korea, Republic of)

    2016-06-15

    Studies on the deformation behavior of materials subjected to impact loads have been carried out in various fields of engineering and industry. The deformation and fracture of members for these machines/structures are known to correspond to the intermediate strain-rate region. Therefore, for the structural design, it is necessary to consider the dynamic deformation behavior in these intermediate strain-rate ranges. However, there have been few reports with useful data about the deformation and fracture behavior at intermediate strain-rate ranges. Because the intermediate strain-rate region is located between quasi-static and high strain-rate regions, it is difficult to obtain the intermediate strain-rate using conventional reasonable test equipment. To solve this problem, in this study, the measurement reliability of the constructed drop-bar impact tensile test apparatus was established and the dynamic behavior at the intermediate strain-rate range of carbon steels was evaluated by utilizing the apparatus.

  15. Use of laser(s) in the process of superplastic forming and diffusion bonding

    Energy Technology Data Exchange (ETDEWEB)

    Jocelyn, A.; Jonik, M.; Keevil, A.; Ackerman, M.; Way, J.; Flower, T. [Aerospace Mfg. Research Centre, Faculty of Computing, Engineering and Mathematical Sciences, Coldharbour Lane, Bristol (United Kingdom); Kar, A. [Univ. of Central Florida, School Optics/CREOL, Orlando, FL (United States)

    2004-07-01

    Superplastic forming and diffusion bonding (SPF/DB) has permitted the manufacture of some of the lightest, strongest, corrosion resistant, complex, and yet often elegant structures ever to be produced. For the last 30 years, all such components have been made by some form of high thermal-mass, isothermal method of production using conventional equipment, such as hot platen presses or furnaces. However, if laser(s) could be used just to heat the material to be superplastically formed, this could provide a novel, low thermal-mass, means of production which could, relatively easily, be integrated into a laser based manufacturing centre. In this paper, a concept is described of how a laser based manufacturing centre, comprised of a number of individual process cells, together with integrated pre and post SPF/DB operations, would work and the benefits that would result. The concept is based on four considerations. Firstly, that it is essential to heat the material directly and quickly. Secondly, the environment must be completely inert so that there is no contamination of components. Thirdly, the complete process of diffusion bonding must only entail the use of laser(s). Lastly, established laser activities such as cutting, welding, hole drilling or trepanning and the removal of surplus material, must be integrated into the process. In addition, the envisaged cells need to be modular in concept so industry can acquire capital plant progressively, thereby spreading the cost over time. (orig.)

  16. Standard test method for determining the superplastic properties of metallic sheet materials

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2008-01-01

    1.1 This test method describes the procedure for determining the superplastic forming properties (SPF) of a metallic sheet material. It includes tests both for the basic SPF properties and also for derived SPF properties. The test for basic properties encompasses effects due to strain hardening or softening. 1.2 This test method covers sheet materials with thicknesses of at least 0.5 mm but not greater than 6 mm. It characterizes the material under a uni-axial tensile stress condition. Note 1—Most industrial applications of superplastic forming involve a multi-axial stress condition in a sheet; however it is more convenient to characterize a material under a uni-axial tensile stress condition. Tests should be performed in different orientations to the rolling direction of the sheet to ascertain initial anisotropy. 1.3 This method has been used successfully between strain rates of 10-5 to 10-1 per second. 1.4 This method has been used successfully on Aluminum and Titanium alloys. The use of the method wi...

  17. Effect of Tempering Time on Microstructure, Tensile Properties, and Deformation Behavior of a Ferritic Light-Weight Steel

    Science.gov (United States)

    Han, Seung Youb; Shin, Sang Yong; Lee, Byeong-Joo; Lee, Sunghak; Kim, Nack J.; Kwak, Jai-Hyun

    2013-01-01

    In the present study, a ferritic light-weight steel was tempered at 973 K (700 °C) for various tempering times, and tensile properties and deformation mechanisms were investigated and correlated to microstructure. κ-carbides precipitated in the tempered band-shaped martensite and ferrite matrix, and the tempered martensite became more decomposed with increasing tempering time. Tempering times for 3 days or longer led to the formation of austenite as irregular thick-film shapes mostly along boundaries between the tempered martensite and the ferrite matrix. Tensile tests of the 1-day-tempered specimen showed that deformation bands were homogeneously spread throughout the specimen, and that the fine carbides were sufficiently deformed inside these deformation bands resulting in high strength and ductility. The 3-day-tempered specimen showed a small amount of boundary austenite, which readily developed voids or cracks and became sites for fracture. This cracking at boundary austenites became more prominent in the 7- and 15-day-tempered specimens, as the volume fraction of boundary austenites increased with increasing tempering time. These findings suggested that, when the steel was tempered at 973 K (700 °C) for an appropriate time, i.e., 1 day, to sufficiently precipitate κ-carbides and to prevent the formation of boundary austenites, that the deformation occurred homogeneously, leading to overall higher mechanical properties.

  18. Analysis of structure and deformation behavior of AISI 316L tensile specimens from the second operational target module at the Spallation Neutron Source

    Science.gov (United States)

    Gussev, M. N.; McClintock, D. A.; Garner, F. A.

    2016-01-01

    In an earlier publication, tensile testing was performed on specimens removed from the first two operational targets of the Spallation Neutron Source (SNS). There were several anomalous features in the results. First, some specimens had very large elongations (up to 57%) while others had significantly smaller values (10-30%). Second, there was a larger than the usual amount of data scatter in the elongation results. Third, the stress-strain diagrams of nominally similar specimens spanned a wide range of behavior ranging from expected irradiation-induced hardening to varying levels of force drop after yield point and indirect signs of "traveling deformation wave" behavior associated with strain-induced martensite formation. To investigate the cause(s) of such variable tensile behavior, several specimens from Target 2, spanning the range of observed tensile behavior, were chosen for detailed microstructural examination using electron backscatter diffraction (EBSD) analysis. It was shown that the steel employed in the construction of the target contained an unexpected bimodal grain size distribution, containing very large out-of-specification grains surrounded by "necklaces" of grains of within-specification sizes. The large grains were frequently comparable to the width of the gauge section of the tensile specimen. The propensity to form martensite during deformation was shown to be accelerated by radiation but also to be very sensitive to the relative orientation of the grains with respect to the tensile axis. Specimens having large grains in the gauge that were most favorably oriented for production of martensite strongly exhibited the traveling deformation wave phenomenon, while those specimens with less favorably oriented grains had lesser or no degree of the wave effect, thereby accounting for the observed data scatter.

  19. Deformation behavior of carbon-fiber reinforced shape-memory-polymer composites used for deployable structures (Conference Presentation)

    Science.gov (United States)

    Lan, Xin; Liu, Liwu; Li, Fengfeng; Pan, Chengtong; Liu, Yanju; Leng, Jinsong

    2017-04-01

    Shape memory polymers (SMPs) are a new type of smart material, they perform large reversible deformation with a certain external stimulus (e.g., heat and electricity). The properties (e.g., stiffness, strength and other mechanically static or quasi-static load-bearing capacity) are primarily considered for conventional resin-based composite materials which are mainly used for structural materials. By contrast, the mechanical actuating performance with finite deformation is considered for the shape memory polymers and their composites which can be used for both structural materials and functional materials. For shape memory polymers and their composites, the performance of active deformation is expected to further promote the development in smart active deformation structures, such as deployable space structures and morphing wing aircraft. The shape memory polymer composites (SMPCs) are also one type of High Strain Composite (HSC). The space deployable structures based on carbon fiber reinforced shape memory polymer composites (SMPCs) show great prospects. Considering the problems that SMPCs are difficult to meet the practical applications in space deployable structures in the recent ten years, this paper aims to research the mechanics of deformation, actuation and failure of SMPCs. In the overall view of the shape memory polymer material's nonlinearity (nonlinearity and stress softening in the process of pre-deformation and recovery, relaxation in storage process, irreversible deformation), by the multiple verifications among theory, finite element and experiments, one obtains the deformation and actuation mechanism for the process of "pre-deformation, energy storage and actuation" and its non-fracture constraint domain. Then, the parameters of SMPCs will be optimized. Theoretical analysis is realized by the strain energy function, additionally considering the interaction strain energy between the fiber and the matrix. For the common resin-based or soft

  20. Comparative behavior of Sr, Nd and Hf isotopic systems during fluid-related deformation at middle crust levels

    Science.gov (United States)

    Luais, Béatrice; Le Carlier de Veslud, Christian; Géraud, Yves; Gauthier-Lafaye, François

    2009-05-01

    We have carried out a comparative Rb-Sr, Sm-Nd and Lu-Hf isotopic study of a progressively deformed hercynian leucogranite from the French Massif Central, belonging to the La Marche ductile shear zone, in order to investigate the respective perturbation of these geochronometers with fluid induced deformation. The one-meter wide outcrop presents a strongly deformed and mylonitized zone at the center, and an asymmetric deformation pattern with a higher deformation gradient on the northern side of the zone. Ten samples have been carefully collected every 10 cm North and South away from the strongest deformed mylonitic zone. They have been analyzed for a complete major, trace element data set, oxygen isotopes, Rb-Sr, Sm-Nd and Lu-Hf isotopic systematics. We show that most of major and trace elements except SiO 2, alkaline elements (K 2O, Rb), and some metal transition elements (Cu), are progressively depleted with increasing deformation. This depletion includes REE + Y, but also HFS elements (Ti, Hf, Zr, Nb) which are commonly considered as immobile elements during upper level processes. Variations in elemental ratios with deformation, e.g. decrease in LREE/MREE- HREE, Nd/Hf, Th/Sr, increase in Rb/Sr, U/Th and constant Sr/Nd, lead to propose the following order of element mobility: U ≫ Th > Sr = Nd ≫ Hf + HREE. We conclude in agreement with previous tectonic and metallogenic studies that trace element patterns across the shear zone result from circulation of oxidizing F-rich hydrothermal fluids associated with deformation. A temperature of the fluid of 470-480 °C can be deduced from the δ 18O equilibrium between quartz-muscovite pairs. Elemental fractionation induces perturbation of the Rb-Sr geochronometer. The well-defined 87Rb/ 86Sr- 87Sr/ 86Sr correlation gives an apparent age of 294 ± 19 Ma, slightly younger than the 323 ± 4 Ma age of leucogranites in this area. This apparent age is interpreted as dating event of intense deformation and fluid circulation

  1. Effect of transformation on residual stress in welding. Part 5. ; Stress releasement by transformation superplasticity. Sohentai ga yosetsu zanryu oryoku ni oyobosu eikyo. 5. ; Hentai chososei ni yoru oryoku kanwa

    Energy Technology Data Exchange (ETDEWEB)

    Murata, H. (Yokogawa Medical System Ltd., Tokyo (Japan)); Kato, N. (Tokyo Inst. of Technology, Tokyo (Japan)); Tamura, H. (Nihon Univ., Tokyo (Japan))

    1993-11-05

    The residual stress and angular deformation occurred in welding are the important factors for the welding design. In the previous report, by measuring the welding angular deformation caused by the welding rod prepared experimentally with the various transformation temperatures, it was shown that the materials, which could transform at a low temperature, have been effective to restrain the welding deformation. In addition, also the elongation and stress variation in transformation after welding have been examined in detail, and consequently it has been shown quantitatively, that not only the transformation expansion, but also the transformation superplasticity have acted effectively for the stress relaxation during transformation depending on the condition. In this report, the same as in the previous report, the welding with the multilayers and multi-passes has been performed by using the welding rod prepared experimentally and of Fe-Ni-Cr system, which could transform at a low temperature and had a high stress releasement effect, and then the effect of phase transformation on the welding residual stress has been investigated. As a result, the phase transformation had a tight relation with the welding residual stress, and furthermore the compression stress has been observed on the welding metal depending on the transformation temperature. In addition, it was found that in the welding metal, the compression stress has occurred, the tensile stress has remained directly under it, and it has been connected with a peak part of the tension, and has been redistributed. 18 refs., 8 figs., 1 tab.

  2. Effect of Strength Coefficient of Bainite on Micromechanical Deformation and Failure Behaviors of Hot-Rolled 590FB Steel during Uniaxial Tension

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Eun-Young; Choi, Shi-Hoon [Sunchon National University, Suncheon (Korea, Republic of); Kim, Sung Il [POSCO Technical Research Laboratories, Gwangyang (Korea, Republic of)

    2016-11-15

    The effect of the strength coefficient (K{sub B}) of bainite on micromechanical deformation and failure behaviors of a hot-rolled 590MPa steel (590FB) during uniaxial tension was simulated using the elasto-plastic finite element method (FEM). The spatial distribution of the constituent phases was obtained using a phase identification technique based on optical microstructure. Empirical equations which depend on chemical composition were used to determine the stress-strain relationship of the constituent phases of the 590FB steel. The stress-strain partitioning and failure behavior were analyzed by increasing the K{sub B} of bainite. The elasto-plastic FEM results revealed that effective strain in the ferrite-bainite boundaries, and maximum principal stress in fibrous bainite, were enhanced as the K{sub B} increased. The elasto-plastic FEM results also demonstrated that the K{sub B} significantly affects the micromechanical deformation and failure behaviors of the hot-rolled 590FB steel during uniaxial tension.

  3. Investigation of Mechanical Properties and Plastic Deformation Behavior of (Ti45Cu40Zr10Ni5100−xAlx Metallic Glasses by Nanoindentation

    Directory of Open Access Journals (Sweden)

    Lanping Huang

    2014-01-01

    Full Text Available The effect of Al addition on mechanical properties and plastic deformation behavior of (Ti45Cu40Zr10Ni5100−xAlx (x = 0, 2, 4, 6 and 8 amorphous alloy ribbons have been investigated by nanoindentation. The hardness and elastic modulus do not simply increase with the increase of Al content. The alloy with 8 at.% Al exhibits the highest hardness and elastic modulus. The serrations or pop-in events are strongly dependent on the loading rate and alloy composition.

  4. Effect of artificial aging on the deformation behavior of an Al-1.01Mg-0.68Si-1.78Cu alloy

    Institute of Scientific and Technical Information of China (English)

    HE Lizi; CHEN Yanbo; ZHANG Haitao; CUI Jianzhong

    2008-01-01

    The influences of artificial aging on the microstructures and mechanical properties of an AI-1.01Mg-0.68Si-1.78Cu alloy were investigated.The detailed fracture surfaces,precipitates,and dislocation structures were also examined through scanning electron microscopy (SEM) and transmission electron microscopy (TEM).The results show that the tensile strengths exhibit two peak values and reach saturated values with increasing aging time,while the elongation decreases sharply to the minimum value and changes slightly later.The deformation and fracture behaviors arc also closely related to the aging conditions.

  5. Nanomechanical Properties and Deformation Behaviors of Multi-Component (AlCrTaTiZrNxSiy High-Entropy Coatings

    Directory of Open Access Journals (Sweden)

    Shao-Yi Lin

    2013-12-01

    Full Text Available In this study multi-component (AlCrTaTiZrNxSiy high-entropy coatings were developed by co-sputtering of AlCrTaTiZr alloy and Si in an Ar/N2 mixed atmosphere with the application of different substrate biases and Si-target powers. Their nanomechanical properties and deformation behaviors were characterized by nanoindentation tests. Because of the effect of high mixing entropies, all the deposited multi-component (AlCrTaTiZrNxSiy high-entropy coatings exhibited a simple face-centered cubic solid-solution structure. With an increased substrate bias and Si-target power, their microstructures changed from large columns with a [111] preferred orientation to a nanocomposite form with ultrafine grains. The hardness, H/E ratio and H3/E2 ratio of (AlCrTaTiZrN1.07Si0.15 coating reached 30.2 GPa, 0.12 and 0.41 GPa, respectively, suggesting markedly suppressed dislocation activities and a very high resistance to wear and plastic deformation, attributable to grain refinements and film densification by the application of substrate bias, a nanocomposite structure by the introduction of silicon nitrides, and a strengthening effect induced by severe lattice distortions. In the deformed regions under indents, stacking faults or partial dislocations were formed, while in the stress-released regions, near-perfect lattices recovered.

  6. Insights into the deformation behavior of the CrMnFeCoNi high-entropy alloy revealed by elevated temperature nanoindentation

    Energy Technology Data Exchange (ETDEWEB)

    Maier-Kiener, Verena [Montanuniversitat Leoben, Leoben (Austria); Schuh, Benjamin [Austrian Academy of Sciences, Leoben (Austria); George, Easo P. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Univ. of Tennessee, Knoxville, TN (United States); Clemens, Helmut [Montanuniversitat Leoben, Leoben (Austria); Hohenwarter, Anton [Austrian Academy of Sciences, Leoben (Austria)

    2017-07-27

    A CrMnFeCoNi high-entropy alloy was investigated by nanoindentation from room temperature to 400 °C in the nanocrystalline state and cast plus homogenized coarse-grained state. In the latter case a < 100 >-orientated grain was selected by electron back scatter diffraction for nanoindentation. It was found that hardness decreases more strongly with increasing temperature than Young’s modulus, especially for the coarse-grained state. The modulus of the nanocrystalline state was slightly higher than that of the coarse-grained one. For the coarse-grained sample a strong thermally activated deformation behavior was found up to 100–150 °C, followed by a diminishing thermally activated contribution at higher testing temperatures. For the nanocrystalline state, different temperature dependent deformation mechanisms are proposed. At low temperatures, the governing processes appear to be similar to those in the coarse-grained sample, but with increasing temperature, dislocation-grain boundary interactions likely become more dominant. Finally, at 400 °C, decomposition of the nanocrystalline alloy causes a further reduction in thermal activation. Furthermore, this is rationalized by a reduction of the deformation controlling internal length scale by precipitate formation in conjunction with a diffusional contribution.

  7. Deformation Behavior and Microstructure Evolution of As-Cast 42CrMo Alloy in Isothermal and Non-isothermal Compression

    Science.gov (United States)

    Qin, Fangcheng; Li, Yongtang; Qi, Huiping; Lv, Zhenhua

    2016-11-01

    The isothermal and non-isothermal multi-pass compression tests of centrifugal casting 42CrMo steel were conducted on a Gleeble-3500 thermal simulation machine. The effects of compression passes and finishing temperatures on deformation behavior and microstructure evolution were investigated. It is found that the microstructure is homogeneous with equiaxed grains, and the flow stress does not show significant change with the increase in passes, while the peak softening coefficient increases first and then decreases during inter-pass. Moreover, the dominant mechanisms of controlled temperature and accumulated static recrystallization for grain refinement and its homogeneous distribution are found after 5 passes deformation. As the finishing temperature increases, the flow stress decreases gradually, but the dynamic recrystallization accelerates and softening effect increases, resulting in the larger grain size and homogeneous microstructure. The microhardness decreases sharply because the sufficient softening occurs in microstructure. When the finishing temperature is 890 °C, the carbide particles are precipitated in the vicinity of the grain boundaries, thus inhibiting the dislocation motion. Thus, the higher finishing temperature (≥970 °C) for centrifugal casting 42CrMo alloy should be avoided in non-isothermal multi-pass deformation, which is beneficial to grain refinement and properties improvement.

  8. Analytical modeling of the thermomechanical behavior of ASTM F-1586 high nitrogen austenitic stainless steel used as a biomaterial under multipass deformation.

    Science.gov (United States)

    Bernardes, Fabiano R; Rodrigues, Samuel F; Silva, Eden S; Reis, Gedeon S; Silva, Mariana B R; Junior, Alberto M J; Balancin, Oscar

    2015-06-01

    Precipitation-recrystallization interactions in ASTM F-1586 austenitic stainless steel were studied by means of hot torsion tests with multipass deformation under continuous cooling, simulating an industrial laminating process. Samples were deformed at 0.2 and 0.3 at a strain rate of 1.0s(-1), in a temperature range of 900 to 1200°C and interpass times varying from 5 to 80s. The tests indicate that the stress level depends on deformation temperature and the slope of the equivalent mean stress (EMS) vs. 1/T presents two distinct behaviors, with a transition at around 1100°C, the non-recrystallization temperature (Tnr). Below the Tnr, strain-induced precipitation of Z-phase (NbCrN) occurs in short interpass times (tpass<30s), inhibiting recrystallization and promoting stepwise stress build-up with strong recovery, which is responsible for increasing the Tnr. At interpass times longer than 30s, the coalescence and dissolution of precipitates promote a decrease in the Tnr and favor the formation of recrystallized grains. Based on this evidence, the physical simulation of controlled processing allows for a domain refined grain with better mechanical properties.

  9. Effect of Vanadium on the Hot Deformation Behavior of Vanadium-Microalloyed Steel for Thin Slab Direct Rolling

    Science.gov (United States)

    Lee, Chang Wook; Seong, Hwan Goo; De Cooman, Bruno C.

    2016-07-01

    The effects of V on hot deformation properties of low-carbon steel were investigated in the temperature range of 1173 K to 1473 K (900 °C to 1200 °C) and for strain rates from 0.1 to 5 s-1 for compositions with a V content in the range of 0 to 0.125 wt pct. The critical stress and strain for dynamic recrystallization (DRX) initiation were obtained from the stress dependence of the strain hardening rate. The hot deformation properties of V-alloyed steel were studied in function of the temperature-corrected strain rate. The experimental results were used to construct a kinetic model of DRX. V was found to have no influence on the hot deformation properties for V contents less than 0.125 pct, indicating the absence of both solute drag and precipitation effects at low V content. When the V content reached 0.125 wt pct, the activation energy for DRX increased and DRX was suppressed in high strain rate condition.

  10. Microstructure and annealing behavior of a modified 9Cr-1Mo steel after dynamic plastic deformation to different strains

    Science.gov (United States)

    Zhang, Z. B.; Mishin, O. V.; Tao, N. R.; Pantleon, W.

    2015-03-01

    The microstructure, hardness and tensile properties of a modified 9Cr-1Mo steel processed by dynamic plastic deformation (DPD) to different strains (0.5 and 2.3) have been investigated in the as-deformed and annealed conditions. It is found that significant structural refinement and a high level of strength can be achieved by DPD to a strain of 2.3, and that the microstructure at this strain contains a large fraction of high angle boundaries. The ductility of the DPD processed steel is however low. Considerable structural coarsening of the deformed microstructure without pronounced recrystallization takes place during annealing of the low-strain and high-strain samples for 1 h at 650 °C and 600 °C, respectively. Both coarsening and partial recrystallization occur in the high-strain sample during annealing at 650 °C for 1 h. For this sample, it is found that whereas coarsening alone results in a loss of strength with only a small gain in ductility, coarsening combined with pronounced partial recrystallization enables a combination of appreciably increased ductility and comparatively high strength.

  11. Microstructure and annealing behavior of a modified 9Cr−1Mo steel after dynamic plastic deformation to different strains

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Z.B.; Mishin, O.V. [Danish-Chinese Center for Nanometals, Section for Materials Science and Advanced Characterization, Department of Wind Energy, Technical University of Denmark, Risø Campus, 4000 Roskilde (Denmark); Sino-Danish Center for Education and Research (China); Sino-Danish Center for Education and Research (Denmark); Tao, N.R. [Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Science, Shenyang 110016 (China); Sino-Danish Center for Education and Research (China); Sino-Danish Center for Education and Research (Denmark); Pantleon, W., E-mail: pawo@dtu.dk [Section for Materials and Surface Engineering, Department of Mechanical Engineering, Technical University of Denmark, 2800 Kgs. Lyngby (Denmark); Sino-Danish Center for Education and Research (China); Sino-Danish Center for Education and Research (Denmark)

    2015-03-15

    The microstructure, hardness and tensile properties of a modified 9Cr−1Mo steel processed by dynamic plastic deformation (DPD) to different strains (0.5 and 2.3) have been investigated in the as-deformed and annealed conditions. It is found that significant structural refinement and a high level of strength can be achieved by DPD to a strain of 2.3, and that the microstructure at this strain contains a large fraction of high angle boundaries. The ductility of the DPD processed steel is however low. Considerable structural coarsening of the deformed microstructure without pronounced recrystallization takes place during annealing of the low-strain and high-strain samples for 1 h at 650 °C and 600 °C, respectively. Both coarsening and partial recrystallization occur in the high-strain sample during annealing at 650 °C for 1 h. For this sample, it is found that whereas coarsening alone results in a loss of strength with only a small gain in ductility, coarsening combined with pronounced partial recrystallization enables a combination of appreciably increased ductility and comparatively high strength.

  12. Hot deformation behavior and dynamic recrystallization kinetics of AZ61 and AZ61 + Sr magnesium alloys

    Directory of Open Access Journals (Sweden)

    S. Aliakbari Sani

    2016-06-01

    Full Text Available In this study, the effect of strontium addition on hot deformation of AZ61 alloy was investigated by hot compression tests. A reference alloy (AZ61 and an Sr-containing alloy (AZ61 + Sr was cast while their average initial grain size were supposed to be about 140 and 40 µm, respectively. In AZ61 + Sr alloy, the Sr-containing precipitations were stable at homogenization temperature. Analysing the hot compression curves, it was revealed that dynamic recrystallization phenomenon had occurred and controlled the thermomechanical behaviour of the alloys. The derived constitutive equations showed that the hot deformation parameters (n and Q in AZ61 + Sr alloy is smaller than those of AZ61 alloy; this can be related to the small initial grain size and the lower amounts of solute aluminium atoms. The analysis of DRX kinetics along with the micrographs of the deformed microstructures showed that at the same condition the development of DRXed microstructure in AZ61 + Sr alloy was faster than AZ61 alloy. The increased recrystallized microstructure was interpretated to be attributed to (1 the more grain boundaries present and (2 the existance of the Al-Mg-Sr precipitations assisted the PSN mechanism. Also, the attenuated intensity of the basal texture of AZ61 + Sr was related to the DRX fraction of microstructure.

  13. Superplastic Solid-Phase Welding of 40 Cr-T10A Steel

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    The microstructure of 40Cr and T10A steel sample and its surface to be welded is ultra-fined through salt-bath cyclic quenching and high frequency hardening, then the surface is cleaned. Under non-vacuum and no shielded gas, the welding parameter of isothermal superplastic solidphase welding and the effect of surface microstructure prior to pressure welding on the quality of joint are studied. At the temperature of 730~750°C and at initial strain rate of (2~4) × 10-4 s-1,the strength of the joint is up to or close to that of 40Cr base metal in 3~5 min pressure welding.

  14. Synthesis and Enhanced Superplasticity of the Zirconia-dispersed Alumina Nanocomposite

    Institute of Scientific and Technical Information of China (English)

    Guoqing CHEN; Kaifeng ZHANG; Wenbo HAN; Junting LUO

    2005-01-01

    A series of alumina-zirconia composites with various grain sizes were prepared from the nano-sized powders with different agglomerations. Microstructural analysis of the sintered compacts indicates that the as-sintered material is a typical intra/inter granular nanocomposite with uniform distribution of the zirconia grains in the alumina matrix.Superplastic deep drawing test under different conditions demonstrates that dense Al2O3/ZrO2 samples with average grain size of 230 nm can be elongated to a dome height of at least 12 mm at the punch rate of 0.6 mm.min-1at 1400℃. Further drawing tests show that for the composites with larger grain size, such elongation cannot be achieved at such a strain rate.

  15. Cryogenic mechanical properties of low density superplastically formable Al-Li alloys

    Science.gov (United States)

    Verzasconi, S. L.; Morris, J. W., Jr.

    1989-01-01

    The aerospace industry is considering the use of low density, superplastically formable (SPF) materials, such as Al-Li alloys in cryogenic tankage. SPF modifications of alloys 8090, 2090, and 2090+In were tested for strength and Kahn tear toughness. The results were compared to those of similar tests of 2219-T87, an alloy currently used in cryogenic tankage, and 2090-T81, a recently studied Al-Li alloy with exceptional cryogenic properties (1-9). With decreasing temperature, all materials showed an increase in strength, while most materials showed an increase in elongation and decrease in Kahn toughness. The indium addition to 2090 increased alloy strength, but did not improve the strength-toughness combination. The fracture mode was predominantly intergranular along small, recrystallized grains, with some transgranular fracture, some ductile rupture, and some delamination on large, unrecrystallized grains.

  16. Measurement of large deformation of nylon cord-rubber composite and effects of perpendicular loads on its stress-strain behaviors

    Institute of Scientific and Technical Information of China (English)

    张丰发; 杜星文; 于增信

    2003-01-01

    Effects of transverse loads on longitudinal stress-strain behaviors and longitudinal constant tensile loads on transverse stress-strain behaviors of single ply of nylon cord-rubber composite are studied respectively under biaxial tensile condition with cruciform specimen. Effects of transverse constant tensile load on longitudinal tensile mechanical properties are indistinctive compared with corresponding uniaxial longitudinal tensile mechanical properties. It can be relative to larger difference between longitudinal and transverse mechanical properties. Its dominating failure mode is typical fiber-dominated mode; However, Experiment results indicate that transverse mechanical properties of nylon cord-rubber composite with longitudinal constant tensile loads are distinct from its uniaxial transverse tensile mechanical properties. It can be attribute to action of longitudinal tension that makes material rigidify in the direction perpendicular to fiber, Mode of failure is representative of matrix-dominated failure. For the measurement of large deformation up to 50 percent, a special CCD imaging method is employed in the experimental investigation that makes measurement of large deformations more precise.

  17. New insight into deformation-dependent hydraulic permeability of gels and cartilage, and dynamic behavior of agarose gels in confined compression.

    Science.gov (United States)

    Gu, W Y; Yao, H; Huang, C Y; Cheung, H S

    2003-04-01

    Equilibrium, creep, and dynamic behaviors of agarose gels (2.0-14.8%) in confined compression were investigated in this study. The hydraulic permeabilities of gels were determined by curve-fitting creep data to the biphasic model (J. Biomech. Eng. 102 (1980) 73) and found to be similar in value to those published in the literature (AIChE J. 42 (1996) 1220). A new relationship between intrinsic permeability and volume fraction of water was found for agarose gel, capable of predicting deformation-dependent permeabilities of bovine articular cartilage and 2% agarose gel published in literature. This relationship is accurate for gels and cartilage over a wide range of permeabilities (four orders of magnitude variation). The dynamic stiffness of the gels increases with gel concentration and loading frequency (0.01-1.0Hz). The increase in dynamic stiffness with loading frequency is less pronounced for gels with higher concentrations. The results of this study provide a new insight into deformation-dependent permeability behavior of agarose gel and cartilage, and are important for understanding biological responses of cells to interstitial fluid flow in gel or in cartilage under dynamic mechanical loading.

  18. Synergistic effect of austenitizing temperature and hot plastic deformation strain on the precipitation behavior in novel HSLA steel

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Chih-Yuan, E-mail: chen6563@gmail.com [Department of Energy Engineering, National United University, Miaoli 36003, Taiwan (China); Department of Materials Science and Engineering, National Taiwan University, Taipei 10617, Taiwan (China); Chen, Chien-Chon [Department of Energy Engineering, National United University, Miaoli 36003, Taiwan (China); Yang, Jer-Ren, E-mail: jryang@ntu.edu.tw [Department of Materials Science and Engineering, National Taiwan University, Taipei 10617, Taiwan (China)

    2015-07-15

    Examination of thin foils of specimens with various austenitizing conditions by transmission electron microscopy revealed randomly homogeneous precipitation in the ferrite for each experimental condition. Though no interphase precipitation was found in the present study, two types of random precipitation morphologies were identified in the ferrite matrix. One was randomly and homogeneously precipitated carbides of smaller size (<10 nm), and the other was randomly precipitated carbides of larger size (10–30 nm). Transmission electron microscopy results provided evidence that both types of precipitation carbides could be associated with the supersaturation of microalloying elements in the ferrite and austenite, respectively. A higher austenitizing temperature treatment can lead to more microalloying elements dissolving in the austenite such that many tiny carbides precipitation at the low isothermal holding temperature, which is believed to effectively strengthen the ferrite. Vickers hardness data revealed that, in specimens austenitized at 1200 °C and deformed at 900 °C with strains of 10% and 30%, the ranges of hardness distribution were 250–360 HV 0.1 and 310–400 HV 0.1, respectively. For specimens austenitized at 1000 °C and deformed at 900 °C with strains of 10% and 30%, the ranges of hardness distribution were 220–250 HV 0.1 and 220–260 HV 0.1, respectively. Therefore, the average Vickers hardness increased with the austenitizing temperature and deformation strain. However, a wider range of hardness distribution occurred in specimens that underwent treatment at higher austenitizing temperatures. The wider Vickers hardness distribution reflects non-uniform precipitation in each ferrite grain.

  19. Research on Hot Deformation Behavior of Hastelloy G-3 Alloy%Hastelloy G-3合金热变形特性研究

    Institute of Scientific and Technical Information of China (English)

    罗坤杰; 张麦仓; 王宝顺; 董建新

    2011-01-01

    利用变形温度为1050~1200℃、应变速率为0.1~10 s-1的恒温热压缩试验系统分析了Hastelloy G-3合金的高温变形特性及变形后的组织特征.对高应变速率下的流动应力进行变形热效应修正,建立了G-3合金热变形过程中峰值应力与变形温度、应变速率关系的本构模型.结果表明:所建立的本构模型在预测G-3合金热变形峰值应力时具有良好的精确度,能够满足工程应用的要求.G-3合金热加工过程的软化机制为动态再结晶,根据热变形后的组织特征确定G-3合金合理的热变形温度为1180~1200℃,应变速率为5~10 s-1.%The hot deformation behavior and the subsequent microstructure characteristics of Hastelloy G-3 alloy were studied by isothermal compression tests at the strain rates of 0.1-10 s-1 and the temperatures of 1050-1200 ℃. The flow-stress at high strain rates were corrected considering the effect of deformation heating, and a new constitutive relationship between peak stress and deformation temperature as well as strain rate for G-3 alloy at high temperature was established. The results show that the built material model has good fitting accuracy to satisfy the engineering need. The softening mechanism of G-3 alloy is dynamic recrystalization during hot working process. According to the microstructures after deformation, for G-3 alloy the proper deformation temperature is 1180-1200 ℃ and the proper strain rate is 5-10 s-1.

  20. Research on hot deformation behavior of 3003 Al alloy%3003铝合金热变形行为

    Institute of Scientific and Technical Information of China (English)

    陈贵清; 傅高升; 颜文煅; 陈鸿玲; 程超增; 邹泽昌

    2011-01-01

    3003 Al alloys with different metallurgical quality were obtained by different melt-treatment methods, which were deformed by isothermal compression in the range of deformation temperature 300℃~500℃ at strain rate 0. 01s-1 ~ 10. 0s-1 with Gleeble-1500 thermal simulator. The results show that the material is sensitive to positive strain rate, the linear relationship between the hot deformation activation energy Q and inclusion content H is Q=35. 62H+171. 58, and the activation energy of 3003 Al alloy prepared by high melt-treatment is the lowest 174. 62kJ · mol-1 which is beneficial to the hot plastic deformation of material. The critical strain of 3003 Al alloy prepared by different melt-treatment methods were calculated with work hardening rate, and the critical conditions to predict the dynamic recrystallization occurrence for the 3003 Al alloys prepared by different melt-treatment methods were obtained.%采用不同熔体处理工艺获得3种不同冶金质量的3003铝合金,通过Gleeble-1500热模拟试验机对3003铝合金进行变形温度为300℃~500℃,应变速率为0.01s-1~10s-1高温等温压缩实验.结果表明,3003铝合金具有正的应变速率敏感性,热变形激活能Q与含杂量H呈线性关系,经高效综合处理的3003铝合金热变形激活能最低为174.62kJ·mol-1,有利于材料热塑性变形.采用加工硬化率计算不同熔体处理的3003铝合金的临界应变值,获得了经不同熔体处理的3003铝合金发生动态再结晶的临界条件.